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HomeMy WebLinkAboutMO-5392_18748_M_RP_20170620 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 June 20, 2017 Mr. Brad Newton NCDEQ-DWM-UST Section Mooresville Regional Office 610 East Center Avenue Mooresville, NC 28115 Re: Water Supply Well Sampling Results Gate #402 2520 Bessemer City Road Bessemer City, Gaston County, NC Ground Water Incident Number: 18748 GRI Project Number: 2451 Dear Mr. Newton: Please find enclosed the referenced analytical results for three water supply wells sampled on June 8, 2017. This sampling event was conducted per Task Authorization #18748-57 dated March 28, 2017, for the above mentioned site. Geological Resources, Inc. sampled WSW-4 at 1053 Dallas-Bessemer City Highway, Bessemer City, NC, WSW-9 at 523 Oates Road, Gastonia, NC and WSW-10 at 101 Fraley Road, Gastonia, NC. Estimated concentrations of benzene, MTBE, tetrachloroethylene, methyl chloride and chloroform that did not exceed the 2L Standards were reported in the water supply well samples collected from WSW-4, WSW-9 and WSW-10. The concentration of 1,2-dichloroethane detected in the sample collected from WSW-4 exceeded the Maximum Allowable Concentration but did not exceed the Maximum Contaminant Level for drinking water. If you have any questions, please contact me at (704) 845-4010. Sincerely, Geological Resources, Inc. W. Scott Ball Sr. Project Manager enclosures cc: Ms. Marlene Talley, Gate Petroleum Company Mr. Ken Czoer, Applied Science and Engineering file 06/16/17 Technical Report for GRI (Geological Resources Inc.) Gate 402; 2520 Bessemer City Rd, Bessemer City, NC 18748/2451 SGS Accutest Job Number: FA44847 Sampling Date: 06/08/17 Report to: GRI 3502 Hayes Rd Monroe, NC 28110 wsb@geologicalresourcesinc.com; carriekennedy@geologicalresourcesinc.com; jjr@geologicalresourcesinc.com; nml@geologicalresourcesinc.com; ATTN: Michael Senglaub Total number of pages in report: Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(L-A-B L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest. Test results relate only to samples analyzed. Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 • http://www.accutest.com Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Muna Mohammed 407-425-6700 Norm Farmer Technical Director Southeast 06/16/17 e-Hardcopy 2.0 Automated Report 22 SGS Accutest is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. Review standard terms at: http://www.sgs.com/en/terms-and-conditions 1 of 22 FA44847 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................3 Section 2: Summary of Hits ....................................................................................................4 Section 3: Sample Results ........................................................................................................5 3.1: FA44847-1: WSW-4 .....................................................................................................6 3.2: FA44847-2: WSW-9 .....................................................................................................8 3.3: FA44847-3: WSW-10 ...................................................................................................10 Section 4: Misc. Forms ............................................................................................................12 4.1: Chain of Custody ...........................................................................................................13 Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................15 5.1: Method Blank Summary ................................................................................................16 5.2: Blank Spike Summary ...................................................................................................18 5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................20 123452 of 22 FA44847 SGS Accutest Sample Summary GRI (Geological Resources Inc.) Job No:FA44847 Gate 402; 2520 Bessemer City Rd, Bessemer City, NC Project No: 18748/2451 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA44847-1 06/08/17 10:53 CB 06/10/17 AQ Ground Water WSW-4 FA44847-2 06/08/17 07:22 CB 06/10/17 AQ Ground Water WSW-9 FA44847-3 06/08/17 07:16 CB 06/10/17 AQ Ground Water WSW-10 3 of 22 FA448471 Summary of Hits Page 1 of 1 Job Number:FA44847 Account:GRI (Geological Resources Inc.) Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC Collected:06/08/17 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA44847-1 WSW-4 Benzene 0.26 J 0.50 0.13 ug/l SM 6200B 1,2-Dichloroethane 0.50 0.50 0.13 ug/l SM 6200B Methyl Tert Butyl Ether 0.18 J 0.50 0.13 ug/l SM 6200B Tetrachloroethylene 0.35 J 0.50 0.13 ug/l SM 6200B FA44847-2 WSW-9 Chloroform 0.36 J 0.50 0.13 ug/l SM 6200B Tetrachloroethylene 0.25 J 0.50 0.13 ug/l SM 6200B FA44847-3 WSW-10 Methyl Chloride 0.22 J 0.50 0.20 ug/l SM 6200B Tetrachloroethylene 0.32 J 0.50 0.13 ug/l SM 6200B 4 of 22 FA448472 SGS Accutest Sample Results Report of Analysis Southeast Section 3 5 of 22 FA448473 SGS Accutest Report of Analysis Page 1 of 2 Client Sample ID:WSW-4 Lab Sample ID:FA44847-1 Date Sampled:06/08/17 Matrix:AQ - Ground Water Date Received:06/10/17 Method:SM 6200B Percent Solids:n/a Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E053392.D 1 06/15/17 17:26 TD n/a n/a VE1779 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene 0.26 0.50 0.13 ug/l J 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane 0.50 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 of 22 FA4484733.1 SGS Accutest Report of Analysis Page 2 of 2 Client Sample ID:WSW-4 Lab Sample ID:FA44847-1 Date Sampled:06/08/17 Matrix:AQ - Ground Water Date Received:06/10/17 Method:SM 6200B Percent Solids:n/a Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 0.18 0.50 0.13 ug/l J 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene 0.35 0.50 0.13 ug/l J 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 98%70-130% 17060-07-0 1,2-Dichloroethane-D4 100%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 102%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 22 FA4484733.1 SGS Accutest Report of Analysis Page 1 of 2 Client Sample ID:WSW-9 Lab Sample ID:FA44847-2 Date Sampled:06/08/17 Matrix:AQ - Ground Water Date Received:06/10/17 Method:SM 6200B Percent Solids:n/a Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E053393.D 1 06/15/17 17:49 TD n/a n/a VE1779 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform 0.36 0.50 0.13 ug/l J 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 of 22 FA4484733.2 SGS Accutest Report of Analysis Page 2 of 2 Client Sample ID:WSW-9 Lab Sample ID:FA44847-2 Date Sampled:06/08/17 Matrix:AQ - Ground Water Date Received:06/10/17 Method:SM 6200B Percent Solids:n/a Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene 0.25 0.50 0.13 ug/l J 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 98%70-130% 17060-07-0 1,2-Dichloroethane-D4 99%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 103%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9 of 22 FA4484733.2 SGS Accutest Report of Analysis Page 1 of 2 Client Sample ID:WSW-10 Lab Sample ID:FA44847-3 Date Sampled:06/08/17 Matrix:AQ - Ground Water Date Received:06/10/17 Method:SM 6200B Percent Solids:n/a Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 E053394.D 1 06/15/17 18:11 TD n/a n/a VE1779 Run #2 Purge Volume Run #1 10.0 ml Run #2 VOA 6200B List CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 22 FA4484733.3 SGS Accutest Report of Analysis Page 2 of 2 Client Sample ID:WSW-10 Lab Sample ID:FA44847-3 Date Sampled:06/08/17 Matrix:AQ - Ground Water Date Received:06/10/17 Method:SM 6200B Percent Solids:n/a Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC VOA 6200B List CAS No.Compound Result RL MDL Units Q 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride 0.22 0.50 0.20 ug/l J 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene 0.32 0.50 0.13 ug/l J 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 97%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 96%70-130% 460-00-4 4-Bromofluorobenzene 103%70-130% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 22 FA4484733.3 SGS Accutest Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Southeast Section 4 12 of 22 FA448474 FA44847: Chain of Custody Page 1 of 2 13 of 22 FA4484744.1 Job Number:FA44847 Client:GRI Date / Time Received:6/10/2017 9:45:00 AM Delivery Method:FED EX Project:GATE 402 Airbill #'s:8054 3409 6157 Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 4. Cooler temp verification 3. Temp criteria achieved 5. Cooler media IR Gun Ice (Bag) Trip Blank Information 1. Trip Blank present / cooler 2. Trip Blank listed on COC 2. Samples preserved properly Sample Information 1. Sample labels present on bottles 5. Sample recvd within HT 4. Condition of sample 3. Sufficient volume/containers recvd for analysis: Intact Comments SM001Rev. Date 05/24/17 SGS Accutest Sample Receipt Summary Cooler Temps (Raw Measured) °C: Cooler Temps (Corrected) °C: Cooler 1: (3.3); Cooler 1: (3.7); 3. Type Of TB Received W or S N/A 6. Dates/Times/IDs on COC match Sample Label 7. VOCs have headspace 8. Bottles received for unspecified tests 9. Compositing instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? Misc. Information 25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals: Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify) Y or N N/A Y or N Therm ID:IR 1; Therm CF:0.4; # of Coolers:1 Y or N N/A 12. Residual Chlorine Present? Residual Chlorine Test Strip Lot #: Technician:Reviewer:SHAYLAP PDS Date:6/13/2017Date:6/10/2017 9:45:00 AM FA44847: Chain of Custody Page 2 of 2 14 of 22 FA4484744.1 SGS Accutest GC/MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Southeast Section 5 15 of 22 FA448475 Method Blank Summary Page 1 of 2 Job Number:FA44847 Account:GRINCC GRI (Geological Resources Inc.) Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE1779-MB E053385.D 1 06/15/17 TD n/a n/a VE1779 The QC reported here applies to the following samples:Method: SM 6200B FA44847-1, FA44847-2, FA44847-3 CAS No.Compound Result RL MDL Units Q 71-43-2 Benzene ND 0.50 0.13 ug/l 108-86-1 Bromobenzene ND 0.50 0.13 ug/l 74-97-5 Bromochloromethane ND 0.50 0.13 ug/l 75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l 75-25-2 Bromoform ND 0.50 0.13 ug/l 104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l 135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l 98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l 56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l 108-90-7 Chlorobenzene ND 0.50 0.13 ug/l 75-00-3 Chloroethane ND 0.50 0.20 ug/l 67-66-3 Chloroform ND 0.50 0.13 ug/l 95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l 106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l 124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l 96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l 106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l 75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l 95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l 541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l 106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l 75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l 107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l 75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l 156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l 156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l 78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l 142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l 594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l 563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l 10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l 10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l 108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l 100-41-4 Ethylbenzene ND 0.50 0.13 ug/l 87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l 98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l 16 of 22 FA4484755.1.1 Method Blank Summary Page 2 of 2 Job Number:FA44847 Account:GRINCC GRI (Geological Resources Inc.) Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE1779-MB E053385.D 1 06/15/17 TD n/a n/a VE1779 The QC reported here applies to the following samples:Method: SM 6200B FA44847-1, FA44847-2, FA44847-3 CAS No.Compound Result RL MDL Units Q 99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l 74-83-9 Methyl Bromide ND 0.50 0.20 ug/l 74-87-3 Methyl Chloride ND 0.50 0.20 ug/l 74-95-3 Methylene Bromide ND 0.50 0.13 ug/l 75-09-2 Methylene Chloride ND 2.0 1.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l 91-20-3 Naphthalene ND 0.50 0.13 ug/l 103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l 100-42-5 Styrene ND 0.50 0.13 ug/l 630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l 79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l 127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l 108-88-3 Toluene ND 0.50 0.13 ug/l 87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l 120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l 71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l 79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l 79-01-6 Trichloroethylene ND 0.50 0.13 ug/l 75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l 96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l 95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l 108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l 75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l m,p-Xylene ND 1.0 0.13 ug/l 95-47-6 o-Xylene ND 0.50 0.13 ug/l 1330-20-7 Xylene (total)ND 1.5 0.25 ug/l CAS No.Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 96%70-130% 17060-07-0 1,2-Dichloroethane-D4 102%70-130% 2037-26-5 Toluene-D8 104%70-130% 460-00-4 4-Bromofluorobenzene 105%70-130% 17 of 22 FA4484755.1.1 Blank Spike Summary Page 1 of 2 Job Number:FA44847 Account:GRINCC GRI (Geological Resources Inc.) Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE1779-BS E053384.D 1 06/15/17 TD n/a n/a VE1779 The QC reported here applies to the following samples:Method: SM 6200B FA44847-1, FA44847-2, FA44847-3 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 71-43-2 Benzene 10 10.0 100 70-130 108-86-1 Bromobenzene 10 10.4 104 70-130 74-97-5 Bromochloromethane 10 10.2 102 70-130 75-27-4 Bromodichloromethane 10 10.0 100 70-130 75-25-2 Bromoform 10 9.2 92 70-130 104-51-8 n-Butylbenzene 10 10.1 101 70-130 135-98-8 sec-Butylbenzene 10 10.1 101 70-130 98-06-6 tert-Butylbenzene 10 10.2 102 70-130 56-23-5 Carbon Tetrachloride 10 10.8 108 70-130 108-90-7 Chlorobenzene 10 9.8 98 70-130 75-00-3 Chloroethane 10 9.0 90 60-140 67-66-3 Chloroform 10 9.4 94 70-130 95-49-8 o-Chlorotoluene 10 10.1 101 70-130 106-43-4 p-Chlorotoluene 10 10.2 102 70-130 124-48-1 Dibromochloromethane 10 9.7 97 70-130 96-12-8 1,2-Dibromo-3-chloropropane 10 10.4 104 70-130 106-93-4 1,2-Dibromoethane 10 10.5 105 70-130 75-71-8 Dichlorodifluoromethane 10 9.6 96 60-140 95-50-1 1,2-Dichlorobenzene 10 10.2 102 70-130 541-73-1 1,3-Dichlorobenzene 10 10.1 101 70-130 106-46-7 1,4-Dichlorobenzene 10 9.9 99 70-130 75-34-3 1,1-Dichloroethane 10 10.2 102 70-130 107-06-2 1,2-Dichloroethane 10 10.4 104 70-130 75-35-4 1,1-Dichloroethylene 10 10.3 103 70-130 156-59-2 cis-1,2-Dichloroethylene 10 10.4 104 70-130 156-60-5 trans-1,2-Dichloroethylene 10 10.3 103 70-130 78-87-5 1,2-Dichloropropane 10 10.2 102 70-130 142-28-9 1,3-Dichloropropane 10 10.4 104 70-130 594-20-7 2,2-Dichloropropane 10 10.8 108 70-130 563-58-6 1,1-Dichloropropene 10 10.4 104 70-130 10061-01-5 cis-1,3-Dichloropropene 10 9.4 94 70-130 10061-02-6 trans-1,3-Dichloropropene 10 9.4 94 70-130 108-20-3 Di-Isopropyl Ether 10 10.4 104 70-130 100-41-4 Ethylbenzene 10 10.3 103 70-130 87-68-3 Hexachlorobutadiene 10 10.6 106 70-130 98-82-8 Isopropylbenzene 10 10.1 101 70-130 * = Outside of Control Limits. 18 of 22 FA4484755.2.1 Blank Spike Summary Page 2 of 2 Job Number:FA44847 Account:GRINCC GRI (Geological Resources Inc.) Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch VE1779-BS E053384.D 1 06/15/17 TD n/a n/a VE1779 The QC reported here applies to the following samples:Method: SM 6200B FA44847-1, FA44847-2, FA44847-3 Spike BSP BSP CAS No.Compound ug/l ug/l %Limits 99-87-6 p-Isopropyltoluene 10 10.1 101 70-130 74-83-9 Methyl Bromide 10 10.1 101 60-140 74-87-3 Methyl Chloride 10 9.7 97 60-140 74-95-3 Methylene Bromide 10 10.2 102 70-130 75-09-2 Methylene Chloride 10 11.0 110 70-130 1634-04-4 Methyl Tert Butyl Ether 10 10.6 106 70-130 91-20-3 Naphthalene 10 11.0 110 70-130 103-65-1 n-Propylbenzene 10 10.0 100 70-130 100-42-5 Styrene 10 9.9 99 70-130 630-20-6 1,1,1,2-Tetrachloroethane 10 10.5 105 70-130 79-34-5 1,1,2,2-Tetrachloroethane 10 10.1 101 70-130 127-18-4 Tetrachloroethylene 10 10.5 105 70-130 108-88-3 Toluene 10 10.2 102 70-130 87-61-6 1,2,3-Trichlorobenzene 10 10.9 109 70-130 120-82-1 1,2,4-Trichlorobenzene 10 11.0 110 70-130 71-55-6 1,1,1-Trichloroethane 10 10.6 106 70-130 79-00-5 1,1,2-Trichloroethane 10 10.3 103 70-130 79-01-6 Trichloroethylene 10 10 100 70-130 75-69-4 Trichlorofluoromethane 10 9.6 96 60-140 96-18-4 1,2,3-Trichloropropane 10 10.3 103 70-130 95-63-6 1,2,4-Trimethylbenzene 10 10.1 101 70-130 108-67-8 1,3,5-Trimethylbenzene 10 10.1 101 70-130 75-01-4 Vinyl Chloride 10 9.6 96 60-140 m,p-Xylene 20 20.4 102 70-130 95-47-6 o-Xylene 10 10.3 103 70-130 1330-20-7 Xylene (total)30 30.8 103 70-130 CAS No.Surrogate Recoveries BSP Limits 1868-53-7 Dibromofluoromethane 100%70-130% 17060-07-0 1,2-Dichloroethane-D4 101%70-130% 2037-26-5 Toluene-D8 102%70-130% 460-00-4 4-Bromofluorobenzene 101%70-130% * = Outside of Control Limits. 19 of 22 FA4484755.2.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number:FA44847 Account:GRINCC GRI (Geological Resources Inc.) Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA44845-1MS E053403.D 50 06/15/17 TD n/a n/a VE1779 FA44845-1MSD E053404.D 50 06/15/17 TD n/a n/a VE1779 FA44845-1 a E053387.D 25 06/15/17 TD n/a n/a VE1779 FA44845-1 a E053396.D 50 06/15/17 TD n/a n/a VE1779 The QC reported here applies to the following samples:Method: SM 6200B FA44847-1, FA44847-2, FA44847-3 FA44845-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 71-43-2 Benzene 1790 b 500 2320 106 500 2160 74 7 70-130/20 108-86-1 Bromobenzene ND 500 510 102 500 473 95 8 70-130/20 74-97-5 Bromochloromethane ND 500 475 95 500 432 86 9 70-130/20 75-27-4 Bromodichloromethane ND 500 463 93 500 438 88 6 70-130/20 75-25-2 Bromoform ND 500 327 65*500 341 68*4 70-130/20 104-51-8 n-Butylbenzene ND 500 506 101 500 464 93 9 70-130/20 135-98-8 sec-Butylbenzene ND 500 532 106 500 494 99 7 70-130/20 98-06-6 tert-Butylbenzene ND 500 524 105 500 488 98 7 70-130/20 56-23-5 Carbon Tetrachloride ND 500 491 98 500 475 95 3 70-130/20 108-90-7 Chlorobenzene ND 500 501 100 500 461 92 8 70-130/20 75-00-3 Chloroethane ND 500 510 102 500 522 104 2 60-140/20 67-66-3 Chloroform ND 500 466 93 500 428 86 9 70-130/20 95-49-8 o-Chlorotoluene ND 500 515 103 500 477 95 8 70-130/20 106-43-4 p-Chlorotoluene ND 500 518 104 500 483 97 7 70-130/20 124-48-1 Dibromochloromethane ND 500 392 78 500 389 78 1 70-130/20 96-12-8 1,2-Dibromo-3-chloropropane ND 500 441 88 500 421 84 5 70-130/20 106-93-4 1,2-Dibromoethane ND 500 502 100 500 464 93 8 70-130/20 75-71-8 Dichlorodifluoromethane ND 500 434 87 500 442 88 2 60-140/20 95-50-1 1,2-Dichlorobenzene ND 500 511 102 500 465 93 9 70-130/20 541-73-1 1,3-Dichlorobenzene ND 500 515 103 500 473 95 9 70-130/20 106-46-7 1,4-Dichlorobenzene ND 500 493 99 500 456 91 8 70-130/20 75-34-3 1,1-Dichloroethane ND 500 530 106 500 486 97 9 70-130/20 107-06-2 1,2-Dichloroethane ND 500 505 101 500 465 93 8 70-130/20 75-35-4 1,1-Dichloroethylene ND 500 507 101 500 469 94 8 70-130/20 156-59-2 cis-1,2-Dichloroethylene ND 500 495 99 500 456 91 8 70-130/20 156-60-5 trans-1,2-Dichloroethylene ND 500 564 113 500 510 102 10 70-130/20 78-87-5 1,2-Dichloropropane ND 500 493 99 500 461 92 7 70-130/20 142-28-9 1,3-Dichloropropane ND 500 469 94 500 436 87 7 70-130/20 594-20-7 2,2-Dichloropropane ND 500 507 101 500 453 91 11 70-130/20 563-58-6 1,1-Dichloropropene ND 500 494 99 500 445 89 10 70-130/20 10061-01-5 cis-1,3-Dichloropropene ND 500 390 78 500 388 78 1 70-130/20 10061-02-6 trans-1,3-Dichloropropene ND 500 414 83 500 414 83 0 70-130/20 108-20-3 Di-Isopropyl Ether 58.3 500 559 100 500 513 91 9 70-130/20 100-41-4 Ethylbenzene 34.6 500 552 103 500 507 94 8 70-130/20 87-68-3 Hexachlorobutadiene ND 500 510 102 500 478 96 6 70-130/20 98-82-8 Isopropylbenzene 4.1 J 500 544 108 500 490 97 10 70-130/20 * = Outside of Control Limits. 20 of 22 FA4484755.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3 Job Number:FA44847 Account:GRINCC GRI (Geological Resources Inc.) Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA44845-1MS E053403.D 50 06/15/17 TD n/a n/a VE1779 FA44845-1MSD E053404.D 50 06/15/17 TD n/a n/a VE1779 FA44845-1 a E053387.D 25 06/15/17 TD n/a n/a VE1779 FA44845-1 a E053396.D 50 06/15/17 TD n/a n/a VE1779 The QC reported here applies to the following samples:Method: SM 6200B FA44847-1, FA44847-2, FA44847-3 FA44845-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD 99-87-6 p-Isopropyltoluene ND 500 524 105 500 483 97 8 70-130/20 74-83-9 Methyl Bromide ND 500 545 109 500 578 116 6 60-140/20 74-87-3 Methyl Chloride ND 500 500 100 500 509 102 2 60-140/20 74-95-3 Methylene Bromide ND 500 503 101 500 463 93 8 70-130/20 75-09-2 Methylene Chloride ND 500 562 112 500 474 95 17 70-130/20 1634-04-4 Methyl Tert Butyl Ether 508 500 1030 104 500 945 87 9 70-130/20 91-20-3 Naphthalene 26.2 500 614 118 500 545 104 12 70-130/20 103-65-1 n-Propylbenzene 9.1 J 500 535 105 500 494 97 8 70-130/20 100-42-5 Styrene ND 500 478 96 500 448 90 6 70-130/20 630-20-6 1,1,1,2-Tetrachloroethane ND 500 513 103 500 479 96 7 70-130/20 79-34-5 1,1,2,2-Tetrachloroethane ND 500 486 97 500 449 90 8 70-130/20 127-18-4 Tetrachloroethylene ND 500 518 104 500 484 97 7 70-130/20 108-88-3 Toluene 20.3 500 534 103 500 488 94 9 70-130/20 87-61-6 1,2,3-Trichlorobenzene ND 500 474 95 500 467 93 1 70-130/20 120-82-1 1,2,4-Trichlorobenzene ND 500 508 102 500 487 97 4 70-130/20 71-55-6 1,1,1-Trichloroethane ND 500 504 101 500 458 92 10 70-130/20 79-00-5 1,1,2-Trichloroethane ND 500 501 100 500 467 93 7 70-130/20 79-01-6 Trichloroethylene ND 500 514 103 500 476 95 8 70-130/20 75-69-4 Trichlorofluoromethane ND 500 543 109 500 551 110 1 60-140/20 96-18-4 1,2,3-Trichloropropane ND 500 498 100 500 467 93 6 70-130/20 95-63-6 1,2,4-Trimethylbenzene 5.0 J 500 530 105 500 481 95 10 70-130/20 108-67-8 1,3,5-Trimethylbenzene ND 500 508 102 500 467 93 8 70-130/20 75-01-4 Vinyl Chloride ND 500 487 97 500 495 99 2 60-140/20 m,p-Xylene 48.1 1000 1100 105 1000 1010 96 9 70-130/20 95-47-6 o-Xylene 6.0 J 500 539 107 500 491 97 9 70-130/20 1330-20-7 Xylene (total)54.0 1500 1640 106 1500 1500 96 9 70-130/20 CAS No.Surrogate Recoveries MS MSD FA44845-1 FA44845-1 Limits 1868-53-7 Dibromofluoromethane 98%98%97%95%70-130% 17060-07-0 1,2-Dichloroethane-D4 98%98%101%100%70-130% 2037-26-5 Toluene-D8 101%101%103%102%70-130% 460-00-4 4-Bromofluorobenzene 101%101%104%103%70-130% (a) Sample was not preserved to a pH < 2; reported results are considered minimum values. * = Outside of Control Limits. 21 of 22 FA4484755.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3 Job Number:FA44847 Account:GRINCC GRI (Geological Resources Inc.) Project:Gate 402; 2520 Bessemer City Rd, Bessemer City, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA44845-1MS E053403.D 50 06/15/17 TD n/a n/a VE1779 FA44845-1MSD E053404.D 50 06/15/17 TD n/a n/a VE1779 FA44845-1 a E053387.D 25 06/15/17 TD n/a n/a VE1779 FA44845-1 a E053396.D 50 06/15/17 TD n/a n/a VE1779 The QC reported here applies to the following samples:Method: SM 6200B FA44847-1, FA44847-2, FA44847-3 (b) Result is from Run #2. * = Outside of Control Limits. 22 of 22 FA4484755.3.1