23057_CharlotteVan&Storage_Soil Export Options EX7-EX8 Package_20211118

November 18, 2021
Sent Via E-mail
Mr. Jeffrey W. Harris
Lennar Multifamily Communities, LLC 500 East Morehead Street, Suite 300 Charlotte, North Carolina 28202 [e-mail]

Subject: Brownfields Soil Management Options for EX-7 and EX-8 Charlotte Van & Storage Co. Brownfield Property Charlotte, Mecklenburg County Brownfields Project No. 23057-19-060

Dear Mr. Harris: The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received a request to export soil from the Charlotte Van & Storage Co. Brownfields Property. This request
was submitted on your behalf by Ms. Haley Martin, PG of Hart & Hickman, PC via email on
November 18, 2021, and requests approval to export approximately 215 cubic yards of soil to a beneficial fill reuse site known as the Fleet Maintenance facility in Mt. Holly, North Carolina. DEQ Brownfields provided letters approving soil export options on September 7, 2021, September 15, 2021, and on October 11, 2021, in response to previous requests.

For this request, DEQ Brownfields reviewed the November 18, 2021, Data Summary Package which includes analytical results for soil samples EX-7 and EX-8, as well as soil analytical data from the proposed Fleet Maintenance receiving facility.
Based on our review of the data, the DEQ Brownfield determines that soils may be exported as
outlined in the table below. Please note that the “Beneficial Fill” option listed in the table below is specifically approved for the Fleet Maintenance facility in Mt. Holly, NC. Other Beneficial Fill and Land Clearing & Inert Debris Landfill (LCID) options may be available; however, DEQ requires that the receiving facility be identified and approved prior to export. The receiving
facility should have metals concentrations which are consistent with those from the Brownfields
Property. Similarly, many site soils, including those with impacts, may be suitable for use at another Brownfields Property that has similar impacts.
Mr. Jeffery Harris November 18, 2021 Page 2

Upon determination of the export facility, whether another Brownfields Property, LCID, or
another beneficial fill reuse, please contact us and we will assist you in determining if additional sampling is needed for the receiving facility.
LOCATION ID DEPTH (Ft)1 MANAGEMENT OPTIONS2
EX-7 0-5 BFILL, LCID, CDLF, MSWLF
EX-8 0-10 BFILL, LCID, CDLF, MSWLF
Notes: 1) Depth listed is total depth of available analytical data. Additional sampling would potentially
be required beyond these depths prior to export. 2) BFILL= Beneficial Fill; LCID = Land Clearing & Inert Debris Landfill; CDLF = Construction & Demolition landfill; MSWLF = Municipal Solid Waste landfill (MSWLF) facility. Per the Charlotte Van & Storage Co.’s approved Environmental Management Plan (EMP), the soils are to be field screened during excavation prior to export from the property. If unanticipated impacts are identified during excavation, please refer to the EMP for further actions and cease
transfer until appropriate characterization can be completed. In addition, and also in accordance with the site’s approved EMP, an annual Redevelopment Summary Report will be submitted to DEQ Brownfields. Details related to the disposition of this soil including but not limited to, total volume, general description of field screening efforts, etc. should be included with the Redevelopment Summary Report.
Please be advised that this approval does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local entities. If you have questions about this correspondence or require additional information, please feel free to contact Pete Doorn by phone at 984-275-5391 or by email at [e-mail].
Sincerely,
Peter L. Doorn, Project Manager
Brownfields Program Ec: Haley Martin, Hart & Hickman, PC Ralph McGee, Hart & Hickman, PC Tracy Wahl, DEQ Brownfields
1
Doorn, Peter L
From:Haley Martin <[e-mail]>
Sent:Thursday, November 18, 2021 9:05 AM
To:Doorn, Peter L
Cc:Ralph McGee
Subject:RE: [External] 25037-19-060 - Charlotte Van and Storage - In Situ Soil Characterization
Sampling
Attachments:Charlotte Van & Storage Co_Data Summary Package.pdf
Follow Up Flag:Follow up
Flag Status:Completed
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Report Spam.

Good Morning Pete,

Please find the attached data summary package for the Charlotte Van and Storage Brownfields Property. On November
3, 2021, H&H collected two 3-point composite sample (EX-7 and EX-8) in the area of a proposed storm structure in the
eastern portion of the Site and in the area of the future pool located in the north-central portion of the Site. H&H
completed in situ soil characterization assessment activities at the Brownfields property to assist in management of
approximately 215 cubic yards of soil expected to be generated during excavation activities.

The composite soil samples selected for laboratory analyses were collected directly into dedicated laboratory supplied
sample containers, labeled with the date, time, and sample identification, and placed in a laboratory supplied sample
cooler with ice. The samples were submitted to Waypoint Analytical (Waypoint) under standard chain of custody
protocols for analysis of semi volatile organic compounds (SVOCs) by EPA Method 8270 and Resource Conservation and
Recovery Act (RCRA) metals plus hexavalent chromium by EPA Methods 6020/7471/7199. In addition to the composite
soil samples described above, one representative grab soil sample was collected from each characterization area. The
grab soil samples were collected from an undisturbed portion of soil directly into laboratory supplied glassware and
submitted to Waypoint under standard chain of custody protocols for analysis of VOCs by EPA Method 8260.

As noted in the attached data summary package, the analytical results for EX-7 and EX-8 did not identify organic
compounds at concentrations above the Preliminary Soil Remediation Goals (PSRGs) and metals appear to be consistent
with background concentrations for the Site and the Fleet Maintenance facility. The PD would like to transport the
approximate the approximate 215 cubic yards of soil expected to be generated during excavation activities to the Fleet
Maintenance facility.

We appreciate your reviewing this data to assist in keeping the construction schedule on track. Please let us know if you
have any questions or concerns.

Thanks,
Haley

Haley Martin, PG, Project Geologist
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 · Charlotte, NC 28203
Direct: 704-526-2045 · Mobile: [phone]
www.harthickman.com
2

From: Doorn, Peter L <[e-mail]>
Sent: Monday, November 1, 2021 9:17 AM
To: Haley Martin <[e-mail]>
Cc: Ralph McGee <[e-mail]>
Subject: RE: [External] 25037-19-060 - Charlotte Van and Storage - In Situ Soil Characterization Sampling

Haley – thanks for letting me know about the plan for the in-situ soil characterization - that approach looks
sound. When we receive the documentation/data package, I’ll make the review a priority to help keep construction on
track.

Regards,

Pete

Peter L. Doorn
Brownfields Program/DWM/NCDEQ
Mobile: [phone]

Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third
parties.

From: Haley Martin <[e-mail]>
Sent: Monday, November 1, 2021 8:05 AM
To: Doorn, Peter L <[e-mail]>
Cc: Ralph McGee <[e-mail]>
Subject: [External] 25037-19-060 - Charlotte Van and Storage - In Situ Soil Characterization Sampling

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.

Good Morning Pete,

The PD at the Charlotte Van and Storage Brownfields property (BPN 23057-19-060) intends to remove excess soil
expected to be generated during the installation of a storm structure in the eastern portion of the Site and in the area of
the future pool located in the north-central portion of the Site. H&H will complete in situ soil characterization
assessment activities at the Brownfields property to assist in management of approximately 215 cubic yards of soil
expected to be generated during excavation activities. Areas that will be excavated are shown in yellow shading in the
attached Figure along with the proposed approximate extent and depths of the excavation areas. Note that the area
and depth of planned cut for excavation has been calculated and approximately 130 cubic yards of soil will be removed
from the proposed pool and approximately 83 cubic yards of excess soil will be removed from the area of the storm
structure.

In accordance with the DEQ-approved EMP, a minimum of 3 aliquot soil borings will be advance in each excavation area.
Continuous soil samples will be collected from each boring advanced in an excavation area. The soil samples will be
combined and homogenized to form one composite soil sample representative of soil that will be generated during
excavation activities in that area. The composite soil samples selected for laboratory analysis will be placed directly into
laboratory supplied glassware, labeled with the sample ID, the date, and requested analysis and placed in a laboratory
supplied cooler with ice. The samples will be delivered to a NC certified laboratory under standard chain of custody
protocols for analysis of semi-volatile organic compounds (SVOCs) by EPA Method 8270 and RCRA metals plus
hexavalent chromium by EPA Methods 6020/7471/7199. In addition, one grab soil sample will be collected in each
3
excavation area from an undisturbed portion of an aliquot soil sample and submitted to laboratory for analysis of VOCs
by EPA method 8260.

If results of the above sampling indicate that there are no impacts above acceptable levels, the PD for the Charlotte Van
and Storage site would like to export the topsoil to Fleet Maintenance facility on Lucia-Riverbend Highway in Mt.
Holly. We will provide a figure depicting the areas of excavation relative to the soil boring locations and a summary of
the analytical results to DEQ for review and approval prior to transporting off the Brownfields property.

We will send the documentation above and a data summary package as soon as they are available. In the meantime,
please let us know if you have questions or require additional information.

Thank you,
Haley

Haley Martin, PG, Project Geologist
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 · Charlotte, NC 28203
Direct: 704-526-2045 · Mobile: [phone]
www.harthickman.com

Table 1
Summary of Soil Analytical Data
Charlotte Van & Storage Co.
Verbena Street and Gilead Street
Charlotte, North Carolina
H&H Job No. LEN-008
Sample ID SB-1 SB-2 SB-3
Sample Type Composite Grab Composite Grab
Depth (ft bgs)0-5 2-3 0-10 8-10
Date Range Range Mean
Units
VOCs (8260D)
Acetone NA 0.003 J NA <0.003 NA NA NA 25 12,000 140,000 -- -- --
Ethanol NA <0.018 NA 0.030 J NA NA NA NE NE NE -- -- --
SVOCs (8270E)ALL BDLs NA ALL BDLs NA NA NA NA -- -- -- -- -- --
Metals (6020/7471/7199)
Arsenic 2.72 NA 0.266 J NA 1.11 J 0.391 J 3.52 5.8 0.68 3.0 1.28 - 3.03 1.0 - 18 4.8
Barium 32.3 NA 115 NA 66.2 44.3 68.7 580 3,100 47,000 38.1 - 94.6 50 - 1,000 356
Cadmium <0.0708 NA <0.0774 NA <0.0655 <0.0649 0.207 J 3.0 14 200 ND - 0.434 1.0 - 10* 4.3
Chromium (total) 53.6 NA 36.2 NA 80.8 30.9 25.7 ---- --47.1 - 59.9 7.0 - 300 65
Hexavalent Chromium <0.26 NA <0.26 NA 1.3 <0.26 <0.26 3.8 0.31 6.5 ND - 0.540 NS NS
Trivalent Chromium 53.6 NA 36.2 NA 79.5 30.9 25.7 360,000 23,000 350,000 47.1 - 59.4 NS NS
Lead 21.6 NA 2.45 NA 6.13 6.3 10.3 270 400 800 7.33 - 11.6 ND - 50 16
Mercury 0.0473 NA <0.0169 NA 0.0155 J <0.0142 <0.0156 NE 4.7 70 0.0365 - 0.0502 0.03 - 0.52 0.121
Selenium <1.16 NA <1.27 NA 10.8 J <1.06 <1.47 2.1 78 1,200 0.586 - 1.04 <0.1 - 0.8 0.42
Silver <0.0528 NA <0.0577 NA <0.0488 <0.0484 <0.0534 3.4 78 1,200 ND ND - 5.0 NS
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021)
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Compound concentrations are reported to the laboratory method detection limits.
Aside from metals, only those compounds detected in at least one sample are shown above.
Laboratory analytical methods are shown in parentheses.
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface
NS= not specified; NA = not analyzed; -- = not applicable; NE = not established; ND = not detected at concentration above laboratory detection limit
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
Screening Criteria EX-7 EX-8
11/3/2021
Sample Location Proposed Swimming Pool Proposed Storm Structure Fleet Maintenance Facility
Protection of
Groundwater
PSRGs (1)
Residential
PSRGs (1)
1-3
8/27/2021
mg/kg
Industrial/
Commercial
PSRGs (1)
Site-Specific
Background
Metals in Soil
Background
Metals (2)Grab
https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Lennar (LEN)/LEN‐008 Verbena Assemblage/In Situ Assessment/Tables/Charlotte Van & Storage Co. (LEN‐008) Data Tables aem.xlsx
11/18/2021
Table 1 (Page 1 of 1)
Hart & Hickman, PC
REVISION NO. 0
JOB NO. LEN-008
DATE: 11-15-21
FIGURE NO. 2
CHARLOTTE VAN & STORAGE CO.
VERBENA STREET AND GILEAD STREET
CHARLOTTE, NORTH CAROLINA
IN SITU SOIL CHARACTERIZATION
SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
FORMER SITE BUILDING FOOTPRINT
IN SITU SOIL CHARACTERIZATION AREA
ALIQUOT SOIL BORING LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
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NOTES:
1.PARCEL DATA AND AERIAL IMAGERY OBTAINED FROM
MECKLENBURG COUNTY GIS (2021).
2.SOIL SAMPLES EX-1 THROUGH EX-6 COLLECTED BY
H&H ON AUGUST 5, 2021.
3. SOIL SAMPLES EX-7 AND E-8 COLLECTED BY H&H ON NOVEMBER 3, 2021.
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Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/11/2021
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 21-306-0024 Client Project Description: LEN-008
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/2/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 54
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-306-0024
Page 2 of 54
Report Number:
Sample Summary Table
Client Project Description:
21-306-0024
LEN-008
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
11/02/2021 08:30Solids 98618 EX-7 11/02/2021 14:50 7199
11/02/2021 08:30Solids 98618 EX-7 11/02/2021 14:50
11/02/2021 09:30Solids 98619 EX-8 11/02/2021 14:50 7199
11/02/2021 09:30Solids 98619 EX-8 11/02/2021 14:50
: Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 54
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-306-0024
Report Limit
Project:LEN-008
V 98618EX-7
2.72 11/06/2021 16:496020BArsenicmg/Kg - dry 0.121
32.3 11/06/2021 16:496020BBariummg/Kg - dry 1.80
53.6 11/06/2021 16:496020BChromiummg/Kg - dry 0.373
21.6 11/06/2021 16:496020BLeadmg/Kg - dry 0.180
0.0473 11/09/2021 12:047471BMercury (Total)mg/Kg - dry 0.0155
J0.003 11/03/2021 12:498260DAcetonemg/Kg - dry 0.003
22.4 11/03/2021 16:29SW-DRYWT Moisture %
V 98619EX-8
J0.266 11/06/2021 16:566020BArsenicmg/Kg - dry 0.132
115 11/06/2021 16:566020BBariummg/Kg - dry 1.97
36.2 11/06/2021 16:566020BChromiummg/Kg - dry 0.408
2.45 11/06/2021 16:566020BLeadmg/Kg - dry 0.197
J0.030 11/03/2021 13:178260DEthanolmg/Kg - dry 0.019
29.0 11/03/2021 16:29SW-DRYWT Moisture %
Page 4 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-7
98618 Matrix:
11/2/2021 8:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.4 %Moisture 1 11/03/21 16:29 SW-DRYWTSMW
2.72 mg/Kg - dry 0.121 1.29Arsenic 10 11/06/21 16:49 6020BEDV
32.3 mg/Kg - dry 1.80 12.9Barium 10 11/06/21 16:49 6020BEDV
<0.0708 mg/Kg - dry 0.0708 0.644Cadmium 10 11/06/21 16:49 6020BEDV
53.6 mg/Kg - dry 0.373 1.29Chromium 10 11/06/21 16:49 6020BEDV
21.6 mg/Kg - dry 0.180 1.29
Lead 10 11/06/21 16:49 6020BEDV
0.0473 mg/Kg - dry 0.0155 0.0387Mercury (Total)1 11/09/21 12:04 7471BEDV
<1.16 mg/Kg - dry 1.16 2.58Selenium 10 11/06/21 16:49 6020BEDV
<0.0528 mg/Kg - dry 0.0528 0.644Silver 10 11/06/21 16:49 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 5 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-7
98618 Matrix:
11/2/2021 8:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V11115 11/03/21 08:00
0.003 J mg/Kg - dry 0.003 0.025Acetone 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 11/03/21 12:49 V11116TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 11/03/21 12:49 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 11/03/21 12:49 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 11/03/21 12:49 V11116TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 11/03/21 12:49 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 11/03/21 12:49 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 11/03/21 12:49 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 11/03/21 12:49 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 11/03/21 12:49 V11116TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 11/03/21 12:49 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 11/03/21 12:49 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 11/03/21 12:49 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 11/03/21 12:49 V11116TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 11/03/21 12:49 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 11/03/21 12:49 V11116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-7
98618 Matrix:
11/2/2021 8:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V11115 11/03/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 11/03/21 12:49 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 11/03/21 12:49 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 11/03/21 12:49 V11116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 11/03/21 12:49 V11116TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 11/03/21 12:49 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 11/03/21 12:49 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 11/03/21 12:49 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 11/03/21 12:49 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 11/03/21 12:49 V11116TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 11/03/21 12:49 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 11/03/21 12:49 V11116TBL
<0.018 mg/Kg - dry 0.018 0.322Ethanol 1 11/03/21 12:49 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 11/03/21 12:49 V11116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-7
98618 Matrix:
11/2/2021 8:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V11115 11/03/21 08:00
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 11/03/21 12:49 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 11/03/21 12:49 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 11/03/21 12:49 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 11/03/21 12:49 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 11/03/21 12:49 V11116TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 11/03/21 12:49 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 11/03/21 12:49 V11116TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 11/03/21 12:49 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 11/03/21 12:49 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 11/03/21 12:49 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 11/03/21 12:49 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 11/03/21 12:49 V11116TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 11/03/21 12:49 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 11/03/21 12:49 V11116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-7
98618 Matrix:
11/2/2021 8:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V11115 11/03/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 11/03/21 12:49 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 11/03/21 12:49 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 11/03/21 12:49 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 11/03/21 12:49 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 11/03/21 12:49 V11116TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 11/03/21 12:49 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 11/03/21 12:49 V11116
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%11/03/21 12:491 TBL V11116
Surrogate: Dibromofluoromethane 105 Limits: 84-123%11/03/21 12:491 TBL V11116
Surrogate: Toluene-d8 105 Limits: 76-129%11/03/21 12:491 TBL V11116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V11087 11/03/21 08:50
<0.149 mg/Kg - dry 0.149 0.851Acenaphthene 1 11/04/21 16:35 V11189JMV
<0.135 mg/Kg - dry 0.135 0.851Acenaphthylene 1 11/04/21 16:35 V11189JMV
<0.195 mg/Kg - dry 0.195 0.851Aniline 1 11/04/21 16:35 V11189JMV
<0.184 mg/Kg - dry 0.184 0.851Anthracene 1 11/04/21 16:35 V11189JMV
<0.179 mg/Kg - dry 0.179 0.851
Benzo(a)anthracene 1 11/04/21 16:35 V11189JMV
<0.189 mg/Kg - dry 0.189 0.851Benzo(a)pyrene 1 11/04/21 16:35 V11189JMV
<0.188 mg/Kg - dry 0.188 0.851Benzo(b)fluoranthene 1 11/04/21 16:35 V11189JMV
<0.175 mg/Kg - dry 0.175 0.851Benzo(g,h,i)perylene 1 11/04/21 16:35 V11189JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-7
98618 Matrix:
11/2/2021 8:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V11087 11/03/21 08:50
<0.176 mg/Kg - dry 0.176 0.851Benzo(k)fluoranthene 1 11/04/21 16:35 V11189JMV
<0.747 mg/Kg - dry 0.747 2.58Benzoic Acid 1 11/04/21 16:35 V11189JMV
<0.135 mg/Kg - dry 0.135 0.851Benzyl alcohol 1 11/04/21 16:35 V11189JMV
<0.152 mg/Kg - dry 0.152 0.851Bis(2-Chloroethoxy)methane 1 11/04/21 16:35 V11189JMV
<0.137 mg/Kg - dry 0.137 0.851Bis(2-Chloroethyl)ether 1 11/04/21 16:35 V11189JMV
<0.175 mg/Kg - dry 0.175 0.426Bis(2-Chloroisopropyl)ether 1 11/04/21 16:35 V11189JMV
<0.154 mg/Kg - dry 0.154 0.851Bis(2-ethylhexyl)phthalate 1 11/04/21 16:35 V11189JMV
<0.140 mg/Kg - dry 0.140 0.8514-Bromophenyl phenyl ether 1 11/04/21 16:35 V11189JMV
<0.145 mg/Kg - dry 0.145 0.426
Butyl benzyl phthalate 1 11/04/21 16:35 V11189JMV
<0.119 mg/Kg - dry 0.119 0.8514-Chloro-3-methylphenol 1 11/04/21 16:35 V11189JMV
<0.144 mg/Kg - dry 0.144 0.4264-Chloroaniline 1 11/04/21 16:35 V11189JMV
<0.149 mg/Kg - dry 0.149 0.8512-Chloronaphthalene 1 11/04/21 16:35 V11189JMV
<0.126 mg/Kg - dry 0.126 0.8512-Chlorophenol 1 11/04/21 16:35 V11189JMV
<0.162 mg/Kg - dry 0.162 1.294-Chlorophenyl phenyl ether 1 11/04/21 16:35 V11189JMV
<0.182 mg/Kg - dry 0.182 0.851Chrysene 1 11/04/21 16:35 V11189JMV
<0.296 mg/Kg - dry 0.296 0.851
Dibenz(a,h)anthracene 1 11/04/21 16:35 V11189JMV
<0.153 mg/Kg - dry 0.153 0.851Dibenzofuran 1 11/04/21 16:35 V11189JMV
<0.121 mg/Kg - dry 0.121 0.8511,2-Dichlorobenzene 1 11/04/21 16:35 V11189JMV
<0.125 mg/Kg - dry 0.125 0.8511,3-Dichlorobenzene 1 11/04/21 16:35 V11189JMV
<0.126 mg/Kg - dry 0.126 0.4261,4-Dichlorobenzene 1 11/04/21 16:35 V11189JMV
<0.189 mg/Kg - dry 0.189 0.8513,3'-Dichlorobenzidine 1 11/04/21 16:35 V11189JMV
<0.123 mg/Kg - dry 0.123 0.8512,4-Dichlorophenol 1 11/04/21 16:35 V11189JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-7
98618 Matrix:
11/2/2021 8:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V11087 11/03/21 08:50
<0.231 mg/Kg - dry 0.231 0.851Diethyl phthalate 1 11/04/21 16:35 V11189JMV
<0.224 mg/Kg - dry 0.224 0.851Dimethyl phthalate 1 11/04/21 16:35 V11189JMV
<0.139 mg/Kg - dry 0.139 0.4262,4-Dimethylphenol 1 11/04/21 16:35 V11189JMV
<0.137 mg/Kg - dry 0.137 0.851Di-n-butyl phthalate 1 11/04/21 16:35 V11189JMV
<0.309 mg/Kg - dry 0.309 1.934,6-Dinitro-2-methylphenol 1 11/04/21 16:35 V11189JMV
<0.670 mg/Kg - dry 0.670 1.932,4-Dinitrophenol 1 11/04/21 16:35 V11189JMV
<0.124 mg/Kg - dry 0.124 0.8512,4-Dinitrotoluene 1 11/04/21 16:35 V11189JMV
<0.139 mg/Kg - dry 0.139 0.8512,6-Dinitrotoluene 1 11/04/21 16:35 V11189JMV
<0.184 mg/Kg - dry 0.184 0.426
Di-n-Octyl Phthalate 1 11/04/21 16:35 V11189JMV
<0.158 mg/Kg - dry 0.158 0.851Fluoranthene 1 11/04/21 16:35 V11189JMV
<0.164 mg/Kg - dry 0.164 0.851Fluorene 1 11/04/21 16:35 V11189JMV
<0.136 mg/Kg - dry 0.136 0.851Hexachlorobenzene 1 11/04/21 16:35 V11189JMV
<0.125 mg/Kg - dry 0.125 0.851Hexachlorobutadiene 1 11/04/21 16:35 V11189JMV
<0.202 mg/Kg - dry 0.202 0.851Hexachlorocyclopentadiene 1 11/04/21 16:35 V11189JMV
<0.102 mg/Kg - dry 0.102 0.851Hexachloroethane 1 11/04/21 16:35 V11189JMV
<0.230 mg/Kg - dry 0.230 0.851
Indeno(1,2,3-cd)pyrene 1 11/04/21 16:35 V11189JMV
<0.246 mg/Kg - dry 0.246 0.851Isophorone 1 11/04/21 16:35 V11189JMV
<0.136 mg/Kg - dry 0.136 0.8511-Methylnaphthalene 1 11/04/21 16:35 V11189JMV
<0.128 mg/Kg - dry 0.128 0.8512-Methylnaphthalene 1 11/04/21 16:35 V11189JMV
<0.125 mg/Kg - dry 0.125 0.8512-Methylphenol 1 11/04/21 16:35 V11189JMV
<0.109 mg/Kg - dry 0.109 0.8513&4 Methylphenol 1 11/04/21 16:35 V11189JMV
<0.185 mg/Kg - dry 0.185 0.851Naphthalene 1 11/04/21 16:35 V11189JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-7
98618 Matrix:
11/2/2021 8:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V11087 11/03/21 08:50
<0.124 mg/Kg - dry 0.124 0.8512-Nitroaniline 1 11/04/21 16:35 V11189JMV
<0.154 mg/Kg - dry 0.154 0.8513-Nitroaniline 1 11/04/21 16:35 V11189JMV
<0.120 mg/Kg - dry 0.120 0.4264-Nitroaniline 1 11/04/21 16:35 V11189JMV
<0.149 mg/Kg - dry 0.149 0.426Nitrobenzene 1 11/04/21 16:35 V11189JMV
<0.114 mg/Kg - dry 0.114 0.8512-Nitrophenol 1 11/04/21 16:35 V11189JMV
<0.150 mg/Kg - dry 0.150 0.8514-Nitrophenol 1 11/04/21 16:35 V11189JMV
<0.338 mg/Kg - dry 0.338 0.851N-Nitrosodimethylamine 1 11/04/21 16:35 V11189JMV
<0.233 mg/Kg - dry 0.233 0.851N-Nitrosodiphenylamine 1 11/04/21 16:35 V11189JMV
<0.152 mg/Kg - dry 0.152 0.851
N-Nitroso-di-n-propylamine 1 11/04/21 16:35 V11189JMV
<0.447 mg/Kg - dry 0.447 1.29Pentachlorophenol 1 11/04/21 16:35 V11189JMV
<0.268 mg/Kg - dry 0.268 0.851Phenanthrene 1 11/04/21 16:35 V11189JMV
<0.144 mg/Kg - dry 0.144 0.851Phenol 1 11/04/21 16:35 V11189JMV
<0.172 mg/Kg - dry 0.172 0.851Pyrene 1 11/04/21 16:35 V11189JMV
<0.102 mg/Kg - dry 0.102 0.426Pyridine 1 11/04/21 16:35 V11189JMV
<0.137 mg/Kg - dry 0.137 0.8511,2,4-Trichlorobenzene 1 11/04/21 16:35 V11189JMV
<0.124 mg/Kg - dry 0.124 0.851
2,4,5-Trichlorophenol 1 11/04/21 16:35 V11189JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-7
98618 Matrix:
11/2/2021 8:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V11087 11/03/21 08:50
<0.124 mg/Kg - dry 0.124 0.8512,4,6-Trichlorophenol 1 11/04/21 16:35 V11189JMV
Surrogate: Phenol-d5 96.1 Limits: 34-121%11/04/21 16:351 JMV V11189
Surrogate: 2-Fluorobiphenyl 96.4 Limits: 44-115%11/04/21 16:351 JMV V11189
Surrogate: 2-Fluorophenol 101 Limits: 35-115%11/04/21 16:351 JMV V11189
Surrogate: Nitrobenzene-d5 76.0 Limits: 37-122%11/04/21 16:351 JMV V11189
Surrogate: 4-Terphenyl-d14 104 Limits: 54-127%11/04/21 16:351 JMV V11189
Surrogate: 2,4,6-Tribromophenol 101 Limits: 39-132%11/04/21 16:351 JMV V11189
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-8
98619 Matrix:
11/2/2021 9:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
29.0 %Moisture 1 11/03/21 16:29 SW-DRYWTSMW
0.266 J mg/Kg - dry 0.132 1.41Arsenic 10 11/06/21 16:56 6020BEDV
115 mg/Kg - dry 1.97 14.1Barium 10 11/06/21 16:56 6020BEDV
<0.0774 mg/Kg - dry 0.0774 0.704Cadmium 10 11/06/21 16:56 6020BEDV
36.2 mg/Kg - dry 0.408 1.41Chromium 10 11/06/21 16:56 6020BEDV
2.45 mg/Kg - dry 0.197 1.41
Lead 10 11/06/21 16:56 6020BEDV
<0.0169 mg/Kg - dry 0.0169 0.0423Mercury (Total)1 11/09/21 12:07 7471BEDV
<1.27 mg/Kg - dry 1.27 2.82Selenium 10 11/06/21 16:56 6020BEDV
<0.0577 mg/Kg - dry 0.0577 0.704Silver 10 11/06/21 16:56 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 14 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-8
98619 Matrix:
11/2/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V11115 11/03/21 08:00
<0.003 mg/Kg - dry 0.003 0.028Acetone 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.028Acrolein 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.028Acrylonitrile 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 11/03/21 13:17 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 11/03/21 13:17 V11116TBL
<0.002 mg/Kg - dry 0.002 0.014
Bromomethane 1 11/03/21 13:17 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 11/03/21 13:17 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 11/03/21 13:17 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 11/03/21 13:17 V11116TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 11/03/21 13:17 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.007Chlorobenzene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007
Chlorodibromomethane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 11/03/21 13:17 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 11/03/21 13:17 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 11/03/21 13:17 V11116TBL
<0.0005 mg/Kg - dry 0.0005 0.0074-Chlorotoluene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 11/03/21 13:17 V11116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-8
98619 Matrix:
11/2/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V11115 11/03/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,2-Dibromoethane 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 11/03/21 13:17 V11116TBL
<0.0004 mg/Kg - dry 0.0004 0.0071,2-Dichlorobenzene 1 11/03/21 13:17 V11116TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,3-Dichlorobenzene 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,4-Dichlorobenzene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.014Dichlorodifluoromethane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007
1,2-Dichloroethane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 11/03/21 13:17 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007
1,1-Dichloropropene 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 11/03/21 13:17 V11116TBL
0.030 J mg/Kg - dry 0.019 0.352Ethanol 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.070Ethyl Tertiary Butyl Ether (ETBE)1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 11/03/21 13:17 V11116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-8
98619 Matrix:
11/2/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V11115 11/03/21 08:00
<0.0009 mg/Kg - dry 0.0009 0.014n-Hexane 1 11/03/21 13:17 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.0282-Hexanone 1 11/03/21 13:17 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.007Isopropylbenzene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 11/03/21 13:17 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.028Methyl Ethyl Ketone (MEK)1 11/03/21 13:17 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 11/03/21 13:17 V11116TBL
<0.021 mg/Kg - dry 0.021 0.0284-Methyl-2-Pentanone 1 11/03/21 13:17 V11116TBL
<0.002 mg/Kg - dry 0.002 0.014Methylene Chloride 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.014
Naphthalene 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 11/03/21 13:17 V11116TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 11/03/21 13:17 V11116TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 11/03/21 13:17 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.007Toluene 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.014
1,2,3-Trichlorobenzene 1 11/03/21 13:17 V11116TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2,4-Trichlorobenzene 1 11/03/21 13:17 V11116TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 11/03/21 13:17 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 11/03/21 13:17 V11116TBL
<0.002 mg/Kg - dry 0.002 0.014Trichlorofluoromethane 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 11/03/21 13:17 V11116TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-8
98619 Matrix:
11/2/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V11115 11/03/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 11/03/21 13:17 V11116TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 11/03/21 13:17 V11116TBL
<0.0006 mg/Kg - dry 0.0006 0.014Vinyl Acetate 1 11/03/21 13:17 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 11/03/21 13:17 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 11/03/21 13:17 V11116TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 11/03/21 13:17 V11116TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 11/03/21 13:17 V11116
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%11/03/21 13:171 TBL V11116
Surrogate: Dibromofluoromethane 105 Limits: 84-123%11/03/21 13:171 TBL V11116
Surrogate: Toluene-d8 107 Limits: 76-129%11/03/21 13:171 TBL V11116
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V11087 11/03/21 08:50
<0.163 mg/Kg - dry 0.163 0.929Acenaphthene 1 11/04/21 16:57 V11189JMV
<0.147 mg/Kg - dry 0.147 0.929Acenaphthylene 1 11/04/21 16:57 V11189JMV
<0.214 mg/Kg - dry 0.214 0.929Aniline 1 11/04/21 16:57 V11189JMV
<0.201 mg/Kg - dry 0.201 0.929Anthracene 1 11/04/21 16:57 V11189JMV
<0.195 mg/Kg - dry 0.195 0.929
Benzo(a)anthracene 1 11/04/21 16:57 V11189JMV
<0.207 mg/Kg - dry 0.207 0.929Benzo(a)pyrene 1 11/04/21 16:57 V11189JMV
<0.205 mg/Kg - dry 0.205 0.929Benzo(b)fluoranthene 1 11/04/21 16:57 V11189JMV
<0.191 mg/Kg - dry 0.191 0.929Benzo(g,h,i)perylene 1 11/04/21 16:57 V11189JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-8
98619 Matrix:
11/2/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V11087 11/03/21 08:50
<0.192 mg/Kg - dry 0.192 0.929Benzo(k)fluoranthene 1 11/04/21 16:57 V11189JMV
<0.816 mg/Kg - dry 0.816 2.82Benzoic Acid 1 11/04/21 16:57 V11189JMV
<0.147 mg/Kg - dry 0.147 0.929Benzyl alcohol 1 11/04/21 16:57 V11189JMV
<0.166 mg/Kg - dry 0.166 0.929Bis(2-Chloroethoxy)methane 1 11/04/21 16:57 V11189JMV
<0.150 mg/Kg - dry 0.150 0.929Bis(2-Chloroethyl)ether 1 11/04/21 16:57 V11189JMV
<0.191 mg/Kg - dry 0.191 0.464Bis(2-Chloroisopropyl)ether 1 11/04/21 16:57 V11189JMV
<0.169 mg/Kg - dry 0.169 0.929Bis(2-ethylhexyl)phthalate 1 11/04/21 16:57 V11189JMV
<0.153 mg/Kg - dry 0.153 0.9294-Bromophenyl phenyl ether 1 11/04/21 16:57 V11189JMV
<0.159 mg/Kg - dry 0.159 0.464
Butyl benzyl phthalate 1 11/04/21 16:57 V11189JMV
<0.130 mg/Kg - dry 0.130 0.9294-Chloro-3-methylphenol 1 11/04/21 16:57 V11189JMV
<0.157 mg/Kg - dry 0.157 0.4644-Chloroaniline 1 11/04/21 16:57 V11189JMV
<0.163 mg/Kg - dry 0.163 0.9292-Chloronaphthalene 1 11/04/21 16:57 V11189JMV
<0.138 mg/Kg - dry 0.138 0.9292-Chlorophenol 1 11/04/21 16:57 V11189JMV
<0.177 mg/Kg - dry 0.177 1.414-Chlorophenyl phenyl ether 1 11/04/21 16:57 V11189JMV
<0.200 mg/Kg - dry 0.200 0.929Chrysene 1 11/04/21 16:57 V11189JMV
<0.323 mg/Kg - dry 0.323 0.929
Dibenz(a,h)anthracene 1 11/04/21 16:57 V11189JMV
<0.167 mg/Kg - dry 0.167 0.929Dibenzofuran 1 11/04/21 16:57 V11189JMV
<0.132 mg/Kg - dry 0.132 0.9291,2-Dichlorobenzene 1 11/04/21 16:57 V11189JMV
<0.137 mg/Kg - dry 0.137 0.9291,3-Dichlorobenzene 1 11/04/21 16:57 V11189JMV
<0.137 mg/Kg - dry 0.137 0.4641,4-Dichlorobenzene 1 11/04/21 16:57 V11189JMV
<0.207 mg/Kg - dry 0.207 0.9293,3'-Dichlorobenzidine 1 11/04/21 16:57 V11189JMV
<0.134 mg/Kg - dry 0.134 0.9292,4-Dichlorophenol 1 11/04/21 16:57 V11189JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-8
98619 Matrix:
11/2/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V11087 11/03/21 08:50
<0.253 mg/Kg - dry 0.253 0.929Diethyl phthalate 1 11/04/21 16:57 V11189JMV
<0.245 mg/Kg - dry 0.245 0.929Dimethyl phthalate 1 11/04/21 16:57 V11189JMV
<0.152 mg/Kg - dry 0.152 0.4642,4-Dimethylphenol 1 11/04/21 16:57 V11189JMV
<0.150 mg/Kg - dry 0.150 0.929Di-n-butyl phthalate 1 11/04/21 16:57 V11189JMV
<0.338 mg/Kg - dry 0.338 2.114,6-Dinitro-2-methylphenol 1 11/04/21 16:57 V11189JMV
<0.732 mg/Kg - dry 0.732 2.112,4-Dinitrophenol 1 11/04/21 16:57 V11189JMV
<0.136 mg/Kg - dry 0.136 0.9292,4-Dinitrotoluene 1 11/04/21 16:57 V11189JMV
<0.152 mg/Kg - dry 0.152 0.9292,6-Dinitrotoluene 1 11/04/21 16:57 V11189JMV
<0.201 mg/Kg - dry 0.201 0.464
Di-n-Octyl Phthalate 1 11/04/21 16:57 V11189JMV
<0.173 mg/Kg - dry 0.173 0.929Fluoranthene 1 11/04/21 16:57 V11189JMV
<0.180 mg/Kg - dry 0.180 0.929Fluorene 1 11/04/21 16:57 V11189JMV
<0.149 mg/Kg - dry 0.149 0.929Hexachlorobenzene 1 11/04/21 16:57 V11189JMV
<0.137 mg/Kg - dry 0.137 0.929Hexachlorobutadiene 1 11/04/21 16:57 V11189JMV
<0.221 mg/Kg - dry 0.221 0.929Hexachlorocyclopentadiene 1 11/04/21 16:57 V11189JMV
<0.111 mg/Kg - dry 0.111 0.929Hexachloroethane 1 11/04/21 16:57 V11189JMV
<0.252 mg/Kg - dry 0.252 0.929
Indeno(1,2,3-cd)pyrene 1 11/04/21 16:57 V11189JMV
<0.269 mg/Kg - dry 0.269 0.929Isophorone 1 11/04/21 16:57 V11189JMV
<0.149 mg/Kg - dry 0.149 0.9291-Methylnaphthalene 1 11/04/21 16:57 V11189JMV
<0.140 mg/Kg - dry 0.140 0.9292-Methylnaphthalene 1 11/04/21 16:57 V11189JMV
<0.136 mg/Kg - dry 0.136 0.9292-Methylphenol 1 11/04/21 16:57 V11189JMV
<0.119 mg/Kg - dry 0.119 0.9293&4 Methylphenol 1 11/04/21 16:57 V11189JMV
<0.202 mg/Kg - dry 0.202 0.929Naphthalene 1 11/04/21 16:57 V11189JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-8
98619 Matrix:
11/2/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V11087 11/03/21 08:50
<0.136 mg/Kg - dry 0.136 0.9292-Nitroaniline 1 11/04/21 16:57 V11189JMV
<0.169 mg/Kg - dry 0.169 0.9293-Nitroaniline 1 11/04/21 16:57 V11189JMV
<0.131 mg/Kg - dry 0.131 0.4644-Nitroaniline 1 11/04/21 16:57 V11189JMV
<0.163 mg/Kg - dry 0.163 0.464Nitrobenzene 1 11/04/21 16:57 V11189JMV
<0.125 mg/Kg - dry 0.125 0.9292-Nitrophenol 1 11/04/21 16:57 V11189JMV
<0.164 mg/Kg - dry 0.164 0.9294-Nitrophenol 1 11/04/21 16:57 V11189JMV
<0.370 mg/Kg - dry 0.370 0.929N-Nitrosodimethylamine 1 11/04/21 16:57 V11189JMV
<0.254 mg/Kg - dry 0.254 0.929N-Nitrosodiphenylamine 1 11/04/21 16:57 V11189JMV
<0.166 mg/Kg - dry 0.166 0.929
N-Nitroso-di-n-propylamine 1 11/04/21 16:57 V11189JMV
<0.488 mg/Kg - dry 0.488 1.41Pentachlorophenol 1 11/04/21 16:57 V11189JMV
<0.292 mg/Kg - dry 0.292 0.929Phenanthrene 1 11/04/21 16:57 V11189JMV
<0.157 mg/Kg - dry 0.157 0.929Phenol 1 11/04/21 16:57 V11189JMV
<0.188 mg/Kg - dry 0.188 0.929Pyrene 1 11/04/21 16:57 V11189JMV
<0.111 mg/Kg - dry 0.111 0.464Pyridine 1 11/04/21 16:57 V11189JMV
<0.150 mg/Kg - dry 0.150 0.9291,2,4-Trichlorobenzene 1 11/04/21 16:57 V11189JMV
<0.135 mg/Kg - dry 0.135 0.929
2,4,5-Trichlorophenol 1 11/04/21 16:57 V11189JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 54
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-306-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/02/2021
LEN-008
Report Date : 11/11/2021
Sample ID :
Lab No :
Sampled:EX-8
98619 Matrix:
11/2/2021 9:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V11087 11/03/21 08:50
<0.136 mg/Kg - dry 0.136 0.9292,4,6-Trichlorophenol 1 11/04/21 16:57 V11189JMV
Surrogate: Phenol-d5 83.4 Limits: 34-121%11/04/21 16:571 JMV V11189
Surrogate: 2-Fluorobiphenyl 83.7 Limits: 44-115%11/04/21 16:571 JMV V11189
Surrogate: 2-Fluorophenol 86.7 Limits: 35-115%11/04/21 16:571 JMV V11189
Surrogate: Nitrobenzene-d5 72.3 Limits: 37-122%11/04/21 16:571 JMV V11189
Surrogate: 4-Terphenyl-d14 94.0 Limits: 54-127%11/04/21 16:571 JMV V11189
Surrogate: 2,4,6-Tribromophenol 88.9 Limits: 39-132%11/04/21 16:571 JMV V11189
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 54
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172Tel: [phone] Fax: [phone] www.pacelabs.com
Report of Analysis
Waypoint Analytical
PO Box 240543Charlotte, NC 28224Attention: Angela Overcash
Project Name: 21-306-0024
Lot Number:WK03117
Date Completed:11/10/2021
11/11/2021 9:04 AMApproved and released by:
Project Manager II:Lucas Odom
Page 1 of 12
Page 23 of 54
PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Waypoint Analytical
Lot Number: WK03117
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header informationassociated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page ordiscussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non-Potable Water: SGT-HEM EPA 1664B,Silica EPA 200.7, Boron, Calcium,Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weightunless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Page 2 of 12
Page 24 of 54
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WK03117

Sample Number Sample ID Matrix Date Sampled Date Received
001 11/02/2021 0830EX-7 Solid 11/03/2021
002 11/02/2021 0930EX-8 Solid 11/03/2021
(2 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 12
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WK03117

Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 12
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
EX-7
WK03117-001
11/02/2021 0830
11/03/2021
Solid
% Solids:77.8 11/04/2021 0111
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 11/09/2021 1524 AMR 11/05/2021 1230 21441
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 12
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
EX-8
WK03117-002
11/02/2021 0930
11/03/2021
Solid
% Solids:77.5 11/04/2021 0111
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 11/09/2021 1537 AMR 11/05/2021 1230 21441
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 12
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 12
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ21441-001
21441 3060A
11/05/2021 1230Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 11/09/2021 12231.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 12
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ21441-002
21441 3060A
11/05/2021 1230Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 8.7 11/09/2021 1249871080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 12
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 12
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 12
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 12
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Metals Analyses
6020B
V11303QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V11234
Associated Lab Samples: 98618, 98619
LRB-V11234 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/06/21 16:231.000.0940<0.0940mg/KgArsenic
11/06/21 16:2310.01.40<1.40mg/KgBarium
11/06/21 16:230.5000.0550<0.0550mg/KgCadmium
11/06/21 16:231.000.290<0.290mg/KgChromium
11/06/21 16:231.000.140<0.140mg/KgLead
11/06/21 16:232.000.900<0.900mg/KgSelenium
11/06/21 16:230.5000.0410<0.0410mg/KgSilver
LCS-V11234Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.011.812.5mg/KgArsenic 80-120
92.011.512.5mg/KgBarium 80-120
98.012.212.5mg/KgCadmium 80-120
99.012.412.5mg/KgChromium 80-120
99.012.412.5mg/KgLead 80-120
10212.812.5mg/KgSelenium 80-120
99.04.945.00mg/KgSilver 80-120
Page 1 of 18Date:11/11/2021 09:24 AM
Page 35 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V11373QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V11340
Associated Lab Samples: 98618, 98619
LRB-V11340 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/09/21 11:160.03000.0120<0.0120mg/KgMercury (Total)
LCS-V11340Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.00.3910.417mg/KgMercury (Total)80-120
V 98288-MS-V11340 V 98288-MSD-V11340Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.462 99.00.4590.4170.4170.0480mg/KgMercury (Total)99.0 80-120 0.6 20
V 98288-PDS-V11340Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/09/21 11:351020.237mg/KgMercury (Total)
Page 2 of 18Date:11/11/2021 09:24 AM
Page 36 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V11116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V11115
Associated Lab Samples: 98618, 98619
LRB-V11115 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/03/21 10:310.0200.002<0.002mg/KgAcetone
11/03/21 10:310.0200.001<0.001mg/KgAcrolein
11/03/21 10:310.0200.0008<0.0008mg/KgAcrylonitrile
11/03/21 10:310.0050.0006<0.0006mg/KgBenzene
11/03/21 10:310.0050.0005<0.0005mg/KgBromobenzene
11/03/21 10:310.0050.0008<0.0008mg/KgBromochloromethane
11/03/21 10:310.0050.001<0.001mg/KgBromodichloromethane
11/03/21 10:310.0050.001<0.001mg/KgBromoform
11/03/21 10:310.0100.001<0.001mg/KgBromomethane
11/03/21 10:310.0050.0005<0.0005mg/Kgn-Butylbenzene
11/03/21 10:310.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/03/21 10:310.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/03/21 10:310.0050.0006<0.0006mg/KgCarbon Disulfide
11/03/21 10:310.0050.001<0.001mg/KgCarbon Tetrachloride
11/03/21 10:310.0050.0007<0.0007mg/KgChlorobenzene
11/03/21 10:310.0050.0009<0.0009mg/KgChlorodibromomethane
11/03/21 10:310.0100.0009<0.0009mg/KgChloroethane
11/03/21 10:310.0050.001<0.001mg/KgChloroform
11/03/21 10:310.0100.0006<0.0006mg/KgChloromethane
11/03/21 10:310.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/03/21 10:310.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/03/21 10:310.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/03/21 10:310.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/03/21 10:310.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/03/21 10:310.0050.0006<0.0006mg/KgDibromomethane
11/03/21 10:310.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/03/21 10:310.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 3 of 18Date:11/11/2021 09:24 AM
Page 37 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V11116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V11115
Associated Lab Samples: 98618, 98619
LRB-V11115 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/03/21 10:310.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/03/21 10:310.0100.001<0.001mg/KgDichlorodifluoromethane
11/03/21 10:310.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/03/21 10:310.0050.001<0.001mg/Kg1,2-Dichloroethane
11/03/21 10:310.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/03/21 10:310.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/03/21 10:310.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/03/21 10:310.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/03/21 10:310.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/03/21 10:310.0050.001<0.001mg/Kg2,2-Dichloropropane
11/03/21 10:310.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/03/21 10:310.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/03/21 10:310.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/03/21 10:310.2500.014<0.014mg/KgEthanol
11/03/21 10:310.0050.0006<0.0006mg/KgEthylbenzene
11/03/21 10:310.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/03/21 10:310.0100.0008<0.0008mg/KgHexachlorobutadiene
11/03/21 10:310.0100.0007<0.0007mg/Kgn-Hexane
11/03/21 10:310.0200.0006<0.0006mg/Kg2-Hexanone
11/03/21 10:310.0050.0005<0.0005mg/KgIsopropylbenzene
11/03/21 10:310.0050.001<0.001mg/Kg4-Isopropyl toluene
11/03/21 10:310.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/03/21 10:310.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/03/21 10:310.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/03/21 10:310.0100.001<0.001mg/KgMethylene Chloride
11/03/21 10:310.0100.0010<0.0010mg/KgNaphthalene
11/03/21 10:310.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 4 of 18Date:11/11/2021 09:24 AM
Page 38 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V11116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V11115
Associated Lab Samples: 98618, 98619
LRB-V11115 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/03/21 10:310.0050.001<0.001mg/KgStyrene
11/03/21 10:310.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/03/21 10:310.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/03/21 10:310.0050.0009<0.0009mg/KgTetrachloroethene
11/03/21 10:310.0050.0007<0.0007mg/KgToluene
11/03/21 10:310.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/03/21 10:310.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/03/21 10:310.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/03/21 10:310.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/03/21 10:310.0050.0009<0.0009mg/KgTrichloroethene
11/03/21 10:310.0100.002<0.002mg/KgTrichlorofluoromethane
11/03/21 10:310.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/03/21 10:310.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
11/03/21 10:310.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/03/21 10:310.0100.0005<0.0005mg/KgVinyl Acetate
11/03/21 10:310.0100.0005<0.0005mg/KgVinyl Chloride
11/03/21 10:310.0050.0005<0.0005mg/Kgo-Xylene
11/03/21 10:310.0100.001<0.001mg/Kgm,p-Xylene
11/03/21 10:314-Bromofluorobenzene (S)101 70-130
11/03/21 10:31Dibromofluoromethane (S)102 84-123
11/03/21 10:31Toluene-d8 (S)104 76-129
LCS-V11115 LCSD-V11115Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.399.60.0990.100mg/KgAcetone 29-198 2.3 20
Page 5 of 18Date:11/11/2021 09:24 AM
Page 39 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V11116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V11115
LCS-V11115 LCSD-V11115Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.099 99.91030.1030.100mg/KgAcrolein 70-130 3.0 20
0.094 94.396.30.0960.100mg/KgAcrylonitrile 65-134 2.0 20
0.045 90.296.20.0480.050mg/KgBenzene 74-127 6.4 20
0.047 95.898.60.0490.050mg/KgBromobenzene 73-125 2.8 20
0.047 95.098.80.0490.050mg/KgBromochloromethane 72-134 3.9 20
0.047 94.896.20.0480.050mg/KgBromodichloromethane 75-122 1.4 20
0.049 99.81010.0500.050mg/KgBromoform 66-135 0.9 20
0.039 78.685.00.0420.050mg/KgBromomethane 20-180 7.8 20
0.047 94.699.20.0490.050mg/Kgn-Butylbenzene 65-135 4.7 20
0.047 94.299.20.0490.050mg/Kgsec-Butyl benzene 66-131 5.1 20
0.046 92.897.60.0480.050mg/Kgtert-Butyl benzene 67-132 5.0 20
0.045 90.297.00.0480.050mg/KgCarbon Disulfide 61-129 7.2 20
0.044 88.296.80.0480.050mg/KgCarbon Tetrachloride 64-143 9.2 20
0.048 96.61000.0500.050mg/KgChlorobenzene 74-118 3.4 20
0.049 99.01020.0510.050mg/KgChlorodibromomethane 73-122 2.9 20
0.039 78.888.60.0440.050mg/KgChloroethane 33-149 11.7 20
0.044 89.694.40.0470.050mg/KgChloroform 73-127 5.2 20
0.045 90.898.00.0490.050mg/KgChloromethane 45-143 7.6 20
0.047 94.498.80.0490.050mg/Kg2-Chlorotoluene 67-124 4.5 20
0.047 94.499.80.0490.050mg/Kg4-Chlorotoluene 71-126 5.5 20
0.049 99.21040.0520.050mg/KgDi-Isopropyl Ether (DIPE)59-159 4.7 20
0.046 93.295.60.0470.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.5 20
0.049 98.81010.0500.050mg/Kg1,2-Dibromoethane 70-132 2.2 20
0.047 95.81010.0500.050mg/KgDibromomethane 74-133 4.8 20
0.047 95.298.80.0490.050mg/Kg1,2-Dichlorobenzene 72-123 3.7 20
0.046 93.296.80.0480.050mg/Kg1,3-Dichlorobenzene 71-120 3.7 20
Page 6 of 18Date:11/11/2021 09:24 AM
Page 40 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V11116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V11115
LCS-V11115 LCSD-V11115Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.047 94.497.00.0480.050mg/Kg1,4-Dichlorobenzene 71-123 2.7 20
0.046 93.41010.0500.050mg/KgDichlorodifluoromethane 26-146 7.8 20
0.045 90.296.60.0480.050mg/Kg1,1-Dichloroethane 74-127 6.8 20
0.047 95.498.80.0490.050mg/Kg1,2-Dichloroethane 68-128 3.5 20
0.044 88.694.60.0470.050mg/Kg1,1-Dichloroethene 67-149 6.5 20
0.046 92.296.60.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 4.6 20
0.045 91.897.20.0480.050mg/Kgtrans-1,2-Dichloroethene 73-132 5.7 20
0.046 92.097.60.0480.050mg/Kg1,2-Dichloropropane 73-130 5.9 20
0.050 1011010.0500.050mg/Kg1,3-Dichloropropane 75-124 0.7 20
0.045 90.497.00.0480.050mg/Kg2,2-Dichloropropane 50-142 7.0 20
0.044 89.496.60.0480.050mg/Kg1,1-Dichloropropene 71-130 7.7 20
0.047 94.01000.0500.050mg/Kgcis-1,3-Dichloropropene 71-125 6.1 20
0.047 95.098.40.0490.050mg/Kgtrans-1,3-Dichloropropene 68-123 3.5 20
1.27 1021021.281.25mg/KgEthanol 70-130 0.7 20
0.047 95.099.60.0490.050mg/KgEthylbenzene 74-128 4.7 20
0.098 98.01020.1020.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 4.0 20
0.046 92.096.20.0480.050mg/KgHexachlorobutadiene 64-125 4.4 20
0.045 90.21010.0500.050mg/Kgn-Hexane 70-130 11.0 20
0.046 93.897.40.0480.050mg/Kg2-Hexanone 61-157 3.7 20
0.047 94.699.60.0490.050mg/KgIsopropylbenzene 68-126 5.1 20
0.047 94.499.20.0490.050mg/Kg4-Isopropyl toluene 68-129 4.9 20
0.046 92.098.20.0490.050mg/KgMethyl Ethyl Ketone (MEK)63-149 6.5 20
0.047 94.897.80.0480.050mg/KgMethyl tert-butyl ether (MTBE)70-130 3.1 20
0.048 96.41010.0500.050mg/Kg4-Methyl-2-Pentanone 57-162 4.8 20
0.046 93.698.00.0490.050mg/KgMethylene Chloride 74-129 4.5 20
0.047 94.096.00.0480.050mg/KgNaphthalene 57-157 2.1 20
Page 7 of 18Date:11/11/2021 09:24 AM
Page 41 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V11116QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V11115
LCS-V11115 LCSD-V11115Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.047 95.01000.0500.050mg/Kgn-Propylbenzene 67-130 5.3 20
0.049 98.01010.0500.050mg/KgStyrene 77-121 3.4 20
0.049 99.01010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 2.1 20
0.048 97.098.20.0490.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.2 20
0.044 88.093.60.0460.050mg/KgTetrachloroethene 68-130 6.1 20
0.045 91.295.80.0470.050mg/KgToluene 71-129 4.9 20
0.047 94.297.00.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 2.9 20
0.048 96.099.00.0490.050mg/Kg1,2,4-Trichlorobenzene 66-125 3.0 20
0.044 89.095.60.0470.050mg/Kg1,1,1-Trichloroethane 67-131 7.1 20
0.049 99.61020.0500.050mg/Kg1,1,2-Trichloroethane 70-133 2.1 20
0.044 88.898.00.0490.050mg/KgTrichloroethene 75-133 9.8 20
0.046 92.81010.0500.050mg/KgTrichlorofluoromethane 44-146 8.0 20
0.047 95.295.00.0470.050mg/Kg1,2,3-Trichloropropane 60-137 0.2 20
0.047 94.298.00.0490.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.9 20
0.046 93.698.60.0490.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.2 20
0.049 99.01010.0500.050mg/KgVinyl Acetate 60-140 2.1 20
0.045 91.098.60.0490.050mg/KgVinyl Chloride 48-147 8.0 20
0.048 96.41000.0500.050mg/Kgo-Xylene 74-126 3.8 20
0.098 98.21020.1020.100mg/Kgm,p-Xylene 75-124 3.7 20
1011014-Bromofluorobenzene (S)70-130
100100Dibromofluoromethane (S)84-123
104103Toluene-d8 (S)76-129
Page 8 of 18Date:11/11/2021 09:24 AM
Page 42 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V11189QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V11087
Associated Lab Samples: 98618, 98619
LRB-V11087 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/04/21 11:470.6600.116<0.116mg/KgAcenaphthene
11/04/21 11:470.6600.105<0.105mg/KgAcenaphthylene
11/04/21 11:470.6600.152<0.152mg/KgAniline
11/04/21 11:470.6600.143<0.143mg/KgAnthracene
11/04/21 11:470.6600.139<0.139mg/KgBenzo(a)anthracene
11/04/21 11:470.6600.147<0.147mg/KgBenzo(a)pyrene
11/04/21 11:470.6600.146<0.146mg/KgBenzo(b)fluoranthene
11/04/21 11:470.6600.136<0.136mg/KgBenzo(g,h,i)perylene
11/04/21 11:470.6600.137<0.137mg/KgBenzo(k)fluoranthene
11/04/21 11:472.000.580<0.580mg/KgBenzoic Acid
11/04/21 11:470.6600.105<0.105mg/KgBenzyl alcohol
11/04/21 11:470.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
11/04/21 11:470.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
11/04/21 11:470.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
11/04/21 11:470.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
11/04/21 11:470.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
11/04/21 11:470.3300.113<0.113mg/KgButyl benzyl phthalate
11/04/21 11:470.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
11/04/21 11:470.3300.112<0.112mg/Kg4-Chloroaniline
11/04/21 11:470.6600.116<0.116mg/Kg2-Chloronaphthalene
11/04/21 11:470.6600.098<0.098mg/Kg2-Chlorophenol
11/04/21 11:471.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
11/04/21 11:470.6600.142<0.142mg/KgChrysene
11/04/21 11:470.6600.230<0.230mg/KgDibenz(a,h)anthracene
11/04/21 11:470.6600.119<0.119mg/KgDibenzofuran
11/04/21 11:470.6600.094<0.094mg/Kg1,2-Dichlorobenzene
11/04/21 11:470.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 9 of 18Date:11/11/2021 09:24 AM
Page 43 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V11189QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V11087
Associated Lab Samples: 98618, 98619
LRB-V11087 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/04/21 11:470.3300.097<0.097mg/Kg1,4-Dichlorobenzene
11/04/21 11:470.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
11/04/21 11:470.6600.095<0.095mg/Kg2,4-Dichlorophenol
11/04/21 11:470.6600.180<0.180mg/KgDiethyl phthalate
11/04/21 11:470.6600.174<0.174mg/KgDimethyl phthalate
11/04/21 11:470.3300.108<0.108mg/Kg2,4-Dimethylphenol
11/04/21 11:470.6600.107<0.107mg/KgDi-n-butyl phthalate
11/04/21 11:471.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
11/04/21 11:471.500.520<0.520mg/Kg2,4-Dinitrophenol
11/04/21 11:470.6600.096<0.096mg/Kg2,4-Dinitrotoluene
11/04/21 11:470.6600.108<0.108mg/Kg2,6-Dinitrotoluene
11/04/21 11:470.3300.143<0.143mg/KgDi-n-Octyl Phthalate
11/04/21 11:470.6600.123<0.123mg/KgFluoranthene
11/04/21 11:470.6600.128<0.128mg/KgFluorene
11/04/21 11:470.6600.106<0.106mg/KgHexachlorobenzene
11/04/21 11:470.6600.097<0.097mg/KgHexachlorobutadiene
11/04/21 11:470.6600.157<0.157mg/KgHexachlorocyclopentadiene
11/04/21 11:470.6600.079<0.079mg/KgHexachloroethane
11/04/21 11:470.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
11/04/21 11:470.6600.191<0.191mg/KgIsophorone
11/04/21 11:470.6600.106<0.106mg/Kg1-Methylnaphthalene
11/04/21 11:470.6600.100<0.100mg/Kg2-Methylnaphthalene
11/04/21 11:470.6600.097<0.097mg/Kg2-Methylphenol
11/04/21 11:470.6600.084<0.084mg/Kg3&4 Methylphenol
11/04/21 11:470.6600.144<0.144mg/KgNaphthalene
11/04/21 11:470.6600.096<0.096mg/Kg2-Nitroaniline
11/04/21 11:470.6600.120<0.120mg/Kg3-Nitroaniline
Page 10 of 18Date:11/11/2021 09:24 AM
Page 44 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V11189QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V11087
Associated Lab Samples: 98618, 98619
LRB-V11087 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/04/21 11:470.3300.093<0.093mg/Kg4-Nitroaniline
11/04/21 11:470.3300.116<0.116mg/KgNitrobenzene
11/04/21 11:470.6600.088<0.088mg/Kg2-Nitrophenol
11/04/21 11:470.6600.117<0.117mg/Kg4-Nitrophenol
11/04/21 11:470.6600.263<0.263mg/KgN-Nitrosodimethylamine
11/04/21 11:470.6600.181<0.181mg/KgN-Nitrosodiphenylamine
11/04/21 11:470.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
11/04/21 11:471.000.347<0.347mg/KgPentachlorophenol
11/04/21 11:470.6600.208<0.208mg/KgPhenanthrene
11/04/21 11:470.6600.112<0.112mg/KgPhenol
11/04/21 11:470.6600.134<0.134mg/KgPyrene
11/04/21 11:470.3300.079<0.079mg/KgPyridine
11/04/21 11:470.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
11/04/21 11:470.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
11/04/21 11:470.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
11/04/21 11:472-Fluorobiphenyl (S)101 44-115
11/04/21 11:472-Fluorophenol (S)102 35-115
11/04/21 11:47Nitrobenzene-d5 (S)88.0 37-122
11/04/21 11:474-Terphenyl-d14 (S)102 54-127
11/04/21 11:472,4,6-Tribromophenol (S)101 39-132
11/04/21 11:47Phenol-d5 (S)97.5 34-121
LCS-V11087Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.21.641.67mg/KgAcenaphthene 40-123
1001.671.67mg/KgAcenaphthylene 32-132
Page 11 of 18Date:11/11/2021 09:24 AM
Page 45 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V11189QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V11087
LCS-V11087Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1001.671.67mg/KgAniline 12-197
1001.671.67mg/KgAnthracene 47-123
95.21.591.67mg/KgBenzo(a)anthracene 49-126
1111.851.67mg/KgBenzo(a)pyrene 45-129
98.81.651.67mg/KgBenzo(b)fluoranthene 45-132
94.61.581.67mg/KgBenzo(g,h,i)perylene 43-134
95.21.591.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.341.67mg/KgBenzoic Acid 10-83
97.01.621.67mg/KgBenzyl alcohol 29-122
93.41.561.67mg/KgBis(2-Chloroethoxy)methane 36-121
96.41.611.67mg/KgBis(2-Chloroethyl)ether 31-120
1071.781.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1031.721.67mg/KgBis(2-ethylhexyl)phthalate 51-133
97.61.631.67mg/Kg4-Bromophenyl phenyl ether 46-124
97.01.621.67mg/KgButyl benzyl phthalate 48-132
88.01.471.67mg/Kg4-Chloro-3-methylphenol 45-122
74.81.251.67mg/Kg4-Chloroaniline 17-106
96.41.611.67mg/Kg2-Chloronaphthalene 41-114
97.01.621.67mg/Kg2-Chlorophenol 34-121
96.41.611.67mg/Kg4-Chlorophenyl phenyl ether 45-121
99.41.661.67mg/KgChrysene 50-124
91.61.531.67mg/KgDibenz(a,h)anthracene 45-134
96.41.611.67mg/KgDibenzofuran 44-120
84.41.411.67mg/Kg1,2-Dichlorobenzene 33-117
81.41.361.67mg/Kg1,3-Dichlorobenzene 30-115
80.81.351.67mg/Kg1,4-Dichlorobenzene 31-115
93.41.561.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 12 of 18* QC Fail Date:11/11/2021 09:24 AM
Page 46 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V11189QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V11087
LCS-V11087Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
88.01.471.67mg/Kg2,4-Dichlorophenol 40-122
95.81.601.67mg/KgDiethyl phthalate 50-124
93.41.561.67mg/KgDimethyl phthalate 48-124
94.01.571.67mg/Kg2,4-Dimethylphenol 30-127
1051.761.67mg/KgDi-n-butyl phthalate 51-128
95.21.591.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
1021.711.67mg/Kg2,4-Dinitrophenol 27-129
1051.751.67mg/Kg2,4-Dinitrotoluene 48-126
1071.791.67mg/Kg2,6-Dinitrotoluene 46-124
98.21.641.67mg/KgDi-n-Octyl Phthalate 45-140
98.21.641.67mg/KgFluoranthene 50-127
97.61.631.67mg/KgFluorene 43-125
1011.691.67mg/KgHexachlorobenzene 45-122
77.81.301.67mg/KgHexachlorobutadiene 32-123
73.01.221.67mg/KgHexachlorocyclopentadiene 32-117
79.01.321.67mg/KgHexachloroethane 28-117
94.61.581.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
77.21.291.67mg/KgIsophorone 30-122
79.61.331.67mg/Kg1-Methylnaphthalene 40-119
81.41.361.67mg/Kg2-Methylnaphthalene 38-122
99.41.661.67mg/Kg2-Methylphenol 32-122
84.41.411.67mg/Kg3&4 Methylphenol 34-119
78.41.311.67mg/KgNaphthalene 35-123
1031.721.67mg/Kg2-Nitroaniline 44-127
92.21.541.67mg/Kg3-Nitroaniline 33-119
84.41.411.67mg/Kg4-Nitroaniline 63-147
76.61.281.67mg/KgNitrobenzene 34-122
Page 13 of 18Date:11/11/2021 09:24 AM
Page 47 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V11189QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V11087
LCS-V11087Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.01.421.67mg/Kg2-Nitrophenol 36-123
94.61.581.67mg/Kg4-Nitrophenol 30-132
76.01.271.67mg/KgN-Nitrosodimethylamine 10-146
1191.991.67mg/KgN-Nitrosodiphenylamine 38-127
87.41.461.67mg/KgN-Nitroso-di-n-propylamine 36-120
1212.021.67mg/KgPentachlorophenol 25-133
98.81.651.67mg/KgPhenanthrene 50-121
97.01.621.67mg/KgPhenol 34-121
98.81.651.67mg/KgPyrene 47-127
66.41.111.67mg/KgPyridine 10-80
77.81.301.67mg/Kg1,2,4-Trichlorobenzene 34-118
98.81.651.67mg/Kg2,4,5-Trichlorophenol 41-124
1011.681.67mg/Kg2,4,6-Trichlorophenol 39-126
92.82-Fluorobiphenyl (S)44-115
98.42-Fluorophenol (S)35-115
73.0Nitrobenzene-d5 (S)37-122
97.64-Terphenyl-d14 (S)54-127
1012,4,6-Tribromophenol (S)39-132
92.1Phenol-d5 (S)34-121
V 98553-MS-V11087 V 98553-MSD-V11087Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.34 80.21.491.671.67<0.116mg/KgAcenaphthene 89.2 40-123 10.6 20
1.43 85.61.601.671.67<0.105mg/KgAcenaphthylene 95.8 32-132 11.2 20
1.14 68.21.441.671.67<0.152mg/KgAniline 86.2 12-197 23.2*20
Page 14 of 18* QC Fail Date:11/11/2021 09:24 AM
Page 48 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V11189QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V11087
V 98553-MS-V11087 V 98553-MSD-V11087Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.42 85.01.601.671.67<0.143mg/KgAnthracene 95.8 47-123 11.9 20
1.34 80.21.511.671.67<0.139mg/KgBenzo(a)anthracene 90.4 49-126 11.9 20
1.52 91.01.741.671.67<0.147mg/KgBenzo(a)pyrene 104 45-129 13.4 20
1.38 82.61.561.671.67<0.146mg/KgBenzo(b)fluoranthene 93.4 45-132 12.2 20
1.26 75.41.471.671.67<0.136mg/KgBenzo(g,h,i)perylene 88.0 43-134 15.3 20
1.29 77.21.471.671.67<0.137mg/KgBenzo(k)fluoranthene 88.0 47-132 13.0 20
0.944 0.0*1.091.671.67<0.580mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.35 80.81.471.671.67<0.105mg/KgBenzyl alcohol 88.0 29-122 8.5 20
1.37 82.01.431.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 85.6 36-121 4.2 20
1.42 85.01.391.671.67<0.107mg/KgBis(2-Chloroethyl)ether 83.2 31-120 2.1 20
1.51 90.41.641.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 98.2 33-131 8.2 20
1.50 89.81.711.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 102 51-133 13.0 20
1.41 84.41.551.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 92.8 46-124 9.4 20
1.39 83.21.601.671.67<0.113mg/KgButyl benzyl phthalate 95.8 48-132 14.0 20
1.26 75.41.401.671.67<0.092mg/Kg4-Chloro-3-methylphenol 83.8 45-122 10.5 20
1.02 61.01.181.671.67<0.112mg/Kg4-Chloroaniline 70.6 17-106 14.5 20
1.40 83.81.531.671.67<0.116mg/Kg2-Chloronaphthalene 91.6 41-114 8.8 20
1.37 82.01.471.671.67<0.098mg/Kg2-Chlorophenol 88.0 34-121 7.0 20
1.35 80.81.551.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 92.8 45-121 13.7 20
1.40 83.81.581.671.67<0.142mg/KgChrysene 94.6 50-124 12.0 20
1.23 73.61.401.671.67<0.230mg/KgDibenz(a,h)anthracene 83.8 45-134 12.9 20
1.38 82.61.551.671.67<0.119mg/KgDibenzofuran 92.8 44-120 11.6 20
1.22 73.01.311.671.67<0.094mg/Kg1,2-Dichlorobenzene 78.4 33-117 7.1 20
1.18 70.61.291.671.67<0.097mg/Kg1,3-Dichlorobenzene 77.2 30-115 8.9 20
1.14 68.21.261.671.67<0.097mg/Kg1,4-Dichlorobenzene 75.4 31-115 10.0 20
1.10 65.81.321.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 79.0 22-121 18.1 20
Page 15 of 18* QC Fail Date:11/11/2021 09:24 AM
Page 49 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V11189QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V11087
V 98553-MS-V11087 V 98553-MSD-V11087Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.26 75.41.381.671.67<0.095mg/Kg2,4-Dichlorophenol 82.6 40-122 9.0 20
1.33 79.61.511.671.67<0.180mg/KgDiethyl phthalate 90.4 50-124 12.6 20
1.31 78.41.491.671.67<0.174mg/KgDimethyl phthalate 89.2 48-124 12.8 30
1.35 80.81.521.671.67<0.108mg/Kg2,4-Dimethylphenol 91.0 30-127 11.8 20
1.49 89.21.681.671.67<0.107mg/KgDi-n-butyl phthalate 101 51-128 11.9 20
0.849 0.0*0.8881.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
0.743 0.0*0.8081.671.67<0.520mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.25 74.81.471.671.67<0.096mg/Kg2,4-Dinitrotoluene 88.0 48-126 16.1 20
1.37 82.01.591.671.67<0.108mg/Kg2,6-Dinitrotoluene 95.2 46-124 14.8 20
1.36 81.41.601.671.67<0.143mg/KgDi-n-Octyl Phthalate 95.8 45-140 16.2 20
1.39 83.21.551.671.67<0.123mg/KgFluoranthene 92.8 50-127 10.8 20
1.39 83.21.551.671.67<0.128mg/KgFluorene 92.8 43-125 10.8 20
1.41 84.41.601.671.67<0.106mg/KgHexachlorobenzene 95.8 45-122 12.6 20
1.11 66.41.211.671.67<0.097mg/KgHexachlorobutadiene 72.4 32-123 8.6 20
0.872 52.20.9651.671.67<0.157mg/KgHexachlorocyclopentadiene 57.7 32-117 10.1 20
1.14 68.21.221.671.67<0.079mg/KgHexachloroethane 73.0 28-117 6.7 20
1.26 75.41.451.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 86.8 45-133 14.0 20
1.11 66.41.221.671.67<0.191mg/KgIsophorone 73.0 30-122 9.4 20
1.20 71.81.301.671.67<0.106mg/Kg1-Methylnaphthalene 77.8 40-119 8.0 20
1.21 72.41.331.671.670.110mg/Kg2-Methylnaphthalene 79.6 38-122 9.4 20
1.45 86.81.571.671.67<0.097mg/Kg2-Methylphenol 94.0 32-122 7.9 20
1.21 72.41.291.671.67<0.084mg/Kg3&4 Methylphenol 77.2 34-119 6.4 20
1.18 70.61.271.671.67<0.144mg/KgNaphthalene 76.0 35-123 7.3 20
1.55 92.81.701.671.67<0.096mg/Kg2-Nitroaniline 102 44-127 9.2 20
1.21 72.41.411.671.67<0.120mg/Kg3-Nitroaniline 84.4 33-119 15.2 20
1.27 76.01.411.671.67<0.093mg/Kg4-Nitroaniline 84.4 63-147 10.4 20
Page 16 of 18* QC Fail Date:11/11/2021 09:24 AM
Page 50 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V11189QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V11087
V 98553-MS-V11087 V 98553-MSD-V11087Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.05 62.81.121.671.67<0.116mg/KgNitrobenzene 67.0 34-122 6.4 20
0.977 58.51.071.671.67<0.088mg/Kg2-Nitrophenol 64.0 32-123 9.0 20
1.28 76.61.401.671.67<0.117mg/Kg4-Nitrophenol 83.8 30-132 8.9 20
1.11 66.41.201.671.67<0.263mg/KgN-Nitrosodimethylamine 71.8 10-146 7.7 30
1.67 1001.901.671.67<0.181mg/KgN-Nitrosodiphenylamine 114 38-127 12.8 20
1.27 76.01.391.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 83.2 36-120 9.0 20
1.64 98.21.871.671.67<0.347mg/KgPentachlorophenol 112 25-133 13.1 20
1.41 84.41.581.671.67<0.208mg/KgPhenanthrene 94.6 50-121 11.3 20
1.34 80.21.481.671.67<0.112mg/KgPhenol 88.6 34-121 9.9 20
1.41 84.41.601.671.67<0.134mg/KgPyrene 95.8 47-127 12.6 20
0.860 51.40.8971.671.67<0.079mg/KgPyridine 53.7 10-80 4.2 20
1.11 66.41.201.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 71.8 34-118 7.7 20
1.37 82.01.561.671.67<0.096mg/Kg2,4,5-Trichlorophenol 93.4 41-124 12.9 20
1.41 84.41.601.671.67<0.096mg/Kg2,4,6-Trichlorophenol 95.8 39-126 12.6 20
79.02-Fluorobiphenyl (S)90.4 44-115
81.62-Fluorophenol (S)91.2 35-115
61.0Nitrobenzene-d5 (S)67.6 37-122
83.24-Terphenyl-d14 (S)97.0 54-127
80.42,4,6-Tribromophenol (S)95.7 39-132
77.7Phenol-d5 (S)87.3 34-121
Page 17 of 18Date:11/11/2021 09:24 AM
Page 51 of 54
Quality Control Data
21-306-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
LEN-008
Dry Weight Determination
SW-DRYWT
V11105QC Analytical Batch:
Analysis Method:
Analysis Description:
V 98553-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/03/21 16:291.717.217.5%Moisture
V 98604-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/03/21 16:290.273.273.0%Moisture
Page 18 of 18Date:11/11/2021 09:24 AM
Page 52 of 54
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-306-0024
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 1.9C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Sarah J. Locklear Date & Time:11/02/2021 16:05:33
Special precautions or instructions included?
Comments:
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