WA-1010_12511_CA_MRP_20131109

November 9, 2013

Danny S. Pender
603 Foxwood Drive
Goldsboro, NC 27530-8461

Reference: Groundwater Monitoring Report
BP Service Center
4673 US Highway 117 North
Pikeville, Wayne County, North Carolina 27863
Incident #12511; Facility ID #0-006989
Risk Classification: High

Dear Mr. Pender:

Please find enclosed a report summarizing groundwater monitoring activities conducted at the
above referenced facility. Previous assessment activities at this site revealed a release of
petroleum in groundwater in the vicinity of the former location of a gasoline UST and dispenser
island. Nineteen on-site monitor wells and four local supply/irrigation wells were sampled in
October, 2013 to evaluate the site for the presence of dissolved gasoline constituents. The
findings of this investigation are summarized herein.

Mr. Pender, if you have questions regarding this report please contact my office.

Sincerely,

Henry Nemargut, P.E.
Henry Nemargut Engineering Services

GROUNDWATER MONITORING REPORT

BP SERVICE CENTER
4673 US HIGHWAY 117 NORTH, PIKEVILLE, WAYNE COUNTY, NC 27863
GROUNDWATER INCIDENT #: 12511
FACILITY ID #: 0-006989

NOVEMBER 9, 2013

UST OWNER/OPERATOR:
MARY P. PENDER (DECEASED)

PROPERTY OWNER:
DANNY S. PENDER
603 FOXWOOD DRIVE, GOLDSBORO, NC 27530-8461
PHONE NUMBER: [phone]

CONSULTANT:
HENRY NEMARGUT ENGINEERING SERVICES
2211 CHESTNUT STREET, WILMINGTON, NC 28405
PHONE NUMBER: [phone]

RELEASE INFORMATION:
DATE DISCOVERED: 12/27/93
ESTIMATED QUANTITY OF RELEASE: UNKNOWN
CAUSE OF RELEASE: UNKNOWN
SOURCE OF RELEASE: UST SYSTEM
SIZE AND CONTENTS: (1) 3,000 GALLON GASOLINE
LATITUDE: N 35o 29'17"; LONGITUDE: W 77o 58’55”

The Monitoring Report for this site has been prepared by Henry Nemargut Engineering Services. All
engineering work performed on this project was conducted under my direct supervision:

Henry Nemargut, P.E.
Henry Nemargut Engineering Services
North Carolina License #17669
TABLE OF CONTENTS

Section Page

1.0 Introduction and Background
1.1 Introduction 1
1.2 Scope of Services 1

2.0 Field Activities 2
2.1 Groundwater Flow Direction and Gradient 2
2.2 Monitor Well Sampling and Analysis 2
2.3 Supply Well Sampling and Analysis 3
2.4 Plume Development 3

3.0 Conclusions and Recommendations
3.1 General Summary 4
3.2 Recommendations 4
3.3 Limitations 5

LIST OF FIGURES

Figure 1: Project Location
Figure 2: Site Layout and Monitor Well Locations
Figure 3: Potentiometric Surface Map (10/29/13)
Figure 4: Benzene Iso-Concentration Map
Figure 5: Total BTEX Iso-Concentration Map
Figure 6: Naphthalene Iso-Concentration Map

LIST OF TABLES

Table 1: Monitoring Well Information and Groundwater Elevations
Table 2: Summary of Groundwater Laboratory Analytical Results
Table 3: Total BTEX vs. Time

APPENDICES

Appendix A: Groundwater Laboratory Analytical Results

Page - 1
GROUNDWATER MONITORING REPORT
BP SERVICE CENTER
4673 US HIGHWAY 117 NORTH
PIKEVILLE, NORTH CAROLINA 27863

1.0 Introduction and Background

1.1 Introduction

Danny S. Pender is the property owner of a site which was formerly operated as the BP Service Center
facility located at 4673 US Highway 117 North in Pikeville, North Carolina. Figure 1 illustrates the
location of this facility on the Pikeville Quadrangle U.S.G.S. Topo Map. This facility contains one
permanent structure which is used as a gasoline convenience store but is currently vacant. The site
formerly contained (1) 3,000 gallon gasoline UST which was removed from this facility on December
27, 1993. A release was noted from this UST during closure activities. Assessment activities including
a LSA report, CSA activities conducted in 1994, and installation of additional monitoring wells have
been conducted at this site through 2010. Most recently, secondary sources (contaminated soil) were
removed from the site in the former pump island area in October, 2012. Figure 2 illustrates the layout of
this site, the UST locations, and the monitor well locations.

The NCDENR recently issued an NORR requesting that the following tasks be conducted at this site
prior to proceeding with development of a Corrective Action Plan for this facility:

• Sample all existing wells and area supply wells
• Submit a groundwater monitoring report

This report contains findings reached following conducting these requested activities at 4673 US
Highway 117 North in Pikeville, NC.

1.2 Scope of Services

This Groundwater monitoring report contains documentation concerning the following activities which
have been conducted at this facility:

o A comprehensive monitoring well sampling event conducted on October 29, 2013, consisting of
sampling of the 19 wells installed in conjunction with the on-site release and sampling of 4
nearby water supply wells.

o Laboratory analyses of groundwater samples conducted by Pace Analytical, Inc. of Huntersville,
NC

o Estimation of the approximate groundwater flow direction and hydraulic gradient at the site.

o Isoconcentration maps illustrating the current contaminant levels in the monitoring wells at the
facility.
Page - 2

2.0 Field Activities

2.1 Ground Water Flow Direction and Gradient

In order to estimate the groundwater flow direction in the vicinity of the petroleum release, elevations of
the monitor well casings were measured using surveying equipment. Static water levels were obtained
from each of the wells and the data was used to compute a potentiometric surface map which is included
as Figure 3.

Groundwater data and monitoring well information, which are summarized in Table 1, were also used to
estimate the hydraulic gradient at the project site. The potentiometric surface shows flow in many
directions from the pump island source area at this site. The steepest horizontal gradient seems to be
towards the northwest. Using the horizontal distance between the monitor wells and the static water
levels, the groundwater was estimated to be flowing in a northwestern direction with a horizontal
hydraulic gradient of approximately 0.024 ft/ft over the monitor well network; however, a portion of the
plume has migrated towards the south with a component of flow also noted in that direction. Drawdown
effects from local supply wells and stagnant drainage ditches appear to influence groundwater flow
patterns at the site.

The vertical groundwater gradient at the site was also calculated based on the observed shallow well
potentiometric surface and the potentiometric head observed in the on-site vertical extent well VEW-1.
The estimated shallow potentiometric surface in the VEW-1 location is 94.3’. The potentiometric head
observed in VEW-1 on October 29, 2013 was 86.58’. These measurements correlate to a downward
vertical gradient at the site of approximately 0.2005 ft/ft (7.72’/38.5’- thickness of aquifer to top of
screen on VEW-1). This data suggests that a very strong downward vertical gradient exists at this site.

2.2 Monitor Well Sampling and Analyses

On October 29, 2013, the nineteen on-site and off-site monitor wells were sampled for analyses utilizing
EPA Methods 6200B plus MTBE, IPE, & EDB. Before sampling, the monitor wells were purged by
removing a minimum of three well volumes to ensure that the samples were representative of the actual
groundwater conditions. The monitor wells were developed using disposable plastic balers suspended
with unused nylon string. Following development of the groundwater monitoring wells, samples were
obtained from the disposable balers.

All samples were placed in laboratory supplied glassware, labeled with sample location, analysis to be
performed, time, date and sampler's name. The sample jars were then immediately placed in a cooler,
chilled with ice to approximately 4oC in preparation of transportation to an analytical laboratory
utilizing EPA approved chain-of-custody procedures.

Laboratory analytical results indicate the presence of 5 compounds above the current listed 2L Standards
in the monitor well network at this site. Total BTEX was detected at a maximum level of 720 ug/l in
off-site well MW-15 and at a maximum on-site level of 430 ug/l in well MW-7. Benzene was detected
Page - 3
at a maximum concentration of 187 ug/l in MW-18, above its 2L standard of 1 ug/l but below its GCL of
5,000 ug/l. No GCL violations were noted at the site. Naphthalene was detected at a maximum
concentration of 307 ug/l in off-site monitoring well MW-15, and at a maximum on-site level of 430
ug/l in well MW-7. Table 2 summarizes the laboratory analytical results, and Appendix A contains a
copy of the laboratory analytical report and chain of custody records. Figure 4 contains a benzene iso-
concentration map, Figure 5 illustrates the estimated Total BTEX concentration map, and Figure 6
illustrates the naphthalene isoconcentration for the site.

2.3 Supply Well Sampling and Analyses

On October 29, 2013, four off-site area supply wells were sampled for analyses utilizing EPA Methods
6200B plus MTBE, IPE, & EDB. Before sampling, the supply wells were purged by pumping from the
wells for approximately 10 minutes to ensure that the samples were representative of the actual
groundwater conditions. After pumping, the flowrate was reduced for collection of samples. Samples
were obtained from spigots closest to the various supply wells. The four supply wells sampled included:
SW-1, owned by Travis Thigpen, used for potable water at the NC Historic Site Mechanics Shop; IW-3,
owned by Mattie Artis, used for irrigation at a private residence; IW-4, owned by Tedaro Reid, used for
irrigation at a private residence; and IW-8, owned by David Daw, used as a water source at JuDee’s Hair
& Body.

All samples were placed in laboratory supplied glassware, labeled with sample location, analysis to be
performed, time, date and sampler's name. The sample jars were then immediately placed in a cooler,
chilled with ice to approximately 4oC in preparation of transportation to an analytical laboratory
utilizing EPA approved chain-of-custody procedures.

Laboratory analytical results indicate the presence of 1 compound above laboratory detection limits in
the sample from the Travis Thigpen well, SW-1, located at the NC Mechanic Shop. 1,2-
Dichloropropane was detected in the SW-1 sample from the at a level of 1.4 ug/l, above its 2L Standard
of 0.60 ug/l. The supply wells owned by David Daw used to supply JuDee’s Hair & Body, IW-8, the
Mattie Artis irrigation well, IW-3, and the Tedaro Reid irrigation well IW-3 failed to show any 6200B
contaminants above laboratory detection limits. Table 2 summarizes the laboratory analytical results,
and Appendix A contains a copy of the laboratory analytical report and chain of custody records.

2.4 Plume Development

In prior sampling events conducted at the site, contaminants have been reported above 2L Standards in
on-site and off-site monitoring wells and in off-site water supply wells. The Travis Thigpen well (SW-
1) continues to show elevated levels of 1,2 Dichloropropane not related to this release. This is the only
supply well with a 2L violation since the Suggs Auto well has been abandoned and his facility
connected to public water.

The contaminant concentrations in source area wells MW-8A, MW-7 and MW-18 have decreased
significantly since the last sampling events conducted on October 6, 2011 and April, 2013, obviously
due to soil remediation conducted in the pump island source area conducted in October, 2012. Benzene
Page - 4
concentration in groundwater in the pump island source area, previously above its GCL, was reduced to
below detection as a result of soil remediation. In general, contaminant concentrations appear to be
reducing at the site, a trend which should continue with the removal of contaminated soils in the pump
island source area. Historical analytical laboratory data are summarized in detail on Table 3.

3.0 Conclusions and Recommendations

3.1 General Summary

A groundwater monitoring sampling event has been conducted at the BP Service Center facility located
at 4673 US Highway 117 North in Pikeville, NC. From a review of all information gathered during this
remediation project, Henry Nemargut Engineering Services makes the following conclusions:

o 5 petroleum compounds were detected in on and off site monitoring wells above 2L Standards
during the October 29, 2013 sampling event. Benzene was noted at a maximum concentration of
187 ug/l in MW-18, far below its GCL of 5,000 ug/l.

o The presence of 1,2 dichloropropane was confirmed at a level of 1.4 ug/l, above 2L standards in
the NC Vehicle Maintenance supply well (owned by Travis Thigpen) during the October 29,
2013 sampling event. This compound is not present in any monitoring wells and does not appear
to be related to the petroleum release from the BP Service Center.

o The contaminant concentrations in MW-7, MW-8A, and MW-18 have decreased significantly
since the last sampling event conducted on April 18, 2013, obviously due to soil remediation
conducted in the pump island source area conducted in October, 2012. Benzene concentration in
groundwater in the pump island source area, previously above its GCL, was reduced to below
detection as a result of soil remediation.

o In general, contaminant concentrations appear to be reducing at the site, a trend which should
continue with the removal of contaminated soils in the pump island source area.

3.2 Recommendations

Based on information obtained during this sampling event, Henry Nemargut Engineering Services
makes the following recommendations for this site:

o Semi-annual monitoring should be continued at this site to measure the effectiveness of soil
remediation on the dissolved contaminant plume emanating from this site.

Page - 5
A copy of this monitoring report has been forwarded to:

Rose Ballance
NCDENR-WaRO UST Section
943 Washington Square Mall
Washington, NC 27889

3.3 Limitations

This report has been prepared for the exclusive use of Danny S. Pender for the specific application to the
referenced site located in Wayne County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by the client. Our findings have been developed in accordance
with generally accepted standards in the practice of Groundwater Monitoring in the State of North
Carolina, available information and our professional judgment. No other warranty is expressed or
implied.

The data presented in this report are indicative of conditions that existed at the precise locations sampled
and at the time the samples were collected. Additionally, the data obtained from the samples would be
interpreted as meaningful with respect to the parameters indicated in the laboratory reports. No
additional information can be logically inferred from this data.

FIGURES

TABLES
TABLE 1Monitoring Well Information and Groundwater ElevationsBP Service Center4673 US Hwy 117 North, Goldsboro, NCWell Number Top of Casing Elevation Top of Screen Elevation Bottom of Screen Elevation Depth to Water Groundwater ElevationMW-1 98.12 93.12 78.12 8.40 89.72MW-2 98.49 93.49 78.49 4.17 94.32MW-3 100.00 95.00 80.00 4.77 95.23MW-4 99.95 94.95 79.95 10.25 89.70MW-5 98.06 93.06 78.06 2.52 95.54MW-6 98.68 93.68 78.68 4.59 94.09MW-7 96.74 91.74 76.74 2.28 94.46MW-8A 97.66 95.16 80.16 2.47 95.19MW-9 96.73 94.23 76.73 2.91 93.82MW-10 95.68 93.18 75.68 1.73 93.95MW-11 96.84 94.34 77.84 2.58 94.26MW-12 97.98 95.48 77.98 8.21 89.77MW-13 98.68 96.18 78.18 8.48 90.20MW-14 98.90 96.40 78.40 9.17 89.73MW-15 98.44 95.44 78.44 8.92 89.52MW-16 97.62 94.62 77.62 8.11 89.51MW-17 97.33 92.33 77.33 7.77 89.56MW-18 97.99 95.49 70.49 3.32 94.67VEW-198.0958.0948.0911.5186.58All measurements taken in feet and based on an arbitrary benchmark of 100.00 feet at MW-3Groundwater levels measured on10/29/13BP Service
Constituent MW-1 MW-2 MW-3 MW-4 GCL 2L Standard

Date 10/29/13 10/29/13 10/29/13 10/29/13
Method 6210D (ug/L)
Benzene 106 23.4 3.6 BDL 5,000 1
Toluene BDL BDL BDL BDL 260,000 600
Ethylbenzene 124 BDL 2.9 BDL 84,500 600
Xylenes (total) 143 2.7 BDL BDL 85,500 500
BTEX (total) 373 26.1 6.5 0 NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene 14.3 6.2 5.3 BDL 25,000 70
Methylene Chloride BDL BDL BDL BDL 5,000 5
Naphthalene 56.5 17 7.6 BDL 6,000 6
n-propylbenzene 32.1 10.4 6.3 BDL 30,000 70
n-butylbenzene BDL BDL BDL BDL 6,900 70
sec-Butylbenzene BDL 1.1 2.3 BDL 15,000 70
tert-Butylbenzene BDL BDL BDL BDL 15,000 70
MTBE 51 42.1 2.3 BDL 20,000 20
1,2-Dichloroethane 3.3 1.7 2.8 BDL 400 0.4
Isopropyl Ether (IPE) BDL BDL BDL BDL 70,000 70
trans-1,2-Dichloroethene BDL BDL BDL BDL 100,000 100
1,2,4-Trimethylbenzene 152 4.7 BDL BDL 28,500 400
1,3,5-Trimethylbenzene 36 0.61 BDL BDL 25,000 400
Lead (3030C) N/A N/A N/A N/A 15,000 15
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 2
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
Constituent MW-5 MW-6 MW-7 MW-8A GCL 2L Standard

Date 10/29/13 10/29/13 10/29/13 10/29/13
Method 6210D (ug/L)
Benzene BDL BDL 85.1 BDL 5,000 1
Toluene BDL BDL 9.7 BDL 260,000 600
Ethylbenzene BDL BDL 335 BDL 84,500 600
Xylenes (total) BDL BDL BDL BDL 85,500 500
BTEX (total) BDL BDL 429.8 0 NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene BDL BDL 40 BDL 25,000 70
Methylene Chloride BDL BDL BDL BDL 5,000 5
Naphthalene BDL BDL 159 BDL 6,000 6
n-propylbenzene BDL BDL 78.9 BDL 30,000 70
n-butylbenzene BDL BDL BDL BDL 6,900 70
sec-Butylbenzene BDL BDL BDL BDL 15,000 70
tert-Butylbenzene BDL BDL BDL BDL 15,000 70
MTBE BDL 25.5 18.4 16.9 20,000 20
1,2-Dichloroethane BDL 0.86 BDL 0.66 400 0.4
Isopropyl Ether (IPE) BDL BDL BDL BDL 70,000 70
trans-1,2-Dichloroethene BDL BDL BDL BDL 100,000 100
1,2,4-Trimethylbenzene BDL BDL 1050 BDL 28,500 400
1,3,5-Trimethylbenzene BDL BDL 334 BDL 25,000 400
Lead (3030C) N/A N/A N/A N/A 15,000 15
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 2 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
Constituent MW-9 MW-10 MW-11 MW-12 GCL 2L Standard

Date 10/29/13 10/29/13 10/29/13 10/29/13
Method 6210D (ug/L)
Benzene 0.64 BDL BDL 8.4 5,000 1
Toluene BDL BDL BDL BDL 260,000 600
Ethylbenzene BDL BDL BDL BDL 84,500 600
Xylenes (total) BDL BDL BDL 0.56 85,500 500
BTEX (total) 0.64 BDL BDL 8.96 NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene BDL BDL BDL 3.4 25,000 70
Methyl Isobutyl Ketone BDL BDL BDL BDL NSE NSE
Naphthalene BDL BDL BDL BDL 6,000 6
n-propylbenzene BDL BDL BDL 0.63 30,000 70
n-butylbenzene BDL BDL BDL 0.54 6,900 70
sec-Butylbenzene BDL BDL BDL 0.87 15,000 70
tert-Butylbenzene BDL BDL BDL BDL 15,000 70
MTBE 0.52 BDL BDL 7.8 20,000 20
1,2-Dichloroethane 18.7 BDL BDL 9.9 400 0.4
Isopropyl Ether (IPE) BDL BDL BDL BDL 70,000 70
Acetone BDL BDL BDL BDL 6,000,000 6,000
1,2,4-Trimethylbenzene BDL BDL BDL BDL 28,500 400
1,3,5-Trimethylbenzene BDL BDL BDL BDL 25,000 400
Lead (3030C) N/A N/A N/A N/A 15,000 15
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 2 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
Constituent MW-13 MW-14 MW-15 MW-16 GCL 2L Standard

Date 10/29/13 10/29/13 10/29/13 10/29/13
Method 6210D (ug/L)
Benzene BDL 2.1 BDL 0.6 5,000 1
Toluene 1.9 BDL BDL BDL 260,000 600
Ethylbenzene BDL 7.7 300 0.62 84,500 600
Xylenes (total) BDL BDL 420 BDL 85,500 500
BTEX (total) 1.9 9.8 720 1.22 NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene BDL 3.2 34.5 1.6 25,000 70
Acetone BDL BDL BDL BDL 6,000,000 6,000
Naphthalene BDL 196 307 42.7 6,000 6
n-propylbenzene BDL 4.8 85.1 2 30,000 70
n-butylbenzene BDL BDL 8.5 1.2 6,900 70
sec-Butylbenzene BDL 2.3 8.5 1.3 15,000 70
tert-Butylbenzene BDL BDL BDL BDL 15,000 70
MTBE BDL BDL BDL BDL 20,000 20
Acetone BDL BDL BDL BDL 6,000,000 6,000
Isopropyl Ether (IPE) BDL BDL BDL BDL 70,000 70
Styrene BDL BDL BDL BDL 70,000 70
1,2,4-Trimethylbenzene BDL 26.6 250 2.1 28,500 400
1,3,5-Trimethylbenzene BDL BDL 64.1 BDL 25,000 400
Lead (3030C) N/A N/A N/A N/A 15,000 15
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 2 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
Constituent MW-17 MW-18 VEW-1 SW-1 GCL 2L Standard

Date 10/29/13 10/29/13 10/29/13 10/29/13
Method 6210D (ug/L)
Benzene 0.94 187 BDL BDL 5,000 1
Toluene BDL BDL BDL BDL 260,000 600
Ethylbenzene BDL 100 BDL BDL 84,500 600
Xylenes (total) BDL 6.3 BDL BDL 85,500 500
BTEX (total) 0.94 293.3 BDL BDL NSE NSE
p-Isopropyltoluene BDL BDL BDL BDL NSE NSE
Isopropylbenzene BDL 13 BDL BDL 25,000 70
Acetone BDL BDL BDL BDL 6,000,000 6,000
Naphthalene 16.3 65.3 BDL BDL 6,000 6
n-propylbenzene BDL 33.8 BDL BDL 30,000 70
n-butylbenzene BDL BDL BDL BDL 6,900 70
sec-Butylbenzene 0.62 2.7 BDL BDL 15,000 70
tert-Butylbenzene BDL BDL BDL BDL 15,000 70
MTBE BDL 294 BDL BDL 20,000 20
1,2-Dichloropropane BDL BDL BDL 1.4 600 0.6
Isopropyl Ether (IPE) BDL BDL BDL BDL 70,000 70
1,2-Dichloroethane BDL 5.9 BDL BDL 400 0.4
1,2,4-Trimethylbenzene BDL 10.9 BDL BDL 28,500 400
1,3,5-Trimethylbenzene BDL BDL BDL BDL 25,000 400
Lead (3030C) N/A N/A N/A N/A 15,000 15
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 2 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
Constituent IW-3 IW-4 SW-8 GCL 2L Standard

Date 10/29/13 10/29/13 10/29/13
Method 6210D (ug/L)
Benzene BDL BDL BDL 5,000 1
Toluene BDL BDL BDL 260,000 600
Ethylbenzene BDL BDL BDL 84,500 600
Xylenes (total) BDL BDL BDL 85,500 500
BTEX (total) BDL BDL BDL NSE NSE
p-Isopropyltoluene BDL BDL BDL NSE NSE
Isopropylbenzene BDL BDL BDL 25,000 70
1,2-Dichloropropane BDL BDL BDL 600 0.6
Naphthalene BDL BDL BDL 6,000 6
n-propylbenzene BDL BDL BDL 30,000 70
n-butylbenzene BDL BDL BDL 6,900 70
sec-Butylbenzene BDL BDL BDL 15,000 70
Methyl Ethyl Ketone BDL BDL BDL 4,000,000 4,000
MTBE BDL BDL BDL 20,000 20
1,2-Dichloroethane BDL BDL BDL 70,000 70
Isopropyl Ether (IPE) BDL BDL BDL 70,000 70
Chloroform BDL BDL BDL 70,000 70
1,2,4-Trimethylbenzene BDL BDL BDL 28,500 400
1,3,5-Trimethylbenzene BDL BDL BDL 25,000 400
Lead (3030C) N/A N/A N/A 15,000 15
Aliphatic Fraction Classes (ug/L)
C5-C8 Volatile Aliphatics N/A N/A N/A NSE 420
C9-C12 Volatile Aliphatics N/A N/A N/A NSE NSE
C9-C18 Extractable Aliphatics N/A N/A N/A NSE 4,200
C9-C18 Aliphatics (total) N/A N/A N/A NSE 4,200
C19-C36 Extractable Aliphatics N/A N/A N/A NSE 42,000
Aromatic Fraction Classes (ug/L)
C9-C10 Volatile Aromatics N/A N/A N/A NSE NSE
C11-C22 Extractable Aromatics N/A N/A N/A NSE NSE
C9-C22 Aromatics (total)N/A N/A N/A NSE 210
N/A = Not Analyzed
BDL = Below Detection Limits
NSE = No Standard Established
TABLE 2 (Continued)
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
BP SERVICE CENTER
4673 US HWY 117 NORTH, GOLDSBORO, NC
TABLE 3TABLE 3Time Based Analytical Data Total BTEXTime Based Analytical Data - Total BTEXBP S i C tBP Service Center4673 N Hwy 117 Pikeville NC4673 N Hwy 117, Pikeville, NCDate of SamplingMW 1MW 2MW 3MW 7MW 8MW 12MW 15MW 18Date of SamplingMW-1MW-2MW-3MW-7MW-8MW-12MW-15MW-185/27/19946 7017431 2115/27/19946,7017431,2117/8/20082 15619157458037 8002097/8/20082,15619157458037,8002093/31/20101 0951462607036 30023/31/20101,0951462607036,30028/6/20102 67934562481547 50094298/6/20102,67934562481547,500942910/6/201113818129245833 900285210/6/201113818129245833,90028524/18/20132603831332200497654/18/201326038313322004976510/29/20133732674300972029310/29/201337326743009720293Results in ug/lResults in ug/l

APPENDIX A

LABORATORY ANALYTICAL RESULTS
#=CL#
November 07, 2013
LIMS USE: FR - HENRY NEMARGUT
LIMS OBJECT ID: 92177732
92177732
Project:
Pace Project No.:
RE:
Henry Nemargut
Henry Nemargut Engineering
2211 Chestnut Street
Wilmington, NC 28405
BP SERVICE CNTR
Dear Henry Nemargut:
Enclosed are the analytical results for sample(s) received by the laboratory on October 31, 2013.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 68
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 68
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Lab ID Sample ID Matrix Date Collected Date Received
92177732001 MW1 Water 10/29/13 08:30 10/31/13 09:30
92177732002 MW2 Water 10/29/13 09:00 10/31/13 09:30
92177732003 MW3 Water 10/29/13 09:30 10/31/13 09:30
92177732004 MW4 Water 10/29/13 10:00 10/31/13 09:30
92177732005 MW5 Water 10/29/13 10:30 10/31/13 09:30
92177732006 MW6 Water 10/29/13 11:00 10/31/13 09:30
92177732007 MW7 Water 10/29/13 11:30 10/31/13 09:30
92177732008 MW8A Water 10/29/13 12:00 10/31/13 09:30
92177732009 MW9 Water 10/29/13 12:30 10/31/13 09:30
92177732010 MW10 Water 10/29/13 13:00 10/31/13 09:30
92177732011 MW11 Water 10/29/13 13:30 10/31/13 09:30
92177732012 MW12 Water 10/29/13 13:50 10/31/13 09:30
92177732013 MW13 Water 10/29/13 14:10 10/31/13 09:30
92177732014 MW14 Water 10/29/13 14:40 10/31/13 09:30
92177732015 MW15 Water 10/29/13 15:00 10/31/13 09:30
92177732016 MW16 Water 10/29/13 15:20 10/31/13 09:30
92177732017 MW17 Water 10/29/13 15:40 10/31/13 09:30
92177732018 MW18 Water 10/29/13 16:00 10/31/13 09:30
92177732019 VEW-1 Water 10/29/13 16:50 10/31/13 09:30
92177732020 SW-1 Water 10/29/13 16:10 10/31/13 09:30
92177732021 IW-8 Water 10/29/13 16:30 10/31/13 09:30
92177732022 IW-3 Water 10/29/13 17:30 10/31/13 09:30
92177732023 IW-4 Water 10/29/13 17:50 10/31/13 09:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 68
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92177732001 MW1 SM 6200B 63 PASI-CCAH
92177732002 MW2 SM 6200B 63 PASI-CCAH
92177732003 MW3 SM 6200B 63 PASI-CCAH
92177732004 MW4 SM 6200B 63 PASI-CCAH
92177732005 MW5 SM 6200B 63 PASI-CCAH
92177732006 MW6 SM 6200B 63 PASI-CCAH
92177732007 MW7 SM 6200B 63 PASI-CCAH
92177732008 MW8A SM 6200B 63 PASI-CCAH
92177732009 MW9 SM 6200B 63 PASI-CCAH
92177732010 MW10 SM 6200B 63 PASI-CCAH
92177732011 MW11 SM 6200B 63 PASI-CCAH
92177732012 MW12 SM 6200B 63 PASI-CCAH
92177732013 MW13 SM 6200B 63 PASI-CCAH
92177732014 MW14 SM 6200B 63 PASI-CCAH
92177732015 MW15 SM 6200B 63 PASI-CCAH
92177732016 MW16 SM 6200B 63 PASI-CCAH
92177732017 MW17 SM 6200B 63 PASI-CCAH
92177732018 MW18 SM 6200B 63 PASI-CCAH
92177732019 VEW-1 SM 6200B 63 PASI-CCAH
92177732020 SW-1 SM 6200B 63 PASI-CCAH
92177732021 IW-8 SM 6200B 63 PASI-CCAH
92177732022 IW-3 SM 6200B 63 PASI-CCAH
92177732023 IW-4 SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 4 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW1 Lab ID: 92177732001 Collected: 10/29/13 08:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 106 ug/L 11/03/13 13:52 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 13:52 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 13:52 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 13:52 75-27-40.50 1
Bromoform ND ug/L 11/03/13 13:52 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 13:52 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 13:52 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 13:52 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 13:52 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 13:52 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 13:52 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 13:52 75-00-31.0 1
Chloroform ND ug/L 11/03/13 13:52 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 13:52 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 13:52 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 13:52 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 13:52 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 13:52 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 13:52 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 13:52 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 13:52 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 13:52 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 13:52 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 13:52 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 13:52 75-34-30.50 1
1,2-Dichloroethane 3.3 ug/L 11/03/13 13:52 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 13:52 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 13:52 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 13:52 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 13:52 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 13:52 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 13:52 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 13:52 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 13:52 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 13:52 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 13:52 108-20-30.50 1
Ethylbenzene 124 ug/L 11/03/13 13:52 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 13:52 87-68-32.0 1
Isopropylbenzene (Cumene)14.3 ug/L 11/03/13 13:52 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 13:52 75-09-22.0 1
Methyl-tert-butyl ether 51.0 ug/L 11/03/13 13:52 1634-04-40.50 1
Naphthalene 56.5 ug/L 11/03/13 13:52 91-20-32.0 1
n-Propylbenzene 32.1 ug/L 11/03/13 13:52 103-65-10.50 1
Styrene ND ug/L 11/03/13 13:52 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 13:52 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 13:52 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 13:52 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 5 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW1 Lab ID: 92177732001 Collected: 10/29/13 08:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 13:52 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 13:52 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 13:52 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 13:52 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 13:52 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 13:52 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 13:52 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 13:52 96-18-40.50 1
1,2,4-Trimethylbenzene 152 ug/L 11/03/13 13:52 95-63-60.50 1
1,3,5-Trimethylbenzene 36.0 ug/L 11/03/13 13:52 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 13:52 75-01-41.0 1
m&p-Xylene 98.1 ug/L 11/03/13 13:52 179601-23-11.0 1
o-Xylene 44.9 ug/L 11/03/13 13:52 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 93 % 11/03/13 13:52 17060-07-070-130 1
4-Bromofluorobenzene (S) 99 % 11/03/13 13:52 460-00-470-130 1
Toluene-d8 (S) 99 % 11/03/13 13:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW2 Lab ID: 92177732002 Collected: 10/29/13 09:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 23.4 ug/L 11/03/13 13:03 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 13:03 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 13:03 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 13:03 75-27-40.50 1
Bromoform ND ug/L 11/03/13 13:03 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 13:03 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 13:03 104-51-80.50 1
sec-Butylbenzene 1.1 ug/L 11/03/13 13:03 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 13:03 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 13:03 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 13:03 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 13:03 75-00-31.0 1
Chloroform ND ug/L 11/03/13 13:03 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 13:03 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 13:03 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 13:03 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 13:03 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 13:03 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 13:03 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 13:03 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 13:03 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 13:03 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 13:03 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 13:03 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 13:03 75-34-30.50 1
1,2-Dichloroethane 1.7 ug/L 11/03/13 13:03 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 13:03 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 13:03 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 13:03 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 13:03 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 13:03 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 13:03 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 13:03 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 13:03 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 13:03 10061-02-60.50 1
Diisopropyl ether 0.58 ug/L 11/03/13 13:03 108-20-30.50 1
Ethylbenzene 15.7 ug/L 11/03/13 13:03 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 13:03 87-68-32.0 1
Isopropylbenzene (Cumene)6.2 ug/L 11/03/13 13:03 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 13:03 75-09-22.0 1
Methyl-tert-butyl ether 42.1 ug/L 11/03/13 13:03 1634-04-40.50 1
Naphthalene 17.0 ug/L 11/03/13 13:03 91-20-32.0 1
n-Propylbenzene 10.4 ug/L 11/03/13 13:03 103-65-10.50 1
Styrene ND ug/L 11/03/13 13:03 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 13:03 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 13:03 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 13:03 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW2 Lab ID: 92177732002 Collected: 10/29/13 09:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 13:03 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 13:03 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 13:03 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 13:03 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 13:03 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 13:03 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 13:03 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 13:03 96-18-40.50 1
1,2,4-Trimethylbenzene 4.7 ug/L 11/03/13 13:03 95-63-60.50 1
1,3,5-Trimethylbenzene 0.61 ug/L 11/03/13 13:03 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 13:03 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 13:03 179601-23-11.0 1
o-Xylene 2.7 ug/L 11/03/13 13:03 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 98 % 11/03/13 13:03 17060-07-070-130 1
4-Bromofluorobenzene (S) 101 % 11/03/13 13:03 460-00-470-130 1
Toluene-d8 (S) 101 % 11/03/13 13:03 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW3 Lab ID: 92177732003 Collected: 10/29/13 09:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 3.6 ug/L 11/03/13 13:19 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 13:19 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 13:19 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 13:19 75-27-40.50 1
Bromoform ND ug/L 11/03/13 13:19 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 13:19 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 13:19 104-51-80.50 1
sec-Butylbenzene 2.3 ug/L 11/03/13 13:19 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 13:19 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 13:19 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 13:19 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 13:19 75-00-31.0 1
Chloroform ND ug/L 11/03/13 13:19 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 13:19 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 13:19 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 13:19 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 13:19 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 13:19 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 13:19 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 13:19 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 13:19 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 13:19 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 13:19 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 13:19 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 13:19 75-34-30.50 1
1,2-Dichloroethane 2.8 ug/L 11/03/13 13:19 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 13:19 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 13:19 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 13:19 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 13:19 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 13:19 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 13:19 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 13:19 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 13:19 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 13:19 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 13:19 108-20-30.50 1
Ethylbenzene 2.9 ug/L 11/03/13 13:19 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 13:19 87-68-32.0 1
Isopropylbenzene (Cumene)5.3 ug/L 11/03/13 13:19 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 13:19 75-09-22.0 1
Methyl-tert-butyl ether 2.3 ug/L 11/03/13 13:19 1634-04-40.50 1
Naphthalene 7.6 ug/L 11/03/13 13:19 91-20-32.0 1
n-Propylbenzene 6.3 ug/L 11/03/13 13:19 103-65-10.50 1
Styrene ND ug/L 11/03/13 13:19 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 13:19 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 13:19 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 13:19 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW3 Lab ID: 92177732003 Collected: 10/29/13 09:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 13:19 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 13:19 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 13:19 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 13:19 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 13:19 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 13:19 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 13:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 13:19 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 13:19 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 13:19 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 13:19 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 13:19 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 13:19 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 95 % 11/03/13 13:19 17060-07-070-130 1
4-Bromofluorobenzene (S) 100 % 11/03/13 13:19 460-00-470-130 1
Toluene-d8 (S) 102 % 11/03/13 13:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW4 Lab ID: 92177732004 Collected: 10/29/13 10:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 08:23 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 08:23 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 08:23 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 08:23 75-27-40.50 1
Bromoform ND ug/L 11/03/13 08:23 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 08:23 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 08:23 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 08:23 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 08:23 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 08:23 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 08:23 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 08:23 75-00-31.0 1
Chloroform ND ug/L 11/03/13 08:23 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 08:23 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 08:23 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 08:23 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 08:23 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 08:23 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 08:23 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 08:23 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 08:23 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 08:23 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 08:23 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 08:23 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 08:23 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 08:23 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 08:23 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 08:23 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 08:23 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 08:23 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 08:23 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 08:23 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 08:23 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 08:23 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 08:23 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 08:23 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 08:23 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 08:23 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 08:23 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 08:23 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 08:23 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 08:23 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 08:23 103-65-10.50 1
Styrene ND ug/L 11/03/13 08:23 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 08:23 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 08:23 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 08:23 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 11 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW4 Lab ID: 92177732004 Collected: 10/29/13 10:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 08:23 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 08:23 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 08:23 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 08:23 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 08:23 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 08:23 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 08:23 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 08:23 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 08:23 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 08:23 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 08:23 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 08:23 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 08:23 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 101 % 11/03/13 08:23 17060-07-070-130 1
4-Bromofluorobenzene (S) 97 % 11/03/13 08:23 460-00-470-130 1
Toluene-d8 (S) 99 % 11/03/13 08:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 12 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW5 Lab ID: 92177732005 Collected: 10/29/13 10:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 10:18 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 10:18 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 10:18 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 10:18 75-27-40.50 1
Bromoform ND ug/L 11/03/13 10:18 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 10:18 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 10:18 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 10:18 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 10:18 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 10:18 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 10:18 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 10:18 75-00-31.0 1
Chloroform ND ug/L 11/03/13 10:18 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 10:18 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 10:18 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 10:18 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 10:18 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 10:18 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 10:18 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 10:18 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 10:18 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 10:18 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 10:18 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 10:18 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 10:18 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 10:18 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 10:18 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 10:18 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 10:18 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 10:18 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 10:18 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 10:18 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 10:18 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 10:18 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 10:18 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 10:18 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 10:18 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 10:18 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 10:18 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 10:18 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 10:18 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 10:18 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 10:18 103-65-10.50 1
Styrene ND ug/L 11/03/13 10:18 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 10:18 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 10:18 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 10:18 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW5 Lab ID: 92177732005 Collected: 10/29/13 10:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 10:18 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 10:18 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 10:18 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 10:18 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 10:18 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 10:18 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 10:18 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 10:18 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 10:18 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 10:18 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 10:18 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 10:18 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 10:18 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 106 % 11/03/13 10:18 17060-07-070-130 1
4-Bromofluorobenzene (S) 96 % 11/03/13 10:18 460-00-470-130 1
Toluene-d8 (S) 99 % 11/03/13 10:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW6 Lab ID: 92177732006 Collected: 10/29/13 11:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 08:39 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 08:39 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 08:39 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 08:39 75-27-40.50 1
Bromoform ND ug/L 11/03/13 08:39 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 08:39 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 08:39 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 08:39 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 08:39 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 08:39 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 08:39 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 08:39 75-00-31.0 1
Chloroform ND ug/L 11/03/13 08:39 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 08:39 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 08:39 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 08:39 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 08:39 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 08:39 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 08:39 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 08:39 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 08:39 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 08:39 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 08:39 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 08:39 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 08:39 75-34-30.50 1
1,2-Dichloroethane 0.86 ug/L 11/03/13 08:39 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 08:39 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 08:39 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 08:39 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 08:39 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 08:39 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 08:39 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 08:39 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 08:39 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 08:39 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 08:39 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 08:39 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 08:39 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 08:39 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 08:39 75-09-22.0 1
Methyl-tert-butyl ether 25.5 ug/L 11/03/13 08:39 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 08:39 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 08:39 103-65-10.50 1
Styrene ND ug/L 11/03/13 08:39 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 08:39 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 08:39 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 08:39 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW6 Lab ID: 92177732006 Collected: 10/29/13 11:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 08:39 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 08:39 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 08:39 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 08:39 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 08:39 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 08:39 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 08:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 08:39 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 08:39 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 08:39 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 08:39 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 08:39 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 08:39 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 105 % 11/03/13 08:39 17060-07-070-130 1
4-Bromofluorobenzene (S) 98 % 11/03/13 08:39 460-00-470-130 1
Toluene-d8 (S) 101 % 11/03/13 08:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 16 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW7 Lab ID: 92177732007 Collected: 10/29/13 11:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 85.1 ug/L 11/03/13 11:40 71-43-25.0 10
Bromobenzene ND ug/L 11/03/13 11:40 108-86-15.0 10
Bromochloromethane ND ug/L 11/03/13 11:40 74-97-55.0 10
Bromodichloromethane ND ug/L 11/03/13 11:40 75-27-45.0 10
Bromoform ND ug/L 11/03/13 11:40 75-25-25.0 10
Bromomethane ND ug/L 11/03/13 11:40 74-83-950.0 10
n-Butylbenzene ND ug/L 11/03/13 11:40 104-51-85.0 10
sec-Butylbenzene ND ug/L 11/03/13 11:40 135-98-85.0 10
tert-Butylbenzene ND ug/L 11/03/13 11:40 98-06-65.0 10
Carbon tetrachloride ND ug/L 11/03/13 11:40 56-23-55.0 10
Chlorobenzene ND ug/L 11/03/13 11:40 108-90-75.0 10
Chloroethane ND ug/L 11/03/13 11:40 75-00-310.0 10
Chloroform ND ug/L 11/03/13 11:40 67-66-35.0 10
Chloromethane ND ug/L 11/03/13 11:40 74-87-310.0 10
2-Chlorotoluene ND ug/L 11/03/13 11:40 95-49-85.0 10
4-Chlorotoluene ND ug/L 11/03/13 11:40 106-43-45.0 10
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 11:40 96-12-810.0 10
Dibromochloromethane ND ug/L 11/03/13 11:40 124-48-15.0 10
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 11:40 106-93-45.0 10
Dibromomethane ND ug/L 11/03/13 11:40 74-95-35.0 10
1,2-Dichlorobenzene ND ug/L 11/03/13 11:40 95-50-15.0 10
1,3-Dichlorobenzene ND ug/L 11/03/13 11:40 541-73-15.0 10
1,4-Dichlorobenzene ND ug/L 11/03/13 11:40 106-46-75.0 10
Dichlorodifluoromethane ND ug/L 11/03/13 11:40 75-71-85.0 10
1,1-Dichloroethane ND ug/L 11/03/13 11:40 75-34-35.0 10
1,2-Dichloroethane ND ug/L 11/03/13 11:40 107-06-25.0 10
1,1-Dichloroethene ND ug/L 11/03/13 11:40 75-35-45.0 10
cis-1,2-Dichloroethene ND ug/L 11/03/13 11:40 156-59-25.0 10
trans-1,2-Dichloroethene ND ug/L 11/03/13 11:40 156-60-55.0 10
1,2-Dichloropropane ND ug/L 11/03/13 11:40 78-87-55.0 10
1,3-Dichloropropane ND ug/L 11/03/13 11:40 142-28-95.0 10
2,2-Dichloropropane ND ug/L 11/03/13 11:40 594-20-75.0 10
1,1-Dichloropropene ND ug/L 11/03/13 11:40 563-58-65.0 10
cis-1,3-Dichloropropene ND ug/L 11/03/13 11:40 10061-01-55.0 10
trans-1,3-Dichloropropene ND ug/L 11/03/13 11:40 10061-02-65.0 10
Diisopropyl ether ND ug/L 11/03/13 11:40 108-20-35.0 10
Ethylbenzene 335 ug/L 11/03/13 11:40 100-41-45.0 10
Hexachloro-1,3-butadiene ND ug/L 11/03/13 11:40 87-68-320.0 10
Isopropylbenzene (Cumene)40.0 ug/L 11/03/13 11:40 98-82-85.0 10
Methylene Chloride ND ug/L 11/03/13 11:40 75-09-220.0 10
Methyl-tert-butyl ether 18.4 ug/L 11/03/13 11:40 1634-04-45.0 10
Naphthalene 159 ug/L 11/03/13 11:40 91-20-320.0 10
n-Propylbenzene 78.9 ug/L 11/03/13 11:40 103-65-15.0 10
Styrene ND ug/L 11/03/13 11:40 100-42-55.0 10
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 11:40 630-20-65.0 10
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 11:40 79-34-55.0 10
Tetrachloroethene ND ug/L 11/03/13 11:40 127-18-45.0 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 17 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW7 Lab ID: 92177732007 Collected: 10/29/13 11:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene 9.7 ug/L 11/03/13 11:40 108-88-35.0 10
1,2,3-Trichlorobenzene ND ug/L 11/03/13 11:40 87-61-620.0 10
1,2,4-Trichlorobenzene ND ug/L 11/03/13 11:40 120-82-120.0 10
1,1,1-Trichloroethane ND ug/L 11/03/13 11:40 71-55-65.0 10
1,1,2-Trichloroethane ND ug/L 11/03/13 11:40 79-00-55.0 10
Trichloroethene ND ug/L 11/03/13 11:40 79-01-65.0 10
Trichlorofluoromethane ND ug/L 11/03/13 11:40 75-69-410.0 10
1,2,3-Trichloropropane ND ug/L 11/03/13 11:40 96-18-45.0 10
1,2,4-Trimethylbenzene 1050 ug/L 11/03/13 11:40 95-63-65.0 10
1,3,5-Trimethylbenzene 334 ug/L 11/03/13 11:40 108-67-85.0 10
Vinyl chloride ND ug/L 11/03/13 11:40 75-01-410.0 10
m&p-Xylene 590 ug/L 11/03/13 11:40 179601-23-110.0 10
o-Xylene 213 ug/L 11/03/13 11:40 95-47-65.0 10
Surrogates
1,2-Dichloroethane-d4 (S) 102 % 11/03/13 11:40 17060-07-070-130 10
4-Bromofluorobenzene (S) 102 % 11/03/13 11:40 460-00-470-130 10
Toluene-d8 (S) 99 % 11/03/13 11:40 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 18 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW8A Lab ID: 92177732008 Collected: 10/29/13 12:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 08:56 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 08:56 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 08:56 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 08:56 75-27-40.50 1
Bromoform ND ug/L 11/03/13 08:56 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 08:56 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 08:56 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 08:56 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 08:56 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 08:56 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 08:56 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 08:56 75-00-31.0 1
Chloroform ND ug/L 11/03/13 08:56 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 08:56 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 08:56 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 08:56 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 08:56 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 08:56 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 08:56 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 08:56 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 08:56 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 08:56 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 08:56 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 08:56 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 08:56 75-34-30.50 1
1,2-Dichloroethane 0.66 ug/L 11/03/13 08:56 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 08:56 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 08:56 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 08:56 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 08:56 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 08:56 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 08:56 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 08:56 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 08:56 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 08:56 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 08:56 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 08:56 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 08:56 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 08:56 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 08:56 75-09-22.0 1
Methyl-tert-butyl ether 16.9 ug/L 11/03/13 08:56 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 08:56 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 08:56 103-65-10.50 1
Styrene ND ug/L 11/03/13 08:56 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 08:56 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 08:56 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 08:56 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 19 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW8A Lab ID: 92177732008 Collected: 10/29/13 12:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 08:56 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 08:56 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 08:56 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 08:56 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 08:56 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 08:56 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 08:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 08:56 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 08:56 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 08:56 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 08:56 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 08:56 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 08:56 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 102 % 11/03/13 08:56 17060-07-070-130 1
4-Bromofluorobenzene (S) 95 % 11/03/13 08:56 460-00-470-130 1
Toluene-d8 (S) 100 % 11/03/13 08:56 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 20 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW9 Lab ID: 92177732009 Collected: 10/29/13 12:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 0.64 ug/L 11/03/13 10:34 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 10:34 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 10:34 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 10:34 75-27-40.50 1
Bromoform ND ug/L 11/03/13 10:34 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 10:34 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 10:34 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 10:34 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 10:34 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 10:34 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 10:34 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 10:34 75-00-31.0 1
Chloroform ND ug/L 11/03/13 10:34 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 10:34 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 10:34 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 10:34 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 10:34 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 10:34 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 10:34 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 10:34 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 10:34 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 10:34 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 10:34 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 10:34 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 10:34 75-34-30.50 1
1,2-Dichloroethane 18.7 ug/L 11/03/13 10:34 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 10:34 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 10:34 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 10:34 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 10:34 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 10:34 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 10:34 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 10:34 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 10:34 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 10:34 10061-02-60.50 1
Diisopropyl ether 4.1 ug/L 11/03/13 10:34 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 10:34 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 10:34 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 10:34 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 10:34 75-09-22.0 1
Methyl-tert-butyl ether 0.52 ug/L 11/03/13 10:34 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 10:34 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 10:34 103-65-10.50 1
Styrene ND ug/L 11/03/13 10:34 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 10:34 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 10:34 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 10:34 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 21 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW9 Lab ID: 92177732009 Collected: 10/29/13 12:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 10:34 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 10:34 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 10:34 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 10:34 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 10:34 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 10:34 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 10:34 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 10:34 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 10:34 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 10:34 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 10:34 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 10:34 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 10:34 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 105 % 11/03/13 10:34 17060-07-070-130 1
4-Bromofluorobenzene (S) 95 % 11/03/13 10:34 460-00-470-130 1
Toluene-d8 (S) 100 % 11/03/13 10:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 22 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW10 Lab ID: 92177732010 Collected: 10/29/13 13:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 09:12 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 09:12 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 09:12 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 09:12 75-27-40.50 1
Bromoform ND ug/L 11/03/13 09:12 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 09:12 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 09:12 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 09:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 09:12 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 09:12 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 09:12 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 09:12 75-00-31.0 1
Chloroform ND ug/L 11/03/13 09:12 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 09:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 09:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 09:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 09:12 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 09:12 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 09:12 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 09:12 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 09:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 09:12 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 09:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 09:12 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 09:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 09:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 09:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 09:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 09:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 09:12 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 09:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 09:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 09:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 09:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 09:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 09:12 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 09:12 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 09:12 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 09:12 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 09:12 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 09:12 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 09:12 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 09:12 103-65-10.50 1
Styrene ND ug/L 11/03/13 09:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 09:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 09:12 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 09:12 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 23 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW10 Lab ID: 92177732010 Collected: 10/29/13 13:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 09:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 09:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 09:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 09:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 09:12 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 09:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 09:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 09:12 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 09:12 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 09:12 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 09:12 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 09:12 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 09:12 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 104 % 11/03/13 09:12 17060-07-070-130 1
4-Bromofluorobenzene (S) 97 % 11/03/13 09:12 460-00-470-130 1
Toluene-d8 (S) 100 % 11/03/13 09:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 24 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW11 Lab ID: 92177732011 Collected: 10/29/13 13:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 09:28 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 09:28 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 09:28 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 09:28 75-27-40.50 1
Bromoform ND ug/L 11/03/13 09:28 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 09:28 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 09:28 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 09:28 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 09:28 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 09:28 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 09:28 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 09:28 75-00-31.0 1
Chloroform ND ug/L 11/03/13 09:28 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 09:28 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 09:28 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 09:28 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 09:28 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 09:28 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 09:28 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 09:28 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 09:28 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 09:28 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 09:28 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 09:28 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 09:28 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 09:28 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 09:28 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 09:28 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 09:28 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 09:28 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 09:28 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 09:28 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 09:28 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 09:28 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 09:28 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 09:28 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 09:28 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 09:28 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 09:28 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 09:28 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 09:28 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 09:28 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 09:28 103-65-10.50 1
Styrene ND ug/L 11/03/13 09:28 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 09:28 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 09:28 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 09:28 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 25 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW11 Lab ID: 92177732011 Collected: 10/29/13 13:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 09:28 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 09:28 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 09:28 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 09:28 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 09:28 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 09:28 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 09:28 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 09:28 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 09:28 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 09:28 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 09:28 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 09:28 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 09:28 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 105 % 11/03/13 09:28 17060-07-070-130 1
4-Bromofluorobenzene (S) 94 % 11/03/13 09:28 460-00-470-130 1
Toluene-d8 (S) 99 % 11/03/13 09:28 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 26 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW12 Lab ID: 92177732012 Collected: 10/29/13 13:50 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 8.4 ug/L 11/03/13 12:46 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 12:46 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 12:46 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 12:46 75-27-40.50 1
Bromoform ND ug/L 11/03/13 12:46 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 12:46 74-83-95.0 1
n-Butylbenzene 0.54 ug/L 11/03/13 12:46 104-51-80.50 1
sec-Butylbenzene 0.87 ug/L 11/03/13 12:46 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 12:46 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 12:46 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 12:46 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 12:46 75-00-31.0 1
Chloroform ND ug/L 11/03/13 12:46 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 12:46 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 12:46 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 12:46 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 12:46 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 12:46 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 12:46 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 12:46 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 12:46 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 12:46 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 12:46 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 12:46 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 12:46 75-34-30.50 1
1,2-Dichloroethane 9.9 ug/L 11/03/13 12:46 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 12:46 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 12:46 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 12:46 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 12:46 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 12:46 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 12:46 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 12:46 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 12:46 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 12:46 10061-02-60.50 1
Diisopropyl ether 2.4 ug/L 11/03/13 12:46 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 12:46 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 12:46 87-68-32.0 1
Isopropylbenzene (Cumene)3.4 ug/L 11/03/13 12:46 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 12:46 75-09-22.0 1
Methyl-tert-butyl ether 7.8 ug/L 11/03/13 12:46 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 12:46 91-20-32.0 1
n-Propylbenzene 0.63 ug/L 11/03/13 12:46 103-65-10.50 1
Styrene ND ug/L 11/03/13 12:46 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 12:46 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 12:46 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 12:46 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 27 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW12 Lab ID: 92177732012 Collected: 10/29/13 13:50 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 12:46 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 12:46 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 12:46 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 12:46 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 12:46 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 12:46 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 12:46 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 12:46 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 12:46 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 12:46 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 12:46 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 12:46 179601-23-11.0 1
o-Xylene 0.56 ug/L 11/03/13 12:46 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 97 % 11/03/13 12:46 17060-07-070-130 1
4-Bromofluorobenzene (S) 99 % 11/03/13 12:46 460-00-470-130 1
Toluene-d8 (S) 99 % 11/03/13 12:46 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 28 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW13 Lab ID: 92177732013 Collected: 10/29/13 14:10 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 10:51 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 10:51 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 10:51 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 10:51 75-27-40.50 1
Bromoform ND ug/L 11/03/13 10:51 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 10:51 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 10:51 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 10:51 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 10:51 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 10:51 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 10:51 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 10:51 75-00-31.0 1
Chloroform ND ug/L 11/03/13 10:51 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 10:51 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 10:51 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 10:51 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 10:51 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 10:51 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 10:51 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 10:51 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 10:51 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 10:51 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 10:51 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 10:51 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 10:51 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 10:51 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 10:51 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 10:51 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 10:51 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 10:51 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 10:51 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 10:51 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 10:51 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 10:51 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 10:51 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 10:51 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 10:51 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 10:51 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 10:51 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 10:51 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 10:51 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 10:51 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 10:51 103-65-10.50 1
Styrene ND ug/L 11/03/13 10:51 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 10:51 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 10:51 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 10:51 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 29 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW13 Lab ID: 92177732013 Collected: 10/29/13 14:10 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene 1.9 ug/L 11/03/13 10:51 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 10:51 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 10:51 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 10:51 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 10:51 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 10:51 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 10:51 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 10:51 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 10:51 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 10:51 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 10:51 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 10:51 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 10:51 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 107 % 11/03/13 10:51 17060-07-070-130 1
4-Bromofluorobenzene (S) 95 % 11/03/13 10:51 460-00-470-130 1
Toluene-d8 (S) 100 % 11/03/13 10:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 30 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW14 Lab ID: 92177732014 Collected: 10/29/13 14:40 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 2.1 ug/L 11/03/13 11:57 71-43-21.0 2
Bromobenzene ND ug/L 11/03/13 11:57 108-86-11.0 2
Bromochloromethane ND ug/L 11/03/13 11:57 74-97-51.0 2
Bromodichloromethane ND ug/L 11/03/13 11:57 75-27-41.0 2
Bromoform ND ug/L 11/03/13 11:57 75-25-21.0 2
Bromomethane ND ug/L 11/03/13 11:57 74-83-910.0 2
n-Butylbenzene ND ug/L 11/03/13 11:57 104-51-81.0 2
sec-Butylbenzene 2.3 ug/L 11/03/13 11:57 135-98-81.0 2
tert-Butylbenzene ND ug/L 11/03/13 11:57 98-06-61.0 2
Carbon tetrachloride ND ug/L 11/03/13 11:57 56-23-51.0 2
Chlorobenzene ND ug/L 11/03/13 11:57 108-90-71.0 2
Chloroethane ND ug/L 11/03/13 11:57 75-00-32.0 2
Chloroform ND ug/L 11/03/13 11:57 67-66-31.0 2
Chloromethane ND ug/L 11/03/13 11:57 74-87-32.0 2
2-Chlorotoluene ND ug/L 11/03/13 11:57 95-49-81.0 2
4-Chlorotoluene ND ug/L 11/03/13 11:57 106-43-41.0 2
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 11:57 96-12-82.0 2
Dibromochloromethane ND ug/L 11/03/13 11:57 124-48-11.0 2
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 11:57 106-93-41.0 2
Dibromomethane ND ug/L 11/03/13 11:57 74-95-31.0 2
1,2-Dichlorobenzene ND ug/L 11/03/13 11:57 95-50-11.0 2
1,3-Dichlorobenzene ND ug/L 11/03/13 11:57 541-73-11.0 2
1,4-Dichlorobenzene ND ug/L 11/03/13 11:57 106-46-71.0 2
Dichlorodifluoromethane ND ug/L 11/03/13 11:57 75-71-81.0 2
1,1-Dichloroethane ND ug/L 11/03/13 11:57 75-34-31.0 2
1,2-Dichloroethane ND ug/L 11/03/13 11:57 107-06-21.0 2
1,1-Dichloroethene ND ug/L 11/03/13 11:57 75-35-41.0 2
cis-1,2-Dichloroethene ND ug/L 11/03/13 11:57 156-59-21.0 2
trans-1,2-Dichloroethene ND ug/L 11/03/13 11:57 156-60-51.0 2
1,2-Dichloropropane ND ug/L 11/03/13 11:57 78-87-51.0 2
1,3-Dichloropropane ND ug/L 11/03/13 11:57 142-28-91.0 2
2,2-Dichloropropane ND ug/L 11/03/13 11:57 594-20-71.0 2
1,1-Dichloropropene ND ug/L 11/03/13 11:57 563-58-61.0 2
cis-1,3-Dichloropropene ND ug/L 11/03/13 11:57 10061-01-51.0 2
trans-1,3-Dichloropropene ND ug/L 11/03/13 11:57 10061-02-61.0 2
Diisopropyl ether ND ug/L 11/03/13 11:57 108-20-31.0 2
Ethylbenzene 7.7 ug/L 11/03/13 11:57 100-41-41.0 2
Hexachloro-1,3-butadiene ND ug/L 11/03/13 11:57 87-68-34.0 2
Isopropylbenzene (Cumene)3.2 ug/L 11/03/13 11:57 98-82-81.0 2
Methylene Chloride ND ug/L 11/03/13 11:57 75-09-24.0 2
Methyl-tert-butyl ether ND ug/L 11/03/13 11:57 1634-04-41.0 2
Naphthalene 196 ug/L 11/03/13 11:57 91-20-34.0 2
n-Propylbenzene 4.8 ug/L 11/03/13 11:57 103-65-11.0 2
Styrene ND ug/L 11/03/13 11:57 100-42-51.0 2
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 11:57 630-20-61.0 2
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 11:57 79-34-51.0 2
Tetrachloroethene ND ug/L 11/03/13 11:57 127-18-41.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 31 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW14 Lab ID: 92177732014 Collected: 10/29/13 14:40 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 11:57 108-88-31.0 2
1,2,3-Trichlorobenzene ND ug/L 11/03/13 11:57 87-61-64.0 2
1,2,4-Trichlorobenzene ND ug/L 11/03/13 11:57 120-82-14.0 2
1,1,1-Trichloroethane ND ug/L 11/03/13 11:57 71-55-61.0 2
1,1,2-Trichloroethane ND ug/L 11/03/13 11:57 79-00-51.0 2
Trichloroethene ND ug/L 11/03/13 11:57 79-01-61.0 2
Trichlorofluoromethane ND ug/L 11/03/13 11:57 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 11/03/13 11:57 96-18-41.0 2
1,2,4-Trimethylbenzene 26.6 ug/L 11/03/13 11:57 95-63-61.0 2
1,3,5-Trimethylbenzene ND ug/L 11/03/13 11:57 108-67-81.0 2
Vinyl chloride ND ug/L 11/03/13 11:57 75-01-42.0 2
m&p-Xylene ND ug/L 11/03/13 11:57 179601-23-12.0 2
o-Xylene ND ug/L 11/03/13 11:57 95-47-61.0 2
Surrogates
1,2-Dichloroethane-d4 (S) 103 % 11/03/13 11:57 17060-07-070-130 2
4-Bromofluorobenzene (S) 99 % 11/03/13 11:57 460-00-470-130 2
Toluene-d8 (S) 100 % 11/03/13 11:57 2037-26-570-130 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 32 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW15 Lab ID: 92177732015 Collected: 10/29/13 15:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 12:13 71-43-22.0 4
Bromobenzene ND ug/L 11/03/13 12:13 108-86-12.0 4
Bromochloromethane ND ug/L 11/03/13 12:13 74-97-52.0 4
Bromodichloromethane ND ug/L 11/03/13 12:13 75-27-42.0 4
Bromoform ND ug/L 11/03/13 12:13 75-25-22.0 4
Bromomethane ND ug/L 11/03/13 12:13 74-83-920.0 4
n-Butylbenzene 8.5 ug/L 11/03/13 12:13 104-51-82.0 4
sec-Butylbenzene 8.5 ug/L 11/03/13 12:13 135-98-82.0 4
tert-Butylbenzene ND ug/L 11/03/13 12:13 98-06-62.0 4
Carbon tetrachloride ND ug/L 11/03/13 12:13 56-23-52.0 4
Chlorobenzene ND ug/L 11/03/13 12:13 108-90-72.0 4
Chloroethane ND ug/L 11/03/13 12:13 75-00-34.0 4
Chloroform ND ug/L 11/03/13 12:13 67-66-32.0 4
Chloromethane ND ug/L 11/03/13 12:13 74-87-34.0 4
2-Chlorotoluene ND ug/L 11/03/13 12:13 95-49-82.0 4
4-Chlorotoluene ND ug/L 11/03/13 12:13 106-43-42.0 4
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 12:13 96-12-84.0 4
Dibromochloromethane ND ug/L 11/03/13 12:13 124-48-12.0 4
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 12:13 106-93-42.0 4
Dibromomethane ND ug/L 11/03/13 12:13 74-95-32.0 4
1,2-Dichlorobenzene ND ug/L 11/03/13 12:13 95-50-12.0 4
1,3-Dichlorobenzene ND ug/L 11/03/13 12:13 541-73-12.0 4
1,4-Dichlorobenzene ND ug/L 11/03/13 12:13 106-46-72.0 4
Dichlorodifluoromethane ND ug/L 11/03/13 12:13 75-71-82.0 4
1,1-Dichloroethane ND ug/L 11/03/13 12:13 75-34-32.0 4
1,2-Dichloroethane ND ug/L 11/03/13 12:13 107-06-22.0 4
1,1-Dichloroethene ND ug/L 11/03/13 12:13 75-35-42.0 4
cis-1,2-Dichloroethene ND ug/L 11/03/13 12:13 156-59-22.0 4
trans-1,2-Dichloroethene ND ug/L 11/03/13 12:13 156-60-52.0 4
1,2-Dichloropropane ND ug/L 11/03/13 12:13 78-87-52.0 4
1,3-Dichloropropane ND ug/L 11/03/13 12:13 142-28-92.0 4
2,2-Dichloropropane ND ug/L 11/03/13 12:13 594-20-72.0 4
1,1-Dichloropropene ND ug/L 11/03/13 12:13 563-58-62.0 4
cis-1,3-Dichloropropene ND ug/L 11/03/13 12:13 10061-01-52.0 4
trans-1,3-Dichloropropene ND ug/L 11/03/13 12:13 10061-02-62.0 4
Diisopropyl ether ND ug/L 11/03/13 12:13 108-20-32.0 4
Ethylbenzene 300 ug/L 11/03/13 12:13 100-41-42.0 4
Hexachloro-1,3-butadiene ND ug/L 11/03/13 12:13 87-68-38.0 4
Isopropylbenzene (Cumene)34.5 ug/L 11/03/13 12:13 98-82-82.0 4
Methylene Chloride ND ug/L 11/03/13 12:13 75-09-28.0 4
Methyl-tert-butyl ether ND ug/L 11/03/13 12:13 1634-04-42.0 4
Naphthalene 307 ug/L 11/03/13 12:13 91-20-38.0 4
n-Propylbenzene 85.1 ug/L 11/03/13 12:13 103-65-12.0 4
Styrene ND ug/L 11/03/13 12:13 100-42-52.0 4
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 12:13 630-20-62.0 4
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 12:13 79-34-52.0 4
Tetrachloroethene ND ug/L 11/03/13 12:13 127-18-42.0 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 33 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW15 Lab ID: 92177732015 Collected: 10/29/13 15:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 12:13 108-88-32.0 4
1,2,3-Trichlorobenzene ND ug/L 11/03/13 12:13 87-61-68.0 4
1,2,4-Trichlorobenzene ND ug/L 11/03/13 12:13 120-82-18.0 4
1,1,1-Trichloroethane ND ug/L 11/03/13 12:13 71-55-62.0 4
1,1,2-Trichloroethane ND ug/L 11/03/13 12:13 79-00-52.0 4
Trichloroethene ND ug/L 11/03/13 12:13 79-01-62.0 4
Trichlorofluoromethane ND ug/L 11/03/13 12:13 75-69-44.0 4
1,2,3-Trichloropropane ND ug/L 11/03/13 12:13 96-18-42.0 4
1,2,4-Trimethylbenzene 250 ug/L 11/03/13 12:13 95-63-62.0 4
1,3,5-Trimethylbenzene 64.1 ug/L 11/03/13 12:13 108-67-82.0 4
Vinyl chloride ND ug/L 11/03/13 12:13 75-01-44.0 4
m&p-Xylene 412 ug/L 11/03/13 12:13 179601-23-14.0 4
o-Xylene 8.0 ug/L 11/03/13 12:13 95-47-62.0 4
Surrogates
1,2-Dichloroethane-d4 (S) 99 % 11/03/13 12:13 17060-07-070-130 4
4-Bromofluorobenzene (S) 101 % 11/03/13 12:13 460-00-470-130 4
Toluene-d8 (S) 102 % 11/03/13 12:13 2037-26-570-130 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 34 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW16 Lab ID: 92177732016 Collected: 10/29/13 15:20 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 0.60 ug/L 11/03/13 13:36 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 13:36 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 13:36 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 13:36 75-27-40.50 1
Bromoform ND ug/L 11/03/13 13:36 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 13:36 74-83-95.0 1
n-Butylbenzene 1.2 ug/L 11/03/13 13:36 104-51-80.50 1
sec-Butylbenzene 1.3 ug/L 11/03/13 13:36 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 13:36 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 13:36 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 13:36 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 13:36 75-00-31.0 1
Chloroform ND ug/L 11/03/13 13:36 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 13:36 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 13:36 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 13:36 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 13:36 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 13:36 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 13:36 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 13:36 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 13:36 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 13:36 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 13:36 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 13:36 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 13:36 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 13:36 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 13:36 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 13:36 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 13:36 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 13:36 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 13:36 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 13:36 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 13:36 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 13:36 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 13:36 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 13:36 108-20-30.50 1
Ethylbenzene 0.62 ug/L 11/03/13 13:36 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 13:36 87-68-32.0 1
Isopropylbenzene (Cumene)1.6 ug/L 11/03/13 13:36 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 13:36 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 13:36 1634-04-40.50 1
Naphthalene 42.7 ug/L 11/03/13 13:36 91-20-32.0 1
n-Propylbenzene 2.0 ug/L 11/03/13 13:36 103-65-10.50 1
Styrene ND ug/L 11/03/13 13:36 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 13:36 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 13:36 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 13:36 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 35 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW16 Lab ID: 92177732016 Collected: 10/29/13 15:20 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 13:36 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 13:36 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 13:36 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 13:36 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 13:36 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 13:36 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 13:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 13:36 96-18-40.50 1
1,2,4-Trimethylbenzene 2.1 ug/L 11/03/13 13:36 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 13:36 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 13:36 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 13:36 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 13:36 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 96 % 11/03/13 13:36 17060-07-070-130 1
4-Bromofluorobenzene (S) 97 % 11/03/13 13:36 460-00-470-130 1
Toluene-d8 (S) 100 % 11/03/13 13:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 36 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW17 Lab ID: 92177732017 Collected: 10/29/13 15:40 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 0.94 ug/L 11/03/13 11:07 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 11:07 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 11:07 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 11:07 75-27-40.50 1
Bromoform ND ug/L 11/03/13 11:07 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 11:07 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 11:07 104-51-80.50 1
sec-Butylbenzene 0.62 ug/L 11/03/13 11:07 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 11:07 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 11:07 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 11:07 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 11:07 75-00-31.0 1
Chloroform ND ug/L 11/03/13 11:07 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 11:07 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 11:07 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 11:07 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 11:07 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 11:07 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 11:07 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 11:07 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 11:07 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 11:07 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 11:07 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 11:07 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 11:07 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 11:07 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 11:07 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 11:07 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 11:07 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 11:07 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 11:07 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 11:07 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 11:07 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 11:07 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 11:07 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 11:07 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 11:07 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 11:07 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 11:07 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 11:07 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 11:07 1634-04-40.50 1
Naphthalene 16.3 ug/L 11/03/13 11:07 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 11:07 103-65-10.50 1
Styrene ND ug/L 11/03/13 11:07 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 11:07 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 11:07 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 11:07 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 37 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW17 Lab ID: 92177732017 Collected: 10/29/13 15:40 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 11:07 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 11:07 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 11:07 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 11:07 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 11:07 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 11:07 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 11:07 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 11:07 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 11:07 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 11:07 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 11:07 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 11:07 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 11:07 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 107 % 11/03/13 11:07 17060-07-070-130 1
4-Bromofluorobenzene (S) 98 % 11/03/13 11:07 460-00-470-130 1
Toluene-d8 (S) 100 % 11/03/13 11:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 38 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW18 Lab ID: 92177732018 Collected: 10/29/13 16:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene 187 ug/L 11/03/13 11:24 71-43-22.0 4
Bromobenzene ND ug/L 11/03/13 11:24 108-86-12.0 4
Bromochloromethane ND ug/L 11/03/13 11:24 74-97-52.0 4
Bromodichloromethane ND ug/L 11/03/13 11:24 75-27-42.0 4
Bromoform ND ug/L 11/03/13 11:24 75-25-22.0 4
Bromomethane ND ug/L 11/03/13 11:24 74-83-920.0 4
n-Butylbenzene ND ug/L 11/03/13 11:24 104-51-82.0 4
sec-Butylbenzene 2.7 ug/L 11/03/13 11:24 135-98-82.0 4
tert-Butylbenzene ND ug/L 11/03/13 11:24 98-06-62.0 4
Carbon tetrachloride ND ug/L 11/03/13 11:24 56-23-52.0 4
Chlorobenzene ND ug/L 11/03/13 11:24 108-90-72.0 4
Chloroethane ND ug/L 11/03/13 11:24 75-00-34.0 4
Chloroform ND ug/L 11/03/13 11:24 67-66-32.0 4
Chloromethane ND ug/L 11/03/13 11:24 74-87-34.0 4
2-Chlorotoluene ND ug/L 11/03/13 11:24 95-49-82.0 4
4-Chlorotoluene ND ug/L 11/03/13 11:24 106-43-42.0 4
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 11:24 96-12-84.0 4
Dibromochloromethane ND ug/L 11/03/13 11:24 124-48-12.0 4
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 11:24 106-93-42.0 4
Dibromomethane ND ug/L 11/03/13 11:24 74-95-32.0 4
1,2-Dichlorobenzene ND ug/L 11/03/13 11:24 95-50-12.0 4
1,3-Dichlorobenzene ND ug/L 11/03/13 11:24 541-73-12.0 4
1,4-Dichlorobenzene ND ug/L 11/03/13 11:24 106-46-72.0 4
Dichlorodifluoromethane ND ug/L 11/03/13 11:24 75-71-82.0 4
1,1-Dichloroethane ND ug/L 11/03/13 11:24 75-34-32.0 4
1,2-Dichloroethane 5.9 ug/L 11/03/13 11:24 107-06-22.0 4
1,1-Dichloroethene ND ug/L 11/03/13 11:24 75-35-42.0 4
cis-1,2-Dichloroethene ND ug/L 11/03/13 11:24 156-59-22.0 4
trans-1,2-Dichloroethene ND ug/L 11/03/13 11:24 156-60-52.0 4
1,2-Dichloropropane ND ug/L 11/03/13 11:24 78-87-52.0 4
1,3-Dichloropropane ND ug/L 11/03/13 11:24 142-28-92.0 4
2,2-Dichloropropane ND ug/L 11/03/13 11:24 594-20-72.0 4
1,1-Dichloropropene ND ug/L 11/03/13 11:24 563-58-62.0 4
cis-1,3-Dichloropropene ND ug/L 11/03/13 11:24 10061-01-52.0 4
trans-1,3-Dichloropropene ND ug/L 11/03/13 11:24 10061-02-62.0 4
Diisopropyl ether ND ug/L 11/03/13 11:24 108-20-32.0 4
Ethylbenzene 100 ug/L 11/03/13 11:24 100-41-42.0 4
Hexachloro-1,3-butadiene ND ug/L 11/03/13 11:24 87-68-38.0 4
Isopropylbenzene (Cumene)13.0 ug/L 11/03/13 11:24 98-82-82.0 4
Methylene Chloride ND ug/L 11/03/13 11:24 75-09-28.0 4
Methyl-tert-butyl ether 294 ug/L 11/03/13 11:24 1634-04-42.0 4
Naphthalene 65.3 ug/L 11/03/13 11:24 91-20-38.0 4
n-Propylbenzene 33.8 ug/L 11/03/13 11:24 103-65-12.0 4
Styrene ND ug/L 11/03/13 11:24 100-42-52.0 4
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 11:24 630-20-62.0 4
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 11:24 79-34-52.0 4
Tetrachloroethene ND ug/L 11/03/13 11:24 127-18-42.0 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 39 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: MW18 Lab ID: 92177732018 Collected: 10/29/13 16:00 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 11:24 108-88-32.0 4
1,2,3-Trichlorobenzene ND ug/L 11/03/13 11:24 87-61-68.0 4
1,2,4-Trichlorobenzene ND ug/L 11/03/13 11:24 120-82-18.0 4
1,1,1-Trichloroethane ND ug/L 11/03/13 11:24 71-55-62.0 4
1,1,2-Trichloroethane ND ug/L 11/03/13 11:24 79-00-52.0 4
Trichloroethene ND ug/L 11/03/13 11:24 79-01-62.0 4
Trichlorofluoromethane ND ug/L 11/03/13 11:24 75-69-44.0 4
1,2,3-Trichloropropane ND ug/L 11/03/13 11:24 96-18-42.0 4
1,2,4-Trimethylbenzene 10.9 ug/L 11/03/13 11:24 95-63-62.0 4
1,3,5-Trimethylbenzene ND ug/L 11/03/13 11:24 108-67-82.0 4
Vinyl chloride ND ug/L 11/03/13 11:24 75-01-44.0 4
m&p-Xylene 6.3 ug/L 11/03/13 11:24 179601-23-14.0 4
o-Xylene ND ug/L 11/03/13 11:24 95-47-62.0 4
Surrogates
1,2-Dichloroethane-d4 (S) 101 % 11/03/13 11:24 17060-07-070-130 4
4-Bromofluorobenzene (S) 98 % 11/03/13 11:24 460-00-470-130 4
Toluene-d8 (S) 99 % 11/03/13 11:24 2037-26-570-130 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 40 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: VEW-1 Lab ID: 92177732019 Collected: 10/29/13 16:50 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 09:45 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 09:45 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 09:45 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 09:45 75-27-40.50 1
Bromoform ND ug/L 11/03/13 09:45 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 09:45 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 09:45 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 09:45 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 09:45 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 09:45 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 09:45 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 09:45 75-00-31.0 1
Chloroform ND ug/L 11/03/13 09:45 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 09:45 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 09:45 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 09:45 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 09:45 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 09:45 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 09:45 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 09:45 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 09:45 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 09:45 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 09:45 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 09:45 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 09:45 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 09:45 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 09:45 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 09:45 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 09:45 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 09:45 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 09:45 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 09:45 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 09:45 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 09:45 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 09:45 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 09:45 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 09:45 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 09:45 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 09:45 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 09:45 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 09:45 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 09:45 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 09:45 103-65-10.50 1
Styrene ND ug/L 11/03/13 09:45 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 09:45 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 09:45 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 09:45 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 41 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: VEW-1 Lab ID: 92177732019 Collected: 10/29/13 16:50 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 09:45 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 09:45 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 09:45 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 09:45 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 09:45 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 09:45 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 09:45 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 09:45 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 09:45 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 09:45 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 09:45 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 09:45 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 09:45 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 106 % 11/03/13 09:45 17060-07-070-130 1
4-Bromofluorobenzene (S) 96 % 11/03/13 09:45 460-00-470-130 1
Toluene-d8 (S) 100 % 11/03/13 09:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 42 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: SW-1 Lab ID: 92177732020 Collected: 10/29/13 16:10 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 10:02 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 10:02 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 10:02 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 10:02 75-27-40.50 1
Bromoform ND ug/L 11/03/13 10:02 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 10:02 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 10:02 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 10:02 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 10:02 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 10:02 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 10:02 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 10:02 75-00-31.0 1
Chloroform ND ug/L 11/03/13 10:02 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 10:02 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 10:02 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 10:02 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 10:02 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 10:02 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 10:02 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 10:02 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 10:02 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 10:02 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 10:02 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 10:02 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 10:02 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 10:02 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 10:02 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 10:02 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 10:02 156-60-50.50 1
1,2-Dichloropropane 1.4 ug/L 11/03/13 10:02 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 10:02 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 10:02 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 10:02 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 10:02 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 10:02 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 10:02 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 10:02 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 10:02 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 10:02 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 10:02 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 10:02 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 10:02 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 10:02 103-65-10.50 1
Styrene ND ug/L 11/03/13 10:02 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 10:02 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 10:02 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 10:02 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 43 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: SW-1 Lab ID: 92177732020 Collected: 10/29/13 16:10 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 10:02 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 10:02 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 10:02 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 10:02 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 10:02 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 10:02 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 10:02 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 10:02 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 10:02 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 10:02 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 10:02 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 10:02 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 10:02 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 106 % 11/03/13 10:02 17060-07-070-130 1
4-Bromofluorobenzene (S) 94 % 11/03/13 10:02 460-00-470-130 1
Toluene-d8 (S) 99 % 11/03/13 10:02 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 44 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: IW-8 Lab ID: 92177732021 Collected: 10/29/13 16:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/06/13 21:39 71-43-20.50 1
Bromobenzene ND ug/L 11/06/13 21:39 108-86-10.50 1
Bromochloromethane ND ug/L 11/06/13 21:39 74-97-50.50 1
Bromodichloromethane ND ug/L 11/06/13 21:39 75-27-40.50 1
Bromoform ND ug/L 11/06/13 21:39 75-25-20.50 1
Bromomethane ND ug/L 11/06/13 21:39 74-83-95.0 1
n-Butylbenzene ND ug/L 11/06/13 21:39 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/06/13 21:39 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/06/13 21:39 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/06/13 21:39 56-23-50.50 1
Chlorobenzene ND ug/L 11/06/13 21:39 108-90-70.50 1
Chloroethane ND ug/L 11/06/13 21:39 75-00-31.0 1
Chloroform ND ug/L 11/06/13 21:39 67-66-30.50 1
Chloromethane ND ug/L 11/06/13 21:39 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/06/13 21:39 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/06/13 21:39 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/06/13 21:39 96-12-81.0 1
Dibromochloromethane ND ug/L 11/06/13 21:39 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/06/13 21:39 106-93-40.50 1
Dibromomethane ND ug/L 11/06/13 21:39 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/06/13 21:39 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/06/13 21:39 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/06/13 21:39 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/06/13 21:39 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/06/13 21:39 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/06/13 21:39 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/06/13 21:39 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/06/13 21:39 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/06/13 21:39 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/06/13 21:39 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/06/13 21:39 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/06/13 21:39 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/06/13 21:39 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/06/13 21:39 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/06/13 21:39 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/06/13 21:39 108-20-30.50 1
Ethylbenzene ND ug/L 11/06/13 21:39 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/06/13 21:39 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/06/13 21:39 98-82-80.50 1
Methylene Chloride ND ug/L 11/06/13 21:39 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/06/13 21:39 1634-04-40.50 1
Naphthalene ND ug/L 11/06/13 21:39 91-20-32.0 1
n-Propylbenzene ND ug/L 11/06/13 21:39 103-65-10.50 1
Styrene ND ug/L 11/06/13 21:39 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/06/13 21:39 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/06/13 21:39 79-34-50.50 1
Tetrachloroethene ND ug/L 11/06/13 21:39 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 45 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: IW-8 Lab ID: 92177732021 Collected: 10/29/13 16:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/06/13 21:39 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/06/13 21:39 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/06/13 21:39 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/06/13 21:39 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/06/13 21:39 79-00-50.50 1
Trichloroethene ND ug/L 11/06/13 21:39 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/06/13 21:39 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/06/13 21:39 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/06/13 21:39 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/06/13 21:39 108-67-80.50 1
Vinyl chloride ND ug/L 11/06/13 21:39 75-01-41.0 1
m&p-Xylene ND ug/L 11/06/13 21:39 179601-23-11.0 1
o-Xylene ND ug/L 11/06/13 21:39 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 103 % 11/06/13 21:39 17060-07-070-130 1
4-Bromofluorobenzene (S) 95 % 11/06/13 21:39 460-00-470-130 1
Toluene-d8 (S) 100 % 11/06/13 21:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 46 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: IW-3 Lab ID: 92177732022 Collected: 10/29/13 17:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 01:32 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 01:32 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 01:32 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 01:32 75-27-40.50 1
Bromoform ND ug/L 11/03/13 01:32 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 01:32 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 01:32 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 01:32 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 01:32 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 01:32 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 01:32 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 01:32 75-00-31.0 1
Chloroform ND ug/L 11/03/13 01:32 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 01:32 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 01:32 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 01:32 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 01:32 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 01:32 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 01:32 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 01:32 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 01:32 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 01:32 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 01:32 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 01:32 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 01:32 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 01:32 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 01:32 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 01:32 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 01:32 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 01:32 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 01:32 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 01:32 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 01:32 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 01:32 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 01:32 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 01:32 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 01:32 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 01:32 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 01:32 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 01:32 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 01:32 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 01:32 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 01:32 103-65-10.50 1
Styrene ND ug/L 11/03/13 01:32 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 01:32 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 01:32 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 01:32 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 47 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: IW-3 Lab ID: 92177732022 Collected: 10/29/13 17:30 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 01:32 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 01:32 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 01:32 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 01:32 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 01:32 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 01:32 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 01:32 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 01:32 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 01:32 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 01:32 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 01:32 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 01:32 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 01:32 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 103 % 11/03/13 01:32 17060-07-070-130 1
4-Bromofluorobenzene (S) 96 % 11/03/13 01:32 460-00-470-130 1
Toluene-d8 (S) 99 % 11/03/13 01:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 48 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: IW-4 Lab ID: 92177732023 Collected: 10/29/13 17:50 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 11/03/13 01:49 71-43-20.50 1
Bromobenzene ND ug/L 11/03/13 01:49 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/13 01:49 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/13 01:49 75-27-40.50 1
Bromoform ND ug/L 11/03/13 01:49 75-25-20.50 1
Bromomethane ND ug/L 11/03/13 01:49 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/13 01:49 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/13 01:49 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/13 01:49 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/13 01:49 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/13 01:49 108-90-70.50 1
Chloroethane ND ug/L 11/03/13 01:49 75-00-31.0 1
Chloroform ND ug/L 11/03/13 01:49 67-66-30.50 1
Chloromethane ND ug/L 11/03/13 01:49 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/13 01:49 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/13 01:49 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/13 01:49 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/13 01:49 124-48-10.50 1
1,2-Dibromoethane (EDB) ND ug/L 11/03/13 01:49 106-93-40.50 1
Dibromomethane ND ug/L 11/03/13 01:49 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/13 01:49 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/13 01:49 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/13 01:49 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/13 01:49 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/13 01:49 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/13 01:49 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/13 01:49 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/13 01:49 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/13 01:49 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/13 01:49 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/13 01:49 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/13 01:49 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/13 01:49 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/13 01:49 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/13 01:49 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/13 01:49 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/13 01:49 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/13 01:49 87-68-32.0 1
Isopropylbenzene (Cumene) ND ug/L 11/03/13 01:49 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/13 01:49 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/13 01:49 1634-04-40.50 1
Naphthalene ND ug/L 11/03/13 01:49 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/13 01:49 103-65-10.50 1
Styrene ND ug/L 11/03/13 01:49 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/13 01:49 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/13 01:49 79-34-50.50 1
Tetrachloroethene ND ug/L 11/03/13 01:49 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 49 of 68
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Sample: IW-4 Lab ID: 92177732023 Collected: 10/29/13 17:50 Received: 10/31/13 09:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
6200B MSV Analytical Method: SM 6200B
Toluene ND ug/L 11/03/13 01:49 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/13 01:49 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/13 01:49 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/13 01:49 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/13 01:49 79-00-50.50 1
Trichloroethene ND ug/L 11/03/13 01:49 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/13 01:49 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/13 01:49 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/13 01:49 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/13 01:49 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/13 01:49 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/13 01:49 179601-23-11.0 1
o-Xylene ND ug/L 11/03/13 01:49 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S) 102 % 11/03/13 01:49 17060-07-070-130 1
4-Bromofluorobenzene (S) 96 % 11/03/13 01:49 460-00-470-130 1
Toluene-d8 (S) 101 % 11/03/13 01:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 50 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/24751
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92177732001, 92177732002, 92177732003, 92177732004, 92177732005, 92177732006, 92177732007,
92177732008, 92177732009, 92177732010, 92177732011, 92177732012, 92177732013, 92177732014,
92177732015, 92177732016, 92177732017, 92177732018, 92177732019, 92177732020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1076701
Associated Lab Samples: 92177732001, 92177732002, 92177732003, 92177732004, 92177732005, 92177732006, 92177732007,
92177732008, 92177732009, 92177732010, 92177732011, 92177732012, 92177732013, 92177732014,
92177732015, 92177732016, 92177732017, 92177732018, 92177732019, 92177732020
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/03/13 08:06
1,1,1-Trichloroethane ug/L ND 0.50 11/03/13 08:06
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/03/13 08:06
1,1,2-Trichloroethane ug/L ND 0.50 11/03/13 08:06
1,1-Dichloroethane ug/L ND 0.50 11/03/13 08:06
1,1-Dichloroethene ug/L ND 0.50 11/03/13 08:06
1,1-Dichloropropene ug/L ND 0.50 11/03/13 08:06
1,2,3-Trichlorobenzene ug/L ND 2.0 11/03/13 08:06
1,2,3-Trichloropropane ug/L ND 0.50 11/03/13 08:06
1,2,4-Trichlorobenzene ug/L ND 2.0 11/03/13 08:06
1,2,4-Trimethylbenzene ug/L ND 0.50 11/03/13 08:06
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/03/13 08:06
1,2-Dibromoethane (EDB) ug/L ND 0.50 11/03/13 08:06
1,2-Dichlorobenzene ug/L ND 0.50 11/03/13 08:06
1,2-Dichloroethane ug/L ND 0.50 11/03/13 08:06
1,2-Dichloropropane ug/L ND 0.50 11/03/13 08:06
1,3,5-Trimethylbenzene ug/L ND 0.50 11/03/13 08:06
1,3-Dichlorobenzene ug/L ND 0.50 11/03/13 08:06
1,3-Dichloropropane ug/L ND 0.50 11/03/13 08:06
1,4-Dichlorobenzene ug/L ND 0.50 11/03/13 08:06
2,2-Dichloropropane ug/L ND 0.50 11/03/13 08:06
2-Chlorotoluene ug/L ND 0.50 11/03/13 08:06
4-Chlorotoluene ug/L ND 0.50 11/03/13 08:06
Benzene ug/L ND 0.50 11/03/13 08:06
Bromobenzene ug/L ND 0.50 11/03/13 08:06
Bromochloromethane ug/L ND 0.50 11/03/13 08:06
Bromodichloromethane ug/L ND 0.50 11/03/13 08:06
Bromoform ug/L ND 0.50 11/03/13 08:06
Bromomethane ug/L ND 5.0 11/03/13 08:06
Carbon tetrachloride ug/L ND 0.50 11/03/13 08:06
Chlorobenzene ug/L ND 0.50 11/03/13 08:06
Chloroethane ug/L ND 1.0 11/03/13 08:06
Chloroform ug/L ND 0.50 11/03/13 08:06
Chloromethane ug/L ND 1.0 11/03/13 08:06
cis-1,2-Dichloroethene ug/L ND 0.50 11/03/13 08:06
cis-1,3-Dichloropropene ug/L ND 0.50 11/03/13 08:06
Dibromochloromethane ug/L ND 0.50 11/03/13 08:06
Dibromomethane ug/L ND 0.50 11/03/13 08:06
Dichlorodifluoromethane ug/L ND 0.50 11/03/13 08:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 51 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1076701
Associated Lab Samples: 92177732001, 92177732002, 92177732003, 92177732004, 92177732005, 92177732006, 92177732007,
92177732008, 92177732009, 92177732010, 92177732011, 92177732012, 92177732013, 92177732014,
92177732015, 92177732016, 92177732017, 92177732018, 92177732019, 92177732020
Matrix: Water
Analyzed
Diisopropyl ether ug/L ND 0.50 11/03/13 08:06
Ethylbenzene ug/L ND 0.50 11/03/13 08:06
Hexachloro-1,3-butadiene ug/L ND 2.0 11/03/13 08:06
Isopropylbenzene (Cumene) ug/L ND 0.50 11/03/13 08:06
m&p-Xylene ug/L ND 1.0 11/03/13 08:06
Methyl-tert-butyl ether ug/L ND 0.50 11/03/13 08:06
Methylene Chloride ug/L ND 2.0 11/03/13 08:06
n-Butylbenzene ug/L ND 0.50 11/03/13 08:06
n-Propylbenzene ug/L ND 0.50 11/03/13 08:06
Naphthalene ug/L ND 2.0 11/03/13 08:06
o-Xylene ug/L ND 0.50 11/03/13 08:06
sec-Butylbenzene ug/L ND 0.50 11/03/13 08:06
Styrene ug/L ND 0.50 11/03/13 08:06
tert-Butylbenzene ug/L ND 0.50 11/03/13 08:06
Tetrachloroethene ug/L ND 0.50 11/03/13 08:06
Toluene ug/L ND 0.50 11/03/13 08:06
trans-1,2-Dichloroethene ug/L ND 0.50 11/03/13 08:06
trans-1,3-Dichloropropene ug/L ND 0.50 11/03/13 08:06
Trichloroethene ug/L ND 0.50 11/03/13 08:06
Trichlorofluoromethane ug/L ND 1.0 11/03/13 08:06
Vinyl chloride ug/L ND 1.0 11/03/13 08:06
1,2-Dichloroethane-d4 (S) % 101 70-130 11/03/13 08:06
4-Bromofluorobenzene (S) % 95 70-130 11/03/13 08:06
Toluene-d8 (S) % 98 70-130 11/03/13 08:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1076702LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.250 104 60-140
1,1,1-Trichloroethane ug/L 49.150 98 60-140
1,1,2,2-Tetrachloroethane ug/L 48.550 97 60-140
1,1,2-Trichloroethane ug/L 49.350 99 60-140
1,1-Dichloroethane ug/L 45.650 91 60-140
1,1-Dichloroethene ug/L 46.650 93 60-140
1,1-Dichloropropene ug/L 48.750 97 60-140
1,2,3-Trichlorobenzene ug/L 53.250 106 60-140
1,2,3-Trichloropropane ug/L 51.750 103 60-140
1,2,4-Trichlorobenzene ug/L 54.050 108 60-140
1,2,4-Trimethylbenzene ug/L 51.850 104 60-140
1,2-Dibromo-3-chloropropane ug/L 48.650 97 60-140
1,2-Dibromoethane (EDB) ug/L 51.750 103 60-140
1,2-Dichlorobenzene ug/L 51.450 103 60-140
1,2-Dichloroethane ug/L 44.050 88 60-140
1,2-Dichloropropane ug/L 51.050 102 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 52 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1076702LABORATORY CONTROL SAMPLE:
LCSSpike
1,3,5-Trimethylbenzene ug/L 49.550 99 60-140
1,3-Dichlorobenzene ug/L 50.350 101 60-140
1,3-Dichloropropane ug/L 51.350 103 60-140
1,4-Dichlorobenzene ug/L 49.050 98 60-140
2,2-Dichloropropane ug/L 44.350 89 60-140
2-Chlorotoluene ug/L 50.750 101 60-140
4-Chlorotoluene ug/L 51.550 103 60-140
Benzene ug/L 48.350 97 60-140
Bromobenzene ug/L 47.750 95 60-140
Bromochloromethane ug/L 45.950 92 60-140
Bromodichloromethane ug/L 51.650 103 60-140
Bromoform ug/L 46.750 93 60-140
Bromomethane ug/L 36.350 73 60-140
Carbon tetrachloride ug/L 49.650 99 60-140
Chlorobenzene ug/L 48.650 97 60-140
Chloroethane ug/L 47.550 95 60-140
Chloroform ug/L 46.350 93 60-140
Chloromethane ug/L 39.350 79 60-140
cis-1,2-Dichloroethene ug/L 46.850 94 60-140
cis-1,3-Dichloropropene ug/L 55.750 111 60-140
Dibromochloromethane ug/L 52.550 105 60-140
Dibromomethane ug/L 49.250 98 60-140
Dichlorodifluoromethane ug/L 49.650 99 60-140
Diisopropyl ether ug/L 49.750 99 60-140
Ethylbenzene ug/L 47.750 95 60-140
Hexachloro-1,3-butadiene ug/L 47.350 95 60-140
Isopropylbenzene (Cumene) ug/L 55.450 111 60-140
m&p-Xylene ug/L 102100 102 60-140
Methyl-tert-butyl ether ug/L 50.850 102 60-140
Methylene Chloride ug/L 50.050 100 60-140
n-Butylbenzene ug/L 50.050 100 60-140
n-Propylbenzene ug/L 49.850 100 60-140
Naphthalene ug/L 54.050 108 60-140
o-Xylene ug/L 54.850 110 60-140
sec-Butylbenzene ug/L 53.950 108 60-140
Styrene ug/L 55.350 111 60-140
tert-Butylbenzene ug/L 54.450 109 60-140
Tetrachloroethene ug/L 50.750 101 60-140
Toluene ug/L 47.550 95 60-140
trans-1,2-Dichloroethene ug/L 45.350 91 60-140
trans-1,3-Dichloropropene ug/L 59.550 119 60-140
Trichloroethene ug/L 48.750 97 60-140
Trichlorofluoromethane ug/L 41.350 83 60-140
Vinyl chloride ug/L 43.950 88 60-140
1,2-Dichloroethane-d4 (S) % 91 70-130
4-Bromofluorobenzene (S) % 102 70-130
Toluene-d8 (S) % 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 53 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1079342MATRIX SPIKE SAMPLE:
MSSpike
Result
92177732008
1,1,1,2-Tetrachloroethane ug/L 20.520 102 60-140ND
1,1,1-Trichloroethane ug/L 22.720 113 60-140ND
1,1,2,2-Tetrachloroethane ug/L 19.520 97 60-140ND
1,1,2-Trichloroethane ug/L 19.420 97 60-140ND
1,1-Dichloroethane ug/L 21.020 105 60-140ND
1,1-Dichloroethene ug/L 20.720 104 60-140ND
1,1-Dichloropropene ug/L 22.320 112 60-140ND
1,2,3-Trichlorobenzene ug/L 20.120 100 60-140ND
1,2,3-Trichloropropane ug/L 20.720 104 60-140ND
1,2,4-Trichlorobenzene ug/L 20.020 100 60-140ND
1,2,4-Trimethylbenzene ug/L 20.620 103 60-140ND
1,2-Dibromo-3-chloropropane ug/L 19.520 98 60-140ND
1,2-Dibromoethane (EDB) ug/L 20.920 104 60-140ND
1,2-Dichlorobenzene ug/L 21.520 107 60-140ND
1,2-Dichloroethane ug/L 21.320 103 60-1400.66
1,2-Dichloropropane ug/L 20.720 104 60-140ND
1,3,5-Trimethylbenzene ug/L 21.020 105 60-140ND
1,3-Dichlorobenzene ug/L 21.120 105 60-140ND
1,3-Dichloropropane ug/L 20.920 105 60-140ND
1,4-Dichlorobenzene ug/L 20.520 103 60-140ND
2,2-Dichloropropane ug/L 20.220 101 60-140ND
2-Chlorotoluene ug/L 21.120 106 60-140ND
4-Chlorotoluene ug/L 21.820 109 60-140ND
Benzene ug/L 19.020 95 60-140ND
Bromobenzene ug/L 19.920 100 60-140ND
Bromochloromethane ug/L 20.720 104 60-140ND
Bromodichloromethane ug/L 20.620 103 60-140ND
Bromoform ug/L 16.420 82 60-140ND
Bromomethane ug/L 14.120 71 60-140ND
Carbon tetrachloride ug/L 22.020 110 60-140ND
Chlorobenzene ug/L 19.820 99 60-140ND
Chloroethane ug/L 20.920 104 60-140ND
Chloroform ug/L 20.720 103 60-140ND
Chloromethane ug/L 18.120 90 60-140ND
cis-1,2-Dichloroethene ug/L 21.120 106 60-140ND
cis-1,3-Dichloropropene ug/L 20.620 103 60-140ND
Dibromochloromethane ug/L 17.320 86 60-140ND
Dibromomethane ug/L 19.720 99 60-140ND
Dichlorodifluoromethane ug/L 22.920 115 60-140ND
Diisopropyl ether ug/L 20.820 104 60-140ND
Ethylbenzene ug/L 20.220 101 60-140ND
Hexachloro-1,3-butadiene ug/L 20.220 101 60-140ND
Isopropylbenzene (Cumene) ug/L 22.920 115 60-140ND
m&p-Xylene ug/L 41.640 104 60-140ND
Methyl-tert-butyl ether ug/L 41.720 124 60-14016.9
Methylene Chloride ug/L 18.720 94 60-140ND
n-Butylbenzene ug/L 20.720 104 60-140ND
n-Propylbenzene ug/L 21.520 107 60-140ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 54 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1079342MATRIX SPIKE SAMPLE:
MSSpike
Result
92177732008
Naphthalene ug/L 20.320 102 60-140ND
o-Xylene ug/L 21.120 106 60-140ND
sec-Butylbenzene ug/L 22.620 113 60-140ND
Styrene ug/L 20.920 104 60-140ND
tert-Butylbenzene ug/L 22.020 110 60-140ND
Tetrachloroethene ug/L 21.220 106 60-140ND
Toluene ug/L 18.320 91 60-140ND
trans-1,2-Dichloroethene ug/L 19.920 99 60-140ND
trans-1,3-Dichloropropene ug/L 21.820 109 60-140ND
Trichloroethene ug/L 20.320 102 60-140ND
Trichlorofluoromethane ug/L 21.320 107 60-140ND
Vinyl chloride ug/L 18.720 94 60-140ND
1,2-Dichloroethane-d4 (S) %98 70-130
4-Bromofluorobenzene (S) %99 70-130
Toluene-d8 (S) %98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 55 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/24761
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92177732022, 92177732023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1076929
Associated Lab Samples:92177732022, 92177732023
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/03/13 01:26
1,1,1-Trichloroethane ug/L ND 0.50 11/03/13 01:26
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/03/13 01:26
1,1,2-Trichloroethane ug/L ND 0.50 11/03/13 01:26
1,1-Dichloroethane ug/L ND 0.50 11/03/13 01:26
1,1-Dichloroethene ug/L ND 0.50 11/03/13 01:26
1,1-Dichloropropene ug/L ND 0.50 11/03/13 01:26
1,2,3-Trichlorobenzene ug/L ND 2.0 11/03/13 01:26
1,2,3-Trichloropropane ug/L ND 0.50 11/03/13 01:26
1,2,4-Trichlorobenzene ug/L ND 2.0 11/03/13 01:26
1,2,4-Trimethylbenzene ug/L ND 0.50 11/03/13 01:26
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/03/13 01:26
1,2-Dibromoethane (EDB) ug/L ND 0.50 11/03/13 01:26
1,2-Dichlorobenzene ug/L ND 0.50 11/03/13 01:26
1,2-Dichloroethane ug/L ND 0.50 11/03/13 01:26
1,2-Dichloropropane ug/L ND 0.50 11/03/13 01:26
1,3,5-Trimethylbenzene ug/L ND 0.50 11/03/13 01:26
1,3-Dichlorobenzene ug/L ND 0.50 11/03/13 01:26
1,3-Dichloropropane ug/L ND 0.50 11/03/13 01:26
1,4-Dichlorobenzene ug/L ND 0.50 11/03/13 01:26
2,2-Dichloropropane ug/L ND 0.50 11/03/13 01:26
2-Chlorotoluene ug/L ND 0.50 11/03/13 01:26
4-Chlorotoluene ug/L ND 0.50 11/03/13 01:26
Benzene ug/L ND 0.50 11/03/13 01:26
Bromobenzene ug/L ND 0.50 11/03/13 01:26
Bromochloromethane ug/L ND 0.50 11/03/13 01:26
Bromodichloromethane ug/L ND 0.50 11/03/13 01:26
Bromoform ug/L ND 0.50 11/03/13 01:26
Bromomethane ug/L ND 5.0 11/03/13 01:26
Carbon tetrachloride ug/L ND 0.50 11/03/13 01:26
Chlorobenzene ug/L ND 0.50 11/03/13 01:26
Chloroethane ug/L ND 1.0 11/03/13 01:26
Chloroform ug/L ND 0.50 11/03/13 01:26
Chloromethane ug/L ND 1.0 11/03/13 01:26
cis-1,2-Dichloroethene ug/L ND 0.50 11/03/13 01:26
cis-1,3-Dichloropropene ug/L ND 0.50 11/03/13 01:26
Dibromochloromethane ug/L ND 0.50 11/03/13 01:26
Dibromomethane ug/L ND 0.50 11/03/13 01:26
Dichlorodifluoromethane ug/L ND 0.50 11/03/13 01:26
Diisopropyl ether ug/L ND 0.50 11/03/13 01:26
Ethylbenzene ug/L ND 0.50 11/03/13 01:26
Hexachloro-1,3-butadiene ug/L ND 2.0 11/03/13 01:26
Isopropylbenzene (Cumene) ug/L ND 0.50 11/03/13 01:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 56 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1076929
Associated Lab Samples:92177732022, 92177732023
Matrix: Water
Analyzed
m&p-Xylene ug/L ND 1.0 11/03/13 01:26
Methyl-tert-butyl ether ug/L ND 0.50 11/03/13 01:26
Methylene Chloride ug/L ND 2.0 11/03/13 01:26
n-Butylbenzene ug/L ND 0.50 11/03/13 01:26
n-Propylbenzene ug/L ND 0.50 11/03/13 01:26
Naphthalene ug/L ND 2.0 11/03/13 01:26
o-Xylene ug/L ND 0.50 11/03/13 01:26
sec-Butylbenzene ug/L ND 0.50 11/03/13 01:26
Styrene ug/L ND 0.50 11/03/13 01:26
tert-Butylbenzene ug/L ND 0.50 11/03/13 01:26
Tetrachloroethene ug/L ND 0.50 11/03/13 01:26
Toluene ug/L ND 0.50 11/03/13 01:26
trans-1,2-Dichloroethene ug/L ND 0.50 11/03/13 01:26
trans-1,3-Dichloropropene ug/L ND 0.50 11/03/13 01:26
Trichloroethene ug/L ND 0.50 11/03/13 01:26
Trichlorofluoromethane ug/L ND 1.0 11/03/13 01:26
Vinyl chloride ug/L ND 1.0 11/03/13 01:26
1,2-Dichloroethane-d4 (S) % 99 70-130 11/03/13 01:26
4-Bromofluorobenzene (S) % 93 70-130 11/03/13 01:26
Toluene-d8 (S) % 101 70-130 11/03/13 01:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1076930LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.150 102 60-140
1,1,1-Trichloroethane ug/L 49.750 99 60-140
1,1,2,2-Tetrachloroethane ug/L 48.850 98 60-140
1,1,2-Trichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethane ug/L 48.050 96 60-140
1,1-Dichloroethene ug/L 48.750 97 60-140
1,1-Dichloropropene ug/L 52.250 104 60-140
1,2,3-Trichlorobenzene ug/L 54.750 109 60-140
1,2,3-Trichloropropane ug/L 49.450 99 60-140
1,2,4-Trichlorobenzene ug/L 55.650 111 60-140
1,2,4-Trimethylbenzene ug/L 52.850 106 60-140
1,2-Dibromo-3-chloropropane ug/L 49.350 99 60-140
1,2-Dibromoethane (EDB) ug/L 50.550 101 60-140
1,2-Dichlorobenzene ug/L 52.250 104 60-140
1,2-Dichloroethane ug/L 43.850 88 60-140
1,2-Dichloropropane ug/L 52.850 106 60-140
1,3,5-Trimethylbenzene ug/L 51.350 103 60-140
1,3-Dichlorobenzene ug/L 52.150 104 60-140
1,3-Dichloropropane ug/L 51.750 103 60-140
1,4-Dichlorobenzene ug/L 49.750 99 60-140
2,2-Dichloropropane ug/L 51.950 104 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 57 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1076930LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorotoluene ug/L 51.850 104 60-140
4-Chlorotoluene ug/L 52.850 106 60-140
Benzene ug/L 49.650 99 60-140
Bromobenzene ug/L 50.350 101 60-140
Bromochloromethane ug/L 48.150 96 60-140
Bromodichloromethane ug/L 50.350 101 60-140
Bromoform ug/L 46.750 93 60-140
Bromomethane ug/L 51.450 103 60-140
Carbon tetrachloride ug/L 47.450 95 60-140
Chlorobenzene ug/L 48.450 97 60-140
Chloroethane ug/L 48.850 98 60-140
Chloroform ug/L 47.750 95 60-140
Chloromethane ug/L 47.050 94 60-140
cis-1,2-Dichloroethene ug/L 49.150 98 60-140
cis-1,3-Dichloropropene ug/L 57.150 114 60-140
Dibromochloromethane ug/L 52.750 105 60-140
Dibromomethane ug/L 47.950 96 60-140
Dichlorodifluoromethane ug/L 51.150 102 60-140
Diisopropyl ether ug/L 53.450 107 60-140
Ethylbenzene ug/L 48.650 97 60-140
Hexachloro-1,3-butadiene ug/L 49.350 99 60-140
Isopropylbenzene (Cumene) ug/L 55.350 111 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 51.450 103 60-140
Methylene Chloride ug/L 53.350 107 60-140
n-Butylbenzene ug/L 52.950 106 60-140
n-Propylbenzene ug/L 52.450 105 60-140
Naphthalene ug/L 55.650 111 60-140
o-Xylene ug/L 55.650 111 60-140
sec-Butylbenzene ug/L 55.950 112 60-140
Styrene ug/L 55.250 110 60-140
tert-Butylbenzene ug/L 55.750 111 60-140
Tetrachloroethene ug/L 50.350 101 60-140
Toluene ug/L 47.850 96 60-140
trans-1,2-Dichloroethene ug/L 45.450 91 60-140
trans-1,3-Dichloropropene ug/L 60.550 121 60-140
Trichloroethene ug/L 49.350 99 60-140
Trichlorofluoromethane ug/L 41.550 83 60-140
Vinyl chloride ug/L 49.150 98 60-140
1,2-Dichloroethane-d4 (S) % 92 70-130
4-Bromofluorobenzene (S) % 101 70-130
Toluene-d8 (S) % 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 58 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/24820
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92177732021
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1080488
Associated Lab Samples:92177732021
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/06/13 18:22
1,1,1-Trichloroethane ug/L ND 0.50 11/06/13 18:22
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/06/13 18:22
1,1,2-Trichloroethane ug/L ND 0.50 11/06/13 18:22
1,1-Dichloroethane ug/L ND 0.50 11/06/13 18:22
1,1-Dichloroethene ug/L ND 0.50 11/06/13 18:22
1,1-Dichloropropene ug/L ND 0.50 11/06/13 18:22
1,2,3-Trichlorobenzene ug/L ND 2.0 11/06/13 18:22
1,2,3-Trichloropropane ug/L ND 0.50 11/06/13 18:22
1,2,4-Trichlorobenzene ug/L ND 2.0 11/06/13 18:22
1,2,4-Trimethylbenzene ug/L ND 0.50 11/06/13 18:22
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/06/13 18:22
1,2-Dibromoethane (EDB) ug/L ND 0.50 11/06/13 18:22
1,2-Dichlorobenzene ug/L ND 0.50 11/06/13 18:22
1,2-Dichloroethane ug/L ND 0.50 11/06/13 18:22
1,2-Dichloropropane ug/L ND 0.50 11/06/13 18:22
1,3,5-Trimethylbenzene ug/L ND 0.50 11/06/13 18:22
1,3-Dichlorobenzene ug/L ND 0.50 11/06/13 18:22
1,3-Dichloropropane ug/L ND 0.50 11/06/13 18:22
1,4-Dichlorobenzene ug/L ND 0.50 11/06/13 18:22
2,2-Dichloropropane ug/L ND 0.50 11/06/13 18:22
2-Chlorotoluene ug/L ND 0.50 11/06/13 18:22
4-Chlorotoluene ug/L ND 0.50 11/06/13 18:22
Benzene ug/L ND 0.50 11/06/13 18:22
Bromobenzene ug/L ND 0.50 11/06/13 18:22
Bromochloromethane ug/L ND 0.50 11/06/13 18:22
Bromodichloromethane ug/L ND 0.50 11/06/13 18:22
Bromoform ug/L ND 0.50 11/06/13 18:22
Bromomethane ug/L ND 5.0 11/06/13 18:22
Carbon tetrachloride ug/L ND 0.50 11/06/13 18:22
Chlorobenzene ug/L ND 0.50 11/06/13 18:22
Chloroethane ug/L ND 1.0 11/06/13 18:22
Chloroform ug/L ND 0.50 11/06/13 18:22
Chloromethane ug/L ND 1.0 11/06/13 18:22
cis-1,2-Dichloroethene ug/L ND 0.50 11/06/13 18:22
cis-1,3-Dichloropropene ug/L ND 0.50 11/06/13 18:22
Dibromochloromethane ug/L ND 0.50 11/06/13 18:22
Dibromomethane ug/L ND 0.50 11/06/13 18:22
Dichlorodifluoromethane ug/L ND 0.50 11/06/13 18:22
Diisopropyl ether ug/L ND 0.50 11/06/13 18:22
Ethylbenzene ug/L ND 0.50 11/06/13 18:22
Hexachloro-1,3-butadiene ug/L ND 2.0 11/06/13 18:22
Isopropylbenzene (Cumene) ug/L ND 0.50 11/06/13 18:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 59 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1080488
Associated Lab Samples:92177732021
Matrix: Water
Analyzed
m&p-Xylene ug/L ND 1.0 11/06/13 18:22
Methyl-tert-butyl ether ug/L ND 0.50 11/06/13 18:22
Methylene Chloride ug/L ND 2.0 11/06/13 18:22
n-Butylbenzene ug/L ND 0.50 11/06/13 18:22
n-Propylbenzene ug/L ND 0.50 11/06/13 18:22
Naphthalene ug/L ND 2.0 11/06/13 18:22
o-Xylene ug/L ND 0.50 11/06/13 18:22
sec-Butylbenzene ug/L ND 0.50 11/06/13 18:22
Styrene ug/L ND 0.50 11/06/13 18:22
tert-Butylbenzene ug/L ND 0.50 11/06/13 18:22
Tetrachloroethene ug/L ND 0.50 11/06/13 18:22
Toluene ug/L ND 0.50 11/06/13 18:22
trans-1,2-Dichloroethene ug/L ND 0.50 11/06/13 18:22
trans-1,3-Dichloropropene ug/L ND 0.50 11/06/13 18:22
Trichloroethene ug/L ND 0.50 11/06/13 18:22
Trichlorofluoromethane ug/L ND 1.0 11/06/13 18:22
Vinyl chloride ug/L ND 1.0 11/06/13 18:22
1,2-Dichloroethane-d4 (S) % 95 70-130 11/06/13 18:22
4-Bromofluorobenzene (S) % 97 70-130 11/06/13 18:22
Toluene-d8 (S) % 100 70-130 11/06/13 18:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1080489LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.250 112 60-140
1,1,1-Trichloroethane ug/L 54.550 109 60-140
1,1,2,2-Tetrachloroethane ug/L 52.850 106 60-140
1,1,2-Trichloroethane ug/L 54.150 108 60-140
1,1-Dichloroethane ug/L 53.150 106 60-140
1,1-Dichloroethene ug/L 51.850 104 60-140
1,1-Dichloropropene ug/L 56.050 112 60-140
1,2,3-Trichlorobenzene ug/L 56.550 113 60-140
1,2,3-Trichloropropane ug/L 54.750 109 60-140
1,2,4-Trichlorobenzene ug/L 56.750 113 60-140
1,2,4-Trimethylbenzene ug/L 54.450 109 60-140
1,2-Dibromo-3-chloropropane ug/L 56.050 112 60-140
1,2-Dibromoethane (EDB) ug/L 57.350 115 60-140
1,2-Dichlorobenzene ug/L 55.950 112 60-140
1,2-Dichloroethane ug/L 47.750 95 60-140
1,2-Dichloropropane ug/L 57.450 115 60-140
1,3,5-Trimethylbenzene ug/L 55.050 110 60-140
1,3-Dichlorobenzene ug/L 54.750 109 60-140
1,3-Dichloropropane ug/L 57.450 115 60-140
1,4-Dichlorobenzene ug/L 54.950 110 60-140
2,2-Dichloropropane ug/L 53.350 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 60 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1080489LABORATORY CONTROL SAMPLE:
LCSSpike
2-Chlorotoluene ug/L 54.750 109 60-140
4-Chlorotoluene ug/L 57.050 114 60-140
Benzene ug/L 50.950 102 60-140
Bromobenzene ug/L 53.250 106 60-140
Bromochloromethane ug/L 54.650 109 60-140
Bromodichloromethane ug/L 55.950 112 60-140
Bromoform ug/L 46.850 94 60-140
Bromomethane ug/L 53.650 107 60-140
Carbon tetrachloride ug/L 53.950 108 60-140
Chlorobenzene ug/L 53.250 106 60-140
Chloroethane ug/L 53.050 106 60-140
Chloroform ug/L 51.650 103 60-140
Chloromethane ug/L 50.350 101 60-140
cis-1,2-Dichloroethene ug/L 53.450 107 60-140
cis-1,3-Dichloropropene ug/L 63.250 126 60-140
Dibromochloromethane ug/L 49.150 98 60-140
Dibromomethane ug/L 52.750 105 60-140
Dichlorodifluoromethane ug/L 50.550 101 60-140
Diisopropyl ether ug/L 57.050 114 60-140
Ethylbenzene ug/L 52.450 105 60-140
Hexachloro-1,3-butadiene ug/L 53.050 106 60-140
Isopropylbenzene (Cumene) ug/L 60.550 121 60-140
m&p-Xylene ug/L 108100 108 60-140
Methyl-tert-butyl ether ug/L 54.150 108 60-140
Methylene Chloride ug/L 53.150 106 60-140
n-Butylbenzene ug/L 54.650 109 60-140
n-Propylbenzene ug/L 56.450 113 60-140
Naphthalene ug/L 58.450 117 60-140
o-Xylene ug/L 57.350 115 60-140
sec-Butylbenzene ug/L 58.950 118 60-140
Styrene ug/L 60.350 121 60-140
tert-Butylbenzene ug/L 58.050 116 60-140
Tetrachloroethene ug/L 54.450 109 60-140
Toluene ug/L 48.850 98 60-140
trans-1,2-Dichloroethene ug/L 49.350 99 60-140
trans-1,3-Dichloropropene ug/L 64.550 129 60-140
Trichloroethene ug/L 53.150 106 60-140
Trichlorofluoromethane ug/L 46.450 93 60-140
Vinyl chloride ug/L 51.550 103 60-140
1,2-Dichloroethane-d4 (S) % 91 70-130
4-Bromofluorobenzene (S) % 102 70-130
Toluene-d8 (S) % 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 61 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1080490MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92178077002
1080491
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 115 60-140112 3 3020ND 23.0 22.4
1,1,1-Trichloroethane ug/L 20 123 60-140121 1 3020ND 24.5 24.3
1,1,2,2-Tetrachloroethane ug/L 20 108 60-140105 3 3020ND 21.6 21.0
1,1,2-Trichloroethane ug/L 20 112 60-140110 2 3020ND 22.4 21.9
1,1-Dichloroethane ug/L 20 109 60-140110 1 3020ND 21.9 22.0
1,1-Dichloroethene ug/L 20 116 60-140115 1 3020ND 23.3 23.0
1,1-Dichloropropene ug/L 20 122 60-140119 3 3020ND 24.4 23.7
1,2,3-Trichlorobenzene ug/L 20 115 60-140111 4 3020ND 22.9 22.1
1,2,3-Trichloropropane ug/L 20 119 60-140116 2 3020ND 23.8 23.3
1,2,4-Trichlorobenzene ug/L 20 111 60-140109 1 3020ND 22.2 21.9
1,2,4-Trimethylbenzene ug/L 20 115 60-140113 2 3020ND 23.0 22.6
1,2-Dibromo-3-chloropropane ug/L 20 116 60-140106 10 3020ND 23.3 21.1
1,2-Dibromoethane (EDB) ug/L 20 113 60-140111 2 3020ND 22.7 22.3
1,2-Dichlorobenzene ug/L 20 118 60-140115 2 3020ND 23.5 23.0
1,2-Dichloroethane ug/L 20 110 60-140106 3 3020ND 21.9 21.3
1,2-Dichloropropane ug/L 20 114 60-140111 2 3020ND 22.8 22.3
1,3,5-Trimethylbenzene ug/L 20 115 60-140113 2 3020ND 23.0 22.7
1,3-Dichlorobenzene ug/L 20 118 60-140112 5 3020ND 23.6 22.5
1,3-Dichloropropane ug/L 20 117 60-140114 3 3020ND 23.3 22.8
1,4-Dichlorobenzene ug/L 20 114 60-140111 3 3020ND 22.8 22.2
2,2-Dichloropropane ug/L 20 108 60-140105 2 3020ND 21.5 21.1
2-Chlorotoluene ug/L 20 116 60-140112 4 3020ND 23.3 22.3
4-Chlorotoluene ug/L 20 120 60-140116 4 3020ND 24.0 23.1
Benzene ug/L 20 104 60-140102 2 3020ND 20.8 20.3
Bromobenzene ug/L 20 112 60-140109 2 3020ND 22.4 21.9
Bromochloromethane ug/L 20 110 60-140110 1 3020ND 22.0 22.1
Bromodichloromethane ug/L 20 113 60-140111 1 3020ND 22.5 22.3
Bromoform ug/L 20 93 60-14093 0 3020ND 18.6 18.6
Bromomethane ug/L 20 90 60-14093 3 3020ND 17.9 18.5
Carbon tetrachloride ug/L 20 121 60-140117 3 3020ND 24.3 23.5
Chlorobenzene ug/L 20 111 60-140108 2 3020ND 22.2 21.7
Chloroethane ug/L 20 118 60-140116 1 3020ND 23.5 23.3
Chloroform ug/L 20 111 60-140108 3 3020ND 22.2 21.6
Chloromethane ug/L 20 93 60-14094 1 3020ND 18.6 18.8
cis-1,2-Dichloroethene ug/L 20 112 60-140109 2 3020ND 22.4 21.9
cis-1,3-Dichloropropene ug/L 20 114 60-140111 3 3020ND 22.9 22.3
Dibromochloromethane ug/L 20 100 60-14097 2 3020ND 19.9 19.4
Dibromomethane ug/L 20 105 60-140101 3 3020ND 20.9 20.2
Dichlorodifluoromethane ug/L 20 125 60-140120 3 3020ND 24.9 24.1
Diisopropyl ether ug/L 20 112 60-140112 0 3020ND 22.4 22.4
Ethylbenzene ug/L 20 111 60-140107 4 3020ND 22.2 21.4
Hexachloro-1,3-butadiene ug/L 20 114 60-140105 9 3020ND 22.8 20.9
Isopropylbenzene (Cumene) ug/L 20 128 60-140123 4 3020ND 25.5 24.6
m&p-Xylene ug/L 40 113 60-140111 1 3040ND 45.2 44.5
Methyl-tert-butyl ether ug/L 20 112 60-140108 4 3020ND 22.5 21.6
Methylene Chloride ug/L 20 98 60-14094 4 3020ND 19.5 18.8
n-Butylbenzene ug/L 20 114 60-140109 5 3020ND 22.9 21.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 62 of 68
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1080490MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92178077002
1080491
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 120 60-140116 4 3020ND 24.1 23.1
Naphthalene ug/L 20 115 60-140111 4 3020ND 23.0 22.2
o-Xylene ug/L 20 117 60-140118 1 3020ND 23.5 23.6
sec-Butylbenzene ug/L 20 126 60-140122 3 3020ND 25.2 24.4
Styrene ug/L 20 114 60-140108 6 3020ND 22.8 21.5
tert-Butylbenzene ug/L 20 123 60-140122 1 3020ND 24.7 24.3
Tetrachloroethene ug/L 20 116 60-140112 3 3020ND 23.1 22.4
Toluene ug/L 20 100 60-14099 1 3020ND 20.0 19.8
trans-1,2-Dichloroethene ug/L 20 111 60-140111 0 3020ND 22.2 22.2
trans-1,3-Dichloropropene ug/L 20 117 60-140121 3 3020ND 23.5 24.1
Trichloroethene ug/L 20 111 60-140112 1 3020ND 22.2 22.5
Trichlorofluoromethane ug/L 20 116 60-140111 5 3020ND 23.3 22.3
Vinyl chloride ug/L 20 98 60-140102 3 3020ND 19.7 20.4
1,2-Dichloroethane-d4 (S) %99 70-13099
4-Bromofluorobenzene (S) % 101 70-130101
Toluene-d8 (S) %98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 63 of 68
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 64 of 68
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92177732
BP SERVICE CNTR
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92177732001 MSV/24751MW1SM 6200B
92177732002 MSV/24751MW2SM 6200B
92177732003 MSV/24751MW3SM 6200B
92177732004 MSV/24751MW4SM 6200B
92177732005 MSV/24751MW5SM 6200B
92177732006 MSV/24751MW6SM 6200B
92177732007 MSV/24751MW7SM 6200B
92177732008 MSV/24751MW8ASM 6200B
92177732009 MSV/24751MW9SM 6200B
92177732010 MSV/24751MW10SM 6200B
92177732011 MSV/24751MW11SM 6200B
92177732012 MSV/24751MW12SM 6200B
92177732013 MSV/24751MW13SM 6200B
92177732014 MSV/24751MW14SM 6200B
92177732015 MSV/24751MW15SM 6200B
92177732016 MSV/24751MW16SM 6200B
92177732017 MSV/24751MW17SM 6200B
92177732018 MSV/24751MW18SM 6200B
92177732019 MSV/24751VEW-1 SM 6200B
92177732020 MSV/24751SW-1 SM 6200B
92177732021 MSV/24820IW-8 SM 6200B
92177732022 MSV/24761IW-3 SM 6200B
92177732023 MSV/24761IW-4 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/07/2013 02:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 65 of 68
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