WA-706_10000_CA_RPTS_20150430_MRP

EXECUTIVE SUMMARY

The former Peele’s Service Station site is located at 2675 Old US Highway 64, Jamesville, Martin
County, North Carolina. According to available information, a petroleum release at the site was
confirmed subsequent to the removal of one 1,000-gallon and one 550-gallon gasoline USTs in
September 1992. The site risk classification is currently ranked as high risk due to forty-seven potable
water supply wells being located within a 1,000-foot radius of the site.

On April 1, 2015, nine Type II monitoring wells, one Type III monitoring well and six water supply wells
were gauged, purged and/or sampled. Free product was not observed in any of these wells during the
April 2015 sampling event. Concentrations of requested method constituents that exceeded the MACs
were reported in the ground water samples collected from MW-2R and MW-11. None of the reported
contaminant concentrations exceeded the gross contamination levels. A concentration of
trichloroethylene that exceeded the MAC was reported in the ground water sample collected from WSW-
56. Concentrations of trichloroethylene that did not exceed the MAC were reported in the ground water
samples collected from WSW-8 and WSW-41.

Based on this information, the results of the April 2015 sampling event should be confirmed in October
2015. If contaminant concentrations remain low and free product is no longer present, a fate and
transport model should be developed to determine if the contaminant plume poses a significant risk the
nearest down-gradient receptor. An update to the sensitive receptor survey should be completed during
the next sampling event.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................... 1
2.0 CURRENT SITE ACTIVITIES ................................................................................................. 1
3.0 GROUND WATER QUALITY ................................................................................................. 1
4.0 CONCLUSIONS AND RECOMMENDATIONS ..................................................................... 2
5.0 LIMITATIONS .......................................................................................................................... 3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results

APPENDIX
Appendix A: Laboratory Report – Ground Water Samples
1

1.0 SITE HISTORY AND CHARACTERIZATION
The former Peele’s Service Station site is located at 2675 Old US Highway 64, Jamesville, Martin
County, North Carolina, in a residential area (Figure 1). According to available information, one 1,000-
gallon and one 550-gallon gasoline underground storage tanks (USTs) were removed from the site on
September 23, 1992. Eighteen Type II monitoring wells (MW-1, MW-2, MW-2R, MW-3 through MW-4
and MW-6 through MW-18) and one Type III monitoring well (MW-5) were installed at the site during
previous ground water assessment and corrective action activities. Previous activities were conducted by
past consultants. Although Geological Resources, Inc. (GRI) cannot verify the accuracy of information
obtained from previous reports, for the purposes of this report, it is assumed to be correct. Please refer to
previous submittals for further historical information regarding the site.

2.0 CURRENT SITE ACTIVITIES
The purpose of this report is to present the results of ground water monitoring activities conducted on
April 1, 2015 at the Peele’s Service Station site. The activities were conducted in accordance with GRI
proposal number 14-713, which was submitted to NCDENR on November 24, 2014 and approved as
Task Authorization No. 10000-54 on February 2, 2015. The purpose of the activities was to obtain
current ground water quality data for the site.

3.0 GROUND WATER QUALITY
Nine Type II monitoring wells (MW-1, MW-2R, MW-4, MW-8, MW-10, MW-11, MW-14, MW-15 and
MW-18), one Type III monitoring well (MW-5) and five water supply wells (WSW-2, WSW-6, WSW-7,
WSW-8, WSW-41 and WSW-56) were gauged, purged and/or sampled on April 1, 2015. Water supply
well WSW-3 was not located and WSW-5 was not operational during the April 2015 sampling event.
Please note, monitoring well MW-17 was located under a large puddle and was not gauged or sampled
during the April 2015 sampling event. No free product was observed in any of the monitoring wells.

Depths to ground water in the Type II monitoring wells measured on April 1, 2015 ranged from 0.93 to
5.54 feet below the tops of well casings. Ground water elevations in the Type II monitoring wells relative
to a temporary benchmark assumed by the previous consultant ranged from 95.34 to 99.78 feet. Based on
the April 2015 gauging data, the ground water flow across the site was generally toward the northeast.
The average horizontal hydraulic gradient in the vicinity of the source area was approximately 0.02 feet
per foot. The vertical hydraulic gradient between paired wells MW-1/MW-5 was approximately 0.59 feet
per foot in the downward direction. A Site Map showing the locations of the monitoring and water
2

supply wells has been included as Figure 2. A Water Table Surface Map based on the April 2015
gauging data is included as Figure 3. Well construction and gauging information is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the above referenced
monitoring and water supply wells for volatile organic compounds (VOCs) using EPA Method 6200B.
Concentrations of benzene, xylenes, naphthalene and/or 1,2,4-trimethylbenzene that exceeded the
maximum allowable concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the
ground water samples collected from MW-2R and MW-11. A concentration of trichloroethylene that
exceeded the MAC was reported in the ground water sample collected from WSW-56. Concentrations of
trichloroethylene that did not exceed the MAC were reported in the ground water samples collected from
WSW-8 and WSW-41. None of the reported contaminant concentrations exceeded the gross
contamination levels (GCLs).

A Ground Water Quality Map based on data collected during the April 2015 sampling event is included
as Figure 4. A summary of ground water sample analytical results is presented in Table 2. A complete
laboratory report has been included as Appendix A.

Subsequent to the April 2015 sampling event, an absorbent boom was re-installed in MW-2R to recover
any free product that may recharge into the well.

4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the Type II monitoring wells during the April 2015 sampling
event was 3.12 feet. Ground water flow across the site during the April 2015 sampling event was
generally toward the northeast with a horizontal hydraulic gradient in the vicinity of the source area
of approximately 0.02 feet per foot. The average vertical hydraulic gradient between paired
monitoring wells MW-1/MW-5 was approximately 0.59 feet per foot in the downward direction.
 Free product was not observed in any of the wells during the April 2015 sampling event.
 Concentrations of benzene, xylenes, naphthalene and/or 1,2,4-trimethylbenzene that exceeded the
MACs were reported in the ground water samples collected from MW-2R and MW-11. None of the
reported contaminant concentrations exceeded the GCLs.
 A concentration of trichloroethylene that exceeded the MAC was reported in the ground water sample
collected from WSW-56. Concentrations of trichloroethylene that did not exceed the MAC were
reported in the ground water samples collected from WSW-8 and WSW-41.
3

 Based on this information, the results of the April 2015 sampling event should be confirmed in
October 2015. The absorbent boom that was installed in MW-2R should be removed no less than
ninety days prior to the next sampling event and should not be re-installed in MW-2R. If contaminant
concentrations remain low and free product is no longer present, a fate and transport model should be
developed to determine if the contaminant plume poses a significant risk the nearest down-gradient
receptor. An update to the sensitive receptor survey should be completed during the next sampling
event.

5.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Martin County, North Carolina. The assessment was conducted based
on the scope of work and level of effort desired by NCDENR and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the March 2007 updated receptor survey and ground water monitoring event were not obtained under
the supervision of GRI. Although the accuracy of this information cannot be verified, for the purpose of
this report GRI assumes that it is correct.

FIGURES

TABLES

03/01/07 3.32 0.00 97.04
08/13/07 DRY 0.00 NM
03/12/09 NM 0.00 NM
08/25/09 DRY 0.00 NM
12/08/11 10.17 0.00 90.19
06/13/12 6.98 0.00 93.38
03/07/13 4.33 0.00 96.03
10/02/13 9.19 0.00 91.17
04/02/14 3.41 0.00 96.95
09/30/14 5.98 0.00 94.38
04/01/15 1.87 0.00 98.49
03/01/07 2.63 0.00 97.91
08/13/07 DRY 0.00 NM
03/12/09 DRY 0.00 NM
08/25/09 DRY 0.00 NM
12/08/11 DRY 0.00 NM
06/13/12 7.07 0.00 93.47
03/07/13 2.60 0.00 97.94
10/02/13 DRY 0.00 NM
12/08/11 10.96 0.00 89.90
06/13/12 8.00 0.17 93.01
01/23/13 7.81 0.10 93.13 Before AFVR
01/23/13 10.05 0.00 90.81 After AFVR
03/07/13 5.66 0.44 95.58
08/27/13 5.73 0.25 95.34 Before AFVR
08/27/13 10.17 0.00 90.69 After AFVR
10/02/13 9.88 0.00 90.98
04/02/14 3.39 0.04 97.50
09/30/14 7.07 0.03 93.82
04/01/15 2.16 0.00 98.70
03/01/07 2.85 0.00 97.77
08/13/07 DRY 0.00 NM
03/12/09 DRY 0.00 NM
08/25/09 DRY 0.00 NM
12/08/11 DRY 0.00 NM
06/13/12 7.38 0.00 93.24
03/07/13 3.22 0.00 97.40
10/02/13 DRY 0.00 NM
03/01/07 3.70 0.00 97.01
08/13/07 DRY 0.00 NM
03/12/09 DRY 0.00 NM
08/25/09 DRY 0.00 NM
12/08/11 10.02 0.00 90.69
06/13/12 6.86 0.00 93.85
03/07/13 1.90 0.00 98.81
10/02/13 9.44 0.00 91.27
04/02/14 1.60 0.00 99.11
09/30/14 6.57 0.00 94.14
04/01/15 0.93 0.00 99.78
03/01/07 16.71 0.00 83.69
08/13/07 19.68 0.00 80.72
03/12/09 21.73 0.00 78.67
08/25/09 21.07 0.00 79.33
12/08/11 19.30 0.00 81.10
06/13/12 18.50 0.00 81.90
03/07/13 17.39 0.00 83.01
10/02/13 18.25 0.00 82.15
04/02/14 15.71 0.00 84.69
09/30/14 17.85 0.00 82.55
04/01/15 15.22 0.00 85.18
03/01/07 4.52 0.00 95.58
08/13/07 11.32 0.00 88.78
03/12/09 DRY 0.00 DRY
08/25/09 12.37 0.00 87.73
12/08/11 10.70 0.00 89.40
06/13/12 7.74 0.00 92.36
03/07/13 5.68 0.00 94.42
10/02/13 NM 0.00 NM
08/25/09 12.05 0.00 88.27
12/08/11 11.03 0.00 89.29
06/13/12 8.38 0.00 91.94
03/07/13 5.52 0.00 94.80
10/02/13 9.89 0.00 90.43
100.32
5 5 - 15 15 100.10
MW-7 05/17/93 2.5 122.5 - 12
MW-3 01/27/93
17 100.86
35 100.40
MW-2R
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation* (ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
PEELE'S SERVICE STATION (INCIDENT NO. 10000)
Facility ID#: 0-0013895Date: 04/14/15
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Comments
12/08/11 7 7 - 17
15 100.71
2 2 - 12 12 100.62
MW-4 05/14/93 5 5 - 15
MW-5 05/18/93 30 30 - 35
MW-6 05/17/93
MW-1 01/26/93 5 5 - 15 15 100.36
MW-2 01/27/93 2 2 - 12 12 100.54
Page 1 of 3
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation* (ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
PEELE'S SERVICE STATION (INCIDENT NO. 10000)
Facility ID#: 0-0013895Date: 04/14/15
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Comments
03/01/07 2.76 0.00 97.47
08/13/07 10.70 0.00 89.53
03/12/09 NM 0.00 NM
08/25/09 10.55 0.00 89.68
12/08/11 9.60 0.00 90.63
06/13/12 5.97 0.00 94.26
03/07/13 2.60 0.00 97.63
10/02/13 8.73 0.00 91.50
04/02/14 3.12 0.00 97.11
09/30/14 5.37 0.00 94.86
04/01/15 2.19 0.00 98.04
03/01/07 3.16 0.00 97.13
08/13/07 10.74 0.00 89.55
03/12/09 DRY 0.00 DRY
08/25/09 10.60 0.00 89.69
12/08/11 9.52 0.00 90.77
06/13/12 6.58 0.00 93.71
03/07/13 4.16 0.00 96.13
10/02/13 NM 0.00 NM
08/25/09 13.00 0.00 87.25
12/08/11 10.86 0.00 89.39
06/13/12 8.28 0.00 91.97
03/07/13 6.84 0.00 93.41
10/02/13 9.58 0.00 90.67
04/02/14 3.09 0.00 97.16
09/30/14 7.67 0.00 92.58
04/01/15 2.29 0.00 97.96
03/01/07 5.93 0.00 94.33
08/13/07 11.97 0.00 88.29
03/12/09 15.51 0.00 84.75
08/25/09 14.19 0.00 86.07
12/08/11 11.88 0.00 88.38
06/13/12 9.51 0.00 90.75
03/07/13 7.53 0.00 92.73
10/02/13 10.40 0.00 89.86
04/02/14 4.64 0.00 95.62
09/30/14 8.86 0.00 91.40
04/01/15 3.70 0.00 96.56
03/01/07 3.61 0.00 96.89
08/13/07 11.10 0.00 89.40
03/12/09 13.44 0.00 87.06
08/25/09 NM 0.00 NM
12/08/11 10.17 0.00 90.33
06/13/12 7.30 0.00 93.20
03/07/13 4.98 0.00 95.52
10/02/13 NM 0.00 NM
03/01/07 4.50 0.00 95.79
08/13/07 11.04 0.00 89.25
03/12/09 13.80 0.00 86.49
08/25/09 NM 0.00 NM
12/08/11 10.72 0.00 89.57
06/13/12 7.57 0.00 92.72
03/07/13 5.67 0.00 94.62
10/02/13 NM 0.00 NM
08/25/09 NM NM Not Located
12/08/11 NM NM Not Located
06/13/12 NM NM Not Located
03/07/13 NM NM Not Located
10/02/13 NM NM Not Located
04/02/14 5.78 0.00 95.63
09/30/14 10.23 0.00 91.18
04/01/15 4.89 0.00 96.52
08/25/09 NM NM Not Located
12/08/11 NM NM Not Located
06/13/12 NM NM Not Located
03/07/13 NM NM Not Located
10/02/13 NM NM Not Located
04/02/14 5.13 0.00 95.47
09/30/14 NM NM Not Located
04/01/15 4.48 0.00 96.12
08/25/09 NM NM Not Located
12/08/11 NM NM Not Located
06/13/12 NM NM Not Located
03/07/13 NM NM Not Located
10/02/13 NM NM Not Located
15 100.23
18 101.41
18 100.60
100.29
15
8 - 18 18 100.87
MW-12 02/16/94 4 4 - 14 14 100.50
MW-9 05/19/93
MW-13 04/27/95 8 8 - 18
8
5 5 - 15
18
100.29
5 5 - 15MW-8 05/19/93
MW-10 02/16/94
MW-16
MW-14 04/27/95 8 8 - 18
MW-15 04/27/95 8 8 - 18
04/27/95
4 4 - 14 14 100.25
MW-11 02/16/94 4 4 - 14 14 100.26
Page 2 of 3
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Groundwater
Elevation* (ft.)
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
PEELE'S SERVICE STATION (INCIDENT NO. 10000)
Facility ID#: 0-0013895Date: 04/14/15
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Comments
03/01/07 2.09 0.00 98.57
08/13/07 12.71 0.00 87.95
03/12/09 14.78 0.00 85.88
08/25/09 NM 0.00 NM
12/08/11 13.29 0.00 87.37
06/13/12 3.12 0.00 97.54
03/07/13 1.04 0.00 99.62
10/02/13 11.08 0.00 89.58
04/02/14 1.04 0.00 99.62
09/30/14 1.78 0.00 98.88
04/01/15 NM NM NM Under Puddle
03/01/07 8.37 0.00 92.51
08/13/07 12.93 0.00 87.95
03/12/09 17.02 0.00 83.86
08/25/09 NM 0.00 NM
12/08/11 14.45 0.00 86.43
06/13/12 11.92 0.00 88.96
03/07/13 10.25 0.00 90.63
10/02/13 11.41 0.00 89.47
04/02/14 6.63 0.00 94.25
09/30/14 10.88 0.00 90.00
04/01/15 5.54 0.00 95.34
Notes:
• * Top-of-casing elevation and well construction data is reproduced from the July 2005 monitoring report prepared by CES Engineering, PC; elevations
relative to a temporary benchmark with an assumed datum of 100.00 feet; data reported in feet.
• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] - [free product thickness x 0.8581]
• ft BGS : feet below ground surface
• NA: Not available.
• NM: Not measured; well not located.
15 100.88
5 5 - 15 15 100.66MW-17 08/16/95
MW-18 08/16/95 5 5 - 15
Page 3 of 3
EPA
Method
6010B/
3030C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 400 400 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 29.9 0.91 21.2 4.0 0.18 J 48.6 0.32 J 18.5 0.16 J NR NR NR NR NR
06/13/12 10.3 2.2 6.3 113 <0.13 54.7 <0.11 130 17.6 NR NR NR NR NR
03/07/13 4.6 2.7 4.3 215 <0.10 49.4 <0.10 162 30.7 NR NR NR NR NR
10/02/13 36.2 13.1 26.6 1,020 0.35 J 228 <0.10 973 214 NR NR NR NR NR
04/02/14 0.77 1.0 2.1 86.1 <0.10 33.4 <0.10 71.7 11.9 NR NR NR NR NR
09/30/14 1.9 J 3.4 J 5.7 326 <1.0 88.7 <1.0 331 56.6 NR NR NR NR NR
04/01/15 <0.17 <0.17 0.29 J 7.1 <0.16 3.3 <0.16 6.6 0.70 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 27.1 22.4 29.7 652 <1.3 60.7 <1.1 278 57.3 NR NR NR NR NR
03/07/13 1.7 3.1 1.1 21.7 <0.10 0.49 J <0.10 4.3 1.3 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 147 2,300 1,310 12,250 <6.5 670 <5.4 2,770 756 NR NR NR NR NR
06/13/12 FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/02/13 729 4,320 1,010 19,210 <25 814 <25 3,640 900 NR NR NR NR NR
04/02/14 FP FP FP FP FP FP FP FP FP FP FP FP FP FP
09/30/14 FP FP FP FP FP FP FP FP FP FP FP FP FP FP
04/01/15 26.2 399 88.6 1,720 <4.1 109 <4.0 641 201 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 1.4 2.8 8.3 117 <0.33 10.1 <0.27 63.2 23.7 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 0.80 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 0.10 J <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 1.72 <1.0 <1.0 <3.0 3.47 <1.0 0.16 I NR NR NR NR NR NR NR
03/12/09 2.0 J <0.70 1.2 J 2.7 J 3.6 J 4.0 JB <1.0 2.2 J 0.54 J 77.9 <100 <200 <100 <200
08/25/09 3.53 <0.330 <0.670 <1.33 4.68 <1.00 <1.67 <0.330 <0.330 103 <100 <195.2 <95.2 <195.2
12/08/11 <0.13 <0.13 <0.15 <0.30 0.26 J <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 0.31 J <0.13 <0.15 <0.30 <0.13 0.28 J <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 0.68 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 0.61 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5 NR NR NR NR NR NR NR
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 2.85 <100 <100 NR <100
12/08/11 <0.13 3.8 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR1,2,4 -TrimethylbenzeneMW-1
Facility ID# 0-0013895
MW-2
Date: 04/14/15
Analytical Method
→
GCL (µg/l)
MW-2R
MADEP Methods EPH & VPH
C19-C36 Aliphatics2L Standard (µg/l)EthylbenzeneTolueneLeadC9-C22 AromaticsBenzeneContaminant of Concern
→XylenesC9-C18 AliphaticsMW-3
MW-7
MW-5
MW-4
TABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
PEELE'S SERVICE STATION (INCIDENT NO. 10000)C5-C8 AliphaticsEPA Method 6200B
1,3,5 -TrimethylbenzeneIPEMTBEMW-6 NaphthalenePage 1 of 4
EPA
Method
6010B/
3030C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 400 400 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE1,2,4 -TrimethylbenzeneFacility ID# 0-0013895Date: 04/14/15
Analytical Method
→
GCL (µg/l)
MADEP Methods EPH & VPH
C19-C36 Aliphatics2L Standard (µg/l)EthylbenzeneTolueneLeadC9-C22 AromaticsBenzeneContaminant of Concern
→XylenesC9-C18 AliphaticsTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
PEELE'S SERVICE STATION (INCIDENT NO. 10000)C5-C8 AliphaticsEPA Method 6200B
1,3,5 -TrimethylbenzeneIPEMTBENaphthalene03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 3.02 <100 <100 NR <100
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
09/07/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 3.12 <100 <100 NR <100
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 5.60 <100 <100 NR <100
12/08/11 <0.13 5.9 0.33 J 0.73 J <0.13 <0.10 <0.11 0.21 J <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 0.16 J <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.27 J <0.10 0.21 J <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 3.58 108 136 1,629 10.6 61.4 15.3 NR NR NR NR NR NR NR
08/13/07 14.2 187 736 9,010 31.3 428 11.2 NR NR NR NR NR NR NR
03/12/09 7.3 <0.70 <0.50 1.9 J 3.2 J 1.7 JB <1.0 0.72 J 1.2 J 2.8 J 176 133 <100 166
08/25/09 7.44 <0.330 1.62 J 7.99 <0.330 2.51 <1.67 1.90 0.332 J 11.6 111 296 <97.1 220
12/08/11 35.8 1.4 218 1,710 1.4 348 1.4 987 354 NR NR NR NR NR
06/13/12 10.6 2.3 J 64.0 429 <0.65 133 <0.54 443 104 NR NR NR NR NR
03/07/13 14.8 2.4 99.9 618 0.32 J 262 <0.10 796 130 NR NR NR NR NR
10/02/13 16.4 4.2 J 147 800 <2.5 248 <2.5 1,020 80.5 NR NR NR NR NR
04/02/14 13.1 3.2 125 916 0.31 J 242 <0.10 911 177 NR NR NR NR NR
09/30/14 6.7 0.61 J 27.9 172 <0.50 135 <0.50 194 20.9 NR NR NR NR NR
04/01/15 1.9 J 1.1 J 28.2 210 <0.82 87.0 <0.80 191 29.2 NR NR NR NR NR
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5 NR NR NR NR NR NR NR
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 8.8 <100 <100 NR <100
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 139 <0.15 <0.30 <0.13 0.17 J <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.65 <0.64 <0.73 <1.5 <0.65 <0.50 <0.54 <0.50 <0.50 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.16 J <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 11.0 0.27 J <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 1.0 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/14 0.76 <0.10 <0.10 <0.20 2.2 1.8 2.1 <0.10 <0.10 NR NR NR NR NR
09/30/14 2.5 0.15 J <0.10 1.3 J 2.0 4.2 1.7 <0.10 0.10 J NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 0.72 <0.12 0.64 <0.14 <0.14 NR NR NR NR NR
12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-16
MW-15
MW-12
MW-13
MW-9
MW-14
MW-8
MW-10
MW-11
Page 2 of 4
EPA
Method
6010B/
3030C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 400 400 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE1,2,4 -TrimethylbenzeneFacility ID# 0-0013895Date: 04/14/15
Analytical Method
→
GCL (µg/l)
MADEP Methods EPH & VPH
C19-C36 Aliphatics2L Standard (µg/l)EthylbenzeneTolueneLeadC9-C22 AromaticsBenzeneContaminant of Concern
→XylenesC9-C18 AliphaticsTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
PEELE'S SERVICE STATION (INCIDENT NO. 10000)C5-C8 AliphaticsEPA Method 6200B
1,3,5 -TrimethylbenzeneIPEMTBENaphthalene03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 1.45 <5 NR NR NR NR NR NR NR
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 <0.13 <0.15 0.36 J <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.16 J <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/01/07 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 NR NR NR NR NR NR NR
08/13/07 <1.0 <1.0 <1.0 <3.0 1.34 <1.0 <5 NR NR NR NR NR NR NR
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 <2.0 <100 <200 <100 <200
08/25/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 0.21 J <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/01/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/01/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5.0 NR NR NR NR NR NR NR
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
WSW-1
WSW-3
MW-17
MW-18
WSW-5
WSW-2
WSW-7
WSW-6
Page 3 of 4
EPA
Method
6010B/
3030C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 70 400 400 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 70,000 28,500 25,000 15,000 NE NE NE NE1,2,4 -TrimethylbenzeneFacility ID# 0-0013895Date: 04/14/15
Analytical Method
→
GCL (µg/l)
MADEP Methods EPH & VPH
C19-C36 Aliphatics2L Standard (µg/l)EthylbenzeneTolueneLeadC9-C22 AromaticsBenzeneContaminant of Concern
→XylenesC9-C18 AliphaticsTABLE 2
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
PEELE'S SERVICE STATION (INCIDENT NO. 10000)C5-C8 AliphaticsEPA Method 6200B
1,3,5 -TrimethylbenzeneIPEMTBENaphthalene03/01/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/13/07 <1.0 <1.0 <1.0 <3.0 <1.0 <1.0 <5 NR NR NR NR NR NR NR
03/12/09 <0.60 <0.70 <0.50 <1.0 <0.50 <0.60 <1.0 <0.70 <0.50 NR NR NR NR NR
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
03/01/07 <0.500 <0.500 <0.500 <1.500 <0.500 <5.00 <0.500 NR <0.500 NR NR NR NR NR
08/13/07 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
03/12/09 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
06/13/12 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/02/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/02/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
08/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <1.67 <0.330 <0.330 NR NR NR NR NR
12/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
06/13/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.11 <0.10 <0.10 NR NR NR NR NR
03/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
10/02/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 NR NR NR NR NR
04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
09/30/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
WSW-62 04/02/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR
Trip Blank 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR NR
Notes:
• Results reported in µg/L (micrograms per liter).
• NS: Not sampled; well dry, insufficient water to sample or not located.
• NE: Standard not established.
• The concentration of trichloroethylene reported in WSW-56 exceeded the MAC on April 1, 2015.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
• Concentrations in bold face type exceeded the 2L standard.
• I or J: Estimated value between the MDL and PQL .
• NR : Analysis not requested.
• < : Less than the method detection limit specified in the laboratory report.
• GCL : Gross contamination level as specified in T15A NCAC 2L.0202.
WSW-55
• 2L Standard : Maximum allowable concentrations as specified in T15A NCAC 2L.0202.
WSW-8
WSW-41/ DW-3
WSW-56
Page 4 of 4

APPENDIX

APPENDIX A
Laboratory Report – Ground Water Samples
04/13/15
Technical Report for
GRI (Geological Resources Inc.)
Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
2516
Accutest Job Number: FA23295
Sampling Date: 04/01/15
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail];
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
04/13/15
e-Hardcopy 2.0
Automated Report
66
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 66
FA23295
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................8
3.1: FA23295-1: MW-1 ........................................................................................................9
3.2: FA23295-2: MW-2R .....................................................................................................11
3.3: FA23295-3: MW-4 ........................................................................................................13
3.4: FA23295-4: MW-5 ........................................................................................................15
3.5: FA23295-5: MW-8 ........................................................................................................17
3.6: FA23295-6: MW-10 ......................................................................................................19
3.7: FA23295-7: MW-11 ......................................................................................................21
3.8: FA23295-8: MW-14 ......................................................................................................23
3.9: FA23295-9: MW-15 ......................................................................................................25
3.10: FA23295-10: MW-18 ..................................................................................................27
3.11: FA23295-11: WSW-2 ..................................................................................................29
3.12: FA23295-12: WSW-6 .................................................................................................31
3.13: FA23295-13: WSW-7 .................................................................................................33
3.14: FA23295-14: WSW-8 .................................................................................................35
3.15: FA23295-15: WSW-41 ...............................................................................................37
3.16: FA23295-16: WSW-56 ...............................................................................................39
3.17: FA23295-17: TRIP BLANK .......................................................................................41
Section 4: Misc. Forms ............................................................................................................43
4.1: Chain of Custody ...........................................................................................................44
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................48
5.1: Method Blank Summary ................................................................................................49
5.2: Blank Spike Summary ...................................................................................................55
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................61 123452 of 66
FA23295
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA23295
Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Project No: 2516
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA23295-1 04/01/15 09:39 HMJ 04/02/15 AQ Ground Water MW-1
FA23295-2 04/01/15 09:33 HMJ 04/02/15 AQ Ground Water MW-2R
FA23295-3 04/01/15 09:26 HMJ 04/02/15 AQ Ground Water MW-4
FA23295-4 04/01/15 09:44 HMJ 04/02/15 AQ Ground Water MW-5
FA23295-5 04/01/15 09:21 HMJ 04/02/15 AQ Ground Water MW-8
FA23295-6 04/01/15 09:14 HMJ 04/02/15 AQ Ground Water MW-10
FA23295-7 04/01/15 09:12 HMJ 04/02/15 AQ Ground Water MW-11
FA23295-8 04/01/15 09:55 HMJ 04/02/15 AQ Ground Water MW-14
FA23295-9 04/01/15 10:01 HMJ 04/02/15 AQ Ground Water MW-15
FA23295-10 04/01/15 10:10 HMJ 04/02/15 AQ Ground Water MW-18
FA23295-11 04/01/15 10:36 HMJ 04/02/15 AQ Ground Water WSW-2
FA23295-12 04/01/15 10:28 HMJ 04/02/15 AQ Ground Water WSW-6
FA23295-13 04/01/15 10:32 HMJ 04/02/15 AQ Ground Water WSW-7
3 of 66
FA23295 1
Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA23295
Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Project No: 2516
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA23295-14 04/01/15 10:22 HMJ 04/02/15 AQ Ground Water WSW-8
FA23295-15 04/01/15 10:13 HMJ 04/02/15 AQ Ground Water WSW-41
FA23295-16 04/01/15 10:18 HMJ 04/02/15 AQ Ground Water WSW-56
FA23295-17 04/01/15 00:00 HMJ 04/02/15 AQ Trip Blank Water TRIP BLANK
4 of 66
FA23295 1
Summary of Hits Page 1 of 3
Job Number:FA23295
Account:GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Collected:04/01/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA23295-1 MW-1
Ethylbenzene 0.29 J 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 0.13 J 0.50 0.12 ug/l SM 6200B
Methyl Chloride 0.20 J 0.50 0.16 ug/l SM 6200B
Naphthalene 3.3 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 0.23 J 0.50 0.16 ug/l SM 6200B
1,2,4-Trimethylbenzene 6.6 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.70 0.50 0.14 ug/l SM 6200B
m,p-Xylene 3.5 1.0 0.30 ug/l SM 6200B
o-Xylene 3.7 0.50 0.13 ug/l SM 6200B
Xylene (total)7.1 1.5 0.43 ug/l SM 6200B
FA23295-2 MW-2R
Benzene 26.2 13 4.3 ug/l SM 6200B
n-Butylbenzene 8.8 J 13 3.6 ug/l SM 6200B
sec-Butylbenzene 4.9 J 13 3.5 ug/l SM 6200B
Ethylbenzene 88.6 13 3.8 ug/l SM 6200B
Isopropylbenzene 6.8 J 13 3.0 ug/l SM 6200B
p-Isopropyltoluene 5.5 J 13 3.1 ug/l SM 6200B
Naphthalene 109 13 3.1 ug/l SM 6200B
n-Propylbenzene 19.6 13 3.9 ug/l SM 6200B
Toluene 399 13 4.2 ug/l SM 6200B
1,2,4-Trimethylbenzene 641 13 3.4 ug/l SM 6200B
1,3,5-Trimethylbenzene 201 13 3.4 ug/l SM 6200B
m,p-Xylene 1130 25 7.4 ug/l SM 6200B
o-Xylene 592 13 3.3 ug/l SM 6200B
Xylene (total)1720 38 11 ug/l SM 6200B
FA23295-3 MW-4
No hits reported in this sample.
FA23295-4 MW-5
Tetrachloroethylene 0.22 J 0.50 0.15 ug/l SM 6200B
FA23295-5 MW-8
No hits reported in this sample.
FA23295-6 MW-10
No hits reported in this sample.
5 of 66
FA23295 2
Summary of Hits Page 2 of 3
Job Number:FA23295
Account:GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Collected:04/01/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA23295-7 MW-11
Benzene 1.9 J 2.5 0.86 ug/l SM 6200B
n-Butylbenzene 3.1 2.5 0.72 ug/l SM 6200B
sec-Butylbenzene 3.1 2.5 0.69 ug/l SM 6200B
Ethylbenzene 28.2 2.5 0.76 ug/l SM 6200B
Isopropylbenzene 11.9 2.5 0.59 ug/l SM 6200B
p-Isopropyltoluene 2.2 J 2.5 0.61 ug/l SM 6200B
Naphthalene 87.0 2.5 0.61 ug/l SM 6200B
n-Propylbenzene 29.5 2.5 0.78 ug/l SM 6200B
Toluene 1.1 J 2.5 0.83 ug/l SM 6200B
1,2,4-Trimethylbenzene 191 2.5 0.68 ug/l SM 6200B
1,3,5-Trimethylbenzene 29.2 2.5 0.68 ug/l SM 6200B
m,p-Xylene 144 5.0 1.5 ug/l SM 6200B
o-Xylene 65.2 2.5 0.67 ug/l SM 6200B
Xylene (total)210 7.5 2.2 ug/l SM 6200B
FA23295-8 MW-14
Di-Isopropyl Ether 0.64 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 0.72 0.50 0.16 ug/l SM 6200B
FA23295-9 MW-15
No hits reported in this sample.
FA23295-10 MW-18
No hits reported in this sample.
FA23295-11 WSW-2
No hits reported in this sample.
FA23295-12 WSW-6
No hits reported in this sample.
FA23295-13 WSW-7
No hits reported in this sample.
6 of 66
FA23295 2
Summary of Hits Page 3 of 3
Job Number:FA23295
Account:GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Collected:04/01/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA23295-14 WSW-8
Trichloroethylene 0.39 J 0.50 0.15 ug/l SM 6200B
FA23295-15 WSW-41
Trichloroethylene 0.43 J 0.50 0.15 ug/l SM 6200B
FA23295-16 WSW-56
Trichloroethylene 3.4 0.50 0.15 ug/l SM 6200B
FA23295-17 TRIP BLANK
No hits reported in this sample.
7 of 66
FA23295 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
8 of 66
FA23295 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA23295-1 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193687.D 1 04/08/15 TD n/a n/a VA1682
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 66
FA23295 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA23295-1 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 0.29 0.50 0.15 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 0.13 0.50 0.12 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.20 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 3.3 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 0.23 0.50 0.16 ug/l J
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 6.6 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.70 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 3.5 1.0 0.30 ug/l
95-47-6 o-Xylene 3.7 0.50 0.13 ug/l
1330-20-7 Xylene (total)7.1 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%70-130%
2037-26-5 Toluene-D8 91%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 66
FA23295 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA23295-2 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193688.D 25 04/08/15 TD n/a n/a VA1682
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 26.2 13 4.3 ug/l
108-86-1 Bromobenzene ND 13 4.0 ug/l
74-97-5 Bromochloromethane ND 13 4.0 ug/l
75-27-4 Bromodichloromethane ND 13 3.7 ug/l
75-25-2 Bromoform ND 13 2.7 ug/l
104-51-8 n-Butylbenzene 8.8 13 3.6 ug/l J
135-98-8 sec-Butylbenzene 4.9 13 3.5 ug/l J
98-06-6 tert-Butylbenzene ND 13 3.6 ug/l
56-23-5 Carbon Tetrachloride ND 13 3.8 ug/l
108-90-7 Chlorobenzene ND 13 4.0 ug/l
75-00-3 Chloroethane ND 13 5.2 ug/l
67-66-3 Chloroform ND 13 4.3 ug/l
95-49-8 o-Chlorotoluene ND 13 3.8 ug/l
106-43-4 p-Chlorotoluene ND 13 3.4 ug/l
124-48-1 Dibromochloromethane ND 13 3.1 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 13 4.9 ug/l
106-93-4 1,2-Dibromoethane ND 13 3.5 ug/l
75-71-8 Dichlorodifluoromethane ND 13 3.2 ug/l
95-50-1 1,2-Dichlorobenzene ND 13 3.2 ug/l
541-73-1 1,3-Dichlorobenzene ND 13 3.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 13 3.8 ug/l
75-34-3 1,1-Dichloroethane ND 13 4.5 ug/l
107-06-2 1,2-Dichloroethane ND 13 4.1 ug/l
75-35-4 1,1-Dichloroethylene ND 13 4.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 13 4.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 13 4.2 ug/l
78-87-5 1,2-Dichloropropane ND 13 4.3 ug/l
142-28-9 1,3-Dichloropropane ND 13 3.7 ug/l
594-20-7 2,2-Dichloropropane ND 13 3.0 ug/l
563-58-6 1,1-Dichloropropene ND 13 4.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 13 3.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 13 3.2 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 66
FA23295 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA23295-2 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 13 4.0 ug/l
100-41-4 Ethylbenzene 88.6 13 3.8 ug/l
87-68-3 Hexachlorobutadiene ND 13 3.1 ug/l
98-82-8 Isopropylbenzene 6.8 13 3.0 ug/l J
99-87-6 p-Isopropyltoluene 5.5 13 3.1 ug/l J
74-83-9 Methyl Bromide ND 13 4.6 ug/l
74-87-3 Methyl Chloride ND 13 4.0 ug/l
74-95-3 Methylene Bromide ND 13 4.3 ug/l
75-09-2 Methylene Chloride ND 50 25 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 13 4.1 ug/l
91-20-3 Naphthalene 109 13 3.1 ug/l
103-65-1 n-Propylbenzene 19.6 13 3.9 ug/l
100-42-5 Styrene ND 13 3.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 13 3.1 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 13 3.6 ug/l
127-18-4 Tetrachloroethylene ND 13 3.7 ug/l
108-88-3 Toluene 399 13 4.2 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 13 3.4 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 13 3.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 13 4.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 13 3.5 ug/l
79-01-6 Trichloroethylene ND 13 3.7 ug/l
75-69-4 Trichlorofluoromethane ND 13 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 13 3.2 ug/l
95-63-6 1,2,4-Trimethylbenzene 641 13 3.4 ug/l
108-67-8 1,3,5-Trimethylbenzene 201 13 3.4 ug/l
75-01-4 Vinyl Chloride ND 13 3.3 ug/l
m,p-Xylene 1130 25 7.4 ug/l
95-47-6 o-Xylene 592 13 3.3 ug/l
1330-20-7 Xylene (total)1720 38 11 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 66
FA23295 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:FA23295-3 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193689.D 1 04/08/15 TD n/a n/a VA1682
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 66
FA23295 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-4
Lab Sample ID:FA23295-3 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 115%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 66
FA23295 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA23295-4 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193698.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 66
FA23295 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA23295-4 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene 0.22 0.50 0.15 ug/l J
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 90%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 66
FA23295 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA23295-5 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193699.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 66
FA23295 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA23295-5 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 66
FA23295 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA23295-6 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193700.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 66
FA23295 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA23295-6 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 66
FA23295 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA23295-7 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193701.D 5 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.9 2.5 0.86 ug/l J
108-86-1 Bromobenzene ND 2.5 0.80 ug/l
74-97-5 Bromochloromethane ND 2.5 0.80 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.74 ug/l
75-25-2 Bromoform ND 2.5 0.55 ug/l
104-51-8 n-Butylbenzene 3.1 2.5 0.72 ug/l
135-98-8 sec-Butylbenzene 3.1 2.5 0.69 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.73 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.77 ug/l
108-90-7 Chlorobenzene ND 2.5 0.79 ug/l
75-00-3 Chloroethane ND 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.86 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.76 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.69 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.62 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 0.99 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.71 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 0.65 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.65 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.70 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.76 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.91 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.82 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.85 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.90 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.85 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.87 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.73 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.61 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.79 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.66 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 66
FA23295 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA23295-7 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 2.5 0.80 ug/l
100-41-4 Ethylbenzene 28.2 2.5 0.76 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.61 ug/l
98-82-8 Isopropylbenzene 11.9 2.5 0.59 ug/l
99-87-6 p-Isopropyltoluene 2.2 2.5 0.61 ug/l J
74-83-9 Methyl Bromide ND 2.5 0.91 ug/l
74-87-3 Methyl Chloride ND 2.5 0.79 ug/l
74-95-3 Methylene Bromide ND 2.5 0.85 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.5 0.82 ug/l
91-20-3 Naphthalene 87.0 2.5 0.61 ug/l
103-65-1 n-Propylbenzene 29.5 2.5 0.78 ug/l
100-42-5 Styrene ND 2.5 0.60 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.71 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.74 ug/l
108-88-3 Toluene 1.1 2.5 0.83 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.68 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.65 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.81 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.70 ug/l
79-01-6 Trichloroethylene ND 2.5 0.73 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 0.81 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.64 ug/l
95-63-6 1,2,4-Trimethylbenzene 191 2.5 0.68 ug/l
108-67-8 1,3,5-Trimethylbenzene 29.2 2.5 0.68 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.65 ug/l
m,p-Xylene 144 5.0 1.5 ug/l
95-47-6 o-Xylene 65.2 2.5 0.67 ug/l
1330-20-7 Xylene (total)210 7.5 2.2 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 66
FA23295 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA23295-8 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193702.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 66
FA23295 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA23295-8 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.64 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.72 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 66
FA23295 33.8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-15
Lab Sample ID:FA23295-9 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193703.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 66
FA23295 33.9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-15
Lab Sample ID:FA23295-9 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 66
FA23295 33.9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-18
Lab Sample ID:FA23295-10 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193704.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 66
FA23295 33.10
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-18
Lab Sample ID:FA23295-10 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 117%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 66
FA23295 33.10
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-2
Lab Sample ID:FA23295-11 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193705.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 66
FA23295 33.11
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-2
Lab Sample ID:FA23295-11 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 109%70-130%
17060-07-0 1,2-Dichloroethane-D4 119%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 66
FA23295 33.11
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-6
Lab Sample ID:FA23295-12 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193706.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 66
FA23295 33.12
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-6
Lab Sample ID:FA23295-12 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 109%70-130%
17060-07-0 1,2-Dichloroethane-D4 120%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 66
FA23295 33.12
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-7
Lab Sample ID:FA23295-13 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193709.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 66
FA23295 33.13
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-7
Lab Sample ID:FA23295-13 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 117%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 66
FA23295 33.13
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-8
Lab Sample ID:FA23295-14 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193710.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 66
FA23295 33.14
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-8
Lab Sample ID:FA23295-14 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene 0.39 0.50 0.15 ug/l J
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 120%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 66
FA23295 33.14
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-41
Lab Sample ID:FA23295-15 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193711.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 66
FA23295 33.15
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-41
Lab Sample ID:FA23295-15 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene 0.43 0.50 0.15 ug/l J
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 109%70-130%
17060-07-0 1,2-Dichloroethane-D4 121%70-130%
2037-26-5 Toluene-D8 93%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 66
FA23295 33.15
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-56
Lab Sample ID:FA23295-16 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193712.D 1 04/09/15 TD n/a n/a VA1683
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 66
FA23295 33.16
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-56
Lab Sample ID:FA23295-16 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene 3.4 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 113%70-130%
17060-07-0 1,2-Dichloroethane-D4 119%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 66
FA23295 33.16
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA23295-17 Date Sampled:04/01/15
Matrix:AQ - Trip Blank Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193728.D 1 04/09/15 TD n/a n/a VA1684
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 66
FA23295 33.17
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA23295-17 Date Sampled:04/01/15
Matrix:AQ - Trip Blank Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 66
FA23295 33.17
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
43 of 66
FA23295 4
FA23295: Chain of Custody
Page 1 of 4
44 of 66
FA23295 44.1
FA23295: Chain of Custody
Page 2 of 4
45 of 66
FA23295 44.1
FA23295: Chain of Custody
Page 3 of 4
46 of 66
FA23295 44.1
FA23295: Chain of Custody
Page 4 of 4
47 of 66
FA23295 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
48 of 66
FA23295 5
Method Blank Summary Page 1 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1682-MB A0193680.D 1 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-1, FA23295-2, FA23295-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
49 of 66
FA23295 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1682-MB A0193680.D 1 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-1, FA23295-2, FA23295-3
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
50 of 66
FA23295 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1683-MB A0193697.D 1 04/09/15 TD n/a n/a VA1683
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-4, FA23295-5, FA23295-6, FA23295-7, FA23295-8, FA23295-9, FA23295-10, FA23295-11, FA23295-12,
FA23295-13, FA23295-14, FA23295-15, FA23295-16
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
51 of 66
FA23295 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1683-MB A0193697.D 1 04/09/15 TD n/a n/a VA1683
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-4, FA23295-5, FA23295-6, FA23295-7, FA23295-8, FA23295-9, FA23295-10, FA23295-11, FA23295-12,
FA23295-13, FA23295-14, FA23295-15, FA23295-16
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
52 of 66
FA23295 55.1.2
Method Blank Summary Page 1 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1684-MB A0193727.D 1 04/09/15 TD n/a n/a VA1684
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-17
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
53 of 66
FA23295 55.1.3
Method Blank Summary Page 2 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1684-MB A0193727.D 1 04/09/15 TD n/a n/a VA1684
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-17
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
54 of 66
FA23295 55.1.3
Blank Spike Summary Page 1 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1682-BS A0193679.D 1 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-1, FA23295-2, FA23295-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.0 110 70-130
108-86-1 Bromobenzene 10 10.9 109 70-130
74-97-5 Bromochloromethane 10 11.1 111 70-130
75-27-4 Bromodichloromethane 10 11.5 115 70-130
75-25-2 Bromoform 10 10.9 109 70-130
104-51-8 n-Butylbenzene 10 11.5 115 70-130
135-98-8 sec-Butylbenzene 10 12.5 125 70-130
98-06-6 tert-Butylbenzene 10 12.4 124 70-130
56-23-5 Carbon Tetrachloride 10 12.1 121 70-130
108-90-7 Chlorobenzene 10 12.4 124 70-130
75-00-3 Chloroethane 10 7.7 77 60-140
67-66-3 Chloroform 10 11.2 112 70-130
95-49-8 o-Chlorotoluene 10 11.8 118 70-130
106-43-4 p-Chlorotoluene 10 12.1 121 70-130
124-48-1 Dibromochloromethane 10 11.3 113 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.8 98 70-130
106-93-4 1,2-Dibromoethane 10 11.0 110 70-130
75-71-8 Dichlorodifluoromethane 10 8.5 85 60-140
95-50-1 1,2-Dichlorobenzene 10 11.4 114 70-130
541-73-1 1,3-Dichlorobenzene 10 11.9 119 70-130
106-46-7 1,4-Dichlorobenzene 10 10.8 108 70-130
75-34-3 1,1-Dichloroethane 10 11.1 111 70-130
107-06-2 1,2-Dichloroethane 10 11.6 116 70-130
75-35-4 1,1-Dichloroethylene 10 12.5 125 70-130
156-59-2 cis-1,2-Dichloroethylene 10 11.1 111 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.4 114 70-130
78-87-5 1,2-Dichloropropane 10 11.1 111 70-130
142-28-9 1,3-Dichloropropane 10 10.8 108 70-130
594-20-7 2,2-Dichloropropane 10 11.7 117 70-130
563-58-6 1,1-Dichloropropene 10 12.4 124 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.0 110 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.9 119 70-130
108-20-3 Di-Isopropyl Ether 10 11.7 117 70-130
100-41-4 Ethylbenzene 10 11.2 112 70-130
87-68-3 Hexachlorobutadiene 10 10.7 107 70-130
98-82-8 Isopropylbenzene 10 12.6 126 70-130
* = Outside of Control Limits.
55 of 66
FA23295 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1682-BS A0193679.D 1 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-1, FA23295-2, FA23295-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 12.4 124 70-130
74-83-9 Methyl Bromide 10 8.3 83 60-140
74-87-3 Methyl Chloride 10 8.5 85 60-140
74-95-3 Methylene Bromide 10 10.9 109 70-130
75-09-2 Methylene Chloride 10 12.9 129 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.5 115 70-130
91-20-3 Naphthalene 10 10.2 102 70-130
103-65-1 n-Propylbenzene 10 12.4 124 70-130
100-42-5 Styrene 10 11.6 116 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.5 115 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.2 102 70-130
127-18-4 Tetrachloroethylene 10 11.4 114 70-130
108-88-3 Toluene 10 11.5 115 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.1 111 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.4 104 70-130
71-55-6 1,1,1-Trichloroethane 10 11.6 116 70-130
79-00-5 1,1,2-Trichloroethane 10 10.9 109 70-130
79-01-6 Trichloroethylene 10 11.9 119 70-130
75-69-4 Trichlorofluoromethane 10 7.2 72 60-140
96-18-4 1,2,3-Trichloropropane 10 10.3 103 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.2 112 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.2 112 70-130
75-01-4 Vinyl Chloride 10 8.3 83 60-140
m,p-Xylene 20 23.4 117 70-130
95-47-6 o-Xylene 10 12.3 123 70-130
1330-20-7 Xylene (total)30 35.6 119 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
56 of 66
FA23295 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1683-BS A0193695.D 1 04/08/15 TD n/a n/a VA1683
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-4, FA23295-5, FA23295-6, FA23295-7, FA23295-8, FA23295-9, FA23295-10, FA23295-11, FA23295-12,
FA23295-13, FA23295-14, FA23295-15, FA23295-16
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.3 103 70-130
108-86-1 Bromobenzene 10 10.4 104 70-130
74-97-5 Bromochloromethane 10 10.5 105 70-130
75-27-4 Bromodichloromethane 10 10.6 106 70-130
75-25-2 Bromoform 10 10.0 100 70-130
104-51-8 n-Butylbenzene 10 10.8 108 70-130
135-98-8 sec-Butylbenzene 10 11.9 119 70-130
98-06-6 tert-Butylbenzene 10 11.8 118 70-130
56-23-5 Carbon Tetrachloride 10 11.2 112 70-130
108-90-7 Chlorobenzene 10 11.7 117 70-130
75-00-3 Chloroethane 10 11.1 111 60-140
67-66-3 Chloroform 10 10.4 104 70-130
95-49-8 o-Chlorotoluene 10 11.3 113 70-130
106-43-4 p-Chlorotoluene 10 11.5 115 70-130
124-48-1 Dibromochloromethane 10 10.5 105 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.2 92 70-130
106-93-4 1,2-Dibromoethane 10 10.3 103 70-130
75-71-8 Dichlorodifluoromethane 10 11.6 116 60-140
95-50-1 1,2-Dichlorobenzene 10 11.0 110 70-130
541-73-1 1,3-Dichlorobenzene 10 11.3 113 70-130
106-46-7 1,4-Dichlorobenzene 10 10.2 102 70-130
75-34-3 1,1-Dichloroethane 10 10.3 103 70-130
107-06-2 1,2-Dichloroethane 10 10.8 108 70-130
75-35-4 1,1-Dichloroethylene 10 11.9 119 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.5 105 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.5 105 70-130
78-87-5 1,2-Dichloropropane 10 10.3 103 70-130
142-28-9 1,3-Dichloropropane 10 10.1 101 70-130
594-20-7 2,2-Dichloropropane 10 9.3 93 70-130
563-58-6 1,1-Dichloropropene 10 11.3 113 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.9 99 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.7 107 70-130
108-20-3 Di-Isopropyl Ether 10 10.9 109 70-130
100-41-4 Ethylbenzene 10 10.6 106 70-130
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
98-82-8 Isopropylbenzene 10 11.9 119 70-130
* = Outside of Control Limits.
57 of 66
FA23295 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1683-BS A0193695.D 1 04/08/15 TD n/a n/a VA1683
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-4, FA23295-5, FA23295-6, FA23295-7, FA23295-8, FA23295-9, FA23295-10, FA23295-11, FA23295-12,
FA23295-13, FA23295-14, FA23295-15, FA23295-16
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.7 117 70-130
74-83-9 Methyl Bromide 10 11.9 119 60-140
74-87-3 Methyl Chloride 10 12.4 124 60-140
74-95-3 Methylene Bromide 10 10.4 104 70-130
75-09-2 Methylene Chloride 10 10.8 108 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.0 110 70-130
91-20-3 Naphthalene 10 9.5 95 70-130
103-65-1 n-Propylbenzene 10 11.9 119 70-130
100-42-5 Styrene 10 10.8 108 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.7 107 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.1 91 70-130
127-18-4 Tetrachloroethylene 10 10.8 108 70-130
108-88-3 Toluene 10 10.8 108 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.5 105 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.9 99 70-130
71-55-6 1,1,1-Trichloroethane 10 10.9 109 70-130
79-00-5 1,1,2-Trichloroethane 10 10.2 102 70-130
79-01-6 Trichloroethylene 10 11.5 115 70-130
75-69-4 Trichlorofluoromethane 10 10.4 104 60-140
96-18-4 1,2,3-Trichloropropane 10 10.2 102 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.6 106 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.6 106 70-130
75-01-4 Vinyl Chloride 10 11.8 118 60-140
m,p-Xylene 20 22.1 111 70-130
95-47-6 o-Xylene 10 11.5 115 70-130
1330-20-7 Xylene (total)30 33.6 112 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
58 of 66
FA23295 55.2.2
Blank Spike Summary Page 1 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1684-BS A0193725.D 1 04/09/15 TD n/a n/a VA1684
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-17
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.9 99 70-130
108-86-1 Bromobenzene 10 10 100 70-130
74-97-5 Bromochloromethane 10 9.9 99 70-130
75-27-4 Bromodichloromethane 10 10.0 100 70-130
75-25-2 Bromoform 10 9.4 94 70-130
104-51-8 n-Butylbenzene 10 10.5 105 70-130
135-98-8 sec-Butylbenzene 10 11.4 114 70-130
98-06-6 tert-Butylbenzene 10 11.0 110 70-130
56-23-5 Carbon Tetrachloride 10 10.1 101 70-130
108-90-7 Chlorobenzene 10 11.2 112 70-130
75-00-3 Chloroethane 10 11.0 110 60-140
67-66-3 Chloroform 10 9.7 97 70-130
95-49-8 o-Chlorotoluene 10 10.8 108 70-130
106-43-4 p-Chlorotoluene 10 11.0 110 70-130
124-48-1 Dibromochloromethane 10 9.9 99 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.7 87 70-130
106-93-4 1,2-Dibromoethane 10 9.9 99 70-130
75-71-8 Dichlorodifluoromethane 10 9.2 92 60-140
95-50-1 1,2-Dichlorobenzene 10 10.6 106 70-130
541-73-1 1,3-Dichlorobenzene 10 10.9 109 70-130
106-46-7 1,4-Dichlorobenzene 10 9.9 99 70-130
75-34-3 1,1-Dichloroethane 10 9.8 98 70-130
107-06-2 1,2-Dichloroethane 10 9.8 98 70-130
75-35-4 1,1-Dichloroethylene 10 10.8 108 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.1 101 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.9 99 70-130
78-87-5 1,2-Dichloropropane 10 10.0 100 70-130
142-28-9 1,3-Dichloropropane 10 9.7 97 70-130
594-20-7 2,2-Dichloropropane 10 10.4 104 70-130
563-58-6 1,1-Dichloropropene 10 10.6 106 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.9 99 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.5 105 70-130
108-20-3 Di-Isopropyl Ether 10 10.3 103 70-130
100-41-4 Ethylbenzene 10 10.1 101 70-130
87-68-3 Hexachlorobutadiene 10 10.2 102 70-130
98-82-8 Isopropylbenzene 10 11.1 111 70-130
* = Outside of Control Limits.
59 of 66
FA23295 55.2.3
Blank Spike Summary Page 2 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1684-BS A0193725.D 1 04/09/15 TD n/a n/a VA1684
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-17
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.2 112 70-130
74-83-9 Methyl Bromide 10 11.7 117 60-140
74-87-3 Methyl Chloride 10 11.2 112 60-140
74-95-3 Methylene Bromide 10 9.6 96 70-130
75-09-2 Methylene Chloride 10 10.3 103 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.5 105 70-130
91-20-3 Naphthalene 10 9.6 96 70-130
103-65-1 n-Propylbenzene 10 11.5 115 70-130
100-42-5 Styrene 10 10.4 104 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.0 100 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.8 98 70-130
127-18-4 Tetrachloroethylene 10 10.1 101 70-130
108-88-3 Toluene 10 10.4 104 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.4 104 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.7 97 70-130
71-55-6 1,1,1-Trichloroethane 10 10 100 70-130
79-00-5 1,1,2-Trichloroethane 10 9.8 98 70-130
79-01-6 Trichloroethylene 10 10.2 102 70-130
75-69-4 Trichlorofluoromethane 10 9.5 95 60-140
96-18-4 1,2,3-Trichloropropane 10 9.7 97 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.2 102 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.2 102 70-130
75-01-4 Vinyl Chloride 10 11.1 111 60-140
m,p-Xylene 20 20.8 104 70-130
95-47-6 o-Xylene 10 10.9 109 70-130
1330-20-7 Xylene (total)30 31.7 106 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
60 of 66
FA23295 55.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA23295-2MS A0193690.D 25 04/08/15 TD n/a n/a VA1682
FA23295-2MSD A0193691.D 25 04/08/15 TD n/a n/a VA1682
FA23295-2 A0193688.D 25 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-1, FA23295-2, FA23295-3
FA23295-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 26.2 250 266 96 250 275 100 3 70-130/20
108-86-1 Bromobenzene ND 250 232 93 250 242 97 4 70-130/20
74-97-5 Bromochloromethane ND 250 255 102 250 257 103 1 70-130/20
75-27-4 Bromodichloromethane ND 250 261 104 250 223 89 16 70-130/20
75-25-2 Bromoform ND 250 207 83 250 175 70 17 70-130/20
104-51-8 n-Butylbenzene 8.8 J 250 255 98 250 268 104 5 70-130/20
135-98-8 sec-Butylbenzene 4.9 J 250 270 106 250 286 112 6 70-130/20
98-06-6 tert-Butylbenzene ND 250 268 107 250 278 111 4 70-130/20
56-23-5 Carbon Tetrachloride ND 250 279 112 250 234 94 18 70-130/20
108-90-7 Chlorobenzene ND 250 272 109 250 278 111 2 70-130/20
75-00-3 Chloroethane ND 250 276 110 250 293 117 6 60-140/20
67-66-3 Chloroform ND 250 258 103 250 259 104 0 70-130/20
95-49-8 o-Chlorotoluene ND 250 279 112 250 289 116 4 70-130/20
106-43-4 p-Chlorotoluene ND 250 259 104 250 271 108 5 70-130/20
124-48-1 Dibromochloromethane ND 250 232 93 250 200 80 15 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 250 257 103 250 250 100 3 70-130/20
106-93-4 1,2-Dibromoethane ND 250 240 96 250 249 100 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 250 320 128 250 310 124 3 60-140/20
95-50-1 1,2-Dichlorobenzene ND 250 253 101 250 262 105 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 250 259 104 250 266 106 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 250 236 94 250 239 96 1 70-130/20
75-34-3 1,1-Dichloroethane ND 250 248 99 250 253 101 2 70-130/20
107-06-2 1,2-Dichloroethane ND 250 279 112 250 273 109 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 250 283 113 250 291 116 3 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 250 244 98 250 248 99 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 250 254 102 250 247 99 3 70-130/20
78-87-5 1,2-Dichloropropane ND 250 247 99 250 254 102 3 70-130/20
142-28-9 1,3-Dichloropropane ND 250 231 92 250 245 98 6 70-130/20
594-20-7 2,2-Dichloropropane ND 250 251 100 250 242 97 4 70-130/20
563-58-6 1,1-Dichloropropene ND 250 268 107 250 269 108 0 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 250 233 93 250 202 81 14 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 250 248 99 250 217 87 13 70-130/20
108-20-3 Di-Isopropyl Ether ND 250 267 107 250 272 109 2 70-130/20
100-41-4 Ethylbenzene 88.6 250 336 99 250 348 104 4 70-130/20
87-68-3 Hexachlorobutadiene ND 250 236 94 250 239 96 1 70-130/20
98-82-8 Isopropylbenzene 6.8 J 250 284 111 250 295 115 4 70-130/20
* = Outside of Control Limits.
61 of 66
FA23295 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA23295-2MS A0193690.D 25 04/08/15 TD n/a n/a VA1682
FA23295-2MSD A0193691.D 25 04/08/15 TD n/a n/a VA1682
FA23295-2 A0193688.D 25 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-1, FA23295-2, FA23295-3
FA23295-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 5.5 J 250 270 106 250 284 111 5 70-130/20
74-83-9 Methyl Bromide ND 250 295 118 250 306 122 4 60-140/20
74-87-3 Methyl Chloride ND 250 316 126 250 312 125 1 60-140/20
74-95-3 Methylene Bromide ND 250 256 102 250 255 102 0 70-130/20
75-09-2 Methylene Chloride ND 250 278 111 250 272 109 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 250 260 104 250 264 106 2 70-130/20
91-20-3 Naphthalene 109 250 341 93 250 352 97 3 70-130/20
103-65-1 n-Propylbenzene 19.6 250 283 105 250 299 112 5 70-130/20
100-42-5 Styrene ND 250 254 102 250 265 106 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 250 254 102 250 241 96 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 250 219 88 250 230 92 5 70-130/20
127-18-4 Tetrachloroethylene ND 250 243 97 250 252 101 4 70-130/20
108-88-3 Toluene 399 250 634 94 250 674 110 6 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 250 249 100 250 253 101 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 250 233 93 250 241 96 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 250 272 109 250 263 105 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 250 260 104 250 273 109 5 70-130/20
79-01-6 Trichloroethylene ND 250 262 105 250 257 103 2 70-130/20
75-69-4 Trichlorofluoromethane ND 250 278 111 250 272 109 2 60-140/20
96-18-4 1,2,3-Trichloropropane ND 250 237 95 250 242 97 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene 641 250 865 90 250 904 105 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 201 250 442 96 250 464 105 5 70-130/20
75-01-4 Vinyl Chloride ND 250 283 113 250 295 118 4 60-140/20
m,p-Xylene 1130 500 1630 100 500 1690 112 4 70-130/20
95-47-6 o-Xylene 592 250 862 108 250 897 122 4 70-130/20
1330-20-7 Xylene (total)1720 750 2490 103 750 2580 115 4 70-130/20
CAS No.Surrogate Recoveries MS MSD FA23295-2 Limits
1868-53-7 Dibromofluoromethane 109%104%106%70-130%
17060-07-0 1,2-Dichloroethane-D4 115%107%116%70-130%
2037-26-5 Toluene-D8 95%100%99%70-130%
460-00-4 4-Bromofluorobenzene 97%100%100%70-130%
* = Outside of Control Limits.
62 of 66
FA23295 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA23386-8MS A0193718.D 50 04/09/15 TD n/a n/a VA1683
FA23386-8MSD A0193719.D 50 04/09/15 TD n/a n/a VA1683
FA23386-8 a A0193715.D 50 04/09/15 TD n/a n/a VA1683
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-4, FA23295-5, FA23295-6, FA23295-7, FA23295-8, FA23295-9, FA23295-10, FA23295-11, FA23295-12,
FA23295-13, FA23295-14, FA23295-15, FA23295-16
FA23386-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 500 457 91 500 473 95 3 70-130/20
108-86-1 Bromobenzene ND 500 438 88 500 474 95 8 70-130/20
74-97-5 Bromochloromethane ND 500 495 99 500 503 101 2 70-130/20
75-27-4 Bromodichloromethane ND 500 531 106 500 504 101 5 70-130/20
75-25-2 Bromoform ND 500 469 94 500 429 86 9 70-130/20
104-51-8 n-Butylbenzene ND 500 419 84 500 456 91 8 70-130/20
135-98-8 sec-Butylbenzene ND 500 483 97 500 516 103 7 70-130/20
98-06-6 tert-Butylbenzene ND 500 497 99 500 531 106 7 70-130/20
56-23-5 Carbon Tetrachloride ND 500 578 116 500 535 107 8 70-130/20
108-90-7 Chlorobenzene ND 500 509 102 500 536 107 5 70-130/20
75-00-3 Chloroethane ND 500 567 113 500 569 114 0 60-140/20
67-66-3 Chloroform ND 500 527 105 500 531 106 1 70-130/20
95-49-8 o-Chlorotoluene ND 500 476 95 500 503 101 6 70-130/20
106-43-4 p-Chlorotoluene ND 500 479 96 500 509 102 6 70-130/20
124-48-1 Dibromochloromethane ND 500 479 96 500 449 90 6 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 500 422 84 500 420 84 0 70-130/20
106-93-4 1,2-Dibromoethane ND 500 453 91 500 461 92 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 500 665 133 500 684 137 3 60-140/20
95-50-1 1,2-Dichlorobenzene ND 500 472 94 500 499 100 6 70-130/20
541-73-1 1,3-Dichlorobenzene ND 500 484 97 500 517 103 7 70-130/20
106-46-7 1,4-Dichlorobenzene ND 500 445 89 500 469 94 5 70-130/20
75-34-3 1,1-Dichloroethane 24.9 J 500 510 97 500 525 100 3 70-130/20
107-06-2 1,2-Dichloroethane ND 500 598 120 500 596 119 0 70-130/20
75-35-4 1,1-Dichloroethylene 100 500 671 114 500 702 120 5 70-130/20
156-59-2 cis-1,2-Dichloroethylene 57.0 500 512 91 500 544 97 6 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 500 497 99 500 506 101 2 70-130/20
78-87-5 1,2-Dichloropropane ND 500 461 92 500 483 97 5 70-130/20
142-28-9 1,3-Dichloropropane ND 500 436 87 500 452 90 4 70-130/20
594-20-7 2,2-Dichloropropane ND 500 362 72 500 369 74 2 70-130/20
563-58-6 1,1-Dichloropropene ND 500 513 103 500 533 107 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 500 418 84 500 402 80 4 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 500 463 93 500 441 88 5 70-130/20
108-20-3 Di-Isopropyl Ether ND 500 515 103 500 538 108 4 70-130/20
100-41-4 Ethylbenzene ND 500 455 91 500 479 96 5 70-130/20
87-68-3 Hexachlorobutadiene ND 500 420 84 500 456 91 8 70-130/20
98-82-8 Isopropylbenzene ND 500 503 101 500 530 106 5 70-130/20
* = Outside of Control Limits.
63 of 66
FA23295 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA23386-8MS A0193718.D 50 04/09/15 TD n/a n/a VA1683
FA23386-8MSD A0193719.D 50 04/09/15 TD n/a n/a VA1683
FA23386-8 a A0193715.D 50 04/09/15 TD n/a n/a VA1683
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-4, FA23295-5, FA23295-6, FA23295-7, FA23295-8, FA23295-9, FA23295-10, FA23295-11, FA23295-12,
FA23295-13, FA23295-14, FA23295-15, FA23295-16
FA23386-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 500 476 95 500 510 102 7 70-130/20
74-83-9 Methyl Bromide ND 500 595 119 500 613 123 3 60-140/20
74-87-3 Methyl Chloride ND 500 637 127 500 675 135 6 60-140/20
74-95-3 Methylene Bromide ND 500 510 102 500 506 101 1 70-130/20
75-09-2 Methylene Chloride ND 500 566 113 500 583 117 3 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 500 515 103 500 537 107 4 70-130/20
91-20-3 Naphthalene ND 500 394 79 500 418 84 6 70-130/20
103-65-1 n-Propylbenzene ND 500 474 95 500 508 102 7 70-130/20
100-42-5 Styrene ND 500 459 92 500 483 97 5 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 500 503 101 500 477 95 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 500 416 83 500 434 87 4 70-130/20
127-18-4 Tetrachloroethylene 68.1 500 525 91 500 544 95 4 70-130/20
108-88-3 Toluene ND 500 442 88 500 480 96 8 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 500 451 90 500 477 95 6 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 500 413 83 500 438 88 6 70-130/20
71-55-6 1,1,1-Trichloroethane 87.0 500 646 112 500 649 112 0 70-130/20
79-00-5 1,1,2-Trichloroethane ND 500 453 91 500 464 93 2 70-130/20
79-01-6 Trichloroethylene 1720 500 2160 88 500 2190 94 1 70-130/20
75-69-4 Trichlorofluoromethane ND 500 604 121 500 597 119 1 60-140/20
96-18-4 1,2,3-Trichloropropane ND 500 448 90 500 469 94 5 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 500 445 89 500 471 94 6 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 500 439 88 500 468 94 6 70-130/20
75-01-4 Vinyl Chloride ND 500 558 112 500 588 118 5 60-140/20
m,p-Xylene ND 1000 960 96 1000 1010 101 5 70-130/20
95-47-6 o-Xylene ND 500 491 98 500 518 104 5 70-130/20
1330-20-7 Xylene (total)ND 1500 1450 97 1500 1530 102 5 70-130/20
CAS No.Surrogate Recoveries MS MSD FA23386-8 Limits
1868-53-7 Dibromofluoromethane 114%110%112%70-130%
17060-07-0 1,2-Dichloroethane-D4 124%117%127%70-130%
2037-26-5 Toluene-D8 93%95%98%70-130%
460-00-4 4-Bromofluorobenzene 95%96%101%70-130%
(a) Confirmation run.
* = Outside of Control Limits.
64 of 66
FA23295 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA23386-5MS A0193740.D 1 04/09/15 TD n/a n/a VA1684
FA23386-5MSD A0193741.D 1 04/09/15 TD n/a n/a VA1684
FA23386-5 A0193729.D 1 04/09/15 TD n/a n/a VA1684
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-17
FA23386-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 10.6 106 10 10.4 104 2 70-130/20
108-86-1 Bromobenzene ND 10 10.4 104 10 10.5 105 1 70-130/20
74-97-5 Bromochloromethane ND 10 10.4 104 10 10.4 104 0 70-130/20
75-27-4 Bromodichloromethane ND 10 10.0 100 10 9.9 99 1 70-130/20
75-25-2 Bromoform ND 10 8.8 88 10 8.9 89 1 70-130/20
104-51-8 n-Butylbenzene ND 10 11.4 114 10 11.1 111 3 70-130/20
135-98-8 sec-Butylbenzene ND 10 12.1 121 10 12.0 120 1 70-130/20
98-06-6 tert-Butylbenzene ND 10 11.5 115 10 11.4 114 1 70-130/20
56-23-5 Carbon Tetrachloride ND 10 10.2 102 10 9.9 99 3 70-130/20
108-90-7 Chlorobenzene ND 10 12.0 120 10 11.8 118 2 70-130/20
67-66-3 Chloroform ND 10 10.0 100 10 9.8 98 2 70-130/20
95-49-8 o-Chlorotoluene ND 10 11.2 112 10 11.0 110 2 70-130/20
106-43-4 p-Chlorotoluene ND 10 11.6 116 10 11.3 113 3 70-130/20
124-48-1 Dibromochloromethane ND 10 9.9 99 10 9.8 98 1 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 9.3 93 10 9.7 97 4 70-130/20
106-93-4 1,2-Dibromoethane ND 10 10.6 106 10 10.4 104 2 70-130/20
95-50-1 1,2-Dichlorobenzene ND 10 11.1 111 10 10.9 109 2 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10 11.5 115 10 11.4 114 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10 10.3 103 10 10.3 103 0 70-130/20
75-34-3 1,1-Dichloroethane ND 10 10.2 102 10 10.0 100 2 70-130/20
107-06-2 1,2-Dichloroethane ND 10 9.8 98 10 9.7 97 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 11.1 111 10 10.8 108 3 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10 10.7 107 10 10.5 105 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 10.1 101 10 10 100 1 70-130/20
78-87-5 1,2-Dichloropropane ND 10 10.7 107 10 10.4 104 3 70-130/20
142-28-9 1,3-Dichloropropane ND 10 10.4 104 10 10.4 104 0 70-130/20
594-20-7 2,2-Dichloropropane ND 10 10.4 104 10 9.8 98 6 70-130/20
563-58-6 1,1-Dichloropropene ND 10 11.2 112 10 11.1 111 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 10.0 100 10 9.8 98 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 10.9 109 10 10.5 105 4 70-130/20
108-20-3 Di-Isopropyl Ether ND 10 10.7 107 10 10.5 105 2 70-130/20
100-41-4 Ethylbenzene ND 10 10.7 107 10 10.5 105 2 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10.0 100 10 9.9 99 1 70-130/20
98-82-8 Isopropylbenzene ND 10 12.0 120 10 11.7 117 3 70-130/20
99-87-6 p-Isopropyltoluene ND 10 11.8 118 10 11.6 116 2 70-130/20
74-95-3 Methylene Bromide ND 10 10.1 101 10 10 100 1 70-130/20
* = Outside of Control Limits.
65 of 66
FA23295 55.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA23295
Account:GRINCC GRI (Geological Resources Inc.)
Project:Peele's Service Station; 2675 Old US Hwy 64, Jamesville, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA23386-5MS A0193740.D 1 04/09/15 TD n/a n/a VA1684
FA23386-5MSD A0193741.D 1 04/09/15 TD n/a n/a VA1684
FA23386-5 A0193729.D 1 04/09/15 TD n/a n/a VA1684
The QC reported here applies to the following samples:Method: SM 6200B
FA23295-17
FA23386-5 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
75-09-2 Methylene Chloride ND 10 10.1 101 10 9.9 99 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 10.9 109 10 10.7 107 2 70-130/20
91-20-3 Naphthalene ND 10 10.3 103 10 10.2 102 1 70-130/20
103-65-1 n-Propylbenzene ND 10 12.2 122 10 12.1 121 1 70-130/20
100-42-5 Styrene ND 10 11.1 111 10 10.9 109 2 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 10.6 106 10 10.3 103 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.4 104 10 10.5 105 1 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.7 107 10 10.5 105 2 70-130/20
108-88-3 Toluene ND 10 11.2 112 10 11.0 110 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 10.6 106 10 10.4 104 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10.1 101 10 9.9 99 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 10.1 101 10 9.9 99 2 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 10.8 108 10 10.5 105 3 70-130/20
79-01-6 Trichloroethylene ND 10 10.6 106 10 10.4 104 2 70-130/20
96-18-4 1,2,3-Trichloropropane ND 10 10.1 101 10 10.2 102 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 10.7 107 10 10.5 105 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 10.8 108 10 10.7 107 1 70-130/20
m,p-Xylene ND 20 22.1 111 20 21.7 109 2 70-130/20
95-47-6 o-Xylene ND 10 11.8 118 10 11.4 114 3 70-130/20
1330-20-7 Xylene (total)ND 30 33.9 113 30 33.1 110 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA23386-5 Limits
1868-53-7 Dibromofluoromethane 95%95%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 89%90%107%70-130%
2037-26-5 Toluene-D8 100%101%99%70-130%
460-00-4 4-Bromofluorobenzene 101%102%101%70-130%
* = Outside of Control Limits.
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FA23295 55.3.3