WA-926_11963_CA_RPTS_20180905_MRP

EXECUTIVE SUMMARY

The Todd’s Service Center and Bowen’s Grocery sites are located at the intersection of US Highway 17
and NC Highway 45 in Merry Hill, Bertie County, North Carolina. According to available information,
two 2,000-gallon gasoline, one 1,000-gallon gasoline, one 1,000-gallon diesel and one 550-gallon waste
oil USTs were reportedly removed from the Todd’s site in December 1993. A release at the site was
discovered when petroleum impacted soil was encountered during the UST closure event. In addition,
two 550-gallon gasoline USTs were removed from the Bowen’s site in December 1994. Another UST
incident (UST Incident Number 31939; Miller’s Country Store) is located adjacent to the Todd’s and
Bowen’s sites and is considered to be commingled with the Todd’s and Bowen’s contaminant plume(s).

The risk classification of the sites is High due to the presence of two out of service water supply wells that
were identified within a 250-foot radius of the site. Municipal water is available to the site and
surrounding properties.

Eleven Type II monitoring wells (MW-1A, MW-2, MW-4, MW-5, MW-15, MW-22, MW-25B, MW-29,
MW-36, MW-43, and MW-44) and one Type III monitoring well (TW-1M) were gauged, purged and
sampled on July 24, 2018. Concentrations of requested method constituents that exceeded the Maximum
Allowable Concentrations specified in T15A NCAC 2L.0202 were reported in the ground water samples
collected from MW-1A, MW-2, MW-4, MW-5, MW-15, MW-22, and MW-29. None of the requested
method constituents exceeded the Gross Contamination Levels.

Upon conclusion of the July 2018 sampling event, Oxygen Releasing Compound (ORC-A) socks were
installed in MW-1A, MW-2, MW4, MW-15, MW-22 and MW-29.

Based on this information, the site should remain high risk. The effectiveness of the ORC-A socks will
be evaluated during the next semi-annual ground water monitoring event. The next semi-annual sampling
event is tentatively scheduled for January 2019.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION ....................................................................... 1
2.0 CURRENT SITE ASSESSMENT ................................................................................................ 2
3.0 GROUND WATER QUALITY .................................................................................................... 2
4.0 CONCLUSIONS AND RECOMMENDATIONS ....................................................................... 3
5.0 LIMITATIONS .............................................................................................................................. 3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results
Table 2A: Summary of Field Parameters Results

APPENDICES
Appendix A: Miller’s Country Store Ground Water Gauging and Sample Information
Appendix B: Laboratory Report - Ground Water Samples
Appendix C: Notice of Intent to Construct or Operate Injection Wells
Appendix D: Injection Event Record

1

1.0 SITE HISTORY AND CHARACTERIZATION
The former Todd’s Service Center and Bowen’s Grocery sites are located at the intersection of US
Highway 17 and NC Highway 45 in Merry Hill, Bertie County, North Carolina (Figure 1). The subject
sites are former petroleum retail facilities. A produce stand now operates at the site. According to
available information, two 2,000-gallon gasoline, one 1,000-gallon gasoline, one 1,000-gallon diesel and
one 550-gallon waste oil underground storage tanks (USTs) were reportedly removed from the Todd’s
site in December 1993. A release at the Todd’s site was discovered when petroleum impacted soil was
encountered during the UST closure event. According to available information, two 550-gallon gasoline
USTs were removed from the Bowen’s site in December 1994. Concentrations of requested method
constituents that exceeded the applicable soil quality standards were reported in two soil samples
collected from the UST pit bottom. Additionally, an incident at the adjacent Miller’s Country Store site
(UST Incident Number 31939) is considered to be commingled with the Todd’s and Bowen’s
contaminant plume(s). Monitoring and remediation efforts for the three sites are conducted concurrently
at the request of the North Carolina Department of Environmental Quality (NCDEQ).

A total of fifty-one Type II (MW-1 through MW-5, MW-7 through MW-48, RW-1, OW-1, AS-1 and VE-
1) and one Type III (MWD-6) monitoring wells have been installed during past assessment activities for
the Todd’s and Bowen’s sites. In addition, three Type II (MW-1M, MW-2M and MW-3M) and one Type
III (TW-1M) monitoring wells have been installed on the adjacent Miller’s Country Store site. Due to
changing site conditions and activities, several monitoring wells have been destroyed and/or replaced.
Destroyed monitoring wells include MW-1, MW-8, MW-9, MW-10, MW-16, MW-18, MW-18A, MW-
23, MW-25, MW-25A, MW-30 and MW-35. Replacement wells MW-1A, MW-9A, MW-10A, MW-
15A, MW-23A, MW-25B and MW-30A were installed during past assessment activities and remain
onsite.

The site risk classification is currently ranked High due to the presence of two water supply wells within a
250-foot radius of the site; however, these wells are not in use. Municipal water is available to the site
and surrounding properties. A Site Vicinity Map showing properties and water supply wells within a
1,500-foot radius of the source area is included as Figure 2. A Site Map showing the locations of
monitoring wells and site structures is included as Figure 3.

Please note that site activities prior to January 2007 were performed by previous consultants. Although
Geological Resources Inc. (GRI) cannot verify the accuracy of this information, for the purpose of this
report, it is assumed to be correct. Any inferences or interpretations made by GRI based on data that may

2

be incorrect are not the responsibility of GRI. Please refer to earlier submittals for additional information
regarding past assessment activities.

2.0 CURRENT SITE ASSESSMENT
The purpose of this report is to present the results of ground water sampling activities conducted on July
24, 2018, at the site. The activities were conducted in accordance with GRI proposal number 17-720
which was submitted to NCDEQ on January 29, 2018, and approved as Task Authorization No. 11963-23
on February 5, 2018. The purpose of the scope of work was to obtain current ground water quality data
for the site, as well as install Oxygen Releasing Compound (ORC-A) treated socks at the site.

3.0 GROUND WATER QUALITY
Eleven Type II monitoring wells (MW-1A, MW-2, MW-4, MW-5, MW-15, MW-22, MW-25, MW-29,
MW-36, MW-43 and MW-44) were gauged, purged and sampled on July 24, 2018. Please also note,
monitoring wells associated with the Miller’s Country Store site (MW-1M, MW-2M, MW-3M and TW-
1M) were gauged, purged and sampled in conjunction with the Todd’s and Bowen’s July 2018 sampling
event. Due to heavy rainstorms, MW-11 and MW-23A were under water and inaccessible. Ground
water gauging and sampling information for the Miller’s Grocery site are included as Appendix A.

The depths to ground water in the Type II monitoring wells during the July 2018 sampling event ranged
from 6.39 to 19.91 feet below the tops of well casings. Ground water elevations in the Type II
monitoring wells relative to a temporary benchmark assumed by the previous consultant ranged from
75.85 to 81.74 feet. Based on this information, ground water flow across the site was generally toward
the southeast. The average horizontal hydraulic gradient was less than 0.01 feet per foot. A Water Table
Surface Map for the July 24, 2018, gauging event has been included as Figure 4. A summary of the well
construction and gauging information has been presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the July 2018 sampling event for volatile organic compounds using EPA Method 6200B.
Concentrations of one or more BTEX constituents, MTBE, naphthalene, o-chlorotoluene,
isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded
the Maximum Allowable Concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the
ground water samples collected from MW-1A, MW-2, MW-4, MW-5, MW-15, MW-22, and MW-29.
None of the reported contaminant concentrations exceeded the Gross Contamination Levels (GCLs). A
Ground Water Quality Map based on data from the July 24, 2018, sampling event has been included as

3

Figure 4. A summary of ground water sample analytical results is presented in Table 2. A complete
laboratory report has been included as Appendix B.

Field parameter data (dissolved oxygen, temperature, pH, conductivity and oxygen reduction potential)
were collected during the July 2018 sampling for use in the evaluation of the ORC-A sock application.
Field parameter results are tabulate in Table 2A. Upon conclusion of the July 2018 sampling event, ORC-
A socks were installed in MW-1A, MW-2, MW4, MW-15, MW-22 and MW-29. A copy of the Notice of
Intent to Construct or Operate Injection Wells is included as Appendix C. A copy of the Injection Event
Record is included as Appendix D.

4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the Type II monitoring wells in July 2018 was 18.11 feet
below the tops of well casings. Ground water flow was generally toward the southeast with an
average horizontal hydraulic gradient of less than 0.01 feet per foot.
 Concentrations of one or more BTEX constituents, MTBE, naphthalene, o-chlorotoluene,
isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that
exceeded the MACs were reported in the ground water samples collected from MW-1A, MW-2,
MW-4, MW-5, MW-15, MW-22, and MW-29. None of the reported contaminant concentrations
exceeded the GCLs.
 Upon conclusion of the July 2018 sampling event, ORC-A treated socks were installed in MW-
1A, MW-2, MW4, MW-15, MW-22 and MW-29.
 Based on this information, the site should remain high risk. The effectiveness of the ORC-A
socks will be evaluated during the next semi-annual ground water monitoring event. The next
semi-annual sampling event is tentatively scheduled for January 2019.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Bertie County, North Carolina. The assessment was conducted based
on the scope of work and level of effort desired by NCDEQ and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations

4

sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from this data. Please note that field data collected prior
to the March 2007 sampling and updated receptor survey event was not obtained under the supervision of
GRI. Although the accuracy of these data cannot be verified, for the purpose of this report GRI assumes
that they are correct.

FIGURES
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"J"J
"J
"J
"J
DH
SITE
6853691071
6853575623
6853482256
6853487302
6853386041
6853592031
6853590189
6853487515
6853496244
6853489091
6853497974
6853482637
6853586821
6853484771
6853487891
6853582419
6853582338
6853582258
6853486737
6
85
35
81
54
86853582178
68 5 3 5 8 1 5 5 4
6853588050
WSW-2
U S 1 7 H W Y
NC 45
HWYU S 1 7 H W Y
WSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-1
WSW-12
WSW-18
WSW-17
WSW-19 WSW-16
WSW-15
WSW-14
WSW-13
WSW-11
WSW-10³
0 300150
Feet
FIGURE 2: SITE VICINITY MAPTODD'S SERVICE CENTER AND BOWEN'S GROCERYUS HIGHWAY 17 & NC ROUTE 45MERRY HILL, BERTIE COUNTYNORTH CAROLINAINCIDENT NOS. 11963 & 13592GRI PROJECT NO. 2458
PREPARED BYGEOLOGICAL RESOURCES, INC.OCTOBER 14, 2009REVISED: FEBRUARY 12, 2013
1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
LEGEND
DH Destroyed Well
"J Water Supply Well
River_Line
Parcel_Polygon
Centerline
Pond_Lake_Polygon
6853487302 PIN Number
CREEK

TABLES
Date: 08/14/18
11/01/07
09/16/09
09/20/10
10/27/11
01/07/13
11/01/07 99.34 21.00 ---78.34
07/20/09 22.00 0.01 78.01 Pre-MMPE
07/24/09 21.25 ---78.75 Post-MMPE
09/16/09 21.57 ---78.43
09/20/10 19.92 ---80.08
10/27/11 19.90 ---80.10
12/03/12 21.45 ---78.55 Pre-MMPE
12/07/12 20.50 ---79.50 Post-MMPE
01/07/13 21.47 ---78.53
06/24/13 21.09 ---78.91 Pre-MMPE
06/28/13 21.19 ---78.81 Post-MMPE
07/29/13 NM NM NM Not Found
05/19/14 19.54 ---80.46 Pre-MMPE
05/23/14 19.45 ---80.55 Post-MMPE
06/23/14 19.68 ---80.32
07/06/15 NM NM NM Not Found
01/27/16 20.13 ---79.87
08/01/16 19.58 ---80.42 Pre-AFVR
08/01/16 19.91 ---80.09 Post-AFVR
09/07/16 20.29 ---79.71
07/24/18 19.91 ---80.09
11/01/07 99.51 20.92 ---78.59
07/20/09 21.07 ---78.79 Pre-MMPE
07/24/09 21.34 ---78.52 Post-MMPE
09/16/09 21.48 ---78.38
09/20/10 19.83 ---80.03
10/27/11 19.86 ---80.00
12/03/12 21.37 ---78.49 Pre-MMPE
12/07/12 21.42 ---78.44 Post-MMPE
01/07/13 21.40 ---78.46
06/24/13 20.91 ---78.95 Pre-MMPE
06/28/13 21.06 ---78.80 Post-MMPE
07/29/13 20.43 ---79.43
05/19/14 19.49 ---80.37 Pre-MMPE
05/23/14 19.44 ---80.42 Post-MMPE
06/23/14 19.62 ---80.24
06/01/15 18.39 ---81.47 Pre-MMPE
06/05/15 18.51 ---81.35 Post-MMPE
07/06/15 19.13 ---80.73
01/27/16 20.07 ---79.79
09/07/16 20.13 ---79.73
07/24/18 19.80 ---80.06
11/01/07 99.59 20.86 ---78.73
09/16/09 21.40 ---78.56
09/20/10 19.74 ---80.22
10/27/11 19.70 ---80.26
01/07/13 21.27 ---78.69
07/29/13 20.31 ---79.65
05/19/14 19.40 ---80.56 Pre-MMPE
05/23/14 19.29 ---80.67 Post-MMPE
06/03/14 19.47 ---80.49
06/01/15 18.22 ---81.74 Pre-MMPE
06/05/15 18.34 ---81.62 Post-MMPE
07/06/15 18.98 ---80.98
01/27/16 19.89 ---80.07
11/01/07 99.57 20.60 ---78.99
09/16/09 NM NM NM
09/20/10 19.47 ---80.10
10/27/11 19.40 ---80.17
12/03/12 21.00 ---78.57 Pre-MMPE
12/07/12 21.06 ---78.51 Post-MMPE
01/07/13 21.03 ---78.54
06/24/13 20.55 ---79.02 Pre-MMPE
06/28/13 20.67 ---78.90 Post-MMPE
07/29/13 NM NM NM Not Found
06/23/14 19.19 ---80.38
07/06/15 18.73 ---80.84
01/27/16 19.64 ---79.93
08/01/16 19.11 ---80.46 Pre-AFVR
08/01/16 19.30 ---80.27 Post-AFVR
09/07/16 19.74 ---79.83
07/24/18 19.42 ---80.15
99.572515-251504/27/94MW-4
Bottom
of Well
(ft. BGS)
MW-1 04/27/94 15 15-25
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Date
Installed
(mm/dd/yy)
Comments
Casing
Collapsed
Casing
Collapsed
Casing
Collapsed Casing Collapsed Casing
Collapsed25
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
99.862515-2515
100.0020-3020 30
25 99.96
11/16/01MW-1A
MW-3 04/27/94 15 15-25
04/27/94MW-2
Page 1 of 5
Date: 08/14/18
Bottom
of Well
(ft. BGS)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Date
Installed
(mm/dd/yy)
Comments
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
11/01/07 99.19 20.29 ---78.90
09/16/09 20.85 ---78.72
09/20/10 19.17 ---80.40
10/27/11 19.10 ---80.47
01/07/13 20.70 ---78.87
07/29/13 19.76 ---79.81
05/19/14 18.69 ---80.88 Pre-MMPE
05/23/14 18.58 ---80.99 Post-MMPE
06/23/14 18.83 ---80.74
07/06/15 18.38 ---81.19
01/27/16 19.25 ---80.32
07/24/18 19.07 ---80.50
11/01/07 99.27 21.20 ---78.07
09/16/09 21.06 ---78.60
09/20/10 19.74 ---79.92
10/27/11 19.48 ---80.18
01/07/13 21.04 ---78.62
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
11/01/07 99.00 20.41 ---78.59
09/16/09 20.96 ---78.44
09/20/10 19.31 ---80.09
10/27/11 19.32 ---80.08
01/07/13 20.84 ---78.56
07/29/13 20.40 ---79.00
06/23/14 19.07 ---80.33
07/06/15 18.59 ---80.81
11/01/07 99.28 20.63 ---78.65
09/16/09 21.20 ---78.47
09/20/10 19.55 ---80.12
10/27/11 19.48 ---80.19
01/07/13 21.07 ---78.60
07/29/13 NM NM NM Not Found
06/23/14 19.25 ---80.42
07/06/15 18.78 ---80.89
11/01/07 99.11 20.45 ---78.66
09/16/09 21.22 ---78.31
09/20/10 19.58 ---79.95
10/27/11 19.55 ---79.98
01/07/13 21.10 ---78.43
07/29/13 20.12 ---79.41
06/23/14 19.30 ---80.23
07/06/15 18.82 ---80.71
11/01/07 98.11 19.73 ---78.38
09/16/09 20.29 ---78.07
09/20/10 18.65 ---79.71
10/27/11 18.68 ---79.68
01/07/13 20.20 ---78.16
07/29/13 19.23 ---79.13
06/23/14 18.36 ---80.00
07/06/15 18.00 ---80.36
01/27/16 18.90 ---79.46
09/07/16 18.47 ---79.89
11/01/07 98.28 19.92 ---78.36
07/20/09 20.03 ---78.63 Pre-MMPE
07/24/09 20.21 ---78.45 Post-MMPE
09/16/09 20.48 ---78.18
09/20/10 18.75 ---79.91
10/27/11 18.87 ---79.79
12/03/12 20.39 ---78.27 Pre-MMPE
12/07/12 20.45 ---78.21 Post-MMPE
01/07/13 20.40 ---78.26
06/24/13 19.83 ---78.83 Pre-MMPE
06/28/13 19.95 ---78.71 Post-MMPE
07/29/13 19.46 ---79.20
05/19/14 18.51 ---80.15 Pre-MMPE
05/23/14 18.43 ---80.23 Post-MMPE
06/23/14 NM NM NM Not Found
09/07/16 NM NM NM Destroyed
11/01/07 98.23 19.85 ---78.38
09/16/09 20.40 ---78.20
09/20/10 18.77 ---79.83
10/27/11 18.81 ---79.79
01/07/13 20.30 ---78.30
07/29/13 19.40 ---79.20
06/23/14 NM NM NM Not Found
11/01/07 98.90 20.17 ---78.73
09/16/09 20.71 ---78.61
09/20/10 19.07 ---80.25
10/27/11 19.01 ---80.31
12/03/12 20.59 ---78.73 Pre-MMPE
12/07/12 20.66 ---78.66 Post-MMPE
01/07/13 20.60 ---78.72
06/24/13 20.11 ---79.21 Pre-MMPE
06/28/13 20.23 ---79.09 Post-MMPE
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
07/06/15 18.30 ---81.02
04/27/94MW-5
39
MW-13 11/30/95
MWD-6 11/22/95 39-44 44 99.66
MW-7 11/24/95 18 18-28 28 99.40
15 15-25
MW-10A 10/31/07 15 15-25
MW-12 12/01/95 18 18-28
25 99.53
98.60
MW-14 11/28/95 15 15-25 25 99.32
15 15-25 25
28 98.66
99.572515-2515
MW-11 12/01/95 18 18-28
25 99.67
28 98.36
MW-9A 10/31/07
Page 2 of 5
Date: 08/14/18
Bottom
of Well
(ft. BGS)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Date
Installed
(mm/dd/yy)
Comments
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
06/23/14 18.94 ---NM
01/27/16 19.34 ---NM
07/24/18 19.46 ---NM
11/01/07 99.34 20.42 ---78.92
09/16/09 20.97 ---78.76
09/20/10 19.23 ---80.50
10/27/11 19.20 ---80.53
01/07/13 20.51 ---79.22
07/29/13 NM NM NM Not Found
05/19/14 18.80 ---80.93 Pre-MMPE
05/23/14 18.78 ---80.95 Post-MMPE
06/23/14 NM NM NM Not Found
11/01/07 98.66 20.26 ---78.40
09/16/09 20.89 ---78.06
09/20/10 19.22 ---79.73
10/27/11 19.22 ---79.73
01/07/13 20.78 ---78.17
07/29/13 19.84 ---79.11
06/23/14 19.00 ---79.95
07/06/15 18.56 ---80.39
11/01/07 98.08 19.57 ---78.51
09/16/09 20.13 ---78.41
09/20/10 18.50 ---80.04
10/27/11 18.51 ---80.03
01/07/13 20.00 ---78.54
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
11/01/07 98.23 20.12 ---78.11
09/16/09 20.73 ---77.90
09/20/10 19.10 ---79.53
10/27/11 19.14 ---79.49
01/07/13 20.65 ---77.98
07/29/13 19.76 ---78.87
06/23/14 18.98 ---79.25
07/06/15 18.50 ---80.13
11/01/07 100.03 20.57 ---79.46
09/16/09 21.18 ---79.21
09/20/10 19.41 ---80.98
10/27/11 19.25 ---81.14
01/07/13 20.95 ---79.44
07/29/13 20.84 ---79.55
06/23/14 18.99 ---81.40
11/01/07 99.07 20.10 ---78.97
09/16/09 20.62 ---78.90
09/20/10 18.94 ---80.58
10/27/11 18.91 ---80.61
01/07/13 20.49 ---79.03
07/29/13 19.44 ---80.08
05/19/14 18.41 ---81.11 Pre-MMPE
05/23/14 18.62 ---80.90 Post-MMPE
06/23/14 18.61 ---80.91
06/01/15 17.35 ---82.17 Pre-MMPE
06/05/15 17.65 ---81.87 Post-MMPE
07/06/15 18.14 ---81.38
01/27/16 19.02 ---80.50
07/24/18 17.78 ---81.74
11/01/07 98.90 20.14 ---78.76
09/16/09 20.69 ---78.80
09/20/10 18.95 ---80.54
10/27/11 18.92 ---80.57
01/07/13 20.54 ---78.95
07/29/13 19.46 ---80.03
06/23/14 18.66 ---80.83
07/06/15 18.19 ---81.30
01/27/16 19.05 ---80.44
11/01/07 99.41 20.10 ---79.31
09/16/09 20.69 ---79.12
09/20/10 NM NM NM
11/01/07 98.43 20.42 ---78.01
09/16/09 21.01 ---77.88
09/20/10 19.38 ---79.51
10/27/11 19.50 ---79.39
01/07/13 20.92 ---77.97
07/29/13 20.07 ---78.82
06/23/14 19.31 ---79.58
07/06/15 18.80 ---80.09
07/24/18 19.54 ---79.35
98.892515-251511/01/07MW-25B
99.522818-281809/24/96MW-22
18 18-28
11/01/07
NM2818-281812/08/95MW-15
99.493020-3020
MW-15A 11/01/07 15 15-25 25 99.73
MW-17 04/19/96 18 18-28 28 98.95
MW-19 04/22/96 18 18-28 28 98.54
100.39
MW-20 04/22/96 18 18-28 28 98.63
MW-23A
MW-21 09/24/96 18 18-28
28
28
99.81MW-24 09/25/96
Page 3 of 5
Date: 08/14/18
Bottom
of Well
(ft. BGS)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Date
Installed
(mm/dd/yy)
Comments
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
11/01/07 97.29 19.57 ---77.72
09/16/09 20.13 ---77.57
09/20/10 18.58 ---79.12
10/27/11 18.65 ---79.05
01/07/13 20.07 ---77.63
07/29/13 19.30 ---78.40
18.24 ---79.46 Pre-AFVR
18.30 ---79.40 Post-AFVR
06/23/14 18.52 ---79.18
06/01/15 17.40 ---80.30 Pre-AFVR
06/01/15 17.44 ---80.26 Post-AFVR
07/06/15 18.05 ---79.65
01/27/16 18.90 ---78.80
09/07/16 18.98 ---78.72
11/01/07 98.36 NM NM NM Well Dry
09/16/09 NM NM NM Well Dry
09/20/10 NM NM NM Well Dry
10/27/11 NM NM NM Well Dry
01/07/13 17.25 ---81.53
07/29/13 NM NM NM Well Dry
06/23/14 NM NM NM Well Dry
07/06/15 NM NM NM Well Dry
11/01/07 95.54 18.14 ---77.40
09/16/09 NM NM NM
09/20/10 NM NM NM
10/27/11 NM NM NM
10/04/12 20.92 ---74.62 Pre-AFVR
10/04/12 20.93 ---74.61 Post-AFVR
01/07/13 NM NM NM
06/23/14 NM NM NM
11/01/07 97.70 20.25 ---77.45
09/16/09 20.85 ---77.30
09/20/10 19.31 ---78.84
10/27/11 19.47 ---78.68
20.81 ---77.34 Pre-AFVR
20.82 ---77.33 Post-AFVR
01/07/13 20.77 ---77.38
20.52 ---77.63 Pre-AFVR
20.52 ---77.63 Post-AFVR
07/29/13 20.05 ---78.10
18.88 ---79.27 Pre-AFVR
19.05 ---79.10 Post-AFVR
06/23/14 19.32 ---78.83
06/01/15 18.23 ---79.92 Pre-AFVR
06/01/15 18.23 ---79.92 Post-AFVR
07/06/15 19.32 ---78.83
01/27/16 19.67 ---78.48
09/07/16 19.77 ---78.38
07/24/18 19.50 ---78.65
11/01/07 96.32 19.34 ---76.98
09/16/09 19.88 ---76.85
09/20/10 NM NM NM
11/01/07 97.86 20.37 ---77.49
09/16/09 20.96 ---77.28
09/20/10 19.42 ---78.82
10/27/11 19.51 ---78.73
01/07/13 20.83 ---77.41
07/29/13 19.14 ---79.10
06/23/14 19.39 ---78.85
07/06/15 18.97 ---79.27
11/01/07 97.64 19.30 ---78.34
09/16/09 19.87 ---78.47
09/20/10 NM NM NM
11/01/07 94.72 18.32 ---76.40
09/16/09 18.81 ---76.38
09/20/10 17.51 ---77.68
10/27/11 17.68 ---77.51
01/07/13 18.78 ---76.41
07/29/13 18.31 ---76.88
06/23/14 17.68 ---77.51
07/06/15 17.30 ---77.89
01/27/16 17.95 ---77.24
09/07/16 18.07 ---77.12
11/01/07 NA 6.53 ------
09/16/09 7.03 ---75.21
09/20/10 6.40 ---75.84
10/27/11 6.47 ---75.77
01/07/13 7.23 ---75.01
07/29/13 6.95 ---75.29
06/23/14 6.69 ---75.55
07/06/15 6.47 ---75.77
07/24/18 6.39 ---75.85
09/16/09 20.36 ---79.16
09/20/10 NM NM NM
3525-352510/15/98MW-29
12/04/12
95.54
18-2818
8 8-18 18 98.78
06/26/13
98.15
MW-28 10/15/98 22 22-32 32
97.7028
MW-31 02/28/01 20 20-30
29 96.73
30 98.24
MW-30A 03/19/01
MW-33 11/07/01 20 30
MW-34
MW-37 09/01/09 10 10-25 25 99.52
10-251003/10/03MW-36
05/22/1409/25/96MW-26
82.2425
19-29
20-30
05/22/14
MW-27 10/03/96
95.193020-302011/07/01
98.34
19
Page 4 of 5
Date: 08/14/18
Bottom
of Well
(ft. BGS)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
TODD'S SERVICE STATION & BOWEN'S GROCERY (INCIDENT NOS. 11963 & 13592)
Facility ID #: 0-022807 & 0-022804
Well ID
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Date
Installed
(mm/dd/yy)
Comments
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
09/16/09 17.58 ---75.75
09/20/10 16.50 ---76.83
10/27/11 16.64 ---76.69
01/07/13 17.67 ---75.66
07/29/13 17.17 ---76.16
06/23/14 16.68 ---76.65
07/06/15 16.35 ---76.98
09/16/09 19.54 ---78.77
09/20/10 NM NM NM
09/16/09 24.24 ---77.82
09/20/10 NM NM NM
09/20/10 19.42 ---81.20
10/27/11 19.19 ---81.43
01/07/13 20.99 ---79.63
06/23/14 18.94 ---81.68
09/20/10 19.74 ---81.01
10/27/11 19.60 ---81.15
01/07/13 21.27 ---79.48
07/29/13 20.13 ---80.62
06/23/14 19.30 ---81.45
07/06/15 18.91 ---81.84
09/20/10 19.15 ---79.47
10/27/11 19.27 ---79.35
01/07/13 20.55 ---78.07
07/29/13 19.85 ---78.77
06/23/14 19.09 ---79.53
07/06/15 18.58 ---80.04
07/24/18 19.23 ---79.39
09/20/10 18.81 ---78.38
10/27/11 18.92 ---78.27
01/07/13 20.19 ---77.00
07/29/13 19.55 ---77.64
06/23/14 18.86 ---78.33
07/06/15 18.42 ---78.77
07/24/18 19.11 ---78.08
09/20/10 18.10 ---78.15
10/27/11 18.31 ---77.94
01/07/13 19.52 ---76.73
07/29/13 14.48 ---81.77
06/23/14 18.22 ---78.03
07/06/15 17.76 ---78.49
09/20/10 17.59 ---77.88
10/27/11 17.77 ---77.70
01/07/13 18.94 ---76.53
07/29/13 18.41 ---77.06
06/23/14 17.71 ---77.76
07/06/15 17.29 ---78.18
09/20/10 17.62 ---77.47
10/27/11 17.79 ---77.30
01/07/13 18.91 ---76.18
07/29/13 18.38 ---76.71
06/23/14 17.79 ---77.30
07/06/15 17.44 ---77.65
09/20/10 14.57 ---76.59
10/27/11 14.70 ---76.46
01/07/13 15.61 ---75.55
07/29/13 15.24 ---75.92
06/23/14 14.80 ---76.36
07/06/15 14.48 ---76.68
11/01/07 NA 20.89 ------
09/16/09 NM NM NM
09/20/10 NM NM NM
10/27/11 NM NM NM
01/07/13 NM NM NM
07/29/13 NM NM NM
06/23/14 NM NM NM
Notes:
• Reference point for elevation measurements: assumed elevation 100.00 ft.
• If free product is present in a well, groundwater elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness
x 0.8581].
• ft BGS: feet below ground surface.
• NA: Data not available.
• Top-of-casing elevations and well construction information for monitoring wells installed prior to 2007 reproduced from previous assessment
reports prepared by CES Engineering, P. C.
• Monitoring wells MW-9A, MW-10A, MW-15A and MW-25B were resurveyed on August 12, 2008 by GRI personnel.
• Monitoring wells MW-41 through MW-48, TW-1M, MW-1M, MW-2M and MW-3M were surveyed on September 17, 2010 by GRI personnel.
MW-43 25
MW-38 09/16/09 10 10-25 25 93.33
MW-39 09/16/09 10 10-25 25 98.31
MW-40 09/16/09 10 10-25 25 102.06
MW-41 09/16/10 10 10-25 25 100.62
MW-42 09/16/10 10 10-25 25 100.75
98.6210-25
1009/15/10
25 95.47
2510-25
1009/15/10
MW-45 09/15/10 10 10-25 25 96.25
95.09
91.16
MW-47
MW-48
09/15/10
09/15/10
10
10
• NM: Not Measured.
10-25
10-25
25
25
MW-46 09/15/10 10 10-25
97.19MW-44
100.033010-301007/22/03RW-1
Page 5 of 5
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
10/31/07 10,100 23,700 1,570 9,290 648 286 33.1 16.0 <5.00 71.6 13.0 14.1 166 988 309 39.8 NR NR NR
09/17/09 2,110 8,190 552 2,660 814 <100 <36.0 <28.0 <48.0 <30.0 <40.0 <40.0 <44.0 313 73.9 J 10.1 2,510 2,080 2,990
09/20/10 9,050 29,400 2,100 11,000 8,740 <250 <250 <250 <120 111 J <100 <100 221 J 1,530 398 J 31.8 NR NR NR
10/27/11 14,400 39,900 2,940 14,200 3,320 391 J <100 <100 <100 133 J <110 <100 262 J 1,840 439 J NR NR NR NR
01/07/13 4,940 25,700 1,980 10,400 2,710 327 <10 <10 <10 74.1 <10 <10 195 1,390 354 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 9,320 36,700 3,200 16,300 6,320 556 20.4 J 16.8 J <10 143 19.4 J <10 362 2,800 698 NR NR NR NR
07/06/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/27/16 7,300 37,800 2,610 12,700 5,880 502 <63 <63 <63 103 J <63 <63 274 1,850 449 NS NS NS NS
09/07/16 10,500 56,000 3,740 19,800 5,610 1,420 <130 <130 <130 142 J <130 <130 358 J 2,270 595 NR NR NR NR
07/24/18 3,460 28,200 2,360 11,600 1,520 483 <63 <63 <63 103 J <63 <63 239 J 1730 455 NR NR NR NR
10/31/07 10,600 39,000 2,420 11,300 1,870 439 37.8 <10.0 <10.0 86.0 11.2 <10.0 175 1,230 356 23.0 NR NR NR
09/17/09 5,830 28,800 2,110 10,600 660 376 <45.0 1,080 <60.0 91.6 J <50.0 <50.0 161 J 1,270 289 29.9 5,000 3,150 4,860
09/20/10 4,680 12,000 1,210 5,650 7,310 137 <50.0 <50.0 <24.0 41.3 J <20.0 <20.0 66.8 J 525 140 116 NR NR NR
10/27/11 3,940 15,000 1,170 6,410 897 149 <20 <20 <21 33.0 J <21 <20 74.8 J 634 144 NR NR NR NR
01/07/13 0.67 3.7 0.41 J 1.70 0.35 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.16 J <0.10 NR NR NR NR
07/30/13 3,130 22,300 1,620 8,970 952 265 <10 <10 <10 43.4 J <10 <10 93.2 825 179 NR NR NR NR
06/24/14 1,450 8,130 752 4,340 769 157 1.5 J 1.5 J <1.0 24.0 3.6 J <1.0 51.7 434 96.0 NR NR NR NR
07/06/15 2,290 11,100 1,420 7,930 4,540 248 <36 <35 <35 42.6 J <40 <31 98.2 J 900 208 NR NR NR NR
01/27/16 <0.13 0.16 J <0.13 <0.31 2.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 1.9 21.5 3.8 12.7 1.7 0.96 <0.13 <0.13 <0.13 0.16 J <0.13 <0.13 0.56 1.4 0.35 J NR NR NR NR
07/24/18 135 2,150 230 1,050 27.8 37.2 <6.3 <6.3 <6.3 9.9 J <6.3 <6.3 23.1 J 173 45.1 NR NR NR NR
02/28/07 15.0 <0.500 3.36 1.43 <0.500 15.5 0.880 0.870 <0.500 2.24 <0.500 0.710 1.57 2.38 <0.500 15.9 NR NR NR
10/31/07 59.1 0.930 14.6 7.97 <0.500 16.4 4.10 4.09 <0.500 11.3 <0.500 4.09 9.58 3.22 4.16 29.9 NR NR NR
09/17/09 20.1 <0.190 2.31 <0.220 <0.250 1.58 <0.180 0.970 J <0.240 2.65 <0.200 <0.200 1.39 0.883 J <0.180 7.05 106 <100 <100
09/20/10 13.7 2.15 0.606 J 1.85 J <0.500 3.61 <1.00 <1.00 <0.480 2.69 <0.400 <0.400 0.776 J 0.488 J <0.360 14.3 NR NR NR
10/27/11 8.4 0.22 J 0.89 1.1 J <0.13 1.8 <0.10 0.42 J <0.10 1.6 <0.11 <0.10 0.93 0.19 J <0.10 NR NR NR NR
01/07/13 0.74 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 1.0 <0.10 <0.10 0.55 J <0.10 <0.10 <0.10 0.14 J <0.10 0.22 J 0.11 J <0.10 0.28 J 0.36 J 0.15 J NR NR NR NR
07/06/15 2.9 <0.17 <0.15 0.62 J <0.16 0.98 0.35 J 0.59 <0.14 0.79 <0.16 <0.12 0.63 1.7 0.16 J NR NR NR NR
01/27/16 0.45 J <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
Facility ID #s: 0-022807 & 0-022804
MW-3 1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-ButylbenzeneMW-1A
MW-2
Page 1 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene09/20/10 1,500 45,000 9,170 53,400 309 J 2,870 1,830 <500 <240 852 J <200 <200 2,410 21,900 5,330 30.6 NR NR NR
10/27/11 1,700 33,200 6,290 33,500 2,880 1,180 201 J 120 J <100 457 J <110 <100 1,290 8,760 2,370 NR NR NR NR
01/07/13 509 19,500 4,620 24,300 737 960 58.1 43.7 J <10 249 <10 22.7 J 761 4,610 1,340 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 894 19,200 4,580 27,300 1,170 858 471 269 <2.5 725 7.6 J 144 920 6,200 1,730 NR NR NR NR
07/06/15 381 14,200 4,810 28,600 620 1,440 98.9 J 59.1 J <35 264 <40 34.7 J 763 7,110 1,890 NR NR NR NR
01/27/16 349 24,200 12,200 68,400 1,810 3,360 879 465 <63 1,170 <63 240 J 4,190 22,100 7,640 NR NR NR NR
09/07/16 146 J 13,000 5,710 35,100 184 J 1,500 260 159 J <63 388 <63 66.9 J 1,320 9,470 2,940 NR NR NR NR
07/24/18 115 4,380 2,900 16,100 <25 628 58.8 J 43.1 J <25 195 <25 <25 550 4,250 1,200 NR NR NR NR
10/31/07 1,120 5,620 1,490 4,130 <5.00 283 36.3 17.0 <5.00 82.5 <5.00 20.2 141 682 287 16.0 NR NR NR
09/17/09 274 2,280 666 1,810 <10.0 168 <7.20 <5.60 <9.60 58.6 <8.00 <8.00 64.8 392 124 12.9 2,770 2,250 1,480
09/20/10 568 1,780 630 2,340 <5.00 95.9 40.7 <10.0 11.5 J 38.0 <4.00 <4.00 52.1 539 160 19.6 NR NR NR
10/27/11 130 456 267 617 <0.13 47.9 3.2 2.4 1.8 26.0 <0.11 3.3 34.0 108 32.8 NR NR NR NR
01/07/13 590 4,770 1,400 5,120 <1.0 391 9.0 8.8 4.9 J 80.0 <1.0 11.9 132 804 248 NR NR NR NR
07/30/13 69.0 705 485 1,670 <2.0 216 6.1 J 5.8 J <2.0 40.2 <2.0 8.0 J 70.3 314 121 NR NR NR NR
06/24/14 14.8 38.1 12.3 79.1 <0.10 8.7 0.29 J 0.26 J 0.30 J 1.8 <0.10 0.39 J 2.2 9.2 4.1 NR NR NR NR
07/06/15 5.3 40.7 9.2 38.4 <0.16 2.0 <0.14 <0.14 <0.14 0.55 <0.16 <0.12 0.86 3.4 1.3 NR NR NR NR
01/27/16 185 1,690 631 2,060 <3.1 187 5.4 J 4.8 J <3.1 40.6 <3.1 6.0 J 63.2 336 111 NR NR NR NR
07/24/18 168 1,860 553 1,930 <6.3 92.2 <6.3 <6.3 <6.3 37.0 <6.3 <6.3 55.1 239 85.3 NR NR NR NR
10/31/07 2.72 3.43 <0.500 1.17 6.10 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 NR NR NR
09/17/09 0.627 J 0.602 J <0.150 <0.220 0.868 J <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.200 <0.150 <0.180 <1.50 <100 <100 <100
09/20/10 <0.700 2.84 J 1.23 J 2.21 J <1.25 <2.50 <2.50 <2.50 <1.20 <0.750 <1.00 <1.00 <1.10 0.756 J <0.900 6.89 NR NR NR
10/27/11 <0.13 0.52 <0.15 0.56 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.38 J 0.46 J <0.10 0.21 J 0.59 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/31/07 36.9 <0.500 14.6 <1.00 <0.500 6.30 1.63 2.71 <0.500 7.20 1.53 3.14 6.78 <0.500 <0.500 <5.00 NR NR NR
09/17/09 10.3 0.366 J 179 3.61 <0.250 58.7 <0.180 7.46 <0.240 57.3 1.75 0.588 J 93.3 2.06 0.795 J <1.50 758 489 481
09/20/10 1.91 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 0.485 J <0.200 <0.200 <0.220 <0.150 <0.180 25.0 NR NR NR
10/27/11 3.7 0.30 J <0.15 <0.30 <0.13 0.53 <0.10 0.41 J <0.10 0.77 0.26 J <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 19.1 <0.10 13.1 <0.22 0.33 J 3.0 1.3 2.9 <0.10 12.5 0.90 1.5 19.2 <0.10 <0.10 NR NR NR NR
07/30/13 7.3 <0.10 7.0 <0.22 0.43 J 1.5 0.46 J 0.78 <0.10 4.7 0.78 0.34 J 7.2 <0.10 <0.10 NR NR NR NR
06/24/14 0.16 J <0.10 0.15 J <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.13 J <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-7
MWD-6
MW-5
MW-4
Page 2 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene11/01/07 0.930 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.7 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 1.79 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 11.3 <100 <100 <100
09/20/10 0.284 J <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 35.1 NR NR NR
10/27/11 0.55 0.23 J <0.15 0.46 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.12 J <0.10 NR NR NR NR
01/07/13 2.9 <0.10 <0.10 <0.22 0.11 J <0.15 <0.10 0.13 J <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 16.7 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 7.29 <100 <100 <100
09/20/10 0.475 J 2.95 0.384 J 1.90 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 0.503 J <0.180 27.9 NR NR NR
10/27/11 <0.13 0.14 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.11 J <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.19 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
10/31/07 617 191 366 652 52.0 132 9.58 4.13 <0.500 28.5 0.640 5.68 43.6 199 81.9 7.17 NR NR NR
09/17/09 1,560 3,120 687 1,920 43.6 J 208 <18.0 <14.0 <24.0 53.3 J <20.0 <20.0 52.5 J 316 88.1 J 12.5 3,150 1,430 1,870
09/20/10 29.2 1.68 0.400 J 13.3 11.1 3.56 <0.500 <0.500 <0.240 1.53 <0.200 <0.200 0.304 J 5.78 <0.180 25.6 NR NR NR
10/27/11 3.4 <0.13 <0.15 <0.30 1.2 0.37 J <0.10 <0.10 <0.10 0.11 J <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 324 E 97.6 114 188.9 121 44.3 1.2 1.5 0.38 J 12.3 0.83 1.6 18.7 55.5 11.3 NR NR NR NR
07/30/13 276 194 66.4 249 98.8 36.9 0.89 0.97 0.30 J 8.6 0.61 1.1 12.7 39.6 7.7 NR NR NR NR
06/24/14 152 20.5 11.5 89.9 29.3 21.9 0.40 J 0.37 J 0.29 J 3.2 <0.10 0.65 3.6 14.9 1.9 NR NR NR NR
07/06/15 33.8 0.38 J 6.5 12.8 7.6 16.0 0.28 J 0.25 J <0.14 1.7 <0.16 0.55 2.2 4.4 <0.14 NR NR NR NR
01/27/16 225 310 144 467 6.7 68.1 1.4 J <1.3 <1.3 11.0 <1.3 2.1 J 15.8 98.9 23.2 NR NR NR NR
09/07/16 27.7 29.5 16.8 32.3 0.25 J 7.1 <0.13 <0.13 <0.13 1.1 <0.13 <0.13 1.5 3.7 0.73 NR NR NR NR
11/01/07 8,470 20,300 2,100 8,390 9,250 449 27.3 8.19 <0.500 76.3 46.0 6.75 154 1,280 420 18.8 NR NR NR
09/17/09 2,560 8,380 778 2,500 330 <100 <36.0 <28.0 <48.0 <30.0 <40.0 <40.0 88.1 J 552 141 J 3.22 2,630 1,700 2,360
09/20/10 1,500 517 260 764 845 76.3 7.59 J <5.00 <2.40 17.7 <2.00 <2.00 32.3 174 65.7 74.5 NR NR NR
10/27/11 3,120 9,080 895 4,130 2,990 128 <20 <20 <21 35.1 J <21 <20 83.9 J 613 160 NR NR NR NR
01/07/13 4,010 15,500 1,400 6,790 1,790 235 <10 <10 <10 52.3 <10 <10 146 1,080 241 NR NR NR NR
07/30/13 1,640 6,850 785 3,230 1,140 152 <25 <25 <25 32.5 J <25 <25 89.0 J 503 126 J NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/07/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-10A
MW-9A
MW-11
MW-12
Page 3 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene11/01/07 12.9 <0.500 2.65 <1.00 <0.500 <5.00 <0.500 2.06 <0.500 2.57 <0.500 <0.500 2.69 <0.500 <0.500 45.0 NR NR NR
09/17/09 8.77 <0.190 43.7 <0.220 <0.250 3.50 <0.180 3.19 <0.240 20.3 <0.200 0.454 J 26.4 <0.150 0.624 J 12.1 246 179 183
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 42.1 NR NR NR
10/27/11 0.15 J 0.24 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 1.2 <0.10 0.11 J <0.22 <0.10 <0.15 <0.10 0.20 J <0.10 0.34 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 0.83 0.14 J <0.10 <0.22 <0.10 <0.15 <0.10 0.11 J <0.10 0.33 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 199 2.45 88.3 101 14.8 63.7 8.79 4.09 <0.500 26.8 <0.500 6.02 20.5 104 36.3 47.6 NR NR NR
10/31/07 212 11.4 280 185 8.98 144 17.4 6.66 <0.500 46.8 <0.500 10.2 54.8 87.4 90.8 12.4 NR NR NR
09/17/09 153 193 261 200 3.32 J 143 <1.80 <1.40 <2.40 22.5 <2.00 <2.00 20.7 62.4 21.5 13.6 1,100 504 506
09/20/10 64.5 6.39 68.7 41.7 <0.250 66.9 2.58 1.94 <0.240 16.6 <0.200 0.391 J 12.3 24.4 0.665 J 50.2 NR NR NR
10/27/11 183 5.0 148 12.2 12.3 78.6 2.7 3.8 <0.52 32.0 <0.54 3.5 23.3 5.0 0.66 J NR NR NR NR
01/07/13 144 170 228 237.8 9.5 135 3.2 3.4 <0.50 26.5 <0.50 2.8 25.6 50.2 10.5 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/06/15 0.89 0.34 J 2.3 2.1 0.20 J 1.5 <0.14 <0.14 <0.14 0.24 J <0.16 <0.12 0.29 J 0.51 0.16 J NR NR NR NR
06/24/14 38.8 282 213 1,120 <0.10 120 4.9 4.3 <0.10 24.8 <0.10 7.2 31.5 224 74.6 NS NS NS NS
01/27/16 114 535 638 1,840 <3.1 250 9.5 J 8.5 J <3.1 64.4 <3.1 11.7 J 95.3 398 177 NS NS NS NS
07/24/18 41.8 249 229 808 <1.3 81.3 5.2 5.0 <1.3 26.5 <1.3 6.0 41.9 201 73.5 NR NR NR NR
11/01/07 358 1,690 1,320 3,240 <0.500 358 36.4 12.0 <0.500 81.5 <0.500 17.1 116 721 333 56.4 NR NR NR
09/17/09 78.6 1,030 513 1,680 <5.00 170 <3.60 <2.80 <4.80 45.4 <4.00 <4.00 44.3 360 112 9.16 2,640 1,100 1,460
09/20/10 551 756 542 1,570 <50.0 343 J <36.0 <28.0 <48.0 576 <40.0 <40.0 413 482 313 64.5 NR NR NR
10/27/11 151 534 458 1,230 <2.6 150 7.1 J 5.5 J <2.1 44.5 <2.1 8.0 J 64.9 287 130 NR NR NR NR
01/07/13 59.0 477 353 885 <2.0 125 5.3 J 5.5 J <2.0 35.9 <2.0 5.1 J 50.7 172 101 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 55.2 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 2.79 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 1.83 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 15.5 NR NR NR
10/27/11 <0.13 0.22 J <0.15 0.36 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-15
MW-14
MW-17
MW-15A
MW-13
Page 4 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene11/01/07 6.58 1.13 10.5 3.33 4.88 25.9 6.63 4.30 <0.500 13.2 0.630 2.50 7.16 2.52 <0.500 45.3 NR NR NR
09/17/09 <0.140 <0.190 37.7 22.6 <0.250 66.2 <0.180 3.38 <0.240 34.8 <0.200 <0.200 41.2 116 47.4 14.6 243 394 505
09/20/10 0.917 J <0.190 <0.150 0.270 J 1.51 1.64 2.65 1.35 <0.240 1.15 <0.200 <0.200 <0.220 <0.150 <0.180 49.2 NR NR NR
10/27/11 <0.13 0.24 J <0.15 0.56 J <0.13 0.25 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.23 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 7.5 12.5 0.12 J 40.4 2.4 2.6 <0.10 16.7 <0.10 0.87 10.4 47.0 1.0 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 13.0 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 16.5 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 1.32 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 <1.50 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 14.3 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 30.6 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 2.69 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.4 NR NR NR
09/17/09 11.1 0.398 J 1.69 11.3 <0.250 <0.500 <0.180 <0.140 <0.240 0.773 J <0.200 <0.200 0.749 J 3.69 1.81 5.70 429 105 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 1.20 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 8.09 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
02/28/07 291 387 345 1,020 34.5 35.3 19.1 6.00 <0.500 33.2 29.4 4.95 75.2 523 115 18.1 NR NR NR
10/31/07 95.7 1,020 795 2,820 <2.50 155 46.4 16.6 <2.50 79.4 <2.50 13.4 224 1,190 373 <5.00 NR NR NR
09/17/09 78.9 J 2,270 1,900 8,570 <50.0 324 <36.0 <28.0 <48.0 156 J <40.0 <40.0 305 2,430 558 3.75 4,900 5,980 393,000
09/20/10 158 58.2 188 156 16.9 20.8 24.0 15.9 <2.40 30.9 30.5 <2.00 60.6 288 53.9 37.2 NR NR NR
10/27/11 69.3 301 487 1,730 <2.6 78.9 16.6 12.7 <2.1 61.0 4.2 J 9.4 J 190 955 267 NR NR NR NR
01/07/13 90.4 261 1,180 4,820 29.5 240 27.3 24.5 <2.0 172 12.4 16.0 542 3,480 828 NR NR NR NR
07/30/13 91.0 199 648 2,480 9.7 J 115 27.0 22.5 J <5.0 99.2 12.5 J 15.6 J 382 1,680 486 NR NR NR NR
06/23/14 8.6 5.3 34.6 111 <0.10 6.4 4.2 3.3 <0.10 8.5 0.73 2.6 28.5 67.8 20.7 NR NR NR NR
07/06/15 12.6 17.4 97.2 379 <0.82 20.3 7.1 4.9 <0.71 13.1 <0.80 3.7 46.3 211 60.0 NR NR NR NR
01/27/16 37.2 82.2 445 1,710 <3.1 106 22.2 16.4 <3.1 47.2 <3.1 12.0 J 159 878 218 NR NR NR NR
07/24/18 5.4 26.0 421 1,390 <1.3 90.6 16.6 12.7 <1.3 58.6 <1.3 8.5 165 954 241 NR NR NR NR
MW-19
MW-22
MW-20
MW-21
Page 5 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene02/28/07 7.39 <0.500 4.73 7.21 <0.500 <5.00 <0.500 0.590 <0.500 1.88 <0.500 0.990 2.42 17.4 2.49 16.2 NR NR NR
10/31/07 3.32 <0.500 1.98 2.58 <0.500 <5.00 <0.500 <0.500 <0.500 1.53 <0.500 <0.500 0.810 6.75 1.27 16.4 NR NR NR
09/17/09 3.86 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 0.792 J <0.200 <0.200 0.387 J 3.64 <0.180 18.7 <100 <100 <100
09/20/10 14.2 0.242 J 2.39 9.05 <0.250 6.07 2.53 3.44 <0.240 6.40 <0.200 0.580 J 1.64 20.4 1.69 20.9 NR NR NR
10/27/11 7.0 0.22 J 3.7 3.1 <0.13 2.3 <0.10 0.61 <0.10 2.0 <0.11 0.95 1.8 6.8 <0.10 NR NR NR NR
01/07/13 1.7 <0.10 <0.10 0.28 J <0.10 0.41 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.96 <0.10 NR NR NR NR
07/30/13 12.3 0.15 J 4.1 5.5 <0.10 3.5 <0.10 1.4 <0.10 3.6 0.16 J 1.8 4.4 15.8 <0.10 NR NR NR NR
06/24/14 7.4 <0.10 3.1 3.0 <0.10 2.3 <0.10 0.83 <0.10 2.1 <0.10 1.1 2.4 8.6 0.14 J NR NR NR NR
07/06/15 22.0 0.47 J 11.7 19.8 <0.16 12.7 0.14 J 1.4 <0.14 4.7 <0.16 2.6 5.0 36.5 1.0 NR NR NR NR
01/27/16 1.1 <0.13 0.21 J <0.31 <0.13 0.46 J <0.13 <0.13 <0.13 0.18 J <0.13 <0.13 0.19 J 0.19 J <0.13 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 13.1 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.0 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 4.67 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 61.5 95.7 46.1 75.8 5.64 12.2 2.94 2.03 <0.500 3.77 5.95 <0.500 7.17 20.6 7.97 32.3 NR NR NR
09/17/09 11.5 <0.190 <0.150 <0.220 10.7 5.35 <0.180 <0.140 <0.240 0.515 J 12.7 <0.200 <0.220 <0.150 <0.180 8.33 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 26.8 NR NR NR
10/27/11 <0.13 0.15 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 0.49 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 0.57 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
02/28/07 4,210 2,780 1,120 2,200 2,350 1,690 12.8 4.70 3.71 53.9 11.0 3.30 96.9 594 143 6.94 NR NR NR
11/01/07 4,130 2,880 1,150 2,220 1,720 190 14.9 6.23 1.65 47.7 9.05 4.76 89.0 509 139 21.6 NR NR NR
09/17/09 3,910 6,350 952 2,950 1,730 172 <18.0 <14.0 <24.0 50.3 J <20.0 <20.0 75.4 J 424 117 4.19 1,950 1,670 83,000
09/20/10 25.1 <0.190 0.827 J <0.220 96.2 0.957 J <0.500 <0.500 <0.240 0.313 J <0.200 <0.200 <0.220 <0.150 <0.180 45.3 NR NR NR
10/27/11 4.1 0.22 J 0.54 <0.30 4.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 257 102 77.0 149.9 147 13.3 <1.0 <1.0 <1.0 4.7 J <1.0 <1.0 10.3 47.7 9.2 NR NR NR NR
07/30/13 180 173 40.7 120 188 7.3 <0.10 0.15 J <0.10 2.1 0.44 J <0.10 3.3 10.1 2.2 NR NR NR NR
06/23/14 14.6 1.6 1.5 4.7 86.5 0.46 J <0.10 <0.10 <0.10 0.15 J 0.13 J <0.10 0.13 J 0.73 <0.10 NR NR NR NR
07/06/15 2.4 <0.17 0.22 J <0.43 12.1 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 9.0 8.3 1.6 5.9 26.4 0.50 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.51 <0.13 NR NR NR NR
09/07/16 0.31 J <0.13 <0.13 <0.31 5.5 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-26
MW-25B
MW-24
MW-23A
Page 6 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene02/28/07 <0.500 <0.500 <0.500 <1.00 3.29 <5.00 <0.500 <0.500 <0.500 <0.500 2.81 <0.500 <0.500 <0.500 <0.500 9.40 NR NR NR
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 19.6 NR NR NR
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 692 90.3 93.4 81.7 120 15.4 3.91 2.96 <0.500 28.0 1.04 1.25 15.0 16.7 5.44 6.88 NR NR NR
11/01/07 3,810 2,110 788 1,580 1,370 148 13.7 6.32 <0.500 40.9 9.59 5.45 67.8 364 92.0 40.5 NR NR NR
09/17/09 2,860 5,780 696 2,320 869 127 <18.0 <14.0 <24.0 37.8 J <20.0 <20.0 61.2 J 370 91.5 J <1.50 1,690 1,280 1,800
09/20/10 1,140 939 266 636 402 <100 <18.0 <14.0 <24.0 28.8 J <20.0 <20.0 37.3 J 156 36.4 J 13.4 NR NR NR
10/28/11 2,130 1,340 487 762 1,060 80.2 6.4 J <5.1 <5.2 32.1 5.9 J <5.0 50.0 236 25.9 NR NR NR NR
01/07/13 2,110 6,130 731 3,300 1,110 150 <5.0 <5.0 <5.0 31.2 <5.0 <5.0 74.5 551 138 NR NR NR NR
07/30/13 1,420 3,280 438 1,590 858 78.8 <10 <10 <10 20.2 J <10 <10 43.0 J 289 69.7 NR NR NR NR
06/23/14 508 2,480 268 1,070 319 67.2 2.6 2.2 <0.10 19.9 1.4 1.4 38.7 206 42.7 NR NR NR NR
07/06/15 525 1,780 317 1,290 157 90.1 <7.2 <6.9 <7.1 21.4 J <8.0 <6.1 35.0 270 65.7 NR NR NR NR
01/27/16 550 1,370 337 1,380 138 106 <3.1 <3.1 <3.1 20.7 <3.1 <3.1 33.0 315 70.5 NR NR NR NR
09/07/16 647 1,330 408 1,920 317 93.4 <6.3 <6.3 <6.3 25.0 <6.3 <6.3 39.5 309 79.9 NR NR NR NR
07/24/18 677 291 409 1,800 627 81.7 <3.1 <3.1 <3.1 20.3 <3.1 <3.1 39.3 312 75.5 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 69.0 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 218 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 28.4 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 12.2 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0500 <0.500 <0.500 90.3 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 13.9 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 27.6 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-29
MW-31
MW-30A
MW-27
MW-28
Page 7 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 91.1 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 35.8 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 97.3 <0.500 <0.500 <1.00 50.9 <5.00 <0.500 <0.500 <0.500 1.13 <0.500 <0.500 <0.500 <0.500 <0.500 58.8 NR NR NR
11/01/07 146 <0.500 <0.500 <1.00 60.8 <5.00 <0.500 <0.500 <0.500 2.00 <0.500 <0.500 <0.500 <0.500 <0.500 165 NR NR NR
09/17/09 102 <0.190 <0.150 <0.220 32.2 <0.500 <0.180 <0.140 <0.240 1.10 <0.200 <0.200 <0.220 <0.150 0.525 J 12.5 <100 <100 <100
09/20/10 72.4 0.908 J 4.77 4.41 78.0 4.60 0.382 J 0.303 J <0.480 2.50 <0.400 <0.400 1.21 J <0.300 <0.360 40.4 NR NR NR
10/28/11 0.13 J 0.15 J <0.15 <0.30 1.9 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.12 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 3.4 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 11.7 J <10 <10 <22 451 <15 <10 <10 <10 <10 <10 <10 <10 <10 <10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 2.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 3.9 <0.17 0.17 J <0.43 5.1 0.45 J <0.14 <0.14 <0.14 0.17 J <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 0.32 J 0.25 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 <0.13 <0.13 <0.13 <0.31 1.5 <0.13 <0.13 <0.13 <0.13 <0.13 0.43 J <0.13 <0.13 <0.13 <0.13 NR NR NR NR
03/01/07 <0.500 <0.500 <0.500 <1.00 2.36 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 28.4 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 19.0 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 3.75 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 0.410 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 24.6 NR NR NR
10/28/11 <0.13 <0.13 <0.15 <0.30 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 1.0 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 20.3 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/17/09 <0.140 <0.190 <0.150 <0.220 3.07 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 39.4 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 0.794 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 77.4 NR NR NR
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-37
MW-33
MW-34
MW-36
MW-38
Page 8 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 25.8 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/17/09 <0.140 1.82 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 14.0 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 0.327 J <0.180 100 <100 <100 <100
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
09/20/10 6.54 1.30 17.4 77.1 <0.250 1.43 J 3.24 0.680 J <0.240 1.85 <0.200 <0.200 4.04 25.8 9.18 80.2 1,450 431 665
10/27/11 10.7 1.3 1.5 11.0 0.15 J 0.12 J 0.14 J <0.10 <0.10 0.21 J <0.11 <0.10 0.29 J 1.6 2.1 NR NR NR NR
01/07/13 18.1 3.1 10.7 39.9 <0.10 <0.15 0.15 J 0.18 J <0.10 1.1 <0.10 0.12 J 2.0 7.7 5.1 NR NR NR NR
07/29/13 5.6 0.31 J 0.27 J 3.5 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.41 J 1.1 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 78.5 <100 <100 <100
10/27/11 <0.13 0.19 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.11 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/20/10 20.4 0.447 J 4.18 1.01 8.18 <1.00 <0.180 <0.140 <0.240 1.11 <0.200 <0.200 0.961 J <0.150 <0.180 104 <100 <100 <100
10/28/11 11.4 0.22 J <0.15 0.36 J 4.8 <0.10 <0.10 <0.10 <0.10 0.24 J <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 5.3 <0.10 0.11 J <0.22 4.6 <0.15 <0.10 <0.10 <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 46.7 0.25 J 2.7 <0.22 11.9 <0.15 0.13 J 0.13 J <0.10 1.1 <0.10 <0.10 0.60 <0.10 <0.10 NR NR NR NR
06/23/14 1.2 <0.10 <0.10 <0.20 2.4 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-39
MW-43
MW-40
MW-42
MW-41
MW-44
Page 9 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 229 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 1.17 <0.190 <0.150 0.276 J 1.99 <1.00 <0.180 <0.140 <0.240 0.415 J 2.32 <0.200 <0.220 <0.150 <0.180 106 <100 <100 <100
10/28/11 <0.13 0.14 J <0.15 0.48 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.17 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 0.17 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 0.25 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 0.40 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 26.6 <0.190 <0.150 <0.220 12.0 <1.00 0.201 J 0.177 J <0.240 1.43 <0.200 <0.200 <0.220 <0.150 <0.180 116 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 101 <0.50 <0.50 <1.08 11.0 <0.74 <0.50 <0.50 <0.50 1.8 J <0.50 <0.50 <0.50 <0.50 <0.50 NR NR NR NR
07/30/13 12.9 <0.10 <0.10 <0.22 1.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 0.502 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 49.9 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.96 <0.10 <0.10 <0.22 1.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 0.18 J <0.10 <0.10 <0.22 0.38 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 0.69 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 9.6 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 3.45 NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 0.189 J <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 2.44 J NR NR NR
10/28/11 <0.13 0.14 J <0.15 <0.30 <0.13 0.11 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
MW-45
MW-46
MW-47
MW-48
WSW-5
WSW-13
Page 10 of 11
Date : 07/31/18
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Facility ID #s: 0-022807 & 0-022804
1,3,5-TrimethylbenzeneBenzeneMAC (mg/l)
GCL (mg/l)C9-C10 Aromatics1,2-DibromoethaneEthylbenzenep-IsopropyltolueneMADEP Method VPHEPA Method 6200BAnalytical Method
n-PropylbenzeneIsopropylbenzeneContaminant of
Concern
C9-C12 AliphaticsC5-C8 AliphaticsLeadn-Butylbenzene TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)TolueneIPEMTBE1,2,4-TrimethylbenzeneNaphthaleneXylenessec-Butylbenzene01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the MACs.
• J: Estimated value.
• E: Value exceeds calibration range.
• <: Less than the method detection limit specified in the laboratory report.
• NR: Analysis not requested.
• NS: Not sampled.
• A concentration of o-chlorotoluene (140 µg/l) that exceeded the MAC was reported in the ground water sample collected from MW-4 on July 24, 2018.
• For other compounds detected that did not exceed the MAC, please refer to the laboratory reports.
• MAC: Maximum allowable concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
WSW-18
Page 11 of 11
Date: 08/14/18 Facility ID #: 0-022807 & 0-022804
Well
ID
Date
Collected
(mm/dd/yy)
DO
(mg/l)pH Temperature
(o C)
Conductivity
(mS/cm)
ORP
(mV)
MW-1A 07/24/18 1.16 5.51 19.80 125 30.0
MW-2 07/24/18 2.06 5.82 19.94 195 106.0
MW-4 07/24/18 0.46 4.70 19.82 59 97.8
MW-15 07/24/18 0.50 5.51 20.04 98 45.2
MW-22 07/24/18 1.85 5.44 20.41 91 69.6
MW-29 07/24/18 1.08 6.03 22.00 189 35.9
TABLE 2A
SUMMARY OF FIELD PARAMETER MEASUREMENTS
TODD’S SERVICE CENTER & BOWEN’S GROCERY (INCIDENT NOS. 11963 & 13592)
1 of 1

APPENDICES

APPENDIX A
Miller’s County Store Ground Water Gauging and Sample Information
Date: 08/14/18
09/20/10 19.38 ---80.81
10/27/11 19.19 ---81.00
01/07/13 20.76 ---79.43
07/29/13 19.85 ---80.34
06/23/14 18.92 ---81.27
07/06/15 18.28 ---81.91
01/27/16 18.85 ---81.34
09/07/16 19.25 ---80.94
07/24/18 18.78 ---81.41
09/17/09 21.10 ---79.01
09/20/10 19.38 ---80.73
10/27/11 19.34 ---80.77
01/07/13 20.93 ---79.18
07/29/13 19.66 ---80.45
05/19/14 18.88 ---81.23 Pre-MMPE
05/23/14 19.21 ---80.90 Post-MMPE
06/23/14 19.06 ---81.05
06/01/15 17.75 ---82.36 Pre-MMPE
06/05/15 18.09 ---82.02 Post-MMPE
07/06/15 18.58 ---81.53
01/27/16 19.40 ---80.71
09/07/16 19.63 ---80.48
07/24/18 19.22 ---80.89
09/20/10 18.73 ---80.49
10/27/11 18.73 ---80.49
01/07/13 NM NM NM
07/29/13 19.35 ---79.87
05/19/14 18.26 ---80.96 Pre-MMPE
05/23/14 18.45 ---80.77 Post-MMPE
06/23/14 18.43 ---80.79
07/06/15 17.93 ---81.29
01/27/16 18.83 ---80.39
09/07/16 19.03 ---80.19
07/24/18 18.63 ---80.59
09/20/10 18.60 ---80.40
10/27/11 18.59 ---80.41
01/07/13 20.17 ---78.83
07/29/13 20.17 ---78.83
05/19/14 18.15 ---80.85 Pre-MMPE
05/23/14 18.26 ---80.74 Post-MMPE
06/23/14 18.31 ---80.69
06/01/15 17.07 ---81.93 Pre-MMPE
06/05/15 17.47 ---81.53 Post-MMPE
07/06/15 17.84 ---81.16
01/27/16 18.75 ---80.25
09/07/16 18.91 ---80.09
07/24/18 18.54 ---80.46
Notes:
• Reference point for elevation measurements: assumed elevation 100.00 ft.
• If free product is present in a well, groundwater elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness
x 0.8581].
• ft BGS: feet below ground surface.
• NA: Data not available.
• Top-of-casing elevations relative to assumed datum of 100.00 feet.
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TW-1M 09/15/10 40 40-45 45 100.19
MW-1M 09/17/09 10 10-25 25 100.11
MW-2M 09/16/10 10 10-25 25 99.22
MW-3M 09/16/10 10 10-25 25 99.00
• NM: Not Measured.
Page 1 of 1
Date : 08/01/18 Facility ID #: 0-022895
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
09/20/10 4.95 4.15 4.89 18.1 <0.500 <2.00 2.10 <0.280 <0.480 5.78 <0.400 <0.400 4.07 2.60 2.52 3.41 <100 <100 <100
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <3.4 570 <3.0 <8.6 <3.3 <2.4 <2.9 <2.8 <2.8 <2.4 <3.2 <2.4 <3.1 <2.7 <2.7 NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
09/07/16 <0.13 47.9 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR
07/24/18 <0.13 6.0 0.66 1.7 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.50 0.15 J NR NR NR NR
09/17/09 1,310 36,100 4,070 22,700 211 J 1,060 <90.0 4,200 <120 265 J <100 642 642 4,900 1,170 4.26 12,200 10,700 15,500
09/20/10 1,130 11,900 1,410 6,210 <100 1,640 608 <56.0 <96.0 1,150 792 <80.0 896 2,850 964 45.3 NR NR NR
10/27/11 1,460 24,100 3,970 22,300 244 J 1,000 <100 <100 <100 263 J 226 J <100 763 5,320 1,430 NR NR NR NR
01/07/13 528 16,300 3,830 21,920 45.6 1,000 50.6 27.8 <5.0 186 73.1 18.5 J 589 4,520 1,090 NR NR NR NR
07/30/13 982 23,500 3,030 15,600 208 J 523 <50 <50 <50 110 J 220 J <50 344 2,400 582 NR NR NR NR
06/24/14 1,210 10,600 2,990 21,600 273 1,930 240 128 J <25 296 491 90.4 J 1,140 11,100 3,000 NR NR NR NR
07/06/15 975 17,100 3,150 20,300 <82 1,100 <72 <69 <71 140 J <80 <61 427 4,270 1,040 NR NR NR NR
01/27/16 466 15,200 3,460 22,000 <25 2,280 421 166 <25 373 <25 113 1,400 12,600 3,340 NR NR NR NR
09/07/16 716 22,000 5,560 36,000 <63 2,350 370 167 J <63 415 <63 90.4 J 1,530 12,000 3,570 NR NR NR NR
07/24/18 150 6,550 972 6,560 <31 320 <31 <31 <31 47.5 J <31 <31 137 1490 420 NR NR NR NR
09/20/10 5.49 4.12 4.89 17.7 3.04 2.27 J 15.7 <0.280 <0.480 5.70 3.73 <0.400 4.07 5.24 6.11 33.2 496 <100 380
10/27/11 <0.13 0.37 J 0.26 J 1.4 J <0.13 0.24 J 6.9 2.6 <0.10 1.6 <0.11 0.59 0.13 J 0.95 3.2 NR NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/30/13 <0.10 0.16 J 0.85 1.9 <0.10 0.99 5.8 2.7 <0.10 2.2 <0.10 0.81 0.27 J 5.9 9.6 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.34 J 0.91 0.40 J <0.10 <0.10 <0.10 0.25 J <0.10 0.32 J 0.34 J NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 2.5 0.92 <0.14 <0.12 <0.16 0.50 <0.16 <0.14 0.34 J NR NR NR NR
01/27/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 2.8 0.84 <0.13 <0.13 <0.13 0.27 J <0.13 <0.13 0.35 J NR NR NR NR
09/07/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 5.8 1.9 <0.13 <0.13 <0.13 0.26 J <0.13 <0.13 0.45 J NR NR NR NR
07/24/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 4.0 1.4 <0.13 <0.13 <0.13 0.47 J <0.13 <0.13 0.24 J NR NR NR NR
Analytical Method
EPA Method 6200B
MAC (mg/l)
GCL (mg/l)n-ButylbenzeneNaphthaleneContaminant of
Concern
BenzeneTolueneMADEP Method VPH
1,2-DibromoethaneIsopropylbenzeneIPEp-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticssec-ButylbenzeneEthylbenzeneXylenesMTBEMW-2M
MW-1M
TW-1M
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Page 1 of 2
Date : 08/01/18 Facility ID #: 0-022895
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
Analytical Method
EPA Method 6200B
MAC (mg/l)
GCL (mg/l)n-ButylbenzeneNaphthaleneContaminant of
Concern
BenzeneTolueneMADEP Method VPH
1,2-DibromoethaneIsopropylbenzeneIPEp-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromaticssec-ButylbenzeneEthylbenzeneXylenesMTBE TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
09/20/10 1,090 4,890 1,020 3,150 159 J 601 J 439 <56.0 <96.0 1,150 641 <80.0 829 1,030 606 28.8 25,900 5,280 16,900
10/27/11 1,430 12,300 1,610 6,600 158 352 <25 <26 <26 91.4 J 116 J <25 207 1,360 363 NR NR NR NR
01/07/13 1,120 13,500 1,670 7,150 54.8 312 <10 <10 <10 64.6 131 <10 192 1,390 319 NR NR NR NR
07/30/13 472 6,790 1,080 4,000 <25 171 <25 <25 <25 45.6 J 54.3 J <25 131 811 195 NR NR NR NR
06/24/14 161 2,150 288 1,290 12.6 J 37.2 <5.0 <5.0 <5.0 13.3 J 18.9 J <5.0 29.4 276 78.1 NR NR NR NR
07/06/15 220 4,690 564 2,660 <33 98.1 J <29 <28 <28 25.9 J <32 <24 65.3 J 503 134 NR NR NR NR
01/27/16 659 16,600 1,690 7,720 <25 425 <25 <25 <25 72.4 J 60.0 J <25 203 1,430 340 NR NR NR NR
09/07/16 524 17,500 1,970 9,400 <63 334 <63 <63 <63 82.1 J 81.3 J <63 220 J 1,330 363 NR NR NR NR
07/24/18 246 9,980 1,190 5,130 <25 177 <25 <25 <25 46.6 J <25 <25 125 894 237 NR NR NR NR
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the MACs.
• J: Estimated value.
• E: Value exceeds calibration range.
• <: Less than the method detection limit specified in the laboratory report.
• NR: Analysis not requested.
• NS: Not sampled.
MW-3M
• MAC: Maximum allowable concentration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• For other compounds detected that did not exceed the MAC, please refer to the laboratory reports.
Page 2 of 2
Date: 08/14/18 Facility ID #: 0-022895
Well
ID
Date
Collected
(mm/dd/yy)
DO
(mg/l)pH Temperature
(o C)
Conductivity
(mS/cm)
ORP
(mV)
MW-1M 07/24/18 1.98 5.34 19.92 111 99.8
MW-3M 07/24/18 0.73 5.72 19.32 138 15.8
TW-1M 07/24/18 3.92 7.69 21.34 87 111.1
Notes:
TABLE 2A
SUMMARY OF FIELD PARAMETER MEASUREMENTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
1 of 1

APPENDIX B
Laboratory Report – Ground Water Samples
07/31/18
Technical Report for
GRI (Geological Resources Inc.)
Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
11963/2458
SGS Job Number: FA56099
Sampling Date: 07/24/18
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Nicole Long
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 07/31/18
e-Hardcopy 2.0
Automated Report
45
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 45
FA56099
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FA56099-1: MW-1A .....................................................................................................8
3.2: FA56099-2: MW-2 ........................................................................................................10
3.3: FA56099-3: MW-4 ........................................................................................................12
3.4: FA56099-4: MW-5 ........................................................................................................14
3.5: FA56099-5: MW-15 ......................................................................................................16
3.6: FA56099-6: MW-22 ......................................................................................................18
3.7: FA56099-7: MW-25 ......................................................................................................20
3.8: FA56099-8: MW-29 ......................................................................................................22
3.9: FA56099-9: MW-36 ......................................................................................................24
3.10: FA56099-10: MW-43 ..................................................................................................26
3.11: FA56099-11: MW-44 ..................................................................................................28
Section 4: Misc. Forms ............................................................................................................30
4.1: Chain of Custody ...........................................................................................................31
Section 5: MS Volatiles - QC Data Summaries .....................................................................33
5.1: Method Blank Summary ................................................................................................34
5.2: Blank Spike Summary ...................................................................................................38
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................42 123452 of 45
FA56099
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA56099
Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Project No: 11963/2458
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA56099-1 07/24/18 15:00 WR 07/25/18 AQ Water MW-1A
FA56099-2 07/24/18 14:46 WR 07/25/18 AQ Water MW-2
FA56099-3 07/24/18 14:32 WR 07/25/18 AQ Water MW-4
FA56099-4 07/24/18 13:53 WR 07/25/18 AQ Water MW-5
FA56099-5 07/24/18 14:28 WR 07/25/18 AQ Water MW-15
FA56099-6 07/24/18 14:04 WR 07/25/18 AQ Water MW-22
FA56099-7 07/24/18 14:30 WR 07/25/18 AQ Water MW-25
FA56099-8 07/24/18 16:05 WR 07/25/18 AQ Water MW-29
FA56099-9 07/24/18 16:25 WR 07/25/18 AQ Water MW-36
FA56099-10 07/24/18 14:29 WR 07/25/18 AQ Water MW-43
FA56099-11 07/24/18 16:36 WR 07/25/18 AQ Water MW-44
3 of 45
FA560991
Summary of Hits Page 1 of 3
Job Number:FA56099
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:07/24/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA56099-1 MW-1A
Benzene 3460 250 63 ug/l SM 6200B
Ethylbenzene 2360 250 63 ug/l SM 6200B
Isopropylbenzene 103 J 250 63 ug/l SM 6200B
Methyl Tert Butyl Ether 1520 250 63 ug/l SM 6200B
Naphthalene 483 250 63 ug/l SM 6200B
n-Propylbenzene 239 J 250 63 ug/l SM 6200B
Toluene 28200 500 130 ug/l SM 6200B
1,2,3-Trichlorobenzene 140 J 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene 1730 250 63 ug/l SM 6200B
1,3,5-Trimethylbenzene 455 250 63 ug/l SM 6200B
m,p-Xylene 7800 500 63 ug/l SM 6200B
o-Xylene 3830 250 63 ug/l SM 6200B
Xylene (total)11600 750 130 ug/l SM 6200B
FA56099-2 MW-2
Benzene 135 25 6.3 ug/l SM 6200B
Ethylbenzene 230 25 6.3 ug/l SM 6200B
Isopropylbenzene 9.9 J 25 6.3 ug/l SM 6200B
Methyl Tert Butyl Ether 27.8 25 6.3 ug/l SM 6200B
Naphthalene 37.2 25 6.3 ug/l SM 6200B
n-Propylbenzene 23.1 J 25 6.3 ug/l SM 6200B
Toluene 2150 25 6.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 173 25 6.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 45.1 25 6.3 ug/l SM 6200B
m,p-Xylene 689 50 6.3 ug/l SM 6200B
o-Xylene 364 25 6.3 ug/l SM 6200B
Xylene (total)1050 75 13 ug/l SM 6200B
FA56099-3 MW-4
Benzene 115 100 25 ug/l SM 6200B
n-Butylbenzene 58.8 J 100 25 ug/l SM 6200B
sec-Butylbenzene 43.1 J 100 25 ug/l SM 6200B
o-Chlorotoluene 140 100 25 ug/l SM 6200B
Ethylbenzene 2900 100 25 ug/l SM 6200B
Isopropylbenzene 195 100 25 ug/l SM 6200B
Naphthalene 628 100 25 ug/l SM 6200B
n-Propylbenzene 550 100 25 ug/l SM 6200B
Toluene 4380 100 25 ug/l SM 6200B
1,2,4-Trimethylbenzene 4250 100 25 ug/l SM 6200B
1,3,5-Trimethylbenzene 1200 100 25 ug/l SM 6200B
m,p-Xylene 11100 200 25 ug/l SM 6200B
4 of 45
FA560992
Summary of Hits Page 2 of 3
Job Number:FA56099
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:07/24/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
o-Xylene 5050 100 25 ug/l SM 6200B
Xylene (total)16100 300 50 ug/l SM 6200B
FA56099-4 MW-5
Benzene 168 25 6.3 ug/l SM 6200B
o-Chlorotoluene 9.3 J 25 6.3 ug/l SM 6200B
Ethylbenzene 553 25 6.3 ug/l SM 6200B
Isopropylbenzene 37.0 25 6.3 ug/l SM 6200B
Naphthalene 92.2 25 6.3 ug/l SM 6200B
n-Propylbenzene 55.1 25 6.3 ug/l SM 6200B
Toluene 1860 25 6.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 239 25 6.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 85.3 25 6.3 ug/l SM 6200B
m,p-Xylene 1400 50 6.3 ug/l SM 6200B
o-Xylene 533 25 6.3 ug/l SM 6200B
Xylene (total)1930 75 13 ug/l SM 6200B
FA56099-5 MW-15
Benzene 41.8 5.0 1.3 ug/l SM 6200B
n-Butylbenzene 5.2 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene 5.0 5.0 1.3 ug/l SM 6200B
o-Chlorotoluene 8.3 5.0 1.3 ug/l SM 6200B
Ethylbenzene 229 5.0 1.3 ug/l SM 6200B
Isopropylbenzene 26.5 5.0 1.3 ug/l SM 6200B
p-Isopropyltoluene 6.0 5.0 1.3 ug/l SM 6200B
Naphthalene 81.3 5.0 1.3 ug/l SM 6200B
n-Propylbenzene 41.9 5.0 1.3 ug/l SM 6200B
Toluene 249 5.0 1.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 201 5.0 1.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 73.5 5.0 1.3 ug/l SM 6200B
m,p-Xylene 584 10 1.3 ug/l SM 6200B
o-Xylene 224 5.0 1.3 ug/l SM 6200B
Xylene (total)808 15 2.5 ug/l SM 6200B
FA56099-6 MW-22
Benzene 5.4 5.0 1.3 ug/l SM 6200B
n-Butylbenzene 16.6 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene 12.7 5.0 1.3 ug/l SM 6200B
o-Chlorotoluene 26.7 5.0 1.3 ug/l SM 6200B
Ethylbenzene 421 5.0 1.3 ug/l SM 6200B
Isopropylbenzene 58.6 5.0 1.3 ug/l SM 6200B
p-Isopropyltoluene 8.5 5.0 1.3 ug/l SM 6200B
5 of 45
FA560992
Summary of Hits Page 3 of 3
Job Number:FA56099
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:07/24/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Naphthalene 90.6 5.0 1.3 ug/l SM 6200B
n-Propylbenzene 165 5.0 1.3 ug/l SM 6200B
Styrene 3.8 J 5.0 1.3 ug/l SM 6200B
Toluene 26.0 5.0 1.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 954 13 3.1 ug/l SM 6200B
1,3,5-Trimethylbenzene 241 5.0 1.3 ug/l SM 6200B
m,p-Xylene 1210 25 3.1 ug/l SM 6200B
o-Xylene 192 5.0 1.3 ug/l SM 6200B
Xylene (total)1390 38 6.3 ug/l SM 6200B
FA56099-7 MW-25
No hits reported in this sample.
FA56099-8 MW-29
Benzene 677 13 3.1 ug/l SM 6200B
o-Chlorotoluene 8.7 J 13 3.1 ug/l SM 6200B
Ethylbenzene 409 13 3.1 ug/l SM 6200B
Isopropylbenzene 20.3 13 3.1 ug/l SM 6200B
Methyl Chloride 11.7 J 13 5.0 ug/l SM 6200B
Methyl Tert Butyl Ether 627 13 3.1 ug/l SM 6200B
Naphthalene 81.7 13 3.1 ug/l SM 6200B
n-Propylbenzene 39.3 13 3.1 ug/l SM 6200B
Styrene 4.2 J 13 3.1 ug/l SM 6200B
Toluene 291 13 3.1 ug/l SM 6200B
1,2,4-Trimethylbenzene 312 13 3.1 ug/l SM 6200B
1,3,5-Trimethylbenzene 75.5 13 3.1 ug/l SM 6200B
m,p-Xylene 1210 25 3.1 ug/l SM 6200B
o-Xylene 590 13 3.1 ug/l SM 6200B
Xylene (total)1800 38 6.3 ug/l SM 6200B
FA56099-9 MW-36
Methyl Tert Butyl Ether 1.0 0.50 0.13 ug/l SM 6200B
FA56099-10 MW-43
No hits reported in this sample.
FA56099-11 MW-44
No hits reported in this sample.
6 of 45
FA560992
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
7 of 45
FA560993
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-1A
Lab Sample ID:FA56099-1 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E059542.D 500 07/27/18 16:20 AB n/a n/a VE2007
Run #2 A0214788.D 1000 07/30/18 11:58 AB n/a n/a VA2434
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3460 250 63 ug/l
108-86-1 Bromobenzene ND 250 63 ug/l
74-97-5 Bromochloromethane ND 250 63 ug/l
75-27-4 Bromodichloromethane ND 250 63 ug/l
75-25-2 Bromoform ND 250 63 ug/l
104-51-8 n-Butylbenzene ND 250 63 ug/l
135-98-8 sec-Butylbenzene ND 250 63 ug/l
98-06-6 tert-Butylbenzene ND 250 63 ug/l
56-23-5 Carbon Tetrachloride ND 250 63 ug/l
108-90-7 Chlorobenzene ND 250 63 ug/l
75-00-3 Chloroethane ND 250 100 ug/l
67-66-3 Chloroform ND 250 63 ug/l
95-49-8 o-Chlorotoluene ND 250 63 ug/l
106-43-4 p-Chlorotoluene ND 250 63 ug/l
124-48-1 Dibromochloromethane ND 250 63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 250 120 ug/l
106-93-4 1,2-Dibromoethane ND 250 63 ug/l
75-71-8 Dichlorodifluoromethane ND 250 100 ug/l
95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l
541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l
106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l
75-34-3 1,1-Dichloroethane ND 250 63 ug/l
107-06-2 1,2-Dichloroethane ND 250 63 ug/l
75-35-4 1,1-Dichloroethylene ND 250 63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l
78-87-5 1,2-Dichloropropane ND 250 63 ug/l
142-28-9 1,3-Dichloropropane ND 250 63 ug/l
594-20-7 2,2-Dichloropropane ND 250 63 ug/l
563-58-6 1,1-Dichloropropene ND 250 63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 45
FA5609933.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-1A
Lab Sample ID:FA56099-1 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 250 63 ug/l
100-41-4 Ethylbenzene 2360 250 63 ug/l
87-68-3 Hexachlorobutadiene ND 250 63 ug/l
98-82-8 Isopropylbenzene 103 250 63 ug/l J
99-87-6 p-Isopropyltoluene ND 250 63 ug/l
74-83-9 Methyl Bromide ND 250 100 ug/l
74-87-3 Methyl Chloride ND 250 100 ug/l
74-95-3 Methylene Bromide ND 250 63 ug/l
75-09-2 Methylene Chloride ND 1000 500 ug/l
1634-04-4 Methyl Tert Butyl Ether 1520 250 63 ug/l
91-20-3 Naphthalene 483 250 63 ug/l
103-65-1 n-Propylbenzene 239 250 63 ug/l J
100-42-5 Styrene ND 250 63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l
127-18-4 Tetrachloroethylene ND 250 63 ug/l
108-88-3 Toluene 28200 a 500 130 ug/l
87-61-6 1,2,3-Trichlorobenzene 140 250 63 ug/l J
120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l
71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l
79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l
79-01-6 Trichloroethylene ND 250 63 ug/l
75-69-4 Trichlorofluoromethane ND 250 100 ug/l
96-18-4 1,2,3-Trichloropropane ND 250 63 ug/l
95-63-6 1,2,4-Trimethylbenzene 1730 250 63 ug/l
108-67-8 1,3,5-Trimethylbenzene 455 250 63 ug/l
75-01-4 Vinyl Chloride ND 250 63 ug/l
m,p-Xylene 7800 500 63 ug/l
95-47-6 o-Xylene 3830 250 63 ug/l
1330-20-7 Xylene (total)11600 750 130 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%107%70-130%
2037-26-5 Toluene-D8 101%101%70-130%
460-00-4 4-Bromofluorobenzene 102%99%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 45
FA5609933.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA56099-2 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E059552.D 50 07/27/18 20:33 AB n/a n/a VE2007
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 135 25 6.3 ug/l
108-86-1 Bromobenzene ND 25 6.3 ug/l
74-97-5 Bromochloromethane ND 25 6.3 ug/l
75-27-4 Bromodichloromethane ND 25 6.3 ug/l
75-25-2 Bromoform ND 25 6.3 ug/l
104-51-8 n-Butylbenzene ND 25 6.3 ug/l
135-98-8 sec-Butylbenzene ND 25 6.3 ug/l
98-06-6 tert-Butylbenzene ND 25 6.3 ug/l
56-23-5 Carbon Tetrachloride ND 25 6.3 ug/l
108-90-7 Chlorobenzene ND 25 6.3 ug/l
75-00-3 Chloroethane ND 25 10 ug/l
67-66-3 Chloroform ND 25 6.3 ug/l
95-49-8 o-Chlorotoluene ND 25 6.3 ug/l
106-43-4 p-Chlorotoluene ND 25 6.3 ug/l
124-48-1 Dibromochloromethane ND 25 6.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 25 12 ug/l
106-93-4 1,2-Dibromoethane ND 25 6.3 ug/l
75-71-8 Dichlorodifluoromethane ND 25 10 ug/l
95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l
75-34-3 1,1-Dichloroethane ND 25 6.3 ug/l
107-06-2 1,2-Dichloroethane ND 25 6.3 ug/l
75-35-4 1,1-Dichloroethylene ND 25 6.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 25 6.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 25 6.3 ug/l
78-87-5 1,2-Dichloropropane ND 25 6.3 ug/l
142-28-9 1,3-Dichloropropane ND 25 6.3 ug/l
594-20-7 2,2-Dichloropropane ND 25 6.3 ug/l
563-58-6 1,1-Dichloropropene ND 25 6.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 25 6.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 45
FA5609933.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA56099-2 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 25 6.3 ug/l
100-41-4 Ethylbenzene 230 25 6.3 ug/l
87-68-3 Hexachlorobutadiene ND 25 6.3 ug/l
98-82-8 Isopropylbenzene 9.9 25 6.3 ug/l J
99-87-6 p-Isopropyltoluene ND 25 6.3 ug/l
74-83-9 Methyl Bromide ND 25 10 ug/l
74-87-3 Methyl Chloride ND 25 10 ug/l
74-95-3 Methylene Bromide ND 25 6.3 ug/l
75-09-2 Methylene Chloride ND 100 50 ug/l
1634-04-4 Methyl Tert Butyl Ether 27.8 25 6.3 ug/l
91-20-3 Naphthalene 37.2 25 6.3 ug/l
103-65-1 n-Propylbenzene 23.1 25 6.3 ug/l J
100-42-5 Styrene ND 25 6.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 25 6.3 ug/l
127-18-4 Tetrachloroethylene ND 25 6.3 ug/l
108-88-3 Toluene 2150 25 6.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 25 6.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 6.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 25 6.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 25 6.3 ug/l
79-01-6 Trichloroethylene ND 25 6.3 ug/l
75-69-4 Trichlorofluoromethane ND 25 10 ug/l
96-18-4 1,2,3-Trichloropropane ND 25 6.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 173 25 6.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 45.1 25 6.3 ug/l
75-01-4 Vinyl Chloride ND 25 6.3 ug/l
m,p-Xylene 689 50 6.3 ug/l
95-47-6 o-Xylene 364 25 6.3 ug/l
1330-20-7 Xylene (total)1050 75 13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 45
FA5609933.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:FA56099-3 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E059543.D 200 07/27/18 16:46 AB n/a n/a VE2007
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 115 100 25 ug/l
108-86-1 Bromobenzene ND 100 25 ug/l
74-97-5 Bromochloromethane ND 100 25 ug/l
75-27-4 Bromodichloromethane ND 100 25 ug/l
75-25-2 Bromoform ND 100 25 ug/l
104-51-8 n-Butylbenzene 58.8 100 25 ug/l J
135-98-8 sec-Butylbenzene 43.1 100 25 ug/l J
98-06-6 tert-Butylbenzene ND 100 25 ug/l
56-23-5 Carbon Tetrachloride ND 100 25 ug/l
108-90-7 Chlorobenzene ND 100 25 ug/l
75-00-3 Chloroethane ND 100 40 ug/l
67-66-3 Chloroform ND 100 25 ug/l
95-49-8 o-Chlorotoluene 140 100 25 ug/l
106-43-4 p-Chlorotoluene ND 100 25 ug/l
124-48-1 Dibromochloromethane ND 100 25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 100 49 ug/l
106-93-4 1,2-Dibromoethane ND 100 25 ug/l
75-71-8 Dichlorodifluoromethane ND 100 40 ug/l
95-50-1 1,2-Dichlorobenzene ND 100 25 ug/l
541-73-1 1,3-Dichlorobenzene ND 100 25 ug/l
106-46-7 1,4-Dichlorobenzene ND 100 25 ug/l
75-34-3 1,1-Dichloroethane ND 100 25 ug/l
107-06-2 1,2-Dichloroethane ND 100 25 ug/l
75-35-4 1,1-Dichloroethylene ND 100 25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 100 25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 100 25 ug/l
78-87-5 1,2-Dichloropropane ND 100 25 ug/l
142-28-9 1,3-Dichloropropane ND 100 25 ug/l
594-20-7 2,2-Dichloropropane ND 100 25 ug/l
563-58-6 1,1-Dichloropropene ND 100 25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 100 25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 100 25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 45
FA5609933.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-4
Lab Sample ID:FA56099-3 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 100 25 ug/l
100-41-4 Ethylbenzene 2900 100 25 ug/l
87-68-3 Hexachlorobutadiene ND 100 25 ug/l
98-82-8 Isopropylbenzene 195 100 25 ug/l
99-87-6 p-Isopropyltoluene ND 100 25 ug/l
74-83-9 Methyl Bromide ND 100 40 ug/l
74-87-3 Methyl Chloride ND 100 40 ug/l
74-95-3 Methylene Bromide ND 100 25 ug/l
75-09-2 Methylene Chloride ND 400 200 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 100 25 ug/l
91-20-3 Naphthalene 628 100 25 ug/l
103-65-1 n-Propylbenzene 550 100 25 ug/l
100-42-5 Styrene ND 100 25 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 100 25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 100 25 ug/l
127-18-4 Tetrachloroethylene ND 100 25 ug/l
108-88-3 Toluene 4380 100 25 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 100 25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 100 25 ug/l
71-55-6 1,1,1-Trichloroethane ND 100 25 ug/l
79-00-5 1,1,2-Trichloroethane ND 100 25 ug/l
79-01-6 Trichloroethylene ND 100 25 ug/l
75-69-4 Trichlorofluoromethane ND 100 40 ug/l
96-18-4 1,2,3-Trichloropropane ND 100 25 ug/l
95-63-6 1,2,4-Trimethylbenzene 4250 100 25 ug/l
108-67-8 1,3,5-Trimethylbenzene 1200 100 25 ug/l
75-01-4 Vinyl Chloride ND 100 25 ug/l
m,p-Xylene 11100 200 25 ug/l
95-47-6 o-Xylene 5050 100 25 ug/l
1330-20-7 Xylene (total)16100 300 50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 45
FA5609933.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA56099-4 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0214789.D 50 07/30/18 12:21 AB n/a n/a VA2434
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 168 25 6.3 ug/l
108-86-1 Bromobenzene ND 25 6.3 ug/l
74-97-5 Bromochloromethane ND 25 6.3 ug/l
75-27-4 Bromodichloromethane ND 25 6.3 ug/l
75-25-2 Bromoform ND 25 6.3 ug/l
104-51-8 n-Butylbenzene ND 25 6.3 ug/l
135-98-8 sec-Butylbenzene ND 25 6.3 ug/l
98-06-6 tert-Butylbenzene ND 25 6.3 ug/l
56-23-5 Carbon Tetrachloride ND 25 6.3 ug/l
108-90-7 Chlorobenzene ND 25 6.3 ug/l
75-00-3 Chloroethane ND 25 10 ug/l
67-66-3 Chloroform ND 25 6.3 ug/l
95-49-8 o-Chlorotoluene 9.3 25 6.3 ug/l J
106-43-4 p-Chlorotoluene ND 25 6.3 ug/l
124-48-1 Dibromochloromethane ND 25 6.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 25 12 ug/l
106-93-4 1,2-Dibromoethane ND 25 6.3 ug/l
75-71-8 Dichlorodifluoromethane ND 25 10 ug/l
95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l
75-34-3 1,1-Dichloroethane ND 25 6.3 ug/l
107-06-2 1,2-Dichloroethane ND 25 6.3 ug/l
75-35-4 1,1-Dichloroethylene ND 25 6.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 25 6.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 25 6.3 ug/l
78-87-5 1,2-Dichloropropane ND 25 6.3 ug/l
142-28-9 1,3-Dichloropropane ND 25 6.3 ug/l
594-20-7 2,2-Dichloropropane ND 25 6.3 ug/l
563-58-6 1,1-Dichloropropene ND 25 6.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 25 6.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 45
FA5609933.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA56099-4 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 25 6.3 ug/l
100-41-4 Ethylbenzene 553 25 6.3 ug/l
87-68-3 Hexachlorobutadiene ND 25 6.3 ug/l
98-82-8 Isopropylbenzene 37.0 25 6.3 ug/l
99-87-6 p-Isopropyltoluene ND 25 6.3 ug/l
74-83-9 Methyl Bromide ND 25 10 ug/l
74-87-3 Methyl Chloride ND 25 10 ug/l
74-95-3 Methylene Bromide ND 25 6.3 ug/l
75-09-2 Methylene Chloride ND 100 50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 25 6.3 ug/l
91-20-3 Naphthalene 92.2 25 6.3 ug/l
103-65-1 n-Propylbenzene 55.1 25 6.3 ug/l
100-42-5 Styrene ND 25 6.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 25 6.3 ug/l
127-18-4 Tetrachloroethylene ND 25 6.3 ug/l
108-88-3 Toluene 1860 25 6.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 25 6.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 6.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 25 6.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 25 6.3 ug/l
79-01-6 Trichloroethylene ND 25 6.3 ug/l
75-69-4 Trichlorofluoromethane ND 25 10 ug/l
96-18-4 1,2,3-Trichloropropane ND 25 6.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 239 25 6.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 85.3 25 6.3 ug/l
75-01-4 Vinyl Chloride ND 25 6.3 ug/l
m,p-Xylene 1400 50 6.3 ug/l
95-47-6 o-Xylene 533 25 6.3 ug/l
1330-20-7 Xylene (total)1930 75 13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 45
FA5609933.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-15
Lab Sample ID:FA56099-5 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0214790.D 10 07/30/18 12:45 AB n/a n/a VA2434
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 41.8 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene 5.2 5.0 1.3 ug/l
135-98-8 sec-Butylbenzene 5.0 5.0 1.3 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene 8.3 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.3 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 45
FA5609933.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-15
Lab Sample ID:FA56099-5 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 5.0 1.3 ug/l
100-41-4 Ethylbenzene 229 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 26.5 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene 6.0 5.0 1.3 ug/l
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.3 ug/l
91-20-3 Naphthalene 81.3 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 41.9 5.0 1.3 ug/l
100-42-5 Styrene ND 5.0 1.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 249 5.0 1.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 201 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 73.5 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 584 10 1.3 ug/l
95-47-6 o-Xylene 224 5.0 1.3 ug/l
1330-20-7 Xylene (total)808 15 2.5 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 45
FA5609933.5
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-22
Lab Sample ID:FA56099-6 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E059546.D 10 07/27/18 18:02 AB n/a n/a VE2007
Run #2 A0214791.D 25 07/30/18 13:08 AB n/a n/a VA2434
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 5.4 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene 16.6 5.0 1.3 ug/l
135-98-8 sec-Butylbenzene 12.7 5.0 1.3 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene 26.7 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane ND 5.0 1.3 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 45
FA5609933.6
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-22
Lab Sample ID:FA56099-6 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 5.0 1.3 ug/l
100-41-4 Ethylbenzene 421 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 58.6 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene 8.5 5.0 1.3 ug/l
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.3 ug/l
91-20-3 Naphthalene 90.6 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 165 5.0 1.3 ug/l
100-42-5 Styrene 3.8 5.0 1.3 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 26.0 5.0 1.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 954 a 13 3.1 ug/l
108-67-8 1,3,5-Trimethylbenzene 241 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 1210 a 25 3.1 ug/l
95-47-6 o-Xylene 192 5.0 1.3 ug/l
1330-20-7 Xylene (total)1390 a 38 6.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%109%70-130%
2037-26-5 Toluene-D8 101%99%70-130%
460-00-4 4-Bromofluorobenzene 98%97%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 45
FA5609933.6
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-25
Lab Sample ID:FA56099-7 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0214785.D 1 07/30/18 10:48 AB n/a n/a VA2434
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 45
FA5609933.7
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-25
Lab Sample ID:FA56099-7 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 45
FA5609933.7
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-29
Lab Sample ID:FA56099-8 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E059548.D 25 07/27/18 18:53 AB n/a n/a VE2007
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 677 13 3.1 ug/l
108-86-1 Bromobenzene ND 13 3.1 ug/l
74-97-5 Bromochloromethane ND 13 3.1 ug/l
75-27-4 Bromodichloromethane ND 13 3.1 ug/l
75-25-2 Bromoform ND 13 3.1 ug/l
104-51-8 n-Butylbenzene ND 13 3.1 ug/l
135-98-8 sec-Butylbenzene ND 13 3.1 ug/l
98-06-6 tert-Butylbenzene ND 13 3.1 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.1 ug/l
108-90-7 Chlorobenzene ND 13 3.1 ug/l
75-00-3 Chloroethane ND 13 5.0 ug/l
67-66-3 Chloroform ND 13 3.1 ug/l
95-49-8 o-Chlorotoluene 8.7 13 3.1 ug/l J
106-43-4 p-Chlorotoluene ND 13 3.1 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 6.2 ug/l
106-93-4 1,2-Dibromoethane ND 13 3.1 ug/l
75-71-8 Dichlorodifluoromethane ND 13 5.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.1 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.1 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.1 ug/l
75-34-3 1,1-Dichloroethane ND 13 3.1 ug/l
107-06-2 1,2-Dichloroethane ND 13 3.1 ug/l
75-35-4 1,1-Dichloroethylene ND 13 3.1 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 3.1 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 3.1 ug/l
78-87-5 1,2-Dichloropropane ND 13 3.1 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.1 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.1 ug/l
563-58-6 1,1-Dichloropropene ND 13 3.1 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 3.1 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 13 3.1 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 45
FA5609933.8
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-29
Lab Sample ID:FA56099-8 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 13 3.1 ug/l
100-41-4 Ethylbenzene 409 13 3.1 ug/l
87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l
98-82-8 Isopropylbenzene 20.3 13 3.1 ug/l
99-87-6 p-Isopropyltoluene ND 13 3.1 ug/l
74-83-9 Methyl Bromide ND 13 5.0 ug/l
74-87-3 Methyl Chloride 11.7 13 5.0 ug/l J
74-95-3 Methylene Bromide ND 13 3.1 ug/l
75-09-2 Methylene Chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether 627 13 3.1 ug/l
91-20-3 Naphthalene 81.7 13 3.1 ug/l
103-65-1 n-Propylbenzene 39.3 13 3.1 ug/l
100-42-5 Styrene 4.2 13 3.1 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.1 ug/l
127-18-4 Tetrachloroethylene ND 13 3.1 ug/l
108-88-3 Toluene 291 13 3.1 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.1 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.1 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 3.1 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.1 ug/l
79-01-6 Trichloroethylene ND 13 3.1 ug/l
75-69-4 Trichlorofluoromethane ND 13 5.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.1 ug/l
95-63-6 1,2,4-Trimethylbenzene 312 13 3.1 ug/l
108-67-8 1,3,5-Trimethylbenzene 75.5 13 3.1 ug/l
75-01-4 Vinyl Chloride ND 13 3.1 ug/l
m,p-Xylene 1210 25 3.1 ug/l
95-47-6 o-Xylene 590 13 3.1 ug/l
1330-20-7 Xylene (total)1800 38 6.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 45
FA5609933.8
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-36
Lab Sample ID:FA56099-9 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E059549.D 1 07/27/18 19:18 AB n/a n/a VE2007
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 45
FA5609933.9
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-36
Lab Sample ID:FA56099-9 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.0 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 45
FA5609933.9
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-43
Lab Sample ID:FA56099-10 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E059550.D 1 07/27/18 19:43 AB n/a n/a VE2007
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 45
FA5609933.10
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-43
Lab Sample ID:FA56099-10 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 45
FA5609933.10
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-44
Lab Sample ID:FA56099-11 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E059551.D 1 07/27/18 20:08 AB n/a n/a VE2007
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 45
FA5609933.11
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-44
Lab Sample ID:FA56099-11 Date Sampled:07/24/18
Matrix:AQ - Water Date Received:07/25/18
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 45
FA5609933.11
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
30 of 45
FA560994
FA56099: Chain of Custody
Page 1 of 2
31 of 45
FA5609944.1
Job Number:FA56099 Client:GRI
Date / Time Received:7/25/2018 9:00:00 AM Delivery Method:FED EX
Project:TODD'S/ BOWENS
Airbill #'s:1015899923610003281100812565568268
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (4.1);
Cooler 1: (4.2);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.1; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP SP Date:7/25/2018Date:7/25/2018 9:00:00 AM
FA56099: Chain of Custody
Page 2 of 2
32 of 45
FA5609944.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
33 of 45
FA560995
Method Blank Summary Page 1 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2007-MB E059529.D 1 07/27/18 AB n/a n/a VE2007
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-2, FA56099-3, FA56099-6, FA56099-8, FA56099-9, FA56099-10, FA56099-11
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
34 of 45
FA5609955.1.1
Method Blank Summary Page 2 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2007-MB E059529.D 1 07/27/18 AB n/a n/a VE2007
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-2, FA56099-3, FA56099-6, FA56099-8, FA56099-9, FA56099-10, FA56099-11
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
35 of 45
FA5609955.1.1
Method Blank Summary Page 1 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2434-MB A0214784.D 1 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-4, FA56099-5, FA56099-6, FA56099-7
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
36 of 45
FA5609955.1.2
Method Blank Summary Page 2 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2434-MB A0214784.D 1 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-4, FA56099-5, FA56099-6, FA56099-7
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
37 of 45
FA5609955.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2007-BS E059527.D 1 07/27/18 AB n/a n/a VE2007
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-2, FA56099-3, FA56099-6, FA56099-8, FA56099-9, FA56099-10, FA56099-11
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.8 98 70-130
108-86-1 Bromobenzene 10 9.5 95 70-130
74-97-5 Bromochloromethane 10 9.0 90 70-130
75-27-4 Bromodichloromethane 10 9.7 97 70-130
75-25-2 Bromoform 10 8.7 87 70-130
104-51-8 n-Butylbenzene 10 10.4 104 70-130
135-98-8 sec-Butylbenzene 10 10.3 103 70-130
98-06-6 tert-Butylbenzene 10 9.9 99 70-130
56-23-5 Carbon Tetrachloride 10 10.3 103 70-130
108-90-7 Chlorobenzene 10 9.8 98 70-130
75-00-3 Chloroethane 10 9.4 94 60-140
67-66-3 Chloroform 10 9.7 97 70-130
95-49-8 o-Chlorotoluene 10 9.8 98 70-130
106-43-4 p-Chlorotoluene 10 9.7 97 70-130
124-48-1 Dibromochloromethane 10 9.2 92 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.3 93 70-130
106-93-4 1,2-Dibromoethane 10 9.2 92 70-130
75-71-8 Dichlorodifluoromethane 10 9.0 90 60-140
95-50-1 1,2-Dichlorobenzene 10 9.4 94 70-130
541-73-1 1,3-Dichlorobenzene 10 9.8 98 70-130
106-46-7 1,4-Dichlorobenzene 10 9.4 94 70-130
75-34-3 1,1-Dichloroethane 10 10.2 102 70-130
107-06-2 1,2-Dichloroethane 10 9.6 96 70-130
75-35-4 1,1-Dichloroethylene 10 10.1 101 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.7 97 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.9 99 70-130
78-87-5 1,2-Dichloropropane 10 9.7 97 70-130
142-28-9 1,3-Dichloropropane 10 9.0 90 70-130
594-20-7 2,2-Dichloropropane 10 10.8 108 70-130
563-58-6 1,1-Dichloropropene 10 10.2 102 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.2 92 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.4 94 70-130
108-20-3 Di-Isopropyl Ether 10 9.2 92 70-130
100-41-4 Ethylbenzene 10 10.1 101 70-130
87-68-3 Hexachlorobutadiene 10 9.7 97 70-130
98-82-8 Isopropylbenzene 10 10.6 106 70-130
* = Outside of Control Limits.
38 of 45
FA5609955.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2007-BS E059527.D 1 07/27/18 AB n/a n/a VE2007
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-2, FA56099-3, FA56099-6, FA56099-8, FA56099-9, FA56099-10, FA56099-11
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.2 102 70-130
74-83-9 Methyl Bromide 10 9.8 98 60-140
74-87-3 Methyl Chloride 10 10.2 102 60-140
74-95-3 Methylene Bromide 10 9.3 93 70-130
75-09-2 Methylene Chloride 10 10.3 103 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.1 91 70-130
91-20-3 Naphthalene 10 9.4 94 70-130
103-65-1 n-Propylbenzene 10 10.0 100 70-130
100-42-5 Styrene 10 9.8 98 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.5 95 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.5 95 70-130
127-18-4 Tetrachloroethylene 10 10.2 102 70-130
108-88-3 Toluene 10 9.9 99 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.7 97 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.6 96 70-130
71-55-6 1,1,1-Trichloroethane 10 10 100 70-130
79-00-5 1,1,2-Trichloroethane 10 9.6 96 70-130
79-01-6 Trichloroethylene 10 9.9 99 70-130
75-69-4 Trichlorofluoromethane 10 10.0 100 60-140
96-18-4 1,2,3-Trichloropropane 10 9.1 91 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.5 95 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.0 100 70-130
75-01-4 Vinyl Chloride 10 8.9 89 60-140
m,p-Xylene 20 20.2 101 70-130
95-47-6 o-Xylene 10 9.8 98 70-130
1330-20-7 Xylene (total)30 29.9 100 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
39 of 45
FA5609955.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2434-BS A0214782.D 1 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-4, FA56099-5, FA56099-6, FA56099-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.5 95 70-130
108-86-1 Bromobenzene 10 8.3 83 70-130
74-97-5 Bromochloromethane 10 8.2 82 70-130
75-27-4 Bromodichloromethane 10 9.1 91 70-130
75-25-2 Bromoform 10 8.0 80 70-130
104-51-8 n-Butylbenzene 10 9.0 90 70-130
135-98-8 sec-Butylbenzene 10 9.4 94 70-130
98-06-6 tert-Butylbenzene 10 9.0 90 70-130
56-23-5 Carbon Tetrachloride 10 10.1 101 70-130
108-90-7 Chlorobenzene 10 9.0 90 70-130
75-00-3 Chloroethane 10 11.2 112 60-140
67-66-3 Chloroform 10 9.3 93 70-130
95-49-8 o-Chlorotoluene 10 9.2 92 70-130
106-43-4 p-Chlorotoluene 10 8.5 85 70-130
124-48-1 Dibromochloromethane 10 8.2 82 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.9 79 70-130
106-93-4 1,2-Dibromoethane 10 7.9 79 70-130
75-71-8 Dichlorodifluoromethane 10 8.2 82 60-140
95-50-1 1,2-Dichlorobenzene 10 8.2 82 70-130
541-73-1 1,3-Dichlorobenzene 10 8.9 89 70-130
106-46-7 1,4-Dichlorobenzene 10 8.6 86 70-130
75-34-3 1,1-Dichloroethane 10 9.9 99 70-130
107-06-2 1,2-Dichloroethane 10 9.4 94 70-130
75-35-4 1,1-Dichloroethylene 10 10.2 102 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.1 91 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.9 99 70-130
78-87-5 1,2-Dichloropropane 10 9.4 94 70-130
142-28-9 1,3-Dichloropropane 10 8.2 82 70-130
594-20-7 2,2-Dichloropropane 10 9.4 94 70-130
563-58-6 1,1-Dichloropropene 10 9.9 99 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.4 84 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.5 85 70-130
108-20-3 Di-Isopropyl Ether 10 9.0 90 70-130
100-41-4 Ethylbenzene 10 9.2 92 70-130
87-68-3 Hexachlorobutadiene 10 8.8 88 70-130
98-82-8 Isopropylbenzene 10 9.6 96 70-130
* = Outside of Control Limits.
40 of 45
FA5609955.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2434-BS A0214782.D 1 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-4, FA56099-5, FA56099-6, FA56099-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.0 90 70-130
74-83-9 Methyl Bromide 10 11.3 113 60-140
74-87-3 Methyl Chloride 10 10.3 103 60-140
74-95-3 Methylene Bromide 10 9.4 94 70-130
75-09-2 Methylene Chloride 10 9.7 97 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.8 88 70-130
91-20-3 Naphthalene 10 7.5 75 70-130
103-65-1 n-Propylbenzene 10 9.2 92 70-130
100-42-5 Styrene 10 8.2 82 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.3 83 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.3 83 70-130
127-18-4 Tetrachloroethylene 10 9.3 93 70-130
108-88-3 Toluene 10 9.1 91 70-130
87-61-6 1,2,3-Trichlorobenzene 10 7.9 79 70-130
120-82-1 1,2,4-Trichlorobenzene 10 7.9 79 70-130
71-55-6 1,1,1-Trichloroethane 10 9.4 94 70-130
79-00-5 1,1,2-Trichloroethane 10 8.2 82 70-130
79-01-6 Trichloroethylene 10 9.4 94 70-130
75-69-4 Trichlorofluoromethane 10 11.2 112 60-140
96-18-4 1,2,3-Trichloropropane 10 8.0 80 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.4 84 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.3 93 70-130
75-01-4 Vinyl Chloride 10 9.5 95 60-140
m,p-Xylene 20 18.6 93 70-130
95-47-6 o-Xylene 10 9.0 90 70-130
1330-20-7 Xylene (total)30 27.6 92 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
41 of 45
FA5609955.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA56099-2MS E059540.D 100 07/27/18 AB n/a n/a VE2007
FA56099-2MSD E059541.D 100 07/27/18 AB n/a n/a VE2007
FA56099-2 E059552.D 50 07/27/18 AB n/a n/a VE2007
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-2, FA56099-3, FA56099-6, FA56099-8, FA56099-9, FA56099-10, FA56099-11
FA56099-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 135 1000 1120 98 1000 1140 100 2 70-130/20
108-86-1 Bromobenzene ND 1000 941 94 1000 989 99 5 70-130/20
74-97-5 Bromochloromethane ND 1000 901 90 1000 929 93 3 70-130/20
75-27-4 Bromodichloromethane ND 1000 966 97 1000 994 99 3 70-130/20
75-25-2 Bromoform ND 1000 821 82 1000 826 83 1 70-130/20
104-51-8 n-Butylbenzene ND 1000 1040 104 1000 1070 107 3 70-130/20
135-98-8 sec-Butylbenzene ND 1000 1030 103 1000 1070 107 4 70-130/20
98-06-6 tert-Butylbenzene ND 1000 993 99 1000 1020 102 3 70-130/20
56-23-5 Carbon Tetrachloride ND 1000 1010 101 1000 1030 103 2 70-130/20
108-90-7 Chlorobenzene ND 1000 986 99 1000 1010 101 2 70-130/20
75-00-3 Chloroethane ND 1000 1020 102 1000 1050 105 3 60-140/20
67-66-3 Chloroform ND 1000 1020 102 1000 1040 104 2 70-130/20
95-49-8 o-Chlorotoluene ND 1000 992 99 1000 1030 103 4 70-130/20
106-43-4 p-Chlorotoluene ND 1000 969 97 1000 1000 100 3 70-130/20
124-48-1 Dibromochloromethane ND 1000 904 90 1000 925 93 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 936 94 1000 935 94 0 70-130/20
106-93-4 1,2-Dibromoethane ND 1000 915 92 1000 940 94 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 1050 105 1000 1070 107 2 60-140/20
95-50-1 1,2-Dichlorobenzene ND 1000 948 95 1000 978 98 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 1000 982 98 1000 1010 101 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 1000 948 95 1000 974 97 3 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 1010 101 1000 1030 103 2 70-130/20
107-06-2 1,2-Dichloroethane ND 1000 980 98 1000 993 99 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 1010 101 1000 1030 103 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 970 97 1000 995 100 3 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 983 98 1000 996 100 1 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 972 97 1000 991 99 2 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 904 90 1000 935 94 3 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 1030 103 1000 1040 104 1 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 1010 101 1000 1030 103 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 902 90 1000 927 93 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 908 91 1000 932 93 3 70-130/20
108-20-3 Di-Isopropyl Ether ND 1000 909 91 1000 928 93 2 70-130/20
100-41-4 Ethylbenzene 230 1000 1240 100 1000 1260 102 2 70-130/20
87-68-3 Hexachlorobutadiene ND 1000 944 94 1000 974 97 3 70-130/20
98-82-8 Isopropylbenzene 9.9 J 1000 1050 105 1000 1080 108 3 70-130/20
* = Outside of Control Limits.
42 of 45
FA5609955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA56099-2MS E059540.D 100 07/27/18 AB n/a n/a VE2007
FA56099-2MSD E059541.D 100 07/27/18 AB n/a n/a VE2007
FA56099-2 E059552.D 50 07/27/18 AB n/a n/a VE2007
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-2, FA56099-3, FA56099-6, FA56099-8, FA56099-9, FA56099-10, FA56099-11
FA56099-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 1000 1020 102 1000 1050 105 3 70-130/20
74-83-9 Methyl Bromide ND 1000 1100 110 1000 1140 114 4 60-140/20
74-87-3 Methyl Chloride ND 1000 1180 118 1000 1160 116 2 60-140/20
74-95-3 Methylene Bromide ND 1000 941 94 1000 968 97 3 70-130/20
75-09-2 Methylene Chloride ND 1000 1030 103 1000 1060 106 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether 27.8 1000 922 89 1000 931 90 1 70-130/20
91-20-3 Naphthalene 37.2 1000 999 95 1000 1000 95 0 70-130/20
103-65-1 n-Propylbenzene 23.1 J 1000 1030 101 1000 1070 105 4 70-130/20
100-42-5 Styrene ND 1000 950 95 1000 977 98 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 940 94 1000 955 96 2 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 962 96 1000 1000 100 4 70-130/20
127-18-4 Tetrachloroethylene ND 1000 1000 100 1000 1020 102 2 70-130/20
108-88-3 Toluene 2150 1000 3160 94 1000 3190 97 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 985 99 1000 975 98 1 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 954 95 1000 969 97 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 986 99 1000 1000 100 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 965 97 1000 985 99 2 70-130/20
79-01-6 Trichloroethylene ND 1000 980 98 1000 997 100 2 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 1180 118 1000 1210 121 3 60-140/20
96-18-4 1,2,3-Trichloropropane ND 1000 890 89 1000 937 94 5 70-130/20
95-63-6 1,2,4-Trimethylbenzene 173 1000 1150 98 1000 1180 101 3 70-130/20
108-67-8 1,3,5-Trimethylbenzene 45.1 1000 1060 101 1000 1090 104 3 70-130/20
75-01-4 Vinyl Chloride ND 1000 1000 100 1000 1030 103 3 60-140/20
m,p-Xylene 689 2000 2710 100 2000 2760 103 2 70-130/20
95-47-6 o-Xylene 364 1000 1350 97 1000 1370 99 1 70-130/20
1330-20-7 Xylene (total)1050 3000 4060 99 3000 4130 101 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA56099-2 Limits
1868-53-7 Dibromofluoromethane 101%102%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%106%105%70-130%
2037-26-5 Toluene-D8 101%102%101%70-130%
460-00-4 4-Bromofluorobenzene 99%101%100%70-130%
* = Outside of Control Limits.
43 of 45
FA5609955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA56100-3MS A0214797.D 200 07/30/18 AB n/a n/a VA2434
FA56100-3MSD A0214798.D 200 07/30/18 AB n/a n/a VA2434
FA56100-3 A0214787.D 200 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-4, FA56099-5, FA56099-6, FA56099-7
FA56100-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 246 2000 2160 96 2000 2230 99 3 70-130/20
108-86-1 Bromobenzene ND 2000 1680 84 2000 1730 87 3 70-130/20
74-97-5 Bromochloromethane ND 2000 1630 82 2000 1690 85 4 70-130/20
75-27-4 Bromodichloromethane ND 2000 1710 86 2000 1830 92 7 70-130/20
75-25-2 Bromoform ND 2000 1210 61*2000 1450 73 18 70-130/20
104-51-8 n-Butylbenzene ND 2000 1830 92 2000 1880 94 3 70-130/20
135-98-8 sec-Butylbenzene ND 2000 1910 96 2000 1970 99 3 70-130/20
98-06-6 tert-Butylbenzene ND 2000 1860 93 2000 1900 95 2 70-130/20
56-23-5 Carbon Tetrachloride ND 2000 1940 97 2000 2020 101 4 70-130/20
108-90-7 Chlorobenzene ND 2000 1860 93 2000 1920 96 3 70-130/20
75-00-3 Chloroethane ND 2000 2160 108 2000 2290 115 6 60-140/20
67-66-3 Chloroform ND 2000 1910 96 2000 1950 98 2 70-130/20
95-49-8 o-Chlorotoluene 28.7 J 2000 1900 94 2000 1960 97 3 70-130/20
106-43-4 p-Chlorotoluene ND 2000 1720 86 2000 1770 89 3 70-130/20
124-48-1 Dibromochloromethane ND 2000 1430 72 2000 1580 79 10 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 2000 1500 75 2000 1590 80 6 70-130/20
106-93-4 1,2-Dibromoethane ND 2000 1540 77 2000 1620 81 5 70-130/20
75-71-8 Dichlorodifluoromethane ND 2000 1540 77 2000 1680 84 9 60-140/20
95-50-1 1,2-Dichlorobenzene ND 2000 1640 82 2000 1720 86 5 70-130/20
541-73-1 1,3-Dichlorobenzene ND 2000 1790 90 2000 1870 94 4 70-130/20
106-46-7 1,4-Dichlorobenzene ND 2000 1760 88 2000 1810 91 3 70-130/20
75-34-3 1,1-Dichloroethane ND 2000 2010 101 2000 2060 103 2 70-130/20
107-06-2 1,2-Dichloroethane ND 2000 1890 95 2000 1960 98 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 2000 2080 104 2000 2130 107 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 2000 1830 92 2000 1920 96 5 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 2000 2010 101 2000 2060 103 2 70-130/20
78-87-5 1,2-Dichloropropane ND 2000 1900 95 2000 1980 99 4 70-130/20
142-28-9 1,3-Dichloropropane ND 2000 1650 83 2000 1700 85 3 70-130/20
594-20-7 2,2-Dichloropropane ND 2000 1900 95 2000 1880 94 1 70-130/20
563-58-6 1,1-Dichloropropene ND 2000 2000 100 2000 2090 105 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 2000 1610 81 2000 1680 84 4 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 2000 1640 82 2000 1690 85 3 70-130/20
108-20-3 Di-Isopropyl Ether ND 2000 1850 93 2000 1910 96 3 70-130/20
100-41-4 Ethylbenzene 1190 2000 3110 96 2000 3140 98 1 70-130/20
87-68-3 Hexachlorobutadiene ND 2000 1740 87 2000 1790 90 3 70-130/20
98-82-8 Isopropylbenzene 46.6 J 2000 2010 98 2000 2080 102 3 70-130/20
* = Outside of Control Limits.
44 of 45
FA5609955.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA56099
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA56100-3MS A0214797.D 200 07/30/18 AB n/a n/a VA2434
FA56100-3MSD A0214798.D 200 07/30/18 AB n/a n/a VA2434
FA56100-3 A0214787.D 200 07/30/18 AB n/a n/a VA2434
The QC reported here applies to the following samples:Method: SM 6200B
FA56099-1, FA56099-4, FA56099-5, FA56099-6, FA56099-7
FA56100-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 2000 1830 92 2000 1900 95 4 70-130/20
74-83-9 Methyl Bromide ND 2000 2110 106 2000 2270 114 7 60-140/20
74-87-3 Methyl Chloride ND 2000 2090 105 2000 2150 108 3 60-140/20
74-95-3 Methylene Bromide ND 2000 1850 93 2000 1900 95 3 70-130/20
75-09-2 Methylene Chloride ND 2000 2000 100 2000 2060 103 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 2000 1730 87 2000 1780 89 3 70-130/20
91-20-3 Naphthalene 177 2000 1700 76 2000 1740 78 2 70-130/20
103-65-1 n-Propylbenzene 125 2000 2010 94 2000 2070 97 3 70-130/20
100-42-5 Styrene 69.4 J 2000 1750 84 2000 1830 88 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 2000 1660 83 2000 1740 87 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 2000 1620 81 2000 1670 84 3 70-130/20
127-18-4 Tetrachloroethylene ND 2000 1880 94 2000 1950 98 4 70-130/20
108-88-3 Toluene 9980 2000 11600 81 2000 11400 71 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 2000 1580 79 2000 1620 81 3 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 2000 1600 80 2000 1650 83 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 2000 1900 95 2000 1950 98 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 2000 1650 83 2000 1700 85 3 70-130/20
79-01-6 Trichloroethylene ND 2000 1870 94 2000 1970 99 5 70-130/20
75-69-4 Trichlorofluoromethane ND 2000 2080 104 2000 2250 113 8 60-140/20
96-18-4 1,2,3-Trichloropropane ND 2000 1530 77 2000 1630 82 6 70-130/20
95-63-6 1,2,4-Trimethylbenzene 894 2000 2690 90 2000 2740 92 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 237 2000 2160 96 2000 2210 99 2 70-130/20
75-01-4 Vinyl Chloride ND 2000 1800 90 2000 1920 96 6 60-140/20
m,p-Xylene 3520 4000 7360 96 4000 7410 97 1 70-130/20
95-47-6 o-Xylene 1600 2000 3470 94 2000 3510 96 1 70-130/20
1330-20-7 Xylene (total)5130 6000 10800 95 6000 10900 96 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA56100-3 Limits
1868-53-7 Dibromofluoromethane 102%102%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%107%109%70-130%
2037-26-5 Toluene-D8 99%98%99%70-130%
460-00-4 4-Bromofluorobenzene 97%97%99%70-130%
* = Outside of Control Limits.
45 of 45
FA5609955.3.2

APPENDIX C
Notice of Intent to Construct or Operate Injection Wells

APPENDIX D:
Injection Event Record