MO-29071_48256_CA_IAR_20221122

Additional Abatement Actions for UST ID No. 2
Charlotte Rescue Mission
907 West 1st Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211506
PREPARED FOR:
Charlotte Rescue Mission
907 West 1st Street
Charlotte, North Carolina 28202
PREPARED BY:
S&ME, Inc.
2016 Ayrsley Town Boulevard, Suite 2-A
Charlotte, North Carolina 28273
November 22, 2022

S&ME, Inc. | 2016 Ayrsley Town Boulevard Suite 2-A | Charlotte, NC 28273 | p 704.523.4726 | www.smeinc.com

November 22, 2022
Charlotte Rescue Mission
907 West 1st Street
Charlotte, North Carolina 28202
Attention: Mr. Ed Price via email: [e-mail]
Reference: Additional Abatement Actions - UST ID No. 2
Charlotte Rescue Mission
907 West 1st Street
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211506
S&ME, Inc. Engineering License Certification No. F-0176
Dear Mr. Price:
S&ME, Inc. (S&ME) is submitting this Additional Abatement Actions Report for the Charlotte Rescue Mission
located at 907 West 1st Street in Charlotte, Mecklenburg County, North Carolina. S&ME’s services were conducted
in general accordance with S&ME Proposal No. 211506I dated March 21, 2022. S&ME appreciates the
opportunity to provide environmental services for this project. Please contact us at your convenience if there are
questions regarding the information contained in this document.
Sincerely,
S&ME, Inc.
John L. Sherrill, P.G. Carl Hewett
Project Geologist Project Manager / Group Leader

Senior Reviewed by Wayne Watterson, P.E., Group Leader/Senior Project Manager

cc: Mr. Dan Bowser
North Carolina Department of Environmental Quality
Division of Waste Management, UST Section
Mooresville Regional Office
610 East Center Avenue
Mooresville, North Carolina 28115

Additional Abatement Actions - UST ID No. 2
Charlotte Rescue Mission
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211506
NCDEQ Incident No. 48256
November 22, 2022 ii
Table of Contents
1.0 Site Information ................................................................................................................ 1
1.1 Site Identification ............................................................................................................................ 1
1.2 Information about Contacts Associated with the Leaking UST System ................................. 1
1.3 Information about the Release ...................................................................................................... 1
1.4 Certification ..................................................................................................................................... 1
2.0 Scope of Services ............................................................................................................... 2
3.0 Background ........................................................................................................................ 2
3.1 Property Information ..................................................................................................................... 2
3.2 Project Background ........................................................................................................................ 2
4.0 Site History and Characterization ................................................................................. 2
4.1 UST Information ............................................................................................................................. 2
4.2 UST Owner and Operator Information ....................................................................................... 3
4.3 Site Characteristics ......................................................................................................................... 3
5.0 Additional Abatement Actions ...................................................................................... 4
5.1 Excavation of Contaminated Soil ................................................................................................. 4
5.2 Sample Collection ........................................................................................................................... 4
5.3 UST Closure Soil Analytical Results ............................................................................................ 4
6.0 Free Product ........................................................................................................................ 5
7.0 Sole Use Statement ........................................................................................................... 5
8.0 Limitations.......................................................................................................................... 5
9.0 Conclusions and Recommendations ............................................................................. 5

Appendices
Appendix I – Figures
Appendix II – Tables
Appendix III – Soil Disposal Manifest
Appendix IV – Soil Analytical Laboratory Report

Additional Abatement Actions - UST ID No. 2
Charlotte Rescue Mission
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211506
NCDEQ Incident No. 48256
November 22, 2022 2
2.0 Scope of Services
The scope of services for this project included over excavation of contaminated soils in the vicinity of
underground storage tank (UST)-2, which was removed from the site on November 30, 2022, the collection of
confirmation soil samples from the excavation limits, and the reporting herein. The removal date and location of
the former dispensers is unknown.
3.0 Background
3.1 Property Information
According to the Mecklenburg County Property Ownership and Land Records System (POLARIS) website, the
subject property is located on a 1.99-acre parcel owned by the Charlotte Rescue Mission, and it is identified as
Mecklenburg County tax parcel 0732-4217. The subject property is developed with office buildings and
dormitories, and it is utilized as a rehabilitation center and donation center. The Charlotte Rescue Mission
purchased the subject property in 1959. Prior to 1959, the subject property operated as a petroleum distribution
facility owned by Standard Oil, Humble Oil, Esso, and Exxon at various times. A Vicinity Map (Figure 1) and Site
Map (Figure 2) are included in Appendix I. The vicinity of the subject property is comprised of commercial and
multi-family residential buildings.
3.2 Project Background
A Geophysical Survey previously conducted by S&ME at the subject property identified two orphan USTs of
unknown size and contents on the south side of the property. Following the identification of the two orphan
USTs, S&ME was contracted to oversee the removal of the two tanks. The USTs, (UST-1 and UST-2), were removed
on November 30, 2022. Soil samples collected during the closure activities confirmed that a release had occurred.
Over excavation was performed at UST-2, and naphthalene was detected in the confirmation sample along the
southern sidewall (sample ID UST-2-SW4) indicated the presence of several petroleum constituents at
concentrations above the residential Maximum Soil Contaminant Concentration (MSCC). Naphthalene was
detected in excess of the Industrial/Commercial MSCC.
S&ME’s services herein were conducted in general accordance with S&ME Proposal No. 211506I dated March 21,
2022.
4.0 Site History and Characterization
4.1 UST Information
Information regarding the former USTs is presented in Table 4-1.

Additional Abatement Actions - UST ID No. 2
Charlotte Rescue Mission
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211506
NCDEQ Incident No. 48256
November 22, 2022 3

Table 4-1: UST System Information
UST ID
Number
Capacity
(gallons) Contents Construction
Details
Tank
Dimensions
(Length x
Diameter)
Use Date Tank
Installed
Status of
UST
Release
Observed?
1 1,000 Unknown Single-wall steel 128” x 48” Unknown Unknown Removed
(11/30/2021) Yes
2 1,000 Unknown Single-wall steel 128” x 48” Unknown Unknown Removed
(11/30/2021) Yes
4.2 UST Owner and Operator Information
Charlotte Rescue Mission does not own or operate the USTs. The former owner and operator is unknown.
4.3 Site Characteristics
 Land Use: The site is currently developed as a rehabilitation center and donation center. The property is
zoned as MUDD (mixed use development district).

 Land Use of Surrounding Area: The site is located in the Uptown area of Charlotte, North Carolina. The
surrounding adjoining properties are zoned as MUDD and UR (urban residential).

 Topography: Based upon the topographic map reviewed (Figure 1, Appendix I), the area of the subject
property slopes downward to the west.

 Surface Water: The nearest downgradient surface water body is an unnamed tributary to Irwin Creek
located approximately 350 feet south of the release location.

 Regional Geology: The property lies within the Charlotte Belt Geologic Province of North Carolina, and it
is underlain by metamorphosed quartz diorite.

 Potential Receptors: Based on-site observations, no water supply wells were observed in the vicinity of
the subject property. Charlotte Mecklenburg Utility provides water to the site and is available to
surrounding properties.

Additional Abatement Actions - UST ID No. 2
Charlotte Rescue Mission
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211506
NCDEQ Incident No. 48256
November 22, 2022 4
5.0 Additional Abatement Actions
5.1 Excavation of Contaminated Soil
On April 5, 2022, S&ME observed CCI conduct the additional excavation activities on the former UST-2 basin.
Using a track-mounted excavator, CCI located the edge of the previous sidewall as excavated on November 30,
2021 during the UST-2 closure activities. The northwest sidewall of UST-2 excavation was over-excavated to a
width of approximately 4 feet wide by approximately 12 feet long feet. The base of the excavation was
approximately 6 feet BGS. Stained soils were observed beginning at a depth of approximately 3 feet BGS. Over-
excavation activities were limited by space concerns and a loading dock area. Groundwater was not encountered
during excavation. The excavated materials were loaded directly into a dump-truck and hauled offsite for disposal
at the Davidson County Landfill in Lexington, North Carolina. The waste manifest for the soils is included in
Appendix III.
The approximate limits of the over-excavation for the basin of UST-2 are shown on Figure 2, Appendix I.
5.2 Sample Collection
S&ME collected soil sample UST-2-SW4-B from the northwest sidewall of the new UST-2 excavation, at a depth of
approximately 6 feet BGS. S&ME screened the soil sample for VOCs with a calibrated MiniRAE 3000 PID. The PID
reading for the confirmation soil sample was 298 ppm. After collection of the confirmation soil sample, the new
excavation area at UST-2 was backfilled using clean, imported soil.
Closure soil sample UST-2-SW4-B was collected approximately 6 foot BGS and was placed in laboratory-supplied
containers, placed in an ice-filled cooler, and shipped under chain of custody procedures to Pace of Huntersville
North Carolina for analysis of Extractable Petroleum Hydrocarbons (EPH) and Volatile Petroleum Hydrocarbons
(VPH) by the Massachusetts Department of Environmental Protection (MADEP) Method, volatile organic
compounds (VOCs) by EPA Method 8260 and semi-volatile organic compounds (SVOCs) by EPA Method 8270.
5.3 UST Closure Soil Analytical Results
Analytical testing for confirmation soil sample UST-2-SW4-B indicated the presence of VOCs, SVOCs and aliphatic
and aromatic ranges at concentrations in excess of their applicable Maximum Soil Contaminant Concentrations
(MSCCs). The analytes detected above their applicable Soil-to-Groundwater MSCCs are as follows:
 VOCs – n-Butylbenzene, sec-Butylbenzene, tert-Butylbenzene, methylene chloride, 4-methyl-2-
pentanone (MIBK), naphthalene, and n-Propylbenzene.
 SVOCs – 1-methylnaphthalene, 2-methylnaphthalene, naphthalene and phenanthrene.
 EPHs and VPHs – C9-C18 Aliphatics and C9-C22 Aromatics.

Additional Abatement Actions - UST ID No. 2
Charlotte Rescue Mission
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211506
NCDEQ Incident No. 48256
November 22, 2022 5
The following analytes were also reported above the NCDEQ Residential Soil Cleanup Levels
 VOCs – Naphthalene
 EPHs and VPHs – C9-C18 Aliphatics and C9-C22 Aromatics.

No analytes were reported above the Industrial/Commercial MSCCs.
A summary of the analytical results is included in Table 1, Appendix II. The laboratory report is included in
Appendix VI.
6.0 Free Product
Groundwater was not encountered during the UST closure activities performed on April 5, 2022.
7.0 Sole Use Statement
Materials and information used for this project were obtained by S&ME. This report is provided for the sole use of
the Charlotte Rescue Mission. Use of this report by any parties other than the Charlotte Rescue Mission will be at
such party's sole risk. S&ME disclaims liability for any use of or reliance on this report by third parties.
8.0 Limitations
The assessment described herein represents the environmental conditions of the property at the date the samples
were collected for laboratory analysis. The assessment data does not represent the future environmental
conditions of the property and should not be construed in this manner.
9.0 Conclusions and Recommendations
The following summarizes the documented release and initial abatement actions for the Charlotte Rescue Mission
property during November 2021 and April 2022:
 Additional abatement actions were performed on the northwest sidewall of UST-2 on April 5, 2022.
 Petroleum odors and elevated PID readings were noted during excavation activities, and during the
collection of soil sample UT-2-SW4-B on April 5, 2022.
 Approximately 14.47 tons of petroleum-impacted soils from the northwest sidewall of the UST-2 basin
were transported off site for disposal at the Davidson County Landfill on April 6, 2022.
 Several VOC and SVOC target analytes were detected in soil sample UST-2-SW4-B at concentrations
that exceed the Soil-to-Water MSCCs.
 Naphthalene (as a VOC), C9-C18 Aliphatics, and C9-C22 Aromatics were detected in soil sample
UST-2-SW4-B above their applicable NCDEQ Residential MSCC.
Additional Abatement Actions - UST ID No. 2
Charlotte Rescue Mission
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 211506
NCDEQ Incident No. 48256
November 22, 2022 6
 Naphthalene (both as a VOC and SVOC) was reported above its applicable NCDEQ
Industrial/Commercial MSCC of 27 mg/kg in soil sample UST-2-SW4, collected in November 2021, at
concentrations of 85.5 mg/kg (VOC) and 28.6 mg/kg (SVOC) from the UST-2 basin. Sample UST-2-SW4-
B collected on April 5, 2022 exhibited concentrations of naphthalene (as a VOC and SVOC) at
concentrations of 12.8 mg/kg (VOC) and 4.5 mg/kg (SVOC), an approximately 85% decrease in
concentration from the sample collected in November 2021.

S&ME understands that the Charlotte Rescue Mission did not own or operate the three USTs removed from the
subject property. The petroleum distributorship on the subject property was previously operated by Standard Oil,
Humble Oil, Esso, and Exxon, and maybe other companies.

Appendices

Appendix I – Figures
^_
^_PROJECT LOCATION
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
11 " = 2,000 '
7-14-22Drawing Path: T:\ENV\Projects\2021\211506_Charlotte_Rescue_Mission_Due_Diligence_Services\Phase 454 - Limited Site Assessment\GIS\1_TOPO VICINITY.mxd plotted by DHomans 07-14-2022TOPOGRAPHIC VICINITY MAP
³
REFERENCE: USGS USA TOPO STREAMING DATASETGIS BASE LAYERS WERE OBTAINED FROM USGS NATIONAL MAP. THIS MAP IS FOR INFORMATIONALPURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASEDON CIVIL SURVEY INFORMATION, UNLESS STATED OTHERWISE.
Service Layer Credits: USGS The National Map: NationalBoundaries Dataset, 3DEP Elevation Program, GeographicNames Information System, National Hydrography
0 2,000 4,000(FEET)
211506
CHARLOTTE RESCUE MISSION907 WEST 1ST STREETCHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
E"J
E"J
E"J
E"J
E"J
E"J
E"J
E"J
E"J
E"J
E"J
UST-1-A (@7' BGS) TPH-DRO: 2,810TPH-GRO: 34.8
UST-1-B (@7' BGS) TPH-DRO: 3,730TPH-GRO: 53.2
UST-2-A (@6.6' BGS) TPH-DRO: 23,000TPH-GRO: 67.2
UST-2-B (@6.6' BGS) TPH-DRO: 9,240TPH-GRO: 247
UST-2-A2 (@8' BGS) sec-Butylbenzene: 2.4Methylene Chloride: 0.097Naphthalene: 14.1/6.41-Methylnaphthalene: 15.32-Methylnaphthalene: 22.9C9-C18 Aliphatics: 3,551C9-C22 Aromatics: 1,222 UST-2-B2 (@8' BGS) sec-Butylbenzene: 4.6Naphthalene: 17.6/7.61-Methylnaphthalene: 15.32-Methylnaphthalene: 22.9C9-C18 Aliphatics: 7,859C9-C22 Aromatics: 1,402
UST-2-SW1 (@6' BGS) n-Butylbenzene: 2.8sec-Butylbenzene: 2.3Methylene Chloride: 0.10Naphthalene: 7.91-Methylnaphthalene: 13.12-Methylnaphthalene: 11.6C9-C18 Aliphatics: 5,483.3C9-C22 Aromatics: 1,579.2
UST-2-SW2 (@6' BGS) Naphthalene: 0.61C9-C22 Aromatics: 79.7
UST-2-SW3 (@6' BGS) Methylene Chloride: 0.090Naphthalene: 4.1/0.821-Methylnaphthalene: 1.82-Methylnaphthalene: 2.7C9-C18 Aliphatics: 1,005.8C9-C22 Aromatics: 308
UST-2-SW4 (@6' BGS) sec-Butylbenzene: 13.1Isopropylbenzene: 2.5Naphthalene: 85.5/28.61-Methylnaphthalene: 53.02-Methylnaphthalene: 75.5C9-C18 Aliphatics: 15,956C9-C22 Aromatics: 2,885
UST-2-SW4-B (@6' BGS) n-Butylbenzene: 3.3sec-Butylbenzene: 2.4Naphthalene: 12.8/4.5n-Propylbenzene: 1.81-Methylnaphthalene: 21.62-Methylnaphthalene: 30.9Phenanthrene: 5.7C9-C18 Aliphatics: 2,851C9-C22 Aromatics: 4,066
E"J CLOSURE SAMPLE
E"J CONFIRMATION SAMPLE
UST (REMOVED)
11/30/2021 EXCAVATION EXTENT
4/5/2022 EXCAVATION EXTENT
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO
.2
1 " = 10 '
9-29-22
211506C
CHARLOTTE RESCUE MISSION907 WEST 1ST STREETCHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINADrawing Path: T:\ENV\Projects\2021\211506_Charlotte_Rescue_Mission_Due_Diligence_Services\Phase 453 - UST Removal Project\1 - November 2021 - UST Removal\GIS\4_Soil_Quality_Map.mxd plotted by jsherrill 09-29-2022SOIL QUALITY MAP
³
NOTES:BGS= Below Ground Surface
Closure samples were assessed for total petroleum hydrocarbons (TPH)diesel range organics (DRO) and gasoline range organics (GRO).Concentrations exceeding the North Carolina Underground StorageTank (UST) Action Level are shown above in milligrams per kilogram(mg/kg).
Over-excavation samples were assessed for volatile organic compounds(VOCs), semi-volatile organic compounds (SVOCs), volatile petroleumhydrocarbons (VPH), and extractable petroleum hydrocarbons (EPH).Concentrations exceeding the North Carolina Soi-to-GroundwaterMaximum Soil Contaminant Concentration Levels (MSCCs) are shownabove in mg/kg.Concentrations exceeding the Residential MSCCs are shown in BoldConcentrations exceeding the Industrial/Commercial MSCCs areshown in Red.TPH concentrations exceeding the NCDEQ Action Limit are shown in
0 10 20(FEET)

Appendix II – Tables
Sample ID Location
Date
Collected
PID
Screening
Result
(ppm)
Sample
Depth
(ft-bgs)TolueneC9-C-22 AromaticsUST-2-A2 North side of UST 2 11/30/2021 215.3 8 ft < 0.016 2.4 0.19 0.039 0.43 0.097 <0.16 14.1 0.50 0.048 15.3 22.9 6.4 < 3.9 41.8 3,551 560 1,222
UST-2-B2 South side of UST 2 11/30/2021 348.0 8 ft < 0.029 4.6 0.35 0.040 0.91 < 0.12 <0.29 17.6 0.98 < 0.029 18.9 25.8 7.6 < 3.8 47.4 7,859 1400 1,402
UST-2-SW1 NE wall of UST 2 11/30/2021 170.2 6 ft 2.8 2.3 0.35 0.053 0.71 0.10 <0.14 7.9 1.0 < 0.014 13.1 11.6 < 3.9 4.3 26.1 5,483.3 1100 1,579.2
UST-2-SW2 SE wall of UST 2 11/30/2021 157.9 6 ft < 0.0064 0.14 < 0.0064 < 0.0064 0.012 < 0.026 <0.064 0.61 0.012 < 0.0064 0.42 0.63 < 0.40 < 0.40 < 3.8 245 38 79.7
UST-2-SW3 SW wall of UST 2 11/30/2021 183.4 6 ft < 0.014 0.94 0.067 < 0.014 0.13 0.090 <0.14 4.1 0.13 < 0.014 1.8 2.7 0.82 < 0.41 12.2 1,005.8 130 308
UST-2-SW4 NW wall of UST 2 11/30/2021 263.5 6 ft < 0.12 13.1 0.89 0.17 2.5 < 0.48 <1.2 85.5 2.4 0.13 53.0 75.5 28.6 < 7.9 20.7 15,956 1600 2,885
UST-2-SW4-B Additional excavation,
NW wall of UST 2 4/5/2022 298 6 ft 3.3 2.4 0.28 0.066 1.0 0.32 0.91 12.8 1.8 <0.036 21.6 30.9 4.5 5.7 53.5 2,851 349 4,066
2.4 2.2 1.7 8 1.3 0.023 0.42 0.2 1.4 5.4 0.054 1.5 0.2 64 68 540 NS-#31
782 1,560 1,560 60.3 1,560 93.8 1,250 5.5 1,560 1,250 22.8 62.5 5.5 469 625 1,560 31,200 467
11,600 23,300 23,300 297 23,300 1,400 18,600 27 23,300 18,600 112 934 27 7,000 9,340 23,300 467,000 7,000
NS = No standard established
NS-# = No standard due to immobile substance
NA = Not analyzed
VPH = Voliatile Petroleum Hydrocarbons
EPH = Extractable Petroleum Hydrocarbons
PID = Photoionization Detector
Guidelines: North Carolina Department of Environmental Quality, Division of Waste Management, UST Section
All concentrations are reported in milligrams per kilogram (mg/kg)
Concentrations exceeding the laboratory detection limits are BOLD.
Concentrations exceeding the State Action Levels and/or Soil-to-Water MSCC's are highlighted in yellow
Concentrations exceeding the Residential Soil Cleanup Level MSCC's are highlighted in orange
Concentrations exceeding the Industrial/Commerical Soil Cleanup Level MSCC's are highlighted in red
Industrial/Commercial Soil Cleanup Levels
Analysis
Constituent
Soil-to-Water Maximum Contaminant Concentration (MSCC's)
Residential Soil Cleanup Levels n-ButylbenzeneNaphthalenen-PropylbenzeneMethylene Chloridesec-Butylbenzenetert-ButylbenzeneIsopropylbenzene (Cumene)4-Methyl-2-pentanone (MIBK)Semi-volatile Organic Compounds by
EPA Method 8270E
2-MethylnaphthaleneNaphthalenePhenanthrene1-MethylnapthaleneTABLE 1
Summary of Soil Sampling Results
Charlotte Rescue Mission
907 W 1st Street
Charlotte, Mecklenburg County, North Carolina
Comprehensive Tables For Corrective Action Guidelines, dated September 7, 2022
EPH and VPH by MADEP Method
S&ME Project No. 211506
C5 - C8 AliphaticsC19-C36 AliphaticsC9 - C18 Aliphatics Volatile Organic Compounds by EPA Method 8260D Ethylbenzene

Appendix III – Soil Disposal Manifest

Appendix IV – Soil Analytical Laboratory Report
#=CL#
April 19, 2022
LIMS USE: FR - SARAH TAYLOR
LIMS OBJECT ID: 92597264
92597264
Project:
Pace Project No.:
RE:
Sarah Taylor
S&ME, Inc.
9751 Southern Pine Boulevard
Charlotte, NC 28273
CRM UST REMOVAL 2
Dear Sarah Taylor:
Enclosed are the analytical results for sample(s) received by the laboratory on April 05, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 37
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 37
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92597264001 DISPENSER-1 EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CMAD
SW-846 1 PASI-CKDF
92597264002 UST-3-A EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CMAD
SW-846 1 PASI-CKDF
92597264003 UST-3-B EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CMAD
SW-846 1 PASI-CKDF
92597264004 UST-2-SW4-B MADEP EPH 8 PANDMG, JN
MADEP VPH 5 PASI-CMAD
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Sample:DISPENSER-1 Lab ID:92597264001 Collected:04/05/22 11:40 Received:04/05/22 14:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)59.1 mg/kg 04/07/22 10:0804/07/22 00:285.8 1
Surrogates
n-Pentacosane (S)70 %04/07/22 10:08 629-99-204/07/22 00:2810-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 04/07/22 05:5604/06/22 15:147.0 1
Surrogates
4-Bromofluorobenzene (S)89 %04/07/22 05:56 460-00-404/06/22 15:1466-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.0 %04/06/22 15:25 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Sample:UST-3-A Lab ID:92597264002 Collected:04/05/22 12:05 Received:04/05/22 14:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)3490 mg/kg 04/07/22 12:2804/07/22 00:2863.9 10
Surrogates
n-Pentacosane (S)0 %04/07/22 12:28 629-99-2 S404/07/22 00:2810-130 10
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)4850 mg/kg 04/07/22 11:1304/06/22 15:1419020
Surrogates
4-Bromofluorobenzene (S)123 %04/07/22 11:13 460-00-404/06/22 15:1466-130 20
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.5 %04/06/22 15:25 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Sample:UST-3-B Lab ID:92597264003 Collected:04/05/22 12:20 Received:04/05/22 14:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)1100 mg/kg 04/07/22 12:2804/07/22 00:2825.7 4
Surrogates
n-Pentacosane (S)79 %04/07/22 12:28 629-99-204/07/22 00:2810-130 4
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)1900 mg/kg 04/07/22 10:1604/06/22 15:1443.8 5
Surrogates
4-Bromofluorobenzene (S)168 %04/07/22 10:16 460-00-4 S204/06/22 15:1466-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.2 %04/06/22 15:25 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Sample:UST-2-SW4-B Lab ID:92597264004 Collected:04/05/22 13:45 Received:04/05/22 14:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MA DEP/NJ DEP
Pace National - Mt. Juliet
TPH by Method MADEPE
Aliphatic (C09-C18)2540 mg/kg 04/15/22 07:5804/11/22 08:4180.2 10
Aliphatic (C19-C36)349 mg/kg 04/12/22 14:5004/11/22 08:418.02 1
Aromatic (C11-C22)878 mg/kg 04/14/22 03:2904/11/22 08:4140.1 5
Total Extractable Hydrocarbons 3770 mg/kg 04/15/22 07:58 TPH-TEH04/11/22 08:4180.2 10
Surrogates
o-Terphenyl (S)0.00 %04/14/22 03:29 84-15-1 SR04/11/22 08:4140.0-140 5
1-Chloro-octadecane (S)35.3 %04/12/22 14:50 3386-33-2 SR04/11/22 08:4140.0-140 1
1-Chloro-octadecane (S)28.2 %04/15/22 07:58 3386-33-2 SR04/11/22 08:4140.0-140 10
2-Fluorobiphenyl (S)0.00 %04/14/22 03:29 321-60-8 SR04/11/22 08:4140.0-140 5
2-Bromonaphthalene (S)0.00 %04/14/22 03:29 580-13-2 SR04/11/22 08:4140.0-140 5
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Soil
Aliphatic (C05-C08)53.5 mg/kg 04/18/22 21:33 N204/18/22 12:254.2 1
Aliphatic(C09-C12) Adjusted 311 mg/kg 04/18/22 21:33 N204/18/22 12:254.2 1
Aromatic (C09-C10)296 mg/kg 04/18/22 21:33 N204/18/22 12:254.2 1
Surrogates
4-Bromofluorobenzene (FID) (S)343 %04/18/22 21:33 460-00-4 S504/18/22 12:2570-130 1
4-Bromofluorobenzene (PID) (S)147 %04/18/22 21:33 460-00-4 S504/18/22 12:2570-130 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 04/07/22 16:18 83-32-904/06/22 04:294.2 10
Acenaphthylene ND mg/kg 04/07/22 16:18 208-96-804/06/22 04:294.2 10
Aniline ND mg/kg 04/07/22 16:18 62-53-304/06/22 04:294.2 10
Anthracene ND mg/kg 04/07/22 16:18 120-12-704/06/22 04:294.2 10
Benzo(a)anthracene ND mg/kg 04/07/22 16:18 56-55-304/06/22 04:294.2 10
Benzo(a)pyrene ND mg/kg 04/07/22 16:18 50-32-804/06/22 04:294.2 10
Benzo(b)fluoranthene ND mg/kg 04/07/22 16:18 205-99-204/06/22 04:294.2 10
Benzo(g,h,i)perylene ND mg/kg 04/07/22 16:18 191-24-204/06/22 04:294.2 10
Benzo(k)fluoranthene ND mg/kg 04/07/22 16:18 207-08-904/06/22 04:294.2 10
Benzoic Acid ND mg/kg 04/07/22 16:18 65-85-004/06/22 04:2921.0 10
Benzyl alcohol ND mg/kg 04/07/22 16:18 100-51-604/06/22 04:298.4 10
4-Bromophenylphenyl ether ND mg/kg 04/07/22 16:18 101-55-304/06/22 04:294.2 10
Butylbenzylphthalate ND mg/kg 04/07/22 16:18 85-68-704/06/22 04:294.2 10
4-Chloro-3-methylphenol ND mg/kg 04/07/22 16:18 59-50-704/06/22 04:298.4 10
4-Chloroaniline ND mg/kg 04/07/22 16:18 106-47-8 IL04/06/22 04:298.4 10
bis(2-Chloroethoxy)methane ND mg/kg 04/07/22 16:18 111-91-104/06/22 04:294.2 10
bis(2-Chloroethyl) ether ND mg/kg 04/07/22 16:18 111-44-404/06/22 04:294.2 10
2-Chloronaphthalene ND mg/kg 04/07/22 16:18 91-58-704/06/22 04:294.2 10
2-Chlorophenol ND mg/kg 04/07/22 16:18 95-57-804/06/22 04:294.2 10
4-Chlorophenylphenyl ether ND mg/kg 04/07/22 16:18 7005-72-304/06/22 04:294.2 10
Chrysene ND mg/kg 04/07/22 16:18 218-01-904/06/22 04:294.2 10
Dibenz(a,h)anthracene ND mg/kg 04/07/22 16:18 53-70-304/06/22 04:294.2 10
Dibenzofuran ND mg/kg 04/07/22 16:18 132-64-904/06/22 04:294.2 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Sample:UST-2-SW4-B Lab ID:92597264004 Collected:04/05/22 13:45 Received:04/05/22 14:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1,2-Dichlorobenzene ND mg/kg 04/07/22 16:18 95-50-104/06/22 04:294.2 10
1,3-Dichlorobenzene ND mg/kg 04/07/22 16:18 541-73-104/06/22 04:294.2 10
1,4-Dichlorobenzene ND mg/kg 04/07/22 16:18 106-46-704/06/22 04:294.2 10
3,3'-Dichlorobenzidine ND mg/kg 04/07/22 16:18 91-94-1 IL04/06/22 04:298.4 10
2,4-Dichlorophenol ND mg/kg 04/07/22 16:18 120-83-204/06/22 04:294.2 10
Diethylphthalate ND mg/kg 04/07/22 16:18 84-66-204/06/22 04:294.2 10
2,4-Dimethylphenol ND mg/kg 04/07/22 16:18 105-67-904/06/22 04:294.2 10
Dimethylphthalate ND mg/kg 04/07/22 16:18 131-11-304/06/22 04:294.2 10
Di-n-butylphthalate ND mg/kg 04/07/22 16:18 84-74-204/06/22 04:294.2 10
4,6-Dinitro-2-methylphenol ND mg/kg 04/07/22 16:18 534-52-104/06/22 04:298.4 10
2,4-Dinitrophenol ND mg/kg 04/07/22 16:18 51-28-504/06/22 04:2921.0 10
2,4-Dinitrotoluene ND mg/kg 04/07/22 16:18 121-14-204/06/22 04:294.2 10
2,6-Dinitrotoluene ND mg/kg 04/07/22 16:18 606-20-204/06/22 04:294.2 10
Di-n-octylphthalate ND mg/kg 04/07/22 16:18 117-84-004/06/22 04:294.2 10
bis(2-Ethylhexyl)phthalate ND mg/kg 04/07/22 16:18 117-81-704/06/22 04:294.2 10
Fluoranthene ND mg/kg 04/07/22 16:18 206-44-004/06/22 04:294.2 10
Fluorene ND mg/kg 04/07/22 16:18 86-73-704/06/22 04:294.2 10
Hexachloro-1,3-butadiene ND mg/kg 04/07/22 16:18 87-68-304/06/22 04:294.2 10
Hexachlorobenzene ND mg/kg 04/07/22 16:18 118-74-104/06/22 04:294.2 10
Hexachlorocyclopentadiene ND mg/kg 04/07/22 16:18 77-47-404/06/22 04:294.2 10
Hexachloroethane ND mg/kg 04/07/22 16:18 67-72-104/06/22 04:294.2 10
Indeno(1,2,3-cd)pyrene ND mg/kg 04/07/22 16:18 193-39-504/06/22 04:294.2 10
Isophorone ND mg/kg 04/07/22 16:18 78-59-104/06/22 04:294.2 10
1-Methylnaphthalene 21.6 mg/kg 04/07/22 16:18 90-12-004/06/22 04:294.2 10
2-Methylnaphthalene 30.9 mg/kg 04/07/22 16:18 91-57-604/06/22 04:294.2 10
2-Methylphenol(o-Cresol)ND mg/kg 04/07/22 16:18 95-48-704/06/22 04:294.2 10
3&4-Methylphenol(m&p Cresol)ND mg/kg 04/07/22 16:18 15831-10-404/06/22 04:294.2 10
Naphthalene 4.5 mg/kg 04/07/22 16:18 91-20-304/06/22 04:294.2 10
2-Nitroaniline ND mg/kg 04/07/22 16:18 88-74-404/06/22 04:2921.0 10
3-Nitroaniline ND mg/kg 04/07/22 16:18 99-09-2 IL04/06/22 04:2921.0 10
4-Nitroaniline ND mg/kg 04/07/22 16:18 100-01-604/06/22 04:298.4 10
Nitrobenzene ND mg/kg 04/07/22 16:18 98-95-304/06/22 04:294.2 10
2-Nitrophenol ND mg/kg 04/07/22 16:18 88-75-504/06/22 04:294.2 10
4-Nitrophenol ND mg/kg 04/07/22 16:18 100-02-704/06/22 04:2921.0 10
N-Nitrosodimethylamine ND mg/kg 04/07/22 16:18 62-75-904/06/22 04:294.2 10
N-Nitroso-di-n-propylamine ND mg/kg 04/07/22 16:18 621-64-704/06/22 04:294.2 10
N-Nitrosodiphenylamine ND mg/kg 04/07/22 16:18 86-30-604/06/22 04:294.2 10
2,2'-Oxybis(1-chloropropane)ND mg/kg 04/07/22 16:18 108-60-104/06/22 04:294.2 10
Pentachlorophenol ND mg/kg 04/07/22 16:18 87-86-504/06/22 04:298.4 10
Phenanthrene 5.7 mg/kg 04/07/22 16:18 85-01-804/06/22 04:294.2 10
Phenol ND mg/kg 04/07/22 16:18 108-95-204/06/22 04:294.2 10
Pyrene ND mg/kg 04/07/22 16:18 129-00-004/06/22 04:294.2 10
Pyridine ND mg/kg 04/07/22 16:18 110-86-104/06/22 04:294.2 10
1,2,4-Trichlorobenzene ND mg/kg 04/07/22 16:18 120-82-104/06/22 04:294.2 10
2,4,5-Trichlorophenol ND mg/kg 04/07/22 16:18 95-95-404/06/22 04:294.2 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Sample:UST-2-SW4-B Lab ID:92597264004 Collected:04/05/22 13:45 Received:04/05/22 14:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,4,6-Trichlorophenol ND mg/kg 04/07/22 16:18 88-06-204/06/22 04:294.2 10
Surrogates
Nitrobenzene-d5 (S)0 %04/07/22 16:18 4165-60-0 D3,S404/06/22 04:2921-130 10
2-Fluorobiphenyl (S)0 %04/07/22 16:18 321-60-8 S404/06/22 04:2919-130 10
Terphenyl-d14 (S)0 %04/07/22 16:18 1718-51-0 S404/06/22 04:2915-130 10
Phenol-d6 (S)0 %04/07/22 16:18 13127-88-3 S404/06/22 04:2918-130 10
2-Fluorophenol (S)0 %04/07/22 16:18 367-12-4 S404/06/22 04:2918-130 10
2,4,6-Tribromophenol (S)0 %04/07/22 16:18 118-79-6 S404/06/22 04:2918-130 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 04/07/22 23:44 67-64-104/07/22 15:020.73 5
Benzene ND mg/kg 04/07/22 23:44 71-43-204/07/22 15:020.036 5
Bromobenzene ND mg/kg 04/07/22 23:44 108-86-104/07/22 15:020.036 5
Bromochloromethane ND mg/kg 04/07/22 23:44 74-97-504/07/22 15:020.036 5
Bromodichloromethane ND mg/kg 04/07/22 23:44 75-27-404/07/22 15:020.036 5
Bromoform ND mg/kg 04/07/22 23:44 75-25-204/07/22 15:020.036 5
Bromomethane ND mg/kg 04/07/22 23:44 74-83-904/07/22 15:020.073 5
2-Butanone (MEK)ND mg/kg 04/07/22 23:44 78-93-304/07/22 15:020.73 5
n-Butylbenzene 3.3 mg/kg 04/07/22 23:44 104-51-804/07/22 15:020.036 5
sec-Butylbenzene 2.4 mg/kg 04/07/22 23:44 135-98-804/07/22 15:020.036 5
tert-Butylbenzene 0.28 mg/kg 04/07/22 23:44 98-06-604/07/22 15:020.036 5
Carbon tetrachloride ND mg/kg 04/07/22 23:44 56-23-504/07/22 15:020.036 5
Chlorobenzene ND mg/kg 04/07/22 23:44 108-90-704/07/22 15:020.036 5
Chloroethane ND mg/kg 04/07/22 23:44 75-00-304/07/22 15:020.073 5
Chloroform ND mg/kg 04/07/22 23:44 67-66-304/07/22 15:020.036 5
Chloromethane ND mg/kg 04/07/22 23:44 74-87-304/07/22 15:020.073 5
2-Chlorotoluene ND mg/kg 04/07/22 23:44 95-49-804/07/22 15:020.036 5
4-Chlorotoluene ND mg/kg 04/07/22 23:44 106-43-404/07/22 15:020.036 5
1,2-Dibromo-3-chloropropane ND mg/kg 04/07/22 23:44 96-12-804/07/22 15:020.036 5
Dibromochloromethane ND mg/kg 04/07/22 23:44 124-48-104/07/22 15:020.036 5
1,2-Dibromoethane (EDB)ND mg/kg 04/07/22 23:44 106-93-404/07/22 15:020.036 5
Dibromomethane ND mg/kg 04/07/22 23:44 74-95-304/07/22 15:020.036 5
1,2-Dichlorobenzene ND mg/kg 04/07/22 23:44 95-50-104/07/22 15:020.036 5
1,3-Dichlorobenzene ND mg/kg 04/07/22 23:44 541-73-104/07/22 15:020.036 5
1,4-Dichlorobenzene ND mg/kg 04/07/22 23:44 106-46-704/07/22 15:020.036 5
Dichlorodifluoromethane ND mg/kg 04/07/22 23:44 75-71-804/07/22 15:020.073 5
1,1-Dichloroethane ND mg/kg 04/07/22 23:44 75-34-304/07/22 15:020.036 5
1,2-Dichloroethane ND mg/kg 04/07/22 23:44 107-06-204/07/22 15:020.036 5
1,1-Dichloroethene ND mg/kg 04/07/22 23:44 75-35-404/07/22 15:020.036 5
cis-1,2-Dichloroethene ND mg/kg 04/07/22 23:44 156-59-204/07/22 15:020.036 5
trans-1,2-Dichloroethene ND mg/kg 04/07/22 23:44 156-60-504/07/22 15:020.036 5
1,2-Dichloropropane ND mg/kg 04/07/22 23:44 78-87-504/07/22 15:020.036 5
1,3-Dichloropropane ND mg/kg 04/07/22 23:44 142-28-904/07/22 15:020.036 5
2,2-Dichloropropane ND mg/kg 04/07/22 23:44 594-20-704/07/22 15:020.036 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 37
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Sample:UST-2-SW4-B Lab ID:92597264004 Collected:04/05/22 13:45 Received:04/05/22 14:52 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloropropene ND mg/kg 04/07/22 23:44 563-58-604/07/22 15:020.036 5
cis-1,3-Dichloropropene ND mg/kg 04/07/22 23:44 10061-01-504/07/22 15:020.036 5
trans-1,3-Dichloropropene ND mg/kg 04/07/22 23:44 10061-02-604/07/22 15:020.036 5
Diisopropyl ether ND mg/kg 04/07/22 23:44 108-20-304/07/22 15:020.036 5
Ethylbenzene 0.066 mg/kg 04/07/22 23:44 100-41-404/07/22 15:020.036 5
Hexachloro-1,3-butadiene ND mg/kg 04/07/22 23:44 87-68-304/07/22 15:020.073 5
2-Hexanone ND mg/kg 04/07/22 23:44 591-78-604/07/22 15:020.36 5
Isopropylbenzene (Cumene)1.0 mg/kg 04/07/22 23:44 98-82-804/07/22 15:020.036 5
p-Isopropyltoluene ND mg/kg 04/07/22 23:44 99-87-604/07/22 15:020.036 5
Methylene Chloride 0.32 mg/kg 04/07/22 23:44 75-09-2 C704/07/22 15:020.15 5
4-Methyl-2-pentanone (MIBK)0.91 mg/kg 04/07/22 23:44 108-10-104/07/22 15:020.36 5
Methyl-tert-butyl ether ND mg/kg 04/07/22 23:44 1634-04-404/07/22 15:020.036 5
Naphthalene 12.8 mg/kg 04/07/22 23:44 91-20-304/07/22 15:020.036 5
n-Propylbenzene 1.8 mg/kg 04/07/22 23:44 103-65-104/07/22 15:020.036 5
Styrene ND mg/kg 04/07/22 23:44 100-42-504/07/22 15:020.036 5
1,1,1,2-Tetrachloroethane ND mg/kg 04/07/22 23:44 630-20-604/07/22 15:020.036 5
1,1,2,2-Tetrachloroethane ND mg/kg 04/07/22 23:44 79-34-504/07/22 15:020.036 5
Tetrachloroethene ND mg/kg 04/07/22 23:44 127-18-404/07/22 15:020.036 5
Toluene ND mg/kg 04/07/22 23:44 108-88-304/07/22 15:020.036 5
1,2,3-Trichlorobenzene ND mg/kg 04/07/22 23:44 87-61-604/07/22 15:020.036 5
1,2,4-Trichlorobenzene ND mg/kg 04/07/22 23:44 120-82-104/07/22 15:020.036 5
1,1,1-Trichloroethane ND mg/kg 04/07/22 23:44 71-55-604/07/22 15:020.036 5
1,1,2-Trichloroethane ND mg/kg 04/07/22 23:44 79-00-504/07/22 15:020.036 5
Trichloroethene ND mg/kg 04/07/22 23:44 79-01-604/07/22 15:020.036 5
Trichlorofluoromethane ND mg/kg 04/07/22 23:44 75-69-404/07/22 15:020.036 5
1,2,3-Trichloropropane ND mg/kg 04/07/22 23:44 96-18-404/07/22 15:020.036 5
1,2,4-Trimethylbenzene ND mg/kg 04/07/22 23:44 95-63-604/07/22 15:020.036 5
1,3,5-Trimethylbenzene ND mg/kg 04/07/22 23:44 108-67-804/07/22 15:020.036 5
Vinyl acetate ND mg/kg 04/07/22 23:44 108-05-404/07/22 15:020.36 5
Vinyl chloride ND mg/kg 04/07/22 23:44 75-01-404/07/22 15:020.073 5
Xylene (Total)ND mg/kg 04/07/22 23:44 1330-20-704/07/22 15:020.073 5
m&p-Xylene ND mg/kg 04/07/22 23:44 179601-23-104/07/22 15:020.073 5
o-Xylene ND mg/kg 04/07/22 23:44 95-47-604/07/22 15:020.036 5
Surrogates
Toluene-d8 (S)100 %04/07/22 23:44 2037-26-504/07/22 15:0270-130 5
4-Bromofluorobenzene (S)115 %04/07/22 23:44 460-00-404/07/22 15:0269-134 5
1,2-Dichloroethane-d4 (S)90 %04/07/22 23:44 17060-07-004/07/22 15:0270-130 5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.6 %04/06/22 15:25 N20.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 81.0 %04/11/22 15:4304/11/22 15:371
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1846573
MA DEP/NJ DEP
MADEP EPH
TPH by Method MADEPE
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92597264004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3780343-1
Associated Lab Samples:92597264004
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 6.50 04/12/22 07:34
Aliphatic (C19-C36)mg/kg ND 6.50 04/12/22 07:34
Total Extractable Hydrocarbons mg/kg ND 6.50 04/12/22 07:34
1-Chloro-octadecane (S)%61.1 40.0-140 04/12/22 07:34
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3780343-4
Associated Lab Samples:92597264004
Matrix:Solid
Analyzed
Aromatic (C11-C22)mg/kg ND 6.50 04/12/22 08:45
Total Extractable Hydrocarbons mg/kg ND 6.50 04/12/22 08:45
o-Terphenyl (S)%67.5 40.0-140 04/12/22 08:45
2-Fluorobiphenyl (S)%80.3 40.0-140 04/12/22 08:45
2-Bromonaphthalene (S)%80.8 40.0-140 04/12/22 08:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3780343-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3780343-3
Aliphatic (C09-C18)mg/kg 25.739.9 64.4 40.0-14063.725.4 1.17 25
Aliphatic (C19-C36)mg/kg 39.953.2 75.0 40.0-14081.443.3 8.17 25
1-Chloro-octadecane (S)%55.1 40.0-14061.7
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3780343-5LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3780343-6
Aromatic (C11-C22)mg/kg 90.4113 80.0 40.0-14085.596.6 6.63 25
o-Terphenyl (S)%72.6 40.0-14073.1
2-Fluorobiphenyl (S)%85.3 40.0-14088.2
2-Bromonaphthalene (S)%86.5 40.0-14089.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3780343-7MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1478246-03
R3780343-8
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aliphatic (C09-C18)mg/kg 40.8 54.0 40.0-14050.9 5.2640.56.08 28.1 26.7
Aliphatic (C19-C36)mg/kg MH54.4 180 40.0-14089.7 21.954.0153 250 201
1-Chloro-octadecane (S)%55.3 40.0-14047.9
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3780343-9MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1478246-03
R3780343-10
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aromatic (C11-C22)mg/kg 115 83.3 40.0-14075.0 9.3511419.3 115 105
o-Terphenyl (S)%72.9 40.0-14070.2
2-Fluorobiphenyl (S)%90.0 40.0-14081.9
2-Bromonaphthalene (S)%91.3 40.0-14086.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
689831
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92597264001, 92597264002, 92597264003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3604676
Associated Lab Samples:92597264001, 92597264002, 92597264003
Matrix:Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 04/07/22 04:01
4-Bromofluorobenzene (S)%87 66-130 04/07/22 04:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3604677LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 46.650.2 93 70-130
4-Bromofluorobenzene (S)%95 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3604679MATRIX SPIKE SAMPLE:
MSSpike
Result
92596482027
Gas Range Organics (C6-C10)mg/kg 254004730 93 65-14621000
4-Bromofluorobenzene (S)%119 66-130
Parameter Units
Dup
Result QualifiersRPDResult
92596634002
3604678SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%8887
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
692335
MADEP VPH
MADEP VPH
VPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92597264004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3617037
Associated Lab Samples:92597264004
Matrix:Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N204/18/22 13:22
Aromatic (C09-C10)mg/kg ND 2.5 N204/18/22 13:22
4-Bromofluorobenzene (FID) (S)%101 70-130 04/18/22 13:22
4-Bromofluorobenzene (PID) (S)%84 70-130 04/18/22 13:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3617038LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3617039
Aliphatic (C05-C08)mg/kg 16.3 N21510970-13010515.8 3 25
Aromatic (C09-C10)mg/kg 3.8 N257670-130743.7 3 25
4-Bromofluorobenzene (FID) (S)%100 70-13099
4-Bromofluorobenzene (PID) (S)%75 70-13074
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
690146
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92597264004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3606535
Associated Lab Samples:92597264004
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 04/07/22 16:03
1,1,1-Trichloroethane mg/kg ND 0.0050 04/07/22 16:03
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 04/07/22 16:03
1,1,2-Trichloroethane mg/kg ND 0.0050 04/07/22 16:03
1,1-Dichloroethane mg/kg ND 0.0050 04/07/22 16:03
1,1-Dichloroethene mg/kg ND 0.0050 04/07/22 16:03
1,1-Dichloropropene mg/kg ND 0.0050 04/07/22 16:03
1,2,3-Trichlorobenzene mg/kg ND 0.0050 04/07/22 16:03
1,2,3-Trichloropropane mg/kg ND 0.0050 04/07/22 16:03
1,2,4-Trichlorobenzene mg/kg ND 0.0050 04/07/22 16:03
1,2,4-Trimethylbenzene mg/kg ND 0.0050 04/07/22 16:03
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 04/07/22 16:03
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 04/07/22 16:03
1,2-Dichlorobenzene mg/kg ND 0.0050 04/07/22 16:03
1,2-Dichloroethane mg/kg ND 0.0050 04/07/22 16:03
1,2-Dichloropropane mg/kg ND 0.0050 04/07/22 16:03
1,3,5-Trimethylbenzene mg/kg ND 0.0050 04/07/22 16:03
1,3-Dichlorobenzene mg/kg ND 0.0050 04/07/22 16:03
1,3-Dichloropropane mg/kg ND 0.0050 04/07/22 16:03
1,4-Dichlorobenzene mg/kg ND 0.0050 04/07/22 16:03
2,2-Dichloropropane mg/kg ND 0.0050 04/07/22 16:03
2-Butanone (MEK)mg/kg ND 0.10 04/07/22 16:03
2-Chlorotoluene mg/kg ND 0.0050 04/07/22 16:03
2-Hexanone mg/kg ND 0.050 04/07/22 16:03
4-Chlorotoluene mg/kg ND 0.0050 04/07/22 16:03
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 04/07/22 16:03
Acetone mg/kg ND 0.10 04/07/22 16:03
Benzene mg/kg ND 0.0050 04/07/22 16:03
Bromobenzene mg/kg ND 0.0050 04/07/22 16:03
Bromochloromethane mg/kg ND 0.0050 04/07/22 16:03
Bromodichloromethane mg/kg ND 0.0050 04/07/22 16:03
Bromoform mg/kg ND 0.0050 04/07/22 16:03
Bromomethane mg/kg ND 0.010 04/07/22 16:03
Carbon tetrachloride mg/kg ND 0.0050 04/07/22 16:03
Chlorobenzene mg/kg ND 0.0050 04/07/22 16:03
Chloroethane mg/kg ND 0.010 04/07/22 16:03
Chloroform mg/kg ND 0.0050 04/07/22 16:03
Chloromethane mg/kg ND 0.010 04/07/22 16:03
cis-1,2-Dichloroethene mg/kg ND 0.0050 04/07/22 16:03
cis-1,3-Dichloropropene mg/kg ND 0.0050 04/07/22 16:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3606535
Associated Lab Samples:92597264004
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 04/07/22 16:03
Dibromomethane mg/kg ND 0.0050 04/07/22 16:03
Dichlorodifluoromethane mg/kg ND 0.010 04/07/22 16:03
Diisopropyl ether mg/kg ND 0.0050 04/07/22 16:03
Ethylbenzene mg/kg ND 0.0050 04/07/22 16:03
Hexachloro-1,3-butadiene mg/kg ND 0.010 04/07/22 16:03
Isopropylbenzene (Cumene)mg/kg ND 0.0050 04/07/22 16:03
m&p-Xylene mg/kg ND 0.010 04/07/22 16:03
Methyl-tert-butyl ether mg/kg ND 0.0050 04/07/22 16:03
Methylene Chloride mg/kg ND 0.020 04/07/22 16:03
n-Butylbenzene mg/kg ND 0.0050 04/07/22 16:03
n-Propylbenzene mg/kg ND 0.0050 04/07/22 16:03
Naphthalene mg/kg ND 0.0050 04/07/22 16:03
o-Xylene mg/kg ND 0.0050 04/07/22 16:03
p-Isopropyltoluene mg/kg ND 0.0050 04/07/22 16:03
sec-Butylbenzene mg/kg ND 0.0050 04/07/22 16:03
Styrene mg/kg ND 0.0050 04/07/22 16:03
tert-Butylbenzene mg/kg ND 0.0050 04/07/22 16:03
Tetrachloroethene mg/kg ND 0.0050 04/07/22 16:03
Toluene mg/kg ND 0.0050 04/07/22 16:03
trans-1,2-Dichloroethene mg/kg ND 0.0050 04/07/22 16:03
trans-1,3-Dichloropropene mg/kg ND 0.0050 04/07/22 16:03
Trichloroethene mg/kg ND 0.0050 04/07/22 16:03
Trichlorofluoromethane mg/kg ND 0.0050 04/07/22 16:03
Vinyl acetate mg/kg ND 0.050 04/07/22 16:03
Vinyl chloride mg/kg ND 0.010 04/07/22 16:03
Xylene (Total)mg/kg ND 0.010 04/07/22 16:03
1,2-Dichloroethane-d4 (S)%96 70-130 04/07/22 16:03
4-Bromofluorobenzene (S)%98 69-134 04/07/22 16:03
Toluene-d8 (S)%98 70-130 04/07/22 16:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3606536LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.31.2 104 70-130
1,1,1-Trichloroethane mg/kg 1.21.2 99 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.21.2 97 70-130
1,1,2-Trichloroethane mg/kg 1.31.2 100 70-130
1,1-Dichloroethane mg/kg 1.21.2 95 70-130
1,1-Dichloroethene mg/kg 1.31.2 102 70-130
1,1-Dichloropropene mg/kg 1.31.2 104 70-130
1,2,3-Trichlorobenzene mg/kg 1.21.2 99 65-130
1,2,3-Trichloropropane mg/kg 1.31.2 100 70-130
1,2,4-Trichlorobenzene mg/kg 1.21.2 99 68-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3606536LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.21.2 100 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.31.2 107 70-130
1,2-Dibromoethane (EDB)mg/kg 1.31.2 103 70-130
1,2-Dichlorobenzene mg/kg 1.21.2 98 70-130
1,2-Dichloroethane mg/kg 1.21.2 97 63-130
1,2-Dichloropropane mg/kg 1.21.2 100 70-130
1,3,5-Trimethylbenzene mg/kg 1.31.2 102 70-130
1,3-Dichlorobenzene mg/kg 1.21.2 97 70-130
1,3-Dichloropropane mg/kg 1.31.2 100 70-130
1,4-Dichlorobenzene mg/kg 1.21.2 96 70-130
2,2-Dichloropropane mg/kg 1.21.2 99 66-130
2-Butanone (MEK)mg/kg 2.42.5 96 70-130
2-Chlorotoluene mg/kg 1.21.2 98 70-130
2-Hexanone mg/kg 2.52.5 101 70-130
4-Chlorotoluene mg/kg 1.21.2 98 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.52.5 99 70-130
Acetone mg/kg 2.22.5 89 69-130
Benzene mg/kg 1.21.2 95 70-130
Bromobenzene mg/kg 1.31.2 104 70-130
Bromochloromethane mg/kg 1.31.2 104 70-130
Bromodichloromethane mg/kg 1.31.2 101 69-130
Bromoform mg/kg 1.41.2 109 70-130
Bromomethane mg/kg 1.41.2 115 52-130
Carbon tetrachloride mg/kg 1.31.2 103 70-130
Chlorobenzene mg/kg 1.31.2 103 70-130
Chloroethane mg/kg 1.51.2 122 65-130
Chloroform mg/kg 1.21.2 99 70-130
Chloromethane mg/kg 1.41.2 111 55-130
cis-1,2-Dichloroethene mg/kg 1.21.2 100 70-130
cis-1,3-Dichloropropene mg/kg 1.31.2 102 70-130
Dibromochloromethane mg/kg 1.31.2 104 70-130
Dibromomethane mg/kg 1.31.2 103 70-130
Dichlorodifluoromethane mg/kg 1.91.2 149 45-156
Diisopropyl ether mg/kg 1.21.2 94 70-130
Ethylbenzene mg/kg 1.21.2 96 70-130
Hexachloro-1,3-butadiene mg/kg 1.31.2 102 66-130
Isopropylbenzene (Cumene)mg/kg 1.31.2 100 70-130
m&p-Xylene mg/kg 2.62.5 103 70-130
Methyl-tert-butyl ether mg/kg 1.21.2 93 70-130
Methylene Chloride mg/kg 1.11.2 88 65-130
n-Butylbenzene mg/kg 1.31.2 101 67-130
n-Propylbenzene mg/kg 1.21.2 99 70-130
Naphthalene mg/kg 1.31.2 101 70-130
o-Xylene mg/kg 1.31.2 104 70-130
p-Isopropyltoluene mg/kg 1.31.2 104 67-130
sec-Butylbenzene mg/kg 1.21.2 99 69-130
Styrene mg/kg 1.41.2 108 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3606536LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.21.2 94 67-130
Tetrachloroethene mg/kg 1.21.2 93 70-130
Toluene mg/kg 1.21.2 97 70-130
trans-1,2-Dichloroethene mg/kg 1.21.2 100 70-130
trans-1,3-Dichloropropene mg/kg 1.21.2 99 68-130
Trichloroethene mg/kg 1.31.2 102 70-130
Trichlorofluoromethane mg/kg 1.41.2 111 70-130
Vinyl acetate mg/kg 2.62.5 105 70-130
Vinyl chloride mg/kg 1.51.2 120 61-130
Xylene (Total)mg/kg 3.93.8 103 70-130
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3606537MATRIX SPIKE SAMPLE:
MSSpike
Result
92597008002
1,1,1,2-Tetrachloroethane mg/kg 0.42 M10.75 56 70-131ND
1,1,1-Trichloroethane mg/kg 0.40 M10.75 54 65-133ND
1,1,2,2-Tetrachloroethane mg/kg 0.37 M10.75 50 66-130ND
1,1,2-Trichloroethane mg/kg 0.40 M10.75 54 66-133ND
1,1-Dichloroethane mg/kg 0.40 M10.75 53 65-130ND
1,1-Dichloroethene mg/kg 0.410.75 55 10-158ND
1,1-Dichloropropene mg/kg 0.42 M10.75 56 68-133ND
1,2,3-Trichlorobenzene mg/kg 0.400.75 53 27-138ND
1,2,3-Trichloropropane mg/kg 0.38 M10.75 51 67-130ND
1,2,4-Trichlorobenzene mg/kg 0.400.75 53 51-134ND
1,2,4-Trimethylbenzene mg/kg 0.43 M10.75 58 63-136ND
1,2-Dibromo-3-chloropropane mg/kg 0.360.75 48 32-130ND
1,2-Dibromoethane (EDB)mg/kg 0.42 M10.75 56 70-130ND
1,2-Dichlorobenzene mg/kg 0.42 M10.75 57 69-130ND
1,2-Dichloroethane mg/kg 0.40 M10.75 53 59-130ND
1,2-Dichloropropane mg/kg 0.43 M10.75 58 70-130ND
1,3,5-Trimethylbenzene mg/kg 0.44 M10.75 59 65-137ND
1,3-Dichlorobenzene mg/kg 0.41 M10.75 55 70-130ND
1,3-Dichloropropane mg/kg 0.41 M10.75 55 70-130ND
1,4-Dichlorobenzene mg/kg 0.41 M10.75 55 68-130ND
2,2-Dichloropropane mg/kg 0.410.75 55 32-130ND
2-Butanone (MEK)mg/kg 0.761.5 50 10-136ND
2-Chlorotoluene mg/kg 0.42 M10.75 56 69-141ND
2-Hexanone mg/kg 0.681.5 46 10-144ND
4-Chlorotoluene mg/kg 0.40 M10.75 54 70-132ND
4-Methyl-2-pentanone (MIBK)mg/kg 0.721.5 48 25-143ND
Acetone mg/kg 0.641.5 43 10-130ND
Benzene mg/kg 0.41 M10.75 56 67-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3606537MATRIX SPIKE SAMPLE:
MSSpike
Result
92597008002
Bromobenzene mg/kg 0.41 M10.75 56 70-130ND
Bromochloromethane mg/kg 0.42 M10.75 56 69-134ND
Bromodichloromethane mg/kg 0.39 M10.75 52 64-130ND
Bromoform mg/kg 0.38 M10.75 50 62-130ND
Bromomethane mg/kg 0.340.75 46 20-176ND
Carbon tetrachloride mg/kg 0.40 M10.75 54 65-140ND
Chlorobenzene mg/kg 0.42 M10.75 56 70-130ND
Chloroethane mg/kg 0.240.75 32 10-130ND
Chloroform mg/kg 0.41 M10.75 54 63-130ND
Chloromethane mg/kg 0.490.75 66 58-130ND
cis-1,2-Dichloroethene mg/kg 0.42 M10.75 56 66-130ND
cis-1,3-Dichloropropene mg/kg 0.41 M10.75 54 67-130ND
Dibromochloromethane mg/kg 0.37 M10.75 50 67-130ND
Dibromomethane mg/kg 0.41 M10.75 55 63-131ND
Dichlorodifluoromethane mg/kg 0.560.75 75 44-180ND
Diisopropyl ether mg/kg 0.39 M10.75 52 63-130ND
Ethylbenzene mg/kg 0.40 M10.75 54 66-130ND
Hexachloro-1,3-butadiene mg/kg 0.38 M10.75 52 64-150ND
Isopropylbenzene (Cumene)mg/kg 0.44 M10.75 59 69-135ND
m&p-Xylene mg/kg 0.85 M11.5 57 60-133ND
Methyl-tert-butyl ether mg/kg 0.38 M10.75 51 65-130ND
Methylene Chloride mg/kg 0.35 M10.75 47 61-130ND
n-Butylbenzene mg/kg 0.40 M10.75 53 65-140ND
n-Propylbenzene mg/kg 0.42 M10.75 56 67-140ND
Naphthalene mg/kg 0.370.75 50 15-145ND
o-Xylene mg/kg 0.43 M10.75 58 66-133ND
p-Isopropyltoluene mg/kg 0.440.75 58 56-14710.7 ug/kg
sec-Butylbenzene mg/kg 0.43 M10.75 57 65-139ND
Styrene mg/kg 0.43 M10.75 57 70-132ND
tert-Butylbenzene mg/kg 0.42 M10.75 56 62-135ND
Tetrachloroethene mg/kg 0.38 M10.75 51 70-135ND
Toluene mg/kg 0.40 M10.75 54 67-130ND
trans-1,2-Dichloroethene mg/kg 0.41 M10.75 55 69-130ND
trans-1,3-Dichloropropene mg/kg 0.38 M10.75 51 62-130ND
Trichloroethene mg/kg 0.42 M10.75 57 70-135ND
Trichlorofluoromethane mg/kg 0.210.75 28 10-130ND
Vinyl acetate mg/kg 0.791.5 53 53-130ND
Vinyl chloride mg/kg 0.510.75 68 61-148ND
Xylene (Total)mg/kg 1.3 MS2.3 57 63-132ND
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92597394001
3606538SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg NDND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg NDND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg NDND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg .005JND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg NDND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92597394001
3606538SAMPLE DUPLICATE:
m&p-Xylene mg/kg NDND
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg 0.0087ND
o-Xylene mg/kg 0.011ND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg NDND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
Xylene (Total)mg/kg .011JND
1,2-Dichloroethane-d4 (S)%9390
4-Bromofluorobenzene (S)%9998
Toluene-d8 (S)%9898
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
689926
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92597264001, 92597264002, 92597264003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3605238
Associated Lab Samples:92597264001, 92597264002, 92597264003
Matrix:Solid
Analyzed
Diesel Range Organics(C10-C28)mg/kg ND 5.1 04/07/22 08:45
n-Pentacosane (S)%89 10-130 04/07/22 08:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3605239LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 47.767.3 71 44-130
n-Pentacosane (S)%87 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3605284MATRIX SPIKE SAMPLE:
MSSpike
Result
92596869001
Diesel Range Organics(C10-C28)mg/kg 470 M181-488 10-130864
n-Pentacosane (S)%93 10-130
Parameter Units
Dup
Result QualifiersRPDResult
92596812001
3605241SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 22000 1325000
n-Pentacosane (S)%0 S40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
689627
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92597264004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3603710
Associated Lab Samples:92597264004
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 04/06/22 09:46
1,2-Dichlorobenzene mg/kg ND 0.33 04/06/22 09:46
1,3-Dichlorobenzene mg/kg ND 0.33 04/06/22 09:46
1,4-Dichlorobenzene mg/kg ND 0.33 04/06/22 09:46
1-Methylnaphthalene mg/kg ND 0.33 04/06/22 09:46
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 04/06/22 09:46
2,4,5-Trichlorophenol mg/kg ND 0.33 04/06/22 09:46
2,4,6-Trichlorophenol mg/kg ND 0.33 04/06/22 09:46
2,4-Dichlorophenol mg/kg ND 0.33 04/06/22 09:46
2,4-Dimethylphenol mg/kg ND 0.33 04/06/22 09:46
2,4-Dinitrophenol mg/kg ND 1.6 04/06/22 09:46
2,4-Dinitrotoluene mg/kg ND 0.33 04/06/22 09:46
2,6-Dinitrotoluene mg/kg ND 0.33 04/06/22 09:46
2-Chloronaphthalene mg/kg ND 0.33 04/06/22 09:46
2-Chlorophenol mg/kg ND 0.33 04/06/22 09:46
2-Methylnaphthalene mg/kg ND 0.33 04/06/22 09:46
2-Methylphenol(o-Cresol)mg/kg ND 0.33 04/06/22 09:46
2-Nitroaniline mg/kg ND 1.6 04/06/22 09:46
2-Nitrophenol mg/kg ND 0.33 04/06/22 09:46
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 04/06/22 09:46
3,3'-Dichlorobenzidine mg/kg ND 0.66 IL04/06/22 09:46
3-Nitroaniline mg/kg ND 1.6 04/06/22 09:46
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 04/06/22 09:46
4-Bromophenylphenyl ether mg/kg ND 0.33 04/06/22 09:46
4-Chloro-3-methylphenol mg/kg ND 0.66 04/06/22 09:46
4-Chloroaniline mg/kg ND 0.66 04/06/22 09:46
4-Chlorophenylphenyl ether mg/kg ND 0.33 04/06/22 09:46
4-Nitroaniline mg/kg ND 0.66 04/06/22 09:46
4-Nitrophenol mg/kg ND 1.6 04/06/22 09:46
Acenaphthene mg/kg ND 0.33 04/06/22 09:46
Acenaphthylene mg/kg ND 0.33 04/06/22 09:46
Aniline mg/kg ND 0.33 04/06/22 09:46
Anthracene mg/kg ND 0.33 04/06/22 09:46
Benzo(a)anthracene mg/kg ND 0.33 04/06/22 09:46
Benzo(a)pyrene mg/kg ND 0.33 04/06/22 09:46
Benzo(b)fluoranthene mg/kg ND 0.33 04/06/22 09:46
Benzo(g,h,i)perylene mg/kg ND 0.33 04/06/22 09:46
Benzo(k)fluoranthene mg/kg ND 0.33 04/06/22 09:46
Benzoic Acid mg/kg ND 1.6 04/06/22 09:46
Benzyl alcohol mg/kg ND 0.66 04/06/22 09:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3603710
Associated Lab Samples:92597264004
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane mg/kg ND 0.33 04/06/22 09:46
bis(2-Chloroethyl) ether mg/kg ND 0.33 04/06/22 09:46
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 04/06/22 09:46
Butylbenzylphthalate mg/kg ND 0.33 04/06/22 09:46
Chrysene mg/kg ND 0.33 04/06/22 09:46
Di-n-butylphthalate mg/kg ND 0.33 04/06/22 09:46
Di-n-octylphthalate mg/kg ND 0.33 v104/06/22 09:46
Dibenz(a,h)anthracene mg/kg ND 0.33 04/06/22 09:46
Dibenzofuran mg/kg ND 0.33 04/06/22 09:46
Diethylphthalate mg/kg ND 0.33 v104/06/22 09:46
Dimethylphthalate mg/kg ND 0.33 04/06/22 09:46
Fluoranthene mg/kg ND 0.33 04/06/22 09:46
Fluorene mg/kg ND 0.33 04/06/22 09:46
Hexachloro-1,3-butadiene mg/kg ND 0.33 04/06/22 09:46
Hexachlorobenzene mg/kg ND 0.33 04/06/22 09:46
Hexachlorocyclopentadiene mg/kg ND 0.33 04/06/22 09:46
Hexachloroethane mg/kg ND 0.33 04/06/22 09:46
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 04/06/22 09:46
Isophorone mg/kg ND 0.33 04/06/22 09:46
N-Nitroso-di-n-propylamine mg/kg ND 0.33 04/06/22 09:46
N-Nitrosodimethylamine mg/kg ND 0.33 04/06/22 09:46
N-Nitrosodiphenylamine mg/kg ND 0.33 04/06/22 09:46
Naphthalene mg/kg ND 0.33 04/06/22 09:46
Nitrobenzene mg/kg ND 0.33 04/06/22 09:46
Pentachlorophenol mg/kg ND 0.66 04/06/22 09:46
Phenanthrene mg/kg ND 0.33 04/06/22 09:46
Phenol mg/kg ND 0.33 04/06/22 09:46
Pyrene mg/kg ND 0.33 04/06/22 09:46
Pyridine mg/kg ND 0.33 04/06/22 09:46
2,4,6-Tribromophenol (S)%72 18-130 04/06/22 09:46
2-Fluorobiphenyl (S)%65 19-130 04/06/22 09:46
2-Fluorophenol (S)%62 18-130 04/06/22 09:46
Nitrobenzene-d5 (S)%61 21-130 04/06/22 09:46
Phenol-d6 (S)%59 18-130 04/06/22 09:46
Terphenyl-d14 (S)%102 15-130 04/06/22 09:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3603711LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.21.6 75 47-130
1,2-Dichlorobenzene mg/kg 1.11.6 69 49-130
1,3-Dichlorobenzene mg/kg 1.11.6 68 48-130
1,4-Dichlorobenzene mg/kg 1.11.6 68 49-130
1-Methylnaphthalene mg/kg 1.31.6 78 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3603711LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.11.6 70 38-130
2,4,5-Trichlorophenol mg/kg 1.41.6 87 49-130
2,4,6-Trichlorophenol mg/kg 1.41.6 85 50-130
2,4-Dichlorophenol mg/kg 1.31.6 81 51-130
2,4-Dimethylphenol mg/kg 1.31.6 80 53-130
2,4-Dinitrophenol mg/kg 7.48.2 91 39-130
2,4-Dinitrotoluene mg/kg 1.51.6 94 53-130
2,6-Dinitrotoluene mg/kg 1.61.6 95 55-130
2-Chloronaphthalene mg/kg 1.31.6 80 48-130
2-Chlorophenol mg/kg 1.21.6 75 54-130
2-Methylnaphthalene mg/kg 1.31.6 78 57-130
2-Methylphenol(o-Cresol)mg/kg 1.21.6 76 50-130
2-Nitroaniline mg/kg 2.83.3 85 49-130
2-Nitrophenol mg/kg 1.21.6 76 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.31.6 77 50-130
3,3'-Dichlorobenzidine mg/kg 2.8 IL3.3 85 47-130
3-Nitroaniline mg/kg 3.03.3 90 45-130
4,6-Dinitro-2-methylphenol mg/kg 3.13.3 95 50-142
4-Bromophenylphenyl ether mg/kg 1.61.6 96 55-130
4-Chloro-3-methylphenol mg/kg 2.73.3 82 52-130
4-Chloroaniline mg/kg 2.53.3 76 49-130
4-Chlorophenylphenyl ether mg/kg 1.41.6 88 53-130
4-Nitroaniline mg/kg 2.83.3 85 51-130
4-Nitrophenol mg/kg 7.08.2 86 40-130
Acenaphthene mg/kg 1.31.6 82 56-130
Acenaphthylene mg/kg 1.41.6 84 58-130
Aniline mg/kg 1.11.6 69 44-130
Anthracene mg/kg 1.41.6 86 60-130
Benzo(a)anthracene mg/kg 1.61.6 96 59-130
Benzo(a)pyrene mg/kg 1.71.6 105 57-130
Benzo(b)fluoranthene mg/kg 1.71.6 103 54-130
Benzo(g,h,i)perylene mg/kg 1.61.6 98 59-130
Benzo(k)fluoranthene mg/kg 1.71.6 106 54-130
Benzoic Acid mg/kg 6.88.2 83 19-130
Benzyl alcohol mg/kg 2.53.3 76 50-130
bis(2-Chloroethoxy)methane mg/kg 1.21.6 76 55-130
bis(2-Chloroethyl) ether mg/kg 1.11.6 70 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.81.6 111 58-130
Butylbenzylphthalate mg/kg 1.81.6 107 46-138
Chrysene mg/kg 1.51.6 94 57-130
Di-n-butylphthalate mg/kg 1.61.6 96 57-130
Di-n-octylphthalate mg/kg 1.9 v11.6 113 57-130
Dibenz(a,h)anthracene mg/kg 1.61.6 100 60-130
Dibenzofuran mg/kg 1.41.6 86 54-130
Diethylphthalate mg/kg 1.5 v11.6 91 55-130
Dimethylphthalate mg/kg 1.51.6 90 57-130
Fluoranthene mg/kg 1.51.6 93 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3603711LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.41.6 87 56-130
Hexachloro-1,3-butadiene mg/kg 1.21.6 75 41-130
Hexachlorobenzene mg/kg 1.51.6 93 53-130
Hexachlorocyclopentadiene mg/kg 1.21.6 74 23-130
Hexachloroethane mg/kg 1.11.6 69 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.61.6 100 61-130
Isophorone mg/kg 1.21.6 73 49-130
N-Nitroso-di-n-propylamine mg/kg 1.21.6 74 52-130
N-Nitrosodimethylamine mg/kg 1.11.6 67 45-130
N-Nitrosodiphenylamine mg/kg 1.51.6 90 56-130
Naphthalene mg/kg 1.21.6 75 56-130
Nitrobenzene mg/kg 1.21.6 73 50-130
Pentachlorophenol mg/kg 3.23.3 96 33-130
Phenanthrene mg/kg 1.51.6 93 60-130
Phenol mg/kg 1.21.6 74 54-130
Pyrene mg/kg 1.61.6 98 61-130
Pyridine mg/kg 0.911.6 55 35-130
2,4,6-Tribromophenol (S)%97 18-130
2-Fluorobiphenyl (S)%78 19-130
2-Fluorophenol (S)%71 18-130
Nitrobenzene-d5 (S)%71 21-130
Phenol-d6 (S)%70 18-130
Terphenyl-d14 (S)%119 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3603712MATRIX SPIKE SAMPLE:
MSSpike
Result
92597196009
1,2,4-Trichlorobenzene mg/kg 1.62.1 73 22-130ND
1,2-Dichlorobenzene mg/kg 1.32.1 61 23-130ND
1,3-Dichlorobenzene mg/kg 1.32.1 59 26-130ND
1,4-Dichlorobenzene mg/kg 1.32.1 60 27-130ND
1-Methylnaphthalene mg/kg 1.72.1 75 30-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.32.1 60 30-130ND
2,4,5-Trichlorophenol mg/kg 1.82.1 84 26-130ND
2,4,6-Trichlorophenol mg/kg 1.82.1 82 23-130ND
2,4-Dichlorophenol mg/kg 1.72.1 79 29-130ND
2,4-Dimethylphenol mg/kg 1.62.1 76 13-130ND
2,4-Dinitrophenol mg/kg 7.710.8 71 10-131ND
2,4-Dinitrotoluene mg/kg 1.82.1 85 28-130ND
2,6-Dinitrotoluene mg/kg 1.92.1 87 36-130ND
2-Chloronaphthalene mg/kg 1.72.1 78 27-130ND
2-Chlorophenol mg/kg 1.42.1 67 29-130ND
2-Methylnaphthalene mg/kg 1.72.1 73 29-130ND
2-Methylphenol(o-Cresol)mg/kg 1.52.1 68 20-130ND
2-Nitroaniline mg/kg 3.74.3 87 29-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
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Page 26 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3603712MATRIX SPIKE SAMPLE:
MSSpike
Result
92597196009
2-Nitrophenol mg/kg 1.52.1 71 26-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.52.1 67 10-176ND
3,3'-Dichlorobenzidine mg/kg 3.2 IL4.3 74 15-130ND
3-Nitroaniline mg/kg 3.74.3 85 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 3.84.3 87 15-132ND
4-Bromophenylphenyl ether mg/kg 2.02.1 93 35-130ND
4-Chloro-3-methylphenol mg/kg 3.34.3 77 30-130ND
4-Chloroaniline mg/kg 2.94.3 68 28-130ND
4-Chlorophenylphenyl ether mg/kg 1.82.1 85 32-130ND
4-Nitroaniline mg/kg 3.34.3 77 30-130ND
4-Nitrophenol mg/kg 8.610.8 80 17-130ND
Acenaphthene mg/kg 1.82.1 82 29-130ND
Acenaphthylene mg/kg 1.82.1 82 31-130ND
Aniline mg/kg 1.32.1 60 10-130ND
Anthracene mg/kg 1.82.1 84 33-130ND
Benzo(a)anthracene mg/kg 1.92.1 90 32-130ND
Benzo(a)pyrene mg/kg 2.12.1 96 32-130ND
Benzo(b)fluoranthene mg/kg 2.02.1 93 33-130ND
Benzo(g,h,i)perylene mg/kg 2.22.1 100 28-130ND
Benzo(k)fluoranthene mg/kg 2.12.1 96 31-130ND
Benzoic Acid mg/kg 5.810.8 53 10-130ND
Benzyl alcohol mg/kg 3.04.3 69 31-130ND
bis(2-Chloroethoxy)methane mg/kg 1.52.1 71 30-130ND
bis(2-Chloroethyl) ether mg/kg 1.3 M12.1 62 68-130ND
bis(2-Ethylhexyl)phthalate mg/kg 2.32.1 103 40-130ND
Butylbenzylphthalate mg/kg 2.12.1 99 40-130ND
Chrysene mg/kg 2.02.1 91 30-130ND
Di-n-butylphthalate mg/kg 2.02.1 90 41-130ND
Di-n-octylphthalate mg/kg 2.4 v12.1 111 42-130ND
Dibenz(a,h)anthracene mg/kg 2.22.1 100 27-130ND
Dibenzofuran mg/kg 1.92.1 90 32-130ND
Diethylphthalate mg/kg 1.8 v12.1 84 40-130ND
Dimethylphthalate mg/kg 1.82.1 83 37-130ND
Fluoranthene mg/kg 1.92.1 90 26-130ND
Fluorene mg/kg 1.92.1 86 31-130ND
Hexachloro-1,3-butadiene mg/kg 1.62.1 72 20-130ND
Hexachlorobenzene mg/kg 1.92.1 89 29-130ND
Hexachlorocyclopentadiene mg/kg 1.42.1 62 10-130ND
Hexachloroethane mg/kg 1.42.1 63 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 2.22.1 99 28-130ND
Isophorone mg/kg 1.42.1 67 32-130ND
N-Nitroso-di-n-propylamine mg/kg 1.42.1 64 31-130ND
N-Nitrosodimethylamine mg/kg 1.32.1 59 20-130ND
N-Nitrosodiphenylamine mg/kg 1.92.1 89 32-130ND
Naphthalene mg/kg 1.62.1 71 30-130ND
Nitrobenzene mg/kg 1.52.1 68 25-130ND
Pentachlorophenol mg/kg 3.84.3 88 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
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Huntersville, NC 28078
[phone]
Page 27 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3603712MATRIX SPIKE SAMPLE:
MSSpike
Result
92597196009
Phenanthrene mg/kg 2.02.1 89 34-130ND
Phenol mg/kg 2.22.1 73 14-130573 ug/kg
Pyrene mg/kg 1.92.1 88 31-130ND
Pyridine mg/kg 0.862.1 40 10-130ND
2,4,6-Tribromophenol (S)%94 18-130
2-Fluorobiphenyl (S)%80 19-130
2-Fluorophenol (S)%66 18-130
Nitrobenzene-d5 (S)%68 21-130
Phenol-d6 (S)%66 18-130
Terphenyl-d14 (S)%108 15-130
Parameter Units
Dup
Result QualifiersRPDResult
92597196010
3603713SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
1-Methylnaphthalene mg/kg NDND
2,2'-Oxybis(1-chloropropane)mg/kg NDND
2,4,5-Trichlorophenol mg/kg NDND
2,4,6-Trichlorophenol mg/kg NDND
2,4-Dichlorophenol mg/kg NDND
2,4-Dimethylphenol mg/kg NDND
2,4-Dinitrophenol mg/kg NDND
2,4-Dinitrotoluene mg/kg NDND
2,6-Dinitrotoluene mg/kg NDND
2-Chloronaphthalene mg/kg NDND
2-Chlorophenol mg/kg NDND
2-Methylnaphthalene mg/kg NDND
2-Methylphenol(o-Cresol)mg/kg NDND
2-Nitroaniline mg/kg NDND
2-Nitrophenol mg/kg NDND
3&4-Methylphenol(m&p Cresol)mg/kg NDND
3,3'-Dichlorobenzidine mg/kg ND ILND
3-Nitroaniline mg/kg NDND
4,6-Dinitro-2-methylphenol mg/kg NDND
4-Bromophenylphenyl ether mg/kg NDND
4-Chloro-3-methylphenol mg/kg NDND
4-Chloroaniline mg/kg NDND
4-Chlorophenylphenyl ether mg/kg NDND
4-Nitroaniline mg/kg NDND
4-Nitrophenol mg/kg NDND
Acenaphthene mg/kg NDND
Acenaphthylene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92597196010
3603713SAMPLE DUPLICATE:
Aniline mg/kg NDND
Anthracene mg/kg NDND
Benzo(a)anthracene mg/kg NDND
Benzo(a)pyrene mg/kg NDND
Benzo(b)fluoranthene mg/kg NDND
Benzo(g,h,i)perylene mg/kg NDND
Benzo(k)fluoranthene mg/kg NDND
Benzoic Acid mg/kg NDND
Benzyl alcohol mg/kg NDND
bis(2-Chloroethoxy)methane mg/kg NDND
bis(2-Chloroethyl) ether mg/kg NDND
bis(2-Ethylhexyl)phthalate mg/kg NDND
Butylbenzylphthalate mg/kg NDND
Chrysene mg/kg NDND
Di-n-butylphthalate mg/kg NDND
Di-n-octylphthalate mg/kg ND v1ND
Dibenz(a,h)anthracene mg/kg NDND
Dibenzofuran mg/kg NDND
Diethylphthalate mg/kg ND v1ND
Dimethylphthalate mg/kg NDND
Fluoranthene mg/kg NDND
Fluorene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Hexachlorobenzene mg/kg NDND
Hexachlorocyclopentadiene mg/kg NDND
Hexachloroethane mg/kg NDND
Indeno(1,2,3-cd)pyrene mg/kg NDND
Isophorone mg/kg NDND
N-Nitroso-di-n-propylamine mg/kg NDND
N-Nitrosodimethylamine mg/kg NDND
N-Nitrosodiphenylamine mg/kg NDND
Naphthalene mg/kg NDND
Nitrobenzene mg/kg NDND
Pentachlorophenol mg/kg NDND
Phenanthrene mg/kg NDND
Phenol mg/kg NDND
Pyrene mg/kg NDND
Pyridine mg/kg NDND
2,4,6-Tribromophenol (S)%8685
2-Fluorobiphenyl (S)%6874
2-Fluorophenol (S)%5363
Nitrobenzene-d5 (S)%5565
Phenol-d6 (S)%5361
Terphenyl-d14 (S)%105101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
689835
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92597264001, 92597264002, 92597264003, 92597264004
Parameter Units
Dup
Result QualifiersRPDResult
92597222005
3604702SAMPLE DUPLICATE:
Percent Moisture %14.2 N2313.8
Parameter Units
Dup
Result QualifiersRPDResult
92597065002
3604703SAMPLE DUPLICATE:
Percent Moisture %36.9 N21342.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 37
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1846408
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92597264004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3780064-1
Associated Lab Samples:92597264004
Matrix:Solid
Analyzed
Total Solids %0.00200 04/11/22 15:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3780064-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result QualifiersRPDResult
L1480219-01
R3780064-3SAMPLE DUPLICATE:
Total Solids %83.3 3.8486.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 37
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 92597264004
TPH by Method MADEPE - Surrogate failure due to matrix interference[1]
ANALYTE QUALIFIERS
Analyte is a possible laboratory contaminant (not present in method blank).C7
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 37
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
ANALYTE QUALIFIERS
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
Surrogate recovery was below laboratory control limits. Results may be biased low.SR
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 37
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92597264
CRM UST REMOVAL 2
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92597264004 1846573 1846573UST-2-SW4-B MA DEP/NJ DEP MADEP EPH
92597264001 689926 690001DISPENSER-1 EPA 3546 EPA 8015C
92597264002 689926 690001UST-3-A EPA 3546 EPA 8015C
92597264003 689926 690001UST-3-B EPA 3546 EPA 8015C
92597264001 689831 689837DISPENSER-1 EPA 5030B EPA 8015C
92597264002 689831 689837UST-3-A EPA 5030B EPA 8015C
92597264003 689831 689837UST-3-B EPA 5030B EPA 8015C
92597264004 692335 692354UST-2-SW4-B MADEP VPH MADEP VPH
92597264004 689627 689767UST-2-SW4-B EPA 3546 EPA 8270E
92597264004 690146 690172UST-2-SW4-B EPA 5035A/5030B EPA 8260D
92597264001 689835DISPENSER-1 SW-846
92597264002 689835UST-3-A SW-846
92597264003 689835UST-3-B SW-846
92597264004 689835UST-2-SW4-B SW-846
92597264004 1846408 1846408UST-2-SW4-B SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2022 04:29 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 37
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