WA-688_9785_CA_MRP_20171218

EXECUTIVE SUMMARY

The former Red Apple Market #21 is located along NC Highway 561 West, in Saint John, Hertford
County, North Carolina. According to available information, two 1,000-gallon gasoline and one 550-
gallon gasoline underground storage tanks (USTs) were removed from the site in October 1992. In
addition, one 550-gallon gasoline UST was closed-in-place in October 1992. The site risk classification
is currently high due to the presence of potable water supply wells within a 1,000-foot radius of the site.

On November 21, 2017, three monitoring wells were gauged, purged and/or sampled. Concentrations of
requested method constituents that exceeded the Maximum Allowable Concentrations specified in T15A
NCAC 2L.0202 were reported in the ground water samples collected from MW-2R, MW-4R, and MW-
5R. A concentration of benzene that exceeded the Gross Contamination Level (GCL) was reported in the
ground water sample collected from MW-2R.

Upon conclusion of the November 2017 sampling event, contaminant absorbent ORC A socks were
reinstalled in MW-2R, MW-4R and MW-5R.

GRI recommends that the ORC-A socks installed in MW-2R, MW-4R and MW-5R be replaced in
January 2018. The application of ORC-A socks should continue at the site in order to allow for further
evaluation of this remediation technology. Semi-annual ground water monitoring should continue at the
site. The next monitoring event is tentatively scheduled for May 2018.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 GROUND WATER QUALITY ................................................................................................ 1
4.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 3
5.0 LIMITATIONS ......................................................................................................................... 3

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Ground Water Flow Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results
Table 2A: Summary of Field Parameters Results

APPENDIX
Appendix A: Laboratory Report – Ground Water Samples

1
1.0 SITE HISTORY AND CHARACTERIZATION
The Red Apple Market #21 site is located along NC Highway 561 West in Saint John, Hertford County,
North Carolina (Figure 1). According to available information, two 1,000-gallon gasoline and one 550-
gallon gasoline underground storage tanks (USTs) were removed from the site in October 1992. In
addition, one 550-gallon gasoline UST was closed-in-place in October 1992. Twenty-seven Type II
monitoring wells (MW-1 through MW-6, MW-8 through MW-23, MW-25 and MW-27 through MW-30),
one Type III monitoring well (MWD-7) and three recovery wells (RW-1, RW-2 and RW-3) were installed
at the site during past ground water assessment and remediation activities. Please note, MW-6, MW-11,
MW-12 and MW-13 have been destroyed. A total of 4,381.57 tons of contaminated soil was removed
from the site between May 16 and June 2, 2011. Prior to the May-June 2011 soil excavation, monitoring
wells MW-1 through MW-5, MWD-7, as well as recovery wells RW-1 and RW-3, were abandoned.
Monitoring wells MW-1R through MW-5R were installed following the completion of the May-June
2011 excavation activities. Ground water samples collected from monitoring wells at the site and nearby
water supply wells have exceeded the Maximum Allowable Concentrations (MACs) during past sampling
events. Free product has been reported in MW-2, MW-3, MW-5, MW-2R, MW-3R, MW-4R and MW-
5R.

Please note that certain information contained in this report was obtained under the supervision of
previous consultants. Although Geological Resources, Inc. (GRI) cannot verify the accuracy of
information obtained from previous reports, for the purposes of this report, it is assumed to be correct.
Please refer to previous submittals for further historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
The purpose of this report is to present the results of ground water monitoring activities conducted on
November 21, 2017, at the Red Apple Market #21 site. The activities were conducted in accordance with
GRI proposal number 17-475 which was submitted to NCDEQ on August 10, 2017, and approved as
Task Authorization No. 9785-067 on September 27, 2017. The purpose of the activities was to obtain
current ground water quality data and evaluate the effectiveness of the ORC-A socks that were installed at
the site in July 2017.

3.0 GROUND WATER QUALITY
Three monitoring wells (MW-2R, MW-4R, and MW-5R) were gauged, purged and sampled on

2
November 21, 2017. Prior to monitoring well gauging, the ORC-A socks that were installed in MW-2R,
MW-4R and MW-5R were removed. The depths to ground water in the monitoring wells during the
November 2017 sampling event ranged from 14.23 to 14.63 feet below the tops of well casings. Ground
water elevations in the Type II monitoring wells relative to mean sea level ranged from 39.66 to 40.00
feet. Based on this information, ground water flow for the site during the November 2017 gauging event
was generally toward the northeast. The average horizontal hydraulic gradient across the site was
approximately 0.02 feet per foot. A Site Map showing the locations of the monitoring wells and the
structures on-site and on surrounding properties has been included as Figure 2. A Water Table Surface
Map for the November 2017 sampling event has been included as Figure 3. A summary of well
construction and gauging information is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the above referenced
monitoring wells during the November 2017 sampling event. The collected ground water samples were
submitted for analyses of volatile organic compounds (VOCs) using EPA Method 6200B.

Concentrations of individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane, n-
propylbenzene and/or 1,2,4-trimethylbenzene that exceeded the Maximum Allowable Concentrations
(MACs) specified in T15A NCAC 2L.0202 were reported in the ground water samples collected from
MW-2R, MW-4R and MW-5R. A concentration of benzene that exceeded the Gross Contamination
Level (GCL) was reported in the ground water sample collected from MW-2R. A Ground Water Quality
Map based on data from the November 2017 sampling event has been included as Figure 4. A summary
of ground water sample analytical results is presented in Table 2. A complete laboratory report has been
included in Appendix A.

Field parameter data (dissolved oxygen, temperature, pH, conductivity and oxygen reduction potential)
were collected during the November 2017 sampling for use in the evaluation of the ORC-A sock
application. Field parameter results are tabulated in Table 2A. Upon conclusion of the November 2017
sampling event, the ORC-A socks were reinstalled in MW-2R, MW-4R, and MW-5R.

Based on a comparison of ground water quality data obtained between the November 2016 and November
2017 sampling events, the total VOCs concentrations (including BTEX constituents, MTBE and
naphthalene) in MW-4R and MW-5R appear to have been significantly reduced as a result of the ORC-A
sock application. The total VOCs concentrations in MW-2R have only been reduced slightly since
November 2016. The total VOCs concentrations reported in MW-2R during the November 2016 and

3
November 2017 ground water sampling events were 11,918 µg/l and 11,794 µg/l, respectively. Based on
this information, total VOCs concentrations in MW-2 have been reduced by approximately 1.04%. The
total VOCs concentrations reported in MW-4R during the November 2016 and November 2017 ground
water sampling events were 2,214 µg/l and 349.9 µg/l, respectively. Based on this information, total
VOCs concentrations in MW-4R have been reduced by approximately 84.20%. The total VOCs
concentrations reported in MW-5R during the November 2016 and November 2017 ground water
sampling events were 146.24 µg/l and 52.87 µg/l, respectively. Based on this information, total VOCs
concentrations in MW-5R have been reduced by approximately 63.85%.

4.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the monitoring wells during the November 2017 sampling
event was 14.44 feet. Ground water flow for the site during the November 2017 gauging event
was generally toward the northeast with an average horizontal hydraulic gradient of
approximately 0.02 feet per foot.
 Concentrations of individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane, n-
propylbenzene and/or 1,2,4-trimethylbenzene that exceeded the MACs were reported in the
ground water samples collected from MW-2R, MW-4R and MW-5R. A concentration of
benzene that exceeded the GCL was reported in the ground water sample collected form MW-2R.
 Contaminant concentrations observed in MW-2R, MW-4R and MW-5R have been reduced by
1.04%, 84.20% and 63.85%, respectively, since the installation of ORC-A socks in November
2016.
 GRI recommends that the ORC-A socks installed in MW-2R, MW-4R and MW-5R be replaced
in January 2018. The application of ORC-A socks should continue at the site in order to allow
for further evaluation of this remediation technology. Semi-annual ground water monitoring
should continue at the site. The next monitoring event is tentatively scheduled for May 2018.
5.0 LIMITATIONS
This report has been prepared for the exclusive use of Red Apple Markets, Inc. for specific application to
the referenced site in Hertford County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

4
The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the July 2007 sampling and updated receptor survey event was not obtained under the supervision of
GRI. Although the accuracy of this information cannot be verified, for the purpose of this report GRI
assumes that it is correct.

FIGURES

TABLES
01/18/07 12.87 0.00 87.13      
06/06/07 13.15 0.00 86.85
06/02/08 14.10 0.00 85.90
12/18/08 16.41 0.00 83.59
03/24/09 14.62 0.00 85.38
06/25/09 15.00 0.00 85.00
09/16/09 15.58 0.02 84.44 Before AFVR
09/16/09 15.64 0.00 84.36 After AFVR
09/21/09 15.66 0.00 84.34
11/17/09 15.42 0.00 84.58 Before AFVR
11/17/09 15.55 0.01 84.46 After AFVR
12/30/09 14.85 0.00 85.15
06/28/10 14.02 0.00 85.98
10/05/10 14.74 0.00 85.26 Abandoned
10/12/11 15.73 0.00 39.03
01/31/12 15.71 0.00 39.05
05/15/12 14.77 0.00 39.99
01/22/13 14.68 0.00 40.08
11/18/13 15.84 0.00 38.92
05/27/14 14.36 0.00 40.40
01/29/15 14.53 0.00 40.23
07/27/15 14.96 0.00 39.80
04/20/16 13.61 0.00 41.15
01/18/07 14.81 3.25 87.58
06/06/07 13.07 0.69 87.12
06/02/08 15.20 2.27 86.35
11/06/08 16.90 2.60 84.93 Before AFVR
11/06/08 15.04 0.16 84.70 After AFVR
12/18/08 15.25 0.69 84.94
03/24/09 16.90 3.54 85.74
06/10/09 15.84 2.12 85.58 Before AFVR
06/10/06 14.29 0.01 85.32 After AFVR
06/25/09 14.90 0.46 85.09
09/16/09 14.85 1.17 85.75 Before AFVR
09/16/09 15.05 0.00 84.55 After AFVR
09/21/09 15.07 0.03 84.56
11/17/09 15.44 0.59 84.67 Before AFVR
11/17/09 14.98 0.02 84.64 After AFVR
12/30/09 14.65 0.33 85.23
06/28/10 15.65 2.04 85.70
10/05/10 15.81 2.79 86.18 Abandoned
10/12/11 14.71 0.00 39.18
01/31/12 14.67 0.22 39.41
05/15/12 13.96 0.23 40.13
12/17/12 15.25 0.75 39.28 Before MMPE
12/21/12 17.94 0.00 35.95 After MMPE
01/22/13 13.85 0.00 40.04
10/07/13 15.00 0.00 38.89 Before MMPE
10/11/13 15.99 0.00 37.90 After MMPE
11/18/13 14.95 0.00 38.94
04/28/14 13.22 0.00 40.67 Before MMPE
05/02/14 16.95 0.00 36.94 After MMPE
05/27/14 13.71 0.00 40.18
10/13/14 14.48 0.00 39.41 Before MMPE
10/17/14 16.70 0.00 37.19 After MMPE
01/29/15 13.86 0.00 40.03
07/27/15 14.18 0.00 39.71
04/20/16 12.96 0.00 40.93
11/01/16 13.32 0.00 40.57
11/21/17 14.23 0.00 39.66
01/18/07 14.02 0.00 86.99
06/06/07 13.86 0.00 87.15
06/02/08 14.77 0.00 86.24
12/18/08 16.27 0.00 84.74
03/24/09 15.90 0.00 85.11
06/25/09 15.80 0.00 85.21
09/16/09 16.72 0.02 84.31 Before AFVR
09/16/09 16.40 0.01 84.62 After AFVR
09/21/09 16.40 0.00 84.61
11/17/09 16.77 0.00 84.24 Before AFVR
11/17/09 16.40 0.01 84.62 After AFVR
12/30/09 13.97 0.00 87.04
06/28/10 15.76 0.00 85.25
10/05/10 15.50 0.00 85.51 Abandoned
53.892010-201010/12/11MW-2R
1010/12/11
10-20
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
20
20 101.01
20
99.60
MW-3 05/07/93 10
Ground
Water
Elevation*
(ft.)
27 100.00
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 11/30/17 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
MW-1 05/06/93 7 7-27
MW-2 05/07/93 10 10-20
MW-1R 10-20 54.76
Page 1 of 6
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 11/30/17 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
10/12/11 14.48 0.00 40.12
01/31/12 15.88 0.00 38.72
05/15/12 14.31 0.00 40.29
12/17/12 14.54 0.00 40.06 Before MMPE
12/21/12 11.85 0.30 43.01 After MMPE
01/22/13 15.09 0.00 39.51
10/07/13 16.20 0.00 38.40 Before MMPE
10/11/13 11.58 0.00 43.02 After MMPE
11/18/13 16.48 0.00 38.12
04/28/14 13.75 0.00 40.85 Before MMPE
05/02/14 10.23 0.00 44.37 After MMPE
05/27/14 16.74 0.00 37.86
10/13/14 15.23 0.00 39.37 Before MMPE
10/17/14 11.74 0.00 42.86 After MMPE
01/29/15 14.62 0.00 39.98
07/27/15 14.61 0.00 39.99
04/20/16 13.66 0.00 40.94
11/01/16 14.01 0.00 40.59
01/18/07 12.69 0.00 87.37
06/14/07 13.06 0.00 87.00
06/02/08 NM NM NM Destroyed
10/12/11 13.28 0.13 40.85
01/31/12 13.12 0.29 41.15
05/15/12 14.13 0.51 40.33
01/22/13 14.22 0.30 40.06
10/07/13 15.16 0.43 39.23 Before MMPE
10/11/13 11.65 0.03 42.40 After MMPE
11/18/13 14.86 0.01 39.17
04/28/14 11.21 0.00 42.81 Before MMPE
05/02/14 11.55 0.45 42.86 After MMPE
05/27/14 13.58 0.00 40.44
10/13/14 15.08 0.02 38.96 Before MMPE
10/17/14 13.64 0.09 40.46 After MMPE
01/29/15 14.15 0.00 39.87
07/27/15 14.00 0.00 40.02
04/20/16 13.01 0.00 41.01
11/01/16 13.21 0.00 40.81
11/21/17 14.63 0.00 39.39
01/18/07 13.02 0.00 87.80
06/06/07 13.23 0.00 87.59
06/02/08 NM NM NM Not Located
12/18/08 NM NM NM Dry
03/24/09 NM NM NM Dry
06/25/09 NM NM NM Dry
09/21/09 15.47 0.00 85.35
12/30/09 14.44 0.00 86.38
06/28/10 13.99 0.00 86.83
10/05/10 14.60 0.00 86.22 Abandoned
10/12/11 14.16 0.02 40.32
01/31/12 15.36 0.00 39.10
05/15/12 14.20 0.00 40.26
12/17/12 14.57 0.00 39.89 Before MMPE
12/21/12 14.10 0.00 40.36 After MMPE
01/22/13 14.45 0.00 40.01
11/18/13 15.44 0.00 39.02
04/28/14 13.97 0.00 40.49 Before MMPE
05/02/14 13.75 0.00 40.71 After MMPE
05/27/14 13.98 0.00 40.48
10/13/14 14.85 0.00 39.61 Before MMPE
10/17/14 14.90 0.00 39.56 After MMPE
01/29/15 14.20 0.00 40.26
07/27/15 14.35 0.00 40.11
04/20/16 13.28 0.00 41.18
11/01/16 13.59 0.00 40.87
11/21/17 14.46 0.00 40.00
MW-6 NA 01/18/07 NA NA NA 100.49 NM NM NM Destroyed
01/18/07 12.35 0.00 87.45
06/06/07 12.43 0.00 87.37
06/02/08 21.80 0.00 78.00
12/18/08 15.27 0.00 84.53
03/24/09 14.55 0.00 85.25
06/25/09 14.85 0.00 84.95
09/21/09 15.52 0.00 84.28
12/30/09 14.70 0.00 85.10
06/28/10 13.87 0.00 85.93
10/05/10 NM NM NM Abandoned
1010/12/11MW-3R
54.462010-201010/12/11MW-5R
NA
54.60
35 99.80
NA NA
NA
2010-20
MW-5 NA NA NA 100.82
MW-4 NA
MWD-7 02/08/94 30 30-35
100.06
54.022010-201010/12/11MW-4R
Page 2 of 6
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 11/30/17 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
01/18/07 8.59 0.00 92.27
06/06/07 12.87 0.00 87.99
06/02/08 NM NM NM Not Located
12/18/08 17.22 0.00 83.64
03/24/09 4.97 0.00 95.89
06/25/09 16.10 0.00 84.76
09/21/09 17.35 0.00 83.51
12/30/09 6.28 0.00 94.58
06/28/10 14.79 0.00 86.07
10/05/10 12.08 0.00 88.78
10/12/11 16.24 0.00 38.52
01/31/12 11.46 0.00 43.30
05/15/12 13.32 0.00 41.44
11/18/13 15.30 0.00 39.46
05/27/14 12.74 0.00 42.02
01/29/15 9.76 0.00 45.00
07/27/15 12.60 0.00 42.16
04/20/16 9.14 0.00 45.62
01/18/07 7.73 0.00 92.95
06/06/07 9.35 0.00 91.33
06/02/08 8.21 0.00 92.47
12/18/08 11.72 0.00 88.96
03/24/09 11.60 0.00 89.08
06/25/09 11.73 0.00 88.95
09/21/09 12.62 0.00 88.06
12/30/09 12.24 0.00 88.44
06/28/10 12.40 0.00 88.28
10/05/10 12.69 0.00 87.99
10/12/11 10.00 0.00 44.67
01/31/12 10.59 0.00 44.08
05/15/12 9.94 0.00 44.73
12/17/12 10.88 0.00 43.79 Before MMPE
12/21/12 9.41 0.00 45.26 After MMPE
01/22/13 5.34 0.00 49.33
11/18/13 11.49 0.00 43.18
05/27/14 9.64 0.00 45.03
01/29/15 10.94 0.00 43.73
07/27/15 12.48 0.00 42.19
04/20/16 11.57 0.00 43.10
11/01/16 11.21 0.00 43.46
01/18/07 14.26 0.00 86.86
06/06/07 14.38 0.00 86.74
06/02/08 15.50 0.00 85.62
12/18/08 16.62 0.00 84.50
03/24/09 15.99 0.00 85.13
06/25/09 16.16 0.00 84.96
09/21/09 16.85 0.00 84.27
12/30/09 15.98 0.00 85.14
06/28/10 15.45 0.00 85.67
10/05/10 15.97 0.00 85.15
10/12/11 16.40 0.00 38.81
01/31/12 16.05 0.00 39.16
05/15/12 NS NS NS Inaccessable
01/22/13 15.50 0.00 39.71
11/18/13 16.48 0.00 38.73
05/27/14 15.12 0.00 40.09
01/29/15 15.34 0.00 39.87
07/27/15 15.66 0.00 39.55
04/20/16 14.46 0.00 40.75
11/01/16 14.99 0.00 40.22
MW-11 NA 01/18/07 NA NA NA 100.08 NM NM NM Destroyed
MW-12 NA 01/18/07 NA NA NA 99.49 NM NM NM Destroyed
01/18/07 12.72 0.00 87.11
06/06/07 12.83 0.00 87.00 Destroyed
01/18/07 13.78 0.00 87.59
06/06/07 13.93 0.00 87.44
06/02/08 14.90 0.00 86.47
12/18/08 16.49 0.00 84.88
03/24/09 13.73 0.00 87.64
06/25/09 15.85 0.00 85.52
09/21/09 16.60 0.00 84.77
12/30/09 15.92 0.00 85.45
06/28/10 14.92 0.00 86.45
10/05/10 15.83 0.00 85.54
10/12/11 16.28 0.00 39.11
01/31/12 16.00 0.00 39.39
01/22/13 15.44 0.00 39.95
11/18/13 16.22 0.00 39.17
05/27/14 14.91 0.00 40.48
01/29/15 15.18 0.00 40.21
1103/14/94MW-10
100.86
55.21
2111-21
101.12
199-199
199-199
03/14/94MW-9
100.68
54.76
54.67
55.39
MW-14
NA NA
04/05/95 12
99.83
12-22
NA NAMW-13
101.37
22
MW-8 03/14/94
Page 3 of 6
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 11/30/17 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
01/18/07 14.32 0.00 87.66
06/06/07 14.43 0.00 87.55
06/02/08 15.47 0.00 86.51
12/18/08 NM NM NM Not Sampled
03/24/09 16.26 0.00 85.72
06/25/09 16.38 0.00 85.60
09/21/09 17.10 0.00 84.88
12/30/09 NM NM NM Not Sampled
06/28/10 15.42 0.00 86.56
10/05/10 16.35 0.00 85.63
10/12/11 16.79 0.00 39.22
01/31/12 16.55 0.00 39.46
11/18/13 16.75 0.00 39.26
05/27/14 15.42 0.00 40.59
01/29/15 15.71 0.00 40.30
01/18/07 NM NM NM
06/06/07 13.34 0.00 87.56
06/02/08 NM NM NM NA
12/18/08 NM NM NM Not Sampled
03/24/09 15.31 0.00 85.59
06/25/09 15.31 0.00 85.59
09/21/09 NM NM NM Not Sampled
12/30/09 NM NM NM Not Sampled
06/28/10 NM NM NM Not Sampled
10/05/10 15.28 0.00 85.62
10/12/11 15.70 0.00 39.18
01/31/12 15.46 0.00 39.42
11/18/13 NM NM NM Not Sampled
05/27/14 14.40 0.00 40.48
01/29/15 NM NM NM Not Sampled
01/18/07 NM NM NM
06/06/07 11.93 0.00 87.36
06/02/08 NM NM NM NA
12/18/08 NM NM NM Not Sampled
03/24/09 13.81 0.00 85.48
06/25/09 13.84 0.00 85.45
09/21/09 NM NM NM Not Sampled
12/30/09 NM NM NM Not Sampled
06/28/10 NM NM NM Not Sampled
10/05/10 13.82 0.00 85.47
10/12/11 14.33 0.00 39.28
01/31/12 14.07 0.00 39.54
11/18/13 NM NM NM Not Sampled
05/27/14 12.49 0.00 41.12
01/29/15 NM NM NM Not Sampled
01/18/07 14.09 0.00 87.89
06/06/07 14.38 0.00 87.60
06/02/08 15.24 0.00 86.74
12/18/08 16.68 0.00 85.30
03/24/09 16.04 0.00 85.94
06/25/09 16.19 0.00 85.79
09/21/09 16.92 0.00 85.06
12/30/09 16.01 0.00 85.97
06/28/10 15.38 0.00 86.60
10/05/10 NM NM NM
10/12/11 16.46 0.00 38.83
01/31/12 16.14 0.00 39.15
05/15/12 NS NS NS Inaccessable
11/18/13 16.46 0.00 38.83
05/27/14 15.23 0.00 40.06
01/29/15 15.42 0.00 39.87
01/18/07 13.14 0.00 86.80
06/06/07 13.27 0.00 86.67
06/02/08 14.15 0.00 85.79
12/18/08 15.52 0.00 84.42
03/24/09 14.81 0.00 85.13
06/25/09 15.03 0.00 84.91
09/21/09 15.73 0.00 84.21
12/30/09 14.87 0.00 85.07
06/28/10 14.19 0.00 85.75
10/05/10 NM NM NM
10/12/11 15.30 0.00 38.76
01/31/12 15.01 0.00 39.05
05/15/12 NS NS NS Inaccessable
11/18/13 15.33 0.00 38.73
05/27/14 14.55 0.00 39.51
01/29/15 12.48 0.00 41.58
NA
10-2204/07/95
99.94
NA
10 22
10-22 22
MW-15 NA NA
101.98
MW-18
MW-19 04/07/95
101.98
100.90
99.29
MW-17
54.06
53.61
55.29
NA
NANA
NA
NA
56.01
NA
54.88
NA
NA
10
MW-16
Page 4 of 6
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 11/30/17 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
01/18/07 12.86 0.00 86.93
06/06/07 13.25 0.00 86.54
06/02/08 14.07 0.00 85.72
12/18/08 15.46 0.00 84.33
03/24/09 14.75 0.00 85.04
06/25/09 14.98 0.00 84.81
09/21/09 15.40 0.00 84.39
12/30/09 14.88 0.00 84.91
06/28/10 14.23 0.00 85.56
10/05/10 NM NM NM
10/12/11 15.28 0.00 38.80
01/31/12 15.02 0.00 39.06
05/15/12 14.20 0.00 39.88
11/18/13 15.30 0.00 38.78
05/27/14 NM NM NM Inaccessable
01/29/15 14.22 0.00 39.86
01/18/07 14.18 0.00 86.51
06/06/07 13.97 0.00 86.72
06/02/08 14.95 0.00 85.74
12/18/08 16.25 0.00 84.44
03/24/09 15.56 0.00 85.13
06/25/09 15.80 0.00 84.89
09/21/09 16.55 0.00 84.14
12/30/09 16.62 0.00 84.07
06/28/10 15.07 0.00 84.93
10/05/10 15.59 0.00 85.10
10/12/11 16.22 0.00 38.62
01/31/12 15.54 0.00 39.30
05/15/12 15.00 0.00 39.84
01/22/13 15.16 0.00 39.68
11/18/13 16.19 0.00 38.65
05/27/14 14.83 0.00 40.01
01/29/15 14.83 0.00 40.01
07/27/15 15.17 0.00 39.67
04/20/16 14.09 0.00 40.75
06/02/08 16.13 0.00 NM
12/18/08 NM NM NM
05/15/12 15.80 0.00 NM
11/18/13 16.88 0.00 NM
05/27/14 NM NM NM Not Sampled
01/29/15 15.58 0.00 NM
07/27/15 16.84 0.00 NM
04/20/16 14.77 0.00 NM
06/02/08 1.69 0.00 NM
12/18/08 NM NM NM
10/12/11 NM NM NM
05/15/12 0.68 0.00 54.09
11/18/13 1.50 0.00 53.27
05/27/14 2.04 0.00 52.73
01/29/15 0.26 0.00 54.51
07/27/15 1.54 0.00 53.23
04/20/16 1.43 0.00 53.34
03/24/09 12.41 0.00 85.25
06/25/09 12.78 0.00 84.88
09/21/09 13.42 0.00 84.24
12/30/09 12.54 0.00 85.12
06/28/10 11.88 0.00 85.78
10/05/10 12.52 0.00 85.14
10/12/11 12.98 0.00 38.89
01/31/12 12.62 0.00 39.25
05/15/12 11.94 0.00 39.93
11/18/13 12.99 0.00 38.88
05/27/14 11.72 0.00 40.15
01/29/15 11.90 0.00 39.97
07/27/15 12.15 0.00 39.72
04/20/16 11.05 0.00 40.82
03/24/09 16.33 0.00 83.26
06/25/09 13.47 0.00 86.12
09/21/09 NM NM NM Not Sampled
12/30/09 11.74 0.00 87.85
06/28/10 11.10 0.00 88.49
10/05/10 10.50 0.00 89.09
10/12/11 13.03 0.00 40.71
01/31/12 11.45 0.00 42.29
11/18/13 14.23 0.00 39.51
05/27/14 12.05 0.00 41.69
01/29/15 11.21 0.00 42.53
100.69
22
54.08
99.79
22
54.77
2010-20
10
NAMW-22
NA
MW-20 04/10/95
54.84
10-22
10-2210
MW-27
97.66
NM
NMNANANA
10
51.87
20
99.59
04/10/95MW-21
10-201003/24/09MW-25
NAMW-23
53.74
03/24/09
NANA
Page 5 of 6
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 11/30/17 Facility ID # : 0-030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
03/24/09 18.06 0.00 82.13
06/25/09 15.00 0.00 85.19
09/21/09 15.65 0.00 84.54
12/30/09 14.96 0.00 85.23
06/28/10 13.96 0.00 86.23
10/05/10 14.68 0.00 85.51
10/12/11 15.25 0.00 39.05
01/31/12 14.89 0.00 39.41
11/18/13 15.19 39.11 39.11
05/27/14 12.53 0.00 41.77
01/29/15 12.60 0.00 41.70
03/24/09 14.55 0.00 85.67
06/25/09 15.20 0.00 85.02
09/21/09 NM NM NM Not Sampled
12/30/09 15.14 0.00 85.08
06/28/10 14.30 0.00 85.92
10/05/10 15.00 0.00 85.22
10/12/11 54.34 NM NM NM Destroyed
03/24/09 13.10 0.00 85.77
06/25/09 13.92 0.00 84.95
09/21/09 14.62 0.00 84.25
12/30/09 13.84 0.00 85.03
06/28/10 13.04 0.00 85.83
10/05/10 13.72 0.00 85.15
10/12/11 14.16 0.00 38.86
01/31/12 13.84 0.00 39.18
05/15/12 13.12 0.00 39.90
11/18/13 14.17 0.00 38.85
05/27/14 12.88 0.00 40.14
01/29/15 13.04 0.00 39.98
07/27/15 13.29 0.00 39.73
04/20/16 12.22 0.00 40.80
Notes:
•  *: Reference point for elevation measurements; assumed elevation 100.00 feet.
•  **: If free product is present in a well, ground water elevation should be calculated by: (Top of Casing Elevation - Depth to Water) +
   (Free Product Thickness x 0.8581)
•  ft BGS : feet below ground surface.
•  NA: Not Available.
•  NM:  Not Measured.
•  Well construction details for monitoring wells installed prior to March 2009 are reproduced from well identification tags, where available.
100.2220
20MW-28 03/24/09
MW-29 03/24/09 10 10-20
100.19
54.30
53.02
2010-201003/24/09
10 10-20
MW-30
98.87
Page 6 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
01/18/07 46.4 5.51 58.8 28.72 25.7 2.54 34.3 NR NR NR NR NR
06/06/07 68.3 4.56 85.7 32.6 21.6 <0.500 43.9 <0.500 9.60 15.9 36.9 6.60
06/02/08 16.5 1.20 21.2 8.35 38.5 0.320 I 9.23 <1.0 2.98 2.98 6.97 1.54
12/18/08 13 <0.50 10 4.9 14 <1.0 5.9 B <0.75 2.1 J 2.4 J 6.2 1.7 J
03/24/09 44 15 40 23 16 <1.6 19 <1.6 6.8 7.4 4.2 J 2.9 J
06/25/09 6.32 <0.330 7.99 <1.33 10.5 <1.67 3.14 <.0330 1.10 J 1.31 0.840 J <0.330
09/21/09 18.5 <0.190 9.24 1.30 12.7 <0.200 3.10 <0.220 1.17 1.74 0.701 J <0.180
12/30/09 26.1 2.13 5.26 3.14 15.1 <0.200 3.51 <0.220 2.04 1.79 1.87 <0.180
06/28/10 20.1 0.618 J 12.2 2.51 11.4 <0.400 7.66 <0.440 2.38 1.23 J 1.71J 0.464 J
10/05/10 32.6 2.78 16.0 8.47 8.91 <0.200 5.69 <0.220 3.87 3.78 5.51 0.85
10/12/11 <0.13 <0.13 <0.15 <0.30 2.1 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 1.2 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.16 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 <0.10 <0.10 <0.22 1.0 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 1.1 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 1.0 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.80 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 0.91 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
04/20/16 <0.13 <0.13 <0.13 <0.31 0.63 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
01/18/07 FP FP FP FP FP FP FP FP FP FP FP FP
06/06/07 FP FP FP FP FP FP FP FP FP FP FP FP
06/02/08 FP FP FP FP FP FP FP FP FP FP FP FP
12/18/08 FP FP FP FP FP FP FP FP FP FP FP FP
03/24/09 FP FP FP FP FP FP FP FP FP FP FP FP
06/25/09 FP FP FP FP FP FP FP FP FP FP FP FP
09/21/09 FP FP FP FP FP FP FP FP FP FP FP FP
12/30/09 FP FP FP FP FP FP FP FP FP FP FP FP
06/28/10 FP FP FP FP FP FP FP FP FP FP FP FP
10/05/10 FP FP FP FP FP FP FP FP FP FP FP FP
10/12/11 9,780 9,700 2,440 10,100 1,220 46.3 J 769 120 146 373 2,390 634
01/31/12 FP FP FP FP FP FP FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP FP FP FP FP FP FP
01/22/13 3,250 7,990 2,070 11,900 519 14.8 J 2,020 50.7 200 703 4,350 1,440
11/18/13 6,580 7,930 2,100 13,800 731 28.8 J 841 97.9 J 122 397 3,740 878
05/27/14 4,160 4,880 1,400 10,500 657 22.3 J 758 73.2 105 263 3,220 879
01/29/15 4,350 3,670 1,360 7,130 739 29.9 J 555 79.6 99.5 285 2,010 597
07/27/15 6,350 3,210 1,730 7,550 1,090 43.7 J 732 123 114 319 2,250 641
04/20/16 6,440 1,990 1,350 4,750 917 39.1 J 397 114 J 62.9 J 217 1,310 361
11/01/16 3,770 966 958 4,650 967 40.9 607 45.1 111 346 1,320 379
11/21/17 5,610 781 962 3,100 981 42.1 J 360 20.2 J 54.5 148 794 251
01/18/07 1,940 5.14 34.3 <15.0 3,800 17.0 <25.0 NR NR NR NR NR
06/06/07 3,030 6.18 69.0 7.61 4,880 16.9 40.3 <0.500 13.7 18.0 3.22 2.92
06/02/08 2,500 4.95 126 14.2 5,490 18.3 60.8 9.44 12.8 18.5 6.14 <1.0
12/18/08 1,700 2.1 J 33 2.6 J 4,200 E <1.0 24 B 8.4 9.1 10 1.1 J 1.3 J
03/24/09 2,900 <16 110 140 J 4,900 20 J 69 J <16 20 J 24 J 26 J <16
06/25/09 2,140 10.3 J 56.4 32.9 J 4,110 <33.4 40 J <6.60 <20 11.2 J 19.4 J <6.60
09/21/09 2,180 <7.60 56.2 <8.80 5,040 18.6 J 69.3 <8.80 13.8 J 22.1 J <6.00 <7.20
12/30/09 1,580 2.29 J 41.1 <1.10 4,200 14.5 23.3 6.35 7.99 7.71 <0.750 <0.900
06/28/10 1,780 <9.50 54.0 <11.0 5,040 <10.0 26.2J <11.0 <7.50 <11.0 <7.50 <9.00
10/05/10 1,830 <9.50 47.8 J <11.0 4,010 18.2 J <25.0 <11.0 11.8 J 14.5 J <7.50 <9.00
10/12/11 3.4 6.1 1.7 6.2 0.36 J <0.11 0.46 J <0.16 0.17 J 0.47 J 1.8 0.67
01/31/12 36.6 2.9 17.9 28.4 6.2 <0.11 0.21 J <0.16 1.8 3.5 12.9 3.8
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 22.1 2.1 19.1 16.2 8.1 <0.10 0.68 <0.10 1.8 4.1 7.6 3.6
11/18/13 12.6 1.4 17.1 14.0 5.9 <0.10 1.2 <0.10 1.9 4.4 11.9 4.6
05/27/14 4.2 <0.10 0.85 0.74 J 5.9 <0.10 0.27 J <0.10 0.44 J 0.56 0.58 <0.10
01/29/15 3.8 0.28 J 4.7 0.68 J 6.5 <0.16 0.18 J <0.16 0.78 1.5 0.29 J 0.15 J
07/27/15 1.9 0.30 J 1.1 1.0 J 5.5 <0.16 0.28 J <0.16 0.32 J 0.32 J 0.50 0.18 J
04/20/16 1.3 0.19 J 1.9 1.2 J 5.0 <0.13 <0.13 <0.13 0.39 J 0.68 0.46 J 0.29 J
11/01/16 1.5 0.28 J 0.70 1.1 J 6.5 <0.13 0.19 J <0.13 0.31 J 0.41 J 0.55 0.34 J
01/18/07 14,900 5,650 1,330 4,850 16,100 288 436 NR NR NR NR NR
06/14/07 15,000 8,240 1,710 6,330 14,300 57.0 489 512 66.6 188 1,460 362
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
MW-3R
MW-2R
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBEDate : 11/30/17
Analytical Method EthylbenzeneContaminant of Concern

TABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneEPA Method 6210D or EPA Method 6200B
1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)
MW-2
MW-1
MW-1R IsopropylbenzeneNaphthaleneTolueneMW-4
MW-3
Page 1 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBEDate : 11/30/17
Analytical Method EthylbenzeneContaminant of Concern

TABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneEPA Method 6210D or EPA Method 6200B
1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene10/12/11 FP FP FP FP FP FP FP FP FP FP FP FP
01/31/12 FP FP FP FP FP FP FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP FP FP FP FP FP FP
01/22/13 FP FP FP FP FP FP FP FP FP FP FP FP
11/18/13 FP FP FP FP FP FP FP FP FP FP FP FP
05/27/14 792 3,720 1,160 5,660 604 <10 550 22.8 J 95.0 356 2,160 605
01/29/15 170 1,930 1,170 6,160 238 <16 496 <16 125 592 3,230 1,140
07/27/15 236 297 448 2,260 367 <4.0 298 14.8 61.7 215 1,590 445
04/20/16 175 94.3 272 1,030 334 <3.1 267 14.0 52.5 198 2,330 601
11/01/16 110 81.0 355 1,110 299 <0.13 259 7.7 79.9 311 2,190 904
11/21/17 18.4 13.9 44.0 131 101 <1.3 41.6 2.7 J 17.1 60.9 367 181
01/18/07 1,040 76.6 116 109.4 836 <5.00 348 NR NR NR NR NR
06/06/07 1,350 90.1 143 119 1,300 9.78 105 31.1 20.6 41.9 29.0 8.31
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/25/09 NS NS NS NS NS NS NS NS NS NS NS NS
09/21/09 403 2.25 J 40.9 37.3 195 3.44 J 61.5 4.47 J 18.1 45.9 19.5 16.4
12/30/09 676 7.35 35.7 12.3 255 3.76 J 43.4 4.58 J 11.6 19.6 4.45 J 3.94 J
06/28/10 817 12.6 J 66.7 55.9 347 <10.0 54.1 <11.0 9.82 J 16.8 J 10.9 J <9.00
10/05/10 308 <19.0 41.1 J 23.0 J 193 <20.0 108 <22.0 24.2 J 46.9 J 29.2 J <18.0
10/12/11 FP FP FP FP FP FP FP FP FP FP FP FP
01/31/12 40.6 2.7 61.4 25.6 156 1.6 42.6 5.2 12.6 31.4 55.6 23.3
05/15/12 871 18.2 134 214.8 93.4 1.7 87.5 2.7 21.4 19.8 111 9.2
01/22/13 143 14.6 114 225 184 1.8 J 128 3.6 22.4 76.2 506 101
11/18/13 34.4 0.45 J 22.7 1.8 99.2 1.2 47.3 1.9 5.7 6.1 13.1 3.1
05/27/14 145 7.8 114 39.9 247 1.9 J 60.7 5.7 15.3 21.5 87.7 11.9
01/29/15 65.8 2.4 28.2 1.5 117 1.1 20.1 2.5 4.8 8.2 7.9 0.26 J
07/27/15 61.2 1.2 J 19.2 10.4 198 1.4 26.1 4.2 6.3 9.6 15.4 1.0 J
04/20/16 27.4 0.87 0.39 J 2.6 96.3 0.94 13.5 1.8 2.3 2.5 1.5 0.28 J
11/01/16 32.5 0.61 0.33 J 2.0 90.0 0.93 20.8 1.6 3.4 5.5 1.3 0.40 J
11/21/17 2.3 0.16 J <0.13 0.61 J 45.4 0.55 4.4 0.89 1.1 0.88 0.15 J <0.13
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <1.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 0.550 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 14 <0.50 <0.65 <1.1 13 <1.0 2.1 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 3.0 J <1.6 <3.0 <5.0 3.6 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.280 <0.380 <0.300 <0.440 <0.500 <0.400 <1.00 <0.440 <0.300 <0.440 <0.300 <0.360
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <1.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
12/18/08 2.3 J <0.50 <0.65 <1.1 <0.50 <1.0 1.2 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.543 J <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 2.30 <0.220 <0.150 <0.220 0.168 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 0.15 J <0.16 <0.12 <0.16 <0.14 <0.14
04/20/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
MW-8
MW-4R
MW-5R
MWD-7
MW-5
MW-6
Page 2 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBEDate : 11/30/17
Analytical Method EthylbenzeneContaminant of Concern

TABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneEPA Method 6210D or EPA Method 6200B
1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene01/18/07 53.6 1.48 27.4 56.3 3.67 3.97 18.3 NR NR NR NR NR
06/06/07 56.8 0.960 24.2 53.8 0.690 0.520 14.3 1.42 3.14 6.14 30.1 2.87
06/02/08 33.6 0.640 I 21.7 9.07 2.18 0.800 I 20.5 1.68 4.48 4.51 12.3 0.290 I
12/18/08 40 1.6 J 27 18 <0.50 <1.0 22 B <0.50 6.2 9.7 B 25 3.1 J
03/24/09 68 <1.6 37 23 2.0 J <1.6 28 2.3 J 6.8 13 28 2.1 J
06/25/09 53.4 0.929 J 15.9 20.7 1.04 <1.67 19.5 1.54 4.62 4.64 18.4 1.28
09/21/09 50.7 0.952 J 25.7 18.5 1.85 1.10 23.2 2.42 7.29 9.19 18.4 1.46
12/30/09 71.9 0.903 J 28.4 16.8 <0.250 0.758 J 21.9 1.71 6.49 10.7 20.9 2.06
06/28/10 66.1 <0.950 22.5 15.2 <1.25 <1.00 19.0 <1.10 4.25 J 5.94 9.47 1.11 J
10/05/10 72.6 3.54 74.2 110 <0.250 1.35 33.7 2.95 10.6 22.7 79.8 14.3
10/12/11 37.3 0.41 J 8.2 12.2 0.92 0.76 17.3 2.1 4.5 4.6 8.3 1.0
01/31/12 54.7 0.78 25.0 21.6 1.5 0.98 24.1 2.4 7.1 13.9 21.7 2.6
05/15/12 65.9 0.58 J 15.7 15.0 1.3 0.86 J 15.9 2.4 4.5 7.7 11.6 0.89 J
01/22/13 73.7 2.3 13.9 74.7 0.43 J 0.42 J 13.6 1.2 1.2 2.1 31.8 6.8
11/18/13 183 3.9 53.5 153 0.91 1.2 40.4 4.0 12.0 26.1 96.0 11.9
05/27/14 227 3.7 60.4 158 1.5 1.7 44.1 6.6 12.9 27.9 108 12.2
01/29/15 162 1.7 36.1 71.5 1.3 1.3 32.6 3.8 8.3 18.8 89.3 6.0
07/27/15 120 1.4 43.9 57.7 1.7 1.4 43.5 4.5 9.1 18.1 51.1 5.1
04/20/16 59.4 0.58 27.1 25.0 1.7 1.2 25.7 3.4 5.9 12.1 33.6 1.5
11/01/16 128 1.8 38.0 83.2 1.5 1.6 39.8 4.5 9.1 18.7 52.4 6.4
01/18/07 1.84 <1.00 <1.00 <3.00 36.6 1.18 <5.00 NR NR NR NR NR
06/06/07 2.05 <0.500 <0.500 <1.00 28.0 0.630 <5.00 2.50 <0.500 <0.500 <0.500 <0.500
06/02/08 45.2 <1.0 <1.0 1.40 I 42.8 2.15 I 1.98 9.21 0.540 I <1.0 0.380 I <1.0
12/18/08 1.7 J <0.50 <0.65 <1.1 35 <1.0 2.6 JB 12 <0.75 <0.55 0.96 J <0.65
03/24/09 1.4 J <1.6 <3.0 <5.0 49 2.5 J <5.0 12 <1.6 <1.6 <1.6 <1.6
06/25/09 6.42 <0.330 <0.670 <1.33 83.8 3.29 J <1.00 20.7 <1.00 <0.330 <0.330 <0.330
09/21/09 2.03 <0.190 <0.150 <0.220 100 4.02 <0.500 23.4 <0.150 <0.220 <0.150 <0.180
12/30/09 1.13 <0.190 <0.150 <0.220 69.4 2.66 1.41 13.6 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 0.774 J <0.190 <0.150 <0.220 98.8 5.00 12.3 24.0 <0.150 <0.220 0.506 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 61.8 3.6 0.32 J 18.2 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 1.4 <0.15 <0.30 60.3 3.1 0.14 J 14.4 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 3.6 <0.20 <0.20 0.38 J 81.8 2.5 0.52 J 9.8 <0.20 <0.20 0.33 J <0.20
11/18/13 0.20 J <0.10 <0.10 <0.22 76.1 3.5 0.61 16.5 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 37.3 1.8 <0.10 7.2 <0.10 <0.10 <0.10 <0.10
01/29/15 0.43 J <0.17 <0.15 <0.43 73.9 3.2 0.74 15.9 <0.12 <0.16 <0.14 <0.14
07/27/15 0.40 J <0.17 <0.15 <0.43 119 4.2 <0.31 21.4 <0.12 <0.16 <0.14 <0.14
04/20/16 <0.13 <0.13 <0.13 <0.31 70.4 2.4 <0.25 11.5 <0.13 <0.13 <0.13 <0.13
11/01/16 <0.13 <0.13 <0.13 <0.31 76.9 3.1 0.37 J 13.7 <0.13 <0.13 0.16 J <0.13
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NS NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 0.86 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 1.09 <0.190 <0.150 <0.220 99.8 2.95 <0.500 25.6 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 0.853 J <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 0.37 J 0.26 J 1.5 J <0.10 <0.10 1.4 <0.10 <0.10 0.14 J 1.0 0.36 J
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
MW-9
MW-10
MW-11
MW-14
MW-12
MW-13
Page 3 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBEDate : 11/30/17
Analytical Method EthylbenzeneContaminant of Concern

TABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneEPA Method 6210D or EPA Method 6200B
1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 0.59 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 0.244 J <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
MW-15
MW-16
MW-17
MW-18
Page 4 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBEDate : 11/30/17
Analytical Method EthylbenzeneContaminant of Concern

TABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneEPA Method 6210D or EPA Method 6200B
1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.32 J <0.10 <0.15 0.12 J <0.10 <0.10 <0.10 <0.10
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
01/29/15 <0.17 <0.17 <0.15 <0.43 0.34 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 <1.00 <1.00 <1.00 <3.00 4.28 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 4.50 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 5.26 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 4.7 J <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 4.2 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 3.10 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 3.02 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 2.33 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 1.21 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 2.34 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 0.97 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 0.77 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 1.1 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 <0.10 <0.10 <0.22 0.24 J <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.52 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.21 J <0.10 <0.10 <0.10 <0.10 <0.10 0.11 J <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.22 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 0.42 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
04/20/16 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
06/02/08 4.11 <1.0 <1.0 <3.0 52.4 1.78 I <1.0 2.61 <1.0 <1.0 <1.0 <1.0
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 <0.13 <0.13 <0.15 <0.30 1.3 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 2.8 <0.10 0.16 J <0.22 3.1 0.12 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
01/29/15 <0.17 <0.17 <0.15 <0.43 0.75 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 0.50 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
04/20/16 0.37 J <0.13 <0.13 <0.31 0.43 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
06/02/08 81.0 15.6 46.7 162 <1.0 <5.0 38.4 13.5 5.67 10.1 121 57.6
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 104 14.2 60.7 19.5 <0.13 <0.11 19.3 12.5 6.3 11.3 49.0 17.9
11/18/13 63.5 4.7 20.0 13.4 <0.10 <0.10 9.8 11.1 3.5 4.1 12.1 4.2
05/27/14 107 4.3 38.7 45.8 <0.10 <0.10 27.4 16.4 8.2 12.0 41.1 6.5
01/29/15 65.2 0.93 6.4 3.9 <0.16 <0.16 10.3 11.3 3.0 3.8 4.4 0.64
07/27/15 175 2.8 22.8 20.7 <0.33 <0.32 39.4 15.9 10.5 17.1 50.8 3.0
04/20/16 54.2 0.80 5.8 9.9 <0.13 <0.13 11.7 4.7 3.4 5.0 5.6 <0.13
MW-23
MW-22
MW-21
MW-19
MW-20
Page 5 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBEDate : 11/30/17
Analytical Method EthylbenzeneContaminant of Concern

TABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneEPA Method 6210D or EPA Method 6200B
1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 0.19 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 0.18 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.19 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.30 J <0.10 <0.15 <0.10 <0.10 <0.10 0.14 J <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.56 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.35 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 0.39 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
04/20/16 <0.13 <0.13 <0.13 <0.31 0.21 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 0.355 J <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.159 J <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.236 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 0.329 J <0.150 0.515 J <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 0.516 J 0.199 J 1.03 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.465 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 0.16 J <0.15 <0.30 1.0 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 0.572 J 6.18 2.38 15.6 <0.250 <0.200 2.46 J <0.220 0.306 J 0.896 J 8.36 2.02
10/05/10 <0.140 1.00 0.464 J 2.84 <0.250 <0.200 0.841 J <0.220 <0.150 0.248 J 1.81 0.506 J
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 1.8 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 1.15 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 1.23 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 1.14 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 0.203 J 1.95 0.881 J 5.17 1.44 <0.200 0.674 J <0.220 0.150 J 0.418 J 1.67 0.779 J
10/05/10 <0.140 <0.190 <0.150 <0.220 1.28 <0.200 <0.500 <0.220 <0.150 <0.220 0.169 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 1.2 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.87 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.33 J <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 0.27 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
07/27/15 <0.17 <0.17 <0.15 <0.43 0.20 J <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
04/20/16 <0.13 <0.13 <0.13 <0.31 0.46 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
WSW-1 06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 0.930 I <1.0 <1.0 <1.0 0.330 I <1.0
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
MW-25
MW-30
MW-27
MW-29
MW-28
WSW-2
WSW-3
Page 6 of 7
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
Facility ID # : 0-030290
GCL (mg/l)XylenesMTBEDate : 11/30/17
Analytical Method EthylbenzeneContaminant of Concern

TABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneEPA Method 6210D or EPA Method 6200B
1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzene2L Standard (mg/l)IsopropylbenzeneNaphthaleneToluene01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 0.53 J <0.13 <0.11 0.23 J <0.16 <0.10 <0.11 0.33 J <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 0.11 J <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.30 J 0.19 J
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 2.14 <0.500 <0.500 0.520 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 1.75 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 29 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 26 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 34.3 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 34.4 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 16.1 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 45.0 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
01/31/12 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/29/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.16 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the 2L standards.
• NR: Not requested.
• < : Less than the method detection limit specified in the laboratory report
• I or J: Estimated value.
• V or B: Present in laboratory blank.
• NS: Not sampled.
• E: Estimated value; above laboratory calibration curve.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
WSW-5
WSW-6
WSW-4
• GCL : Gross contamination level.
• 2L Standard: as specified in T15A NCAC 2L.0202.
Page 7 of 7
Well No.Sampled Date
(mm/dd/yy)
DO
(mg/L)Temp (oC)pH ORP
(mv)
Methane
(μg/L)
Nitrate
(μg/L)
Sulfate
(μg/L)
Ferrous Iron
(μg/L)
MW-1R 10/12/11 4.7 19 5.8 168 4.17 180 <2,000 <1,000
10/12/11 6.9 21 6.1 130 97.2 100 <2,000 5,700
11/21/17 5.77 19.05 7.21 37.1 NR NR NR NR
MW-3R 10/12/11 6.9 21 6.5 114 2,010 240 2,300 970
10/12/11 FP FP FP FP FP FP FP FP
11/21/17 4.16 18.55 7.35 -69.2 NR NR NR NR
10/12/11 FP FP FP FP FP FP FP FP
11/21/17 5.25 18.54 7.25 7.5 NR NR NR NR
MW-9 10/12/11 4.6 20 6.9 36 20.6 <100 <2,000 570
MW-14 10/12/11 7.6 18 6.5 76 <0.16 1,900 6,600 <500
MW-21 10/12/11 5.8 20 6.3 112 <0.16 1,200 <2,000 <1,000
MW-30 10/12/11 7.3 20 6.2 121 1.86 1,100 <2,000 <2,500
Notes:
• <: Less than the method detection limit specified in the laboratory report.
• J: Estimated concentration.
• FP: Free Product.
MW-5R
MW-4R
MW-2R
• NR: Not requested.
TABLE 2A
SUMMARY OF FIELD PARAMETER RESULTS
RED APPLE MARKET #21 (INCIDENT NO. 9785)
Date: 11/30/17
• Analyses for nitrate and sulfate by Method SW846/9056; analyses for methane by Method RSK 175; analyses for ferrous iron by EPA Method SM
3500 Fe-D. Field measurements of dissolved oxygen, temperature, pH and ORP were collected during sampling using a field meter.
Facility ID # : 0-030290

APPENDIX

APPENDIX A
Laboratory Report – Ground Water Samples
11/30/17
Technical Report for
GRI (Geological Resources Inc.)
Ram 21, 1121 NC561 W, Saint John, NC
9785/2486
SGS Accutest Job Number: FA49617
Sampling Date: 11/21/17
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(L-A-B L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Southeast 11/30/17
e-Hardcopy 2.0
Automated Report
28
SGS Accutest is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
1 of 28
FA49617
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA49617-1: MW-2R .....................................................................................................7
3.2: FA49617-2: MW-4R .....................................................................................................9
3.3: FA49617-3: MW-5R .....................................................................................................11
Section 4: Misc. Forms ............................................................................................................13
4.1: Chain of Custody ...........................................................................................................14
Section 5: MS Volatiles - QC Data Summaries .....................................................................16
5.1: Method Blank Summary ................................................................................................17
5.2: Blank Spike Summary ...................................................................................................21
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................25 123452 of 28
FA49617
SGS Accutest
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA49617
Ram 21, 1121 NC561 W, Saint John, NC
Project No: 9785/2486
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA49617-1 11/21/17 10:00 HM 11/22/17 AQ Ground Water MW-2R
FA49617-2 11/21/17 10:15 HM 11/22/17 AQ Ground Water MW-4R
FA49617-3 11/21/17 09:45 HM 11/22/17 AQ Ground Water MW-5R
3 of 28
FA496171
Summary of Hits Page 1 of 2
Job Number:FA49617
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:11/21/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA49617-1 MW-2R
Benzene 5610 100 25 ug/l SM 6200B
n-Butylbenzene 15.7 J 50 13 ug/l SM 6200B
1,2-Dichloroethane 20.2 J 50 13 ug/l SM 6200B
Di-Isopropyl Ether 42.1 J 50 13 ug/l SM 6200B
Ethylbenzene 962 50 13 ug/l SM 6200B
Isopropylbenzene 54.5 50 13 ug/l SM 6200B
Methyl Tert Butyl Ether 981 50 13 ug/l SM 6200B
Naphthalene 360 50 13 ug/l SM 6200B
n-Propylbenzene 148 50 13 ug/l SM 6200B
Toluene 781 50 13 ug/l SM 6200B
1,2,4-Trimethylbenzene 794 50 13 ug/l SM 6200B
1,3,5-Trimethylbenzene 251 50 13 ug/l SM 6200B
m,p-Xylene 2270 100 13 ug/l SM 6200B
o-Xylene 837 50 13 ug/l SM 6200B
Xylene (total)3100 150 25 ug/l SM 6200B
FA49617-2 MW-4R
Benzene 18.4 5.0 1.3 ug/l SM 6200B
n-Butylbenzene 29.2 5.0 1.3 ug/l SM 6200B
sec-Butylbenzene 12.5 5.0 1.3 ug/l SM 6200B
1,2-Dichloroethane 2.7 J 5.0 1.3 ug/l SM 6200B
Ethylbenzene 44.0 5.0 1.3 ug/l SM 6200B
Isopropylbenzene 17.1 5.0 1.3 ug/l SM 6200B
p-Isopropyltoluene 10.7 5.0 1.3 ug/l SM 6200B
Methyl Tert Butyl Ether 101 5.0 1.3 ug/l SM 6200B
Naphthalene 41.6 5.0 1.3 ug/l SM 6200B
n-Propylbenzene 60.9 5.0 1.3 ug/l SM 6200B
Toluene 13.9 5.0 1.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 367 5.0 1.3 ug/l SM 6200B
1,3,5-Trimethylbenzene 181 5.0 1.3 ug/l SM 6200B
m,p-Xylene 114 10 1.3 ug/l SM 6200B
o-Xylene 17.4 5.0 1.3 ug/l SM 6200B
Xylene (total)131 15 2.5 ug/l SM 6200B
FA49617-3 MW-5R
Benzene 2.3 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.22 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 1.3 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 0.25 J 0.50 0.13 ug/l SM 6200B
1,2-Dichloroethane 0.89 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.55 0.50 0.13 ug/l SM 6200B
4 of 28
FA496172
Summary of Hits Page 2 of 2
Job Number:FA49617
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:11/21/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Isopropylbenzene 1.1 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.46 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 45.4 0.50 0.13 ug/l SM 6200B
Naphthalene 4.4 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 0.88 0.50 0.13 ug/l SM 6200B
Toluene 0.16 J 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.15 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.46 J 1.0 0.13 ug/l SM 6200B
o-Xylene 0.15 J 0.50 0.13 ug/l SM 6200B
Xylene (total)0.61 J 1.5 0.25 ug/l SM 6200B
5 of 28
FA496172
SGS Accutest
Sample Results
Report of Analysis
Southeast
Section 3
6 of 28
FA496173
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA49617-1 Date Sampled:11/21/17
Matrix:AQ - Ground Water Date Received:11/22/17
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0210223.D 100 11/25/17 21:09 TD n/a n/a VA2264
Run #2 A0210251.D 200 11/27/17 19:43 TD n/a n/a VA2265
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 5610 a 100 25 ug/l
108-86-1 Bromobenzene ND 50 13 ug/l
74-97-5 Bromochloromethane ND 50 13 ug/l
75-27-4 Bromodichloromethane ND 50 13 ug/l
75-25-2 Bromoform ND 50 13 ug/l
104-51-8 n-Butylbenzene 15.7 50 13 ug/l J
135-98-8 sec-Butylbenzene ND 50 13 ug/l
98-06-6 tert-Butylbenzene ND 50 13 ug/l
56-23-5 Carbon Tetrachloride ND 50 13 ug/l
108-90-7 Chlorobenzene ND 50 13 ug/l
75-00-3 Chloroethane ND 50 20 ug/l
67-66-3 Chloroform ND 50 13 ug/l
95-49-8 o-Chlorotoluene ND 50 13 ug/l
106-43-4 p-Chlorotoluene ND 50 13 ug/l
124-48-1 Dibromochloromethane ND 50 13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 25 ug/l
106-93-4 1,2-Dibromoethane ND 50 13 ug/l
75-71-8 Dichlorodifluoromethane ND 50 20 ug/l
95-50-1 1,2-Dichlorobenzene ND 50 13 ug/l
541-73-1 1,3-Dichlorobenzene ND 50 13 ug/l
106-46-7 1,4-Dichlorobenzene ND 50 13 ug/l
75-34-3 1,1-Dichloroethane ND 50 13 ug/l
107-06-2 1,2-Dichloroethane 20.2 50 13 ug/l J
75-35-4 1,1-Dichloroethylene ND 50 13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 13 ug/l
78-87-5 1,2-Dichloropropane ND 50 13 ug/l
142-28-9 1,3-Dichloropropane ND 50 13 ug/l
594-20-7 2,2-Dichloropropane ND 50 13 ug/l
563-58-6 1,1-Dichloropropene ND 50 13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 28
FA4961733.1
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA49617-1 Date Sampled:11/21/17
Matrix:AQ - Ground Water Date Received:11/22/17
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 42.1 50 13 ug/l J
100-41-4 Ethylbenzene 962 50 13 ug/l
87-68-3 Hexachlorobutadiene ND 50 13 ug/l
98-82-8 Isopropylbenzene 54.5 50 13 ug/l
99-87-6 p-Isopropyltoluene ND 50 13 ug/l
74-83-9 Methyl Bromide ND 50 20 ug/l
74-87-3 Methyl Chloride ND 50 20 ug/l
74-95-3 Methylene Bromide ND 50 13 ug/l
75-09-2 Methylene Chloride ND 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether 981 50 13 ug/l
91-20-3 Naphthalene 360 50 13 ug/l
103-65-1 n-Propylbenzene 148 50 13 ug/l
100-42-5 Styrene ND 50 13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 50 13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 13 ug/l
127-18-4 Tetrachloroethylene ND 50 13 ug/l
108-88-3 Toluene 781 50 13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 13 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 13 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 13 ug/l
79-01-6 Trichloroethylene ND 50 13 ug/l
75-69-4 Trichlorofluoromethane ND 50 20 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 13 ug/l
95-63-6 1,2,4-Trimethylbenzene 794 50 13 ug/l
108-67-8 1,3,5-Trimethylbenzene 251 50 13 ug/l
75-01-4 Vinyl Chloride ND 50 13 ug/l
m,p-Xylene 2270 100 13 ug/l
95-47-6 o-Xylene 837 50 13 ug/l
1330-20-7 Xylene (total)3100 150 25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%96%70-130%
2037-26-5 Toluene-D8 99%96%70-130%
460-00-4 4-Bromofluorobenzene 100%99%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 28
FA4961733.1
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-4R
Lab Sample ID:FA49617-2 Date Sampled:11/21/17
Matrix:AQ - Ground Water Date Received:11/22/17
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0210252.D 10 11/27/17 20:06 TD n/a n/a VA2265
Run #2 A0210224.D 25 11/25/17 21:31 TD n/a n/a VA2264
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 18.4 5.0 1.3 ug/l
108-86-1 Bromobenzene ND 5.0 1.3 ug/l
74-97-5 Bromochloromethane ND 5.0 1.3 ug/l
75-27-4 Bromodichloromethane ND 5.0 1.3 ug/l
75-25-2 Bromoform ND 5.0 1.3 ug/l
104-51-8 n-Butylbenzene 29.2 5.0 1.3 ug/l
135-98-8 sec-Butylbenzene 12.5 5.0 1.3 ug/l
98-06-6 tert-Butylbenzene ND 5.0 1.3 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 1.3 ug/l
108-90-7 Chlorobenzene ND 5.0 1.3 ug/l
75-00-3 Chloroethane ND 5.0 2.0 ug/l
67-66-3 Chloroform ND 5.0 1.3 ug/l
95-49-8 o-Chlorotoluene ND 5.0 1.3 ug/l
106-43-4 p-Chlorotoluene ND 5.0 1.3 ug/l
124-48-1 Dibromochloromethane ND 5.0 1.3 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.5 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 1.3 ug/l
75-71-8 Dichlorodifluoromethane ND a 13 5.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 1.3 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 1.3 ug/l
106-46-7 1,4-Dichlorobenzene ND 5.0 1.3 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 1.3 ug/l
107-06-2 1,2-Dichloroethane 2.7 5.0 1.3 ug/l J
75-35-4 1,1-Dichloroethylene ND 5.0 1.3 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.3 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 1.3 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 1.3 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 1.3 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 1.3 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.3 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 28
FA4961733.2
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-4R
Lab Sample ID:FA49617-2 Date Sampled:11/21/17
Matrix:AQ - Ground Water Date Received:11/22/17
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 5.0 1.3 ug/l
100-41-4 Ethylbenzene 44.0 5.0 1.3 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 1.3 ug/l
98-82-8 Isopropylbenzene 17.1 5.0 1.3 ug/l
99-87-6 p-Isopropyltoluene 10.7 5.0 1.3 ug/l
74-83-9 Methyl Bromide ND 5.0 2.0 ug/l
74-87-3 Methyl Chloride ND 5.0 2.0 ug/l
74-95-3 Methylene Bromide ND 5.0 1.3 ug/l
75-09-2 Methylene Chloride ND 20 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 101 5.0 1.3 ug/l
91-20-3 Naphthalene 41.6 5.0 1.3 ug/l
103-65-1 n-Propylbenzene 60.9 5.0 1.3 ug/l
100-42-5 Styrene ND 5.0 1.3 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.3 ug/l
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/l
108-88-3 Toluene 13.9 5.0 1.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.3 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.3 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 1.3 ug/l
79-00-5 1,1,2-Trichloroethane ND 5.0 1.3 ug/l
79-01-6 Trichloroethylene ND 5.0 1.3 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/l
95-63-6 1,2,4-Trimethylbenzene 367 5.0 1.3 ug/l
108-67-8 1,3,5-Trimethylbenzene 181 5.0 1.3 ug/l
75-01-4 Vinyl Chloride ND 5.0 1.3 ug/l
m,p-Xylene 114 10 1.3 ug/l
95-47-6 o-Xylene 17.4 5.0 1.3 ug/l
1330-20-7 Xylene (total)131 15 2.5 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%98%70-130%
2037-26-5 Toluene-D8 98%98%70-130%
460-00-4 4-Bromofluorobenzene 100%102%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 28
FA4961733.2
SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:MW-5R
Lab Sample ID:FA49617-3 Date Sampled:11/21/17
Matrix:AQ - Ground Water Date Received:11/22/17
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0210225.D 1 11/25/17 21:54 TD n/a n/a VA2264
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.3 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.22 0.50 0.13 ug/l J
135-98-8 sec-Butylbenzene 1.3 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.25 0.50 0.13 ug/l J
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane 0.89 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 28
FA4961733.3
SGS Accutest
Report of Analysis Page 2 of 2
Client Sample ID:MW-5R
Lab Sample ID:FA49617-3 Date Sampled:11/21/17
Matrix:AQ - Ground Water Date Received:11/22/17
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.55 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 1.1 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.46 0.50 0.13 ug/l J
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 45.4 0.50 0.13 ug/l
91-20-3 Naphthalene 4.4 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 0.88 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.16 0.50 0.13 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.15 0.50 0.13 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.46 1.0 0.13 ug/l J
95-47-6 o-Xylene 0.15 0.50 0.13 ug/l J
1330-20-7 Xylene (total)0.61 1.5 0.25 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 28
FA4961733.3
SGS Accutest
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
13 of 28
FA496174
FA49617: Chain of Custody
Page 1 of 2
14 of 28
FA4961744.1
Job Number:FA49617 Client:GRI
Date / Time Received:11/22/2017 9:30:00 AM Delivery Method:FEDEX
Project:2486
Airbill #'s:800605782113
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Accutest Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.8);
Cooler 1: (4.2);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.4; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:SHAYLAP BR Date:11/22/2017Date:11/22/2017 9:30:00 A
FA49617: Chain of Custody
Page 2 of 2
15 of 28
FA4961744.1
SGS Accutest
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
16 of 28
FA496175
Method Blank Summary Page 1 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2264-MB A0210207.D 1 11/25/17 TD n/a n/a VA2264
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2, FA49617-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
17 of 28
FA4961755.1.1
Method Blank Summary Page 2 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2264-MB A0210207.D 1 11/25/17 TD n/a n/a VA2264
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2, FA49617-3
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
18 of 28
FA4961755.1.1
Method Blank Summary Page 1 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2265-MB A0210241.D 1 11/27/17 TD n/a n/a VA2265
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
19 of 28
FA4961755.1.2
Method Blank Summary Page 2 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2265-MB A0210241.D 1 11/27/17 TD n/a n/a VA2265
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2
CAS No.Compound Result RL MDL Units Q
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
20 of 28
FA4961755.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2264-BS A0210199.D 1 11/25/17 TD n/a n/a VA2264
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2, FA49617-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.2 102 70-130
108-86-1 Bromobenzene 10 10.6 106 70-130
74-97-5 Bromochloromethane 10 11.0 110 70-130
75-27-4 Bromodichloromethane 10 10.7 107 70-130
75-25-2 Bromoform 10 10.9 109 70-130
104-51-8 n-Butylbenzene 10 10.1 101 70-130
135-98-8 sec-Butylbenzene 10 10.2 102 70-130
98-06-6 tert-Butylbenzene 10 10.0 100 70-130
56-23-5 Carbon Tetrachloride 10 12.8 128 70-130
108-90-7 Chlorobenzene 10 10.5 105 70-130
75-00-3 Chloroethane 10 8.6 86 60-140
67-66-3 Chloroform 10 10.2 102 70-130
95-49-8 o-Chlorotoluene 10 10.5 105 70-130
106-43-4 p-Chlorotoluene 10 10.4 104 70-130
124-48-1 Dibromochloromethane 10 11.0 110 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.9 99 70-130
106-93-4 1,2-Dibromoethane 10 10.8 108 70-130
75-71-8 Dichlorodifluoromethane 10 8.2 82 60-140
95-50-1 1,2-Dichlorobenzene 10 10.7 107 70-130
541-73-1 1,3-Dichlorobenzene 10 10.6 106 70-130
106-46-7 1,4-Dichlorobenzene 10 10.4 104 70-130
75-34-3 1,1-Dichloroethane 10 10.3 103 70-130
107-06-2 1,2-Dichloroethane 10 10.3 103 70-130
75-35-4 1,1-Dichloroethylene 10 9.8 98 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.8 108 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.2 102 70-130
78-87-5 1,2-Dichloropropane 10 10.3 103 70-130
142-28-9 1,3-Dichloropropane 10 10.6 106 70-130
594-20-7 2,2-Dichloropropane 10 10.6 106 70-130
563-58-6 1,1-Dichloropropene 10 10.2 102 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.8 98 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10 100 70-130
108-20-3 Di-Isopropyl Ether 10 10 100 70-130
100-41-4 Ethylbenzene 10 10.3 103 70-130
87-68-3 Hexachlorobutadiene 10 8.8 88 70-130
98-82-8 Isopropylbenzene 10 10.4 104 70-130
* = Outside of Control Limits.
21 of 28
FA4961755.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2264-BS A0210199.D 1 11/25/17 TD n/a n/a VA2264
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2, FA49617-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.2 102 70-130
74-83-9 Methyl Bromide 10 7.1 71 60-140
74-87-3 Methyl Chloride 10 8.4 84 60-140
74-95-3 Methylene Bromide 10 10.7 107 70-130
75-09-2 Methylene Chloride 10 10.3 103 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.7 107 70-130
91-20-3 Naphthalene 10 9.6 96 70-130
103-65-1 n-Propylbenzene 10 10.2 102 70-130
100-42-5 Styrene 10 10.4 104 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.6 116 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 11.0 110 70-130
127-18-4 Tetrachloroethylene 10 10.2 102 70-130
108-88-3 Toluene 10 10 100 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.0 100 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.1 101 70-130
71-55-6 1,1,1-Trichloroethane 10 10.8 108 70-130
79-00-5 1,1,2-Trichloroethane 10 10.6 106 70-130
79-01-6 Trichloroethylene 10 10.0 100 70-130
75-69-4 Trichlorofluoromethane 10 9.8 98 60-140
96-18-4 1,2,3-Trichloropropane 10 11.2 112 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.4 104 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.4 104 70-130
75-01-4 Vinyl Chloride 10 7.6 76 60-140
m,p-Xylene 20 20.8 104 70-130
95-47-6 o-Xylene 10 10.3 103 70-130
1330-20-7 Xylene (total)30 31.2 104 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
22 of 28
FA4961755.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2265-BS A0210237.D 1 11/27/17 TD n/a n/a VA2265
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.7 97 70-130
108-86-1 Bromobenzene 10 10.1 101 70-130
74-97-5 Bromochloromethane 10 9.6 96 70-130
75-27-4 Bromodichloromethane 10 10.2 102 70-130
75-25-2 Bromoform 10 9.6 96 70-130
104-51-8 n-Butylbenzene 10 10.4 104 70-130
135-98-8 sec-Butylbenzene 10 10.6 106 70-130
98-06-6 tert-Butylbenzene 10 10.0 100 70-130
56-23-5 Carbon Tetrachloride 10 12.5 125 70-130
108-90-7 Chlorobenzene 10 10.1 101 70-130
75-00-3 Chloroethane 10 11.0 110 60-140
67-66-3 Chloroform 10 9.4 94 70-130
95-49-8 o-Chlorotoluene 10 10.3 103 70-130
106-43-4 p-Chlorotoluene 10 10.2 102 70-130
124-48-1 Dibromochloromethane 10 10.3 103 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.8 88 70-130
106-93-4 1,2-Dibromoethane 10 9.9 99 70-130
95-50-1 1,2-Dichlorobenzene 10 9.9 99 70-130
541-73-1 1,3-Dichlorobenzene 10 10.3 103 70-130
106-46-7 1,4-Dichlorobenzene 10 9.8 98 70-130
75-34-3 1,1-Dichloroethane 10 10.1 101 70-130
107-06-2 1,2-Dichloroethane 10 9.5 95 70-130
75-35-4 1,1-Dichloroethylene 10 9.3 93 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.0 100 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.9 99 70-130
78-87-5 1,2-Dichloropropane 10 9.6 96 70-130
142-28-9 1,3-Dichloropropane 10 9.5 95 70-130
594-20-7 2,2-Dichloropropane 10 10.4 104 70-130
563-58-6 1,1-Dichloropropene 10 9.7 97 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.0 90 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.7 97 70-130
108-20-3 Di-Isopropyl Ether 10 8.7 87 70-130
100-41-4 Ethylbenzene 10 9.9 99 70-130
87-68-3 Hexachlorobutadiene 10 9.5 95 70-130
98-82-8 Isopropylbenzene 10 10.5 105 70-130
99-87-6 p-Isopropyltoluene 10 10.6 106 70-130
* = Outside of Control Limits.
23 of 28
FA4961755.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2265-BS A0210237.D 1 11/27/17 TD n/a n/a VA2265
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
74-83-9 Methyl Bromide 10 6.6 66 60-140
74-87-3 Methyl Chloride 10 9.0 90 60-140
74-95-3 Methylene Bromide 10 9.8 98 70-130
75-09-2 Methylene Chloride 10 9.4 94 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.0 90 70-130
91-20-3 Naphthalene 10 9.1 91 70-130
103-65-1 n-Propylbenzene 10 10.3 103 70-130
100-42-5 Styrene 10 9.8 98 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.7 107 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.3 103 70-130
127-18-4 Tetrachloroethylene 10 10.2 102 70-130
108-88-3 Toluene 10 9.7 97 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.6 96 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.9 99 70-130
71-55-6 1,1,1-Trichloroethane 10 9.6 96 70-130
79-00-5 1,1,2-Trichloroethane 10 10 100 70-130
79-01-6 Trichloroethylene 10 10 100 70-130
75-69-4 Trichlorofluoromethane 10 11.1 111 60-140
96-18-4 1,2,3-Trichloropropane 10 9.8 98 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.1 101 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.5 105 70-130
75-01-4 Vinyl Chloride 10 8.5 85 60-140
m,p-Xylene 20 20.2 101 70-130
95-47-6 o-Xylene 10 9.6 96 70-130
1330-20-7 Xylene (total)30 29.8 99 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
24 of 28
FA4961755.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA49597-6MS A0210226.D 1000 11/25/17 TD n/a n/a VA2264
FA49597-6MSD A0210227.D 1000 11/25/17 TD n/a n/a VA2264
FA49597-6 A0210222.D 1000 11/25/17 TD n/a n/a VA2264
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2, FA49617-3
FA49597-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 375 J 10000 9590 92 10000 9430 91 2 70-130/20
108-86-1 Bromobenzene ND 10000 9280 93 10000 9390 94 1 70-130/20
74-97-5 Bromochloromethane ND 10000 9040 90 10000 8870 89 2 70-130/20
75-27-4 Bromodichloromethane ND 10000 9460 95 10000 8890 89 6 70-130/20
75-25-2 Bromoform ND 10000 8100 81 10000 7240 72 11 70-130/20
104-51-8 n-Butylbenzene ND 10000 9310 93 10000 9180 92 1 70-130/20
135-98-8 sec-Butylbenzene ND 10000 9630 96 10000 9530 95 1 70-130/20
98-06-6 tert-Butylbenzene ND 10000 9270 93 10000 9200 92 1 70-130/20
56-23-5 Carbon Tetrachloride ND 10000 11100 111 10000 10500 105 6 70-130/20
108-90-7 Chlorobenzene ND 10000 9590 96 10000 9470 95 1 70-130/20
75-00-3 Chloroethane ND 10000 10900 109 10000 10400 104 5 60-140/20
67-66-3 Chloroform ND 10000 8940 89 10000 8790 88 2 70-130/20
95-49-8 o-Chlorotoluene ND 10000 9420 94 10000 9390 94 0 70-130/20
106-43-4 p-Chlorotoluene ND 10000 9250 93 10000 9200 92 1 70-130/20
124-48-1 Dibromochloromethane ND 10000 9240 92 10000 8490 85 8 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10000 8380 84 10000 8780 88 5 70-130/20
106-93-4 1,2-Dibromoethane ND 10000 9710 97 10000 9600 96 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 10000 15400 154*10000 15100 151*2 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10000 9300 93 10000 9420 94 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10000 9560 96 10000 9540 95 0 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10000 9180 92 10000 9110 91 1 70-130/20
75-34-3 1,1-Dichloroethane ND 10000 9530 95 10000 9340 93 2 70-130/20
107-06-2 1,2-Dichloroethane ND 10000 9080 91 10000 8850 89 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 10000 8720 87 10000 8590 86 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10000 9480 95 10000 9320 93 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10000 9200 92 10000 9030 90 2 70-130/20
78-87-5 1,2-Dichloropropane ND 10000 9260 93 10000 9020 90 3 70-130/20
142-28-9 1,3-Dichloropropane ND 10000 9230 92 10000 9200 92 0 70-130/20
594-20-7 2,2-Dichloropropane ND 10000 8360 84 10000 7980 80 5 70-130/20
563-58-6 1,1-Dichloropropene ND 10000 9160 92 10000 8880 89 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10000 8000 80 10000 7670 77 4 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10000 8720 87 10000 8380 84 4 70-130/20
108-20-3 Di-Isopropyl Ether 518 10000 8800 83 10000 8750 82 1 70-130/20
100-41-4 Ethylbenzene ND 10000 9450 95 10000 9320 93 1 70-130/20
87-68-3 Hexachlorobutadiene ND 10000 8780 88 10000 8890 89 1 70-130/20
98-82-8 Isopropylbenzene ND 10000 9930 99 10000 9650 97 3 70-130/20
* = Outside of Control Limits.
25 of 28
FA4961755.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA49597-6MS A0210226.D 1000 11/25/17 TD n/a n/a VA2264
FA49597-6MSD A0210227.D 1000 11/25/17 TD n/a n/a VA2264
FA49597-6 A0210222.D 1000 11/25/17 TD n/a n/a VA2264
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2, FA49617-3
FA49597-6 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10000 9710 97 10000 9500 95 2 70-130/20
74-83-9 Methyl Bromide ND 10000 9470 95 10000 9360 94 1 60-140/20
74-87-3 Methyl Chloride ND 10000 14000 140 10000 14100 141*1 60-140/20
74-95-3 Methylene Bromide ND 10000 9310 93 10000 9080 91 3 70-130/20
75-09-2 Methylene Chloride ND 10000 9150 92 10000 9000 90 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether 38900 10000 47200 83 10000 47500 86 1 70-130/20
91-20-3 Naphthalene ND 10000 9590 96 10000 10500 105 9 70-130/20
103-65-1 n-Propylbenzene ND 10000 9230 92 10000 9120 91 1 70-130/20
100-42-5 Styrene ND 10000 8670 87 10000 8040 80 8 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10000 10200 102 10000 9860 99 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10000 9580 96 10000 9830 98 3 70-130/20
127-18-4 Tetrachloroethylene ND 10000 9690 97 10000 9350 94 4 70-130/20
108-88-3 Toluene ND 10000 9510 95 10000 9250 93 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10000 9370 94 10000 10200 102 8 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10000 9440 94 10000 9800 98 4 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10000 8940 89 10000 8730 87 2 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10000 9670 97 10000 9590 96 1 70-130/20
79-01-6 Trichloroethylene ND 10000 9490 95 10000 9210 92 3 70-130/20
75-69-4 Trichlorofluoromethane ND 10000 15100 151*10000 14500 145*4 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10000 9230 92 10000 9440 94 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10000 8990 90 10000 8650 87 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10000 9250 93 10000 8770 88 5 70-130/20
75-01-4 Vinyl Chloride ND 10000 13200 132 10000 13300 133 1 60-140/20
m,p-Xylene ND 20000 19000 95 20000 18200 91 4 70-130/20
95-47-6 o-Xylene ND 10000 9080 91 10000 8820 88 3 70-130/20
1330-20-7 Xylene (total)ND 30000 28000 93 30000 27000 90 4 70-130/20
CAS No.Surrogate Recoveries MS MSD FA49597-6 Limits
1868-53-7 Dibromofluoromethane 102%100%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%98%102%70-130%
2037-26-5 Toluene-D8 102%100%97%70-130%
460-00-4 4-Bromofluorobenzene 98%99%101%70-130%
* = Outside of Control Limits.
26 of 28
FA4961755.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA49617-2MS A0210253.D 10 11/27/17 TD n/a n/a VA2265
FA49617-2MSD A0210254.D 10 11/27/17 TD n/a n/a VA2265
FA49617-2 A0210252.D 10 11/27/17 TD n/a n/a VA2265
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2
FA49617-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 18.4 100 119 101 100 116 98 3 70-130/20
108-86-1 Bromobenzene ND 100 101 101 100 100 100 1 70-130/20
74-97-5 Bromochloromethane ND 100 95.8 96 100 93.9 94 2 70-130/20
75-27-4 Bromodichloromethane ND 100 104 104 100 99.1 99 5 70-130/20
75-25-2 Bromoform ND 100 80.5 81 100 78.4 78 3 70-130/20
104-51-8 n-Butylbenzene 29.2 100 126 97 100 127 98 1 70-130/20
135-98-8 sec-Butylbenzene 12.5 100 115 103 100 114 102 1 70-130/20
98-06-6 tert-Butylbenzene ND 100 102 102 100 100 100 2 70-130/20
56-23-5 Carbon Tetrachloride ND 100 117 117 100 109 109 7 70-130/20
108-90-7 Chlorobenzene ND 100 102 102 100 99.9 100 2 70-130/20
75-00-3 Chloroethane ND 100 89.3 89 100 83.9 84 6 60-140/20
67-66-3 Chloroform ND 100 98.7 99 100 97.2 97 2 70-130/20
95-49-8 o-Chlorotoluene ND 100 118 118 100 116 116 2 70-130/20
106-43-4 p-Chlorotoluene ND 100 101 101 100 99.7 100 1 70-130/20
124-48-1 Dibromochloromethane ND 100 95.4 95 100 90.8 91 5 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 100 133 133*100 135 135*1 70-130/20
106-93-4 1,2-Dibromoethane ND 100 105 105 100 104 104 1 70-130/20
95-50-1 1,2-Dichlorobenzene ND 100 101 101 100 101 101 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 100 104 104 100 103 103 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 100 98.4 98 100 97.6 98 1 70-130/20
75-34-3 1,1-Dichloroethane ND 100 100 100 100 98.3 98 2 70-130/20
107-06-2 1,2-Dichloroethane 2.7 J 100 97.1 94 100 94.9 92 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 100 90.5 91 100 88.2 88 3 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 100 102 102 100 100 100 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 100 95.3 95 100 93.0 93 2 70-130/20
78-87-5 1,2-Dichloropropane ND 100 99.9 100 100 97.3 97 3 70-130/20
142-28-9 1,3-Dichloropropane ND 100 98.5 99 100 97.0 97 2 70-130/20
594-20-7 2,2-Dichloropropane ND 100 86.4 86 100 87.2 87 1 70-130/20
563-58-6 1,1-Dichloropropene ND 100 97.4 97 100 94.8 95 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 100 90.2 90 100 79.0 79 13 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 100 96.1 96 100 85.6 86 12 70-130/20
108-20-3 Di-Isopropyl Ether ND 100 87.3 87 100 87.2 87 0 70-130/20
100-41-4 Ethylbenzene 44.0 100 144 100 100 142 98 1 70-130/20
87-68-3 Hexachlorobutadiene ND 100 91.1 91 100 92.8 93 2 70-130/20
98-82-8 Isopropylbenzene 17.1 100 125 108 100 123 106 2 70-130/20
99-87-6 p-Isopropyltoluene 10.7 100 115 104 100 114 103 1 70-130/20
* = Outside of Control Limits.
27 of 28
FA4961755.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA49617
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA49617-2MS A0210253.D 10 11/27/17 TD n/a n/a VA2265
FA49617-2MSD A0210254.D 10 11/27/17 TD n/a n/a VA2265
FA49617-2 A0210252.D 10 11/27/17 TD n/a n/a VA2265
The QC reported here applies to the following samples:Method: SM 6200B
FA49617-1, FA49617-2
FA49617-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
74-83-9 Methyl Bromide ND 100 58.9 59*100 58.6 59*1 60-140/20
74-87-3 Methyl Chloride ND 100 146 146*100 145 145*1 60-140/20
74-95-3 Methylene Bromide ND 100 101 101 100 98.2 98 3 70-130/20
75-09-2 Methylene Chloride ND 100 88.0 88 100 86.5 87 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether 101 100 188 87 100 191 90 2 70-130/20
91-20-3 Naphthalene 41.6 100 144 102 100 161 119 11 70-130/20
103-65-1 n-Propylbenzene 60.9 100 158 97 100 156 95 1 70-130/20
100-42-5 Styrene ND 100 99.1 99 100 99.0 99 0 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 100 112 112 100 108 108 4 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 100 102 102 100 105 105 3 70-130/20
127-18-4 Tetrachloroethylene ND 100 106 106 100 101 101 5 70-130/20
108-88-3 Toluene 13.9 100 115 101 100 112 98 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 100 106 106 100 114 114 7 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 100 106 106 100 109 109 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 100 94.1 94 100 91.6 92 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 100 215 215*100 229 229*6 70-130/20
79-01-6 Trichloroethylene ND 100 106 106 100 103 103 3 70-130/20
75-69-4 Trichlorofluoromethane ND 100 101 101 100 98.2 98 3 60-140/20
96-18-4 1,2,3-Trichloropropane ND 100 96.8 97 100 101 101 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene 367 100 436 69* a 100 433 66* a 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene 181 100 270 89 100 266 85 1 70-130/20
75-01-4 Vinyl Chloride ND 100 86.1 86 100 85.0 85 1 60-140/20
m,p-Xylene 114 200 317 102 200 312 99 2 70-130/20
95-47-6 o-Xylene 17.4 100 119 102 100 118 101 1 70-130/20
1330-20-7 Xylene (total)131 300 436 102 300 430 100 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA49617-2 Limits
1868-53-7 Dibromofluoromethane 100%100%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%99%102%70-130%
2037-26-5 Toluene-D8 102%102%98%70-130%
460-00-4 4-Bromofluorobenzene 101%102%100%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
28 of 28
FA4961755.3.2