WA-803_11086_CA_MRP_20190228

EXECUTIVE SUMMARY

The former Red Apple Market #40 site is located at 925 East Memorial Drive in Ahoskie, Hertford
County, North Carolina. The building on-site is currently occupied by Mizelle’s Drug Store. A release
was discovered during UST closure activities conducted at the site in September 1993.

On February 19, 2019, four monitoring wells were gauged, purged and sampled. No free product was
measured in any of the monitoring wells. Concentrations of requested method constituents that exceeded
the Maximum Allowable Concentrations specified in T15A NCAC 2L.0202 were reported in the ground
water samples collected from MW-2, MW-10, MW-11 and PMW-6. No concentrations of requested
method constituents that exceeded the Gross Contamination Levels (GCLs) were reported in the ground
water samples collected in February 2019.

Based on this information, a comprehensive ground water sampling event should be conducted in order to
confirm the February 2019 results. If contaminant concentrations remain below the GCLs, then the site
risk classification can be reevaluated. The next sampling event should be conducted before August 2019.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION ......................................................................... 1
2.0 CURRENT SITE ASSESSMENT .................................................................................................. 1
3.0 GROUND WATER QUALITY ...................................................................................................... 2
4.0 CONCLUSIONS AND RECOMMENDATIONS ........................................................................ 2
5.0 LIMITATIONS................................................................................................................................ 3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Ground Water Flow Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Laboratory Report – Ground Water Samples

1

1.0 SITE HISTORY AND CHARACTERIZATION
The former Red Apple Market #40 site is located at 925 East Memorial Drive in Ahoskie, Hertford
County, North Carolina (Figure 1). The building on-site is currently occupied by Mizelle’s Drug Store.
The site is located in a mixed use area along US Highway 13/Memorial Drive in Ahoskie. The area
surrounding the site is characterized by commercial properties. The remaining properties in the
immediate area are residential or undeveloped.

A release was discovered during UST closure activities conducted at the site in September 1993. Eleven
Type II monitoring wells (MW-1 through MW-6 and MW-8 through MW-12) and one Type III
monitoring well (MW-7) were installed on-site during site assessment activities. The North Carolina
Department of Environmental Quality (NCDEQ) approved a CAP in November 1996, which proposed
utilizing a ground water pump and treat remediation system, coupled with air sparging. As part of the
ground water remediation system, three ground water recovery wells were installed on October 31 and
November 1, 2000. The corrective action system is not currently in operation.

Based on a January 2013 conference call between NCDEQ, the responsible parties of the RAM #40 and
Pepsi Bottling Company Ahoskie (Pepsi) site located across Memorial Drive from RAM #40 and their
respective consultants, it was agreed that since the ground water contaminant plumes are likely
commingled, that the remediation efforts be conducted in unison. In addition, it was discussed during this
meeting that the risk rankings of the sites should be reduced to intermediate based on the lack of high risk
receptors. It was further agreed that Mobile Multi-Phase Extraction (MMPE) events would be conducted
to eliminate free product and reduce contaminant concentrations to below the Gross Contamination
Levels (GCLs) for both incidents. A Site Map showing the monitoring wells and structures on both
properties is presented as Figure 2.

2.0 CURRENT SITE ASSESSMENT
This report presents the results of ground water sampling activities conducted in February 2019. The
activities were conducted in accordance with Geological Resources, Inc. (GRI) proposal number 18-526,
which was submitted to NCDEQ on September 19, 2018, and approved as Task Authorization No. 11086-
51 on February 14, 2019. The purpose of the activities was to obtain current ground water quality data
for the site.

2

3.0 GROUND WATER QUALITY
On February 19, 2019, four monitoring wells (MW-2, MW-10, MW-11 and PMW-6) were gauged,
purged and sampled. No free product was measured in any of the monitoring wells. Depths to ground
water in the Type II monitoring wells ranged from 9.53 to 11.87 feet below the tops of well casings.
Relative ground water elevations in monitoring wells ranged from 88.24 to 88.72 feet. Based on the
February 2019 data, the ground water flow direction was generally toward the southwest with an average
horizontal hydraulic gradient of less than 0.01 feet per foot. A summary of ground water elevation data
obtained in February 2019 is presented in Table 1. A Ground Water Flow Map based on the February
2019 data has been included as Figure 3.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the February 2019 sampling event for VOCs using EPA Method 6200B. Concentrations of one or
more BTEX constituents, naphthalene, n-butylbenzene, n-propylbenzene, tetrachloroethene, o-
chlorotoluene, cis-1,2-dichloroethene, p-isopropyltoluene, 1,2,4-trimethylbenzene and/or 1,3,5-
trimethylbenzene that exceeded the Maximum Allowable Concentrations (MACs) specified in T15A
NCAC 2L.0202 were reported in the ground water samples collected from MW-2, MW-10, MW-11 and
PMW-6. No concentrations of requested method constituents that exceeded the Gross Contamination
Levels (GCLs) were reported in the ground water samples collected on February 19, 2019. A Ground
Water Quality Map based on data from the February 19, 2019, sampling event has been included as
Figure 4. A summary of ground water sample analytical results is presented in Table 5. A copy of the
laboratory report for the ground water samples collected in February 2019 is included as Appendix A.

4.0 CONCLUSIONS AND RECOMMENDATIONS

 The average depth to water during the February 2019 sampling event was 10.43 feet below the
tops of well casings. The ground water flow direction was generally toward the southwest with
an average horizontal hydraulic gradient of less than 0.01 feet per foot.
 Concentrations of one or more BTEX constituents, naphthalene, n-butylbenzene, n-
propylbenzene, tetrachloroethene, o-chlorotoluene, cis-1,2-dichloroethene, p-isopropyltoluene,
1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs were reported in
the ground water samples collected from MW-2, MW-10, MW-11 and PMW-6. No
concentrations of requested method constituents that exceeded the GCL were reported in the
ground water samples collected on February 19, 2019.

3

 Based on this information, a comprehensive ground water sampling event should be conducted in
order to confirm the February 2019 results. If contaminant concentrations remain below the
GCLs, then the site risk classification can be reevaluated. The next sampling event should be
conducted before August 2019.
5.0 LIMITATIONS
This report has been prepared for the exclusive use of Red Apple Markets, Inc. for specific application to
the referenced site in Hertford County, North Carolina. The site activities were conducted based on the
scope of work and level of effort specified by NCDEQ and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of geology and
hydrogeology practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES

TABLES
Date: 02/19/19
06/30/09 12.05 ---87.95
04/08/10 10.97 ---89.03
11/09/10 11.89 ---88.11
12/11/12 12.15 ---87.85
07/02/13 11.80 ---88.20
06/12/14 11.41 ---88.59
04/29/09 11.06 0.01 87.91
06/30/09 11.25 0.08 87.78
10.48 ---88.48 Pre-AFVR
10.91 ---88.05 Post-AFVR
04/08/10 10.03 ---88.93
11/09/10 10.96 ---88.00
12/11/12 11.33 0.12 87.73
05/13/13 10.68 ---88.28 Before MMPE
05/17/13 10.99 ---87.97 After MMPE
07/02/13 10.88 ---88.08
06/12/14 NM NM NM Covered
02/19/19 10.11 ----88.72
04/29/09 12.87 ---87.93
06/30/09 12.98 ---87.82
04/08/10 11.80 ---89.00
11/09/10 12.79 ---88.01
12/11/12 13.04 ---87.76
07/02/13 12.70 ---88.10
06/12/14 100.84 12.27 ---88.57
04/29/09 11.74 ---87.88
06/30/09 11.87 ---87.75
04/08/10 10.73 ---88.89
11/09/10 11.70 ---87.92
12/11/12 11.93 ---87.69
07/02/13 11.61 ---88.01
05/12/14 11.20 ---88.42 Before MMPE
05/16/14 11.61 ---88.01 After MMPE
06/12/14 11.22 ---88.38
08/25/14 11.43 ---88.17 Before MMPE
08/29/14 11.59 ---88.01 After MMPE
06/08/15 11.17 0.01 88.44 Before MMPE
06/12/15 11.40 ---88.20 After MMPE
06/30/09 12.04 ---88.16
04/08/10 10.88 ---89.32
11/09/10 11.87 ---88.33
12/11/12 12.09 ---88.11
07/02/13 NM NM NM
06/12/14 100.10 11.32 ---88.78
06/30/09 11.59 ---88.32
04/08/10 10.46 ---89.45
11/09/10 11.43 ---88.48
12/11/12 11.70 ---88.21
07/02/13 NM NM NM
06/12/14 99.80 10.90 ---88.90
06/30/09 12.38 ---87.75
04/08/10 11.39 ---88.74
11/09/10 12.09 ---88.04
12/11/12 12.37 ---87.76
07/02/13 NM NM NM
06/12/14 100.30 11.69 ---88.61
MW-8 02/25/94 04/29/09 8 8-18 18 97.73 NM NM NM DESTROYED
06/30/09 NM NM NM Not Found
04/08/10 8.68 ---88.94
11/09/10 9.30 ---88.32
12/11/12 9.63 ---87.99
07/02/13 NM NM NM
06/12/14 97.09 8.91 ---88.18
18 100.00
MW-6 08/10/93 8 8-18 18
MW-3 08/09/93
MW-5 08/09/93
99.62
03/02/10
MW-4
MW-2 08/06/93 8 18
08/09/93
MW-1 08/06/93 8 8-18
98.96
100.80
99.60
8 8-18 18
8-18 18
188-188
8
98.83
8-18
02/24/94MW-7 2520-2520
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 40 (INCIDENT NO. 11086)
Well ID Date Installed
(mm/dd/yy)
Free Product
Thickness**
(ft.)
Top of
Casing
Elevation*
(ft.)
Total
Depth of
Well
(ft. BGS)
Groundwater
Elevation
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Facility ID # : 0-000719
100.20
99.91
100.13
97.62MW-9 02/25/94 8
8-18 18
Page 1 of 4
Date: 02/19/19
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 40 (INCIDENT NO. 11086)
Well ID Date Installed
(mm/dd/yy)
Free Product
Thickness**
(ft.)
Top of
Casing
Elevation*
(ft.)
Total
Depth of
Well
(ft. BGS)
Groundwater
Elevation
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Facility ID # : 0-000719
04/29/09 10.92 ---87.46
06/30/09 10.58 ---87.80
10.35 ---88.03 Pre-AFVR
10.62 ---87.76 Post-AFVR
04/08/10 9.92 ---88.46
10/04/10 10.81 ---87.57 Before MMPE
10/08/10 11.08 ---87.30 After MMPE
11/09/10 10.95 ---87.43
12/11/12 11.93 ---86.45
07/02/13 11.21 ---87.17
05/12/14 10.45 ---87.93 Before MMPE
05/16/14 10.57 ---87.81 After MMPE
06/12/14 10.53 ---87.92
08/25/14 10.84 ---87.61 Before MMPE
08/29/14 10.89 ---87.56 After MMPE
10/03/14 10.94 ---87.51
05/18/15 10.20 ---88.25
06/08/15 10.48 ---87.97 Before MMPE
06/12/15 10.68 ---87.77 After MMPE
07/13/15 10.66 ---87.79
11/16/15 10.88 ---87.57 Before MMPE
11/20/15 11.08 ---87.37 After MMPE
11/30/15 10.80 ---87.65 Before MMPE
12/04/15 10.98 ---87.47 After MMPE
01/05/16 10.42 ---88.03
10/13/16 10.13 ---88.32
11/06/17 10.99 ---87.46
02/19/19 10.21 ----88.24
04/29/09 10.31 ---87.50
06/30/09 11.18 ---86.63
9.75 ---88.06 Pre-AFVR
9.72 ---88.09 Post-AFVR
04/08/10 9.34 ---88.47
10/04/10 10.13 ---87.68 Before MMPE
10/08/10 10.44 ---87.37 After MMPE
11/09/10 10.35 ---87.46
12/11/12 10.53 ---87.28
07/02/13 10.27 ---87.54
05/12/14 9.85 ---87.96 Before MMPE
05/16/14 10.01 ---87.80 After MMPE
06/12/14 9.92 ---87.87
08/25/14 10.11 ---87.68 Before MMPE
08/29/14 10.32 ---87.47 After MMPE
10/03/14 10.34 ---87.45
05/18/15 9.64 ---88.15
06/08/15 9.89 0.01 87.91 Before MMPE
06/12/15 10.10 ---87.69 After MMPE
07/13/15 10.06 ---87.73
11/16/15 10.30 0.02 87.51 Before MMPE
11/20/15 10.49 ---87.30 After MMPE
11/30/15 10.22 ---87.57 Before MMPE
12/04/15 10.43 ---87.36 After MMPE
01/05/16 9.82 ---87.97
10/13/16 9.47 ---88.32
11/06/17 10.36 ---87.43
02/19/19 9.53 ----88.26
04/29/09 11.29 ---87.60
06/30/09 11.51 ---87.38
10.69 ---88.20 Pre-AFVR
10.79 ---88.10 Post-AFVR
04/08/10 10.22 ---88.67
10/04/10 11.21 ---87.68 Before MMPE
10/08/10 11.32 ---87.57 After MMPE
11/09/10 11.29 ---87.60
12/11/12 11.22 ---87.67
07/02/13 11.22 ---87.67
06/12/14 98.88 10.64 ---88.24
MW-13 05/30/95 04/08/10 8 8-18 18 NA NM NM NM
06/30/09 DRY ---NA
12/11/12 NM NM NM Pump Stuck
05/13/13 10.50 ---88.22 Before MMPE
05/17/13 10.89 ---87.83 After MMPE
07/02/13 10.61 ---88.11
06/12/14 NM 9.89 ---NM
98.38
24.59.5-24.59.5
98.89
97.81
05/10/94MW-12
10/31/00RW-1
7-17 177
03/03/10
03/03/10
98.45
MW-11 05/10/94 7 7-17 17
97.79
03/03/10
98.72
MW-10 05/10/94 7 7-17 17
Page 2 of 4
Date: 02/19/19
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 40 (INCIDENT NO. 11086)
Well ID Date Installed
(mm/dd/yy)
Free Product
Thickness**
(ft.)
Top of
Casing
Elevation*
(ft.)
Total
Depth of
Well
(ft. BGS)
Groundwater
Elevation
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Facility ID # : 0-000719
06/30/09 DRY NM NM
12/11/12 11.50 ---87.68
05/13/13 11.02 ---88.16 Before MMPE
05/17/13 11.22 ---87.96 After MMPE
07/02/13 11.16 ---88.02
06/12/14 NM 10.74 ---NM
06/30/09 DRY NM NM
12/11/12 NM NM NM Pump Stuck
05/13/13 11.36 ---88.41 Before MMPE
05/17/13 11.54 ---88.23 After MMPE
07/02/13 11.55 ---88.22
05/12/14 11.14 ---88.63 Before MMPE
05/16/14 11.48 ---88.29 After MMPE
06/12/14 11.14 ---NM
08/25/14 11.35 ---NM Before MMPE
08/29/14 10.74 ---NM After MMPE
10/03/14 11.58 ---NM
05/18/15 10.84 ---NM
06/08/12 10.72 0.01 NM Before MMPE
06/12/15 11.06 ---NM After MMPE
07/13/15 10.94 ---NM
01/05/16 11.28 ---NM
10/13/16 10.81 ---NM
11/06/17 11.67 ---NM
04/08/10 11.97 ---41.68
11/09/10 12.12 ---41.53
12/11/12 12.39 ---41.26
07/02/13 NM NM NM
06/12/14 13.79 ---85.71
12.04 ---87.46 Before AFVR
13.59 ---85.91 After AFVR
04/08/10 10.81 ---42.49
11/09/10 12.03 ---41.27
12/11/12 12.12 ---41.18
07/02/13 NM NM NM
06/12/14 99.32 11.54 ---87.78
04/08/10 10.68 ---42.49
11/09/10 11.84 ---41.33
12/11/12 12.00 ---41.17
06/03/13 11.61 ---41.56 Before MMPE
06/07/13 11.69 ---41.48 After MMPE
07/02/13 11.71 ---41.46
06/12/14 11.36 ---87.67
10/03/14 11.77 ---87.26
05/18/15 11.04 ---87.99
07/13/15 11.50 ---87.53
11.63 ---87.40 Before AFVR
11.66 ---87.37 After AFVR
01/05/16 11.10 ---87.93
10/13/16 10.89 ---88.14
11/06/17 11.81 ---87.22
04/08/10 18.78 ---34.85
11/09/10 19.72 ---33.91
12/11/12 20.55 ---33.08
07/02/13 NM NM NM
06/12/14 99.49 19.39 ---80.10
04/08/10 11.11 ---41.66
11/09/10 12.55 ---40.22
12/11/12 12.60 ---40.17
06/03/13 11.48 ---41.29 Before MMPE
06/07/13 11.58 ---41.19 After MMPE
07/02/13 11.59 ---41.18
06/12/14 98.59 11.24 ---87.35
04/08/10 11.70 ---42.56
11/09/10 12.82 ---41.44
12/11/12 13.00 ---41.26
07/02/13 12.68 ---41.58
06/12/14 12.32 ---NM
10/03/14 12.73 ---NM
05/18/15 12.01 ---NM
07/13/15 12.48 ---NM
12.77 ---NM Before AFVR
12.99 ---NM After AFVR
12.70 ---NM Before AFVR
12.75 ---NM After AFVR
01/05/16 12.17 ---NM
10/13/16 11.88 ---NM
11/06/17 11.79 ---NM
02/19/19 11.87 ----NM
11/19/15
12/03/15
12/03/15
52.77
PMW-6
99.03
17.57.5-17.517.507/29-30/91PMW-3
08/13-14/91 17 7-17 17
NM
99.50
NM
PMW-5 08/13-14/91 16.5 6.5-16.5 16.5
1607/29-30/91PMW-1
11/19/15
25.510.5-25.510.511/01/00RW-3
3227-3232
1707/29-30/91PMW-2
25.5
08/13-14/91PMW-4D
RW-2 10/31/00 10.5 10.5-25.5
166-16
53.63
54.26
99.77
17.07-17
99.18
53.65
53.30
53.17
Page 3 of 4
Date: 02/19/19
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 40 (INCIDENT NO. 11086)
Well ID Date Installed
(mm/dd/yy)
Free Product
Thickness**
(ft.)
Top of
Casing
Elevation*
(ft.)
Total
Depth of
Well
(ft. BGS)
Groundwater
Elevation
(ft.)
Depth to
Water
from Top
of Casing
(ft.)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Facility ID # : 0-000719
04/08/10 19.40 ---33.92
11/09/10 20.37 ---32.95
12/11/12 20.72 ---32.60
07/02/13 NM NM NM
06/12/14 99.17 19.87 ---79.30
04/08/10 NM NM NM Not located
11/09/10 NM NM NM Not located
12/11/12 NM NM NM Not located
07/02/13 NM NM NM
06/12/14 NM NM ---NM DESTROYED
04/08/10 8.03 ---43.95
11/09/10 9.91 ---42.07
12/11/12 10.93 ---41.05
07/02/13 NM NM NM
06/12/14 NM NM ---NM Not Found
04/08/10 8.66 ---42.39
11/09/10 9.65 ---41.40
12/11/12 9.83 ---41.22
05/20/13 10.75 ---40.30 Before MMPE
05/24/13 10.98 ---40.07 After MMPE
07/02/13 NM NM NM
06/12/14 96.87 9.23 ---87.64
04/08/10 11.33 ---41.77
11/09/10 Dry NA
12/11/12 Dry NA
05/20/13 10.13 ---42.97 Before MMPE
05/24/13 10.36 ---42.74 After MMPE
07/02/13 NM NM NM
06/12/14 98.72 11.96 ---86.76
04/08/10 7.33 ---39.43
11/09/10 8.49 ---38.27
12/11/12 8.58 ---38.18
07/02/13 NM NM NM
06/12/14 10.29 ---82.11
11/06/17 11.34 ---81.06
04/08/10 8.70 ---41.84
11/09/10 9.96 ---40.58
12/11/12 10.05 ---40.49
07/02/13 NM NM NM
06/12/14 96.26 11.57 ---84.69
04/08/10 6.21 ---NA
11/09/10 7.49 ---NA
12/11/12 7.55 ---NA
07/02/13 NM NM NM
06/12/14 94.35 NM ---NM Not Found
04/08/10 7.95 ---40.30
11/09/10 8.80 ---39.45
12/11/12 8.31 ---39.94
07/02/13 NM NM NM
06/12/14 94.19 8.48 ---85.71
Notes:
• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness
• ft BGS : feet below ground surface.
• Top of casing elevations and well construction details for MW-1 through MW-12 and RW-1 through RW-3 are reproduced from the report
entitled 'Semiannual Ground Water Monitoring Report (June 2004)', dated September 14, 2004 prepared by CES Engineering, P.C.
• Top of casing elevations and well construction details for PMW-1 through PMW-15 are reproduced from the reports entitled ' Comprehensive Site
Assessment' and 'First Addendum to Comprehensive Site Assessment Report' dated October 4, 1991 and August 18, 1992, respectively,
prepared by Law Engineering.
• Top of casing elevations for MW-1 through MW-12, PMW-1 through PMW-5, PMW-7 and PMW-10 through PMW-15 were resurveyed on October
9, 2013 by Roanoke Land Surveying.
• NA: not available.
NA15
NA NA
1992-93 16.5 NA
PMW-8
05/18-21/92PMW-9
PMW-10
1992-93PMW-12
05/18-21/92 16.5
PMW-11 1992-93 17
46-515105/18-21/92PMW-7D 53.32
x 0.8581].
PMW-15 1992-93 17.5 NA
PMW-13 1992-93 14 NA
NA141992-93PMW-14
48.25
NA
50.54
51
53.03
51.98
16.5
16.5
NA
NA
NA
NA
92.40
NA
51.05
53.10
46.76
• NM: Not measured.
6.5-16.5
6.5-16.516.5
Page 4 of 4
Date: 02/26/19
EPA Method
6010B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 0.02 0.4 70 70 0.7 3 400 400 15
5,000 260,000 84,500 85,500 20,000 6,000 6,900 50 400 25,000 30,000 700 3,000 28,500 25,000 15,000
06/30/09 25.6 1.10 1.95 J 2.65 J <0.330 1.55 J 1.52 <0.330 <0.330 2.76 1.39 8.50 3.28 1.43 0.614 J NR
04/08/10 2.31 <1.00 <0.150 5.90 <0.250 1.13 <0.180 <0.240 <0.220 2.52 <0.220 0.499 J 1.04 <0.150 <0.180 NR
11/09/10 16.6 <2.00 0.588 J <0.440 <0.500 <1.00 <0.360 <0.480 <0.440 2.14 0.753 J <0.340 <1.00 <0.300 <0.360 NR
12/11/12 75.4 E 11.8 19.7 6.25 J <0.10 0.49 J 0.65 <0.10 <0.10 4.0 8.8 <0.10 <0.10 0.83 2.3 8.5
07/02/13 20.4 1.6 3.2 0.76 J <0.10 2.9 <0.10 <0.10 <0.10 1.1 1.5 0.64 0.98 0.37 J 0.37 J NR
06/12/14 1.6 <0.10 <0.10 <0.20 <0.10 0.42 J <0.10 <0.10 <0.10 0.53 <0.10 0.91 1.5 <0.10 <0.10 NR
06/30/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
04/08/10 309 4,140 398 6,900 9.15 J 938 237 <2.40 <2.20 48.4 103 9.31 J <5.00 1,950 972 NR
11/09/10 313 1,120 62.5 J 1,640 <25.0 86.8 J 43.1 J <24.0 <22.0 <15.0 24.3 J <17.0 <50.0 569 177 NR
12/11/12 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
07/02/13 154 553 121 2,910 <1.0 233 10.5 <1.0 <1.0 14.6 29.7 11.6 8.6 991 287 NR
06/12/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/19/19 302 2,800 334 5,210 <13 580 87.0 <13 <13 23.4 J 51.8 58.70 101 2,950 1,190 NR
06/30/09 517 12,600 1,950 12,000 <33.0 1,130 296 <33.0 <33.0 <100 191 <33.0 <33.0 2,660 984 NR
04/08/10 854 10,100 1,810 13,500 126 1,390 298 <2.40 <2.20 89.0 244 <1.70 20.6 2,330 1,340 NR
11/09/10 740 13,300 2,390 11,700 28.7 J 1,010 130 <24.0 <22.0 77.9 J 178 <17.0 <50.0 2,150 759 NR
12/11/12 461 9,990 2,090 12,770 <10 816 <10 <10 <10 57.3 172 <10 21.1 J 1,890 493 96.9
07/02/13 295 5,980 1,430 8,020 37.2 J 705 <20 <20 <20 52.5 J 170 21.3 J 21.9 J 1,440 509 NR
06/12/14 64.4 368 116 1,030 28.9 123 5.7 <1.0 <1.0 11.0 43.1 <1.0 <1.0 304 149 NR
06/30/09 441 1,540 196 1,070 44.3 J 52.2 J 24.8 J <16.5 <16.5 <50.0 26.4 J 29.2 J <16.5 210 62.7 NR
04/08/10 2,720 4,830 690 4,230 265 204 77.1 8.14 J 6.03 J 64.6 167 39.8 7.11 J 1,020 360 NR
11/09/10 863 2,700 292 1,550 13.1 J 41.4 J 22.3 J <12.0 <11.0 21.0 J 52.2 37.4 J <25.0 298 76.3 NR
12/11/12 348 1,450 110 968 <5.0 33.4 <5.0 <5.0 <5.0 <5.0 17.3 J 33.5 17.6 J 225 54.9 <5.0
07/02/13 1,680 4,120 187 1,660 122 73.8 <10 <10 <10 <10 14.1 J 50.7 28.9 J 184 48.7 J NR
06/12/14 120 958 144 1,190 <2.0 63.9 6.6 J <2.0 <2.0 8.8 J 34.0 93.7 56.3 302 83.3 NR
06/30/09 0.983 J <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <0.330 <0.330 <1.00 0.554 J 55.1 9.39 <0.330 <0.330 NR
04/08/10 5.23 1.29 6.97 1.65 <0.250 <0.500 0.989 J <0.240 <0.220 4.43 4.98 9.22 1.77 0.389 J 1.04 NR
11/09/10 0.404 J <2.00 0.353 J 0.943 J <0.500 <1.00 <0.360 <0.480 <0.440 0.308 J 0.464 J 53.4 7.39 0.621 J <0.360 NR
12/11/12 1.2 J 0.27 J 0.57 0.16 J <0.10 <0.15 <0.10 <0.10 <0.10 0.54 0.57 31.5 J 6.7 J <0.10 0.19 J 5.1
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 1.2 0.35 J 1.5 0.45 J <0.10 <0.10 <0.10 <0.10 <0.10 0.99 2.4 5.7 3.5 0.15 J <0.10 NR
06/30/09 0.705 J <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <0.330 <0.330 <1.00 <0.330 3.59 2.34 <0.330 <0.330 NR
04/08/10 0.853 J 0.557 J <0.150 <0.220 <0.250 <0.500 <0.180 <0.240 <0.220 2.13 <0.220 1.85 1.12 <0.150 <0.180 NR
11/09/10 0.385 J <1.00 0.176 J 0.918 J <0.250 1.09 <0.180 <0.240 <0.220 0.241 J <0.220 3.70 2.23 0.986 J 0.298 J NR
12/11/12 0.39 J 0.15 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 0.54 J 0.52 J <0.10 <0.10 21.4
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 0.24 J <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.68 0.62 <0.10 <0.10 NR
MW-4
MW-5
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET # 40 (INCIDENT NO. 11086)n-PropylbenzeneTrichloroethyleneTetrachloroethene1,2-Dichloroethane1,3,5-TrimethylbenzeneEDB1,2,4-TrimethylbenzeneNaphthalenen-ButylbenzeneContaminant of Concern BenzeneMW-1
Analytical Method TolueneFacility ID No.: 0-000719
Lead2L Standard (mg/l)
GCL (mg/l)
EPA Method 6200B
EthylbenzeneXylenesIsopropylbenzeneMTBEMW-2
MW-3
MW-6
Page 1 of 6
Date: 02/26/19
EPA Method
6010B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 0.02 0.4 70 70 0.7 3 400 400 15
5,000 260,000 84,500 85,500 20,000 6,000 6,900 50 400 25,000 30,000 700 3,000 28,500 25,000 15,000
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET # 40 (INCIDENT NO. 11086)n-PropylbenzeneTrichloroethyleneTetrachloroethene1,2-Dichloroethane1,3,5-TrimethylbenzeneEDB1,2,4-TrimethylbenzeneNaphthalenen-ButylbenzeneContaminant of Concern BenzeneAnalytical Method TolueneFacility ID No.: 0-000719
Lead2L Standard (mg/l)
GCL (mg/l)
EPA Method 6200B
EthylbenzeneXylenesIsopropylbenzeneMTBE06/30/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <0.330 <0.330 <1.00 <0.330 35.1 0.997 J <0.330 <0.330 NR
04/08/10 0.155 J 1.19 J 0.264 J 6.91 <0.250 1.34 <0.180 <0.240 <0.220 <0.150 <0.220 28.7 1.79 <0.150 <0.180 NR
11/09/10 <0.140 <1.00 <0.150 0.736 J <0.250 0.503 J <0.180 <0.240 <0.220 <0.150 <0.220 28.0 3.77 0.653 J <0.180 NR
12/11/12 0.12 J 0.61 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 48.2 10.8 <0.10 <0.10 <5.0
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 120 31.2 <0.10 <0.10 NR
06/30/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NR
04/08/10 <0.140 <1.00 0.150 J 6.47 <0.250 1.36 0.487 J <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
11/09/10 <0.700 <5.00 <0.750 <1.10 <1.25 <2.50 <0.900 <1.20 <1.10 <0.750 <1.10 <0.850 <2.50 <0.750 <0.900 NR
12/11/12 0.78 J 0.13 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 35.5
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 <0.10 0.22 J <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
10/03/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/30/09 20,000 28,100 2,490 9,870 1,940 675 112 J 134 J 234 J <250 176 J <82.5 <82.5 1,380 346 NR
04/08/10 15,400 18,700 1,520 6,430 1,110 412 62.7 13.6 J 99.0 65.7 59.1 <3.40 <10.0 763 190 NR
11/09/10 21,000 33,500 3,290 14,900 961 1,930 308 J <120 <110 192 J 566 <85.0 <250 4,640 1,090 NR
12/11/12 16,600 J 32,800 2,220 10,710 767 J 910 <100 <100 138 J <100 270 J <100 <100 1,980 477 J 176
07/02/13 0.21 J 14.4 0.20 J 0.78 J <0.10 0.19 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.18 J <0.10 NR
06/12/14 13,700 27,600 2,470 12,100 493 560 25.9 J 62.6 J 69.3 J 86.3 J 314 <20 <20 1,920 494 NR
10/03/14 2,820 2,400 122 673 <10 48.3 J <10 20.9 J 23.9 J <10 44.2 J <10 <10 286 101 NR
05/18/15 11,700 18,200 1,410 6,110 405 391 <72 <71 96.0 J <59 114 J <74 <73 900 188 J NR
07/13/15 16,700 29,400 2,410 12,000 597 653 <72 <71 93.8 J 76.5 J 239 J <74 <73 1,830 478 NR
01/05/16 1,110 854 201 938 45.0 94.1 17.8 6.3 4.4 18.8 93.8 0.69 <0.13 524 165 NR
10/13/16 84.8 10.9 12.2 23.0 2.60 7.4 0.37 J <0.13 0.30 J 0.82 2.5 <0.13 <0.13 <0.14 2.8 NR
11/06/17 15,500 31,700 2,560 12,300 373 J 1,800 <130 <130 <130 <130 229 J <130 <130 1,660 518 NR
02/19/19 0.17 J <0.13 1.4 1.4 J <0.13 0.89 <0.13 <0.13 <0.13 0.15 J 0.53 <0.13 <0.13 2.8 0.78 NR
06/30/09 12,300 25,500 2,140 9,750 <82.5 721 124 J 245 J 131 J <250 182 J <82.5 <82.5 1,410 373 NR
04/08/10 13,400 15,600 1,220 5,040 81.3 483 75.3 84.1 70.6 65.0 69.0 <3.40 <10.0 958 214 NR
11/09/10 20,000 42,900 4,140 17,900 169 J 2,880 377 J 326 J 137 J 205 J 754 <85.0 <250 6,060 1,550 NR
12/11/12 10,800 J 29,400 1,990 9,790 <100 1,570 <100 <100 131 J <100 249 J <100 <100 2,030 451 J 839
07/02/13 11,700 30,200 2,650 12,800 <100 704 <100 162 J 123 J <100 335 J <100 <100 2,010 540 NR
06/12/14 1,890 6,550 1,310 6,420 <10 381 23.1 J 22.4 J 13.3 J 78.1 306 <10 <10 1,760 485 NR
10/03/14 5,690 13,900 1,700 8,920 <50 445 <50 95.1 J 83.8 J 64.3 J 214 J <50 <50 1,500 399 NR
05/18/15 3,890 7,330 732 3,230 <33 245 <29 <28 52.5 J 45.8 J 200 <30 <29 1,300 332 NR
07/13/15 8,230 24,700 2,650 12,300 <33 825 67.0 J 128 86.6 J 139 469 <30 <29 3,090 845 NR
01/05/16 3,180 6,880 1,730 7,920 28.4 J 590 96.1 J <25 41.3 J 127 489 <25 <25 2,820 820 NR
10/13/16 244 584 125 556 2.7 J 57.7 6.1 <1.3 3.3 J 7.2 28.4 <1.3 <1.3 180 56.2 NR
11/06/17 7,210 15,000 1,100 4,430 <130 8,590 <130 <130 <130 <130 <130 <130 <130 555 178 J NR
02/19/19 1,510 3,770 411 1,660 <13 122 <13 <13 <13 16.7 J 42.7 J <13 <13 297 85.5 NR
MW-11
MW-10
MW-9
MW-7
Page 2 of 6
Date: 02/26/19
EPA Method
6010B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 0.02 0.4 70 70 0.7 3 400 400 15
5,000 260,000 84,500 85,500 20,000 6,000 6,900 50 400 25,000 30,000 700 3,000 28,500 25,000 15,000
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET # 40 (INCIDENT NO. 11086)n-PropylbenzeneTrichloroethyleneTetrachloroethene1,2-Dichloroethane1,3,5-TrimethylbenzeneEDB1,2,4-TrimethylbenzeneNaphthalenen-ButylbenzeneContaminant of Concern BenzeneAnalytical Method TolueneFacility ID No.: 0-000719
Lead2L Standard (mg/l)
GCL (mg/l)
EPA Method 6200B
EthylbenzeneXylenesIsopropylbenzeneMTBE06/30/09 2,070 6,540 1,460 7,530 37.2 J 539 118 <33.0 <33.0 <100 168 <33.0 <33.0 1,680 467 NR
04/08/10 1,060 3,610 700 1,570 <5.00 171 23.0 <4.80 <4.40 66.3 44.9 <3.40 <10.0 337 73.4 NR
11/09/10 328 164 217 203 <2.50 96.3 <1.80 <2.40 <2.20 19.2 51.9 <1.70 <5.00 258 58.6 NR
12/11/12 758 8,390 1,010 3,710 <20 204 <20 <20 <20 <20 71.9 J <20 <20 465 111 297
07/02/13 7.4 0.88 7.4 5.6 <0.10 4.1 0.23 J <0.10 <0.10 0.31 J 1.0 <0.10 <0.10 2.4 0.30 J NR
06/12/14 2.3 29.0 7.3 18.2 <0.10 2.9 <0.10 <0.10 <0.10 0.30 J 0.94 <0.10 <0.10 3.3 <0.10 NR
06/30/09 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
12/11/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/02/13 0.77 1.8 0.23 J 1.8 0.46 J 0.16 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.37 J 0.17 J NR
06/12/14 0.29 J 0.28 J <0.10 2.5 0.20 J 0.28 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.14 J 0.34 J NR
06/30/09 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
12/11/12 369 228 1.2 J 395 21.9 4.3 J <1.0 <1.0 <1.0 <1.0 <1.0 5.2 2.9 J 18.2 12.4 95.9
07/02/13 69.6 212 16.4 665 2.7 38.1 0.91 <0.10 0.23 J 1.3 2.7 3.7 <0.10 198 70.6 NR
06/12/14 26.3 42.9 0.77 264 1.1 2.2 <0.10 <0.10 <0.10 <0.10 <0.10 1.1 0.62 14.2 10.0 NR
06/30/09 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
12/11/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/02/13 5,160 24,400 1,250 17,300 570 724 <50 <50 <50 <50 99.6 J <50 <50 2,740 715 NR
06/12/14 3,660 16,400 621 15,200 1,010 688 <50 <50 <50 <50 <50 <50 <50 2,350 816 NR
10/03/14 3,830 11,700 1,930 11,500 <25 547 <25 <25 <25 58.6 J 192 <25 <25 1,970 470 NR
05/18/15 2,320 7,800 660 8,940 677 436 <29 <28 <33 <24 63.2 J <30 <29 1,600 609 NR
07/13/15 15.5 20.1 0.69 86.7 0.37 J 4.0 <0.14 <0.14 <0.16 <0.12 <0.16 0.74 <0.15 16.4 12.3 NR
01/05/16 2,960 14,500 1,450 16,000 361 960 37.8 J <25 <25 50.3 J 136 <25 <25 3,020 1,040 NR
10/13/16 1,310 6,480 412 7,920 183 374 <25 <25 <25 <25 44.2 J <25 <25 1,260 503 NR
11/06/17 3,120 17,900 1,300 17,000 219 475 B <25 <25 <25 33.9 J 76.3 J <25 <25 2,490 737 NR
04/08/10 25.4 4,310 1,830 10,500 <5.00 1,510 587 <4.80 <4.40 209 667 <3.40 <10.0 6,100 2,830 NR
11/09/10 <1.40 64.3 107 1,300 <2.50 389 308 <2.40 <2.20 33.8 119 <1.70 <5.00 1,200 1,030 NR
12/11/12 <1.0 25.5 27.8 430 <1.0 105 13.0 <1.0 <1.0 13.4 37.9 <1.0 <1.0 979 329 734
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
04/08/10 0.902 J 3.31 J 2.63 J 114 <1.25 28.3 38.1 <1.20 <1.10 37.1 94.3 <0.850 <2.50 634 174 NR
11/09/10 <0.700 <5.00 <0.750 29.5 <1.25 6.95 6.57 <1.20 <1.10 8.93 15.9 <0.850 <2.50 170 34.4 NR
12/11/12 1.1 0.28 J 0.39 J 4.6 0.22 J 1.5 0.63 <0.10 <0.10 3.3 2.4 <0.10 <0.10 79.0 3.3 42.7
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 <0.10 <0.10 <0.10 0.37 J <0.10 0.48 J 0.35 J <0.10 <0.10 1.2 3.5 <0.10 <0.10 9.4 0.53 NR
PMW-1
PMW-2
RW-3
RW-1
MW-12
RW-2
Page 3 of 6
Date: 02/26/19
EPA Method
6010B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 0.02 0.4 70 70 0.7 3 400 400 15
5,000 260,000 84,500 85,500 20,000 6,000 6,900 50 400 25,000 30,000 700 3,000 28,500 25,000 15,000
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET # 40 (INCIDENT NO. 11086)n-PropylbenzeneTrichloroethyleneTetrachloroethene1,2-Dichloroethane1,3,5-TrimethylbenzeneEDB1,2,4-TrimethylbenzeneNaphthalenen-ButylbenzeneContaminant of Concern BenzeneAnalytical Method TolueneFacility ID No.: 0-000719
Lead2L Standard (mg/l)
GCL (mg/l)
EPA Method 6200B
EthylbenzeneXylenesIsopropylbenzeneMTBE04/08/10 10,400 18,400 2,550 16,700 <5.00 812 63.8 206 <4.40 112 216 <3.40 <10.0 2,570 721 NR
11/09/10 5,010 13,500 1,560 9,070 <25.0 762 <18.0 <24.0 <22.0 63.0 J 135 <17.0 <50.0 1,580 343 NR
12/11/12 5,620 21,600 1,500 9,980 <50 466 <50 <50 <50 <50 99.0 J <50 <50 1,340 280 110
07/02/13 1,130 5,020 906 5,630 <20 281 <20 <20 <20 28.8 J 95.9 J <20 <20 907 213 NR
06/12/14 790 2,590 583 3,190 <2.5 223 7.8 J <2.5 <2.5 23.5 91.7 <2.5 <2.5 858 235 NR
10/03/14 3,600 20,200 1,310 16,100 429 717 <50 <50 <50 <50 59.9 J <50 <50 2,270 655 NR
05/18/15 5,340 17,600 2,800 16,500 <82 985 <72 <71 <82 78.0 J 289 <74 <73 3,130 714 NR
07/13/15 3,490 11,500 2,370 13,000 <33 733 <29 <28 <33 76.3 J 248 <30 <29 2,510 650 NR
01/05/16 2,750 11,600 2,390 11,700 <31 751 <31 <31 <31 96.1 J 293 <31 <31 2,320 604 NR
10/13/16 936 5,270 1,230 6,220 <25 392 <25 <25 <25 44.3 J 156 <25 <25 1,240 348 NR
11/06/17 1,820 9,750 1,760 8,660 <13 486 B 14.2 J <13 <13 63.5 208 <13 <13 1,790 503 NR
04/08/10 24.3 147 97.0 466 0.785 J 29.0 7.99 <0.240 <0.220 8.36 26.7 0.555 J <0.500 145 60.6 NR
11/09/10 0.743 J 5.78 2.68 15.7 <0.500 1.59 J 0.573 J <0.480 <0.440 <0.300 0.834 J <0.340 <1.00 5.27 2.13 NR
12/11/12 10.3 98.8 46.6 239.8 <0.10 22.6 2.1 <0.10 <0.10 6.4 19.5 0.21 J <0.10 81.8 39.4 <5.0
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
04/08/10 4,630 4,670 709 3,010 6.53 J 1,880 39.1 279 5.26 J 55.1 124 <1.70 <5.00 1,520 355 NR
11/09/10 2,550 6,510 890 6,730 <25.0 1,550 <18.0 172 <22.0 59.5 J 161 <17.0 <50.0 2,150 459 NR
12/11/12 493 199 203 1,049 <2.0 391 7.1 J 13.9 <2.0 19.0 71.9 <2.0 <2.0 1,330 213 318
07/02/13 214 214 172 1,400 <2.0 331 4.0 J 43.8 <2.0 20.1 71.1 <2.0 <2.0 989 208 NR
06/12/14 27.6 6.4 11.8 25.1 0.17 J 84.5 0.30 J 1.2 0.20 J 1.1 2.6 <0.10 <0.10 37.5 8.5 NR
04/08/10 6,710 42,400 5,110 25,600 <12.5 943 135 125 <11.0 203 331 <8.50 <25.0 3,800 1,010 NR
11/09/10 3,580 24,900 2,410 14,600 <50.0 585 <36.0 85.5 J <44.0 68.2 J 163 J <34.0 <100 1,830 470 NR
12/11/12 3,490 58,300 3,560 18,760 <200 590 J <200 <200 <200 <200 246 J <200 <200 1,500 435 J 132
07/02/13 2,620 37,000 3,020 20,100 <20 467 <20 37.2 J <20 52.3 J 160 <20 <20 1,740 460 NR
06/12/14 1,990 27,200 3,030 20,600 <20 549 24.6 J <20 <20 30.8 J 100 <20 <20 1,880 642 NR
10/03/14 2,670 34,000 2,940 19,000 <100 426 J <100 <100 <100 <100 <100 <100 <100 1,370 396 J NR
05/18/15 2,670 36,500 3,420 20,000 <33 512 <29 <28 <33 55.7 J 156 <30 <29 1,780 438 NR
07/13/15 3,140 39,500 3,720 21,100 <33 581 <29 <28 <33 67.5 J 167 <30 <29 2,080 551 NR
01/05/16 1,850 29,200 4,700 21,000 <63 705 <63 <63 <63 148 J 506 <63 <63 3,400 934 NR
10/13/16 1,590 31,200 3,050 16,700 <63 439 <63 <63 <63 <63 201 J <63 <63 1,610 482 NR
11/06/17 1,720 36,300 3,760 21,000 <31 893 B <31 <31 <31 92.9 J 278 <31 <31 2,340 649 NR
02/19/19 1,100 35,800 3,980 21,100 <130 507 <130 <130 <130 <130 295 J <130 <130 2,210 673 NR
04/08/10 <0.140 0.680 J 0.163 J 0.555 J <0.250 <0.500 <0.180 <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
11/09/10 13.5 <1.00 <0.150 <0.220 67.4 <0.500 <0.180 <0.240 0.906 J <0.150 <0.220 <0.170 2.34 <0.150 <0.180 NR
12/11/12 0.12 J <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <5.0
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 0.17 J <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
PMWD-4
PMW-5
PMWD-7
PMW-3
PMW-6
Page 4 of 6
Date: 02/26/19
EPA Method
6010B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 0.02 0.4 70 70 0.7 3 400 400 15
5,000 260,000 84,500 85,500 20,000 6,000 6,900 50 400 25,000 30,000 700 3,000 28,500 25,000 15,000
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET # 40 (INCIDENT NO. 11086)n-PropylbenzeneTrichloroethyleneTetrachloroethene1,2-Dichloroethane1,3,5-TrimethylbenzeneEDB1,2,4-TrimethylbenzeneNaphthalenen-ButylbenzeneContaminant of Concern BenzeneAnalytical Method TolueneFacility ID No.: 0-000719
Lead2L Standard (mg/l)
GCL (mg/l)
EPA Method 6200B
EthylbenzeneXylenesIsopropylbenzeneMTBE04/08/10 4.60 0.602 J 0.631 J 1.96 1.43 3.62 0.465 J <0.240 0.903 J 2.05 <0.220 <0.170 <0.500 <0.150 <0.180 NR
11/09/10 <0.140 <1.00 <0.150 <0.220 <0.250 <0.500 <0.180 <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
12/11/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 6.1
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/08/10 <0.140 0.508 J <0.150 <0.220 <0.250 <0.500 <0.180 <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
11/09/10 <0.140 <1.00 <0.150 <0.220 <0.250 <0.500 <0.180 <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
12/11/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 0.21 J <0.10 <0.10 <0.10 <5.0
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
04/08/10 <0.140 0.306 J <0.150 <0.220 <0.250 1.10 <0.180 <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
11/09/10 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
12/11/12 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
04/08/10 <0.140 0.294 J <0.150 <0.220 <0.250 <0.500 <0.180 <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
11/09/10 <0.140 <1.00 <0.150 <0.220 <0.250 <0.500 <0.180 <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
12/11/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 7.6
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 <0.10 <0.10 <0.10 <0.20 4.8 <0.10 <0.10 <0.10 0.14 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR
11/06/17 0.64 <0.13 <0.13 <0.25 3.6 <0.13 <0.13 <0.13 0.50 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
04/08/10 <0.140 0.206 J <0.150 <0.220 <0.250 <0.500 <0.180 <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
11/09/10 <0.140 <1.00 <0.150 <0.220 <0.250 <0.500 <0.180 <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
12/11/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 27.1
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 28.1 0.21 J 1.1 <0.20 0.17 J 0.83 0.34 J <0.10 <0.10 0.90 0.62 <0.10 <0.10 <0.10 <0.10 NR
04/08/10 <0.140 0.464 J <0.150 <0.220 <0.250 <0.500 <0.180 <0.240 <0.220 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
11/09/10 <0.140 <1.00 <0.150 <0.220 0.262 J <0.500 <0.180 <0.240 <0.220 <0.150 <0.220 0.181 J <0.500 <0.150 <0.180 NR
12/11/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 12.0
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
PMW-9
PMW-13
PMW-10
PMW-11
PMW-12
PMW-14
Page 5 of 6
Date: 02/26/19
EPA Method
6010B
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 70 0.02 0.4 70 70 0.7 3 400 400 15
5,000 260,000 84,500 85,500 20,000 6,000 6,900 50 400 25,000 30,000 700 3,000 28,500 25,000 15,000
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET # 40 (INCIDENT NO. 11086)n-PropylbenzeneTrichloroethyleneTetrachloroethene1,2-Dichloroethane1,3,5-TrimethylbenzeneEDB1,2,4-TrimethylbenzeneNaphthalenen-ButylbenzeneContaminant of Concern BenzeneAnalytical Method TolueneFacility ID No.: 0-000719
Lead2L Standard (mg/l)
GCL (mg/l)
EPA Method 6200B
EthylbenzeneXylenesIsopropylbenzeneMTBE04/08/10 7.83 0.243 J <0.150 <0.220 106 <0.500 <0.180 <0.240 1.74 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
11/09/10 11.7 <1.00 <0.150 <0.220 135 1.07 <0.180 <0.240 4.68 <0.150 <0.220 <0.170 <0.500 <0.150 <0.180 NR
12/11/12 1.5 <0.10 <0.10 <0.22 24.7 <0.15 <0.10 <0.10 0.31 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 28.1
07/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/12/14 140 <0.10 <0.10 <0.20 22.4 0.65 1.4 <0.10 4.9 2.6 0.35 J <0.10 <0.10 <0.10 <0.10 NR
Notes:
• 2L Standard are also known as the maximum allowable concentrations (MACs) specified in Title 15A NCAC 2L.0202.
• Concentrations in bold face type exceeded the 2L standards; concentrations in bold face type and italics exceed the GCLs.
• FP: Free product.
• NE: No standard specified.
• J: Estimated concentration.
• E: Value exceeds calibration range.
• Concentrations of o-chlorotoluene (125 µg/l), cis-1,2-Dichloroethene (149 µg/l) and p-Isopropyltoluenethat (50.3 µg/l) that exceeded the 2L Standards were reported in the ground water sample collected from
MW-2 on 02/19/19.
• Refer to laboratory report for additional detectable constituents which did not exceed the 2L Standards.
• NS: Not sampled.
PMW-15
• GCL : Gross contamination level.
• Results reported in μg/l.
Page 6 of 6

APPENDIX

APPENDIX A
Laboratory Report – Ground Water Samples

02/25/19
Technical Report for
GRI (Geological Resources Inc.)
Ram 40; 925 E Memorial Dr, Ahoskie, NC
11086/2830
SGS Job Number: FA61714
Sampling Date: 02/19/19
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: Nicole Long
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 02/25/19
e-Hardcopy 2.0
Automated Report
31
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
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1 of 31
FA61714
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA61714-1: MW-2 ........................................................................................................7
3.2: FA61714-2: MW-10 ......................................................................................................9
3.3: FA61714-3: MW-11 ......................................................................................................11
3.4: FA61714-4: PMW-6 .....................................................................................................13
Section 4: Misc. Forms ............................................................................................................15
4.1: Chain of Custody ...........................................................................................................16
Section 5: MS Volatiles - QC Data Summaries .....................................................................18
5.1: Method Blank Summary ................................................................................................19
5.2: Blank Spike Summary ...................................................................................................23
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................27 123452 of 31
FA61714
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA61714
Ram 40; 925 E Memorial Dr, Ahoskie, NC
Project No: 11086/2830
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA61714-1 02/19/19 12:36 ER 02/20/19 AQ Ground Water MW-2
FA61714-2 02/19/19 13:08 ER 02/20/19 AQ Ground Water MW-10
FA61714-3 02/19/19 13:17 ER 02/20/19 AQ Ground Water MW-11
FA61714-4 02/19/19 13:33 ER 02/20/19 AQ Ground Water PMW-6
3 of 31
FA617141
Summary of Hits Page 1 of 2
Job Number:FA61714
Account:GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Collected:02/19/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA61714-1 MW-2
Benzene 302 50 13 ug/l SM 6200B
n-Butylbenzene 87.0 50 13 ug/l SM 6200B
sec-Butylbenzene 43.8 J 50 13 ug/l SM 6200B
o-Chlorotoluene 125 50 13 ug/l SM 6200B
cis-1,2-Dichloroethylene 149 50 13 ug/l SM 6200B
Ethylbenzene 334 50 13 ug/l SM 6200B
Isopropylbenzene 23.4 J 50 13 ug/l SM 6200B
p-Isopropyltoluene 50.3 50 13 ug/l SM 6200B
Naphthalene 580 50 13 ug/l SM 6200B
n-Propylbenzene 51.8 50 13 ug/l SM 6200B
Tetrachloroethylene 58.7 50 13 ug/l SM 6200B
Toluene 2800 50 13 ug/l SM 6200B
Trichloroethylene 101 50 13 ug/l SM 6200B
1,2,4-Trimethylbenzene 2950 50 13 ug/l SM 6200B
1,3,5-Trimethylbenzene 1190 50 13 ug/l SM 6200B
m,p-Xylene 3250 100 13 ug/l SM 6200B
o-Xylene 1970 50 13 ug/l SM 6200B
Xylene (total)5210 150 25 ug/l SM 6200B
FA61714-2 MW-10
Benzene 0.17 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene 1.4 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.15 J 0.50 0.13 ug/l SM 6200B
Naphthalene 0.89 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 0.53 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 2.8 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.71 0.50 0.13 ug/l SM 6200B
m,p-Xylene 1.3 1.0 0.13 ug/l SM 6200B
o-Xylene 0.14 J 0.50 0.13 ug/l SM 6200B
Xylene (total)1.4 J 1.5 0.25 ug/l SM 6200B
FA61714-3 MW-11
Benzene 1510 50 13 ug/l SM 6200B
Ethylbenzene 411 50 13 ug/l SM 6200B
Isopropylbenzene 16.7 J 50 13 ug/l SM 6200B
Naphthalene 122 50 13 ug/l SM 6200B
n-Propylbenzene 42.7 J 50 13 ug/l SM 6200B
Toluene 3770 50 13 ug/l SM 6200B
1,2,4-Trimethylbenzene 297 50 13 ug/l SM 6200B
1,3,5-Trimethylbenzene 85.5 50 13 ug/l SM 6200B
m,p-Xylene 1090 100 13 ug/l SM 6200B
4 of 31
FA617142
Summary of Hits Page 2 of 2
Job Number:FA61714
Account:GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Collected:02/19/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
o-Xylene 569 50 13 ug/l SM 6200B
Xylene (total)1660 150 25 ug/l SM 6200B
FA61714-4 PMW-6
Benzene 1100 500 130 ug/l SM 6200B
Ethylbenzene 3980 500 130 ug/l SM 6200B
Naphthalene 507 500 130 ug/l SM 6200B
n-Propylbenzene 295 J 500 130 ug/l SM 6200B
Toluene 35800 500 130 ug/l SM 6200B
1,2,4-Trimethylbenzene 2210 500 130 ug/l SM 6200B
1,3,5-Trimethylbenzene 673 500 130 ug/l SM 6200B
m,p-Xylene 14500 1000 130 ug/l SM 6200B
o-Xylene 6540 500 130 ug/l SM 6200B
Xylene (total)21100 1500 250 ug/l SM 6200B
5 of 31
FA617142
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
6 of 31
FA617143
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA61714-1 Date Sampled:02/19/19
Matrix:AQ - Ground Water Date Received:02/20/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217152.D 100 02/21/19 15:54 AB n/a n/a VA2534
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 302 50 13 ug/l
108-86-1 Bromobenzene ND 50 13 ug/l
74-97-5 Bromochloromethane ND 50 13 ug/l
75-27-4 Bromodichloromethane ND 50 13 ug/l
75-25-2 Bromoform ND 50 13 ug/l
104-51-8 n-Butylbenzene 87.0 50 13 ug/l
135-98-8 sec-Butylbenzene 43.8 50 13 ug/l J
98-06-6 tert-Butylbenzene ND 50 13 ug/l
56-23-5 Carbon Tetrachloride ND 50 13 ug/l
108-90-7 Chlorobenzene ND 50 13 ug/l
75-00-3 Chloroethane ND 50 20 ug/l
67-66-3 Chloroform ND 50 13 ug/l
95-49-8 o-Chlorotoluene 125 50 13 ug/l
106-43-4 p-Chlorotoluene ND 50 13 ug/l
124-48-1 Dibromochloromethane ND 50 13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 25 ug/l
106-93-4 1,2-Dibromoethane ND 50 13 ug/l
75-71-8 Dichlorodifluoromethane a ND 50 20 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 13 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 13 ug/l
75-34-3 1,1-Dichloroethane ND 50 13 ug/l
107-06-2 1,2-Dichloroethane ND 50 13 ug/l
75-35-4 1,1-Dichloroethylene ND 50 13 ug/l
156-59-2 cis-1,2-Dichloroethylene 149 50 13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 13 ug/l
78-87-5 1,2-Dichloropropane ND 50 13 ug/l
142-28-9 1,3-Dichloropropane ND 50 13 ug/l
594-20-7 2,2-Dichloropropane ND 50 13 ug/l
563-58-6 1,1-Dichloropropene ND 50 13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 31
FA6171433.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA61714-1 Date Sampled:02/19/19
Matrix:AQ - Ground Water Date Received:02/20/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 50 13 ug/l
100-41-4 Ethylbenzene 334 50 13 ug/l
87-68-3 Hexachlorobutadiene ND 50 13 ug/l
98-82-8 Isopropylbenzene 23.4 50 13 ug/l J
99-87-6 p-Isopropyltoluene 50.3 50 13 ug/l
74-83-9 Methyl Bromide ND 50 20 ug/l
74-87-3 Methyl Chloride ND 50 20 ug/l
74-95-3 Methylene Bromide ND 50 13 ug/l
75-09-2 Methylene Chloride ND 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 50 13 ug/l
91-20-3 Naphthalene 580 50 13 ug/l
103-65-1 n-Propylbenzene 51.8 50 13 ug/l
100-42-5 Styrene ND 50 13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 13 ug/l
127-18-4 Tetrachloroethylene 58.7 50 13 ug/l
108-88-3 Toluene 2800 50 13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 13 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 13 ug/l
79-01-6 Trichloroethylene 101 50 13 ug/l
75-69-4 Trichlorofluoromethane ND 50 20 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 13 ug/l
95-63-6 1,2,4-Trimethylbenzene 2950 50 13 ug/l
108-67-8 1,3,5-Trimethylbenzene 1190 50 13 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 3250 100 13 ug/l
95-47-6 o-Xylene 1970 50 13 ug/l
1330-20-7 Xylene (total)5210 150 25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 31
FA6171433.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA61714-2 Date Sampled:02/19/19
Matrix:AQ - Ground Water Date Received:02/20/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217151.D 1 02/21/19 15:31 AB n/a n/a VA2534
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.17 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 31
FA6171433.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA61714-2 Date Sampled:02/19/19
Matrix:AQ - Ground Water Date Received:02/20/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 1.4 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.15 0.50 0.13 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 0.89 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 0.53 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 2.8 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.71 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 1.3 1.0 0.13 ug/l
95-47-6 o-Xylene 0.14 0.50 0.13 ug/l J
1330-20-7 Xylene (total)1.4 1.5 0.25 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 91%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 31
FA6171433.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA61714-3 Date Sampled:02/19/19
Matrix:AQ - Ground Water Date Received:02/20/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0217153.D 100 02/21/19 16:17 AB n/a n/a VA2534
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1510 50 13 ug/l
108-86-1 Bromobenzene ND 50 13 ug/l
74-97-5 Bromochloromethane ND 50 13 ug/l
75-27-4 Bromodichloromethane ND 50 13 ug/l
75-25-2 Bromoform ND 50 13 ug/l
104-51-8 n-Butylbenzene ND 50 13 ug/l
135-98-8 sec-Butylbenzene ND 50 13 ug/l
98-06-6 tert-Butylbenzene ND 50 13 ug/l
56-23-5 Carbon Tetrachloride ND 50 13 ug/l
108-90-7 Chlorobenzene ND 50 13 ug/l
75-00-3 Chloroethane ND 50 20 ug/l
67-66-3 Chloroform ND 50 13 ug/l
95-49-8 o-Chlorotoluene ND 50 13 ug/l
106-43-4 p-Chlorotoluene ND 50 13 ug/l
124-48-1 Dibromochloromethane ND 50 13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 25 ug/l
106-93-4 1,2-Dibromoethane ND 50 13 ug/l
75-71-8 Dichlorodifluoromethane a ND 50 20 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 13 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 13 ug/l
75-34-3 1,1-Dichloroethane ND 50 13 ug/l
107-06-2 1,2-Dichloroethane ND 50 13 ug/l
75-35-4 1,1-Dichloroethylene ND 50 13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 13 ug/l
78-87-5 1,2-Dichloropropane ND 50 13 ug/l
142-28-9 1,3-Dichloropropane ND 50 13 ug/l
594-20-7 2,2-Dichloropropane ND 50 13 ug/l
563-58-6 1,1-Dichloropropene ND 50 13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 31
FA6171433.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA61714-3 Date Sampled:02/19/19
Matrix:AQ - Ground Water Date Received:02/20/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 50 13 ug/l
100-41-4 Ethylbenzene 411 50 13 ug/l
87-68-3 Hexachlorobutadiene ND 50 13 ug/l
98-82-8 Isopropylbenzene 16.7 50 13 ug/l J
99-87-6 p-Isopropyltoluene ND 50 13 ug/l
74-83-9 Methyl Bromide ND 50 20 ug/l
74-87-3 Methyl Chloride ND 50 20 ug/l
74-95-3 Methylene Bromide ND 50 13 ug/l
75-09-2 Methylene Chloride ND 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 50 13 ug/l
91-20-3 Naphthalene 122 50 13 ug/l
103-65-1 n-Propylbenzene 42.7 50 13 ug/l J
100-42-5 Styrene ND 50 13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 13 ug/l
127-18-4 Tetrachloroethylene ND 50 13 ug/l
108-88-3 Toluene 3770 50 13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 13 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 13 ug/l
79-01-6 Trichloroethylene ND 50 13 ug/l
75-69-4 Trichlorofluoromethane ND 50 20 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 13 ug/l
95-63-6 1,2,4-Trimethylbenzene 297 50 13 ug/l
108-67-8 1,3,5-Trimethylbenzene 85.5 50 13 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 1090 100 13 ug/l
95-47-6 o-Xylene 569 50 13 ug/l
1330-20-7 Xylene (total)1660 150 25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 93%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 31
FA6171433.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:PMW-6
Lab Sample ID:FA61714-4 Date Sampled:02/19/19
Matrix:AQ - Ground Water Date Received:02/20/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E098071.D 1000 02/21/19 13:29 AB n/a n/a VE2078
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1100 500 130 ug/l
108-86-1 Bromobenzene ND 500 130 ug/l
74-97-5 Bromochloromethane ND 500 130 ug/l
75-27-4 Bromodichloromethane ND 500 130 ug/l
75-25-2 Bromoform ND 500 130 ug/l
104-51-8 n-Butylbenzene ND 500 130 ug/l
135-98-8 sec-Butylbenzene ND 500 130 ug/l
98-06-6 tert-Butylbenzene ND 500 130 ug/l
56-23-5 Carbon Tetrachloride ND 500 130 ug/l
108-90-7 Chlorobenzene ND 500 130 ug/l
75-00-3 Chloroethane a ND 500 200 ug/l
67-66-3 Chloroform ND 500 130 ug/l
95-49-8 o-Chlorotoluene ND 500 130 ug/l
106-43-4 p-Chlorotoluene ND 500 130 ug/l
124-48-1 Dibromochloromethane ND 500 130 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 500 250 ug/l
106-93-4 1,2-Dibromoethane ND 500 130 ug/l
75-71-8 Dichlorodifluoromethane ND 500 200 ug/l
95-50-1 1,2-Dichlorobenzene ND 500 130 ug/l
541-73-1 1,3-Dichlorobenzene ND 500 130 ug/l
106-46-7 1,4-Dichlorobenzene ND 500 130 ug/l
75-34-3 1,1-Dichloroethane ND 500 130 ug/l
107-06-2 1,2-Dichloroethane ND 500 130 ug/l
75-35-4 1,1-Dichloroethylene ND 500 130 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 500 130 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 500 130 ug/l
78-87-5 1,2-Dichloropropane ND 500 130 ug/l
142-28-9 1,3-Dichloropropane ND 500 130 ug/l
594-20-7 2,2-Dichloropropane b ND 500 130 ug/l
563-58-6 1,1-Dichloropropene ND 500 130 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 500 130 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 500 130 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 31
FA6171433.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:PMW-6
Lab Sample ID:FA61714-4 Date Sampled:02/19/19
Matrix:AQ - Ground Water Date Received:02/20/19
Method:SM 6200B Percent Solids:n/a
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 500 130 ug/l
100-41-4 Ethylbenzene 3980 500 130 ug/l
87-68-3 Hexachlorobutadiene ND 500 130 ug/l
98-82-8 Isopropylbenzene ND 500 130 ug/l
99-87-6 p-Isopropyltoluene ND 500 130 ug/l
74-83-9 Methyl Bromide ND 500 200 ug/l
74-87-3 Methyl Chloride ND 500 200 ug/l
74-95-3 Methylene Bromide ND 500 130 ug/l
75-09-2 Methylene Chloride ND 2000 1000 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 500 130 ug/l
91-20-3 Naphthalene 507 500 130 ug/l
103-65-1 n-Propylbenzene 295 500 130 ug/l J
100-42-5 Styrene ND 500 130 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 500 130 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 500 130 ug/l
127-18-4 Tetrachloroethylene ND 500 130 ug/l
108-88-3 Toluene 35800 500 130 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 500 130 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 500 130 ug/l
71-55-6 1,1,1-Trichloroethane ND 500 130 ug/l
79-00-5 1,1,2-Trichloroethane ND 500 130 ug/l
79-01-6 Trichloroethylene ND 500 130 ug/l
75-69-4 Trichlorofluoromethane ND 500 200 ug/l
96-18-4 1,2,3-Trichloropropane ND 500 130 ug/l
95-63-6 1,2,4-Trimethylbenzene 2210 500 130 ug/l
108-67-8 1,3,5-Trimethylbenzene 673 500 130 ug/l
75-01-4 Vinyl Chloride ND 500 130 ug/l
m,p-Xylene 14500 1000 130 ug/l
95-47-6 o-Xylene 6540 500 130 ug/l
1330-20-7 Xylene (total)21100 1500 250 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
(a) Associated CCV outside control limits high.
(b) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 31
FA6171433.4
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
15 of 31
FA617144
FA61714: Chain of Custody
Page 1 of 2
16 of 31
FA6171444.1
Job Number:FA61714 Client:GRI
Date / Time Received:2/20/2019 9:30:00 AM Delivery Method:FED EX
Project:RAM 40
Airbill #'s:1015899912860003281100812565573234
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (4.0);
Cooler 1: (3.8);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:-0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP Date:Date:2/20/2019 9:30:00 AM
FA61714: Chain of Custody
Page 2 of 2
17 of 31
FA6171444.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
18 of 31
FA617145
Method Blank Summary Page 1 of 2
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2078-MB E098063.D 1 02/21/19 AB n/a n/a VE2078
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
19 of 31
FA6171455.1.1
Method Blank Summary Page 2 of 2
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2078-MB E098063.D 1 02/21/19 AB n/a n/a VE2078
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-4
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
20 of 31
FA6171455.1.1
Method Blank Summary Page 1 of 2
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2534-MB A0217148.D 1 02/21/19 AB n/a n/a VA2534
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-1, FA61714-2, FA61714-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
21 of 31
FA6171455.1.2
Method Blank Summary Page 2 of 2
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2534-MB A0217148.D 1 02/21/19 AB n/a n/a VA2534
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-1, FA61714-2, FA61714-3
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 91%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
22 of 31
FA6171455.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2078-BS E098061.D 1 02/21/19 AB n/a n/a VE2078
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10 100 70-130
108-86-1 Bromobenzene 10 9.6 96 70-130
74-97-5 Bromochloromethane 10 9.7 97 70-130
75-27-4 Bromodichloromethane 10 10.2 102 70-130
75-25-2 Bromoform 10 8.8 88 70-130
104-51-8 n-Butylbenzene 10 10.6 106 70-130
135-98-8 sec-Butylbenzene 10 10.4 104 70-130
98-06-6 tert-Butylbenzene 10 10.3 103 70-130
56-23-5 Carbon Tetrachloride 10 10.9 109 70-130
108-90-7 Chlorobenzene 10 9.6 96 70-130
75-00-3 Chloroethane 10 12.8 128 60-140
67-66-3 Chloroform 10 10.9 109 70-130
95-49-8 o-Chlorotoluene 10 10.1 101 70-130
106-43-4 p-Chlorotoluene 10 10 100 70-130
124-48-1 Dibromochloromethane 10 9.5 95 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.9 89 70-130
106-93-4 1,2-Dibromoethane 10 9.5 95 70-130
75-71-8 Dichlorodifluoromethane 10 9.5 95 60-140
95-50-1 1,2-Dichlorobenzene 10 9.4 94 70-130
541-73-1 1,3-Dichlorobenzene 10 9.9 99 70-130
106-46-7 1,4-Dichlorobenzene 10 9.5 95 70-130
75-34-3 1,1-Dichloroethane 10 10.8 108 70-130
107-06-2 1,2-Dichloroethane 10 10.5 105 70-130
75-35-4 1,1-Dichloroethylene 10 10.6 106 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.2 102 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.3 103 70-130
78-87-5 1,2-Dichloropropane 10 10 100 70-130
142-28-9 1,3-Dichloropropane 10 9.2 92 70-130
594-20-7 2,2-Dichloropropane 10 13.2 132*70-130
563-58-6 1,1-Dichloropropene 10 10.9 109 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.0 90 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.2 92 70-130
108-20-3 Di-Isopropyl Ether 10 9.8 98 70-130
100-41-4 Ethylbenzene 10 10.2 102 70-130
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
98-82-8 Isopropylbenzene 10 10.8 108 70-130
* = Outside of Control Limits.
23 of 31
FA6171455.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2078-BS E098061.D 1 02/21/19 AB n/a n/a VE2078
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.3 103 70-130
74-83-9 Methyl Bromide 10 8.9 89 60-140
74-87-3 Methyl Chloride 10 10.6 106 60-140
74-95-3 Methylene Bromide 10 10.2 102 70-130
75-09-2 Methylene Chloride 10 9.7 97 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.3 103 70-130
91-20-3 Naphthalene 10 9.6 96 70-130
103-65-1 n-Propylbenzene 10 10.1 101 70-130
100-42-5 Styrene 10 9.8 98 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.9 99 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.7 97 70-130
127-18-4 Tetrachloroethylene 10 10.0 100 70-130
108-88-3 Toluene 10 9.9 99 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.7 97 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.6 96 70-130
71-55-6 1,1,1-Trichloroethane 10 11.1 111 70-130
79-00-5 1,1,2-Trichloroethane 10 9.7 97 70-130
79-01-6 Trichloroethylene 10 10.1 101 70-130
75-69-4 Trichlorofluoromethane 10 10.5 105 60-140
96-18-4 1,2,3-Trichloropropane 10 9.7 97 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.8 98 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.1 101 70-130
75-01-4 Vinyl Chloride 10 8.5 85 60-140
m,p-Xylene 20 20.5 103 70-130
95-47-6 o-Xylene 10 10.3 103 70-130
1330-20-7 Xylene (total)30 30.8 103 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
* = Outside of Control Limits.
24 of 31
FA6171455.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2534-BS A0217146.D 1 02/21/19 AB n/a n/a VA2534
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-1, FA61714-2, FA61714-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.9 109 70-130
108-86-1 Bromobenzene 10 9.1 91 70-130
74-97-5 Bromochloromethane 10 10.6 106 70-130
75-27-4 Bromodichloromethane 10 10.6 106 70-130
75-25-2 Bromoform 10 8.4 84 70-130
104-51-8 n-Butylbenzene 10 9.2 92 70-130
135-98-8 sec-Butylbenzene 10 9.7 97 70-130
98-06-6 tert-Butylbenzene 10 8.7 87 70-130
56-23-5 Carbon Tetrachloride 10 11.4 114 70-130
108-90-7 Chlorobenzene 10 9.3 93 70-130
75-00-3 Chloroethane 10 10.8 108 60-140
67-66-3 Chloroform 10 11.0 110 70-130
95-49-8 o-Chlorotoluene 10 9.3 93 70-130
106-43-4 p-Chlorotoluene 10 9.1 91 70-130
124-48-1 Dibromochloromethane 10 8.6 86 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.1 81 70-130
106-93-4 1,2-Dibromoethane 10 8.9 89 70-130
75-71-8 Dichlorodifluoromethane 10 12.9 129 60-140
95-50-1 1,2-Dichlorobenzene 10 8.9 89 70-130
541-73-1 1,3-Dichlorobenzene 10 9.3 93 70-130
106-46-7 1,4-Dichlorobenzene 10 8.9 89 70-130
75-34-3 1,1-Dichloroethane 10 11.4 114 70-130
107-06-2 1,2-Dichloroethane 10 9.9 99 70-130
75-35-4 1,1-Dichloroethylene 10 12.4 124 70-130
156-59-2 cis-1,2-Dichloroethylene 10 11.2 112 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.9 109 70-130
78-87-5 1,2-Dichloropropane 10 10.5 105 70-130
142-28-9 1,3-Dichloropropane 10 8.5 85 70-130
594-20-7 2,2-Dichloropropane 10 12.5 125 70-130
563-58-6 1,1-Dichloropropene 10 11.4 114 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.9 89 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.3 83 70-130
108-20-3 Di-Isopropyl Ether 10 10.4 104 70-130
100-41-4 Ethylbenzene 10 9.8 98 70-130
87-68-3 Hexachlorobutadiene 10 9.4 94 70-130
98-82-8 Isopropylbenzene 10 10.8 108 70-130
* = Outside of Control Limits.
25 of 31
FA6171455.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2534-BS A0217146.D 1 02/21/19 AB n/a n/a VA2534
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-1, FA61714-2, FA61714-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.2 92 70-130
74-83-9 Methyl Bromide 10 9.7 97 60-140
74-87-3 Methyl Chloride 10 12.3 123 60-140
74-95-3 Methylene Bromide 10 10.3 103 70-130
75-09-2 Methylene Chloride 10 10.6 106 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.7 107 70-130
91-20-3 Naphthalene 10 8.9 89 70-130
103-65-1 n-Propylbenzene 10 9.3 93 70-130
100-42-5 Styrene 10 9.1 91 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.9 99 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.0 90 70-130
127-18-4 Tetrachloroethylene 10 9.9 99 70-130
108-88-3 Toluene 10 9.5 95 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.2 92 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.3 93 70-130
71-55-6 1,1,1-Trichloroethane 10 11.1 111 70-130
79-00-5 1,1,2-Trichloroethane 10 9.2 92 70-130
79-01-6 Trichloroethylene 10 10.7 107 70-130
75-69-4 Trichlorofluoromethane 10 10.6 106 60-140
96-18-4 1,2,3-Trichloropropane 10 8.6 86 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.1 91 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.5 95 70-130
75-01-4 Vinyl Chloride 10 11.7 117 60-140
m,p-Xylene 20 19.7 99 70-130
95-47-6 o-Xylene 10 9.9 99 70-130
1330-20-7 Xylene (total)30 29.6 99 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
* = Outside of Control Limits.
26 of 31
FA6171455.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA61691-2MS E098073.D 5 02/21/19 AB n/a n/a VE2078
FA61691-2MSD E098074.D 5 02/21/19 AB n/a n/a VE2078
FA61691-2 a E098072.D 1 02/21/19 AB n/a n/a VE2078
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-4
FA61691-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 7.4 50 52.0 89 50 52.7 91 1 70-130/20
108-86-1 Bromobenzene ND 50 45.0 90 50 46.5 93 3 70-130/20
74-97-5 Bromochloromethane ND 50 45.9 92 50 46.5 93 1 70-130/20
75-27-4 Bromodichloromethane ND 50 45.3 91 50 46.9 94 3 70-130/20
75-25-2 Bromoform ND 50 30.7 61*50 30.7 61*0 70-130/20
104-51-8 n-Butylbenzene ND 50 49.5 99 50 51.6 103 4 70-130/20
135-98-8 sec-Butylbenzene ND 50 49.4 99 50 51.3 103 4 70-130/20
98-06-6 tert-Butylbenzene ND 50 50.0 100 50 51.2 102 2 70-130/20
56-23-5 Carbon Tetrachloride ND 50 50.7 101 50 51.6 103 2 70-130/20
108-90-7 Chlorobenzene ND 50 45.9 92 50 46.6 93 2 70-130/20
75-00-3 Chloroethane ND 50 56.2 112 50 65.8 132 16 60-140/20
67-66-3 Chloroform ND 50 52.4 105 50 53.2 106 2 70-130/20
95-49-8 o-Chlorotoluene 0.40 J 50 48.4 96 50 50.0 99 3 70-130/20
106-43-4 p-Chlorotoluene ND 50 48.7 97 50 50.1 100 3 70-130/20
124-48-1 Dibromochloromethane ND 50 37.8 76 50 38.7 77 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 42.6 85 50 42.1 84 1 70-130/20
106-93-4 1,2-Dibromoethane ND 50 44.8 90 50 45.6 91 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 42.4 85 50 47.9 96 12 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 44.4 89 50 45.8 92 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 47.0 94 50 48.5 97 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 45.7 91 50 46.6 93 2 70-130/20
75-34-3 1,1-Dichloroethane ND 50 51.2 102 50 52.3 105 2 70-130/20
107-06-2 1,2-Dichloroethane ND 50 51.9 104 50 53.2 106 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 50.8 102 50 51.6 103 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 47.7 95 50 48.7 97 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 48.3 97 50 49.1 98 2 70-130/20
78-87-5 1,2-Dichloropropane ND 50 48.7 97 50 48.5 97 0 70-130/20
142-28-9 1,3-Dichloropropane ND 50 43.3 87 50 44.8 90 3 70-130/20
594-20-7 2,2-Dichloropropane ND 50 58.2 116 50 59.3 119 2 70-130/20
563-58-6 1,1-Dichloropropene ND 50 52.2 104 50 53.2 106 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 35.2 70 50 35.4 71 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 37.1 74 50 36.4 73 2 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 46.3 93 50 47.2 94 2 70-130/20
100-41-4 Ethylbenzene 10.1 50 53.8 87 50 55.4 91 3 70-130/20
87-68-3 Hexachlorobutadiene ND 50 46.1 92 50 48.8 98 6 70-130/20
98-82-8 Isopropylbenzene 0.56 50 51.7 102 50 52.7 104 2 70-130/20
* = Outside of Control Limits.
27 of 31
FA6171455.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA61691-2MS E098073.D 5 02/21/19 AB n/a n/a VE2078
FA61691-2MSD E098074.D 5 02/21/19 AB n/a n/a VE2078
FA61691-2 a E098072.D 1 02/21/19 AB n/a n/a VE2078
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-4
FA61691-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 48.9 98 50 50.5 101 3 70-130/20
74-83-9 Methyl Bromide ND 50 44.7 89 50 47.1 94 5 60-140/20
74-87-3 Methyl Chloride ND 50 44.7 89 50 47.0 94 5 60-140/20
74-95-3 Methylene Bromide ND 50 48.5 97 50 49.3 99 2 70-130/20
75-09-2 Methylene Chloride ND 50 46.8 94 50 47.1 94 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether 14.0 50 59.7 91 50 61.2 94 2 70-130/20
91-20-3 Naphthalene 5.0 50 45.3 81 50 47.3 85 4 70-130/20
103-65-1 n-Propylbenzene 1.5 50 48.9 95 50 50.3 98 3 70-130/20
100-42-5 Styrene ND 50 42.7 85 50 44.1 88 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 46.9 94 50 47.7 95 2 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 46.8 94 50 48.0 96 3 70-130/20
127-18-4 Tetrachloroethylene ND 50 47.6 95 50 48.5 97 2 70-130/20
108-88-3 Toluene 44.8 50 69.4 49*50 70.9 52*2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 41.0 82 50 44.1 88 7 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 42.9 86 50 45.6 91 6 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 52.8 106 50 54.5 109 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 45.5 91 50 46.9 94 3 70-130/20
79-01-6 Trichloroethylene ND 50 48.8 98 50 49.3 99 1 70-130/20
75-69-4 Trichlorofluoromethane ND 50 47.2 94 50 52.5 105 11 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 45.7 91 50 47.4 95 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene 15.8 50 55.8 80 50 57.2 83 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 3.2 50 50.5 95 50 51.7 97 2 70-130/20
75-01-4 Vinyl Chloride ND 50 38.2 76 50 42.4 85 10 60-140/20
m,p-Xylene 54.1 100 127 73 100 130 76 2 70-130/20
95-47-6 o-Xylene 25.4 50 61.9 73 50 62.8 75 1 70-130/20
1330-20-7 Xylene (total)79.5 150 189 73 150 192 75 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA61691-2 Limits
1868-53-7 Dibromofluoromethane 106%107%105%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%117%115%70-130%
2037-26-5 Toluene-D8 99%99%97%70-130%
460-00-4 4-Bromofluorobenzene 103%103%102%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values. Confirmation
* = Outside of Control Limits.
28 of 31
FA6171455.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA61691-2MS E098073.D 5 02/21/19 AB n/a n/a VE2078
FA61691-2MSD E098074.D 5 02/21/19 AB n/a n/a VE2078
FA61691-2 a E098072.D 1 02/21/19 AB n/a n/a VE2078
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-4
run.
* = Outside of Control Limits.
29 of 31
FA6171455.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA61714-2MS A0217154.D 5 02/21/19 AB n/a n/a VA2534
FA61714-2MSD A0217155.D 5 02/21/19 AB n/a n/a VA2534
FA61714-2 A0217151.D 1 02/21/19 AB n/a n/a VA2534
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-1, FA61714-2, FA61714-3
FA61714-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 0.17 J 50 55.4 110 50 56.5 113 2 70-130/20
108-86-1 Bromobenzene ND 50 46.9 94 50 48.1 96 3 70-130/20
74-97-5 Bromochloromethane ND 50 51.6 103 50 53.5 107 4 70-130/20
75-27-4 Bromodichloromethane ND 50 51.4 103 50 51.7 103 1 70-130/20
75-25-2 Bromoform ND 50 36.0 72 50 34.1 68*5 70-130/20
104-51-8 n-Butylbenzene ND 50 46.1 92 50 47.9 96 4 70-130/20
135-98-8 sec-Butylbenzene ND 50 49.5 99 50 51.4 103 4 70-130/20
98-06-6 tert-Butylbenzene ND 50 45.3 91 50 46.5 93 3 70-130/20
56-23-5 Carbon Tetrachloride ND 50 52.3 105 50 54.5 109 4 70-130/20
108-90-7 Chlorobenzene ND 50 47.1 94 50 48.5 97 3 70-130/20
75-00-3 Chloroethane ND 50 41.7 83 50 49.6 99 17 60-140/20
67-66-3 Chloroform ND 50 53.1 106 50 54.9 110 3 70-130/20
95-49-8 o-Chlorotoluene ND 50 47.6 95 50 49.4 99 4 70-130/20
106-43-4 p-Chlorotoluene ND 50 46.9 94 50 48.1 96 3 70-130/20
124-48-1 Dibromochloromethane ND 50 40.4 81 50 39.5 79 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 41.1 82 50 42.4 85 3 70-130/20
106-93-4 1,2-Dibromoethane ND 50 45.4 91 50 46.8 94 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 54.1 108 50 60.0 120 10 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 45.7 91 50 47.6 95 4 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 47.7 95 50 49.3 99 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 45.7 91 50 46.4 93 2 70-130/20
75-34-3 1,1-Dichloroethane ND 50 55.0 110 50 56.6 113 3 70-130/20
107-06-2 1,2-Dichloroethane ND 50 49.7 99 50 51.0 102 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 53.5 107 50 61.0 122 13 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 54.4 109 50 55.7 111 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 52.7 105 50 54.9 110 4 70-130/20
78-87-5 1,2-Dichloropropane ND 50 53.8 108 50 55.1 110 2 70-130/20
142-28-9 1,3-Dichloropropane ND 50 43.7 87 50 44.7 89 2 70-130/20
594-20-7 2,2-Dichloropropane ND 50 57.6 115 50 57.0 114 1 70-130/20
563-58-6 1,1-Dichloropropene ND 50 56.5 113 50 58.0 116 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 44.0 88 50 43.3 87 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 42.5 85 50 42.3 85 0 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 50.8 102 50 52.8 106 4 70-130/20
100-41-4 Ethylbenzene 1.4 50 49.3 96 50 51.0 99 3 70-130/20
87-68-3 Hexachlorobutadiene ND 50 45.4 91 50 47.8 96 5 70-130/20
98-82-8 Isopropylbenzene 0.15 J 50 52.3 104 50 54.4 109 4 70-130/20
* = Outside of Control Limits.
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FA6171455.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA61714
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 40; 925 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA61714-2MS A0217154.D 5 02/21/19 AB n/a n/a VA2534
FA61714-2MSD A0217155.D 5 02/21/19 AB n/a n/a VA2534
FA61714-2 A0217151.D 1 02/21/19 AB n/a n/a VA2534
The QC reported here applies to the following samples:Method: SM 6200B
FA61714-1, FA61714-2, FA61714-3
FA61714-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 46.7 93 50 48.8 98 4 70-130/20
74-83-9 Methyl Bromide ND 50 36.6 73 50 41.4 83 12 60-140/20
74-87-3 Methyl Chloride ND 50 52.9 106 50 56.4 113 6 60-140/20
74-95-3 Methylene Bromide ND 50 52.7 105 50 53.7 107 2 70-130/20
75-09-2 Methylene Chloride ND 50 52.9 106 50 54.9 110 4 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 51.1 102 50 53.1 106 4 70-130/20
91-20-3 Naphthalene 0.89 50 43.7 86 50 48.1 94 10 70-130/20
103-65-1 n-Propylbenzene 0.53 50 48.6 96 50 50.3 100 3 70-130/20
100-42-5 Styrene ND 50 45.1 90 50 45.9 92 2 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 46.9 94 50 48.8 98 4 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 46.9 94 50 49.4 99 5 70-130/20
127-18-4 Tetrachloroethylene ND 50 49.7 99 50 51.2 102 3 70-130/20
108-88-3 Toluene ND 50 47.7 95 50 48.9 98 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 43.9 88 50 48.3 97 10 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 45.3 91 50 48.2 96 6 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 52.6 105 50 54.4 109 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 46.8 94 50 48.4 97 3 70-130/20
79-01-6 Trichloroethylene ND 50 53.7 107 50 54.6 109 2 70-130/20
75-69-4 Trichlorofluoromethane ND 50 41.8 84 50 47.0 94 12 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 43.3 87 50 44.8 90 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2.8 50 49.4 93 50 51.3 97 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 0.71 50 49.2 97 50 50.7 100 3 70-130/20
75-01-4 Vinyl Chloride ND 50 48.9 98 50 53.8 108 10 60-140/20
m,p-Xylene 1.3 100 98.0 97 100 102 101 4 70-130/20
95-47-6 o-Xylene 0.14 J 50 48.1 96 50 50.6 101 5 70-130/20
1330-20-7 Xylene (total)1.4 J 150 146 96 150 152 100 4 70-130/20
CAS No.Surrogate Recoveries MS MSD FA61714-2 Limits
1868-53-7 Dibromofluoromethane 104%104%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%98%103%70-130%
2037-26-5 Toluene-D8 92%93%91%70-130%
460-00-4 4-Bromofluorobenzene 100%98%98%70-130%
* = Outside of Control Limits.
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