25032_Domestic Laundry_Construction Fill Export Approval Package_20230127

January 27, 2023

Sent Via E-mail
Bennett Thompson & Steven Garrett The Charlotte-Mecklenburg Hospital Authority P.O. Box 32861 Charlotte, NC 28232-2861
[e-mail] [e-mail] Subject: Construction Fill Export Approval
Domestic Laundry Brownfields Project Charlotte, Mecklenburg County Brownfields Project Number 25032-21-060 Dear Mr. Thompson and Mr. Garrett,
The North Carolina Department of Environmental Quality’s Brownfields Redevelopment Section (DEQ Brownfields) received a request to export approximately 1,500 cubic yards of construction and demolition fill material from the former Domestic Laundry Brownfields Property. This email request was submitted on your behalf by Ms. Amy Kenwell with Geosyntec Consultants of NC,
P.C., on January 26, 2023, and requests approval to export the fill to Republic Services’ Charlotte Motor Speedway Landfill in Concord, North Carolina. For this request, DEQ Brownfields reviewed the January 26, 2023 email and the analytical report. Based on our review of the data, the DEQ Brownfield determines that the construction fill
material may be exported to Republic Services’ Charlotte Motor Speedway Landfill in Concord, North Carolina. If another export facility is selected, please contact us and we will assist you in determining if additional sampling is needed for the receiving facility.
In accordance with the approved Environmental Management Plan (EMP), materials are to be field screened during excavation prior to export from the property. If unanticipated impacts are
identified during excavation, please refer to the EMP for further actions and cease transfer until appropriate characterization can be completed. In addition, and also in accordance with the site’s approved EMP, an annual Redevelopment Summary Report will be submitted to DEQ Brownfields. Details related to the disposition of the fill including but not limited to, total volume, general description of field screening efforts, etc. should be included with the Redevelopment
Summary Report.
Mr. Thompson and Mr. Garrett January 27, 2023 Page 2

Please be advised that this approval does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local entities. If you have questions about this correspondence or require additional information, please feel free to contact Pete Doorn by phone at 984-275-5391 or by email at [e-mail].

Sincerely,
Peter L. Doorn, Project Manager
Brownfields Program
ec: Amy Kenwell, Geosyntec Consultants of NC Jeff Tyburzski, Geosyntec Consultants of NC
Jeff Ahrens, Geosyntec Consultants of NC
McKenzie Publicover, Kimley Horn & Associates Ryan Lewis, Kimley-Horn & Associates Tracy Wahl, DEQ Brownfields Program
1
Doorn, Peter L
From:Amy Kenwell <[e-mail]>
Sent:Thursday, January 26, 2023 3:12 PM
To:Doorn, Peter L
Cc:Jeff Ahrens; Jeff Tyburski; 'Publicover, McKenzie'; Lewis, Ryan
Subject:[External] RE: Former Domestic Laundry (25032-21-060) Fill Materials
Attachments:23A0886_2 EA_Level2 01 25 2023 1637.pdf
Follow Up Flag:Follow up
Flag Status:Completed
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Report Spam.

Good afternoon Pete,

We’ve received the analytical results back from these fill materials (attached) and request permission for disposal at
Republic Services’ Charlotte Motor Speedway landfill in Concord, NC. We estimate up to 1,500 cy now that the removal
is complete and it is in a loose pile.

Thank you,
Amy

Amy Kenwell, P.G. (NC, SC)
Senior Geologist
Geosyntec Consultants of NC, P.C.
1300 S. Mint Street, Suite 300
Charlotte, North Carolina 28203
Phone: [phone] (x2843) Mobile: [phone]

From: Amy Kenwell
Sent: Thursday, January 19, 2023 12:22 PM
To: Doorn, Peter L <[e-mail]>
Cc: Jeff Ahrens <[e-mail]>; Jeff Tyburski <[e-mail]>; 'Publicover, McKenzie'
<[e-mail]>; Lewis, Ryan <[e-mail]>
Subject: Former Domestic Laundry (25032-21-060) Fill Materials

Good afternoon Pete,

As we discussed Tuesday, additional construction and demolition fill material (containing asphalt, concrete, and railroad
ties) was encountered at the Former Domestic Laundry Brownfields Property on 16 January 2023. The fill is located
adjacent to Baxter Street at 801 South McDowell Street just south of Area A. We estimate that approximately 750 cy will
be excavated and stockpiled in accordance with EMP-1. There was no evidence of staining and the photoionization
detector did not detect evidence of volatiles. We have collected a sample of the soils to characterize the materials for
disposal. I’ll let you know once we have those results.

Thank you,
Amy
2

Amy Kenwell, P.G. (NC, SC)
Senior Geologist
Geosyntec Consultants of NC, P.C.
1300 S. Mint Street, Suite 300
Charlotte, North Carolina 28203
Phone: [phone] (x2843) Mobile: [phone]

1941 Reymet Road l Richmond, Virginia 23237 l Tel: [phone] Fax: [phone]
Laboratory Order ID 23A0886
Certificate of Analysis
Client Name:
Enclosed are the results of analyses for samples received by the laboratory on 01/19/2023 09:24. If you have
any questions concerning this report, please feel free to contact the laboratory.
Sincerely,
Ted Soyars
Technical Director
Charlotte, NC 28203
1300 S. Mint Street, Suite 300
Purchase Order:
[none]Project Number:
Date Issued:
Date Received:
Submitted To:
Client Site I.D.:
January 25, 2023 16:37
January 19, 2023 9:24Geosyntec Consultants - Charlotte, NC
Amy Kenwell
End Notes:
The test results listed in this report relate only to the samples submitted to the laboratory and as received by the Laboratory.
Unless otherwise noted, the test results for solid materials are calculated on a wet weight basis. Analyses for pH, dissolved oxygen,
temperature, residual chlorine and sulfite that are performed in the laboratory do not meet NELAC requirements due to extremely
short holding times. These analyses should be performed in the field. The results of field analyses performed by the Sampler
included in the Certificate of Analysis are done so at the client’s request and are not included in the laboratory’s fields of certification
nor have they been audited for adherence to a reference method or procedure.
The signature on the final report certifies that these results conform to all applicable NELAC standards unless otherwise specified.
For a complete list of the Laboratory’s NELAC certified parameters please contact customer service.
This report shall not be reproduced except in full without the expressed and written approval of an authorized representative of
Enthalpy Analytical.
Project Lookout
Final Report
Page 1 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
ANALYTICAL REPORT FOR SAMPLES
Laboratory Order ID 23A0886
MatrixSample ID Laboratory ID Date Sampled Date Received
BAXTERFILL-G-20230118 23A0886-01 01/19/2023 09:24Solids01/18/2023 09:20
BAXTERFILL-C-20230118 23A0886-02 01/19/2023 09:24Solids01/18/2023 09:20
Page 2 of 28
Page 2 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Laboratory Order ID: 23A0886
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
BAXTERFILL-G-20230118 Laboratory Sample ID:Sample I.D.23A0886-01
Analytical Results
Grab Date/Time:01/18/2023 09:20
Field Residual Cl:Field pH:
TCLP Volatile Organic Compounds by GCMS
SW1311 1 #RJB--101 01/23/23 14:00 01/23/23 14:19TCLP Extraction Fluid, ZHE
SW8260D RJB<0.02 mg/L 0.02 101 01/24/23 00:00 01/24/23 13:32TCLP 1,1-Dichloroethylene
SW8260D RJB<0.02 mg/L 0.02 101 01/24/23 00:00 01/24/23 13:32TCLP 1,2-Dichloroethane
SW8260D RJB<0.02 mg/L 0.02 101 01/24/23 00:00 01/24/23 13:32TCLP 1,4-Dichlorobenzene
SW8260D RJB<0.20 mg/L 0.20 101 01/24/23 00:00 01/24/23 13:32TCLP 2-Butanone (MEK)
SW8260D RJB<0.05 mg/L 0.05 101 01/24/23 00:00 01/24/23 13:32TCLP Benzene
SW8260D RJB<0.02 mg/L 0.02 101 01/24/23 00:00 01/24/23 13:32TCLP Carbon tetrachloride
SW8260D RJB<0.02 mg/L 0.02 101 01/24/23 00:00 01/24/23 13:32TCLP Chlorobenzene
SW8260D RJB<0.02 mg/L 0.02 101 01/24/23 00:00 01/24/23 13:32TCLP Chloroform
SW8260D RJB<0.05 mg/L 0.05 101 01/24/23 00:00 01/24/23 13:32TCLP Tetrachloroethylene
(PCE)
SW8260D RJB<0.02 mg/L 0.02 101 01/24/23 00:00 01/24/23 13:32TCLP Trichloroethylene
SW8260D RJB<0.02 mg/L 0.02 101 01/24/23 00:00 01/24/23 13:32TCLP Vinyl chloride
70-120103 %Surr: 1,2-Dichloroethane-d4
(Surr)
RJB01SW8260D01/24/23 00:00 01/24/23 13:32
75-12098.3 %Surr: 4-Bromofluorobenzene
(Surr)
RJB01SW8260D01/24/23 00:00 01/24/23 13:32
80-119102 %Surr: Dibromofluoromethane
(Surr)
RJB01SW8260D01/24/23 00:00 01/24/23 13:32
85-120101 %Surr: Toluene-d8 (Surr)RJB01SW8260D01/24/23 00:00 01/24/23 13:32
Wet Chemistry Analysis
SM22
2540G-2011
83.3 %NBT0.10 101 01/19/23 12:25 01/19/23 12:25Percent Solids
Page 3 of 28
Page 3 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Laboratory Order ID: 23A0886
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
BAXTERFILL-C-20230118 Laboratory Sample ID:Sample I.D.23A0886-02
Analytical Results
Grab Date/Time:01/18/2023 09:20
Field Residual Cl:Field pH:
Metals (Total) by EPA 6000/7000 Series Methods
SW7471B 0.091 mg/kg SGT0.008 102 01/20/23 10:45 01/20/23 14:44Mercury
TCLP Metals by 6000/7000 Series Methods
SW6010D ACM<0.100 mg/L 0.100 102 01/20/23 10:15 01/24/23 11:29TCLP Silver
SW6010D ACM<0.100 mg/L 0.100 102 01/20/23 10:15 01/24/23 11:29TCLP Arsenic
SW6010D ACM<5.00 mg/L 5.00 102 01/20/23 10:15 01/24/23 11:29TCLP Barium
SW6010D ACM<0.0400 mg/L 0.0400 102 01/20/23 10:15 01/24/23 11:29TCLP Cadmium
SW6010D ACM<0.100 mg/L 0.100 102 01/20/23 10:15 01/24/23 11:29TCLP Chromium
SW7470A SGT<0.008 mg/L 0.008 102 01/23/23 12:00 01/23/23 16:01TCLP Mercury
SW6010D ACM<0.100 mg/L 0.100 102 01/20/23 10:15 01/24/23 11:29TCLP Lead
SW6010D ACM<0.250 mg/L 0.250 102 01/20/23 10:15 01/24/23 11:29TCLP Selenium
SW1311 1 #ESW--102 01/19/23 15:30 01/19/23 15:30TCLP Extraction Fluid,
Metals
TCLP Semivolatile Organic Compounds
SW1311 1 #ATG--102 01/19/23 15:30 01/19/23 15:30TCLP Extraction Fluid, SV
Organics
TCLP Semivolatile Organic Compounds by GCMS
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP 2,4,5-Trichlorophenol
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP 2,4,6-Trichlorophenol
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP 2,4-Dinitrotoluene
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP Hexachlorobenzene
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP Hexachlorobutadiene
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP Hexachloroethane
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP m+p-Cresols
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP Nitrobenzene
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP o+m+p-Cresols
Page 4 of 28
Page 4 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Laboratory Order ID: 23A0886
ResultParameter
Reporting
LimitMethodQual Analyst
Analysis
Date/TimeD.F. Samp ID
Sample Prep
Date/Time
BAXTERFILL-C-20230118 Laboratory Sample ID:Sample I.D.23A0886-02
Analytical Results
Grab Date/Time:01/18/2023 09:20
Field Residual Cl:Field pH:
TCLP Semivolatile Organic Compounds by GCMS
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP o-Cresol
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP Pentachlorophenol
SW8270E MGG<0.02 mg/L 0.02 102 01/20/23 09:00 01/20/23 22:13TCLP Pyridine
7-15032.2 %Surr: 2,4,6-Tribromophenol
(Surr)
MGG02SW8270E01/20/23 09:00 01/20/23 22:13
5-12534.5 %Surr: 2-Fluorobiphenyl (Surr)MGG02SW8270E01/20/23 09:00 01/20/23 22:13
5-8021.8 %Surr: 2-Fluorophenol (Surr)MGG02SW8270E01/20/23 09:00 01/20/23 22:13
5-11740.2 %Surr: Nitrobenzene-d5 (Surr)MGG02SW8270E01/20/23 09:00 01/20/23 22:13
5-6013.9 %Surr: Phenol-d5 (Surr)MGG02SW8270E01/20/23 09:00 01/20/23 22:13
19.3-15059.1 %Surr: p-Terphenyl-d14 (Surr)MGG02SW8270E01/20/23 09:00 01/20/23 22:13
Wet Chemistry Analysis
SW7196A 3.62 mg/kg dry MWL0.24 102 01/19/23 12:30 01/19/23 12:30Chromium, Hexavalent
SM22
2540G-2011
81.5 %LAM0.10 102 01/23/23 10:45 01/23/23 10:45Percent Solids
Page 5 of 28
Page 5 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Analytical Summary
Preparation Method:
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
No Prep Wet ChemPreparation Method:Wet Chemistry Analysis
23A0886-01 BGA0595 SGA0573SM22 2540G-2011 10.0 g / 10.0 mL
No Prep Wet ChemPreparation Method:Wet Chemistry Analysis
23A0886-02 BGA0678 SGA0658SM22 2540G-2011 10.0 g / 10.0 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW1311 MetalsPreparation Method:TCLP Metals by 6000/7000 Series Methods
23A0886-02 BGA0614 SGA0595SW1311 100 g / 2000 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW1311 ZHEPreparation Method:TCLP Volatile Organic Compounds by GCMS
23A0886-01 BGA0690 SGA0666SW1311 15.0 g / 300 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3010APreparation Method:TCLP Metals by 6000/7000 Series Methods
23A0886-02 BGA0626 SGA0702SW6010D AA3013010.0 mL / 50.0 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3060APreparation Method:Wet Chemistry Analysis
23A0886-02 BGA0692 SGA0680SW7196A AA301272.54 g / 100 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3510C/EPA600-MSPreparation Method:TCLP Semivolatile Organic Compounds by GCMS
23A0886-02 BGA0629 SGA0656SW8270E AI20189100 mL / 1.00 mL
Page 6 of 28
Page 6 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3580A-MSPreparation Method:TCLP Semivolatile Organic Compounds
23A0886-02 BGA0625 SGA0602SW1311 AL20040100 g / 2000 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW5030B-MSPreparation Method:TCLP Volatile Organic Compounds by GCMS
23A0886-01 BGA0724 SGA0727SW8260D AA300740.250 mL / 5.00 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW7470APreparation Method:TCLP Metals by 6000/7000 Series Methods
23A0886-02 BGA0666 SGA0682SW7470A AA301251.00 mL / 20.0 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW7471BPreparation Method:Metals (Total) by EPA 6000/7000 Series Methods
23A0886-02 BGA0620 SGA0637SW7471B AA301200.508 g / 20.0 mL
Page 7 of 28
Page 7 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
QC Analytical Summary
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
No Prep Wet ChemPreparation Method:Wet Chemistry Analysis
BGA0595-BLK1 BGA0595 SGA0573SM22 2540G-2011 10.0 g / 10.0 mL
BGA0595-DUP1 BGA0595 SGA0573SM22 2540G-2011 10.0 g / 10.0 mL
BGA0678-BLK1 BGA0678 SGA0658SM22 2540G-2011 10.0 g / 10.0 mL
BGA0678-DUP1 BGA0678 SGA0658SM22 2540G-2011 10.0 g / 10.0 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW1311 MetalsPreparation Method:TCLP Metals by 6000/7000 Series Methods
BGA0614-BLK1 BGA0614 SGA0595SW1311 100 g / 2000 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW1311 ZHEPreparation Method:TCLP Volatile Organic Compounds by GCMS
BGA0690-BLK1 BGA0690 SGA0666SW1311 15.0 g / 300 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3010APreparation Method:TCLP Metals by 6000/7000 Series Methods
BGA0626-BLK1 BGA0626 SGA0702SW6010D AA3013010.0 mL / 50.0 mL
BGA0626-BS1 BGA0626 SGA0702SW6010D AA3013010.0 mL / 50.0 mL
BGA0626-MS1 BGA0626 SGA0702SW6010D AA3013010.0 mL / 50.0 mL
BGA0626-MSD1 BGA0626 SGA0702SW6010D AA3013010.0 mL / 50.0 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3060APreparation Method:Wet Chemistry Analysis
BGA0692-BLK1 BGA0692 SGA0680SW7196A AA301272.55 g / 100 mL
BGA0692-BS1 BGA0692 SGA0680SW7196A AA301272.50 g / 100 mL
BGA0692-MS1 BGA0692 SGA0680SW7196A AA301272.51 g / 100 mL
BGA0692-MS2 BGA0692 SGA0680SW7196A AA301272.50 g / 100 mL
BGA0692-MSD1 BGA0692 SGA0680SW7196A AA301272.52 g / 100 mL
Page 8 of 28
Page 8 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3060APreparation Method:Wet Chemistry Analysis
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3510C/EPA600-MSPreparation Method:TCLP Semivolatile Organic Compounds by GCMS
BGA0629-BLK1 BGA0629 SGA0656SW8270E AI20189100 mL / 1.00 mL
BGA0629-BS1 BGA0629 SGA0656SW8270E AI20189100 mL / 1.00 mL
BGA0629-MS1 BGA0629 SGA0656SW8270E AI20189100 mL / 1.00 mL
BGA0629-MSD1 BGA0629 SGA0656SW8270E AI20189100 mL / 1.00 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW3580A-MSPreparation Method:TCLP Semivolatile Organic Compounds
BGA0625-BLK1 BGA0625 SGA0602SW1311 AL20040100 g / 2000 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW5030B-MSPreparation Method:TCLP Volatile Organic Compounds by GCMS
BGA0724-BLK1 BGA0724 SGA0727SW8260D AA300745.00 mL / 5.00 mL
BGA0724-BS1 BGA0724 SGA0727SW8260D AA300745.00 mL / 5.00 mL
BGA0724-MS1 BGA0724 SGA0727SW8260D AA300740.250 mL / 5.00 mL
BGA0724-MSD1 BGA0724 SGA0727SW8260D AA300740.250 mL / 5.00 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW7470APreparation Method:TCLP Metals by 6000/7000 Series Methods
BGA0666-BLK1 BGA0666 SGA0682SW7470A AA301251.00 mL / 20.0 mL
BGA0666-BS1 BGA0666 SGA0682SW7470A AA301251.00 mL / 20.0 mL
BGA0666-MS1 BGA0666 SGA0682SW7470A AA301251.00 mL / 20.0 mL
BGA0666-MSD1 BGA0666 SGA0682SW7470A AA301251.00 mL / 20.0 mL
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW7471BPreparation Method:Metals (Total) by EPA 6000/7000 Series Methods
BGA0620-BLK1 BGA0620 SGA0637SW7471B AA301200.509 g / 20.0 mL
BGA0620-BS1 BGA0620 SGA0637SW7471B AA301200.505 g / 20.0 mL
BGA0620-MS1 BGA0620 SGA0637SW7471B AA301200.516 g / 20.0 mL
Page 9 of 28
Page 9 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Sample ID Preparation Factors
Initial / Final Sequence ID Calibration IDBatch IDMethod
SW7471BPreparation Method:Metals (Total) by EPA 6000/7000 Series Methods
BGA0620-MSD1 BGA0620 SGA0637SW7471B AA301200.505 g / 20.0 mL
Page 10 of 28
Page 10 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals (Total) by EPA 6000/7000 Series Methods - Quality Control
Enthalpy Analytical
Batch BGA0620 - SW7471B
Blank (BGA0620-BLK1)Prepared & Analyzed: 01/20/2023
0.008 mg/kg<0.008 mg/kgMercury
LCS (BGA0620-BS1)Prepared & Analyzed: 01/20/2023
0.008 0.0990 80-12084.8mg/kg0.084 mg/kg mg/kgMercury
Matrix Spike (BGA0620-MS1)Prepared & Analyzed: 01/20/2023Source: 23A0886-02
0.008 0.0969 80-12079.6mg/kg0.168 mg/kg 0.091 mg/kgMercury M
Matrix Spike Dup (BGA0620-MSD1)Prepared & Analyzed: 01/20/2023Source: 23A0886-02
0.008 0.0990 2080-120122 22.9mg/kg0.211 mg/kg 0.091 mg/kgMercury M, P
Page 11 of 28
Page 11 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Enthalpy Analytical
Batch BGA0614 - SW1311 Metals
Blank (BGA0614-BLK1)Prepared & Analyzed: 01/19/2023
0 #1 #Extraction Fluid, Metals
Batch BGA0626 - SW3010A
Blank (BGA0626-BLK1)Prepared: 01/20/2023 Analyzed: 01/24/2023
0.100 mg/L<0.100 mg/LArsenic
5.00 mg/L<5.00 mg/LBarium
0.0400 mg/L<0.0400 mg/LCadmium
0.100 mg/L<0.100 mg/LChromium
0.100 mg/L<0.100 mg/LLead
0.250 mg/L<0.250 mg/LSelenium
0.100 mg/L<0.100 mg/LSilver
LCS (BGA0626-BS1)Prepared: 01/20/2023 Analyzed: 01/24/2023
0.100 2.50 80-12099.1mg/L2.48 mg/L mg/LArsenic
5.00 2.50 80-120100mg/L<5.00 mg/L mg/LBarium
0.0400 2.50 80-120104mg/L2.61 mg/L mg/LCadmium
0.100 2.50 80-120104mg/L2.60 mg/L mg/LChromium
0.100 2.50 80-120103mg/L2.57 mg/L mg/LLead
0.250 2.50 80-12096.2mg/L2.40 mg/L mg/LSelenium
0.100 0.500 80-12098.5mg/L0.492 mg/L mg/LSilver
Matrix Spike (BGA0626-MS1)Prepared: 01/20/2023 Analyzed: 01/24/2023Source: 23A0886-02
0.100 2.50 75-12596.7mg/L2.42 mg/L <0.100 mg/LArsenic
5.00 2.50 75-125133mg/L<5.00 mg/L <5.00 mg/LBarium M
0.0400 2.50 75-12599.7mg/L2.49 mg/L <0.0400 mg/LCadmium
0.100 2.50 75-125100mg/L2.51 mg/L <0.100 mg/LChromium
0.100 2.50 75-125100mg/L2.50 mg/L <0.100 mg/LLead
0.250 2.50 75-12593.1mg/L2.33 mg/L <0.250 mg/LSelenium
0.100 0.500 75-125105mg/L0.523 mg/L <0.100 mg/LSilver
Page 12 of 28
Page 12 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Metals by 6000/7000 Series Methods - Quality Control
Enthalpy Analytical
Batch BGA0626 - SW3010A
Matrix Spike Dup (BGA0626-MSD1)Prepared: 01/20/2023 Analyzed: 01/24/2023Source: 23A0886-02
0.100 2.50 2075-12598.1 1.42mg/L2.45 mg/L <0.100 mg/LArsenic
5.00 2.50 2075-125131 1.33mg/L<5.00 mg/L <5.00 mg/LBarium M
0.0400 2.50 2075-125101 1.10mg/L2.52 mg/L <0.0400 mg/LCadmium
0.100 2.50 2075-125102 1.31mg/L2.54 mg/L <0.100 mg/LChromium
0.100 2.50 2075-125101 1.09mg/L2.53 mg/L <0.100 mg/LLead
0.250 2.50 2075-12594.2 1.11mg/L2.35 mg/L <0.250 mg/LSelenium
0.100 0.500 2075-125112 6.65mg/L0.559 mg/L <0.100 mg/LSilver
Batch BGA0666 - SW7470A
Blank (BGA0666-BLK1)Prepared & Analyzed: 01/23/2023
0.008 mg/L<0.008 mg/LMercury
LCS (BGA0666-BS1)Prepared & Analyzed: 01/23/2023
0.008 0.0500 80-12089.1mg/L0.045 mg/L mg/LMercury
Matrix Spike (BGA0666-MS1)Prepared & Analyzed: 01/23/2023Source: 23A0925-07
0.008 0.0500 80-12063.7mg/L0.032 mg/L <0.008 mg/LMercury M
Matrix Spike Dup (BGA0666-MSD1)Prepared & Analyzed: 01/23/2023Source: 23A0925-07
0.008 0.0500 2080-12089.0 33.1mg/L0.044 mg/L <0.008 mg/LMercury P
Page 13 of 28
Page 13 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Volatile Organic Compounds by GCMS - Quality Control
Enthalpy Analytical
Batch BGA0690 - SW1311 ZHE
Blank (BGA0690-BLK1)Prepared & Analyzed: 01/23/2023
0 #1 #Extraction Fluid, ZHE
Batch BGA0724 - SW5030B-MS
Blank (BGA0724-BLK1)Prepared & Analyzed: 01/24/2023
0.02 mg/L<0.02 mg/L1,1-Dichloroethylene
0.02 mg/L<0.02 mg/L1,2-Dichloroethane
0.02 mg/L<0.02 mg/L1,4-Dichlorobenzene
0.20 mg/L<0.20 mg/L2-Butanone (MEK)
0.05 mg/L<0.05 mg/LBenzene
0.02 mg/L<0.02 mg/LCarbon tetrachloride
0.02 mg/L<0.02 mg/LChlorobenzene
0.02 mg/L<0.02 mg/LChloroform
0.05 mg/L<0.05 mg/LTetrachloroethylene (PCE)
0.02 mg/L<0.02 mg/LTrichloroethylene
0.02 mg/L<0.02 mg/LVinyl chloride
50.0 70-120Surr: 1,2-Dichloroethane-d4 (Surr)10351.6 ug/L
50.0 75-120Surr: 4-Bromofluorobenzene (Surr)98.849.4 ug/L
50.0 80-119Surr: Dibromofluoromethane (Surr)10351.5 ug/L
50.0 85-120Surr: Toluene-d8 (Surr)10050.0 ug/L
LCS (BGA0724-BS1)Prepared & Analyzed: 01/24/2023
20 50.0 70-13081.6ug/L40.8 ug/L ug/L1,1-Dichloroethylene
20 50.0 70-13089.1ug/L44.6 ug/L ug/L1,2-Dichloroethane
20 50.0 75-125106ug/L53.0 ug/L ug/L1,4-Dichlorobenzene
200 50.0 30-15099.1ug/L< 200 ug/L ug/L2-Butanone (MEK)
50 50.0 80-12095.4ug/L< 50 ug/L ug/LBenzene
20 50.0 65-14093.3ug/L46.7 ug/L ug/LCarbon tetrachloride
20 50.0 80-120101ug/L50.7 ug/L ug/LChlorobenzene
20 50.0 65-13598.5ug/L49.2 ug/L ug/LChloroform
50 50.0 45-15097.8ug/L< 50 ug/L ug/LTetrachloroethylene (PCE)
20 50.0 70-12598.7ug/L49.3 ug/L ug/LTrichloroethylene
Page 14 of 28
Page 14 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Volatile Organic Compounds by GCMS - Quality Control
Enthalpy Analytical
Batch BGA0724 - SW5030B-MS
LCS (BGA0724-BS1)Prepared & Analyzed: 01/24/2023
20 50.0 50-14582.5ug/L41.2 ug/L ug/LVinyl chloride
50.0 70-120Surr: 1,2-Dichloroethane-d4 (Surr)10351.4 ug/L ug/L
50.0 75-120Surr: 4-Bromofluorobenzene (Surr)98.949.4 ug/L ug/L
50.0 80-119Surr: Dibromofluoromethane (Surr)10452.2 ug/L ug/L
50.0 85-120Surr: Toluene-d8 (Surr)10251.2 ug/L ug/L
Matrix Spike (BGA0724-MS1)Prepared & Analyzed: 01/24/2023Source: 23A1027-01
20 50.0 70-13078.3ug/L39.2 ug/L < 20 mg/L1,1-Dichloroethylene
20 50.0 70-13089.7ug/L44.8 ug/L < 20 mg/L1,2-Dichloroethane
20 50.0 75-125103ug/L51.4 ug/L < 20 mg/L1,4-Dichlorobenzene
200 50.0 30-15085.7ug/L< 200 ug/L < 200 mg/L2-Butanone (MEK)
50 50.0 80-12092.2ug/L< 50 ug/L < 50 mg/LBenzene
20 50.0 65-14089.8ug/L44.9 ug/L < 20 mg/LCarbon tetrachloride
20 50.0 80-12099.3ug/L49.7 ug/L < 20 mg/LChlorobenzene
20 50.0 65-13594.7ug/L47.4 ug/L < 20 mg/LChloroform
50 50.0 45-15094.1ug/L< 50 ug/L < 50 mg/LTetrachloroethylene (PCE)
20 50.0 70-12593.9ug/L47.0 ug/L < 20 mg/LTrichloroethylene
20 50.0 50-14578.2ug/L39.1 ug/L < 20 mg/LVinyl chloride
50.0 70-120Surr: 1,2-Dichloroethane-d4 (Surr)10251.2 ug/L ug/L
50.0 75-120Surr: 4-Bromofluorobenzene (Surr)98.349.2 ug/L ug/L
50.0 80-119Surr: Dibromofluoromethane (Surr)10351.6 ug/L ug/L
50.0 85-120Surr: Toluene-d8 (Surr)10251.2 ug/L ug/L
Matrix Spike Dup (BGA0724-MSD1)Prepared & Analyzed: 01/24/2023Source: 23A1027-01
20 50.0 3070-13078.6 0.408ug/L39.3 ug/L < 20 mg/L1,1-Dichloroethylene
20 50.0 3070-13090.3 0.733ug/L45.2 ug/L < 20 mg/L1,2-Dichloroethane
20 50.0 3075-125102 0.722ug/L51.1 ug/L < 20 mg/L1,4-Dichlorobenzene
200 50.0 3030-15089.2 3.98ug/L< 200 ug/L < 200 mg/L2-Butanone (MEK)
50 50.0 3080-12091.6 0.696ug/L< 50 ug/L < 50 mg/LBenzene
20 50.0 3065-14089.2 0.737ug/L44.6 ug/L < 20 mg/LCarbon tetrachloride
20 50.0 3080-12098.1 1.28ug/L49.0 ug/L < 20 mg/LChlorobenzene
20 50.0 3065-13595.6 0.946ug/L47.8 ug/L < 20 mg/LChloroform
Page 15 of 28
Page 15 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Volatile Organic Compounds by GCMS - Quality Control
Enthalpy Analytical
Batch BGA0724 - SW5030B-MS
Matrix Spike Dup (BGA0724-MSD1)Prepared & Analyzed: 01/24/2023Source: 23A1027-01
50 50.0 3045-15092.4 1.80ug/L< 50 ug/L < 50 mg/LTetrachloroethylene (PCE)
20 50.0 3070-12592.9 1.09ug/L46.4 ug/L < 20 mg/LTrichloroethylene
20 50.0 3050-14580.5 2.87ug/L40.2 ug/L < 20 mg/LVinyl chloride
50.0 70-120Surr: 1,2-Dichloroethane-d4 (Surr)10753.6 ug/L ug/L
50.0 75-120Surr: 4-Bromofluorobenzene (Surr)98.849.4 ug/L ug/L
50.0 80-119Surr: Dibromofluoromethane (Surr)10452.2 ug/L ug/L
50.0 85-120Surr: Toluene-d8 (Surr)10351.6 ug/L ug/L
Page 16 of 28
Page 16 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Semivolatile Organic Compounds - Quality Control
Enthalpy Analytical
Batch BGA0625 - SW3580A-MS
Blank (BGA0625-BLK1)Prepared & Analyzed: 01/19/2023
0 #1 #Extraction Fluid, SV Organics
Page 17 of 28
Page 17 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Semivolatile Organic Compounds by GCMS - Quality Control
Enthalpy Analytical
Batch BGA0629 - SW3510C/EPA600-MS
Blank (BGA0629-BLK1)Prepared & Analyzed: 01/20/2023
0.02 mg/L<0.02 mg/L2,4,5-Trichlorophenol
0.02 mg/L<0.02 mg/L2,4,6-Trichlorophenol
0.02 mg/L<0.02 mg/L2,4-Dinitrotoluene
0.02 mg/L<0.02 mg/LHexachlorobenzene
0.02 mg/L<0.02 mg/LHexachlorobutadiene
0.02 mg/L<0.02 mg/LHexachloroethane
0.02 mg/L<0.02 mg/Lm+p-Cresols
0.02 mg/L<0.02 mg/LNitrobenzene
0.02 mg/L<0.02 mg/Lo+m+p-Cresols
0.02 mg/L<0.02 mg/Lo-Cresol
0.02 mg/L<0.02 mg/LPentachlorophenol
0.02 mg/L<0.02 mg/LPyridine
1.00 7-150Surr: 2,4,6-Tribromophenol (Surr)25.20.252 mg/L
0.500 5-125Surr: 2-Fluorobiphenyl (Surr)30.50.152 mg/L
1.00 5-80Surr: 2-Fluorophenol (Surr)19.10.191 mg/L
0.500 5-117Surr: Nitrobenzene-d5 (Surr)37.90.190 mg/L
1.00 5-60Surr: Phenol-d5 (Surr)12.40.124 mg/L
0.500 19.3-150Surr: p-Terphenyl-d14 (Surr)65.50.327 mg/L
LCS (BGA0629-BS1)Prepared & Analyzed: 01/20/2023
0.01 0.500 8-12035.8mg/L0.18 mg/L mg/L1,2,4-Trichlorobenzene
0.01 0.500 3-9736.3mg/L0.18 mg/L mg/L1,2-Dichlorobenzene
0.01 0.500 3-11234.5mg/L0.17 mg/L mg/L1,3-Dichlorobenzene
0.01 0.500 3-11235.5mg/L0.18 mg/L mg/L1,4-Dichlorobenzene
0.02 0.500 11-14541.3mg/L0.21 mg/L mg/L2,4,6-Trichlorophenol
0.01 0.500 11-7544.3mg/L0.22 mg/L mg/L2,4-Dichlorophenol
0.005 0.500 11-12140.7mg/L0.20 mg/L mg/L2,4-Dimethylphenol
0.05 0.500 11-16543.9mg/L0.22 mg/L mg/L2,4-Dinitrophenol
0.02 0.500 17-15556.7mg/L0.28 mg/L mg/L2,4-Dinitrotoluene
0.01 0.500 15-12548.5mg/L0.24 mg/L mg/L2,6-Dinitrotoluene
0.01 0.500 12-11341.7mg/L0.21 mg/L mg/L2-Chloronaphthalene
0.01 0.500 15-11046.3mg/L0.23 mg/L mg/L2-Chlorophenol
Page 18 of 28
Page 18 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Semivolatile Organic Compounds by GCMS - Quality Control
Enthalpy Analytical
Batch BGA0629 - SW3510C/EPA600-MS
LCS (BGA0629-BS1)Prepared & Analyzed: 01/20/2023
0.01 0.500 11-12547.3mg/L0.24 mg/L mg/L2-Nitrophenol
0.05 0.500 25-15352.8mg/L0.26 mg/L mg/L4,6-Dinitro-2-methylphenol
0.01 0.500 15-11341.6mg/L0.21 mg/L mg/L4-Bromophenyl phenyl ether
0.01 0.500 15-11042.2mg/L0.21 mg/L mg/L4-Chlorophenyl phenyl ether
0.05 0.500 12-7019.3mg/L0.10 mg/L mg/L4-Nitrophenol
0.01 0.500 18-11942.4mg/L0.21 mg/L mg/LAcenaphthene
0.01 0.500 20-11746.5mg/L0.23 mg/L mg/LAcenaphthylene
0.01 0.500 16-11852.4mg/L0.26 mg/L mg/LAnthracene
0.01 0.500 28-12953.1mg/L0.27 mg/L mg/LBenzo (a) anthracene
0.01 0.500 23-13158.6mg/L0.29 mg/L mg/LBenzo (a) pyrene
0.01 0.500 20-14170.3mg/L0.35 mg/L mg/LBenzo (b) fluoranthene
0.01 0.500 9-13854.0mg/L0.27 mg/L mg/LBenzo (g,h,i) perylene
0.01 0.500 21-13855.4mg/L0.28 mg/L mg/LBenzo (k) fluoranthene
0.01 0.500 25-11037.3mg/L0.19 mg/L mg/Lbis (2-Chloroethoxy) methane
0.01 0.500 8-10742.8mg/L0.21 mg/L mg/Lbis (2-Chloroethyl) ether
0.01 0.500 8-11242.0mg/L0.21 mg/L mg/L2,2'-Oxybis (1-chloropropane)
0.01 0.500 14-14750.6mg/L0.25 mg/L mg/Lbis (2-Ethylhexyl) phthalate
0.01 0.500 20-14648.8mg/L0.24 mg/L mg/LButyl benzyl phthalate
0.002 0.500 0-20050.6mg/L0.25 mg/L mg/LCarbazole
0.01 0.500 21-13652.5mg/L0.26 mg/L mg/LChrysene
0.01 0.500 14-14262.3mg/L0.31 mg/L mg/LDibenz (a,h) anthracene
0.01 0.500 11-12157.4mg/L0.29 mg/L mg/LDiethyl phthalate
0.01 0.500 3-12554.6mg/L0.27 mg/L mg/LDimethyl phthalate
0.01 0.500 35-11559.6mg/L0.30 mg/L mg/LDi-n-butyl phthalate
0.01 0.500 25-17569.4mg/L0.35 mg/L mg/LDi-n-octyl phthalate
0.01 0.500 25-13558.4mg/L0.29 mg/L mg/LFluoranthene
0.01 0.500 15-12247.0mg/L0.24 mg/L mg/LFluorene
0.02 0.500 25-12547.6mg/L0.24 mg/L mg/LHexachlorobenzene
0.02 0.500 25-12540.2mg/L0.20 mg/L mg/LHexachlorobutadiene
0.01 0.500 25-12526.8mg/L0.13 mg/L mg/LHexachlorocyclopentadiene
0.02 0.500 3-12536.4mg/L0.18 mg/L mg/LHexachloroethane
Page 19 of 28
Page 19 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Semivolatile Organic Compounds by GCMS - Quality Control
Enthalpy Analytical
Batch BGA0629 - SW3510C/EPA600-MS
LCS (BGA0629-BS1)Prepared & Analyzed: 01/20/2023
0.01 0.500 16-13759.7mg/L0.30 mg/L mg/LIndeno (1,2,3-cd) pyrene
0.01 0.500 6-11020.9mg/L0.10 mg/L mg/LIsophorone
0.01 0.500 12-10543.1mg/L0.22 mg/L mg/LNaphthalene
0.02 0.500 9-11953.7mg/L0.27 mg/L mg/LNitrobenzene
0.01 0.500 10-8530.2mg/L0.15 mg/L mg/Ln-Nitrosodimethylamine
0.01 0.500 8-10848.0mg/L0.24 mg/L mg/Ln-Nitrosodi-n-propylamine
0.01 0.500 12-9740.4mg/L0.20 mg/L mg/Ln-Nitrosodiphenylamine
0.01 0.500 10-12844.2mg/L0.22 mg/L mg/Lp-Chloro-m-cresol
0.02 0.500 11-11739.2mg/L0.20 mg/L mg/LPentachlorophenol
0.01 0.500 17-12857.6mg/L0.29 mg/L mg/LPhenanthrene
0.02 0.505 3-8016.7mg/L0.08 mg/L mg/LPhenol
0.01 0.500 15-14152.3mg/L0.26 mg/L mg/LPyrene
0.02 0.500 0-20032.2mg/L0.16 mg/L mg/LPyridine
1.00 7-150Surr: 2,4,6-Tribromophenol (Surr)51.10.511 mg/L mg/L
0.500 5-125Surr: 2-Fluorobiphenyl (Surr)46.30.231 mg/L mg/L
1.00 5-80Surr: 2-Fluorophenol (Surr)30.00.300 mg/L mg/L
0.500 5-117Surr: Nitrobenzene-d5 (Surr)55.90.280 mg/L mg/L
1.00 5-60Surr: Phenol-d5 (Surr)19.90.199 mg/L mg/L
0.500 19.3-150Surr: p-Terphenyl-d14 (Surr)52.10.260 mg/L mg/L
Matrix Spike (BGA0629-MS1)Prepared & Analyzed: 01/20/2023Source: 23A0886-02
0.01 0.500 9-10475.7mg/L0.38 mg/L <0.01 mg/L1,2,4-Trichlorobenzene
0.01 0.500 3-10577.5mg/L0.39 mg/L <0.01 mg/L1,2-Dichlorobenzene
0.01 0.500 6-10873.4mg/L0.37 mg/L <0.01 mg/L1,3-Dichlorobenzene
0.01 0.500 3-9073.0mg/L0.37 mg/L <0.01 mg/L1,4-Dichlorobenzene
0.02 0.500 17-12378.4mg/L0.39 mg/L <0.02 mg/L2,4,6-Trichlorophenol
0.01 0.500 35-12878.1mg/L0.39 mg/L <0.01 mg/L2,4-Dichlorophenol
0.005 0.500 30-11470.7mg/L0.35 mg/L <0.005 mg/L2,4-Dimethylphenol
0.05 0.500 15-19087.4mg/L0.44 mg/L <0.05 mg/L2,4-Dinitrophenol
0.02 0.500 17-14191.6mg/L0.46 mg/L <0.02 mg/L2,4-Dinitrotoluene
0.01 0.500 15-12784.1mg/L0.42 mg/L <0.01 mg/L2,6-Dinitrotoluene
0.01 0.500 27-12187.9mg/L0.44 mg/L <0.01 mg/L2-Chloronaphthalene
Page 20 of 28
Page 20 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Semivolatile Organic Compounds by GCMS - Quality Control
Enthalpy Analytical
Batch BGA0629 - SW3510C/EPA600-MS
Matrix Spike (BGA0629-MS1)Prepared & Analyzed: 01/20/2023Source: 23A0886-02
0.01 0.500 19-11679.3mg/L0.40 mg/L <0.01 mg/L2-Chlorophenol
0.01 0.500 10-13382.2mg/L0.41 mg/L <0.01 mg/L2-Nitrophenol
0.05 0.500 15-15793.9mg/L0.47 mg/L <0.05 mg/L4,6-Dinitro-2-methylphenol
0.01 0.500 15-12369.7mg/L0.35 mg/L <0.01 mg/L4-Bromophenyl phenyl ether
0.01 0.500 15-11475.5mg/L0.38 mg/L <0.01 mg/L4-Chlorophenyl phenyl ether
0.05 0.500 12-7043.0mg/L0.21 mg/L <0.05 mg/L4-Nitrophenol
0.01 0.500 24-12887.6mg/L0.44 mg/L <0.01 mg/LAcenaphthene
0.01 0.500 16-12193.4mg/L0.47 mg/L <0.01 mg/LAcenaphthylene
0.01 0.500 11-12894.5mg/L0.47 mg/L <0.01 mg/LAnthracene
0.01 0.500 18-13992.9mg/L0.46 mg/L <0.01 mg/LBenzo (a) anthracene
0.01 0.500 15-175106mg/L0.53 mg/L <0.01 mg/LBenzo (a) pyrene
0.01 0.500 1-167112mg/L0.56 mg/L <0.01 mg/LBenzo (b) fluoranthene
0.01 0.500 40-14294.1mg/L0.47 mg/L <0.01 mg/LBenzo (g,h,i) perylene
0.01 0.500 45-209101mg/L0.51 mg/L <0.01 mg/LBenzo (k) fluoranthene
0.01 0.500 11-11573.9mg/L0.37 mg/L <0.01 mg/Lbis (2-Chloroethoxy) methane
0.01 0.500 6-11781.5mg/L0.41 mg/L <0.01 mg/Lbis (2-Chloroethyl) ether
0.01 0.500 8-11986.0mg/L0.43 mg/L <0.01 mg/L2,2'-Oxybis (1-chloropropane)
0.01 0.500 4-15684.2mg/L0.42 mg/L <0.01 mg/Lbis (2-Ethylhexyl) phthalate
0.01 0.500 15-15172.8mg/L0.36 mg/L <0.01 mg/LButyl benzyl phthalate
0.002 0.500 0-20087.8mg/L0.44 mg/L <0.002 mg/LCarbazole
0.01 0.500 11-14680.1mg/L0.40 mg/L <0.01 mg/LChrysene
0.01 0.500 10-149111mg/L0.56 mg/L <0.01 mg/LDibenz (a,h) anthracene
0.01 0.500 9-128108mg/L0.54 mg/L <0.01 mg/LDiethyl phthalate
0.01 0.500 3-125102mg/L0.51 mg/L <0.01 mg/LDimethyl phthalate
0.01 0.500 6-15261.1mg/L0.31 mg/L <0.01 mg/LDi-n-butyl phthalate
0.01 0.500 9-214132mg/L0.66 mg/L <0.01 mg/LDi-n-octyl phthalate
0.01 0.500 3-154107mg/L0.53 mg/L <0.01 mg/LFluoranthene
0.01 0.500 10-13292.8mg/L0.46 mg/L <0.01 mg/LFluorene
0.02 0.500 10-12583.2mg/L0.42 mg/L <0.02 mg/LHexachlorobenzene
0.02 0.500 7-12581.0mg/L0.40 mg/L <0.02 mg/LHexachlorobutadiene
0.01 0.500 10-9060.5mg/L0.30 mg/L <0.01 mg/LHexachlorocyclopentadiene
Page 21 of 28
Page 21 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Semivolatile Organic Compounds by GCMS - Quality Control
Enthalpy Analytical
Batch BGA0629 - SW3510C/EPA600-MS
Matrix Spike (BGA0629-MS1)Prepared & Analyzed: 01/20/2023Source: 23A0886-02
0.02 0.500 3-12574.8mg/L0.37 mg/L <0.02 mg/LHexachloroethane
0.01 0.500 4-142104mg/L0.52 mg/L <0.01 mg/LIndeno (1,2,3-cd) pyrene
0.01 0.500 6-11046.0mg/L0.23 mg/L <0.01 mg/LIsophorone
0.01 0.500 7-11787.3mg/L0.44 mg/L <0.01 mg/LNaphthalene
0.02 0.500 10-12193.0mg/L0.47 mg/L <0.02 mg/LNitrobenzene
0.01 0.500 10-9045.7mg/L0.23 mg/L <0.01 mg/Ln-Nitrosodimethylamine
0.01 0.500 7-11681.3mg/L0.41 mg/L <0.01 mg/Ln-Nitrosodi-n-propylamine
0.01 0.500 7-10268.9mg/L0.34 mg/L <0.01 mg/Ln-Nitrosodiphenylamine
0.01 0.500 10-13583.9mg/L0.42 mg/L <0.01 mg/Lp-Chloro-m-cresol
0.02 0.500 7-13869.9mg/L0.35 mg/L <0.02 mg/LPentachlorophenol
0.01 0.500 5-139101mg/L0.51 mg/L <0.01 mg/LPhenanthrene
0.02 0.505 3-7033.9mg/L0.17 mg/L <0.02 mg/LPhenol
0.01 0.500 8-15282.0mg/L0.41 mg/L <0.01 mg/LPyrene
0.02 0.500 0-20055.2mg/L0.28 mg/L <0.02 mg/LPyridine
1.00 7-150Surr: 2,4,6-Tribromophenol (Surr)79.80.798 mg/L mg/L
0.500 5-125Surr: 2-Fluorobiphenyl (Surr)92.70.464 mg/L mg/L
1.00 5-80Surr: 2-Fluorophenol (Surr)48.90.489 mg/L mg/L
0.500 5-117Surr: Nitrobenzene-d5 (Surr)94.80.474 mg/L mg/L
1.00 5-60Surr: Phenol-d5 (Surr)39.00.390 mg/L mg/L
0.500 19.3-150Surr: p-Terphenyl-d14 (Surr)81.20.406 mg/L mg/L
Matrix Spike Dup (BGA0629-MSD1)Prepared & Analyzed: 01/20/2023Source: 23A0886-02
0.01 0.500 209-10470.4 7.31mg/L0.35 mg/L <0.01 mg/L1,2,4-Trichlorobenzene
0.01 0.500 203-10571.8 7.64mg/L0.36 mg/L <0.01 mg/L1,2-Dichlorobenzene
0.01 0.500 206-10867.7 8.08mg/L0.34 mg/L <0.01 mg/L1,3-Dichlorobenzene
0.01 0.500 203-9067.2 8.39mg/L0.34 mg/L <0.01 mg/L1,4-Dichlorobenzene
0.02 0.500 2017-12374.8 4.70mg/L0.37 mg/L <0.02 mg/L2,4,6-Trichlorophenol
0.01 0.500 2035-12874.3 5.01mg/L0.37 mg/L <0.01 mg/L2,4-Dichlorophenol
0.005 0.500 2030-11467.1 5.14mg/L0.34 mg/L <0.005 mg/L2,4-Dimethylphenol
0.05 0.500 2015-19088.4 1.21mg/L0.44 mg/L <0.05 mg/L2,4-Dinitrophenol
0.02 0.500 2017-14188.5 3.44mg/L0.44 mg/L <0.02 mg/L2,4-Dinitrotoluene
0.01 0.500 2015-12780.0 5.02mg/L0.40 mg/L <0.01 mg/L2,6-Dinitrotoluene
Page 22 of 28
Page 22 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Semivolatile Organic Compounds by GCMS - Quality Control
Enthalpy Analytical
Batch BGA0629 - SW3510C/EPA600-MS
Matrix Spike Dup (BGA0629-MSD1)Prepared & Analyzed: 01/20/2023Source: 23A0886-02
0.01 0.500 2027-12179.2 10.3mg/L0.40 mg/L <0.01 mg/L2-Chloronaphthalene
0.01 0.500 2019-11675.9 4.41mg/L0.38 mg/L <0.01 mg/L2-Chlorophenol
0.01 0.500 2010-13377.1 6.50mg/L0.39 mg/L <0.01 mg/L2-Nitrophenol
0.05 0.500 2015-15792.1 1.91mg/L0.46 mg/L <0.05 mg/L4,6-Dinitro-2-methylphenol
0.01 0.500 2015-12364.9 7.16mg/L0.32 mg/L <0.01 mg/L4-Bromophenyl phenyl ether
0.01 0.500 2015-11472.4 4.22mg/L0.36 mg/L <0.01 mg/L4-Chlorophenyl phenyl ether
0.05 0.500 2012-7045.1 4.90mg/L0.23 mg/L <0.05 mg/L4-Nitrophenol
0.01 0.500 2024-12880.5 8.52mg/L0.40 mg/L <0.01 mg/LAcenaphthene
0.01 0.500 2016-12185.7 8.57mg/L0.43 mg/L <0.01 mg/LAcenaphthylene
0.01 0.500 2011-12883.8 12.0mg/L0.42 mg/L <0.01 mg/LAnthracene
0.01 0.500 2018-13984.2 9.78mg/L0.42 mg/L <0.01 mg/LBenzo (a) anthracene
0.01 0.500 2015-17596.1 9.67mg/L0.48 mg/L <0.01 mg/LBenzo (a) pyrene
0.01 0.500 201-167103 8.38mg/L0.52 mg/L <0.01 mg/LBenzo (b) fluoranthene
0.01 0.500 2040-14280.3 15.9mg/L0.40 mg/L <0.01 mg/LBenzo (g,h,i) perylene
0.01 0.500 2045-20993.3 8.12mg/L0.47 mg/L <0.01 mg/LBenzo (k) fluoranthene
0.01 0.500 2011-11566.8 10.0mg/L0.33 mg/L <0.01 mg/Lbis (2-Chloroethoxy) methane
0.01 0.500 206-11777.1 5.55mg/L0.39 mg/L <0.01 mg/Lbis (2-Chloroethyl) ether
0.01 0.500 208-11979.7 7.60mg/L0.40 mg/L <0.01 mg/L2,2'-Oxybis (1-chloropropane)
0.01 0.500 204-15678.4 7.11mg/L0.39 mg/L <0.01 mg/Lbis (2-Ethylhexyl) phthalate
0.01 0.500 2015-15168.4 6.23mg/L0.34 mg/L <0.01 mg/LButyl benzyl phthalate
0.002 0.500 200-20081.0 8.08mg/L0.40 mg/L <0.002 mg/LCarbazole
0.01 0.500 2011-14675.0 6.60mg/L0.37 mg/L <0.01 mg/LChrysene
0.01 0.500 2010-14995.0 15.7mg/L0.48 mg/L <0.01 mg/LDibenz (a,h) anthracene
0.01 0.500 209-128100 7.64mg/L0.50 mg/L <0.01 mg/LDiethyl phthalate
0.01 0.500 203-12595.9 6.11mg/L0.48 mg/L <0.01 mg/LDimethyl phthalate
0.01 0.500 206-152103 51.2mg/L0.52 mg/L <0.01 mg/LDi-n-butyl phthalate P
0.01 0.500 209-214142 7.40mg/L0.71 mg/L <0.01 mg/LDi-n-octyl phthalate
0.01 0.500 203-15493.6 13.0mg/L0.47 mg/L <0.01 mg/LFluoranthene
0.01 0.500 2010-13288.4 4.86mg/L0.44 mg/L <0.01 mg/LFluorene
0.02 0.500 2010-12578.2 6.15mg/L0.39 mg/L <0.02 mg/LHexachlorobenzene
0.02 0.500 207-12575.7 6.69mg/L0.38 mg/L <0.02 mg/LHexachlorobutadiene
Page 23 of 28
Page 23 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
TCLP Semivolatile Organic Compounds by GCMS - Quality Control
Enthalpy Analytical
Batch BGA0629 - SW3510C/EPA600-MS
Matrix Spike Dup (BGA0629-MSD1)Prepared & Analyzed: 01/20/2023Source: 23A0886-02
0.01 0.500 2010-9057.2 5.61mg/L0.29 mg/L <0.01 mg/LHexachlorocyclopentadiene
0.02 0.500 203-12570.0 6.74mg/L0.35 mg/L <0.02 mg/LHexachloroethane
0.01 0.500 204-14290.4 14.1mg/L0.45 mg/L <0.01 mg/LIndeno (1,2,3-cd) pyrene
0.01 0.500 206-11041.5 10.3mg/L0.21 mg/L <0.01 mg/LIsophorone
0.01 0.500 207-11779.4 9.46mg/L0.40 mg/L <0.01 mg/LNaphthalene
0.02 0.500 2010-12186.7 7.08mg/L0.43 mg/L <0.02 mg/LNitrobenzene
0.01 0.500 2010-9041.1 10.6mg/L0.21 mg/L <0.01 mg/Ln-Nitrosodimethylamine
0.01 0.500 207-11676.5 6.16mg/L0.38 mg/L <0.01 mg/Ln-Nitrosodi-n-propylamine
0.01 0.500 207-10265.7 4.66mg/L0.33 mg/L <0.01 mg/Ln-Nitrosodiphenylamine
0.01 0.500 2010-13577.3 8.16mg/L0.39 mg/L <0.01 mg/Lp-Chloro-m-cresol
0.02 0.500 207-13870.1 0.314mg/L0.35 mg/L <0.02 mg/LPentachlorophenol
0.01 0.500 205-13991.2 10.3mg/L0.46 mg/L <0.01 mg/LPhenanthrene
0.02 0.505 203-7032.0 6.01mg/L0.16 mg/L <0.02 mg/LPhenol
0.01 0.500 208-15275.0 8.89mg/L0.38 mg/L <0.01 mg/LPyrene
0.02 0.500 200-20055.6 0.722mg/L0.28 mg/L <0.02 mg/LPyridine
1.00 7-150Surr: 2,4,6-Tribromophenol (Surr)73.80.738 mg/L mg/L
0.500 5-125Surr: 2-Fluorobiphenyl (Surr)85.10.426 mg/L mg/L
1.00 5-80Surr: 2-Fluorophenol (Surr)46.80.468 mg/L mg/L
0.500 5-117Surr: Nitrobenzene-d5 (Surr)89.40.447 mg/L mg/L
1.00 5-60Surr: Phenol-d5 (Surr)37.30.373 mg/L mg/L
0.500 19.3-150Surr: p-Terphenyl-d14 (Surr)75.70.379 mg/L mg/L
Page 24 of 28
Page 24 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Wet Chemistry Analysis - Quality Control
Enthalpy Analytical
Batch BGA0595 - No Prep Wet Chem
Blank (BGA0595-BLK1)Prepared & Analyzed: 01/19/2023
0.10 %100 %Percent Solids
Duplicate (BGA0595-DUP1)Prepared & Analyzed: 01/19/2023Source: 23A0886-01
0.10 201.94%81.6 %83.3 %Percent Solids
Batch BGA0678 - No Prep Wet Chem
Blank (BGA0678-BLK1)Prepared & Analyzed: 01/23/2023
0.10 %100 %Percent Solids
Duplicate (BGA0678-DUP1)Prepared & Analyzed: 01/23/2023Source: 23A0962-01
0.10 201.64%88.8 %90.3 %Percent Solids
Batch BGA0692 - SW3060A
Blank (BGA0692-BLK1)Prepared & Analyzed: 01/19/2023
0.20 mg/kg wet<0.20 mg/kg wetChromium, Hexavalent
LCS (BGA0692-BS1)Prepared & Analyzed: 01/19/2023
0.20 3.99 80-12094.0mg/kg wet3.75 mg/kg wet mg/kg wetChromium, Hexavalent
Matrix Spike (BGA0692-MS1)Prepared & Analyzed: 01/19/2023Source: 23A0812-01
0.20 3.99 75-12523.0mg/kg wet0.92 mg/kg wet <0.20 mg/kgChromium, Hexavalent M
Matrix Spike Dup (BGA0692-MSD1)Prepared & Analyzed: 01/19/2023Source: 23A0812-01
0.20 3.97 2075-12524.0 3.70mg/kg wet0.95 mg/kg wet <0.20 mg/kgChromium, Hexavalent M
Page 25 of 28
Page 25 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
SW1311 in Solids
Extraction Fluid, Metals VELAP
Extraction Fluid, SV Organics VELAP
Extraction Fluid, ZHE VELAP
SW6010D in Non-Potable Water
Arsenic VELAP,WVDEP
Barium VELAP,WVDEP
Cadmium VELAP,WVDEP
Chromium VELAP,WVDEP
Lead VELAP,WVDEP
Selenium VELAP,WVDEP
Silver VELAP,WVDEP
SW7196A in Solids
Chromium, Hexavalent VELAP
SW7470A in Non-Potable Water
Mercury VELAP,WVDEP
SW7471B in Solids
Mercury VELAP,PADEP,NCDEQ,WVDEP
SW8260D in Non-Potable Water
1,1-Dichloroethylene VELAP,NCDEQ
1,2-Dichloroethane VELAP,NCDEQ
1,4-Dichlorobenzene VELAP,NCDEQ
2-Butanone (MEK)VELAP,NCDEQ
Benzene VELAP,NCDEQ
Carbon tetrachloride VELAP,NCDEQ
Chlorobenzene VELAP,NCDEQ
Chloroform VELAP,NCDEQ
Tetrachloroethylene (PCE)VELAP,NCDEQ
Trichloroethylene VELAP,NCDEQ
Vinyl chloride VELAP,NCDEQ
SW8270E in Non-Potable Water
2,4,5-Trichlorophenol WVDEP
2,4,6-Trichlorophenol VELAP,WVDEP
2,4-Dinitrotoluene VELAP,WVDEP
Hexachlorobenzene VELAP,WVDEP
Hexachlorobutadiene VELAP,WVDEP
Page 26 of 28
Page 26 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Certified Analyses included in this Report
CertificationsAnalyte
Hexachloroethane VELAP,WVDEP
m+p-Cresols WVDEP
Nitrobenzene VELAP,WVDEP
o+m+p-Cresols WVDEP
o-Cresol VELAP,WVDEP
Pentachlorophenol VELAP,WVDEP
Pyridine WVDEP
Code Description Laboratory ID Expires
341 12/31/2023Maryland DE Drinking WaterMdDOE
495 07/31/2023North Carolina DENRNC
495 07/31/2023North Carolina DEQNCDEQ
51714 07/31/2023North Carolina Department of HealthNCDOH
12096 04/01/2023New York DOH Drinking WaterNYDOH
68-03503 10/31/2023NELAP-Pennsylvania Certificate #008PADEP
460021 06/14/2023NELAP-Virginia Certificate #12157VELAP
350 11/30/2023West Virginia DEPWVDEP
Page 27 of 28
Page 27 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Summary of Data Qualifiers
M Matrix spike recovery is outside established acceptance limits
P Duplicate analysis does not meet the acceptance criteria for precision
Relative Percent DifferenceRPD
QualifersQual
Denotes sample was re-analyzed-RE
Dilution Factor. Please also see the Preparation Factor in the Analysis Summary section.D.F.
TIC Tentatively Identified Compounds are compounds that are identified by comparing the analyte mass spectral pattern with the NIST spectral
library. A TIC spectral match is reported when the pattern is at least 75% consistent with the published pattern. Compound concentrations
are estimated and are calculated using an internal standard response factor of 1.
PCBs, Total Total PCBs are defined as the sum of detected Aroclors 1016, 1221, 1232, 1248, 1254, 1260, 1262, and 1268.
Page 28 of 28
Page 28 of 30
Page 29 of 30
Client Site I.D.:
Project Number:
Submitted To:
Date Issued:Geosyntec Consultants - Charlotte, NC
1300 S. Mint Street, Suite 300 [none]
Amy Kenwell
Charlotte NC, 28203
1941 Reymet Road l Richmond, Virginia 23230 l Tel: [phone] Fax: [phone]
Certificate of Analysis
Client Name:
Purchase Order:
January 25, 2023 16:37
Project Lookout
Final Report
Samples Received at:0.60°C
How were samples received?
NA
Sample Conditions Checklist
NA
No
Yes
Yes
Yes
Yes
Yes
Yes
No
Yes
FedEx Express
Were Custody Seals used? If so, were they received intact?
Are the custody papers filled out completely and correctly?
Do all bottle labels agree with custody papers?
Is the temperature blank or representative sample within acceptable limits or received on ice, and recently taken?
Are all samples within holding time for requested laboratory tests?
Is a sufficient amount of sample provided to perform the tests included?
Are all samples in appropriate containers for the analyses requested?
Were volatile organic containers received?
Are all volatile organic and TOX containers free of headspace?
Is a trip blank provided for each VOC sample set? VOC sample sets include EPA8011, EPA504, EPA8260, EPA624,
EPA8015 GRO, EPA8021, EPA524, and RSK-175.
Are all samples received appropriately preserved? Note that metals containers do not require field preservation but lab
preservation may delay analysis.
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