WA-688_9785_CA_MRP_20140619

EXECUTIVE SUMMARY

The former Red Apple Market #21 is located along NC Highway 561 West, in Saint John, Hertford
County, North Carolina (Figure 1). According to information obtained from the file and a Semi-Annual
Ground Water Monitoring Report dated November 18, 2004, prepared by CES Engineering, PC (CES),
the site previously operated as a petroleum retail facility. Two 1,000-gallon gasoline USTs and one 550-
gallon gasoline UST were removed from the site in October 1992. In addition, one 550-gallon gasoline
UST was closed-in-place in October 1992. The site risk classification is currently high due to the
presence of potable water supply wells within a 1,000-foot radius of the site.

On May 27, 2014, twenty monitoring wells and two water supply wells were gauged, purged and/or
sampled. Concentrations of requested method constituents that exceeded the Maximum Allowable
Concentrations specified in T15A NCAC 2L.0202 were reported in the ground water samples collected
from MW-2R, MW-3R, MW-4R, MW-5R, MW-9, MW-10 and MW-23. Concentrations of
dibormochloromethane and bromodichloromethane that exceeded the MACs were reported in the ground
water sample collected from WSW-6. None of the contaminant concentrations exceeded the gross
contamination levels.

The total volatile organic compound (VOC) concentrations reported in monitoring wells MW-2R, MW-
3R and MW-5R in the November 2013 and May 2014 ground water sampling events were 32,240 g/l
and 22,980 g/l, respectively. Based on this information, total VOC concentrations in monitoring wells
MW-2R, MW-3R and MW-5R have been reduced by approximately 28.7% by completing the Mobile
Multi-Phase Extraction (MMPE) activities conducted in April-May 2014. Furthermore, monitoring well
MW-4R had measurable free product prior to the MMPE event. Free product was removed from the well
and total VOC concentrations were significantly reduced.

GRI recommends that MMPE events and semi-annual ground water monitoring should continue at the
site until contaminant concentrations are reduced. The next monitoring event is tentatively scheduled for
November 2014.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 GROUND WATER QUALITY ................................................................................................ 1
4.0 CORRECTIVE ACTION EVALUATION .............................................................................. 3
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 4
6.0 LIMITATIONS ......................................................................................................................... 5

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map
Figure 5: Benzene Isoconcentration Map
Figure 6: MTBE Isoconcentration Map
Figure 7: Naphthalene Isoconcentration Map
Figure 8: 1,2,-Dichloroethane Isoconcentration Map

TABLES
Table 1: Well Construction and Gauging Information
Table 2: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Laboratory Report –Ground Water Samples
Appendix B: Graphs of Individual VOC Concentrations vs. Time
Appendix C: Graphs of Total VOC Concentrations vs. Depths to Ground Water

1
1.0 SITE HISTORY AND CHARACTERIZATION
The Red Apple Market #21 site is located along NC Highway 561 West in Saint John, Hertford County,
North Carolina (Figure 1). According to available information, two 1,000-gallon gasoline and one 550-
gallon gasoline underground storage tanks (USTs) were removed from the site in October 1992. In
addition, one 550-gallon gasoline UST was closed-in-place in October 1992. Twenty-seven Type II
monitoring wells (MW-1 through MW-6, MW-8 through MW-23, MW-25 and MW-27 through MW-30),
one Type III monitoring well (MWD-7) and three recovery wells (RW-1 through RW-3) were installed at
the site during past ground water assessment and remediation activities. Please note, monitoring wells
MW-6, MW-11, MW-12 and MW-13 have been destroyed. A total of 4,381.57 tons of contaminated soil
was removed from the site between May 16 and June 2, 2011. Prior to the May-June 2011 soil
excavation, monitoring wells MW-1 through MW-5, MWD-7 as well as recovery wells RW-1 and RW-3
were abandoned. Monitoring wells MW-1R through MW-5R were installed following the completion of
the May-June 2011 excavation activities. Ground water samples collected from monitoring wells at the
site and nearby water supply wells have exceeded the maximum allowable concentrations (MACs) during
past sampling events. Free product has been reported in monitoring wells MW-2, MW-3, MW-5, MW-
2R, MW-3R, MW-4R and MW-5R.

Please note that certain information contained in this report was obtained under the supervision of
previous consultants. Although Geological Resources, Inc. (GRI) cannot verify the accuracy of
information obtained from previous reports, for the purposes of this report, it is assumed to be correct.
Please refer to previous submittals for further historical information regarding the site.

2.0 CURRENT SITE ASSESSMENT
The purpose of this report is to present the results of ground water assessment activities conducted on
May 27, 2014, at the Red Apple Market #21 site. The activities were conducted in accordance with GRI
proposal number 14-072 which was submitted to North Carolina Department of Environment and Natural
Resources (NCDENR) on February 13, 2014 and approved as Task Authorization No. 9785-059 on
March 24, 2014. The purpose of the activities was to obtain current ground water quality data for the site
following the April 2014 Mobile Multi-Phase Extraction (MMPE) activities conducted at the site.

3.0 GROUND WATER QUALITY
Twenty monitoring wells (MW-1R through MW-5R, MW-8 through MW-10, MW-14 through MW-19,

2
MW-21, MW-23, MW-25, MW-27, MW-28 and MW-30) and two water supply wells (WSW-4 and
WSW-6) were gauged, purged and/or sampled on May 27, 2014. Please note, monitoring wells MW-20
and MW-22 were inaccessible and WSW-5 was inactive, therefore, these wells were not sampled. The
depths to ground water in the monitoring wells during the May 2014 sampling event ranged from 9.64 to
16.74 feet below the tops of well casings. Ground water elevations in the Type II monitoring wells
relative to mean sea level ranged from 37.86 to 45.03 feet. Please note, the depth to water and ground
water elevation for MW-23 appear to be anomalies and were not included in the May 27, 2014 gauging
data. Based on this information, ground water flow for the site during the May 2014 gauging event was
radial outward from MW-9 toward the May-June 2011 excavation area. The average horizontal hydraulic
gradient in the vicinity of the May-June 2011 excavation area was approximately 0.08 feet per foot. A
Site Map showing the locations of the monitoring wells and the structures on-site and on surrounding
properties has been included as Figure 2. A Water Table Surface Map for the May 2014 sampling event
has been included as Figure 3. A summary of well construction and gauging information is presented in
Table 1.

Laboratory analyses were performed on the ground water samples collected from the referenced
monitoring wells during the May 2014 sampling event. The collected ground water samples were
submitted for analyses of volatile organic compounds (VOCs) using EPA Method 6200B.

Concentrations of individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane,
isopropylbenzene, n-propylbenzene, 1,3,5-trimethylbenzene and/or 1,2,4-trimethylbenzene that exceeded
the Maximum Allowable Concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the
ground water samples collected from MW-2R, MW-3R, MW-4R, MW-5R, MW-9, MW-10 and MW-23.
Concentrations of dibromochloromethane and bromodichloromethane that exceeded the MAC were
reported in the ground water sample collected from WSW-6. None of the contaminant concentrations
exceeded the gross contamination levels (GCLs). A Ground Water Quality Map based on data from the
May 2014 sampling event has been included as Figure 4. Contaminant specific isoconcentration maps
for benzene, MTBE, naphthalene and 1,2-dichloroethane are included as Figures 5 through 8,
respectively. A summary of ground water sample analytical results is presented in Table 2. A complete
laboratory report has been included in Appendix A. Please note that the absorbent boom that had been
installed in MW-4R was removed prior to gauging on May 27, 2014. Since no free product was observed
in MW-4R, the absorbent boom was not replaced.

3
4.0 CORRECTIVE ACTION EVALUATION
In accordance with the System Enhancement Report dated May 14, 2010, Soil and Ground Water
Monitoring Report dated November 19, 2010, and the NCDENR correspondence dated June 10, 2010,
soil excavation activities were conducted as the new method for corrective action for this incident. Please
note that a pump and treat remediation system reportedly operated at the site from February 1999 to
September 2005 and October 2008 to May 2010. Between May 26 and June 2, 2011, a total of 4,381.57
tons of contaminated soil were removed from the site and transported to a permitted disposal facility.

Based on a comparison of ground water quality data obtained from the October 2010 and May 2014
sampling events, the total VOC concentrations (including BTEX constituents, MTBE, and naphthalene)
from monitoring wells MW-1/1R, MW-3/3R and MW-5/5R have been significantly reduced as a result of
the soil excavation and dewatering activities. A comparison of data between October 2010 and May 2014
indicates a contaminant reduction of approximately 98.7% in MW-1/1R (from 74.45 g/l in October 2010
to 1.0 g/l in May 2014); approximately 99.8% in MW-3/3R (from 5,888 g/l in October 2010 to 11 g/l
in May 2014), and approximately 8.8% in MW-5/5R (from 673 g/l in October 2010 to 614 g/l in May
2014). Please note, MW-2 contained a free product thicknesses of 2.04 feet during the October 2010
sampling event. MW-4 was not located during the October 2010 sampling event. After the excavation
activities, MW-2R and MW-4R have periodically contained free product. The contaminant
concentrations in all wells should continue to naturally attenuate and reduce over time since the secondary
source has been removed.

The MMPE events have been conducted at the site in order to recover free product, with the most recent
event being conducted on monitoring wells MW-2R, MW-3R, MW-4R and MW-5R between April 28,
2014 and May 2, 2014. Based on a comparison of ground water quality data obtained from the November
2013 and May 2014 sampling events, the total VOC concentrations (including BTEX constituents,
MTBE, and naphthalene) from monitoring wells MW-2/2R, MW-3/3R and MW-5/5R have been reduced
as a result of the MMPE activities. A comparison of data between November 2013 and May 2014
indicates a contaminant reduction of approximately 30.1% in MW-2R (from 31,982 g/l in November
2013 to 22,355 g/l in May 2014) and approximately 78.8% in MW-3R (from 52 g/l in November 2013
to 11 g/l in May 2014). Contaminant concentrations increased in MW-5R approximately 198.1% (from
206 g/l in November 2013 to 614 g/l in May 2014) likely due to the MMPE activities drawing
contaminants from underneath the site building. A free product thickness of 0.01 feet was observed in
MW-4R during the November 2013 sampling event. No free product was observed in MW-4R during the

4
May 2014 sampling event. Graphs showing variations in individual BTEX constituents, MTBE and
naphthalene concentrations versus time and variations in total VOCs versus depths to ground water in
each of the affected wells have been included as Appendices B and C, respectively.

5.0 CONCLUSIONS AND RECOMMENDATIONS
 The average depth to ground water in the monitoring wells during the May 2014 sampling event
was 13.73 feet. Ground water flow for the site during the May 2014 gauging event was radial,
outward from MW-9 toward the May-June 2011 excavation area. The average horizontal
hydraulic gradient in the vicinity of the May-June 2011 excavation area was approximately 0.08
feet per foot.
 Concentrations of individual BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane,
isopropylbenzene, n-propylbenzene, 1,3,5-trimethylbenzene and/or 1,2,4-trimethylbenzene that
exceeded the MACs were reported in the ground water samples collected from MW-2R, MW-3R,
MW-5R, MW-4R, MW-9, MW-10 and MW-23. None of the contaminant concentrations
exceeded the GCL.
 Concentrations of dibromochloromethane and bromodichloromethane that exceeded the MACs
were reported in the ground water sample collected from WSW-6 during the May 2014 sampling
event. Dibromochloromethane and bromodichloromethane are common water treatment
chemicals. An evaluation should be made on the sample collection source during the next
sampling event to determine if municipal water is being sampled at the WSW-6 spigot. An
attempt should be made to sample WSW-6 at the wellhead. Additionally, receptor information
should be updated for this incident.
 Total VOC concentrations in monitoring wells MW-2R, MW-3R and MW-5R have been reduced
by approximately 28.7% by completing the April-May 2014 MMPE activities. Furthermore,
monitoring well MW-4R had measurable free product prior to the MMPE event. Free product
was removed from the well and total VOC concentrations were significantly reduced.
 The absorbent boom that had been installed in MW-4R was removed prior to gauging on May 27,
2014. Since no free product was observed in MW-4R during the May 2014 sampling event, the
boom was not replaced.
 Based on these results, GRI recommends that additional MMPE events should be conducted at
the site in order reduce contaminant concentrations. Semi-annual ground water monitoring
should continue at the site until contaminant concentrations are reduced. The next semi-annual
ground water monitoring event is tentatively scheduled for November 2014.

5
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Red Apple Markets, Inc. for specific application to
the referenced site in Hertford County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDENR and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the July 2007 sampling and updated receptor survey event was not obtained under the supervision of
GRI. Although the accuracy of this information cannot be verified, for the purpose of this report GRI
assumes that it is correct.

FIGURES

TABLES
01/18/07 12.87 0.00 87.13      
06/06/07 13.15 0.00 86.85
06/02/08 14.10 0.00 85.90
12/18/08 16.41 0.00 83.59
03/24/09 14.62 0.00 85.38
06/25/09 15.00 0.00 85.00
09/16/09 15.58 0.02 84.44 Before AFVR
09/16/09 15.64 0.00 84.36 After AFVR
09/21/09 15.66 0.00 84.34
11/17/09 15.42 0.00 84.58 Before AFVR
11/17/09 15.55 0.01 84.46 After AFVR
12/30/09 14.85 0.00 85.15
06/28/10 14.02 0.00 85.98
10/05/10 14.74 0.00 85.26 Abandoned
10/12/11 15.73 0.00 39.03
01/31/12 15.71 0.00 39.05
05/15/12 14.77 0.00 39.99
01/22/13 14.68 0.00 40.08
11/18/13 15.84 0.00 38.92
05/27/14 14.36 0.00 40.40
01/18/07 14.81 3.25 87.58
06/06/07 13.07 0.69 87.12
06/02/08 15.20 2.27 86.35
11/06/08 16.90 2.60 84.93 Before AFVR
11/06/08 15.04 0.16 84.70 After AFVR
12/18/08 15.25 0.69 84.94
03/24/09 16.90 3.54 85.74
06/10/09 15.84 2.12 85.58 Before AFVR
06/10/06 14.29 0.01 85.32 After AFVR
06/25/09 14.90 0.46 85.09
09/16/09 14.85 1.17 85.75 Before AFVR
09/16/09 15.05 0.00 84.55 After AFVR
09/21/09 15.07 0.03 84.56
11/17/09 15.44 0.59 84.67 Before AFVR
11/17/09 14.98 0.02 84.64 After AFVR
12/30/09 14.65 0.33 85.23
06/28/10 15.65 2.04 85.70
10/05/10 15.81 2.79 86.18 Abandoned
10/12/11 14.71 0.00 39.18
01/31/12 14.67 0.22 39.41
05/15/12 13.96 0.23 40.13
12/17/12 15.25 0.75 39.28 Before MMPE
12/21/12 17.94 0.00 35.95 After MMPE
01/22/13 13.85 0.00 40.04
10/07/13 15.00 0.00 38.89 Before MMPE
10/11/13 15.99 0.00 37.90 After MMPE
11/18/13 14.95 0.00 38.94
04/28/14 13.22 0.00 40.67 Before MMPE
05/02/14 16.95 0.00 36.94 After MMPE
05/27/14 13.71 0.00 40.18
01/18/07 14.02 0.00 86.99
06/06/07 13.86 0.00 87.15
06/02/08 14.77 0.00 86.24
12/18/08 16.27 0.00 84.74
03/24/09 15.90 0.00 85.11
06/25/09 15.80 0.00 85.21
09/16/09 16.72 0.02 84.31 Before AFVR
09/16/09 16.40 0.01 84.62 After AFVR
09/21/09 16.40 0.00 84.61
11/17/09 16.77 0.00 84.24 Before AFVR
11/17/09 16.40 0.01 84.62 After AFVR
12/30/09 13.97 0.00 87.04
06/28/10 15.76 0.00 85.25
10/05/10 15.50 0.00 85.51 Abandoned
10/12/11 14.48 0.00 40.12
01/31/12 15.88 0.00 38.72
05/15/12 14.31 0.00 40.29
12/17/12 14.54 0.00 40.06 Before MMPE
12/21/12 11.85 0.30 43.01 After MMPE
01/22/13 15.09 0.00 39.51
10/07/13 16.20 0.00 38.40 Before MMPE
10/11/13 11.58 0.00 43.02 After MMPE
11/18/13 16.48 0.00 38.12
04/28/14 13.75 0.00 40.85 Before MMPE
05/02/14 10.23 0.00 44.37 After MMPE
05/27/14 16.74 0.00 37.86
01/18/07 12.69 0.00 87.37
06/14/07 13.06 0.00 87.00
06/02/08 NM NM NM Destroyed
99.60
53.89
MW-1 05/06/93 7 7-27
MW-2 05/07/93 10 10-20
54.76
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 05/13/14 Facility ID # : 00-0-0000030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
101.01
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
27 100.00
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
20
MW-3R
MW-3 05/07/93 10 10-20 20
MW-4 NA NA NA NA 100.06
2010-201010/12/11MW-1R
2010-201010/12/11MW-2R
54.602010-201010/12/11
Page 1 of 5
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 05/13/14 Facility ID # : 00-0-0000030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
10/12/11 13.28 0.13 40.85
01/31/12 13.12 0.29 41.15
05/15/12 14.13 0.51 40.33
01/22/13 14.22 0.30 40.06
10/07/13 15.16 0.43 39.23 Before MMPE
10/11/13 11.65 0.03 42.40 After MMPE
11/18/13 14.86 0.01 39.17
04/28/14 11.21 0.00 42.81 Before MMPE
05/02/14 11.55 0.45 42.86 After MMPE
05/27/14 13.58 0.00 40.44
01/18/07 13.02 0.00 87.80
06/06/07 13.23 0.00 87.59
06/02/08 NM NM NM Not Located
12/18/08 NM NM NM Dry
03/24/09 NM NM NM Dry
06/25/09 NM NM NM Dry
09/21/09 15.47 0.00 85.35
12/30/09 14.44 0.00 86.38
06/28/10 13.99 0.00 86.83
10/05/10 14.60 0.00 86.22 Abandoned
10/12/11 14.16 0.02 40.32
01/31/12 15.36 0.00 39.10
05/15/12 14.20 0.00 40.26
12/17/12 14.57 0.00 39.89 Before MMPE
12/21/12 14.10 0.00 40.36 After MMPE
01/22/13 14.45 0.00 40.01
11/18/13 15.44 0.00 39.02
04/28/14 13.97 0.00 40.49 Before MMPE
05/02/14 13.75 0.00 40.71 After MMPE
05/27/14 13.98 0.00 40.48
MW-6 NA 01/18/07 NA NA NA 100.49 NM NM NM Destroyed
01/18/07 12.35 0.00 87.45
06/06/07 12.43 0.00 87.37
06/02/08 21.80 0.00 78.00
12/18/08 15.27 0.00 84.53
03/24/09 14.55 0.00 85.25
06/25/09 14.85 0.00 84.95
09/21/09 15.52 0.00 84.28
12/30/09 14.70 0.00 85.10
06/28/10 13.87 0.00 85.93
10/05/10 NM NM NM Abandoned
01/18/07 8.59 0.00 92.27
06/06/07 12.87 0.00 87.99
06/02/08 NM NM NM Not Located
12/18/08 17.22 0.00 83.64
03/24/09 4.97 0.00 95.89
06/25/09 16.10 0.00 84.76
09/21/09 17.35 0.00 83.51
12/30/09 6.28 0.00 94.58
06/28/10 14.79 0.00 86.07
10/05/10 12.08 0.00 88.78
10/12/11 16.24 0.00 38.52
01/31/12 11.46 0.00 43.30
05/15/12 13.32 0.00 41.44
11/18/13 15.30 0.00 39.46
05/27/14 12.74 0.00 42.02
01/18/07 7.73 0.00 92.95
06/06/07 9.35 0.00 91.33
06/02/08 8.21 0.00 92.47
12/18/08 11.72 0.00 88.96
03/24/09 11.60 0.00 89.08
06/25/09 11.73 0.00 88.95
09/21/09 12.62 0.00 88.06
12/30/09 12.24 0.00 88.44
06/28/10 12.40 0.00 88.28
10/05/10 12.69 0.00 87.99
10/12/11 10.00 0.00 44.67
01/31/12 10.59 0.00 44.08
05/15/12 9.94 0.00 44.73
12/17/12 10.88 0.00 43.79 Before MMPE
12/21/12 9.41 0.00 45.26 After MMPE
01/22/13 5.34 0.00 49.33
11/18/13 11.49 0.00 43.18
05/27/14 9.64 0.00 45.03
MWD-7 02/08/94 30 30-35
54.02MW-4R 10/12/11 10 10-20
MW-5R
NA 100.82
20
54.76
199-19
10-2010
MW-5 NA NA NA
10/12/11
903/14/94
35 99.80
100.86
MW-8
54.4620
903/14/94MW-9
100.68
54.67
199-19
Page 2 of 5
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 05/13/14 Facility ID # : 00-0-0000030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
01/18/07 14.26 0.00 86.86
06/06/07 14.38 0.00 86.74
06/02/08 15.50 0.00 85.62
12/18/08 16.62 0.00 84.50
03/24/09 15.99 0.00 85.13
06/25/09 16.16 0.00 84.96
09/21/09 16.85 0.00 84.27
12/30/09 15.98 0.00 85.14
06/28/10 15.45 0.00 85.67
10/05/10 15.97 0.00 85.15
10/12/11 16.40 0.00 38.81
01/31/12 16.05 0.00 39.16
05/15/12 NS NS NS Inaccessable
01/22/13 15.50 0.00 39.71
11/18/13 16.48 0.00 38.73
05/27/14 15.12 0.00 40.09
MW-11 NA 01/18/07 NA NA NA 100.08 NM NM NM Destroyed
MW-12 NA 01/18/07 NA NA NA 99.49 NM NM NM Destroyed
01/18/07 12.72 0.00 87.11
06/06/07 12.83 0.00 87.00 Destroyed
01/18/07 13.78 0.00 87.59
06/06/07 13.93 0.00 87.44
06/02/08 14.90 0.00 86.47
12/18/08 16.49 0.00 84.88
03/24/09 13.73 0.00 87.64
06/25/09 15.85 0.00 85.52
09/21/09 16.60 0.00 84.77
12/30/09 15.92 0.00 85.45
06/28/10 14.92 0.00 86.45
10/05/10 15.83 0.00 85.54
10/12/11 16.28 0.00 39.11
01/31/12 16.00 0.00 39.39
01/22/13 15.44 0.00 39.95
11/18/13 16.22 0.00 39.17
05/27/14 14.91 0.00 40.48
01/18/07 14.32 0.00 87.66
06/06/07 14.43 0.00 87.55
06/02/08 15.47 0.00 86.51
12/18/08 NM NM NM Not Sampled
03/24/09 16.26 0.00 85.72
06/25/09 16.38 0.00 85.60
09/21/09 17.10 0.00 84.88
12/30/09 NM NM NM Not Sampled
06/28/10 15.42 0.00 86.56
10/05/10 16.35 0.00 85.63
10/12/11 16.79 0.00 39.22
01/31/12 16.55 0.00 39.46
11/18/13 16.75 0.00 39.26
05/27/14 15.42 0.00 40.59
01/18/07 NM NM NM
06/06/07 13.34 0.00 87.56
06/02/08 NM NM NM NA
12/18/08 NM NM NM Not Sampled
03/24/09 15.31 0.00 85.59
06/25/09 15.31 0.00 85.59
09/21/09 NM NM NM Not Sampled
12/30/09 NM NM NM Not Sampled
06/28/10 NM NM NM Not Sampled
10/05/10 15.28 0.00 85.62
10/12/11 15.70 0.00 39.18
01/31/12 15.46 0.00 39.42
11/18/13 NM NM NM Not Sampled
05/27/14 14.40 0.00 40.48
01/18/07 NM NM NM
06/06/07 11.93 0.00 87.36
06/02/08 NM NM NM NA
12/18/08 NM NM NM Not Sampled
03/24/09 13.81 0.00 85.48
06/25/09 13.84 0.00 85.45
09/21/09 NM NM NM Not Sampled
12/30/09 NM NM NM Not Sampled
06/28/10 NM NM NM Not Sampled
10/05/10 13.82 0.00 85.47
10/12/11 14.33 0.00 39.28
01/31/12 14.07 0.00 39.54
11/18/13 NM NM NM Not Sampled
05/27/14 12.49 0.00 41.12
MW-13 NA NA NA NA 99.83
100.90
54.88
NANA
101.98
101.37
55.39
2212-22
55.21
2111-211103/14/94MW-10
101.12
1204/05/95MW-14
56.01
NANANANAMW-15
NANAMW-16
53.61
NANANANAMW-17
99.29
Page 3 of 5
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 05/13/14 Facility ID # : 00-0-0000030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
01/18/07 14.09 0.00 87.89
06/06/07 14.38 0.00 87.60
06/02/08 15.24 0.00 86.74
12/18/08 16.68 0.00 85.30
03/24/09 16.04 0.00 85.94
06/25/09 16.19 0.00 85.79
09/21/09 16.92 0.00 85.06
12/30/09 16.01 0.00 85.97
06/28/10 15.38 0.00 86.60
10/05/10 NM NM NM
10/12/11 16.46 0.00 38.83
01/31/12 16.14 0.00 39.15
05/15/12 NS NS NS Inaccessable
11/18/13 16.46 0.00 38.83
05/27/14 15.23 0.00 40.06
01/18/07 13.14 0.00 86.80
06/06/07 13.27 0.00 86.67
06/02/08 14.15 0.00 85.79
12/18/08 15.52 0.00 84.42
03/24/09 14.81 0.00 85.13
06/25/09 15.03 0.00 84.91
09/21/09 15.73 0.00 84.21
12/30/09 14.87 0.00 85.07
06/28/10 14.19 0.00 85.75
10/05/10 NM NM NM
10/12/11 15.30 0.00 38.76
01/31/12 15.01 0.00 39.05
05/15/12 NS NS NS Inaccessable
11/18/13 15.33 0.00 38.73
05/27/14 14.55 0.00 39.51
01/18/07 12.86 0.00 86.93
06/06/07 13.25 0.00 86.54
06/02/08 14.07 0.00 85.72
12/18/08 15.46 0.00 84.33
03/24/09 14.75 0.00 85.04
06/25/09 14.98 0.00 84.81
09/21/09 15.40 0.00 84.39
12/30/09 14.88 0.00 84.91
06/28/10 14.23 0.00 85.56
10/05/10 NM NM NM
10/12/11 15.28 0.00 38.80
01/31/12 15.02 0.00 39.06
05/15/12 14.20 0.00 39.88
11/18/13 15.30 0.00 38.78
05/27/14 NM NM NM Inaccessable
01/18/07 14.18 0.00 86.51
06/06/07 13.97 0.00 86.72
06/02/08 14.95 0.00 85.74
12/18/08 16.25 0.00 84.44
03/24/09 15.56 0.00 85.13
06/25/09 15.80 0.00 84.89
09/21/09 16.55 0.00 84.14
12/30/09 16.62 0.00 84.07
06/28/10 15.07 0.00 84.93
10/05/10 15.59 0.00 85.10
10/12/11 16.22 0.00 38.62
01/31/12 15.54 0.00 39.30
05/15/12 15.00 0.00 39.84
01/22/13 15.16 0.00 39.68
11/18/13 16.19 0.00 38.65
05/27/14 14.83 0.00 40.01
06/02/08 16.13 0.00 NM
12/18/08 NM NM NM
05/15/12 15.80 0.00 NM
11/18/13 16.88 0.00 NM
05/27/14 NM NM NM Not Sampled
06/02/08 1.69 0.00 NM
12/18/08 NM NM NM
10/12/11 NM NM NM
05/15/12 0.68 0.00 54.09
11/18/13 1.50 0.00 53.27
05/27/14 2.04 0.00 52.73
03/24/09 12.41 0.00 85.25
06/25/09 12.78 0.00 84.88
09/21/09 13.42 0.00 84.24
12/30/09 12.54 0.00 85.12
06/28/10 11.88 0.00 85.78
10/05/10 12.52 0.00 85.14
10/12/11 12.98 0.00 38.89
01/31/12 12.62 0.00 39.25
05/15/12 11.94 0.00 39.93
11/18/13 12.99 0.00 38.88
05/27/14 11.72 0.00 40.15
99.79
54.08
2210-22
99.94
101.98
55.29
2210-22
97.66
51.87
2010-20
NM
NMNANA
1004/07/95MW-18
54.06
2210-221004/07/95MW-19
1004/10/95MW-20
54.84
2210-221004/10/95MW-21
100.69
NAMW-22
54.77
NANANANAMW-23
NA
1003/24/09MW-25
Page 4 of 5
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET # 21 (INCIDENT NO. 9785)
Date: 05/13/14 Facility ID # : 00-0-0000030290
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Bottom
of Well
(ft. BGS)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y
ft. BGS)
Ground
Water
Elevation*
(ft.)
Top of
Casing
Elevation*
(ft.)
Depth to Water
from Top of
Casing
(ft.)
Free Product
Thickness**
(ft.)
03/24/09 16.33 0.00 83.26
06/25/09 13.47 0.00 86.12
09/21/09 NM NM NM Not Sampled
12/30/09 11.74 0.00 87.85
06/28/10 11.10 0.00 88.49
10/05/10 10.50 0.00 89.09
10/12/11 13.03 0.00 40.71
01/31/12 11.45 0.00 42.29
11/18/13 14.23 0.00 39.51
05/27/14 12.05 0.00 41.69
03/24/09 18.06 0.00 82.13
06/25/09 15.00 0.00 85.19
09/21/09 15.65 0.00 84.54
12/30/09 14.96 0.00 85.23
06/28/10 13.96 0.00 86.23
10/05/10 14.68 0.00 85.51
10/12/11 15.25 0.00 39.05
01/31/12 14.89 0.00 39.41
11/18/13 15.19 39.11 39.11
05/27/14 12.53 0.00 41.77
03/24/09 14.55 0.00 85.67
06/25/09 15.20 0.00 85.02
09/21/09 NM NM NM Not Sampled
12/30/09 15.14 0.00 85.08
06/28/10 14.30 0.00 85.92
10/05/10 15.00 0.00 85.22
10/12/11 54.34 NM NM NM Destroyed
03/24/09 13.10 0.00 85.77
06/25/09 13.92 0.00 84.95
09/21/09 14.62 0.00 84.25
12/30/09 13.84 0.00 85.03
06/28/10 13.04 0.00 85.83
10/05/10 13.72 0.00 85.15
10/12/11 14.16 0.00 38.86
01/31/12 13.84 0.00 39.18
05/15/12 13.12 0.00 39.90
11/18/13 14.17 0.00 38.85
05/27/14 12.88 0.00 40.14
Notes:
•  *: Reference point for elevation measurements; assumed elevation 100.00 feet.
•  **: If free product is present in a well, ground water elevation should be calculated by: (Top of Casing Elevation - Depth to Water) +
   (Free Product Thickness x 0.8581)
•  ft BGS : feet below ground surface.
•  NA: Not Available.
•  NM:  Not Measured.
•  Well construction details for monitoring wells installed prior to March 2009 are reproduced from well identification tags, where available.
98.87
100.19
MW-29 03/24/09 10 10-20 20 100.22
54.30
20
53.74
2010-201003/24/09MW-27
99.59
10-201003/24/09MW-28
53.02
2010-201003/24/09MW-30
Page 5 of 5
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
01/18/07 46.4 5.51 58.8 28.72 25.7 2.54 34.3 NR NR NR NR NR
06/06/07 68.3 4.56 85.7 32.6 21.6 <0.500 43.9 <0.500 9.60 15.9 36.9 6.60
06/02/08 16.5 1.20 21.2 8.35 38.5 0.320 I 9.23 <1.0 2.98 2.98 6.97 1.54
12/18/08 13 <0.50 10 4.9 14 <1.0 5.9 B <0.75 2.1 J 2.4 J 6.2 1.7 J
03/24/09 44 15 40 23 16 <1.6 19 <1.6 6.8 7.4 4.2 J 2.9 J
06/25/09 6.32 <0.330 7.99 <1.33 10.5 <1.67 3.14 <.0330 1.10 J 1.31 0.840 J <0.330
09/21/09 18.5 <0.190 9.24 1.30 12.7 <0.200 3.10 <0.220 1.17 1.74 0.701 J <0.180
12/30/09 26.1 2.13 5.26 3.14 15.1 <0.200 3.51 <0.220 2.04 1.79 1.87 <0.180
06/28/10 20.1 0.618 J 12.2 2.51 11.4 <0.400 7.66 <0.440 2.38 1.23 J 1.71J 0.464 J
10/05/10 32.6 2.78 16.0 8.47 8.91 <0.200 5.69 <0.220 3.87 3.78 5.51 0.85
10/12/11 <0.13 <0.13 <0.15 <0.30 2.1 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 1.2 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.16 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 <0.10 <0.10 <0.22 1.0 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 1.1 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 1.0 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/18/07 FP FP FP FP FP FP FP FP FP FP FP FP
06/06/07 FP FP FP FP FP FP FP FP FP FP FP FP
06/02/08 FP FP FP FP FP FP FP FP FP FP FP FP
12/18/08 FP FP FP FP FP FP FP FP FP FP FP FP
03/24/09 FP FP FP FP FP FP FP FP FP FP FP FP
06/25/09 FP FP FP FP FP FP FP FP FP FP FP FP
09/21/09 FP FP FP FP FP FP FP FP FP FP FP FP
12/30/09 FP FP FP FP FP FP FP FP FP FP FP FP
06/28/10 FP FP FP FP FP FP FP FP FP FP FP FP
10/05/10 FP FP FP FP FP FP FP FP FP FP FP FP
10/12/11 9,780 9,700 2,440 10,100 1,220 46.3 J 769 120 146 373 2,390 634
01/31/12 FP FP FP FP FP FP FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP FP FP FP FP FP FP
01/22/13 3,250 7,990 2,070 11,900 519 14.8 J 2,020 50.7 200 703 4,350 1,440
11/18/13 6,580 7,930 2,100 13,800 731 28.8 J 841 97.9 J 122 397 3,740 878
05/27/14 4,160 4,880 1,400 10,500 657 22.3 J 758 73.2 105 263 3,220 879
01/18/07 1,940 5.14 34.3 <15.0 3,800 17.0 <25.0 NR NR NR NR NR
06/06/07 3,030 6.18 69.0 7.61 4,880 16.9 40.3 <0.500 13.7 18.0 3.22 2.92
06/02/08 2,500 4.95 126 14.2 5,490 18.3 60.8 9.44 12.8 18.5 6.14 <1.0
12/18/08 1,700 2.1 J 33 2.6 J 4,200 E <1.0 24 B 8.4 9.1 10 1.1 J 1.3 J
03/24/09 2,900 <16 110 140 J 4,900 20 J 69 J <16 20 J 24 J 26 J <16
06/25/09 2,140 10.3 J 56.4 32.9 J 4,110 <33.4 40 J <6.60 <20 11.2 J 19.4 J <6.60
09/21/09 2,180 <7.60 56.2 <8.80 5,040 18.6 J 69.3 <8.80 13.8 J 22.1 J <6.00 <7.20
12/30/09 1,580 2.29 J 41.1 <1.10 4,200 14.5 23.3 6.35 7.99 7.71 <0.750 <0.900
06/28/10 1,780 <9.50 54.0 <11.0 5,040 <10.0 26.2J <11.0 <7.50 <11.0 <7.50 <9.00
10/05/10 1,830 <9.50 47.8 J <11.0 4,010 18.2 J <25.0 <11.0 11.8 J 14.5 J <7.50 <9.00
10/12/11 3.4 6.1 1.7 6.2 0.36 J <0.11 0.46 J <0.16 0.17 J 0.47 J 1.8 0.67
01/31/12 36.6 2.9 17.9 28.4 6.2 <0.11 0.21 J <0.16 1.8 3.5 12.9 3.8
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 22.1 2.1 19.1 16.2 8.1 <0.10 0.68 <0.10 1.8 4.1 7.6 3.6
11/18/13 12.6 1.4 17.1 14.0 5.9 <0.10 1.2 <0.10 1.9 4.4 11.9 4.6
05/27/14 4.2 <0.10 0.85 0.74 J 5.9 <0.10 0.27 J <0.10 0.44 J 0.56 0.58 <0.10
01/18/07 14,900 5,650 1,330 4,850 16,100 288 436 NR NR NR NR NR
06/14/07 15,000 8,240 1,710 6,330 14,300 57.0 489 512 66.6 188 1,460 362
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 FP FP FP FP FP FP FP FP FP FP FP FP
01/31/12 FP FP FP FP FP FP FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP FP FP FP FP FP FP
01/22/13 FP FP FP FP FP FP FP FP FP FP FP FP
11/18/13 FP FP FP FP FP FP FP FP FP FP FP FP
05/27/14 792 3,720 1,160 5,660 604 <10 550 22.8 J 95.0 356 2,160 605
01/18/07 1,040 76.6 116 109.4 836 <5.00 348 NR NR NR NR NR
06/06/07 1,350 90.1 143 119 1,300 9.78 105 31.1 20.6 41.9 29.0 8.31
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/25/09 NS NS NS NS NS NS NS NS NS NS NS NS
09/21/09 403 2.25 J 40.9 37.3 195 3.44 J 61.5 4.47 J 18.1 45.9 19.5 16.4
12/30/09 676 7.35 35.7 12.3 255 3.76 J 43.4 4.58 J 11.6 19.6 4.45 J 3.94 J
06/28/10 817 12.6 J 66.7 55.9 347 <10.0 54.1 <11.0 9.82 J 16.8 J 10.9 J <9.00
10/05/10 308 <19.0 41.1 J 23.0 J 193 <20.0 108 <22.0 24.2 J 46.9 J 29.2 J <18.0
10/12/11 FP FP FP FP FP FP FP FP FP FP FP FP
01/31/12 40.6 2.7 61.4 25.6 156 1.6 42.6 5.2 12.6 31.4 55.6 23.3
05/15/12 871 18.2 134 214.8 93.4 1.7 87.5 2.7 21.4 19.8 111 9.2
01/22/13 143 14.6 114 225 184 1.8 J 128 3.6 22.4 76.2 506 101
11/18/13 34.4 0.45 J 22.7 1.8 99.2 1.2 47.3 1.9 5.7 6.1 13.1 3.1
05/27/14 145 7.8 114 39.9 247 1.9 J 60.7 5.7 15.3 21.5 87.7 11.9
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
EPA Method 6210D or EPA Method 6200B
MW-1
MW-4 IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzeneEthylbenzeneContaminant of Concern

MW-4R
MW-3
MW-5
2L Standard (mg/l)XylenesMTBEMW-2R
TABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 06/05/14
Analytical Method 
MW-6
MW-2
MW-1R
Facility ID # : 00-0-0000030290
MW-3R
MW-5R
GCL (mg/l)
Page 1 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
EPA Method 6210D or EPA Method 6200B
IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzeneEthylbenzeneContaminant of Concern

2L Standard (mg/l)XylenesMTBETABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 06/05/14
Analytical Method 
Facility ID # : 00-0-0000030290
GCL (mg/l)
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <1.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 0.550 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 14 <0.50 <0.65 <1.1 13 <1.0 2.1 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 3.0 J <1.6 <3.0 <5.0 3.6 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.280 <0.380 <0.300 <0.440 <0.500 <0.400 <1.00 <0.440 <0.300 <0.440 <0.300 <0.360
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <1.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
12/18/08 2.3 J <0.50 <0.65 <1.1 <0.50 <1.0 1.2 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.543 J <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 2.30 <0.220 <0.150 <0.220 0.168 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/18/07 53.6 1.48 27.4 56.3 3.67 3.97 18.3 NR NR NR NR NR
06/06/07 56.8 0.960 24.2 53.8 0.690 0.520 14.3 1.42 3.14 6.14 30.1 2.87
06/02/08 33.6 0.640 I 21.7 9.07 2.18 0.800 I 20.5 1.68 4.48 4.51 12.3 0.290 I
12/18/08 40 1.6 J 27 18 <0.50 <1.0 22 B <0.50 6.2 9.7 B 25 3.1 J
03/24/09 68 <1.6 37 23 2.0 J <1.6 28 2.3 J 6.8 13 28 2.1 J
06/25/09 53.4 0.929 J 15.9 20.7 1.04 <1.67 19.5 1.54 4.62 4.64 18.4 1.28
09/21/09 50.7 0.952 J 25.7 18.5 1.85 1.10 23.2 2.42 7.29 9.19 18.4 1.46
12/30/09 71.9 0.903 J 28.4 16.8 <0.250 0.758 J 21.9 1.71 6.49 10.7 20.9 2.06
06/28/10 66.1 <0.950 22.5 15.2 <1.25 <1.00 19.0 <1.10 4.25 J 5.94 9.47 1.11 J
10/05/10 72.6 3.54 74.2 110 <0.250 1.35 33.7 2.95 10.6 22.7 79.8 14.3
10/12/11 37.3 0.41 J 8.2 12.2 0.92 0.76 17.3 2.1 4.5 4.6 8.3 1.0
01/31/12 54.7 0.78 25.0 21.6 1.5 0.98 24.1 2.4 7.1 13.9 21.7 2.6
05/15/12 65.9 0.58 J 15.7 15.0 1.3 0.86 J 15.9 2.4 4.5 7.7 11.6 0.89 J
01/22/13 73.7 2.3 13.9 74.7 0.43 J 0.42 J 13.6 1.2 1.2 2.1 31.8 6.8
11/18/13 183 3.9 53.5 153 0.91 1.2 40.4 4.0 12.0 26.1 96.0 11.9
05/27/14 227 3.7 60.4 158 1.5 1.7 44.1 6.6 12.9 27.9 108 12.2
01/18/07 1.84 <1.00 <1.00 <3.00 36.6 1.18 <5.00 NR NR NR NR NR
06/06/07 2.05 <0.500 <0.500 <1.00 28.0 0.630 <5.00 2.50 <0.500 <0.500 <0.500 <0.500
06/02/08 45.2 <1.0 <1.0 1.40 I 42.8 2.15 I 1.98 9.21 0.540 I <1.0 0.380 I <1.0
12/18/08 1.7 J <0.50 <0.65 <1.1 35 <1.0 2.6 JB 12 <0.75 <0.55 0.96 J <0.65
03/24/09 1.4 J <1.6 <3.0 <5.0 49 2.5 J <5.0 12 <1.6 <1.6 <1.6 <1.6
06/25/09 6.42 <0.330 <0.670 <1.33 83.8 3.29 J <1.00 20.7 <1.00 <0.330 <0.330 <0.330
09/21/09 2.03 <0.190 <0.150 <0.220 100 4.02 <0.500 23.4 <0.150 <0.220 <0.150 <0.180
12/30/09 1.13 <0.190 <0.150 <0.220 69.4 2.66 1.41 13.6 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 0.774 J <0.190 <0.150 <0.220 98.8 5.00 12.3 24.0 <0.150 <0.220 0.506 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 61.8 3.6 0.32 J 18.2 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 1.4 <0.15 <0.30 60.3 3.1 0.14 J 14.4 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 3.6 <0.20 <0.20 0.38 J 81.8 2.5 0.52 J 9.8 <0.20 <0.20 0.33 J <0.20
11/18/13 0.20 J <0.10 <0.10 <0.22 76.1 3.5 0.61 16.5 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 37.3 1.8 <0.10 7.2 <0.10 <0.10 <0.10 <0.10
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NS NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
MW-10
MW-12
MW-8
MW-9
MW-13
MWD-7
MW-11
Page 2 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
EPA Method 6210D or EPA Method 6200B
IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzeneEthylbenzeneContaminant of Concern

2L Standard (mg/l)XylenesMTBETABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 06/05/14
Analytical Method 
Facility ID # : 00-0-0000030290
GCL (mg/l)
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 0.86 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 1.09 <0.190 <0.150 <0.220 99.8 2.95 <0.500 25.6 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 0.853 J <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 0.37 J 0.26 J 1.5 J <0.10 <0.10 1.4 <0.10 <0.10 0.14 J 1.0 0.36 J
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
06/28/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 0.59 JB <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 0.244 J <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
MW-14
MW-15
MW-16
MW-17
MW-18
Page 3 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
EPA Method 6210D or EPA Method 6200B
IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzeneEthylbenzeneContaminant of Concern

2L Standard (mg/l)XylenesMTBETABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 06/05/14
Analytical Method 
Facility ID # : 00-0-0000030290
GCL (mg/l)
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
01/18/07 <1.00 <1.00 <1.00 <3.00 <1.00 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.32 J <0.10 <0.15 0.12 J <0.10 <0.10 <0.10 <0.10
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 <1.00 <1.00 <1.00 <3.00 4.28 <1.00 <5.00 NR NR NR NR NR
06/06/07 <0.500 <0.500 <0.500 <1.00 4.50 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 5.26 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 4.7 J <1.0 <0.50 <0.50 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 4.2 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 3.10 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 3.02 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 2.33 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 1.21 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 2.34 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 0.97 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 0.77 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 1.1 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/22/13 <0.10 <0.10 <0.10 <0.22 0.24 J <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.52 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.21 J <0.10 <0.10 <0.10 <0.10 <0.10 0.11 J <0.10
06/02/08 4.11 <1.0 <1.0 <3.0 52.4 1.78 I <1.0 2.61 <1.0 <1.0 <1.0 <1.0
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 <0.13 <0.13 <0.15 <0.30 1.3 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 2.8 <0.10 0.16 J <0.22 3.1 0.12 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
06/02/08 81.0 15.6 46.7 162 <1.0 <5.0 38.4 13.5 5.67 10.1 121 57.6
12/18/08 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 104 14.2 60.7 19.5 <0.13 <0.11 19.3 12.5 6.3 11.3 49.0 17.9
11/18/13 63.5 4.7 20.0 13.4 <0.10 <0.10 9.8 11.1 3.5 4.1 12.1 4.2
05/27/14 107 4.3 38.7 45.8 <0.10 <0.10 27.4 16.4 8.2 12.0 41.1 6.5
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 0.19 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 0.18 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.19 J <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.30 J <0.10 <0.15 <0.10 <0.10 <0.10 0.14 J <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.56 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
MW-19
MW-25
MW-20
MW-21
MW-22
MW-23
Page 4 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
EPA Method 6210D or EPA Method 6200B
IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzeneEthylbenzeneContaminant of Concern

2L Standard (mg/l)XylenesMTBETABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 06/05/14
Analytical Method 
Facility ID # : 00-0-0000030290
GCL (mg/l)
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 0.355 J <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.159 J <0.180
10/05/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.236 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 0.329 J <0.150 0.515 J <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 <0.140 0.516 J 0.199 J 1.03 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 0.465 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 0.16 J <0.15 <0.30 1.0 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 0.572 J 6.18 2.38 15.6 <0.250 <0.200 2.46 J <0.220 0.306 J 0.896 J 8.36 2.02
10/05/10 <0.140 1.00 0.464 J 2.84 <0.250 <0.200 0.841 J <0.220 <0.150 0.248 J 1.81 0.506 J
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 1.8 J <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 1.15 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 1.23 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 1.14 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 0.203 J 1.95 0.881 J 5.17 1.44 <0.200 0.674 J <0.220 0.150 J 0.418 J 1.67 0.779 J
10/05/10 <0.140 <0.190 <0.150 <0.220 1.28 <0.200 <0.500 <0.220 <0.150 <0.220 0.169 J <0.180
10/12/11 <0.13 <0.13 <0.15 <0.30 1.2 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.87 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 0.33 J <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
WSW-1 06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 0.930 I <1.0 <1.0 <1.0 0.330 I <1.0
03/24/09 NS NS NS NS NS NS NS NS NS NS NS NS
12/30/09 NS NS NS NS NS NS NS NS NS NS NS NS
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 0.53 J <0.13 <0.11 0.23 J <0.16 <0.10 <0.11 0.33 J <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 0.11 J <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 NS NS NS NS NS NS NS NS NS NS NS NS
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.30 J 0.19 J
WSW-2
WSW-3
MW-29
MW-27
MW-28
MW-30
WSW-4
Page 5 of 6
Well ID Date Collected
(mm/dd/yy)
1 600 600 500 20 70 6 0.4 70 70 400 400
5,000 260,000 84,500 85,500 20,000 70,000 6,000 400 25,000 30,000 28,500 25,000
EPA Method 6210D or EPA Method 6200B
IsopropylbenzeneNaphthaleneToluene1,2,4-Trimethylbenzene1,2-DichloroethaneIPEBenzeneEthylbenzeneContaminant of Concern

2L Standard (mg/l)XylenesMTBETABLE 2
SUMMARY OF GROUND WATER SAMPLING RESULTS
RED APPLE MARKET # 21 (INCIDENT NO. 9785)n-Propylbenzene1,3,5-TrimethylbenzeneDate : 06/05/14
Analytical Method 
Facility ID # : 00-0-0000030290
GCL (mg/l)
01/18/07 NS NS NS NS NS NS NS NS NS NS NS NS
06/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 <5.00 2.14 <0.500 <0.500 0.520 <0.500
06/02/08 <1.0 <1.0 <1.0 <3.0 <1.0 <5.0 <1.0 1.75 <1.0 <1.0 <1.0 <1.0
12/18/08 <0.55 <0.50 <0.65 <1.1 <0.50 <1.0 <0.50 29 <0.75 <0.55 <0.50 <0.65
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 26 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 34.3 <1.00 <0.330 <0.330 <0.330
09/21/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 34.4 <0.150 <0.220 <0.150 <0.180
12/30/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 16.1 <0.150 <0.220 <0.150 <0.180
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 45.0 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 NS NS NS NS NS NS NS NS NS NS NS NS
01/31/12 NS NS NS NS NS NS NS NS NS NS NS NS
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 NS NS NS NS NS NS NS NS NS NS NS NS
05/27/14 NS NS NS NS NS NS NS NS NS NS NS NS
06/02/08 NS NS NS NS NS NS NS NS NS NS NS NS
03/24/09 <1.0 <1.6 <3.0 <5.0 <1.6 <1.6 <5.0 <1.6 <1.6 <1.6 <1.6 <1.6
06/25/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.67 <1.00 <0.330 <1.00 <0.330 <0.330 <0.330
06/28/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.200 <0.500 <0.220 <0.150 <0.220 <0.150 <0.180
10/05/10 NS NS NS NS NS NS NS NS NS NS NS NS
10/12/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.16 <0.10 <0.11 <0.10 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.11 <0.10 <0.10 <0.10 <0.11 <0.10 <0.10
05/15/12 NS NS NS NS NS NS NS NS NS NS NS NS
01/22/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
11/18/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10
05/27/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the 2L standards.
• NR: Not requested.
• < : Less than the method detection limit specified in the laboratory report
• I or J: Estimated value.
• V or B: Present in laboratory blank.
• NS: Not sampled.
• E: Estimated value; above laboratory calibration curve.
• Concentrations of dibromochloromethane (2.1 µg/l in WSW-6) and bromodichloromethane (1.2 µg/l in WSW-6) that exceeded
the MACs were reported in the ground water sample collected on May 27, 2014.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
• GCL : Gross contamination level.
• 2L Standard: as specified in T15A NCAC 2L.0202.
WSW-5
WSW-6
Page 6 of 6

APPENDICES

APPENDIX A
Laboratory Report – Ground Water Samples

06/05/14
Technical Report for
GRI (Geological Resources Inc.)
Ram 21, 1121 NC561 W, Saint John, NC
9785
Accutest Job Number: FA15341
Sampling Date: 05/27/14
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail];
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
06/05/14
e-Hardcopy 2.0
Automated Report
90
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 90
FA15341
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................10
3.1: FA15341-1: MW-1R .....................................................................................................11
3.2: FA15341-2: MW-2R .....................................................................................................13
3.3: FA15341-3: MW-3R .....................................................................................................15
3.4: FA15341-4: MW-4R .....................................................................................................17
3.5: FA15341-5: MW-5R .....................................................................................................19
3.6: FA15341-6: MW-8 ........................................................................................................21
3.7: FA15341-7: MW-9 ........................................................................................................23
3.8: FA15341-8: MW-10 ......................................................................................................25
3.9: FA15341-9: MW-14 ......................................................................................................27
3.10: FA15341-10: MW-15 ..................................................................................................29
3.11: FA15341-11: MW-16 ..................................................................................................31
3.12: FA15341-12: MW-17 ..................................................................................................33
3.13: FA15341-13: MW-18 ..................................................................................................35
3.14: FA15341-14: MW-19 ..................................................................................................37
3.15: FA15341-15: MW-21 ..................................................................................................39
3.16: FA15341-16: MW-23 ..................................................................................................41
3.17: FA15341-17: MW-25 ..................................................................................................43
3.18: FA15341-18: MW-27 ..................................................................................................45
3.19: FA15341-19: MW-28 ..................................................................................................47
3.20: FA15341-20: MW-30 ..................................................................................................49
3.21: FA15341-21: WSW-4 .................................................................................................51
3.22: FA15341-22: WSW-6 .................................................................................................53
Section 4: Misc. Forms ............................................................................................................55
4.1: Chain of Custody ...........................................................................................................56
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................60
5.1: Method Blank Summary ................................................................................................61
5.2: Blank Spike Summary ...................................................................................................71
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................81 123452 of 90
FA15341
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA15341
Ram 21, 1121 NC561 W, Saint John, NC
Project No: 9785
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA15341-1 05/27/14 11:43 HM 05/28/14 AQ Ground Water MW-1R
FA15341-2 05/27/14 11:50 HM 05/28/14 AQ Ground Water MW-2R
FA15341-3 05/27/14 12:10 HM 05/28/14 AQ Ground Water MW-3R
FA15341-4 05/27/14 11:59 HM 05/28/14 AQ Ground Water MW-4R
FA15341-5 05/27/14 12:18 HM 05/28/14 AQ Ground Water MW-5R
FA15341-6 05/27/14 12:42 HM 05/28/14 AQ Ground Water MW-8
FA15341-7 05/27/14 11:02 HM 05/28/14 AQ Ground Water MW-9
FA15341-8 05/27/14 13:05 HM 05/28/14 AQ Ground Water MW-10
FA15341-9 05/27/14 14:07 HM 05/28/14 AQ Ground Water MW-14
FA15341-10 05/27/14 14:16 HM 05/28/14 AQ Ground Water MW-15
FA15341-11 05/27/14 14:38 HM 05/28/14 AQ Ground Water MW-16
FA15341-12 05/27/14 14:51 HM 05/28/14 AQ Ground Water MW-17
FA15341-13 05/27/14 13:17 HM 05/28/14 AQ Ground Water MW-18
3 of 90
FA15341 1
Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA15341
Ram 21, 1121 NC561 W, Saint John, NC
Project No: 9785
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA15341-14 05/27/14 13:28 HM 05/28/14 AQ Ground Water MW-19
FA15341-15 05/27/14 13:41 HM 05/28/14 AQ Ground Water MW-21
FA15341-16 05/27/14 12:51 HM 05/28/14 AQ Ground Water MW-23
FA15341-17 05/27/14 13:52 HM 05/28/14 AQ Ground Water MW-25
FA15341-18 05/27/14 11:13 HM 05/28/14 AQ Ground Water MW-27
FA15341-19 05/27/14 11:22 HM 05/28/14 AQ Ground Water MW-28
FA15341-20 05/27/14 11:35 HM 05/28/14 AQ Ground Water MW-30
FA15341-21 05/27/14 15:08 HM 05/28/14 AQ Ground Water WSW-4
FA15341-22 05/27/14 15:12 HM 05/28/14 AQ Ground Water WSW-6
4 of 90
FA15341 1
Summary of Hits Page 1 of 5
Job Number:FA15341
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:05/27/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA15341-1 MW-1R
Methyl Tert Butyl Ether 1.0 0.50 0.10 ug/l SM 6200B
FA15341-2 MW-2R
Benzene 4160 50 10 ug/l SM 6200B
n-Butylbenzene 52.3 50 10 ug/l SM 6200B
sec-Butylbenzene 30.3 J 50 10 ug/l SM 6200B
1,2-Dichloroethane 73.2 50 10 ug/l SM 6200B
Di-Isopropyl ether 22.3 J 50 10 ug/l SM 6200B
Ethylbenzene 1400 50 10 ug/l SM 6200B
Isopropylbenzene 105 50 10 ug/l SM 6200B
p-Isopropyltoluene 22.3 J 50 10 ug/l SM 6200B
Methyl Tert Butyl Ether 657 50 10 ug/l SM 6200B
Naphthalene 758 50 10 ug/l SM 6200B
n-Propylbenzene 263 50 10 ug/l SM 6200B
Styrene 16.7 J 50 10 ug/l SM 6200B
1,2,4-Trimethylbenzene 3220 50 10 ug/l SM 6200B
1,3,5-Trimethylbenzene 879 50 10 ug/l SM 6200B
Toluene 4880 50 10 ug/l SM 6200B
Xylene (total)10500 150 20 ug/l SM 6200B
m,p-Xylene 6890 100 10 ug/l SM 6200B
o-Xylene 3590 50 10 ug/l SM 6200B
FA15341-3 MW-3R
Benzene 4.2 0.50 0.10 ug/l SM 6200B
n-Butylbenzene 0.15 J 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 0.18 J 0.50 0.10 ug/l SM 6200B
Ethylbenzene 0.85 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 0.44 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 5.9 0.50 0.10 ug/l SM 6200B
Naphthalene 0.27 J 0.50 0.10 ug/l SM 6200B
n-Propylbenzene 0.56 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.58 0.50 0.10 ug/l SM 6200B
Xylene (total)0.74 J 1.5 0.20 ug/l SM 6200B
m,p-Xylene 0.44 J 1.0 0.10 ug/l SM 6200B
o-Xylene 0.29 J 0.50 0.10 ug/l SM 6200B
FA15341-4 MW-4R
Benzene 792 50 10 ug/l SM 6200B
n-Butylbenzene 55.7 50 10 ug/l SM 6200B
sec-Butylbenzene 27.2 J 50 10 ug/l SM 6200B
5 of 90
FA15341 2
Summary of Hits Page 2 of 5
Job Number:FA15341
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:05/27/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
o-Chlorotoluene 79.1 50 10 ug/l SM 6200B
1,2-Dichloroethane 22.8 J 50 10 ug/l SM 6200B
Ethylbenzene 1160 50 10 ug/l SM 6200B
Isopropylbenzene 95.0 50 10 ug/l SM 6200B
p-Isopropyltoluene 13.3 J 50 10 ug/l SM 6200B
Methyl Tert Butyl Ether 604 50 10 ug/l SM 6200B
Naphthalene 550 50 10 ug/l SM 6200B
n-Propylbenzene 356 50 10 ug/l SM 6200B
Styrene 14.7 J 50 10 ug/l SM 6200B
1,2,4-Trimethylbenzene 2160 50 10 ug/l SM 6200B
1,3,5-Trimethylbenzene 605 50 10 ug/l SM 6200B
Toluene 3720 50 10 ug/l SM 6200B
Xylene (total)5660 150 20 ug/l SM 6200B
m,p-Xylene 3950 100 10 ug/l SM 6200B
o-Xylene 1710 50 10 ug/l SM 6200B
FA15341-5 MW-5R
Benzene 145 2.5 0.50 ug/l SM 6200B
n-Butylbenzene a 2.7 J 2.5 0.50 ug/l SM 6200B
sec-Butylbenzene 4.3 2.5 0.50 ug/l SM 6200B
tert-Butylbenzene a 0.70 J 2.5 0.50 ug/l SM 6200B
1,2-Dichloroethane 5.7 2.5 0.50 ug/l SM 6200B
Di-Isopropyl ether 1.9 J 2.5 0.50 ug/l SM 6200B
Ethylbenzene 114 2.5 0.50 ug/l SM 6200B
Isopropylbenzene 15.3 2.5 0.50 ug/l SM 6200B
p-Isopropyltoluene 2.8 2.5 0.50 ug/l SM 6200B
Methyl Tert Butyl Ether 247 2.5 0.50 ug/l SM 6200B
Naphthalene 60.7 2.5 0.50 ug/l SM 6200B
n-Propylbenzene 21.5 2.5 0.50 ug/l SM 6200B
1,2,4-Trimethylbenzene 87.7 2.5 0.50 ug/l SM 6200B
1,3,5-Trimethylbenzene 11.9 2.5 0.50 ug/l SM 6200B
Toluene 7.8 2.5 0.50 ug/l SM 6200B
m,p-Xylene 25.6 5.0 0.50 ug/l SM 6200B
o-Xylene 14.3 2.5 0.50 ug/l SM 6200B
FA15341-6 MW-8
No hits reported in this sample.
FA15341-7 MW-9
Benzene 227 5.0 1.0 ug/l SM 6200B
n-Butylbenzene 4.2 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 3.5 0.50 0.10 ug/l SM 6200B
6 of 90
FA15341 2
Summary of Hits Page 3 of 5
Job Number:FA15341
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:05/27/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
1,2-Dichloroethane 6.6 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 1.7 0.50 0.10 ug/l SM 6200B
Ethylbenzene 60.4 5.0 1.0 ug/l SM 6200B
Isopropylbenzene 12.9 0.50 0.10 ug/l SM 6200B
p-Isopropyltoluene 1.3 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 1.5 0.50 0.10 ug/l SM 6200B
Naphthalene 44.1 5.0 1.0 ug/l SM 6200B
n-Propylbenzene 27.9 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 108 5.0 1.0 ug/l SM 6200B
1,3,5-Trimethylbenzene 12.2 0.50 0.10 ug/l SM 6200B
Toluene 3.7 0.50 0.10 ug/l SM 6200B
Xylene (total)158 15 2.0 ug/l SM 6200B
m,p-Xylene 114 10 1.0 ug/l SM 6200B
o-Xylene 44.1 5.0 1.0 ug/l SM 6200B
FA15341-8 MW-10
1,2-Dichloroethane 7.2 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 1.8 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 37.3 0.50 0.10 ug/l SM 6200B
FA15341-9 MW-14
No hits reported in this sample.
FA15341-10 MW-15
No hits reported in this sample.
FA15341-11 MW-16
No hits reported in this sample.
FA15341-12 MW-17
No hits reported in this sample.
FA15341-13 MW-18
No hits reported in this sample.
FA15341-14 MW-19
No hits reported in this sample.
7 of 90
FA15341 2
Summary of Hits Page 4 of 5
Job Number:FA15341
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:05/27/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA15341-15 MW-21
Methyl Tert Butyl Ether 0.21 J 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.11 J 0.50 0.10 ug/l SM 6200B
FA15341-16 MW-23
Benzene 107 1.3 0.25 ug/l SM 6200B
n-Butylbenzene 0.95 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 1.3 0.50 0.10 ug/l SM 6200B
Chloroethane 1.4 0.50 0.12 ug/l SM 6200B
1,2-Dichloroethane 16.4 0.50 0.10 ug/l SM 6200B
Ethylbenzene 38.7 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 8.2 0.50 0.10 ug/l SM 6200B
p-Isopropyltoluene 2.2 0.50 0.10 ug/l SM 6200B
Naphthalene 27.4 0.50 0.10 ug/l SM 6200B
n-Propylbenzene 12.0 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 41.1 0.50 0.10 ug/l SM 6200B
1,3,5-Trimethylbenzene 6.5 0.50 0.10 ug/l SM 6200B
Toluene 4.3 0.50 0.10 ug/l SM 6200B
Xylene (total)45.8 1.5 0.20 ug/l SM 6200B
m,p-Xylene 33.0 1.0 0.10 ug/l SM 6200B
o-Xylene 12.7 0.50 0.10 ug/l SM 6200B
FA15341-17 MW-25
Methyl Tert Butyl Ether 0.56 0.50 0.10 ug/l SM 6200B
FA15341-18 MW-27
No hits reported in this sample.
FA15341-19 MW-28
No hits reported in this sample.
FA15341-20 MW-30
Methyl Tert Butyl Ether 0.25 J 0.50 0.10 ug/l SM 6200B
FA15341-21 WSW-4
1,2,4-Trimethylbenzene 0.30 J 0.50 0.10 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.19 J 0.50 0.10 ug/l SM 6200B
8 of 90
FA15341 2
Summary of Hits Page 5 of 5
Job Number:FA15341
Account:GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Collected:05/27/14
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA15341-22 WSW-6
Bromodichloromethane 1.2 0.50 0.10 ug/l SM 6200B
Bromoform 2.9 0.50 0.10 ug/l SM 6200B
Chloroform 0.82 0.50 0.10 ug/l SM 6200B
Dibromochloromethane 2.1 0.50 0.10 ug/l SM 6200B
(a) Associated CCV outside control limits.
9 of 90
FA15341 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
10 of 90
FA15341 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1R
Lab Sample ID:FA15341-1 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187171.D 1 06/03/14 TD n/a n/a VA1475
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 90
FA15341 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1R
Lab Sample ID:FA15341-1 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.0 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 90
FA15341 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA15341-2 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E030967.D 100 06/02/14 TD n/a n/a VE1039
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 4160 50 10 ug/l
108-86-1 Bromobenzene ND 50 10 ug/l
74-97-5 Bromochloromethane ND 50 10 ug/l
75-27-4 Bromodichloromethane ND 50 10 ug/l
75-25-2 Bromoform ND 50 10 ug/l
104-51-8 n-Butylbenzene 52.3 50 10 ug/l
135-98-8 sec-Butylbenzene 30.3 50 10 ug/l J
98-06-6 tert-Butylbenzene ND 50 10 ug/l
108-90-7 Chlorobenzene ND 50 10 ug/l
75-00-3 Chloroethane ND 50 12 ug/l
67-66-3 Chloroform ND 50 10 ug/l
95-49-8 o-Chlorotoluene ND 50 10 ug/l
106-43-4 p-Chlorotoluene ND 50 10 ug/l
56-23-5 Carbon tetrachloride ND 50 10 ug/l
75-34-3 1,1-Dichloroethane ND 50 10 ug/l
75-35-4 1,1-Dichloroethylene ND 50 10 ug/l
563-58-6 1,1-Dichloropropene ND 50 10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 17 ug/l
106-93-4 1,2-Dibromoethane ND 50 10 ug/l
107-06-2 1,2-Dichloroethane 73.2 50 10 ug/l
78-87-5 1,2-Dichloropropane ND 50 10 ug/l
142-28-9 1,3-Dichloropropane ND 50 10 ug/l
108-20-3 Di-Isopropyl ether 22.3 50 10 ug/l J
594-20-7 2,2-Dichloropropane ND 50 10 ug/l
124-48-1 Dibromochloromethane ND 50 10 ug/l
75-71-8 Dichlorodifluoromethane ND 50 10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 10 ug/l
541-73-1 m-Dichlorobenzene ND 50 10 ug/l
95-50-1 o-Dichlorobenzene ND 50 10 ug/l
106-46-7 p-Dichlorobenzene ND 50 10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 90
FA15341 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA15341-2 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 50 10 ug/l
100-41-4 Ethylbenzene 1400 50 10 ug/l
87-68-3 Hexachlorobutadiene ND 50 10 ug/l
98-82-8 Isopropylbenzene 105 50 10 ug/l
99-87-6 p-Isopropyltoluene 22.3 50 10 ug/l J
74-83-9 Methyl bromide ND 50 10 ug/l
74-87-3 Methyl chloride ND 50 10 ug/l
74-95-3 Methylene bromide ND 50 10 ug/l
75-09-2 Methylene chloride ND 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether 657 50 10 ug/l
91-20-3 Naphthalene 758 50 10 ug/l
103-65-1 n-Propylbenzene 263 50 10 ug/l
100-42-5 Styrene 16.7 50 10 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 50 10 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 10 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 10 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 10 ug/l
95-63-6 1,2,4-Trimethylbenzene 3220 50 10 ug/l
108-67-8 1,3,5-Trimethylbenzene 879 50 10 ug/l
127-18-4 Tetrachloroethylene ND 50 10 ug/l
108-88-3 Toluene 4880 50 10 ug/l
79-01-6 Trichloroethylene ND 50 10 ug/l
75-69-4 Trichlorofluoromethane ND 50 10 ug/l
75-01-4 Vinyl chloride ND 50 10 ug/l
1330-20-7 Xylene (total)10500 150 20 ug/l
m,p-Xylene 6890 100 10 ug/l
95-47-6 o-Xylene 3590 50 10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 94%70-130%
17060-07-0 1,2-Dichloroethane-D4 88%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 90
FA15341 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3R
Lab Sample ID:FA15341-3 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E030968.D 1 06/02/14 TD n/a n/a VE1039
Run #2 E031006.D 1 06/04/14 TD n/a n/a VE1041
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 4.2 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene 0.15 0.50 0.10 ug/l J
135-98-8 sec-Butylbenzene 0.18 0.50 0.10 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 90
FA15341 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3R
Lab Sample ID:FA15341-3 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 0.85 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 0.44 0.50 0.10 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 5.9 0.50 0.10 ug/l
91-20-3 Naphthalene 0.27 a 0.50 0.10 ug/l J
103-65-1 n-Propylbenzene 0.56 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.58 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)0.74 1.5 0.20 ug/l J
m,p-Xylene 0.44 1.0 0.10 ug/l J
95-47-6 o-Xylene 0.29 0.50 0.10 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%106%70-130%
17060-07-0 1,2-Dichloroethane-D4 94%107%70-130%
2037-26-5 Toluene-D8 102%101%70-130%
460-00-4 4-Bromofluorobenzene 103%105%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 90
FA15341 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4R
Lab Sample ID:FA15341-4 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187179.D 100 06/03/14 TD n/a n/a VA1475
Run #2 a A0187172.D 1 06/03/14 TD n/a n/a VA1475
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 792 50 10 ug/l
108-86-1 Bromobenzene ND 50 10 ug/l
74-97-5 Bromochloromethane ND 50 10 ug/l
75-27-4 Bromodichloromethane ND 50 10 ug/l
75-25-2 Bromoform ND 50 10 ug/l
104-51-8 n-Butylbenzene 55.7 50 10 ug/l
135-98-8 sec-Butylbenzene 27.2 50 10 ug/l J
98-06-6 tert-Butylbenzene ND 50 10 ug/l
108-90-7 Chlorobenzene ND 50 10 ug/l
75-00-3 Chloroethane ND 50 12 ug/l
67-66-3 Chloroform ND 50 10 ug/l
95-49-8 o-Chlorotoluene 79.1 50 10 ug/l
106-43-4 p-Chlorotoluene ND 50 10 ug/l
56-23-5 Carbon tetrachloride ND 50 10 ug/l
75-34-3 1,1-Dichloroethane ND 50 10 ug/l
75-35-4 1,1-Dichloroethylene ND 50 10 ug/l
563-58-6 1,1-Dichloropropene ND 50 10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 17 ug/l
106-93-4 1,2-Dibromoethane ND 50 10 ug/l
107-06-2 1,2-Dichloroethane 22.8 50 10 ug/l J
78-87-5 1,2-Dichloropropane ND 50 10 ug/l
142-28-9 1,3-Dichloropropane ND 50 10 ug/l
108-20-3 Di-Isopropyl ether ND 50 10 ug/l
594-20-7 2,2-Dichloropropane ND 50 10 ug/l
124-48-1 Dibromochloromethane ND 50 10 ug/l
75-71-8 Dichlorodifluoromethane ND 50 10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 50 10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 50 10 ug/l
541-73-1 m-Dichlorobenzene ND 50 10 ug/l
95-50-1 o-Dichlorobenzene ND 50 10 ug/l
106-46-7 p-Dichlorobenzene ND 50 10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 50 10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 90
FA15341 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-4R
Lab Sample ID:FA15341-4 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 50 10 ug/l
100-41-4 Ethylbenzene 1160 50 10 ug/l
87-68-3 Hexachlorobutadiene ND 50 10 ug/l
98-82-8 Isopropylbenzene 95.0 50 10 ug/l
99-87-6 p-Isopropyltoluene 13.3 50 10 ug/l J
74-83-9 Methyl bromide ND 50 10 ug/l
74-87-3 Methyl chloride ND 50 10 ug/l
74-95-3 Methylene bromide ND 50 10 ug/l
75-09-2 Methylene chloride ND 200 100 ug/l
1634-04-4 Methyl Tert Butyl Ether 604 50 10 ug/l
91-20-3 Naphthalene 550 50 10 ug/l
103-65-1 n-Propylbenzene 356 50 10 ug/l
100-42-5 Styrene 14.7 50 10 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 50 10 ug/l
71-55-6 1,1,1-Trichloroethane ND 50 10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 50 10 ug/l
79-00-5 1,1,2-Trichloroethane ND 50 11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 50 10 ug/l
96-18-4 1,2,3-Trichloropropane ND 50 12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 50 10 ug/l
95-63-6 1,2,4-Trimethylbenzene 2160 50 10 ug/l
108-67-8 1,3,5-Trimethylbenzene 605 50 10 ug/l
127-18-4 Tetrachloroethylene ND 50 10 ug/l
108-88-3 Toluene 3720 50 10 ug/l
79-01-6 Trichloroethylene ND 50 10 ug/l
75-69-4 Trichlorofluoromethane ND 50 10 ug/l
75-01-4 Vinyl chloride ND 50 10 ug/l
1330-20-7 Xylene (total)5660 150 20 ug/l
m,p-Xylene 3950 100 10 ug/l
95-47-6 o-Xylene 1710 50 10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 89%52% b 70-130%
17060-07-0 1,2-Dichloroethane-D4 82%131% b 70-130%
2037-26-5 Toluene-D8 100%97%70-130%
460-00-4 4-Bromofluorobenzene 96%129%70-130%
(a) Confirmation run for internal standard areas.
(b) Outside control limits due to matrix interference.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 90
FA15341 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5R
Lab Sample ID:FA15341-5 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031007.D 5 06/04/14 TD n/a n/a VE1041
Run #2 a A0187204.D 1 06/04/14 TD n/a n/a VA1476
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 145 2.5 0.50 ug/l
108-86-1 Bromobenzene ND 2.5 0.50 ug/l
74-97-5 Bromochloromethane ND 2.5 0.50 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.50 ug/l
75-25-2 Bromoform ND 2.5 0.50 ug/l
104-51-8 n-Butylbenzene b 2.7 2.5 0.50 ug/l J
135-98-8 sec-Butylbenzene 4.3 2.5 0.50 ug/l
98-06-6 tert-Butylbenzene b 0.70 2.5 0.50 ug/l J
108-90-7 Chlorobenzene ND 2.5 0.50 ug/l
75-00-3 Chloroethane ND 2.5 0.61 ug/l
67-66-3 Chloroform ND 2.5 0.50 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.50 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.50 ug/l
56-23-5 Carbon tetrachloride ND 2.5 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.50 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.50 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.50 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 0.86 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.50 ug/l
107-06-2 1,2-Dichloroethane 5.7 2.5 0.50 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.50 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.50 ug/l
108-20-3 Di-Isopropyl ether 1.9 2.5 0.50 ug/l J
594-20-7 2,2-Dichloropropane ND 2.5 0.50 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.50 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 0.50 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.50 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.50 ug/l
541-73-1 m-Dichlorobenzene ND 2.5 0.50 ug/l
95-50-1 o-Dichlorobenzene ND 2.5 0.50 ug/l
106-46-7 p-Dichlorobenzene ND 2.5 0.50 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.50 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 90
FA15341 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5R
Lab Sample ID:FA15341-5 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.50 ug/l
100-41-4 Ethylbenzene 114 2.5 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.50 ug/l
98-82-8 Isopropylbenzene 15.3 2.5 0.50 ug/l
99-87-6 p-Isopropyltoluene 2.8 2.5 0.50 ug/l
74-83-9 Methyl bromide ND 2.5 0.50 ug/l
74-87-3 Methyl chloride ND 2.5 0.50 ug/l
74-95-3 Methylene bromide ND 2.5 0.50 ug/l
75-09-2 Methylene chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 247 2.5 0.50 ug/l
91-20-3 Naphthalene 60.7 2.5 0.50 ug/l
103-65-1 n-Propylbenzene 21.5 2.5 0.50 ug/l
100-42-5 Styrene ND 2.5 0.50 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.50 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.50 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.53 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.59 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.50 ug/l
95-63-6 1,2,4-Trimethylbenzene 87.7 2.5 0.50 ug/l
108-67-8 1,3,5-Trimethylbenzene 11.9 2.5 0.50 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.50 ug/l
108-88-3 Toluene 7.8 2.5 0.50 ug/l
79-01-6 Trichloroethylene ND 2.5 0.50 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 0.50 ug/l
75-01-4 Vinyl chloride ND 2.5 0.50 ug/l
m,p-Xylene 25.6 5.0 0.50 ug/l
95-47-6 o-Xylene 14.3 2.5 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 115%110%70-130%
17060-07-0 1,2-Dichloroethane-D4 121%126%70-130%
2037-26-5 Toluene-D8 100%95%70-130%
460-00-4 4-Bromofluorobenzene 104%99%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
(b) Associated CCV outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 90
FA15341 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA15341-6 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187201.D 1 06/04/14 TD n/a n/a VA1476
Run #2 A0187180.D 1 06/03/14 TD n/a n/a VA1475
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND a 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND a 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 90
FA15341 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA15341-6 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%91%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%82%70-130%
2037-26-5 Toluene-D8 95%97%70-130%
460-00-4 4-Bromofluorobenzene 103%95%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 90
FA15341 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA15341-7 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E030982.D 1 06/03/14 TD n/a n/a VE1040
Run #2 E030992.D 10 06/03/14 TD n/a n/a VE1040
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 227 a 5.0 1.0 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene 4.2 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 3.5 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane 6.6 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 1.7 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 90
FA15341 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA15341-7 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 60.4 a 5.0 1.0 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 12.9 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene 1.3 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 1.5 0.50 0.10 ug/l
91-20-3 Naphthalene 44.1 a 5.0 1.0 ug/l
103-65-1 n-Propylbenzene 27.9 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 108 a 5.0 1.0 ug/l
108-67-8 1,3,5-Trimethylbenzene 12.2 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 3.7 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)158 a 15 2.0 ug/l
m,p-Xylene 114 a 10 1.0 ug/l
95-47-6 o-Xylene 44.1 a 5.0 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%102%70-130%
2037-26-5 Toluene-D8 96%101%70-130%
460-00-4 4-Bromofluorobenzene 102%105%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 90
FA15341 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA15341-8 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187202.D 1 06/04/14 TD n/a n/a VA1476
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane 7.2 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 1.8 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 90
FA15341 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA15341-8 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 37.3 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 115%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 90
FA15341 33.8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA15341-9 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187203.D 1 06/04/14 TD n/a n/a VA1476
Run #2 a A0187182.D 1 06/03/14 TD n/a n/a VA1475
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 90
FA15341 33.9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA15341-9 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%93%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%87%70-130%
2037-26-5 Toluene-D8 94%95%70-130%
460-00-4 4-Bromofluorobenzene 102%98%70-130%
(a) Confirmation run for internal standard areas.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 90
FA15341 33.9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-15
Lab Sample ID:FA15341-10 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187183.D 1 06/03/14 TD n/a n/a VA1475
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 90
FA15341 33.10
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-15
Lab Sample ID:FA15341-10 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 93%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 90
FA15341 33.10
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-16
Lab Sample ID:FA15341-11 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187184.D 1 06/03/14 TD n/a n/a VA1475
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 90
FA15341 33.11
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-16
Lab Sample ID:FA15341-11 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 90
FA15341 33.11
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-17
Lab Sample ID:FA15341-12 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187185.D 1 06/03/14 TD n/a n/a VA1475
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 90
FA15341 33.12
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-17
Lab Sample ID:FA15341-12 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 90
FA15341 33.12
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-18
Lab Sample ID:FA15341-13 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E030993.D 1 06/03/14 TD n/a n/a VE1040
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 90
FA15341 33.13
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-18
Lab Sample ID:FA15341-13 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 90
FA15341 33.13
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-19
Lab Sample ID:FA15341-14 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031012.D 1 06/04/14 TD n/a n/a VE1041
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 90
FA15341 33.14
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-19
Lab Sample ID:FA15341-14 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 94%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 90
FA15341 33.14
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-21
Lab Sample ID:FA15341-15 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E031010.D 1 06/04/14 TD n/a n/a VE1041
Run #2 E030995.D 1 06/03/14 TD n/a n/a VE1040
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 90
FA15341 33.15
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-21
Lab Sample ID:FA15341-15 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.21 0.50 0.10 ug/l J
91-20-3 Naphthalene ND a 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.11 0.50 0.10 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 93%107%70-130%
17060-07-0 1,2-Dichloroethane-D4 89%112%70-130%
2037-26-5 Toluene-D8 102%99%70-130%
460-00-4 4-Bromofluorobenzene 102%105%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 90
FA15341 33.15
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-23
Lab Sample ID:FA15341-16 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E030996.D 1 06/03/14 TD n/a n/a VE1040
Run #2 E031008.D 2.5 06/04/14 TD n/a n/a VE1041
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 107 a 1.3 0.25 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene 0.95 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 1.3 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane 1.4 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane 16.4 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 90
FA15341 33.16
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-23
Lab Sample ID:FA15341-16 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 38.7 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 8.2 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene 2.2 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene 27.4 0.50 0.10 ug/l
103-65-1 n-Propylbenzene 12.0 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 41.1 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene 6.5 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 4.3 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)45.8 1.5 0.20 ug/l
m,p-Xylene 33.0 1.0 0.10 ug/l
95-47-6 o-Xylene 12.7 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%105%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%109%70-130%
2037-26-5 Toluene-D8 98%99%70-130%
460-00-4 4-Bromofluorobenzene 104%103%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 90
FA15341 33.16
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-25
Lab Sample ID:FA15341-17 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E030997.D 1 06/03/14 TD n/a n/a VE1040
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
43 of 90
FA15341 33.17
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-25
Lab Sample ID:FA15341-17 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.56 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 90
FA15341 33.17
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-27
Lab Sample ID:FA15341-18 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187186.D 1 06/03/14 TD n/a n/a VA1475
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
45 of 90
FA15341 33.18
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-27
Lab Sample ID:FA15341-18 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 91%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 90
FA15341 33.18
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-28
Lab Sample ID:FA15341-19 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187196.D 1 06/04/14 TD n/a n/a VA1476
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
47 of 90
FA15341 33.19
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-28
Lab Sample ID:FA15341-19 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
48 of 90
FA15341 33.19
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-30
Lab Sample ID:FA15341-20 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187197.D 1 06/04/14 TD n/a n/a VA1476
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
49 of 90
FA15341 33.20
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-30
Lab Sample ID:FA15341-20 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.25 0.50 0.10 ug/l J
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
50 of 90
FA15341 33.20
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-4
Lab Sample ID:FA15341-21 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187198.D 1 06/04/14 TD n/a n/a VA1476
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
51 of 90
FA15341 33.21
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-4
Lab Sample ID:FA15341-21 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.30 0.50 0.10 ug/l J
108-67-8 1,3,5-Trimethylbenzene 0.19 0.50 0.10 ug/l J
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
52 of 90
FA15341 33.21
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-6
Lab Sample ID:FA15341-22 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0187199.D 1 06/04/14 TD n/a n/a VA1476
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane 1.2 0.50 0.10 ug/l
75-25-2 Bromoform 2.9 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform 0.82 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane 2.1 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
53 of 90
FA15341 33.22
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-6
Lab Sample ID:FA15341-22 Date Sampled:05/27/14
Matrix:AQ - Ground Water Date Received:05/28/14
Method:SM 6200B Percent Solids:n/a
Project:Ram 21, 1121 NC561 W, Saint John, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
54 of 90
FA15341 33.22
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
55 of 90
FA15341 4
FA15341: Chain of Custody
Page 1 of 4
56 of 90
FA15341 44.1
FA15341: Chain of Custody
Page 2 of 4
57 of 90
FA15341 44.1
FA15341: Chain of Custody
Page 3 of 4
58 of 90
FA15341 44.1
FA15341: Chain of Custody
Page 4 of 4
59 of 90
FA15341 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
60 of 90
FA15341 5
Method Blank Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1039-MB E030943.D 1 06/02/14 TD n/a n/a VE1039
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-2, FA15341-3
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
61 of 90
FA15341 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1039-MB E030943.D 1 06/02/14 TD n/a n/a VE1039
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-2, FA15341-3
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
62 of 90
FA15341 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1040-MB E030976.D 1 06/03/14 TD n/a n/a VE1040
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-7, FA15341-13, FA15341-15, FA15341-16, FA15341-17
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
63 of 90
FA15341 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1040-MB E030976.D 1 06/03/14 TD n/a n/a VE1040
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-7, FA15341-13, FA15341-15, FA15341-16, FA15341-17
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
64 of 90
FA15341 55.1.2
Method Blank Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1475-MB A0187162.D 1 06/03/14 TD n/a n/a VA1475
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-1, FA15341-4, FA15341-6, FA15341-10, FA15341-11, FA15341-12, FA15341-18
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
65 of 90
FA15341 55.1.3
Method Blank Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1475-MB A0187162.D 1 06/03/14 TD n/a n/a VA1475
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-1, FA15341-4, FA15341-6, FA15341-10, FA15341-11, FA15341-12, FA15341-18
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 95%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
66 of 90
FA15341 55.1.3
Method Blank Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1041-MB E031005.D 1 06/04/14 TD n/a n/a VE1041
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-3, FA15341-5, FA15341-14, FA15341-15, FA15341-16
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
67 of 90
FA15341 55.1.4
Method Blank Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1041-MB E031005.D 1 06/04/14 TD n/a n/a VE1041
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-3, FA15341-5, FA15341-14, FA15341-15, FA15341-16
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
68 of 90
FA15341 55.1.4
Method Blank Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1476-MB A0187195.D 1 06/04/14 TD n/a n/a VA1476
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-6, FA15341-8, FA15341-9, FA15341-19, FA15341-20, FA15341-21, FA15341-22
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.12 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.17 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
69 of 90
FA15341 55.1.5
Method Blank Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1476-MB A0187195.D 1 06/04/14 TD n/a n/a VA1476
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-6, FA15341-8, FA15341-9, FA15341-19, FA15341-20, FA15341-21, FA15341-22
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.10 ug/l
74-87-3 Methyl chloride ND 0.50 0.10 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.10 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.11 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.12 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.20 ug/l
m,p-Xylene ND 1.0 0.10 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 108%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
70 of 90
FA15341 55.1.5
Blank Spike Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1039-BS E030942.D 1 06/02/14 TD n/a n/a VE1039
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-2, FA15341-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.8 98 70-130
108-86-1 Bromobenzene 10 10.1 101 70-130
74-97-5 Bromochloromethane 10 10.1 101 70-130
75-27-4 Bromodichloromethane 10 10.0 100 70-130
75-25-2 Bromoform 10 9.7 97 70-130
104-51-8 n-Butylbenzene 10 10.3 103 70-130
135-98-8 sec-Butylbenzene 10 11.5 115 70-130
98-06-6 tert-Butylbenzene 10 11.6 116 70-130
108-90-7 Chlorobenzene 10 10.7 107 70-130
75-00-3 Chloroethane 10 9.4 94 60-140
67-66-3 Chloroform 10 9.7 97 70-130
95-49-8 o-Chlorotoluene 10 11.1 111 70-130
106-43-4 p-Chlorotoluene 10 11.5 115 70-130
56-23-5 Carbon tetrachloride 10 10.6 106 70-130
75-34-3 1,1-Dichloroethane 10 10.0 100 70-130
75-35-4 1,1-Dichloroethylene 10 10.9 109 70-130
563-58-6 1,1-Dichloropropene 10 11.0 110 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.4 94 70-130
106-93-4 1,2-Dibromoethane 10 10.2 102 70-130
107-06-2 1,2-Dichloroethane 10 10.2 102 70-130
78-87-5 1,2-Dichloropropane 10 9.5 95 70-130
142-28-9 1,3-Dichloropropane 10 9.8 98 70-130
108-20-3 Di-Isopropyl ether 10 9.5 95 70-130
594-20-7 2,2-Dichloropropane 10 11.1 111 70-130
124-48-1 Dibromochloromethane 10 10.2 102 70-130
75-71-8 Dichlorodifluoromethane 10 8.7 87 60-140
156-59-2 cis-1,2-Dichloroethylene 10 10.2 102 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.8 98 70-130
541-73-1 m-Dichlorobenzene 10 11.3 113 70-130
95-50-1 o-Dichlorobenzene 10 10.9 109 70-130
106-46-7 p-Dichlorobenzene 10 9.8 98 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10 100 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.0 110 70-130
100-41-4 Ethylbenzene 10 10.0 100 70-130
87-68-3 Hexachlorobutadiene 10 10.8 108 70-130
98-82-8 Isopropylbenzene 10 11.6 116 70-130
* = Outside of Control Limits.
71 of 90
FA15341 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1039-BS E030942.D 1 06/02/14 TD n/a n/a VE1039
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-2, FA15341-3
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.7 117 70-130
74-83-9 Methyl bromide 10 9.9 99 60-140
74-87-3 Methyl chloride 10 9.4 94 60-140
74-95-3 Methylene bromide 10 9.6 96 70-130
75-09-2 Methylene chloride 10 9.7 97 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.4 104 70-130
91-20-3 Naphthalene 10 9.9 99 70-130
103-65-1 n-Propylbenzene 10 11.3 113 70-130
100-42-5 Styrene 10 10.2 102 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.4 104 70-130
71-55-6 1,1,1-Trichloroethane 10 10.6 106 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.6 96 70-130
79-00-5 1,1,2-Trichloroethane 10 9.4 94 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.9 99 70-130
96-18-4 1,2,3-Trichloropropane 10 9.9 99 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10 100 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.5 105 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.6 106 70-130
127-18-4 Tetrachloroethylene 10 10.4 104 70-130
108-88-3 Toluene 10 9.9 99 70-130
79-01-6 Trichloroethylene 10 10.0 100 70-130
75-69-4 Trichlorofluoromethane 10 9.3 93 60-140
75-01-4 Vinyl chloride 10 9.6 96 60-140
1330-20-7 Xylene (total)30 33.1 110 70-130
m,p-Xylene 20 21.7 109 70-130
95-47-6 o-Xylene 10 11.4 114 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
* = Outside of Control Limits.
72 of 90
FA15341 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1040-BS E030974.D 1 06/03/14 TD n/a n/a VE1040
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-7, FA15341-13, FA15341-15, FA15341-16, FA15341-17
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.8 98 70-130
108-86-1 Bromobenzene 10 10.2 102 70-130
74-97-5 Bromochloromethane 10 10.2 102 70-130
75-27-4 Bromodichloromethane 10 9.6 96 70-130
75-25-2 Bromoform 10 9.5 95 70-130
104-51-8 n-Butylbenzene 10 10.5 105 70-130
135-98-8 sec-Butylbenzene 10 11.7 117 70-130
98-06-6 tert-Butylbenzene 10 11.3 113 70-130
108-90-7 Chlorobenzene 10 10.7 107 70-130
75-00-3 Chloroethane 10 10.9 109 60-140
67-66-3 Chloroform 10 9.5 95 70-130
95-49-8 o-Chlorotoluene 10 11.0 110 70-130
106-43-4 p-Chlorotoluene 10 11.7 117 70-130
56-23-5 Carbon tetrachloride 10 9.7 97 70-130
75-34-3 1,1-Dichloroethane 10 9.7 97 70-130
75-35-4 1,1-Dichloroethylene 10 10.3 103 70-130
563-58-6 1,1-Dichloropropene 10 10.5 105 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.2 92 70-130
106-93-4 1,2-Dibromoethane 10 10.4 104 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
78-87-5 1,2-Dichloropropane 10 9.6 96 70-130
142-28-9 1,3-Dichloropropane 10 10.2 102 70-130
108-20-3 Di-Isopropyl ether 10 9.4 94 70-130
594-20-7 2,2-Dichloropropane 10 10.1 101 70-130
124-48-1 Dibromochloromethane 10 10.0 100 70-130
75-71-8 Dichlorodifluoromethane 10 9.4 94 60-140
156-59-2 cis-1,2-Dichloroethylene 10 10 100 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.6 96 70-130
541-73-1 m-Dichlorobenzene 10 11.1 111 70-130
95-50-1 o-Dichlorobenzene 10 10.8 108 70-130
106-46-7 p-Dichlorobenzene 10 10.0 100 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.6 96 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.8 108 70-130
100-41-4 Ethylbenzene 10 10.1 101 70-130
87-68-3 Hexachlorobutadiene 10 10.5 105 70-130
98-82-8 Isopropylbenzene 10 11.5 115 70-130
* = Outside of Control Limits.
73 of 90
FA15341 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1040-BS E030974.D 1 06/03/14 TD n/a n/a VE1040
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-7, FA15341-13, FA15341-15, FA15341-16, FA15341-17
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.7 117 70-130
74-83-9 Methyl bromide 10 11.1 111 60-140
74-87-3 Methyl chloride 10 11.0 110 60-140
74-95-3 Methylene bromide 10 9.1 91 70-130
75-09-2 Methylene chloride 10 9.3 93 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.1 101 70-130
91-20-3 Naphthalene 10 10.5 105 70-130
103-65-1 n-Propylbenzene 10 11.4 114 70-130
100-42-5 Styrene 10 10.2 102 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.1 101 70-130
71-55-6 1,1,1-Trichloroethane 10 9.7 97 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10 100 70-130
79-00-5 1,1,2-Trichloroethane 10 9.9 99 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.8 98 70-130
96-18-4 1,2,3-Trichloropropane 10 10.0 100 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.0 100 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.1 101 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.6 106 70-130
127-18-4 Tetrachloroethylene 10 10.4 104 70-130
108-88-3 Toluene 10 10.2 102 70-130
79-01-6 Trichloroethylene 10 9.7 97 70-130
75-69-4 Trichlorofluoromethane 10 10.0 100 60-140
75-01-4 Vinyl chloride 10 11.5 115 60-140
1330-20-7 Xylene (total)30 32.8 109 70-130
m,p-Xylene 20 21.5 108 70-130
95-47-6 o-Xylene 10 11.3 113 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 96%70-130%
17060-07-0 1,2-Dichloroethane-D4 93%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
* = Outside of Control Limits.
74 of 90
FA15341 55.2.2
Blank Spike Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1475-BS A0187160.D 1 06/03/14 TD n/a n/a VA1475
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-1, FA15341-4, FA15341-6, FA15341-10, FA15341-11, FA15341-12, FA15341-18
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.4 94 70-130
108-86-1 Bromobenzene 10 8.5 85 70-130
74-97-5 Bromochloromethane 10 9.5 95 70-130
75-27-4 Bromodichloromethane 10 8.3 83 70-130
75-25-2 Bromoform 10 7.9 79 70-130
104-51-8 n-Butylbenzene 10 8.4 84 70-130
135-98-8 sec-Butylbenzene 10 9.2 92 70-130
98-06-6 tert-Butylbenzene 10 8.2 82 70-130
108-90-7 Chlorobenzene 10 9.1 91 70-130
75-00-3 Chloroethane 10 8.6 86 60-140
67-66-3 Chloroform 10 8.4 84 70-130
95-49-8 o-Chlorotoluene 10 8.6 86 70-130
106-43-4 p-Chlorotoluene 10 9.0 90 70-130
56-23-5 Carbon tetrachloride 10 7.8 78 70-130
75-34-3 1,1-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 9.5 95 70-130
563-58-6 1,1-Dichloropropene 10 9.2 92 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.3 73 70-130
106-93-4 1,2-Dibromoethane 10 9.1 91 70-130
107-06-2 1,2-Dichloroethane 10 8.5 85 70-130
78-87-5 1,2-Dichloropropane 10 10 100 70-130
142-28-9 1,3-Dichloropropane 10 9.0 90 70-130
108-20-3 Di-Isopropyl ether 10 10.5 105 70-130
594-20-7 2,2-Dichloropropane 10 8.1 81 70-130
124-48-1 Dibromochloromethane 10 8.2 82 70-130
75-71-8 Dichlorodifluoromethane 10 9.3 93 60-140
156-59-2 cis-1,2-Dichloroethylene 10 9.2 92 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.9 89 70-130
541-73-1 m-Dichlorobenzene 10 9.3 93 70-130
95-50-1 o-Dichlorobenzene 10 8.9 89 70-130
106-46-7 p-Dichlorobenzene 10 8.4 84 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.0 90 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.1 91 70-130
100-41-4 Ethylbenzene 10 8.2 82 70-130
87-68-3 Hexachlorobutadiene 10 7.8 78 70-130
98-82-8 Isopropylbenzene 10 8.8 88 70-130
* = Outside of Control Limits.
75 of 90
FA15341 55.2.3
Blank Spike Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1475-BS A0187160.D 1 06/03/14 TD n/a n/a VA1475
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-1, FA15341-4, FA15341-6, FA15341-10, FA15341-11, FA15341-12, FA15341-18
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 8.8 88 70-130
74-83-9 Methyl bromide 10 8.0 80 60-140
74-87-3 Methyl chloride 10 11.3 113 60-140
74-95-3 Methylene bromide 10 8.9 89 70-130
75-09-2 Methylene chloride 10 10.5 105 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.0 90 70-130
91-20-3 Naphthalene 10 8.5 85 70-130
103-65-1 n-Propylbenzene 10 9.1 91 70-130
100-42-5 Styrene 10 8.8 88 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 7.9 79 70-130
71-55-6 1,1,1-Trichloroethane 10 7.9 79 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.8 88 70-130
79-00-5 1,1,2-Trichloroethane 10 9.2 92 70-130
87-61-6 1,2,3-Trichlorobenzene 10 8.3 83 70-130
96-18-4 1,2,3-Trichloropropane 10 8.6 86 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.2 82 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.0 80 70-130
108-67-8 1,3,5-Trimethylbenzene 10 7.9 79 70-130
127-18-4 Tetrachloroethylene 10 8.4 84 70-130
108-88-3 Toluene 10 8.3 83 70-130
79-01-6 Trichloroethylene 10 8.5 85 70-130
75-69-4 Trichlorofluoromethane 10 7.7 77 60-140
75-01-4 Vinyl chloride 10 9.1 91 60-140
1330-20-7 Xylene (total)30 25.6 85 70-130
m,p-Xylene 20 16.8 84 70-130
95-47-6 o-Xylene 10 8.8 88 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 96%70-130%
17060-07-0 1,2-Dichloroethane-D4 92%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
76 of 90
FA15341 55.2.3
Blank Spike Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1041-BS E031003.D 1 06/04/14 TD n/a n/a VE1041
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-3, FA15341-5, FA15341-14, FA15341-15, FA15341-16
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.0 110 70-130
108-86-1 Bromobenzene 10 11.4 114 70-130
74-97-5 Bromochloromethane 10 11.0 110 70-130
75-27-4 Bromodichloromethane 10 10.8 108 70-130
75-25-2 Bromoform 10 10.6 106 70-130
104-51-8 n-Butylbenzene 10 11.9 119 70-130
135-98-8 sec-Butylbenzene 10 12.7 127 70-130
98-06-6 tert-Butylbenzene 10 12.9 129 70-130
108-90-7 Chlorobenzene 10 11.7 117 70-130
75-00-3 Chloroethane 10 11.0 110 60-140
67-66-3 Chloroform 10 10.7 107 70-130
95-49-8 o-Chlorotoluene 10 12.5 125 70-130
106-43-4 p-Chlorotoluene 10 12.9 129 70-130
56-23-5 Carbon tetrachloride 10 11.2 112 70-130
75-34-3 1,1-Dichloroethane 10 10.6 106 70-130
75-35-4 1,1-Dichloroethylene 10 11.6 116 70-130
563-58-6 1,1-Dichloropropene 10 11.9 119 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10.7 107 70-130
106-93-4 1,2-Dibromoethane 10 11.4 114 70-130
107-06-2 1,2-Dichloroethane 10 10.4 104 70-130
78-87-5 1,2-Dichloropropane 10 10.5 105 70-130
142-28-9 1,3-Dichloropropane 10 11.0 110 70-130
108-20-3 Di-Isopropyl ether 10 10.2 102 70-130
594-20-7 2,2-Dichloropropane 10 12.0 120 70-130
124-48-1 Dibromochloromethane 10 11.2 112 70-130
75-71-8 Dichlorodifluoromethane 10 9.5 95 60-140
156-59-2 cis-1,2-Dichloroethylene 10 11.1 111 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.8 108 70-130
541-73-1 m-Dichlorobenzene 10 12.5 125 70-130
95-50-1 o-Dichlorobenzene 10 11.9 119 70-130
106-46-7 p-Dichlorobenzene 10 11.3 113 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.6 106 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.9 119 70-130
100-41-4 Ethylbenzene 10 11.0 110 70-130
87-68-3 Hexachlorobutadiene 10 12.1 121 70-130
98-82-8 Isopropylbenzene 10 12.7 127 70-130
* = Outside of Control Limits.
77 of 90
FA15341 55.2.4
Blank Spike Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1041-BS E031003.D 1 06/04/14 TD n/a n/a VE1041
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-3, FA15341-5, FA15341-14, FA15341-15, FA15341-16
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 13.0 130 70-130
74-83-9 Methyl bromide 10 11.5 115 60-140
74-87-3 Methyl chloride 10 10.5 105 60-140
74-95-3 Methylene bromide 10 10.7 107 70-130
75-09-2 Methylene chloride 10 10.2 102 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.3 113 70-130
91-20-3 Naphthalene 10 11.3 113 70-130
103-65-1 n-Propylbenzene 10 12.8 128 70-130
100-42-5 Styrene 10 11.3 113 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.1 111 70-130
71-55-6 1,1,1-Trichloroethane 10 11.3 113 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 11.0 110 70-130
79-00-5 1,1,2-Trichloroethane 10 10.9 109 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.1 111 70-130
96-18-4 1,2,3-Trichloropropane 10 11.3 113 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.0 110 70-130
95-63-6 1,2,4-Trimethylbenzene 10 12.0 120 70-130
108-67-8 1,3,5-Trimethylbenzene 10 12.0 120 70-130
127-18-4 Tetrachloroethylene 10 11.2 112 70-130
108-88-3 Toluene 10 11.1 111 70-130
79-01-6 Trichloroethylene 10 11.0 110 70-130
75-69-4 Trichlorofluoromethane 10 7.0 70 60-140
75-01-4 Vinyl chloride 10 11.5 115 60-140
1330-20-7 Xylene (total)30 36.1 120 70-130
m,p-Xylene 20 23.6 118 70-130
95-47-6 o-Xylene 10 12.5 125 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 95%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
* = Outside of Control Limits.
78 of 90
FA15341 55.2.4
Blank Spike Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1476-BS A0187193.D 1 06/04/14 TD n/a n/a VA1476
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-6, FA15341-8, FA15341-9, FA15341-19, FA15341-20, FA15341-21, FA15341-22
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.2 102 70-130
108-86-1 Bromobenzene 10 9.3 93 70-130
74-97-5 Bromochloromethane 10 10.4 104 70-130
75-27-4 Bromodichloromethane 10 10.1 101 70-130
75-25-2 Bromoform 10 9.3 93 70-130
104-51-8 n-Butylbenzene 10 9.3 93 70-130
135-98-8 sec-Butylbenzene 10 10.3 103 70-130
98-06-6 tert-Butylbenzene 10 9.7 97 70-130
108-90-7 Chlorobenzene 10 10.1 101 70-130
75-00-3 Chloroethane 10 8.2 82 60-140
67-66-3 Chloroform 10 9.6 96 70-130
95-49-8 o-Chlorotoluene 10 9.6 96 70-130
106-43-4 p-Chlorotoluene 10 10.1 101 70-130
56-23-5 Carbon tetrachloride 10 9.6 96 70-130
75-34-3 1,1-Dichloroethane 10 10.3 103 70-130
75-35-4 1,1-Dichloroethylene 10 11.0 110 70-130
563-58-6 1,1-Dichloropropene 10 10.4 104 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.8 88 70-130
106-93-4 1,2-Dibromoethane 10 10.0 100 70-130
107-06-2 1,2-Dichloroethane 10 10.4 104 70-130
78-87-5 1,2-Dichloropropane 10 11.1 111 70-130
142-28-9 1,3-Dichloropropane 10 10.2 102 70-130
108-20-3 Di-Isopropyl ether 10 12.2 122 70-130
594-20-7 2,2-Dichloropropane 10 9.9 99 70-130
124-48-1 Dibromochloromethane 10 9.7 97 70-130
75-71-8 Dichlorodifluoromethane 10 9.8 98 60-140
156-59-2 cis-1,2-Dichloroethylene 10 10.1 101 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.4 104 70-130
541-73-1 m-Dichlorobenzene 10 10.2 102 70-130
95-50-1 o-Dichlorobenzene 10 10 100 70-130
106-46-7 p-Dichlorobenzene 10 9.2 92 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.2 102 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.9 109 70-130
100-41-4 Ethylbenzene 10 9.2 92 70-130
87-68-3 Hexachlorobutadiene 10 8.8 88 70-130
98-82-8 Isopropylbenzene 10 10.3 103 70-130
* = Outside of Control Limits.
79 of 90
FA15341 55.2.5
Blank Spike Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1476-BS A0187193.D 1 06/04/14 TD n/a n/a VA1476
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-6, FA15341-8, FA15341-9, FA15341-19, FA15341-20, FA15341-21, FA15341-22
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.9 99 70-130
74-83-9 Methyl bromide 10 8.2 82 60-140
74-87-3 Methyl chloride 10 11.5 115 60-140
74-95-3 Methylene bromide 10 10.5 105 70-130
75-09-2 Methylene chloride 10 12.4 124 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.2 102 70-130
91-20-3 Naphthalene 10 9.7 97 70-130
103-65-1 n-Propylbenzene 10 10.1 101 70-130
100-42-5 Styrene 10 9.8 98 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.3 93 70-130
71-55-6 1,1,1-Trichloroethane 10 9.6 96 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.6 96 70-130
79-00-5 1,1,2-Trichloroethane 10 9.9 99 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.3 93 70-130
96-18-4 1,2,3-Trichloropropane 10 9.4 94 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.1 91 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.0 90 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.8 88 70-130
127-18-4 Tetrachloroethylene 10 9.5 95 70-130
108-88-3 Toluene 10 9.2 92 70-130
79-01-6 Trichloroethylene 10 9.9 99 70-130
75-69-4 Trichlorofluoromethane 10 8.3 83 60-140
75-01-4 Vinyl chloride 10 9.2 92 60-140
1330-20-7 Xylene (total)30 29.2 97 70-130
m,p-Xylene 20 19.0 95 70-130
95-47-6 o-Xylene 10 10.2 102 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
* = Outside of Control Limits.
80 of 90
FA15341 55.2.5
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15305-22MS E030952.D 100 06/02/14 TD n/a n/a VE1039
FA15305-22MSD E030954.D 100 06/02/14 TD n/a n/a VE1039
FA15305-22 E030950.D 100 06/02/14 TD n/a n/a VE1039
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-2, FA15341-3
FA15305-22 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 3580 1000 4500 92 1000 4350 77 3 70-130/20
108-86-1 Bromobenzene ND 1000 1040 104 1000 1030 103 1 70-130/20
74-97-5 Bromochloromethane ND 1000 1030 103 1000 1050 105 2 70-130/20
75-27-4 Bromodichloromethane ND 1000 1130 113 1000 951 95 17 70-130/20
75-25-2 Bromoform ND 1000 1050 105 1000 722 72 37*70-130/20
104-51-8 n-Butylbenzene 54.0 1000 1490 144*1000 1440 139*3 70-130/20
135-98-8 sec-Butylbenzene 32.1 J 1000 1430 140*1000 1390 136*3 70-130/20
98-06-6 tert-Butylbenzene ND 1000 1320 132*1000 1200 120 10 70-130/20
108-90-7 Chlorobenzene ND 1000 1140 114 1000 1090 109 4 70-130/20
75-00-3 Chloroethane ND 1000 954 95 1000 819 82 15 60-140/20
67-66-3 Chloroform ND 1000 1170 117 1000 1050 105 11 70-130/20
95-49-8 o-Chlorotoluene ND 1000 1360 136*1000 1300 130 5 70-130/20
106-43-4 p-Chlorotoluene ND 1000 1240 124 1000 1190 119 4 70-130/20
56-23-5 Carbon tetrachloride ND 1000 1200 120 1000 997 100 18 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 1060 106 1000 982 98 8 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 1200 120 1000 1070 107 11 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 1170 117 1000 1090 109 7 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 1190 119 1000 1080 108 10 70-130/20
106-93-4 1,2-Dibromoethane ND 1000 1110 111 1000 1140 114 3 70-130/20
107-06-2 1,2-Dichloroethane ND 1000 1190 119 1000 1020 102 15 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 1050 105 1000 1010 101 4 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 1050 105 1000 1090 109 4 70-130/20
108-20-3 Di-Isopropyl ether 36.0 J 1000 1040 100 1000 1020 98 2 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 1210 121 1000 1000 100 19 70-130/20
124-48-1 Dibromochloromethane ND 1000 1120 112 1000 902 90 22*70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 918 92 1000 732 73 23*60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 1050 105 1000 1040 104 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 1050 105 1000 998 100 5 70-130/20
541-73-1 m-Dichlorobenzene ND 1000 1200 120 1000 1140 114 5 70-130/20
95-50-1 o-Dichlorobenzene ND 1000 1160 116 1000 1140 114 2 70-130/20
106-46-7 p-Dichlorobenzene ND 1000 1080 108 1000 1040 104 4 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 1060 106 1000 964 96 9 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 1210 121 1000 1140 114 6 70-130/20
100-41-4 Ethylbenzene 4240 1000 7430 319* a 1000 7050 281* a 5 70-130/20
87-68-3 Hexachlorobutadiene ND 1000 1210 121 1000 1040 104 15 70-130/20
98-82-8 Isopropylbenzene 201 1000 1850 165*1000 1750 155*6 70-130/20
* = Outside of Control Limits.
81 of 90
FA15341 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15305-22MS E030952.D 100 06/02/14 TD n/a n/a VE1039
FA15305-22MSD E030954.D 100 06/02/14 TD n/a n/a VE1039
FA15305-22 E030950.D 100 06/02/14 TD n/a n/a VE1039
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-2, FA15341-3
FA15305-22 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 19.4 J 1000 1380 136*1000 1330 131*4 70-130/20
74-83-9 Methyl bromide ND 1000 999 100 1000 867 87 14 60-140/20
74-87-3 Methyl chloride ND 1000 885 89 1000 797 80 10 60-140/20
74-95-3 Methylene bromide ND 1000 1140 114 1000 1060 106 7 70-130/20
75-09-2 Methylene chloride ND 1000 1050 105 1000 988 99 6 70-130/20
1634-04-4 Methyl Tert Butyl Ether 771 1000 1860 109 1000 1820 105 2 70-130/20
91-20-3 Naphthalene 790 1000 2640 185*1000 2590 180*2 70-130/20
103-65-1 n-Propylbenzene 659 1000 3150 249*1000 3090 243*2 70-130/20
100-42-5 Styrene ND 1000 1150 115 1000 1090 109 5 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 1160 116 1000 1060 106 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 1190 119 1000 996 100 18 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 1070 107 1000 1150 115 7 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 1030 103 1000 1110 111 7 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 1110 111 1000 1010 101 9 70-130/20
96-18-4 1,2,3-Trichloropropane ND 1000 1140 114 1000 1110 111 3 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 1130 113 1000 1040 104 8 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2710 1000 8060 535* a 1000 7810 510* a 3 70-130/20
108-67-8 1,3,5-Trimethylbenzene 420 1000 2360 194*1000 2300 188*3 70-130/20
127-18-4 Tetrachloroethylene ND 1000 1100 110 1000 1040 104 6 70-130/20
108-88-3 Toluene 391 1000 1480 109 1000 1470 108 1 70-130/20
79-01-6 Trichloroethylene ND 1000 1200 120 1000 1090 109 10 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 999 100 1000 784 78 24*60-140/20
75-01-4 Vinyl chloride ND 1000 939 94 1000 839 84 11 60-140/20
1330-20-7 Xylene (total)4800 3000 11200 213*3000 10500 190*6 70-130/20
m,p-Xylene 4700 2000 9770 254* a 2000 9080 219* a 7 70-130/20
95-47-6 o-Xylene 103 1000 1460 136*1000 1370 127 6 70-130/20
CAS No.Surrogate Recoveries MS MSD FA15305-22 Limits
1868-53-7 Dibromofluoromethane 101%95%105%70-130%
17060-07-0 1,2-Dichloroethane-D4 116%100%112%70-130%
2037-26-5 Toluene-D8 98%103%100%70-130%
460-00-4 4-Bromofluorobenzene 108%110%105%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
82 of 90
FA15341 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15340-8MS E030987.D 50 06/03/14 TD n/a n/a VE1040
FA15340-8MSD E030988.D 50 06/03/14 TD n/a n/a VE1040
FA15340-8 a E030984.D 50 06/03/14 TD n/a n/a VE1040
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-7, FA15341-13, FA15341-15, FA15341-16, FA15341-17
FA15340-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 546 500 1100 111 500 1050 101 5 70-130/20
108-86-1 Bromobenzene ND 500 567 113 500 555 111 2 70-130/20
74-97-5 Bromochloromethane ND 500 576 115 500 549 110 5 70-130/20
75-27-4 Bromodichloromethane ND 500 572 114 500 565 113 1 70-130/20
75-25-2 Bromoform ND 500 523 105 500 497 99 5 70-130/20
104-51-8 n-Butylbenzene ND 500 587 117 500 577 115 2 70-130/20
135-98-8 sec-Butylbenzene ND 500 655 131*500 640 128 2 70-130/20
98-06-6 tert-Butylbenzene ND 500 668 134*500 648 130 3 70-130/20
108-90-7 Chlorobenzene ND 500 609 122 500 585 117 4 70-130/20
75-00-3 Chloroethane ND 500 540 108 500 520 104 4 60-140/20
67-66-3 Chloroform ND 500 564 113 500 548 110 3 70-130/20
95-49-8 o-Chlorotoluene ND 500 634 127 500 613 123 3 70-130/20
106-43-4 p-Chlorotoluene ND 500 662 132*500 637 127 4 70-130/20
56-23-5 Carbon tetrachloride ND 500 611 122 500 573 115 6 70-130/20
75-34-3 1,1-Dichloroethane ND 500 560 112 500 544 109 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 500 610 122 500 577 115 6 70-130/20
563-58-6 1,1-Dichloropropene ND 500 628 126 500 592 118 6 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 500 559 112 500 544 109 3 70-130/20
106-93-4 1,2-Dibromoethane ND 500 595 119 500 565 113 5 70-130/20
107-06-2 1,2-Dichloroethane 9.9 J 500 599 118 500 569 112 5 70-130/20
78-87-5 1,2-Dichloropropane ND 500 544 109 500 517 103 5 70-130/20
142-28-9 1,3-Dichloropropane ND 500 564 113 500 555 111 2 70-130/20
108-20-3 Di-Isopropyl ether 92.1 500 633 108 500 610 104 4 70-130/20
594-20-7 2,2-Dichloropropane ND 500 638 128 500 606 121 5 70-130/20
124-48-1 Dibromochloromethane ND 500 575 115 500 546 109 5 70-130/20
75-71-8 Dichlorodifluoromethane ND 500 491 98 500 472 94 4 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 500 564 113 500 554 111 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 500 565 113 500 533 107 6 70-130/20
541-73-1 m-Dichlorobenzene ND 500 625 125 500 616 123 1 70-130/20
95-50-1 o-Dichlorobenzene ND 500 615 123 500 597 119 3 70-130/20
106-46-7 p-Dichlorobenzene ND 500 568 114 500 552 110 3 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 500 562 112 500 539 108 4 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 500 638 128 500 607 121 5 70-130/20
100-41-4 Ethylbenzene 177 500 761 117 500 731 111 4 70-130/20
87-68-3 Hexachlorobutadiene ND 500 586 117 500 600 120 2 70-130/20
98-82-8 Isopropylbenzene 5.8 J 500 676 134*500 640 127 5 70-130/20
* = Outside of Control Limits.
83 of 90
FA15341 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15340-8MS E030987.D 50 06/03/14 TD n/a n/a VE1040
FA15340-8MSD E030988.D 50 06/03/14 TD n/a n/a VE1040
FA15340-8 a E030984.D 50 06/03/14 TD n/a n/a VE1040
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-7, FA15341-13, FA15341-15, FA15341-16, FA15341-17
FA15340-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 500 669 134*500 651 130 3 70-130/20
74-83-9 Methyl bromide ND 500 565 113 500 556 111 2 60-140/20
74-87-3 Methyl chloride ND 500 531 106 500 508 102 4 60-140/20
74-95-3 Methylene bromide ND 500 562 112 500 526 105 7 70-130/20
75-09-2 Methylene chloride ND 500 550 110 500 524 105 5 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 500 590 118 500 574 115 3 70-130/20
91-20-3 Naphthalene 54.1 500 616 112 500 627 115 2 70-130/20
103-65-1 n-Propylbenzene 18.2 J 500 664 129 500 639 124 4 70-130/20
100-42-5 Styrene 15.2 J 500 613 120 500 583 114 5 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 500 594 119 500 573 115 4 70-130/20
71-55-6 1,1,1-Trichloroethane ND 500 609 122 500 576 115 6 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 500 556 111 500 535 107 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 500 558 112 500 535 107 4 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 500 536 107 500 555 111 3 70-130/20
96-18-4 1,2,3-Trichloropropane ND 500 571 114 500 559 112 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 500 550 110 500 559 112 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene 130 500 765 127 500 728 120 5 70-130/20
108-67-8 1,3,5-Trimethylbenzene 33.1 500 644 122 500 624 118 3 70-130/20
127-18-4 Tetrachloroethylene ND 500 593 119 500 561 112 6 70-130/20
108-88-3 Toluene 1030 500 1610 116 500 1520 98 6 70-130/20
79-01-6 Trichloroethylene ND 500 562 112 500 543 109 3 70-130/20
75-69-4 Trichlorofluoromethane ND 500 542 108 500 525 105 3 60-140/20
75-01-4 Vinyl chloride ND 500 549 110 500 534 107 3 60-140/20
1330-20-7 Xylene (total)928 1500 2870 129 1500 2730 120 5 70-130/20
m,p-Xylene 608 1000 1880 127 1000 1780 117 5 70-130/20
95-47-6 o-Xylene 320 500 996 135*500 950 126 5 70-130/20
CAS No.Surrogate Recoveries MS MSD FA15340-8 Limits
1868-53-7 Dibromofluoromethane 103%103%103%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%105%108%70-130%
2037-26-5 Toluene-D8 103%102%101%70-130%
460-00-4 4-Bromofluorobenzene 104%105%103%70-130%
(a) Confirmation for internal standard areas.
* = Outside of Control Limits.
84 of 90
FA15341 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15341-1MS A0187173.D 1 06/03/14 TD n/a n/a VA1475
FA15341-1MSD A0187174.D 1 06/03/14 TD n/a n/a VA1475
FA15341-1 A0187171.D 1 06/03/14 TD n/a n/a VA1475
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-1, FA15341-4, FA15341-6, FA15341-10, FA15341-11, FA15341-12, FA15341-18
FA15341-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 11.7 117 10 11.6 116 1 70-130/20
108-86-1 Bromobenzene ND 10 10.1 101 10 10.2 102 1 70-130/20
74-97-5 Bromochloromethane ND 10 11.1 111 10 10.8 108 3 70-130/20
75-27-4 Bromodichloromethane ND 10 8.8 88 10 8.7 87 1 70-130/20
75-25-2 Bromoform ND 10 8.9 89 10 8.9 89 0 70-130/20
104-51-8 n-Butylbenzene ND 10 10.7 107 10 10.5 105 2 70-130/20
135-98-8 sec-Butylbenzene ND 10 10.4 104 10 10.5 105 1 70-130/20
98-06-6 tert-Butylbenzene ND 10 9.0 90 10 8.9 89 1 70-130/20
108-90-7 Chlorobenzene ND 10 10.4 104 10 10.5 105 1 70-130/20
75-00-3 Chloroethane ND 10 9.2 92 10 9.1 91 1 60-140/20
67-66-3 Chloroform ND 10 8.9 89 10 8.9 89 0 70-130/20
95-49-8 o-Chlorotoluene ND 10 9.7 97 10 9.7 97 0 70-130/20
106-43-4 p-Chlorotoluene ND 10 9.6 96 10 9.8 98 2 70-130/20
56-23-5 Carbon tetrachloride ND 10 8.1 81 10 8.0 80 1 70-130/20
75-34-3 1,1-Dichloroethane ND 10 10.2 102 10 10.3 103 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 10.1 101 10 10.0 100 1 70-130/20
563-58-6 1,1-Dichloropropene ND 10 10.1 101 10 10.2 102 1 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 8.2 82 10 8.0 80 2 70-130/20
106-93-4 1,2-Dibromoethane ND 10 10.7 107 10 10.6 106 1 70-130/20
107-06-2 1,2-Dichloroethane ND 10 8.1 81 10 8.0 80 1 70-130/20
78-87-5 1,2-Dichloropropane ND 10 11.8 118 10 11.9 119 1 70-130/20
142-28-9 1,3-Dichloropropane ND 10 10.8 108 10 10.8 108 0 70-130/20
108-20-3 Di-Isopropyl ether ND 10 11.5 115 10 11.5 115 0 70-130/20
594-20-7 2,2-Dichloropropane ND 10 8.8 88 10 8.7 87 1 70-130/20
124-48-1 Dibromochloromethane ND 10 9.1 91 10 9.0 90 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 7.6 76 10 7.6 76 0 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 10 11.1 111 10 11.1 111 0 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 10.4 104 10 10.3 103 1 70-130/20
541-73-1 m-Dichlorobenzene ND 10 10.1 101 10 10.2 102 1 70-130/20
95-50-1 o-Dichlorobenzene ND 10 10.1 101 10 9.9 99 2 70-130/20
106-46-7 p-Dichlorobenzene ND 10 9.9 99 10 9.9 99 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 10.1 101 10 10.1 101 0 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 10 100 10 9.7 97 3 70-130/20
100-41-4 Ethylbenzene ND 10 10.2 102 10 10.2 102 0 70-130/20
87-68-3 Hexachlorobutadiene ND 10 8.4 84 10 8.5 85 1 70-130/20
98-82-8 Isopropylbenzene ND 10 10.1 101 10 10.1 101 0 70-130/20
* = Outside of Control Limits.
85 of 90
FA15341 55.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15341-1MS A0187173.D 1 06/03/14 TD n/a n/a VA1475
FA15341-1MSD A0187174.D 1 06/03/14 TD n/a n/a VA1475
FA15341-1 A0187171.D 1 06/03/14 TD n/a n/a VA1475
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-1, FA15341-4, FA15341-6, FA15341-10, FA15341-11, FA15341-12, FA15341-18
FA15341-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 10.2 102 10 10.2 102 0 70-130/20
74-83-9 Methyl bromide ND 10 7.7 77 10 7.7 77 0 60-140/20
74-87-3 Methyl chloride ND 10 11.0 110 10 10.5 105 5 60-140/20
74-95-3 Methylene bromide ND 10 9.9 99 10 9.7 97 2 70-130/20
75-09-2 Methylene chloride ND 10 11.4 114 10 11.2 112 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether 1.0 10 9.9 89 10 9.9 89 0 70-130/20
91-20-3 Naphthalene ND 10 17.9 179*10 11.2 112 46*70-130/20
103-65-1 n-Propylbenzene ND 10 10.4 104 10 10.6 106 2 70-130/20
100-42-5 Styrene ND 10 11.0 110 10 10.9 109 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 9.2 92 10 9.2 92 0 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 8.2 82 10 8.2 82 0 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 11.1 111 10 11.0 110 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 11.7 117 10 11.1 111 5 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 9.5 95 10 9.6 96 1 70-130/20
96-18-4 1,2,3-Trichloropropane ND 10 9.2 92 10 9.2 92 0 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 9.7 97 10 9.7 97 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 11.9 119 10 10.8 108 10 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 10.4 104 10 10.2 102 2 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.0 100 10 10.1 101 1 70-130/20
108-88-3 Toluene ND 10 11.2 112 10 11.2 112 0 70-130/20
79-01-6 Trichloroethylene ND 10 9.6 96 10 9.7 97 1 70-130/20
75-69-4 Trichlorofluoromethane ND 10 5.0 50*10 4.9 49*2 60-140/20
75-01-4 Vinyl chloride ND 10 9.8 98 10 9.4 94 4 60-140/20
1330-20-7 Xylene (total)ND 30 30.9 103 30 30.6 102 1 70-130/20
m,p-Xylene ND 20 20.4 102 20 20.2 101 1 70-130/20
95-47-6 o-Xylene ND 10 10.5 105 10 10.4 104 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA15341-1 Limits
1868-53-7 Dibromofluoromethane 87%86%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 76%75%110%70-130%
2037-26-5 Toluene-D8 100%100%94%70-130%
460-00-4 4-Bromofluorobenzene 95%95%102%70-130%
* = Outside of Control Limits.
86 of 90
FA15341 55.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15342-2MS E031017.D 1 06/04/14 TD n/a n/a VE1041
FA15342-2MSD E031018.D 1 06/04/14 TD n/a n/a VE1041
FA15342-2 E031013.D 1 06/04/14 TD n/a n/a VE1041
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-3, FA15341-5, FA15341-14, FA15341-15, FA15341-16
FA15342-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 10.6 106 10 10.4 104 2 70-130/20
108-86-1 Bromobenzene ND 10 10.8 108 10 10.6 106 2 70-130/20
74-97-5 Bromochloromethane ND 10 10.6 106 10 10.6 106 0 70-130/20
75-27-4 Bromodichloromethane ND 10 10.1 101 10 9.8 98 3 70-130/20
75-25-2 Bromoform ND 10 9.5 95 10 9.1 91 4 70-130/20
104-51-8 n-Butylbenzene ND 10 10.9 109 10 10.9 109 0 70-130/20
135-98-8 sec-Butylbenzene ND 10 12.3 123 10 12.0 120 2 70-130/20
98-06-6 tert-Butylbenzene ND 10 12.0 120 10 11.8 118 2 70-130/20
108-90-7 Chlorobenzene ND 10 11.3 113 10 11.2 112 1 70-130/20
75-00-3 Chloroethane ND 10 9.9 99 10 10 100 1 60-140/20
67-66-3 Chloroform ND 10 10.1 101 10 10.1 101 0 70-130/20
95-49-8 o-Chlorotoluene ND 10 11.7 117 10 11.4 114 3 70-130/20
106-43-4 p-Chlorotoluene ND 10 12.3 123 10 12.1 121 2 70-130/20
56-23-5 Carbon tetrachloride ND 10 10.6 106 10 10.2 102 4 70-130/20
75-34-3 1,1-Dichloroethane ND 10 10.2 102 10 10.1 101 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 10.8 108 10 10.9 109 1 70-130/20
563-58-6 1,1-Dichloropropene ND 10 11.5 115 10 11.1 111 4 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 10.2 102 10 10.0 100 2 70-130/20
106-93-4 1,2-Dibromoethane ND 10 10.8 108 10 10.9 109 1 70-130/20
107-06-2 1,2-Dichloroethane ND 10 10.1 101 10 10.1 101 0 70-130/20
78-87-5 1,2-Dichloropropane ND 10 10.0 100 10 10.0 100 0 70-130/20
142-28-9 1,3-Dichloropropane ND 10 10.6 106 10 10.5 105 1 70-130/20
108-20-3 Di-Isopropyl ether ND 10 9.6 96 10 9.6 96 0 70-130/20
594-20-7 2,2-Dichloropropane ND 10 11.4 114 10 11.2 112 2 70-130/20
124-48-1 Dibromochloromethane ND 10 10.3 103 10 9.9 99 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 8.6 86 10 8.8 88 2 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 10 10.8 108 10 10.5 105 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 10 100 10 9.5 95 5 70-130/20
541-73-1 m-Dichlorobenzene ND 10 12.0 120 10 11.5 115 4 70-130/20
95-50-1 o-Dichlorobenzene ND 10 11.6 116 10 11.1 111 4 70-130/20
106-46-7 p-Dichlorobenzene ND 10 10.7 107 10 10.5 105 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 10.1 101 10 9.9 99 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 11.2 112 10 11.0 110 2 70-130/20
100-41-4 Ethylbenzene ND 10 10.6 106 10 10.5 105 1 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10.3 103 10 10.3 103 0 70-130/20
98-82-8 Isopropylbenzene ND 10 12.2 122 10 12.1 121 1 70-130/20
* = Outside of Control Limits.
87 of 90
FA15341 55.3.4
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15342-2MS E031017.D 1 06/04/14 TD n/a n/a VE1041
FA15342-2MSD E031018.D 1 06/04/14 TD n/a n/a VE1041
FA15342-2 E031013.D 1 06/04/14 TD n/a n/a VE1041
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-3, FA15341-5, FA15341-14, FA15341-15, FA15341-16
FA15342-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 12.5 125 10 12.1 121 3 70-130/20
74-83-9 Methyl bromide ND 10 10.5 105 10 10.5 105 0 60-140/20
74-87-3 Methyl chloride ND 10 8.9 89 10 9.7 97 9 60-140/20
74-95-3 Methylene bromide ND 10 10.2 102 10 10 100 2 70-130/20
75-09-2 Methylene chloride ND 10 9.5 95 10 9.6 96 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 10 11.0 110 10 10.8 108 2 70-130/20
91-20-3 Naphthalene ND 10 11.8 118 10 10.9 109 8 70-130/20
103-65-1 n-Propylbenzene ND 10 12.2 122 10 11.7 117 4 70-130/20
100-42-5 Styrene ND 10 10.6 106 10 10.3 103 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 10.7 107 10 10.6 106 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 10.7 107 10 10.6 106 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.8 108 10 10.4 104 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 10.3 103 10 10.4 104 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 9.7 97 10 10.2 102 5 70-130/20
96-18-4 1,2,3-Trichloropropane ND 10 10.8 108 10 10.7 107 1 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 10.0 100 10 10.2 102 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 11.5 115 10 11.0 110 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 11.3 113 10 10.8 108 5 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.8 108 10 10.7 107 1 70-130/20
108-88-3 Toluene ND 10 10.6 106 10 10.6 106 0 70-130/20
79-01-6 Trichloroethylene ND 10 10.4 104 10 10.2 102 2 70-130/20
75-69-4 Trichlorofluoromethane ND 10 9.3 93 10 9.4 94 1 60-140/20
75-01-4 Vinyl chloride ND 10 9.7 97 10 10.6 106 9 60-140/20
1330-20-7 Xylene (total)ND 30 34.8 116 30 34.2 114 2 70-130/20
m,p-Xylene ND 20 22.7 114 20 22.3 112 2 70-130/20
95-47-6 o-Xylene ND 10 12.1 121 10 11.9 119 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA15342-2 Limits
1868-53-7 Dibromofluoromethane 99%99%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%97%99%70-130%
2037-26-5 Toluene-D8 101%102%101%70-130%
460-00-4 4-Bromofluorobenzene 104%102%105%70-130%
* = Outside of Control Limits.
88 of 90
FA15341 55.3.4
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15341-20MS A0187205.D 1 06/04/14 TD n/a n/a VA1476
FA15341-20MSD A0187206.D 1 06/04/14 TD n/a n/a VA1476
FA15341-20 A0187197.D 1 06/04/14 TD n/a n/a VA1476
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-6, FA15341-8, FA15341-9, FA15341-19, FA15341-20, FA15341-21, FA15341-22
FA15341-20 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 11.5 115 10 10.4 104 10 70-130/20
108-86-1 Bromobenzene ND 10 10.2 102 10 9.2 92 10 70-130/20
74-97-5 Bromochloromethane ND 10 11.2 112 10 10.3 103 8 70-130/20
75-27-4 Bromodichloromethane ND 10 9.8 98 10 8.6 86 13 70-130/20
75-25-2 Bromoform ND 10 9.2 92 10 8.0 80 14 70-130/20
104-51-8 n-Butylbenzene ND 10 10.0 100 10 9.0 90 11 70-130/20
135-98-8 sec-Butylbenzene ND 10 11.1 111 10 10.2 102 8 70-130/20
98-06-6 tert-Butylbenzene ND 10 9.9 99 10 8.9 89 11 70-130/20
108-90-7 Chlorobenzene ND 10 11.0 110 10 10 100 10 70-130/20
75-00-3 Chloroethane ND 10 8.6 86 10 7.6 76 12 60-140/20
67-66-3 Chloroform ND 10 9.6 96 10 8.6 86 11 70-130/20
95-49-8 o-Chlorotoluene ND 10 10.2 102 10 9.5 95 7 70-130/20
106-43-4 p-Chlorotoluene ND 10 10.8 108 10 9.9 99 9 70-130/20
56-23-5 Carbon tetrachloride ND 10 9.5 95 10 8.0 80 17 70-130/20
75-34-3 1,1-Dichloroethane ND 10 11.0 110 10 10.1 101 9 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 11.6 116 10 10.4 104 11 70-130/20
563-58-6 1,1-Dichloropropene ND 10 11.4 114 10 10.1 101 12 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 8.3 83 10 7.4 74 11 70-130/20
106-93-4 1,2-Dibromoethane ND 10 10.8 108 10 9.7 97 11 70-130/20
107-06-2 1,2-Dichloroethane ND 10 9.7 97 10 8.3 83 16 70-130/20
78-87-5 1,2-Dichloropropane ND 10 12.3 123 10 10.8 108 13 70-130/20
142-28-9 1,3-Dichloropropane ND 10 10.8 108 10 9.7 97 11 70-130/20
108-20-3 Di-Isopropyl ether ND 10 12.6 126 10 11.4 114 10 70-130/20
594-20-7 2,2-Dichloropropane ND 10 10.3 103 10 8.9 89 15 70-130/20
124-48-1 Dibromochloromethane ND 10 9.6 96 10 8.4 84 13 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 9.3 93 10 8.3 83 11 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 10 11.3 113 10 10.1 101 11 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 10.9 109 10 9.3 93 16 70-130/20
541-73-1 m-Dichlorobenzene ND 10 11.2 112 10 10.1 101 10 70-130/20
95-50-1 o-Dichlorobenzene ND 10 10.7 107 10 9.7 97 10 70-130/20
106-46-7 p-Dichlorobenzene ND 10 9.9 99 10 9.2 92 7 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 10.8 108 10 9.6 96 12 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 11.2 112 10 9.5 95 16 70-130/20
100-41-4 Ethylbenzene ND 10 10 100 10 9.1 91 9 70-130/20
87-68-3 Hexachlorobutadiene ND 10 8.6 86 10 7.6 76 12 70-130/20
98-82-8 Isopropylbenzene ND 10 11.1 111 10 9.9 99 11 70-130/20
* = Outside of Control Limits.
89 of 90
FA15341 55.3.5
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA15341
Account:GRINCC GRI (Geological Resources Inc.)
Project:Ram 21, 1121 NC561 W, Saint John, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA15341-20MS A0187205.D 1 06/04/14 TD n/a n/a VA1476
FA15341-20MSD A0187206.D 1 06/04/14 TD n/a n/a VA1476
FA15341-20 A0187197.D 1 06/04/14 TD n/a n/a VA1476
The QC reported here applies to the following samples:Method: SM 6200B
FA15341-6, FA15341-8, FA15341-9, FA15341-19, FA15341-20, FA15341-21, FA15341-22
FA15341-20 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 10.7 107 10 9.7 97 10 70-130/20
74-83-9 Methyl bromide ND 10 8.0 80 10 7.2 72 11 60-140/20
74-87-3 Methyl chloride ND 10 11.3 113 10 10.1 101 11 60-140/20
74-95-3 Methylene bromide ND 10 10.4 104 10 9.3 93 11 70-130/20
75-09-2 Methylene chloride ND 10 12.6 126 10 11.2 112 12 70-130/20
1634-04-4 Methyl Tert Butyl Ether 0.25 J 10 10.7 105 10 9.6 94 11 70-130/20
91-20-3 Naphthalene ND 10 11.1 111 10 9.3 93 18 70-130/20
103-65-1 n-Propylbenzene ND 10 11.0 110 10 10.1 101 9 70-130/20
100-42-5 Styrene ND 10 10.7 107 10 9.6 96 11 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 9.7 97 10 8.6 86 12 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 9.6 96 10 8.3 83 15 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.9 109 10 9.9 99 10 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 10.8 108 10 10 100 8 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 9.4 94 10 8.7 87 8 70-130/20
96-18-4 1,2,3-Trichloropropane ND 10 9.6 96 10 8.7 87 10 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 9.7 97 10 8.8 88 10 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 9.9 99 10 8.8 88 12 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 9.4 94 10 8.7 87 8 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.3 103 10 9.4 94 9 70-130/20
108-88-3 Toluene ND 10 10.3 103 10 9.5 95 8 70-130/20
79-01-6 Trichloroethylene ND 10 10.3 103 10 8.9 89 15 70-130/20
75-69-4 Trichlorofluoromethane ND 10 7.7 77 10 6.6 66 15 60-140/20
75-01-4 Vinyl chloride ND 10 9.3 93 10 8.3 83 11 60-140/20
1330-20-7 Xylene (total)ND 30 31.3 104 30 27.9 93 11 70-130/20
m,p-Xylene ND 20 20.4 102 20 18.2 91 11 70-130/20
95-47-6 o-Xylene ND 10 10.9 109 10 9.7 97 12 70-130/20
CAS No.Surrogate Recoveries MS MSD FA15341-20 Limits
1868-53-7 Dibromofluoromethane 94%93%106%70-130%
17060-07-0 1,2-Dichloroethane-D4 91%87%112%70-130%
2037-26-5 Toluene-D8 97%99%98%70-130%
460-00-4 4-Bromofluorobenzene 95%96%102%70-130%
* = Outside of Control Limits.
90 of 90
FA15341 55.3.5

APPENDIX B
Graphs of Individual VOC Concentrations vs. Time

APPENDIX B
SUMMARY OF GROUND WATER QUALITY DATA
RED APPLE MARKET #21
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 46.4 5.51 58.8 28.72 25.7 34.3
06/06/07 68.3 4.56 85.7 32.6 21.6 43.9
06/02/08 16.5 1.20 21.2 8.35 38.5 9.23
12/18/08 13 <0.50 10 4.9 14 5.9
03/24/09 44 15 40 23 16 19
06/25/09 6.32 <0.330 7.99 <1.33 10.5 3.14
09/21/09 18.5 <0.190 9.24 1.30 12.7 3.10
12/30/09 26.1 2.13 5.26 3.14 15.1 3.51
06/28/10 20.1 0.62 12.2 2.51 11.4 7.66
10/05/10 32.6 2.78 16.0 8.47 8.91 5.69
10/12/11 <0.13 <0.13 <0.15 <0.30 2.1 <0.10
01/31/12 <0.13 <0.13 <0.15 <0.30 1.2 <0.10
05/15/12 <0.13 <0.13 <0.15 <0.30 0.16 <0.10
01/22/13 <0.10 <0.10 <0.10 <0.22 1.0 <0.15
11/18/13 <0.10 <0.10 <0.10 <0.22 1.1 <0.15
05/27/14 <0.10 <0.10 <0.10 <0.20 1.0 <0.10
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 FP FP FP FP FP FP
06/06/07 FP FP FP FP FP FP
06/02/08 FP FP FP FP FP FP
12/18/08 FP FP FP FP FP FP
03/24/09 FP FP FP FP FP FP
06/25/09 FP FP FP FP FP FP
09/21/09 FP FP FP FP FP FP
12/30/09 FP FP FP FP FP FP
06/28/10 FP FP FP FP FP FP
10/05/10 FP FP FP FP FP FP
10/12/11 9,780 9,700 2,440 10,100 1,220 769
01/31/12 FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP
01/22/13 3,250 7,990 2,070 11,900 519 2,020
11/18/13 6,580 7,930 2,100 13,800 731 841
05/27/14 4,160 4,880 1,400 10,500 657 758
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 1,940 5.14 34.3 <15.0 3,800 <25.0
06/06/07 3,030 6.18 69.0 7.61 4,880 40.3
06/02/08 2,500 4.95 126 14.2 5,490 60.8
12/18/08 1,700 2.1 33 2.6 4,200 24
03/24/09 2,900 <16 110 140 4,900 69
06/25/09 2,140 10.3 56.4 32.9 4,110 40
09/21/09 2,180 <7.60 56.2 <8.80 5,040 69.3
12/30/09 1,580 2.29 41.1 <1.10 4,200 23.3
06/28/10 1,780 <9.50 54.0 <11.0 5,040 26.2
10/05/10 1,830 <9.50 47.8 <11.0 4,010 <25.0
10/12/11 3.4 6.1 1.7 6.2 0.36 0.46
01/31/12 36.6 2.9 17.9 28.4 6.2 0.21
05/15/12 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10
01/22/13 22.1 2.1 19.1 16.2 8.1 0.68
11/18/13 12.6 1.4 17.1 14.0 5.9 1.2
05/27/14 4.2 <0.10 0.85 0.74 J 5.9 0.27
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 14,900 5,650 1,330 4,850 16,100 436
06/14/07 15,000 8,240 1,710 6,330 14,300 489
06/02/08 NS NS NS NS NS NS
10/12/11 FP FP FP FP FP FP
01/31/12 FP FP FP FP FP FP
05/15/12 FP FP FP FP FP FP
01/22/13 FP FP FP FP FP FP
11/18/13 FP FP FP FP FP FP
05/27/14 792 3,720 1,160 5,660 604 550.0
MW-1/MW-1R
MW-2/MW-2R
MW-3/MW-3R
MW-4/MW-4R
Note:
Concentrations in mg/L.Page 1 of 2
APPENDIX B
SUMMARY OF GROUND WATER QUALITY DATA
RED APPLE MARKET #21
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 1,040 76.6 116 109.4 836 348
06/06/07 1,350 90.1 143 119 1,300 105
06/02/08 NS NS NS NS NS NS
12/18/08 NS NS NS NS NS NS
03/24/09 NS NS NS NS NS NS
06/25/09 NS NS NS NS NS NS
09/21/09 403 2.25 40.9 37.3 195 61.5
12/30/09 676 7.35 35.7 12.3 255 43.4
06/28/10 817 12.60 66.7 55.9 347 54.1
10/05/10 308 <19.0 41.1 23.0 193 108
10/12/11 FP FP FP FP FP FP
01/31/12 40.6 2.7 61.4 25.6 156 42.6
05/15/12 871 18.2 134 214.8 93.4 87.5
01/22/13 143 14.6 114 225 184 128
11/18/13 34.4 0.45 22.7 1.8 99.2 47.3
05/27/14 145 7.8 114 39.9 247 60.7
MW-9
Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
MAC 1 600 600 500 20 6
01/18/07 53.6 1.48 27.4 56.3 3.67 18.3
06/06/07 56.8 0.960 24.2 53.8 0.690 14.3
06/02/08 33.6 0.640 21.7 9.07 2.18 20.5
12/18/08 40 1.600 27 18 <0.50 22
03/24/09 68 <1.6 37 23 2.0 28
06/25/09 53.4 0.929 15.9 20.7 1.04 19.5
09/21/09 50.7 0.952 25.7 18.5 1.85 23.2
12/30/09 71.9 0.903 28.4 16.8 <0.250 21.9
06/28/10 66.1 <0.950 22.5 15.2 <1.25 19.0
10/05/10 72.6 3.54 74.2 110 <0.250 33.7
10/12/11 37.3 0.41 8.2 12.2 0.92 17.3
01/31/12 54.7 0.78 25.0 21.6 1.5 24.1
05/15/12 65.9 0.58 15.7 15.0 1.3 15.9
01/22/13 73.7 2.3 13.9 74.7 0.43 13.6
11/18/13 183 3.9 53.5 153 0.91 40.4
05/27/14 227 3.7 60.4 158 1.5 44.1
MW-5/MW-5R
Note:
Concentrations in mg/L.Page 2 of 2
0
100
200
300
400
500
600
700
MAC 01/18/07 06/06/07 06/02/08 12/18/08 03/24/09 06/25/09 09/21/09 12/30/09 06/28/10 10/05/10 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-1/MW-1R
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
0
2000
4000
6000
8000
10000
12000
14000
16000
MAC 01/18/07 06/06/07 06/02/08 12/18/08 03/24/09 06/25/09 09/21/09 12/30/09 06/28/10 10/05/10 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-2/MW-2R
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
3.54 ft.
FP
0.69 ft.
FP
2.27 ft.
FP
0.69 ft.
FP
0.23 ft.
FP
3.25 ft.
FP
0.46 ft.
FP
0.03 ft.
FP
0.33 ft.
FP
2.79 ft.
FP
2.04 ft.
FP
0.22 ft.
FP
0
1000
2000
3000
4000
5000
6000
MAC 01/18/07 06/06/07 06/02/08 12/18/08 03/24/09 06/25/09 09/21/09 12/30/09 06/28/10 10/05/10 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-3/MW-3R
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
0
2000
4000
6000
8000
10000
12000
14000
16000
18000
MAC 01/18/07 06/14/07 06/02/08 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-4/MW-4R
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
FPNS FP FP FP FP
0
200
400
600
800
1000
1200
1400
1600
MAC 01/18/07 06/06/07 06/02/08 12/18/08 03/24/09 06/25/09 09/21/09 12/30/09 06/28/10 10/05/10 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-5/MW-5R
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene
NS NS NS NS 0.02 ft.
FP
0
100
200
300
400
500
600
700
MAC 01/18/07 06/06/07 06/02/08 12/18/08 03/24/09 06/25/09 09/21/09 12/30/09 06/28/10 10/05/10 10/12/11 01/31/12 05/15/12 01/22/13 11/18/13 05/27/14Concentration (ug/L)Sample Date
Ground Water Quality Chart -MW-9
Red Apple Market #21
Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene

APPENDIX C
Graphs of Total VOC Concentrations vs. Depths to Ground Water

APPENDIX C
TOTAL VOC'S vs DEPTH TO WATER
RED APPLE MARKET #21
TOTAL VOC'S INCLUDE BTEX, MTBE AND NAPHTHALENE
MW-1/1R
Date Total VOC's Depth to Water
01/18/07 199.43 12.87
06/06/07 256.66 13.15
06/02/08 94.98 14.10
12/18/08 41.90 16.41
03/24/09 157.00 14.62
06/25/09 27.95 15.00
09/21/09 44.84 15.66
12/30/09 55.24 14.85
06/28/10 54.488 14.02
10/05/10 74.45 14.74
10/12/11 2.1 15.73
01/31/12 1.2 15.71
05/15/12 0.16 14.77
01/22/13 1 14.68
11/18/13 1.1 15.84
05/27/14 1 14.36
MW-2/2R
Date Total VOC's Depth to Water
01/18/07 FP 14.81
06/06/07 FP 13.07
06/02/08 FP 15.20
12/18/08 FP 15.25
03/24/09 FP 16.90
06/25/09 FP 14.90
09/21/09 FP 15.07
12/30/09 FP 14.65
06/28/10 FP 15.65
10/05/10 FP 15.81
10/12/11 34,009 14.71
01/31/12 FP 14.67
05/15/12 FP 13.96
01/22/13 27,749 13.85
11/18/13 31,982 14.95
05/27/14 22,355 13.71
MW-3/3R
Date Total VOC's Depth to Water
01/18/07 5,779.44 14.02
06/06/07 8,033.09 13.86
06/02/08 8195.95 14.77
12/18/08 5937.70 16.27
03/24/09 8,050.00 15.90
06/25/09 6,349.60 15.80
09/21/09 7,345.50 16.40
12/30/09 5,846.69 13.97
06/28/10 6,900.20 15.76
10/05/10 5,887.80 15.50
10/12/11 18.22 14.48
01/31/12 92.21 15.88
05/15/12 0.00 14.31
01/22/13 68.28 15.09
11/18/13 52.20 16.48
05/27/14 11.22 16.74
MW-4/4R
Date Total VOC's Depth to Water
01/18/07 43266 12.69
06/14/07 46069 13.06
06/02/08 0.00 NM
10/12/11 0.00 13.28
01/31/12 0.00 13.12
05/15/12 0.00 14.13
01/22/13 0.00 14.22
11/18/13 0.00 14.86
05/27/14 12,486.00 13.58
Note:
Concentrations in mg/L; Depths to water reported in feet.Page 1 of 2
APPENDIX C
TOTAL VOC'S vs DEPTH TO WATER
RED APPLE MARKET #21
TOTAL VOC'S INCLUDE BTEX, MTBE AND NAPHTHALENE
MW-5/5R
Date Total VOC's Depth to Water
01/18/07 2,526.0 13.02
06/06/07 3,107.10 13.23
06/02/08 0.00 NM
12/18/08 0.00 NM
03/24/09 0.00 NM
06/25/09 0.00 NM
09/21/09 739.95 15.47
12/30/09 1,029.75 14.44
06/28/10 1,353.30 13.99
10/05/10 673.10 14.60
10/12/11 0.00 14.16
01/31/12 328.90 15.36
05/15/12 1,418.90 14.20
01/22/13 808.60 14.45
11/18/13 205.85 15.44
05/27/14 614.40 13.98
MW-9
Date Total VOC's Depth to Water
01/18/07 160.75 7.73
06/06/07 150.75 9.35
06/02/08 87.69 8.21
12/18/08 86.60 11.72
03/24/09 158.00 11.60
06/25/09 111.47 11.73
09/21/09 120.90 12.62
12/30/09 139.90 12.24
06/28/10 122.80 12.40
10/05/10 294.04 12.69
10/12/11 76.33 10.00
01/31/12 127.68 10.59
05/15/12 114.38 9.94
01/22/13 178.63 5.34
11/18/13 434.71 11.49
05/27/14 494.70 9.64
Note:
Concentrations in mg/L; Depths to water reported in feet.Page 2 of 2
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
18.00
0
50
100
150
200
250
300
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW-1/MW-1R
Total VOC's
Depth to Water
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
18.00
0
5,000
10,000
15,000
20,000
25,000
30,000
35,000
40,000
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW-2MW-/2R
Total VOC's
Depth to Water
FPFPFPFPFPFPFPFP FP FP FPFP
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
18.00
0
1,000
2,000
3,000
4,000
5,000
6,000
7,000
8,000
9,000
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW-3/MW-3R
Total VOC's
Depth to Water
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
0
5,000
10,000
15,000
20,000
25,000
30,000
35,000
40,000
45,000
50,000
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW-4/MW-4R
Total VOC's
Depth to Water
NS FP FP FP FP FP
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
16.00
18.00
0
500
1,000
1,500
2,000
2,500
3,000
3,500
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW5
Total VOC's
Depth to Water
NS NS NS NS FP
0.00
2.00
4.00
6.00
8.00
10.00
12.00
14.00
0
100
200
300
400
500
600
Depth to Water (ft.)Total VOC's Concentration (ug/L)Sample Date
Ground Water Quality vs. Depth to Water
Red Apple Market #21 -MW9
Total VOC's
Depth to Water