WA-802_11085_CA_MRP_20180228

EXECUTIVE SUMMARY
The Granny’s Grill & Leggett’s Grocery sites are located at the northwestern and southwestern corners of the
intersection of Early Station Road and US Highway 13 in Windsor, Bertie County, North Carolina. According to
available information, two 1,000-gallon and one 550-gallon USTs were removed from the Granny’s Grill site in
September 1993. The Leggett’s Grocery site contained four USTs (three 2,000 gallon gasoline and one 1,000
gallon diesel), which were removed in February 1994. A Corrective Action Plan, proposing the installation of a
ground water pump and treat system, was submitted for the site on October 15, 1996. The corrective action
system (CAS), along with four associated recovery wells (RW-1 through RW-4), were installed in October and
November of 1999. The CAS was activated on February 7, 2000 and ran until May 2005, when it was
deactivated due to lack of funding. The site is currently ranked high risk due to inactive water supply wells within
250-feet and potable water supply wells within 1,000-feet of the source area.

Three Type II monitoring wells were gauged, purged and sampled on February 13, 2018. Concentrations of
requested method constituents that exceeded the MACs were reported in the ground water samples. None of the
reported concentrations exceeded the gross contamination levels.

Upon completion of the ground water sampling event, oxygen releasing compound (ORC-A) socks were installed
in MW-3, MW-10 and MW-17.

Based on this information, GRI recommends that semi-annual ground water monitoring continue at the site. Field
parameter readings including dissolved oxygen, temperature, pH, conductivity and oxygen reduction potential
should be collected in order to evaluate the ORC-A socks effectiveness. The ORC-A socks installed in MW-3,
MW-10 and MW-17 should be replaced following the next ground water monitoring event. The next ground
water monitoring event is tentatively scheduled for August 2018.

TABLE OF CONTENTS
1.0 SITE HISTORY AND CHARACTERIZATION .............................................................................. 1
2.0 CURRENT SITE ACTIVITIES .......................................................................................................... 1
3.0 GROUND WATER QUALITY ........................................................................................................... 2
4.0 CONCLUSIONS AND RECOMMENDATIONS .............................................................................. 2
5.0 LIMITATIONS...................................................................................................................................... 3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results
Table 2A: Summary of Field Parameters Results

APPENDICES
Appendix A: Laboratory Report - Ground Water Samples
Appendix B: Injection Event Record

1

1.0 SITE HISTORY AND CHARACTERIZATION
According to the available information, two 1,000-gallon and one 550-gallon gasoline underground storage tanks
(USTs) were removed from the Granny’s Grill site in September 1993. A total of fourteen Type II monitoring
wells (MW-1 through MW-3, MW-5 through MW-11, and MW-13 through MW-16) and two Type III
monitoring wells (MWD-4 and MWD-12) were installed during previous ground water assessment and corrective
action activities. Monitoring wells MW-1, MWD-4 and MWD-12 were abandoned during past ground water
assessment activities and were replaced with the installation of MW-17 and MWD-18. The Leggett’s Grocery
site contained four USTs (three 2,000 gallon gasoline and one 1,000 gallon diesel), which were removed in
February 1994. Five monitoring wells (LMW-1 through LMW-5) were installed to evaluate the Leggett’s
Grocery release. A Corrective Action Plan, proposing the installation of a ground water pump and treat system,
was submitted for the site on October 15, 1996. The corrective action system (CAS), along with four associated
recovery wells (RW-1 through RW-4), were installed in October and November of 1999. The CAS was activated
on February 7, 2000, and operated until May 2005, when it was deactivated due to lack of funding.

Assessment and corrective action activities prior to January 2010 were conducted by past consultants. Although
Geological Resources, Inc. (GRI) cannot verify the accuracy of information obtained from past reports, for the
purposes of this report, it is assumed to be correct. Please refer to previous submittals for further historical
information regarding the site.

2.0 CURRENT SITE ACTIVITIES
This report presents the results of the ground water monitoring activities conducted on February 13, 2018, at the
Granny’s Grill & Leggett’s Grocery site, located at the northwestern and southwestern corners of the intersection
of Early Station Road and US Highway 13 in Windsor, Bertie County, North Carolina (Figures 1 and 2). The
activities were conducted in accordance with GRI proposal number 17-270, which was submitted to NCDEQ on
April 12, 2017, and approved as Task Authorization No. 11085-054 on April 17, 2017, and also GRI proposal
number 18-049, which was submitted to NCDEQ on January 29, 2018, and approved as Task Authorization No.
11085-055 on February 1, 2018. The purpose of the activities was to obtain current ground water quality data for
the site and to install Oxygen Releasing Compound-Advanced (ORC-A) socks.

2

3.0 GROUND WATER QUALITY
Three Type II monitoring wells (MW-3, MW-10, and MW-17) were gauged, purged and sampled on February 13,
2018. The depths to ground water in the Type II monitoring wells measured during the February 2018 sampling
event ranged from 0.70 to 0.74 feet below the tops of well casings. Ground water elevations in the Type II
monitoring wells relative to mean sea level ranged from 44.34 to 45.95 feet. The horizontal hydraulic gradient
was approximately 0.02 feet per foot. A Site Map showing the location of the site and other structures is included
as Figure 3. A Water Table Surface Map for the February 13, 2018, gauging event has been included as Figure
4. A summary of well construction information including ground water elevation data is presented in Table 1.

The collected ground water samples were submitted for laboratory analyses of volatile organic compounds using
EPA Method 6200B.

Concentrations of one or more BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane, 1,2-dichlorobenzene,
1,4-dichlorobenzene, n-propylbenzene and/or 1,2,4-trimethylbenzene that exceeded the Maximum Allowable
Concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the ground water samples collected
from MW-3, MW-10 and MW-17. None of the reported concentrations exceeded the Gross Contamination
Levels (GCLs). A Ground Water Quality Map based on data from the February 2018 sampling event has been
included as Figure 5. A summary of ground water sample analytical results is presented in Table 2. A complete
laboratory report has been included as Appendix A.

Field parameter data (dissolved oxygen, temperature, pH and oxygen reduction potential) were collected before
and after each well was purged during the February 2018 sampling event. After each well had been sampled and
field parameters had been taken, ORC-A socks were installed in MW-3, MW-10 and MW-17. A summary of the
field parameter results is included as Table 2A. A copy of the injection event record for the ORC-A socks is
included as Appendix B.

4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to water in the Type II monitoring wells during the February 2018 sampling event was
0.72 feet below the tops of well casings.

3

 Concentrations of one or more BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane, 1,2-
dichlorobenzene, 1,4-dichlorobenzene, n-propylbenzene and/or 1,2,4-trimethylbenzene that exceeded the
MACs were reported in the ground water samples collected from MW-3, MW-10 and MW-17. None of
the reported contaminant concentrations exceeded the GCLs.
 ORC-A socks were installed in MW-3, MW-10 and MW-17 upon completion of the February 2018
sampling event.
 Based on this information, GRI recommends that semi-annual ground water monitoring continue at the
site. Field parameter readings including dissolved oxygen, temperature, pH, conductivity and oxygen
reduction potential should be collected in order to evaluate the ORC-A socks effectiveness. The ORC-A
socks installed in MW-3, MW-10 and MW-17 should be replaced following the next ground water
monitoring event. The next ground water monitoring event is tentatively scheduled for August 2018.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for the specific application
to the reference site in Bertie County, North Carolina. The assessment was conducted based on the scope of work
and level of effort desired by NCDEQ and with resources adequate only for that scope of work. Our findings
have been developed in accordance with generally accepted standards of environmental practices in the State of
North Carolina, available information, and our professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations sampled
and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as
being meaningful with respect to parameters indicated in the laboratory report. No additional information can
logically be inferred from these data. Please note that field data collected prior to the January 2010 Aggressive
Fluid-Vapor Recovery event were not obtained under the supervision of GRI. Although the accuracy of these data
cannot be verified, for the purpose of this report GRI assumes that they are correct.

FIGURES
"J
DW-1
"JDW-2
"J DW-3
"J
WSW-1
"JWSW-2
"JWSW-3
"J
WSW-4
"J
WSW-5
"J
WSW-6"J
WSW-7
"J
WSW-8
Granny's Grill
Leggett's Grocery
6806098753
6806187674
6806187674US 13ASKEWVILLE
EARLY STATION
6806084171
6806194725
6806087461
6806191138
5896999373
6806096195
6806194163
6806280504
6806180013
6806089788
6806088695
68061819266806089992
RED BUD³
FIGURE 2SITE VICINITY MAPGRANNY'S GRILL & LEGGETT'S GROCERY1727 & 1731 U.S. HIGHWAY 13 NORTHWINDSOR, BERTIE COUNTY,NORTH CAROLINAINCIDENT NO.'s 11085 / 12111GRI PROJECT NO. 2924
PREPARED BY:GEOLOGICAL RESOURCES, INC.MARCH 3, 2016
NOTE:THIS MAP IS BASED ON DATA FROM THE BERTIE COUNTY GIS OF NC.
Legend
Road Centerline
Stream or Creek Line
6806191138 Parcel ID Number
Water Supply Well
"J Potable
"J Non-potable
"J Inactive; no electricity
0 300 600150Feet
SCALE: 1 INCH = 300 FEET
250-FT RADIUS
1,000-FT RADIUS
1,500-FT RADIUS
White Oak Swamp Creek
ApproximateSite Center

TABLES
Facility ID #s: 0-000732 & 0-025021
02/22/10 1.45 96.13
08/16/10 2.58 95.00
03/02/11 1.75 43.02
01/26/12 1.67 43.10
12/05/12 NM NM
07/25/13 0.53 44.24
05/07/14 1.43 43.34
10/28/14 3.17 41.60
05/05/15 1.50 43.27
02/22/10 0.75 96.39
08/16/10 1.62 95.52
03/02/11 0.80 43.52
01/26/12 0.43 43.89
12/05/12 NM NM
07/25/13 NM NM
02/22/10 2.20 95.04
08/16/10 3.24 94.00
03/02/11 1.60 42.82
01/26/12 0.83 43.59
12/05/12 3.92 40.50
07/25/13 1.86 42.56
05/09/14 2.98 41.44
10/28/14 1.62 42.80
05/05/15 1.68 42.74
02/22/10 1.45 96.05
08/16/10 2.92 94.58
03/02/11 2.38 42.35
01/26/12 0.89 43.84
12/05/12 2.78 41.95
07/25/13 2.11 42.62
05/09/14 1.07 43.66
10/28/14 2.54 42.19
05/05/15 1.37 43.36
02/22/10 1.37 94.97
08/16/10 4.40 91.94
03/02/11 1.25 42.34
01/26/12 0.65 42.94
12/05/12 1.00 42.59
07/25/13 1.99 41.60
05/07/14 1.56 42.03
10/28/14 2.42 41.17
05/05/15 1.36 42.23
02/22/10 0.65 99.35
08/16/10 4.75 95.25
03/02/11 1.73 45.47
01/26/12 1.10 46.10
12/05/12 NM NM Abandoned
02/22/10 1.69 97.79
08/16/10 4.19 95.29
03/02/11 2.23 44.34
01/26/12 1.56 45.01
12/05/12 3.54 43.03
07/25/13 2.11 44.46
05/07/14 1.71 44.86
10/28/14 3.41 43.16
05/05/15 1.64 44.93
02/06/17 2.09 44.48
02/22/10 1.31 98.00
08/16/10 4.35 94.96
03/02/11 1.78 44.90
01/26/12 0.88 45.80
12/05/12 3.53 43.15
07/25/13 1.78 44.90
05/07/14 1.25 45.43
10/28/14 3.55 43.13
05/05/15 1.48 45.20
02/06/17 1.83 44.85
02/13/18 0.73 45.95
44.77
3-133
5
08/01/94
MW-2
LMW-3 3-13
11/17/95
43.59
3
11/17/95LMW-4 3
44.42
3
97.50
44.73
3-13
12/13/93
Comments
12/13/93
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
LMW-5
Screened
Interval
(x to y ft. BGS)
Depth to Water
from Top of
Casing
(ft.)
Groundwater
Elevation*
(ft.)
Well ID
96.34
100.00
MW-1 5
07/29/94LMW-1
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
Top of Casing
Elevation*
(ft.)
Free Product
Thickness**
(ft.)
97.58
LMW-2
97.14
97.24
46.57
5-15
99.31
47.20
99.48
3-13
Date: 02/23/18
08/01/94
44.32
3-133
46.68
5-15512/13/93
5-15
MW-3
Page 1 of 3
Facility ID #s: 0-000732 & 0-025021
Comments
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Depth to Water
from Top of
Casing
(ft.)
Groundwater
Elevation*
(ft.)
Well ID
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
Top of Casing
Elevation*
(ft.)
Free Product
Thickness**
(ft.)
Date: 02/23/18
02/22/10 4.64 95.58
08/16/10 5.98 94.24
03/02/11 5.40 41.99
01/26/12 6.12 41.27
12/05/12 NM NM Abandoned
02/22/10 1.22 98.91
08/16/10 5.43 94.70
03/02/11 2.02 45.24
01/26/12 1.56 45.70
12/05/12 NM NM
07/25/13 NM NM
02/22/10 NM NM Not Found
08/16/10 NM NM Not Found
01/26/12 NM NM Not Found
12/05/12 NM NM Not Found
07/25/13 NM NM Not Found
02/22/10 1.27 98.80
08/16/10 4.35 95.72
03/02/11 0.91 45.51
01/26/12 0.41 46.01
12/05/12 NM NM
07/25/13 NM NM
02/22/10 1.30 97.40
08/16/10 3.93 94.77
03/02/11 2.73 43.12
01/26/12 2.24 43.61
12/05/12 3.14 42.71
07/25/13 1.68 44.17
05/07/14 1.49 44.36
10/28/14 3.00 42.85
05/05/15 1.25 44.60
02/06/17 1.60 44.25
02/22/10 0.68 96.54
08/16/10 2.75 94.47
03/02/11 1.78 42.47
01/26/12 0.21 44.04
12/05/12 2.39 41.86
07/25/13 1.54 42.71
05/07/14 0.28 43.97
10/28/14 2.35 41.90
05/05/15 0.42 43.83
02/06/17 0.72 43.53
02/22/10 0.73 98.07
08/16/10 3.47 95.33
03/02/11 1.53 43.51
01/26/12 0.53 44.51
12/05/12 2.58 42.46
07/25/13 1.48 43.56
05/07/14 0.82 44.22
10/28/14 2.85 42.19
05/05/15 0.90 44.14
02/06/17 1.07 43.97
02/13/18 0.70 44.34
02/22/10 1.15 97.53
08/16/10 6.09 92.59
03/02/11 1.52 44.36
01/26/12 0.95 44.93
12/05/12 3.04 42.84
07/25/13 2.38 43.50
05/07/14 1.31 44.57
10/28/14 3.44 42.44
05/05/15 1.50 44.38
02/06/17 1.52 44.36
02/22/10 6.04 93.65
08/16/10 8.77 90.92
03/02/11 6.71 40.18
01/26/12 5.64 41.25
12/05/12 NM NM Abandoned
5
10/05/99
06/21/95
5
34
MW-11
MW-9A
98.80
44.25
5-15
45.88
5-15
MW-8 5-15506/20/95
MW-7
MW-6
MW-5
1.5 1.5-11.5
100.07
1.5
MWD-12
99.69
46.89
34-39
MWD-4
100.13
47.39
1.504/26/94
45.85
47.26
98.70
100.22
100.23
25-30
97.22
11/15/95
04/26/94
04/26/94
98.68
5-15506/21/95
1.5-11.5
04/25/94
46.42
MW-10
1.5-11.5
25
45.04
Page 2 of 3
Facility ID #s: 0-000732 & 0-025021
Comments
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft. BGS)
Depth to Water
from Top of
Casing
(ft.)
Groundwater
Elevation*
(ft.)
Well ID
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
Top of Casing
Elevation*
(ft.)
Free Product
Thickness**
(ft.)
Date: 02/23/18
02/22/10 2.37 97.61
08/16/10 5.01 94.97
03/02/11 2.71 44.44
01/26/12 2.39 44.76
12/05/12 4.28 42.87
07/25/13 2.59 44.56
05/07/14 2.39 44.76
10/28/14 3.52 43.63
05/05/15 2.13 45.02
02/22/10 2.35 95.92
08/16/10 4.14 94.13
03/02/11 2.10 43.37
01/26/12 1.60 43.87
12/05/12 3.05 42.42
07/25/13 2.31 43.16
05/07/14 1.41 44.06
10/28/14 3.15 42.32
02/22/10 2.10 96.23
08/16/10 3.84 94.49
03/02/11 2.14 43.63
01/26/12 1.83 43.94
12/05/12 3.76 42.01
07/25/13 2.38 43.39
05/07/14 2.26 43.51
10/28/14 3.69 42.08
05/05/15 1.70 44.07
02/22/10 2.25 94.38
08/16/10 3.16 93.47
03/02/11 1.03 42.74
01/26/12 0.91 42.86
12/05/12 2.32 41.45
07/25/13 1.85 41.92
05/07/14 2.75 41.02
10/28/14 2.60 41.17
05/05/15 0.95 42.82
02/06/17 1.56 42.21
12/05/12 3.11 42.57
07/25/13 1.52 44.16
05/07/14 0.95 44.73
10/28/14 3.13 42.55
05/05/15 NM NM Top of Casing
02/06/17 1.43 44.25
02/13/18 0.74 44.94
12/05/12 6.52 38.57
07/25/13 4.66 40.43
05/07/14 2.19 42.90
10/28/14 5.50 39.59
05/05/15 2.87 42.22
02/06/17 3.61 41.48
05/07/14 3.29 42.26
10/28/14 6.06 39.49
05/05/15 3.42 42.13
RW-1 10/04/99 02/06/17 10 10-35 NM 4.04 NM
Notes:
• *ft BGS : feet below ground surface
• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
• Original top-of-casing elevations and well construction information are reproduced from previous report titled, 'Semiannual Groundwater Monitoring Event
(October 2004)' dated May 3, 2005, by Coastal Environmental Services, Inc.
• Top-of-casing elevations re-surveyed in April 2011 by The East Group.
• NM: Not measured.
45.0925-302505/09/12MWD-18
MW-16
3
311/17/95
MW-15
MW-14
45.77
96.63
6005/07/14TW-1
3-13
43.77
3-13
98.33
99.98
98.27
47.15
3-13
11/17/95
311/17/95MW-13
3-13311/16/95
45.5560-65
45.47
45.683-13305/09/12MW-17
Page 3 of 3
Date : 02/26/18 Facility ID #s: 0-000732 & 0-025021
EPA
Method
610
EPA
Method
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 30,000 700 28,500 25,000 12,500 15,000 NE NE NE NE
02/22/10 0.508 J <0.190 0.187 J <0.220 3.80 <0.500 <0.220 0.454 J <0.220 <0.170 <0.150 <0.180 <0.680 9.25 <100 112 225 <270
08/17/10 0.285 J <0.190 0.157 J 0.335 J 6.63 0.691 J <0.220 0.726 J <0.220 <0.170 0.169 J <0.180 NR NR NR NR NR NR
03/02/11 <0.700 <0.950 <0.750 <1.10 3.73 J <2.50 <1.10 <0.750 <1.10 <0.850 <0.750 <0.900 NR 6.54 <100 <198.0 <196 <267
01/26/12 0.49 J <0.13 0.17 J <0.30 3.3 0.37 J <0.16 0.33 J <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 53.7
12/05/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/25/13 0.15 J <0.10 0.21 J <0.22 4.7 1.2 J <0.10 0.74 0.13 J <0.10 <0.10 <0.10 NR 6.3 63.1 J 133 <96 <175
05/08/14 0.25 J <0.10 <0.10 <0.20 0.83 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <5.0 <35 <165 <130 <235
10/28/14 <0.10 <0.10 <0.10 <0.20 3.4 0.32 J <0.10 0.33 J <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
05/05/15 <0.17 <0.17 <0.15 <0.43 0.34 J <0.12 <0.16 <0.12 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
02/22/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 <0.756 6.33 <100 <211 <222 <289
08/17/10 <0.140 <0.190 <0.150 <0.220 0.476 J <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 4.67 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR 46.3 <100 <196.2 <192 <263
01/26/12 <0.13 <0.13 <0.15 <0.30 1.2 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/25/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/22/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 <0.680 22.8 <100 <200 <200 <270
08/17/10 <0.140 <0.190 <0.150 <0.220 1.24 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 0.639 J <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR 5.58 <100 98.6 <185 <257
01/26/12 <0.13 <0.13 <0.15 <0.30 0.86 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 <0.10 <0.10 <0.10 <0.22 2.3 0.17 J <0.10 0.13 J <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
07/25/13 <0.10 <0.10 <0.10 <0.22 1.2 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR 9.1 <35 <131 <96 <175
05/08/14 <0.10 <0.10 <0.10 <0.20 0.96 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR 10.9 <35 <135 <100 <185
10/28/14 <0.10 <0.10 <0.10 <0.20 1.4 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
05/05/15 <0.17 <0.17 <0.15 <0.43 1.5 <0.12 <0.16 <0.12 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
GCL (mg/l)
LMW-3
LMW-1
LMW-2 EthylbenzeneIsopropylbenzeneMTBE2L Standard (mg/l)
Contaminant of Concern C19-C36 Aliphatics1,3,5-Trimethylbenzene1,2-DichloroethaneXylenes1,2,4-TrimethylbenzeneNaphthalenen-PropylbenzeneAnalytical Method
→ C9-C22 AromaticsEPA Method 6200B
C5-C8 AliphaticsC9-C18 AliphaticsTolueneTetrachloroetheneLeadBenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
MADEP Method
VPH/EPH
2-MethylnaphthalenePage 1 of 8
Date : 02/26/18 Facility ID #s: 0-000732 & 0-025021
EPA
Method
610
EPA
Method
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 30,000 700 28,500 25,000 12,500 15,000 NE NE NE NEGCL (mg/l)EthylbenzeneIsopropylbenzeneMTBE2L Standard (mg/l)
Contaminant of Concern C19-C36 Aliphatics1,3,5-Trimethylbenzene1,2-DichloroethaneXylenes1,2,4-TrimethylbenzeneNaphthalenen-PropylbenzeneAnalytical Method
→ C9-C22 AromaticsEPA Method 6200B
C5-C8 AliphaticsC9-C18 AliphaticsTolueneTetrachloroetheneLeadBenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
MADEP Method
VPH/EPH
2-Methylnaphthalene02/22/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 <0.680 <1.50 <100 <200 <200 <270
08/17/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR <1.50 <100 <196.2 <192 <263
01/26/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
07/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <5.0 <35 <132 <97 <185
05/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <5.0 <35 <135 <100 <185
10/28/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
05/05/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
02/22/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 <0.716 11.1 <100 <205 <211 <279
08/17/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR 7.40 NR NR NR NR
01/26/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
07/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR 6.0 <35 <131 <96 <175
05/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <5.0 <35 <135 <100 <185
10/28/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
05/05/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
02/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 <0.680 5.18 1,060 128 <200 508
08/17/10 <0.140 <0.190 <0.150 <0.220 0.266 J <0.500 <0.220 <0.150 <0.220 0.312 J <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR 13.2 NR NR NR NR
01/27/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-1
(Abandoned)
LMW-5
LMW-4
Page 2 of 8
Date : 02/26/18 Facility ID #s: 0-000732 & 0-025021
EPA
Method
610
EPA
Method
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 30,000 700 28,500 25,000 12,500 15,000 NE NE NE NEGCL (mg/l)EthylbenzeneIsopropylbenzeneMTBE2L Standard (mg/l)
Contaminant of Concern C19-C36 Aliphatics1,3,5-Trimethylbenzene1,2-DichloroethaneXylenes1,2,4-TrimethylbenzeneNaphthalenen-PropylbenzeneAnalytical Method
→ C9-C22 AromaticsEPA Method 6200B
C5-C8 AliphaticsC9-C18 AliphaticsTolueneTetrachloroetheneLeadBenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
MADEP Method
VPH/EPH
2-Methylnaphthalene02/23/10 0.778 J <0.190 0.446 J <0.220 1.40 <0.500 <0.220 0.349 J 0.309 J <0.170 <0.150 <0.180 <0.680 1.58 <100 <200 <200 <270
08/17/10 0.329 J <0.190 <0.150 <0.220 1.69 0.972 J <0.220 0.460 J <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 4.48 <0.190 4.35 1.26 1.44 3.12 <0.220 1.38 1.16 <0.170 1.06 0.748 J NR 4.98 <100 121 <196 <267
01/27/12 0.71 <0.13 0.35 <0.30 1.2 1.1 <0.16 0.44 J 0.19 J <0.14 0.14 J <0.10 NR NR 37.8 9.2 <100 37.9
12/05/12 0.44 J <0.10 0.33 J <0.22 1.3 0.76 <0.10 0.47 J 0.20 J <0.10 <0.10 <0.10 NR NR NR NR NR NR
07/25/13 0.19 J <0.10 0.14 J <0.22 1.0 0.68 <0.10 0.43 J <0.10 <0.10 <0.10 <0.10 NR <5.0 41.0 J 61.8 J <97 <185
05/08/14 2.7 <0.10 1.5 1.2 J 0.69 2.9 <0.10 3.1 1.4 <0.10 0.69 0.20 J NR <5.0 55.5 J <135 <100 113
10/28/14 1.1 0.13 J 0.55 0.51 J 0.77 4.1 <0.10 2.1 0.62 <0.10 0.29 J <0.10 NR NR NR NR NR NR
05/05/15 3.8 0.57 1.9 0.95 J 0.85 6.9 <0.16 3.8 1.7 <0.15 0.55 <0.14 NR NR NR NR NR NR
02/06/17 0.76 <0.13 0.78 <0.25 0.56 1.1 <0.13 0.66 0.52 <0.13 <0.13 <0.13 NR NR NR NR NR NR
MW-3 02/23/10 1,440 9,860 1,530 9,990 <50.0 534 <44.0 76.6 J 203 <34.0 2,850 656 189 13.1 10,900 2,012 <200 5,050
08/17/10 2,330 5,640 512 2,820 <50.0 424 55.0 J 41.0 J 72.0 J <34.0 681 165 J NR NR NR NR NR NR
03/02/11 741 3,540 599 2,890 <125 379 J <110 <75.0 <110 <85.0 778 192 J NR 20.6 13,800 12,190 <196 7,710
01/27/12 132 798 175 1,170 <2.6 111 <3.3 15.3 55.4 <2.7 513 136 NR NR 3,020 3,630 <100 5,540
12/05/12 5,800 19,300 1,870 8,140 59.8 J 411 41.3 J 41.7 J 160 <25 1,230 292 NR NR NR NR NR NR
07/25/13 503 2,470 546 2,310 <5.0 197 <5.0 18.4 J 66.3 <5.0 558 123 NR 9.7 506 J 5,850 26,200 1,700
05/08/14 348 880 415 1,000 2.8 108 2.0 20.7 47.2 <0.10 410 44.0 NR 436 1,000 225 <100 1,460
10/28/14 832 2,320 582 2,060 <2.5 235 6.5 J 22.7 72.3 <2.5 646 99.3 NR NR NR NR NR NR
05/05/15 243 636 198 389 <3.3 73.8 3.5 J 9.2 J 30.4 <3.0 254 18.8 NR NR NR NR NR NR
02/06/17 250 291 367 685 <1.3 200 1.6 J 11.9 35.8 <1.3 523 5.6 NR NR NR NR NR NR
02/13/18 1,590 2,560 1,160 3,280 22.5 378 16.3 45.1 130 <3.1 1,100 261 NR NR NR NR NR NR
02/23/10 0.618 J 0.365 J 0.510 J 1.82 0.463 J <0.500 <0.220 <0.150 <0.220 <0.170 0.991 J 0.349 J <0.680 1.93 <100 <200 <200 <270
08/17/10 1.61 0.509 J 0.865 J 2.60 0.690 J 0.521 J <0.220 0.160 J 0.245 J <0.170 1.43 0.411 J NR NR NR NR NR NR
03/02/11 0.538 J 0.321 J 0.535 J 1.51 0.326 J <0.500 <0.220 <0.150 <0.220 <0.170 0.974 J 0.341 J NR <1.50 <100 <193.5 <187 <259
01/27/12 0.58 0.25 J 0.46 J 1.3 J 0.38 J 0.24 J <0.16 <0.10 0.12 J <0.14 0.77 0.25 J NR NR <35 <100 <100 <135
12/05/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-3
MWD-4
(Abandoned)
MW-2
Page 3 of 8
Date : 02/26/18 Facility ID #s: 0-000732 & 0-025021
EPA
Method
610
EPA
Method
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 30,000 700 28,500 25,000 12,500 15,000 NE NE NE NEGCL (mg/l)EthylbenzeneIsopropylbenzeneMTBE2L Standard (mg/l)
Contaminant of Concern C19-C36 Aliphatics1,3,5-Trimethylbenzene1,2-DichloroethaneXylenes1,2,4-TrimethylbenzeneNaphthalenen-PropylbenzeneAnalytical Method
→ C9-C22 AromaticsEPA Method 6200B
C5-C8 AliphaticsC9-C18 AliphaticsTolueneTetrachloroetheneLeadBenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
MADEP Method
VPH/EPH
2-Methylnaphthalene02/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 <0.680 2.16 <100 <200 <200 <270
08/17/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR 7.73 NR NR NR NR
01/27/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/25/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 <0.680 3.70 <100 <200 <200 <270
08/17/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR 10.0 NR NR NR NR
01/26/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/25/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/23/10 59.9 5.73 72.3 72.9 <1.25 68.1 <1.10 18.6 12.7 <0.850 54.1 5.05 4.64 49.9 648 144 <200 283
08/17/10 62.6 3.15 J 55.3 39.3 <1.25 57.3 <1.10 <0.750 12.8 <0.850 35.3 2.88 J NR NR NR NR NR NR
03/02/11 72.6 2.94 J 69.8 43.5 <2.50 109 <2.20 20.1 15.9 <1.70 50.0 <1.80 NR 53.2 890 517 <200 883
01/27/12 78.6 3.2 73.6 36.8 0.40 J 111 0.41 J 22.2 19.5 <0.27 40.2 1.1 NR NR 1250 163 <100 1325
12/05/12 82.7 3.5 90.2 32.1 0.40 J 98.8 0.32 J 25.9 24.5 <0.10 28.4 2.5 NR NR NR NR NR NR
07/25/13 107 4.2 130 99.6 0.34 J 112 0.48 J 26.4 27.4 <0.10 82.3 5.0 NR 34.7 529 956 <96 713
05/08/14 173 31.8 142 267 0.38 J 165 0.67 40.4 35.5 <0.10 126 17.8 NR 50.7 1,140 512 <100 1,537
10/28/14 91.7 3.2 91.2 72.2 <0.20 80.8 1.3 52.7 39.8 <0.20 63.3 4.1 NR NR NR NR NR NR
05/05/15 142 22.9 256 396 <1.6 196 <1.6 41.0 43.2 <1.5 220 35.0 NR NR NR NR NR NR
02/06/17 10.5 0.21 J 6.9 0.80 J <0.13 11.2 <0.13 2.0 1.6 <0.13 0.46 J <0.13 NR NR NR NR NR NR
MW-5
MW-8
MW-7
Page 4 of 8
Date : 02/26/18 Facility ID #s: 0-000732 & 0-025021
EPA
Method
610
EPA
Method
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 30,000 700 28,500 25,000 12,500 15,000 NE NE NE NEGCL (mg/l)EthylbenzeneIsopropylbenzeneMTBE2L Standard (mg/l)
Contaminant of Concern C19-C36 Aliphatics1,3,5-Trimethylbenzene1,2-DichloroethaneXylenes1,2,4-TrimethylbenzeneNaphthalenen-PropylbenzeneAnalytical Method
→ C9-C22 AromaticsEPA Method 6200B
C5-C8 AliphaticsC9-C18 AliphaticsTolueneTetrachloroetheneLeadBenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
MADEP Method
VPH/EPH
2-Methylnaphthalene02/23/10 7.72 <0.950 5.70 10.3 51.9 12.2 188 2.46 J 2.33 J <0.850 5.02 2.28 J <0.680 13.6 462 <200 <200 <270
08/17/10 1.49 J 4.50 J 1.15 J <1.10 17.7 10.3 89.8 <0.750 <1.10 <0.850 1.32 J <0.900 NR NR NR NR NR NR
03/02/11 16.5 <1.90 6.08 J 10.8 39.7 24.6 203 4.08 J 4.27 J <1.70 10.2 3.69 J NR 11.1 653 110 <196 105
01/27/12 11.7 <0.13 4.2 4.83 J 32.2 29.0 121 4.1 6.2 0.34 J 5.0 0.29 J NR NR 682 <35 NR NR
12/05/12 2.1 <0.10 0.19 J 0.67 J 34.7 13.9 123 0.40 J 0.25 J 0.19 J 1.3 <0.10 NR NR NR NR NR NR
07/25/13 12.8 0.19 J 4.9 2.6 29.1 30.8 205 3.9 5.7 0.26 J 4.5 0.12 J NR 9.0 554 158 <97 35.8 J
05/08/14 15.0 0.48 J 9.9 23.9 24.0 22.7 108 3.8 6.8 0.24 J 16.3 6.8 NR <5.0 310 <135 <100 318
10/28/14 0.66 J <0.25 0.38 J <0.50 18.7 9.9 115 0.87 J 0.35 J <0.25 <0.25 <0.25 NR NR NR NR NR NR
05/05/15 43.0 0.49 J 27.0 33.1 25.5 81.1 96.5 12.8 23.0 0.48 J 45.1 <0.27 NR NR NR NR NR NR
02/06/17 0.26 J <0.13 <0.13 <0.25 1.5 0.24 J 6.3 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
02/22/10 1,280 520 327 1,220 <5.00 73.9 111 27.0 62.1 <3.40 362 59.6 4.66 29.4 <100 <200 <200 225
08/17/10 292 25.7 44.2 97.5 <2.50 47.5 85.0 <1.50 27.4 <1.70 55.7 8.02 J NR NR NR NR NR NR
03/02/11 340 189 91.2 339 <2.50 44.2 48.3 8.56 J 18.1 <1.70 109 17.9 NR 24.0 1,780 816 <196 597
01/26/12 714 692 318 1,344 <2.6 105 61.4 18.1 52.2 <2.7 370 79.2 NR NR 4,360 840 <100 3,400
12/05/12 334 44.7 77.7 197 <1.0 53.9 56.1 12.6 40.1 <1.0 66.1 8.6 NR NR NR NR NR NR
07/25/13 304 34.6 124 262 <0.10 72.9 11.9 16.1 34.2 <0.10 144 38.4 NR 10.8 443 813 <96 574
05/08/14 633 219 282 1,220 <2.5 117 53.5 16.7 54.0 <2.5 405 101 NR 15.8 808 <280 <100 1,611
10/28/14 442 75.2 159 408 <1.0 165 33.4 23.9 65.5 <1.0 219 39.5 NR NR NR NR NR NR
05/05/15 727 387 378 1,460 <3.3 190 74.1 30.4 87.9 <3.0 628 118 NR NR NR NR NR NR
02/06/17 744 71.2 440 1,080 <3.1 288 64.1 38.0 120 <3.1 714 154 NR NR NR NR NR NR
02/13/18 786 99.6 412 970 <3.1 300 79.7 51.2 141 <3.1 597 179 NR NR NR NR NR NR
02/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 0.692 J <0.150 <0.220 <0.170 <0.150 <0.180 <0.756 15.6 <100 <205 <211 <279
08/17/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR 16.3 NR NR NR NR
01/26/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 0.13 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
07/25/13 <0.10 0.23 J <0.10 <0.22 <0.10 <0.15 0.46 J <0.10 <0.10 <0.10 <0.10 <0.10 NR 46.3 <35 <132 <97 <185
05/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR 14.6 <35 <135 <100 <185
10/28/14 <0.10 0.83 <0.10 <0.20 <0.10 <0.10 0.15 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
05/05/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 0.36 J <0.12 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
02/06/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
MW-9A
MW-11
MW-10
Page 5 of 8
Date : 02/26/18 Facility ID #s: 0-000732 & 0-025021
EPA
Method
610
EPA
Method
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 30,000 700 28,500 25,000 12,500 15,000 NE NE NE NEGCL (mg/l)EthylbenzeneIsopropylbenzeneMTBE2L Standard (mg/l)
Contaminant of Concern C19-C36 Aliphatics1,3,5-Trimethylbenzene1,2-DichloroethaneXylenes1,2,4-TrimethylbenzeneNaphthalenen-PropylbenzeneAnalytical Method
→ C9-C22 AromaticsEPA Method 6200B
C5-C8 AliphaticsC9-C18 AliphaticsTolueneTetrachloroetheneLeadBenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
MADEP Method
VPH/EPH
2-Methylnaphthalene02/23/10 0.321 J 0.198 J <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 2.20 <0.150 <0.180 <0.680 69.7 <100 <200 228 <270
08/17/10 0.454 J 0.200 J <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 0.843 J <0.150 <0.180 NR NR NR NR NR NR
03/02/11 0.339 J <0.190 <0.150 0.280 J <0.250 <0.500 <0.220 <0.150 <0.220 0.394 J <0.150 <0.180 NR <3.00 NR NR NR NR
01/27/12 0.29 J <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 1.5 <0.10 <0.10 NR NR <35 <35 NA NA
12/05/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/23/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 3.68 <0.150 <0.180 <0.680 <1.50 <100 <200 <200 <270
08/17/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 1.89 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 2.77 <0.150 <0.180 NR 1.71 J <100 <196.2 <192 <263
01/27/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 2.0 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 1.9 <0.10 <0.10 NR NR NR NR NR NR
07/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 2.2 <0.10 <0.10 NR <5.0 <35 <133 <98 <185
05/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 1.2 <0.10 <0.10 NR <5.0 <35 <135 <100 <185
10/28/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 2.2 <0.10 <0.10 NR NR NR NR NR NR
05/05/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 1.4 <0.14 <0.14 NR NR NR NR NR NR
02/22/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 <0.680 <1.50 <100 <200 <200 <270
08/17/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR <1.50 NR NR NR NR
01/26/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
07/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <5.0 <35 <133 <98 <185
05/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <5.0 <35 <135 <100 <185
10/28/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
02/22/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 <0.680 3.70 <100 <200 <200 <270
08/17/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR <1.50 NR NR NR NR
01/26/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
07/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <5.0 <35 <131 <98 <175
05/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR 6.7 <35 <135 <100 <185
10/28/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
05/05/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
MW-13
MW-15
MW-14
MWD-12
(Abandoned)
Page 6 of 8
Date : 02/26/18 Facility ID #s: 0-000732 & 0-025021
EPA
Method
610
EPA
Method
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 30,000 700 28,500 25,000 12,500 15,000 NE NE NE NEGCL (mg/l)EthylbenzeneIsopropylbenzeneMTBE2L Standard (mg/l)
Contaminant of Concern C19-C36 Aliphatics1,3,5-Trimethylbenzene1,2-DichloroethaneXylenes1,2,4-TrimethylbenzeneNaphthalenen-PropylbenzeneAnalytical Method
→ C9-C22 AromaticsEPA Method 6200B
C5-C8 AliphaticsC9-C18 AliphaticsTolueneTetrachloroetheneLeadBenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
MADEP Method
VPH/EPH
2-Methylnaphthalene02/22/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 <0.680 29.5 <100 <200 <200 <270
08/17/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.220 <0.150 <0.220 <0.170 <0.150 <0.180 NR NR NR NR NR NR
03/02/11 <0.700 <0.950 <0.750 <1.10 <1.25 <2.50 <1.10 <0.750 <1.10 <0.850 <0.750 <0.900 NR 24.1 NR NR NR NR
01/26/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.14 <0.10 <0.10 NR NR <35 <100 <100 <135
12/05/12 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
07/25/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <5.0 <35 <132 <97 <185
05/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR <5.0 <35 <134 <99 <185
10/28/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
05/05/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
02/06/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
12/05/12 1,760 276 407 1,400 <5.0 80.8 76.9 11.3 J 39.0 <5.0 301 83.3 NR NR NR NR NR NR
07/25/13 884 120 86.7 191 <2.5 34.3 69.1 4.0 J 11.0 J <2.5 41.4 15.3 NR 38.7 699 632 J <96 554
05/08/14 1,610 1,930 520 2,400 <5.0 171 59.7 22.8 J 62.3 <5.0 643 181 NR <5.0 2,550 513 <100 2,871
10/28/14 614 319 134 844 <2.0 176 32.8 4.9 J 16.2 <2.0 365 40.4 NR NR NR NR NR NR
05/05/15 4,040 2,040 1,290 3,500 <16 432 129 51.2 155 <15 1,390 324 NR NR NR NR NR NR
02/06/17 3,910 4,530 1,350 2,780 <25 339 57.7 J 31.8 J 110 <25 989 203 NR NR NR NR NR NR
02/13/18 2,880 4,150 1,190 3,740 <6.3 565 37.9 48.7 143 <6.3 1,190 284 NR NR NR NR NR NR
12/05/12 70.0 5.9 10.1 3.4 <0.20 1.3 13.0 0.41 J 0.75 J <0.20 1.2 0.30 J NR NR NR NR NR NR
07/25/13 440 434 78.7 177 <0.10 32.7 1.2 3.1 9.5 0.58 64.4 13.7 NR <5.0 468 513 <96 227
05/08/14 86.9 155 67.2 429 <2.5 55.6 <2.5 8.8 J 39.1 <2.5 366 106 NR 100 1,500 716 <99 1,934
10/28/14 11.2 0.51 3.6 <0.20 <0.10 0.41 J <0.10 0.32 J 0.80 0.13 J 1.6 0.10 J NR NR NR NR NR NR
05/05/15 20.5 1.8 5.1 8.0 <0.16 1.3 0.18 J 0.20 J 0.52 <0.15 3.9 <0.14 NR NR NR NR NR NR
02/06/17 <0.13 0.20 J <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
05/08/14 0.88 2.4 1.1 5.8 <0.10 3.3 <0.10 0.15 J 0.74 <0.10 2.7 0.93 NR <10 <35 <133 128 J 70.2 J
10/28/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
05/05/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
MW-17
TW-1
MWD-18
MW-16
Page 7 of 8
Date : 02/26/18 Facility ID #s: 0-000732 & 0-025021
EPA
Method
610
EPA
Method
3030C
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 0.7 400 400 30 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 30,000 700 28,500 25,000 12,500 15,000 NE NE NE NEGCL (mg/l)EthylbenzeneIsopropylbenzeneMTBE2L Standard (mg/l)
Contaminant of Concern C19-C36 Aliphatics1,3,5-Trimethylbenzene1,2-DichloroethaneXylenes1,2,4-TrimethylbenzeneNaphthalenen-PropylbenzeneAnalytical Method
→ C9-C22 AromaticsEPA Method 6200B
C5-C8 AliphaticsC9-C18 AliphaticsTolueneTetrachloroetheneLeadBenzeneTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NOS. 11085 & 12111)
MADEP Method
VPH/EPH
2-MethylnaphthaleneRW-1 02/06/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR
Notes:
• Results reported in µg/l (micrograms per liter).
• 2L Standard as specified in T15A NCAC 2L.0202.
• GCL : Gross contamination level.
• < : Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L Standards.
• NR: Analysis not requested.
• NA: Not analyzed
• J: Estimated value.
• Other reported concentrations which exceeded the 2L Standard during the February 13, 2018, sampling event: 1,2-dichlorobenzene (31.5 µg/L in MW-3) and 1,4-dichlorobenzene (µg/L in MW-3).
• Please refer to the lab report for detectable concentrations which did not exceed the 2L Standards, or for which no standard has been established.
Page 8 of 8
Date: 02/23/18
Well No.Sample Date
(mm/dd/yy)DO (mg/L)Temp(oC)pH
Oxidation-
Reduction
Potential (mV)
Methane
(μg/L)
Nitrate
(mg/L)
Sulfate
(mg/L)
Ferrous Iron
(mg/L)
08/17/10 1.36 26.6 4.68 NA 52.4 <0.0330 6.27 9.14
1/26/12 7.1 13.53 4.45 239.3 191 <0.20 5.1 21.4
08/17/10 1.05 27.7 6.57 NA 38.7 0.0890 J 5.97 1.26
01/26/12 5.5 11.31 5.93 17.4 187 <0.20 <4.0 4.3
08/17/10 1.02 26.7 5.29 NA 65.2 <0.0330 23.7 1.50
01/26/12 6.5 14.53 4.16 262.6 87.0 <0.20 28.5 3.3
08/17/10 0.96 22.8 4.40 NA 18.1 <0.0330 11.2 3.68
01/26/12 7.5 14.68 4.15 288.7 72.0 <0.20 13.4 6.6
08/17/10 0.65 22.5 4.28 NA 2.10 J <0.0330 7.58 1.94
01/26/12 10.4 13.16 4.09 367.3 4.80 <0.20 16.3 1.0
08/17/10 1.29 22.0 4.97 NA 2.96 J 0.0340 J 24.2 0.202
01/27/12 13.0 14.72 3.37 349.4 0.24 J 0.15 b 23.5 <0.10
08/17/10 1.45 24.4 4.60 NA 23.6 <0.0330 1.74 1.93
01/27/12 4.0 16.54 4.91 238.4 17.6 <0.10 b <2.0 1.0
08/17/10 NA NA NA NA 289 <0.0330 <0.330 5.59
01/27/12 2.1 17.54 6.27 24.1 34.8 <0.20 b 12.2 <0.20
02/13/18 1.16 16.46 6.95 -29.1 NR NR NR NR
MW-1
TABLE 3
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NATURAL ATTENUATION PARAMETERS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NO. 11085 & 12111)
Facility ID #: 0-000732 & 0-025021
MW-2
LMW-1
LMW-2
LMW-3
LMW-4
LMW-5
MW-3
Page 1 of 3
Date: 02/23/18
Well No.Sample Date
(mm/dd/yy)DO (mg/L)Temp(oC)pH
Oxidation-
Reduction
Potential (mV)
Methane
(μg/L)
Nitrate
(mg/L)
Sulfate
(mg/L)
Ferrous Iron
(mg/L)
TABLE 3
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NATURAL ATTENUATION PARAMETERS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NO. 11085 & 12111)
Facility ID #: 0-000732 & 0-025021
08/17/10 2.69 19.4 11.84 NA 48.6 0.0840 J 0.614 J 3.63
01/27/12 50.0 17.16 12.42 -115.9 45.2 0.20 b <2.0 <0.10
08/17/10 1.00 24.0 4.91 NA <1.00 0.0400 J 50.3 1.14
01/27/12 16.1 14.98 3.01 354.8 <0.16 <0.10 58.6 0.18
08/17/10 NF NF NF NF NF NF NF NF
01/27/12 NF NF NF NF NF NF NF NF
08/17/10 1.13 22.2 4.84 NA 5.27 0.0580 J 38.7 1.00
01/26/12 10.1 12.10 3.32 249.6 20.5 0.34 16.7 0.52
08/17/10 0.66 26.4 6.05 NA 238 <0.0330 0.363 J 7.55
01/27/12 4.2 16.10 6.10 -17.0 1,920 <0.20 b <4.0 14.2
08/17/10 0.95 26.3 5.12 NA 160 <0.0330 3.80 11.0
01/27/12 8.2 16.93 4.57 215.2 149 <0.20 b <4.0 7.4
08/17/10 1.02 27.6 5.63 NA 162 <0.0330 12.9 12.4
01/26/12 8.9 15.20 5.35 13.3 152 <0.50 <10 <0.50
02/13/18 2.35 14.77 6.14 -47.2 NR NR NR NR
08/17/10 0.70 21.9 5.47 NA 98.5 <0.0330 2.08 5.80
01/26/12 3.5 14.96 4.79 102.8 21.2 <0.50 <10 <0.50
MWD-4
MW-5
MW-6
MW-7
MW-8
MW-9A
MW-11
MW-10
Page 2 of 3
Date: 02/23/18
Well No.Sample Date
(mm/dd/yy)DO (mg/L)Temp(oC)pH
Oxidation-
Reduction
Potential (mV)
Methane
(μg/L)
Nitrate
(mg/L)
Sulfate
(mg/L)
Ferrous Iron
(mg/L)
TABLE 3
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
NATURAL ATTENUATION PARAMETERS
GRANNY'S GRILL & LEGGETT'S GROCERY (INCIDENT NO. 11085 & 12111)
Facility ID #: 0-000732 & 0-025021
08/17/10 2.09 19.1 11.96 NA 19.1 0.0510 J 1.70 1.38
01/27/12 18.9 17.53 12.52 -96.4 44.7 0.11 b <2.0 <0.10
08/17/10 0.97 24.5 4.68 NA 2.30 J <0.0330 <0.330 4.12
01/27/12 18.8 16.64 4.82 194.9 29.2 0.12 b <2.0 7.6
08/17/10 1.23 23.0 4.39 NA 1.45 J 0.0400 J 7.04 0.633
01/26/12 4.1 13.63 4.10 325.3 5.48 <0.20 7.0 11.3
08/17/10 1.88 23.6 4.43 NA 2.08 J <0.0330 6.11 1.66
01/26/12 7.5 14.17 4.92 255.2 9.27 <0.10 3.4 <0.10
08/17/10 2.32 22.9 4.04 NA 4.68 0.0400 J 11.0 4.82
01/26/12 13.9 14.92 4.49 279.5 0.50 <0.50 13.7 0.0
MW-17 02/13/18 1.62 13.43 6.36 -48.0 NR NR NR NR
Notes:
• Field measurements of dissolved oxygen, temperature and pH were collected during sampling using a field meter. ORP readings are not available
on 08/17/10 due to an equipment malfunction.
MWD-12
MW-13
• <: Less than the method detection limit specified in the laboratory report.
• NA: Not Available.
• J: Estimated value.
• b: Holding time was exceeded prior to analysis.
MW-14
MW-15
MW-16
• Analyses for nitrate and sulfate by EPA Method 300.0; analyses for methane by Method RSK 175; analyses for ferrous iron by Method SM-3500-FE
Page 3 of 3

APPENDICES

APPENDIX A
Laboratory Report - Ground Water Samples
02/26/18
Technical Report for
GRI (Geological Resources Inc.)
Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
11085/2924
SGS Job Number: FA51757
Sampling Date: 02/13/18
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Nicole Long
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 02/26/18
e-Hardcopy 2.0
Automated Report
32
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
1 of 32
FA51757
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA51757-1: MW-3 ........................................................................................................7
3.2: FA51757-2: MW-10 ......................................................................................................10
3.3: FA51757-3: MW-17 ......................................................................................................12
Section 4: Misc. Forms ............................................................................................................14
4.1: Chain of Custody ...........................................................................................................15
Section 5: MS Volatiles - QC Data Summaries .....................................................................17
5.1: Method Blank Summary ................................................................................................18
5.2: Blank Spike Summary ...................................................................................................23
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................28 123452 of 32
FA51757
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA51757
Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Project No: 11085/2924
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA51757-1 02/13/18 15:00 WR 02/14/18 AQ Ground Water MW-3
FA51757-2 02/13/18 15:07 WR 02/14/18 AQ Ground Water MW-10
FA51757-3 02/13/18 15:21 WR 02/14/18 AQ Ground Water MW-17
3 of 32
FA517571
Summary of Hits Page 1 of 2
Job Number:FA51757
Account:GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Collected:02/13/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA51757-1 MW-3
Benzene 1590 25 6.3 ug/l SM 6200B
n-Butylbenzene 11.5 J 13 3.1 ug/l SM 6200B
sec-Butylbenzene 7.5 J 13 3.1 ug/l SM 6200B
1,2-Dichlorobenzene 31.5 13 3.1 ug/l SM 6200B
1,3-Dichlorobenzene 48.2 13 3.1 ug/l SM 6200B
1,4-Dichlorobenzene 41.2 13 3.1 ug/l SM 6200B
1,2-Dichloroethane 16.3 13 3.1 ug/l SM 6200B
Di-Isopropyl Ether 41.7 13 3.1 ug/l SM 6200B
Ethylbenzene 1160 13 3.1 ug/l SM 6200B
Isopropylbenzene 45.1 13 3.1 ug/l SM 6200B
p-Isopropyltoluene 5.7 J 13 3.1 ug/l SM 6200B
Methyl Chloride 14.5 13 5.0 ug/l SM 6200B
Methyl Tert Butyl Ether 22.5 13 3.1 ug/l SM 6200B
Naphthalene 378 13 3.1 ug/l SM 6200B
n-Propylbenzene 130 13 3.1 ug/l SM 6200B
Toluene a 2560 50 13 ug/l SM 6200B
1,2,4-Trimethylbenzene 1100 13 3.1 ug/l SM 6200B
1,3,5-Trimethylbenzene 261 13 3.1 ug/l SM 6200B
m,p-Xylene 2250 25 3.1 ug/l SM 6200B
o-Xylene 1030 13 3.1 ug/l SM 6200B
Xylene (total)3280 38 6.3 ug/l SM 6200B
FA51757-2 MW-10
Benzene 786 13 3.1 ug/l SM 6200B
n-Butylbenzene 10.1 J 13 3.1 ug/l SM 6200B
sec-Butylbenzene 8.0 J 13 3.1 ug/l SM 6200B
1,2-Dichloroethane 79.7 13 3.1 ug/l SM 6200B
Di-Isopropyl Ether 19.5 13 3.1 ug/l SM 6200B
Ethylbenzene 412 13 3.1 ug/l SM 6200B
Isopropylbenzene 51.2 13 3.1 ug/l SM 6200B
Naphthalene 300 13 3.1 ug/l SM 6200B
n-Propylbenzene 141 13 3.1 ug/l SM 6200B
Toluene 99.6 13 3.1 ug/l SM 6200B
1,2,4-Trimethylbenzene 597 13 3.1 ug/l SM 6200B
1,3,5-Trimethylbenzene 179 13 3.1 ug/l SM 6200B
m,p-Xylene 517 25 3.1 ug/l SM 6200B
o-Xylene 454 13 3.1 ug/l SM 6200B
Xylene (total)970 38 6.3 ug/l SM 6200B
FA51757-3 MW-17
Benzene 2880 100 25 ug/l SM 6200B
4 of 32
FA517572
Summary of Hits Page 2 of 2
Job Number:FA51757
Account:GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Collected:02/13/18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
n-Butylbenzene 15.4 J 25 6.3 ug/l SM 6200B
sec-Butylbenzene 9.3 J 25 6.3 ug/l SM 6200B
o-Chlorotoluene 32.3 25 6.3 ug/l SM 6200B
1,2-Dichloroethane 37.9 25 6.3 ug/l SM 6200B
Di-Isopropyl Ether 13.5 J 25 6.3 ug/l SM 6200B
Ethylbenzene 1190 25 6.3 ug/l SM 6200B
Isopropylbenzene 48.7 25 6.3 ug/l SM 6200B
Naphthalene 565 100 25 ug/l SM 6200B
n-Propylbenzene 143 25 6.3 ug/l SM 6200B
Toluene 4150 100 25 ug/l SM 6200B
1,2,4-Trimethylbenzene 1190 25 6.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 284 25 6.3 ug/l SM 6200B
m,p-Xylene 2250 50 6.3 ug/l SM 6200B
o-Xylene 1490 25 6.3 ug/l SM 6200B
Xylene (total)3740 75 13 ug/l SM 6200B
(a) Sample vial(s) contained bubbles greater than 6mm; reported results are considered minimum values.
5 of 32
FA517572
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
6 of 32
FA517573
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:FA51757-1 Date Sampled:02/13/18
Matrix:AQ - Ground Water Date Received:02/14/18
Method:SM 6200B Percent Solids:n/a
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211697.D 25 02/15/18 23:40 TD n/a n/a VA2319
Run #2 A0211720.D 50 02/21/18 16:06 MM n/a n/a VA2320
Run #3 a A0211734.D 100 02/22/18 10:30 MM n/a n/a VA2321
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
Run #3 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1590 b 25 6.3 ug/l
108-86-1 Bromobenzene ND 13 3.1 ug/l
74-97-5 Bromochloromethane ND 13 3.1 ug/l
75-27-4 Bromodichloromethane ND 13 3.1 ug/l
75-25-2 Bromoform ND 13 3.1 ug/l
104-51-8 n-Butylbenzene 11.5 13 3.1 ug/l J
135-98-8 sec-Butylbenzene 7.5 13 3.1 ug/l J
98-06-6 tert-Butylbenzene ND 13 3.1 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.1 ug/l
108-90-7 Chlorobenzene ND 13 3.1 ug/l
75-00-3 Chloroethane ND 13 5.0 ug/l
67-66-3 Chloroform ND 13 3.1 ug/l
95-49-8 o-Chlorotoluene ND 13 3.1 ug/l
106-43-4 p-Chlorotoluene ND 13 3.1 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 6.2 ug/l
106-93-4 1,2-Dibromoethane ND 13 3.1 ug/l
75-71-8 Dichlorodifluoromethane ND 13 5.0 ug/l
95-50-1 1,2-Dichlorobenzene 31.5 13 3.1 ug/l
541-73-1 1,3-Dichlorobenzene 48.2 13 3.1 ug/l
106-46-7 1,4-Dichlorobenzene 41.2 13 3.1 ug/l
75-34-3 1,1-Dichloroethane ND 13 3.1 ug/l
107-06-2 1,2-Dichloroethane 16.3 13 3.1 ug/l
75-35-4 1,1-Dichloroethylene ND 13 3.1 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 3.1 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 3.1 ug/l
78-87-5 1,2-Dichloropropane ND 13 3.1 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.1 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.1 ug/l
563-58-6 1,1-Dichloropropene ND 13 3.1 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 32
FA5175733.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:FA51757-1 Date Sampled:02/13/18
Matrix:AQ - Ground Water Date Received:02/14/18
Method:SM 6200B Percent Solids:n/a
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-01-5 cis-1,3-Dichloropropene ND 13 3.1 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 13 3.1 ug/l
108-20-3 Di-Isopropyl Ether 41.7 13 3.1 ug/l
100-41-4 Ethylbenzene 1160 13 3.1 ug/l
87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l
98-82-8 Isopropylbenzene 45.1 13 3.1 ug/l
99-87-6 p-Isopropyltoluene 5.7 13 3.1 ug/l J
74-83-9 Methyl Bromide ND 13 5.0 ug/l
74-87-3 Methyl Chloride 14.5 13 5.0 ug/l
74-95-3 Methylene Bromide ND 13 3.1 ug/l
75-09-2 Methylene Chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether 22.5 13 3.1 ug/l
91-20-3 Naphthalene 378 13 3.1 ug/l
103-65-1 n-Propylbenzene 130 13 3.1 ug/l
100-42-5 Styrene ND 13 3.1 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.1 ug/l
127-18-4 Tetrachloroethylene ND 13 3.1 ug/l
108-88-3 Toluene 2560 c 50 13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.1 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.1 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 3.1 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.1 ug/l
79-01-6 Trichloroethylene ND 13 3.1 ug/l
75-69-4 Trichlorofluoromethane ND 13 5.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.1 ug/l
95-63-6 1,2,4-Trimethylbenzene 1100 13 3.1 ug/l
108-67-8 1,3,5-Trimethylbenzene 261 13 3.1 ug/l
75-01-4 Vinyl Chloride ND 13 3.1 ug/l
m,p-Xylene 2250 25 3.1 ug/l
95-47-6 o-Xylene 1030 13 3.1 ug/l
1330-20-7 Xylene (total)3280 38 6.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Run# 3 Limits
1868-53-7 Dibromofluoromethane 99%100%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%97%96%70-130%
2037-26-5 Toluene-D8 100%97%98%70-130%
460-00-4 4-Bromofluorobenzene 101%97%99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 32
FA5175733.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:FA51757-1 Date Sampled:02/13/18
Matrix:AQ - Ground Water Date Received:02/14/18
Method:SM 6200B Percent Solids:n/a
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(a) Sample vial(s) contained bubbles greater than 6mm; reported results are considered minimum values.
(b) Result is from Run# 2
(c) Result is from Run# 3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 32
FA5175733.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA51757-2 Date Sampled:02/13/18
Matrix:AQ - Ground Water Date Received:02/14/18
Method:SM 6200B Percent Solids:n/a
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211698.D 25 02/16/18 00:04 TD n/a n/a VA2319
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 786 13 3.1 ug/l
108-86-1 Bromobenzene ND 13 3.1 ug/l
74-97-5 Bromochloromethane ND 13 3.1 ug/l
75-27-4 Bromodichloromethane ND 13 3.1 ug/l
75-25-2 Bromoform ND 13 3.1 ug/l
104-51-8 n-Butylbenzene 10.1 13 3.1 ug/l J
135-98-8 sec-Butylbenzene 8.0 13 3.1 ug/l J
98-06-6 tert-Butylbenzene ND 13 3.1 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.1 ug/l
108-90-7 Chlorobenzene ND 13 3.1 ug/l
75-00-3 Chloroethane ND 13 5.0 ug/l
67-66-3 Chloroform ND 13 3.1 ug/l
95-49-8 o-Chlorotoluene ND 13 3.1 ug/l
106-43-4 p-Chlorotoluene ND 13 3.1 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 6.2 ug/l
106-93-4 1,2-Dibromoethane ND 13 3.1 ug/l
75-71-8 Dichlorodifluoromethane ND 13 5.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.1 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.1 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.1 ug/l
75-34-3 1,1-Dichloroethane ND 13 3.1 ug/l
107-06-2 1,2-Dichloroethane 79.7 13 3.1 ug/l
75-35-4 1,1-Dichloroethylene ND 13 3.1 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 3.1 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 3.1 ug/l
78-87-5 1,2-Dichloropropane ND 13 3.1 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.1 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.1 ug/l
563-58-6 1,1-Dichloropropene ND 13 3.1 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 3.1 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 13 3.1 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 32
FA5175733.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA51757-2 Date Sampled:02/13/18
Matrix:AQ - Ground Water Date Received:02/14/18
Method:SM 6200B Percent Solids:n/a
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 19.5 13 3.1 ug/l
100-41-4 Ethylbenzene 412 13 3.1 ug/l
87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l
98-82-8 Isopropylbenzene 51.2 13 3.1 ug/l
99-87-6 p-Isopropyltoluene ND 13 3.1 ug/l
74-83-9 Methyl Bromide ND 13 5.0 ug/l
74-87-3 Methyl Chloride ND 13 5.0 ug/l
74-95-3 Methylene Bromide ND 13 3.1 ug/l
75-09-2 Methylene Chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 13 3.1 ug/l
91-20-3 Naphthalene 300 13 3.1 ug/l
103-65-1 n-Propylbenzene 141 13 3.1 ug/l
100-42-5 Styrene ND 13 3.1 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.1 ug/l
127-18-4 Tetrachloroethylene ND 13 3.1 ug/l
108-88-3 Toluene 99.6 13 3.1 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.1 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.1 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 3.1 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.1 ug/l
79-01-6 Trichloroethylene ND 13 3.1 ug/l
75-69-4 Trichlorofluoromethane ND 13 5.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.1 ug/l
95-63-6 1,2,4-Trimethylbenzene 597 13 3.1 ug/l
108-67-8 1,3,5-Trimethylbenzene 179 13 3.1 ug/l
75-01-4 Vinyl Chloride ND 13 3.1 ug/l
m,p-Xylene 517 25 3.1 ug/l
95-47-6 o-Xylene 454 13 3.1 ug/l
1330-20-7 Xylene (total)970 38 6.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 32
FA5175733.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-17
Lab Sample ID:FA51757-3 Date Sampled:02/13/18
Matrix:AQ - Ground Water Date Received:02/14/18
Method:SM 6200B Percent Solids:n/a
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0211722.D 50 02/21/18 16:52 MM n/a n/a VA2320
Run #2 A0211699.D 200 02/16/18 00:27 TD n/a n/a VA2319
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2880 a 100 25 ug/l
108-86-1 Bromobenzene ND 25 6.3 ug/l
74-97-5 Bromochloromethane ND 25 6.3 ug/l
75-27-4 Bromodichloromethane ND 25 6.3 ug/l
75-25-2 Bromoform ND 25 6.3 ug/l
104-51-8 n-Butylbenzene 15.4 25 6.3 ug/l J
135-98-8 sec-Butylbenzene 9.3 25 6.3 ug/l J
98-06-6 tert-Butylbenzene ND 25 6.3 ug/l
56-23-5 Carbon Tetrachloride ND 25 6.3 ug/l
108-90-7 Chlorobenzene ND 25 6.3 ug/l
75-00-3 Chloroethane ND 25 10 ug/l
67-66-3 Chloroform ND 25 6.3 ug/l
95-49-8 o-Chlorotoluene 32.3 25 6.3 ug/l
106-43-4 p-Chlorotoluene ND 25 6.3 ug/l
124-48-1 Dibromochloromethane ND 25 6.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 25 12 ug/l
106-93-4 1,2-Dibromoethane ND 25 6.3 ug/l
75-71-8 Dichlorodifluoromethane ND 25 10 ug/l
95-50-1 1,2-Dichlorobenzene ND 25 6.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 25 6.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 25 6.3 ug/l
75-34-3 1,1-Dichloroethane ND 25 6.3 ug/l
107-06-2 1,2-Dichloroethane 37.9 25 6.3 ug/l
75-35-4 1,1-Dichloroethylene ND 25 6.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 25 6.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 25 6.3 ug/l
78-87-5 1,2-Dichloropropane ND 25 6.3 ug/l
142-28-9 1,3-Dichloropropane ND 25 6.3 ug/l
594-20-7 2,2-Dichloropropane ND 25 6.3 ug/l
563-58-6 1,1-Dichloropropene ND 25 6.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 25 6.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 32
FA5175733.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-17
Lab Sample ID:FA51757-3 Date Sampled:02/13/18
Matrix:AQ - Ground Water Date Received:02/14/18
Method:SM 6200B Percent Solids:n/a
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 13.5 25 6.3 ug/l J
100-41-4 Ethylbenzene 1190 25 6.3 ug/l
87-68-3 Hexachlorobutadiene ND 25 6.3 ug/l
98-82-8 Isopropylbenzene 48.7 25 6.3 ug/l
99-87-6 p-Isopropyltoluene ND 25 6.3 ug/l
74-83-9 Methyl Bromide ND 25 10 ug/l
74-87-3 Methyl Chloride ND 25 10 ug/l
74-95-3 Methylene Bromide ND 25 6.3 ug/l
75-09-2 Methylene Chloride ND 100 50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 25 6.3 ug/l
91-20-3 Naphthalene 565 a 100 25 ug/l
103-65-1 n-Propylbenzene 143 25 6.3 ug/l
100-42-5 Styrene ND 25 6.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 25 6.3 ug/l
127-18-4 Tetrachloroethylene ND 25 6.3 ug/l
108-88-3 Toluene 4150 a 100 25 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 25 6.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 6.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 25 6.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 25 6.3 ug/l
79-01-6 Trichloroethylene ND 25 6.3 ug/l
75-69-4 Trichlorofluoromethane ND 25 10 ug/l
96-18-4 1,2,3-Trichloropropane ND 25 6.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 1190 25 6.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 284 25 6.3 ug/l
75-01-4 Vinyl Chloride ND 25 6.3 ug/l
m,p-Xylene 2250 50 6.3 ug/l
95-47-6 o-Xylene 1490 25 6.3 ug/l
1330-20-7 Xylene (total)3740 75 13 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%97%70-130%
2037-26-5 Toluene-D8 96%99%70-130%
460-00-4 4-Bromofluorobenzene 99%100%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 32
FA5175733.3
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
14 of 32
FA517574
FA51757: Chain of Custody
Page 1 of 2
15 of 32
FA5175744.1
Job Number:FA51757 Client:GRI
Date / Time Received:2/14/2018 9:45:00 AM Delivery Method:FX
Project:GRANNYS
Airbill #'s:1015899951960003281100811062252423
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (2.6);
Cooler 1: (3.0);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:JORGEC P.H Date:2/14/2018Date:2/14/2018 9:45:00 AM
FA51757: Chain of Custody
Page 2 of 2
16 of 32
FA5175744.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
17 of 32
FA517575
Method Blank Summary Page 1 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2319-MB A0211692.D 1 02/15/18 TD n/a n/a VA2319
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-2, FA51757-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
18 of 32
FA5175755.1.1
Method Blank Summary Page 2 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2319-MB A0211692.D 1 02/15/18 TD n/a n/a VA2319
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-2, FA51757-3
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
19 of 32
FA5175755.1.1
Method Blank Summary Page 1 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2320-MB A0211719.D 1 02/21/18 MM n/a n/a VA2320
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
20 of 32
FA5175755.1.2
Method Blank Summary Page 2 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2320-MB A0211719.D 1 02/21/18 MM n/a n/a VA2320
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-3
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
21 of 32
FA5175755.1.2
Method Blank Summary Page 1 of 1
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2321-MB A0211733.D 1 02/22/18 MM n/a n/a VA2321
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1
CAS No.Compound Result RL MDL Units Q
108-88-3 Toluene ND 0.50 0.13 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 94%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
22 of 32
FA5175755.1.3
Blank Spike Summary Page 1 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2319-BS A0211689.D 1 02/15/18 TD n/a n/a VA2319
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-2, FA51757-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.2 102 70-130
108-86-1 Bromobenzene 10 10.3 103 70-130
74-97-5 Bromochloromethane 10 10.6 106 70-130
75-27-4 Bromodichloromethane 10 10.2 102 70-130
75-25-2 Bromoform 10 9.7 97 70-130
104-51-8 n-Butylbenzene 10 10.8 108 70-130
135-98-8 sec-Butylbenzene 10 10.8 108 70-130
98-06-6 tert-Butylbenzene 10 10.7 107 70-130
56-23-5 Carbon Tetrachloride 10 10.4 104 70-130
108-90-7 Chlorobenzene 10 10.3 103 70-130
75-00-3 Chloroethane 10 9.8 98 60-140
67-66-3 Chloroform 10 10.1 101 70-130
95-49-8 o-Chlorotoluene 10 10.3 103 70-130
106-43-4 p-Chlorotoluene 10 10.6 106 70-130
124-48-1 Dibromochloromethane 10 10.4 104 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10.2 102 70-130
106-93-4 1,2-Dibromoethane 10 10.4 104 70-130
75-71-8 Dichlorodifluoromethane 10 9.0 90 60-140
95-50-1 1,2-Dichlorobenzene 10 10.4 104 70-130
541-73-1 1,3-Dichlorobenzene 10 10.4 104 70-130
106-46-7 1,4-Dichlorobenzene 10 10 100 70-130
75-34-3 1,1-Dichloroethane 10 10.3 103 70-130
107-06-2 1,2-Dichloroethane 10 10.1 101 70-130
75-35-4 1,1-Dichloroethylene 10 10.4 104 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.2 102 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.3 103 70-130
78-87-5 1,2-Dichloropropane 10 10.3 103 70-130
142-28-9 1,3-Dichloropropane 10 10.6 106 70-130
594-20-7 2,2-Dichloropropane 10 9.8 98 70-130
563-58-6 1,1-Dichloropropene 10 10.5 105 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.8 108 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10 100 70-130
108-20-3 Di-Isopropyl Ether 10 10.5 105 70-130
100-41-4 Ethylbenzene 10 10.3 103 70-130
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
98-82-8 Isopropylbenzene 10 10.7 107 70-130
* = Outside of Control Limits.
23 of 32
FA5175755.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2319-BS A0211689.D 1 02/15/18 TD n/a n/a VA2319
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-2, FA51757-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.8 108 70-130
74-83-9 Methyl Bromide 10 9.0 90 60-140
74-87-3 Methyl Chloride 10 10.6 106 60-140
74-95-3 Methylene Bromide 10 10.1 101 70-130
75-09-2 Methylene Chloride 10 10.1 101 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.6 106 70-130
91-20-3 Naphthalene 10 9.7 97 70-130
103-65-1 n-Propylbenzene 10 10.5 105 70-130
100-42-5 Styrene 10 10.9 109 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.4 104 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.2 102 70-130
127-18-4 Tetrachloroethylene 10 10.4 104 70-130
108-88-3 Toluene 10 10.2 102 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.4 104 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.4 104 70-130
71-55-6 1,1,1-Trichloroethane 10 10.4 104 70-130
79-00-5 1,1,2-Trichloroethane 10 10.4 104 70-130
79-01-6 Trichloroethylene 10 10.4 104 70-130
75-69-4 Trichlorofluoromethane 10 9.7 97 60-140
96-18-4 1,2,3-Trichloropropane 10 10.3 103 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.6 106 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.7 107 70-130
75-01-4 Vinyl Chloride 10 9.5 95 60-140
m,p-Xylene 20 21.6 108 70-130
95-47-6 o-Xylene 10 10.5 105 70-130
1330-20-7 Xylene (total)30 32.1 107 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
24 of 32
FA5175755.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2320-BS A0211715.D 1 02/21/18 MM n/a n/a VA2320
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.2 102 70-130
108-86-1 Bromobenzene 10 9.8 98 70-130
74-97-5 Bromochloromethane 10 10.1 101 70-130
75-27-4 Bromodichloromethane 10 10.3 103 70-130
75-25-2 Bromoform 10 9.6 96 70-130
104-51-8 n-Butylbenzene 10 10.6 106 70-130
135-98-8 sec-Butylbenzene 10 10.5 105 70-130
98-06-6 tert-Butylbenzene 10 10 100 70-130
56-23-5 Carbon Tetrachloride 10 10.3 103 70-130
108-90-7 Chlorobenzene 10 9.8 98 70-130
75-00-3 Chloroethane 10 12.8 128 60-140
67-66-3 Chloroform 10 9.8 98 70-130
95-49-8 o-Chlorotoluene 10 9.8 98 70-130
106-43-4 p-Chlorotoluene 10 9.9 99 70-130
124-48-1 Dibromochloromethane 10 10.1 101 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.2 92 70-130
106-93-4 1,2-Dibromoethane 10 9.8 98 70-130
75-71-8 Dichlorodifluoromethane 10 8.6 86 60-140
95-50-1 1,2-Dichlorobenzene 10 9.7 97 70-130
541-73-1 1,3-Dichlorobenzene 10 10.0 100 70-130
106-46-7 1,4-Dichlorobenzene 10 9.5 95 70-130
75-34-3 1,1-Dichloroethane 10 10.7 107 70-130
107-06-2 1,2-Dichloroethane 10 9.7 97 70-130
75-35-4 1,1-Dichloroethylene 10 10.6 106 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.8 108 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.7 107 70-130
78-87-5 1,2-Dichloropropane 10 10.2 102 70-130
142-28-9 1,3-Dichloropropane 10 9.3 93 70-130
594-20-7 2,2-Dichloropropane 10 10.7 107 70-130
563-58-6 1,1-Dichloropropene 10 10.3 103 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.3 103 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.5 95 70-130
108-20-3 Di-Isopropyl Ether 10 9.9 99 70-130
100-41-4 Ethylbenzene 10 9.8 98 70-130
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
98-82-8 Isopropylbenzene 10 10.8 108 70-130
* = Outside of Control Limits.
25 of 32
FA5175755.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2320-BS A0211715.D 1 02/21/18 MM n/a n/a VA2320
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.6 106 70-130
74-83-9 Methyl Bromide 10 9.8 98 60-140
74-87-3 Methyl Chloride 10 10.4 104 60-140
74-95-3 Methylene Bromide 10 10.2 102 70-130
75-09-2 Methylene Chloride 10 9.6 96 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.9 99 70-130
103-65-1 n-Propylbenzene 10 10 100 70-130
100-42-5 Styrene 10 10.4 104 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.9 99 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.9 99 70-130
127-18-4 Tetrachloroethylene 10 10.1 101 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.5 95 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.0 100 70-130
71-55-6 1,1,1-Trichloroethane 10 9.9 99 70-130
79-00-5 1,1,2-Trichloroethane 10 9.9 99 70-130
79-01-6 Trichloroethylene 10 10.4 104 70-130
75-69-4 Trichlorofluoromethane 10 10.9 109 60-140
96-18-4 1,2,3-Trichloropropane 10 9.4 94 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.9 99 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.3 103 70-130
75-01-4 Vinyl Chloride 10 10 100 60-140
m,p-Xylene 20 20.5 103 70-130
95-47-6 o-Xylene 10 9.9 99 70-130
1330-20-7 Xylene (total)30 30.4 101 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
26 of 32
FA5175755.2.2
Blank Spike Summary Page 1 of 1
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2321-BS A0211738.D 1 02/22/18 MM n/a n/a VA2321
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
108-88-3 Toluene 10 9.6 96 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
27 of 32
FA5175755.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51761-2MS A0211706.D 50 02/16/18 TD n/a n/a VA2319
FA51761-2MSD A0211707.D 50 02/16/18 TD n/a n/a VA2319
FA51761-2 a A0211701.D 50 02/16/18 TD n/a n/a VA2319
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-2, FA51757-3
FA51761-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 242 500 736 99 500 728 97 1 70-130/20
108-86-1 Bromobenzene ND 500 510 102 500 499 100 2 70-130/20
74-97-5 Bromochloromethane ND 500 481 96 500 485 97 1 70-130/20
75-27-4 Bromodichloromethane ND 500 483 97 500 443 89 9 70-130/20
75-25-2 Bromoform ND 500 406 81 500 376 75 8 70-130/20
104-51-8 n-Butylbenzene ND 500 528 106 500 530 106 0 70-130/20
135-98-8 sec-Butylbenzene ND 500 539 108 500 531 106 1 70-130/20
98-06-6 tert-Butylbenzene ND 500 517 103 500 512 102 1 70-130/20
56-23-5 Carbon Tetrachloride ND 500 492 98 500 455 91 8 70-130/20
108-90-7 Chlorobenzene ND 500 503 101 500 493 99 2 70-130/20
75-00-3 Chloroethane ND 500 590 118 500 548 110 7 60-140/20
67-66-3 Chloroform ND 500 481 96 500 471 94 2 70-130/20
95-49-8 o-Chlorotoluene ND 500 513 103 500 500 100 3 70-130/20
106-43-4 p-Chlorotoluene ND 500 503 101 500 492 98 2 70-130/20
124-48-1 Dibromochloromethane ND 500 465 93 500 428 86 8 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 500 492 98 500 469 94 5 70-130/20
106-93-4 1,2-Dibromoethane 6.9 J 500 508 100 500 503 99 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 500 403 81 500 385 77 5 60-140/20
95-50-1 1,2-Dichlorobenzene ND 500 499 100 500 489 98 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 500 512 102 500 499 100 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 500 483 97 500 469 94 3 70-130/20
75-34-3 1,1-Dichloroethane ND 500 524 105 500 515 103 2 70-130/20
107-06-2 1,2-Dichloroethane 6.8 J 500 486 96 500 477 94 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 500 511 102 500 507 101 1 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 500 507 101 500 501 100 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 500 515 103 500 500 100 3 70-130/20
78-87-5 1,2-Dichloropropane ND 500 498 100 500 497 99 0 70-130/20
142-28-9 1,3-Dichloropropane ND 500 481 96 500 480 96 0 70-130/20
594-20-7 2,2-Dichloropropane ND 500 417 83 500 406 81 3 70-130/20
563-58-6 1,1-Dichloropropene ND 500 502 100 500 486 97 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 500 423 85 500 398 80 6 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 500 433 87 500 401 80 8 70-130/20
108-20-3 Di-Isopropyl Ether ND 500 488 98 500 485 97 1 70-130/20
100-41-4 Ethylbenzene 96.6 500 597 100 500 585 98 2 70-130/20
87-68-3 Hexachlorobutadiene ND 500 508 102 500 493 99 3 70-130/20
98-82-8 Isopropylbenzene ND 500 554 111 500 549 110 1 70-130/20
* = Outside of Control Limits.
28 of 32
FA5175755.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51761-2MS A0211706.D 50 02/16/18 TD n/a n/a VA2319
FA51761-2MSD A0211707.D 50 02/16/18 TD n/a n/a VA2319
FA51761-2 a A0211701.D 50 02/16/18 TD n/a n/a VA2319
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-2, FA51757-3
FA51761-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 500 546 109 500 531 106 3 70-130/20
74-83-9 Methyl Bromide ND 500 428 86 500 440 88 3 60-140/20
74-87-3 Methyl Chloride ND 500 503 101 500 498 100 1 60-140/20
74-95-3 Methylene Bromide ND 500 491 98 500 487 97 1 70-130/20
75-09-2 Methylene Chloride ND 500 481 96 500 472 94 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 500 491 98 500 496 99 1 70-130/20
91-20-3 Naphthalene 192 500 679 97 500 741 110 9 70-130/20
103-65-1 n-Propylbenzene 15.0 J 500 529 103 500 510 99 4 70-130/20
100-42-5 Styrene ND 500 529 106 500 516 103 2 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 500 510 102 500 486 97 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 500 511 102 500 531 106 4 70-130/20
127-18-4 Tetrachloroethylene ND 500 511 102 500 492 98 4 70-130/20
108-88-3 Toluene 931 500 1420 98 500 1380 90 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 500 506 101 500 524 105 3 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 500 518 104 500 520 104 0 70-130/20
71-55-6 1,1,1-Trichloroethane ND 500 482 96 500 464 93 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 500 520 104 500 521 104 0 70-130/20
79-01-6 Trichloroethylene ND 500 498 100 500 487 97 2 70-130/20
75-69-4 Trichlorofluoromethane ND 500 522 104 500 467 93 11 60-140/20
96-18-4 1,2,3-Trichloropropane ND 500 482 96 500 487 97 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene 170 500 691 104 500 678 102 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 38.7 500 570 106 500 558 104 2 70-130/20
75-01-4 Vinyl Chloride ND 500 476 95 500 475 95 0 60-140/20
m,p-Xylene 421 1000 1470 105 1000 1440 102 2 70-130/20
95-47-6 o-Xylene 251 500 765 103 500 751 100 2 70-130/20
1330-20-7 Xylene (total)672 1500 2230 104 1500 2190 101 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA51761-2 Limits
1868-53-7 Dibromofluoromethane 99%99%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%97%96%70-130%
2037-26-5 Toluene-D8 99%100%99%70-130%
460-00-4 4-Bromofluorobenzene 99%99%98%70-130%
(a) Confirmation run.
* = Outside of Control Limits.
29 of 32
FA5175755.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51868-1MS A0211726.D 50 02/21/18 MM n/a n/a VA2320
FA51868-1MSD A0211727.D 50 02/21/18 MM n/a n/a VA2320
FA51868-1 A0211723.D 50 02/21/18 MM n/a n/a VA2320
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-3
FA51868-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 710 500 1130 84 500 1170 92 3 70-130/20
108-86-1 Bromobenzene ND 500 511 102 500 517 103 1 70-130/20
74-97-5 Bromochloromethane ND 500 524 105 500 532 106 2 70-130/20
75-27-4 Bromodichloromethane ND 500 496 99 500 506 101 2 70-130/20
75-25-2 Bromoform ND 500 337 67*500 365 73 8 70-130/20
104-51-8 n-Butylbenzene 27.1 500 562 107 500 572 109 2 70-130/20
135-98-8 sec-Butylbenzene 21.7 J 500 546 105 500 564 108 3 70-130/20
98-06-6 tert-Butylbenzene ND 500 517 103 500 520 104 1 70-130/20
56-23-5 Carbon Tetrachloride ND 500 527 105 500 522 104 1 70-130/20
108-90-7 Chlorobenzene ND 500 492 98 500 501 100 2 70-130/20
75-00-3 Chloroethane ND 500 650 130 500 590 118 10 60-140/20
67-66-3 Chloroform ND 500 511 102 500 507 101 1 70-130/20
95-49-8 o-Chlorotoluene 60.7 500 551 98 500 564 101 2 70-130/20
106-43-4 p-Chlorotoluene ND 500 504 101 500 517 103 3 70-130/20
124-48-1 Dibromochloromethane ND 500 431 86 500 440 88 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 500 535 107 500 536 107 0 70-130/20
106-93-4 1,2-Dibromoethane ND 500 517 103 500 519 104 0 70-130/20
75-71-8 Dichlorodifluoromethane ND 500 423 85 500 402 80 5 60-140/20
95-50-1 1,2-Dichlorobenzene ND 500 506 101 500 509 102 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 500 518 104 500 525 105 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 500 486 97 500 488 98 0 70-130/20
75-34-3 1,1-Dichloroethane ND 500 553 111 500 558 112 1 70-130/20
107-06-2 1,2-Dichloroethane ND 500 507 101 500 500 100 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 500 549 110 500 535 107 3 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 500 542 108 500 546 109 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 500 561 112 500 549 110 2 70-130/20
78-87-5 1,2-Dichloropropane ND 500 531 106 500 539 108 1 70-130/20
142-28-9 1,3-Dichloropropane ND 500 492 98 500 498 100 1 70-130/20
594-20-7 2,2-Dichloropropane ND 500 516 103 500 516 103 0 70-130/20
563-58-6 1,1-Dichloropropene ND 500 531 106 500 531 106 0 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 500 495 99 500 523 105 6 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 500 466 93 500 491 98 5 70-130/20
108-20-3 Di-Isopropyl Ether ND 500 521 104 500 520 104 0 70-130/20
100-41-4 Ethylbenzene 1830 500 2020 38* a 500 2110 56* a 4 70-130/20
87-68-3 Hexachlorobutadiene ND 500 515 103 500 532 106 3 70-130/20
98-82-8 Isopropylbenzene 155 500 691 107 500 716 112 4 70-130/20
* = Outside of Control Limits.
30 of 32
FA5175755.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51868-1MS A0211726.D 50 02/21/18 MM n/a n/a VA2320
FA51868-1MSD A0211727.D 50 02/21/18 MM n/a n/a VA2320
FA51868-1 A0211723.D 50 02/21/18 MM n/a n/a VA2320
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1, FA51757-3
FA51868-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 11.5 J 500 543 106 500 561 110 3 70-130/20
74-83-9 Methyl Bromide ND 500 504 101 500 467 93 8 60-140/20
74-87-3 Methyl Chloride ND 500 527 105 500 502 100 5 60-140/20
74-95-3 Methylene Bromide ND 500 552 110 500 553 111 0 70-130/20
75-09-2 Methylene Chloride ND 500 511 102 500 496 99 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether 47.5 500 562 103 500 564 103 0 70-130/20
103-65-1 n-Propylbenzene 387 500 826 88 500 862 95 4 70-130/20
100-42-5 Styrene ND 500 531 106 500 552 110 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 500 516 103 500 515 103 0 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 500 513 103 500 520 104 1 70-130/20
127-18-4 Tetrachloroethylene ND 500 523 105 500 524 105 0 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 500 493 99 500 528 106 7 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 500 533 107 500 536 107 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 500 508 102 500 502 100 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 500 552 110 500 568 114 3 70-130/20
79-01-6 Trichloroethylene ND 500 539 108 500 540 108 0 70-130/20
75-69-4 Trichlorofluoromethane ND 500 522 104 500 491 98 6 60-140/20
96-18-4 1,2,3-Trichloropropane ND 500 477 95 500 483 97 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene 1150 500 1460 62* a 500 1550 80 6 70-130/20
108-67-8 1,3,5-Trimethylbenzene 529 500 959 86 500 1000 94 4 70-130/20
75-01-4 Vinyl Chloride ND 500 506 101 500 490 98 3 60-140/20
m,p-Xylene 1300 1000 2140 84 1000 2210 91 3 70-130/20
95-47-6 o-Xylene 54.6 500 564 102 500 576 104 2 70-130/20
1330-20-7 Xylene (total)1360 1500 2710 90 1500 2790 95 3 70-130/20
CAS No.Surrogate Recoveries MS MSD FA51868-1 Limits
1868-53-7 Dibromofluoromethane 100%99%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%94%98%70-130%
2037-26-5 Toluene-D8 98%98%97%70-130%
460-00-4 4-Bromofluorobenzene 99%100%99%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
31 of 32
FA5175755.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA51757
Account:GRINCC GRI (Geological Resources Inc.)
Project:Grannys Grill/Leggetts Grocery; 1727 & 1731 US Hwy 13 N, Windsor, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA51757-1MS A0211739.D 100 02/22/18 MM n/a n/a VA2321
FA51757-1MSD A0211740.D 100 02/22/18 MM n/a n/a VA2321
FA51757-1 a A0211734.D 100 02/22/18 MM n/a n/a VA2321
The QC reported here applies to the following samples:Method: SM 6200B
FA51757-1
FA51757-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
108-88-3 Toluene 2560 1000 3530 97 1000 3560 100 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA51757-1 Limits
1868-53-7 Dibromofluoromethane 99%98%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%97%96%70-130%
2037-26-5 Toluene-D8 100%99%98%70-130%
460-00-4 4-Bromofluorobenzene 100%99%99%70-130%
(a) Sample vial(s) contained bubbles greater than 6mm; reported results are considered minimum values.
* = Outside of Control Limits.
32 of 32
FA5175755.3.3

APPENDIX B
Injection Event Record