WA-765_10673_CA_MMPE_20160128

EXECUTIVE SUMMARY
The former Red Apple Market # 3 site is located at 1332 East Memorial Drive in Ahoskie, Hertford County,
North Carolina. According to available information, two 12,000-gallon gasoline, one 8,000-gallon gasoline
and one 550-gallon kerosene underground storage tanks were removed from the site on June 3, 1993. Forty
monitoring wells have been installed at the site and adjacent properties during past ground water assessment
and corrective action activities. Free product had been previously measured in monitoring wells MW-7, MW-
8 and MW-15.

A Mobile Multi-Phase Extraction (MMPE) event was conducted on MW-2 and MW-7 between December 7
and December 11, 2015. No free product was measured in the monitoring wells prior to the MMPE event. A
total of 18,657 gallons of affected ground water was recovered during the MMPE event. At the conclusion of
the event, no measurable free product was observed in MW-2 or MW-7. The average fluid recovery rate was
194.34 gallons per hour. Based on mass-removal calculations, approximately 304.77 pounds or 48.76 gallons
of vapor phase hydrocarbons were removed during the event.

On January 11, 2016, eight monitoring wells were gauged, purged and sampled. Concentrations of requested
method constituents that exceeded the Maximum Allowable Concentrations (MACs) specified in T15A NCAC
2L.0202 were reported in the ground water samples collected from MW-2, MW-3A, MW-6, MW-7, MW-9,
MW-14 and MW-17. The concentration of benzene reported in MW-7 exceeded the Gross Contamination
Level (GCL).

Based on the January 2016 sampling results, Geological Resources, Inc. recommends that additional MMPE
events should be conducted on MW-7 in order to reduce contaminant concentrations at the site. Semi-annual
ground water monitoring should continue at the site until contaminant concentrations are reduced to below the
GCLs. The next semi-annual ground water monitoring event is tentatively scheduled for July 2016.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 MMPE EVENT ......................................................................................................................... 1
4.0 GROUND WATER QUALITY ............................................................................................... 2
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 3
6.0 LIMITATIONS........................................................................................................................ 4

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Free Product Recovery Results
Table 3: Free Product Recovery Event Information
Table 4: Free Product Recovery Cost Summary
Table 5: Laboratory Analytical Results – Ground Water Samples

APPENDICES
Appendix A: MMPE Data and Calculations
Appendix B: Disposal Manifests
Appendix C: Laboratory Report - Ground Water Samples

1

1.0 SITE HISTORY AND CHARACTERIZATION
According to available information, two 12,000-gallon gasoline, one 8,000-gallon gasoline and one 550-
gallon kerosene underground storage tanks (USTs) were removed from the site on June 3, 1993. Forty
monitoring wells have been installed at the site and adjacent properties during past ground water
assessment and corrective action activities. The site is currently ranked as Intermediate risk due to the
presence of free product that was historically measured in MW-7, MW-8 and MW-15. The site is located
within the designated wellhead protection area for the Town of Ahoskie.

Site activities performed prior to May 2008 were conducted by previous consultants. Although
Geological Resources, Inc. (GRI) cannot verify the accuracy of information obtained from previous
reports, for the purposes of this report, it is assumed to be correct. Please refer to previous submittals for
further historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
This report presents the results of the MMPE event and ground water assessment activities conducted
between December 2015 and January 2016 at the former Red Apple Market # 3 site located at 1332 East
Memorial Drive in Ahoskie, Hertford County, North Carolina (Figure 1). The activities were conducted
in accordance with GRI proposal number 15-514, which was submitted to NCDEQ on September 4,
2015, and approved as Task Authorization No. 10673-14 on September 18, 2015. The purpose of these
activities was to reduce contaminant concentrations and to obtain current ground water quality data for
the site.

3.0 MMPE EVENT
A MMPE event was conducted at the site by Greenwood Applied Services, Inc. under the supervision of
GRI beginning on December 7, 2015 and ending on December 11, 2015. The MMPE equipment included
a liquid ring pump, a 6,500-gallon capacity tanker, flexible vacuum hoses, 1-inch diameter PVC stinger
pipes and associated couplings and pipe fittings to manifold to two monitoring wells simultaneously. The
MMPE system was rated at 24 in. Hg at 280 cfm. Vacuum monitoring wells MW-2 and MW-7 and
observation monitoring wells MW-3A and MW-8 were gauged on December 7, 2015, prior to the event.
No free product was measured in the monitoring wells. The stinger pipes were initially set at depths of
9.35 feet and 8.84 in MW-2 and MW-7, respectively.

Monitoring wells MW-2 and MW-7 were each vacuumed continuously for the 96 hour event. During the

2

event, measurements of relative humidity, temperature, vacuum, exhaust velocity and off-gas
concentrations were recorded at the discharge stack a minimum of two times per 24-hour period.
Vacuum at the extraction wells ranged from 7.0 to 18.0 in. Hg. System vacuum ranged from 11.0 to 17.0
in. Hg. Exhaust velocities ranged from 1,289 to 3,051 fpm. Temperatures ranged from 50.1 to 70.0 ̊F
and relative humidity ranged from 40.2 to 72.4 percent. Total VOC off-gas concentrations ranged from
114.1 to 505.7 ppm during the event. A summary of the gauging data obtained before start up and at the
conclusion of the MMPE event is presented in Table 1. A copy of the MMPE data and calculations has
been included as Appendix A.

The results of the MMPE event indicate that a total of 18,657 gallons of liquids was removed during the
event. Based on 96 hours of operation, the average liquid recovery rate was 194.34 gallons per hour.
Based on mass-removal calculations, an additional 304.77 pounds (48.76 gallons) of vapor phase
hydrocarbons were removed during the MMPE event. Based on the total amount of fluids removed
during the event, the cost per gallon of fluid removed was approximately $0.63. A summary of free
product recovery data has been included as Table 2. Summaries of MMPE event information and cost
analysis are provided in Tables 3 and 4, respectively. At the conclusion of the MMPE event, all
wastewater was transported to a permitted facility for disposal. Copies of the disposal manifests have
been included as Appendix B.

4.0 GROUND WATER QUALITY
Eight monitoring wells (MW-1A, MW-2, MW-3A, MW-6, MW-7, MW-9, MW-14 and MW-17) were
gauged, purged and sampled on January 11, 2016. Please note, MW-8 was located under a disabled
vehicle and was not sampled. The depths to ground water in the Type II monitoring wells during the
January 2016 sampling event ranged from 7.80 to 8.83 feet below the tops of well casings. Ground water
elevations in the Type II monitoring wells relative to a temporary benchmark with an assumed datum of
100.00 feet ranged from 91.58 to 92.09 feet. Based on this information, ground water flow across the site
was generally toward the south with an average horizontal hydraulic gradient of less than 0.01 feet per
foot. A Site Map showing the locations of monitoring wells and structures onsite is included as Figure 2.
A Water Table Surface Map for the January 2016 sampling event has been included as Figure 3. Well
construction and gauging information are presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the January 2016 sampling event for volatile organic compounds using EPA Method 6200B.
Concentrations of one or more BTEX constituents, MTBE, naphthalene, bromodichloromethane,

3

dibromochloromethane, IPE, n-butylbenzene, sec-butylbenzene, 1,2-dichloroethane, isopropylbenzene, n-
propylbenzene, p-isopropyltoluene, 1,2-dibromoethane, styrene, 1,3,5-trimethylbenzene and/or 1,2,4-
trimethylbenzene that exceeded the Maximum Allowable Concentrations (MACs) specified in T15A
NCAC 2L.0202 were reported in the ground water samples collected from MW-2, MW-3A, MW-6, MW-
7, MW-9, MW-14 and MW-17. The concentration of benzene reported in the ground water sample
collected from MW-7 exceeded the Gross Contamination Level (GCL). A Ground Water Quality Map
based on data from the January 2016 monitoring well sampling event has been included as Figure 4. A
summary of ground water sample analytical results is presented in Table 5. A complete laboratory report
has been included in Appendix C.

5.0 CONCLUSIONS AND RECOMMENDATIONS
 A MMPE event was conducted on MW-2 and MW-7 between December 7 and December 11,
2015. A total of 18,657 gallons of affected ground water was recovered during the MMPE event.
 No measurable free product was observed in MW-2 or MW-7 before or after the event. The
average fluid recovery rate was 194.34 gallons per hour. Based on mass-removal calculations,
approximately 304.77 pounds or 48.76 gallons vapor phase hydrocarbons were removed at an
average of 0.51 gallons per hour by the MMPE system. The cost of total fluids recovered per
gallon during the December 2015 MMPE event was $0.63.
 The average depth to ground water in the monitoring wells during the January 2016 sampling
event was 8.20 feet. Ground water flow during the January 2016 sampling event was generally
toward the south with an average horizontal hydraulic gradient of less than 0.01 feet per foot.
 Concentrations of one or more BTEX constituents, MTBE, naphthalene, bromodichloromethane,
dibromochloromethane, IPE, n-butylbenzene, sec-butylbenzene, 1,2-dichloroethane,
isopropylbenzene, n-propylbenzene, p-isopropyltoluene, 1,2-dibromoethane, styrene, 1,3,5-
trimethylbenzene and/or 1,2,4-trimethylbenzene that exceeded the MACs were reported in the
ground water samples collected from MW-2, MW-3A, MW-6, MW-7, MW-9, MW-14 and MW-
17. The concentration of benzene reported in the ground water sample collected from MW-7
exceeded the GCL.
 GRI recommends that additional MMPE events should be conducted at the site in order to reduce
contaminant concentrations in MW-7. Semi-annual ground water monitoring should continue at
the site until the contaminant concentrations are reduced to below the GCLs. The next semi-
annual sampling event is tentatively scheduled for July 2016.

4

6.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Hertford County, North Carolina. The assessment was conducted
based on the scope of work and level of effort desired by NCDEQ and with resources adequate only for
that scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the May 2008 sampling and updated receptor survey event were not obtained under the supervision of
GRI. Although the accuracy of these data cannot be verified, for the purpose of this report GRI assumes
that they are correct.

FIGURES

TABLES
MW-1 Unknown 04/23/08 NA NA NA 99.29 9.43 0.00 89.86      
01/07/09 9.94 0.00 89.35
05/11/10 8.89 0.00 90.40
05/02/11 8.90 0.00 91.10
07/23/12 9.39 0.00 89.90 Before MMPE
07/27/12 9.49 0.00 89.80 After MMPE
08/28/12 9.10 0.00 90.90
08/19/13 9.42 0.00 90.58
07/08/14 9.13 0.00 90.87
03/24/15 8.02 0.00 91.98
01/11/16 8.25 0.00 91.75
04/23/08 9.85 0.00 90.25
10.28 0.00 89.82 Before AFVR
10.35 0.01 89.76 After AFVR
01/07/09 10.40 0.00 89.70
05/11/10 9.45 0.00 90.65
03/28/11 9.53 0.00 90.57 Before MMPE
04/01/11 9.50 0.00 90.60 After MMPE
05/02/11 9.38 0.00 91.03
07/23/12 9.89 0.00 90.52 Before MMPE
07/27/12 10.12 0.00 90.29 After MMPE
08/28/12 9.52 0.00 90.89
07/15/13 9.30 0.00 91.11 Before MMPE
07/19/13 9.90 0.00 90.51 After MMPE
08/19/13 NM NM NM
9.21 0.00 91.20 Before AFVR
9.73 0.00 90.68 After AFVR
07/08/14 9.69 0.00 90.72
03/24/15 8.01 0.00 92.40
12/07/15 9.30 0.00 91.11 Before MMPE
12/11/15 9.55 0.00 90.86 After MMPE
01/11/16 8.79 0.00 91.62
MW-3 Unknown 04/23/08 NA NA NA 99.93 10.03 0.00 89.90
01/07/09 10.55 0.00 89.38
05/11/10 9.59 0.00 90.34
05/02/11 9.52 0.00 91.03
07/23/12 10.24 0.00 90.31 Before MMPE
07/27/12 10.24 0.00 90.31 After MMPE
08/28/12 9.65 0.00 90.90
08/19/13 10.01 0.00 90.54
07/08/14 9.80 0.00 90.75
03/24/15 8.56 0.00 91.99
01/11/16 8.83 0.00 91.72
04/23/08 9.39 0.00 90.30
01/07/09 9.93 0.00 89.76
05/11/10 9.75 0.00 89.94
05/02/11 9.53 0.00 90.57
08/28/12 9.62 0.00 90.48
08/19/13 NM NM NM
04/23/08 NM NM NM Not Located
01/07/09 NM NM NM Not Located
05/02/11 NM NM NM Covered
08/28/12 NM NM NM Covered
08/19/13 NM NM NM No Access
07/08/14 NM NM NM Not Located
04/23/08 NM NM NM Not Located
01/07/09 9.52 0.00 89.59
05/11/10 8.68 0.00 90.43
05/02/11 8.61 0.00 90.77
08/28/12 8.64 0.00 90.74
08/19/13 9.26 0.00 90.12
07/08/14 8.92 0.00 90.46
03/24/15 7.64 0.00 91.74
01/11/16 7.80 0.00 91.58
08/13/08
MW-2
100.55
20NANAUnknownMW-3A
06/05/14
100.10
18.4NANAUnknownMW-1A
100.41
188-18809/15/93
99.38
166-16601/07/94MW-6
99.42
Depth to
Water from
Top of
Casing
(ft.)
99.93
99.69
99.29
100.00
Free Product
Thickness**
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation*
(ft.)
CommentsWell ID Date Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
MW-5 01/07/94
MWD-4 01/07/94
100.10
NM
Date: 01/12/16
20 20-25
99.11
16
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
25
6 6-16
Page 1 of 5
Depth to
Water from
Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation*
(ft.)
CommentsWell ID Date Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Date: 01/12/16
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
04/23/08 NM NM NM Not Located
10.30 0.00 89.17 Before AFVR
10.27 0.71 89.81 After AFVR
10.80 1.11 89.62 Before AFVR
10.53 0.01 88.95 After AFVR
01/07/09 10.25 0.45 89.61
04/05/10 8.10 0.31 91.64 Before MMPE
04/09/10 8.80 0.00 90.67 After MMPE
05/11/10 8.90 0.00 90.57
03/28/11 9.02 0.02 90.47 Before MMPE
04/01/11 9.09 0.00 90.38 After MMPE
05/02/11 8.85 0.00 91.12
07/23/12 9.34 0.00 90.63 Before MMPE
07/27/12 9.57 0.00 90.40 After MMPE
08/28/12 8.97 0.00 91.00
07/15/13 8.77 0.00 91.20 Before MMPE
07/19/13 9.17 0.00 90.80 After MMPE
08/19/13 9.43 0.00 90.54
8.73 0.07 91.30 Before AFVR
9.12 0.00 90.85 After AFVR
07/08/14 9.11 0.00 90.86
03/24/15 6.88 0.00 93.09
12/07/15 8.79 0.00 91.18 Before MMPE
12/11/15 9.12 0.00 90.85 After MMPE
01/11/16 8.13 0.00 91.84
04/23/08 10.64 1.71 89.97
11.10 1.80 89.58 Before AFVR
9.71 0.30 89.69 After AFVR
11.40 1.82 89.30 Before AFVR
9.99 0.00 89.15 After AFVR
01/07/09 10.50 0.90 89.41
04/05/10 7.71 0.00 91.43 Before MMPE
04/09/10 8.60 0.00 90.54 After MMPE
05/11/10 8.80 0.00 90.34
03/28/11 9.05 0.21 90.27 Before MMPE
04/01/11 9.92 0.00 89.22 After MMPE
05/02/11 8.78 0.03 91.05
07/23/12 9.29 0.06 90.56 Before MMPE
07/27/12 9.43 0.00 90.37 After MMPE
08/28/12 8.80 0.00 91.00
08/19/13 9.33 0.00 90.47
07/08/14 9.05 0.00 90.75
03/24/15 7.79 0.00 92.01
04/23/08 NM NM NM Not Located
01/07/09 NM NM NM Not Located
05/11/10 NM NM NM Under Junk Cars
05/02/11 NM NM NM Under Junk Cars
07/23/12 9.29 0.00 90.78 Before MMPE
07/27/12 9.39 0.00 90.68 After MMPE
08/28/12 8.77 0.00 91.30
08/19/13 9.41 0.00 90.66
07/08/14 9.09 0.00 90.98
03/24/15 7.76 0.00 92.31
01/11/16 8.00 0.00 92.07
04/23/08 7.04 0.00 90.58
01/07/09 7.70 0.00 89.92
05/11/10 7.18 0.00 90.44
05/02/11 7.04 0.00 90.43
08/28/12 6.95 0.00 90.52
08/19/13 7.71 0.00 89.76
07/08/14 7.43 0.00 90.04
03/24/15 6.08 0.00 91.39
04/23/08 8.69 0.00 90.26
01/07/09 9.42 0.00 89.53
05/11/10 8.71 0.00 90.24
05/02/11 8.57 0.00 90.73
08/28/12 8.46 0.00 90.84
08/19/13 9.23 0.00 90.07
07/08/14 8.96 0.00 90.34
03/24/15 7.57 0.00 91.73
04/23/08 8.25 0.00 90.39      
01/07/09 8.95 0.00 89.69
05/11/10 8.12 0.00 90.52
05/02/11 8.05 0.00 90.47
08/28/12 8.05 0.00 90.47
08/19/13 8.64 0.00 89.88
07/08/14 8.40 0.00 90.12
03/24/15 7.13 0.00 91.39
99.14
08/13/08
12/29/08
12/29/08
08/13/08
NA
97.47
MW-8 01/10/94
MW-7
11/25/94 6 6-16
Unknown NA NA
6
16
16MW-11 11/25/94
6-16601/10/94
MW-12
6 6-16
MW-10
99.97
98.95
99.15
99.30
98.52
99.80
97.62
99.47
100.07
6
166-16
06/05/14
6-16 16
16
MW-9
98.64
01/10/94
Page 2 of 5
Depth to
Water from
Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation*
(ft.)
CommentsWell ID Date Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Date: 01/12/16
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
04/23/08 NM NM NM Not Located
01/07/09 9.45 0.00 89.37
05/11/10 8.27 0.00 90.55
05/02/11 8.50 0.00 90.99
03/28/11 8.61 0.00 90.88 Before MMPE
04/01/11 8.72 0.00 90.77 After MMPE
08/28/12 8.51 0.00 90.98
08/19/13 9.12 0.00 90.37
07/08/14 8.81 0.00 90.68
03/24/15 NM NM NM Not Located
04/23/08 9.11 0.00 90.07      
01/07/09 9.73 0.00 89.45
05/11/10 8.69 0.00 90.49
05/02/11 8.66 0.00 91.19
08/28/12 8.77 0.00 91.08
08/19/13 9.29 0.00 90.56
07/08/14 8.96 0.00 90.89
03/24/15 7.67 0.00 92.18
01/11/16 7.94 0.00 91.91
04/23/08 9.06 0.00 89.98      
01/07/09 9.76 0.03 89.31
05/11/10 9.07 0.00 89.97
05/02/11 8.94 0.00 90.82
08/28/12 8.80 0.00 90.96
08/19/13 9.67 0.00 90.09
07/08/14 NM NM NM Behind Locked Fence
03/24/15 NM NM NM Behind Locked Fence
MW-16 Unknown 04/23/08 NA NA NA 97.03 6.26 0.00 90.77      
01/07/09 6.78 0.00 90.25
05/12/10 6.91 0.00 90.12
05/02/11 6.68 0.00 90.26
08/28/12 6.25 0.00 90.69
08/19/13 7.42 0.00 89.52
07/08/14 NM NM NM Not Located
03/24/15 NM NM NM Not Located
04/23/08 9.18 0.00 90.05      
01/07/09 9.79 0.00 89.44
05/11/10 8.54 0.00 90.69
05/02/11 8.59 0.00 91.39
08/28/12 8.76 0.00 91.22
08/19/13 9.16 0.00 90.82
07/08/14 8.68 0.00 91.30
03/24/15 7.59 0.00 92.39
01/11/16 7.89 0.00 92.09
04/23/08 7.25 0.00 89.47      
01/07/09 7.80 0.00 88.92
05/02/11 6.79 0.00 90.66
08/28/12 7.00 0.00 90.45
08/19/13 7.23 0.00 90.22
07/08/14 7.00 0.00 90.45
03/24/15 6.09 0.00 91.36
04/23/08 7.76 0.00 89.29
01/07/09 8.38 0.00 88.67
05/12/10 7.56 0.00 89.49
05/02/11 7.49 0.00 90.31
08/28/12 7.66 0.00 90.14
08/19/13 8.02 0.00 89.78
07/08/14 7.77 0.00 90.03
03/24/15 6.91 0.00 90.89
04/23/08 9.29 0.00 90.13
01/07/09 9.92 0.00 89.50
05/11/10 8.65 0.00 90.77
05/02/11 8.74 0.00 91.38
08/28/12 8.95 0.00 91.17
08/19/13 9.29 0.00 90.83
07/08/14 8.96 0.00 91.16
03/24/15 7.79 0.00 92.33
04/23/08 9.29 0.00 90.12
01/07/09 9.98 0.00 89.43
05/02/11 8.77 0.00 91.34
08/28/12 8.93 0.00 91.18
08/19/13 9.34 0.00 90.77
07/08/14 8.88 0.00 91.23
03/24/15 7.74 0.00 92.37
04/23/08 8.39 0.00 89.85
01/07/09 8.94 0.00 89.30
05/12/10 8.24 0.00 90.00
05/02/11 8.15 0.00 89.97
08/28/12 8.25 0.00 89.87
08/19/13 8.65 0.00 89.47
07/08/14 8.41 0.00 89.71
03/24/15 7.53 0.00 90.59
605/17/96MW-17
6MW-15 166-16
MW-16A
98.24
97.05
166-16611/25/94
166-16
96.72
100.11
98.12
99.41
99.42
MW-22 08/07/00 7
16
7-17 17
MW-21 05/18/96 6 6-16 16
MW-20 05/18/96 6 6-16
100.12
MW-18 05/17/96
05/17/96 6-16 16
99.85
99.76
MW-14
11/25/94MW-13
NAUnknown
16
97.45
97.80
6 6-16 16
99.49
6-16
99.04
98.82
99.18
6
99.98
97.03
99.23
05/15/96
96.94
20NA
MW-19
6
Page 3 of 5
Depth to
Water from
Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation*
(ft.)
CommentsWell ID Date Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Date: 01/12/16
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
04/23/08 7.11 0.00 89.87
01/07/09 7.62 0.00 89.36
05/12/10 6.85 0.00 90.13
05/02/11 6.79 0.00 90.09
08/28/12 6.94 0.00 89.94
08/19/13 NM NM NM
04/23/08 NM NM NM Not Located
01/07/09 4.72 0.00 90.78
05/12/10 NM NM NM Not Located
05/02/11 5.12 0.00 90.25
08/28/12 4.32 0.00 91.05
08/19/13 5.83 0.00 89.54
07/08/14 5.64 0.00 89.73
03/24/15 NM NM NM Not Located
04/23/08 1.70 0.00 93.66
01/07/09 2.39 0.00 92.97
05/02/11 4.32 0.00 90.89
08/28/12 NM NM NM Not Located
08/19/13 6.14 0.00 89.07
07/08/14 4.89 0.00 90.32
03/24/15 2.30 0.00 92.91
04/23/08 8.71 0.00 90.81
01/07/09 9.50 0.00 90.02
05/02/11 8.92 0.00 90.47
08/28/12 8.53 0.00 90.86
08/19/13 9.64 0.00 89.75
07/08/14 9.39 0.00 90.00
03/24/15 NM NM NM Not Located
04/23/08 NM NM NM Not Located
01/07/09 7.55 0.00 90.21
05/02/11 7.40 0.00 90.23
08/28/12 6.74 0.00 90.89
08/19/13 NM NM NM
04/23/08 9.53 0.00 89.48
01/07/09 10.00 0.00 89.01
05/02/11 9.30 0.00 89.60
08/28/12 9.42 0.00 89.48
08/19/13 NM NM NM
03/24/15 8.88 0.00 90.02
04/23/08 NM NM NM Not Located
01/07/09 11.58 0.00 88.43
05/12/10 12.01 0.00 88.00
05/02/11 11.53 0.00 88.40
08/28/12 10.97 0.00 88.96
08/19/13 12.49 0.00 87.44
07/08/14 12.14 0.00 87.79
03/24/15 10.56 0.00 89.37
04/23/08 NM NM NM Not Located
01/07/09 NM NM NM Not Located
05/12/10 NM NM NM Not Located
05/02/11 NM NM NM Destroyed
08/28/12 NM NM NM Destroyed
04/23/08 NM NM NM Not Located
01/07/09 6.63 0.00 90.14
05/12/10 6.47 0.00 90.30
05/02/11 6.35 0.00 90.27
08/28/12 NM NM NM Not Located
08/19/13 NM NM NM
03/24/15 5.24 0.00 91.38
04/23/08 10.15 0.00 90.15
01/07/09 10.72 0.00 89.58
05/12/10 9.37 0.00 90.93
05/02/11 9.49 0.00 91.55
08/28/12 9.70 0.00 91.34
08/19/13 NM NM NM
03/24/15 NM NM NM Not Located
04/23/08 NM NM NM Not Located
01/07/09 4.42 0.00 NA
05/12/10 5.66 0.00 NA
05/02/11 4.90 0.00 87.52
08/28/12 3.38 0.00 89.04
08/19/13 5.85 0.00 86.57
07/08/14 5.70 0.00 86.72
03/24/15 3.60 0.00 88.82
05/12/10 96.60 9.29 0.00 87.31
05/02/11 8.70 0.00 87.76
08/28/12 7.90 0.00 88.56
08/19/13 9.68 0.00 86.78
07/08/14 9.38 0.00 87.08
03/24/15 7.66 0.00 88.80
5 5-15
NM
Unknown
100.30
96.77
100.01
99.01
99.93
95.36
97.76
Unknown NA NA NA
92.42
93.19
15
25
97.63
2003/11/10 5 5-20 96.46
MW-33
15
MW-30 05/01/01
05/02/01 5 5-15 15
96.62
96.98
MW-29 05/01/01
NA
MW-34
MW-31
15-25
MW-28 05/01/01 10 10-20.5 20.00
MW-27 05/02/01 5 5-15 15
15
95.21
17
15
MW-26 08/08/00 5 15
99.39
99.52
5-15
MW-25 08/07/00 5 5-15
08/07/00 7 7-17
MW-24 08/07/00
95.37
96.88
95.50
5-155
MW-23
101.04
18NANA
98.90
MW-32
Page 4 of 5
Depth to
Water from
Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Facility ID # : 0-017539
Groundwater
Elevation*
(ft.)
CommentsWell ID Date Installed
(mm/dd/yy)
Top of Casing
Elevation*
(ft.)
Screened
Interval
(x to y ft. 
BGS)
Bottom of
Well
(ft. BGS)
Date: 01/12/16
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
05/12/10 99.13 8.73 0.00 90.40
05/02/11 8.60 0.00 90.48
08/28/12 8.27 0.00 90.81
08/19/13 NM NM NM
05/12/10 100.56 9.33 0.00 91.23
05/02/11 9.35 0.00 91.04
08/28/12 9.54 0.00 90.85
08/19/13 NM NM NM
05/02/11 7.96 0.00 86.01
08/28/12 6.07 0.00 87.90
08/19/13 NM NM NM
03/24/15 5.80 0.00 88.17
05/02/11 6.31 0.00 87.00
08/28/12 5.34 0.00 87.97
08/19/13 NM NM NM
03/24/15 5.22 0.00 88.09
05/02/11 8.18 0.00 89.09
08/28/12 6.90 0.00 90.37
08/19/13 NM NM NM
03/24/15 7.40 0.00 89.87
05/02/11 8.69 0.00 91.21
08/28/12 8.78 0.00 91.12
08/19/13 9.27 0.00 90.63
07/08/14 8.88 0.00 91.02
03/24/15 7.63 0.00 92.27
Notes:
•  * : Reference point for elevation measurements, Assumed elevation 100.00 ft.
•  ** : If free product is present in a well, groundwater elevation should be calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness 
   x 0.8581].
•  ft BGS : feet below ground surface.
•  NA: Not available.
•  NM: Not measured; well could not be located or was inaccessible.
MW-39 05/02/11 5-15
6-16 16 100.39
05/02/11 5MW-37 5-15
MW-36
MW-35 6 6-16
03/11/10 6
03/11/10 16 99.08
•  Top of casing elevations were surveyed by Coastal Engineering & Surveying, Inc. in May 2011.
MW-40 05/02/11 5 5-15 15 99.90
5
15 93.97
97.2715
93.31155-15505/02/11MW-38
Page 5 of 5
Date: 01/21/16
Method of Measurement:
Well ID Product Type
(gas, diesel, etc.)
Date of
Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product
Thickness Before
Recovery
(feet)
Product
Thickness After
Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of
Product
Recovered
(gallons)
MW-8 08/13/08 AFVR 2 1.80 0.30 350 6.60
MW-7 2 1.11 0.01
MW-8 2 1.82 0.01
MW-7 2 0.31 -
MW-8 2 --
MW-2 2 --
MW-7 2 0.02 -
MW-8 2 0.21 -
MW-2 2 --
MW-7 2 --
MW-8 2 0.06 -
MW-2 2 --
MW-7 2 --
MW-2 2 --
MW-7 2 0.07 -
MW-2 2 --
MW-7 2 --
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
Gasoline and
Kerosene
12/29/08 AFVR 3,078 2.80
04/05/10 to
04/09/10 0.0014,915MMPE
TABLE 2
FREE PRODUCT RECOVERY RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Interface probe at top-of-casing
03/28/11 to
04/01/11 MMPE 14,454 0.00
Facility ID#: 0-017539
07/23/12 to
07/27/12 MMPE 14,774 0.00
07/15/13 to
07/19/13 MMPE 14,135 0.00
06/05/14 AFVR 2,964 0.00
12/07/15 to
12/11/15 MMPE 18,657 0.00
Date: 01/21/16
MW-8 08/13/08 AFVR 7,805.81 227.76 67.18 2.30 350 6.60 8.90
MW-7
MW-8
MW-7
MW-8
MW-2
MW-7
MW-8
MW-2
MW-7
MW-8
MW-2
MW-7
MW-2
MW-7
MW-2
MW-7
69.49 83,327 9.40 78.89
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.25
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
6,787.80
6,674.00
MMPE
AFVR
04/05/10 to
04/09/10
12/29/08
3.17
2.92
196.93
385.75
139.93
189.78
Facility ID #: 0-017539
3.17
5.72
0.00
2.80
14,915
3,078
48.76
TABLE 3
FREE PRODUCT RECOVERY EVENT INFORMATION
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Well ID Date
(mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average
Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
Total Amount of
Product
Recovered
(gallons)
03/28/11 to
04/01/11 MMPE 927.60 104.2 431.5 2.33 14,454 0.00 2.33
07/23/12 to
07/27/12 MMPE 4,218.27 147.48 301.57 6.12 14,774 0.00 6.12
07/15/13 to
07/19/13 MMPE 3,949.00 151.34 326.61 3.16 14,135 0.00 3.16
06/05/14 AFVR 3,933.00 224.52 60.38 0.72 2,964 0.00
Total To Date 83,396.49 78.89
0.72
Totals
SUMMARY OF FLUID REMOVAL
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
12/07/15 to
12/11/15 224.93 48.76 18,657
Current Event 18,705.76 48.76
MMPE 2,260.75 59.23 0.00
Date: 01/21/16
Wells Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Fluids
Recovered (gallons)
Cost of Free
Product Recovery
Event
Cost Per
Gallon
MW-7, MW-8 MMPE 04/05/10 to
04/09/10 14,918.17 $10,182.65 $0.68
MW-2, MW-7,
MW-8 MMPE 03/28/11 to
04/01/11 14,460.99 $11,351.50 $0.78
MW-2, MW-7,
MW-8 MMPE 07/23/12 to
07/27/12 14,780.12 $11,598.50 $0.78
MW-2 and MW-7 MMPE 07/15/13 to
07/19/13 14,138.16 $11,355.65 $0.80
MW-2 and MW-7 AFVR 06/05/14 2,964.72 $3,093.45 $1.04
MW-2 and MW-7 MMPE 12/07/15 to
12/11/15 18,705.76 $11,773.50 $0.63
79,967.92 $59,355.25 $0.74
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, report preparation and project management.
Facility ID #: 0-017539
TOTAL (to date)
TABLE 4
FREE PRODUCT RECOVERY COST SUMMARY
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Comments
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
MW-1 04/23/08 <0.31 0.620 I 1.14 4.63 <0.12 17.3 <0.14 1.16 0.900 I <0.12 0.380 I <0.15 1.02 <0.33 10.2 2.23 33.5 <100 <100 3,020 1,110 194 2,760
01/09/09 0.65 J <0.70 0.60 J 1.9 J 1.7 J 2.3 JB <0.90 12 B <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 1.1 J <0.50 27.5 <100 <100 <105 <105 <100 <105
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 39.9 <100 <100 <97.1 <97.1 <100 <97.1
05/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 30.0 <35 <35 <110 <110 <35 <160
07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 58.3 <35 <35 <100 <100 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
01/11/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
04/23/08 1,100 446 203 599 427 186 <1.4 <3.9 <4.7 7.90 I 18.6 15.4 I 27.9 <3.3 248 70.4 16.3 4,120 <100 133 <75 1,680 170
01/09/09 410 28 31 80 110 95 B <1.8 <1.7 2.5 J 3.2 J 9.8 J 14 J 6.6 J <1.6 21 6.4 J 14.8 1,820 241 <100 <100 247 124
05/12/10 4,030 2,610 1,040 2,820 785 478 <0.500 34.2 8.27 <0.500 59.3 59.6 121 <0.500 753 304 15.6 17,300 2,550 <100 <100 2,680 230
05/02/11 6,070 9,230 1,370 4,839 1,260 256 <29 <25 <26 47.6 J 34.6 J 55.5 J 118 J <34 848 256 NR NR NR NR NR NR NR
08/28/12 6,630 9,660 1,450 5,110 1,320 400 <23 <20 <20 <33 41.4 J 62.1 J 128 <27 932 275 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/09/14 3,030 2,060 1,160 2,500 759 372 <10 <10 <10 <10 44.5 J 39.7 J 138 <10 685 232 <5.0 6,620 <350 1,550 <400 2,630 <600
03/24/15 1,730 1,260 155 791 734 131 <1.5 2.1 J <1.4 4.0 J 11.6 33.5 24.9 <1.5 194 67.2 NR NR NR NR NR NR NR
01/11/16 2,480 2,220 261 1,530 887 117 <13 <13 <13 16.4 J 13.9 J 39.9 J 32.9 J <13 288 86.7 NR NR NR NR NR NR NR
MW-3 04/23/08 <0.31 <0.28 <0.31 1.39 I 5.30 <0.41 1.13 <0.39 <0.47 <0.12 <0.24 1.45 I <0.30 <0.33 0.860 I 0.290 I 48.0 <100 <100 <75 <75 <100 77.0
01/09/09 2.2 J <0.70 <0.50 <1.0 1.8 J 3.8 JB <0.90 <0.85 <0.70 <1.1 <0.55 2.7 J <0.75 <0.80 <0.70 <0.50 21.1 <100 <100 <105 <105 <100 <105
05/12/10 1.66 <0.500 <0.500 <1.00 4.10 <5.00 <0.500 <0.500 <0.500 0.910 <0.500 5.11 <0.500 <0.500 <0.500 <0.500 34.9 <100 <100 <99.0 <99.0 <100 <99.0
05/02/11 3.6 <0.13 <0.15 <0.30 3.4 0.17 J <0.12 <0.10 0.19 J 1.4 <0.10 7.3 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 11.5 0.28 J <0.15 1.2 J 1.8 0.37 J <0.12 <0.10 0.44 J 0.87 0.50 3.6 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 60.0 2.3 6.0 2.9 5.8 3.0 <0.10 0.27 J 1.6 1.4 3.8 8.3 1.9 <0.10 0.19 J 0.21 J 7.8 220 148 128 J <100 149 <160
07/09/14 0.85 <0.10 <0.10 <0.20 3.3 0.17 J <0.10 <0.10 0.38 J 0.63 0.13 J 3.5 <0.10 <0.10 <0.10 <0.10 10.8 60.8 J <35 <100 <100 <35 213
03/24/15 2.6 <0.17 <0.15 <0.43 0.41 J 0.15 J 0.81 <0.14 <0.14 <0.16 <0.12 0.34 J <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
01/11/16 4.1 <0.13 <0.13 <0.31 1.4 0.18 J 1.3 <0.13 <0.13 0.29 J <0.13 0.87 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
04/23/08 <0.31 <0.28 <0.31 <1.2 0.650 I <0.41 0.810 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 6.06 <100 <100 <75 76.6 <100 77.3
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 1.1 JB 0.93 J 12 B <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 <1.5 <100 <100 <100 <100 <100 <100
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 10.8 <100 <100 <99.0 <99.0 <100 <99.0
05/02/11 <0.13 <0.13 <0.15 <0.30 0.39 J <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 0.51 <0.10 3.7 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-5 04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Contaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 Aliphaticsn-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 01/21/16 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-DichloroethaneMWD-4
2L Standard (mg/l)
GCL (mg/l)
MW-2
MW-3A
MW-1A
Page 1 of 9
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
Contaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 Aliphaticsn-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 01/21/16 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (mg/l)
GCL (mg/l)
04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/09/09 480 76 8.0 J 160 1,200 36 B <1.8 <1.7 <1.4 13 3.2 J 28 J <1.5 <1.6 43 6.3 J 13.9 <500 223 <105 <105 160 <105
05/12/10 3.41 0.770 <0.500 <1.00 37.8 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 1.23 <0.500 <0.500 <0.500 <0.500 45.9 <100 <100 <99.0 <99.0 <100 <99.0
05/02/11 0.26 J <0.13 <0.15 <0.30 11.3 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 724 80 37.9 418 1,040 42.5 <2.3 <2.0 <2.0 11.3 4.2 J 30.6 3.6 J <2.7 82.9 13.6 NR NR NR NR NR NR NR
08/19/13 0.19 J <0.10 <0.10 <0.22 21.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 0.45 J <0.10 <0.10 <0.10 <0.10 39.1 <35 <35 <110 <110 <35 <160
07/09/14 2.2 0.92 0.64 0.83 J 28.8 0.56 <0.10 <0.10 <0.10 <0.10 0.14 J 0.83 <0.10 <0.10 0.32 J <0.10 76.9 <35 <35 <100 <100 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 0.33 J <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
01/11/16 0.59 <0.13 <0.13 <0.31 90.1 0.14 J <0.13 <0.13 <0.13 2.3 <0.13 4.2 <0.13 <0.13 <0.13 <0.13 NR NR NR NR NR NR NR
04/28/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/12/10 13,100 31,400 5,480 25,000 5,960 1,850 <0.500 196 37.4 <0.500 144 194 1,770 <0.500 4,850 3,160 142 83,800 24,000 16,500 226 20,000 7,390
05/02/11 12,000 47,400 3,490 17,980 5,860 819 <29 126 J 48.4 J 258 172 177 631 <34 4,970 1,280 NR NR NR NR NR NR NR
08/28/12 10,800 25,600 2,980 14,500 4,470 638 <120 <100 <100 276 J <100 137 J 335 J <140 2,410 607 NR NR NR NR NR NR NR
08/19/13 7,140 17,600 1,920 11,600 2,540 384 <10 19.0 J 11.7 J 139 66.3 87.9 253 <10 1,890 446 124 13,100 16,800 3,930 <100 7,290 J 339
07/09/14 8,360 18,600 2,030 10,100 4,240 465 <5.0 23.8 J 14.2 J 204 84.7 146 300 <5.0 2,000 499 270 17,300 <1,800 3,500 <400 6,960 639 J
03/24/15 11,500 23,800 3,190 18,000 6,290 1,110 <74 104 J <69 270 182 J 273 645 <74 4,730 1,300 NR NR NR NR NR NR NR
01/11/16 13,800 31,700 6,140 31,800 4,400 2,550 <31 520 214 250 484 227 2,010 <31 5,470 3,740 NR NR NR NR NR NR NR
04/23/08 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
01/07/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/12/10 777 148 131 340 185 417 <0.500 135 75.0 <0.500 52.4 50.7 95.8 3.30 380 148 12.2 3,740 1,780 231,000 50,800 1,940 88,200
05/02/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP NR NR NR NR NR NR NR
08/28/12 377 58.3 69.8 177 94.5 269 <1.2 12.2 15.0 14.4 16.2 17.3 26.1 1.5 J 200 52.2 NR NR NR NR NR NR NR
08/19/13 329 11.5 42.9 82.5 106 141 <1.0 13.1 17.8 14.3 14.4 18.4 25.6 3.0 J 116 19.7 22.6 544 J 2,500 90,800 25,600 1,580 15,200
07/09/14 274 9.3 43.7 87.1 217 197 <1.0 40.8 45.3 22.5 25.4 32.4 38.3 3.0 J 189 54.2 12.1 1,140 J 4,310 74,300 29,500 4,730 36,800
03/24/15 101 7.2 9.5 40.2 21.4 115 <0.74 8.0 10.9 3.7 9.8 4.7 11.3 1.5 J 79.0 24.1 NR NR NR NR NR NR NR
01/11/16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/28/12 319 237 599 1,150 <1.3 237 <1.2 62.2 27.1 <1.6 75.1 6.4 339 <1.4 1,930 651 NR NR NR NR NR NR NR
08/19/13 153 98.9 432 1,270 20.7 229 <1.0 126 54.2 6.1 133 <1.0 419 <1.0 1,190 673 15.4 4,170 J 5,640 5,910 227 7,010 967 J
07/09/14 201 142 488 981 6.4 J 205 <2.5 183 68.2 <2.5 112 3.1 J 542 <2.5 1,830 968 48.9 6,360 <1,800 17,100 1,930 J 6,600 2,880
03/24/15 164 149 343 1,080 6.7 J 136 <3.7 54.9 24.5 <4.1 65.2 <4.0 291 <3.7 2,820 E 1,150 NR NR NR NR NR NR NR
01/11/16 349 160 405 1,160 26.6 J 352 <13 414 128 <13 133 <13 770 <13 <13 1,320 NR NR NR NR NR NR NR
MW-9
MW-8
MW-7
MW-6
Page 2 of 9
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
Contaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 Aliphaticsn-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 01/21/16 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (mg/l)
GCL (mg/l)
04/23/08 205 L 0.690 I <0.31 22.5 17.4 45.2 <0.14 0.530 I <0.47 2.44 2.50 4.51 I <0.30 3.88 1.12 <0.27 33.3 527 187 308 723 <100 345
01/07/09 160 <0.70 <0.50 31 <0.50 38 B <0.90 13 <0.70 <1.1 4.0 J 4.5 J <0.75 2.4 J 1.0 J <0.50 29.6 536 <100 <111 <111 <100 249
05/12/10 13.3 <0.500 <0.500 1.69 0.810 <5.00 <0.500 <0.500 <0.500 <0.500 0.540 <0.500 <0.500 <0.500 <0.500 <0.500 37.9 122 <100 <99.0 <99.0 <100 <99.0
05/03/11 7.7 <0.13 <0.15 2.7 0.82 1.1 <0.12 <0.10 <0.10 0.19 J 0.19 J 0.23 J <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 70.5 0.25 J <0.15 28.2 3.8 17.8 <0.13 0.46 J 0.32 J 0.94 2.8 1.5 <0.11 0.23 J 0.88 <0.10 NR NR NR NR NR NR NR
08/19/13 6.5 <0.10 <0.10 1.2 J 0.77 1.2 <0.10 <0.10 <0.10 0.26 J 0.45 J 0.36 J <0.10 <0.10 <0.10 <0.10 14.9 <35 <35 <110 <110 <35 <160
07/08/14 26.3 0.16 J <0.10 3.0 0.91 7.0 <0.10 0.20 J 0.17 J 0.27 J 1.6 0.46 J <0.10 <0.10 0.30 J <0.10 85.0 148 <35 <100 <100 <35 465
03/24/15 2.1 <0.17 <0.15 0.79 J 0.81 0.61 <0.15 <0.14 <0.14 <0.16 0.23 J 0.36 J <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/23/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 33.7 <100 <100 133 147 <100 122
01/07/09 27 2.7 J 3.5 J 2.9 J <0.50 18 B <0.90 <0.85 <0.70 <1.1 1.9 J <1.0 <0.75 <0.80 1.0 J 1.3 J 77.3 253 <100 <111 <111 <100 262
05/12/10 126 522 176 206 2.25 73.5 <0.500 3.94 1.48 <0.500 13.9 1.43 23.2 <0.500 54.4 10.8 40.1 3,590 314 <99.0 <99.0 389 <99.0
05/03/11 105 1,090 237 534 <3.3 43.0 <2.9 <2.5 <2.6 <4.1 6.3 J <2.7 19.7 <3.4 102 12.9 J NR NR NR NR NR NR NR
08/28/12 7.0 15.5 8.4 17.1 <0.13 4.3 <0.12 <0.10 <0.10 <0.16 0.41 J <0.11 0.81 <0.14 2.9 <0.10 NR NR NR NR NR NR NR
08/19/13 28.6 260 69.4 139 <1.0 20.4 <1.0 <1.0 <1.0 <1.0 3.2 J <1.0 6.9 <1.0 38.0 7.4 49.8 291 222 107 J <100 127 <150
07/08/14 42.8 284 74.7 167 <0.10 30.6 <0.10 1.0 0.52 <0.10 4.3 0.14 J 10.4 <0.10 38.6 4.5 111 902 <35 <100 <100 241 <150
03/24/15 <0.17 0.65 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/23/08 108 <1.4 <1.6 <5.8 415 9.30 <0.70 <2.0 <2.4 6.75 <1.2 4.30 I <1.5 <1.7 1.70 I <1.4 6.07 225 122 361 206 <100 440
01/07/09 92 <0.70 <0.50 2.5 J 820 8.2 B <0.90 <0.85 <0.70 16 1.2 J 13 J <0.75 <0.80 <0.70 <0.50 23.5 10,100 <100 <111 <111 <100 <111
05/12/10 17.1 <0.500 <0.500 <1.00 357 <5.00 <0.500 <0.500 <0.500 9.90 <0.500 8.94 <0.500 <0.500 <0.500 <0.500 23.9 316 <100 <100 <100 <100 <100
05/03/11 7.6 <1.3 <1.5 <3.0 461 <1.0 <1.2 <1.0 <1.0 7.5 <1.0 10.1 <1.1 <1.4 <1.0 <1.0 NR NR NR NR NR NR NR
08/28/12 8.9 <0.13 <0.15 <0.30 114 0.87 <0.12 <0.10 <0.10 3.1 0.13 J 2.5 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 37.5 <1.0 <1.0 <2.2 326 3.4 J <1.0 <1.0 <1.0 8.2 <1.0 7.9 <1.0 <1.0 2.2 J <1.0 6.7 <35 <35 <100 <100 <35 <150
07/08/14 27.9 0.12 J <0.10 1.4 J 492 2.6 <0.10 <0.10 0.39 J 10.8 0.61 12.9 <0.10 <0.10 <0.10 <0.10 34.6 <70 <70 <100 <100 <70 162 J
03/24/15 14.7 0.59 <0.15 1.0 J 118 1.6 <0.15 <0.14 0.26 J 7.8 0.50 7.1 <0.16 0.19 J <0.14 <0.14 NR NR NR NR NR NR NR
04/23/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/09/09 70 140 53 140 4.5 J 34 B <0.90 <0.85 <0.70 <1.1 5.1 5.6 J 6.6 3.1 J 47 14 4.8 272 157 <105 <105 119 <105
05/12/10 234 200 217 323 2.07 94.5 <0.500 11.0 2.70 <0.500 17.1 20.2 34.9 1.31 153 64.1 6.40 1,590 513 <99.0 <99.0 609 <99.0
05/02/11 158 168 138 198.1 0.94 J 57.3 <0.59 1.5 J 0.92 J 4.1 7.9 9.3 20.8 0.76 J 98.4 31.9 NR NR NR NR NR NR NR
08/28/12 97.0 76.7 96.8 113 0.80 46.9 <0.12 0.94 1.0 3.4 6.0 9.0 7.6 1.2 20.6 6.5 NR NR NR NR NR NR NR
08/19/13 36.0 39.6 30.8 64.0 0.26 J 24.4 <0.10 0.73 0.73 1.3 3.8 3.0 3.6 1.3 11.7 2.0 54.5 106 202 <100 <100 127 <150
07/09/14 45.7 12.3 27.0 54.1 0.44 J 22.7 <0.10 0.65 0.67 1.5 3.6 3.9 2.9 1.4 13.2 3.0 28.5 133 <35 <95 <95 61.9 J 145 J
MW-13
MW-10
MW-11
MW-12
Page 3 of 9
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
Contaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 Aliphaticsn-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 01/21/16 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (mg/l)
GCL (mg/l)
04/24/08 0.510 I <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 0.330 I <0.30 0.790 I <0.26 <0.27 238 <100 <100 <75 130 <100 <50
01/09/09 1.0 J 1.1 J 0.54 J <1.0 <0.50 3.2 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 1.5 J <0.70 <0.50 80.4 <100 <100 <105 <105 <100 <105
05/12/10 23.5 0.710 0.620 6.97 <0.500 19.6 <0.500 <0.500 0.980 <0.500 2.44 3.36 0.600 1.66 2.69 <0.500 77.6 <100 <100 <99.0 <99.0 <100 <99.0
05/02/11 28.8 3.0 16.8 30.0 <0.13 15.9 <0.12 0.25 J 1.2 1.1 2.7 3.4 2.8 1.3 14.7 4.3 NR NR NR NR NR NR NR
08/28/12 57.7 1.9 60.6 33.5 0.21 J 26.7 <0.12 0.60 2.6 1.5 4.4 4.4 8.0 0.63 37.7 6.7 NR NR NR NR NR NR NR
08/19/13 10.9 0.40 J 12.7 9.3 <0.10 6.5 <0.10 0.12 J 0.74 0.46 J 1.0 1.5 2.0 0.77 7.5 1.3 94.8 36.8 J 72.0 J <100 193 J 58.6 J <150
07/09/14 12.5 0.27 J 4.3 8.3 0.13 J 7.7 <0.10 <0.10 1.5 0.63 1.2 2.2 0.70 0.77 4.1 0.59 46.4 51.2 J <35 <95 <95 37.4 J <140
03/24/15 31.2 1.3 2.2 13.4 <0.16 4.4 <0.15 <0.14 1.5 1.1 1.6 3.8 0.57 0.30 J 4.9 0.90 NR NR NR NR NR NR NR
01/11/16 79.8 1.1 27.9 32.5 0.29 J 29.6 <0.13 0.61 1.9 2.0 7.4 6.8 5.9 0.33 J 35.0 3.9 NR NR NR NR NR NR NR
04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 60.1 <100 <100 370 6,660 <100 642
01/07/09 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 52.8 <100 <100 <100 <100 <100 <100
05/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 0.23 J <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 6.0 <35 <35 <110 <110 <35 <160
07/08/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-16 04/23/08 4.17 <0.28 <0.31 <1.2 0.580 I 0.770 I <0.14 <0.39 <0.47 <0.12 0.370 I 0.290 I <0.30 <0.33 0.280 I <0.27 15.3 <100 <100 205 466 <100 279
01/07/09 15 <0.70 <0.50 <1.0 1.5 J 2.8 JB <0.90 <0.85 <0.70 <1.1 1.6 J 1.1 J <0.75 <0.80 <0.70 <0.50 15.7 117 <100 <111 <111 <100 <111
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 34.0 <100 <100 <105 <105 <100 <105
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 0.57 <0.13 <0.15 <0.30 0.13 J 0.12 J <0.12 <0.10 <0.10 <0.16 <0.10 0.17 J <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 10.8 0.16 J <0.10 0.40 J 0.29 J 1.7 <0.10 <0.10 0.23 J 0.17 J 1.6 0.31 J <0.10 <0.10 <0.10 <0.10 12.4 63.6 J <35 <100 <100 <35 <160
07/08/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/24/08 176 48.6 39.4 84.8 5.42 1.65 <0.14 0.610 I 0.540 I 2.57 2.55 4.07 I 6.10 <0.33 42.9 13.4 21.0 851 <100 93.1 94.2 204 96.0
01/09/09 52 11 12 13 J <0.50 1.4 JB <0.90 <0.85 <0.70 <1.1 1.4 J <1.0 2.4 J <0.80 10 2.0 J 4.8 465 <100 <100 <100 <100 <100
05/12/10 115 4.08 11.5 9.63 5.62 <5.00 <0.500 0.840 0.580 <0.500 2.31 4.03 2.97 <0.500 15.0 1.68 37.7 867 <100 <100 <100 <100 <100
05/02/11 138 7.3 17.1 10.0 J 2.7 1.2 J <0.59 <0.50 <0.51 1.2 J 1.0 J 2.2 J 2.9 <0.69 7.5 1.9 J NR NR NR NR NR NR NR
08/28/12 107 2.4 15.6 6.4 2.2 0.49 J <0.12 0.24 J 0.31 J 0.90 1.1 2.0 2.8 0.35 J 6.9 2.3 NR NR NR NR NR NR NR
08/19/13 33.1 0.54 7.3 2.5 0.94 0.20 J <0.10 0.18 J 0.22 J 0.42 J 0.72 0.96 2.0 0.20 J 2.8 1.3 18.1 90.5 J 56.4 J <100 <100 <35 <160
07/09/14 39.7 0.40 J 3.5 1.2 J 1.3 0.35 J <0.10 <0.10 0.20 J 0.41 J 0.45 J 1.4 0.82 0.27 J 2.7 0.61 11.3 86.4 J <35 <96 <96 <35 <140
03/24/15 183 4.0 4.7 <2.2 4.5 2.1 J <0.74 <0.72 <0.69 2.1 J 0.94 J 3.5 1.2 J <0.74 5.2 <0.68 NR NR NR NR NR NR NR
01/11/16 5.6 <0.13 0.18 J <0.31 0.58 <0.13 <0.13 <0.13 <0.13 0.24 J 0.23 J 0.74 <0.13 0.31 J 0.78 <0.13 NR NR NR NR NR NR NR
MW-15
MW-16A
MW-14
MW-17
Page 4 of 9
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
Contaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 Aliphaticsn-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 01/21/16 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (mg/l)
GCL (mg/l)
04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 20.4 <100 <100 167 212 <100 216
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 13.8 <100 <100 <105 <105 <100 <105
05/12/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 15.6 <35 <35 <110 <110 <35 <160
07/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 29.9 <35 <35 <99 <99 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/24/08 286 0.320 I <0.31 4.89 197 12.9 <0.14 <0.39 <0.47 10.5 1.97 14.3 <0.30 <0.33 <0.26 <0.27 7.21 539 117 152 196 <100 179
01/09/09 130 <0.70 <0.50 3.0 J 78 6.7 B <0.90 <0.85 <0.70 4.5 J 1.3 J 11 J <0.75 <0.80 <0.70 <0.50 13.1 461 <100 <105 <105 <100 <105
05/12/10 119 <0.500 <0.500 3.94 224 7.61 <0.500 <0.500 0.520 9.43 1.72 11.6 <0.500 <0.500 <0.500 <0.500 12.8 445 <100 <103 <103 <100 <103
05/03/11 42.2 <0.13 <0.15 0.34 J 100 2.7 <0.12 <0.10 0.14 J 3.0 0.15 J 6.6 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 28.0 <0.13 <0.15 0.62 J 102 2.3 <0.12 <0.10 0.26 J 7.8 0.13 J 7.8 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 8.6 <0.10 <0.10 0.26 J 75.5 0.44 J <0.10 <0.10 0.37 J 2.1 0.23 J 8.5 <0.10 <0.10 <0.10 <0.10 14.0 36.3 J <35 <100 <100 <35 <150
07/08/14 9.3 <0.10 <0.10 0.41 J 120 0.37 J <0.10 <0.10 0.59 1.7 0.63 10.1 <0.10 <0.10 <0.10 <0.10 25.9 87.7 J <35 <99 <99 <35 249
03/24/15 4.3 <0.83 <0.76 <2.2 211 <0.61 <0.74 <0.72 0.73 J 2.5 1.4 J 12.0 <0.78 <0.74 <0.68 <0.68 NR NR NR NR NR NR NR
04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 34.1 <100 <100 <75 <75 <100 <50
01/09/09 1.4 J <0.70 <0.50 <1.0 <0.50 0.67 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 24.0 <100 <100 <105 <105 <100 <105
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 44.2 <100 <100 <102 <102 <100 <102
05/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 0.45 J <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 28.2 <35 <35 <100 <100 <35 <150
07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 60.3 <35 <35 <96 <96 <35 <140
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 0.410 I <0.26 <0.27 32.9 <100 <100 <75 <75 <100 <50
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 53.0 <100 <100 <105 <105 <100 <105
05/02/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 5.6 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 39.1 <35 <35 <100 <100 <35 <150
07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 75.2 <35 <35 <96 <96 <35 141 J
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
MW-18
MW-21
MW-19
MW-20
Page 5 of 9
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
Contaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 Aliphaticsn-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 01/21/16 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (mg/l)
GCL (mg/l)
04/24/08 19.2 <0.28 <0.31 <1.2 9.01 1.54 <0.14 <0.39 <0.47 1.35 <0.24 1.96 I <0.30 <0.33 <0.26 <0.27 24.6 <100 <100 <75 90.9 <100 <50
01/09/09 <0.60 <0.70 <0.50 <1.0 3.2 J <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 25.6 <100 <100 <105 <105 <100 <105
05/12/10 3.90 <0.500 <0.500 <1.00 6.17 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 1.14 <0.500 <0.500 <0.500 <0.500 21.5 <100 <100 <108 <108 <100 <108
05/03/11 0.33 J <0.13 <0.15 <0.30 5.3 <0.10 <0.12 <0.10 <0.10 0.38 J <0.10 0.58 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 2.8 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 1.5 <0.15 <0.10 <0.10 <0.10 0.25 J <0.10 0.64 <0.10 <0.10 <0.10 <0.10 18.2 <35 <35 <110 <110 <35 <160
07/08/14 0.13 J <0.10 <0.10 <0.20 1.5 <0.10 <0.10 <0.10 <0.10 0.23 J <0.10 0.76 <0.10 <0.10 <0.10 <0.10 29.0 <35 <35 <200 827 <35 716
03/24/15 1.1 <0.17 <0.15 <0.43 2.9 <0.12 <0.15 <0.14 <0.14 0.23 J <0.12 0.88 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/24/08 <0.31 <0.28 <0.31 <1.2 0.380 I <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 32.7 <100 <100 <75 <75 <100 <50
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 40.0 <100 <100 <105 <105 <100 <105
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 60.9 <100 <100 <108 <108 <100 <108
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/09 0.68 J <0.70 <0.50 <1.0 <0.50 0.68 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 17.1 <100 <100 <111 <111 <100 <111
05/12/10 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 18.6 <35 <35 <110 <110 <35 <160
07/08/14 <0.10 0.11 J <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 6.6 <35 <35 <100 <100 <35 <150
04/23/08 <0.31 <0.28 <0.31 <1.2 <0.12 0.800 I <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 9.66 <100 <100 96.4 88.3 <100 133
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 14.6 <100 <100 <105 <105 <100 <105
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 17.0 <35 <35 <110 <110 <35 <170
07/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 32.5 <35 <35 <99 <99 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/23/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 42.4 <100 <100 <75 <75 <100 87.2
01/07/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 38.3 <100 <100 <111 <111 <100 <111
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 0.42 J <0.10 <0.11 <0.11 0.93 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 0.48 J <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.40 J <0.10 <0.10 32.8 <35 <35 <110 <110 <35 <160
07/08/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 0.31 J <0.10 0.74 <0.10 0.29 J <0.10 <0.10 41.0 <35 <35 <100 <100 <35 <150
MW-22
MW-26
MW-24
MW-25
MW-23
Page 6 of 9
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
Contaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 Aliphaticsn-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 01/21/16 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (mg/l)
GCL (mg/l)
04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 53.5 <100 <100 <111 <111 <100 <111
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/24/08 <0.31 <0.28 <0.31 <1.2 0.680 I <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 59.1 <100 <100 <75 94.6 <100 <50
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 40.4 <100 <100 <105 <105 <100 <105
05/03/11 <0.13 <0.13 <0.15 <0.30 0.20 J <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 0.22 J <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/09/09 200 <0.70 <0.50 4.0 J <0.50 28 B <0.90 13 B 0.75 J <1.1 3.7 J <1.0 <0.75 2.1 J <0.70 <0.50 3.5 627 <100 <105 <105 <100 <105
05/12/10 149 <0.500 <0.500 2.52 3.79 20.0 <0.500 0.520 <0.500 <0.500 3.59 1.72 <0.500 1.11 <0.500 <0.500 15.7 519 <100 <108 <108 <100 <108
05/03/11 35.3 <0.13 <0.15 0.35 J 1.4 2.7 <0.12 <0.10 <0.10 0.41 J 0.61 0.47 J <0.11 0.24 J <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 6.2 <0.13 <0.15 <0.30 1.7 0.39 J <0.12 <0.10 <0.10 0.41 J 0.43 J 0.37 J <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 1.0 <0.10 <0.10 <0.22 1.6 <0.15 <0.10 <0.10 <0.10 0.47 J <0.10 0.49 J <0.10 <0.10 <0.10 <0.10 7.7 <35 <35 <110 <110 <35 <160
07/08/14 <0.10 <0.10 <0.10 <0.20 1.7 <0.10 <0.10 <0.10 <0.10 0.38 J <0.10 0.41 J <0.10 <0.10 <0.10 <0.10 20.9 <35 <35 <100 <100 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 0.34 J <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
MW-30 04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 11.0 <100 <100 <111 <111 <100 <111
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 69.9 <100 <100 <108 <108 <100 <108
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
04/24/08 <0.31 <0.28 <0.31 <1.2 <0.12 <0.41 <0.14 <0.39 <0.47 <0.12 <0.24 <0.15 <0.30 <0.33 <0.26 <0.27 41.6 <100 <100 <75 94.6 <100 88.1
01/09/09 1.7 J <0.70 <0.50 <1.0 <0.50 2.7 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <70 <0.50 29.1 <100 <100 <105 <105 <100 <105
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 46.8 <100 <100 <108 <108 <100 <108
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 0.29 J <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 0.28 J <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-27
MW-32
MW-28
MW-29
MW-31
Page 7 of 9
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
Contaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 Aliphaticsn-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 01/21/16 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (mg/l)
GCL (mg/l)
04/24/08 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/09/09 <0.60 <0.70 <0.50 <1.0 <0.50 0.84 JB <0.90 <0.85 <0.70 <1.1 <0.55 <1.0 <0.75 <0.80 <0.70 <0.50 18.9 <100 <100 <105 <105 <100 <105
05/12/10 1.41 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 45.0 <100 <100 <111 <111 <100 <111
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 28.7 <35 <35 <110 <110 <35 <160
07/08/14 <0.10 0.34 J <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 76.4 <35 <35 <100 <100 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
05/12/10 59.1 <0.500 <0.500 <1.00 1.37 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 1.17 <0.500 6.52 <0.500 <0.500 146 120 <100 <118 <118 <100 <118
05/03/11 41.5 <0.13 <0.15 0.12 J 1.0 3.3 <0.12 <0.10 <0.10 0.38 J 0.14 J 0.62 <0.11 4.9 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 8.6 <0.13 <0.15 <0.30 0.31 J 0.69 <0.12 <.010 <0.10 <0.16 <0.10 0.18 J <0.11 1.1 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 10.6 <0.10 <0.10 <0.22 0.63 1.2 <0.10 <0.10 <0.10 0.26 J <0.10 0.47 J <0.10 1.6 <0.10 <0.10 12.3 <35 <35 <110 <110 <35 <160
07/08/14 6.2 0.11 J <0.10 <0.20 0.58 0.80 <0.10 <0.10 <0.10 0.22 J <0.10 0.45 J <0.10 1.1 <0.10 <0.10 46.8 <35 <35 <99 <99 <35 <150
03/24/15 0.49 J <0.17 <0.15 <0.43 0.39 J <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 0.27 J <0.16 0.53 <0.14 <0.14 NR NR NR NR NR NR NR
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 381 <100 <100 <121 <121 <100 <121
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/12/10 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 314 <100 <100 <118 <118 <100 <118
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
05/03/11 3.4 <0.13 <0.15 <0.30 0.29 J 0.19 J <0.12 <0.10 <0.10 <0.16 <0.10 0.19 J <0.11 1.1 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 0.47 J <0.13 <0.15 <0.30 0.21 J <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 0.16 J <0.11 0.69 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 0.17 J <0.14 <0.14 NR NR NR NR NR NR NR
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
MW-33
MW-34
MW-37
MW-38
MW-35
MW-36
MW-39
Page 8 of 9
EPA
Method
6010B
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.6 70 70 0.4 70 70 70 0.7 400 400 15 400 700 700 10,000 200 200
5,000 260,000 84,500 85,500 20,000 6,000 NE 6,900 8,500 400 25,000 70,000 30,000 700 28,500 25,000 15,000 NE NE NE NE NE NE
Contaminant of
Concern C9-C10 AromaticsLeadNaphthaleneIPETolueneEthylbenzeneXylenesTetrachloroetheneC9-C18 AliphaticsC9-C12 Aliphatics1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneC5-C8 AliphaticsC11-C22 AromaticsC19-C36 Aliphaticsn-PropylbenzeneMTBETABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #3 (INCIDENT NO. 10673)
Analytical Method

Date: 01/21/16 Facility ID #: 0-017539
EPA Method 6200B MADEP Methods VPH and EPH
BenzeneIsopropylbenzenen-ButylbenzeneBromodichloromethanesec-Butylbenzene1,2-Dichloroethane2L Standard (mg/l)
GCL (mg/l)
05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.12 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/28/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 3.3 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
08/19/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 0.81 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 81.7 <35 <35 <110 <110 <35 <160
07/09/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 0.21 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 129 <35 <35 <97 <97 <35 <150
03/24/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.15 <0.14 <0.14 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR NR
Spigot -1 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 10.4 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-2 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 3.4 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-3 05/03/11 <0.13 <0.13 <0.15 <0.30 0.19 J <0.10 8.3 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-4 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 6.5 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-5 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 6.7 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-6 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 0.18 J 7.7 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-7 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 7.5 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Spigot-8 05/03/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 6.7 <0.10 <0.10 <0.16 <0.10 <0.11 <0.11 <0.14 <0.10 <0.10 NR NR NR NR NR NR NR
Notes:
• Results reported in mg/l (micrograms per liter).
• 2L Standard: as specified in T15A NCAC 2L.0202
• GCL : Gross contamination level.
• < : Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L Standards; concentrations in italics exceeded the GCLs.
• FP: Free Product.
• NE: Not established.
• NS: Not sampled; well not located.
• NR: Analyses not requested.
• J or I: Estimated value.
• B: Present in laboratory blank.
• Concentrations of dibromochloromethane (0.68 µg/l in MW-3A), 1,2-dibromoethane (112 J µg/l in MW-7), p-isopropyltoluene (113 J µg/l in MW-7 and 76.7 µg/l MW-9) and styrene (146 µg/l in MW-7) that weceeded the MACs were reported in the
ground water samples collected on January 11, 2016.
• Refer to laboratory report for other compounds detected which did not exceed the 2L Standards.
MW-40
Page 9 of 9

APPENDICES

APPENDIX A
MMPE Data and Calculations
Site Name :Red Apple Market #3 Incident Number :10673
Site Location:1332 East Memorial Drive, Ahoskie, NC
Client Name:North East Oil Co., Inc
Blower Specifications For Vacuum Truck (e.g: 2500 cfm @ 24 in. of Hg) :280 cfm @ 24 in. of Hg Stack Diameter (inches):2
Start Time :8:55 Start Date:12/07/15 End Time :8:55 End Date:12/11/15
Note: Take all the readings listed below about 3 to 4 times every day at approximately the same time.
MMPE Contractor:Greenwood Applied Services Consultant:Geological Resources, Inc.
EXTRACTION WELL INFORMATION:
MW-2 MW-7
2 2
9.35 8.84
9.35 8.84
Date Time System Vacuum Exhaust Velocity Temperature Rel. Humidity OVA
(in. of Hg)(ft/min)(°F)(%)(ppm)
9:15 17.00 2,025 61.5 72.4 505.7 0.0
12:00 17.00 3,051 70.0 55.9 454.9 12.0
16:00 14.00 2,236 64.4 67.5 263.8 21.0
6:00 12.00 1,289 60.5 51.4 338.8 47.0
18:30 12.00 2,549 60.4 48.6 244.3 65.0
7:00 11.00 2,428 60.0 56.3 160.1 41.0
12:00 11.00 2,302 60.2 40.2 132.9 46.0
16:00 11.00 2,151 59.9 40.9 128.4 13.0
7:00 11.00 2,287 51.2 55.5 117.9 22.0
12:00 11.00 2,451 50.1 51.8 118.2 31.0
16:00 11.00 2,358 51.1 53.4 120.1 34.0
12/11/15 8:45 11.00 2,002 61.4 47.0 114.1 42.0
FLUID RECOVERY SUMMARY:
Day 1 (24 hours)Day 2 (48 hrs)Day 3 (72 hrs)Day 4 (96 hrs)
Total Fluid Recovered (gallons)7,295 4,878 3,591 2,893
Total Product Recovered (gallons)---------------
Day
MOBILE MULTI-PHASE EXTRACTION EVENT DATA SHEET - FIELD LOG 1
Well Number
Diameter (inch)
Initial Stinger Depth (ft.)
12/08/15
12/07/15
12/09/15
12/10/15
TOTAL (event)
18,657
Final Stinger Depth (ft.)
Tank Stick
(inch)
Vol. Rec.
(gal)
Page 1 of 2
Site Name :Red Apple Market #3 Incident Number :10673
Site Location:1332 East Memorial Drive, Ahoskie, NC
Client Name:North East Oil Co., Inc
Start Time :8:55 12/11/15
Note: Take all the readings listed below about 3 to 4 times every day at approximately the same time.
MMPE Contractor:Greenwood Applied Services Consultant:Geological Resources, Inc.
MW-2 MW-7
Initial DTW (ft.)9.30 8.79
Initial DTP (ft.)------
Final DTW (ft.)9.55 9.12
Final DTP (ft.)------
DTW = Depth to Water; DTP = Depth to Product
OBSERVATION WELLS (VACUUM /WATER LEVELS)
Well 1 Well 2 Well 3 Well 4 Well 5 Well 6
Vacuum Water Lvl Vacuum Water Lvl Vacuum Water Lvl
(in. H2O)(ft.)(in. H2O)(ft.)(in. H2O)(ft.)
9:15 14.00 15.00
12:00 17.00 18.00 0.50 0.80
16:00 15.00 14.00 0.50 0.80
6:00 11.00 11.00 0.30 0.80
18:30 12.00 11.00 0.50 9.51 0.60 8.68
7:00 8.00 8.00 0.50 0.60
12:00 11.00 9.00 0.10 0.30
16:00 11.00 7.00 0.20 9.79 0.20 8.83
7:00 10.00 8.00 0.20 0.20
12:00 8.00 7.00 0.20 0.20
16:00 8.00 7.00 0.20 9.82 0.20 8.85
12/11/15 8:45 9.00 8.00
8.80
------
------
Start Date:8:55 12/07/15
9.47 8.66
MW-8MW-3A
12/10/15
EXTRACTION POINTS - VACUUM (inches of Hg)
MOBILE MULTI-PHASE EXTRACTION EVENT DATA SHEET - FIELD LOG 2
MW-3A
End Date:End Time:
Water/Product Levels
12/08/15
DATE TIME
12/07/15
12/09/15
MW-2 MW-7
OBSERVATION WELLS (WATER LEVELS)
EXTRACTION POINTS - VACUUM (inches of Hg)
MW-8
9.64
Page 2 of 2
MOBILE MULTI-PHASE EXTRACTION EVENT
SITE NAME:Red Apple Market #3
INCIDENT NUMBER:10673
AVERAGE DEPTH TO GROUNDWATER:9.06 ft.
DESCRIBE SOIL IN THE SATURATED ZONE:sand
INDICATE AVERAGE HYDRAULIC CONDUCTIVITY (if known): 0.05 feet/day.
IDENTIFY THE WELL AND THE I.D. OF EACH WELL USED FOR MMPE:MW-2 and MW-7
PROVIDE BLOWER SPECIFICATIONS OF THE VACUUM TRUCK (cfm @ in Hg):280 CFM @ 24" Hg
TOTAL NUMBER OF DATA POINTS :12 (No. of readings taken during MMPE event)
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd)
Vacuum Velocity Pipe ID Temp Rel Humid Water Qstd
(inches of Hg)(ft/min)(in)(°F)(%)Vapor (%)(flow)
12/07/15 9:15 17.00 2,025 2 61.5 72.40 0.0084 44.35
12/07/15 12:00 17.00 3,051 2 70.0 55.90 0.0087 65.73
12/07/15 16:00 14.00 2,236 2 64.4 67.50 0.0087 48.69
12/08/15 6:00 12.00 1,289 2 60.5 51.40 0.0057 28.36
12/08/15 18:30 12.00 2,549 2 60.4 48.60 0.0054 56.12
12/09/15 7:00 11.00 2,428 2 60.0 56.30 0.0062 53.45
12/09/15 12:00 11.00 2,302 2 60.2 40.20 0.0044 50.75
12/09/15 16:00 11.00 2,151 2 59.9 40.90 0.0045 47.45
12/10/15 7:00 11.00 2,287 2 51.2 55.50 0.0044 51.31
12/10/15 12:00 11.00 2,451 2 50.1 51.80 0.0040 55.13
12/10/15 16:00 11.00 2,358 2 51.1 53.40 0.0042 52.92
12/11/15 8:45 11.00 2,002 2 61.4 47.00 0.0054 43.99
Averages --12.42 2260.75 2.00 59.23 53.41 0.0058 49.85
NOTES
Qstd = Flow at DSCFM
Vacuum = The level of vacuum being applied should be recorded from the vacuum truck tank (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the vacuum truck)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)
Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Water Vapor in % = Pounds of water per pound of dry air, derived from the Psychrometric chart
(temp Vs relative humidity)
EQUATION
Qstd = (1-Water Vapor) * velocity * (PI * (diameter/24)^2) * (528°R/(Temp + 460))
Date Time
EMISSION CALCULATIONS
20 44.35 505.7 4 2,022.80 10,756.89 0.000671553 1.79 0.60
185 65.73 454.9 4 1,819.60 9,676.31 0.000604092 2.38 7.35
425 48.69 263.8 4 1,055.20 5,611.37 0.000350318 1.02 7.25
1265 28.36 338.8 4 1,355.20 7,206.71 0.000449915 0.77 16.14
2015 56.12 244.3 4 977.20 5,196.58 0.000324422 1.09 36.68
2765 53.45 160.1 4 640.40 3,405.53 0.000212607 0.68 31.42
3065 50.75 132.9 4 531.60 2,826.95 0.000176487 0.54 27.45
3305 47.45 128.4 4 513.60 2,731.23 0.000170511 0.49 26.74
4205 51.31 117.9 4 471.60 2,507.89 0.000156567 0.48 33.78
4505 55.13 118.2 4 472.80 2,514.27 0.000156966 0.52 38.98
4745 52.92 120.1 4 480.40 2,554.68 0.000159489 0.51 40.05
5750 43.99 114.1 4 456.40 2,427.05 0.000151521 0.40 38.33
Averages 41.78 224.93 4.00 899.73 4784.62 0.000298704 0.89 25.40
Total emissions in pounds 304.77
NOTES
PPM measured = Actual measurements (ppm) taken with a OVA or TVA at the blower discharge piping
K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, or Hexane K = 6)
PPMg = PPMv, Volumetric concentration as gasoline emission, dry basis at STP
Cg:m = mg/dsm3, mass concentration of gasoline emission
Mg = 128 mg/mg-mole, molecular weight of gasoline (this value may vary depending on contaminant)
K3 = 24.07 dsm^3/1E6 mg-mole, mass to volume conversion factor at STP
Cg = lb/dcsf, mass concentration of gasoline emission, dry basis at STP
PMRg = lb/hr, pollutant mass removal rate of gasoline emission
PMR = pollutant mass removal of gasoline emission over time
NM = Not measured due to OVA malfunction.
EQUATIONS
PPMg = PPM measured * K
Cg:m = PPMg * (Mg / K3)
Cg = Cg:m * 62.43E-09 lb-m^3/mg-ft^3
PMRg = Cg * Qstd * 60 min/hr
PMR = PMRg * ((T2 - T1) / 60)
PMRg
(lb/hr)
PMR
(lb)
PPM
measured
(ppm)
K
(#C-gas)PPMg
Cg:m
(mg/dsm^3)
Elapsed
Time
(min)
Flow
(DSCFM)
Cg
(lb/dscf)

APPENDIX B
Disposal Manifests

APPENDIX C
Laboratory Report – Ground Water Samples

01/20/16
Technical Report for
GRI (Geological Resources Inc.)
Ram 3; 1332 E Memorial Dr, Ahoskie, NC
10673/2677
Accutest Job Number: FA30628
Sampling Date: 01/11/16
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Nicky Long
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
01/20/16
e-Hardcopy 2.0
Automated Report
41
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
Effective January 1, 2016, SGS has acquired all of the assets of Accutest Laboratories and will continue to
operate as SGS-Accutest. SGS-Accutest is part of SGS, the world's leading inspection, verification, testing and
certification company.
1 of 41
FA30628
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FA30628-1: MW-1A .....................................................................................................8
3.2: FA30628-2: MW-2 ........................................................................................................10
3.3: FA30628-3: MW-3A .....................................................................................................12
3.4: FA30628-4: MW-6 ........................................................................................................14
3.5: FA30628-5: MW-7 ........................................................................................................16
3.6: FA30628-6: MW-9 ........................................................................................................18
3.7: FA30628-7: MW-14 ......................................................................................................20
3.8: FA30628-8: MW-17 ......................................................................................................23
Section 4: Misc. Forms ............................................................................................................25
4.1: Chain of Custody ...........................................................................................................26
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................29
5.1: Method Blank Summary ................................................................................................30
5.2: Blank Spike Summary ...................................................................................................34
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................38 123452 of 41
FA30628
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA30628
Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Project No: 10673/2677
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA30628-1 01/11/16 14:41 JH 01/12/16 AQ Ground Water MW-1A
FA30628-2 01/11/16 14:52 JH 01/12/16 AQ Ground Water MW-2
FA30628-3 01/11/16 12:03 JH 01/12/16 AQ Ground Water MW-3A
FA30628-4 01/11/16 15:16 JH 01/12/16 AQ Ground Water MW-6
FA30628-5 01/11/16 15:22 JH 01/12/16 AQ Ground Water MW-7
FA30628-6 01/11/16 15:39 JH 01/12/16 AQ Ground Water MW-9
FA30628-7 01/11/16 14:14 JH 01/12/16 AQ Ground Water MW-14
FA30628-8 01/11/16 14:27 JH 01/12/16 AQ Ground Water MW-17
3 of 41
FA30628 1
Summary of Hits Page 1 of 3
Job Number:FA30628
Account:GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Collected:01/11/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA30628-1 MW-1A
No hits reported in this sample.
FA30628-2 MW-2
Benzene 2480 50 13 ug/l SM 6200B
Chloroform 13.8 J 50 13 ug/l SM 6200B
1,2-Dichloroethane 16.4 J 50 13 ug/l SM 6200B
Di-Isopropyl Ether 39.9 J 50 13 ug/l SM 6200B
Ethylbenzene 261 50 13 ug/l SM 6200B
Isopropylbenzene 13.9 J 50 13 ug/l SM 6200B
Methylene Chloride 290 200 100 ug/l SM 6200B
Methyl Tert Butyl Ether 887 50 13 ug/l SM 6200B
Naphthalene 117 50 13 ug/l SM 6200B
n-Propylbenzene 32.9 J 50 13 ug/l SM 6200B
Toluene 2220 50 13 ug/l SM 6200B
1,2,4-Trimethylbenzene 288 50 13 ug/l SM 6200B
1,3,5-Trimethylbenzene 86.7 50 13 ug/l SM 6200B
m,p-Xylene 1060 100 18 ug/l SM 6200B
o-Xylene 469 50 13 ug/l SM 6200B
Xylene (total)1530 150 31 ug/l SM 6200B
FA30628-3 MW-3A
Benzene 4.1 0.50 0.13 ug/l SM 6200B
Bromodichloromethane 1.3 0.50 0.13 ug/l SM 6200B
Chloroform 2.0 0.50 0.13 ug/l SM 6200B
Dibromochloromethane 0.68 0.50 0.13 ug/l SM 6200B
1,2-Dichloroethane 0.29 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.87 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 1.4 0.50 0.13 ug/l SM 6200B
Naphthalene 0.18 J 0.50 0.13 ug/l SM 6200B
FA30628-4 MW-6
Benzene 0.59 0.50 0.13 ug/l SM 6200B
Chloroform 0.18 J 0.50 0.13 ug/l SM 6200B
1,2-Dichloroethane 2.3 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 4.2 0.50 0.13 ug/l SM 6200B
Methylene Chloride 5.3 5.0 2.5 ug/l SM 6200B
Methyl Tert Butyl Ether 90.1 1.3 0.31 ug/l SM 6200B
Naphthalene 0.14 J 0.50 0.13 ug/l SM 6200B
4 of 41
FA30628 2
Summary of Hits Page 2 of 3
Job Number:FA30628
Account:GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Collected:01/11/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA30628-5 MW-7
Benzene 13800 500 130 ug/l SM 6200B
n-Butylbenzene 520 130 31 ug/l SM 6200B
sec-Butylbenzene 214 130 31 ug/l SM 6200B
1,2-Dibromoethane 112 J 130 31 ug/l SM 6200B
1,2-Dichloroethane 250 130 31 ug/l SM 6200B
Di-Isopropyl Ether 227 130 31 ug/l SM 6200B
Ethylbenzene 6140 130 31 ug/l SM 6200B
Isopropylbenzene 484 130 31 ug/l SM 6200B
p-Isopropyltoluene 113 J 130 31 ug/l SM 6200B
Methyl Tert Butyl Ether 4400 130 31 ug/l SM 6200B
Naphthalene 2550 130 31 ug/l SM 6200B
n-Propylbenzene 2010 130 31 ug/l SM 6200B
Styrene 146 130 31 ug/l SM 6200B
Toluene 31700 500 130 ug/l SM 6200B
1,2,4-Trimethylbenzene 5470 500 130 ug/l SM 6200B
1,3,5-Trimethylbenzene 3740 130 31 ug/l SM 6200B
m,p-Xylene 22200 250 46 ug/l SM 6200B
o-Xylene 9600 130 31 ug/l SM 6200B
Xylene (total)31800 380 77 ug/l SM 6200B
FA30628-6 MW-9
Benzene 349 50 13 ug/l SM 6200B
n-Butylbenzene 414 50 13 ug/l SM 6200B
sec-Butylbenzene 128 50 13 ug/l SM 6200B
Ethylbenzene 405 50 13 ug/l SM 6200B
Isopropylbenzene 133 50 13 ug/l SM 6200B
p-Isopropyltoluene 76.7 50 13 ug/l SM 6200B
Methylene Chloride 233 200 100 ug/l SM 6200B
Methyl Tert Butyl Ether 26.6 J 50 13 ug/l SM 6200B
Naphthalene 352 50 13 ug/l SM 6200B
n-Propylbenzene 770 50 13 ug/l SM 6200B
Toluene 160 50 13 ug/l SM 6200B
1,3,5-Trimethylbenzene 1320 50 13 ug/l SM 6200B
m,p-Xylene 920 100 18 ug/l SM 6200B
o-Xylene 237 50 13 ug/l SM 6200B
Xylene (total)1160 150 31 ug/l SM 6200B
FA30628-7 MW-14
Benzene 79.8 1.0 0.25 ug/l SM 6200B
n-Butylbenzene 0.61 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 1.9 0.50 0.13 ug/l SM 6200B
5 of 41
FA30628 2
Summary of Hits Page 3 of 3
Job Number:FA30628
Account:GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Collected:01/11/16
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
tert-Butylbenzene 0.25 J 0.50 0.13 ug/l SM 6200B
1,2-Dichloroethane 2.0 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 6.8 0.50 0.13 ug/l SM 6200B
Ethylbenzene 27.9 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 7.4 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.19 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.29 J 0.50 0.13 ug/l SM 6200B
Naphthalene 29.6 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 5.9 0.50 0.13 ug/l SM 6200B
Tetrachloroethylene 0.33 J 0.50 0.13 ug/l SM 6200B
Toluene 1.1 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 35.0 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 3.9 0.50 0.13 ug/l SM 6200B
m,p-Xylene 25.8 1.0 0.18 ug/l SM 6200B
o-Xylene 6.7 0.50 0.13 ug/l SM 6200B
Xylene (total)32.5 1.5 0.31 ug/l SM 6200B
FA30628-8 MW-17
Benzene 5.6 0.50 0.13 ug/l SM 6200B
1,2-Dichloroethane 0.24 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.74 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.18 J 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.23 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.58 0.50 0.13 ug/l SM 6200B
Tetrachloroethylene 0.31 J 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.78 0.50 0.13 ug/l SM 6200B
6 of 41
FA30628 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
7 of 41
FA30628 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1A
Lab Sample ID:FA30628-1 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043375.D 1 01/18/16 TD n/a n/a VE1435
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 41
FA30628 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1A
Lab Sample ID:FA30628-1 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 107%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 41
FA30628 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA30628-2 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043381.D 100 01/18/16 TD n/a n/a VE1435
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2480 50 13 ug/l
108-86-1 Bromobenzene ND 50 13 ug/l
74-97-5 Bromochloromethane ND 50 13 ug/l
75-27-4 Bromodichloromethane ND 50 13 ug/l
75-25-2 Bromoform ND 50 13 ug/l
104-51-8 n-Butylbenzene ND 50 13 ug/l
135-98-8 sec-Butylbenzene ND 50 13 ug/l
98-06-6 tert-Butylbenzene ND 50 13 ug/l
56-23-5 Carbon Tetrachloride ND 50 13 ug/l
108-90-7 Chlorobenzene ND 50 13 ug/l
75-00-3 Chloroethane ND 50 20 ug/l
67-66-3 Chloroform 13.8 50 13 ug/l J
95-49-8 o-Chlorotoluene ND 50 13 ug/l
106-43-4 p-Chlorotoluene ND 50 13 ug/l
124-48-1 Dibromochloromethane ND 50 13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 29 ug/l
106-93-4 1,2-Dibromoethane ND 50 13 ug/l
75-71-8 Dichlorodifluoromethane ND 50 20 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 13 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 13 ug/l
75-34-3 1,1-Dichloroethane ND 50 13 ug/l
107-06-2 1,2-Dichloroethane 16.4 50 13 ug/l J
75-35-4 1,1-Dichloroethylene ND 50 13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 13 ug/l
78-87-5 1,2-Dichloropropane ND 50 13 ug/l
142-28-9 1,3-Dichloropropane ND 50 13 ug/l
594-20-7 2,2-Dichloropropane ND 50 13 ug/l
563-58-6 1,1-Dichloropropene ND 50 13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 41
FA30628 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA30628-2 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 39.9 50 13 ug/l J
100-41-4 Ethylbenzene 261 50 13 ug/l
87-68-3 Hexachlorobutadiene ND 50 13 ug/l
98-82-8 Isopropylbenzene 13.9 50 13 ug/l J
99-87-6 p-Isopropyltoluene ND 50 13 ug/l
74-83-9 Methyl Bromide ND 50 20 ug/l
74-87-3 Methyl Chloride ND 50 20 ug/l
74-95-3 Methylene Bromide ND 50 13 ug/l
75-09-2 Methylene Chloride 290 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether 887 50 13 ug/l
91-20-3 Naphthalene 117 50 13 ug/l
103-65-1 n-Propylbenzene 32.9 50 13 ug/l J
100-42-5 Styrene ND 50 13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 13 ug/l
127-18-4 Tetrachloroethylene ND 50 13 ug/l
108-88-3 Toluene 2220 50 13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 13 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 13 ug/l
79-01-6 Trichloroethylene ND 50 13 ug/l
75-69-4 Trichlorofluoromethane ND 50 20 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 14 ug/l
95-63-6 1,2,4-Trimethylbenzene 288 50 13 ug/l
108-67-8 1,3,5-Trimethylbenzene 86.7 50 13 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 1060 100 18 ug/l
95-47-6 o-Xylene 469 50 13 ug/l
1330-20-7 Xylene (total)1530 150 31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 41
FA30628 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3A
Lab Sample ID:FA30628-3 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043374.D 1 01/18/16 TD n/a n/a VE1435
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 4.1 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane 1.3 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform 2.0 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane 0.68 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane 0.29 0.50 0.13 ug/l J
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 41
FA30628 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3A
Lab Sample ID:FA30628-3 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.87 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.4 0.50 0.13 ug/l
91-20-3 Naphthalene 0.18 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 107%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 41
FA30628 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-6
Lab Sample ID:FA30628-4 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043347.D 1 01/16/16 TD n/a n/a VE1434
Run #2 E043380.D 2.5 01/18/16 TD n/a n/a VE1435
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.59 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND a 1.3 0.50 ug/l
67-66-3 Chloroform 0.18 0.50 0.13 ug/l J
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND a 1.3 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane 2.3 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 41
FA30628 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-6
Lab Sample ID:FA30628-4 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 4.2 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND a 1.3 0.50 ug/l
74-87-3 Methyl Chloride ND a 1.3 0.50 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride 5.3 a 5.0 2.5 ug/l
1634-04-4 Methyl Tert Butyl Ether 90.1 a 1.3 0.31 ug/l
91-20-3 Naphthalene 0.14 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND a 1.3 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND a 1.3 0.31 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%107%70-130%
2037-26-5 Toluene-D8 96%95%70-130%
460-00-4 4-Bromofluorobenzene 107%105%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 41
FA30628 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:FA30628-5 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043348.D 250 01/16/16 TD n/a n/a VE1434
Run #2 E043382.D 1000 01/18/16 TD n/a n/a VE1435
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 13800 a 500 130 ug/l
108-86-1 Bromobenzene ND 130 31 ug/l
74-97-5 Bromochloromethane ND 130 31 ug/l
75-27-4 Bromodichloromethane ND 130 31 ug/l
75-25-2 Bromoform ND 130 31 ug/l
104-51-8 n-Butylbenzene 520 130 31 ug/l
135-98-8 sec-Butylbenzene 214 130 31 ug/l
98-06-6 tert-Butylbenzene ND 130 31 ug/l
56-23-5 Carbon Tetrachloride ND 130 31 ug/l
108-90-7 Chlorobenzene ND 130 31 ug/l
75-00-3 Chloroethane ND a 500 200 ug/l
67-66-3 Chloroform ND 130 31 ug/l
95-49-8 o-Chlorotoluene ND 130 31 ug/l
106-43-4 p-Chlorotoluene ND 130 31 ug/l
124-48-1 Dibromochloromethane ND 130 31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 130 72 ug/l
106-93-4 1,2-Dibromoethane 112 130 31 ug/l J
75-71-8 Dichlorodifluoromethane ND a 500 200 ug/l
95-50-1 1,2-Dichlorobenzene ND 130 31 ug/l
541-73-1 1,3-Dichlorobenzene ND 130 31 ug/l
106-46-7 1,4-Dichlorobenzene ND 130 31 ug/l
75-34-3 1,1-Dichloroethane ND 130 31 ug/l
107-06-2 1,2-Dichloroethane 250 130 31 ug/l
75-35-4 1,1-Dichloroethylene ND 130 31 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 130 31 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 130 31 ug/l
78-87-5 1,2-Dichloropropane ND 130 31 ug/l
142-28-9 1,3-Dichloropropane ND 130 31 ug/l
594-20-7 2,2-Dichloropropane ND 130 31 ug/l
563-58-6 1,1-Dichloropropene ND 130 31 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 130 31 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 130 31 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 41
FA30628 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-7
Lab Sample ID:FA30628-5 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 227 130 31 ug/l
100-41-4 Ethylbenzene 6140 130 31 ug/l
87-68-3 Hexachlorobutadiene ND 130 31 ug/l
98-82-8 Isopropylbenzene 484 130 31 ug/l
99-87-6 p-Isopropyltoluene 113 130 31 ug/l J
74-83-9 Methyl Bromide ND a 500 200 ug/l
74-87-3 Methyl Chloride ND a 500 200 ug/l
74-95-3 Methylene Bromide ND 130 31 ug/l
75-09-2 Methylene Chloride b ND 500 250 ug/l
1634-04-4 Methyl Tert Butyl Ether 4400 130 31 ug/l
91-20-3 Naphthalene 2550 130 31 ug/l
103-65-1 n-Propylbenzene 2010 130 31 ug/l
100-42-5 Styrene 146 130 31 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 130 31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 130 31 ug/l
127-18-4 Tetrachloroethylene ND 130 31 ug/l
108-88-3 Toluene 31700 a 500 130 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 130 31 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 130 31 ug/l
71-55-6 1,1,1-Trichloroethane ND 130 31 ug/l
79-00-5 1,1,2-Trichloroethane ND 130 31 ug/l
79-01-6 Trichloroethylene ND 130 31 ug/l
75-69-4 Trichlorofluoromethane ND a 500 200 ug/l
96-18-4 1,2,3-Trichloropropane ND 130 35 ug/l
95-63-6 1,2,4-Trimethylbenzene 5470 a 500 130 ug/l
108-67-8 1,3,5-Trimethylbenzene 3740 130 31 ug/l
75-01-4 Vinyl Chloride ND a 500 130 ug/l
m,p-Xylene 22200 250 46 ug/l
95-47-6 o-Xylene 9600 130 31 ug/l
1330-20-7 Xylene (total)31800 380 77 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%107%70-130%
2037-26-5 Toluene-D8 98%98%70-130%
460-00-4 4-Bromofluorobenzene 103%109%70-130%
(a) Result is from Run# 2
(b) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 41
FA30628 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA30628-6 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043383.D 100 01/18/16 TD n/a n/a VE1435
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 349 50 13 ug/l
108-86-1 Bromobenzene ND 50 13 ug/l
74-97-5 Bromochloromethane ND 50 13 ug/l
75-27-4 Bromodichloromethane ND 50 13 ug/l
75-25-2 Bromoform ND 50 13 ug/l
104-51-8 n-Butylbenzene 414 50 13 ug/l
135-98-8 sec-Butylbenzene 128 50 13 ug/l
98-06-6 tert-Butylbenzene ND 50 13 ug/l
56-23-5 Carbon Tetrachloride ND 50 13 ug/l
108-90-7 Chlorobenzene ND 50 13 ug/l
75-00-3 Chloroethane ND 50 20 ug/l
67-66-3 Chloroform ND 50 13 ug/l
95-49-8 o-Chlorotoluene ND 50 13 ug/l
106-43-4 p-Chlorotoluene ND 50 13 ug/l
124-48-1 Dibromochloromethane ND 50 13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 29 ug/l
106-93-4 1,2-Dibromoethane ND 50 13 ug/l
75-71-8 Dichlorodifluoromethane ND 50 20 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 13 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 13 ug/l
75-34-3 1,1-Dichloroethane ND 50 13 ug/l
107-06-2 1,2-Dichloroethane ND 50 13 ug/l
75-35-4 1,1-Dichloroethylene ND 50 13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 13 ug/l
78-87-5 1,2-Dichloropropane ND 50 13 ug/l
142-28-9 1,3-Dichloropropane ND 50 13 ug/l
594-20-7 2,2-Dichloropropane ND 50 13 ug/l
563-58-6 1,1-Dichloropropene ND 50 13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 41
FA30628 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA30628-6 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 50 13 ug/l
100-41-4 Ethylbenzene 405 50 13 ug/l
87-68-3 Hexachlorobutadiene ND 50 13 ug/l
98-82-8 Isopropylbenzene 133 50 13 ug/l
99-87-6 p-Isopropyltoluene 76.7 50 13 ug/l
74-83-9 Methyl Bromide ND 50 20 ug/l
74-87-3 Methyl Chloride ND 50 20 ug/l
74-95-3 Methylene Bromide ND 50 13 ug/l
75-09-2 Methylene Chloride 233 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether 26.6 50 13 ug/l J
91-20-3 Naphthalene 352 50 13 ug/l
103-65-1 n-Propylbenzene 770 50 13 ug/l
100-42-5 Styrene ND 50 13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 13 ug/l
127-18-4 Tetrachloroethylene ND 50 13 ug/l
108-88-3 Toluene 160 50 13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 13 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 13 ug/l
79-01-6 Trichloroethylene ND 50 13 ug/l
75-69-4 Trichlorofluoromethane ND 50 20 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 50 13 ug/l
108-67-8 1,3,5-Trimethylbenzene 1320 50 13 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 920 100 18 ug/l
95-47-6 o-Xylene 237 50 13 ug/l
1330-20-7 Xylene (total)1160 150 31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 41
FA30628 33.6
Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-14
Lab Sample ID:FA30628-7 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043350.D 1 01/16/16 TD n/a n/a VE1434
Run #2 E043384.D 2 01/18/16 TD n/a n/a VE1435
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 79.8 a 1.0 0.25 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.61 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 1.9 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.25 0.50 0.13 ug/l J
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND a 1.0 0.40 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND a 1.0 0.40 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane 2.0 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 41
FA30628 33.7
Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-14
Lab Sample ID:FA30628-7 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 6.8 0.50 0.13 ug/l
100-41-4 Ethylbenzene 27.9 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 7.4 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.19 0.50 0.13 ug/l J
74-83-9 Methyl Bromide ND a 1.0 0.40 ug/l
74-87-3 Methyl Chloride ND a 1.0 0.40 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride b ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.29 0.50 0.13 ug/l J
91-20-3 Naphthalene 29.6 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 5.9 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene 0.33 0.50 0.13 ug/l J
108-88-3 Toluene 1.1 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND a 1.0 0.40 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene 35.0 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 3.9 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND a 1.0 0.25 ug/l
m,p-Xylene 25.8 1.0 0.18 ug/l
95-47-6 o-Xylene 6.7 0.50 0.13 ug/l
1330-20-7 Xylene (total)32.5 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%108%70-130%
2037-26-5 Toluene-D8 97%96%70-130%
460-00-4 4-Bromofluorobenzene 106%106%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 41
FA30628 33.7
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-14
Lab Sample ID:FA30628-7 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(b) Associated BS recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 41
FA30628 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-17
Lab Sample ID:FA30628-8 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E043376.D 1 01/18/16 TD n/a n/a VE1435
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 5.6 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane 0.24 0.50 0.13 ug/l J
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 41
FA30628 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-17
Lab Sample ID:FA30628-8 Date Sampled:01/11/16
Matrix:AQ - Ground Water Date Received:01/12/16
Method:SM 6200B Percent Solids:n/a
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.74 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.18 0.50 0.13 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.23 0.50 0.13 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.58 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene 0.31 0.50 0.13 ug/l J
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.78 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 93%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 41
FA30628 33.8
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
25 of 41
FA30628 4
FA30628: Chain of Custody
Page 1 of 3
26 of 41
FA30628 44.1
FA30628: Chain of Custody
Page 2 of 3
27 of 41
FA30628 44.1
FA30628: Chain of Custody
Page 3 of 3
28 of 41
FA30628 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
29 of 41
FA30628 5
Method Blank Summary Page 1 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1434-MB E043337.D 1 01/16/16 TD n/a n/a VE1434
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-4, FA30628-5, FA30628-7
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
30 of 41
FA30628 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1434-MB E043337.D 1 01/16/16 TD n/a n/a VE1434
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-4, FA30628-5, FA30628-7
CAS No.Compound Result RL MDL Units Q
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.5 1.3 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
31 of 41
FA30628 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1435-MB E043373.D 1 01/18/16 TD n/a n/a VE1435
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-1, FA30628-2, FA30628-3, FA30628-4, FA30628-5, FA30628-6, FA30628-7, FA30628-8
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.29 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
32 of 41
FA30628 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1435-MB E043373.D 1 01/18/16 TD n/a n/a VE1435
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-1, FA30628-2, FA30628-3, FA30628-4, FA30628-5, FA30628-6, FA30628-7, FA30628-8
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.14 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.18 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.31 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
33 of 41
FA30628 55.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1434-BS E043336.D 1 01/16/16 TD n/a n/a VE1434
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-4, FA30628-5, FA30628-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.3 113 70-130
108-86-1 Bromobenzene 10 11.6 116 70-130
74-97-5 Bromochloromethane 10 11.5 115 70-130
75-27-4 Bromodichloromethane 10 11.2 112 70-130
75-25-2 Bromoform 10 9.5 95 70-130
104-51-8 n-Butylbenzene 10 11.5 115 70-130
135-98-8 sec-Butylbenzene 10 11.6 116 70-130
98-06-6 tert-Butylbenzene 10 11.5 115 70-130
56-23-5 Carbon Tetrachloride 10 11.8 118 70-130
108-90-7 Chlorobenzene 10 11.1 111 70-130
67-66-3 Chloroform 10 11.4 114 70-130
95-49-8 o-Chlorotoluene 10 11.8 118 70-130
106-43-4 p-Chlorotoluene 10 11.7 117 70-130
124-48-1 Dibromochloromethane 10 10.4 104 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.6 96 70-130
106-93-4 1,2-Dibromoethane 10 11.2 112 70-130
95-50-1 1,2-Dichlorobenzene 10 11.1 111 70-130
541-73-1 1,3-Dichlorobenzene 10 11.4 114 70-130
106-46-7 1,4-Dichlorobenzene 10 11.2 112 70-130
75-34-3 1,1-Dichloroethane 10 11.9 119 70-130
107-06-2 1,2-Dichloroethane 10 11.8 118 70-130
75-35-4 1,1-Dichloroethylene 10 12.1 121 70-130
156-59-2 cis-1,2-Dichloroethylene 10 11.4 114 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.9 119 70-130
78-87-5 1,2-Dichloropropane 10 11.7 117 70-130
142-28-9 1,3-Dichloropropane 10 11.6 116 70-130
594-20-7 2,2-Dichloropropane 10 11.7 117 70-130
563-58-6 1,1-Dichloropropene 10 11.7 117 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.2 112 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.4 114 70-130
108-20-3 Di-Isopropyl Ether 10 11.8 118 70-130
100-41-4 Ethylbenzene 10 11.2 112 70-130
87-68-3 Hexachlorobutadiene 10 11.1 111 70-130
98-82-8 Isopropylbenzene 10 11.0 110 70-130
99-87-6 p-Isopropyltoluene 10 11.4 114 70-130
74-95-3 Methylene Bromide 10 11.4 114 70-130
* = Outside of Control Limits.
34 of 41
FA30628 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1434-BS E043336.D 1 01/16/16 TD n/a n/a VE1434
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-4, FA30628-5, FA30628-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
75-09-2 Methylene Chloride 10 13.4 134*70-130
108-10-1 4-Methyl-2-pentanone (MIBK)50 54.7 109 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.4 114 70-130
91-20-3 Naphthalene 10 10.9 109 70-130
103-65-1 n-Propylbenzene 10 11.8 118 70-130
100-42-5 Styrene 10 10.6 106 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.9 109 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 11.5 115 70-130
127-18-4 Tetrachloroethylene 10 11.2 112 70-130
108-88-3 Toluene 10 10.7 107 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.4 114 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.2 112 70-130
71-55-6 1,1,1-Trichloroethane 10 11.6 116 70-130
79-00-5 1,1,2-Trichloroethane 10 11.3 113 70-130
79-01-6 Trichloroethylene 10 11.7 117 70-130
96-18-4 1,2,3-Trichloropropane 10 11.2 112 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.2 112 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.4 114 70-130
m,p-Xylene 20 22.3 112 70-130
95-47-6 o-Xylene 10 10.8 108 70-130
1330-20-7 Xylene (total)30 33.1 110 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
* = Outside of Control Limits.
35 of 41
FA30628 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1435-BS E043371.D 1 01/18/16 TD n/a n/a VE1435
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-1, FA30628-2, FA30628-3, FA30628-4, FA30628-5, FA30628-6, FA30628-7, FA30628-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.3 103 70-130
108-86-1 Bromobenzene 10 10.5 105 70-130
74-97-5 Bromochloromethane 10 10.5 105 70-130
75-27-4 Bromodichloromethane 10 10.2 102 70-130
75-25-2 Bromoform 10 8.9 89 70-130
104-51-8 n-Butylbenzene 10 10.5 105 70-130
135-98-8 sec-Butylbenzene 10 10.6 106 70-130
98-06-6 tert-Butylbenzene 10 10.5 105 70-130
56-23-5 Carbon Tetrachloride 10 10.6 106 70-130
108-90-7 Chlorobenzene 10 10.1 101 70-130
75-00-3 Chloroethane 10 12.7 127 60-140
67-66-3 Chloroform 10 10.3 103 70-130
95-49-8 o-Chlorotoluene 10 10.6 106 70-130
106-43-4 p-Chlorotoluene 10 10.5 105 70-130
124-48-1 Dibromochloromethane 10 9.5 95 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.8 98 70-130
106-93-4 1,2-Dibromoethane 10 10.4 104 70-130
75-71-8 Dichlorodifluoromethane 10 9.9 99 60-140
95-50-1 1,2-Dichlorobenzene 10 10.5 105 70-130
541-73-1 1,3-Dichlorobenzene 10 10.4 104 70-130
106-46-7 1,4-Dichlorobenzene 10 10.4 104 70-130
75-34-3 1,1-Dichloroethane 10 10.7 107 70-130
107-06-2 1,2-Dichloroethane 10 10.7 107 70-130
75-35-4 1,1-Dichloroethylene 10 10.9 109 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.2 102 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.7 107 70-130
78-87-5 1,2-Dichloropropane 10 10.5 105 70-130
142-28-9 1,3-Dichloropropane 10 10.4 104 70-130
594-20-7 2,2-Dichloropropane 10 10.5 105 70-130
563-58-6 1,1-Dichloropropene 10 10.6 106 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10 100 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.3 103 70-130
108-20-3 Di-Isopropyl Ether 10 10.7 107 70-130
100-41-4 Ethylbenzene 10 10.1 101 70-130
87-68-3 Hexachlorobutadiene 10 11.1 111 70-130
98-82-8 Isopropylbenzene 10 9.9 99 70-130
* = Outside of Control Limits.
36 of 41
FA30628 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1435-BS E043371.D 1 01/18/16 TD n/a n/a VE1435
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-1, FA30628-2, FA30628-3, FA30628-4, FA30628-5, FA30628-6, FA30628-7, FA30628-8
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.4 104 70-130
74-83-9 Methyl Bromide 10 12.1 121 60-140
74-87-3 Methyl Chloride 10 11.2 112 60-140
74-95-3 Methylene Bromide 10 10.3 103 70-130
75-09-2 Methylene Chloride 10 11.8 118 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.4 104 70-130
91-20-3 Naphthalene 10 11.3 113 70-130
103-65-1 n-Propylbenzene 10 10.7 107 70-130
100-42-5 Styrene 10 9.4 94 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.8 98 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.8 108 70-130
127-18-4 Tetrachloroethylene 10 10.2 102 70-130
108-88-3 Toluene 10 9.5 95 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.8 118 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.2 112 70-130
71-55-6 1,1,1-Trichloroethane 10 10.6 106 70-130
79-00-5 1,1,2-Trichloroethane 10 10.2 102 70-130
79-01-6 Trichloroethylene 10 10.6 106 70-130
75-69-4 Trichlorofluoromethane 10 12.2 122 60-140
96-18-4 1,2,3-Trichloropropane 10 10.3 103 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.2 102 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.4 104 70-130
75-01-4 Vinyl Chloride 10 11.6 116 60-140
m,p-Xylene 20 20.1 101 70-130
95-47-6 o-Xylene 10 9.7 97 70-130
1330-20-7 Xylene (total)30 29.8 99 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
* = Outside of Control Limits.
37 of 41
FA30628 55.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA30648-4MS E043362.D 25 01/16/16 TD n/a n/a VE1434
FA30648-4MSD E043363.D 25 01/16/16 TD n/a n/a VE1434
FA30648-4 E043354.D 25 01/16/16 TD n/a n/a VE1434
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-4, FA30628-5, FA30628-7
FA30648-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 830 250 1070 96 250 927 39* a 14 70-130/20
108-86-1 Bromobenzene ND 250 182 73 250 150 60*19 70-130/20
74-97-5 Bromochloromethane ND 250 173 69*250 148 59*16 70-130/20
75-27-4 Bromodichloromethane ND 250 156 62*250 133 53*16 70-130/20
75-25-2 Bromoform ND 250 80.6 32*250 75.5 30*7 70-130/20
104-51-8 n-Butylbenzene ND 250 172 69*250 146 58*16 70-130/20
135-98-8 sec-Butylbenzene 5.5 J 250 190 74 250 158 61*18 70-130/20
98-06-6 tert-Butylbenzene ND 250 183 73 250 152 61*19 70-130/20
56-23-5 Carbon Tetrachloride ND 250 187 75 250 151 60*21*70-130/20
108-90-7 Chlorobenzene ND 250 179 72 250 153 61*16 70-130/20
67-66-3 Chloroform ND 250 186 74 250 163 65*13 70-130/20
95-49-8 o-Chlorotoluene ND 250 197 79 250 163 65*19 70-130/20
106-43-4 p-Chlorotoluene ND 250 184 74 250 153 61*18 70-130/20
124-48-1 Dibromochloromethane ND 250 114 46*250 101 40*12 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 250 142 57*250 116 46*20 70-130/20
106-93-4 1,2-Dibromoethane ND 250 174 70 250 151 60*14 70-130/20
95-50-1 1,2-Dichlorobenzene ND 250 174 70 250 147 59*17 70-130/20
541-73-1 1,3-Dichlorobenzene ND 250 179 72 250 151 60*17 70-130/20
106-46-7 1,4-Dichlorobenzene ND 250 176 70 250 146 58*19 70-130/20
75-34-3 1,1-Dichloroethane ND 250 202 81 250 174 70 15 70-130/20
107-06-2 1,2-Dichloroethane ND 250 193 77 250 169 68*13 70-130/20
75-35-4 1,1-Dichloroethylene ND 250 212 85 250 182 73 15 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 250 174 70 250 153 61*13 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 250 215 86 250 186 74 14 70-130/20
78-87-5 1,2-Dichloropropane ND 250 190 76 250 164 66*15 70-130/20
142-28-9 1,3-Dichloropropane ND 250 176 70 250 154 62*13 70-130/20
594-20-7 2,2-Dichloropropane ND 250 173 69*250 150 60*14 70-130/20
563-58-6 1,1-Dichloropropene ND 250 191 76 250 166 66*14 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 250 155 62*250 118 47*27*70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 250 161 64*250 125 50*25*70-130/20
108-20-3 Di-Isopropyl Ether 165 250 369 82 250 319 62*15 70-130/20
100-41-4 Ethylbenzene 359 250 553 78 250 480 48*14 70-130/20
87-68-3 Hexachlorobutadiene ND 250 149 60*250 132 53*12 70-130/20
98-82-8 Isopropylbenzene 31.0 250 207 70 250 179 59*15 70-130/20
99-87-6 p-Isopropyltoluene ND 250 176 70 250 147 59*18 70-130/20
74-95-3 Methylene Bromide ND 250 189 76 250 162 65*15 70-130/20
* = Outside of Control Limits.
38 of 41
FA30628 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA30648-4MS E043362.D 25 01/16/16 TD n/a n/a VE1434
FA30648-4MSD E043363.D 25 01/16/16 TD n/a n/a VE1434
FA30648-4 E043354.D 25 01/16/16 TD n/a n/a VE1434
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-4, FA30628-5, FA30628-7
FA30648-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
75-09-2 Methylene Chloride ND 250 245 98 250 211 84 15 70-130/20
108-10-1 4-Methyl-2-pentanone (MIBK)ND 1250 957 77 1250 837 67*13 70-130/20
1634-04-4 Methyl Tert Butyl Ether 18.1 250 197 72 250 169 60*15 70-130/20
91-20-3 Naphthalene 163 250 256 37*250 230 27*11 70-130/20
103-65-1 n-Propylbenzene 60.4 250 257 79 250 213 61*19 70-130/20
100-42-5 Styrene ND 250 150 60*250 132 53*13 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 250 166 66*250 142 57*16 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 250 181 72 250 151 60*18 70-130/20
127-18-4 Tetrachloroethylene ND 250 170 68*250 148 59*14 70-130/20
108-88-3 Toluene 9.5 J 250 175 66*250 154 58*13 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 250 157 63*250 142 57*10 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 250 155 62*250 140 56*10 70-130/20
71-55-6 1,1,1-Trichloroethane ND 250 192 77 250 164 66*16 70-130/20
79-00-5 1,1,2-Trichloroethane ND 250 180 72 250 159 64*12 70-130/20
79-01-6 Trichloroethylene ND 250 186 74 250 163 65*13 70-130/20
96-18-4 1,2,3-Trichloropropane ND 250 177 71 250 152 61*15 70-130/20
95-63-6 1,2,4-Trimethylbenzene 163 250 341 71 250 286 49*18 70-130/20
108-67-8 1,3,5-Trimethylbenzene 41.9 250 222 72 250 185 57*18 70-130/20
m,p-Xylene 205 500 571 73 500 494 58*14 70-130/20
95-47-6 o-Xylene ND 250 172 69*250 150 60*14 70-130/20
1330-20-7 Xylene (total)205 750 743 72 750 643 58*14 70-130/20
CAS No.Surrogate Recoveries MS MSD FA30648-4 Limits
1868-53-7 Dibromofluoromethane 99%99%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%109%104%70-130%
2037-26-5 Toluene-D8 97%97%98%70-130%
460-00-4 4-Bromofluorobenzene 107%103%104%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
39 of 41
FA30628 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA30628-6MS E043396.D 100 01/18/16 TD n/a n/a VE1435
FA30628-6MSD E043397.D 100 01/18/16 TD n/a n/a VE1435
FA30628-6 E043383.D 100 01/18/16 TD n/a n/a VE1435
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-1, FA30628-2, FA30628-3, FA30628-4, FA30628-5, FA30628-6, FA30628-7, FA30628-8
FA30628-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 349 1000 1100 75 1000 987 64*11 70-130/20
108-86-1 Bromobenzene ND 1000 734 73 1000 656 66*11 70-130/20
74-97-5 Bromochloromethane ND 1000 704 70 1000 662 66*6 70-130/20
75-27-4 Bromodichloromethane ND 1000 675 68*1000 633 63*6 70-130/20
75-25-2 Bromoform ND 1000 409 41*1000 431 43*5 70-130/20
104-51-8 n-Butylbenzene 414 1000 1190 78 1000 1000 59*17 70-130/20
135-98-8 sec-Butylbenzene 128 1000 913 79 1000 785 66*15 70-130/20
98-06-6 tert-Butylbenzene ND 1000 770 77 1000 661 66*15 70-130/20
56-23-5 Carbon Tetrachloride ND 1000 806 81 1000 713 71 12 70-130/20
108-90-7 Chlorobenzene ND 1000 747 75 1000 672 67*11 70-130/20
75-00-3 Chloroethane ND 1000 650 65 1000 553 55*16 60-140/20
67-66-3 Chloroform ND 1000 811 81 1000 728 73 11 70-130/20
95-49-8 o-Chlorotoluene ND 1000 942 94 1000 819 82 14 70-130/20
106-43-4 p-Chlorotoluene ND 1000 767 77 1000 662 66*15 70-130/20
124-48-1 Dibromochloromethane ND 1000 546 55*1000 544 54*0 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 726 73 1000 624 62*15 70-130/20
106-93-4 1,2-Dibromoethane ND 1000 724 72 1000 665 67*8 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 661 66 1000 574 57*14 60-140/20
95-50-1 1,2-Dichlorobenzene ND 1000 754 75 1000 656 66*14 70-130/20
541-73-1 1,3-Dichlorobenzene ND 1000 768 77 1000 664 66*15 70-130/20
106-46-7 1,4-Dichlorobenzene ND 1000 745 75 1000 644 64*15 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 827 83 1000 747 75 10 70-130/20
107-06-2 1,2-Dichloroethane ND 1000 793 79 1000 727 73 9 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 873 87 1000 776 78 12 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 733 73 1000 671 67*9 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 889 89 1000 789 79 12 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 782 78 1000 709 71 10 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 742 74 1000 666 67*11 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 810 81 1000 725 73 11 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 827 83 1000 719 72 14 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 684 68*1000 637 64*7 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 737 74 1000 676 68*9 70-130/20
108-20-3 Di-Isopropyl Ether ND 1000 788 79 1000 715 72 10 70-130/20
100-41-4 Ethylbenzene 405 1000 1160 76 1000 1020 62*13 70-130/20
87-68-3 Hexachlorobutadiene ND 1000 702 70 1000 605 61*15 70-130/20
98-82-8 Isopropylbenzene 133 1000 906 77 1000 796 66*13 70-130/20
* = Outside of Control Limits.
40 of 41
FA30628 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA30628
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 3; 1332 E Memorial Dr, Ahoskie, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA30628-6MS E043396.D 100 01/18/16 TD n/a n/a VE1435
FA30628-6MSD E043397.D 100 01/18/16 TD n/a n/a VE1435
FA30628-6 E043383.D 100 01/18/16 TD n/a n/a VE1435
The QC reported here applies to the following samples:Method: SM 6200B
FA30628-1, FA30628-2, FA30628-3, FA30628-4, FA30628-5, FA30628-6, FA30628-7, FA30628-8
FA30628-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 76.7 1000 831 75 1000 719 64*14 70-130/20
74-83-9 Methyl Bromide ND 1000 599 60 1000 527 53*13 60-140/20
74-87-3 Methyl Chloride ND 1000 654 65 1000 590 59*10 60-140/20
74-95-3 Methylene Bromide ND 1000 773 77 1000 709 71 9 70-130/20
75-09-2 Methylene Chloride 233 1000 995 76 1000 904 67*10 70-130/20
1634-04-4 Methyl Tert Butyl Ether 26.6 J 1000 749 72 1000 698 67*7 70-130/20
91-20-3 Naphthalene 352 1000 1160 81 1000 1060 71 9 70-130/20
103-65-1 n-Propylbenzene 770 1000 1540 77 1000 1330 56*15 70-130/20
100-42-5 Styrene ND 1000 681 68*1000 614 61*10 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 716 72 1000 636 64*12 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 744 74 1000 700 70 6 70-130/20
127-18-4 Tetrachloroethylene ND 1000 754 75 1000 652 65*15 70-130/20
108-88-3 Toluene 160 1000 866 71 1000 762 60*13 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 724 72 1000 682 68*6 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 733 73 1000 661 66*10 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 800 80 1000 717 72 11 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 873 87 1000 789 79 10 70-130/20
79-01-6 Trichloroethylene ND 1000 828 83 1000 730 73 13 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 601 60 1000 511 51*16 60-140/20
96-18-4 1,2,3-Trichloropropane ND 1000 725 73 1000 684 68*6 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 1000 3890 389*1000 3360 336*15 70-130/20
108-67-8 1,3,5-Trimethylbenzene 1320 1000 2030 71 1000 1750 43*15 70-130/20
75-01-4 Vinyl Chloride ND 1000 637 64 1000 552 55*14 60-140/20
m,p-Xylene 920 2000 2420 75 2000 2120 60*13 70-130/20
95-47-6 o-Xylene 237 1000 974 74 1000 866 63*12 70-130/20
1330-20-7 Xylene (total)1160 3000 3390 74 3000 2990 61*13 70-130/20
CAS No.Surrogate Recoveries MS MSD FA30628-6 Limits
1868-53-7 Dibromofluoromethane 99%99%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%109%108%70-130%
2037-26-5 Toluene-D8 99%97%97%70-130%
460-00-4 4-Bromofluorobenzene 102%101%106%70-130%
* = Outside of Control Limits.
41 of 41
FA30628 55.3.2