23057_CharlotteVan&Storage_Soil Export Options EX9-11 and SP1215 1-5 Package_20220104

January 4, 2022
Sent Via E-mail
Mr. Jeffrey W. Harris Lennar Multifamily Communities, LLC 500 East Morehead Street, Suite 300 Charlotte, North Carolina 28202
[e-mail] Subject: Brownfields Soil Management Options EX-9, EX-10, EX-11 and SP-1215-1 through SP-1215-5 Charlotte Van & Storage Co. Brownfield Property
Charlotte, Mecklenburg County Brownfields Project No. 23057-19-060 Dear Mr. Harris:
The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received a request to export soil from the Charlotte Van & Storage Co. Brownfields Property. This request was submitted on your behalf by Ms. Haley Martin, PG of Hart & Hickman, PC via email on January 4, 2022, and requests approval to export approximately 5,000 cubic yards of stockpiled soil, and approximately 3,000 cubic yards of soil from planned grading activities to a beneficial
fill reuse site known as the Fleet Maintenance facility in Mt. Holly, North Carolina. DEQ Brownfields provided letters approving soil export options on September 7 and 15, October 11, November 18, 2021, and December 29, 2021, in response to previous requests. For this request, DEQ Brownfields reviewed the January 3, 2022, Data Summary Package which
includes analytical results for soil samples EX-9, EX-10, EX-11 (and DUP), and SP-1215-1 through SP-1215-5, as well as soil analytical data from the proposed Fleet Maintenance receiving facility. Based on our review of the data, the DEQ Brownfield determines that soils may be exported as
outlined in the table below. Please note that the “Beneficial Fill” option listed in the table below is specifically approved for the Fleet Maintenance facility in Mt. Holly, NC. Other Beneficial Fill and Land Clearing & Inert Debris Landfill (LCID) options may be available; however, DEQ requires that the receiving facility be identified and approved prior to export. The receiving facility should have metals concentrations which are consistent with those from the Brownfields
Property. Similarly, many site soils, including those with impacts, may be suitable for use at another Brownfields Property that has similar impacts.
Mr. Jeffery Harris January 4, 2022 Page 2

Upon determination of the export facility, whether another Brownfields Property, LCID, or
another beneficial fill reuse, please contact us and we will assist you in determining if additional sampling is needed for the receiving facility.
LOCATION ID DEPTH (Ft)1 MANAGEMENT OPTIONS2
EX-9 0-1.5 BFILL, LCID, CDLF, MSWLF
EX-10 0-1.5 CDLF, MSWLF
EX-11/DUP 0-1.5 BFILL, LCID, CDLF, MSWLF
SP-1215-1 stockpile BFILL, LCID, CDLF, MSWLF
SP-1215-2 stockpile BFILL, LCID, CDLF, MSWLF
SP-1215-3 stockpile BFILL, LCID, CDLF, MSWLF
SP-1215-4 stockpile BFILL, LCID, CDLF, MSWLF
SP-1215-5 stockpile BFILL, LCID, CDLF, MSWLF
Notes: 1) Depth listed is total depth of available analytical data. Additional sampling would potentially be required beyond these depths prior to export. 2) BFILL= Beneficial Fill; LCID = Land Clearing & Inert Debris Landfill; CDLF = Construction & Demolition landfill; MSWLF = Municipal Solid Waste landfill (MSWLF) facility.
Per the Charlotte Van & Storage Co.’s approved Environmental Management Plan (EMP), the
soils are to be field screened during excavation prior to export from the property. If unanticipated impacts are identified during excavation, please refer to the EMP for further actions and cease transfer until appropriate characterization can be completed. In addition, and also in accordance with the site’s approved EMP, an annual Redevelopment Summary Report will be submitted to
DEQ Brownfields. Details related to the disposition of this soil including but not limited to, total
volume, general description of field screening efforts, etc. should be included with the Redevelopment Summary Report. Please be advised that this approval does not waive any applicable requirement to obtain any
necessary permits, licenses or certifications which may be required from other state or local entities.
If you have questions about this correspondence or require additional information, please feel free to contact Pete Doorn by phone at 984-275-5391 or by email at [e-mail]. Sincerely,
Peter L. Doorn, Project Manager Brownfields Program
Ec: Haley Martin, Hart & Hickman, PC
Ralph McGee, Hart & Hickman, PC Tracy Wahl, DEQ Brownfields
1
Doorn, Peter L
From:Haley Martin <[e-mail]>
Sent:Tuesday, January 4, 2022 8:12 AM
To:Doorn, Peter L
Subject:RE: [External] 23057-19-060 Charlotte Van and Storage - In Situ Soil Characterization
Sampling
Attachments:Charlotte Van & Storage Co. - Data Summary Package 20220103.pdf
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Pete,

As indicated in the email below, the PD at the Charlotte Van and Storage Co. Brownfields property (BPN 23057-19-060)
plans to complete limited grading activities in a proposed paved parking area located south of proposed Building 1 (see
attached Figure). On December 15, 2021, H&H completed soil sampling activities in accordance with the proposed
scope of work outlined below to assist in management of approximately 3,000 cubic yards of soil that will be generated
during limited grading activities in the parking area. In situ soil assessment activities included dividing the proposed area
of limited grading into three (3) in situ soil characterization sections based on proposed shallow cut depths
(approximately 1.5 ft bgs). Areas that will be cut are outlined in red in the attached Figure along with the evaluation
areas and aliquot soil boring locations. Note that the area and depth of planned cut for stripping has been calculated so
that each evaluation area represents approximately 1,000 cubic yards of soil. Each composite soil sample was
comprised of aliquot soil samples collected from five soil borings advanced within in each evaluation area. Soil sample
aliquots collected from each depth interval in an evaluation area were homogenized to form composite soil samples
representative of soil conditions in each area for a total of 3 composite soil samples (EX-9 through EX-11).

The three composite soil samples selected for laboratory analyses were collected directly into dedicated laboratory
supplied sample containers, labeled with the date, time, and sample identification, and placed in a laboratory supplied
sample cooler with ice. The samples were submitted to Waypoint Analytical (Waypoint) under standard chain of custody
protocols for analysis of semi volatile organic compounds (SVOCs) by EPA Method 8270 and Resource Conservation and
Recovery Act (RCRA) metals plus hexavalent chromium by EPA Methods 6020/7471/7199. In addition to the composite
soil samples described above, one representative grab soil sample was collected from each evaluation area and the on-
Site stockpile for a total of three grab samples. The grab soil samples were collected from undisturbed portions of soil
directly into laboratory supplied glassware and submitted to Waypoint under standard chain of custody protocols for
analysis of VOCs by EPA Method 8260.

H&H collected five soil samples (SP-1215-1 through SP-1215-5) to characterize an approximate 1,000 cubic yard
stockpile and one 4,000 cubic yard stockpile generated during grading activities at Site. H&H collected 5 aliquot soil
samples from each 1,000 cubic yard section of the stockpiled material. The aliquots collected from the stockpiles were
homogenized to form a composite soil sample representative of the 1,000 cubic yard section of stockpile. The
composite soil samples were collected directly into laboratory supplied glassware, labeled with the sample ID, date, and
requested analyses and placed in a laboratory supplied cooler with ice. Additionally, one grab sample was collected
from undisturbed portions of a select aliquot soil sample prior to homogenization for each composite soil sample. The
soil samples were submitted for the same analyses as the in situ soil samples described above.

2
We have prepared the attached Data Summary Package which includes a tabular summary of the in situ soil sample
laboratory analytical results and the stockpile soil sample laboratory analytical results, a Figure depicting the soil boring
locations, and the laboratory analytical report. A general summary of the sampling results is provided below for each
evaluation area:

In Situ Soil Sample Results
 EX-9 – no organic compounds were detected at concentrations above the PSRGs and metals appear to be
consistent with background levels
 EX-10 – an estimated concentration of benzo(a)pyrene (0.603 J mg/kg) was detected above the Residential and
Protection of Groundwater PSRGs and benzo(a)anthracene (0.58 J mg/kg) was detected above the Protection of
Groundwater PSRG – metals appear to be consistent with background levels
 EX-11/DUP – no organic compounds were detected at concentrations above the PSRGS – a low level of
hexavalent chromium (up to 3.6 mg/kg) was detected at a concentration above the Residential PSRG, but below
the Protection of Groundwater and Industrial/Commercial PSRGs

Stockpile Soil Sample Results
 SP-1215-1 – no organic compounds above PSRGS and metals appear to be consistent with background levels
 SP-1215-2 – no organic compounds above PSRGS and metals appear to be consistent with background levels
 SP-1215-3 – no organic compounds above PSRGS and metals appear to be consistent with background levels
 SP-1215-4 – no organic compounds above PSRGS and metals appear to be consistent with background levels
 SP-1215-5 – no organic compounds above PSRGS and metals appear to be consistent with background levels

As noted in the email below, the PD would like to transport soil to the Fleet facility. Based on the proposed placement
of the fill beneath parking areas/loading docks at the Fleet industrial facility and the detected compound concentrations
below the DEQ IHSB Industrial/Commercial PSRGs, the PD requests DEQ approval to transport soil from evaluation areas
EX-9 through EX-11 and the on-Site stockpiles to the Fleet facility.

As you know, grading and construction work is ongoing. We appreciate your reviewing this data prior to submittal of the
report to assist in keeping the construction schedule on track. In the meantime, please let us know if you have any
questions or concerns.

Thank you,
Haley

Haley Martin, PG, Project Geologist
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 · Charlotte, NC 28203
Direct: 704-526-2045 · Mobile: [phone]
www.harthickman.com

From: Doorn, Peter L <[e-mail]>
Sent: Thursday, December 16, 2021 8:44 AM
To: Haley Martin <[e-mail]>
Subject: RE: [External] 23057-19-060 Charlotte Van and Storage - In Situ Soil Characterization Sampling

Good morning, Haley

Thanks for providing the details of the sampling strategy for soil from the area to be paved, and for the two stockpiles
from site grading activities. The proposed sampling approach is approved. Once we receive the data package, I’ll review
it and respond with options for disposition.

3
Best regards,

-Pete

Peter L. Doorn
Brownfields Program/DWM/NCDEQ
Mobile: [phone]

Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third
parties.

From: Haley Martin <[e-mail]>
Sent: Thursday, December 16, 2021 7:50 AM
To: Doorn, Peter L <[e-mail]>
Subject: RE: [External] 23057-19-060 Charlotte Van and Storage - In Situ Soil Characterization Sampling

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.

Pete,

As discussed on our call on Tuesday, the PD at Charlotte Van and Storage intends to begin paving activities in the area
located south of Building 1 located in the northern portion of the Site. H&H will complete in situ soil characterization
assessment activities at the Brownfields property to assist in management of approximately 3,000 cubic yards of soil
expected to be generated prior to paving activities. In situ soil assessment activities will include dividing the proposed
paved area into three (3) in situ soil characterizations sections (EX-9 through EX-11) based on information provided by
the on-Site superintendent and proposed shallow (approximately 1.5 ft bgs) cut depths. Areas that will be paved are
outlined in red in the attached Figure along with the proposed evaluation areas and aliquot soil boring locations. Note
that the area and depth of planned cut for paving has been calculated so that each evaluation area represents
approximately 1,000 cubic yards of soil.

In addition to the in situ sampling outlined above, H&H will assist with soil characterization sampling of one approximate
1,000 cubic yard stockpile and one approximate 4,000 cubic yard stockpile generated during mass grading activities at
the Site. A total of five (5) soil characterization samples will be collected from the stockpiled material at the Site. In situ
soil characterization sampling and stockpile sampling will be conducted in accordance with the sampling methodology
outlined in the email below dated August 3, 2021 and in accordance with the DEQ approved EMP. We will send a data
summary package with the analytical results as soon as they are available. In the meantime, please let us know if you
have questions or require additional information.

Thank you,
Haley

Haley Martin, PG, Project Geologist
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 · Charlotte, NC 28203
Direct: 704-526-2045 · Mobile: [phone]
www.harthickman.com

From: Doorn, Peter L <[e-mail]>
Sent: Monday, August 9, 2021 11:11 AM
To: Haley Martin <[e-mail]>
4
Cc: Patrick Foster <[e-mail]>; Ralph McGee <[e-mail]>
Subject: RE: [External] 23057-19-060 Charlotte Van and Storage - In Situ Soil Characterization Sampling

Haley,

Thanks for sending the details of the sampling strategy to evaluate shallow soils from the grubbing/stripping activities
for the Charlotte Van & Storage project. Your proposed strategy looks sound.

I also appreciate the 2019 example soil export letter for the Block 42 project. When you send the document package,
please include a brief description of the intended use of the soil at the Fleet Maintenance facility.

If you encounter any previously unidentified impacts during grubbing/stripping activities, just let me know.

Thanks,

-Pete

Pete Doorn
Brownfields Program/DWM/NCDEQ
Mobile: [phone]

Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third
parties.

From: Haley Martin <[e-mail]>
Sent: Tuesday, August 3, 2021 11:35 AM
To: Doorn, Peter L <[e-mail]>
Cc: Patrick Foster <[e-mail]>; Ralph McGee <[e-mail]>
Subject: [External] 23057-19-060 Charlotte Van and Storage - In Situ Soil Characterization Sampling

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.

Pete,

The PD at the Charlotte Van and Storage Brownfields property (BPN 23057-19-060) is planning to complete grubbing
and stripping of topsoil in undeveloped and vegetated portions of the Brownfields property prior to mass grading
activities. H&H will complete in situ soil characterization assessment activities at the Brownfields property to assist in
management of approximately 5,600 cubic yards of topsoil expected to be generated during grubbing/stripping
activities. In situ soil assessment activities will include dividing the proposed area of limited grubbing into six (6) in situ
soil characterizations sections (EX-1 through EX-6) based on information provided by the on-Site superintendent and
proposed shallow (approximately 2 ft bgs) grubbing depths. Areas that will be stripped are shown in green shading in the
attached Figure along with the proposed evaluation areas and aliquot soil boring locations. Note that the area and
depth of planned cut for stripping has been calculated so that each evaluation area represents approximately 1,000
cubic yards of topsoil/organics.

In accordance with the DEQ-approved EMP, a minimum of 3 aliquot soil borings will be advance in each evaluation area.
Continuous soil samples will be collected from each boring advanced in an evaluation area. The soil samples will be
combined and homogenized to form one composite soil sample representative of soil that will be generated during
grubbing in that section. The composite soil samples selected for laboratory analysis will be placed directly into
laboratory supplied glassware, labeled with the sample ID, the date, and requested analysis and placed in a laboratory
supplied cooler with ice. The samples will be delivered to a NC certified laboratory under standard chain of custody
5
protocols for analysis of semi-volatile organic compounds (SVOCs) by EPA Method 8270 and RCRA metals plus
hexavalent chromium by EPA Methods 6020/7471/7199. In addition, one grab soil sample will be collected in each
evaluation area from an undisturbed portion of an aliquot soil sample and submitted to laboratory for analysis of VOCs
by EPA method 8260. One duplicate soil sample will also be collected for the same analyses as the parent sample.

In addition to the in situ soil characterization soil sampling described above, H&H will collect a soil sample to
characterize an approximate 450 cubic yard stockpile generated during installation of erosion control measures in the
western portion of the Site. H&H will collect 5 aliquot soil samples from stockpile. The aliquots collected from the
stockpile will be homogenized to form a composite soil sample representative of the stockpile. The composite soil
sample will be collected directly into laboratory supplied glassware, labeled with the sample ID, date, and requested
analyses and placed in a laboratory supplied cooler with ice. Additionally, one grab sample will be collected from
undisturbed portions of a select aliquot soil sample prior to homogenization for the composite soil sample. The soil
sample will be submitted for the same analyses as the in situ soil samples described above.

If results of the above sampling indicate that there are no impacts above acceptable levels, the PD for the Charlotte Van
and Storage site would like to export the topsoil to Fleet Maintenance facility on Lucia-Riverbend Highway in Mt.
Holly. The PD has previously obtained approval from Josyelyn Harriger and Ervin Lane to export soil from the Market 42
Brownfields property (BPN 2124-17-060) to the Fleet Maintenance facility in 2019 (see attached letter for ease of
reference). In accordance with the DEQ-approved EMP, we are putting together a package to provide the following for
export approval:
 A letter indicating the PD’s request for DEQ approval for transfer of soil from the Charlotte Van and Storage
property to the Fleet Maintenance property;
 Written acceptance of the Charlotte Van and Storage soil from the owner of the Fleet Maintenance facility;
 A figure depicting the areas of cut relative to soil sample locations; and
 Cumulative hypothetical worst-case risk calculators using soil sample laboratory analytical results for the
receiving property.

We will send the documentation above and a data summary package as soon as they are available. In the meantime,
please let us know if you have questions or require additional information.

Thank you,
Haley

Haley Martin, PG, Project Geologist
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 · Charlotte, NC 28203
Direct: 704-526-2045 · Mobile: [phone]
www.harthickman.com

Table 1
Summary of Soil Analytical Data
Charlotte Van Storage Co.
Verbena Street and Gilead Street
Charlotte, North Carolina
H&H Job No. LEN-008
Sample ID SB-1 SB-2 SB-3
Sample Type Composite Grab Composite Grab Composite Grab Composite Grab
Depth (ft bgs)
Date Range Range Mean
Units
VOCs (8260B)
Acetone NA 0.006 J NA 0.012 J NA 0.039 NA 0.032 NA NA NA 25 12,000 140,000 -- -- --
Carbon Disulfide NA <0.0008 NA <0.0008 NA 0.003 J NA 0.002 J NA NA NA 4.1 160 740 -- -- --
Ethanol NA <0.017 NA <0.017 NA 0.133 J NA 0.134 J NA NA NA NE NE NE -- -- --
2-Butanone NA <0.0008 NA 0.001 J NA 0.002 J NA <0.0010 NA NA NA 17 5,500 40,000 -- -- --
1,2,4-Trimethylbenzene NA <0.0006 NA <0.0006 NA <0.0006 NA <0.0007 NA NA NA 12 63 370 -- -- --
SVOCs (8270D)
Anthracene <0.182 NA 0.180 J NA <0.181 NA <0.181 NA NA NA NA 1,300 3,600 45,000 -- -- --
Benzo(a)anthracene <0.177 NA 0.568 J NA <0.176 NA <0.176 NA NA NA NA 0.35 1.1 21 -- -- --
Benzo(a)pyrene <0.187 NA 0.603 J NA <0.186 NA <0.186 NA NA NA NA 0.12 0.11 2.1 -- -- --
Benzo(b)fluoranthene <0.186 NA 0.787 J NA 0.222 J NA <0.185 NA NA NA NA 1.2 1.1 21 -- -- --
Benzo(g,h,i)perylene <0.173 NA 0.360 J NA <0.172 NA <0.172 NA NA NA NA NE NE NE -- -- --
Benzo(k)fluoranthene <0.174 NA 0.274 J NA <0.174 NA <0.173 NA NA NA NA 12 11 210 -- -- --
Chrysene <0.181 NA 0.516 J NA <0.180 NA <0.179 NA NA NA NA 36 110 2,100 -- -- --
Fluoranthene <0.157 NA 1.36 NA 0.312 J NA <0.155 NA NA NA NA 670 480 6,000 -- -- --
Ideno(1,2,3-cd)pyrene <0.228 NA 0.425 J NA <0.227 NA <0.226 NA NA NA NA 3.9 1.1 21 -- -- --
Phenanthrene <0.265 NA 1.09 NA <0.264 NA <0.263 NA NA NA NA NE NE NE -- -- --
Pyrene <0.171 NA 1.16 NA 0.269 J NA <0.169 NA NA NA NA 440 360.00 4500.00 -- -- --
Metals (6020/7471/7199)
Arsenic 1.86 NA 1.73 NA 2.39 NA 1.27 NA 1.11 J 0.391 J 3.52 5.8 0.68 3.0 1.28 - 3.03 1.0 - 18 4.8
Barium 109 NA 50.5 NA 113 NA 96.5 NA 66.2 44.3 68.7 580 3,100 47,000 38.1 - 94.6 50 - 1,000 356
Cadmium <0.0702 NA <0.0680 NA <0.0698 NA <0.0697 NA <0.0655 <0.0649 0.207 J 3 14 200 ND - 0.434 1.0 - 10 4.3
Chromium (total) 66.4 NA 50.6 NA 45.4 NA 43.7 NA 80.8 30.9 25.7 ---- --47.1 - 59.9 7.0 - 300 65
Hexavalent Chromium 0.48 J NA 0.57 J NA 3.6 NA 3.1 NA 1.3 <0.26 <0.26 3.8 0.31 6.5 ND - 0.540 NS NS
Trivalent Chromium 65.92 NA 50.03 NA 41.8 NA 40.6 NA 79.5 30.9 25.7 360,000 23,000 350,000 47.1 - 59.4 NS NS
Lead 9.78 NA 10.5 NA 13.0 NA 6.50 NA 6.13 6.3 10.3 270 400 800 7.33 - 11.6 ND - 50 16
Mercury 0.0186 J NA 0.0275 J NA 0.0161 J NA <0.0152 NA 0.0155 J <0.0142 <0.0156 NE 4.7 70 0.0365 - 0.0502 0.03 - 0.52 0.121
Selenium <1.15 NA <1.11 NA <1.14 NA <1.14 NA 10.8 J <1.06 <1.47 J 2.1 78 1,200 0.586 - 1.04 <0.1 - 0.8 0.42
Silver <0.0523 NA <0.0507 NA <0.0520 NA <0.0519 NA <0.0488 <0.0484 <0.0534 3.4 78 1,200 ND ND - 5.0 NS
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021)
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Compound concentrations are reported to the laboratory method detection limits.
Aside from metals, only those compounds detected in at least one sample are shown above.
Laboratory analytical methods are shown in parentheses.
Shaded values exceed the Protection of Groundwater PSRG.
Bold values exceed the Residential PSRG.
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface
NS= not specified; NA = not analyzed; -- = not applicable; NE = not established; ND = not detected at concentration above laboratory detection limit
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
mg/kg mg/kg
EX-10
0-1.5
12/15/2021
EX-11/DUP
Building 1 - Proposed Parking Area
1-3
8/27/2021
Protection of
Groundwater
PSRGs (1)
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Site-Specific
Background
Metals in Soil
Regional Background
Metals in Soil (2)Grab
EX-9 Screening Criteria
Sample Location Fleet Maintenance Facility
https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Lennar (LEN)/LEN‐008 Verbena Assemblage/Site Work/Charlotte Van & Storage Co. (LEN‐008) Stockpile.xlsx
1/3/2022
Table 1 (Page 1 of 2)
Hart & Hickman, PC
Table 1
Summary of Soil Analytical Data
Charlotte Van Storage Co.
Verbena Street and Gilead Street
Charlotte, North Carolina
H&H Job No. LEN-008
Sample ID SB-1 SB-2 SB-3
Sample Type Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab
Depth (ft bgs)
Date Range Range Mean
Units
VOCs (8260B)
Acetone NA 0.007 J NA 0.012 J NA 0.020 J NA 0.016 J NA 0.009 J NA NA NA 25 12,000 140,000 -- -- --
Carbon Disulfide NA <0.0008 NA <0.0008 NA <0.0008 NA <0.001 NA <0.0008 NA NA NA 4.1 160 740 -- -- --
Ethanol NA 0.034 J NA <0.018 NA <0.017 NA 0.095 J NA 0.021 J NA NA NA NE NE NE -- -- --
2-Butanone NA <0.0008 NA <0.0008 NA <0.0008 NA <0.001 NA <0.0008 NA NA NA 17 5,500 40,000 -- -- --
1,2,4-Trimethylbenzene NA 0.0009 J NA <0.0006 NA <0.0006 NA <0.0008 NA <0.0006 NA NA NA 12 63 370 -- -- --
SVOCs (8270D)
Anthracene <0.180 NA <0.184 NA <0.175 NA <0.229 NA <0.176 NA NA NA NA 1,300 3,600 45,000 -- -- --
Benzo(a)anthracene <0.175 NA <0.179 NA <0.170 NA <0.223 NA <0.171 NA NA NA NA 0.35 1.1 21 -- -- --
Benzo(a)pyrene <0.185 NA <0.189 NA <0.180 NA <0.236 NA <0.181 NA NA NA NA 0.12 0.11 2.1 -- -- --
Benzo(b)fluoranthene <0.184 NA <0.188 NA <0.179 NA 0.234 J NA <0.180 NA NA NA NA 1.2 1.1 21 -- -- --
Benzo(g,h,i)perylene <0.171 NA <0.175 NA <0.166 NA <0.218 NA <0.168 NA NA NA NA NE NE NE -- -- --
Benzo(k)fluoranthene <0.172 NA <0.176 NA <0.168 NA <0.220 NA <0.169 NA NA NA NA 12 11 210 -- -- --
Chrysene <0.179 NA <0.183 NA <0.174 NA <0.228 NA <0.175 NA NA NA NA 36 110 2,100 -- -- --
Fluoranthene <0.155 NA <0.158 NA <0.150 NA 0.231 J NA <0.152 NA NA NA NA 670 480 6,000 -- -- --
Ideno(1,2,3-cd)pyrene <0.226 NA <0.230 NA <0.219 NA <0.287 NA <0.221 NA NA NA NA 3.9 1.1 21 -- -- --
Phenanthrene <0.262 NA <0.268 NA <0.255 NA <0.334 NA <0.257 NA NA NA NA NE NE NE -- -- --
Pyrene <0.169 NA <0.172 NA <0.164 NA 0.228 J NA <0.165 NA NA NA NA 440 360.00 4500.00 -- -- --
Metals (6020/7471/7199)
Arsenic 1.65 NA 1.42 NA 1.28 NA 1.98 NA 1.17 J NA 1.11 J 0.391 J 3.52 5.8 0.68 3.0 1.28 - 3.03 1.0 - 18 4.8
Barium 138 NA 109 NA 106 NA 99.7 NA 525 NA 66.2 44.3 68.7 580 3,100 47,000 38.1 - 94.6 50 - 1,000 356
Cadmium <0.0694 NA <0.0709 NA <0.0674 NA 0.167 J NA <0.0679 NA <0.0655 <0.0649 0.207 J 3 14 200 ND - 0.434 1.0 - 10* 4.3
Chromium (total) 41.4 NA 45.4 NA 55.3 NA 47.7 NA 39.4 NA 80.8 30.9 25.7 ---- --47.1 - 59.9 7.0 - 300 65
Hexavalent Chromium 0.44 J NA <0.25 NA 0.41 J NA 0.50 J NA 0.29 J NA 1.3 <0.26 <0.26 3.8 0.31 6.5 ND - 0.540 NS NS
Trivalent Chromium 40.96 NA 45.4 NA 54.89 NA 47.2 NA 39.1 NA 79.5 30.9 25.7 360,000 23,000 350,000 47.1 - 59.4 NS NS
Lead 22.2 NA 11.5 NA 13.3 NA 33.3 NA 4.03 NA 6.13 6.3 10.3 270 400 800 7.33 - 11.6 ND - 50 16
Mercury 0.0188 J NA 0.0526 NA <0.0147 NA 0.0297 J NA <0.0148 NA 0.0155 J <0.0142 <0.0156 NE 4.7 70 0.0365 - 0.0502 0.03 - 0.52 0.121
Selenium <1.14 NA <1.16 NA <1.10 NA <1.45 NA <1.11 NA 10.8 J <1.06 <1.47 J 2.1 78 1,200 0.586 - 1.04 <0.1 - 0.8 0.42
Silver <0.0517 NA <0.0529 NA 0.0509 J NA <0.0659 NA <0.0506 NA <0.0488 <0.0484 <0.0534 3.4 78 1,200 ND ND - 5.0 NS
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021)
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Compound concentrations are reported to the laboratory method detection limits.
Aside from metals, only those compounds detected in at least one sample are shown above.
Laboratory analytical methods are shown in parentheses.
Shaded values exceed the Protection of Groundwater PSRG.
Bold values exceed the Residential PSRG.
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface
NS= not specified; NA = not analyzed; -- = not applicable; NE = not established; ND = not detected at concentration above laboratory detection limit
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
mg/kg mg/kg
SP-1215-4
--
12/15/2021
Regional Background
Metals in Soil (2)Grab
1-3
8/27/2021
Screening Criteria
Sample Location Stockpile Fleet Maintenance Facility
Protection of
Groundwater
PSRGs (1)
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Site-Specific
Background
Metals in Soil
SP-1215-1 SP-1215-2 SP-1215-3 SP-1215-5
https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Lennar (LEN)/LEN‐008 Verbena Assemblage/Site Work/Charlotte Van & Storage Co. (LEN‐008) Stockpile.xlsx
1/3/2022
Table 1 (Page 2 of 2)
Hart & Hickman, PC
!(
!(
!(
!(
!(
!(
!(
!(
!(!(
!(
!(
!(
!(
!(
EX-9
(950 yd3)
EX-10
(952 yd3)
EX-11/DUP
(955 yd3)

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/29/2021
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 21-350-0013 Client Project Description: LEN.008
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 12/16/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 129
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-350-0013
Page 2 of 129
Report Number:
Sample Summary Table
Client Project Description:
21-350-0013
LEN.008
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
12/15/2021 10:20Solids 90731 Ex-9 12/16/2021 12:34 7199
12/15/2021 10:20Solids 90731 Ex-9 12/16/2021 12:34
12/15/2021 09:50Solids 90732 Ex-10 12/16/2021 12:34 7199
12/15/2021 09:50Solids 90732 Ex-10 12/16/2021 12:34
12/15/2021 09:20Solids 90733 Ex-11 12/16/2021 12:34 7199
12/15/2021 09:20Solids 90733 Ex-11 12/16/2021 12:34
12/15/2021 09:20Solids 90734 DUP 12/16/2021 12:34 7199
12/15/2021 09:20Solids 90734 DUP 12/16/2021 12:34
12/15/2021 11:15Solids 90735 SP-1215-1 12/16/2021 12:34 7199
12/15/2021 11:15Solids 90735 SP-1215-1 12/16/2021 12:34
12/15/2021 11:45Solids 90736 SP-1215-2 12/16/2021 12:34 7199
12/15/2021 11:45Solids 90736 SP-1215-2 12/16/2021 12:34
12/15/2021 12:20Solids 90737 SP-1215-3 12/16/2021 12:34 7199
12/15/2021 12:20Solids 90737 SP-1215-3 12/16/2021 12:34
12/15/2021 13:00Solids 90738 SP-1215-4 12/16/2021 12:34 7199
12/15/2021 13:00Solids 90738 SP-1215-4 12/16/2021 12:34
12/15/2021 10:40Solids 90739 SP-1215-5 12/16/2021 12:34 7199
12/15/2021 10:40Solids 90739 SP-1215-5 12/16/2021 12:34
: Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 129
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-350-0013
Report Limit
Project:LEN.008
V 90731Ex-9
1.86 12/20/2021 22:516020BArsenicmg/Kg - dry 0.120
109 12/20/2021 22:516020BBariummg/Kg - dry 1.79
66.4 12/20/2021 22:516020BChromiummg/Kg - dry 0.370
9.78 12/20/2021 22:516020BLeadmg/Kg - dry 0.179
J0.0186 12/21/2021 17:327471BMercury (Total)mg/Kg - dry 0.0153
J0.006 12/17/2021 14:198260DAcetonemg/Kg - dry 0.003
21.7 12/21/2021 17:16SW-DRYWT Moisture %
V 90732Ex-10
1.73 12/20/2021 22:576020BArsenicmg/Kg - dry 0.116
50.5 12/20/2021 22:576020BBariummg/Kg - dry 1.73
50.6 12/20/2021 22:576020BChromiummg/Kg - dry 0.358
10.5 12/20/2021 22:576020BLeadmg/Kg - dry 0.173
J0.0275 12/21/2021 17:407471BMercury (Total)mg/Kg - dry 0.0149
J0.012 12/17/2021 14:478260DAcetonemg/Kg - dry 0.002
J0.001 12/17/2021 14:478260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.180 12/27/2021 19:058270EAnthracenemg/Kg - dry 0.176
J0.568 12/27/2021 19:058270EBenzo(a)anthracene mg/Kg - dry 0.172
J0.603 12/27/2021 19:058270EBenzo(a)pyrene mg/Kg - dry 0.181
J0.787 12/27/2021 19:058270EBenzo(b)fluoranthene mg/Kg - dry 0.180
J0.360 12/27/2021 19:058270EBenzo(g,h,i)perylene mg/Kg - dry 0.168
J0.274 12/27/2021 19:058270EBenzo(k)fluoranthene mg/Kg - dry 0.169
J0.516 12/27/2021 19:058270EChrysenemg/Kg - dry 0.175
1.36 12/27/2021 19:058270EFluoranthenemg/Kg - dry 0.152
J0.425 12/27/2021 19:058270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.221
1.09 12/27/2021 19:058270EPhenanthrenemg/Kg - dry 0.257
1.16 12/27/2021 19:058270EPyrenemg/Kg - dry 0.165
19.2 12/21/2021 17:16SW-DRYWT Moisture %
V 90733Ex-11
2.39 12/20/2021 23:046020BArsenicmg/Kg - dry 0.119
113 12/20/2021 23:046020BBariummg/Kg - dry 1.78
45.4 12/20/2021 23:046020BChromiummg/Kg - dry 0.368
13.0 12/20/2021 23:046020BLeadmg/Kg - dry 0.178
J0.0161 12/21/2021 17:437471BMercury (Total)mg/Kg - dry 0.0152
0.039 12/17/2021 15:158260DAcetonemg/Kg - dry 0.003
J0.003 12/17/2021 15:158260DCarbon Disulfide mg/Kg - dry 0.0008
J0.133 12/17/2021 15:158260DEthanolmg/Kg - dry 0.017
Page 4 of 129
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-350-0013
Report Limit
Project:LEN.008
V 90733Ex-11
J0.002 12/17/2021 15:158260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.222 12/27/2021 19:288270EBenzo(b)fluoranthene mg/Kg - dry 0.185
J0.312 12/27/2021 19:288270EFluoranthenemg/Kg - dry 0.156
J0.269 12/27/2021 19:288270EPyrenemg/Kg - dry 0.170
21.3 12/21/2021 17:16SW-DRYWT Moisture %
V 90734DUP
1.27 12/20/2021 23:106020BArsenicmg/Kg - dry 0.119
96.5 12/20/2021 23:106020BBariummg/Kg - dry 1.77
43.7 12/20/2021 23:106020BChromiummg/Kg - dry 0.367
6.50 12/20/2021 23:106020BLeadmg/Kg - dry 0.177
0.032 12/17/2021 15:428260DAcetonemg/Kg - dry 0.003
J0.002 12/17/2021 15:428260DCarbon Disulfide mg/Kg - dry 0.001
J0.134 12/17/2021 15:428260DEthanolmg/Kg - dry 0.021
21.1 12/21/2021 17:16SW-DRYWT Moisture %
V 90735SP-1215-1
1.65 12/20/2021 23:176020BArsenicmg/Kg - dry 0.119
138 12/20/2021 23:176020BBariummg/Kg - dry 1.77
41.4 12/20/2021 23:176020BChromiummg/Kg - dry 0.366
22.2 12/20/2021 23:176020BLeadmg/Kg - dry 0.177
J0.0188 12/21/2021 17:507471BMercury (Total)mg/Kg - dry 0.0152
J0.007 12/17/2021 16:108260DAcetonemg/Kg - dry 0.003
J0.034 12/17/2021 16:108260DEthanolmg/Kg - dry 0.017
J0.0009 12/17/2021 16:108260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
20.8 12/21/2021 17:16SW-DRYWT Moisture %
V 90736SP-1215-2
1.42 12/20/2021 23:366020BArsenicmg/Kg - dry 0.121
109 12/20/2021 23:366020BBariummg/Kg - dry 1.81
45.4 12/20/2021 23:366020BChromiummg/Kg - dry 0.374
11.5 12/20/2021 23:366020BLeadmg/Kg - dry 0.181
0.0526 12/21/2021 17:557471BMercury (Total)mg/Kg - dry 0.0155
J0.012 12/17/2021 16:388260DAcetonemg/Kg - dry 0.003
22.5 12/21/2021 17:16SW-DRYWT Moisture %
V 90737SP-1215-3
1.28 12/20/2021 23:436020BArsenicmg/Kg - dry 0.115
Page 5 of 129
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-350-0013
Report Limit
Project:LEN.008
V 90737SP-1215-3
106 12/20/2021 23:436020BBariummg/Kg - dry 1.72
55.3 12/20/2021 23:436020BChromiummg/Kg - dry 0.355
13.3 12/20/2021 23:436020BLeadmg/Kg - dry 0.172
J0.0509 12/20/2021 23:436020BSilvermg/Kg - dry 0.0503
J0.020 12/17/2021 17:068260DAcetonemg/Kg - dry 0.002
18.5 12/21/2021 17:16SW-DRYWT Moisture %
V 90738SP-1215-4
1.98 12/20/2021 23:496020BArsenicmg/Kg - dry 0.151
99.7 12/20/2021 23:496020BBariummg/Kg - dry 2.25
J0.167 12/20/2021 23:496020BCadmiummg/Kg - dry 0.0884
47.7 12/20/2021 23:496020BChromiummg/Kg - dry 0.466
33.3 12/20/2021 23:496020BLeadmg/Kg - dry 0.225
J0.0297 12/21/2021 18:157471BMercury (Total)mg/Kg - dry 0.0193
J0.016 12/17/2021 17:348260DAcetonemg/Kg - dry 0.003
J0.095 12/17/2021 17:348260DEthanolmg/Kg - dry 0.022
J0.234 12/27/2021 21:238270EBenzo(b)fluoranthene mg/Kg - dry 0.234
J0.231 12/27/2021 21:238270EFluoranthenemg/Kg - dry 0.197
J0.228 12/27/2021 21:238270EPyrenemg/Kg - dry 0.215
37.8 12/21/2021 17:16SW-DRYWT Moisture %
V 90739SP-1215-5
J1.17 12/20/2021 23:566020BArsenicmg/Kg - dry 0.116
525 12/20/2021 23:566020BBariummg/Kg - dry 1.73
39.4 12/20/2021 23:566020BChromiummg/Kg - dry 0.358
4.03 12/20/2021 23:566020BLeadmg/Kg - dry 0.173
J0.009 12/17/2021 18:018260DAcetonemg/Kg - dry 0.002
J0.021 12/17/2021 18:018260DEthanolmg/Kg - dry 0.017
19.1 12/21/2021 17:16SW-DRYWT Moisture %
Page 6 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-9
90731 Matrix:
12/15/2021 10:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.7 %Moisture 1 12/21/21 17:16 SW-DRYWTCEG
1.86 mg/Kg - dry 0.120 1.28Arsenic 10 12/20/21 22:51 6020BEDV
109 mg/Kg - dry 1.79 12.8Barium 10 12/20/21 22:51 6020BEDV
<0.0702 mg/Kg - dry 0.0702 0.639Cadmium 10 12/20/21 22:51 6020BEDV
66.4 mg/Kg - dry 0.370 1.28Chromium 10 12/20/21 22:51 6020BEDV
9.78 mg/Kg - dry 0.179 1.28
Lead 10 12/20/21 22:51 6020BEDV
0.0186 J mg/Kg - dry 0.0153 0.0383Mercury (Total)1 12/21/21 17:32 7471BEDV
<1.15 mg/Kg - dry 1.15 2.55Selenium 10 12/20/21 22:51 6020BEDV
<0.0523 mg/Kg - dry 0.0523 0.639Silver 10 12/20/21 22:51 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 7 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-9
90731 Matrix:
12/15/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
0.006 J mg/Kg - dry 0.003 0.025Acetone 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 12/17/21 14:19 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 12/17/21 14:19 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/17/21 14:19 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/17/21 14:19 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/17/21 14:19 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/17/21 14:19 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/17/21 14:19 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/17/21 14:19 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/17/21 14:19 V12995TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/17/21 14:19 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/17/21 14:19 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/17/21 14:19 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/17/21 14:19 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/17/21 14:19 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/17/21 14:19 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-9
90731 Matrix:
12/15/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 12/17/21 14:19 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 12/17/21 14:19 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/17/21 14:19 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/17/21 14:19 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/17/21 14:19 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/17/21 14:19 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/17/21 14:19 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/17/21 14:19 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/17/21 14:19 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 12/17/21 14:19 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/17/21 14:19 V12995TBL
<0.017 mg/Kg - dry 0.017 0.319Ethanol 1 12/17/21 14:19 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 12/17/21 14:19 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-9
90731 Matrix:
12/15/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 12/17/21 14:19 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 12/17/21 14:19 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/17/21 14:19 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 12/17/21 14:19 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/17/21 14:19 V12995TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/17/21 14:19 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/17/21 14:19 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/17/21 14:19 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 12/17/21 14:19 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 12/17/21 14:19 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/17/21 14:19 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/17/21 14:19 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/17/21 14:19 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/17/21 14:19 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-9
90731 Matrix:
12/15/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/17/21 14:19 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/17/21 14:19 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/17/21 14:19 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/17/21 14:19 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/17/21 14:19 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/17/21 14:19 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/17/21 14:19 V12995
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%12/17/21 14:191 TBL V12995
Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/17/21 14:191 TBL V12995
Surrogate: Toluene-d8 87.4 Limits: 76-129%12/17/21 14:191 TBL V12995
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.148 mg/Kg - dry 0.148 0.844Acenaphthene 1 12/27/21 18:41 V13287JMV
<0.134 mg/Kg - dry 0.134 0.844Acenaphthylene 1 12/27/21 18:41 V13287JMV
<0.194 mg/Kg - dry 0.194 0.844Aniline 1 12/27/21 18:41 V13287JMV
<0.182 mg/Kg - dry 0.182 0.844Anthracene 1 12/27/21 18:41 V13287JMV
<0.177 mg/Kg - dry 0.177 0.844
Benzo(a)anthracene 1 12/27/21 18:41 V13287JMV
<0.187 mg/Kg - dry 0.187 0.844Benzo(a)pyrene 1 12/27/21 18:41 V13287JMV
<0.186 mg/Kg - dry 0.186 0.844Benzo(b)fluoranthene 1 12/27/21 18:41 V13287JMV
<0.173 mg/Kg - dry 0.173 0.844Benzo(g,h,i)perylene 1 12/27/21 18:41 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-9
90731 Matrix:
12/15/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.174 mg/Kg - dry 0.174 0.844Benzo(k)fluoranthene 1 12/27/21 18:41 V13287JMV
<0.740 mg/Kg - dry 0.740 2.55Benzoic Acid 1 12/27/21 18:41 V13287JMV
<0.134 mg/Kg - dry 0.134 0.844Benzyl alcohol 1 12/27/21 18:41 V13287JMV
<0.150 mg/Kg - dry 0.150 0.844Bis(2-Chloroethoxy)methane 1 12/27/21 18:41 V13287JMV
<0.136 mg/Kg - dry 0.136 0.844Bis(2-Chloroethyl)ether 1 12/27/21 18:41 V13287JMV
<0.173 mg/Kg - dry 0.173 0.422Bis(2-Chloroisopropyl)ether 1 12/27/21 18:41 V13287JMV
<0.153 mg/Kg - dry 0.153 0.844Bis(2-ethylhexyl)phthalate 1 12/27/21 18:41 V13287JMV
<0.139 mg/Kg - dry 0.139 0.8444-Bromophenyl phenyl ether 1 12/27/21 18:41 V13287JMV
<0.144 mg/Kg - dry 0.144 0.422
Butyl benzyl phthalate 1 12/27/21 18:41 V13287JMV
<0.118 mg/Kg - dry 0.118 0.8444-Chloro-3-methylphenol 1 12/27/21 18:41 V13287JMV
<0.143 mg/Kg - dry 0.143 0.4224-Chloroaniline 1 12/27/21 18:41 V13287JMV
<0.148 mg/Kg - dry 0.148 0.8442-Chloronaphthalene 1 12/27/21 18:41 V13287JMV
<0.125 mg/Kg - dry 0.125 0.8442-Chlorophenol 1 12/27/21 18:41 V13287JMV
<0.160 mg/Kg - dry 0.160 1.284-Chlorophenyl phenyl ether 1 12/27/21 18:41 V13287JMV
<0.181 mg/Kg - dry 0.181 0.844Chrysene 1 12/27/21 18:41 V13287JMV
<0.293 mg/Kg - dry 0.293 0.844
Dibenz(a,h)anthracene 1 12/27/21 18:41 V13287JMV
<0.151 mg/Kg - dry 0.151 0.844Dibenzofuran 1 12/27/21 18:41 V13287JMV
<0.120 mg/Kg - dry 0.120 0.8441,2-Dichlorobenzene 1 12/27/21 18:41 V13287JMV
<0.124 mg/Kg - dry 0.124 0.8441,3-Dichlorobenzene 1 12/27/21 18:41 V13287JMV
<0.124 mg/Kg - dry 0.124 0.4221,4-Dichlorobenzene 1 12/27/21 18:41 V13287JMV
<0.187 mg/Kg - dry 0.187 0.8443,3'-Dichlorobenzidine 1 12/27/21 18:41 V13287JMV
<0.122 mg/Kg - dry 0.122 0.8442,4-Dichlorophenol 1 12/27/21 18:41 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-9
90731 Matrix:
12/15/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.229 mg/Kg - dry 0.229 0.844Diethyl phthalate 1 12/27/21 18:41 V13287JMV
<0.222 mg/Kg - dry 0.222 0.844Dimethyl phthalate 1 12/27/21 18:41 V13287JMV
<0.137 mg/Kg - dry 0.137 0.4222,4-Dimethylphenol 1 12/27/21 18:41 V13287JMV
<0.136 mg/Kg - dry 0.136 0.844Di-n-butyl phthalate 1 12/27/21 18:41 V13287JMV
<0.306 mg/Kg - dry 0.306 1.924,6-Dinitro-2-methylphenol 1 12/27/21 18:41 V13287JMV
<0.664 mg/Kg - dry 0.664 1.922,4-Dinitrophenol 1 12/27/21 18:41 V13287JMV
<0.123 mg/Kg - dry 0.123 0.8442,4-Dinitrotoluene 1 12/27/21 18:41 V13287JMV
<0.137 mg/Kg - dry 0.137 0.8442,6-Dinitrotoluene 1 12/27/21 18:41 V13287JMV
<0.182 mg/Kg - dry 0.182 0.422
Di-n-Octyl Phthalate 1 12/27/21 18:41 V13287JMV
<0.157 mg/Kg - dry 0.157 0.844Fluoranthene 1 12/27/21 18:41 V13287JMV
<0.163 mg/Kg - dry 0.163 0.844Fluorene 1 12/27/21 18:41 V13287JMV
<0.135 mg/Kg - dry 0.135 0.844Hexachlorobenzene 1 12/27/21 18:41 V13287JMV
<0.124 mg/Kg - dry 0.124 0.844Hexachlorobutadiene 1 12/27/21 18:41 V13287JMV
<0.200 mg/Kg - dry 0.200 0.844Hexachlorocyclopentadiene 1 12/27/21 18:41 V13287JMV
<0.101 mg/Kg - dry 0.101 0.844Hexachloroethane 1 12/27/21 18:41 V13287JMV
<0.228 mg/Kg - dry 0.228 0.844
Indeno(1,2,3-cd)pyrene 1 12/27/21 18:41 V13287JMV
<0.243 mg/Kg - dry 0.243 0.844Isophorone 1 12/27/21 18:41 V13287JMV
<0.135 mg/Kg - dry 0.135 0.8441-Methylnaphthalene 1 12/27/21 18:41 V13287JMV
<0.127 mg/Kg - dry 0.127 0.8442-Methylnaphthalene 1 12/27/21 18:41 V13287JMV
<0.124 mg/Kg - dry 0.124 0.8442-Methylphenol 1 12/27/21 18:41 V13287JMV
<0.108 mg/Kg - dry 0.108 0.8443&4 Methylphenol 1 12/27/21 18:41 V13287JMV
<0.183 mg/Kg - dry 0.183 0.844Naphthalene 1 12/27/21 18:41 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-9
90731 Matrix:
12/15/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.123 mg/Kg - dry 0.123 0.8442-Nitroaniline 1 12/27/21 18:41 V13287JMV
<0.153 mg/Kg - dry 0.153 0.8443-Nitroaniline 1 12/27/21 18:41 V13287JMV
<0.119 mg/Kg - dry 0.119 0.4224-Nitroaniline 1 12/27/21 18:41 V13287JMV
<0.148 mg/Kg - dry 0.148 0.422Nitrobenzene 1 12/27/21 18:41 V13287JMV
<0.113 mg/Kg - dry 0.113 0.8442-Nitrophenol 1 12/27/21 18:41 V13287JMV
<0.149 mg/Kg - dry 0.149 0.8444-Nitrophenol 1 12/27/21 18:41 V13287JMV
<0.335 mg/Kg - dry 0.335 0.844N-Nitrosodimethylamine 1 12/27/21 18:41 V13287JMV
<0.231 mg/Kg - dry 0.231 0.844N-Nitrosodiphenylamine 1 12/27/21 18:41 V13287JMV
<0.150 mg/Kg - dry 0.150 0.844
N-Nitroso-di-n-propylamine 1 12/27/21 18:41 V13287JMV
<0.443 mg/Kg - dry 0.443 1.28Pentachlorophenol 1 12/27/21 18:41 V13287JMV
<0.265 mg/Kg - dry 0.265 0.844Phenanthrene 1 12/27/21 18:41 V13287JMV
<0.143 mg/Kg - dry 0.143 0.844Phenol 1 12/27/21 18:41 V13287JMV
<0.171 mg/Kg - dry 0.171 0.844Pyrene 1 12/27/21 18:41 V13287JMV
<0.101 mg/Kg - dry 0.101 0.422Pyridine 1 12/27/21 18:41 V13287JMV
<0.136 mg/Kg - dry 0.136 0.8441,2,4-Trichlorobenzene 1 12/27/21 18:41 V13287JMV
<0.122 mg/Kg - dry 0.122 0.844
2,4,5-Trichlorophenol 1 12/27/21 18:41 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-9
90731 Matrix:
12/15/2021 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.123 mg/Kg - dry 0.123 0.8442,4,6-Trichlorophenol 1 12/27/21 18:41 V13287JMV
Surrogate: Phenol-d5 73.4 Limits: 34-121%12/27/21 18:411 JMV V13287
Surrogate: 2-Fluorobiphenyl 71.9 Limits: 44-115%12/27/21 18:411 JMV V13287
Surrogate: 2-Fluorophenol 74.6 Limits: 35-115%12/27/21 18:411 JMV V13287
Surrogate: Nitrobenzene-d5 63.5 Limits: 37-122%12/27/21 18:411 JMV V13287
Surrogate: 4-Terphenyl-d14 82.6 Limits: 54-127%12/27/21 18:411 JMV V13287
Surrogate: 2,4,6-Tribromophenol 56.0 Limits: 39-132%12/27/21 18:411 JMV V13287
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-10
90732 Matrix:
12/15/2021 9:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.2 %Moisture 1 12/21/21 17:16 SW-DRYWTCEG
1.73 mg/Kg - dry 0.116 1.24Arsenic 10 12/20/21 22:57 6020BEDV
50.5 mg/Kg - dry 1.73 12.4Barium 10 12/20/21 22:57 6020BEDV
<0.0680 mg/Kg - dry 0.0680 0.619Cadmium 10 12/20/21 22:57 6020BEDV
50.6 mg/Kg - dry 0.358 1.24Chromium 10 12/20/21 22:57 6020BEDV
10.5 mg/Kg - dry 0.173 1.24
Lead 10 12/20/21 22:57 6020BEDV
0.0275 J mg/Kg - dry 0.0149 0.0371Mercury (Total)1 12/21/21 17:40 7471BEDV
<1.11 mg/Kg - dry 1.11 2.48Selenium 10 12/20/21 22:57 6020BEDV
<0.0507 mg/Kg - dry 0.0507 0.619Silver 10 12/20/21 22:57 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 16 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-10
90732 Matrix:
12/15/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
0.012 J mg/Kg - dry 0.002 0.024Acetone 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 12/17/21 14:47 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/17/21 14:47 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/17/21 14:47 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/17/21 14:47 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/17/21 14:47 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/17/21 14:47 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/17/21 14:47 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 12/17/21 14:47 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/17/21 14:47 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/17/21 14:47 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 12/17/21 14:47 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/17/21 14:47 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/17/21 14:47 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-10
90732 Matrix:
12/15/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/17/21 14:47 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/17/21 14:47 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/17/21 14:47 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/17/21 14:47 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/17/21 14:47 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/17/21 14:47 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/17/21 14:47 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 12/17/21 14:47 V12995TBL
<0.017 mg/Kg - dry 0.017 0.309Ethanol 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 12/17/21 14:47 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 12/17/21 14:47 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-10
90732 Matrix:
12/15/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 12/17/21 14:47 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 12/17/21 14:47 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/17/21 14:47 V12995TBL
0.001 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 12/17/21 14:47 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/17/21 14:47 V12995TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/17/21 14:47 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/17/21 14:47 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 12/17/21 14:47 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/17/21 14:47 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/17/21 14:47 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/17/21 14:47 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/17/21 14:47 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-10
90732 Matrix:
12/15/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/17/21 14:47 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/17/21 14:47 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/17/21 14:47 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/17/21 14:47 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/17/21 14:47 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/17/21 14:47 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/17/21 14:47 V12995
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%12/17/21 14:471 TBL V12995
Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/17/21 14:471 TBL V12995
Surrogate: Toluene-d8 87.2 Limits: 76-129%12/17/21 14:471 TBL V12995
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.143 mg/Kg - dry 0.143 0.818Acenaphthene 1 12/27/21 19:05 V13287JMV
<0.129 mg/Kg - dry 0.129 0.818Acenaphthylene 1 12/27/21 19:05 V13287JMV
<0.188 mg/Kg - dry 0.188 0.818Aniline 1 12/27/21 19:05 V13287JMV
0.180 J mg/Kg - dry 0.176 0.818Anthracene 1 12/27/21 19:05 V13287JMV
0.568 J
mg/Kg - dry 0.172 0.818
Benzo(a)anthracene 1 12/27/21 19:05 V13287JMV
0.603 J mg/Kg - dry 0.181 0.818Benzo(a)pyrene 1 12/27/21 19:05 V13287JMV
0.787 J mg/Kg - dry 0.180 0.818Benzo(b)fluoranthene 1 12/27/21 19:05 V13287JMV
0.360 J mg/Kg - dry 0.168 0.818Benzo(g,h,i)perylene 1 12/27/21 19:05 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-10
90732 Matrix:
12/15/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
0.274 J mg/Kg - dry 0.169 0.818Benzo(k)fluoranthene 1 12/27/21 19:05 V13287JMV
<0.717 mg/Kg - dry 0.717 2.48Benzoic Acid 1 12/27/21 19:05 V13287JMV
<0.129 mg/Kg - dry 0.129 0.818Benzyl alcohol 1 12/27/21 19:05 V13287JMV
<0.146 mg/Kg - dry 0.146 0.818Bis(2-Chloroethoxy)methane 1 12/27/21 19:05 V13287JMV
<0.132 mg/Kg - dry 0.132 0.818Bis(2-Chloroethyl)ether 1 12/27/21 19:05 V13287JMV
<0.168 mg/Kg - dry 0.168 0.409Bis(2-Chloroisopropyl)ether 1 12/27/21 19:05 V13287JMV
<0.148 mg/Kg - dry 0.148 0.818Bis(2-ethylhexyl)phthalate 1 12/27/21 19:05 V13287JMV
<0.134 mg/Kg - dry 0.134 0.8184-Bromophenyl phenyl ether 1 12/27/21 19:05 V13287JMV
<0.139 mg/Kg - dry 0.139 0.409
Butyl benzyl phthalate 1 12/27/21 19:05 V13287JMV
<0.114 mg/Kg - dry 0.114 0.8184-Chloro-3-methylphenol 1 12/27/21 19:05 V13287JMV
<0.138 mg/Kg - dry 0.138 0.4094-Chloroaniline 1 12/27/21 19:05 V13287JMV
<0.143 mg/Kg - dry 0.143 0.8182-Chloronaphthalene 1 12/27/21 19:05 V13287JMV
<0.121 mg/Kg - dry 0.121 0.8182-Chlorophenol 1 12/27/21 19:05 V13287JMV
<0.155 mg/Kg - dry 0.155 1.244-Chlorophenyl phenyl ether 1 12/27/21 19:05 V13287JMV
0.516 J mg/Kg - dry 0.175 0.818Chrysene 1 12/27/21 19:05 V13287JMV
<0.284 mg/Kg - dry 0.284 0.818
Dibenz(a,h)anthracene 1 12/27/21 19:05 V13287JMV
<0.147 mg/Kg - dry 0.147 0.818Dibenzofuran 1 12/27/21 19:05 V13287JMV
<0.116 mg/Kg - dry 0.116 0.8181,2-Dichlorobenzene 1 12/27/21 19:05 V13287JMV
<0.120 mg/Kg - dry 0.120 0.8181,3-Dichlorobenzene 1 12/27/21 19:05 V13287JMV
<0.121 mg/Kg - dry 0.121 0.4091,4-Dichlorobenzene 1 12/27/21 19:05 V13287JMV
<0.181 mg/Kg - dry 0.181 0.8183,3'-Dichlorobenzidine 1 12/27/21 19:05 V13287JMV
<0.118 mg/Kg - dry 0.118 0.8182,4-Dichlorophenol 1 12/27/21 19:05 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-10
90732 Matrix:
12/15/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.222 mg/Kg - dry 0.222 0.818Diethyl phthalate 1 12/27/21 19:05 V13287JMV
<0.215 mg/Kg - dry 0.215 0.818Dimethyl phthalate 1 12/27/21 19:05 V13287JMV
<0.133 mg/Kg - dry 0.133 0.4092,4-Dimethylphenol 1 12/27/21 19:05 V13287JMV
<0.132 mg/Kg - dry 0.132 0.818Di-n-butyl phthalate 1 12/27/21 19:05 V13287JMV
<0.297 mg/Kg - dry 0.297 1.864,6-Dinitro-2-methylphenol 1 12/27/21 19:05 V13287JMV
<0.643 mg/Kg - dry 0.643 1.862,4-Dinitrophenol 1 12/27/21 19:05 V13287JMV
<0.119 mg/Kg - dry 0.119 0.8182,4-Dinitrotoluene 1 12/27/21 19:05 V13287JMV
<0.133 mg/Kg - dry 0.133 0.8182,6-Dinitrotoluene 1 12/27/21 19:05 V13287JMV
<0.176 mg/Kg - dry 0.176 0.409
Di-n-Octyl Phthalate 1 12/27/21 19:05 V13287JMV
1.36 mg/Kg - dry 0.152 0.818Fluoranthene 1 12/27/21 19:05 V13287JMV
<0.158 mg/Kg - dry 0.158 0.818Fluorene 1 12/27/21 19:05 V13287JMV
<0.131 mg/Kg - dry 0.131 0.818Hexachlorobenzene 1 12/27/21 19:05 V13287JMV
<0.120 mg/Kg - dry 0.120 0.818Hexachlorobutadiene 1 12/27/21 19:05 V13287JMV
<0.194 mg/Kg - dry 0.194 0.818Hexachlorocyclopentadiene 1 12/27/21 19:05 V13287JMV
<0.098 mg/Kg - dry 0.098 0.818Hexachloroethane 1 12/27/21 19:05 V13287JMV
0.425 J
mg/Kg - dry 0.221 0.818
Indeno(1,2,3-cd)pyrene 1 12/27/21 19:05 V13287JMV
<0.236 mg/Kg - dry 0.236 0.818Isophorone 1 12/27/21 19:05 V13287JMV
<0.131 mg/Kg - dry 0.131 0.8181-Methylnaphthalene 1 12/27/21 19:05 V13287JMV
<0.123 mg/Kg - dry 0.123 0.8182-Methylnaphthalene 1 12/27/21 19:05 V13287JMV
<0.120 mg/Kg - dry 0.120 0.8182-Methylphenol 1 12/27/21 19:05 V13287JMV
<0.105 mg/Kg - dry 0.105 0.8183&4 Methylphenol 1 12/27/21 19:05 V13287JMV
<0.178 mg/Kg - dry 0.178 0.818Naphthalene 1 12/27/21 19:05 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-10
90732 Matrix:
12/15/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.119 mg/Kg - dry 0.119 0.8182-Nitroaniline 1 12/27/21 19:05 V13287JMV
<0.148 mg/Kg - dry 0.148 0.8183-Nitroaniline 1 12/27/21 19:05 V13287JMV
<0.115 mg/Kg - dry 0.115 0.4094-Nitroaniline 1 12/27/21 19:05 V13287JMV
<0.143 mg/Kg - dry 0.143 0.409Nitrobenzene 1 12/27/21 19:05 V13287JMV
<0.110 mg/Kg - dry 0.110 0.8182-Nitrophenol 1 12/27/21 19:05 V13287JMV
<0.144 mg/Kg - dry 0.144 0.8184-Nitrophenol 1 12/27/21 19:05 V13287JMV
<0.325 mg/Kg - dry 0.325 0.818N-Nitrosodimethylamine 1 12/27/21 19:05 V13287JMV
<0.224 mg/Kg - dry 0.224 0.818N-Nitrosodiphenylamine 1 12/27/21 19:05 V13287JMV
<0.146 mg/Kg - dry 0.146 0.818
N-Nitroso-di-n-propylamine 1 12/27/21 19:05 V13287JMV
<0.429 mg/Kg - dry 0.429 1.24Pentachlorophenol 1 12/27/21 19:05 V13287JMV
1.09 mg/Kg - dry 0.257 0.818Phenanthrene 1 12/27/21 19:05 V13287JMV
<0.138 mg/Kg - dry 0.138 0.818Phenol 1 12/27/21 19:05 V13287JMV
1.16 mg/Kg - dry 0.165 0.818Pyrene 1 12/27/21 19:05 V13287JMV
<0.098 mg/Kg - dry 0.098 0.409Pyridine 1 12/27/21 19:05 V13287JMV
<0.132 mg/Kg - dry 0.132 0.8181,2,4-Trichlorobenzene 1 12/27/21 19:05 V13287JMV
<0.119 mg/Kg - dry 0.119 0.818
2,4,5-Trichlorophenol 1 12/27/21 19:05 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-10
90732 Matrix:
12/15/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.119 mg/Kg - dry 0.119 0.8182,4,6-Trichlorophenol 1 12/27/21 19:05 V13287JMV
Surrogate: Phenol-d5 83.5 Limits: 34-121%12/27/21 19:051 JMV V13287
Surrogate: 2-Fluorobiphenyl 79.6 Limits: 44-115%12/27/21 19:051 JMV V13287
Surrogate: 2-Fluorophenol 85.3 Limits: 35-115%12/27/21 19:051 JMV V13287
Surrogate: Nitrobenzene-d5 69.5 Limits: 37-122%12/27/21 19:051 JMV V13287
Surrogate: 4-Terphenyl-d14 89.2 Limits: 54-127%12/27/21 19:051 JMV V13287
Surrogate: 2,4,6-Tribromophenol 79.9 Limits: 39-132%12/27/21 19:051 JMV V13287
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-11
90733 Matrix:
12/15/2021 9:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.3 %Moisture 1 12/21/21 17:16 SW-DRYWTCEG
2.39 mg/Kg - dry 0.119 1.27Arsenic 10 12/20/21 23:04 6020BEDV
113 mg/Kg - dry 1.78 12.7Barium 10 12/20/21 23:04 6020BEDV
<0.0698 mg/Kg - dry 0.0698 0.635Cadmium 10 12/20/21 23:04 6020BEDV
45.4 mg/Kg - dry 0.368 1.27Chromium 10 12/20/21 23:04 6020BEDV
13.0 mg/Kg - dry 0.178 1.27
Lead 10 12/20/21 23:04 6020BEDV
0.0161 J mg/Kg - dry 0.0152 0.0381Mercury (Total)1 12/21/21 17:43 7471BEDV
<1.14 mg/Kg - dry 1.14 2.54Selenium 10 12/20/21 23:04 6020BEDV
<0.0520 mg/Kg - dry 0.0520 0.635Silver 10 12/20/21 23:04 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-11
90733 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
0.039 mg/Kg - dry 0.003 0.025Acetone 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 12/17/21 15:15 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 12/17/21 15:15 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/17/21 15:15 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/17/21 15:15 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/17/21 15:15 V12995TBL
0.003 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/17/21 15:15 V12995TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/17/21 15:15 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/17/21 15:15 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 12/17/21 15:15 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/17/21 15:15 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/17/21 15:15 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-11
90733 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 12/17/21 15:15 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 12/17/21 15:15 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/17/21 15:15 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/17/21 15:15 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/17/21 15:15 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/17/21 15:15 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/17/21 15:15 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/17/21 15:15 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 12/17/21 15:15 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/17/21 15:15 V12995TBL
0.133 J mg/Kg - dry 0.017 0.317Ethanol 1 12/17/21 15:15 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 12/17/21 15:15 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-11
90733 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 12/17/21 15:15 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/17/21 15:15 V12995TBL
0.002 J mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 12/17/21 15:15 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/17/21 15:15 V12995TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/17/21 15:15 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/17/21 15:15 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/17/21 15:15 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 12/17/21 15:15 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 12/17/21 15:15 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/17/21 15:15 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/17/21 15:15 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/17/21 15:15 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-11
90733 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/17/21 15:15 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/17/21 15:15 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/17/21 15:15 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/17/21 15:15 V12995
Surrogate: 4-Bromofluorobenzene 98.3 Limits: 70-130%12/17/21 15:151 TBL V12995
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/17/21 15:151 TBL V12995
Surrogate: Toluene-d8 88.3 Limits: 76-129%12/17/21 15:151 TBL V12995
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.147 mg/Kg - dry 0.147 0.838Acenaphthene 1 12/27/21 19:28 V13287JMV
<0.133 mg/Kg - dry 0.133 0.838Acenaphthylene 1 12/27/21 19:28 V13287JMV
<0.193 mg/Kg - dry 0.193 0.838Aniline 1 12/27/21 19:28 V13287JMV
<0.181 mg/Kg - dry 0.181 0.838Anthracene 1 12/27/21 19:28 V13287JMV
<0.176 mg/Kg - dry 0.176 0.838
Benzo(a)anthracene 1 12/27/21 19:28 V13287JMV
<0.186 mg/Kg - dry 0.186 0.838Benzo(a)pyrene 1 12/27/21 19:28 V13287JMV
0.222 J mg/Kg - dry 0.185 0.838Benzo(b)fluoranthene 1 12/27/21 19:28 V13287JMV
<0.172 mg/Kg - dry 0.172 0.838Benzo(g,h,i)perylene 1 12/27/21 19:28 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-11
90733 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.174 mg/Kg - dry 0.174 0.838Benzo(k)fluoranthene 1 12/27/21 19:28 V13287JMV
<0.736 mg/Kg - dry 0.736 2.54Benzoic Acid 1 12/27/21 19:28 V13287JMV
<0.133 mg/Kg - dry 0.133 0.838Benzyl alcohol 1 12/27/21 19:28 V13287JMV
<0.149 mg/Kg - dry 0.149 0.838Bis(2-Chloroethoxy)methane 1 12/27/21 19:28 V13287JMV
<0.135 mg/Kg - dry 0.135 0.838Bis(2-Chloroethyl)ether 1 12/27/21 19:28 V13287JMV
<0.172 mg/Kg - dry 0.172 0.419Bis(2-Chloroisopropyl)ether 1 12/27/21 19:28 V13287JMV
<0.152 mg/Kg - dry 0.152 0.838Bis(2-ethylhexyl)phthalate 1 12/27/21 19:28 V13287JMV
<0.138 mg/Kg - dry 0.138 0.8384-Bromophenyl phenyl ether 1 12/27/21 19:28 V13287JMV
<0.143 mg/Kg - dry 0.143 0.419
Butyl benzyl phthalate 1 12/27/21 19:28 V13287JMV
<0.117 mg/Kg - dry 0.117 0.8384-Chloro-3-methylphenol 1 12/27/21 19:28 V13287JMV
<0.142 mg/Kg - dry 0.142 0.4194-Chloroaniline 1 12/27/21 19:28 V13287JMV
<0.147 mg/Kg - dry 0.147 0.8382-Chloronaphthalene 1 12/27/21 19:28 V13287JMV
<0.124 mg/Kg - dry 0.124 0.8382-Chlorophenol 1 12/27/21 19:28 V13287JMV
<0.160 mg/Kg - dry 0.160 1.274-Chlorophenyl phenyl ether 1 12/27/21 19:28 V13287JMV
<0.180 mg/Kg - dry 0.180 0.838Chrysene 1 12/27/21 19:28 V13287JMV
<0.292 mg/Kg - dry 0.292 0.838
Dibenz(a,h)anthracene 1 12/27/21 19:28 V13287JMV
<0.151 mg/Kg - dry 0.151 0.838Dibenzofuran 1 12/27/21 19:28 V13287JMV
<0.119 mg/Kg - dry 0.119 0.8381,2-Dichlorobenzene 1 12/27/21 19:28 V13287JMV
<0.123 mg/Kg - dry 0.123 0.8381,3-Dichlorobenzene 1 12/27/21 19:28 V13287JMV
<0.123 mg/Kg - dry 0.123 0.4191,4-Dichlorobenzene 1 12/27/21 19:28 V13287JMV
<0.186 mg/Kg - dry 0.186 0.8383,3'-Dichlorobenzidine 1 12/27/21 19:28 V13287JMV
<0.121 mg/Kg - dry 0.121 0.8382,4-Dichlorophenol 1 12/27/21 19:28 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-11
90733 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.228 mg/Kg - dry 0.228 0.838Diethyl phthalate 1 12/27/21 19:28 V13287JMV
<0.221 mg/Kg - dry 0.221 0.838Dimethyl phthalate 1 12/27/21 19:28 V13287JMV
<0.137 mg/Kg - dry 0.137 0.4192,4-Dimethylphenol 1 12/27/21 19:28 V13287JMV
<0.135 mg/Kg - dry 0.135 0.838Di-n-butyl phthalate 1 12/27/21 19:28 V13287JMV
<0.304 mg/Kg - dry 0.304 1.914,6-Dinitro-2-methylphenol 1 12/27/21 19:28 V13287JMV
<0.660 mg/Kg - dry 0.660 1.912,4-Dinitrophenol 1 12/27/21 19:28 V13287JMV
<0.122 mg/Kg - dry 0.122 0.8382,4-Dinitrotoluene 1 12/27/21 19:28 V13287JMV
<0.137 mg/Kg - dry 0.137 0.8382,6-Dinitrotoluene 1 12/27/21 19:28 V13287JMV
<0.181 mg/Kg - dry 0.181 0.419
Di-n-Octyl Phthalate 1 12/27/21 19:28 V13287JMV
0.312 J mg/Kg - dry 0.156 0.838Fluoranthene 1 12/27/21 19:28 V13287JMV
<0.162 mg/Kg - dry 0.162 0.838Fluorene 1 12/27/21 19:28 V13287JMV
<0.134 mg/Kg - dry 0.134 0.838Hexachlorobenzene 1 12/27/21 19:28 V13287JMV
<0.124 mg/Kg - dry 0.124 0.838Hexachlorobutadiene 1 12/27/21 19:28 V13287JMV
<0.199 mg/Kg - dry 0.199 0.838Hexachlorocyclopentadiene 1 12/27/21 19:28 V13287JMV
<0.100 mg/Kg - dry 0.100 0.838Hexachloroethane 1 12/27/21 19:28 V13287JMV
<0.227 mg/Kg - dry 0.227 0.838
Indeno(1,2,3-cd)pyrene 1 12/27/21 19:28 V13287JMV
<0.242 mg/Kg - dry 0.242 0.838Isophorone 1 12/27/21 19:28 V13287JMV
<0.134 mg/Kg - dry 0.134 0.8381-Methylnaphthalene 1 12/27/21 19:28 V13287JMV
<0.127 mg/Kg - dry 0.127 0.8382-Methylnaphthalene 1 12/27/21 19:28 V13287JMV
<0.123 mg/Kg - dry 0.123 0.8382-Methylphenol 1 12/27/21 19:28 V13287JMV
<0.107 mg/Kg - dry 0.107 0.8383&4 Methylphenol 1 12/27/21 19:28 V13287JMV
<0.182 mg/Kg - dry 0.182 0.838Naphthalene 1 12/27/21 19:28 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-11
90733 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.122 mg/Kg - dry 0.122 0.8382-Nitroaniline 1 12/27/21 19:28 V13287JMV
<0.152 mg/Kg - dry 0.152 0.8383-Nitroaniline 1 12/27/21 19:28 V13287JMV
<0.118 mg/Kg - dry 0.118 0.4194-Nitroaniline 1 12/27/21 19:28 V13287JMV
<0.147 mg/Kg - dry 0.147 0.419Nitrobenzene 1 12/27/21 19:28 V13287JMV
<0.112 mg/Kg - dry 0.112 0.8382-Nitrophenol 1 12/27/21 19:28 V13287JMV
<0.148 mg/Kg - dry 0.148 0.8384-Nitrophenol 1 12/27/21 19:28 V13287JMV
<0.334 mg/Kg - dry 0.334 0.838N-Nitrosodimethylamine 1 12/27/21 19:28 V13287JMV
<0.229 mg/Kg - dry 0.229 0.838N-Nitrosodiphenylamine 1 12/27/21 19:28 V13287JMV
<0.149 mg/Kg - dry 0.149 0.838
N-Nitroso-di-n-propylamine 1 12/27/21 19:28 V13287JMV
<0.440 mg/Kg - dry 0.440 1.27Pentachlorophenol 1 12/27/21 19:28 V13287JMV
<0.264 mg/Kg - dry 0.264 0.838Phenanthrene 1 12/27/21 19:28 V13287JMV
<0.142 mg/Kg - dry 0.142 0.838Phenol 1 12/27/21 19:28 V13287JMV
0.269 J mg/Kg - dry 0.170 0.838Pyrene 1 12/27/21 19:28 V13287JMV
<0.100 mg/Kg - dry 0.100 0.419Pyridine 1 12/27/21 19:28 V13287JMV
<0.135 mg/Kg - dry 0.135 0.8381,2,4-Trichlorobenzene 1 12/27/21 19:28 V13287JMV
<0.122 mg/Kg - dry 0.122 0.838
2,4,5-Trichlorophenol 1 12/27/21 19:28 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 32 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:Ex-11
90733 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.122 mg/Kg - dry 0.122 0.8382,4,6-Trichlorophenol 1 12/27/21 19:28 V13287JMV
Surrogate: Phenol-d5 64.9 Limits: 34-121%12/27/21 19:281 JMV V13287
Surrogate: 2-Fluorobiphenyl 72.3 Limits: 44-115%12/27/21 19:281 JMV V13287
Surrogate: 2-Fluorophenol 25.9 *Limits: 35-115%12/27/21 19:281 JMV V13287
Surrogate: Nitrobenzene-d5 61.4 Limits: 37-122%12/27/21 19:281 JMV V13287
Surrogate: 4-Terphenyl-d14 81.9 Limits: 54-127%12/27/21 19:281 JMV V13287
Surrogate: 2,4,6-Tribromophenol 45.0 Limits: 39-132%12/27/21 19:281 JMV V13287
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 33 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:DUP
90734 Matrix:
12/15/2021 9:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.1 %Moisture 1 12/21/21 17:16 SW-DRYWTCEG
1.27 mg/Kg - dry 0.119 1.27Arsenic 10 12/20/21 23:10 6020BEDV
96.5 mg/Kg - dry 1.77 12.7Barium 10 12/20/21 23:10 6020BEDV
<0.0697 mg/Kg - dry 0.0697 0.634Cadmium 10 12/20/21 23:10 6020BEDV
43.7 mg/Kg - dry 0.367 1.27Chromium 10 12/20/21 23:10 6020BEDV
6.50 mg/Kg - dry 0.177 1.27
Lead 10 12/20/21 23:10 6020BEDV
<0.0152 mg/Kg - dry 0.0152 0.0380Mercury (Total)1 12/21/21 17:45 7471BEDV
<1.14 mg/Kg - dry 1.14 2.53Selenium 10 12/20/21 23:10 6020BEDV
<0.0519 mg/Kg - dry 0.0519 0.634Silver 10 12/20/21 23:10 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 34 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:DUP
90734 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
0.032 mg/Kg - dry 0.003 0.030Acetone 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.030Acrolein 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.030Acrylonitrile 1 12/17/21 15:42 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.007Benzene 1 12/17/21 15:42 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.007Bromobenzene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 12/17/21 15:42 V12995TBL
<0.002 mg/Kg - dry 0.002 0.015
Bromomethane 1 12/17/21 15:42 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 12/17/21 15:42 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.007sec-Butyl benzene 1 12/17/21 15:42 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.007tert-Butyl benzene 1 12/17/21 15:42 V12995TBL
0.002 J mg/Kg - dry 0.0010 0.007Carbon Disulfide 1 12/17/21 15:42 V12995TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorobenzene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007
Chlorodibromomethane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.015Chloroethane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 12/17/21 15:42 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.015Chloromethane 1 12/17/21 15:42 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0072-Chlorotoluene 1 12/17/21 15:42 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0074-Chlorotoluene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 12/17/21 15:42 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 35 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:DUP
90734 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0151,2-Dibromo-3-Chloropropane 1 12/17/21 15:42 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,2-Dibromoethane 1 12/17/21 15:42 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.007Dibromomethane 1 12/17/21 15:42 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,2-Dichlorobenzene 1 12/17/21 15:42 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,3-Dichlorobenzene 1 12/17/21 15:42 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,4-Dichlorobenzene 1 12/17/21 15:42 V12995TBL
<0.002 mg/Kg - dry 0.002 0.015Dichlorodifluoromethane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 12/17/21 15:42 V12995TBL
<0.002 mg/Kg - dry 0.002 0.007
1,2-Dichloroethane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 12/17/21 15:42 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,2-Dichloropropane 1 12/17/21 15:42 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007
1,1-Dichloropropene 1 12/17/21 15:42 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 12/17/21 15:42 V12995TBL
0.134 J mg/Kg - dry 0.021 0.382Ethanol 1 12/17/21 15:42 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.007Ethylbenzene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.076Ethyl Tertiary Butyl Ether (ETBE)1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.015Hexachlorobutadiene 1 12/17/21 15:42 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 36 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:DUP
90734 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.001 mg/Kg - dry 0.001 0.015n-Hexane 1 12/17/21 15:42 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.0302-Hexanone 1 12/17/21 15:42 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.007Isopropylbenzene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 12/17/21 15:42 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.030Methyl Ethyl Ketone (MEK)1 12/17/21 15:42 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 12/17/21 15:42 V12995TBL
<0.023 mg/Kg - dry 0.023 0.0304-Methyl-2-Pentanone 1 12/17/21 15:42 V12995TBL
<0.002 mg/Kg - dry 0.002 0.015Methylene Chloride 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.015
Naphthalene 1 12/17/21 15:42 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 12/17/21 15:42 V12995TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 12/17/21 15:42 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007Toluene 1 12/17/21 15:42 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.015
1,2,3-Trichlorobenzene 1 12/17/21 15:42 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.0151,2,4-Trichlorobenzene 1 12/17/21 15:42 V12995TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 12/17/21 15:42 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 12/17/21 15:42 V12995TBL
<0.003 mg/Kg - dry 0.003 0.015Trichlorofluoromethane 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 12/17/21 15:42 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 37 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:DUP
90734 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 12/17/21 15:42 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 12/17/21 15:42 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.015Vinyl Acetate 1 12/17/21 15:42 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.015Vinyl Chloride 1 12/17/21 15:42 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.007o-Xylene 1 12/17/21 15:42 V12995TBL
<0.001 mg/Kg - dry 0.001 0.015m,p-Xylene 1 12/17/21 15:42 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.007Xylene (Total)1 12/17/21 15:42 V12995
Surrogate: 4-Bromofluorobenzene 97.5 Limits: 70-130%12/17/21 15:421 TBL V12995
Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/17/21 15:421 TBL V12995
Surrogate: Toluene-d8 89.3 Limits: 76-129%12/17/21 15:421 TBL V12995
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.147 mg/Kg - dry 0.147 0.836Acenaphthene 1 12/27/21 19:51 V13287JMV
<0.133 mg/Kg - dry 0.133 0.836Acenaphthylene 1 12/27/21 19:51 V13287JMV
<0.192 mg/Kg - dry 0.192 0.836Aniline 1 12/27/21 19:51 V13287JMV
<0.181 mg/Kg - dry 0.181 0.836Anthracene 1 12/27/21 19:51 V13287JMV
<0.176 mg/Kg - dry 0.176 0.836
Benzo(a)anthracene 1 12/27/21 19:51 V13287JMV
<0.186 mg/Kg - dry 0.186 0.836Benzo(a)pyrene 1 12/27/21 19:51 V13287JMV
<0.185 mg/Kg - dry 0.185 0.836Benzo(b)fluoranthene 1 12/27/21 19:51 V13287JMV
<0.172 mg/Kg - dry 0.172 0.836Benzo(g,h,i)perylene 1 12/27/21 19:51 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 38 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:DUP
90734 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.173 mg/Kg - dry 0.173 0.836Benzo(k)fluoranthene 1 12/27/21 19:51 V13287JMV
<0.735 mg/Kg - dry 0.735 2.53Benzoic Acid 1 12/27/21 19:51 V13287JMV
<0.133 mg/Kg - dry 0.133 0.836Benzyl alcohol 1 12/27/21 19:51 V13287JMV
<0.149 mg/Kg - dry 0.149 0.836Bis(2-Chloroethoxy)methane 1 12/27/21 19:51 V13287JMV
<0.135 mg/Kg - dry 0.135 0.836Bis(2-Chloroethyl)ether 1 12/27/21 19:51 V13287JMV
<0.172 mg/Kg - dry 0.172 0.418Bis(2-Chloroisopropyl)ether 1 12/27/21 19:51 V13287JMV
<0.152 mg/Kg - dry 0.152 0.836Bis(2-ethylhexyl)phthalate 1 12/27/21 19:51 V13287JMV
<0.138 mg/Kg - dry 0.138 0.8364-Bromophenyl phenyl ether 1 12/27/21 19:51 V13287JMV
<0.143 mg/Kg - dry 0.143 0.418
Butyl benzyl phthalate 1 12/27/21 19:51 V13287JMV
<0.117 mg/Kg - dry 0.117 0.8364-Chloro-3-methylphenol 1 12/27/21 19:51 V13287JMV
<0.141 mg/Kg - dry 0.141 0.4184-Chloroaniline 1 12/27/21 19:51 V13287JMV
<0.147 mg/Kg - dry 0.147 0.8362-Chloronaphthalene 1 12/27/21 19:51 V13287JMV
<0.124 mg/Kg - dry 0.124 0.8362-Chlorophenol 1 12/27/21 19:51 V13287JMV
<0.159 mg/Kg - dry 0.159 1.274-Chlorophenyl phenyl ether 1 12/27/21 19:51 V13287JMV
<0.179 mg/Kg - dry 0.179 0.836Chrysene 1 12/27/21 19:51 V13287JMV
<0.291 mg/Kg - dry 0.291 0.836
Dibenz(a,h)anthracene 1 12/27/21 19:51 V13287JMV
<0.150 mg/Kg - dry 0.150 0.836Dibenzofuran 1 12/27/21 19:51 V13287JMV
<0.119 mg/Kg - dry 0.119 0.8361,2-Dichlorobenzene 1 12/27/21 19:51 V13287JMV
<0.123 mg/Kg - dry 0.123 0.8361,3-Dichlorobenzene 1 12/27/21 19:51 V13287JMV
<0.123 mg/Kg - dry 0.123 0.4181,4-Dichlorobenzene 1 12/27/21 19:51 V13287JMV
<0.186 mg/Kg - dry 0.186 0.8363,3'-Dichlorobenzidine 1 12/27/21 19:51 V13287JMV
<0.121 mg/Kg - dry 0.121 0.8362,4-Dichlorophenol 1 12/27/21 19:51 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 39 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:DUP
90734 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.228 mg/Kg - dry 0.228 0.836Diethyl phthalate 1 12/27/21 19:51 V13287JMV
<0.220 mg/Kg - dry 0.220 0.836Dimethyl phthalate 1 12/27/21 19:51 V13287JMV
<0.136 mg/Kg - dry 0.136 0.4182,4-Dimethylphenol 1 12/27/21 19:51 V13287JMV
<0.135 mg/Kg - dry 0.135 0.836Di-n-butyl phthalate 1 12/27/21 19:51 V13287JMV
<0.304 mg/Kg - dry 0.304 1.904,6-Dinitro-2-methylphenol 1 12/27/21 19:51 V13287JMV
<0.659 mg/Kg - dry 0.659 1.902,4-Dinitrophenol 1 12/27/21 19:51 V13287JMV
<0.122 mg/Kg - dry 0.122 0.8362,4-Dinitrotoluene 1 12/27/21 19:51 V13287JMV
<0.136 mg/Kg - dry 0.136 0.8362,6-Dinitrotoluene 1 12/27/21 19:51 V13287JMV
<0.181 mg/Kg - dry 0.181 0.418
Di-n-Octyl Phthalate 1 12/27/21 19:51 V13287JMV
<0.155 mg/Kg - dry 0.155 0.836Fluoranthene 1 12/27/21 19:51 V13287JMV
<0.162 mg/Kg - dry 0.162 0.836Fluorene 1 12/27/21 19:51 V13287JMV
<0.134 mg/Kg - dry 0.134 0.836Hexachlorobenzene 1 12/27/21 19:51 V13287JMV
<0.123 mg/Kg - dry 0.123 0.836Hexachlorobutadiene 1 12/27/21 19:51 V13287JMV
<0.198 mg/Kg - dry 0.198 0.836Hexachlorocyclopentadiene 1 12/27/21 19:51 V13287JMV
<0.100 mg/Kg - dry 0.100 0.836Hexachloroethane 1 12/27/21 19:51 V13287JMV
<0.226 mg/Kg - dry 0.226 0.836
Indeno(1,2,3-cd)pyrene 1 12/27/21 19:51 V13287JMV
<0.242 mg/Kg - dry 0.242 0.836Isophorone 1 12/27/21 19:51 V13287JMV
<0.134 mg/Kg - dry 0.134 0.8361-Methylnaphthalene 1 12/27/21 19:51 V13287JMV
<0.126 mg/Kg - dry 0.126 0.8362-Methylnaphthalene 1 12/27/21 19:51 V13287JMV
<0.122 mg/Kg - dry 0.122 0.8362-Methylphenol 1 12/27/21 19:51 V13287JMV
<0.107 mg/Kg - dry 0.107 0.8363&4 Methylphenol 1 12/27/21 19:51 V13287JMV
<0.182 mg/Kg - dry 0.182 0.836Naphthalene 1 12/27/21 19:51 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 40 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:DUP
90734 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.122 mg/Kg - dry 0.122 0.8362-Nitroaniline 1 12/27/21 19:51 V13287JMV
<0.152 mg/Kg - dry 0.152 0.8363-Nitroaniline 1 12/27/21 19:51 V13287JMV
<0.118 mg/Kg - dry 0.118 0.4184-Nitroaniline 1 12/27/21 19:51 V13287JMV
<0.147 mg/Kg - dry 0.147 0.418Nitrobenzene 1 12/27/21 19:51 V13287JMV
<0.112 mg/Kg - dry 0.112 0.8362-Nitrophenol 1 12/27/21 19:51 V13287JMV
<0.148 mg/Kg - dry 0.148 0.8364-Nitrophenol 1 12/27/21 19:51 V13287JMV
<0.333 mg/Kg - dry 0.333 0.836N-Nitrosodimethylamine 1 12/27/21 19:51 V13287JMV
<0.229 mg/Kg - dry 0.229 0.836N-Nitrosodiphenylamine 1 12/27/21 19:51 V13287JMV
<0.149 mg/Kg - dry 0.149 0.836
N-Nitroso-di-n-propylamine 1 12/27/21 19:51 V13287JMV
<0.439 mg/Kg - dry 0.439 1.27Pentachlorophenol 1 12/27/21 19:51 V13287JMV
<0.263 mg/Kg - dry 0.263 0.836Phenanthrene 1 12/27/21 19:51 V13287JMV
<0.141 mg/Kg - dry 0.141 0.836Phenol 1 12/27/21 19:51 V13287JMV
<0.169 mg/Kg - dry 0.169 0.836Pyrene 1 12/27/21 19:51 V13287JMV
<0.100 mg/Kg - dry 0.100 0.418Pyridine 1 12/27/21 19:51 V13287JMV
<0.135 mg/Kg - dry 0.135 0.8361,2,4-Trichlorobenzene 1 12/27/21 19:51 V13287JMV
<0.121 mg/Kg - dry 0.121 0.836
2,4,5-Trichlorophenol 1 12/27/21 19:51 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 41 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:DUP
90734 Matrix:
12/15/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.122 mg/Kg - dry 0.122 0.8362,4,6-Trichlorophenol 1 12/27/21 19:51 V13287JMV
Surrogate: Phenol-d5 74.5 Limits: 34-121%12/27/21 19:511 JMV V13287
Surrogate: 2-Fluorobiphenyl 76.5 Limits: 44-115%12/27/21 19:511 JMV V13287
Surrogate: 2-Fluorophenol 43.2 Limits: 35-115%12/27/21 19:511 JMV V13287
Surrogate: Nitrobenzene-d5 66.9 Limits: 37-122%12/27/21 19:511 JMV V13287
Surrogate: 4-Terphenyl-d14 87.3 Limits: 54-127%12/27/21 19:511 JMV V13287
Surrogate: 2,4,6-Tribromophenol 45.3 Limits: 39-132%12/27/21 19:511 JMV V13287
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 42 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-1
90735 Matrix:
12/15/2021 11:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.8 %Moisture 1 12/21/21 17:16 SW-DRYWTCEG
1.65 mg/Kg - dry 0.119 1.26Arsenic 10 12/20/21 23:17 6020BEDV
138 mg/Kg - dry 1.77 12.6Barium 10 12/20/21 23:17 6020BEDV
<0.0694 mg/Kg - dry 0.0694 0.631Cadmium 10 12/20/21 23:17 6020BEDV
41.4 mg/Kg - dry 0.366 1.26Chromium 10 12/20/21 23:17 6020BEDV
22.2 mg/Kg - dry 0.177 1.26
Lead 10 12/20/21 23:17 6020BEDV
0.0188 J mg/Kg - dry 0.0152 0.0379Mercury (Total)1 12/21/21 17:50 7471BEDV
<1.14 mg/Kg - dry 1.14 2.53Selenium 10 12/20/21 23:17 6020BEDV
<0.0517 mg/Kg - dry 0.0517 0.631Silver 10 12/20/21 23:17 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 43 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-1
90735 Matrix:
12/15/2021 11:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
0.007 J mg/Kg - dry 0.003 0.025Acetone 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 12/17/21 16:10 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 12/17/21 16:10 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/17/21 16:10 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/17/21 16:10 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/17/21 16:10 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 12/17/21 16:10 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/17/21 16:10 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 12/17/21 16:10 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/17/21 16:10 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/17/21 16:10 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 44 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-1
90735 Matrix:
12/15/2021 11:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 12/17/21 16:10 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 12/17/21 16:10 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/17/21 16:10 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/17/21 16:10 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/17/21 16:10 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/17/21 16:10 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/17/21 16:10 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/17/21 16:10 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/17/21 16:10 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 12/17/21 16:10 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/17/21 16:10 V12995TBL
0.034 J mg/Kg - dry 0.017 0.315Ethanol 1 12/17/21 16:10 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 12/17/21 16:10 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 12/17/21 16:10 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 45 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-1
90735 Matrix:
12/15/2021 11:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 12/17/21 16:10 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/17/21 16:10 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 12/17/21 16:10 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/17/21 16:10 V12995TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/17/21 16:10 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/17/21 16:10 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/17/21 16:10 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 12/17/21 16:10 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 12/17/21 16:10 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/17/21 16:10 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/17/21 16:10 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/17/21 16:10 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 46 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-1
90735 Matrix:
12/15/2021 11:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
0.0009 J mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/17/21 16:10 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/17/21 16:10 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/17/21 16:10 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/17/21 16:10 V12995
Surrogate: 4-Bromofluorobenzene 98.7 Limits: 70-130%12/17/21 16:101 TBL V12995
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/17/21 16:101 TBL V12995
Surrogate: Toluene-d8 86.9 Limits: 76-129%12/17/21 16:101 TBL V12995
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.146 mg/Kg - dry 0.146 0.833Acenaphthene 1 12/27/21 20:14 V13287JMV
<0.132 mg/Kg - dry 0.132 0.833Acenaphthylene 1 12/27/21 20:14 V13287JMV
<0.191 mg/Kg - dry 0.191 0.833Aniline 1 12/27/21 20:14 V13287JMV
<0.180 mg/Kg - dry 0.180 0.833Anthracene 1 12/27/21 20:14 V13287JMV
<0.175 mg/Kg - dry 0.175 0.833
Benzo(a)anthracene 1 12/27/21 20:14 V13287JMV
<0.185 mg/Kg - dry 0.185 0.833Benzo(a)pyrene 1 12/27/21 20:14 V13287JMV
<0.184 mg/Kg - dry 0.184 0.833Benzo(b)fluoranthene 1 12/27/21 20:14 V13287JMV
<0.171 mg/Kg - dry 0.171 0.833Benzo(g,h,i)perylene 1 12/27/21 20:14 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 47 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-1
90735 Matrix:
12/15/2021 11:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.172 mg/Kg - dry 0.172 0.833Benzo(k)fluoranthene 1 12/27/21 20:14 V13287JMV
<0.732 mg/Kg - dry 0.732 2.53Benzoic Acid 1 12/27/21 20:14 V13287JMV
<0.132 mg/Kg - dry 0.132 0.833Benzyl alcohol 1 12/27/21 20:14 V13287JMV
<0.148 mg/Kg - dry 0.148 0.833Bis(2-Chloroethoxy)methane 1 12/27/21 20:14 V13287JMV
<0.135 mg/Kg - dry 0.135 0.833Bis(2-Chloroethyl)ether 1 12/27/21 20:14 V13287JMV
<0.171 mg/Kg - dry 0.171 0.416Bis(2-Chloroisopropyl)ether 1 12/27/21 20:14 V13287JMV
<0.151 mg/Kg - dry 0.151 0.833Bis(2-ethylhexyl)phthalate 1 12/27/21 20:14 V13287JMV
<0.137 mg/Kg - dry 0.137 0.8334-Bromophenyl phenyl ether 1 12/27/21 20:14 V13287JMV
<0.142 mg/Kg - dry 0.142 0.416
Butyl benzyl phthalate 1 12/27/21 20:14 V13287JMV
<0.116 mg/Kg - dry 0.116 0.8334-Chloro-3-methylphenol 1 12/27/21 20:14 V13287JMV
<0.141 mg/Kg - dry 0.141 0.4164-Chloroaniline 1 12/27/21 20:14 V13287JMV
<0.146 mg/Kg - dry 0.146 0.8332-Chloronaphthalene 1 12/27/21 20:14 V13287JMV
<0.123 mg/Kg - dry 0.123 0.8332-Chlorophenol 1 12/27/21 20:14 V13287JMV
<0.159 mg/Kg - dry 0.159 1.264-Chlorophenyl phenyl ether 1 12/27/21 20:14 V13287JMV
<0.179 mg/Kg - dry 0.179 0.833Chrysene 1 12/27/21 20:14 V13287JMV
<0.290 mg/Kg - dry 0.290 0.833
Dibenz(a,h)anthracene 1 12/27/21 20:14 V13287JMV
<0.150 mg/Kg - dry 0.150 0.833Dibenzofuran 1 12/27/21 20:14 V13287JMV
<0.119 mg/Kg - dry 0.119 0.8331,2-Dichlorobenzene 1 12/27/21 20:14 V13287JMV
<0.122 mg/Kg - dry 0.122 0.8331,3-Dichlorobenzene 1 12/27/21 20:14 V13287JMV
<0.123 mg/Kg - dry 0.123 0.4161,4-Dichlorobenzene 1 12/27/21 20:14 V13287JMV
<0.185 mg/Kg - dry 0.185 0.8333,3'-Dichlorobenzidine 1 12/27/21 20:14 V13287JMV
<0.120 mg/Kg - dry 0.120 0.8332,4-Dichlorophenol 1 12/27/21 20:14 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 48 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-1
90735 Matrix:
12/15/2021 11:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.227 mg/Kg - dry 0.227 0.833Diethyl phthalate 1 12/27/21 20:14 V13287JMV
<0.219 mg/Kg - dry 0.219 0.833Dimethyl phthalate 1 12/27/21 20:14 V13287JMV
<0.136 mg/Kg - dry 0.136 0.4162,4-Dimethylphenol 1 12/27/21 20:14 V13287JMV
<0.135 mg/Kg - dry 0.135 0.833Di-n-butyl phthalate 1 12/27/21 20:14 V13287JMV
<0.303 mg/Kg - dry 0.303 1.894,6-Dinitro-2-methylphenol 1 12/27/21 20:14 V13287JMV
<0.656 mg/Kg - dry 0.656 1.892,4-Dinitrophenol 1 12/27/21 20:14 V13287JMV
<0.121 mg/Kg - dry 0.121 0.8332,4-Dinitrotoluene 1 12/27/21 20:14 V13287JMV
<0.136 mg/Kg - dry 0.136 0.8332,6-Dinitrotoluene 1 12/27/21 20:14 V13287JMV
<0.180 mg/Kg - dry 0.180 0.416
Di-n-Octyl Phthalate 1 12/27/21 20:14 V13287JMV
<0.155 mg/Kg - dry 0.155 0.833Fluoranthene 1 12/27/21 20:14 V13287JMV
<0.161 mg/Kg - dry 0.161 0.833Fluorene 1 12/27/21 20:14 V13287JMV
<0.133 mg/Kg - dry 0.133 0.833Hexachlorobenzene 1 12/27/21 20:14 V13287JMV
<0.123 mg/Kg - dry 0.123 0.833Hexachlorobutadiene 1 12/27/21 20:14 V13287JMV
<0.198 mg/Kg - dry 0.198 0.833Hexachlorocyclopentadiene 1 12/27/21 20:14 V13287JMV
<0.100 mg/Kg - dry 0.100 0.833Hexachloroethane 1 12/27/21 20:14 V13287JMV
<0.226 mg/Kg - dry 0.226 0.833
Indeno(1,2,3-cd)pyrene 1 12/27/21 20:14 V13287JMV
<0.241 mg/Kg - dry 0.241 0.833Isophorone 1 12/27/21 20:14 V13287JMV
<0.133 mg/Kg - dry 0.133 0.8331-Methylnaphthalene 1 12/27/21 20:14 V13287JMV
<0.126 mg/Kg - dry 0.126 0.8332-Methylnaphthalene 1 12/27/21 20:14 V13287JMV
<0.122 mg/Kg - dry 0.122 0.8332-Methylphenol 1 12/27/21 20:14 V13287JMV
<0.107 mg/Kg - dry 0.107 0.8333&4 Methylphenol 1 12/27/21 20:14 V13287JMV
<0.181 mg/Kg - dry 0.181 0.833Naphthalene 1 12/27/21 20:14 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 49 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-1
90735 Matrix:
12/15/2021 11:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.122 mg/Kg - dry 0.122 0.8332-Nitroaniline 1 12/27/21 20:14 V13287JMV
<0.151 mg/Kg - dry 0.151 0.8333-Nitroaniline 1 12/27/21 20:14 V13287JMV
<0.117 mg/Kg - dry 0.117 0.4164-Nitroaniline 1 12/27/21 20:14 V13287JMV
<0.146 mg/Kg - dry 0.146 0.416Nitrobenzene 1 12/27/21 20:14 V13287JMV
<0.112 mg/Kg - dry 0.112 0.8332-Nitrophenol 1 12/27/21 20:14 V13287JMV
<0.147 mg/Kg - dry 0.147 0.8334-Nitrophenol 1 12/27/21 20:14 V13287JMV
<0.332 mg/Kg - dry 0.332 0.833N-Nitrosodimethylamine 1 12/27/21 20:14 V13287JMV
<0.228 mg/Kg - dry 0.228 0.833N-Nitrosodiphenylamine 1 12/27/21 20:14 V13287JMV
<0.148 mg/Kg - dry 0.148 0.833
N-Nitroso-di-n-propylamine 1 12/27/21 20:14 V13287JMV
<0.438 mg/Kg - dry 0.438 1.26Pentachlorophenol 1 12/27/21 20:14 V13287JMV
<0.262 mg/Kg - dry 0.262 0.833Phenanthrene 1 12/27/21 20:14 V13287JMV
<0.141 mg/Kg - dry 0.141 0.833Phenol 1 12/27/21 20:14 V13287JMV
<0.169 mg/Kg - dry 0.169 0.833Pyrene 1 12/27/21 20:14 V13287JMV
<0.100 mg/Kg - dry 0.100 0.416Pyridine 1 12/27/21 20:14 V13287JMV
<0.135 mg/Kg - dry 0.135 0.8331,2,4-Trichlorobenzene 1 12/27/21 20:14 V13287JMV
<0.121 mg/Kg - dry 0.121 0.833
2,4,5-Trichlorophenol 1 12/27/21 20:14 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 50 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-1
90735 Matrix:
12/15/2021 11:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.121 mg/Kg - dry 0.121 0.8332,4,6-Trichlorophenol 1 12/27/21 20:14 V13287JMV
Surrogate: Phenol-d5 83.5 Limits: 34-121%12/27/21 20:141 JMV V13287
Surrogate: 2-Fluorobiphenyl 77.1 Limits: 44-115%12/27/21 20:141 JMV V13287
Surrogate: 2-Fluorophenol 85.9 Limits: 35-115%12/27/21 20:141 JMV V13287
Surrogate: Nitrobenzene-d5 69.3 Limits: 37-122%12/27/21 20:141 JMV V13287
Surrogate: 4-Terphenyl-d14 91.0 Limits: 54-127%12/27/21 20:141 JMV V13287
Surrogate: 2,4,6-Tribromophenol 81.1 Limits: 39-132%12/27/21 20:141 JMV V13287
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 51 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-2
90736 Matrix:
12/15/2021 11:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.5 %Moisture 1 12/21/21 17:16 SW-DRYWTCEG
1.42 mg/Kg - dry 0.121 1.29Arsenic 10 12/20/21 23:36 6020BEDV
109 mg/Kg - dry 1.81 12.9Barium 10 12/20/21 23:36 6020BEDV
<0.0709 mg/Kg - dry 0.0709 0.645Cadmium 10 12/20/21 23:36 6020BEDV
45.4 mg/Kg - dry 0.374 1.29Chromium 10 12/20/21 23:36 6020BEDV
11.5 mg/Kg - dry 0.181 1.29
Lead 10 12/20/21 23:36 6020BEDV
0.0526 mg/Kg - dry 0.0155 0.0387Mercury (Total)1 12/21/21 17:55 7471BEDV
<1.16 mg/Kg - dry 1.16 2.58Selenium 10 12/20/21 23:36 6020BEDV
<0.0529 mg/Kg - dry 0.0529 0.645Silver 10 12/20/21 23:36 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 52 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-2
90736 Matrix:
12/15/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
0.012 J mg/Kg - dry 0.003 0.025Acetone 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 12/17/21 16:38 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 12/17/21 16:38 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/17/21 16:38 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/17/21 16:38 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/17/21 16:38 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/17/21 16:38 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/17/21 16:38 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/17/21 16:38 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/17/21 16:38 V12995TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/17/21 16:38 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/17/21 16:38 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/17/21 16:38 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/17/21 16:38 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/17/21 16:38 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/17/21 16:38 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 53 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-2
90736 Matrix:
12/15/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 12/17/21 16:38 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 12/17/21 16:38 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/17/21 16:38 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/17/21 16:38 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/17/21 16:38 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/17/21 16:38 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/17/21 16:38 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/17/21 16:38 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/17/21 16:38 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 12/17/21 16:38 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/17/21 16:38 V12995TBL
<0.018 mg/Kg - dry 0.018 0.322Ethanol 1 12/17/21 16:38 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 12/17/21 16:38 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 54 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-2
90736 Matrix:
12/15/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 12/17/21 16:38 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 12/17/21 16:38 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/17/21 16:38 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 12/17/21 16:38 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/17/21 16:38 V12995TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/17/21 16:38 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/17/21 16:38 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/17/21 16:38 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/17/21 16:38 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 12/17/21 16:38 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/17/21 16:38 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/17/21 16:38 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/17/21 16:38 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/17/21 16:38 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 55 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-2
90736 Matrix:
12/15/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/17/21 16:38 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/17/21 16:38 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/17/21 16:38 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/17/21 16:38 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/17/21 16:38 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/17/21 16:38 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/17/21 16:38 V12995
Surrogate: 4-Bromofluorobenzene 97.6 Limits: 70-130%12/17/21 16:381 TBL V12995
Surrogate: Dibromofluoromethane 105 Limits: 84-123%12/17/21 16:381 TBL V12995
Surrogate: Toluene-d8 88.0 Limits: 76-129%12/17/21 16:381 TBL V12995
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.149 mg/Kg - dry 0.149 0.851Acenaphthene 1 12/27/21 20:37 V13287JMV
<0.135 mg/Kg - dry 0.135 0.851Acenaphthylene 1 12/27/21 20:37 V13287JMV
<0.196 mg/Kg - dry 0.196 0.851Aniline 1 12/27/21 20:37 V13287JMV
<0.184 mg/Kg - dry 0.184 0.851Anthracene 1 12/27/21 20:37 V13287JMV
<0.179 mg/Kg - dry 0.179 0.851
Benzo(a)anthracene 1 12/27/21 20:37 V13287JMV
<0.189 mg/Kg - dry 0.189 0.851Benzo(a)pyrene 1 12/27/21 20:37 V13287JMV
<0.188 mg/Kg - dry 0.188 0.851Benzo(b)fluoranthene 1 12/27/21 20:37 V13287JMV
<0.175 mg/Kg - dry 0.175 0.851Benzo(g,h,i)perylene 1 12/27/21 20:37 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 56 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-2
90736 Matrix:
12/15/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.176 mg/Kg - dry 0.176 0.851Benzo(k)fluoranthene 1 12/27/21 20:37 V13287JMV
<0.748 mg/Kg - dry 0.748 2.58Benzoic Acid 1 12/27/21 20:37 V13287JMV
<0.135 mg/Kg - dry 0.135 0.851Benzyl alcohol 1 12/27/21 20:37 V13287JMV
<0.152 mg/Kg - dry 0.152 0.851Bis(2-Chloroethoxy)methane 1 12/27/21 20:37 V13287JMV
<0.138 mg/Kg - dry 0.138 0.851Bis(2-Chloroethyl)ether 1 12/27/21 20:37 V13287JMV
<0.175 mg/Kg - dry 0.175 0.425Bis(2-Chloroisopropyl)ether 1 12/27/21 20:37 V13287JMV
<0.154 mg/Kg - dry 0.154 0.851Bis(2-ethylhexyl)phthalate 1 12/27/21 20:37 V13287JMV
<0.140 mg/Kg - dry 0.140 0.8514-Bromophenyl phenyl ether 1 12/27/21 20:37 V13287JMV
<0.145 mg/Kg - dry 0.145 0.425
Butyl benzyl phthalate 1 12/27/21 20:37 V13287JMV
<0.119 mg/Kg - dry 0.119 0.8514-Chloro-3-methylphenol 1 12/27/21 20:37 V13287JMV
<0.144 mg/Kg - dry 0.144 0.4254-Chloroaniline 1 12/27/21 20:37 V13287JMV
<0.149 mg/Kg - dry 0.149 0.8512-Chloronaphthalene 1 12/27/21 20:37 V13287JMV
<0.126 mg/Kg - dry 0.126 0.8512-Chlorophenol 1 12/27/21 20:37 V13287JMV
<0.162 mg/Kg - dry 0.162 1.294-Chlorophenyl phenyl ether 1 12/27/21 20:37 V13287JMV
<0.183 mg/Kg - dry 0.183 0.851Chrysene 1 12/27/21 20:37 V13287JMV
<0.296 mg/Kg - dry 0.296 0.851
Dibenz(a,h)anthracene 1 12/27/21 20:37 V13287JMV
<0.153 mg/Kg - dry 0.153 0.851Dibenzofuran 1 12/27/21 20:37 V13287JMV
<0.121 mg/Kg - dry 0.121 0.8511,2-Dichlorobenzene 1 12/27/21 20:37 V13287JMV
<0.125 mg/Kg - dry 0.125 0.8511,3-Dichlorobenzene 1 12/27/21 20:37 V13287JMV
<0.125 mg/Kg - dry 0.125 0.4251,4-Dichlorobenzene 1 12/27/21 20:37 V13287JMV
<0.189 mg/Kg - dry 0.189 0.8513,3'-Dichlorobenzidine 1 12/27/21 20:37 V13287JMV
<0.123 mg/Kg - dry 0.123 0.8512,4-Dichlorophenol 1 12/27/21 20:37 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 57 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-2
90736 Matrix:
12/15/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.232 mg/Kg - dry 0.232 0.851Diethyl phthalate 1 12/27/21 20:37 V13287JMV
<0.224 mg/Kg - dry 0.224 0.851Dimethyl phthalate 1 12/27/21 20:37 V13287JMV
<0.139 mg/Kg - dry 0.139 0.4252,4-Dimethylphenol 1 12/27/21 20:37 V13287JMV
<0.138 mg/Kg - dry 0.138 0.851Di-n-butyl phthalate 1 12/27/21 20:37 V13287JMV
<0.309 mg/Kg - dry 0.309 1.944,6-Dinitro-2-methylphenol 1 12/27/21 20:37 V13287JMV
<0.670 mg/Kg - dry 0.670 1.942,4-Dinitrophenol 1 12/27/21 20:37 V13287JMV
<0.124 mg/Kg - dry 0.124 0.8512,4-Dinitrotoluene 1 12/27/21 20:37 V13287JMV
<0.139 mg/Kg - dry 0.139 0.8512,6-Dinitrotoluene 1 12/27/21 20:37 V13287JMV
<0.184 mg/Kg - dry 0.184 0.425
Di-n-Octyl Phthalate 1 12/27/21 20:37 V13287JMV
<0.158 mg/Kg - dry 0.158 0.851Fluoranthene 1 12/27/21 20:37 V13287JMV
<0.165 mg/Kg - dry 0.165 0.851Fluorene 1 12/27/21 20:37 V13287JMV
<0.136 mg/Kg - dry 0.136 0.851Hexachlorobenzene 1 12/27/21 20:37 V13287JMV
<0.125 mg/Kg - dry 0.125 0.851Hexachlorobutadiene 1 12/27/21 20:37 V13287JMV
<0.202 mg/Kg - dry 0.202 0.851Hexachlorocyclopentadiene 1 12/27/21 20:37 V13287JMV
<0.102 mg/Kg - dry 0.102 0.851Hexachloroethane 1 12/27/21 20:37 V13287JMV
<0.230 mg/Kg - dry 0.230 0.851
Indeno(1,2,3-cd)pyrene 1 12/27/21 20:37 V13287JMV
<0.246 mg/Kg - dry 0.246 0.851Isophorone 1 12/27/21 20:37 V13287JMV
<0.136 mg/Kg - dry 0.136 0.8511-Methylnaphthalene 1 12/27/21 20:37 V13287JMV
<0.129 mg/Kg - dry 0.129 0.8512-Methylnaphthalene 1 12/27/21 20:37 V13287JMV
<0.125 mg/Kg - dry 0.125 0.8512-Methylphenol 1 12/27/21 20:37 V13287JMV
<0.109 mg/Kg - dry 0.109 0.8513&4 Methylphenol 1 12/27/21 20:37 V13287JMV
<0.185 mg/Kg - dry 0.185 0.851Naphthalene 1 12/27/21 20:37 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 58 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-2
90736 Matrix:
12/15/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.124 mg/Kg - dry 0.124 0.8512-Nitroaniline 1 12/27/21 20:37 V13287JMV
<0.154 mg/Kg - dry 0.154 0.8513-Nitroaniline 1 12/27/21 20:37 V13287JMV
<0.120 mg/Kg - dry 0.120 0.4254-Nitroaniline 1 12/27/21 20:37 V13287JMV
<0.149 mg/Kg - dry 0.149 0.425Nitrobenzene 1 12/27/21 20:37 V13287JMV
<0.114 mg/Kg - dry 0.114 0.8512-Nitrophenol 1 12/27/21 20:37 V13287JMV
<0.150 mg/Kg - dry 0.150 0.8514-Nitrophenol 1 12/27/21 20:37 V13287JMV
<0.339 mg/Kg - dry 0.339 0.851N-Nitrosodimethylamine 1 12/27/21 20:37 V13287JMV
<0.233 mg/Kg - dry 0.233 0.851N-Nitrosodiphenylamine 1 12/27/21 20:37 V13287JMV
<0.152 mg/Kg - dry 0.152 0.851
N-Nitroso-di-n-propylamine 1 12/27/21 20:37 V13287JMV
<0.447 mg/Kg - dry 0.447 1.29Pentachlorophenol 1 12/27/21 20:37 V13287JMV
<0.268 mg/Kg - dry 0.268 0.851Phenanthrene 1 12/27/21 20:37 V13287JMV
<0.144 mg/Kg - dry 0.144 0.851Phenol 1 12/27/21 20:37 V13287JMV
<0.172 mg/Kg - dry 0.172 0.851Pyrene 1 12/27/21 20:37 V13287JMV
<0.102 mg/Kg - dry 0.102 0.425Pyridine 1 12/27/21 20:37 V13287JMV
<0.138 mg/Kg - dry 0.138 0.8511,2,4-Trichlorobenzene 1 12/27/21 20:37 V13287JMV
<0.124 mg/Kg - dry 0.124 0.851
2,4,5-Trichlorophenol 1 12/27/21 20:37 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 59 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-2
90736 Matrix:
12/15/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.124 mg/Kg - dry 0.124 0.8512,4,6-Trichlorophenol 1 12/27/21 20:37 V13287JMV
Surrogate: Phenol-d5 75.4 Limits: 34-121%12/27/21 20:371 JMV V13287
Surrogate: 2-Fluorobiphenyl 73.1 Limits: 44-115%12/27/21 20:371 JMV V13287
Surrogate: 2-Fluorophenol 76.3 Limits: 35-115%12/27/21 20:371 JMV V13287
Surrogate: Nitrobenzene-d5 64.1 Limits: 37-122%12/27/21 20:371 JMV V13287
Surrogate: 4-Terphenyl-d14 84.4 Limits: 54-127%12/27/21 20:371 JMV V13287
Surrogate: 2,4,6-Tribromophenol 77.5 Limits: 39-132%12/27/21 20:371 JMV V13287
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 60 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-3
90737 Matrix:
12/15/2021 12:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.5 %Moisture 1 12/21/21 17:16 SW-DRYWTCEG
1.28 mg/Kg - dry 0.115 1.23Arsenic 10 12/20/21 23:43 6020BEDV
106 mg/Kg - dry 1.72 12.3Barium 10 12/20/21 23:43 6020BEDV
<0.0674 mg/Kg - dry 0.0674 0.613Cadmium 10 12/20/21 23:43 6020BEDV
55.3 mg/Kg - dry 0.355 1.23Chromium 10 12/20/21 23:43 6020BEDV
13.3 mg/Kg - dry 0.172 1.23
Lead 10 12/20/21 23:43 6020BEDV
<0.0147 mg/Kg - dry 0.0147 0.0368Mercury (Total)1 12/21/21 18:00 7471BEDV
<1.10 mg/Kg - dry 1.10 2.45Selenium 10 12/20/21 23:43 6020BEDV
0.0509 J mg/Kg - dry 0.0503 0.613Silver 10 12/20/21 23:43 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 61 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-3
90737 Matrix:
12/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
0.020 J mg/Kg - dry 0.002 0.024Acetone 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 12/17/21 17:06 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/17/21 17:06 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/17/21 17:06 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/17/21 17:06 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/17/21 17:06 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/17/21 17:06 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/17/21 17:06 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 12/17/21 17:06 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/17/21 17:06 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/17/21 17:06 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 12/17/21 17:06 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/17/21 17:06 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/17/21 17:06 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 62 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-3
90737 Matrix:
12/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/17/21 17:06 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/17/21 17:06 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/17/21 17:06 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/17/21 17:06 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/17/21 17:06 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/17/21 17:06 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/17/21 17:06 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 12/17/21 17:06 V12995TBL
<0.017 mg/Kg - dry 0.017 0.306Ethanol 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 12/17/21 17:06 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 12/17/21 17:06 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 63 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-3
90737 Matrix:
12/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 12/17/21 17:06 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 12/17/21 17:06 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/17/21 17:06 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 12/17/21 17:06 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/17/21 17:06 V12995TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/17/21 17:06 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/17/21 17:06 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 12/17/21 17:06 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/17/21 17:06 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/17/21 17:06 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/17/21 17:06 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/17/21 17:06 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 64 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-3
90737 Matrix:
12/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/17/21 17:06 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/17/21 17:06 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/17/21 17:06 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/17/21 17:06 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/17/21 17:06 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/17/21 17:06 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/17/21 17:06 V12995
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/17/21 17:061 TBL V12995
Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/17/21 17:061 TBL V12995
Surrogate: Toluene-d8 86.7 Limits: 76-129%12/17/21 17:061 TBL V12995
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.142 mg/Kg - dry 0.142 0.809Acenaphthene 1 12/27/21 21:00 V13287JMV
<0.128 mg/Kg - dry 0.128 0.809Acenaphthylene 1 12/27/21 21:00 V13287JMV
<0.186 mg/Kg - dry 0.186 0.809Aniline 1 12/27/21 21:00 V13287JMV
<0.175 mg/Kg - dry 0.175 0.809Anthracene 1 12/27/21 21:00 V13287JMV
<0.170 mg/Kg - dry 0.170 0.809
Benzo(a)anthracene 1 12/27/21 21:00 V13287JMV
<0.180 mg/Kg - dry 0.180 0.809Benzo(a)pyrene 1 12/27/21 21:00 V13287JMV
<0.179 mg/Kg - dry 0.179 0.809Benzo(b)fluoranthene 1 12/27/21 21:00 V13287JMV
<0.166 mg/Kg - dry 0.166 0.809Benzo(g,h,i)perylene 1 12/27/21 21:00 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 65 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-3
90737 Matrix:
12/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.168 mg/Kg - dry 0.168 0.809Benzo(k)fluoranthene 1 12/27/21 21:00 V13287JMV
<0.711 mg/Kg - dry 0.711 2.45Benzoic Acid 1 12/27/21 21:00 V13287JMV
<0.128 mg/Kg - dry 0.128 0.809Benzyl alcohol 1 12/27/21 21:00 V13287JMV
<0.144 mg/Kg - dry 0.144 0.809Bis(2-Chloroethoxy)methane 1 12/27/21 21:00 V13287JMV
<0.131 mg/Kg - dry 0.131 0.809Bis(2-Chloroethyl)ether 1 12/27/21 21:00 V13287JMV
<0.166 mg/Kg - dry 0.166 0.404Bis(2-Chloroisopropyl)ether 1 12/27/21 21:00 V13287JMV
<0.147 mg/Kg - dry 0.147 0.809Bis(2-ethylhexyl)phthalate 1 12/27/21 21:00 V13287JMV
<0.133 mg/Kg - dry 0.133 0.8094-Bromophenyl phenyl ether 1 12/27/21 21:00 V13287JMV
<0.138 mg/Kg - dry 0.138 0.404
Butyl benzyl phthalate 1 12/27/21 21:00 V13287JMV
<0.113 mg/Kg - dry 0.113 0.8094-Chloro-3-methylphenol 1 12/27/21 21:00 V13287JMV
<0.137 mg/Kg - dry 0.137 0.4044-Chloroaniline 1 12/27/21 21:00 V13287JMV
<0.142 mg/Kg - dry 0.142 0.8092-Chloronaphthalene 1 12/27/21 21:00 V13287JMV
<0.120 mg/Kg - dry 0.120 0.8092-Chlorophenol 1 12/27/21 21:00 V13287JMV
<0.154 mg/Kg - dry 0.154 1.234-Chlorophenyl phenyl ether 1 12/27/21 21:00 V13287JMV
<0.174 mg/Kg - dry 0.174 0.809Chrysene 1 12/27/21 21:00 V13287JMV
<0.282 mg/Kg - dry 0.282 0.809
Dibenz(a,h)anthracene 1 12/27/21 21:00 V13287JMV
<0.146 mg/Kg - dry 0.146 0.809Dibenzofuran 1 12/27/21 21:00 V13287JMV
<0.115 mg/Kg - dry 0.115 0.8091,2-Dichlorobenzene 1 12/27/21 21:00 V13287JMV
<0.119 mg/Kg - dry 0.119 0.8091,3-Dichlorobenzene 1 12/27/21 21:00 V13287JMV
<0.119 mg/Kg - dry 0.119 0.4041,4-Dichlorobenzene 1 12/27/21 21:00 V13287JMV
<0.180 mg/Kg - dry 0.180 0.8093,3'-Dichlorobenzidine 1 12/27/21 21:00 V13287JMV
<0.117 mg/Kg - dry 0.117 0.8092,4-Dichlorophenol 1 12/27/21 21:00 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 66 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-3
90737 Matrix:
12/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.220 mg/Kg - dry 0.220 0.809Diethyl phthalate 1 12/27/21 21:00 V13287JMV
<0.213 mg/Kg - dry 0.213 0.809Dimethyl phthalate 1 12/27/21 21:00 V13287JMV
<0.132 mg/Kg - dry 0.132 0.4042,4-Dimethylphenol 1 12/27/21 21:00 V13287JMV
<0.131 mg/Kg - dry 0.131 0.809Di-n-butyl phthalate 1 12/27/21 21:00 V13287JMV
<0.294 mg/Kg - dry 0.294 1.844,6-Dinitro-2-methylphenol 1 12/27/21 21:00 V13287JMV
<0.638 mg/Kg - dry 0.638 1.842,4-Dinitrophenol 1 12/27/21 21:00 V13287JMV
<0.118 mg/Kg - dry 0.118 0.8092,4-Dinitrotoluene 1 12/27/21 21:00 V13287JMV
<0.132 mg/Kg - dry 0.132 0.8092,6-Dinitrotoluene 1 12/27/21 21:00 V13287JMV
<0.175 mg/Kg - dry 0.175 0.404
Di-n-Octyl Phthalate 1 12/27/21 21:00 V13287JMV
<0.150 mg/Kg - dry 0.150 0.809Fluoranthene 1 12/27/21 21:00 V13287JMV
<0.157 mg/Kg - dry 0.157 0.809Fluorene 1 12/27/21 21:00 V13287JMV
<0.130 mg/Kg - dry 0.130 0.809Hexachlorobenzene 1 12/27/21 21:00 V13287JMV
<0.119 mg/Kg - dry 0.119 0.809Hexachlorobutadiene 1 12/27/21 21:00 V13287JMV
<0.192 mg/Kg - dry 0.192 0.809Hexachlorocyclopentadiene 1 12/27/21 21:00 V13287JMV
<0.097 mg/Kg - dry 0.097 0.809Hexachloroethane 1 12/27/21 21:00 V13287JMV
<0.219 mg/Kg - dry 0.219 0.809
Indeno(1,2,3-cd)pyrene 1 12/27/21 21:00 V13287JMV
<0.234 mg/Kg - dry 0.234 0.809Isophorone 1 12/27/21 21:00 V13287JMV
<0.130 mg/Kg - dry 0.130 0.8091-Methylnaphthalene 1 12/27/21 21:00 V13287JMV
<0.122 mg/Kg - dry 0.122 0.8092-Methylnaphthalene 1 12/27/21 21:00 V13287JMV
<0.119 mg/Kg - dry 0.119 0.8092-Methylphenol 1 12/27/21 21:00 V13287JMV
<0.104 mg/Kg - dry 0.104 0.8093&4 Methylphenol 1 12/27/21 21:00 V13287JMV
<0.176 mg/Kg - dry 0.176 0.809Naphthalene 1 12/27/21 21:00 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 67 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-3
90737 Matrix:
12/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.118 mg/Kg - dry 0.118 0.8092-Nitroaniline 1 12/27/21 21:00 V13287JMV
<0.147 mg/Kg - dry 0.147 0.8093-Nitroaniline 1 12/27/21 21:00 V13287JMV
<0.114 mg/Kg - dry 0.114 0.4044-Nitroaniline 1 12/27/21 21:00 V13287JMV
<0.142 mg/Kg - dry 0.142 0.404Nitrobenzene 1 12/27/21 21:00 V13287JMV
<0.108 mg/Kg - dry 0.108 0.8092-Nitrophenol 1 12/27/21 21:00 V13287JMV
<0.143 mg/Kg - dry 0.143 0.8094-Nitrophenol 1 12/27/21 21:00 V13287JMV
<0.322 mg/Kg - dry 0.322 0.809N-Nitrosodimethylamine 1 12/27/21 21:00 V13287JMV
<0.222 mg/Kg - dry 0.222 0.809N-Nitrosodiphenylamine 1 12/27/21 21:00 V13287JMV
<0.144 mg/Kg - dry 0.144 0.809
N-Nitroso-di-n-propylamine 1 12/27/21 21:00 V13287JMV
<0.425 mg/Kg - dry 0.425 1.23Pentachlorophenol 1 12/27/21 21:00 V13287JMV
<0.255 mg/Kg - dry 0.255 0.809Phenanthrene 1 12/27/21 21:00 V13287JMV
<0.137 mg/Kg - dry 0.137 0.809Phenol 1 12/27/21 21:00 V13287JMV
<0.164 mg/Kg - dry 0.164 0.809Pyrene 1 12/27/21 21:00 V13287JMV
<0.097 mg/Kg - dry 0.097 0.404Pyridine 1 12/27/21 21:00 V13287JMV
<0.131 mg/Kg - dry 0.131 0.8091,2,4-Trichlorobenzene 1 12/27/21 21:00 V13287JMV
<0.118 mg/Kg - dry 0.118 0.809
2,4,5-Trichlorophenol 1 12/27/21 21:00 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 68 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-3
90737 Matrix:
12/15/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.118 mg/Kg - dry 0.118 0.8092,4,6-Trichlorophenol 1 12/27/21 21:00 V13287JMV
Surrogate: Phenol-d5 83.5 Limits: 34-121%12/27/21 21:001 JMV V13287
Surrogate: 2-Fluorobiphenyl 80.7 Limits: 44-115%12/27/21 21:001 JMV V13287
Surrogate: 2-Fluorophenol 84.7 Limits: 35-115%12/27/21 21:001 JMV V13287
Surrogate: Nitrobenzene-d5 71.7 Limits: 37-122%12/27/21 21:001 JMV V13287
Surrogate: 4-Terphenyl-d14 89.2 Limits: 54-127%12/27/21 21:001 JMV V13287
Surrogate: 2,4,6-Tribromophenol 79.9 Limits: 39-132%12/27/21 21:001 JMV V13287
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 69 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-4
90738 Matrix:
12/15/2021 13:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
37.8 %Moisture 1 12/21/21 17:16 SW-DRYWTCEG
1.98 mg/Kg - dry 0.151 1.61Arsenic 10 12/20/21 23:49 6020BEDV
99.7 mg/Kg - dry 2.25 16.1Barium 10 12/20/21 23:49 6020BEDV
0.167 J mg/Kg - dry 0.0884 0.804Cadmium 10 12/20/21 23:49 6020BEDV
47.7 mg/Kg - dry 0.466 1.61Chromium 10 12/20/21 23:49 6020BEDV
33.3 mg/Kg - dry 0.225 1.61
Lead 10 12/20/21 23:49 6020BEDV
0.0297 J mg/Kg - dry 0.0193 0.0482Mercury (Total)1 12/21/21 18:15 7471BEDV
<1.45 mg/Kg - dry 1.45 3.22Selenium 10 12/20/21 23:49 6020BEDV
<0.0659 mg/Kg - dry 0.0659 0.804Silver 10 12/20/21 23:49 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 70 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-4
90738 Matrix:
12/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
0.016 J mg/Kg - dry 0.003 0.032Acetone 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.032Acrolein 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.032Acrylonitrile 1 12/17/21 17:34 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.008Benzene 1 12/17/21 17:34 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.008Bromobenzene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008Bromochloromethane 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008Bromodichloromethane 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008Bromoform 1 12/17/21 17:34 V12995TBL
<0.002 mg/Kg - dry 0.002 0.016
Bromomethane 1 12/17/21 17:34 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.008n-Butylbenzene 1 12/17/21 17:34 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.008sec-Butyl benzene 1 12/17/21 17:34 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.008tert-Butyl benzene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008Carbon Disulfide 1 12/17/21 17:34 V12995TBL
<0.002 mg/Kg - dry 0.002 0.008Carbon Tetrachloride 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008Chlorobenzene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008
Chlorodibromomethane 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.016Chloroethane 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008Chloroform 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.016Chloromethane 1 12/17/21 17:34 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0082-Chlorotoluene 1 12/17/21 17:34 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0084-Chlorotoluene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008Di-Isopropyl Ether (DIPE)1 12/17/21 17:34 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 71 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-4
90738 Matrix:
12/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0161,2-Dibromo-3-Chloropropane 1 12/17/21 17:34 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0081,2-Dibromoethane 1 12/17/21 17:34 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.008Dibromomethane 1 12/17/21 17:34 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0081,2-Dichlorobenzene 1 12/17/21 17:34 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0081,3-Dichlorobenzene 1 12/17/21 17:34 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.0081,4-Dichlorobenzene 1 12/17/21 17:34 V12995TBL
<0.002 mg/Kg - dry 0.002 0.016Dichlorodifluoromethane 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0081,1-Dichloroethane 1 12/17/21 17:34 V12995TBL
<0.002 mg/Kg - dry 0.002 0.008
1,2-Dichloroethane 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0081,1-Dichloroethene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008cis-1,2-Dichloroethene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008trans-1,2-Dichloroethene 1 12/17/21 17:34 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0081,2-Dichloropropane 1 12/17/21 17:34 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0081,3-Dichloropropane 1 12/17/21 17:34 V12995TBL
<0.002 mg/Kg - dry 0.002 0.0082,2-Dichloropropane 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008
1,1-Dichloropropene 1 12/17/21 17:34 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.008cis-1,3-Dichloropropene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008trans-1,3-Dichloropropene 1 12/17/21 17:34 V12995TBL
0.095 J mg/Kg - dry 0.022 0.401Ethanol 1 12/17/21 17:34 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.008Ethylbenzene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.080Ethyl Tertiary Butyl Ether (ETBE)1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.016Hexachlorobutadiene 1 12/17/21 17:34 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 72 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-4
90738 Matrix:
12/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.001 mg/Kg - dry 0.001 0.016n-Hexane 1 12/17/21 17:34 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.0322-Hexanone 1 12/17/21 17:34 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.008Isopropylbenzene 1 12/17/21 17:34 V12995TBL
<0.002 mg/Kg - dry 0.002 0.0084-Isopropyl toluene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.032Methyl Ethyl Ketone (MEK)1 12/17/21 17:34 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.008Methyl tert-butyl ether (MTBE)1 12/17/21 17:34 V12995TBL
<0.024 mg/Kg - dry 0.024 0.0324-Methyl-2-Pentanone 1 12/17/21 17:34 V12995TBL
<0.002 mg/Kg - dry 0.002 0.016Methylene Chloride 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.016
Naphthalene 1 12/17/21 17:34 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.008n-Propylbenzene 1 12/17/21 17:34 V12995TBL
<0.002 mg/Kg - dry 0.002 0.008Styrene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0081,1,1,2-Tetrachloroethane 1 12/17/21 17:34 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0081,1,2,2-Tetrachloroethane 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008Tetrachloroethene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008Toluene 1 12/17/21 17:34 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.016
1,2,3-Trichlorobenzene 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0161,2,4-Trichlorobenzene 1 12/17/21 17:34 V12995TBL
<0.002 mg/Kg - dry 0.002 0.0081,1,1-Trichloroethane 1 12/17/21 17:34 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0081,1,2-Trichloroethane 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.008Trichloroethene 1 12/17/21 17:34 V12995TBL
<0.003 mg/Kg - dry 0.003 0.016Trichlorofluoromethane 1 12/17/21 17:34 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0081,2,3-Trichloropropane 1 12/17/21 17:34 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 73 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-4
90738 Matrix:
12/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0081,2,4-Trimethylbenzene 1 12/17/21 17:34 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0081,3,5-Trimethylbenzene 1 12/17/21 17:34 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.016Vinyl Acetate 1 12/17/21 17:34 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.016Vinyl Chloride 1 12/17/21 17:34 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.008o-Xylene 1 12/17/21 17:34 V12995TBL
<0.002 mg/Kg - dry 0.002 0.016m,p-Xylene 1 12/17/21 17:34 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.008Xylene (Total)1 12/17/21 17:34 V12995
Surrogate: 4-Bromofluorobenzene 97.1 Limits: 70-130%12/17/21 17:341 TBL V12995
Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/17/21 17:341 TBL V12995
Surrogate: Toluene-d8 88.8 Limits: 76-129%12/17/21 17:341 TBL V12995
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.186 mg/Kg - dry 0.186 1.06Acenaphthene 1 12/27/21 21:23 V13287JMV
<0.168 mg/Kg - dry 0.168 1.06Acenaphthylene 1 12/27/21 21:23 V13287JMV
<0.244 mg/Kg - dry 0.244 1.06Aniline 1 12/27/21 21:23 V13287JMV
<0.229 mg/Kg - dry 0.229 1.06Anthracene 1 12/27/21 21:23 V13287JMV
<0.223 mg/Kg - dry 0.223 1.06
Benzo(a)anthracene 1 12/27/21 21:23 V13287JMV
<0.236 mg/Kg - dry 0.236 1.06Benzo(a)pyrene 1 12/27/21 21:23 V13287JMV
0.234 J mg/Kg - dry 0.234 1.06Benzo(b)fluoranthene 1 12/27/21 21:23 V13287JMV
<0.218 mg/Kg - dry 0.218 1.06Benzo(g,h,i)perylene 1 12/27/21 21:23 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 74 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-4
90738 Matrix:
12/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.220 mg/Kg - dry 0.220 1.06Benzo(k)fluoranthene 1 12/27/21 21:23 V13287JMV
<0.932 mg/Kg - dry 0.932 3.22Benzoic Acid 1 12/27/21 21:23 V13287JMV
<0.168 mg/Kg - dry 0.168 1.06Benzyl alcohol 1 12/27/21 21:23 V13287JMV
<0.189 mg/Kg - dry 0.189 1.06Bis(2-Chloroethoxy)methane 1 12/27/21 21:23 V13287JMV
<0.172 mg/Kg - dry 0.172 1.06Bis(2-Chloroethyl)ether 1 12/27/21 21:23 V13287JMV
<0.218 mg/Kg - dry 0.218 0.530Bis(2-Chloroisopropyl)ether 1 12/27/21 21:23 V13287JMV
<0.192 mg/Kg - dry 0.192 1.06Bis(2-ethylhexyl)phthalate 1 12/27/21 21:23 V13287JMV
<0.175 mg/Kg - dry 0.175 1.064-Bromophenyl phenyl ether 1 12/27/21 21:23 V13287JMV
<0.181 mg/Kg - dry 0.181 0.530
Butyl benzyl phthalate 1 12/27/21 21:23 V13287JMV
<0.148 mg/Kg - dry 0.148 1.064-Chloro-3-methylphenol 1 12/27/21 21:23 V13287JMV
<0.180 mg/Kg - dry 0.180 0.5304-Chloroaniline 1 12/27/21 21:23 V13287JMV
<0.186 mg/Kg - dry 0.186 1.062-Chloronaphthalene 1 12/27/21 21:23 V13287JMV
<0.157 mg/Kg - dry 0.157 1.062-Chlorophenol 1 12/27/21 21:23 V13287JMV
<0.202 mg/Kg - dry 0.202 1.614-Chlorophenyl phenyl ether 1 12/27/21 21:23 V13287JMV
<0.228 mg/Kg - dry 0.228 1.06Chrysene 1 12/27/21 21:23 V13287JMV
<0.369 mg/Kg - dry 0.369 1.06
Dibenz(a,h)anthracene 1 12/27/21 21:23 V13287JMV
<0.191 mg/Kg - dry 0.191 1.06Dibenzofuran 1 12/27/21 21:23 V13287JMV
<0.151 mg/Kg - dry 0.151 1.061,2-Dichlorobenzene 1 12/27/21 21:23 V13287JMV
<0.156 mg/Kg - dry 0.156 1.061,3-Dichlorobenzene 1 12/27/21 21:23 V13287JMV
<0.156 mg/Kg - dry 0.156 0.5301,4-Dichlorobenzene 1 12/27/21 21:23 V13287JMV
<0.236 mg/Kg - dry 0.236 1.063,3'-Dichlorobenzidine 1 12/27/21 21:23 V13287JMV
<0.154 mg/Kg - dry 0.154 1.062,4-Dichlorophenol 1 12/27/21 21:23 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 75 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-4
90738 Matrix:
12/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.289 mg/Kg - dry 0.289 1.06Diethyl phthalate 1 12/27/21 21:23 V13287JMV
<0.279 mg/Kg - dry 0.279 1.06Dimethyl phthalate 1 12/27/21 21:23 V13287JMV
<0.173 mg/Kg - dry 0.173 0.5302,4-Dimethylphenol 1 12/27/21 21:23 V13287JMV
<0.172 mg/Kg - dry 0.172 1.06Di-n-butyl phthalate 1 12/27/21 21:23 V13287JMV
<0.385 mg/Kg - dry 0.385 2.414,6-Dinitro-2-methylphenol 1 12/27/21 21:23 V13287JMV
<0.836 mg/Kg - dry 0.836 2.412,4-Dinitrophenol 1 12/27/21 21:23 V13287JMV
<0.155 mg/Kg - dry 0.155 1.062,4-Dinitrotoluene 1 12/27/21 21:23 V13287JMV
<0.173 mg/Kg - dry 0.173 1.062,6-Dinitrotoluene 1 12/27/21 21:23 V13287JMV
<0.229 mg/Kg - dry 0.229 0.530
Di-n-Octyl Phthalate 1 12/27/21 21:23 V13287JMV
0.231 J mg/Kg - dry 0.197 1.06Fluoranthene 1 12/27/21 21:23 V13287JMV
<0.205 mg/Kg - dry 0.205 1.06Fluorene 1 12/27/21 21:23 V13287JMV
<0.170 mg/Kg - dry 0.170 1.06Hexachlorobenzene 1 12/27/21 21:23 V13287JMV
<0.156 mg/Kg - dry 0.156 1.06Hexachlorobutadiene 1 12/27/21 21:23 V13287JMV
<0.252 mg/Kg - dry 0.252 1.06Hexachlorocyclopentadiene 1 12/27/21 21:23 V13287JMV
<0.127 mg/Kg - dry 0.127 1.06Hexachloroethane 1 12/27/21 21:23 V13287JMV
<0.287 mg/Kg - dry 0.287 1.06
Indeno(1,2,3-cd)pyrene 1 12/27/21 21:23 V13287JMV
<0.307 mg/Kg - dry 0.307 1.06Isophorone 1 12/27/21 21:23 V13287JMV
<0.170 mg/Kg - dry 0.170 1.061-Methylnaphthalene 1 12/27/21 21:23 V13287JMV
<0.160 mg/Kg - dry 0.160 1.062-Methylnaphthalene 1 12/27/21 21:23 V13287JMV
<0.155 mg/Kg - dry 0.155 1.062-Methylphenol 1 12/27/21 21:23 V13287JMV
<0.136 mg/Kg - dry 0.136 1.063&4 Methylphenol 1 12/27/21 21:23 V13287JMV
<0.231 mg/Kg - dry 0.231 1.06Naphthalene 1 12/27/21 21:23 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 76 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-4
90738 Matrix:
12/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.155 mg/Kg - dry 0.155 1.062-Nitroaniline 1 12/27/21 21:23 V13287JMV
<0.192 mg/Kg - dry 0.192 1.063-Nitroaniline 1 12/27/21 21:23 V13287JMV
<0.150 mg/Kg - dry 0.150 0.5304-Nitroaniline 1 12/27/21 21:23 V13287JMV
<0.186 mg/Kg - dry 0.186 0.530Nitrobenzene 1 12/27/21 21:23 V13287JMV
<0.142 mg/Kg - dry 0.142 1.062-Nitrophenol 1 12/27/21 21:23 V13287JMV
<0.188 mg/Kg - dry 0.188 1.064-Nitrophenol 1 12/27/21 21:23 V13287JMV
<0.422 mg/Kg - dry 0.422 1.06N-Nitrosodimethylamine 1 12/27/21 21:23 V13287JMV
<0.290 mg/Kg - dry 0.290 1.06N-Nitrosodiphenylamine 1 12/27/21 21:23 V13287JMV
<0.189 mg/Kg - dry 0.189 1.06
N-Nitroso-di-n-propylamine 1 12/27/21 21:23 V13287JMV
<0.557 mg/Kg - dry 0.557 1.61Pentachlorophenol 1 12/27/21 21:23 V13287JMV
<0.334 mg/Kg - dry 0.334 1.06Phenanthrene 1 12/27/21 21:23 V13287JMV
<0.180 mg/Kg - dry 0.180 1.06Phenol 1 12/27/21 21:23 V13287JMV
0.228 J mg/Kg - dry 0.215 1.06Pyrene 1 12/27/21 21:23 V13287JMV
<0.127 mg/Kg - dry 0.127 0.530Pyridine 1 12/27/21 21:23 V13287JMV
<0.172 mg/Kg - dry 0.172 1.061,2,4-Trichlorobenzene 1 12/27/21 21:23 V13287JMV
<0.154 mg/Kg - dry 0.154 1.06
2,4,5-Trichlorophenol 1 12/27/21 21:23 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 77 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-4
90738 Matrix:
12/15/2021 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.155 mg/Kg - dry 0.155 1.062,4,6-Trichlorophenol 1 12/27/21 21:23 V13287JMV
Surrogate: Phenol-d5 83.2 Limits: 34-121%12/27/21 21:231 JMV V13287
Surrogate: 2-Fluorobiphenyl 72.3 Limits: 44-115%12/27/21 21:231 JMV V13287
Surrogate: 2-Fluorophenol 84.7 Limits: 35-115%12/27/21 21:231 JMV V13287
Surrogate: Nitrobenzene-d5 84.3 Limits: 37-122%12/27/21 21:231 JMV V13287
Surrogate: 4-Terphenyl-d14 83.7 Limits: 54-127%12/27/21 21:231 JMV V13287
Surrogate: 2,4,6-Tribromophenol 73.3 Limits: 39-132%12/27/21 21:231 JMV V13287
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 78 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-5
90739 Matrix:
12/15/2021 10:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.1 %Moisture 1 12/21/21 17:16 SW-DRYWTCEG
1.17 J mg/Kg - dry 0.116 1.24Arsenic 10 12/20/21 23:56 6020BEDV
525 mg/Kg - dry 1.73 12.4Barium 10 12/20/21 23:56 6020BEDV
<0.0679 mg/Kg - dry 0.0679 0.618Cadmium 10 12/20/21 23:56 6020BEDV
39.4 mg/Kg - dry 0.358 1.24Chromium 10 12/20/21 23:56 6020BEDV
4.03 mg/Kg - dry 0.173 1.24
Lead 10 12/20/21 23:56 6020BEDV
<0.0148 mg/Kg - dry 0.0148 0.0371Mercury (Total)1 12/21/21 17:48 7471BEDV
<1.11 mg/Kg - dry 1.11 2.47Selenium 10 12/20/21 23:56 6020BEDV
<0.0506 mg/Kg - dry 0.0506 0.618Silver 10 12/20/21 23:56 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 79 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-5
90739 Matrix:
12/15/2021 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
0.009 J mg/Kg - dry 0.002 0.024Acetone 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 12/17/21 18:01 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/17/21 18:01 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/17/21 18:01 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/17/21 18:01 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/17/21 18:01 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/17/21 18:01 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/17/21 18:01 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 12/17/21 18:01 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/17/21 18:01 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/17/21 18:01 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 12/17/21 18:01 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/17/21 18:01 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/17/21 18:01 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 80 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-5
90739 Matrix:
12/15/2021 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/17/21 18:01 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/17/21 18:01 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/17/21 18:01 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/17/21 18:01 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/17/21 18:01 V12995TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/17/21 18:01 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/17/21 18:01 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 12/17/21 18:01 V12995TBL
0.021 J mg/Kg - dry 0.017 0.309Ethanol 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 12/17/21 18:01 V12995TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 12/17/21 18:01 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 81 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-5
90739 Matrix:
12/15/2021 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 12/17/21 18:01 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 12/17/21 18:01 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/17/21 18:01 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 12/17/21 18:01 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/17/21 18:01 V12995TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/17/21 18:01 V12995TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/17/21 18:01 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 12/17/21 18:01 V12995TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/17/21 18:01 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/17/21 18:01 V12995TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/17/21 18:01 V12995TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/17/21 18:01 V12995TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 82 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-5
90739 Matrix:
12/15/2021 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V12994 12/17/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/17/21 18:01 V12995TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/17/21 18:01 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/17/21 18:01 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/17/21 18:01 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/17/21 18:01 V12995TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/17/21 18:01 V12995TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/17/21 18:01 V12995
Surrogate: 4-Bromofluorobenzene 98.5 Limits: 70-130%12/17/21 18:011 TBL V12995
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/17/21 18:011 TBL V12995
Surrogate: Toluene-d8 87.4 Limits: 76-129%12/17/21 18:011 TBL V12995
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.143 mg/Kg - dry 0.143 0.815Acenaphthene 1 12/27/21 21:46 V13287JMV
<0.129 mg/Kg - dry 0.129 0.815Acenaphthylene 1 12/27/21 21:46 V13287JMV
<0.187 mg/Kg - dry 0.187 0.815Aniline 1 12/27/21 21:46 V13287JMV
<0.176 mg/Kg - dry 0.176 0.815Anthracene 1 12/27/21 21:46 V13287JMV
<0.171 mg/Kg - dry 0.171 0.815
Benzo(a)anthracene 1 12/27/21 21:46 V13287JMV
<0.181 mg/Kg - dry 0.181 0.815Benzo(a)pyrene 1 12/27/21 21:46 V13287JMV
<0.180 mg/Kg - dry 0.180 0.815Benzo(b)fluoranthene 1 12/27/21 21:46 V13287JMV
<0.168 mg/Kg - dry 0.168 0.815Benzo(g,h,i)perylene 1 12/27/21 21:46 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 83 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-5
90739 Matrix:
12/15/2021 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.169 mg/Kg - dry 0.169 0.815Benzo(k)fluoranthene 1 12/27/21 21:46 V13287JMV
<0.716 mg/Kg - dry 0.716 2.47Benzoic Acid 1 12/27/21 21:46 V13287JMV
<0.129 mg/Kg - dry 0.129 0.815Benzyl alcohol 1 12/27/21 21:46 V13287JMV
<0.145 mg/Kg - dry 0.145 0.815Bis(2-Chloroethoxy)methane 1 12/27/21 21:46 V13287JMV
<0.132 mg/Kg - dry 0.132 0.815Bis(2-Chloroethyl)ether 1 12/27/21 21:46 V13287JMV
<0.168 mg/Kg - dry 0.168 0.407Bis(2-Chloroisopropyl)ether 1 12/27/21 21:46 V13287JMV
<0.148 mg/Kg - dry 0.148 0.815Bis(2-ethylhexyl)phthalate 1 12/27/21 21:46 V13287JMV
<0.134 mg/Kg - dry 0.134 0.8154-Bromophenyl phenyl ether 1 12/27/21 21:46 V13287JMV
<0.139 mg/Kg - dry 0.139 0.407
Butyl benzyl phthalate 1 12/27/21 21:46 V13287JMV
<0.114 mg/Kg - dry 0.114 0.8154-Chloro-3-methylphenol 1 12/27/21 21:46 V13287JMV
<0.138 mg/Kg - dry 0.138 0.4074-Chloroaniline 1 12/27/21 21:46 V13287JMV
<0.143 mg/Kg - dry 0.143 0.8152-Chloronaphthalene 1 12/27/21 21:46 V13287JMV
<0.121 mg/Kg - dry 0.121 0.8152-Chlorophenol 1 12/27/21 21:46 V13287JMV
<0.155 mg/Kg - dry 0.155 1.244-Chlorophenyl phenyl ether 1 12/27/21 21:46 V13287JMV
<0.175 mg/Kg - dry 0.175 0.815Chrysene 1 12/27/21 21:46 V13287JMV
<0.284 mg/Kg - dry 0.284 0.815
Dibenz(a,h)anthracene 1 12/27/21 21:46 V13287JMV
<0.147 mg/Kg - dry 0.147 0.815Dibenzofuran 1 12/27/21 21:46 V13287JMV
<0.116 mg/Kg - dry 0.116 0.8151,2-Dichlorobenzene 1 12/27/21 21:46 V13287JMV
<0.120 mg/Kg - dry 0.120 0.8151,3-Dichlorobenzene 1 12/27/21 21:46 V13287JMV
<0.120 mg/Kg - dry 0.120 0.4071,4-Dichlorobenzene 1 12/27/21 21:46 V13287JMV
<0.181 mg/Kg - dry 0.181 0.8153,3'-Dichlorobenzidine 1 12/27/21 21:46 V13287JMV
<0.118 mg/Kg - dry 0.118 0.8152,4-Dichlorophenol 1 12/27/21 21:46 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 84 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-5
90739 Matrix:
12/15/2021 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.222 mg/Kg - dry 0.222 0.815Diethyl phthalate 1 12/27/21 21:46 V13287JMV
<0.215 mg/Kg - dry 0.215 0.815Dimethyl phthalate 1 12/27/21 21:46 V13287JMV
<0.133 mg/Kg - dry 0.133 0.4072,4-Dimethylphenol 1 12/27/21 21:46 V13287JMV
<0.132 mg/Kg - dry 0.132 0.815Di-n-butyl phthalate 1 12/27/21 21:46 V13287JMV
<0.296 mg/Kg - dry 0.296 1.854,6-Dinitro-2-methylphenol 1 12/27/21 21:46 V13287JMV
<0.642 mg/Kg - dry 0.642 1.852,4-Dinitrophenol 1 12/27/21 21:46 V13287JMV
<0.119 mg/Kg - dry 0.119 0.8152,4-Dinitrotoluene 1 12/27/21 21:46 V13287JMV
<0.133 mg/Kg - dry 0.133 0.8152,6-Dinitrotoluene 1 12/27/21 21:46 V13287JMV
<0.176 mg/Kg - dry 0.176 0.407
Di-n-Octyl Phthalate 1 12/27/21 21:46 V13287JMV
<0.152 mg/Kg - dry 0.152 0.815Fluoranthene 1 12/27/21 21:46 V13287JMV
<0.158 mg/Kg - dry 0.158 0.815Fluorene 1 12/27/21 21:46 V13287JMV
<0.131 mg/Kg - dry 0.131 0.815Hexachlorobenzene 1 12/27/21 21:46 V13287JMV
<0.120 mg/Kg - dry 0.120 0.815Hexachlorobutadiene 1 12/27/21 21:46 V13287JMV
<0.194 mg/Kg - dry 0.194 0.815Hexachlorocyclopentadiene 1 12/27/21 21:46 V13287JMV
<0.097 mg/Kg - dry 0.097 0.815Hexachloroethane 1 12/27/21 21:46 V13287JMV
<0.221 mg/Kg - dry 0.221 0.815
Indeno(1,2,3-cd)pyrene 1 12/27/21 21:46 V13287JMV
<0.236 mg/Kg - dry 0.236 0.815Isophorone 1 12/27/21 21:46 V13287JMV
<0.131 mg/Kg - dry 0.131 0.8151-Methylnaphthalene 1 12/27/21 21:46 V13287JMV
<0.123 mg/Kg - dry 0.123 0.8152-Methylnaphthalene 1 12/27/21 21:46 V13287JMV
<0.119 mg/Kg - dry 0.119 0.8152-Methylphenol 1 12/27/21 21:46 V13287JMV
<0.104 mg/Kg - dry 0.104 0.8153&4 Methylphenol 1 12/27/21 21:46 V13287JMV
<0.177 mg/Kg - dry 0.177 0.815Naphthalene 1 12/27/21 21:46 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 85 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-5
90739 Matrix:
12/15/2021 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.119 mg/Kg - dry 0.119 0.8152-Nitroaniline 1 12/27/21 21:46 V13287JMV
<0.148 mg/Kg - dry 0.148 0.8153-Nitroaniline 1 12/27/21 21:46 V13287JMV
<0.115 mg/Kg - dry 0.115 0.4074-Nitroaniline 1 12/27/21 21:46 V13287JMV
<0.143 mg/Kg - dry 0.143 0.407Nitrobenzene 1 12/27/21 21:46 V13287JMV
<0.109 mg/Kg - dry 0.109 0.8152-Nitrophenol 1 12/27/21 21:46 V13287JMV
<0.144 mg/Kg - dry 0.144 0.8154-Nitrophenol 1 12/27/21 21:46 V13287JMV
<0.325 mg/Kg - dry 0.325 0.815N-Nitrosodimethylamine 1 12/27/21 21:46 V13287JMV
<0.223 mg/Kg - dry 0.223 0.815N-Nitrosodiphenylamine 1 12/27/21 21:46 V13287JMV
<0.145 mg/Kg - dry 0.145 0.815
N-Nitroso-di-n-propylamine 1 12/27/21 21:46 V13287JMV
<0.428 mg/Kg - dry 0.428 1.24Pentachlorophenol 1 12/27/21 21:46 V13287JMV
<0.257 mg/Kg - dry 0.257 0.815Phenanthrene 1 12/27/21 21:46 V13287JMV
<0.138 mg/Kg - dry 0.138 0.815Phenol 1 12/27/21 21:46 V13287JMV
<0.165 mg/Kg - dry 0.165 0.815Pyrene 1 12/27/21 21:46 V13287JMV
<0.097 mg/Kg - dry 0.097 0.407Pyridine 1 12/27/21 21:46 V13287JMV
<0.132 mg/Kg - dry 0.132 0.8151,2,4-Trichlorobenzene 1 12/27/21 21:46 V13287JMV
<0.118 mg/Kg - dry 0.118 0.815
2,4,5-Trichlorophenol 1 12/27/21 21:46 V13287JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 86 of 129
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-350-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 12/16/2021
LEN.008
Report Date : 12/29/2021
Sample ID :
Lab No :
Sampled:SP-1215-5
90739 Matrix:
12/15/2021 10:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V12959 12/17/21 09:13
<0.119 mg/Kg - dry 0.119 0.8152,4,6-Trichlorophenol 1 12/27/21 21:46 V13287JMV
Surrogate: Phenol-d5 89.2 Limits: 34-121%12/27/21 21:461 JMV V13287
Surrogate: 2-Fluorobiphenyl 76.6 Limits: 44-115%12/27/21 21:461 JMV V13287
Surrogate: 2-Fluorophenol 92.5 Limits: 35-115%12/27/21 21:461 JMV V13287
Surrogate: Nitrobenzene-d5 88.6 Limits: 37-122%12/27/21 21:461 JMV V13287
Surrogate: 4-Terphenyl-d14 88.6 Limits: 54-127%12/27/21 21:461 JMV V13287
Surrogate: 2,4,6-Tribromophenol 78.1 Limits: 39-132%12/27/21 21:461 JMV V13287
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 87 of 129
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172Tel: [phone] Fax: [phone] www.pacelabs.com
Report of Analysis
Waypoint Analytical
PO Box 240543Charlotte, NC 28224Attention: Angela Overcash
Project Name: 21-350-0013
Lot Number:WL17099
Date Completed:12/28/2021
12/28/2021 11:46 AMApproved and released by:
Project Manager II:Lucas Odom
Page 1 of 21
Page 88 of 129
PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Waypoint Analytical
Lot Number: WL17099
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header informationassociated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page ordiscussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non-Potable Water: SGT-HEM EPA 1664B,Silica EPA 200.7, Boron, Calcium,Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weightunless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Page 2 of 21
Page 89 of 129
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WL17099

Sample Number Sample ID Matrix Date Sampled Date Received
001 12/15/2021 1020Ex-9 Solid 12/17/2021
002 12/15/2021 0950Ex-10 Solid 12/17/2021
003 12/15/2021 0920Ex-11 Solid 12/17/2021
004 12/15/2021 0920DUPSolid 12/17/2021
005 12/15/2021 1115SP-1215-1 Solid 12/17/2021
006 12/15/2021 1145SP-1215-2 Solid 12/17/2021
007 12/15/2021 1220SP-1215-3 Solid 12/17/2021
008 12/15/2021 1300SP-1215-4 Solid 12/17/2021
009 12/15/2021 1040SP-1215-5 Solid 12/17/2021
(9 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 21
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WL17099

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 Ex-9 Solid Hexavalent Chromium 7199 0.48 J mg/kg 5
002 Ex-10 Solid Hexavalent Chromium 7199 0.57 J mg/kg 6
003 Ex-11 Solid Hexavalent Chromium 7199 3.6 mg/kg 7
004 DUP Solid Hexavalent Chromium 7199 3.1 mg/kg 8
005 SP-1215-1 Solid Hexavalent Chromium 7199 0.44 J mg/kg 9
007 SP-1215-3 Solid Hexavalent Chromium 7199 0.41 J mg/kg 11
008 SP-1215-4 Solid Hexavalent Chromium 7199 0.50 J mg/kg 12
009 SP-1215-5 Solid Hexavalent Chromium 7199 0.29 J mg/kg 13
(8 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 21
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
Ex-9
WL17099-001
12/15/2021 1020
12/17/2021
Solid
% Solids:78.0 12/23/2021 0237
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 12/23/2021 1840 AAB 12/22/2021 1046 26440
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.48 J 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 21
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
Ex-10
WL17099-002
12/15/2021 0950
12/17/2021
Solid
% Solids:75.6 12/22/2021 0223
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 12/23/2021 1853 AAB 12/22/2021 1046 26440
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.57 J 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 21
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
Ex-11
WL17099-003
12/15/2021 0920
12/17/2021
Solid
% Solids:82.5 12/23/2021 0237
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 12/23/2021 2024 AAB 12/23/2021 1034 26515
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 3.6 1mg/kg0.241.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 21
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
DUP
WL17099-004
12/15/2021 0920
12/17/2021
Solid
% Solids:77.4 12/22/2021 0223
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 3060A (Hexavalent C) 7199 1 12/24/2021 1337 AAB 12/23/2021 1034 26515
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 3.1 2mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 21
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
SP-1215-1
WL17099-005
12/15/2021 1115
12/17/2021
Solid
% Solids:78.1 12/23/2021 0237
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 12/23/2021 2050 AAB 12/23/2021 1034 26515
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.44 J 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 21
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
SP-1215-2
WL17099-006
12/15/2021 1145
12/17/2021
Solid
% Solids:80.2 12/22/2021 0223
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 12/23/2021 2103 AAB 12/23/2021 1034 26515
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.251.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 21
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
SP-1215-3
WL17099-007
12/15/2021 1220
12/17/2021
Solid
% Solids:78.0 12/22/2021 0223
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 12/23/2021 2116 AAB 12/23/2021 1034 26515
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.41 J 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 21
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
SP-1215-4
WL17099-008
12/15/2021 1300
12/17/2021
Solid
% Solids:79.2 12/22/2021 0223
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 12/23/2021 2128 AAB 12/23/2021 1034 26515
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.50 J 1mg/kg0.251.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 21
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
SP-1215-5
WL17099-009
12/15/2021 1040
12/17/2021
Solid
% Solids:90.9 12/22/2021 0223
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 12/23/2021 2141 AAB 12/23/2021 1034 26515
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.29 J 1mg/kg0.221.1
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 21
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 21
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ26440-001
26440 3060A
12/22/2021 1046Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 12/23/2021 12381.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 15 of 21
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ26440-002
26440 3060A
12/22/2021 1046Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 9.4 12/23/2021 1251941080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 16 of 21
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ26515-001
26515 3060A
12/23/2021 1034Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 12/23/2021 19581.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 17 of 21
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ26515-002
26515 3060A
12/23/2021 1034Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 9.0 12/23/2021 2011901080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 18 of 21
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 19 of 21
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 20 of 21
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 21 of 21
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Metals Analyses
6020B
V13051QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V13010
Associated Lab Samples: 90731, 90732, 90733, 90734, 90735, 90736, 90737, 90738, 90739
LRB-V13010 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/20/21 21:401.000.0940<0.0940mg/KgArsenic
12/20/21 21:4010.01.40<1.40mg/KgBarium
12/20/21 21:400.5000.0550<0.0550mg/KgCadmium
12/20/21 21:401.000.290<0.290mg/KgChromium
12/20/21 21:401.000.140<0.140mg/KgLead
12/20/21 21:402.000.900<0.900mg/KgSelenium
12/20/21 21:400.5000.0410<0.0410mg/KgSilver
LCS-V13010Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
93.011.612.5mg/KgArsenic 80-120
93.011.612.5mg/KgBarium 80-120
99.012.412.5mg/KgCadmium 80-120
90.011.312.5mg/KgChromium 80-120
94.011.812.5mg/KgLead 80-120
94.011.812.5mg/KgSelenium 80-120
96.04.825.00mg/KgSilver 80-120
V 90743-MS-V13010 V 90743-MSD-V13010Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
10.4 83.011.012.512.50.656mg/KgArsenic 88.0 75-125 5.6 20
112 11010312.512.598.2mg/KgBarium 38.0*75-125 8.3 20
12.5 10012.412.512.50.0768mg/KgCadmium 99.0 75-125 0.8 20
24.4 80.026.312.512.514.4mg/KgChromium 95.0 75-125 7.4 20
Page 1 of 19* QC Fail Date:12/29/2021 03:16 PM
Page 109 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Metals Analyses
6020B
V13051QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V13010
V 90743-MS-V13010 V 90743-MSD-V13010Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
52.9 164*45.512.512.532.4mg/KgLead 105 75-125 15.0 20
10.2 82.011.212.512.5<0.900mg/KgSelenium 90.0 75-125 9.3 20
4.82 96.04.595.005.00<0.0410mg/KgSilver 92.0 75-125 4.8 20
V 90743-PDS-V13010Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/20/21 22:2596.012.0mg/KgArsenic
12/20/21 22:2510464.2mg/KgBarium
12/20/21 22:2598.012.2mg/KgCadmium
12/20/21 22:2591.017.9mg/KgChromium
12/20/21 22:2593.026.8mg/KgLead
12/20/21 22:2595.011.9mg/KgSelenium
12/20/21 22:2595.011.8mg/KgSilver
Page 2 of 19Date:12/29/2021 03:16 PM
Page 110 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V13114QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V13080
Associated Lab Samples: 90731, 90732, 90733, 90734, 90735, 90736, 90737, 90738, 90739
LRB-V13080 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/21/21 16:460.03000.0120<0.0120mg/KgMercury (Total)
LCS-V13080Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1010.4220.417mg/KgMercury (Total)80-120
V 90593-MS-V13080 V 90593-MSD-V13080Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.400 96.00.4150.4170.417<0.0120mg/KgMercury (Total)100 80-120 3.6 20
V 90593-PDS-V13080Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/21/21 17:1098.00.205mg/KgMercury (Total)
Page 3 of 19Date:12/29/2021 03:16 PM
Page 111 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12994
Associated Lab Samples: 90731, 90732, 90733, 90734, 90735, 90736, 90737, 90738, 90739
LRB-V12994 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/17/21 11:040.0200.002<0.002mg/KgAcetone
12/17/21 11:040.0200.001<0.001mg/KgAcrolein
12/17/21 11:040.0200.0008<0.0008mg/KgAcrylonitrile
12/17/21 11:040.0050.0006<0.0006mg/KgBenzene
12/17/21 11:040.0050.0005<0.0005mg/KgBromobenzene
12/17/21 11:040.0050.0008<0.0008mg/KgBromochloromethane
12/17/21 11:040.0050.001<0.001mg/KgBromodichloromethane
12/17/21 11:040.0050.001<0.001mg/KgBromoform
12/17/21 11:040.0100.001<0.001mg/KgBromomethane
12/17/21 11:040.0050.0005<0.0005mg/Kgn-Butylbenzene
12/17/21 11:040.0050.0006<0.0006mg/Kgsec-Butyl benzene
12/17/21 11:040.0050.0005<0.0005mg/Kgtert-Butyl benzene
12/17/21 11:040.0050.0006<0.0006mg/KgCarbon Disulfide
12/17/21 11:040.0050.001<0.001mg/KgCarbon Tetrachloride
12/17/21 11:040.0050.0007<0.0007mg/KgChlorobenzene
12/17/21 11:040.0050.0009<0.0009mg/KgChlorodibromomethane
12/17/21 11:040.0100.0009<0.0009mg/KgChloroethane
12/17/21 11:040.0050.001<0.001mg/KgChloroform
12/17/21 11:040.0100.0006<0.0006mg/KgChloromethane
12/17/21 11:040.0050.0005<0.0005mg/Kg2-Chlorotoluene
12/17/21 11:040.0050.0004<0.0004mg/Kg4-Chlorotoluene
12/17/21 11:040.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
12/17/21 11:040.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
12/17/21 11:040.0050.0006<0.0006mg/Kg1,2-Dibromoethane
12/17/21 11:040.0050.0006<0.0006mg/KgDibromomethane
12/17/21 11:040.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
12/17/21 11:040.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 19Date:12/29/2021 03:16 PM
Page 112 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12994
Associated Lab Samples: 90731, 90732, 90733, 90734, 90735, 90736, 90737, 90738, 90739
LRB-V12994 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/17/21 11:040.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
12/17/21 11:040.0100.001<0.001mg/KgDichlorodifluoromethane
12/17/21 11:040.0050.0008<0.0008mg/Kg1,1-Dichloroethane
12/17/21 11:040.0050.001<0.001mg/Kg1,2-Dichloroethane
12/17/21 11:040.0050.0007<0.0007mg/Kg1,1-Dichloroethene
12/17/21 11:040.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
12/17/21 11:040.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
12/17/21 11:040.0050.0004<0.0004mg/Kg1,2-Dichloropropane
12/17/21 11:040.0050.0006<0.0006mg/Kg1,3-Dichloropropane
12/17/21 11:040.0050.001<0.001mg/Kg2,2-Dichloropropane
12/17/21 11:040.0050.0008<0.0008mg/Kg1,1-Dichloropropene
12/17/21 11:040.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
12/17/21 11:040.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
12/17/21 11:040.2500.014<0.014mg/KgEthanol
12/17/21 11:040.0050.0006<0.0006mg/KgEthylbenzene
12/17/21 11:040.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
12/17/21 11:040.0100.0008<0.0008mg/KgHexachlorobutadiene
12/17/21 11:040.0100.0007<0.0007mg/Kgn-Hexane
12/17/21 11:040.0200.0006<0.0006mg/Kg2-Hexanone
12/17/21 11:040.0050.0005<0.0005mg/KgIsopropylbenzene
12/17/21 11:040.0050.001<0.001mg/Kg4-Isopropyl toluene
12/17/21 11:040.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
12/17/21 11:040.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
12/17/21 11:040.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
12/17/21 11:040.0100.001<0.001mg/KgMethylene Chloride
12/17/21 11:040.0100.0010<0.0010mg/KgNaphthalene
12/17/21 11:040.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 19Date:12/29/2021 03:16 PM
Page 113 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12994
Associated Lab Samples: 90731, 90732, 90733, 90734, 90735, 90736, 90737, 90738, 90739
LRB-V12994 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/17/21 11:040.0050.001<0.001mg/KgStyrene
12/17/21 11:040.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
12/17/21 11:040.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
12/17/21 11:040.0050.0009<0.0009mg/KgTetrachloroethene
12/17/21 11:040.0050.0007<0.0007mg/KgToluene
12/17/21 11:040.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
12/17/21 11:040.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
12/17/21 11:040.0050.001<0.001mg/Kg1,1,1-Trichloroethane
12/17/21 11:040.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
12/17/21 11:040.0050.0009<0.0009mg/KgTrichloroethene
12/17/21 11:040.0100.002<0.002mg/KgTrichlorofluoromethane
12/17/21 11:040.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
12/17/21 11:040.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
12/17/21 11:040.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
12/17/21 11:040.0100.0005<0.0005mg/KgVinyl Acetate
12/17/21 11:040.0100.0005<0.0005mg/KgVinyl Chloride
12/17/21 11:040.0050.0005<0.0005mg/Kgo-Xylene
12/17/21 11:040.0100.001<0.001mg/Kgm,p-Xylene
12/17/21 11:044-Bromofluorobenzene (S)97.8 70-130
12/17/21 11:04Dibromofluoromethane (S)98.6 84-123
12/17/21 11:04Toluene-d8 (S)89.6 76-129
LCS-V12994 LCSD-V12994Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.123 1231230.1230.100mg/KgAcetone 29-198 0.0 20
Page 6 of 19Date:12/29/2021 03:16 PM
Page 114 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12994
LCS-V12994 LCSD-V12994Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.115 1151150.1150.100mg/KgAcrolein 70-130 0.0 20
0.106 1061050.1050.100mg/KgAcrylonitrile 65-134 0.9 20
0.052 1051110.0550.050mg/KgBenzene 74-127 5.7 20
0.042 84.489.40.0440.050mg/KgBromobenzene 73-125 5.7 20
0.054 1091130.0560.050mg/KgBromochloromethane 72-134 3.0 20
0.052 1051090.0540.050mg/KgBromodichloromethane 75-122 3.7 20
0.048 96.298.60.0490.050mg/KgBromoform 66-135 2.4 20
0.048 96.41050.0520.050mg/KgBromomethane 20-180 8.3 20
0.043 87.894.40.0470.050mg/Kgn-Butylbenzene 65-135 7.2 20
0.043 87.292.20.0460.050mg/Kgsec-Butyl benzene 66-131 5.5 20
0.042 84.891.00.0450.050mg/Kgtert-Butyl benzene 67-132 7.0 20
0.051 1031100.0550.050mg/KgCarbon Disulfide 61-129 7.1 20
0.051 1031160.0570.050mg/KgCarbon Tetrachloride 64-143 11.3 20
0.046 92.697.20.0480.050mg/KgChlorobenzene 74-118 4.8 20
0.047 95.498.60.0490.050mg/KgChlorodibromomethane 73-122 3.2 20
0.055 1101150.0570.050mg/KgChloroethane 33-149 4.0 20
0.051 1021070.0530.050mg/KgChloroform 73-127 4.0 20
0.055 1121190.0590.050mg/KgChloromethane 45-143 6.5 20
0.042 85.690.00.0450.050mg/Kg2-Chlorotoluene 67-124 5.0 20
0.042 84.889.20.0440.050mg/Kg4-Chlorotoluene 71-126 5.0 20
0.054 1091110.0550.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.3 20
0.042 85.289.00.0440.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 4.3 20
0.047 94.497.40.0480.050mg/Kg1,2-Dibromoethane 70-132 3.1 20
0.053 1061080.0540.050mg/KgDibromomethane 74-133 2.0 20
0.043 86.089.40.0440.050mg/Kg1,2-Dichlorobenzene 72-123 3.8 20
0.043 87.489.80.0440.050mg/Kg1,3-Dichlorobenzene 71-120 2.7 20
Page 7 of 19Date:12/29/2021 03:16 PM
Page 115 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12994
LCS-V12994 LCSD-V12994Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.043 86.090.40.0450.050mg/Kg1,4-Dichlorobenzene 71-123 4.9 20
0.058 1181260.0630.050mg/KgDichlorodifluoromethane 26-146 7.0 20
0.052 1041100.0540.050mg/Kg1,1-Dichloroethane 74-127 5.0 20
0.053 1071090.0540.050mg/Kg1,2-Dichloroethane 68-128 1.6 20
0.051 1021120.0550.050mg/Kg1,1-Dichloroethene 67-149 8.5 20
0.051 1041080.0540.050mg/Kgcis-1,2-Dichloroethene 76-134 4.3 20
0.051 1041110.0550.050mg/Kgtrans-1,2-Dichloroethene 73-132 6.3 20
0.052 1051090.0540.050mg/Kg1,2-Dichloropropane 73-130 4.1 20
0.047 94.696.20.0480.050mg/Kg1,3-Dichloropropane 75-124 1.6 20
0.051 1031110.0550.050mg/Kg2,2-Dichloropropane 50-142 7.0 20
0.051 1031120.0550.050mg/Kg1,1-Dichloropropene 71-130 8.3 20
0.054 1091100.0550.050mg/Kgcis-1,3-Dichloropropene 71-125 0.9 20
0.054 1081120.0560.050mg/Kgtrans-1,3-Dichloropropene 68-123 3.8 20
1.22 97.692.01.151.25mg/KgEthanol 70-130 5.9 20
0.045 91.298.20.0490.050mg/KgEthylbenzene 74-128 7.3 20
0.111 1111130.1130.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.7 20
0.042 85.491.40.0450.050mg/KgHexachlorobutadiene 64-125 6.7 20
0.052 1051160.0570.050mg/Kgn-Hexane 70-130 9.4 20
0.051 1021030.0510.050mg/Kg2-Hexanone 61-157 0.5 20
0.042 85.490.80.0450.050mg/KgIsopropylbenzene 68-126 6.1 20
0.044 88.093.60.0460.050mg/Kg4-Isopropyl toluene 68-129 6.1 20
0.055 1101110.0550.050mg/KgMethyl Ethyl Ketone (MEK)63-149 0.3 20
0.053 1071090.0540.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.0 20
0.053 1061040.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 1.7 20
0.046 93.697.40.0480.050mg/KgMethylene Chloride 74-129 3.9 20
0.042 84.686.00.0430.050mg/KgNaphthalene 57-157 1.6 20
Page 8 of 19Date:12/29/2021 03:16 PM
Page 116 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V12995QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V12994
LCS-V12994 LCSD-V12994Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 85.891.40.0450.050mg/Kgn-Propylbenzene 67-130 6.3 20
0.047 94.21000.0500.050mg/KgStyrene 77-121 6.1 20
0.046 92.699.20.0490.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 6.8 20
0.041 82.684.20.0420.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.9 20
0.051 1031100.0550.050mg/KgTetrachloroethene 68-130 6.9 20
0.051 1031090.0540.050mg/KgToluene 71-129 5.0 20
0.041 83.685.80.0420.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.5 20
0.042 85.889.60.0440.050mg/Kg1,2,4-Trichlorobenzene 66-125 4.3 20
0.050 1021100.0550.050mg/Kg1,1,1-Trichloroethane 67-131 7.9 20
0.046 93.496.60.0480.050mg/Kg1,1,2-Trichloroethane 70-133 3.3 20
0.052 1041120.0550.050mg/KgTrichloroethene 75-133 7.0 20
0.055 1111220.0610.050mg/KgTrichlorofluoromethane 44-146 9.2 20
0.042 85.085.40.0420.050mg/Kg1,2,3-Trichloropropane 60-137 0.4 20
0.043 86.091.40.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 6.0 20
0.043 86.291.00.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.4 20
0.055 1111100.0540.050mg/KgVinyl Acetate 60-140 0.9 20
0.054 1081170.0580.050mg/KgVinyl Chloride 48-147 7.8 20
0.046 92.499.00.0490.050mg/Kgo-Xylene 74-126 6.8 20
0.093 93.51010.1010.100mg/Kgm,p-Xylene 75-124 7.7 20
97.298.44-Bromofluorobenzene (S)70-130
99.099.4Dibromofluoromethane (S)84-123
89.291.4Toluene-d8 (S)76-129
Page 9 of 19Date:12/29/2021 03:16 PM
Page 117 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V13287QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12959
Associated Lab Samples: 90731, 90732, 90733, 90734, 90735, 90736, 90737, 90738, 90739
LRB-V12959 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/27/21 16:230.6600.116<0.116mg/KgAcenaphthene
12/27/21 16:230.6600.105<0.105mg/KgAcenaphthylene
12/27/21 16:230.6600.152<0.152mg/KgAniline
12/27/21 16:230.6600.143<0.143mg/KgAnthracene
12/27/21 16:230.6600.139<0.139mg/KgBenzo(a)anthracene
12/27/21 16:230.6600.147<0.147mg/KgBenzo(a)pyrene
12/27/21 16:230.6600.146<0.146mg/KgBenzo(b)fluoranthene
12/27/21 16:230.6600.136<0.136mg/KgBenzo(g,h,i)perylene
12/27/21 16:230.6600.137<0.137mg/KgBenzo(k)fluoranthene
12/27/21 16:232.000.580<0.580mg/KgBenzoic Acid
12/27/21 16:230.6600.105<0.105mg/KgBenzyl alcohol
12/27/21 16:230.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
12/27/21 16:230.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
12/27/21 16:230.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
12/27/21 16:230.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
12/27/21 16:230.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
12/27/21 16:230.3300.113<0.113mg/KgButyl benzyl phthalate
12/27/21 16:230.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
12/27/21 16:230.3300.112<0.112mg/Kg4-Chloroaniline
12/27/21 16:230.6600.116<0.116mg/Kg2-Chloronaphthalene
12/27/21 16:230.6600.098<0.098mg/Kg2-Chlorophenol
12/27/21 16:231.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
12/27/21 16:230.6600.142<0.142mg/KgChrysene
12/27/21 16:230.6600.230<0.230mg/KgDibenz(a,h)anthracene
12/27/21 16:230.6600.119<0.119mg/KgDibenzofuran
12/27/21 16:230.6600.094<0.094mg/Kg1,2-Dichlorobenzene
12/27/21 16:230.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 10 of 19Date:12/29/2021 03:16 PM
Page 118 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V13287QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12959
Associated Lab Samples: 90731, 90732, 90733, 90734, 90735, 90736, 90737, 90738, 90739
LRB-V12959 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/27/21 16:230.3300.097<0.097mg/Kg1,4-Dichlorobenzene
12/27/21 16:230.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
12/27/21 16:230.6600.095<0.095mg/Kg2,4-Dichlorophenol
12/27/21 16:230.6600.180<0.180mg/KgDiethyl phthalate
12/27/21 16:230.6600.174<0.174mg/KgDimethyl phthalate
12/27/21 16:230.3300.108<0.108mg/Kg2,4-Dimethylphenol
12/27/21 16:230.6600.107<0.107mg/KgDi-n-butyl phthalate
12/27/21 16:231.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
12/27/21 16:231.500.520<0.520mg/Kg2,4-Dinitrophenol
12/27/21 16:230.6600.096<0.096mg/Kg2,4-Dinitrotoluene
12/27/21 16:230.6600.108<0.108mg/Kg2,6-Dinitrotoluene
12/27/21 16:230.3300.143<0.143mg/KgDi-n-Octyl Phthalate
12/27/21 16:230.6600.123<0.123mg/KgFluoranthene
12/27/21 16:230.6600.128<0.128mg/KgFluorene
12/27/21 16:230.6600.106<0.106mg/KgHexachlorobenzene
12/27/21 16:230.6600.097<0.097mg/KgHexachlorobutadiene
12/27/21 16:230.6600.157<0.157mg/KgHexachlorocyclopentadiene
12/27/21 16:230.6600.079<0.079mg/KgHexachloroethane
12/27/21 16:230.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
12/27/21 16:230.6600.191<0.191mg/KgIsophorone
12/27/21 16:230.6600.106<0.106mg/Kg1-Methylnaphthalene
12/27/21 16:230.6600.100<0.100mg/Kg2-Methylnaphthalene
12/27/21 16:230.6600.097<0.097mg/Kg2-Methylphenol
12/27/21 16:230.6600.084<0.084mg/Kg3&4 Methylphenol
12/27/21 16:230.6600.144<0.144mg/KgNaphthalene
12/27/21 16:230.6600.096<0.096mg/Kg2-Nitroaniline
12/27/21 16:230.6600.120<0.120mg/Kg3-Nitroaniline
Page 11 of 19Date:12/29/2021 03:16 PM
Page 119 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V13287QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12959
Associated Lab Samples: 90731, 90732, 90733, 90734, 90735, 90736, 90737, 90738, 90739
LRB-V12959 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/27/21 16:230.3300.093<0.093mg/Kg4-Nitroaniline
12/27/21 16:230.3300.116<0.116mg/KgNitrobenzene
12/27/21 16:230.6600.088<0.088mg/Kg2-Nitrophenol
12/27/21 16:230.6600.117<0.117mg/Kg4-Nitrophenol
12/27/21 16:230.6600.263<0.263mg/KgN-Nitrosodimethylamine
12/27/21 16:230.6600.181<0.181mg/KgN-Nitrosodiphenylamine
12/27/21 16:230.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
12/27/21 16:231.000.347<0.347mg/KgPentachlorophenol
12/27/21 16:230.6600.208<0.208mg/KgPhenanthrene
12/27/21 16:230.6600.112<0.112mg/KgPhenol
12/27/21 16:230.6600.134<0.134mg/KgPyrene
12/27/21 16:230.3300.079<0.079mg/KgPyridine
12/27/21 16:230.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
12/27/21 16:230.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
12/27/21 16:230.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
12/27/21 16:232-Fluorobiphenyl (S)83.8 44-115
12/27/21 16:232-Fluorophenol (S)89.1 35-115
12/27/21 16:23Nitrobenzene-d5 (S)79.0 37-122
12/27/21 16:234-Terphenyl-d14 (S)91.0 54-127
12/27/21 16:232,4,6-Tribromophenol (S)75.6 39-132
12/27/21 16:23Phenol-d5 (S)84.0 34-121
LCS-V12959Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
90.41.511.67mg/KgAcenaphthene 40-123
94.01.571.67mg/KgAcenaphthylene 32-132
Page 12 of 19Date:12/29/2021 03:16 PM
Page 120 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V13287QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12959
LCS-V12959Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.81.651.67mg/KgAniline 12-197
94.01.571.67mg/KgAnthracene 47-123
94.01.571.67mg/KgBenzo(a)anthracene 49-126
1272.121.67mg/KgBenzo(a)pyrene 45-129
1131.891.67mg/KgBenzo(b)fluoranthene 45-132
1071.791.67mg/KgBenzo(g,h,i)perylene 43-134
1111.861.67mg/KgBenzo(k)fluoranthene 47-132
0.0*0.8801.67mg/KgBenzoic Acid 10-83
83.21.391.67mg/KgBenzyl alcohol 29-122
98.81.651.67mg/KgBis(2-Chloroethoxy)methane 36-121
80.21.341.67mg/KgBis(2-Chloroethyl)ether 31-120
86.81.451.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1021.711.67mg/KgBis(2-ethylhexyl)phthalate 51-133
89.21.491.67mg/Kg4-Bromophenyl phenyl ether 46-124
98.21.641.67mg/KgButyl benzyl phthalate 48-132
98.21.641.67mg/Kg4-Chloro-3-methylphenol 45-122
84.41.411.67mg/Kg4-Chloroaniline 17-106
88.61.481.67mg/Kg2-Chloronaphthalene 41-114
89.81.501.67mg/Kg2-Chlorophenol 34-121
89.21.491.67mg/Kg4-Chlorophenyl phenyl ether 45-121
91.01.521.67mg/KgChrysene 50-124
89.81.501.67mg/KgDibenz(a,h)anthracene 45-134
89.81.501.67mg/KgDibenzofuran 44-120
78.41.311.67mg/Kg1,2-Dichlorobenzene 33-117
77.81.301.67mg/Kg1,3-Dichlorobenzene 30-115
78.41.311.67mg/Kg1,4-Dichlorobenzene 31-115
72.41.211.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 13 of 19* QC Fail Date:12/29/2021 03:16 PM
Page 121 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V13287QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12959
LCS-V12959Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.81.551.67mg/Kg2,4-Dichlorophenol 40-122
92.81.551.67mg/KgDiethyl phthalate 50-124
91.61.531.67mg/KgDimethyl phthalate 48-124
1041.731.67mg/Kg2,4-Dimethylphenol 30-127
1041.741.67mg/KgDi-n-butyl phthalate 51-128
0.0*1.411.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
0.0*1.331.67mg/Kg2,4-Dinitrophenol 27-129
96.41.611.67mg/Kg2,4-Dinitrotoluene 48-126
97.61.631.67mg/Kg2,6-Dinitrotoluene 46-124
1091.821.67mg/KgDi-n-Octyl Phthalate 45-140
94.61.581.67mg/KgFluoranthene 50-127
91.61.531.67mg/KgFluorene 43-125
86.81.451.67mg/KgHexachlorobenzene 45-122
80.81.351.67mg/KgHexachlorobutadiene 32-123
62.81.051.67mg/KgHexachlorocyclopentadiene 32-117
77.81.301.67mg/KgHexachloroethane 28-117
1051.751.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
83.21.391.67mg/KgIsophorone 30-122
85.61.431.67mg/Kg1-Methylnaphthalene 40-119
86.21.441.67mg/Kg2-Methylnaphthalene 38-122
91.01.521.67mg/Kg2-Methylphenol 32-122
78.41.311.67mg/Kg3&4 Methylphenol 34-119
82.01.371.67mg/KgNaphthalene 35-123
93.41.561.67mg/Kg2-Nitroaniline 44-127
91.61.531.67mg/Kg3-Nitroaniline 33-119
87.41.461.67mg/Kg4-Nitroaniline 63-147
83.21.391.67mg/KgNitrobenzene 34-122
Page 14 of 19* QC Fail Date:12/29/2021 03:16 PM
Page 122 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V13287QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12959
LCS-V12959Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.81.401.67mg/Kg2-Nitrophenol 36-123
96.41.611.67mg/Kg4-Nitrophenol 30-132
69.41.161.67mg/KgN-Nitrosodimethylamine 10-146
1111.851.67mg/KgN-Nitrosodiphenylamine 38-127
86.21.441.67mg/KgN-Nitroso-di-n-propylamine 36-120
92.21.541.67mg/KgPentachlorophenol 25-133
94.01.571.67mg/KgPhenanthrene 50-121
88.01.471.67mg/KgPhenol 34-121
97.01.621.67mg/KgPyrene 47-127
61.01.021.67mg/KgPyridine 10-80
79.61.331.67mg/Kg1,2,4-Trichlorobenzene 34-118
93.41.561.67mg/Kg2,4,5-Trichlorophenol 41-124
91.01.521.67mg/Kg2,4,6-Trichlorophenol 39-126
76.62-Fluorobiphenyl (S)44-115
81.32-Fluorophenol (S)35-115
69.4Nitrobenzene-d5 (S)37-122
80.24-Terphenyl-d14 (S)54-127
80.72,4,6-Tribromophenol (S)39-132
78.0Phenol-d5 (S)34-121
V 90743-MS-V12959 V 90743-MSD-V12959Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.21 72.81.401.671.66<0.116mg/KgAcenaphthene 83.8 40-123 14.5 20
1.24 74.61.451.671.66<0.105mg/KgAcenaphthylene 86.8 32-132 15.6 20
1.10 66.21.311.671.66<0.152mg/KgAniline 78.4 12-197 17.4 20
Page 15 of 19Date:12/29/2021 03:16 PM
Page 123 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V13287QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12959
V 90743-MS-V12959 V 90743-MSD-V12959Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.26 75.91.431.671.66<0.143mg/KgAnthracene 85.6 47-123 12.6 20
1.21 72.81.461.671.66<0.139mg/KgBenzo(a)anthracene 87.4 49-126 18.7 20
1.71 1032.011.671.66<0.147mg/KgBenzo(a)pyrene 120 45-129 16.1 20
1.51 90.91.801.671.66<0.146mg/KgBenzo(b)fluoranthene 108 45-132 17.5 20
1.52 91.51.761.671.66<0.136mg/KgBenzo(g,h,i)perylene 105 43-134 14.6 20
1.49 89.71.611.671.66<0.137mg/KgBenzo(k)fluoranthene 96.4 47-132 7.7 20
<0.580 0.0*<0.5801.671.66<0.580mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.16 69.81.311.671.66<0.105mg/KgBenzyl alcohol 78.4 29-122 12.1 20
1.35 81.31.381.671.66<0.118mg/KgBis(2-Chloroethoxy)methane 82.6 36-121 2.1 20
1.23 74.01.411.671.66<0.107mg/KgBis(2-Chloroethyl)ether 84.4 31-120 13.6 20
1.22 73.41.401.671.66<0.136mg/KgBis(2-Chloroisopropyl)ether 83.8 33-131 13.7 20
1.35 81.31.681.671.66<0.120mg/KgBis(2-ethylhexyl)phthalate 101 51-133 21.7*20
1.18 71.01.421.671.66<0.109mg/Kg4-Bromophenyl phenyl ether 85.0 46-124 18.4 20
1.35 81.31.651.671.66<0.113mg/KgButyl benzyl phthalate 98.8 48-132 20.0 20
1.31 78.91.381.671.66<0.092mg/Kg4-Chloro-3-methylphenol 82.6 45-122 5.2 20
1.06 63.81.131.671.66<0.112mg/Kg4-Chloroaniline 67.6 17-106 6.3 20
1.21 72.81.391.671.66<0.116mg/Kg2-Chloronaphthalene 83.2 41-114 13.8 20
1.26 75.91.381.671.66<0.098mg/Kg2-Chlorophenol 82.6 34-121 9.0 20
1.16 69.81.361.671.66<0.126mg/Kg4-Chlorophenyl phenyl ether 81.4 45-121 15.8 20
1.24 74.61.421.671.66<0.142mg/KgChrysene 85.0 50-124 13.5 20
1.32 79.51.511.671.66<0.230mg/KgDibenz(a,h)anthracene 90.4 45-134 13.4 20
1.19 71.61.411.671.66<0.119mg/KgDibenzofuran 84.4 44-120 16.9 20
1.08 65.01.241.671.66<0.094mg/Kg1,2-Dichlorobenzene 74.2 33-117 13.7 20
1.10 66.21.221.671.66<0.097mg/Kg1,3-Dichlorobenzene 73.0 30-115 10.3 20
1.07 64.41.221.671.66<0.097mg/Kg1,4-Dichlorobenzene 73.0 31-115 13.1 20
0.902 54.31.271.671.66<0.147mg/Kg3,3'-Dichlorobenzidine 76.0 22-121 33.8*20
Page 16 of 19* QC Fail Date:12/29/2021 03:16 PM
Page 124 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V13287QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12959
V 90743-MS-V12959 V 90743-MSD-V12959Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.28 77.11.301.671.66<0.095mg/Kg2,4-Dichlorophenol 77.8 40-122 1.5 20
1.19 71.61.401.671.66<0.180mg/KgDiethyl phthalate 83.8 50-124 16.2 20
1.20 72.21.411.671.66<0.174mg/KgDimethyl phthalate 84.4 48-124 16.0 30
1.35 81.31.371.671.66<0.108mg/Kg2,4-Dimethylphenol 82.0 30-127 1.4 20
1.35 81.31.591.671.66<0.107mg/KgDi-n-butyl phthalate 95.2 51-128 16.3 20
0.983 0.0*1.201.671.66<0.240mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
0.912 0.0*1.101.671.66<0.520mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.20 72.21.441.671.66<0.096mg/Kg2,4-Dinitrotoluene 86.2 48-126 18.1 20
1.27 76.51.461.671.66<0.108mg/Kg2,6-Dinitrotoluene 87.4 46-124 13.9 20
1.52 91.51.851.671.66<0.143mg/KgDi-n-Octyl Phthalate 111 45-140 19.5 20
1.20 72.21.401.671.66<0.123mg/KgFluoranthene 83.8 50-127 15.3 20
1.19 71.61.411.671.66<0.128mg/KgFluorene 84.4 43-125 16.9 20
1.10 66.21.351.671.66<0.106mg/KgHexachlorobenzene 80.8 45-122 20.4*20
1.16 69.81.141.671.66<0.097mg/KgHexachlorobutadiene 68.2 32-123 1.7 20
0.718 43.20.8131.671.66<0.157mg/KgHexachlorocyclopentadiene 48.6 32-117 12.4 20
1.08 65.01.241.671.66<0.079mg/KgHexachloroethane 74.2 28-117 13.7 20
1.50 90.31.671.671.66<0.179mg/KgIndeno(1,2,3-cd)pyrene 100 45-133 10.7 20
1.13 68.01.141.671.66<0.191mg/KgIsophorone 68.2 30-122 0.8 20
1.19 71.61.191.671.66<0.106mg/Kg1-Methylnaphthalene 71.2 40-119 0.0 20
1.19 71.61.231.671.66<0.100mg/Kg2-Methylnaphthalene 73.6 38-122 3.3 20
1.25 75.31.461.671.66<0.097mg/Kg2-Methylphenol 87.4 32-122 15.4 20
1.07 64.41.251.671.66<0.084mg/Kg3&4 Methylphenol 74.8 34-119 15.5 20
1.18 71.01.201.671.66<0.144mg/KgNaphthalene 71.8 35-123 1.6 20
1.26 75.91.451.671.66<0.096mg/Kg2-Nitroaniline 86.8 44-127 14.0 20
1.20 72.21.441.671.66<0.120mg/Kg3-Nitroaniline 86.2 33-119 18.1 20
1.08 65.01.271.671.66<0.093mg/Kg4-Nitroaniline 76.0 63-147 16.1 20
Page 17 of 19* QC Fail Date:12/29/2021 03:16 PM
Page 125 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V13287QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V12959
V 90743-MS-V12959 V 90743-MSD-V12959Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.15 69.21.151.671.66<0.116mg/KgNitrobenzene 68.8 34-122 0.0 20
1.09 65.61.151.671.66<0.088mg/Kg2-Nitrophenol 68.8 32-123 5.3 20
1.21 72.81.461.671.66<0.117mg/Kg4-Nitrophenol 87.4 30-132 18.7 20
1.01 60.80.9921.671.66<0.263mg/KgN-Nitrosodimethylamine 59.4 10-146 1.7 30
1.47 88.51.751.671.66<0.181mg/KgN-Nitrosodiphenylamine 105 38-127 17.3 20
1.16 69.81.341.671.66<0.118mg/KgN-Nitroso-di-n-propylamine 80.2 36-120 14.4 20
1.14 68.61.371.671.66<0.347mg/KgPentachlorophenol 82.0 25-133 18.3 20
1.24 74.61.461.671.66<0.208mg/KgPhenanthrene 87.4 50-121 16.2 20
1.21 72.81.471.671.66<0.112mg/KgPhenol 88.0 34-121 19.4 20
1.33 80.11.571.671.66<0.134mg/KgPyrene 94.0 47-127 16.5 20
0.773 46.50.7041.671.66<0.079mg/KgPyridine 42.1 10-80 9.3 20
1.12 67.41.141.671.66<0.107mg/Kg1,2,4-Trichlorobenzene 68.2 34-118 1.7 20
1.18 71.01.451.671.66<0.096mg/Kg2,4,5-Trichlorophenol 86.8 41-124 20.5*20
1.17 70.41.371.671.66<0.096mg/Kg2,4,6-Trichlorophenol 82.0 39-126 15.7 20
63.82-Fluorobiphenyl (S)70.6 44-115
70.22-Fluorophenol (S)75.6 35-115
62.0Nitrobenzene-d5 (S)58.4 37-122
68.64-Terphenyl-d14 (S)77.2 54-127
58.22,4,6-Tribromophenol (S)69.6 39-132
65.7Phenol-d5 (S)72.3 34-121
Page 18 of 19* QC Fail Date:12/29/2021 03:16 PM
Page 126 of 129
Quality Control Data
21-350-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN.008
Dry Weight Determination
SW-DRYWT
V13104QC Analytical Batch:
Analysis Method:
Analysis Description:
V 90805-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/21/21 17:166.718.720.0%Moisture
V 90831-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/21/21 17:162.317.216.8%Moisture
Page 19 of 19Date:12/29/2021 03:16 PM
Page 127 of 129
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-350-0013
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.0 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Sarah J. Locklear Date & Time:12/16/2021 13:24:11
Special precautions or instructions included?
Comments:
Page 128 of 129
Page 129 of 129