RA-29352_48506_CA_20-DAY_20220606

2725 E. Millbrook Road
Suite 121
Raleigh, NC 27604
Tel: [phone]
Fax: [phone]

www.oneatlas.com
N.C. Engineering License No. C-1598

June 6, 2022

Mr. Mark Powers
State of North Carolina
Department of Environment and Natural Resources
Raleigh Regional Office
Division of Waste Management – UST Section
1628 Mail Service Center
Raleigh, North Carolina 27699-1628

Re: 20-Day Report
Circle K Store #2720104
4835 Hope Valley Road
Durham, Durham County, North Carolina
NCDEQ Facility ID #00-0-0000015130

Dear Mr. Powers:

ATC Associates of North Carolina, P.C. (ATC), on behalf of Circle K Stores, Inc. is submitting this 20-
Day Report for the referenced facility. Please feel free to contact me at [phone] should you
have any questions or comments.

Sincerely,
ATC Associates of North Carolina, P.C.

Maureen A. Jackson, P.G.
Senior Project Manager

cc: Mr. Alan Cubberley, Circle K Stores, Inc.

20-Day Report
Circle K Store #2720104

4835 Hope Valley Road
Durham, Durham County, North Carolina

Prepared for:
Circle K Stores, Inc.
1100 Situs Court, Suite 100
Raleigh, NC 27606

Prepared by:
ATC Associates of North Carolina, P.C.
2725 E. Millbrook Road, Suite 121
Raleigh, North Carolina 27604

20-Day Report ATC Associates of N.C.
Circle K Store #2720104 June 6, 2022

TABLE OF CONTENTS
1.0 Site Information.................................................................................................................... 1
1.1 Site Identification ...................................................................................................... 1
1.2 Contact Information .................................................................................................. 1
1.3 Release Information ................................................................................................. 1
2.0 History and Characterization .............................................................................................. 2
3.0 UST Closure ......................................................................................................................... 3
3.1 Preparations for UST Closure .................................................................................. 3
3.2 Closure Activities ...................................................................................................... 4
3.3 Initial Response Actions ........................................................................................... 4
3.4 Soil Excavation Activities .......................................................................................... 4
3.5 Soil Sampling Procedures ........................................................................................ 4
3.6 Quality Control Measures ......................................................................................... 5
3.7 Groundwater Sampling Procedures .......................................................................... 5
3.8 Laboratory Analytical Results ................................................................................... 5
4.0 Summary and Conclusions ................................................................................................. 7

Tables
Table 1 Soil Analytical Results

Figures

Figure 1 Topographic Map
Figure 2 Site Map

Appendices

Appendix A UST-3 and UST-2
Appendix B Laboratory Reports and Chains-of-Custody Documents

20-Day Report
Circle K Storc#2720'104 ATC Associates of N C
June 6,2022
1.0 SITE INFORMATION
1.1 Siteldentification
Date of R 6,2022
Facility l.D.: 00-0-0000015130 -UST tncident Number (if known):
Site Name. Circle K Store #2720104
Site Street Address: 4835 Hope Vallev Road
City/Town: Durham Zip Code:27707 County: Durham
Description of Geographical Data Point (e.9., diesel fill port): UST basin
Location Method (GPS, topographical map, other): Gooqle Earth
Latitude (decimal degrees): 35.9192700 N, Longitude (decimal degrees): 78.9603820 W
1.2 CONTACTINFORMATION
UST Owner. Circte K Stores, lrc
Address: 1100 Situs Court, Suite 100, Raleiqh, NC 27606
UST Operator: Circle K Stores, lnc.
Tel.: [phone]
Address: 1 100 Situs Court, Suite 100, Raleioh, NC 27606 Tel.: [phone]
Property Owner: Domar Corporation, lnc.
Address: 1919 Wilshire Drive Durham, NC 27707 Tel.: Unknown
Property Occupant: Vacant
Address: 4835 Hope Vallev Road Durham, NC 27701 Tel.: N/A
Consultant: ATC Associates of North Carolina, P.C.
Address: 2725E. Millbrook Road, Suite 121 Raleiqh, NC 27604 Tel [phone]
Contractor: Zebra Environmental and lndustrial Services
Address: 901 East Sprinqfield Road Hiqh Point, NC 27263 Tel. [phone]
State Certification No. 402
Tel. [phone]
Analytical Laboratory: Wavpoint Analvtical
Address: 449 Sprinqbrook Road Charlotte, NC 28217
1.3 Releaselnformation
Date Di 11. 2022
Estimated Quantity of Release: Unknown
Cause of Release: UST Svstem Operations
Source of Release (Dispenser/Piping/UST): UST system
Sizes and contents of UST system(s)from which the release occurred): Two 10.OOO-qallon
l, Maureen
certify that
knowledge
AJ logist for ATC
ip report is
; Associates of North Carolina, P.C., do
correct and accurate to the best of mythe
(Please Affix
ATC Associates is
The certification num is C-1598.
neering (circle one or both) in North Carolina.
20-Day Report ATC Associates of N.C.
Circle K Store #2720104 June 6, 2022

2

2.0 HISTORY AND CHARACTERIZATION
The Circle K Store #2720104 (Facility ID No. 00-0-0000015130) is currently an inactive retail fuel
outlet and convenience store. The site is located at 4835 Hope Valley Road Durham, Durham
County, North Carolina. The site consists of a single-story convenience store. Two 10,000-gallon
gasoline, one 8,000-gallon gasoline, and one 8,000-gallon diesel USTs and their appurtenances
were removed from the facility. The cover at the site consists of asphalt and concrete. The site is
zoned for commercial purposes. Immediately adjacent properties are zoned for commercial
purposes. A topographic map is presented as Figure 1, and a site map is presented as Figure 2.
UST system information is summarized on the following table.
UST
ID PRODUCT CAPACITY
(gals.) MATERIALS INSTALLATION
DATE
UST
STATUS
RELEASE
ASSOCIATED
(Yes/No)
1 Gasoline 10,000
UST: Steel
w/Internal
Lining
Piping: SW
Fiberglass
1/1/1982 Removed Yes
2 Gasoline 10,000
UST: Steel
w/Internal
Lining
Piping: SW
Fiberglass
1/1/1982 Removed Yes
3 Gasoline 8,000
UST: Steel
w/Internal
Lining
Piping: SW
FIberglass
1/1/1968 Removed Yes
4 Diesel 8,000
UST: Steel
w/Internal
Lining
Piping: SW
Fiberglass
1/1/1968 Removed Yes

20-Day Report ATC Associates of N.C.
Circle K Store #2720104 June 6, 2022

3

Between May 9, 2022 and May 12, 2022, two 10,000-gallon gasoline, one 8.000-gallon gasoline
UST, and one 8,000-gallon diesel underground storage tanks (USTs) and their appurtenances were
removed from the facility. The UST closure activity details are presented below.

It should be noted two previous releases have been noted for the property (assigned UST incident
#24490 and 39800). The release associated with incident #24490 was discovered in May 1996
during a property transaction. The incident was ranked as Intermediate risk with a land use of
residential. This release was issued a Notice of No Further Action (NFA) on Septembe 12, 2007.
The release associated with incident #39800 was caused when a customer pulled the hose off
dispenser ½ causing the premium gasoline meter seal to rupture. This release was issued a NFA
on June 17, 2016. Reports regarding these two incident numbers are on file at the North Carolina
Department of Environmental Quality (NCDEQ) Raleigh Regional Office.

3.0 UST CLOSURE
This section presents information regarding the removal of the USTs, associated piping, and
dispensers.

3.1 Preparations for UST Closure
Prior to the UST closure activities, a Notice of Intent to permanently close the UST systems was
made to the NCDEQ by ATC via a UST-3 form dated March 23, 2022 (Appendix A). Post closure
information is included on the Site Investigation Report Form (UST-2), which is included in Appendix
A.

The UST owner removed as much of the remaining product from the gasoline USTs as possible prior
to the closure activities. Prior to the removal of the USTs from the UST basin, Zebra Environmental
and Industrial Services (Zebra) cleaned the tanks and liquid nitrogen was then used to purge the
USTs prior to their removal from the ground.

On May 11, 2022, a UST-61: 24-Hour Release and UST Leak Reporting Form was submitted by
ATC via email to the NCDEQ. A copy of the form is provided in Appendix A.

20-Day Report ATC Associates of N.C.
Circle K Store #2720104 June 6, 2022

4

3.2 Closure Activities
Closure activities at the Site were conducted May 9, 2022 and May 12, 2022. Zebra performed the
UST closure activities. The four USTs and their appurtenances were removed from the facility.
Figure 2 depicts the site map. Upon removal from the ground, the USTs were noted to be in fair
condition with no noticeable holes.

The dispensers were disconnected from the associated piping, loaded onto a trailer, and transported
off-site.

Disposal manifests are not available at the time of this report.

3.3 Initial Response Actions
Petroleum-related impacts to soil (odor and visual staining) were noted in the overburden soil in the UST
basin; therefore, this soil was loaded into truck and transported off-site for property disposal. Four
stockpile soil samples were collected for disposal purposes. The stockpile soil samples for analyzed by
Total Petroleum Hydrocarbons (TPH) – Gasoline Range Organics (GRO) and Diesel Range Organics
(DRO). Laboratory analytical results are tabulated on Table 1 and the laboratory report and
chain-of-custody documents are provided in Appendix B.

3.4 Soil Excavation Activities
See Section 4.3 for a discuss regarding soil excavation activities.

3.5 Soil Sampling Procedures
Soil samples were collected along the sidewalls of the UST basin (W-1 through W-14) due to the
presence of groundwater in the UST basin. The soil samples were submitted to the project laboratory
for analyses by EPA Method 8015C for TPH-GRO and/or TPH-DRO and/or EPA Method 8260,
depending on sampling location.

A soil sample was collected under each dispenser (D-1 through D-6) and along the product lines (L-1
through L-8) to document environmental conditions. The soil samples were submitted to the project
laboratory for analyses by EPA Method 8015C for TPH-GRO and/or TPH-DRO, and/or EPA Method
8260, depending on sampling location. The locations of the soil samples are provided in Figure 2.
20-Day Report ATC Associates of N.C.
Circle K Store #2720104 June 6, 2022

5

It should be noted groundwater was noted in the UST basin at a depth of approximately 11 feet bgs.
Light non-aqueous phase liquid (LNAPL) was not noted on the accumulated groundwater.

3.6 Quality Control Measures
The soil samples selected for analyses were properly labelled and placed on ice in a cooler pending
transport to Waypoint Analytical in Charlotte, North Carolina. Strict chain-of-custody and sample
preservation protocols were observed for shipping and delivering the samples.

3.7 Groundwater Sampling Procedures
Due to the presence of groundwater in the UST basin following UST removal, a groundwater
monitoring well will be installed in the former UST basin area. Circle K is presently negotiating an
access agreement to the property as the current lease has expired. As soon as access is granted
by the property owner, drilling activities will be scheduled.

3.8 Laboratory Analytical Results
Laboratory analytical results of soil samples collected from the UST basin (soil samples W-1, W-7,
W-11, W-12, and W-14), along the product line (soil samples L-6 and L-7), and under a dispenser
(soil sample D-2) detected TPH-GRO and/or TPH-DRO and/or EPA Method 8260 concentrations
above the established State Action Level and/or STGW-MSCCs. Table 1 provides a summary of the
soil analytical results. A copy of the laboratory report is provided in Appendix B.

4.0 SUMMARY AND CONCLUSIONS
Two 10,000-gallon gasoline, one 8,000-gallon gasoline, and one 8,000-gallon diesel USTs and their
appurtenances were closed by removal during May 2022. The USTs and their appurtenances were
owned by Circle K Stores of Raleigh, North Carolina.

Laboratory analytical results of soil samples collected from the UST basin (soil samples W-1, W-7,
W-11, W-12, and W-14), along the product line (soil samples L-6 and L-7), and under a dispenser
(soil sample D-2) detected TPH-GRO and/or TPH-DRO and/or EPA Method 8260 concentrations
above the established State Action Level and/or STGW-MSCCs.

20-Day Report ATC Associates of N.C.
Circle K Store #2720104 June 6, 2022

6

Due to the presence of groundwater in the UST basin following UST removal, a groundwater
monitoring well will be installed in the former UST basin area. Circle K is presently negotiating an
access agreement to the property as the current lease has expired. As soon as access is granted
by the property owner, drilling activities will be scheduled.

At this time, ATC respectfully requests an extension on the due date for the Initial Abatement Action
Report (IAAR). The new due date is requested to be August 30, 2022. This date will be dependent
on the approval for access to the property and driller availability. ATC will keep the NCDEQ Raleigh
Regional office informed of the progress.

TABLE

TABLE 1
SOIL ANALYTICAL RESULTS
CIRCLE K STORE #27201044835 HOPE VALLEY ROAD
DURHAM, DURHAM COUNTY, NORTH CAROLINA
NCDEQ FACILITY ID #00-0-0000015130
MADEP
Method for
VPH
Sample ID
Date
Sampled
Sample
Location
Sample
Depth
(feet)
PID
Reading
(ppm)TPH-GROTPH-DROAcetoneBenzenen-Butylbenzenesec-ButylbenzeneCarbon DisulfideChloroformEthylbenzenen-HexaneIPEIsopropylbenzenep-IsopropyltolueneMethyl Ethyl KetoneMethylene ChlorideMTBENaphthalenen-PropylbenzeneTetrachloroetheneTolueneTrichloroethene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesC5-C8 AliphaticsW-1 5/11/2022 UST Basin 5 82.3 2.63J 109 0.023 0.002J <0.0006 <0.0007 0.026 <0.001 <0.0007 0.002J <0.0005 <0.0005 <0.001 0.006J <0.001 <0.0007 <0.001 <0.0006 <0.001 0.001J <0.001 0.0008J <0.0006 0.0009J --
W-2 5/11/2022 UST Basin 5 5.8 2.46J 32.7 ----------------------------------------------
W-3 5/11/2022 UST Basin 5 0.6 <2.36 <5.30 0.011J <0.0007 <0.0006 <0.0006 <0.0007 <0.001 <0.0007 <0.0008 <0.0008 <0.0005 <0.001 0.001J <0.001 <0.0007 <0.001 <0.0006 <0.001 <0.0008 <0.001 <0.0006 <0.0006 <0.0006 --
W-4 5/11/2022 UST Basin 5 0.0 3.84J <5.55 0.016J <0.0007 <0.0006 <0.0007 <0.0008 <0.001 <0.0007 <0.0008 <0.0009 <0.0005 <0.001 0.002J <0.001 <0.0007 <0.001 <0.0006 <0.001 <0.0008 <0.001 <0.0006 <0.0006 <0.0006 --
W-5 5/11/2022 UST Basin 5 12.1 <2.64 13.0 0.017J 0.003J 0.0007J <0.0007 0.008 <0.001 0.001J 0.011J <0.0009 <0.0006 <0.001 0.006J <0.001 <0.0008 <0.001 <0.0007 <0.001 0.012 <0.001 0.009 0.005J 0.026 --
W-6 5/11/2022 UST Basin 5 136.8 10.3 9.06J ----------------------------------------------
W-7 5/11/2022 UST Basin 5 43.2 13.9 23.2 0.035 0.003J <0.0006 <0.0007 0.004J 6.36 <0.0008 <0.0009 <0.0010 <0.0006 <0.001 <0.0009 0.023 <0.0008 <0.001 <0.0007 0.002J 0.001J 0.006J <0.0006 <0.0007 0.0009J --
W-8 5/11/2022 UST Basin 5 1.3 2.64J <5.23 0.044 0.002J <0.0006 <0.0006 <0.0007 <0.001 <0.0007 0.002J 0.0008J <0.005 <0.001 <0.0007 <0.001 <0.0007 <0.001 <0.0006 <0.001 <0.0007 <0.001 <0.0006 <0.0005 <0.0006 --
W-9 5/11/2022 UST Basin 5 37.8 4.68J 15.9 ----------------------------------------------
W-10 5/11/2022 UST Basin 5 27.0 33.6 <6.09 0.017J <0.0008 <0.0006 <0.0007 <0.0008 <0.001 <0.0008 <0.0009 <0.0010 <0.0006 <0.001 <0.0009 <0.001 <0.0008 <0.001 <0.0007 <0.001 <0.0009 <0.001 <0.0006 <0.0007 <0.0007 --
W-11 5/11/2022 UST Basin 5 2,608 63.5 37.4 ----------------------------------------------
W-12 5/11/2022 UST Basin 5 1,907 75.7 53.2 <0.074 0.304 0.491 0.163 <0.019 <0.032 3.30 3.05 <0.022 0.339 0.067J <0.020 <0.045 <0.019 1.13 1.37 <0.028 2.56 <0.028 7.11 1.95 14.5 --
W-13 5/11/2022 UST Basin 5 5.5 7.63 5.87J 0.022J <0.0007 <0.0005 <0.0006 <0.0007 <0.001 <0.0007 <0.0007 <0.0008 <0.0005 <0.001 0.005J <0.001 <0.0007 <0.001 <0.0006 <0.001 <0.0007 <0.001 <0.0005 <0.0006 <0.0006 --
W-14 5/11/2022 UST Basin 5 49.9 5.10J 115 0.008J <0.0006 <0.0006 <0.0006 <0.0007 <0.001 <0.0006 <0.0007 <0.0008 <0.0005 <0.001 0.001J <0.001 <0.0007 <0.001 <0.0006 <0.0010 <0.0007 <0.001 <0.0005 <0.0006 <0.0005 --
D-1 5/11/2022 Gasoline
Dispenser 3 5.4 39.1 --0.049 0.002J <0.0006 <0.0007 0.003J <0.001 <0.0007 0.001J <0.0009 <0.0006 <0.001 0.006J <0.001 <0.0008 0.002J <0.0007 <0.001 0.001J <0.001 0.002J 0.0008J 0.003J --
D-2 5/11/2022 Gasoline
Dispenser 3 14.5 3.64J --0.006J 0.015 <0.0006 <0.0007 <0.0008 <0.001 0.005J <0.0009 0.016 0.003J <0.001 <0.0009 <0.001 0.170 0.004J 0.002J <0.001 0.012 <0.001 0.003J 0.001J 0.006J --
D-3 5/11/2022 Gasoline
Dispenser 3 37.0 2.68J --0.013J 0.001J <0.0006 <0.0006 0.002J <0.001 0.0009J 0.004J <0.0008 <0.0005 <0.001 <0.0007 <0.001 <0.0007 0.001J 0.0007J <0.0010 0.003J <0.001 0.003J 0.002J 0.010J --
D-4 5/12/2022 Gasoline
Dispenser 3 2.8 2.99J --0.017J 0.002J <0.0007 <0.0008 <0.0009 <0.001 0.001J <0.0009 <0.0010 0.001J <0.001 <0.0009 <0.001 0.012 <0.001 0.001J <0.001 <0.0009 <0.001 0.008 0.001J 0.015J --
D-5 5/12/2022 Gasoline
Dispenser 3 235 2.75J --0.158 0.002J <0.0005 <0.0006 <0.0007 <0.001 <0.0006 0.005J 0.0009J <0.0005 <0.001 0.049 <0.001 <0.0007 <0.001 <0.0006 <0.001 <0.0007 <0.001 <0.0005 0.0007J 0.006J --
D-6 5/12/2022 Gasoline/Diesel
Dispenser 3 5.7 5.64 77.2 ----------------------------------------------
L-1 5/12/2022 Product Line 3 0.0 2.51J --0.037 <0.0007 <0.0006 <0.0006 0.002J <0.001 <0.0007 <0.0008 <0.0008 <0.0005 <0.001 0.007J <0.001 <0.0007 <0.001 <0.0006 <0.001 0.001J <0.001 <0.0006 <0.0006 <0.0006 --
L-2 5/12/2022 Product Line 3 6.0 <2.67 --0.019J <0.0007 <0.0006 <0.0007 <0.0008 <0.001 <0.0007 <0.0009 <0.0009 <0.0006 <0.001 0.005J <0.001 0.002J <0.001 <0.0007 <0.001 <0.0009 <0.001 <0.0006 <0.0007 <0.0006 --
L-3 5/12/2022 Product Line 3 44.0 25.9 --0.025 0.001J <0.0006 <0.0006 <0.0007 <0.001 0.001J 0.004J <0.0008 <0.0005 <0.001 <0.0007 <0.001 0.004J <0.001 0.0006J <0.001 0.006 <0.001 0.002J 0.001J 0.007J --
L-4 5/12/2022 Product Line 3 22.5 2.78J --0.012J 0.003J <0.0007 <0.0008 <0.0009 <0.001 <0.0008 <0.0009 0.003J <0.0006 <0.001 0.001J <0.001 0.023 <0.001 <0.0007 <0.001 0.001J <0.001 0.001J <0.0007 0.001J --
L-5 5/12/2022 Product Line 3 4.0 <2.59 --0.005J 0.002J <0.0006 <0.0007 <0.0008 <0.001 0.0009J 0.002J 0.001J <0.0006 <0.001 <0.0008 <0.001 0.034 <0.001 <0.0007 <0.001 0.008 <0.001 0.0010J <0.0007 0.004J --
L-6 5/12/2022 Product Line 3 9.0 <2.74 --0.030 0.021 <0.0006 <0.0007 <0.0008 0.001J <0.0008 0.002J <0.0010 <0.0006 <0.001 <0.0009 <0.001 <0.0008 <0.001 <0.0007 <0.001 0.010 <0.001 0.0008J 0.0009J 0.004J --
L-7 5/12/2022 Gasoline Product
Line 3 300 <2.49 --0.047 0.084 0.0007J <0.0007 <0.0008 <0.001 0.003J 0.004J <0.0009 <0.0006 <0.001 0.010J <0.001 <0.0007 0.002J <0.0006 <0.001 0.117 <0.001 0.002J 0.0007J 0.031 1.59J
L-8 5/12/2022 Gasoline Product
Line 3 18.6 <2.38 --0.016J <0.0007 <0.0006 <0.0006 0.002J <0.001 <0.0007 <0.0008 <0.0008 <0.0005 <0.001 0.003J <0.001 <0.0007 0.001J <0.0006 <0.001 0.001J <0.001 0.001J <0.0006 0.002J --
Stockpile 1 5/10/2022 ---->15,000 4,770 759 ----------------------------------------------
Stock 2 5/10/2022 ---->15,000 525 100 ----------------------------------------------
Stock 3 5/10/2022 ---->15,000 2,080 445 ----------------------------------------------
Stock 4 5/10/2022 ----125.4 1,610 153 ----------------------------------------------
50 100 ----------------------------------------------
----24 0.0072 2.4 2.2 3.7 0.34 8 NE 0.32 1.3 0.12 16 0.023 0.085 0.2 1.4 0.005 5.4 0.017 6.6 6.6 6 68
----14,000 12 782 1,560 1,560 21 60.3 NE 156 1,560 1,560 9,380 93.8 156 5.5 1,560 93.8 1,250 7.82 156 156 3,120 939
Notes:
1. Concentrations reported in milligrams per kilogram (mg/kg).
2. "<" = not detected at or above the laboratory reporting limit.
3. Bold type denotes concentration is equal to or exceeds state action level or Soil-to-Groundwater MSCC.
4. MSCC denotes maximum soil contaminant concentration.
5. J denotes concentration estimated by project laboratory.
6. NE denotes not established.
ANALTYICAL METHOD
State Action Level (mg/kg)
EPA Method 8260
Soil-to-Groundwater MSCC (mg/kg)
Residential MSCC (mg/kg)
EPA Method 8015

FIGURES

HOPE VALLEY ROAD
WEST STATE HIGHWAY
54FORMERCIRCLE K #27201042

APPENDIX A
UST-3, UST-2 and UST-61

UST-3 Notice of lntent: UST Permanent Closure or Change-in-service
Return completed form to:
The DWM Regional Office located in the area where the facility is located Also send a copy to the Central Office in RaleiqhSEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE'ADDRESSES
STATE USE ONLY
tD #
Date Received
TNSTRUCTTONS (READ THtS FTRST)
Complete and return a UST-3 form at least thirty (30) days prior to closure or change-in-service activities lf a professional Engineer (p E ) or a LicensedGeologist (L G.) provides supervision for closure or change-in-service site assessment activities and signs and seals all closure reports then at least a five(5) working days' notice is acceptable
Completed UST closure or change-in-service site assessment reports, along with a copy of the UST-2A andtor 28 forms, should be submitted to theappropriate Division of Waste Management (DWM) Regional Office within thirty (30) days following closure activities The UST-2 form should also besubmitted to the Central Office in Raleigh so that the status of the tanks may be changed to permanently closed and your tank fee account can be closed outNote: Tank fees may be due for unregistered tanks.
UST closure and change-in-service site assessments must be completed in accordance with the latest version of the Guidetines for Site Checks, Tank Ctosureand lnitial Response. The guidelines can be obtained at Note: To close tanks in place you mustobtain prior approval from the DWM Regional office located in the region where the facility is located
You must make sure that UST_s removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will betaken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and-must be performed by a qualified company. Tanksdisposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment lf your tanks aie diiposed of imiroferly, youcould be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS il. LOCATTON
Owner Name (Corporation, lndividual, Public Agency, or Other Entity)
Circle K Stores, lnc
Facility Name or Company
Circle K Slore #2720104Street Address
1100 Situs Court, Suite 100
Facility lD # (lf known)
00-0-000001 51 30city countyRaleigh Wake Street Address
4835 Hope Valley Road
State
NC
Zip Code
27606 City County Zip CodeDurham Durham 27707Phone Number I Emait919-774-6700 | [e-mail]
Phone Number
91977467ooIII. CONTACT PERSONNEL
Company Name:
Circle K Stores
Name:
Alan Cubberlev Job Title:
Sr Manaqer Risk Control
Phone Number
91977467(c).-)IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE-IN SERVICE
a P E or L G , with all closure site assessment
reports bearing the signature and seal of the
P E orLG lf a release has notoccurred, the
supervision, signature or seal of a P.E or L.G
is not required
Keep closure records for three (3) years
6
7
51
2
Contact local fire marshal
Plan entire closure event.
Conduct Site Soil Assessment
lf removing tanks or closing in place, refer toAPI Publication 2015 Cleaning Petroleum
Sforage Tanks and 1604 Removat and
Disposa/ of Used Underground Petroleum
Storage Tanks
Provide a sketch locating piping, tanks and
soil sampling locations
Submit a closure report in the format of UST-
12 (including the form UST-2) within thirty
(30) days following the site investigation
lf a release from the tanks has occurred, the
site assessment portion of the tank closure
must be conducted under the supervision of
V. WORKTO BE PERFORMED BY
Contractor Name:
Jeremy DeVore
Contractor Company Name:
Zebra Environmental
Address:
901 East Springfield Road
State:
NC
Zip Code:
27263
Phone No:
336-442-1129
Primary Consultant Name:
Maureen A Jackson, PG
Primary Consultant Company Name:
ATC Associates of NC
Consultant Phone No:
91 9-561 -3893
VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE-IN-SERVICE
Tank lD No Size in Gallons Last Contents
Proposed Activity
Closure Change-l n-Service
Removal Abandonment in Place New Contents Stored
1 1 0000 Gasoline, Gas Mix
2 1 0000 Gasoline, Gas Mix
J 8000 Gasoline, Gas Mix x
4 8000 Dielsel, Dielsel Mix x trtrtr
Regional OfficeVII. OWNER OR OWNER'S AUTHORIZED REPRESENTATIVE
Has a release from a UST system occurred at this location? [ ves E ruo ! Unknown
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs
Print name and official title: Maureen A Jackson PG Sr PM ATC on behalf of Circle K Stores
/Erg(alure^ I;Y h 'r^r-'^hbb Date Signed
03123t2022
SCHEDULED REMOVAL DATE
Week of May 2,2022
Notify your DWM Regional Office
48 hours before this date if
scheduled removal date changes
UST-3 Rev 3/2020
8
UST-2A Site lnvestigation Report for Permanent Closure or Change-in-
Service of
REGISTERED UST
Return completed form to:
NC OEQ / DWM / UST SECTION
1646 MAIL SERVICE CENTER
RALE|GH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING
phone [phone] fax [phone] r r : _:: .:: _ r_ tr_ I
Facility lD #
Date Received
STATE USE ONLY
INSTRUCTIONS (READ THIS FIRST)
1 UST permanent closure or change in service must be completed in accordance with the latest version ol lhe Guidelines for Slte Checks, Tank
Closurc and lnitial Response and Abatement. The guidelines can be obtained at
2 Permanent closure: Complete all sections of this form
3. Chanqe-in-service: Where a UST system will be converted from storing a regulated substance to a non-regulated substance, complete sections l, ll,
lll, lV, and Vl
4 For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit
a wriften request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-2 form. The annual tank
,fee will be prorated based on the date of permanent closure.
6 UNREGISTERED USTs use Form UST-28
I. OWNERSHIP OF TANKS II. LOCATION OF TANKS
Orrrner Name (Corporation, lndividual, Public Agency, or Other Entity)Circle K Stores- lnc.Facility Name or Company
Circle K Store #2720104
Street Addressll00 Situs Coud- Suite 100 Facility lD # (lf known)
00-0-00000rsr30
"'t'*u,",an countY wake Street Address
4R15 Hnne Vallerr Rnqd
State - -^ Zip CodeNC 27606
Citv County Zip Code'Durham Durhani 2770':-
Phone Number (9t9) 77 4-6700
Phone Number
(919\'774-6700
III. CONTACT PERSONNEL
Contact for Facility:
Alan Cubberly
Job Title:
Environmental [phone]
#Phone
Closure Contractor Name:
Shawn Tucker
closure contractor company:
Zebra Environmental
Address:.r,,, E Springfierd Rd
Hrgh Pornt NC 272(,1
Phone #
(336) 628-827 4
Primary Consultant Name:
Maureen Jackson. PC
Pnmary Consultant company:
A]'C Associates ol NC
Address:1,1pa plner Rd surle r r5
Wilmrnglon NC 28.109
Phone #
[phone]
IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
UNREGISTERED USTs use Form UST-28
V. EXCAVATION CONDITION
anK llJ
No
Size rn
Gallons
LaSt
Contents
Last
Use
Date
Permanent
Close Date
Method of Permanent Closure:
lndicate REMOVED or enter fill
material, such as foam/
concrete/ sand
Change-in-
Service
Date
Water in
excavation Free product
Notable
odor or
visible soil
@ntaminatio
n
Yes No Yes No Y No
I t0.000 Gasoline 05t09t22 051 I 112022 Removed tr tr tr E E tr
2 10.000 Casoline 0st09t22 05ilU2022 Removed tr m tr EI E tr
J 8.000 Casoline 05t09t22 0sfiv2022 Removed tr E]tr ts EE tr
4 8.000 Diesel 05109122 05fi12022 Removed E tl tr E ts tr
tr tr tr tr tr tr
tr tr tr tr tr D
VI. CERTIFICATION
I certi! under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate
and complete
Print name and official title of owner or owner's authorized representative
Maureen A. Jackson, PG Sr. Project Ma4dgqATC on behalf of Circle K Stores
May 12.2022
NORTH CAROLINA DEPAXTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH. NC 27699-1646 PHONE [phone] FAX (919) 7'15-1117 ; i,. i ,,.:j,, :.':'.: i:r : :,. 1120'16
U5T.61 24-Hour Release and UST Leak
For Releases
in NG
This form should be completed and submitted to the UST Section's regional office following a known or suspected release fromanundergroundstoragetank(UST) system Thisformisrequiredtobesubmittedwithin24hoursofdiscoveryofaknownor
suspected release
(DWM USE ONLY)
lncident # Risk (H,|,L,U)_
Received On _ Received By _
Reported by (circle one): Phone, Fax or Report
Region
Suspected Contamination? (Y/N) Y
Confirmed GW Contaminationz 1Vltl1 f,Confirmed Soil Contamination ?(Y/N) Y
Samples Taken?(Y/N) Y
Free Producl? (Y/N) L-n[l Yes. State Greatest
Thickness
Facilitv lD Number 0-00000 l5 130
Date iea k Di ""or" rJd---OilTTZOfT
Comm/Non-Commercial? Comm
Reg/Non-regulated? Req
lncident Name: Circle K Store #Z72OyO4
INCIDENT DESCRIPTION
Address: 4835 Hope Valley Road County: Durham
City/Town: Durham I Zip Code: 27707
e one): Asheville, Mooresville, Fayetteville,
, Wilmington, Winston-Salem
Latitude (oeomat oesrees): 35.91 9270-N Longitude (deqmat desrees
Briefly describe suspected or confirmed release (including but not limited
Petroleum-impacted soil was identified during UST closure activ
HOW RELEASE WAS DISCOVERED lnereasecoael
(Check one)
lRetease Detection Equipment or Methods | flvsuauOoo, I ! Groundwater Contamination
!Sr.face Water ContaminationI During UST Closure/Removal
!eroperty Transfer
lWater in Tank
!Water Supply Well Contamination !otne, (specify)
Source of Release
(Check primary source)
[lranr
! Ripins
! Dirp"nse.
! Submersible Turbine Pump
! oetivery Problem
! spitt auctet
!otn",
! unkno*n
Definitions presented on reverse
SOURCE OF CONTAMINATION
Product Tvpe Released
(Check primary product type released)
Cause of Release
(Check primary cause)
f]spitr
! overfitt
! conosion
! Physical/Mechanical
Damage
! lnstall Problem
! otn",
ffi unkno*n
Definitions presented on reverse
Tvpe of Release
(Check one)
ff R"trot"r,
fl Non-Petroleum
! eotn
Location
(Check one)
IFacility
!Residence
!otn"'.
$Gasoline/ Diesel/
Kerosene
! Heating Oil
E otn"r Petroleum
Products
! uetats
! otner lnorganics
! other organics
! DieselA/eg Oit
Blend
! Vegetable Oil 100%
! ero - rzo
lrzr -ra+
! eas - ess
flEthanol 1oo%
! eor - eos
Ownership1 Municipal 2 Military 3 Unknown 5 Federal 6 County 7 State
Operation Tvoe'1 Public Service 2 Agricultural 3 Residential 4 EducationiRelig 5 lndustriat Mining
UST Form 61 (02/19)Page 1 of 2
Water Supply Wells Affected? .1 Yes
TER SUPPLIES
Number of Water Supply Wells Affected
Water Supply Wells
1
2.
3 -lncluae
users Names, Addresses and Numters-attacn aOOitional sheet if necessaryl
UST SYSTEM OWNER
UST Owner/ComPanY
Circle K Stores. Inc.
Address
I 100 Situs Court, Suite 100
Telephone Number
[phone]
UST SYSTEM OPERATOR
Address
ll00 Situs Couft, Suite 100
UST Operator/ComPanY
Circle K Stores, lnc.
LANDOWNER AT LOCATION OF UST INCIDENT
Address
l9l9 Wilshire Drive
Landowner
Domar Corporation, lnc.
Draw Sketch of Area (showing two major road intersections) or Attach Map
Site map attached
Date May 11,2022Address 2725 E. Millbrook Rd, Suite l2!
orm 61 (o2t1e)Page 2 ol 2
Delinitions ofSourcesTank: means the tank that stores the product and is part ofthe underground storage tank system
piping: means the piping and connectors running lrom the tank or sub]nersible turbine pump to the dispenser or other end-use equipment (vent, vapor recovery' or flll
lines are excluded )
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e g, a release fiom a suction pump or from components located above
the shear valve)
Submersible Turbine pump (STp) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak deteclor, and the piping that
connects the submersible turbine pump to the tank
Delivery problem. identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills )
other; serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases lrom vent lines. vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an over;ll occurs (e.g., oueifills may occur tiom the fill pipe at the tank or when the nozzle fails to shut off at the d ispenser)
Physical or Mechanical Damage: fittlngs' broken
components, and com
Corrosion:use when a metal tank
lnstallation Problem: use when
+ cr:-r^ ^^- ^r+ha ^ lls)Other: use this option when the cause is known but does not fit lnto one ofthe p o monltorrng we
Unknown: use when the cause has not been detennined
Circle K Store #2720104
4835 Hope Valley Road
Durham, NC

APPENDIX B
Laboratory Reports and
Chains-of-Custody Documents

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/23/2022
ATC Group Services, LLC - Raleigh, NC Maureen Jackson
609A Piner Road Suite 115 Wilminton, NC, 28409
Ref: Analytical Testing
Lab Report Number: 22-133-0023 Client Project Description: Circle K 2720104
Dear Maureen Jackson:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/13/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 166
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-133-0023
Page 2 of 166
Report Number:
Sample Summary Table
Client Project Description:
22-133-0023
Circle K 2720104
Lab No Client Sample ID Matrix Date Collected Date Received
05/10/2022 13:10Solids 89765 Stockpile 1 05/13/2022 11:00
05/10/2022 10:10Solids 89766 Stock 2 05/13/2022 11:00
05/10/2022 10:15Solids 89767 Stock 3 05/13/2022 11:00
05/10/2022 10:20Solids 89768 Stock 4 05/13/2022 11:00
05/11/2022 09:10Solids 89769 D-1 05/13/2022 11:00
05/11/2022 09:15Solids 89770 D-2 05/13/2022 11:00
05/11/2022 15:40Solids 89771 D-3 05/13/2022 11:00
05/11/2022 10:30Solids 89772 W-1 05/13/2022 11:00
05/11/2022 10:35Solids 89773 W-2 05/13/2022 11:00
05/11/2022 10:40Solids 89774 W-3 05/13/2022 11:00
05/11/2022 10:45Solids 89775 W-4 05/13/2022 11:00
05/11/2022 10:50Solids 89776 W-5 05/13/2022 11:00
05/11/2022 13:00Solids 89777 W-6 05/13/2022 11:00
05/11/2022 13:05Solids 89778 W-7 05/13/2022 11:00
05/11/2022 14:30Solids 89779 W-8 05/13/2022 11:00
05/11/2022 14:35Solids 89780 W-9 05/13/2022 11:00
05/11/2022 14:40Solids 89781 W-10 05/13/2022 11:00
05/11/2022 16:15Solids 89782 W-11 05/13/2022 11:00
05/11/2022 16:20Solids 89783 W-12 05/13/2022 11:00
05/11/2022 16:25Solids 89784 W-13 05/13/2022 11:00
05/11/2022 16:30Solids 89785 W-14 05/13/2022 11:00
05/12/2022 08:10Solids 89786 D-4 05/13/2022 11:00
05/12/2022 08:00Solids 89787 L-1 05/13/2022 11:00
05/12/2022 08:05Solids 89788 L-2 05/13/2022 11:00
05/12/2022 11:00Solids 89789 L-3 05/13/2022 11:00
05/12/2022 11:05Solids 89790 L-4 05/13/2022 11:00
05/12/2022 11:10Solids 89791 L-5 05/13/2022 11:00
Page 3 of 166
Report Number:
Sample Summary Table
Client Project Description:
22-133-0023
Circle K 2720104
Lab No Client Sample ID Matrix Date Collected Date Received
05/12/2022 13:30Solids 89792 L-6 05/13/2022 11:00
Page 4 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89765Stockpile 1
759 05/19/2022 22:498015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 106
4770 05/16/2022 18:258015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 23.6
12.2 05/20/2022 12:52SW-DRYWT Moisture %
V 89766Stock 2
100 05/19/2022 23:108015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.61
525 05/16/2022 17:578015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.50
17.1 05/19/2022 10:40SW-DRYWT Moisture %
V 89767Stock 3
445 05/20/2022 13:308015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 26.9
2080 05/16/2022 18:538015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 23.9
13.3 05/19/2022 10:40SW-DRYWT Moisture %
V 89768Stock 4
153 05/19/2022 23:538015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.80
1610 05/16/2022 19:218015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 25.8
19.8 05/19/2022 10:40SW-DRYWT Moisture %
V 89769D-1
39.1 05/16/2022 11:538015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.55
0.049 05/16/2022 17:428260DAcetonemg/Kg - dry 0.002
J0.002 05/16/2022 17:428260DBenzenemg/Kg - dry 0.0007
J0.003 05/16/2022 17:428260DCarbon Disulfide mg/Kg - dry 0.0008
J0.001 05/16/2022 17:428260Dn-Hexane mg/Kg - dry 0.0008
J0.006 05/16/2022 17:428260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.002 05/16/2022 17:428260DNaphthalenemg/Kg - dry 0.001
J0.001 05/16/2022 17:428260DToluenemg/Kg - dry 0.0008
J0.002 05/16/2022 17:428260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0008 05/16/2022 17:428260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/16/2022 17:428260Do-Xylene mg/Kg - dry 0.0006
J0.001 05/16/2022 17:428260Dm,p-Xylene mg/Kg - dry 0.001
J0.003 05/16/2022 17:428260DXylene (Total)mg/Kg - dry 0.0006
18.7 05/18/2022 11:01SW-DRYWT Moisture %
V 89770D-2
J3.64 05/16/2022 12:218015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.72
J0.006 05/16/2022 18:108260DAcetonemg/Kg - dry 0.003
0.015 05/16/2022 18:108260DBenzenemg/Kg - dry 0.0008
Page 5 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89770D-2
0.016 05/16/2022 18:108260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.001
J0.005 05/16/2022 18:108260DEthylbenzenemg/Kg - dry 0.0008
J0.003 05/16/2022 18:108260DIsopropylbenzenemg/Kg - dry 0.0006
0.170 05/16/2022 18:108260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.004 05/16/2022 18:108260DNaphthalenemg/Kg - dry 0.001
J0.002 05/16/2022 18:108260Dn-Propylbenzene mg/Kg - dry 0.0007
0.012 05/16/2022 18:108260DToluenemg/Kg - dry 0.0009
J0.003 05/16/2022 18:108260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.001 05/16/2022 18:108260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/16/2022 18:108260Do-Xylene mg/Kg - dry 0.0007
J0.005 05/16/2022 18:108260Dm,p-Xylene mg/Kg - dry 0.001
J0.006 05/16/2022 18:108260DXylene (Total)mg/Kg - dry 0.0007
23.8 05/18/2022 11:01SW-DRYWT Moisture %
V 89771D-3
J2.68 05/16/2022 12:498015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.28
J0.013 05/16/2022 18:388260DAcetonemg/Kg - dry 0.002
J0.001 05/16/2022 18:388260DBenzenemg/Kg - dry 0.0006
J0.002 05/16/2022 18:388260DCarbon Disulfide mg/Kg - dry 0.0007
J0.0009 05/16/2022 18:388260DEthylbenzenemg/Kg - dry 0.0006
J0.004 05/16/2022 18:388260Dn-Hexane mg/Kg - dry 0.0007
J0.001 05/16/2022 18:388260DNaphthalenemg/Kg - dry 0.001
J0.0007 05/16/2022 18:388260Dn-Propylbenzene mg/Kg - dry 0.0006
J0.003 05/16/2022 18:388260DToluenemg/Kg - dry 0.0007
J0.003 05/16/2022 18:388260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0005
J0.002 05/16/2022 18:388260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
0.006 05/16/2022 18:388260Do-Xylene mg/Kg - dry 0.0006
J0.004 05/16/2022 18:388260Dm,p-Xylene mg/Kg - dry 0.001
J0.010 05/16/2022 18:388260DXylene (Total)mg/Kg - dry 0.0006
9.36 05/18/2022 11:01SW-DRYWT Moisture %
V 89772W-1
109 05/20/2022 00:148015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.46
J2.63 05/16/2022 13:178015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.43
0.023 05/16/2022 19:068260DAcetonemg/Kg - dry 0.002
J0.002 05/16/2022 19:068260DBenzenemg/Kg - dry 0.0007
0.026 05/16/2022 19:068260DCarbon Disulfide mg/Kg - dry 0.0008
J0.002 05/16/2022 19:068260Dn-Hexane mg/Kg - dry 0.0008
Page 6 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89772W-1
J0.006 05/16/2022 19:068260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.001 05/16/2022 19:068260DToluenemg/Kg - dry 0.0008
J0.0008 05/16/2022 19:068260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0009 05/16/2022 19:068260Do-Xylene mg/Kg - dry 0.0006
J0.0009 05/16/2022 19:068260DXylene (Total)mg/Kg - dry 0.0006
14.8 05/18/2022 11:01SW-DRYWT Moisture %
V 89773W-2
32.7 05/20/2022 00:358015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.22
J2.46 05/16/2022 13:458015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.33
11.0 05/18/2022 11:01SW-DRYWT Moisture %
V 89774W-3
J0.011 05/16/2022 20:018260DAcetonemg/Kg - dry 0.002
J0.001 05/16/2022 20:018260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
12.3 05/18/2022 11:01SW-DRYWT Moisture %
V 89775W-4
J3.84 05/16/2022 14:418015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.47
J0.016 05/16/2022 20:288260DAcetonemg/Kg - dry 0.002
J0.002 05/16/2022 20:288260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
16.2 05/18/2022 11:01SW-DRYWT Moisture %
V 89776W-5
13.0 05/20/2022 02:218015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.92
J0.017 05/16/2022 20:568260DAcetonemg/Kg - dry 0.003
J0.003 05/16/2022 20:568260DBenzenemg/Kg - dry 0.0007
J0.0007 05/16/2022 20:568260Dn-Butylbenzene mg/Kg - dry 0.0006
0.008 05/16/2022 20:568260DCarbon Disulfide mg/Kg - dry 0.0008
J0.001 05/16/2022 20:568260DEthylbenzenemg/Kg - dry 0.0007
J0.011 05/16/2022 20:568260Dn-Hexane mg/Kg - dry 0.0008
J0.006 05/16/2022 20:568260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
0.012 05/16/2022 20:568260DToluenemg/Kg - dry 0.0008
0.009 05/16/2022 20:568260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.005 05/16/2022 20:568260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
0.008 05/16/2022 20:568260Do-Xylene mg/Kg - dry 0.0006
0.018 05/16/2022 20:568260Dm,p-Xylene mg/Kg - dry 0.001
0.026 05/16/2022 20:568260DXylene (Total)mg/Kg - dry 0.0006
Page 7 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89776W-5
21.5 05/18/2022 11:01SW-DRYWT Moisture %
V 89777W-6
J9.06 05/20/2022 02:428015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.73
10.3 05/16/2022 16:058015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.55
18.9 05/18/2022 11:01SW-DRYWT Moisture %
V 89778W-7
23.2 05/20/2022 03:048015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 6.09
13.9 05/16/2022 16:338015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.71
0.035 05/16/2022 21:248260DAcetonemg/Kg - dry 0.003
J0.003 05/16/2022 21:248260DBenzenemg/Kg - dry 0.0008
J0.004 05/16/2022 21:248260DCarbon Disulfide mg/Kg - dry 0.0008
6.36 05/17/2022 23:578260DChloroformmg/Kg - dry 0.344
0.023 05/16/2022 21:248260DMethylene Chloride mg/Kg - dry 0.001
J0.002 05/16/2022 21:248260DTetrachloroethenemg/Kg - dry 0.001
J0.001 05/16/2022 21:248260DToluenemg/Kg - dry 0.0009
J0.006 05/16/2022 21:248260DTrichloroethenemg/Kg - dry 0.001
J0.0009 05/16/2022 21:248260Do-Xylene mg/Kg - dry 0.0007
J0.0009 05/16/2022 21:248260DXylene (Total)mg/Kg - dry 0.0007
23.6 05/19/2022 10:40SW-DRYWT Moisture %
V 89779W-8
J2.64 05/16/2022 17:008015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.33
0.044 05/17/2022 23:298260DAcetonemg/Kg - dry 0.002
J0.002 05/17/2022 23:298260DBenzenemg/Kg - dry 0.0007
J0.0008 05/17/2022 23:298260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.0008
J0.002 05/17/2022 23:298260Dn-Hexane mg/Kg - dry 0.0007
11.1 05/19/2022 10:40SW-DRYWT Moisture %
V 89780W-9
15.9 05/20/2022 03:468015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.74
J4.68 05/16/2022 17:298015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.56
19.0 05/19/2022 10:40SW-DRYWT Moisture %
V 89781W-10
33.6 05/17/2022 15:248015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.71
J0.017 05/16/2022 22:198260DAcetonemg/Kg - dry 0.003
Page 8 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89781W-10
23.7 05/19/2022 10:40SW-DRYWT Moisture %
V 89782W-11
37.4 05/20/2022 04:298015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.88
63.5 05/17/2022 20:318015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.62
20.9 05/19/2022 10:40SW-DRYWT Moisture %
V 89783W-12
53.2 05/20/2022 04:508015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.80
75.7 05/17/2022 20:598015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.58
0.304 05/20/2022 13:218260DBenzenemg/Kg - dry 0.018
0.491 05/20/2022 13:218260Dn-Butylbenzene mg/Kg - dry 0.015
0.163 05/20/2022 13:218260Dsec-Butyl benzene mg/Kg - dry 0.017
3.30 05/20/2022 13:218260DEthylbenzenemg/Kg - dry 0.018
3.05 05/20/2022 13:218260Dn-Hexane mg/Kg - dry 0.020
0.339 05/20/2022 13:218260DIsopropylbenzenemg/Kg - dry 0.014
J0.067 05/20/2022 13:218260D4-Isopropyl toluene mg/Kg - dry 0.040
1.13 05/20/2022 13:218260DNaphthalenemg/Kg - dry 0.030
1.37 05/20/2022 13:218260Dn-Propylbenzene mg/Kg - dry 0.016
2.56 05/20/2022 13:218260DToluenemg/Kg - dry 0.020
7.11 05/20/2022 13:218260D1,2,4-Trimethylbenzene mg/Kg - dry 0.015
1.95 05/20/2022 13:218260D1,3,5-Trimethylbenzene mg/Kg - dry 0.016
3.39 05/20/2022 13:218260Do-Xylene mg/Kg - dry 0.015
11.1 05/20/2022 13:218260Dm,p-Xylene mg/Kg - dry 0.039
14.5 05/20/2022 13:218260DXylene (Total)mg/Kg - dry 0.015
19.8 05/19/2022 10:40SW-DRYWT Moisture %
V 89784W-13
J5.87 05/20/2022 05:548015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.21
7.63 05/17/2022 15:528015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.41
J0.022 05/17/2022 21:388260DAcetonemg/Kg - dry 0.002
J0.005 05/17/2022 21:388260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
10.8 05/19/2022 10:40SW-DRYWT Moisture %
V 89785W-14
115 05/20/2022 06:158015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.10
J5.10 05/17/2022 16:208015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.27
J0.008 05/20/2022 12:268260DAcetonemg/Kg - dry 0.002
Page 9 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89785W-14
J0.001 05/20/2022 12:268260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
8.78 05/19/2022 10:40SW-DRYWT Moisture %
V 89786D-4
J2.99 05/17/2022 16:488015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.81
J0.017 05/16/2022 22:478260DAcetonemg/Kg - dry 0.003
J0.002 05/16/2022 22:478260DBenzenemg/Kg - dry 0.0008
J0.001 05/16/2022 22:478260DEthylbenzenemg/Kg - dry 0.0008
J0.001 05/16/2022 22:478260DIsopropylbenzenemg/Kg - dry 0.0006
0.012 05/16/2022 22:478260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.001 05/16/2022 22:478260Dn-Propylbenzene mg/Kg - dry 0.0007
0.008 05/16/2022 22:478260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/16/2022 22:478260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/16/2022 22:478260Do-Xylene mg/Kg - dry 0.0007
0.013 05/16/2022 22:478260Dm,p-Xylene mg/Kg - dry 0.001
J0.015 05/16/2022 22:478260DXylene (Total)mg/Kg - dry 0.0007
26.3 05/19/2022 10:40SW-DRYWT Moisture %
V 89787L-1
J2.51 05/17/2022 17:168015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.40
0.037 05/16/2022 23:158260DAcetonemg/Kg - dry 0.002
J0.002 05/16/2022 23:158260DCarbon Disulfide mg/Kg - dry 0.0007
J0.007 05/16/2022 23:158260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.001 05/16/2022 23:158260DToluenemg/Kg - dry 0.0008
13.8 05/19/2022 10:40SW-DRYWT Moisture %
V 89788L-2
J0.019 05/16/2022 23:428260DAcetonemg/Kg - dry 0.003
J0.005 05/16/2022 23:428260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.002 05/16/2022 23:428260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
22.4 05/19/2022 10:40SW-DRYWT Moisture %
V 89789L-3
25.9 05/17/2022 18:128015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.34
0.025 05/17/2022 13:478260DAcetonemg/Kg - dry 0.002
J0.001 05/17/2022 13:478260DBenzenemg/Kg - dry 0.0007
J0.001 05/17/2022 13:478260DEthylbenzenemg/Kg - dry 0.0007
J0.004 05/17/2022 13:478260Dn-Hexane mg/Kg - dry 0.0007
Page 10 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89789L-3
J0.004 05/17/2022 13:478260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0007
J0.0006 05/17/2022 13:478260Dn-Propylbenzene mg/Kg - dry 0.0006
0.006 05/17/2022 13:478260DToluenemg/Kg - dry 0.0007
J0.002 05/17/2022 13:478260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.001 05/17/2022 13:478260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
J0.002 05/17/2022 13:478260Do-Xylene mg/Kg - dry 0.0006
J0.005 05/17/2022 13:478260Dm,p-Xylene mg/Kg - dry 0.001
J0.007 05/17/2022 13:478260DXylene (Total)mg/Kg - dry 0.0006
11.7 05/19/2022 10:40SW-DRYWT Moisture %
V 89790L-4
J2.78 05/17/2022 18:408015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.78
J0.012 05/17/2022 14:158260DAcetonemg/Kg - dry 0.003
J0.003 05/17/2022 14:158260DBenzenemg/Kg - dry 0.0008
J0.003 05/17/2022 14:158260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.001
J0.001 05/17/2022 14:158260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
0.023 05/17/2022 14:158260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.001 05/17/2022 14:158260DToluenemg/Kg - dry 0.0009
J0.001 05/17/2022 14:158260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/17/2022 14:158260Do-Xylene mg/Kg - dry 0.0007
J0.001 05/17/2022 14:158260DXylene (Total)mg/Kg - dry 0.0007
25.6 05/19/2022 10:40SW-DRYWT Moisture %
V 89791L-5
J0.005 05/17/2022 14:438260DAcetonemg/Kg - dry 0.003
J0.002 05/17/2022 14:438260DBenzenemg/Kg - dry 0.0007
J0.001 05/17/2022 14:438260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.0009
J0.0009 05/17/2022 14:438260DEthylbenzenemg/Kg - dry 0.0007
J0.002 05/17/2022 14:438260Dn-Hexane mg/Kg - dry 0.0008
0.034 05/17/2022 14:438260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
0.008 05/17/2022 14:438260DToluenemg/Kg - dry 0.0008
J0.0010 05/17/2022 14:438260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.001 05/17/2022 14:438260Do-Xylene mg/Kg - dry 0.0006
J0.002 05/17/2022 14:438260Dm,p-Xylene mg/Kg - dry 0.001
J0.004 05/17/2022 14:438260DXylene (Total)mg/Kg - dry 0.0006
20.0 05/19/2022 10:40SW-DRYWT Moisture %
Page 11 of 166
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-133-0023
Report Limit
Project:Circle K 2720104
V 89792L-6
0.030 05/17/2022 15:108260DAcetonemg/Kg - dry 0.003
0.021 05/17/2022 15:108260DBenzenemg/Kg - dry 0.0008
J0.001 05/17/2022 15:108260DChloroformmg/Kg - dry 0.001
J0.002 05/17/2022 15:108260Dn-Hexane mg/Kg - dry 0.0009
0.010 05/17/2022 15:108260DToluenemg/Kg - dry 0.0009
J0.0008 05/17/2022 15:108260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0009 05/17/2022 15:108260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.001 05/17/2022 15:108260Do-Xylene mg/Kg - dry 0.0007
J0.003 05/17/2022 15:108260Dm,p-Xylene mg/Kg - dry 0.001
J0.004 05/17/2022 15:108260DXylene (Total)mg/Kg - dry 0.0007
24.4 05/19/2022 10:40SW-DRYWT Moisture %
Page 12 of 166

Client: ATC Group Services, LLC - Raleigh, NC CASE NARRATIVE
Project: Circle K 2720104 Lab Report Number: 22-133-0023
Date: 5/23/2022
Total Petroleum Hydrocarbons - Extractable Method 8015C DRO Sample 89767 (Stock 3) QC Batch No: V18982/V18830
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Total Petroleum Hydrocarbons - Volatile Method 8015C GRO
Sample 89772 (W-1) Analyte: a,a,a-Trifluorotoluene
QC Batch No: V18714/V18713 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Sample 89773 (W-2)
Analyte: a,a,a-Trifluorotoluene QC Batch No: V18714/V18713
Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits. Sample 89774 (W-3) Analyte: a,a,a-Trifluorotoluene
QC Batch No: V18714/V18713 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Chloroethane QC Batch No: V18810/V18747
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Chloroethane QC Batch No: V18871/V18747 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 13 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stockpile 1
89765 Matrix:
5/10/2022 13:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.2 %Moisture 1 05/20/22 12:52 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stockpile 1
89765 Matrix:
5/10/2022 13:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
759 mg/Kg - dry 106 228Diesel Range Organics (C10-C28)20 05/19/22 22:49 V18982JLK
8015C DROSurrogate: OTP Surrogate 82.0 Limits: 31-123%05/19/22 22:4920 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
4770 mg/Kg - dry 23.6 56.9Gasoline Range Organics (C6-C10)500 05/16/22 18:25 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 124 Limits: 50-137%05/16/22 18:25500 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 2
89766 Matrix:
5/10/2022 10:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.1 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 2
89766 Matrix:
5/10/2022 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
100 mg/Kg - dry 5.61 12.1Diesel Range Organics (C10-C28)1 05/19/22 23:10 V18982JLK
8015C DROSurrogate: OTP Surrogate 83.5 Limits: 31-123%05/19/22 23:101 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
525 mg/Kg - dry 2.50 6.03Gasoline Range Organics (C6-C10)50 05/16/22 17:57 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 77.0 Limits: 50-137%05/16/22 17:5750 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 3
89767 Matrix:
5/10/2022 10:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.3 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 3
89767 Matrix:
5/10/2022 10:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
445 mg/Kg - dry 26.9 57.7Diesel Range Organics (C10-C28)5 05/20/22 13:30 V18982JLK
8015C DROSurrogate: OTP Surrogate 75.9 Limits: 31-123%05/20/22 13:305 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
2080 mg/Kg - dry 23.9 57.7Gasoline Range Organics (C6-C10)500 05/16/22 18:53 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 125 Limits: 50-137%05/16/22 18:53500 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 4
89768 Matrix:
5/10/2022 10:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.8 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:Stock 4
89768 Matrix:
5/10/2022 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
153 mg/Kg - dry 5.80 12.5Diesel Range Organics (C10-C28)1 05/19/22 23:53 V18982JLK
8015C DROSurrogate: OTP Surrogate 92.5 Limits: 31-123%05/19/22 23:531 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
1610 mg/Kg - dry 25.8 62.3Gasoline Range Organics (C6-C10)500 05/16/22 19:21 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 85.4 Limits: 50-137%05/16/22 19:21500 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-1
89769 Matrix:
5/11/2022 9:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.7 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-1
89769 Matrix:
5/11/2022 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
39.1 mg/Kg - dry 2.55 6.15Gasoline Range Organics (C6-C10)50 05/16/22 11:53 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 134 Limits: 50-137%05/16/22 11:5350 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.049 mg/Kg - dry 0.002 0.024Acetone 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 05/16/22 17:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 05/16/22 17:42 V18748TBL
0.002 J mg/Kg - dry 0.0007 0.006Benzene 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Bromobenzene 1 05/16/22 17:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/16/22 17:42 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
tert-Butyl benzene 1 05/16/22 17:42 V18748TBL
0.003 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 05/16/22 17:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 17:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-1
89769 Matrix:
5/11/2022 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/16/22 17:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/16/22 17:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 17:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 17:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 17:42 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 17:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 17:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloroethene 1 05/16/22 17:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 17:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 17:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 05/16/22 17:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-1
89769 Matrix:
5/11/2022 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 17:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 17:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 05/16/22 17:42 V18748TBL
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 05/16/22 17:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 17:42 V18748TBL
0.006 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 05/16/22 17:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 17:42 V18748TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/16/22 17:42 V18748TBL
0.002 J mg/Kg - dry 0.001 0.012Naphthalene 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 17:42 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 17:42 V18748TBL
0.001 J mg/Kg - dry 0.0008 0.006Toluene 1 05/16/22 17:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/16/22 17:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/16/22 17:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-1
89769 Matrix:
5/11/2022 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/16/22 17:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 17:42 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/16/22 17:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 17:42 V18748TBL
0.002 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 17:42 V18748TBL
0.0008 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/16/22 17:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 05/16/22 17:42 V18748TBL
0.001 J mg/Kg - dry 0.0006 0.006o-Xylene 1 05/16/22 17:42 V18748TBL
0.001 J mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/16/22 17:42 V18748TBL
0.003 J mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/16/22 17:42 V18748
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/16/22 17:421 TBL V18748
Surrogate: Dibromofluoromethane 106 Limits: 84-123%05/16/22 17:421 TBL V18748
Surrogate: Toluene-d8 86.1 Limits: 76-129%05/16/22 17:421 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-2
89770 Matrix:
5/11/2022 9:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.8 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-2
89770 Matrix:
5/11/2022 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
3.64 J mg/Kg - dry 2.72 6.56Gasoline Range Organics (C6-C10)50 05/16/22 12:21 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 131 Limits: 50-137%05/16/22 12:2150 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.006 J mg/Kg - dry 0.003 0.026Acetone 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/16/22 18:10 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/16/22 18:10 V18748TBL
0.015 mg/Kg - dry 0.0008 0.006Benzene 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Bromobenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/16/22 18:10 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
tert-Butyl benzene 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 18:10 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 18:10 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 18:10 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-2
89770 Matrix:
5/11/2022 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/16/22 18:10 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 18:10 V18748TBL
0.016 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 18:10 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 18:10 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 18:10 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloroethene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 18:10 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/16/22 18:10 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-2
89770 Matrix:
5/11/2022 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/16/22 18:10 V18748TBL
0.005 J mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/16/22 18:10 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/16/22 18:10 V18748TBL
0.003 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 18:10 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/16/22 18:10 V18748TBL
0.170 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 18:10 V18748TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/16/22 18:10 V18748TBL
0.004 J mg/Kg - dry 0.001 0.013Naphthalene 1 05/16/22 18:10 V18748TBL
0.002 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 18:10 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 18:10 V18748TBL
0.012 mg/Kg - dry 0.0009 0.006Toluene 1 05/16/22 18:10 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/16/22 18:10 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/16/22 18:10 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-2
89770 Matrix:
5/11/2022 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/16/22 18:10 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 18:10 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/16/22 18:10 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 18:10 V18748TBL
0.003 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 18:10 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/16/22 18:10 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 05/16/22 18:10 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/16/22 18:10 V18748TBL
0.005 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/16/22 18:10 V18748TBL
0.006 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/16/22 18:10 V18748
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/16/22 18:101 TBL V18748
Surrogate: Dibromofluoromethane 103 Limits: 84-123%05/16/22 18:101 TBL V18748
Surrogate: Toluene-d8 88.7 Limits: 76-129%05/16/22 18:101 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-3
89771 Matrix:
5/11/2022 15:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.36 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 32 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-3
89771 Matrix:
5/11/2022 15:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
2.68 J mg/Kg - dry 2.28 5.52Gasoline Range Organics (C6-C10)50 05/16/22 12:49 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 134 Limits: 50-137%05/16/22 12:4950 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.013 J mg/Kg - dry 0.002 0.022Acetone 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/16/22 18:38 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 05/16/22 18:38 V18748TBL
0.001 J mg/Kg - dry 0.0006 0.005Benzene 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Bromobenzene 1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/16/22 18:38 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
tert-Butyl benzene 1 05/16/22 18:38 V18748TBL
0.002 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 05/16/22 18:38 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 05/16/22 18:38 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 33 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-3
89771 Matrix:
5/11/2022 15:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/16/22 18:38 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/16/22 18:38 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/16/22 18:38 V18748TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 05/16/22 18:38 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/16/22 18:38 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloroethene 1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/16/22 18:38 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 05/16/22 18:38 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 34 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-3
89771 Matrix:
5/11/2022 15:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/16/22 18:38 V18748TBL
0.0009 J mg/Kg - dry 0.0006 0.005Ethylbenzene 1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 18:38 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/16/22 18:38 V18748TBL
0.004 J mg/Kg - dry 0.0007 0.011n-Hexane 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/16/22 18:38 V18748TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/16/22 18:38 V18748TBL
0.001 J mg/Kg - dry 0.001 0.011Naphthalene 1 05/16/22 18:38 V18748TBL
0.0007 J mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Styrene 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/16/22 18:38 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/16/22 18:38 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 05/16/22 18:38 V18748TBL
0.003 J mg/Kg - dry 0.0007 0.005Toluene 1 05/16/22 18:38 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/16/22 18:38 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/16/22 18:38 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 35 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-3
89771 Matrix:
5/11/2022 15:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/16/22 18:38 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/16/22 18:38 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/16/22 18:38 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/16/22 18:38 V18748TBL
0.003 J mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 05/16/22 18:38 V18748TBL
0.002 J mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/16/22 18:38 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/16/22 18:38 V18748TBL
0.006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/16/22 18:38 V18748TBL
0.004 J mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/16/22 18:38 V18748TBL
0.010 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/16/22 18:38 V18748
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%05/16/22 18:381 TBL V18748
Surrogate: Dibromofluoromethane 102 Limits: 84-123%05/16/22 18:381 TBL V18748
Surrogate: Toluene-d8 88.2 Limits: 76-129%05/16/22 18:381 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 36 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-1
89772 Matrix:
5/11/2022 10:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.8 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 37 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-1
89772 Matrix:
5/11/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
109 mg/Kg - dry 5.46 11.7Diesel Range Organics (C10-C28)1 05/20/22 00:14 V18982JLK
8015C DROSurrogate: OTP Surrogate 96.2 Limits: 31-123%05/20/22 00:141 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
2.63 J mg/Kg - dry 2.43 5.87Gasoline Range Organics (C6-C10)50 05/16/22 13:17 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 155 *Limits: 50-137%05/16/22 13:1750 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.023 mg/Kg - dry 0.002 0.023
Acetone 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/16/22 19:06 V18748TBL
0.002 J mg/Kg - dry 0.0007 0.005Benzene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/16/22 19:06 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/16/22 19:06 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 38 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-1
89772 Matrix:
5/11/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/16/22 19:06 V18748TBL
0.026 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/16/22 19:06 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/16/22 19:06 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 05/16/22 19:06 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005
Dibromomethane 1 05/16/22 19:06 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/16/22 19:06 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/16/22 19:06 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/16/22 19:06 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 39 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-1
89772 Matrix:
5/11/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/16/22 19:06 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/16/22 19:06 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 19:06 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/16/22 19:06 V18748TBL
0.002 J mg/Kg - dry 0.0008 0.011n-Hexane 1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/16/22 19:06 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/16/22 19:06 V18748TBL
0.006 J mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 05/16/22 19:06 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/16/22 19:06 V18748TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/16/22 19:06 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 40 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-1
89772 Matrix:
5/11/2022 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/16/22 19:06 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/16/22 19:06 V18748TBL
0.001 J mg/Kg - dry 0.0008 0.005Toluene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/16/22 19:06 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,1,2-Trichloroethane 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/16/22 19:06 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/16/22 19:06 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/16/22 19:06 V18748TBL
0.0008 J mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/16/22 19:06 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/16/22 19:06 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.011
Vinyl Chloride 1 05/16/22 19:06 V18748TBL
0.0009 J mg/Kg - dry 0.0006 0.005o-Xylene 1 05/16/22 19:06 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/16/22 19:06 V18748TBL
0.0009 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/16/22 19:06 V18748
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/16/22 19:061 TBL V18748
Surrogate: Dibromofluoromethane 106 Limits: 84-123%05/16/22 19:061 TBL V18748
Surrogate: Toluene-d8 87.6 Limits: 76-129%05/16/22 19:061 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 41 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-2
89773 Matrix:
5/11/2022 10:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.0 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 42 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-2
89773 Matrix:
5/11/2022 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
32.7 mg/Kg - dry 5.22 11.2Diesel Range Organics (C10-C28)1 05/20/22 00:35 V18982JLK
8015C DROSurrogate: OTP Surrogate 87.2 Limits: 31-123%05/20/22 00:351 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
2.46 J mg/Kg - dry 2.33 5.62Gasoline Range Organics (C6-C10)50 05/16/22 13:45 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 157 *Limits: 50-137%05/16/22 13:4550 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 43 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-3
89774 Matrix:
5/11/2022 10:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.3 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 44 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-3
89774 Matrix:
5/11/2022 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
<5.30 mg/Kg - dry 5.30 11.4Diesel Range Organics (C10-C28)1 05/20/22 01:39 V18982JLK
8015C DROSurrogate: OTP Surrogate 87.3 Limits: 31-123%05/20/22 01:391 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
<2.36 mg/Kg - dry 2.36 5.70Gasoline Range Organics (C6-C10)50 05/16/22 14:13 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 153 *Limits: 50-137%05/16/22 14:1350 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.011 J
mg/Kg - dry 0.002 0.022
Acetone 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/16/22 20:01 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/16/22 20:01 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 45 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-3
89774 Matrix:
5/11/2022 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/16/22 20:01 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/16/22 20:01 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/16/22 20:01 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/16/22 20:01 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/16/22 20:01 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/16/22 20:01 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 46 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-3
89774 Matrix:
5/11/2022 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.057Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 20:01 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/16/22 20:01 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/16/22 20:01 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/16/22 20:01 V18748TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/16/22 20:01 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 47 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-3
89774 Matrix:
5/11/2022 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/16/22 20:01 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/16/22 20:01 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/16/22 20:01 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005
1,1,2-Trichloroethane 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/16/22 20:01 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/16/22 20:01 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/16/22 20:01 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/16/22 20:01 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/16/22 20:01 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/16/22 20:01 V18748
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/16/22 20:011 TBL V18748
Surrogate: Dibromofluoromethane 104 Limits: 84-123%05/16/22 20:011 TBL V18748
Surrogate: Toluene-d8 87.7 Limits: 76-129%05/16/22 20:011 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 48 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-4
89775 Matrix:
5/11/2022 10:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.2 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 49 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-4
89775 Matrix:
5/11/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
<5.55 mg/Kg - dry 5.55 11.9Diesel Range Organics (C10-C28)1 05/20/22 02:00 V18982JLK
8015C DROSurrogate: OTP Surrogate 91.8 Limits: 31-123%05/20/22 02:001 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
3.84 J mg/Kg - dry 2.47 5.97Gasoline Range Organics (C6-C10)50 05/16/22 14:41 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 120 Limits: 50-137%05/16/22 14:4150 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.016 J
mg/Kg - dry 0.002 0.023
Acetone 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/16/22 20:28 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.005Bromochloromethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/16/22 20:28 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/16/22 20:28 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 50 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-4
89775 Matrix:
5/11/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.011Chloromethane 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005
Dibromomethane 1 05/16/22 20:28 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/16/22 20:28 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/16/22 20:28 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 51 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-4
89775 Matrix:
5/11/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/16/22 20:28 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.005
trans-1,3-Dichloropropene 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/16/22 20:28 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/16/22 20:28 V18748TBL
0.002 J mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 05/16/22 20:28 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/16/22 20:28 V18748TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/16/22 20:28 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 52 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-4
89775 Matrix:
5/11/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/16/22 20:28 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/16/22 20:28 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,1,2-Trichloroethane 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/16/22 20:28 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/16/22 20:28 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/16/22 20:28 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.011
Vinyl Chloride 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/16/22 20:28 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/16/22 20:28 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/16/22 20:28 V18748
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/16/22 20:281 TBL V18748
Surrogate: Dibromofluoromethane 108 Limits: 84-123%05/16/22 20:281 TBL V18748
Surrogate: Toluene-d8 88.1 Limits: 76-129%05/16/22 20:281 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 53 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-5
89776 Matrix:
5/11/2022 10:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.5 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 54 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-5
89776 Matrix:
5/11/2022 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
13.0 mg/Kg - dry 5.92 12.7Diesel Range Organics (C10-C28)1 05/20/22 02:21 V18982JLK
8015C DROSurrogate: OTP Surrogate 98.5 Limits: 31-123%05/20/22 02:211 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
<2.64 mg/Kg - dry 2.64 6.37Gasoline Range Organics (C6-C10)50 05/16/22 15:09 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 122 Limits: 50-137%05/16/22 15:0950 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.017 J
mg/Kg - dry 0.003 0.025
Acetone 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 05/16/22 20:56 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 05/16/22 20:56 V18748TBL
0.003 J mg/Kg - dry 0.0007 0.006Benzene 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromoform 1 05/16/22 20:56 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/16/22 20:56 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 55 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-5
89776 Matrix:
5/11/2022 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.0007 J mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 05/16/22 20:56 V18748TBL
0.008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 20:56 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 20:56 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Chloroform 1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/16/22 20:56 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 20:56 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 20:56 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 20:56 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 20:56 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 56 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-5
89776 Matrix:
5/11/2022 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 20:56 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,3-Dichloropropene 1 05/16/22 20:56 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 05/16/22 20:56 V18748TBL
0.011 J mg/Kg - dry 0.0008 0.012n-Hexane 1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 20:56 V18748TBL
0.006 J mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 20:56 V18748TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 20:56 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 57 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-5
89776 Matrix:
5/11/2022 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 20:56 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 20:56 V18748TBL
0.012 mg/Kg - dry 0.0008 0.006Toluene 1 05/16/22 20:56 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/16/22 20:56 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
1,1,2-Trichloroethane 1 05/16/22 20:56 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 20:56 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/16/22 20:56 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 20:56 V18748TBL
0.009 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 20:56 V18748TBL
0.005 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/16/22 20:56 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 05/16/22 20:56 V18748TBL
0.008 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/16/22 20:56 V18748TBL
0.018 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/16/22 20:56 V18748TBL
0.026 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/16/22 20:56 V18748
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/16/22 20:561 TBL V18748
Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/16/22 20:561 TBL V18748
Surrogate: Toluene-d8 87.6 Limits: 76-129%05/16/22 20:561 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 58 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-6
89777 Matrix:
5/11/2022 13:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.9 %Moisture 1 05/18/22 11:01 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 59 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-6
89777 Matrix:
5/11/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
9.06 J mg/Kg - dry 5.73 12.3Diesel Range Organics (C10-C28)1 05/20/22 02:42 V18982JLK
8015C DROSurrogate: OTP Surrogate 88.0 Limits: 31-123%05/20/22 02:421 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
10.3 mg/Kg - dry 2.55 6.17Gasoline Range Organics (C6-C10)50 05/16/22 16:05 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 136 Limits: 50-137%05/16/22 16:0550 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 60 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.6 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 61 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
23.2 mg/Kg - dry 6.09 13.1Diesel Range Organics (C10-C28)1 05/20/22 03:04 V18982JLK
8015C DROSurrogate: OTP Surrogate 91.0 Limits: 31-123%05/20/22 03:041 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
13.9 mg/Kg - dry 2.71 6.54Gasoline Range Organics (C6-C10)50 05/16/22 16:33 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 127 Limits: 50-137%05/16/22 16:3350 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00 V18870 05/17/22 08:00
0.035 mg/Kg - dry 0.003 0.026
Acetone 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/16/22 21:24 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/16/22 21:24 V18748TBL
0.003 J mg/Kg - dry 0.0008 0.006Benzene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromoform 1 05/16/22 21:24 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/16/22 21:24 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 62 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00 V18870 05/17/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 05/16/22 21:24 V18748TBL
0.004 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 21:24 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 21:24 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/16/22 21:24 V18748TBL
6.36 mg/Kg - dry 0.344 1.64
Chloroform 500 05/17/22 23:57 V18871TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/16/22 21:24 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 21:24 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 21:24 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 21:24 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 21:24 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 63 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00 V18870 05/17/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 21:24 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,3-Dichloropropene 1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/16/22 21:24 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 21:24 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 21:24 V18748TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/16/22 21:24 V18748TBL
0.023 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 21:24 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 64 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00 V18870 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 21:24 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 21:24 V18748TBL
0.002 J mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 21:24 V18748TBL
0.001 J mg/Kg - dry 0.0009 0.006Toluene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/16/22 21:24 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
1,1,2-Trichloroethane 1 05/16/22 21:24 V18748TBL
0.006 J mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 21:24 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/16/22 21:24 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 21:24 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/16/22 21:24 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 05/16/22 21:24 V18748TBL
0.0009 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/16/22 21:24 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/16/22 21:24 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 65 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-7
89778 Matrix:
5/11/2022 13:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00 V18870 05/17/22 08:00
0.0009 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/16/22 21:24 V18748
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/16/22 21:241 TBL V18748
Surrogate: Dibromofluoromethane 112 Limits: 84-123%05/16/22 21:241 TBL V18748
Surrogate: Toluene-d8 87.1 Limits: 76-129%05/16/22 21:241 TBL V18748
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/17/22 23:57500 TBL V18871
Surrogate: Dibromofluoromethane 102 Limits: 70-130%05/17/22 23:57500 TBL V18871
Surrogate: Toluene-d8 88.9 Limits: 76-129%05/17/22 23:57500 TBL V18871
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 66 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-8
89779 Matrix:
5/11/2022 14:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.1 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 67 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-8
89779 Matrix:
5/11/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
<5.23 mg/Kg - dry 5.23 11.2Diesel Range Organics (C10-C28)1 05/20/22 03:25 V18982JLK
8015C DROSurrogate: OTP Surrogate 95.5 Limits: 31-123%05/20/22 03:251 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
2.64 J mg/Kg - dry 2.33 5.62Gasoline Range Organics (C6-C10)50 05/16/22 17:00 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 126 Limits: 50-137%05/16/22 17:0050 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.044 mg/Kg - dry 0.002 0.022
Acetone 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/17/22 23:29 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 05/17/22 23:29 V18810TBL
0.002 J mg/Kg - dry 0.0007 0.005Benzene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/17/22 23:29 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/17/22 23:29 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 68 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-8
89779 Matrix:
5/11/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/17/22 23:29 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/17/22 23:29 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/17/22 23:29 V18810TBL
0.0008 J mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/17/22 23:29 V18810TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 05/17/22 23:29 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/17/22 23:29 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 69 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-8
89779 Matrix:
5/11/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 23:29 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/17/22 23:29 V18810TBL
0.002 J mg/Kg - dry 0.0007 0.011n-Hexane 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/17/22 23:29 V18810TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/17/22 23:29 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 70 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-8
89779 Matrix:
5/11/2022 14:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/17/22 23:29 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/17/22 23:29 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.005
1,1,2-Trichloroethane 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/17/22 23:29 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/17/22 23:29 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/17/22 23:29 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/17/22 23:29 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/17/22 23:29 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/17/22 23:29 V18810
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/17/22 23:291 TBL V18810
Surrogate: Dibromofluoromethane 102 Limits: 84-123%05/17/22 23:291 TBL V18810
Surrogate: Toluene-d8 87.2 Limits: 76-129%05/17/22 23:291 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 71 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-9
89780 Matrix:
5/11/2022 14:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.0 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 72 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-9
89780 Matrix:
5/11/2022 14:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
15.9 mg/Kg - dry 5.74 12.3Diesel Range Organics (C10-C28)1 05/20/22 03:46 V18982JLK
8015C DROSurrogate: OTP Surrogate 84.2 Limits: 31-123%05/20/22 03:461 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18713 05/16/22 08:00
4.68 J mg/Kg - dry 2.56 6.17Gasoline Range Organics (C6-C10)50 05/16/22 17:29 V18714TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 122 Limits: 50-137%05/16/22 17:2950 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 73 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-10
89781 Matrix:
5/11/2022 14:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.7 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 74 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-10
89781 Matrix:
5/11/2022 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
<6.09 mg/Kg - dry 6.09 13.1Diesel Range Organics (C10-C28)1 05/20/22 04:07 V18982JLK
8015C DROSurrogate: OTP Surrogate 89.5 Limits: 31-123%05/20/22 04:071 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
33.6 mg/Kg - dry 2.71 6.55Gasoline Range Organics (C6-C10)50 05/17/22 15:24 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 114 Limits: 50-137%05/17/22 15:2450 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.017 J
mg/Kg - dry 0.003 0.026
Acetone 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/16/22 22:19 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Bromoform 1 05/16/22 22:19 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/16/22 22:19 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 75 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-10
89781 Matrix:
5/11/2022 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 22:19 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 22:19 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Chloroform 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/16/22 22:19 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 22:19 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 22:19 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 22:19 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 22:19 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 76 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-10
89781 Matrix:
5/11/2022 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 22:19 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,3-Dichloropropene 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/16/22 22:19 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 22:19 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 22:19 V18748TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 22:19 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 77 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-10
89781 Matrix:
5/11/2022 14:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 22:19 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 22:19 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/16/22 22:19 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
1,1,2-Trichloroethane 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 22:19 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/16/22 22:19 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/16/22 22:19 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 05/16/22 22:19 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/16/22 22:19 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/16/22 22:19 V18748
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/16/22 22:191 TBL V18748
Surrogate: Dibromofluoromethane 102 Limits: 84-123%05/16/22 22:191 TBL V18748
Surrogate: Toluene-d8 85.3 Limits: 76-129%05/16/22 22:191 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 78 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-11
89782 Matrix:
5/11/2022 16:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.9 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 79 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-11
89782 Matrix:
5/11/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
37.4 mg/Kg - dry 5.88 12.6Diesel Range Organics (C10-C28)1 05/20/22 04:29 V18982JLK
8015C DROSurrogate: OTP Surrogate 84.3 Limits: 31-123%05/20/22 04:291 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
63.5 mg/Kg - dry 2.62 6.32Gasoline Range Organics (C6-C10)50 05/17/22 20:31 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 110 Limits: 50-137%05/17/22 20:3150 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 80 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-12
89783 Matrix:
5/11/2022 16:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.8 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 81 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-12
89783 Matrix:
5/11/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
53.2 mg/Kg - dry 5.80 12.5Diesel Range Organics (C10-C28)1 05/20/22 04:50 V18982JLK
8015C DROSurrogate: OTP Surrogate 94.0 Limits: 31-123%05/20/22 04:501 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
75.7 mg/Kg - dry 2.58 6.23Gasoline Range Organics (C6-C10)50 05/17/22 20:59 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 112 Limits: 50-137%05/17/22 20:5950 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V18988 05/20/22 08:00
<0.074 mg/Kg - dry 0.074 0.623
Acetone 50 05/20/22 13:21 V18989TBL
<0.037 mg/Kg - dry 0.037 0.623Acrolein 50 05/20/22 13:21 V18989TBL
<0.023 mg/Kg - dry 0.023 0.623Acrylonitrile 50 05/20/22 13:21 V18989TBL
0.304 mg/Kg - dry 0.018 0.155Benzene 50 05/20/22 13:21 V18989TBL
<0.015 mg/Kg - dry 0.015 0.155Bromobenzene 50 05/20/22 13:21 V18989TBL
<0.024 mg/Kg - dry 0.024 0.155Bromochloromethane 50 05/20/22 13:21 V18989TBL
<0.037 mg/Kg - dry 0.037 0.155Bromodichloromethane 50 05/20/22 13:21 V18989TBL
<0.031 mg/Kg - dry 0.031 0.155
Bromoform 50 05/20/22 13:21 V18989TBL
<0.056 mg/Kg - dry 0.056 0.311Bromomethane 50 05/20/22 13:21 V18989TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 82 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-12
89783 Matrix:
5/11/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V18988 05/20/22 08:00
0.491 mg/Kg - dry 0.015 0.155n-Butylbenzene 50 05/20/22 13:21 V18989TBL
0.163 mg/Kg - dry 0.017 0.155sec-Butyl benzene 50 05/20/22 13:21 V18989TBL
<0.015 mg/Kg - dry 0.015 0.155tert-Butyl benzene 50 05/20/22 13:21 V18989TBL
<0.019 mg/Kg - dry 0.019 0.155Carbon Disulfide 50 05/20/22 13:21 V18989TBL
<0.049 mg/Kg - dry 0.049 0.155Carbon Tetrachloride 50 05/20/22 13:21 V18989TBL
<0.020 mg/Kg - dry 0.020 0.155Chlorobenzene 50 05/20/22 13:21 V18989TBL
<0.027 mg/Kg - dry 0.027 0.155Chlorodibromomethane 50 05/20/22 13:21 V18989TBL
<0.027 mg/Kg - dry 0.027 0.311Chloroethane 50 05/20/22 13:21 V18989TBL
<0.032 mg/Kg - dry 0.032 0.155
Chloroform 50 05/20/22 13:21 V18989TBL
<0.019 mg/Kg - dry 0.019 0.311Chloromethane 50 05/20/22 13:21 V18989TBL
<0.015 mg/Kg - dry 0.015 0.1552-Chlorotoluene 50 05/20/22 13:21 V18989TBL
<0.012 mg/Kg - dry 0.012 0.1554-Chlorotoluene 50 05/20/22 13:21 V18989TBL
<0.022 mg/Kg - dry 0.022 0.155Di-Isopropyl Ether (DIPE)50 05/20/22 13:21 V18989TBL
<0.013 mg/Kg - dry 0.013 0.3111,2-Dibromo-3-Chloropropane 50 05/20/22 13:21 V18989TBL
<0.018 mg/Kg - dry 0.018 0.1551,2-Dibromoethane 50 05/20/22 13:21 V18989TBL
<0.030 mg/Kg - dry 0.030 0.155
Dibromomethane 50 05/20/22 13:21 V18989TBL
<0.009 mg/Kg - dry 0.009 0.1551,2-Dichlorobenzene 50 05/20/22 13:21 V18989TBL
<0.011 mg/Kg - dry 0.011 0.1551,3-Dichlorobenzene 50 05/20/22 13:21 V18989TBL
<0.018 mg/Kg - dry 0.018 0.1551,4-Dichlorobenzene 50 05/20/22 13:21 V18989TBL
<0.041 mg/Kg - dry 0.041 0.311Dichlorodifluoromethane 50 05/20/22 13:21 V18989TBL
<0.025 mg/Kg - dry 0.025 0.1551,1-Dichloroethane 50 05/20/22 13:21 V18989TBL
<0.043 mg/Kg - dry 0.043 0.1551,2-Dichloroethane 50 05/20/22 13:21 V18989TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 83 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-12
89783 Matrix:
5/11/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V18988 05/20/22 08:00
<0.022 mg/Kg - dry 0.022 0.1551,1-Dichloroethene 50 05/20/22 13:21 V18989TBL
<0.024 mg/Kg - dry 0.024 0.155cis-1,2-Dichloroethene 50 05/20/22 13:21 V18989TBL
<0.032 mg/Kg - dry 0.032 0.155trans-1,2-Dichloroethene 50 05/20/22 13:21 V18989TBL
<0.013 mg/Kg - dry 0.013 0.1551,2-Dichloropropane 50 05/20/22 13:21 V18989TBL
<0.017 mg/Kg - dry 0.017 0.1551,3-Dichloropropane 50 05/20/22 13:21 V18989TBL
<0.039 mg/Kg - dry 0.039 0.1552,2-Dichloropropane 50 05/20/22 13:21 V18989TBL
<0.023 mg/Kg - dry 0.023 0.1551,1-Dichloropropene 50 05/20/22 13:21 V18989TBL
<0.016 mg/Kg - dry 0.016 0.155cis-1,3-Dichloropropene 50 05/20/22 13:21 V18989TBL
<0.024 mg/Kg - dry 0.024 0.155
trans-1,3-Dichloropropene 50 05/20/22 13:21 V18989TBL
3.30 mg/Kg - dry 0.018 0.155Ethylbenzene 50 05/20/22 13:21 V18989TBL
<0.025 mg/Kg - dry 0.025 3.12Ethyl Tertiary Butyl Ether (ETBE)50 05/20/22 13:21 V18989TBL
<0.024 mg/Kg - dry 0.024 0.311Hexachlorobutadiene 50 05/20/22 13:21 V18989TBL
3.05 mg/Kg - dry 0.020 0.311n-Hexane 50 05/20/22 13:21 V18989TBL
<0.019 mg/Kg - dry 0.019 0.6232-Hexanone 50 05/20/22 13:21 V18989TBL
0.339 mg/Kg - dry 0.014 0.155Isopropylbenzene 50 05/20/22 13:21 V18989TBL
0.067 J
mg/Kg - dry 0.040 0.155
4-Isopropyl toluene 50 05/20/22 13:21 V18989TBL
<0.020 mg/Kg - dry 0.020 0.623Methyl Ethyl Ketone (MEK)50 05/20/22 13:21 V18989TBL
<0.019 mg/Kg - dry 0.019 0.155Methyl tert-butyl ether (MTBE)50 05/20/22 13:21 V18989TBL
<0.467 mg/Kg - dry 0.467 0.6234-Methyl-2-Pentanone 50 05/20/22 13:21 V18989TBL
<0.045 mg/Kg - dry 0.045 0.155Methylene Chloride 50 05/20/22 13:21 V18989TBL
1.13 mg/Kg - dry 0.030 0.311Naphthalene 50 05/20/22 13:21 V18989TBL
1.37 mg/Kg - dry 0.016 0.155n-Propylbenzene 50 05/20/22 13:21 V18989TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 84 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-12
89783 Matrix:
5/11/2022 16:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V18988 05/20/22 08:00
<0.044 mg/Kg - dry 0.044 0.155Styrene 50 05/20/22 13:21 V18989TBL
<0.032 mg/Kg - dry 0.032 0.1551,1,1,2-Tetrachloroethane 50 05/20/22 13:21 V18989TBL
<0.009 mg/Kg - dry 0.009 0.1551,1,2,2-Tetrachloroethane 50 05/20/22 13:21 V18989TBL
<0.028 mg/Kg - dry 0.028 0.155Tetrachloroethene 50 05/20/22 13:21 V18989TBL
2.56 mg/Kg - dry 0.020 0.155Toluene 50 05/20/22 13:21 V18989TBL
<0.016 mg/Kg - dry 0.016 0.3111,2,3-Trichlorobenzene 50 05/20/22 13:21 V18989TBL
<0.019 mg/Kg - dry 0.019 0.3111,2,4-Trichlorobenzene 50 05/20/22 13:21 V18989TBL
<0.044 mg/Kg - dry 0.044 0.1551,1,1-Trichloroethane 50 05/20/22 13:21 V18989TBL
<0.014 mg/Kg - dry 0.014 0.155
1,1,2-Trichloroethane 50 05/20/22 13:21 V18989TBL
<0.028 mg/Kg - dry 0.028 0.155Trichloroethene 50 05/20/22 13:21 V18989TBL
<0.065 mg/Kg - dry 0.065 0.311Trichlorofluoromethane 50 05/20/22 13:21 V18989TBL
<0.022 mg/Kg - dry 0.022 0.1551,2,3-Trichloropropane 50 05/20/22 13:21 V18989TBL
7.11 mg/Kg - dry 0.015 0.1551,2,4-Trimethylbenzene 50 05/20/22 13:21 V18989TBL
1.95 mg/Kg - dry 0.016 0.1551,3,5-Trimethylbenzene 50 05/20/22 13:21 V18989TBL
<0.014 mg/Kg - dry 0.014 0.311Vinyl Acetate 50 05/20/22 13:21 V18989TBL
<0.014 mg/Kg - dry 0.014 0.311
Vinyl Chloride 50 05/20/22 13:21 V18989TBL
3.39 mg/Kg - dry 0.015 0.155o-Xylene 50 05/20/22 13:21 V18989TBL
11.1 mg/Kg - dry 0.039 0.311m,p-Xylene 50 05/20/22 13:21 V18989TBL
14.5 mg/Kg - dry 0.015 0.155Xylene (Total)50 05/20/22 13:21 V18989
Surrogate: 4-Bromofluorobenzene 97.2 Limits: 70-130%05/20/22 13:2150 TBL V18989
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%05/20/22 13:2150 TBL V18989
Surrogate: Toluene-d8 86.6 Limits: 76-129%05/20/22 13:2150 TBL V18989
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 85 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-13
89784 Matrix:
5/11/2022 16:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
10.8 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 86 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-13
89784 Matrix:
5/11/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
5.87 J mg/Kg - dry 5.21 11.2Diesel Range Organics (C10-C28)1 05/20/22 05:54 V18982JLK
8015C DROSurrogate: OTP Surrogate 102 Limits: 31-123%05/20/22 05:541 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
7.63 mg/Kg - dry 2.41 5.83Gasoline Range Organics (C6-C10)50 05/17/22 15:52 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 131 Limits: 50-137%05/17/22 15:5250 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.022 J
mg/Kg - dry 0.002 0.022
Acetone 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/17/22 21:38 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/17/22 21:38 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/17/22 21:38 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 87 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-13
89784 Matrix:
5/11/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/17/22 21:38 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/17/22 21:38 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 05/17/22 21:38 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/17/22 21:38 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/17/22 21:38 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/17/22 21:38 V18810TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 05/17/22 21:38 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/17/22 21:38 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 88 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-13
89784 Matrix:
5/11/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 21:38 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/17/22 21:38 V18810TBL
0.005 J mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/17/22 21:38 V18810TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/17/22 21:38 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 89 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-13
89784 Matrix:
5/11/2022 16:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/17/22 21:38 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/17/22 21:38 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.005
1,1,2-Trichloroethane 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/17/22 21:38 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/17/22 21:38 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/17/22 21:38 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/17/22 21:38 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/17/22 21:38 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/17/22 21:38 V18810
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/17/22 21:381 TBL V18810
Surrogate: Dibromofluoromethane 103 Limits: 84-123%05/17/22 21:381 TBL V18810
Surrogate: Toluene-d8 86.7 Limits: 76-129%05/17/22 21:381 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 90 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-14
89785 Matrix:
5/11/2022 16:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
8.78 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 91 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-14
89785 Matrix:
5/11/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
115 mg/Kg - dry 5.10 11.0Diesel Range Organics (C10-C28)1 05/20/22 06:15 V18982JLK
8015C DROSurrogate: OTP Surrogate 106 Limits: 31-123%05/20/22 06:151 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
5.10 J mg/Kg - dry 2.27 5.48Gasoline Range Organics (C6-C10)50 05/17/22 16:20 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 131 Limits: 50-137%05/17/22 16:2050 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18986 05/20/22 08:00
0.008 J
mg/Kg - dry 0.002 0.021
Acetone 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 05/20/22 12:26 V18987TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005
Bromoform 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.010Bromomethane 1 05/20/22 12:26 V18987TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 92 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-14
89785 Matrix:
5/11/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18986 05/20/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 05/20/22 12:26 V18987TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 05/20/22 12:26 V18987TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005
Chloroform 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/20/22 12:26 V18987TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/20/22 12:26 V18987TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/20/22 12:26 V18987TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 05/20/22 12:26 V18987TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/20/22 12:26 V18987TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 93 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-14
89785 Matrix:
5/11/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18986 05/20/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/20/22 12:26 V18987TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.005
trans-1,3-Dichloropropene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.054Ethyl Tertiary Butyl Ether (ETBE)1 05/20/22 12:26 V18987TBL
<0.0009 mg/Kg - dry 0.0009 0.010Hexachlorobutadiene 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/20/22 12:26 V18987TBL
0.001 J mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/20/22 12:26 V18987TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/20/22 12:26 V18987TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 94 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:W-14
89785 Matrix:
5/11/2022 16:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18986 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/20/22 12:26 V18987TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/20/22 12:26 V18987TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 05/20/22 12:26 V18987TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005
1,1,2-Trichloroethane 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/20/22 12:26 V18987TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 05/20/22 12:26 V18987TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 05/20/22 12:26 V18987TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.010
Vinyl Chloride 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 05/20/22 12:26 V18987TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 05/20/22 12:26 V18987TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 05/20/22 12:26 V18987
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%05/20/22 12:261 TBL V18987
Surrogate: Dibromofluoromethane 104 Limits: 84-123%05/20/22 12:261 TBL V18987
Surrogate: Toluene-d8 85.0 Limits: 76-129%05/20/22 12:261 TBL V18987
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 95 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-4
89786 Matrix:
5/12/2022 8:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
26.3 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 96 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-4
89786 Matrix:
5/12/2022 8:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
2.99 J mg/Kg - dry 2.81 6.78Gasoline Range Organics (C6-C10)50 05/17/22 16:48 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 116 Limits: 50-137%05/17/22 16:4850 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.017 J mg/Kg - dry 0.003 0.027Acetone 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 05/16/22 22:47 V18748TBL
0.002 J mg/Kg - dry 0.0008 0.006Benzene 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Bromobenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/16/22 22:47 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 05/16/22 22:47 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
tert-Butyl benzene 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 05/16/22 22:47 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 22:47 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 97 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-4
89786 Matrix:
5/12/2022 8:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/16/22 22:47 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 22:47 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 22:47 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/16/22 22:47 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 22:47 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 05/16/22 22:47 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 22:47 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 22:47 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 22:47 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloroethene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 22:47 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 05/16/22 22:47 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 98 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-4
89786 Matrix:
5/12/2022 8:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/16/22 22:47 V18748TBL
0.001 J mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/16/22 22:47 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0272-Hexanone 1 05/16/22 22:47 V18748TBL
0.001 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 05/16/22 22:47 V18748TBL
0.012 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 22:47 V18748TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/16/22 22:47 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 22:47 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/16/22 22:47 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 05/16/22 22:47 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 99 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:D-4
89786 Matrix:
5/12/2022 8:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 22:47 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/16/22 22:47 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 22:47 V18748TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/16/22 22:47 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 05/16/22 22:47 V18748TBL
0.008 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 05/16/22 22:47 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 22:47 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/16/22 22:47 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.013
Vinyl Chloride 1 05/16/22 22:47 V18748TBL
0.001 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/16/22 22:47 V18748TBL
0.013 mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/16/22 22:47 V18748TBL
0.015 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/16/22 22:47 V18748
Surrogate: 4-Bromofluorobenzene 91.2 Limits: 70-130%05/16/22 22:471 TBL V18748
Surrogate: Dibromofluoromethane 105 Limits: 84-123%05/16/22 22:471 TBL V18748
Surrogate: Toluene-d8 87.6 Limits: 76-129%05/16/22 22:471 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 100 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-1
89787 Matrix:
5/12/2022 8:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.8 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 101 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-1
89787 Matrix:
5/12/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
2.51 J mg/Kg - dry 2.40 5.80Gasoline Range Organics (C6-C10)50 05/17/22 17:16 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 128 Limits: 50-137%05/17/22 17:1650 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.037 mg/Kg - dry 0.002 0.023Acetone 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Bromobenzene 1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/16/22 23:15 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
tert-Butyl benzene 1 05/16/22 23:15 V18748TBL
0.002 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/16/22 23:15 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/16/22 23:15 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 102 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-1
89787 Matrix:
5/12/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 05/16/22 23:15 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/16/22 23:15 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/16/22 23:15 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/16/22 23:15 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/16/22 23:15 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloroethene 1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/16/22 23:15 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 103 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-1
89787 Matrix:
5/12/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/16/22 23:15 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 23:15 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/16/22 23:15 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/16/22 23:15 V18748TBL
0.007 J mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/16/22 23:15 V18748TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005
Styrene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/16/22 23:15 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/16/22 23:15 V18748TBL
0.001 J mg/Kg - dry 0.0008 0.005Toluene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/16/22 23:15 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/16/22 23:15 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 104 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-1
89787 Matrix:
5/12/2022 8:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/16/22 23:15 V18748TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/16/22 23:15 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/16/22 23:15 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.011
Vinyl Chloride 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/16/22 23:15 V18748TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/16/22 23:15 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/16/22 23:15 V18748
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/16/22 23:151 TBL V18748
Surrogate: Dibromofluoromethane 99.8 Limits: 84-123%05/16/22 23:151 TBL V18748
Surrogate: Toluene-d8 85.9 Limits: 76-129%05/16/22 23:151 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 105 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-2
89788 Matrix:
5/12/2022 8:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.4 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 106 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-2
89788 Matrix:
5/12/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
<2.67 mg/Kg - dry 2.67 6.44Gasoline Range Organics (C6-C10)50 05/17/22 17:44 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 115 Limits: 50-137%05/17/22 17:4450 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
0.019 J mg/Kg - dry 0.003 0.025Acetone 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 05/16/22 23:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Bromobenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/16/22 23:42 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006
tert-Butyl benzene 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/16/22 23:42 V18748TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/16/22 23:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 107 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-2
89788 Matrix:
5/12/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/16/22 23:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/16/22 23:42 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/16/22 23:42 V18748TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloroethene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/16/22 23:42 V18748TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/16/22 23:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 108 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-2
89788 Matrix:
5/12/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/16/22 23:42 V18748TBL
0.005 J mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 05/16/22 23:42 V18748TBL
0.002 J mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/16/22 23:42 V18748TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/16/22 23:42 V18748TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/16/22 23:42 V18748TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/16/22 23:42 V18748TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 109 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-2
89788 Matrix:
5/12/2022 8:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18747 05/16/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/16/22 23:42 V18748TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/16/22 23:42 V18748TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/16/22 23:42 V18748TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/16/22 23:42 V18748TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/16/22 23:42 V18748TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/16/22 23:42 V18748
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/16/22 23:421 TBL V18748
Surrogate: Dibromofluoromethane 100 Limits: 84-123%05/16/22 23:421 TBL V18748
Surrogate: Toluene-d8 91.1 Limits: 76-129%05/16/22 23:421 TBL V18748
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 110 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-3
89789 Matrix:
5/12/2022 11:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.7 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 111 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-3
89789 Matrix:
5/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
25.9 mg/Kg - dry 2.34 5.66Gasoline Range Organics (C6-C10)50 05/17/22 18:12 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 133 Limits: 50-137%05/17/22 18:1250 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.025 mg/Kg - dry 0.002 0.022Acetone 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/17/22 13:47 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 05/17/22 13:47 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.005Benzene 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Bromobenzene 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/17/22 13:47 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005
tert-Butyl benzene 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/17/22 13:47 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/17/22 13:47 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 112 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-3
89789 Matrix:
5/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/17/22 13:47 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/17/22 13:47 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/17/22 13:47 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/17/22 13:47 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/17/22 13:47 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloroethene 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/17/22 13:47 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 113 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-3
89789 Matrix:
5/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/17/22 13:47 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 13:47 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/17/22 13:47 V18810TBL
0.004 J mg/Kg - dry 0.0007 0.011n-Hexane 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/17/22 13:47 V18810TBL
0.004 J mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/17/22 13:47 V18810TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/17/22 13:47 V18810TBL
0.0006 J mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005
Styrene 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/17/22 13:47 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/17/22 13:47 V18810TBL
0.006 mg/Kg - dry 0.0007 0.005Toluene 1 05/17/22 13:47 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/17/22 13:47 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/17/22 13:47 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 114 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-3
89789 Matrix:
5/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/17/22 13:47 V18810TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/17/22 13:47 V18810TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/17/22 13:47 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/17/22 13:47 V18810TBL
0.002 J mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/17/22 13:47 V18810TBL
0.001 J mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/17/22 13:47 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/17/22 13:47 V18810TBL
0.002 J mg/Kg - dry 0.0006 0.005o-Xylene 1 05/17/22 13:47 V18810TBL
0.005 J mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/17/22 13:47 V18810TBL
0.007 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/17/22 13:47 V18810
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/17/22 13:471 TBL V18810
Surrogate: Dibromofluoromethane 106 Limits: 84-123%05/17/22 13:471 TBL V18810
Surrogate: Toluene-d8 89.0 Limits: 76-129%05/17/22 13:471 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 115 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-4
89790 Matrix:
5/12/2022 11:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.6 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 116 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-4
89790 Matrix:
5/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
2.78 J mg/Kg - dry 2.78 6.72Gasoline Range Organics (C6-C10)50 05/17/22 18:40 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 113 Limits: 50-137%05/17/22 18:4050 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.012 J mg/Kg - dry 0.003 0.026Acetone 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 05/17/22 14:15 V18810TBL
0.003 J mg/Kg - dry 0.0008 0.006Benzene 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Bromobenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/17/22 14:15 V18810TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
tert-Butyl benzene 1 05/17/22 14:15 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 05/17/22 14:15 V18810TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/17/22 14:15 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/17/22 14:15 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 117 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-4
89790 Matrix:
5/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/17/22 14:15 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/17/22 14:15 V18810TBL
0.003 J mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006
Dibromomethane 1 05/17/22 14:15 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/17/22 14:15 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/17/22 14:15 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloroethene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 05/17/22 14:15 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 118 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-4
89790 Matrix:
5/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/17/22 14:15 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 05/17/22 14:15 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/17/22 14:15 V18810TBL
0.001 J mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/17/22 14:15 V18810TBL
0.023 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/17/22 14:15 V18810TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/17/22 14:15 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/17/22 14:15 V18810TBL
0.001 J mg/Kg - dry 0.0009 0.006Toluene 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/17/22 14:15 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 05/17/22 14:15 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 119 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-4
89790 Matrix:
5/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/17/22 14:15 V18810TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/17/22 14:15 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 05/17/22 14:15 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 05/17/22 14:15 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/17/22 14:15 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 05/17/22 14:15 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/17/22 14:15 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/17/22 14:15 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/17/22 14:15 V18810
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/17/22 14:151 TBL V18810
Surrogate: Dibromofluoromethane 103 Limits: 84-123%05/17/22 14:151 TBL V18810
Surrogate: Toluene-d8 87.8 Limits: 76-129%05/17/22 14:151 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 120 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-5
89791 Matrix:
5/12/2022 11:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.0 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 121 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-5
89791 Matrix:
5/12/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
<2.59 mg/Kg - dry 2.59 6.25Gasoline Range Organics (C6-C10)50 05/17/22 19:08 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 113 Limits: 50-137%05/17/22 19:0850 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.005 J mg/Kg - dry 0.003 0.025Acetone 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 05/17/22 14:43 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 05/17/22 14:43 V18810TBL
0.002 J mg/Kg - dry 0.0007 0.006Benzene 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Bromobenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/17/22 14:43 V18810TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006
tert-Butyl benzene 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/17/22 14:43 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 122 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-5
89791 Matrix:
5/12/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/17/22 14:43 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/17/22 14:43 V18810TBL
0.001 J mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/17/22 14:43 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/17/22 14:43 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/17/22 14:43 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloroethene 1 05/17/22 14:43 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/17/22 14:43 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/17/22 14:43 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 123 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-5
89791 Matrix:
5/12/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/17/22 14:43 V18810TBL
0.0009 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 14:43 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 05/17/22 14:43 V18810TBL
0.002 J mg/Kg - dry 0.0008 0.012n-Hexane 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 05/17/22 14:43 V18810TBL
0.034 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/17/22 14:43 V18810TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/17/22 14:43 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/17/22 14:43 V18810TBL
0.008 mg/Kg - dry 0.0008 0.006Toluene 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/17/22 14:43 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/17/22 14:43 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 124 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-5
89791 Matrix:
5/12/2022 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/17/22 14:43 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/17/22 14:43 V18810TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/17/22 14:43 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/17/22 14:43 V18810TBL
0.0010 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/17/22 14:43 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/17/22 14:43 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 05/17/22 14:43 V18810TBL
0.001 J mg/Kg - dry 0.0006 0.006o-Xylene 1 05/17/22 14:43 V18810TBL
0.002 J mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/17/22 14:43 V18810TBL
0.004 J mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/17/22 14:43 V18810
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%05/17/22 14:431 TBL V18810
Surrogate: Dibromofluoromethane 104 Limits: 84-123%05/17/22 14:431 TBL V18810
Surrogate: Toluene-d8 87.9 Limits: 76-129%05/17/22 14:431 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 125 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-6
89792 Matrix:
5/12/2022 13:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.4 %Moisture 1 05/19/22 10:40 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 126 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-6
89792 Matrix:
5/12/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18784 05/17/22 08:00
<2.74 mg/Kg - dry 2.74 6.61Gasoline Range Organics (C6-C10)50 05/17/22 19:36 V18785TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 104 Limits: 50-137%05/17/22 19:3650 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
0.030 mg/Kg - dry 0.003 0.026Acetone 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 05/17/22 15:10 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 05/17/22 15:10 V18810TBL
0.021 mg/Kg - dry 0.0008 0.006Benzene 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Bromobenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/17/22 15:10 V18810TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
tert-Butyl benzene 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/17/22 15:10 V18810TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 05/17/22 15:10 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/17/22 15:10 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 127 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-6
89792 Matrix:
5/12/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 05/17/22 15:10 V18810TBL
0.001 J mg/Kg - dry 0.001 0.006Chloroform 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 05/17/22 15:10 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/17/22 15:10 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/17/22 15:10 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/17/22 15:10 V18810TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/17/22 15:10 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloroethene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 05/17/22 15:10 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 128 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-6
89792 Matrix:
5/12/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.066Ethyl Tertiary Butyl Ether (ETBE)1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 05/17/22 15:10 V18810TBL
0.002 J mg/Kg - dry 0.0009 0.013n-Hexane 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/17/22 15:10 V18810TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/17/22 15:10 V18810TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/17/22 15:10 V18810TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/17/22 15:10 V18810TBL
0.010 mg/Kg - dry 0.0009 0.006Toluene 1 05/17/22 15:10 V18810TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 05/17/22 15:10 V18810TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 05/17/22 15:10 V18810TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 129 of 166
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-133-0023
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/13/2022
Circle K 2720104
Report Date : 05/23/2022
Sample ID :
Lab No :
Sampled:L-6
89792 Matrix:
5/12/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18807 05/17/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/17/22 15:10 V18810TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/17/22 15:10 V18810TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 05/17/22 15:10 V18810TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 05/17/22 15:10 V18810TBL
0.0008 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/17/22 15:10 V18810TBL
0.0009 J mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 05/17/22 15:10 V18810TBL
<0.0006 mg/Kg - dry 0.0006 0.013
Vinyl Chloride 1 05/17/22 15:10 V18810TBL
0.001 J mg/Kg - dry 0.0007 0.006o-Xylene 1 05/17/22 15:10 V18810TBL
0.003 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 05/17/22 15:10 V18810TBL
0.004 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 05/17/22 15:10 V18810
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%05/17/22 15:101 TBL V18810
Surrogate: Dibromofluoromethane 104 Limits: 84-123%05/17/22 15:101 TBL V18810
Surrogate: Toluene-d8 89.7 Limits: 76-129%05/17/22 15:101 TBL V18810
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 130 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V18982QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18830
Associated Lab Samples: 89765, 89766, 89767, 89768, 89772, 89773, 89774, 89775, 89776, 89777, 89778, 89779, 89780, 89781, 89782,
89783, 89784, 89785
LRB-V18830 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/19/22 21:2410.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
05/19/22 21:24OTP Surrogate (S)96.2 31-123
LCS-V18830Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10469.566.7mg/KgDiesel Range Organics (C10-C28)46-126
84.9OTP Surrogate (S)31-123
V 89767-MS-V18830 V 89767-MSD-V18830Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
291 -140*28266.666.6386mg/KgDiesel Range Organics (C10-C28)-140*50-117 3.1 24
70.9OTP Surrogate (S)67.3 31-123
Page 1 of 31* QC Fail Date:05/23/2022 04:56 PM
Page 131 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V18714QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18713
Associated Lab Samples: 89765, 89766, 89767, 89768, 89769, 89770, 89771, 89772, 89773, 89774, 89775, 89776, 89777, 89778, 89779,
89780
LRB-V18713 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/16/22 10:305.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
05/16/22 10:30a,a,a-Trifluorotoluene (S)105 50-137
LCS-V18713Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.249.150.0mg/KgGasoline Range Organics (C6-C10)41-138
119a,a,a-Trifluorotoluene (S)50-137
V 89612-MS-V18713 V 89612-MSD-V18713Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
59.2 11855.550.050.02.60mg/KgGasoline Range Organics (C6-C10)111 41-138 6.4 34
126a,a,a-Trifluorotoluene (S)121 50-137
Page 2 of 31Date:05/23/2022 04:56 PM
Page 132 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V18785QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18784
Associated Lab Samples: 89781, 89782, 89783, 89784, 89785, 89786, 89787, 89788, 89789, 89790, 89791, 89792
LRB-V18784 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/17/22 14:565.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
05/17/22 14:56a,a,a-Trifluorotoluene (S)126 50-137
LCS-V18784Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10853.950.0mg/KgGasoline Range Organics (C6-C10)41-138
121a,a,a-Trifluorotoluene (S)50-137
V 89781-MS-V18784 V 89781-MSD-V18784Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
55.2 59.254.950.050.025.6mg/KgGasoline Range Organics (C6-C10)58.6 41-138 0.5 34
135a,a,a-Trifluorotoluene (S)135 50-137
Page 3 of 31Date:05/23/2022 04:56 PM
Page 133 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
Associated Lab Samples: 89769, 89770, 89771, 89772, 89774, 89775, 89776, 89778, 89781, 89786, 89787, 89788
LRB-V18747 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/16/22 12:100.0200.002<0.002mg/KgAcetone
05/16/22 12:100.0200.001<0.001mg/KgAcrolein
05/16/22 12:100.0200.0008<0.0008mg/KgAcrylonitrile
05/16/22 12:100.0050.0006<0.0006mg/KgBenzene
05/16/22 12:100.0050.0005<0.0005mg/KgBromobenzene
05/16/22 12:100.0050.0008<0.0008mg/KgBromochloromethane
05/16/22 12:100.0050.001<0.001mg/KgBromodichloromethane
05/16/22 12:100.0050.001<0.001mg/KgBromoform
05/16/22 12:100.0100.001<0.001mg/KgBromomethane
05/16/22 12:100.0050.0005<0.0005mg/Kgn-Butylbenzene
05/16/22 12:100.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/16/22 12:100.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/16/22 12:100.0050.0006<0.0006mg/KgCarbon Disulfide
05/16/22 12:100.0050.001<0.001mg/KgCarbon Tetrachloride
05/16/22 12:100.0050.0007<0.0007mg/KgChlorobenzene
05/16/22 12:100.0050.0009<0.0009mg/KgChlorodibromomethane
05/16/22 12:100.0100.0009<0.0009mg/KgChloroethane
05/16/22 12:100.0050.001<0.001mg/KgChloroform
05/16/22 12:100.0100.0006<0.0006mg/KgChloromethane
05/16/22 12:100.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/16/22 12:100.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/16/22 12:100.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/16/22 12:100.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/16/22 12:100.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/16/22 12:100.0050.0006<0.0006mg/KgDibromomethane
05/16/22 12:100.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/16/22 12:100.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 31Date:05/23/2022 04:56 PM
Page 134 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
Associated Lab Samples: 89769, 89770, 89771, 89772, 89774, 89775, 89776, 89778, 89781, 89786, 89787, 89788
LRB-V18747 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/16/22 12:100.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/16/22 12:100.0100.001<0.001mg/KgDichlorodifluoromethane
05/16/22 12:100.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/16/22 12:100.0050.001<0.001mg/Kg1,2-Dichloroethane
05/16/22 12:100.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/16/22 12:100.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/16/22 12:100.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/16/22 12:100.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/16/22 12:100.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/16/22 12:100.0050.001<0.001mg/Kg2,2-Dichloropropane
05/16/22 12:100.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/16/22 12:100.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/16/22 12:100.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/16/22 12:100.0050.0006<0.0006mg/KgEthylbenzene
05/16/22 12:100.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/16/22 12:100.0100.0008<0.0008mg/KgHexachlorobutadiene
05/16/22 12:100.0100.0007<0.0007mg/Kgn-Hexane
05/16/22 12:100.0200.0006<0.0006mg/Kg2-Hexanone
05/16/22 12:100.0050.0005<0.0005mg/KgIsopropylbenzene
05/16/22 12:100.0050.001<0.001mg/Kg4-Isopropyl toluene
05/16/22 12:100.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/16/22 12:100.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/16/22 12:100.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/16/22 12:100.0100.001<0.001mg/KgMethylene Chloride
05/16/22 12:100.0100.0010<0.0010mg/KgNaphthalene
05/16/22 12:100.0050.0005<0.0005mg/Kgn-Propylbenzene
05/16/22 12:100.0050.001<0.001mg/KgStyrene
Page 5 of 31Date:05/23/2022 04:56 PM
Page 135 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
Associated Lab Samples: 89769, 89770, 89771, 89772, 89774, 89775, 89776, 89778, 89781, 89786, 89787, 89788
LRB-V18747 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/16/22 12:100.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/16/22 12:100.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/16/22 12:100.0050.0009<0.0009mg/KgTetrachloroethene
05/16/22 12:100.0050.0007<0.0007mg/KgToluene
05/16/22 12:100.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/16/22 12:100.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/16/22 12:100.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/16/22 12:100.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/16/22 12:100.0050.0009<0.0009mg/KgTrichloroethene
05/16/22 12:100.0100.002<0.002mg/KgTrichlorofluoromethane
05/16/22 12:100.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/16/22 12:100.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/16/22 12:100.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/16/22 12:100.0100.0005<0.0005mg/KgVinyl Acetate
05/16/22 12:100.0100.0005<0.0005mg/KgVinyl Chloride
05/16/22 12:100.0050.0005<0.0005mg/Kgo-Xylene
05/16/22 12:100.0100.001<0.001mg/Kgm,p-Xylene
05/16/22 12:104-Bromofluorobenzene (S)101 70-130
05/16/22 12:10Dibromofluoromethane (S)101 84-123
05/16/22 12:10Toluene-d8 (S)89.0 76-129
LCS-V18747 LCSD-V18747Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.112 1121080.1080.100mg/KgAcetone 29-198 3.6 20
0.093 93.592.30.0920.100mg/KgAcrolein 70-130 1.2 20
Page 6 of 31Date:05/23/2022 04:56 PM
Page 136 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
LCS-V18747 LCSD-V18747Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.110 1101090.1090.100mg/KgAcrylonitrile 65-134 0.9 20
0.051 1041060.0530.050mg/KgBenzene 74-127 2.2 20
0.043 86.285.80.0420.050mg/KgBromobenzene 73-125 0.4 20
0.057 1151160.0570.050mg/KgBromochloromethane 72-134 0.5 20
0.055 1111100.0550.050mg/KgBromodichloromethane 75-122 0.7 20
0.048 97.897.80.0480.050mg/KgBromoform 66-135 0.0 20
0.042 85.286.80.0430.050mg/KgBromomethane 20-180 1.8 20
0.043 86.490.40.0450.050mg/Kgn-Butylbenzene 65-135 4.5 20
0.041 82.686.00.0430.050mg/Kgsec-Butyl benzene 66-131 4.0 20
0.041 83.086.20.0430.050mg/Kgtert-Butyl benzene 67-132 3.7 20
0.048 97.21050.0520.050mg/KgCarbon Disulfide 61-129 7.5 20
0.048 96.61020.0510.050mg/KgCarbon Tetrachloride 64-143 5.4 20
0.046 93.495.60.0470.050mg/KgChlorobenzene 74-118 2.3 20
0.048 96.696.20.0480.050mg/KgChlorodibromomethane 73-122 0.4 20
0.056 1141080.0530.050mg/KgChloroethane 33-149 5.2 20
0.052 1051080.0540.050mg/KgChloroform 73-127 3.0 20
0.043 86.285.20.0420.050mg/KgChloromethane 45-143 1.1 20
0.042 85.686.00.0430.050mg/Kg2-Chlorotoluene 67-124 0.4 20
0.042 85.086.20.0430.050mg/Kg4-Chlorotoluene 71-126 1.4 20
0.052 1061070.0530.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.3 20
0.049 98.492.80.0460.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 5.8 20
0.048 96.898.20.0490.050mg/Kg1,2-Dibromoethane 70-132 1.4 20
0.056 1121110.0550.050mg/KgDibromomethane 74-133 1.4 20
0.044 89.087.20.0430.050mg/Kg1,2-Dichlorobenzene 72-123 2.0 20
0.044 88.288.20.0440.050mg/Kg1,3-Dichlorobenzene 71-120 0.0 20
0.044 88.487.60.0430.050mg/Kg1,4-Dichlorobenzene 71-123 0.9 20
Page 7 of 31Date:05/23/2022 04:56 PM
Page 137 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
LCS-V18747 LCSD-V18747Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.038 76.685.00.0420.050mg/KgDichlorodifluoromethane 26-146 10.3 20
0.051 1021050.0520.050mg/Kg1,1-Dichloroethane 74-127 3.0 20
0.053 1081070.0530.050mg/Kg1,2-Dichloroethane 68-128 0.3 20
0.046 92.81010.0500.050mg/Kg1,1-Dichloroethene 67-149 8.6 20
0.051 1031030.0510.050mg/Kgcis-1,2-Dichloroethene 76-134 0.7 20
0.049 98.81040.0520.050mg/Kgtrans-1,2-Dichloroethene 73-132 5.3 20
0.053 1071060.0530.050mg/Kg1,2-Dichloropropane 73-130 0.5 20
0.048 96.095.20.0470.050mg/Kg1,3-Dichloropropane 75-124 0.8 20
0.050 1021090.0540.050mg/Kg2,2-Dichloropropane 50-142 6.4 20
0.048 96.41040.0510.050mg/Kg1,1-Dichloropropene 71-130 7.3 20
0.055 1111100.0550.050mg/Kgcis-1,3-Dichloropropene 71-125 0.5 20
0.056 1121120.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.7 20
0.044 88.694.00.0470.050mg/KgEthylbenzene 74-128 5.9 20
0.117 1171160.1160.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.8 20
0.043 86.689.40.0440.050mg/KgHexachlorobutadiene 64-125 3.1 20
0.048 97.01070.0530.050mg/Kgn-Hexane 70-130 9.8 20
0.044 88.290.60.0450.050mg/Kg2-Hexanone 61-157 2.6 20
0.041 83.486.60.0430.050mg/KgIsopropylbenzene 68-126 3.7 20
0.042 84.887.00.0430.050mg/Kg4-Isopropyl toluene 68-129 2.5 20
0.044 88.289.00.0440.050mg/KgMethyl Ethyl Ketone (MEK)63-149 0.9 20
0.054 1091090.0540.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.0 20
0.054 1081080.0540.050mg/Kg4-Methyl-2-Pentanone 57-162 0.1 20
0.049 99.61010.0500.050mg/KgMethylene Chloride 74-129 1.7 20
0.053 1071070.0530.050mg/KgNaphthalene 57-157 0.3 20
0.042 84.687.60.0430.050mg/Kgn-Propylbenzene 67-130 3.4 20
0.048 96.098.20.0490.050mg/KgStyrene 77-121 2.2 20
Page 8 of 31Date:05/23/2022 04:56 PM
Page 138 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18748QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18747
LCS-V18747 LCSD-V18747Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.047 94.297.60.0480.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 3.5 20
0.044 89.487.60.0430.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.0 20
0.050 1011070.0530.050mg/KgTetrachloroethene 68-130 6.3 20
0.051 1031060.0530.050mg/KgToluene 71-129 3.4 20
0.048 96.094.60.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.4 20
0.047 95.093.80.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.2 20
0.049 99.61060.0520.050mg/Kg1,1,1-Trichloroethane 67-131 6.0 20
0.048 96.497.80.0480.050mg/Kg1,1,2-Trichloroethane 70-133 1.4 20
0.051 1031070.0530.050mg/KgTrichloroethene 75-133 3.6 20
0.045 90.298.00.0490.050mg/KgTrichlorofluoromethane 44-146 8.2 20
0.043 87.889.80.0440.050mg/Kg1,2,3-Trichloropropane 60-137 2.2 20
0.043 86.286.60.0430.050mg/Kg1,2,4-Trimethylbenzene 69-129 0.4 20
0.042 85.287.80.0430.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.0 20
0.051 1031020.0500.050mg/KgVinyl Acetate 60-140 1.5 20
0.042 84.684.80.0420.050mg/KgVinyl Chloride 48-147 0.2 20
0.045 91.894.60.0470.050mg/Kgo-Xylene 74-126 3.0 20
0.092 92.395.60.0950.100mg/Kgm,p-Xylene 75-124 3.5 20
97.695.44-Bromofluorobenzene (S)70-130
101101Dibromofluoromethane (S)84-123
88.490.8Toluene-d8 (S)76-129
Page 9 of 31Date:05/23/2022 04:56 PM
Page 139 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
Associated Lab Samples: 89779, 89784, 89789, 89790, 89791, 89792
LRB-V18807 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/17/22 12:520.0200.002<0.002mg/KgAcetone
05/17/22 12:520.0200.001<0.001mg/KgAcrolein
05/17/22 12:520.0200.0008<0.0008mg/KgAcrylonitrile
05/17/22 12:520.0050.0006<0.0006mg/KgBenzene
05/17/22 12:520.0050.0005<0.0005mg/KgBromobenzene
05/17/22 12:520.0050.0008<0.0008mg/KgBromochloromethane
05/17/22 12:520.0050.001<0.001mg/KgBromodichloromethane
05/17/22 12:520.0050.001<0.001mg/KgBromoform
05/17/22 12:520.0100.001<0.001mg/KgBromomethane
05/17/22 12:520.0050.0005<0.0005mg/Kgn-Butylbenzene
05/17/22 12:520.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/17/22 12:520.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/17/22 12:520.0050.0006<0.0006mg/KgCarbon Disulfide
05/17/22 12:520.0050.001<0.001mg/KgCarbon Tetrachloride
05/17/22 12:520.0050.0007<0.0007mg/KgChlorobenzene
05/17/22 12:520.0050.0009<0.0009mg/KgChlorodibromomethane
05/17/22 12:520.0100.0009<0.0009mg/KgChloroethane
05/17/22 12:520.0050.001<0.001mg/KgChloroform
05/17/22 12:520.0100.0006<0.0006mg/KgChloromethane
05/17/22 12:520.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/17/22 12:520.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/17/22 12:520.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/17/22 12:520.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/17/22 12:520.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/17/22 12:520.0050.0006<0.0006mg/KgDibromomethane
05/17/22 12:520.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/17/22 12:520.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 10 of 31Date:05/23/2022 04:56 PM
Page 140 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
Associated Lab Samples: 89779, 89784, 89789, 89790, 89791, 89792
LRB-V18807 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/17/22 12:520.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/17/22 12:520.0100.001<0.001mg/KgDichlorodifluoromethane
05/17/22 12:520.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/17/22 12:520.0050.001<0.001mg/Kg1,2-Dichloroethane
05/17/22 12:520.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/17/22 12:520.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/17/22 12:520.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/17/22 12:520.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/17/22 12:520.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/17/22 12:520.0050.001<0.001mg/Kg2,2-Dichloropropane
05/17/22 12:520.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/17/22 12:520.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/17/22 12:520.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/17/22 12:520.0050.0006<0.0006mg/KgEthylbenzene
05/17/22 12:520.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/17/22 12:520.0100.0008<0.0008mg/KgHexachlorobutadiene
05/17/22 12:520.0100.0007<0.0007mg/Kgn-Hexane
05/17/22 12:520.0200.0006<0.0006mg/Kg2-Hexanone
05/17/22 12:520.0050.0005<0.0005mg/KgIsopropylbenzene
05/17/22 12:520.0050.001<0.001mg/Kg4-Isopropyl toluene
05/17/22 12:520.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/17/22 12:520.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/17/22 12:520.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/17/22 12:520.0100.001<0.001mg/KgMethylene Chloride
05/17/22 12:520.0100.0010<0.0010mg/KgNaphthalene
05/17/22 12:520.0050.0005<0.0005mg/Kgn-Propylbenzene
05/17/22 12:520.0050.001<0.001mg/KgStyrene
Page 11 of 31Date:05/23/2022 04:56 PM
Page 141 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
Associated Lab Samples: 89779, 89784, 89789, 89790, 89791, 89792
LRB-V18807 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/17/22 12:520.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/17/22 12:520.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/17/22 12:520.0050.0009<0.0009mg/KgTetrachloroethene
05/17/22 12:520.0050.0007<0.0007mg/KgToluene
05/17/22 12:520.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/17/22 12:520.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/17/22 12:520.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/17/22 12:520.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/17/22 12:520.0050.0009<0.0009mg/KgTrichloroethene
05/17/22 12:520.0100.002<0.002mg/KgTrichlorofluoromethane
05/17/22 12:520.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/17/22 12:520.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/17/22 12:520.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/17/22 12:520.0100.0005<0.0005mg/KgVinyl Acetate
05/17/22 12:520.0100.0005<0.0005mg/KgVinyl Chloride
05/17/22 12:520.0050.0005<0.0005mg/Kgo-Xylene
05/17/22 12:520.0100.001<0.001mg/Kgm,p-Xylene
05/17/22 12:524-Bromofluorobenzene (S)104 70-130
05/17/22 12:52Dibromofluoromethane (S)105 84-123
05/17/22 12:52Toluene-d8 (S)87.8 76-129
LCS-V18807 LCSD-V18807Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.125 1251140.1140.100mg/KgAcetone 29-198 9.2 20
0.105 1051040.1040.100mg/KgAcrolein 70-130 0.9 20
Page 12 of 31Date:05/23/2022 04:56 PM
Page 142 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
LCS-V18807 LCSD-V18807Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.110 1101070.1070.100mg/KgAcrylonitrile 65-134 2.7 20
0.054 1091140.0570.050mg/KgBenzene 74-127 4.2 20
0.043 86.890.40.0450.050mg/KgBromobenzene 73-125 4.0 20
0.057 1161180.0590.050mg/KgBromochloromethane 72-134 2.0 20
0.057 1151170.0580.050mg/KgBromodichloromethane 75-122 1.2 20
0.049 99.41000.0500.050mg/KgBromoform 66-135 1.0 20
0.042 84.084.40.0420.050mg/KgBromomethane 20-180 0.4 20
0.045 90.495.60.0470.050mg/Kgn-Butylbenzene 65-135 5.5 20
0.043 87.293.20.0460.050mg/Kgsec-Butyl benzene 66-131 6.6 20
0.043 87.292.20.0460.050mg/Kgtert-Butyl benzene 67-132 5.5 20
0.054 1101170.0580.050mg/KgCarbon Disulfide 61-129 6.7 20
0.054 1091160.0580.050mg/KgCarbon Tetrachloride 64-143 6.2 20
0.048 96.61000.0500.050mg/KgChlorobenzene 74-118 3.4 20
0.049 98.61000.0500.050mg/KgChlorodibromomethane 73-122 1.6 20
0.059 11890.00.0450.050mg/KgChloroethane 33-149 27.0*20
0.055 1111160.0580.050mg/KgChloroform 73-127 4.5 20
0.044 88.487.40.0430.050mg/KgChloromethane 45-143 1.1 20
0.043 87.092.20.0460.050mg/Kg2-Chlorotoluene 67-124 5.8 20
0.044 88.891.80.0450.050mg/Kg4-Chlorotoluene 71-126 3.3 20
0.053 1081100.0540.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.8 20
0.045 90.887.60.0430.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.5 20
0.049 99.298.80.0490.050mg/Kg1,2-Dibromoethane 70-132 0.4 20
0.057 1151150.0570.050mg/KgDibromomethane 74-133 0.5 20
0.045 90.292.20.0460.050mg/Kg1,2-Dichlorobenzene 72-123 2.1 20
0.044 89.092.60.0460.050mg/Kg1,3-Dichlorobenzene 71-120 3.9 20
0.044 89.492.40.0460.050mg/Kg1,4-Dichlorobenzene 71-123 3.3 20
Page 13 of 31* QC Fail Date:05/23/2022 04:56 PM
Page 143 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
LCS-V18807 LCSD-V18807Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.058 1171060.0530.050mg/KgDichlorodifluoromethane 26-146 9.6 20
0.053 1081120.0550.050mg/Kg1,1-Dichloroethane 74-127 3.6 20
0.055 1121120.0560.050mg/Kg1,2-Dichloroethane 68-128 0.5 20
0.051 1041100.0550.050mg/Kg1,1-Dichloroethene 67-149 6.3 20
0.053 1061100.0550.050mg/Kgcis-1,2-Dichloroethene 76-134 3.3 20
0.052 1051090.0540.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.7 20
0.054 1091090.0540.050mg/Kg1,2-Dichloropropane 73-130 0.3 20
0.048 96.897.00.0480.050mg/Kg1,3-Dichloropropane 75-124 0.2 20
0.054 1091170.0580.050mg/Kg2,2-Dichloropropane 50-142 7.6 20
0.053 1071130.0560.050mg/Kg1,1-Dichloropropene 71-130 5.8 20
0.056 1131150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 2.1 20
0.056 1131160.0570.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.9 20
0.047 94.298.60.0490.050mg/KgEthylbenzene 74-128 4.5 20
0.109 1091100.1100.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.044 88.691.80.0450.050mg/KgHexachlorobutadiene 64-125 3.5 20
0.057 1161220.0600.050mg/Kgn-Hexane 70-130 5.0 20
0.047 95.491.60.0450.050mg/Kg2-Hexanone 61-157 4.0 20
0.043 87.092.20.0460.050mg/KgIsopropylbenzene 68-126 5.8 20
0.044 89.094.20.0470.050mg/Kg4-Isopropyl toluene 68-129 5.6 20
0.056 1131040.0520.050mg/KgMethyl Ethyl Ketone (MEK)63-149 7.9 20
0.054 1081080.0540.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.3 20
0.054 1081040.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 3.3 20
0.054 1081110.0550.050mg/KgMethylene Chloride 74-129 2.0 20
0.047 94.693.60.0460.050mg/KgNaphthalene 57-157 1.0 20
0.044 89.294.40.0470.050mg/Kgn-Propylbenzene 67-130 5.6 20
0.050 1001020.0510.050mg/KgStyrene 77-121 1.9 20
Page 14 of 31Date:05/23/2022 04:56 PM
Page 144 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18810QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18807
LCS-V18807 LCSD-V18807Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 98.61020.0510.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 3.3 20
0.044 88.490.40.0450.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.2 20
0.053 1081130.0560.050mg/KgTetrachloroethene 68-130 4.8 20
0.054 1081140.0560.050mg/KgToluene 71-129 4.8 20
0.046 92.094.00.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.1 20
0.045 91.294.20.0470.050mg/Kg1,2,4-Trichlorobenzene 66-125 3.2 20
0.054 1091140.0570.050mg/Kg1,1,1-Trichloroethane 67-131 4.8 20
0.048 97.898.40.0490.050mg/Kg1,1,2-Trichloroethane 70-133 0.6 20
0.054 1091150.0570.050mg/KgTrichloroethene 75-133 5.3 20
0.056 1131140.0560.050mg/KgTrichlorofluoromethane 44-146 0.3 20
0.045 90.890.00.0450.050mg/Kg1,2,3-Trichloropropane 60-137 0.8 20
0.043 87.892.20.0460.050mg/Kg1,2,4-Trimethylbenzene 69-129 4.8 20
0.044 89.093.20.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 4.6 20
0.054 1081170.0580.050mg/KgVinyl Acetate 60-140 7.2 20
0.054 1091140.0570.050mg/KgVinyl Chloride 48-147 5.0 20
0.047 95.298.40.0490.050mg/Kgo-Xylene 74-126 3.3 20
0.096 96.41010.1010.100mg/Kgm,p-Xylene 75-124 4.6 20
98.298.44-Bromofluorobenzene (S)70-130
104102Dibromofluoromethane (S)84-123
89.088.6Toluene-d8 (S)76-129
Page 15 of 31Date:05/23/2022 04:56 PM
Page 145 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18871QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18870
Associated Lab Samples: 89778
LRB-V18870 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/17/22 12:520.0050.001<0.001mg/KgChloroform
05/17/22 12:524-Bromofluorobenzene (S)104 70-130
05/17/22 12:52Dibromofluoromethane (S)105 70-130
05/17/22 12:52Toluene-d8 (S)87.8 76-129
LCS-V18870 LCSD-V18870Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.055 1111160.0580.050mg/KgChloroform 73-127 4.5 20
98.298.44-Bromofluorobenzene (S)70-130
104102Dibromofluoromethane (S)70-130
89.088.6Toluene-d8 (S)76-129
Page 16 of 31Date:05/23/2022 04:56 PM
Page 146 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
Associated Lab Samples: 89785
LRB-V18986 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0200.002<0.002mg/KgAcetone
05/20/22 11:580.0200.001<0.001mg/KgAcrolein
05/20/22 11:580.0200.0008<0.0008mg/KgAcrylonitrile
05/20/22 11:580.0050.0006<0.0006mg/KgBenzene
05/20/22 11:580.0050.0005<0.0005mg/KgBromobenzene
05/20/22 11:580.0050.0008<0.0008mg/KgBromochloromethane
05/20/22 11:580.0050.001<0.001mg/KgBromodichloromethane
05/20/22 11:580.0050.001<0.001mg/KgBromoform
05/20/22 11:580.0100.001<0.001mg/KgBromomethane
05/20/22 11:580.0050.0005<0.0005mg/Kgn-Butylbenzene
05/20/22 11:580.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/20/22 11:580.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/20/22 11:580.0050.0006<0.0006mg/KgCarbon Disulfide
05/20/22 11:580.0050.001<0.001mg/KgCarbon Tetrachloride
05/20/22 11:580.0050.0007<0.0007mg/KgChlorobenzene
05/20/22 11:580.0050.0009<0.0009mg/KgChlorodibromomethane
05/20/22 11:580.0100.0009<0.0009mg/KgChloroethane
05/20/22 11:580.0050.001<0.001mg/KgChloroform
05/20/22 11:580.0100.0006<0.0006mg/KgChloromethane
05/20/22 11:580.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/20/22 11:580.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/20/22 11:580.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/20/22 11:580.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/20/22 11:580.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/20/22 11:580.0050.0006<0.0006mg/KgDibromomethane
05/20/22 11:580.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/20/22 11:580.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 17 of 31Date:05/23/2022 04:56 PM
Page 147 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
Associated Lab Samples: 89785
LRB-V18986 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/20/22 11:580.0100.001<0.001mg/KgDichlorodifluoromethane
05/20/22 11:580.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/20/22 11:580.0050.001<0.001mg/Kg1,2-Dichloroethane
05/20/22 11:580.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/20/22 11:580.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/20/22 11:580.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/20/22 11:580.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/20/22 11:580.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/20/22 11:580.0050.001<0.001mg/Kg2,2-Dichloropropane
05/20/22 11:580.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/20/22 11:580.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/20/22 11:580.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/20/22 11:580.0050.0006<0.0006mg/KgEthylbenzene
05/20/22 11:580.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/20/22 11:580.0100.0008<0.0008mg/KgHexachlorobutadiene
05/20/22 11:580.0100.0007<0.0007mg/Kgn-Hexane
05/20/22 11:580.0200.0006<0.0006mg/Kg2-Hexanone
05/20/22 11:580.0050.0005<0.0005mg/KgIsopropylbenzene
05/20/22 11:580.0050.001<0.001mg/Kg4-Isopropyl toluene
05/20/22 11:580.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/20/22 11:580.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/20/22 11:580.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/20/22 11:580.0100.001<0.001mg/KgMethylene Chloride
05/20/22 11:580.0100.0010<0.0010mg/KgNaphthalene
05/20/22 11:580.0050.0005<0.0005mg/Kgn-Propylbenzene
05/20/22 11:580.0050.001<0.001mg/KgStyrene
Page 18 of 31Date:05/23/2022 04:56 PM
Page 148 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
Associated Lab Samples: 89785
LRB-V18986 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/20/22 11:580.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/20/22 11:580.0050.0009<0.0009mg/KgTetrachloroethene
05/20/22 11:580.0050.0007<0.0007mg/KgToluene
05/20/22 11:580.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/20/22 11:580.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/20/22 11:580.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/20/22 11:580.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/20/22 11:580.0050.0009<0.0009mg/KgTrichloroethene
05/20/22 11:580.0100.002<0.002mg/KgTrichlorofluoromethane
05/20/22 11:580.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/20/22 11:580.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/20/22 11:580.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/20/22 11:580.0100.0005<0.0005mg/KgVinyl Acetate
05/20/22 11:580.0100.0005<0.0005mg/KgVinyl Chloride
05/20/22 11:580.0050.0005<0.0005mg/Kgo-Xylene
05/20/22 11:580.0100.001<0.001mg/Kgm,p-Xylene
05/20/22 11:584-Bromofluorobenzene (S)103 70-130
05/20/22 11:58Dibromofluoromethane (S)101 84-123
05/20/22 11:58Toluene-d8 (S)86.6 76-129
LCS-V18986 LCSD-V18986Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.093 93.882.00.0820.100mg/KgAcetone 29-198 13.4 20
0.090 90.488.40.0880.100mg/KgAcrolein 70-130 2.2 20
Page 19 of 31Date:05/23/2022 04:56 PM
Page 149 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
LCS-V18986 LCSD-V18986Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.090 90.386.00.0860.100mg/KgAcrylonitrile 65-134 4.8 20
0.055 1101140.0570.050mg/KgBenzene 74-127 3.9 20
0.044 89.691.00.0450.050mg/KgBromobenzene 73-125 1.5 20
0.057 1151170.0580.050mg/KgBromochloromethane 72-134 2.4 20
0.058 1171200.0590.050mg/KgBromodichloromethane 75-122 2.0 20
0.052 1041000.0500.050mg/KgBromoform 66-135 3.7 20
0.047 95.61010.0500.050mg/KgBromomethane 20-180 5.4 20
0.046 92.697.20.0480.050mg/Kgn-Butylbenzene 65-135 4.8 20
0.044 88.693.00.0460.050mg/Kgsec-Butyl benzene 66-131 4.8 20
0.043 86.691.60.0450.050mg/Kgtert-Butyl benzene 67-132 5.6 20
0.051 1041110.0550.050mg/KgCarbon Disulfide 61-129 6.5 20
0.054 1101180.0590.050mg/KgCarbon Tetrachloride 64-143 7.5 20
0.049 98.498.20.0490.050mg/KgChlorobenzene 74-118 0.2 20
0.050 10197.20.0480.050mg/KgChlorodibromomethane 73-122 3.4 20
0.062 1241260.0620.050mg/KgChloroethane 33-149 0.9 20
0.056 1131160.0580.050mg/KgChloroform 73-127 2.6 20
0.034 69.674.80.0370.050mg/KgChloromethane 45-143 7.2 20
0.044 89.492.00.0460.050mg/Kg2-Chlorotoluene 67-124 2.8 20
0.044 89.893.00.0460.050mg/Kg4-Chlorotoluene 71-126 3.5 20
0.042 85.487.20.0430.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.0 20
0.045 91.489.00.0440.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.6 20
0.050 10097.20.0480.050mg/Kg1,2-Dibromoethane 70-132 3.2 20
0.060 1201190.0590.050mg/KgDibromomethane 74-133 1.5 20
0.044 88.489.60.0440.050mg/Kg1,2-Dichlorobenzene 72-123 1.3 20
0.043 87.890.60.0450.050mg/Kg1,3-Dichlorobenzene 71-120 3.1 20
0.044 88.290.80.0450.050mg/Kg1,4-Dichlorobenzene 71-123 2.9 20
Page 20 of 31Date:05/23/2022 04:56 PM
Page 150 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
LCS-V18986 LCSD-V18986Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.052 1061130.0560.050mg/KgDichlorodifluoromethane 26-146 6.9 20
0.050 1001040.0510.050mg/Kg1,1-Dichloroethane 74-127 3.3 20
0.053 1071090.0540.050mg/Kg1,2-Dichloroethane 68-128 1.4 20
0.045 91.097.40.0480.050mg/Kg1,1-Dichloroethene 67-149 6.7 20
0.047 95.898.40.0490.050mg/Kgcis-1,2-Dichloroethene 76-134 2.6 20
0.046 93.096.00.0480.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.1 20
0.051 1021040.0520.050mg/Kg1,2-Dichloropropane 73-130 1.7 20
0.048 96.296.00.0480.050mg/Kg1,3-Dichloropropane 75-124 0.2 20
0.056 1131190.0590.050mg/Kg2,2-Dichloropropane 50-142 5.5 20
0.054 1091130.0560.050mg/Kg1,1-Dichloropropene 71-130 3.4 20
0.056 1131150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 2.1 20
0.058 1161140.0570.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.9 20
0.049 98.21010.0500.050mg/KgEthylbenzene 74-128 2.4 20
0.094 94.294.80.0940.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.6 20
0.043 87.892.60.0460.050mg/KgHexachlorobutadiene 64-125 5.3 20
0.054 1081120.0560.050mg/Kgn-Hexane 70-130 3.9 20
0.035 70.468.40.0340.050mg/Kg2-Hexanone 61-157 2.8 20
0.044 88.291.80.0450.050mg/KgIsopropylbenzene 68-126 4.0 20
0.044 88.692.20.0460.050mg/Kg4-Isopropyl toluene 68-129 3.9 20
0.045 90.092.80.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 3.0 20
0.052 1041040.0510.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.7 20
0.043 87.685.40.0420.050mg/Kg4-Methyl-2-Pentanone 57-162 2.5 20
0.041 82.090.20.0450.050mg/KgMethylene Chloride 74-129 9.5 20
0.047 94.488.60.0440.050mg/KgNaphthalene 57-157 6.3 20
0.045 91.295.60.0470.050mg/Kgn-Propylbenzene 67-130 4.7 20
0.049 99.41010.0500.050mg/KgStyrene 77-121 1.3 20
Page 21 of 31Date:05/23/2022 04:56 PM
Page 151 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18987QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18986
LCS-V18986 LCSD-V18986Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 99.01000.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.044 88.487.40.0430.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.1 20
0.055 1111160.0580.050mg/KgTetrachloroethene 68-130 4.5 20
0.055 1111150.0570.050mg/KgToluene 71-129 3.5 20
0.045 90.689.40.0440.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.3 20
0.046 92.092.00.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.0 20
0.057 1161190.0590.050mg/Kg1,1,1-Trichloroethane 67-131 2.8 20
0.049 98.299.00.0490.050mg/Kg1,1,2-Trichloroethane 70-133 0.8 20
0.055 1111160.0580.050mg/KgTrichloroethene 75-133 4.7 20
0.051 1031110.0550.050mg/KgTrichlorofluoromethane 44-146 7.5 20
0.044 89.085.80.0420.050mg/Kg1,2,3-Trichloropropane 60-137 3.6 20
0.044 88.690.20.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.7 20
0.044 88.291.60.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.7 20
0.059 1181160.0570.050mg/KgVinyl Acetate 60-140 2.2 20
0.044 89.692.60.0460.050mg/KgVinyl Chloride 48-147 3.2 20
0.049 99.099.60.0490.050mg/Kgo-Xylene 74-126 0.6 20
0.099 99.91020.1020.100mg/Kgm,p-Xylene 75-124 2.0 20
1011024-Bromofluorobenzene (S)70-130
102101Dibromofluoromethane (S)84-123
87.085.6Toluene-d8 (S)76-129
Page 22 of 31Date:05/23/2022 04:56 PM
Page 152 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
Associated Lab Samples: 89783
LRB-V18988 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0200.002<0.002mg/KgAcetone
05/20/22 11:580.0200.001<0.001mg/KgAcrolein
05/20/22 11:580.0200.0008<0.0008mg/KgAcrylonitrile
05/20/22 11:580.0050.0006<0.0006mg/KgBenzene
05/20/22 11:580.0050.0005<0.0005mg/KgBromobenzene
05/20/22 11:580.0050.0008<0.0008mg/KgBromochloromethane
05/20/22 11:580.0050.001<0.001mg/KgBromodichloromethane
05/20/22 11:580.0050.001<0.001mg/KgBromoform
05/20/22 11:580.0100.001<0.001mg/KgBromomethane
05/20/22 11:580.0050.0005<0.0005mg/Kgn-Butylbenzene
05/20/22 11:580.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/20/22 11:580.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/20/22 11:580.0050.0006<0.0006mg/KgCarbon Disulfide
05/20/22 11:580.0050.001<0.001mg/KgCarbon Tetrachloride
05/20/22 11:580.0050.0007<0.0007mg/KgChlorobenzene
05/20/22 11:580.0050.0009<0.0009mg/KgChlorodibromomethane
05/20/22 11:580.0100.0009<0.0009mg/KgChloroethane
05/20/22 11:580.0050.001<0.001mg/KgChloroform
05/20/22 11:580.0100.0006<0.0006mg/KgChloromethane
05/20/22 11:580.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/20/22 11:580.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/20/22 11:580.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/20/22 11:580.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/20/22 11:580.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/20/22 11:580.0050.0010<0.0010mg/KgDibromomethane
05/20/22 11:580.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/20/22 11:580.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 23 of 31Date:05/23/2022 04:56 PM
Page 153 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
Associated Lab Samples: 89783
LRB-V18988 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/20/22 11:580.0100.001<0.001mg/KgDichlorodifluoromethane
05/20/22 11:580.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/20/22 11:580.0050.001<0.001mg/Kg1,2-Dichloroethane
05/20/22 11:580.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/20/22 11:580.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/20/22 11:580.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/20/22 11:580.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/20/22 11:580.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/20/22 11:580.0050.001<0.001mg/Kg2,2-Dichloropropane
05/20/22 11:580.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/20/22 11:580.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/20/22 11:580.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/20/22 11:580.0050.0006<0.0006mg/KgEthylbenzene
05/20/22 11:580.1000.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/20/22 11:580.0100.0008<0.0008mg/KgHexachlorobutadiene
05/20/22 11:580.0100.0007<0.0007mg/Kgn-Hexane
05/20/22 11:580.0200.0006<0.0006mg/Kg2-Hexanone
05/20/22 11:580.0050.0005<0.0005mg/KgIsopropylbenzene
05/20/22 11:580.0050.001<0.001mg/Kg4-Isopropyl toluene
05/20/22 11:580.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/20/22 11:580.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/20/22 11:580.0050.001<0.001mg/KgMethylene Chloride
05/20/22 11:580.0100.0010<0.0010mg/KgNaphthalene
05/20/22 11:580.0050.0005<0.0005mg/Kgn-Propylbenzene
05/20/22 11:580.0050.001<0.001mg/KgStyrene
05/20/22 11:580.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
Page 24 of 31Date:05/23/2022 04:56 PM
Page 154 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
Associated Lab Samples: 89783
LRB-V18988 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/20/22 11:580.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/20/22 11:580.0050.0009<0.0009mg/KgTetrachloroethene
05/20/22 11:580.0050.0007<0.0007mg/KgToluene
05/20/22 11:580.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/20/22 11:580.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/20/22 11:580.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/20/22 11:580.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/20/22 11:580.0050.0009<0.0009mg/KgTrichloroethene
05/20/22 11:580.0100.002<0.002mg/KgTrichlorofluoromethane
05/20/22 11:580.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/20/22 11:580.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/20/22 11:580.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/20/22 11:580.0100.0005<0.0005mg/KgVinyl Acetate
05/20/22 11:580.0100.0005<0.0005mg/KgVinyl Chloride
05/20/22 11:580.0050.0005<0.0005mg/Kgo-Xylene
05/20/22 11:580.0100.001<0.001mg/Kgm,p-Xylene
05/20/22 11:584-Bromofluorobenzene (S)103 70-130
05/20/22 11:58Dibromofluoromethane (S)101 70-130
05/20/22 11:58Toluene-d8 (S)86.6 76-129
LCS-V18988 LCSD-V18988Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.093 93.882.00.0820.100mg/KgAcetone 29-198 13.4 20
0.090 90.488.40.0880.100mg/KgAcrolein 70-130 2.2 20
0.090 90.386.00.0860.100mg/KgAcrylonitrile 65-134 4.8 20
Page 25 of 31Date:05/23/2022 04:56 PM
Page 155 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
LCS-V18988 LCSD-V18988Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.055 1101140.0570.050mg/KgBenzene 74-127 3.9 20
0.044 89.691.00.0450.050mg/KgBromobenzene 73-125 1.5 20
0.057 1151170.0580.050mg/KgBromochloromethane 72-134 2.4 20
0.058 1171200.0590.050mg/KgBromodichloromethane 75-122 2.0 20
0.052 1041000.0500.050mg/KgBromoform 66-135 3.7 20
0.047 95.61010.0500.050mg/KgBromomethane 20-180 5.4 20
0.046 92.697.20.0480.050mg/Kgn-Butylbenzene 65-135 4.8 20
0.044 88.693.00.0460.050mg/Kgsec-Butyl benzene 66-131 4.8 20
0.043 86.691.60.0450.050mg/Kgtert-Butyl benzene 67-132 5.6 20
0.051 1041110.0550.050mg/KgCarbon Disulfide 61-129 6.5 20
0.054 1101180.0590.050mg/KgCarbon Tetrachloride 64-143 7.5 20
0.049 98.498.20.0490.050mg/KgChlorobenzene 74-118 0.2 20
0.050 10197.20.0480.050mg/KgChlorodibromomethane 73-122 3.4 20
0.062 1241260.0620.050mg/KgChloroethane 33-149 0.9 20
0.056 1131160.0580.050mg/KgChloroform 73-127 2.6 20
0.034 69.674.80.0370.050mg/KgChloromethane 45-143 7.2 20
0.044 89.492.00.0460.050mg/Kg2-Chlorotoluene 67-124 2.8 20
0.044 89.893.00.0460.050mg/Kg4-Chlorotoluene 71-126 3.5 20
0.042 85.487.20.0430.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.0 20
0.045 91.489.00.0440.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.6 20
0.050 10097.20.0480.050mg/Kg1,2-Dibromoethane 70-132 3.2 20
0.060 1201190.0590.050mg/KgDibromomethane 74-133 1.5 20
0.044 88.489.60.0440.050mg/Kg1,2-Dichlorobenzene 72-123 1.3 20
0.043 87.890.60.0450.050mg/Kg1,3-Dichlorobenzene 71-120 3.1 20
0.044 88.290.80.0450.050mg/Kg1,4-Dichlorobenzene 71-123 2.9 20
0.052 1061130.0560.050mg/KgDichlorodifluoromethane 26-146 6.9 20
Page 26 of 31Date:05/23/2022 04:56 PM
Page 156 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
LCS-V18988 LCSD-V18988Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1001040.0510.050mg/Kg1,1-Dichloroethane 74-127 3.3 20
0.053 1071090.0540.050mg/Kg1,2-Dichloroethane 68-128 1.4 20
0.045 91.097.40.0480.050mg/Kg1,1-Dichloroethene 67-149 6.7 20
0.047 95.898.40.0490.050mg/Kgcis-1,2-Dichloroethene 76-134 2.6 20
0.046 93.096.00.0480.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.1 20
0.051 1021040.0520.050mg/Kg1,2-Dichloropropane 73-130 1.7 20
0.048 96.296.00.0480.050mg/Kg1,3-Dichloropropane 75-124 0.2 20
0.056 1131190.0590.050mg/Kg2,2-Dichloropropane 50-142 5.5 20
0.054 1091130.0560.050mg/Kg1,1-Dichloropropene 71-130 3.4 20
0.056 1131150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 2.1 20
0.058 1161140.0570.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.9 20
0.049 98.21010.0500.050mg/KgEthylbenzene 74-128 2.4 20
0.094 94.294.80.0940.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.6 20
0.043 87.892.60.0460.050mg/KgHexachlorobutadiene 64-125 5.3 20
0.054 1081120.0560.050mg/Kgn-Hexane 70-130 3.9 20
0.035 70.468.40.0340.050mg/Kg2-Hexanone 61-157 2.8 20
0.044 88.291.80.0450.050mg/KgIsopropylbenzene 68-126 4.0 20
0.044 88.692.20.0460.050mg/Kg4-Isopropyl toluene 68-129 3.9 20
0.045 90.092.80.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 3.0 20
0.052 1041040.0510.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.7 20
0.041 82.090.20.0450.050mg/KgMethylene Chloride 74-129 9.5 20
0.047 94.488.60.0440.050mg/KgNaphthalene 57-157 6.3 20
0.045 91.295.60.0470.050mg/Kgn-Propylbenzene 67-130 4.7 20
0.049 99.41010.0500.050mg/KgStyrene 77-121 1.3 20
0.049 99.01000.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.044 88.487.40.0430.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.1 20
Page 27 of 31Date:05/23/2022 04:56 PM
Page 157 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18989QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18988
LCS-V18988 LCSD-V18988Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.055 1111160.0580.050mg/KgTetrachloroethene 68-130 4.5 20
0.055 1111150.0570.050mg/KgToluene 71-129 3.5 20
0.045 90.689.40.0440.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.3 20
0.046 92.092.00.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.0 20
0.057 1161190.0590.050mg/Kg1,1,1-Trichloroethane 67-131 2.8 20
0.049 98.299.00.0490.050mg/Kg1,1,2-Trichloroethane 70-133 0.8 20
0.055 1111160.0580.050mg/KgTrichloroethene 75-133 4.7 20
0.051 1031110.0550.050mg/KgTrichlorofluoromethane 44-146 7.5 20
0.044 89.085.80.0420.050mg/Kg1,2,3-Trichloropropane 60-137 3.6 20
0.044 88.690.20.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.7 20
0.044 88.291.60.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.7 20
0.059 1181160.0570.050mg/KgVinyl Acetate 60-140 2.2 20
0.044 89.692.60.0460.050mg/KgVinyl Chloride 48-147 3.2 20
0.049 99.099.60.0490.050mg/Kgo-Xylene 74-126 0.6 20
0.099 99.91020.1020.100mg/Kgm,p-Xylene 75-124 2.0 20
1011024-Bromofluorobenzene (S)70-130
102101Dibromofluoromethane (S)70-130
87.085.6Toluene-d8 (S)76-129
Page 28 of 31Date:05/23/2022 04:56 PM
Page 158 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
Dry Weight Determination
SW-DRYWT
V18823QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89427-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/18/22 11:010.013.913.9%Moisture
V 89775-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/18/22 11:011.815.916.2%Moisture
Page 29 of 31Date:05/23/2022 04:56 PM
Page 159 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
Dry Weight Determination
SW-DRYWT
V18876QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89785-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/19/22 10:402.49.008.78%Moisture
V 89793-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/19/22 10:400.824.724.9%Moisture
Page 30 of 31Date:05/23/2022 04:56 PM
Page 160 of 166
Quality Control Data
22-133-0023Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
Dry Weight Determination
SW-DRYWT
V18961QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89795-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/20/22 12:520.910.210.1%Moisture
V 90119-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/20/22 12:521.821.922.3%Moisture
Page 31 of 31Date:05/23/2022 04:56 PM
Page 161 of 166
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-133-0023
ATC Group Services, LLC - Raleigh, NC
01024
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 6.0 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:05/13/2022 15:55:14
Special precautions or instructions included?
Comments:
Page 162 of 166
Page 163 of 166
Page 164 of 166
Page 165 of 166
Page 166 of 166

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/25/2022
ATC Group Services, LLC - Raleigh, NC Maureen Jackson
609A Piner Road Suite 115 Wilminton, NC, 28409
Ref: Analytical Testing
Lab Report Number: 22-137-0007 Client Project Description: Circle K 2720104
Dear Maureen Jackson:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 5/17/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 36
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-137-0007
Page 2 of 36
Report Number:
Sample Summary Table
Client Project Description:
22-137-0007
Circle K 2720104
Lab No Client Sample ID Matrix Date Collected Date Received
05/12/2022 13:40Solids 89999 L-7 05/17/2022 14:19
05/12/2022 13:50Solids 90000 L-8 05/17/2022 14:19
05/12/2022 13:35Solids 90001 D-5 05/17/2022 14:19
05/12/2022 13:45Solids 90002 D-6 05/17/2022 14:19
Page 3 of 36
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-137-0007
Report Limit
Project:Circle K 2720104
V 89999L-7
0.047 05/21/2022 09:418260DAcetonemg/Kg - dry 0.002
0.084 05/21/2022 09:418260DBenzenemg/Kg - dry 0.0007
J0.0007 05/21/2022 09:418260Dn-Butylbenzene mg/Kg - dry 0.0006
J0.003 05/21/2022 09:418260DEthylbenzenemg/Kg - dry 0.0007
J0.004 05/21/2022 09:418260Dn-Hexane mg/Kg - dry 0.0008
J0.010 05/21/2022 09:418260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.002 05/21/2022 09:418260DNaphthalenemg/Kg - dry 0.001
0.117 05/21/2022 09:418260DToluenemg/Kg - dry 0.0008
J0.002 05/21/2022 09:418260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0007 05/21/2022 09:418260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
0.009 05/21/2022 09:418260Do-Xylene mg/Kg - dry 0.0006
0.022 05/21/2022 09:418260Dm,p-Xylene mg/Kg - dry 0.001
0.031 05/21/2022 09:418260DXylene (Total)mg/Kg - dry 0.0006
J1.59 05/18/2022 19:16MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 1.47
16.9 05/23/2022 13:13SW-DRYWT Moisture %
V 90000L-8
J0.016 05/21/2022 10:088260DAcetonemg/Kg - dry 0.002
J0.002 05/21/2022 10:088260DCarbon Disulfide mg/Kg - dry 0.0007
J0.003 05/21/2022 10:088260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.001 05/21/2022 10:088260DNaphthalenemg/Kg - dry 0.001
J0.001 05/21/2022 10:088260DToluenemg/Kg - dry 0.0008
J0.001 05/21/2022 10:088260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.0010 05/21/2022 10:088260Do-Xylene mg/Kg - dry 0.0006
J0.001 05/21/2022 10:088260Dm,p-Xylene mg/Kg - dry 0.001
J0.002 05/21/2022 10:088260DXylene (Total)mg/Kg - dry 0.0006
13.1 05/23/2022 13:13SW-DRYWT Moisture %
V 90001D-5
J2.75 05/18/2022 14:098015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.31
0.158 05/21/2022 10:368260DAcetonemg/Kg - dry 0.002
J0.002 05/21/2022 10:368260DBenzenemg/Kg - dry 0.0006
J0.0009 05/21/2022 10:368260DDi-Isopropyl Ether (DIPE)mg/Kg - dry 0.0008
J0.005 05/21/2022 10:368260Dn-Hexane mg/Kg - dry 0.0007
0.049 05/21/2022 10:368260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.0007 05/21/2022 10:368260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0006
J0.003 05/21/2022 10:368260Do-Xylene mg/Kg - dry 0.0006
J0.003 05/21/2022 10:368260Dm,p-Xylene mg/Kg - dry 0.001
Page 4 of 36
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-137-0007
Report Limit
Project:Circle K 2720104
V 90001D-5
J0.006 05/21/2022 10:368260DXylene (Total)mg/Kg - dry 0.0006
10.2 05/23/2022 13:13SW-DRYWT Moisture %
V 90002D-6
77.2 05/20/2022 06:578015C DRO Diesel Range Organics (C10-C28)mg/Kg - dry 5.08
5.64 05/18/2022 14:378015C GRO Gasoline Range Organics (C6-C10)mg/Kg - dry 2.26
8.39 05/23/2022 13:13SW-DRYWT Moisture %
Page 5 of 36

Client: ATC Group Services, LLC - Raleigh, NC CASE NARRATIVE
Project: Circle K 2720104 Lab Report Number: 22-137-0007
Date: 5/24/2022
Total Petroleum Hydrocarbons - Extractable Method 8015C DRO Sample 89767 (Stock 3) QC Batch No: V18982/V18830
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Total Petroleum Hydrocarbons - Volatile Method 8015C GRO
Sample 89999 (L-7) Analyte: a,a,a-Trifluorotoluene
QC Batch No: V18834/V18833 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Acetone QC Batch No: V18991/V18990
CCV result is below control limits but within method parameters. A standard at or below the RL was analyzed and found acceptable. No further action taken.

Page 6 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.9 %Moisture 1 05/23/22 13:13 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 7 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18833 05/18/22 08:00
<2.49 mg/Kg - dry 2.49 6.02Gasoline Range Organics (C6-C10)50 05/18/22 13:13 V18834TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 142 *Limits: 50-137%05/18/22 13:1350 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
0.047 mg/Kg - dry 0.002 0.024Acetone 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 05/21/22 09:41 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 05/21/22 09:41 V18991TBL
0.084 mg/Kg - dry 0.0007 0.006Benzene 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.006
Bromobenzene 1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/21/22 09:41 V18991TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/21/22 09:41 V18991TBL
0.0007 J mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.006
tert-Butyl benzene 1 05/21/22 09:41 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 05/21/22 09:41 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/21/22 09:41 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/21/22 09:41 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/21/22 09:41 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/21/22 09:41 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/21/22 09:41 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.006
Dibromomethane 1 05/21/22 09:41 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/21/22 09:41 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/21/22 09:41 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloroethene 1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/21/22 09:41 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/21/22 09:41 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 05/21/22 09:41 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 05/21/22 09:41 V18991TBL
0.003 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.060Ethyl Tertiary Butyl Ether (ETBE)1 05/21/22 09:41 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 05/21/22 09:41 V18991TBL
0.004 J mg/Kg - dry 0.0008 0.012n-Hexane 1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0242-Hexanone 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006
4-Isopropyl toluene 1 05/21/22 09:41 V18991TBL
0.010 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 05/21/22 09:41 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 05/21/22 09:41 V18991TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/21/22 09:41 V18991TBL
0.002 J mg/Kg - dry 0.001 0.012Naphthalene 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Propylbenzene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006
Styrene 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/21/22 09:41 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/21/22 09:41 V18991TBL
0.117 mg/Kg - dry 0.0008 0.006Toluene 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,3-Trichlorobenzene 1 05/21/22 09:41 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/21/22 09:41 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/21/22 09:41 V18991TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/21/22 09:41 V18991TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/21/22 09:41 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/21/22 09:41 V18991TBL
0.002 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/21/22 09:41 V18991TBL
0.0007 J mg/Kg - dry 0.0006 0.0061,3,5-Trimethylbenzene 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/21/22 09:41 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Vinyl Chloride 1 05/21/22 09:41 V18991TBL
0.009 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/21/22 09:41 V18991TBL
0.022 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/21/22 09:41 V18991TBL
0.031 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/21/22 09:41 V18991
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%05/21/22 09:411 TBL V18991
Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/21/22 09:411 TBL V18991
Surrogate: Toluene-d8 84.3 Limits: 76-129%05/21/22 09:411 TBL V18991
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-7
89999 Matrix:
5/12/2022 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V18846 05/18/22 08:00
1.59 J mg/Kg - dry 1.47 9.63Aliphatic C5-C8 100 05/18/22 19:16 V18847TBL
<5.49 mg/Kg - dry 5.49 9.63Aliphatic C9-C12 100 05/18/22 19:16 V18847TBL
<0.750 mg/Kg - dry 0.750 9.63Aromatic C9-C10 100 05/18/22 19:16 V18847TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)101 Limits: 70-130%05/18/22 19:16100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)102 Limits: 70-130%05/18/22 19:16100 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-8
90000 Matrix:
5/12/2022 13:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.1 %Moisture 1 05/23/22 13:13 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-8
90000 Matrix:
5/12/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18833 05/18/22 08:00
<2.38 mg/Kg - dry 2.38 5.75Gasoline Range Organics (C6-C10)50 05/18/22 13:42 V18834TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 128 Limits: 50-137%05/18/22 13:4250 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
0.016 J mg/Kg - dry 0.002 0.023Acetone 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Bromobenzene 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/21/22 10:08 V18991TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
tert-Butyl benzene 1 05/21/22 10:08 V18991TBL
0.002 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/21/22 10:08 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/21/22 10:08 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-8
90000 Matrix:
5/12/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/21/22 10:08 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/21/22 10:08 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/21/22 10:08 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/21/22 10:08 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/21/22 10:08 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/21/22 10:08 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloroethene 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/21/22 10:08 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/21/22 10:08 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-8
90000 Matrix:
5/12/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/21/22 10:08 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 05/21/22 10:08 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/21/22 10:08 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/21/22 10:08 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/21/22 10:08 V18991TBL
0.003 J mg/Kg - dry 0.0007 0.023Methyl Ethyl Ketone (MEK)1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/21/22 10:08 V18991TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/21/22 10:08 V18991TBL
0.001 J mg/Kg - dry 0.001 0.011Naphthalene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005
Styrene 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/21/22 10:08 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/21/22 10:08 V18991TBL
0.001 J mg/Kg - dry 0.0008 0.005Toluene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/21/22 10:08 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/21/22 10:08 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:L-8
90000 Matrix:
5/12/2022 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/21/22 10:08 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/21/22 10:08 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/21/22 10:08 V18991TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/21/22 10:08 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/21/22 10:08 V18991TBL
0.001 J mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/21/22 10:08 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/21/22 10:08 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.011
Vinyl Chloride 1 05/21/22 10:08 V18991TBL
0.0010 J mg/Kg - dry 0.0006 0.005o-Xylene 1 05/21/22 10:08 V18991TBL
0.001 J mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/21/22 10:08 V18991TBL
0.002 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/21/22 10:08 V18991
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%05/21/22 10:081 TBL V18991
Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/21/22 10:081 TBL V18991
Surrogate: Toluene-d8 85.8 Limits: 76-129%05/21/22 10:081 TBL V18991
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-5
90001 Matrix:
5/12/2022 13:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
10.2 %Moisture 1 05/23/22 13:13 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-5
90001 Matrix:
5/12/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18833 05/18/22 08:00
2.75 J mg/Kg - dry 2.31 5.57Gasoline Range Organics (C6-C10)50 05/18/22 14:09 V18834TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 136 Limits: 50-137%05/18/22 14:0950 TBL
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
0.158 mg/Kg - dry 0.002 0.022Acetone 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/21/22 10:36 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 05/21/22 10:36 V18991TBL
0.002 J mg/Kg - dry 0.0006 0.005Benzene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Bromobenzene 1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/21/22 10:36 V18991TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
tert-Butyl benzene 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 05/21/22 10:36 V18991TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 05/21/22 10:36 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-5
90001 Matrix:
5/12/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/21/22 10:36 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/21/22 10:36 V18991TBL
0.0009 J mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005
Dibromomethane 1 05/21/22 10:36 V18991TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 05/21/22 10:36 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/21/22 10:36 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloroethene 1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/21/22 10:36 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 05/21/22 10:36 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-5
90001 Matrix:
5/12/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 05/21/22 10:36 V18991TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/21/22 10:36 V18991TBL
0.005 J mg/Kg - dry 0.0007 0.011n-Hexane 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005
4-Isopropyl toluene 1 05/21/22 10:36 V18991TBL
0.049 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/21/22 10:36 V18991TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005
Styrene 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/21/22 10:36 V18991TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 05/21/22 10:36 V18991TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/21/22 10:36 V18991TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/21/22 10:36 V18991TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-5
90001 Matrix:
5/12/2022 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V18990 05/20/22 08:00
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/21/22 10:36 V18991TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/21/22 10:36 V18991TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/21/22 10:36 V18991TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 05/21/22 10:36 V18991TBL
0.0007 J mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/21/22 10:36 V18991TBL
<0.0005 mg/Kg - dry 0.0005 0.011
Vinyl Chloride 1 05/21/22 10:36 V18991TBL
0.003 J mg/Kg - dry 0.0006 0.005o-Xylene 1 05/21/22 10:36 V18991TBL
0.003 J mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/21/22 10:36 V18991TBL
0.006 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/21/22 10:36 V18991
Surrogate: 4-Bromofluorobenzene 99.5 Limits: 70-130%05/21/22 10:361 TBL V18991
Surrogate: Dibromofluoromethane 99.5 Limits: 84-123%05/21/22 10:361 TBL V18991
Surrogate: Toluene-d8 86.0 Limits: 76-129%05/21/22 10:361 TBL V18991
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-6
90002 Matrix:
5/12/2022 13:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
8.39 %Moisture 1 05/23/22 13:13 SW-DRYWTADC
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 36
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28409
22-137-0007
01024
ATC Group Services, LLC - Raleigh, NC
609A Piner Road Suite 115
Maureen Jackson
Wilminton
Received : 05/17/2022
Circle K 2720104
Report Date : 05/25/2022
Sample ID :
Lab No :
Sampled:D-6
90002 Matrix:
5/12/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8015C DRO Prep Batch(es):V18830 05/18/22 09:18
77.2 mg/Kg - dry 5.08 10.9Diesel Range Organics (C10-C28)1 05/20/22 06:57 V18982JLK
8015C DROSurrogate: OTP Surrogate 97.7 Limits: 31-123%05/20/22 06:571 JLK
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8015C GRO Prep Batch(es):V18833 05/18/22 08:00
5.64 mg/Kg - dry 2.26 5.46Gasoline Range Organics (C6-C10)50 05/18/22 14:37 V18834TBL
8015C GROSurrogate: a,a,a-Trifluorotoluene 130 Limits: 50-137%05/18/22 14:3750 TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Extractable
8015C DRO
V18982QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V18830
Associated Lab Samples: 90002
LRB-V18830 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/19/22 21:2410.04.65<4.65mg/KgDiesel Range Organics (C10-C28)
05/19/22 21:24OTP Surrogate (S)96.2 31-123
LCS-V18830Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10469.566.7mg/KgDiesel Range Organics (C10-C28)46-126
84.9OTP Surrogate (S)31-123
V 89767-MS-V18830 V 89767-MSD-V18830Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
291 -140*28266.666.6386mg/KgDiesel Range Organics (C10-C28)-140*50-117 3.1 24
70.9OTP Surrogate (S)67.3 31-123
Page 1 of 10* QC Fail Date:05/25/2022 02:51 PM
Page 25 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Total Petroleum Hydrocarbons - Volatile
8015C GRO
V18834QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V18833
Associated Lab Samples: 89999, 90000, 90001, 90002
LRB-V18833 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/18/22 12:455.002.07<2.07mg/KgGasoline Range Organics (C6-C10)
05/18/22 12:45a,a,a-Trifluorotoluene (S)129 50-137
LCS-V18833Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10452.050.0mg/KgGasoline Range Organics (C6-C10)41-138
128a,a,a-Trifluorotoluene (S)50-137
V 89999-MS-V18833 V 89999-MSD-V18833Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
59.4 11958.350.050.0<2.07mg/KgGasoline Range Organics (C6-C10)117 41-138 1.8 34
137a,a,a-Trifluorotoluene (S)135 50-137
Page 2 of 10Date:05/25/2022 02:51 PM
Page 26 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
Associated Lab Samples: 89999, 90000, 90001
LRB-V18990 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/21/22 02:170.0200.002<0.002mg/KgAcetone
05/21/22 02:170.0200.001<0.001mg/KgAcrolein
05/21/22 02:170.0200.0008<0.0008mg/KgAcrylonitrile
05/21/22 02:170.0050.0006<0.0006mg/KgBenzene
05/21/22 02:170.0050.0005<0.0005mg/KgBromobenzene
05/21/22 02:170.0050.0008<0.0008mg/KgBromochloromethane
05/21/22 02:170.0050.001<0.001mg/KgBromodichloromethane
05/21/22 02:170.0050.001<0.001mg/KgBromoform
05/21/22 02:170.0100.001<0.001mg/KgBromomethane
05/21/22 02:170.0050.0005<0.0005mg/Kgn-Butylbenzene
05/21/22 02:170.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/21/22 02:170.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/21/22 02:170.0050.0006<0.0006mg/KgCarbon Disulfide
05/21/22 02:170.0050.001<0.001mg/KgCarbon Tetrachloride
05/21/22 02:170.0050.0007<0.0007mg/KgChlorobenzene
05/21/22 02:170.0050.0009<0.0009mg/KgChlorodibromomethane
05/21/22 02:170.0100.0009<0.0009mg/KgChloroethane
05/21/22 02:170.0050.001<0.001mg/KgChloroform
05/21/22 02:170.0100.0006<0.0006mg/KgChloromethane
05/21/22 02:170.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/21/22 02:170.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/21/22 02:170.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/21/22 02:170.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/21/22 02:170.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/21/22 02:170.0050.0006<0.0006mg/KgDibromomethane
05/21/22 02:170.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/21/22 02:170.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 3 of 10Date:05/25/2022 02:51 PM
Page 27 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
Associated Lab Samples: 89999, 90000, 90001
LRB-V18990 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/21/22 02:170.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/21/22 02:170.0100.001<0.001mg/KgDichlorodifluoromethane
05/21/22 02:170.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/21/22 02:170.0050.001<0.001mg/Kg1,2-Dichloroethane
05/21/22 02:170.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/21/22 02:170.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/21/22 02:170.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/21/22 02:170.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/21/22 02:170.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/21/22 02:170.0050.001<0.001mg/Kg2,2-Dichloropropane
05/21/22 02:170.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/21/22 02:170.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/21/22 02:170.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/21/22 02:170.0050.0006<0.0006mg/KgEthylbenzene
05/21/22 02:170.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/21/22 02:170.0100.0008<0.0008mg/KgHexachlorobutadiene
05/21/22 02:170.0100.0007<0.0007mg/Kgn-Hexane
05/21/22 02:170.0200.0006<0.0006mg/Kg2-Hexanone
05/21/22 02:170.0050.0005<0.0005mg/KgIsopropylbenzene
05/21/22 02:170.0050.001<0.001mg/Kg4-Isopropyl toluene
05/21/22 02:170.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/21/22 02:170.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/21/22 02:170.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/21/22 02:170.0100.001<0.001mg/KgMethylene Chloride
05/21/22 02:170.0100.0010<0.0010mg/KgNaphthalene
05/21/22 02:170.0050.0005<0.0005mg/Kgn-Propylbenzene
05/21/22 02:170.0050.001<0.001mg/KgStyrene
Page 4 of 10Date:05/25/2022 02:51 PM
Page 28 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
Associated Lab Samples: 89999, 90000, 90001
LRB-V18990 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/21/22 02:170.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/21/22 02:170.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/21/22 02:170.0050.0009<0.0009mg/KgTetrachloroethene
05/21/22 02:170.0050.0007<0.0007mg/KgToluene
05/21/22 02:170.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/21/22 02:170.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/21/22 02:170.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/21/22 02:170.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/21/22 02:170.0050.0009<0.0009mg/KgTrichloroethene
05/21/22 02:170.0100.002<0.002mg/KgTrichlorofluoromethane
05/21/22 02:170.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/21/22 02:170.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/21/22 02:170.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/21/22 02:170.0100.0005<0.0005mg/KgVinyl Acetate
05/21/22 02:170.0100.0005<0.0005mg/KgVinyl Chloride
05/21/22 02:170.0050.0005<0.0005mg/Kgo-Xylene
05/21/22 02:170.0100.001<0.001mg/Kgm,p-Xylene
05/21/22 02:174-Bromofluorobenzene (S)104 70-130
05/21/22 02:17Dibromofluoromethane (S)105 84-123
05/21/22 02:17Toluene-d8 (S)86.8 76-129
LCS-V18990 LCSD-V18990Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.090 90.181.00.0810.100mg/KgAcetone 29-198 10.6 20
0.078 78.393.80.0930.100mg/KgAcrolein 70-130 18.0 20
Page 5 of 10Date:05/25/2022 02:51 PM
Page 29 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
LCS-V18990 LCSD-V18990Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.085 85.080.80.0800.100mg/KgAcrylonitrile 65-134 5.0 20
0.057 1151120.0550.050mg/KgBenzene 74-127 2.8 20
0.044 88.889.20.0440.050mg/KgBromobenzene 73-125 0.4 20
0.056 1131130.0560.050mg/KgBromochloromethane 72-134 0.5 20
0.060 1211150.0570.050mg/KgBromodichloromethane 75-122 4.7 20
0.047 94.091.80.0450.050mg/KgBromoform 66-135 2.3 20
0.054 1091050.0520.050mg/KgBromomethane 20-180 3.3 20
0.046 92.094.40.0470.050mg/Kgn-Butylbenzene 65-135 2.5 20
0.044 89.290.60.0450.050mg/Kgsec-Butyl benzene 66-131 1.5 20
0.043 87.288.60.0440.050mg/Kgtert-Butyl benzene 67-132 1.5 20
0.055 1121080.0540.050mg/KgCarbon Disulfide 61-129 3.2 20
0.054 1081070.0530.050mg/KgCarbon Tetrachloride 64-143 1.6 20
0.047 95.093.20.0460.050mg/KgChlorobenzene 74-118 1.9 20
0.047 94.293.00.0460.050mg/KgChlorodibromomethane 73-122 1.2 20
0.060 1201180.0590.050mg/KgChloroethane 33-149 1.8 20
0.057 1161120.0550.050mg/KgChloroform 73-127 3.5 20
0.042 84.087.80.0430.050mg/KgChloromethane 45-143 4.4 20
0.044 88.288.60.0440.050mg/Kg2-Chlorotoluene 67-124 0.4 20
0.045 90.291.60.0450.050mg/Kg4-Chlorotoluene 71-126 1.5 20
0.045 90.487.40.0430.050mg/KgDi-Isopropyl Ether (DIPE)59-159 3.3 20
0.040 81.481.60.0400.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 0.2 20
0.047 95.094.20.0470.050mg/Kg1,2-Dibromoethane 70-132 0.8 20
0.058 1171150.0570.050mg/KgDibromomethane 74-133 1.9 20
0.043 86.686.80.0430.050mg/Kg1,2-Dichlorobenzene 72-123 0.2 20
0.043 87.887.20.0430.050mg/Kg1,3-Dichlorobenzene 71-120 0.6 20
0.043 86.486.40.0430.050mg/Kg1,4-Dichlorobenzene 71-123 0.0 20
Page 6 of 10Date:05/25/2022 02:51 PM
Page 30 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
LCS-V18990 LCSD-V18990Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.057 1151120.0560.050mg/KgDichlorodifluoromethane 26-146 1.9 20
0.052 1041020.0510.050mg/Kg1,1-Dichloroethane 74-127 1.5 20
0.053 1071040.0510.050mg/Kg1,2-Dichloroethane 68-128 2.8 20
0.047 95.894.20.0470.050mg/Kg1,1-Dichloroethene 67-149 1.6 20
0.049 99.696.00.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 3.6 20
0.048 97.693.80.0460.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.9 20
0.052 1051010.0500.050mg/Kg1,2-Dichloropropane 73-130 4.6 20
0.046 93.692.00.0460.050mg/Kg1,3-Dichloropropane 75-124 1.7 20
0.057 1141120.0550.050mg/Kg2,2-Dichloropropane 50-142 2.1 20
0.055 1101080.0540.050mg/Kg1,1-Dichloropropene 71-130 1.8 20
0.057 1151110.0550.050mg/Kgcis-1,3-Dichloropropene 71-125 2.8 20
0.056 1131100.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.5 20
0.047 95.094.60.0470.050mg/KgEthylbenzene 74-128 0.4 20
0.097 97.092.60.0920.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 4.6 20
0.041 83.687.20.0430.050mg/KgHexachlorobutadiene 64-125 4.2 20
0.057 1151100.0540.050mg/Kgn-Hexane 70-130 4.6 20
0.031 62.862.80.0310.050mg/Kg2-Hexanone 61-157 0.0 20
0.044 89.890.40.0450.050mg/KgIsopropylbenzene 68-126 0.6 20
0.044 88.089.60.0440.050mg/Kg4-Isopropyl toluene 68-129 1.8 20
0.049 99.493.40.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 6.2 20
0.052 10498.80.0490.050mg/KgMethyl tert-butyl ether (MTBE)70-130 5.1 20
0.042 84.079.80.0390.050mg/Kg4-Methyl-2-Pentanone 57-162 5.1 20
0.045 90.290.80.0450.050mg/KgMethylene Chloride 74-129 0.6 20
0.043 87.687.20.0430.050mg/KgNaphthalene 57-157 0.4 20
0.046 93.694.20.0470.050mg/Kgn-Propylbenzene 67-130 0.6 20
0.048 96.896.60.0480.050mg/KgStyrene 77-121 0.2 20
Page 7 of 10Date:05/25/2022 02:51 PM
Page 31 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V18991QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V18990
LCS-V18990 LCSD-V18990Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.048 96.495.40.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.043 86.685.00.0420.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.8 20
0.054 1101080.0540.050mg/KgTetrachloroethene 68-130 1.4 20
0.056 1131110.0550.050mg/KgToluene 71-129 2.5 20
0.042 84.685.00.0420.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.4 20
0.042 85.085.80.0420.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.9 20
0.058 1161110.0550.050mg/Kg1,1,1-Trichloroethane 67-131 4.9 20
0.047 95.294.00.0470.050mg/Kg1,1,2-Trichloroethane 70-133 1.2 20
0.056 1131110.0550.050mg/KgTrichloroethene 75-133 1.7 20
0.051 1041050.0520.050mg/KgTrichlorofluoromethane 44-146 0.9 20
0.042 85.084.40.0420.050mg/Kg1,2,3-Trichloropropane 60-137 0.7 20
0.043 87.288.80.0440.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.8 20
0.044 89.290.60.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 1.5 20
0.048 97.893.80.0460.050mg/KgVinyl Acetate 60-140 4.1 20
0.047 95.295.00.0470.050mg/KgVinyl Chloride 48-147 0.2 20
0.047 95.695.20.0470.050mg/Kgo-Xylene 74-126 0.4 20
0.096 96.296.60.0960.100mg/Kgm,p-Xylene 75-124 0.4 20
1001014-Bromofluorobenzene (S)70-130
101101Dibromofluoromethane (S)84-123
87.286.2Toluene-d8 (S)76-129
Page 8 of 10Date:05/25/2022 02:51 PM
Page 32 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V18847QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V18846
Associated Lab Samples: 89999
LRB-V18846 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/18/22 17:418.001.22<1.22mg/KgAliphatic C5-C8
05/18/22 17:418.004.56<4.56mg/KgAliphatic C9-C12
05/18/22 17:418.000.624<0.624mg/KgAromatic C9-C10
05/18/22 17:412,5-Dibromotoluene (FID) (S)84.0 70-130
05/18/22 17:412,5-Dibromotoluene (PID) (S)96.2 70-130
LCS-V18846 LCSD-V18846Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
33.7 10510333.032.0mg/KgAliphatic C5-C8 70-130 2.0 50
34.9 10911336.132.0mg/KgAliphatic C9-C12 70-130 3.3 50
12.6 11811912.710.7mg/KgAromatic C9-C10 70-130 0.7 50
85.886.92,5-Dibromotoluene (FID) (S)70-130
86.594.32,5-Dibromotoluene (PID) (S)70-130
Page 9 of 10Date:05/25/2022 02:51 PM
Page 33 of 36
Quality Control Data
22-137-0007Report No:
Project Description:
Client ID:ATC Group Services, LLC - Raleigh, NC
Circle K 2720104
Dry Weight Determination
SW-DRYWT
V19044QC Analytical Batch:
Analysis Method:
Analysis Description:
V 89998-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/23/22 13:130.89.839.75%Moisture
V 90064-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 05/23/22 13:130.517.917.8%Moisture
Page 10 of 10Date:05/25/2022 02:51 PM
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Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-137-0007
ATC Group Services, LLC - Raleigh, NC
01024
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 3.0 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:05/17/2022 14:59:08
Special precautions or instructions included?
Comments:
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