25101_Press Club Cleaners_Brownfields Assessment Report_20230120

Via Email

January 9, 2023

NCDEQ – Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attn: Mr. Peter Dorn

Re: Brownfields Assessment Report
Former Press Club Cleaners
Charlotte, North Carolina
Brownfields Project No. 25101-21-060
DSCA Site ID No. DC600090
H&H Project No. TCR-003

Dear Pete:

On behalf of CH MF BTH III/Charlotte LoSo, L.L.C., please find the enclosed Brownfields Assessment
Report prepared for the above-referenced Site. Should you have questions or need additional information,
please do not hesitate to contact us at [phone].

Sincerely,
Hart & Hickman, PC
Haley Martin, PG Ralph McGee, PG
Senior Project Geologist Project Manager

Enclosures

cc: Mr. Mark Mathews, Trammel Crow Residential (via email)
Mr. Sean Allen, Trammel Crow Residential (via email)
Ms. Mary Katherine Stukes, Moore & Van Allen, PLLC (via email)
Ms. Laura Boorman Truesdale, Moore & Van Allen, PLLC (via email)
Mr. Mike Cunningham, DEQ DWM DSCA Program (via email)
Mr. Billy Meyer, DEQ DWM DSCA Program (via email)
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Brownfields Assessment Report
Former Press Club Cleaners
South Boulevard and Hartford Avenue
Charlotte, North Carolina
H&H Job No. TCR-003

Table of Contents

1.0 Introduction and Background ...............................................................................................1 
1.1 Site Background Information ................................................................................................1 
1.2 Previous Assessment Activities .............................................................................................2 
1.3 Planned Environment Related Redevelopment Activities.....................................................6 
2.0 Brownfields Soil Assessment Activities .................................................................................8 
3.0 Soil Assessment Activities .....................................................................................................10 
3.1 Soil Sampling Activities ......................................................................................................10 
3.2 Soil Sampling Analytical Results ........................................................................................14 
3.2.1 Additional Dry Cleaner Release Delineation Sampling Analytical Results (Table 1) .14 
3.2.2 Southeastern Shallow Soil Confirmation Sample Analytical Results (Table 2) ...........14 
3.2.3 In-Situ Soil Characterization Sampling Analytical Results (Table 3) ..........................16 
3.3 Direct Contact Risk Evaluation ...........................................................................................17 
3.4 Soil Management Options ...................................................................................................19 
4.0 Quality Assurance – Quality Control ..................................................................................21 
5.0 Summary and Conclusions ..................................................................................................22 

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List of Tables

Table 1 Summary of Dry Cleaner Release Delineation Soil Sample Analytical Results
Table 2 Summary of Confirmation Soil Sample Analytical Results
Table 3 Summary of In Situ Soil Sample Analytical Results

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Sample Location Map

List of Appendices

Appendix A June 2022 Phase II ESA Data Tables and Sample Location Map
Appendix B Boring Logs
Appendix C Laboratory Analytical Reports
Appendix D DEQ Risk Calculators
Appendix E Comparison Detected Metals in Uncontaminated Export to LCID Background

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Brownfields Assessment Report
Former Press Club Cleaners
South Boulevard and Hartford Avenue
Charlotte, North Carolina
H&H Job No. TCR-003

1.0 Introduction and Background

On behalf of CH MF BTH III/Charlotte LoSo, L.L.C. (Prospective Developer or PD), Hart &
Hickman, PC (H&H) has prepared this Brownfields Assessment Report for the former Press
Club Cleaners Brownfields property (Brownfields Project No. [BPN] 25101-21-060) located at
3305 and 3309 South Boulevard and 121, 127, 133, and 139 Hartford Avenue in Charlotte,
Mecklenburg County, North Carolina (Site). The Site consists of three contiguous parcels
(Parcel Identification Numbers 14705111, 14705124, and 14705112) that collectively total
approximately 2.3 acres of land located in the lower South End neighborhood in close proximity
to the LYNX Blue Line light rail corridor and uptown Charlotte.

The Site is developed with an approximately 10,000 square-foot (sq ft) vacant multi-tenant
commercial building that consists of two units and a basement. The northern portion of the Site
building was most recently operated as a dry-cleaning facility known as Press Club Cleaners.
Remaining portions of the Site consists of paved parking areas, driveways, and vegetated areas.
A Site location map is provided as Figure 1, and the Site and surrounding area are shown in
Figure 2.

Proposed redevelopment of the Brownfields property includes razing the existing Site building
for construction of a mixed-use apartment building with an associated multi-story podium style
parking deck and access drives.

1.1 Site Background Information

As early as 1905, the Site consisted of cleared land developed with a residence or agricultural
structure in the southern portion of the Site. The Site remained unchanged until the current
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commercial building was constructed in 1945. The Site building has been utilized for dry
cleaning operations by multiple tenants since construction including Maxey’s One Hour Cleaners
& Laundry (the late 1960s-1970s), One Hour Martinizing (mid-1980s to early 1990s), KNP
Cleaners (1990s), Town Cleaners (2000s), and Press Club Cleaners (mid-2010s). Other Site
occupants have included grocery stores, restaurants, a pawn shop, retail stores, and social clubs.

1.2 Previous Assessment Activities

Dry Cleaner Release
Historical on-Site dry-cleaning operations and unknown sources associated with nearby off-Site
operations have resulted in groundwater, soil, and soil gas impacts at the Site. Although results
of previous assessment activities completed at the Site suggest select organic compounds
detected in Site media are likely attributable to historical operations on nearby off-Site
properties, the primary environmental concern at the Site is related to chlorinated solvents
attributable to releases associated with historical on-Site dry-cleaning operations. Therefore, the
Site was entered into the North Carolina Department of Environmental Quality (DEQ) Dry-
Cleaning Solvent Cleanup Act (DSCA) Program in October 2016 (DSCA Site ID No.
DC600090).

Following entry into the DSCA Program, DEQ contracted with H&H to complete a prioritization
assessment at the Site that included installation and sample collection from ten (10) shallow and
ten (10) deep temporary monitoring wells and collection of eighteen soil samples from ten (10)
soil boring locations. Results of soil sampling activities identified the dry-cleaning solvent
tetrachloroethylene (PCE; up to 10 milligrams per kilogram [mg/kg]) and vinyl chloride (up to
0.017 mg/kg) at concentration above the DSCA Tier 1 Risk-Based Screening Levels of 0.023
mg/kg and 0.00079 mg/kg, respectively. Extensive supplemental soil assessments were
completed at the Site by DSCA to delineate the extents of chlorinated solvents in April 2017,
May 2018, August 2021, and March 2022.

Results of groundwater sampling activities completed in 2016 identified PCE (up to 84
micrograms per liter [µg/L]), trichloroethylene (TCE; up to 3.4 µg/L), 1,2-dichloroethane (up to
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4.1 µg/L), and carbon tetrachloride (up to 2.5 µg/L) at concentrations above the North Carolina
Administrative Code (NCAC) 15A 2L Groundwater Standards (2L Standards) in groundwater
samples collected in the vicinity of and downgradient of the Press Club Cleaners facility.
Additional Press Club Dry Cleaner assessment activities completed under purview of the DSCA
Program have included installation and monitoring of on-Site and off-Site permanent
groundwater monitoring wells. The most recent groundwater sampling event reported by DSCA
was conducted in December 2020 and included sample collection from five groundwater
monitoring wells for laboratory analysis. Laboratory analytical results for the groundwater
samples identified PCE, TCE, vinyl chloride, and 1,2-dichloroethane at concentrations above the
2L Standards in monitoring wells located downgradient of the Site building.

DSCA has also completed extensive vapor intrusion assessments including collection of on-Site
and off-Site soil gas samples for laboratory analysis. Results of on-Site vapor intrusion
assessment activities identified compounds of concern above acceptable risk levels in samples
collected from within the basement of the Site building. Results of off-Site vapor intrusion
assessment activities have not identified risks to off-Site properties at unacceptable levels.

Property Transaction Due Diligence
To address environmental concerns associated with historical on-Site and nearby off-Site
operations, the PD elected to enter the Site into the DEQ Brownfields Program and submitted a
Brownfields Property Application on December 30, 2021. The Site received eligibility into the
Brownfields Program in a letter dated April 29, 2022.

Although the Site received eligibility into the Brownfields Program in April 2022, a DEQ
Brownfields Project Manager was not assigned to the Site until October 2022. Due to time
constraints associated with the property transaction process, H&H conducted Phase II
Environmental Site Assessment (ESA) activities at the Site as part of property transaction due
diligence activities in June 2022. Because the Site was entered into the DEQ Brownfields
Program, but the Project Manager had not been assigned, the Phase II ESA sampling activities
were designed to be consistent with a typical Brownfields assessment for evaluating potential
risks associated with redevelopment of the Site.
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Phase II ESA activities completed at the Site included the collection of additional soil,
groundwater, and soil gas samples for laboratory analysis. As noted above, extensive soil
sampling was previously conducted on the Site by the DSCA Program. Therefore, as part of the
Phase II ESA activities, H&H collected two (2) composite soil samples (COMP-1 and COMP-2)
for laboratory analysis from ten soil borings advanced in areas of planned soil disturbance to
assist in the management of shallow soil during future grading and redevelopment activities
outside of the area of dry-cleaning soil impacts. H&H also sampled four (4) existing on-Site
groundwater monitoring wells (MW-1 through MW-4) to further evaluate the potential for
impact from historical on-Site and nearby off-Site operations. To evaluate the potential for
structural vapor intrusion into the proposed Site building, H&H collected soil gas samples within
the footprint of the proposed apartment building and associated parking deck.

Results of soil sampling activities completed in areas planned for shallow soil disturbance during
future grading and redevelopment of the Site identified several polynuclear aromatic
hydrocarbons (PAHs) at concentrations above the DEQ Preliminary Soil Remediation Goals
(PSRGs) including benzo(a)pyrene (3.91 mg/kg), benzo(a)anthracene (5.23 mg/kg),
benzo(b)fluoranthene (6.95 mg/kg), and indeno(1,2,3-cd)pyrene (2.42 J mg/kg) in the duplicate
sample (COMP-DUP) for composite soil sample COMP-2 collected in the southeastern portion
of the Site. Concentrations of lead (up to 405 mg/kg) and hexavalent chromium (up to 1.67
mg/kg) were detected at concentrations above the DEQ Residential PSRGs and regional
background levels for metals in the COMP-2 soil sample and/or its duplicate soil sample.

Results of Phase II ESA groundwater sampling identified several organic compounds at
concentrations above the 2L Standards and/or DEQ Residential and Non-Residential Vapor
Intrusion Groundwater Screening Levels (GWSLs) including chloroform (up to 1.7 J micrograms
per liter [µg/L]), cis-1,2-dichloroethylene (up to 165 µg/L), PCE (up to 2,370 µg/L),
trichloroethylene or TCE (up to 183 µg/L), and vinyl chloride (up to 20.5 µg/L). The chlorinated
volatile organic compounds identified above 2L Standards and/or DEQ Residential and Non-
Residential Vapor Intrusion GWSLs were primarily detected in MW-1 located adjacent to and
downgradient of the former Press Club Cleaners tenant space. No semi-volatile organic
compounds or metals were identified at concentrations above the 2L Standards or DEQ
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Residential or Non-Residential Vapor Intrusion GWSLs. The results of Phase II ESA
groundwater sampling activities are generally consistent with the results of groundwater
assessment activities previously completed at the Site by the DEQ DSCA Program.

As part of Phase II ESA activities, H&H also collected one sub-slab soil gas sample (BF-SSV-1)
and six (6) exterior soil gas samples (BF-SG-1 and BF-SG-3 through BF-SG-7) for laboratory
analysis to evaluate the potential for structural vapor intrusion into the proposed apartment
building. Results of the exterior and sub-slab soil gas assessment activities identified several
compounds at concentrations above the DEQ Residential and Non-Residential Vapor Intrusion
Sub-slab and Exterior Soil Gas Screening Levels (SGSLs).

The chlorinated compounds PCE (3,549 micrograms per cubic meter [µg/m3]), TCE (10,011
µg/m3), and vinyl chloride (6,778 µg/m3) were detected at concentrations above the DEQ
Residential and Non-Residential Vapor Intrusion SGLSs in a soil gas sample collected adjacent
to and downgradient of the former Press Club Cleaners tenant space. The compounds benzene,
ethylbenzene, n-heptane, n-hexane, naphthalene, chloroform, 1,3-butadiene, m&p-xylene, and
1,1,2,2-tetrachloroethane were also detected at concentrations above the DEQ Residential and/or
Non-Residential Vapor Intrusion SGSLs in soil gas samples collected at the Site.

H&H utilized the DEQ Risk Calculator assuming residential land use scenario to further evaluate
potential cumulative risks for the soil gas to indoor air vapor intrusion pathway for the proposed
apartment building. One risk calculator was completed using soil gas data for samples collected
within the proposed parking deck and one risk calculator was completed using soil gas data for
samples collected within occupiable ground-level components of the proposed building. Results
of the risk calculators indicated that potential vapor intrusion risks exceed acceptable levels
within the footprint of the parking deck but are below acceptable levels for samples collected
within occupiable ground-level components of the proposed building.

Copies of the Phase II ESA data summary tables, and a copy of the Phase II ESA sample
location map are provided in Appendix A for ease of reference.
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1.3 Planned Environment Related Redevelopment Activities

Site work as part of the planned redevelopment includes razing the existing Site building and
grading to level the Site for the planned apartment building and parking deck. Review of
grading plans and cut-fill analysis indicates that excavations to achieve proposed final grade
elevations are planned in the northern and northwestern portions of the Site along South
Boulevard, in the western and southwestern portions of the Site along Hartford Avenue, and in
the southeastern portion of the Site near the southern Site boundary. Fill will be needed to
achieve final grade elevations in the central and northeastern portions of the Site. An overlay of
the cut-fill analysis is shown in Figure 3.

Extensive soil sampling has previously been completed to evaluate the extent of dry-cleaning
solvent impacts at the Site by the DEQ DSCA Program. Based on the results of soil assessment
activities completed by the DSCA Program, the “DSCA Soil Management Area” shown in
Figure 3 depicts the extent of soil containing PCE at concentrations above the unrestricted use
level of 0.0074 mg/kg outlined in the DEQ Contained In Policy for Soil Contaminated with
Listed Hazardous Waste dated June 28, 2016 (Contained In Policy) and the July 2022 DEQ
Protection of Groundwater PRSG of 0.0064 mg/kg.

Based on discussions with the PD and the project geotechnical and civil engineers, and review of
the most recent versions of the grading plans and cut/fill analysis for the Site, H&H understands
that grading and construction activities for the proposed redevelopment will generate excess soil
that will likely need to be transported off-Site to achieve proposed final grade elevations. Areas
planned for cut during grading are also located in the area of soil impacts associated with the dry
cleaner release and will need to be managed in accordance with the DEQ Contained In Policy
and a DEQ-approved Environmental Management Plan (EMP).

An EMP was prepared and submitted to DEQ for review and approval on October 10, 2022. The
DEQ Brownfields Program provided initial comments to the EMP in an email dated October 26,
2022. Generally, initial comments provided by the DEQ Brownfields Program included requests
for the collection of additional soil samples north and west of the DSCA delineated soil impacts
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to further confirm the extent of the DSCA Soil Management Area that will need to be managed
using the DEQ Contained In Policy. In addition, the DEQ Brownfields Program requested
collection of discrete soil samples in the area of composite soil sample COMP-2 to further
evaluate the presence of lead and PAHs in soil and to address discrepancies in analytical results
between the COMP-2 parent soil sample and its duplicate soil sample (COMP-DUP). Although
not requested by DEQ, H&H proposed completion of in situ soil assessment activities within
areas proposed for cut to evaluate the potential for impact and assist in export of non-impacted
soil during grading activities.

To further assist with soil management during the redevelopment of the Site, and to address DEQ
Brownfields Program requests for additional soil assessment, H&H prepared an In Situ Soil
Characterization Work Plan – Revision 1 (Work Plan) for DEQ review and approval. The Work
Plan received DEQ-approval in a letter dated November 23, 2022.

A summary of the soil assessment activities conducted in accordance with the DEQ-approved
Work Plan is provided in the following sections.
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2.0 Brownfields Soil Assessment Activities

Brownfields soil assessment activities were completed in November 2022. With the goal of
obtaining additional information to assist in the management of soil during proposed
redevelopment activities, the primary objectives of the soil assessment activities included the
following:

 Delineation of the northern and western sides of the DSCA Soil Management Area to
define the area at the Site where disturbed soil will be managed in accordance with the
DEQ Contained In Policy;
 Confirm the location(s) of lead and PAH impacts identified in the COMP-2 evaluation
area to assist in management of shallow soil disturbed as part of planned grubbing and
grading; and
 Complete in situ soil sampling to assist in the management of soil in areas planned for cut
during grading activities.

The DEQ-approved Work Plan also includes collection of soil samples in an off-Site
construction easement located along the northeastern Site boundary. The proposed construction
easement is located on the southern boundary of the adjacent Radio Center Brownfields property
(Brownfields Project No. 19072-15-060). The PD has not completed negotiating access terms of
the easement agreement. Therefore, soil samples proposed for the construction easement were
not collected in November 2022 but will be collected at a later date when access details for the
construction easement have been finalized. The proposed construction easement and proposed
soil sample locations are shown in Figure 3.

Prior to conducting field activities, H&H contacted North Carolina 811, the public utility locator,
to mark subsurface utilities at the Site. H&H also contracted with a private utility locator to
mark utilities which were not identified by the public locator. In addition, H&H directed the
drilling contractor to hand clear each boring to a depth of approximately 5 ft below ground
surface (bgs) to further screen the boring locations for the presence of subsurface utilities prior to
utilizing mechanical drilling equipment.
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The assessment activities were completed in general accordance with DEQ Inactive Hazardous
Sites Branch (IHSB) Guidelines for Assessment and Cleanup of Contaminated Sites (Guidelines)
dated September 2022, the most recent versions of the U.S. Environmental Protection Agency
(EPA) Region IV Laboratory Services and Applied Science Division (LSASD) Field Branches
Quality System and Technical Procedures guidance, and the DEQ-approved Work Plan.

A summary of the soil assessment activities is provided in Section 3.0, a description of the
quality assurance and quality control measures are provided in Section 4.0, and summary and
conclusions based on results of the assessment activities are provided in Section 5.0.
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3.0 Soil Assessment Activities

In November 2022, H&H and Mid-South Environmental (Mid-South) advanced six (6) soil
borings and collected soil samples for laboratory analysis adjacent to the northern and western
sides of the DSCA Soil Management Area to further delineate the soil impacts associated with
the dry cleaner release(s). Five (5) shallow soil borings were advanced in the southeastern
portion of the Site to determine the location(s) of lead and PAH impacts in the COMP-2
evaluation area to assist in management of shallow soil during grading and grubbing. In
addition, twelve (12) composite soil samples were collected from twenty-three (23) soil borings
advanced to assist in management of soil in areas where cut is proposed during grading activities.
The locations of the soil borings are shown in Figure 3.

Soil borings were advanced utilizing a decontaminated stainless-steel hand auger or a
track-mounted direct push technology (DPT) drill rig. During boring advancement, continuous
soil samples were collected from the center of the hand auger bucket or from acetate lined
macrocore DPT sleeves. The soil samples were logged for lithologic description, observed for
obvious evidence of staining and unusual odors, and field screened for the presence of volatile
organic vapors using a calibrated photoionization detector (PID). Obvious evidence of staining
or odor and elevated PID readings were not observed by field personnel during soil boring
advancement. Boring logs including lithologic descriptions and field screening results for each
soil boring are provided in Appendix B.

A discussion of the soil sampling activities and results is provided in the following sections.

3.1 Soil Sampling Activities
Additional Dry Cleaner Release Delineation
Results of previous soil assessments completed by DSCA in the area of the former on-Site dry
cleaner have delineated soil impacted by the dry cleaner release(s) for the purposes of evaluating
potential exposure risks (see the DSCA Soil Management Area on Figure 3). Five soil borings
(BF-SB-01 through BF-SB-05) were advanced along the northern and western sides of the
DSCA Soil Management Area to further delineate the limits of soil that will need to be managed
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using methods outlined in the DEQ Contained-In Policy. In addition, and out of an abundance of
caution, additional dry cleaner release soil delineation samples were collected from soil boring
EX-5A which was advanced along the southwestern side of the DSCA Soil Management Area
(Figure 3) as part of the in situ soil characterization assessment activities discussed further
below.

Soil borings were advanced to a depth of approximately 8 ft bgs along the northern, western, and
southwestern sides of the DSCA Soil Management Area which corresponds to the deepest
planned cut depths based on review of the grading plans and cut-fill analysis. Based on field
observations, one shallow soil sample (between 0 ft bgs and 4 ft bgs) and one deeper soil sample
(between 4 ft bgs and 8 ft bgs) were collected from a 2 ft depth interval at each boring location
(BF-SB-01 through BF-SB-05 and EX-5A) for a total of twelve (12) soil samples. Although no
obvious evidence of impact was observed during the field screening and PID readings were
generally low, a soil sample was collected at each boring from the shallow and deep depth
intervals with the highest PID readings to represent worst-case conditions along the northern,
western, and southwestern sides of the DSCA Soil Management Area.

The soil samples selected for laboratory analysis were placed in dedicated laboratory supplied
sample containers, labeled with the sample identification, date, and requested analysis, and
placed in a laboratory supplied cooler with ice. The samples were delivered to Waypoint
Analytical (Waypoint), a North Carolina certified laboratory, under standard chain of custody
protocols for laboratory analysis. Soil samples were analyzed for PCE, TCE, cis-1,2-
dichloroethene, trans-1,2-dichloroethene, and vinyl chloride by EPA Method 8260.

Confirming Impacts in Southeastern Shallow Soil
Five shallow soil borings (COMP-2A through COMP-2E) were advanced to a depth of
approximately 2 ft bgs in the southeastern portion of the Site to identify the discrete location(s)
of lead and PAH impacts discovered in the Phase II ESA COMP-2 composite soil sample and its
duplicate soil sample. No obvious evidence of impact was observed during field screening
(Appendix B). To be consistent with Phase II ESA soil sampling activities, soil samples for
laboratory analysis were collected from shallow soil (0-2 ft bgs) at each soil boring location.
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The soil samples selected for laboratory analysis were placed in dedicated laboratory supplied
sample containers, labeled with the sample identification, date, and requested analysis, and
placed in a laboratory supplied cooler with ice. The samples were delivered to Waypoint, under
standard chain of custody protocols for laboratory analysis of semi-VOCs (SVOCs) by EPA
Method 8270 and lead by EPA Method 6020.

In-Situ Soil Characterization Sampling
To assist in management of soil generated during grading activities, H&H collected twelve (12)
soil samples from twenty-three (23) soil borings in areas at the Site planned for cut during
grading activities. Based on discussions with the PD and the development engineers, and review
of the most recent version of the cut-fill analysis prepared for the Site, H&H understands that
grading and construction activities for the proposed redevelopment will generate up to
approximately 8,000 cubic yards of soil that will likely need to be transported off-Site to achieve
proposed final grade elevations. An overlay of the most recent version of the cut-fill analysis
prepared by LandDesign is included in Figure 3.

The proposed cut depths in the vicinity of the proposed apartment building range from
approximately 1 to 8 ft bgs. Based on proposed cut depths and the volume of planned export,
H&H divided the areas of proposed cut into five (5) in-situ soil characterization sections (EX-1
through EX-5) and collected soil samples for laboratory analysis in each soil characterization
section. The in-situ soil characterization sections (denoted by EX nomenclature) are depicted on
Figure 3.

Based on proposed excavation depths, five (5) soil borings were advanced to approximately 5 ft
bgs within in situ soil characterization section EX-1 located in the south-central portion of the
Site. Five (5) soil borings were advanced to approximately 2 ft bgs within in situ soil
characterization section EX-2 which is also located in the south-central portion of the Site
(Figure 3). Continuous soil sample aliquots were collected from each soil boring advanced in
each evaluation section and homogenized to form composite samples representative of cut soil in
EX-1 and in EX-2 for a total of two composite soil samples (one for each evaluation section).
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Cut in the area of in situ evaluation area EX-3 will range from approximately 2 to 6 ft bgs and
borings in this evaluation area were advanced to depths corresponding to proposed cut depths at
each boring location. Continuous soil sample aliquots from section EX-3 were homogenized to
form composite samples representative of soil from 0-3 ft bgs and 3-6 ft bgs for a total of two
EX-3 soil samples.

Eight (8) soil borings were advanced to approximately 8 ft bgs in the northern and northeastern
portions of the Site which are identified as in situ soil characterizations sections EX-4 and EX-5
(Figure 3). For each evaluation area, continuous soil samples were collected from each of the
soil borings and homogenized to form composite soil samples representative cut soil from 0-2 ft
bgs, 2-4 ft bgs, 4-6 ft bgs, and 6-8 ft bgs for a total of four EX 4 soil samples and a total of four
EX-5 soil samples.

Composite soil samples selected for laboratory analyses were collected directly into dedicated
laboratory supplied sample containers, labeled with the date, time, and sample identification, and
placed in a laboratory supplied sample cooler with ice. The samples were submitted to Waypoint
under standard chain of custody protocols for analysis of SVOCs by EPA Method 8270 and
RCRA metals plus hexavalent chromium by EPA Methods 6020/7471/7199. One representative
grab soil sample was also collected from each soil characterization section, at each discrete depth
interval represented by a composite soil sample for a total of twelve grab soil samples. The grab
soil samples were collected from undisturbed portions of soil that were not used for field
screening. The samples were collected directly into laboratory supplied glassware and submitted
to Waypoint under standard chain of custody protocols for analysis of VOCs by EPA Method
8260.

Following sampling activities, the soil borings were abandoned and the surfaces were repaired
similar to pre-drilling conditions. Each soil boring location was estimated by measuring from
known benchmarks within the Site building for interior soil boring locations or using a hand-held
global positioning system (GPS) unit for exterior boring locations.
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3.2 Soil Sampling Analytical Results

A tabular summary of the additional dry cleaner release delineation soil sample analytical results
is provided as Table 1, a summary of the COMP-2 confirmation soil sample analytical data is
provided as Table 2, and the in situ soil sample analytical results are summarized in Table 3.
The laboratory analytical reports and chain of custody records are provided in Appendix C.

The laboratory analytical results were compared to the most recent versions of the DEQ PSRGs
dated July 2022. In addition, dry cleaner release delineation soil sample analytical results were
compared to the DEQ Contained-In Policy Unrestricted Use Levels dated June 2016.

Discussions of the laboratory analytical results in comparison to the regulatory screening levels
for each evaluation are included in the following sections.

3.2.1 Additional Dry Cleaner Release Delineation Sampling Analytical Results (Table 1)

As shown in Table 1, a trace level of acetone (0.008 J mg/kg) was detected in additional
delineation boring EX-5A (0-2 ft bgs) at a concentration above the laboratory method detection
limits, but below the DEQ Protection of Groundwater and Residential PSRGs. The “J-flag”
designation indicates the compound was detected above the laboratory method detection limit,
but below the laboratory reporting limit resulting in a laboratory estimated concentration. No
other organic compounds were detected at concentrations above laboratory method detection
limits in the soil samples collected along the northern, western, or southwestern sides of the
DSCA Soil Management Area.

3.2.2 Southeastern Shallow Soil Confirmation Sample Analytical Results (Table 2)

PAHs
Composite soil sample COMP-2 confirmation sample laboratory analytical results are
summarized in Table 2 and indicate that benzo(a)pyrene (6.32 mg/kg) was detected at a
concentration above the DEQ Residential and Industrial/Commercial PSRGs in COMP-2E
collected in an area planned for fill in the northeastern portion of the COMP-2 evaluation area
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(Figure 3). Laboratory analytical results also indicate that benzo(a)anthracene (6.44 mg/kg),
benzo(b)fluoranthene (8.65 mg/kg), dibenzo(a,h)anthracene (0.361 J mg/kg), and indeno(1,2,3-
cd)pyrene (3.80 mg/kg) were detected in soil sample COMP-2E at concentrations above their
respective DEQ Residential PSRGs.

The compound benzo(a)pyrene (0.523 J mg/kg) was also detected at a concentration above the
DEQ Residential PSRG in soil sample COMP-2B collected in an area planned for fill in the
south-central portion of the COMP-2 evaluation area (Figure 3).

No other PAHs were detected at concentrations above the DEQ PSRGs in the remaining
southeastern shallow soil confirmation samples.

Lead
Lead was detected at concentrations above laboratory method detection limits in each
confirmation soil sample collected in the southeastern portion of the Site. Lead was detected in
COMP-2B (490 mg/kg) at a concentration above background levels for the Site area and above
the DEQ Residential PSRG (400 mg/kg). As noted above, soil sample COMP-2B was collected
in an area planned for fill in the south-central portion of the COMP-2 evaluation area.

Lead was also detected in soil sample COMP-2C (125 mg/kg) at a concentration above
background levels for the Site area, but below the DEQ Residential PSRG. Soil sample COMP-
2C was collected in an area planned for shallow cut in the southeastern portion of the Site
(Figure 3).

Because the lead concentrations in the COMP-2B and COMP-2C samples exceed the “Rule of
20” of 100 mg/kg for potentially characteristically hazardous levels, these samples were
submitted for lead analysis by Toxicity Characteristic Leaching Potential (TCLP) methods to
further assist in management of shallow soil within the COMP-2 evaluation area. Results of lead
TCLP analysis indicate that lead concentrations in COMP-2B (0.166 milligrams per liter
{mg/L}) and COMP-2C (0.020 mg/L) do not exceed the Maximum Concentration for Toxicity
Characteristics of 5 mg/L. Therefore, lead concentrations in these samples are not considered to
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be at or above characteristically hazardous levels.

The lead concentrations detected in the remaining COMP-2 confirmation soil samples are below
the DEQ PSRGs, the Rule of 20, and are generally consistent with published background levels
for North Carolina soil.

3.2.3 In-Situ Soil Characterization Sampling Analytical Results (Table 3)

Soil samples were collected in areas of planned cut to assist in management of soil that may need
to be transported off-Site during grading activities for the proposed redevelopment. As discussed
above, soil samples were collected within the EX-1 through EX-5 evaluation sections to
represent soil conditions based on planned cut depths in each evaluation section.

Organic Compounds
As shown in Table 3, in situ soil sample laboratory analytical results identified trace levels of
acetone (up to 0.021 J mg/kg) and n-hexane (up to 0.001 J mg/kg) at concentrations above the
laboratory method detection limits, but below the DEQ Residential and Industrial/Commercial
PSRGs. No other organic compounds were detected at concentrations above the laboratory
method detection limits in the in situ soil samples collected at the Site.

Metals
As expected, several metals were detected at concentrations above laboratory method detection
limits in the soil samples collected at the Site. Hexavalent chromium (1.74 mg/kg) was detected
in sample EX-4 (4-6) at a concentration above the DEQ Residential PSRG of 0.31 mg/kg, but
below the DEQ Industrial/Commercial PSRG of 6.5 mg/kg and appears to be present at
background levels. Cadmium (17.9 mg/kg) was detected at a concentration above the DEQ
Residential PSRG and background levels in characterization sample EX-2.

Lead was detected in EX-2 (2,640 mg/kg) at a concentration above background levels for the
Site area and above the DEQ Residential and Industrial/Commercial PSRGs of 400 mg/kg and
800 mg/kg, respectively. Lead was also detected in the soil sample EX-3 (3-6) at a concentration
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(142 mg/kg) above background levels for the Site area, but below the DEQ Residential PSRG.

Because the lead concentrations in the EX-2 and EX-3 (3-6) soil samples exceed the Rule of 20
of 100 mg/kg for potentially characteristically hazardous levels, these samples were submitted
for lead analysis by TCLP methods to further assist in the management of soil during grading in
these areas of the Site. Results of lead TCLP analysis indicate that lead concentrations in EX-2
(0.060 mg/L) and EX-3 (0.074 mg/L) do not exceed the Maximum Concentration for Toxicity
Characteristics of 5 mg/L. Therefore, lead concentrations in these samples are not considered to
be at or above characteristically hazardous levels.

The remaining metals concentrations detected in the in situ soil samples are consistent with
background concentrations established for the Site area, are below the DEQ Residential PSRGs,
and the Rule of 20 for potentially characteristically hazardous levels.

3.3 Direct Contact Risk Evaluation

The DEQ PSRGs used for comparison to the laboratory analytical results are conservative and
based upon a Target Cancer Risk (TCR) of 1 x 10-6 for potential carcinogenic effects and a
Target Hazard Quotient (THQ) of 0.2 for potential non-carcinogenic effects. The DEQ and EPA
acceptable level for potential carcinogenic risks is a cumulative lifetime incremental
carcinogenic risk (LICR) of 1 x 10-4 or less, and the acceptable level for non-carcinogenic risks
is a cumulative hazard index (HI) of 1.0 or less.

To further evaluate potential direct exposure risks and assist in the management of soil during
redevelopment activities, H&H utilized the DEQ Risk Calculator (July 2022) under hypothetical
“worst-case” residential, non-residential worker, construction worker, and recreator/trespasser
scenarios.

Because compound concentrations were detected above the DEQ PSRGs in the in the COMP-2
confirmation soil samples and in the EX-2 in situ soil characterization section, worst-case risk
calculators were completed for each of these evaluation areas using the highest detected
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compound concentrations. Because no compounds were detected at concentrations above the
DEQ PSRGs (or background levels in the case of metals) in the EX-1, EX-3, EX-4, and EX-5 in
situ soil characterization sections, a combined worst-case risk calculator was completed using the
highest concentration of any compound detected in any of the EX-1, EX-3, EX-4, or EX-5
evaluation areas. Copies of the completed DEQ Risk Calculators are provided in Appendix D,
and tabular summaries of the risk calculator results for each evaluation area and each use
scenario are provided below.

Worst Case COMP-2 Confirmation Soil Samples
Use Scenario LICR HI Risks Exceeded?
Residential 8.5 x 10-5 0.62 No
Non-Residential 5.3 x 10-6 0.047 No
Construction Worker 1.1 x 10-6 0.90 No
Trespasser 4.7 x 10-5 0.34 No

As shown in the table above, results of cumulative risk calculations using the highest compound
concentrations detected in the COMP-2 evaluation area confirmation soil samples indicate that
there are no unacceptable potential carcinogenic or noncarcinogenic risks for a resident, a non-
residential worker, a construction worker, or a trespasser.

EX-2 In Situ Soil Characterization Section
Use Scenario LICR HI Risks Exceeded?
Residential 2.3 x 10-5 3.0 Yes
Non-Residential 5.1 x 10-6 0.21 No
Construction Worker 9.5 x 10-7 0.88 No
Trespasser 1.3 x 10-5 1.7 Yes

Based on the EX-2 in situ soil sample laboratory analytical results, potential cumulative non-
carcinogenic risks for a resident and a trespasser exceed the acceptable risk criteria. There are no
potential cumulative carcinogenic or noncarcinogenic risks for a construction worker or a non-
residential worker in the EX-2 evaluation area.
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Worst Case EX-1, EX-3, EX-4, and EX-5 In Situ Soil Characterization Sections
Use Scenario LICR HI Risks Exceeded?
Residential 1.1 x 10-5 0.19 No
Non-Residential 1.4 x 10-6 0.013 No
Construction Worker 6.8 x 10-7 0.10 No
Trespasser 6.0 x 10-6 0.10 No

Results of cumulative risk calculations using the highest compound concentrations detected in
the EX-1, EX-3, EX-4, or EX-5 evaluation areas indicate that there are no unacceptable potential
carcinogenic or noncarcinogenic risks for a resident, a non-residential worker, a construction
worker, or a trespasser.

3.4 Soil Management Options

As described in the EMP prepared for the Site dated October 10, 2022, soil located outside the
DSCA Soil Management Area that does not have compounds at concentrations above the DEQ
Residential risk thresholds can be reused on-Site in proposed fill areas without restriction.
Because soil sample results indicate compound concentrations within the EX-2 evaluation area
exceed the cumulative noncarcinogenic risks for a resident, soil excavated during grading in this
area can be reused on-Site beneath impervious surfaces or a minimum of 2 ft of demonstrably
clean fill material in accordance with the EMP. Results of DSCA soil assessments and the
supplemental DSCA Soil Management Area delineation samples described in this report indicate
compounds of concern attributable to the on-Site dry cleaner release(s) are not present at
detectable levels outside the extents of the DSCA Soil Management Area shown in Figure 3.
Soil disturbed within the DSCA Soil Management Area during redevelopment activities will be
managed in accordance with the DEQ Contained In Policy.

Soil disturbed during redevelopment activities outside of the DSCA Soil Management Area can
be managed in accordance with a DEQ approved EMP. Based on results of soil assessment
activities completed at the Site, the table below has been prepared to outline soil management
options for soil disturbed outside of the DSCA Soil Management Area.
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Characterization Section Depth
(ft bgs) Management Options Grading
Area
EX-1 0-5 LCID, CDLF, MSWLF, BFP Cut
EX-2 0-2 MSWLF, BFP under cap Cut
EX-3 / COMP-2C / COMP-2D 0-3 LCID, CDLF, MSWLF, BFP Cut
3-6 LCID, CDLF, MSWLF, BFP Cut
EX-4
0-2 LCID, CDLF, MSWLF, BFP Cut
2-4 LCID, CDLF, MSWLF, BFP Cut
4-6 LCID, CDLF, MSWLF, BFP Cut
6-8 LCID, CDLF, MSWLF, BFP Cut
EX-5
0-2 LCID, CDLF, MSWLF, BFP Cut
2-4 LCID, CDLF, MSWLF, BFP Cut
4-6 LCID, CDLF, MSWLF, BFP Cut
6-8 LCID, CDLF, MSWLF, BFP Cut
COMP-2A / COMP-2B / COMP-2E 0-2 MSWLF, BFP under cap Fill

Notes:
Depth listed is based on feet below the existing grade.
LCID = Land Clearing and Inert Debris landfill such as the Old 27 Landfill at 114 Tate Street, Mount Holly, NC
(Old 27) or the Reeves Landfill located at 2323 Salome Church Road, Charlotte, NC (Reeves)
CDLF = Construction & Demolition landfill
MSWLF = Municipal Solid Waste landfill (MSWLF) facility
BFP= Press Club Cleaners Brownfields Property

It is important to note that the above soil management options are based on soil assessment
results in comparison to the DEQ PSRGs and the results of worst-case scenario risk calculations.
If cut depths in an evaluation area extend deeper than the depths of the soil samples, additional
sampling may be required. DEQ Brownfields Program approval will be needed prior to
transporting soil off-Site to a facility other than a Municipal Solid Waste Landfill. Metals
detected in uncontaminated export soil at the Site that is approvable for transport to an LCID
landfill and LCID background metals data for the Old 27 and Reeves Landfills are summarized
in a comparison table provided in Appendix E for ease of reference.
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4.0 Quality Assurance – Quality Control

For quality assurance and quality control purposes (QA/QC), non-dedicated equipment and tools
were decontaminated prior to use at each boring or sampling location or following exposure to
soil or groundwater. Field QA/QC samples were analyzed along with the investigative samples
to determine potential variability introduced in sampling, handling, shipping, and analysis.

Duplicate soil samples were collected to evaluate the precision of the field sampling procedures,
sample matrix variability, and analytical reproducibility. Duplicate soil samples were collected
directly into individual laboratory supplied sample containers using sampling methodologies
described in previous sections. The samples were analyzed for the same parameters as the parent
samples, and the analytical results were compared with those of the parent sample. The
analytical results of the parent sample and the duplicate sample were used to evaluate the
cumulative precision of the analytical method, sample matrix, and sample collection techniques.

Duplicate sample laboratory analytical results for soil samples are presented in the summary
tables (Table 1 for dry cleaner release delineation soil samples and Table 3 for in situ soil
samples). Review of the duplicate sample results for the soil samples did not indicate significant
variability compared with the results of the parent samples.

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5.0 Summary and Conclusions

H&H completed Brownfields soil assessment activities at the Former Press Club Cleaners
Brownfields property located in Charlotte, North Carolina. The assessment activities were
conducted in general accordance with the DEQ Brownfields approved Work Plan dated
November 22, 2022. Brownfields assessment activities included collection of soil samples for
laboratory analysis to further evaluate potential risks associated with the Site and to assist in
management of soil during future redevelopment activities. A brief summary of the Brownfields
soil assessment activities is provided below.

 Laboratory analytical results did not indicate the presence of organic compounds at
concentrations above the DEQ PSRGs or the DEQ Contained In Policy Unrestricted Use
Levels in the supplemental dry cleaner release delineation soil samples. Based on the
results of delineation soil samples, the extent of the DSCA Soil Management Area has
been adequately delineated and will be used to manage soil in accordance with the DEQ
Contained In Policy during grading activities.

 Results of the COMP-2 confirmation soil samples collected from shallow soil in the
southeastern portion of the Site confirm the presence of select PAHs and lead at
concentrations above the DEQ Residential and/or Industrial/Commercial PSRGs. No
other organic compounds were detected at concentrations above the DEQ PSRGs in the
southeastern shallow soil confirmation samples.

Based on results of the confirmation soil sampling activities, PAHs detected in the
original COMP-2 composite soil sample are attributable to conditions at the COMP-2B
and COMP-2E aliquot boring locations with higher concentrations present at COMP-2E.
The COMP-2B and COMP-2E boring locations are in areas planned for fill during future
grading activities (Figure 3) and will be covered with impervious surfaces upon
completion of the proposed development.

Results of confirmation soil sampling activities indicate that the lead concentration
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detected in the original COMP-2 composite soil sample is attributable to conditions at the
COMP-2B aliquot boring location. As noted above, the COMP-2B boring location is
within an area planned for fill during future grading activities and will be below
impervious surfaces upon completion of the proposed development.

Lead was detected in COMP-2B (490 mg/kg) at a concentration above background levels
for the Site area and above the DEQ Residential PSRG. A lower level of lead was also
detected in soil sample COMP-2C (125 mg/kg) at a concentration below the DEQ
Residential PSRG.

Lead concentrations in the COMP-2B and COMP-2C soil samples both exceed the Rule
of 20 (100 mg/kg) for potentially characteristically hazardous levels. Therefore, these
samples were submitted for lead TCLP analysis to further evaluate the detected
concentrations and assist in management of soil during redevelopment activities. TCLP
analytical results indicate that lead concentrations in COMP-2B and COMP-2C do not
exceed the Maximum Concentration for Toxicity Characteristics for lead. Based on
results of the soil assessment activities, lead is not present at characteristically hazardous
levels in the COMP-2 evaluation area.

 Results of the in-situ soil characterization soil assessment completed in areas of proposed
cut did not identify organic compounds at concentrations above the DEQ PSRGs. Lead
(2,640 mg/kg) and cadmium (17.9 mg/kg) were detected at concentrations above
background levels and the DEQ Residential and/or Commercial/Industrial PSRG in
evaluation area EX-2. The remaining concentrations of metals detected in the in situ soil
characterization samples were generally consistent with published background levels for
North Carolina Soil and/or below the DEQ PSRGs.

The lead concentration in the EX-2 soil sample exceeds the Rule of 20 (100 mg/kg) for
potentially characteristically hazardous levels. Therefore, the sample was submitted for
lead TCLP analysis to further evaluate the detected concentration and assist in
management of soil during redevelopment activities. TCLP analytical results indicate
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that lead concentrations in the EX-2 soil sample do not exceed the Maximum
Concentration for Toxicity Characteristics for lead. Based on results of the soil
assessment activities, lead is not present at characteristically hazardous levels in the EX-2
evaluation area.

In summary, results of soil assessment activities have adequately delineated the DSCA Soil
Management Area and soil disturbed within the DSCA Soil Management Area will be managed
in accordance with the DEQ Contained In Policy. Soil sampling results outside of the DSCA
Soil Management Area indicate impacts on the Site are limited to PAHs and metals in select
areas, which is common on historically commercial and industrial use properties in urban areas.
Based on results of the Brownfields soil assessment activities, soil outside of the DSCA Soil
Management Area can easily be managed in accordance with a DEQ Brownfields approved
EMP.

In addition, based on results of the in-situ soil assessment activities, with the exception of excess
soil generated during grading in evaluation area EX-2, export soil can be considered for transport
off-Site to other Brownfields properties, Land Clearing and Inert Debris landfills, Construction
and Debris landfills, and/or other development sites with DEQ prior approval.

Excess soil generated in the area of COMP-2B and COMP-2E and in soil characterization
section EX-2 can be reused as fill on-Site if placed beneath a future building or hardscaped
surfaces, or otherwise will be transported off-Site for disposal at a Municipal Solid Waste
landfill or transported to other Brownfields properties with DEQ prior approval.

Table 1
Summary of Dry Cleaner Release Delineation Soil Sample Analytical Results
Former Press Club Cleaners
Charlotte, North Carolina
Brownfields Project No. 25101-21-060
H&H Job No. TCR-003
Evaluation Area
Sample ID
Date
Depth (ft bgs)0-2 4-6 2-4 2-4 4-6 0-2 6-8 2-4 4-6 0-2 6-8
Sample Type
Units
VOCs (8260D)
Acetone NA NA NA NA NA NA NA NA NA NA NA 0.008 J <0.002 2.8 25 14,000 210,000
cis-1,2-Dichloroethene <0.001 <0.001 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.001 <0.0010 <0.001 <0.001 <0.001 0.35 0.41 31 470
trans-1,2-Dichloroethene <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.54 0.62 15 64
Tetrachloroethene <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0074 0.0063 17 82
Trichloroethene <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.018 0.021 0.87 4.0
Vinyl Chloride <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0006 <0.0007 <0.0006 <0.0006 <0.0007 <0.0006 0.000095 0.00021 0.061 1.7
Notes:1) North Carolina Department of Environmental Quality (DEQ) Division of Waste Management Hazardous Waste Section Contained-In Policy Unrestricted Use Levels (June 2016).
Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.
VOCs = volatile organic compounds; ft bgs= feet below ground surface; NA = not analyzed J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
2) DEQ Preliminary Soil Remediation Goals (PSRGs) dated July 2022.
Dry Cleaner Release Delineation
EX-5A
11/29/2022
mg/kg
Screening Criteria
Unrestricted
Use Level (1)
11/28/2022
4-6 (DUP)
Protection of
Groundwater
PSRGs (2)
Grab
Industrial/
Commercial
PSRGs (2)
Residential
PSRGs (2)
11/28/2022 11/28/2022 11/28/2022 11/28/2022
BF-SB-01 BF-SB-02 / BF-SB-DUP BF-SB-03 BF-SB-04 BF-SB-05
Grab Grab Grab Grab Grab
https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Trammell Crow Residential ‐ TCR/TCR‐003 Press Club Cleaners/Brownfields/In Situ/Report/Data Tables_Press Club Cleaners
12/27/2022
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Table 2
Summary of Shallow Soil Confirmation Soil Sample Analytical Results
Former Press Club Cleaners
Charlotte, North Carolina
Brownfields Project No. 25101-21-060
H&H Job No. TCR-003
Evaluation Area
Sample ID COMP-2A COMP-2B COMP-2C COMP-2D COMP-2E
Date 11/29/2022 11/29/2022 11/29/2022 11/29/2022 11/29/2022
Depth (ft bgs)0-2 0-2 0-2 0-2 0-2
Sample Type Grab Composite Grab Composite Grab Grab Grab Grab Grab Range
Units mg/L
VOCs (8260D)
2-Butanone (MEK)0.0459 J NA 0.0401 J NA NA NA NA NA NA 5,500 40,000 ----
Ethylbenzene 0.0043 J NA 0.0033 J NA NA NA NA NA NA 6.1 27 ----
Naphthalene 0.0062 J NA 0.0048 J NA NA NA NA NA NA 2.1 9 ----
Toluene 0.0085 NA 0.0070 NA NA NA NA NA NA 990 9,700 ----
1,2,4-Trimethylbenzene <0.0021 NA 0.0037 J NA NA NA NA NA NA 63 370 ----
m&p-Xylene 0.0116 J NA 0.0090 J NA NA NA NA NA NA 120 510 ----
o-Xylene 0.0076 J NA 0.0068 NA NA NA NA NA NA 140 590 ----
Xylene (Total)0.0191 NA 0.0159 NA NA NA NA NA NA 120 530 ----
SVOCs (8270E)
Acenaphthylene NA <1.270 NA <1.270 <0.117 <0.116 <0.126 <0.132 0.301 J NE NE -- --
Anthracene NA <1.180 NA 1.450 J <0.160 <0.158 <0.172 <0.179 1.68 3,600 45,000 ----
Benzo(a)anthracene NA <1.200 NA 5.230 <0.156 0.359 J <0.167 <0.174 6.44 1.1 21 ----
Benzo(a)pyrene NA <1.250 NA 3.910 <0.164 0.523 J <0.177 <0.184 6.32 0.11 2.1 ----
Benzo(b)fluoranthene NA <1.200 NA 6.950 0.168 J 0.685 J <0.176 <0.183 8.65 1.1 21 ----
Benzo(g,h,i)perylene NA <1.400 NA 2.560 J <0.152 0.356 J <0.164 <0.171 3.15 NE NE ----
Benzo(k)fluoranthene NA <1.270 NA 3.020 J <0.153 0.183 J <0.165 <0.172 3.05 11 210 ----
Chrysene NA <1.310 NA 7.120 <0.159 0.353 J <0.171 <0.178 5.67 110 2,100 ----
Dibenz(a,h)anthracene NA <1.390 NA <1.390 <0.258 <0.255 <0.277 <0.289 0.361 J 0.11 2.1 ----
Dibenzofuran NA <1.300 NA <1.310 <0.133 <0.132 <0.143 <0.149 0.178 J 16 230 ----
Fluoranthene NA 1.730 J NA 14.300 <0.138 0.469 J <0.148 <0.154 12.4 480 6,000 ----
Fluorene NA <1.270 NA <1.270 <0.143 <0.142 <0.154 <0.161 0.258 J 480 6,000 ----
Indeno(1,2,3-cd)pyrene NA <1.420 NA 2.420 J <0.200 0.372 J <0.215 <0.225 3.80 1.1 21 ----
Naphthalene NA <1.220 NA <1.230 <0.161 <0.159 <0.173 <0.181 0.176 J 2.1 8.8 ----
Phenanthrene NA <1.180 NA 13.300 <0.233 <0.230 <0.250 <0.261 4.01 NE NE ----
Phenol NA <1.610 NA <1.610 <0.125 <0.124 <0.135 <0.140 0.559 J 3,800 49,000 ----
Pyrene NA <1.460 NA 10.000 <0.150 0.482 J <0.161 <0.168 11.1 360 4,500 ----
Metals (6020B/7471B/7199)
Arsenic NA 2.7 NA 2.2 NA NA NA NA NA 0.68 3.0 1.0 - 18 --
Barium NA 75.3 NA 92.3 NA NA NA NA NA 3,100 47,000 50 - 1,000 --
Cadmium NA 1.7 NA 1.3 NA NA NA NA NA 1.4 20 1.0 - 10 --
Chromium (total)NA 38.3 NA 45.5 NA NA NA NA NA NE NE 7.0 - 300 --
Hexavalent Chromium NA 1.67 NA 0.941 J NA NA NA NA NA 0.31 6.5 NS --
Trivalent Chromium NA 36.63 NA 44.56 NA NA NA NA NA 23,000 350,000 NS --
Lead NA 405 NA 296 20.1 490 125 35.1 37.5 400 800 ND - 50 --
Mercury NA 0.070 NA 0.11 NA NA NA NA NA 2.3 9.7 0.03 - 0.52 --
Selenium NA 0.50 J NA 0.39 J NA NA NA NA NA 78 1,200 <0.1 - 0.8 --
Silver NA 0.40 J NA 0.33 J NA NA NA NA NA 78 1,200 ND - 5.0 --
TCLP (6010D)
Lead NA 0.49 mg/L NA 0.60 mg/L NA 0.166 mg/L 0.020 mg/L NA NA -- -- --5
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022.
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. 3) Environmental Protection Agency (EPA) Maximum Concentration of Contaminants for Toxicity Characteristic Leaching Procedure (TCLP) regulatory level dated November 2004.
Concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise shown.Aside from metals, only those compounds detected in at least one sample are shown in the table above. Concentrations are reported to the laboratory method detection limitsLaboratory analytical methods are shown in parentheses.
Bold value indicates an exceedance of the Residential PSRG and background levels in the case of metals
Underlined value indicates an exceedance of the Industrial/Commercial PSRG and background levels in the case of metals. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; NE = not established; ft bgs= feet below ground surface; NS = not specified; -- = not applicable; ND = not detected; NA = not analyzed; mg/L = milligrams per literJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
Screening CriteriaSoutheastern Shallow Soil
0-2
mg/kg
Residential
PSRGs (1)
COMP-2/COMP-DUP
6/15/2022 Industrial/
Commercial
PSRGs (1)
Regional
Background
Metals (2)
Maximum
Concentration
for TCLP (3)
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Table 2 (Page 1 of 1)
Hart & Hickman, PC
Table 3
Summary of In Situ Soil Sample Analytical Results
Former Press Club Cleaners
Charlotte, North Carolina
Brownfields Project No. 25101-21-060
H&H Job No. TCR-003
Evaluation Area
Sample ID COMP-2C COMP-2D
Date 11/29/2022 11/29/2022
Depth (ft bgs)2-4 0-5 0-2 0-2 0-2 0-3 0-2 0-2
Sample Type Grab Composite Grab Composite Grab Composite Grab Grab Range
Units mg/L
VOCs (8260D)
Acetone 0.002 J NA 0.011 J NA 0.018 J NA NA NA 14,000 210,000 -- --
n-Hexane <0.0007 NA 0.001 J NA <0.0008 NA NA NA 160 740 -- --
SVOCs (8270E)--------
Metals (6020B/7471B/7199)
Arsenic NA 0.593 J NA 15.4 NA 1.67 NA NA 0.68 3.0 1.0 - 18 --
Barium NA 62.5 NA 178 NA 51.9 NA NA 3,100 47,000 50 - 1,000 --
Cadmium NA <0.0728 NA 17.9 NA 0.183 J NA NA 1.4 20 1.0 - 10 --
Chromium (total)NA 7.43 NA 92.1 NA 53.7 NA NA NE NE 7.0 - 300 --
Hexavalent Chromium NA <0.160 NA <0.158 NA <0.168 NA NA 0.31 6.5 NS --
Trivalent Chromium NA 7.43 NA 92.1 NA 53.7 NA NA 23,000 350,000 NS --
Lead NA 1.54 NA 2,640 NA 49.3 125 35.1 400 800 ND - 50 --
Mercury NA <0.0133 NA 0.194 NA 0.0481 NA NA 2.3 9.7 0.03 - 0.52 --
Selenium NA <0.818 NA 1.48 J NA <0.884 NA NA 78 1,200 <0.1 - 0.8 --
Silver NA <0.0519 NA 4.62 NA 0.0638 J NA NA 78 1,200 ND - 5.0 --
TCLP (6010D)
Lead NA NA NA 0.060 mg/L NA NA 0.020 mg/L NA -- -- --5
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022.
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. 3) Environmental Protection Agency (EPA) Maximum Concentration of Contaminants for Toxicity Characteristic Leaching Procedure (TCLP) regulatory level dated November 2004. Concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise shown.
Aside from metals, only those compounds detected in at least one sample are shown in the table above. Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.
Bold value indicates an exceedance of the Residential PSRG and background levels in the case of metals.Underlined value indicates an exceedance of the Industrial/Commercial PSRG and background levels in the case of metals. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; NE = not established; ft bgs= feet below ground surface; NS = not specified; -- = not applicable; ND = not detected; NA = not analyzedBDL = below the laboratory detection limit; mg/L = milligrams per liter
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
Screening Criteria
EX-1
11/29/2022
EX-2
11/29/2022
EX-3
11/29/2022 Maximum
Concentration
for TCLP (3)
Regional
Background
Metals (2)Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Proposed Area of Cut
All BDL
mg/kg
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Table 3 (Page 1 of 3)
Hart & Hickman, PC
Table 3
Summary of In Situ Soil Sample Analytical Results
Former Press Club Cleaners
Charlotte, North Carolina
Brownfields Project No. 25101-21-060
H&H Job No. TCR-003
Evaluation Area
Sample ID
Date
Depth (ft bgs)4-6 3-6
Sample Type Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Range
Units mg/L
VOCs (8260D)
Acetone 0.021 J NA 0.006 J NA 0.003 J NA <0.003 NA <0.003 NA <0.003 NA 14,000 210,000 -- --
n-Hexane <0.0008 NA <0.0009 NA <0.0008 NA <0.0009 NA <0.0009 NA <0.0009 NA 160 740 -- --
SVOCs (8270E)--------
Metals (6020B/7471B/7199)
Arsenic NA 2.96 NA 3.43 NA 1.87 NA 1.50 NA 1.06 J NA 0.967 J 0.68 3.0 1.0 - 18 --
Barium NA 79.8 NA 31.2 NA 20.8 NA 11.3 J NA 20.5 NA 19.7 3,100 47,000 50 - 1,000 --
Cadmium NA 0.450 J NA <0.0854 NA <0.0837 NA <0.0890 NA <0.0888 NA <0.0917 1.4 20 1.0 - 10 --
Chromium (total)NA 49.2 NA 42.6 NA 97.2 NA 61.5 NA 61.4 NA 97.5 NE NE 7.0 - 300 --
Hexavalent Chromium NA <0.171 NA <0.187 NA <0.184 NA 1.74 NA <0.189 NA <0.198 0.31 6.5 NS --
Trivalent Chromium NA 49.2 NA 42.6 NA 97.2 NA 59.8 NA 61.4 NA 97.5 23,000 350,000 NS --
Lead NA 142 NA 9.24 NA 8.27 NA 6.28 NA 7.99 NA 8.55 400 800 ND - 50 --
Mercury NA 0.0636 NA 0.140 NA 0.0994 NA <0.0162 NA <0.0162 NA <0.0167 2.3 9.7 0.03 - 0.52 --
Selenium NA <0.876 NA <0.959 NA <0.940 NA <1.00 NA <0.997 NA <1.03 78 1,200 <0.1 - 0.8 --
Silver NA 0.205 J NA <0.0608 NA <0.0596 NA <0.0634 NA <0.0632 NA <0.0653 78 1,200 ND - 5.0 --
TCLP (6010D)
Lead NA 0.074 mg/L NA NA NA NA NA NA NA NA NA NA -- -- --5
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022.
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. 3) Environmental Protection Agency (EPA) Maximum Concentration of Contaminants for Toxicity Characteristic Leaching Procedure (TCLP) regulatory level dated November 2004. Concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise shown.
Aside from metals, only those compounds detected in at least one sample are shown in the table above. Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.
Bold value indicates an exceedance of the Residential PSRG and background levels in the case of metals.Underlined value indicates an exceedance of the Industrial/Commercial PSRG and background levels in the case of metals. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; NE = not established; ft bgs= feet below ground surface; NS = not specified; -- = not applicable; ND = not detected; NA = not analyzedBDL = below the laboratory detection limit; mg/L = milligrams per liter
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
6-8 (DUP)4-6 6-8
EX-3
11/29/2022
EX-4
11/28/2022
0-2
Screening Criteria
Maximum
Concentration
for TCLP (3)
Industrial/
Commercial
PSRGs (1)
Proposed Area of Cut
EX-4 / EX-DUP
mg/kg
EX-4 EX-4
Residential
PSRGs (1)
11/28/2022 11/28/2022 11/28/2022
Regional
Background
Metals (2)2-4
11/28/2022
All BDL
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Table 3 (Page 2 of 3)
Hart & Hickman, PC
Table 3
Summary of In Situ Soil Sample Analytical Results
Former Press Club Cleaners
Charlotte, North Carolina
Brownfields Project No. 25101-21-060
H&H Job No. TCR-003
Evaluation Area
Sample ID
Date
Depth (ft bgs)0-2 0-2 2-4 2-4 4-6 4-6 6-8 6-8
Sample Type Grab Composite Grab Composite Grab Composite Grab Composite Range
Units mg/L
VOCs ( 260D)
Acetone 0.018 J NA 0.005 J NA <0.003 NA <0.003 NA 14,000 210,000 -- --
n-Hexane <0.0009 NA <0.0009 NA <0.0009 NA <0.0009 NA 160 740 -- --
SVOCs (8270E)--------
Metals (6020B/7471B/7199)
Arsenic NA 2.66 NA 1.05 J NA 2.00 NA 1.97 0.68 3.0 1.0 - 18 --
Barium NA 18.5 NA 89.8 NA 19.1 NA 41.3 3,100 47,000 50 - 1,000 --
Cadmium NA <0.0856 NA <0.0932 NA <0.0861 NA <0.0890 1.4 20 1.0 - 10 --
Chromium (total)NA 63.7 NA 37.9 NA 46.5 NA 60.3 NE NE 7.0 - 300 --
Hexavalent Chromium NA <0.188 NA <0.199 NA <0.184 NA <0.190 0.31 6.5 NS --
Trivalent Chromium NA 63.7 NA 37.9 NA 46.5 NA 60.3 23,000 350,000 NS --
Lead NA 8.73 NA 14.1 NA 9.01 NA 6.10 400 800 ND - 50 --
Mercury NA 0.0969 NA 0.0363 J NA 0.0504 NA <0.0162 2.3 9.7 0.03 - 0.52 --
Selenium NA 0.968 J NA <1.05 NA 1.48 J NA 1.27 J 78 1,200 <0.1 - 0.8 --
Silver NA <0.0609 NA <0.0663 NA <0.0613 NA <0.0634 78 1,200 ND - 5.0 --
TCLP (6010D)
Lead NA NA NA NA NA NA NA NA -- -- --5
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022.
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. 3) Environmental Protection Agency (EPA) Maximum Concentration of Contaminants for Toxicity Characteristic Leaching Procedure (TCLP) regulatory level dated November 2004. Concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise shown.
Aside from metals, only those compounds detected in at least one sample are shown in the table above. Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.
Bold value indicates an exceedance of the Residential PSRG and background levels in the case of metals.Underlined value indicates an exceedance of the Industrial/Commercial PSRG and background levels in the case of metals. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; NE = not established; ft bgs= feet below ground surface; NS = not specified; -- = not applicable; ND = not detected; NA = not analyzedBDL = below the laboratory detection limit; mg/L = milligrams per liter
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
Proposed Area of Cut
EX-5 EX-5 EX-5 EX-5
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Regional
Background
Metals (2)
mg/kg
Screening Criteria
Maximum
Concentration
for TCLP (3)
11/28/202211/28/2022 11/28/2022 11/28/2022
ALL BDL
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Table 3 (Page 3 of 3)
Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; USGS Global Ecosystems; U.S. Census
Bureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S.Department of State Humanitarian Information Unit; and NOAA NationalCenters for Environmental Information, U.S. Coastal Relief Model. Datarefreshed June, 2022.
SITE LOCATION MAP
FORMER PRESS CLUB CLEANERSSOUTH BOULEVARD AND HARTFORD AVENUECHARLOTTE, NORTH CAROLINA
DATE: 12-16-22
JOB NO: TCR-003
REVISION NO: 0
FIGURE NO: 1
3921 Sunset Ridge Road, Ste. 301Raleigh, North Carolina 27607919-847-4241 (p) 919-847-4261 (f)License # C-1269 / # C-245 Geology
TITLE
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CHARLOTTE EAST, NORTH CAROLINA 2019CHARLOTTE WEST, NORTH CAROLINA 2019
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
MW-2
MW-4MW-3
MW-1
REVISION NO. 0
JOB NO. TCR-003
DATE: 12-16-22
FIGURE NO. 2
FORMER PRESS CLUB CLEANERSSOUTH BOULEVARD AND HARTFORD AVENUE
CHARLOTTE, NORTH CAROLINA
SITE MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
CATS LIGHT RAIL
POLE-MOUNTED TRANSFORMER
AIR COMPRESSOR
MONITORING WELL
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURGCOUNTY GIS, 2022.
2. BASE DATA OBTAINED FROM MECKLENBURG COUNTYGIS, 2022.
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
(3229 SOUTH BOULEVARD)
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MULTI-TENANT COMMERCIAL
(3401 SOUTH BOULEVARD)
NEFCO(3316 SOUTH BOULEVARD)
BLACK CLOUD TATTOO(3324 SOUTH BOULEVARD)
QUIKTRIP(116 CLANTON ROAD)
FORMER DRY-CLEANING
EQUIPMENT
FORMER BOILER ROOM
UNDER
CONSTRUCTION
RETAINING WALL
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REVISION NO. 0
JOB NO. TCR-003
DATE:12-16-22
FIGURE NO. 3
FORMER PRESS CLUB CLEANERSSOUTH BOULEVARD AND HARTFORD AVENUE
CHARLOTTE, NORTH CAROLINA
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL LINE
CATS LIGHT RAIL
EXISTING BUILDING FOOTPRINT
APPROXIMATE CONTAINED-IN SOIL
MANAGEMENT AREA
EVALUATION AREA
ALIQUOT SOIL BORING LOCATION
SOIL BORING LOCATION
PROPOSED OFF-SITE ALIQUOT SOIL BORING LOCATION
PROPOSED CONSTRUCTION EASEMENT
NOTES:
1. PARCEL DATA OBTAINED FROM MECKLENBURG COUNTYGIS, 2022.
2. CLIENT PROVIDED CUT/FILL HEAT MAP DATED 5/19/22.
3. FT BGS = FEET BELOW GROUND SURFACE.
4. YRD³ = CUBIC YARDS
5. DUE TO ACCESS ISSUES, SAMPLES RCBF-SB-01,RCBF-SB-02, AND RCBF-COMP-1 WERE NOT COLLECTEDDURING NOVEMBER 2022 ASSESMENT ACTIVITIES.
EX-
1
EX-
2
EX-3
SAMPLE ID BORING DEPTH
(FT BGS)
VOLUME OF SOILCHARACTERIZED PER
SAMPLE (YRD³)
EX-1 0-5 888
EX-2 0-2 385
EX-3 0-3 800
3-6 800
EX-4
0-2 445
2-4 445
4-6 445
6-8 445
EX-5
0-2 530
2-4 530
4-6 530
6-8 530
EX-
4
BF-SB-01
BF-SB-02
BF-SB-03
BF-SB-04
BF-SB-05
COMP-2A
COMP-2B
COMP-2E
COMP-2D
COMP-2C
EX-
5
RCBF-SB-01
RCBF-SB-02
RCBF-COMP-1
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Appendix A

June 2022 Phase II ESA Data Tables and Sample Location Map
Table 1
Summary of Soil Analytical Data
Former Press Club Cleaners
Charlotte, North Carolina
H&H Job No. TCR-003
Evaluation Area Western Portion
of the Site
Sample ID COMP-1
Date
Depth (ft bgs)0-2 0-2 0-2
Sample Type Range Mean Range
Units
VOCs (8260D)
2-Butanone (MEK)0.0612 J, C7 0.0459 J, C7 0.0401 J, C7 5,500 40,000 --------
Ethylbenzene <0.0033 0.0043 J 0.0033 J 6.1 27 --------
Naphthalene <0.0038 0.0062 J 0.0048 J 2.1 8.8 --------
Tetrachloroethylene 0.0064 J, C8 <0.0025 <0.0020 17 82 --------
Toluene <0.0020 0.0085 IK 0.0070 IK 990 9,700 --------
1,2,4-Trimethylbenzene <0.0020 <0.0021 0.0037 J 63 370 --------
m&p-Xylene <0.0049 0.0116 J 0.0090 J 120 510 --------
o-Xylene <0.0032 0.0076 J 0.0068 140 590 --------
Xylene (Total)<0.0041 0.0191 0.0159 120 530
SVOCs (8270E)
Anthracene <0.137 <1.180 1.450 J 3,600 45,000 ---- -- --
Benzo(a)anthracene <0.140 <1.200 5.230 1.1 21 --------
Benzo(a)pyrene <0.145 <1.250 3.910 0.11 2.1 ---- -- --
Benzo(b)fluoranthene <0.140 <1.200 6.950 1.1 21 --------
Benzo(g,h,i)perylene <0.163 <1.400 2.560 J NE NE --------
Benzo(k)fluoranthene <0.147 <1.270 3.020 J 11 210 --------
Chrysene <0.152 <1.310 7.120 110 2,100 --------
Fluoranthene <0.143 1.730 J 14.300 480 6,000 --------
Indeno(1,2,3-cd)pyrene <0.165 <1.420 2.420 J 1.1 21 --------
Phenanthrene <0.137 <1.180 13.300 NE NE --------
Pyrene <0.170 <1.460 10.000 360 4,500 --------
Metals (6020B/7471B/7199)
Arsenic 2.3 2.7 2.2 0.68 3.0 --1.0 - 18 4.8 1.28 - 3.03
Barium 41.3 75.3 92.3 3,100 47,000 --50 - 1,000 356 38.1 - 159
Cadmium 0.043 J 1.7 1.3 1.4 20 --1.0 - 10 4.3 ND - 2.49
Chromium (total)44.1 38.3 45.5 NE NE --7.0 - 300 65 59.7 - 174
Chromium (VI)<0.319 1.67 0.941 J 0.31 6.5 --NS NS ND - 0.837
Chromium (III)44.1 36.63 44.56 23,000 350,000 --NS NS 47.1 - 173
Lead 16.8 405 296 400 800 --ND - 50 16 7.33 - 296
Mercury 0.027 0.070 0.11 4.7 70 --0.03 - 0.52 0.121 0.0365 - 0.615
Selenium 0.57 J 0.50 J 0.39 J 78 1,200 --<0.1 - 0.8 0.42 0.566 - 1.04
Silver <0.18 0.40 J 0.33 J 78 1,200 --ND - 5.0 NS ND - 0.716
Metals (6010 TCLP)
Lead --0.49 mg/L 0.60 mg/L -- --5 mg/L -- -- --
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022
2) Environmental Protection Agency (EPA) Maximum Concentrations of Contaminants for Toxicity Characteristics Leaching Procedure (TCLP) regulatory level dated November 2004.
3) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils
4) Local metal background soil sample results from Charlotte Van and Storage and Quality Products Company Brownfields (Brownfields Project No. 23057-19-060).
Soil concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise noted.
Compound concentrations are reported to the laboratory method detection limits
Laboratory analytical methods are shown in parentheses
With the exception of metals, only constituents detected in at least one sample are shown in the table above
Composite soil samples that were analyzed for VOCs were collected from undisturbed portions of soil and placed directly into laboratory supplied glassware
Bold values exceed the Residential PSRGs and background levels in the case of metals.
Underlined values exceed the Industrial/Commercial PSRGs.
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface; NS = not specified; NE = not established; -- = not applicable; ND = not detected; mg/L = milligrams per lite
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
C7 = Analyte is a possible laboratory contaminant (not present in method blank)
C8 = Result may be biased high due to carryover from previously analyzed sample.
IK = The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria. The laboratory reported concentration should be considered an estimated value
mg/kg
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Local Background
Metals in Soil (4)
Composite
COMP-2/COMP-DUP
Maximum
Concentration for
TCLP (2)
Eastern Portion of Site
6/15/2022 Regional Background Metals
in Soil (3)
Screening Criteria
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Table 1 (Page 1 of 1)
Hart & Hickman, PC
Table 2
Summary of Well Construction and Groundwater Depth Data
Former Press Club Cleaners
Charlotte, North Carolina
H&H Job No. TCR-003
Well ID Total Depth
(ft bgs)
Screen Length
(ft)
Screen Interval
(ft bgs)
Depth to
Groundwater (ft bgs)
TOC Elevation
(ft above msl)
Groundwater
Elevation (ft above msl)
MW-1 14 10 4-14 3.86 732.34 728.48
MW-2 20 10 10-20 11.44 739.79 728.35
MW-3 19 10 9-19 11.66 736.78 725.12
MW-4 14 10 4-14 3.24 714.98 711.74
Notes:
Depth to groundwater measurements were collected by H&H on June 15, 2022.
Benchmark elevations estalished by Pittman Professional Land Surveying on May 4, 2017.
TOC = top of casing; ft bgs = feet below ground surface; msl = mean sea level
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Trammell Crow Residential - TCR/TCR-003 Press Club Cleaners/Phase II ESA/Tables/Data Tables 20220727.xlsx8/4/2022
Table 2 (Page 1 of 1)
Hart & Hickman, PC
Table 3
Summary of Groundwater Analytical Data
Former Press Club Cleaners
Charlotte, North Carolina
H&H Job No. TCR-003
Evaluation Area
Sample ID MW-1 MW-2 MW-4
Date
Units
VOCs (8260D)
Chloroform <5.4 <0.43 1.7 1.7 0.83 J 70 0.81 3.6
cis-1,2-Dichloroethylene 165 <0.38 <0.38 <0.38 2.6 70 NE NE
Tetrachloroethylene 2,370 <0.29 <0.29 <0.29 65.6 0.7 12 48
Trichloroethylene 183 <0.38 <0.38 <0.38 1.8 31.04.4
Vinyl Chloride 20.5 <0.39 <0.39 <0.39 <0.39 0.03 0.15 2.5
SVOCs (8270E)ALL BDL ALL BDL ALL BDL ALL BDL ALL BDL ------
Metals (6020B/7470A)
Arsenic <0.087 0.82 J <0.087 <0.087 <0.087 10 NE NE
Barium 21.3 142 165 164 38.3 700 NE NE
Cadmium <0.060 <0.060 0.073 J 0.069 J <0.060 2NENE
Chromium (Total)1.3 0.90 J 2.3 2.3 0.50 J 10 NE NE
Lead <0.077 0.35 J <0.077 0.34 J <0.077 15 NE NE
Mercury <0.12 <0.12 <0.12 <0.12 <0.12 1 0.18 0.75
Selenium 0.10 J 0.14 J <0.072 <0.072 0.093 J 20 NE NE
Silver <0.070 <0.070 <0.070 <0.070 <0.070 20 NE NE
Notes:
1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) dated April 2022.
2) DEQ Division of Waste Management (DWM) Vapor Intrusion Groundwater Screening Levels (GWSLs) dated July 2022.
Concentrations are reported in micrograms per liter (µg/L).
Compound concentrations are reported to the laboratory method detection limits.
Laboratory analytical methods are shown in parentheses.
With the exception of metals, only constituents detected in at least one sample are shown in the table above.
Bold values exceed the 2L Standard.
Underlined values exceed the DWM Residential Vapor Intrusion GWSLs.
Shaded values exceed the DWM Non-Residential Vapor Intrusion GWSLs.
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; NE = not established; -- = not applicable; BDL = below laboratory detection limit
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
µg/L
Screening Criteria
2L Standards (1) Residential
GWSLs (2)
Non-Residential
GWSLs (2)
MW-3/GW-DUP
6/17/2022
Upgradient Downgradient
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9/9/2022
Table 3 (Page 1 of 1)
Hart & Hickman, PC
Table 4
Summary of Exterior and Sub-Slab Soil Gas Analytical Data
Former Press Club Cleaners
Charlotte, North Carolina
H&H Job No. TCR-003
Evaluation Area
Sample ID BF-SSV-1 BF-SG-1 BF-SG-3 BF-SG-5 BF-SG-6 BF-SG-7
Sample Date
Sample Type Sub-Slab Soil Vapor
Units
VOCs (TO-15)
Acetone 190 M 187 M 88.3 M 36.7 M 38.8 M 60.5 38.4 M 13.5 M NE NE
Benzene 0.413 153 159 12.3 10.8 19.9 9.28 0.981 12 160
Bromodichloromethane 29.0 <12.5 <12.2 <12.5 <0.616 <3.18 <12.7 <0.639 2.5 33
1,3-Butadiene <0.190 <4.14 31.8 <4.12 0.914 2.72 <4.20 <0.211 3.1 41
2-Butanone (MEK)10.5 <5.51 21.1 10.6 9.24 18.6 8.91 1.86 35,000 440,000
Carbon disulfide 1.42 965 32.7 7.57 6.43 9.39 <5.91 2.11 4,900 61,000
Carbon tetrachloride 0.790 <11.8 <11.4 <11.7 <0.578 <2.98 <11.9 <0.600 16 200
Chlorobenzene <0.396 <8.60 <41.9 <8.57 0.464 J <2.18 <8.74 <0.439 350 4,400
Chlorodibromomethane 2.09 <15.9 <77.5 <15.9 <0.783 <4.04 <16.2 <0.813 NE NE
Chloroethane <0.227 <4.93 <4.80 <4.91 0.244 JM 1.78 M <5.01 <0.252 28,000 350,000
Chloroform 257 12.6 <8.88 <9.09 0.710 <2.31 <9.27 <0.466 4.1 53
Chloromethane 0.247 M <3.86 <3.76 <3.85 0.378 <0.979 <3.92 0.258 630 7,900
Cyclohexane 2.70 12.1 M <6.26 6.42 J 4.07 M <1.63 <6.53 3.35 M 42,000 530,000
Dichlorodifluoromethane (Freon 12) 2.74 <9.24 <9.00 <9.21 2.58 3.42 <9.39 1.15 700 8,800
1,1-Dichloroethene <0.341 71.8 <7.21 <7.38 <0.365 <1.88 <7.53 <0.378 NE NE
cis-1,2-Dichloroethene 1.88 32,873 20.5 <7.38 0.917 <1.88 <7.53 <0.378 NE NE
trans-1,2-Dichloroethene <0.341 371 <7.21 <7.38 <0.365 <1.88 <7.53 <0.378 NE NE
1,2-Dichloropropane <0.398 <8.64 <8.41 <8.61 0.478 J <2.19 <8.77 <0.441 25 330
Ethanol 114 14.2 J 9.49 J 9.10 J 7.99 7.72 58.2 3.61 NE NE
Ethyl acetate 3.13 <7.68 <7.48 <7.66 2.14 4.24 <7.80 0.891 490 6,100
Ethylbenzene <0.374 185 83.5 M 35.6 39.1 24.8 <8.24 0.546 37 490
4-Ethyltoluene <0.423 32.5 M <44.7 9.43 J 13.4 4.41 M <9.33 <0.469 NE NE
n-Heptane 0.639 42.6 8,348 <7.63 6.20 3,484 53.7 7.29 2,800 35,000
n-Hexane 1.10 216 10,615 7.56 J 6.61 2,687 197 16.8 4,900 61,000
2-Hexanone 1.90 <7.66 <37.3 <7.63 1.31 <1.94 <7.78 0.538 210 2,600
Isopropyl alcohol 9.32 <4.59 <4.47 <4.58 2.47 4.01 J 5.52 J 1.1 J 1,400 18,000
Methyl-tert-butyl ether (MTBE)<0.310 <6.74 <6.56 <6.72 1.46 <1.71 6.84 <0.344 360 4,700
Methyl isobutyl ketone (MIBK) 0.809 M 9.89 <7.45 8.17 J 7.76 <1.94 <7.78 0.438 J 21,000 260,000
Methylene Chloride 1.77 9.97 7.88 <6.47 0.869 M <1.65 10.6 1.05 3,400 53,000
Naphthalene <0.451 <9.80 <47.7 <9.76 0.988 <2.49 <9.95 4.33 2.8 36
Propylene 2.94 110 2,517 68.4 M 74.9 124 M 687 7.27 21,000 260,000
1,1,2,2-Tetrachloroethane <0.591 <12.8 <62.5 <12.8 <0.631 29.7 <13.0 <0.655 1.6 21
Tetrachloroethylene 526 3,549 <61.7 15.6 14.8 4.42 <12.9 1.80 280 3,500
Toluene 0.603 1,135 140 92.2 89.1 41.7 8.36 1.68 35,000 440,000
1,1,1-Trichloroethane 1.46 <10.2 <9.93 <10.2 <0.502 <2.59 <10.4 <0.521 35,000 440,000
Trichloroethylene 7.83 10,011 <9.78 <10.0 1.55 <2.55 <10.2 <0.513 14 180
Trichlorofluoromethane (Freon 11) 2.42 <10.5 <10.2 <10.5 1.25 2.88 J <10.7 0.804 NE NE
1,1,2-Trichlorotrifluoroethane (Freon 113) 0.718 J, M <14.3 <13.9 <14.3 <0.705 <3.63 <14.5 <0.731 35,000 440,000
1,2,4-Trimethylbenzene <0.423 45.3 <44.7 16.9 M 27.1 4.53 <9.33 0.506 J, M 420 5,300
1,3,5-Trimethylbenzene <0.423 19.4 <44.7 <9.16 6.99 <2.33 <9.33 <0.469 420 5,300
Vinyl chloride 0.572 6,778 <5.31 <4.76 0.726 <1.21 <4.85 <0.244 5.6 280
o-Xylene <0.428 175 <39.5 27.3 36.1 11.3 <8.24 0.721 700 8,800
m&p-Xylene 0.412 J 703 74.7 80.0 93.3 27.3 9.78 M 1.44 700 8,800
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Vapor Intrusion Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs) dated July 2022.
Concentrations are reported in micrograms per cubic meter (µg/m3).
Compound concentrations are reported to the laboratory method detection limits.
Laboratory analytical method is shown in parentheses.
Only compounds detected in at least one sample are shown in the above table.
Bold values exceed the DWM Residential Vapor Intrusion SGSL.
Underlined values indicate an exceedance of DWM Non-Residential SGSL.
VOCs = volatile organic compounds; NE = not established
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
M = Laboratory manual integration.
µg/m3
Screening Criteria
Residential
SGSLs (1)
Non-Residential
SGSLs (1)6/16/2022
Exterior Soil Gas
BF-SG-4/BF-SG-DUP
Proposed Residential UnitsProposed Parking Deck
https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Trammell Crow Residential ‐ TCR/TCR‐003 Press Club Cleaners/Phase II ESA/Tables/Data Tables 20220817_ABM
9/9/2022
Table 4 (Page 1 of 1)
Hart & Hickman, PC
MW-2
MW-4MW-3
MW-1
REVISION NO. 0
JOB NO. TCR-003
DATE: 8-5-22
FIGURE NO. 3
FORMER PRESS CLUB CLEANERS
SOUTH BOULEVARD AND HARTFORD AVENUE
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
CATS LIGHT RAIL
EXISTING BUILDING FOOTPRINT
MONITORING WELL
PROPOSED RESIDENTIAL UNITS
PROPOSED PARKING DECK
SUB-SLAB SOIL GAS MONITORINGPOINT
EXTERIOR SOIL GAS ANDMONITORING POINT
ALIQUOT SOIL BORING LOCATION
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURGCOUNTY GIS, 2022.
2. BASE DATA OBTAINED FROM MECKLENBURG COUNTYGIS, 2022.
3. PROPOSED REDEVELOPMENT PLAN BASED ON SITE PLANPREPARED BY HORD, COPLAN, AND MACHT DATEDOCTOBER 27, 2021.
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
VACANT LAND(3229 SOUTH BOULEVARD)
WES
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RESIDENTIAL
MULTI-TENANT COMMERCIAL(3401 SOUTH BOULEVARD)
BLUME SUPPLY INC.(3316 SOUTH BOULEVARD)
GRACIE BARRABRIZILLIAN JIU-JITSU(3324 SOUTH BOULEVARD)
QUIKTRIP(116 CLANTON ROAD)
STAIRWELL
ELEVATOR PIT
STAIRWELL
ELEVATOR PIT
ELEVATOR PIT
STAIRWELL
COMP-1
COMP-2
BF-SG-1
BF-SSV-1
BF-SG-2
BF-SG-4
BF-SG-5
BF-SG-3
BF-SG-6
BF-SG-7
S:
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Appendix B

Boring Logs
NOTES: Hole precleared by MidSouth using hand auger. Boring hand cleared to 5 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-01
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Direct Push
GeoProbe
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT (ML); little clay, stiff, moist, reddish orange
(2') SILT (ML); little clay, medium stiff, moist, reddish orange
(6') SILT (ML); little clay, medium stiff, moist, reddish orange with tan mottling
4.3
4.1
5.5
4.3
BF-SB-01
(0-2)
BF-SB-01
(4-6)
0
5
10
(8') Boring terminated
NOTES: Hole precleared by MidSouth using hand auger. Boring hand cleared to 5 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-02
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Direct Push
GeoProbe
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT (ML); little clay, medium stiff, moist, reddish orange
(3') SILT (ML); little clay, medium stiff, moist, reddish orange, few gravel
(5') SILT (ML); little clay, medium stiff, moist, reddish orange with tan mottling, few
gravel
(8') Boring terminated
3.9
4.2
5.8
2.7
BF-SB-02
(2-4)
BF-SB-02
(4-6)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring hand cleared to 5 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-03
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Direct Push
GeoProbe
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT (ML); little clay, stiff, moist, reddish orange
(2') SILT (ML); little clay, medium stiff, moist, reddish orange
(7') SILT (ML); little clay, medium stiff, moist, reddish orange with tan mottling
(8') Boring terminated
2.4
2.6
3.7
3.5
BF-SB-03
(2-4)
BF-SB-03
(4-6)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring hand cleared to 5 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-04
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Direct Push
GeoProbe
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT (ML); little clay, medium stiff, moist, reddish orange
(5') SILT (ML); little clay, medium stiff, moist, tan with orange mottling
(8') Boring terminated
2.1
2.0
4.7
4.8
BF-SB-04
(0-2)
BF-SB-04
(6-8)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 8 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
BF-SB-05
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Concrete
(0.5') SILT (ML); little clay, medium stiff, moist, reddish orange
(8') Boring terminated
2.2
3.8
2.1
1.5
BF-SB-05
(2-4)
BF-SB-05
(4-6)
0
5
10
NOTES: Hole precleared by Mid-South using hand auger. Boring advanced with hand auger to 8 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-5A
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
Mid-South
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Concrete
(0.5') SILT (ML); little clay, medium stiff, moist, reddish orange and brown, some
organic matter, slight organic odor
(2') SILT (ML); little clay, medium stiff, moist, reddish orange
(8') Boring terminated
2.7
2.6
2.7
2.8
EX-5A(0-2)
EX-5A(6-8)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
COMP-2A
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') Well-graded GRAVEL (GW); /grass/asphalt
(0.25') SILT (ML); little clay, medium stiff, moist, reddish brown, trace asphalt
(2') Boring terminated
0.2 COMP-2A
0
1
2
3
4
5
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
COMP-2B
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') Asphalt
(0.25') Well-graded SAND (SW); little silt, medium dense, moist, white
(1') SILT (ML); little fine-medium sand, medium stiff, moist, black, chunks of
consolidated sand, little asphalt
(2') Boring terminated
0.3 COMP-2B
0
1
2
3
4
5
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
COMP-2C
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') ORGANIC SOIL (OL)
(0.25') SILT (ML); little clay, medium stiff, moist, reddish orange and brown, trace
asphalt
(2') Boring terminated
0.5 COMP-2C
0
1
2
3
4
5
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
COMP-2D
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') ORGANIC SOIL (OL)
(0.25') SILT (ML); little clay, medium stiff, moist, reddish orange and brown, trace
asphalt
(2') Boring terminated
0.5 COMP-2D
0
1
2
3
4
5
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
COMP-2E
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Grab
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') ORGANIC SOIL (OL)
(0.25') SILT (ML); little clay, medium stiff, moist, reddish orange and brown, little
organic matter
(1') SILT (ML); little fine-medium sand, medium stiff, moist, black and light gray, some
chunks of consolidated yellow/red sand, trace asphalt
(2') Boring terminated
1.1 COMP-2E
0
1
2
3
4
5
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 5 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-1 (A)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT with sand (ML); little fine-medium sand, medium stiff, moist, light brown
(5') Boring terminated
2.8
4.6
5.5
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 5 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-1 (B)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT (ML); medium stiff, moist, brown
(1') Asphalt
(2') SILT (ML); medium stiff, moist, tan and orange
(5') Boring terminated
4.3
5.3
3.5
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 5 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-1 (C)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5
3.25
Grab/Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT with sand (ML); little fine-medium sand, medium stiff, moist, brown
(2') Asphalt
(2.5') SILT (ML); little clay, medium stiff, moist, red and orange mottled
(5') Boring terminated
4.2
5.7
0.7
EX-1(0-5)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 5 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-1 (D)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT (ML); little clay, medium stiff, moist, reddish orange
(5') Boring terminated
2.0
3.7
2.9
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 5 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-1 (E)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
5.0
3.25
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') Well-graded SAND with silt (SW-SM); little silt, medium dense, moist, light brown
(3') Asphalt
(3.5') SILT (ML); few fine-medium sand, medium stiff, moist, black/yellow/red
(5') Boring terminated
3.1
2.2
1.5
0
5
10
Composite
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-2 (A)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') Well-graded GRAVEL (GW)
(0.25') Poorly graded SAND with silt (SP-SM); few silt, medium dense, moist, light
brown
(1') Poorly graded SAND with silt (SP-SM); few silt, medium dense, moist, dark brown,
0.1
0
1
2
3
4
5
some ashpalt
(2') Boring terminated
NOTES: Hole precleared by MidSouth using hand auger. Boring hand cleared to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-2 (B)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') Asphalt
(0.25') Well-graded SAND with silt (SW-SM); little silt, medium dense, moist, black
(1.5') Well-graded SAND with silt (SW-SM); little silt, medium dense, moist, white,
some gravel
(2') Boring terminated
1.2
0
1
2
3
4
5
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-2 (C)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Grab/Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') Asphalt
(0.5') SILT (ML); little clay, medium stiff, moist, reddish brown, little asphalt
(1') Well-graded SAND with silt (SW-SM); little silt, medium dense, moist, black, clumps
of yellow sand
(2') Boring terminated
2.9 EX-2(0-2)
0
1
2
3
4
5
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-2 (D)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') Asphalt
(0.25') SILT (ML); little clay, medium stiff, moist, reddish brown with tan mottling, some
asphalt
(2') Boring terminated
0.9
0
1
2
3
4
5
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-2 (E)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
MidSouth
Other
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') Asphalt
(0.25') SILT (ML); little clay, medium stiff, moist, reddish brown, some asphalt
(2') Boring terminated
0.6
0
1
2
3
4
5
11/29/22
11/29/22
Hand Auger
Don Warren
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-3 (A)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') ORGANIC SOIL (OL); few fine-coarse gravel
(0.25') SILT (ML); little clay, medium stiff, moist, reddish orange and brown, little
asphalt and organic matter
(1') Well-graded GRAVEL (GW); with asphalt
1.5
0
1
2
3
4
5
(2') Boring terminated
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 6 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-3 (B)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') ORGANIC SOIL (OL)
(0.25') SILT (ML); little clay, medium stiff, moist, reddish orange and brown, little
organic matter and asphalt
(6') Boring terminated
1.8
2.7
3.0
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 6 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-3 (C)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6
3.25
Grab/Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') ORGANIC SOIL (OL)
(0.25') SILT (ML); little clay, medium stiff, moist, reddish orange and brown
(6') Boring terminated
4.5
4.1
4.2
EX-3(0-3)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 6 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-3 (D)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6
3.25
Grab/Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') ORGANIC SOIL (OL)
(0.25') SILT (ML); little clay, medium stiff, moist, reddish orange and brown, little
asphalt
(6') Boring terminated
2.7
5.0
4.6
EX-3(3-6)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 2 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-3 (E)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/29/22
11/29/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
1
2
3
4
5
(0') ORGANIC SOIL (OL)
(0.25') SILT (ML); little clay, medium stiff, moist, reddish orange and brown, little
organic matter and asphalt
(2') Boring terminated
2.2
0
1
2
3
4
5
NOTES: Hole precleared by MidSouth using hand auger. Boring hand cleared to 5 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-4 (A)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
141/28/22
11/28/22
MidSouth
Direct Push
GeoProbe
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT (ML); little clay, medium stiff, moist, reddish orange
(6') SILT (ML); little clay, medium stiff, moist, reddish orange with tan mottling
3.5
2.5
5.0
5.1
0
5
10
(8') Boring terminated
NOTES: Hole precleared by MidSouth using hand auger. Boring hand cleared to 5 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-4 (B)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Direct Push
GeoProbe
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab/Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT (ML); little clay, medium stiff, moist, reddish orange
(6') SILT (ML); little clay, medium stiff, moist, reddish orange with tan mottling
(8') Boring terminated
1.3
2.6
7.4
7.6
EX-4(4-6)
EX-4(6-8)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 8 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-4 (C)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab/Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Concrete
(0.5') SILT (ML); little clay, medium stiff, moist, reddish orange
(5') SILT (ML); little clay, medium stiff, moist, reddish orange with tan mottling
(8') Boring terminated
3.6
3.9
3.2
2.7
EX-4(0-2)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring hand cleared to 5 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-4 (D)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Direct Push
GeoProbe
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab/Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT (ML); little clay, medium stiff, moist, reddish orange
(6') SILT (ML); little clay, medium stiff, moist, reddish orange with tan mottling
(8') Boring terminated
2.9
4.0
5.4
6.2
EX-4(2-4)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 8 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-5 (A)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Concrete
(0.5') SILT (ML); little clay, medium stiff, moist, black, trace organic matter, slight
organic odor
(1') SILT (ML); little clay, medium stiff, moist, reddish orange, little gravel
1.1
2.2
2.7
2.8
0
5
10
(8') Boring terminated
NOTES: Hole precleared by MidSouth using hand auger. Boring hand cleared to 5 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-5 (B)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Direct Push
GeoProbe
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab/Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.25') SILT (ML); little clay, medium stiff, moist, reddish orange
(5') SILT (ML); little clay, medium stiff, moist, reddish orange with tan and black mottling
(8') Boring terminated
7.1
3.9
5.5
7.5
EX-5(0-2)
EX-5(4-6)
EX-5(6-8)
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring hand cleared to 5 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-5 (C)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Direct Push
GeoProbe
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.25') SILT (ML); little clay, medium stiff, moist, reddish orange
(5') SILT (ML); little clay, medium stiff, moist, reddish orange with tan and black mottling
(8') Boring terminated
4.0
2.4
4.5
6.0
0
5
10
NOTES: Hole precleared by MidSouth using hand auger. Boring advanced to 8 ft bgs with hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Trammell Crow Residential
TCR-003
South Blvd & Hartford Ave,Charlotte, NC
BORING LOG
Boring No.
Page:
EX-5 (D)
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
11/28/22
11/28/22
MidSouth
Other
Hand Auger
Don Warren
Erin Lash
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
8
3.25
Grab/Composite
DE
P
T
H

(
f
t
)
LI
T
H
O
L
O
G
Y
WA
T
E
R

L
E
V
E
L
BO
R
I
N
G
CO
M
P
L
E
T
I
O
N
COLLECT
Sa
m
p
l
e

T
y
p
e
Ti
m
e
Bl
o
w

C
o
u
n
t
s
Re
c
o
v
e
r
y

(
f
t
)
SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PI
D

(
p
p
m
)
La
b

S
a
m
p
l
e
DE
P
T
H

(
f
t
)
0
5
10
(0') Asphalt
(0.5') SILT (ML); little clay, medium stiff, moist, reddish orange
(5') SILT (ML); little clay, medium stiff, moist, reddish orange with tan mottling
(8') Boring terminated
1.2
5.2
2.5
1.1
EX-5(2-4)
0
5
10

Appendix C

Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/21/2022
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-334-0100 Client Project Description: TCR-003
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 11/30/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 220
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2022KY90047State ProgramKentucky
12/31/2022LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2022415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
02/11/202302027State ProgramTennessee
09/30/2022T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/22-334-0100
Page 2 of 220
Report Number:
Sample Summary Table
Client Project Description:
22-334-0100
TCR-003
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
11/29/2022 15:10Solids 94336 EX-1 (0-5)11/30/2022 13:44
11/29/2022 15:10Solids 94336 EX-1 (0-5)11/30/2022 13:44 SW-7199 WP MTN -
11/29/2022 14:15Solids 94337 EX-2 (0-2)11/30/2022 13:44
11/29/2022 14:15Solids 94337 EX-2 (0-2)11/30/2022 13:44 SW-7199 WP MTN -
11/29/2022 13:20Solids 94338 EX-3 (0-3)11/30/2022 13:44
11/29/2022 13:20Solids 94338 EX-3 (0-3)11/30/2022 13:44 SW-7199 WP MTN -
11/29/2022 13:25Solids 94339 EX-3 (3-6)11/30/2022 13:44
11/29/2022 13:25Solids 94339 EX-3 (3-6)11/30/2022 13:44 SW-7199 WP MTN -
11/28/2022 13:30Solids 94340 EX-4 (0-2)11/30/2022 13:44
11/28/2022 13:30Solids 94340 EX-4 (0-2)11/30/2022 13:44 SW-7199 WP MTN -
11/28/2022 13:45Solids 94341 EX-4 (2-4)11/30/2022 13:44
11/28/2022 13:45Solids 94341 EX-4 (2-4)11/30/2022 13:44 SW-7199 WP MTN -
11/28/2022 13:55Solids 94342 EX-4 (4-6)11/30/2022 13:44
11/28/2022 13:55Solids 94342 EX-4 (4-6)11/30/2022 13:44 SW-7199 WP MTN -
11/28/2022 14:00Solids 94343 EX-4 (6-8)11/30/2022 13:44
11/28/2022 14:00Solids 94343 EX-4 (6-8)11/30/2022 13:44 SW-7199 WP MTN -
11/28/2022 14:50Solids 94344 EX-5 (0-2)11/30/2022 13:44
11/28/2022 14:50Solids 94344 EX-5 (0-2)11/30/2022 13:44 SW-7199 WP MTN -
11/28/2022 15:00Solids 94345 EX-5 (2-4)11/30/2022 13:44
11/28/2022 15:00Solids 94345 EX-5 (2-4)11/30/2022 13:44 SW-7199 WP MTN -
11/28/2022 15:10Solids 94346 EX-5 (4-6)11/30/2022 13:44
11/28/2022 15:10Solids 94346 EX-5 (4-6)11/30/2022 13:44 SW-7199 WP MTN -
11/28/2022 15:20Solids 94347 EX-5 (6-8)11/30/2022 13:44
11/28/2022 15:20Solids 94347 EX-5 (6-8)11/30/2022 13:44 SW-7199 WP MTN -
11/29/2022 09:45Solids 94348 EX-5A (0-2)11/30/2022 13:44
11/29/2022 09:50Solids 94349 EX-5A (6-8)11/30/2022 13:44
11/28/2022Solids 94350 EX-Dup 11/30/2022 13:44
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 220
Report Number:
Sample Summary Table
Client Project Description:
22-334-0100
TCR-003
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
11/28/2022Solids 94350 EX-Dup 11/30/2022 13:44 SW-7199 WP MTN -
11/28/2022 12:15Solids 94351 BF-SB-01 (0-2)11/30/2022 13:44
11/28/2022 12:20Solids 94352 BF-SB-01 (4-6)11/30/2022 13:44
11/28/2022 12:30Solids 94353 BF-SB-02 (2-4)11/30/2022 13:44
11/28/2022 12:35Solids 94354 BF-SB-02 (4-6)11/30/2022 13:44
11/28/2022 11:35Solids 94355 BF-SB-03 (2-4)11/30/2022 13:44
11/28/2022 11:40Solids 94356 BF-SB-03 (4-6)11/30/2022 13:44
11/28/2022 11:55Solids 94357 BF-SB-04 (0-2)11/30/2022 13:44
11/28/2022 12:00Solids 94358 BF-SB-04 (6-8)11/30/2022 13:44
11/28/2022 10:20Solids 94359 BF-SB-05 (2-4)11/30/2022 13:44
11/28/2022 10:25Solids 94360 BF-SB-05 (4-6)11/30/2022 13:44
11/28/2022Solids 94361 BF-SB-DUP 11/30/2022 13:44
11/29/2022 12:20Solids 94362 COMP-2A 11/30/2022 13:44
11/29/2022 12:20Solids 94362 COMP-2A 11/30/2022 13:44 6020B WP MTN -
11/29/2022 12:25Solids 94363 COMP-2B 11/30/2022 13:44
11/29/2022 12:25Solids 94363 COMP-2B 11/30/2022 13:44 6020B WP MTN -
11/29/2022 11:35Solids 94364 COMP-2C 11/30/2022 13:44
11/29/2022 11:35Solids 94364 COMP-2C 11/30/2022 13:44 6020B WP MTN -
11/29/2022 11:45Solids 94365 COMP-2D 11/30/2022 13:44
11/29/2022 11:45Solids 94365 COMP-2D 11/30/2022 13:44 6020B WP MTN -
11/29/2022 12:30Solids 94366 COMP-2E 11/30/2022 13:44
11/29/2022 12:30Solids 94366 COMP-2E 11/30/2022 13:44 6020B WP MTN -
11/29/2022 14:15TCLP 95246 EX-2 (0-2)11/30/2022 13:44
11/29/2022 13:25TCLP 95247 EX-3 (3-6)11/30/2022 13:44
11/29/2022 12:25TCLP 95652 COMP-2B 11/30/2022 13:44
11/29/2022 11:35TCLP 95653 COMP-2C 11/30/2022 13:44
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 4 of 220
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-334-0100
Report Limit
Project:TCR-003
V 94336EX-1 (0-5)
J0.593 12/08/2022 19:116020BArsenicmg/Kg - dry 0.151
62.5 12/08/2022 19:116020BBariummg/Kg - dry 1.55
7.43 12/08/2022 19:116020BChromiummg/Kg - dry 0.218
1.54 12/08/2022 19:116020BLeadmg/Kg - dry 0.161
J0.002 12/01/2022 13:268260DAcetonemg/Kg - dry 0.002
9.46 12/01/2022 18:23SW-DRYWT Moisture %
V 94337EX-2 (0-2)
15.4 12/08/2022 16:366020BArsenicmg/Kg - dry 0.153
178 12/08/2022 16:366020BBariummg/Kg - dry 1.56
17.9 12/08/2022 16:366020BCadmiummg/Kg - dry 0.0735
92.1 12/08/2022 16:366020BChromiummg/Kg - dry 0.220
2640 12/08/2022 17:226020BLeadmg/Kg - dry 0.814
J1.48 12/08/2022 16:366020BSeleniummg/Kg - dry 0.826
4.62 12/08/2022 16:366020BSilvermg/Kg - dry 0.0523
0.194 12/05/2022 13:487471BMercury (Total)mg/Kg - dry 0.0134
J0.011 12/01/2022 13:548260DAcetonemg/Kg - dry 0.002
J0.001 12/01/2022 13:548260Dn-Hexane mg/Kg - dry 0.0007
10.3 12/01/2022 18:23SW-DRYWT Moisture %
V 94338EX-3 (0-3)
1.67 12/08/2022 17:296020BArsenicmg/Kg - dry 0.163
51.9 12/08/2022 17:296020BBariummg/Kg - dry 1.67
J0.183 12/08/2022 17:296020BCadmiummg/Kg - dry 0.0787
53.7 12/08/2022 17:296020BChromiummg/Kg - dry 0.236
49.3 12/08/2022 17:296020BLeadmg/Kg - dry 0.174
J0.0638 12/08/2022 17:296020BSilvermg/Kg - dry 0.0560
0.0481 12/05/2022 13:577471BMercury (Total)mg/Kg - dry 0.0143
J0.018 12/01/2022 14:218260DAcetonemg/Kg - dry 0.002
16.2 12/01/2022 18:23SW-DRYWT Moisture %
V 94339EX-3 (3-6)
2.96 12/08/2022 17:356020BArsenicmg/Kg - dry 0.162
79.8 12/08/2022 17:356020BBariummg/Kg - dry 1.66
J0.450 12/08/2022 17:356020BCadmiummg/Kg - dry 0.0781
49.2 12/08/2022 17:356020BChromiummg/Kg - dry 0.234
142 12/08/2022 17:356020BLeadmg/Kg - dry 0.173
J0.205 12/08/2022 17:356020BSilvermg/Kg - dry 0.0556
Page 5 of 220
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-334-0100
Report Limit
Project:TCR-003
V 94339EX-3 (3-6)
0.0636 12/05/2022 14:007471BMercury (Total)mg/Kg - dry 0.0142
J0.021 12/01/2022 14:498260DAcetonemg/Kg - dry 0.002
15.5 12/01/2022 18:23SW-DRYWT Moisture %
V 94340EX-4 (0-2)
3.43 12/08/2022 18:006020BArsenicmg/Kg - dry 0.177
31.2 12/08/2022 18:006020BBariummg/Kg - dry 1.81
42.6 12/08/2022 18:006020BChromiummg/Kg - dry 0.256
9.24 12/08/2022 18:006020BLeadmg/Kg - dry 0.189
0.140 12/07/2022 10:357471BMercury (Total)mg/Kg - dry 0.0155
J0.006 12/01/2022 15:168260DAcetonemg/Kg - dry 0.003
22.8 12/01/2022 18:23SW-DRYWT Moisture %
V 94341EX-4 (2-4)
1.87 12/08/2022 18:076020BArsenicmg/Kg - dry 0.174
20.8 12/08/2022 18:076020BBariummg/Kg - dry 1.78
97.2 12/08/2022 18:076020BChromiummg/Kg - dry 0.251
8.27 12/08/2022 18:076020BLeadmg/Kg - dry 0.185
0.0994 12/05/2022 14:027471BMercury (Total)mg/Kg - dry 0.0152
J0.003 12/01/2022 15:438260DAcetonemg/Kg - dry 0.003
21.2 12/01/2022 18:23SW-DRYWT Moisture %
V 94342EX-4 (4-6)
1.50 12/08/2022 18:136020BArsenicmg/Kg - dry 0.185
J11.3 12/08/2022 18:136020BBariummg/Kg - dry 1.89
61.5 12/08/2022 18:136020BChromiummg/Kg - dry 0.267
6.28 12/08/2022 18:136020BLeadmg/Kg - dry 0.197
1.74 12/06/2022 19:29SW-7199 Chromium, Hexavalent mg/Kg - dry 0.195
25.9 12/01/2022 18:23SW-DRYWT Moisture %
V 94343EX-4 (6-8)
J1.06 12/08/2022 18:206020BArsenicmg/Kg - dry 0.184
20.5 12/08/2022 18:206020BBariummg/Kg - dry 1.88
61.4 12/08/2022 18:206020BChromiummg/Kg - dry 0.266
7.99 12/08/2022 18:206020BLeadmg/Kg - dry 0.197
25.7 12/01/2022 18:23SW-DRYWT Moisture %
V 94344EX-5 (0-2)
2.66 12/08/2022 18:266020BArsenicmg/Kg - dry 0.178
Page 6 of 220
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-334-0100
Report Limit
Project:TCR-003
V 94344EX-5 (0-2)
18.5 12/08/2022 18:266020BBariummg/Kg - dry 1.82
63.7 12/08/2022 18:266020BChromiummg/Kg - dry 0.256
8.73 12/08/2022 18:266020BLeadmg/Kg - dry 0.189
J0.968 12/08/2022 18:266020BSeleniummg/Kg - dry 0.961
0.0969 12/05/2022 14:057471BMercury (Total)mg/Kg - dry 0.0156
J0.018 12/01/2022 17:058260DAcetonemg/Kg - dry 0.003
22.9 12/01/2022 18:23SW-DRYWT Moisture %
V 94345EX-5 (2-4)
J1.05 12/08/2022 18:326020BArsenicmg/Kg - dry 0.194
89.8 12/08/2022 18:326020BBariummg/Kg - dry 1.98
37.9 12/08/2022 18:326020BChromiummg/Kg - dry 0.279
14.1 12/08/2022 18:326020BLeadmg/Kg - dry 0.206
J0.0363 12/05/2022 14:077471BMercury (Total)mg/Kg - dry 0.0169
J0.005 12/01/2022 17:338260DAcetonemg/Kg - dry 0.003
29.2 12/01/2022 18:23SW-DRYWT Moisture %
V 94346EX-5 (4-6)
2.00 12/08/2022 18:396020BArsenicmg/Kg - dry 0.179
19.1 12/08/2022 18:396020BBariummg/Kg - dry 1.83
46.5 12/08/2022 18:396020BChromiummg/Kg - dry 0.258
9.01 12/08/2022 18:396020BLeadmg/Kg - dry 0.191
J1.48 12/08/2022 18:396020BSeleniummg/Kg - dry 0.967
0.0504 12/05/2022 14:107471BMercury (Total)mg/Kg - dry 0.0157
23.4 12/02/2022 12:17SW-DRYWT Moisture %
V 94347EX-5 (6-8)
1.97 12/08/2022 18:456020BArsenicmg/Kg - dry 0.185
41.3 12/08/2022 18:456020BBariummg/Kg - dry 1.89
60.3 12/08/2022 18:456020BChromiummg/Kg - dry 0.267
6.10 12/08/2022 18:456020BLeadmg/Kg - dry 0.197
J1.27 12/08/2022 18:456020BSeleniummg/Kg - dry 1.00
25.9 12/02/2022 12:17SW-DRYWT Moisture %
V 94348EX-5A (0-2)
J0.008 12/01/2022 18:558260DAcetonemg/Kg - dry 0.003
29.0 12/02/2022 12:17SW-DRYWT Moisture %
Page 7 of 220
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-334-0100
Report Limit
Project:TCR-003
V 94349EX-5A (6-8)
18.4 12/02/2022 12:17SW-DRYWT Moisture %
V 94350EX-Dup
J0.967 12/08/2022 18:516020BArsenicmg/Kg - dry 0.191
19.7 12/08/2022 18:516020BBariummg/Kg - dry 1.95
97.5 12/08/2022 18:516020BChromiummg/Kg - dry 0.275
8.55 12/08/2022 18:516020BLeadmg/Kg - dry 0.203
28.1 12/02/2022 12:17SW-DRYWT Moisture %
V 94351BF-SB-01 (0-2)
23.1 12/02/2022 12:17SW-DRYWT Moisture %
V 94352BF-SB-01 (4-6)
25.6 12/02/2022 12:17SW-DRYWT Moisture %
V 94353BF-SB-02 (2-4)
18.8 12/02/2022 12:17SW-DRYWT Moisture %
V 94354BF-SB-02 (4-6)
19.1 12/02/2022 12:17SW-DRYWT Moisture %
V 94355BF-SB-03 (2-4)
19.0 12/02/2022 12:17SW-DRYWT Moisture %
V 94356BF-SB-03 (4-6)
20.1 12/02/2022 12:17SW-DRYWT Moisture %
V 94357BF-SB-04 (0-2)
19.2 12/02/2022 12:17SW-DRYWT Moisture %
V 94358BF-SB-04 (6-8)
29.0 12/02/2022 12:17SW-DRYWT Moisture %
V 94359BF-SB-05 (2-4)
20.6 12/02/2022 12:17SW-DRYWT Moisture %
V 94360BF-SB-05 (4-6)
24.5 12/02/2022 12:17SW-DRYWT Moisture %
V 94361BF-SB-DUP
18.5 12/02/2022 12:17SW-DRYWT Moisture %
Page 8 of 220
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-334-0100
Report Limit
Project:TCR-003
V 94362COMP-2A
20.1 12/13/2022 21:336020BLeadmg/Kg - dry 0.0347
J0.168 12/06/2022 22:058270EBenzo(b)fluoranthene mg/Kg - dry 0.163
10.9 12/02/2022 12:17SW-DRYWT Moisture %
V 94363COMP-2B
490 12/13/2022 21:396020BLeadmg/Kg - dry 1.38
J0.359 12/06/2022 22:288270EBenzo(a)anthracene mg/Kg - dry 0.154
J0.523 12/06/2022 22:288270EBenzo(a)pyrene mg/Kg - dry 0.163
J0.685 12/06/2022 22:288270EBenzo(b)fluoranthene mg/Kg - dry 0.161
J0.356 12/06/2022 22:288270EBenzo(g,h,i)perylene mg/Kg - dry 0.150
J0.183 12/06/2022 22:288270EBenzo(k)fluoranthene mg/Kg - dry 0.152
J0.353 12/06/2022 22:288270EChrysenemg/Kg - dry 0.157
J0.469 12/06/2022 22:288270EFluoranthenemg/Kg - dry 0.136
J0.372 12/06/2022 22:288270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.198
J0.482 12/06/2022 22:288270EPyrenemg/Kg - dry 0.148
9.87 12/02/2022 12:17SW-DRYWT Moisture %
V 94364COMP-2C
125 12/13/2022 21:436020BLeadmg/Kg - dry 0.150
17.1 12/02/2022 12:17SW-DRYWT Moisture %
V 94365COMP-2D
35.1 12/08/2022 19:006020BLeadmg/Kg - dry 0.0389
20.5 12/02/2022 12:17SW-DRYWT Moisture %
V 94366COMP-2E
37.5 12/08/2022 19:076020BLeadmg/Kg - dry 0.0341
J0.301 12/06/2022 23:358270EAcenaphthylenemg/Kg - dry 0.115
1.68 12/06/2022 23:358270EAnthracenemg/Kg - dry 0.157
6.44 12/06/2022 23:358270EBenzo(a)anthracene mg/Kg - dry 0.152
6.32 12/06/2022 23:358270EBenzo(a)pyrene mg/Kg - dry 0.161
8.65 12/09/2022 01:078270EBenzo(b)fluoranthene mg/Kg - dry 0.642
3.15 12/06/2022 23:358270EBenzo(g,h,i)perylene mg/Kg - dry 0.149
3.05 12/06/2022 23:358270EBenzo(k)fluoranthene mg/Kg - dry 0.150
5.67 12/06/2022 23:358270EChrysenemg/Kg - dry 0.156
J0.361 12/06/2022 23:358270EDibenz(a,h)anthracene mg/Kg - dry 0.253
J0.178 12/06/2022 23:358270EDibenzofuranmg/Kg - dry 0.130
12.4 12/09/2022 01:078270EFluoranthenemg/Kg - dry 0.541
Page 9 of 220
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-334-0100
Report Limit
Project:TCR-003
V 94366COMP-2E
J0.258 12/06/2022 23:358270EFluorenemg/Kg - dry 0.140
3.80 12/06/2022 23:358270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.197
J0.176 12/06/2022 23:358270ENaphthalenemg/Kg - dry 0.158
4.01 12/06/2022 23:358270EPhenanthrenemg/Kg - dry 0.228
J0.559 12/06/2022 23:358270EPhenolmg/Kg - dry 0.123
11.1 12/09/2022 01:078270EPyrenemg/Kg - dry 0.589
9.15 12/02/2022 12:44SW-DRYWT Moisture %
V 95246EX-2 (0-2)
0.060 12/13/2022 14:476010DTCLP Lead mg/L 0.008
Leachate 12/12/2022 17:03SW-1311 TCLP Metals Extraction
V 95247EX-3 (3-6)
0.074 12/13/2022 14:546010DTCLP Lead mg/L 0.008
Leachate 12/12/2022 17:03SW-1311 TCLP Metals Extraction
V 95652COMP-2B
0.166 12/20/2022 18:486010DTCLP Lead mg/L 0.008
Leachate 12/20/2022 16:12SW-1311 TCLP Metals Extraction
V 95653COMP-2C
J0.020 12/20/2022 19:016010DTCLP Lead mg/L 0.008
Leachate 12/20/2022 16:12SW-1311 TCLP Metals Extraction
Page 10 of 220

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: TCR-003 Lab Report Number: 22-334-0100
Date: 12/21/2022
Report Comments Revised Report: Revision 1 TCLP lead has been added to Comp-2B and Comp-2C.
Metals Analyses Method 6020B
Sample 94366 (COMP-2E) Analyte: Arsenic
QC Batch No: L653002/L651943 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94366 (COMP-2E)
Analyte: Barium QC Batch No: L653002/L651943
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 94366 (COMP-2E)
Analyte: Chromium QC Batch No: L653002/L651943 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 94366 (COMP-2E)
Analyte: Lead QC Batch No: L653746/L651943
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94337 (EX-2 (0-2))
Analyte: Barium QC Batch No: V27539/V27451
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94337 (EX-2 (0-2)) Analyte: Cadmium
QC Batch No: V27539/V27451 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94337 (EX-2 (0-2)) Analyte: Chromium
Page 11 of 220

QC Batch No: V27539/V27451
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94337 (EX-2 (0-2))
Analyte: Lead QC Batch No: V27539/V27451
DT result used for both sample and Dilution Test.
Sample 94337 (EX-2 (0-2)) Analyte: Lead
QC Batch No: V27628/V27451 The MS/MSD recoveries are outside QC limits due to the level of analyte present in the parent sample relative to
the spike level. RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates. Hexavalent Chromium by Ion Chromatography Method SW-7199 QC Batch No: L651985
Insoluble Hexavalent Chromium spike data.
QC Batch No: L652184 Insoluble Hexavalent Chromium spike data.
Solids Total Mercury Analysis - CVAA Method 7471B Sample 94342 (EX-4 (4-6)) Analyte: Mercury
QC Batch No: V27185/V27161 ICV failed high. Sample concentration BRL. Result not affected.
Sample 94343 (EX-4 (6-8)) Analyte: Mercury QC Batch No: V27185/V27161 ICV failed high. Sample concentration BRL. Result not affected.
Sample 94347 (EX-5 (6-8)) Analyte: Mercury
QC Batch No: V27185/V27161 ICV failed high. Sample concentration BRL. Result not affected. Sample 94350 (EX-Dup) Analyte: Mercury QC Batch No: V27185/V27161
ICV failed high. Sample concentration BRL. Result not affected. Sample 94534 (11/28 - 11/30 Gypsum Composite) Analyte: Mercury QC Batch No: V27185/V27161 ICV failed high. Sample concentration BRL. Result not affected. Volatile Organic Compounds - GC/MS Method 8260D Analyte: Hexane QC Batch No: V27134/V27133 CCV result is above control limits but within method parameters. Results are reported but considered estimated.
Page 12 of 220

Analyte: Hexane
QC Batch No: V27136/V27133 CCV result is above control limits but within method parameters. Results are reported but considered estimated.
Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: Benzoic Acid QC Batch No: V27410/V27192
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Sample 94281 Analyte: Benzoic Acid
QC Batch No: V27410/V27192 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Analyte: Benzoic Acid QC Batch No: V27495/V27192
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias. This target analyte was flagged for recoveries outside QC limits in the associated LCS. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
Sample 94691
Analyte: Aniline QC Batch No: V27495/V27278 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 94691 Analyte: Bis(2-chloroethyl)ether
QC Batch No: V27495/V27278 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Sample 94691 Analyte: Bis(2-chloroethyl)ether QC Batch No: V27495/V27278 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference.
Sample 94691 Analyte: Hexachlorocyclopentadiene QC Batch No: V27495/V27278 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 13 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-1 (0-5)
94336 Matrix:
11/29/2022 15:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.46 %Moisture 1 12/01/22 18:23 SW-DRYWTAMB
<0.160 mg/Kg - dry 0.160 0.228Chromium, Hexavalent 1 12/06/22 17:28 SW-7199SAR
0.593 J mg/Kg - dry 0.151 1.10Arsenic 10 12/08/22 19:11 6020BEDV
62.5 mg/Kg - dry 1.55 11.0Barium 10 12/08/22 19:11 6020BEDV
<0.0728 mg/Kg - dry 0.0728 0.552Cadmium 10 12/08/22 19:11 6020BEDV
7.43 mg/Kg - dry 0.218 1.10
Chromium 10 12/08/22 19:11 6020BEDV
1.54 mg/Kg - dry 0.161 1.10Lead 10 12/08/22 19:11 6020BEDV
<0.0133 mg/Kg - dry 0.0133 0.0331Mercury (Total)1 12/05/22 14:48 7471BEDV
<0.818 mg/Kg - dry 0.818 2.21Selenium 10 12/08/22 19:11 6020BEDV
<0.0519 mg/Kg - dry 0.0519 0.552Silver 10 12/08/22 19:11 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 14 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-1 (0-5)
94336 Matrix:
11/29/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
0.002 J mg/Kg - dry 0.002 0.022Acetone 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 12/01/22 13:26 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 12/01/22 13:26 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 12/01/22 13:26 V27134TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 12/01/22 13:26 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 12/01/22 13:26 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 12/01/22 13:26 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 12/01/22 13:26 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 12/01/22 13:26 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 12/01/22 13:26 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 12/01/22 13:26 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 12/01/22 13:26 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 12/01/22 13:26 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 15 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-1 (0-5)
94336 Matrix:
11/29/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 12/01/22 13:26 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 12/01/22 13:26 V27134TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 12/01/22 13:26 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 12/01/22 13:26 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 12/01/22 13:26 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 12/01/22 13:26 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 12/01/22 13:26 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 12/01/22 13:26 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 12/01/22 13:26 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 12/01/22 13:26 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 12/01/22 13:26 V27134TBL
<0.015 mg/Kg - dry 0.015 0.276Ethanol 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 12/01/22 13:26 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 13:26 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 12/01/22 13:26 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 16 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-1 (0-5)
94336 Matrix:
11/29/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 12/01/22 13:26 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 12/01/22 13:26 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 12/01/22 13:26 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 12/01/22 13:26 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 12/01/22 13:26 V27134TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 12/01/22 13:26 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 12/01/22 13:26 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 12/01/22 13:26 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 12/01/22 13:26 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 12/01/22 13:26 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/01/22 13:26 V27134TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 12/01/22 13:26 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 12/01/22 13:26 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 17 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-1 (0-5)
94336 Matrix:
11/29/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 12/01/22 13:26 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 12/01/22 13:26 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 12/01/22 13:26 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 12/01/22 13:26 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 12/01/22 13:26 V27134
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/01/22 13:261 TBL V27134
Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/01/22 13:261 TBL V27134
Surrogate: Toluene-d8 95.5 Limits: 76-129%12/01/22 13:261 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.128 mg/Kg - dry 0.128 0.730Acenaphthene 1 12/04/22 15:19 V27410JMV
<0.115 mg/Kg - dry 0.115 0.730Acenaphthylene 1 12/04/22 15:19 V27410JMV
<0.167 mg/Kg - dry 0.167 0.730Aniline 1 12/04/22 15:19 V27410JMV
<0.157 mg/Kg - dry 0.157 0.730Anthracene 1 12/04/22 15:19 V27410JMV
<0.153 mg/Kg - dry 0.153 0.730
Benzo(a)anthracene 1 12/04/22 15:19 V27410JMV
<0.162 mg/Kg - dry 0.162 0.730Benzo(a)pyrene 1 12/04/22 15:19 V27410JMV
<0.161 mg/Kg - dry 0.161 0.730Benzo(b)fluoranthene 1 12/04/22 15:19 V27410JMV
<0.150 mg/Kg - dry 0.150 0.730Benzo(g,h,i)perylene 1 12/04/22 15:19 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 18 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-1 (0-5)
94336 Matrix:
11/29/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.151 mg/Kg - dry 0.151 0.730Benzo(k)fluoranthene 1 12/04/22 15:19 V27410JMV
<0.640 M
mg/Kg - dry 0.640 2.21
Benzoic Acid 1 12/04/22 15:19 V27410JMV
<0.115 mg/Kg - dry 0.115 0.730Benzyl alcohol 1 12/04/22 15:19 V27410JMV
<0.130 mg/Kg - dry 0.130 0.730Bis(2-Chloroethoxy)methane 1 12/04/22 15:19 V27410JMV
<0.118 mg/Kg - dry 0.118 0.730Bis(2-Chloroethyl)ether 1 12/04/22 15:19 V27410JMV
<0.150 mg/Kg - dry 0.150 0.365Bis(2-Chloroisopropyl)ether 1 12/04/22 15:19 V27410JMV
<0.132 mg/Kg - dry 0.132 0.730Bis(2-ethylhexyl)phthalate 1 12/04/22 15:19 V27410JMV
<0.120 mg/Kg - dry 0.120 0.7304-Bromophenyl phenyl ether 1 12/04/22 15:19 V27410JMV
<0.124 mg/Kg - dry 0.124 0.365
Butyl benzyl phthalate 1 12/04/22 15:19 V27410JMV
<0.102 mg/Kg - dry 0.102 0.7304-Chloro-3-methylphenol 1 12/04/22 15:19 V27410JMV
<0.123 mg/Kg - dry 0.123 0.3654-Chloroaniline 1 12/04/22 15:19 V27410JMV
<0.128 mg/Kg - dry 0.128 0.7302-Chloronaphthalene 1 12/04/22 15:19 V27410JMV
<0.108 mg/Kg - dry 0.108 0.7302-Chlorophenol 1 12/04/22 15:19 V27410JMV
<0.139 mg/Kg - dry 0.139 1.104-Chlorophenyl phenyl ether 1 12/04/22 15:19 V27410JMV
<0.156 mg/Kg - dry 0.156 0.730Chrysene 1 12/04/22 15:19 V27410JMV
<0.254 mg/Kg - dry 0.254 0.730Dibenz(a,h)anthracene 1 12/04/22 15:19 V27410JMV
<0.131 mg/Kg - dry 0.131 0.730Dibenzofuran 1 12/04/22 15:19 V27410JMV
<0.104 mg/Kg - dry 0.104 0.7301,2-Dichlorobenzene 1 12/04/22 15:19 V27410JMV
<0.107 mg/Kg - dry 0.107 0.7301,3-Dichlorobenzene 1 12/04/22 15:19 V27410JMV
<0.108 mg/Kg - dry 0.108 0.3651,4-Dichlorobenzene 1 12/04/22 15:19 V27410JMV
<0.162 mg/Kg - dry 0.162 0.7303,3'-Dichlorobenzidine 1 12/04/22 15:19 V27410JMV
<0.105 mg/Kg - dry 0.105 0.7302,4-Dichlorophenol 1 12/04/22 15:19 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 19 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-1 (0-5)
94336 Matrix:
11/29/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.198 mg/Kg - dry 0.198 0.730Diethyl phthalate 1 12/04/22 15:19 V27410JMV
<0.192 mg/Kg - dry 0.192 0.730
Dimethyl phthalate 1 12/04/22 15:19 V27410JMV
<0.119 mg/Kg - dry 0.119 0.3652,4-Dimethylphenol 1 12/04/22 15:19 V27410JMV
<0.118 mg/Kg - dry 0.118 0.730Di-n-butyl phthalate 1 12/04/22 15:19 V27410JMV
<0.265 mg/Kg - dry 0.265 1.664,6-Dinitro-2-methylphenol 1 12/04/22 15:19 V27410JMV
<0.574 mg/Kg - dry 0.574 1.662,4-Dinitrophenol 1 12/04/22 15:19 V27410JMV
<0.106 mg/Kg - dry 0.106 0.7302,4-Dinitrotoluene 1 12/04/22 15:19 V27410JMV
<0.119 mg/Kg - dry 0.119 0.7302,6-Dinitrotoluene 1 12/04/22 15:19 V27410JMV
<0.157 mg/Kg - dry 0.157 0.365
Di-n-Octyl Phthalate 1 12/04/22 15:19 V27410JMV
<0.135 mg/Kg - dry 0.135 0.730Fluoranthene 1 12/04/22 15:19 V27410JMV
<0.141 mg/Kg - dry 0.141 0.730Fluorene 1 12/04/22 15:19 V27410JMV
<0.117 mg/Kg - dry 0.117 0.730Hexachlorobenzene 1 12/04/22 15:19 V27410JMV
<0.107 mg/Kg - dry 0.107 0.730Hexachlorobutadiene 1 12/04/22 15:19 V27410JMV
<0.173 mg/Kg - dry 0.173 0.730Hexachlorocyclopentadiene 1 12/04/22 15:19 V27410JMV
<0.087 mg/Kg - dry 0.087 0.730Hexachloroethane 1 12/04/22 15:19 V27410JMV
<0.197 mg/Kg - dry 0.197 0.730Indeno(1,2,3-cd)pyrene 1 12/04/22 15:19 V27410JMV
<0.210 mg/Kg - dry 0.210 0.730Isophorone 1 12/04/22 15:19 V27410JMV
<0.117 mg/Kg - dry 0.117 0.7301-Methylnaphthalene 1 12/04/22 15:19 V27410JMV
<0.110 mg/Kg - dry 0.110 0.7302-Methylnaphthalene 1 12/04/22 15:19 V27410JMV
<0.107 mg/Kg - dry 0.107 0.7302-Methylphenol 1 12/04/22 15:19 V27410JMV
<0.093 mg/Kg - dry 0.093 0.7303&4 Methylphenol 1 12/04/22 15:19 V27410JMV
<0.159 mg/Kg - dry 0.159 0.730Naphthalene 1 12/04/22 15:19 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 20 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-1 (0-5)
94336 Matrix:
11/29/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.106 mg/Kg - dry 0.106 0.7302-Nitroaniline 1 12/04/22 15:19 V27410JMV
<0.132 mg/Kg - dry 0.132 0.730
3-Nitroaniline 1 12/04/22 15:19 V27410JMV
<0.103 mg/Kg - dry 0.103 0.3654-Nitroaniline 1 12/04/22 15:19 V27410JMV
<0.128 mg/Kg - dry 0.128 0.365Nitrobenzene 1 12/04/22 15:19 V27410JMV
<0.098 mg/Kg - dry 0.098 0.7302-Nitrophenol 1 12/04/22 15:19 V27410JMV
<0.129 mg/Kg - dry 0.129 0.7304-Nitrophenol 1 12/04/22 15:19 V27410JMV
<0.290 mg/Kg - dry 0.290 0.730N-Nitrosodimethylamine 1 12/04/22 15:19 V27410JMV
<0.199 mg/Kg - dry 0.199 0.730N-Nitrosodiphenylamine 1 12/04/22 15:19 V27410JMV
<0.130 mg/Kg - dry 0.130 0.730
N-Nitroso-di-n-propylamine 1 12/04/22 15:19 V27410JMV
<0.383 mg/Kg - dry 0.383 1.10Pentachlorophenol 1 12/04/22 15:19 V27410JMV
<0.229 mg/Kg - dry 0.229 0.730Phenanthrene 1 12/04/22 15:19 V27410JMV
<0.123 mg/Kg - dry 0.123 0.730Phenol 1 12/04/22 15:19 V27410JMV
<0.148 mg/Kg - dry 0.148 0.730Pyrene 1 12/04/22 15:19 V27410JMV
<0.087 mg/Kg - dry 0.087 0.365Pyridine 1 12/04/22 15:19 V27410JMV
<0.118 mg/Kg - dry 0.118 0.7301,2,4-Trichlorobenzene 1 12/04/22 15:19 V27410JMV
<0.106 mg/Kg - dry 0.106 0.7302,4,5-Trichlorophenol 1 12/04/22 15:19 V27410JMV
<0.106 mg/Kg - dry 0.106 0.7302,4,6-Trichlorophenol 1 12/04/22 15:19 V27410JMV
8270ESurrogate: Phenol-d5 70.1 Limits: 34-121%12/04/22 15:191 JMV
Surrogate: 2-Fluorobiphenyl 96.4 Limits: 44-115%12/04/22 15:191 JMV V27410
Surrogate: 2-Fluorophenol 78.4 Limits: 35-115%12/04/22 15:191 JMV V27410
Surrogate: Nitrobenzene-d5 88.0 Limits: 37-122%12/04/22 15:191 JMV V27410
Surrogate: 4-Terphenyl-d14 108 Limits: 54-127%12/04/22 15:191 JMV V27410
Surrogate: 2,4,6-Tribromophenol 90.1 Limits: 39-132%12/04/22 15:191 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 21 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-2 (0-2)
94337 Matrix:
11/29/2022 14:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
10.3 %Moisture 1 12/01/22 18:23 SW-DRYWTAMB
<0.158 mg/Kg - dry 0.158 0.225Chromium, Hexavalent 1 12/06/22 18:12 SW-7199SAR
15.4 mg/Kg - dry 0.153 1.11Arsenic 10 12/08/22 16:36 6020BEDV
178 mg/Kg - dry 1.56 11.1Barium 10 12/08/22 16:36 6020BEDV
17.9 mg/Kg - dry 0.0735 0.557Cadmium 10 12/08/22 16:36 6020BEDV
92.1 mg/Kg - dry 0.220 1.11
Chromium 10 12/08/22 16:36 6020BEDV
2640 mg/Kg - dry 0.814 5.57Lead 50 12/08/22 17:22 6020BEDV
0.194 mg/Kg - dry 0.0134 0.0334Mercury (Total)1 12/05/22 13:48 7471BEDV
1.48 J mg/Kg - dry 0.826 2.23Selenium 10 12/08/22 16:36 6020BEDV
4.62 mg/Kg - dry 0.0523 0.557Silver 10 12/08/22 16:36 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 22 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-2 (0-2)
94337 Matrix:
11/29/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
0.011 J mg/Kg - dry 0.002 0.022Acetone 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.022
Acrolein 1 12/01/22 13:54 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 12/01/22 13:54 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 12/01/22 13:54 V27134TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 12/01/22 13:54 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 12/01/22 13:54 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 12/01/22 13:54 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 12/01/22 13:54 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 12/01/22 13:54 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 12/01/22 13:54 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 12/01/22 13:54 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 12/01/22 13:54 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 12/01/22 13:54 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 23 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-2 (0-2)
94337 Matrix:
11/29/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 12/01/22 13:54 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 12/01/22 13:54 V27134TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 12/01/22 13:54 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 12/01/22 13:54 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 12/01/22 13:54 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 12/01/22 13:54 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 12/01/22 13:54 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 12/01/22 13:54 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 12/01/22 13:54 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 12/01/22 13:54 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 12/01/22 13:54 V27134TBL
<0.015 mg/Kg - dry 0.015 0.278Ethanol 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 12/01/22 13:54 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 13:54 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 12/01/22 13:54 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 24 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-2 (0-2)
94337 Matrix:
11/29/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
0.001 J mg/Kg - dry 0.0007 0.011n-Hexane 1 12/01/22 13:54 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.022
2-Hexanone 1 12/01/22 13:54 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 12/01/22 13:54 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 12/01/22 13:54 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 12/01/22 13:54 V27134TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 12/01/22 13:54 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/01/22 13:54 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 12/01/22 13:54 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 12/01/22 13:54 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/01/22 13:54 V27134TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 12/01/22 13:54 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 12/01/22 13:54 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 25 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-2 (0-2)
94337 Matrix:
11/29/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 12/01/22 13:54 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 12/01/22 13:54 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 12/01/22 13:54 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 12/01/22 13:54 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 12/01/22 13:54 V27134
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%12/01/22 13:541 TBL V27134
Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/01/22 13:541 TBL V27134
Surrogate: Toluene-d8 96.5 Limits: 76-129%12/01/22 13:541 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.129 mg/Kg - dry 0.129 0.736Acenaphthene 1 12/04/22 15:42 V27410JMV
<0.117 mg/Kg - dry 0.117 0.736Acenaphthylene 1 12/04/22 15:42 V27410JMV
<0.169 mg/Kg - dry 0.169 0.736Aniline 1 12/04/22 15:42 V27410JMV
<0.159 mg/Kg - dry 0.159 0.736Anthracene 1 12/04/22 15:42 V27410JMV
<0.154 mg/Kg - dry 0.154 0.736
Benzo(a)anthracene 1 12/04/22 15:42 V27410JMV
<0.163 mg/Kg - dry 0.163 0.736Benzo(a)pyrene 1 12/04/22 15:42 V27410JMV
<0.162 mg/Kg - dry 0.162 0.736Benzo(b)fluoranthene 1 12/04/22 15:42 V27410JMV
<0.151 mg/Kg - dry 0.151 0.736Benzo(g,h,i)perylene 1 12/04/22 15:42 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 26 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-2 (0-2)
94337 Matrix:
11/29/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.152 mg/Kg - dry 0.152 0.736Benzo(k)fluoranthene 1 12/04/22 15:42 V27410JMV
<0.646 M
mg/Kg - dry 0.646 2.23
Benzoic Acid 1 12/04/22 15:42 V27410JMV
<0.117 mg/Kg - dry 0.117 0.736Benzyl alcohol 1 12/04/22 15:42 V27410JMV
<0.131 mg/Kg - dry 0.131 0.736Bis(2-Chloroethoxy)methane 1 12/04/22 15:42 V27410JMV
<0.119 mg/Kg - dry 0.119 0.736Bis(2-Chloroethyl)ether 1 12/04/22 15:42 V27410JMV
<0.151 mg/Kg - dry 0.151 0.369Bis(2-Chloroisopropyl)ether 1 12/04/22 15:42 V27410JMV
<0.133 mg/Kg - dry 0.133 0.736Bis(2-ethylhexyl)phthalate 1 12/04/22 15:42 V27410JMV
<0.121 mg/Kg - dry 0.121 0.7364-Bromophenyl phenyl ether 1 12/04/22 15:42 V27410JMV
<0.125 mg/Kg - dry 0.125 0.369
Butyl benzyl phthalate 1 12/04/22 15:42 V27410JMV
<0.103 mg/Kg - dry 0.103 0.7364-Chloro-3-methylphenol 1 12/04/22 15:42 V27410JMV
<0.124 mg/Kg - dry 0.124 0.3694-Chloroaniline 1 12/04/22 15:42 V27410JMV
<0.129 mg/Kg - dry 0.129 0.7362-Chloronaphthalene 1 12/04/22 15:42 V27410JMV
<0.109 mg/Kg - dry 0.109 0.7362-Chlorophenol 1 12/04/22 15:42 V27410JMV
<0.140 mg/Kg - dry 0.140 1.114-Chlorophenyl phenyl ether 1 12/04/22 15:42 V27410JMV
<0.158 mg/Kg - dry 0.158 0.736Chrysene 1 12/04/22 15:42 V27410JMV
<0.256 mg/Kg - dry 0.256 0.736Dibenz(a,h)anthracene 1 12/04/22 15:42 V27410JMV
<0.132 mg/Kg - dry 0.132 0.736Dibenzofuran 1 12/04/22 15:42 V27410JMV
<0.105 mg/Kg - dry 0.105 0.7361,2-Dichlorobenzene 1 12/04/22 15:42 V27410JMV
<0.108 mg/Kg - dry 0.108 0.7361,3-Dichlorobenzene 1 12/04/22 15:42 V27410JMV
<0.109 mg/Kg - dry 0.109 0.3691,4-Dichlorobenzene 1 12/04/22 15:42 V27410JMV
<0.163 mg/Kg - dry 0.163 0.7363,3'-Dichlorobenzidine 1 12/04/22 15:42 V27410JMV
<0.106 mg/Kg - dry 0.106 0.7362,4-Dichlorophenol 1 12/04/22 15:42 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 27 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-2 (0-2)
94337 Matrix:
11/29/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.200 mg/Kg - dry 0.200 0.736Diethyl phthalate 1 12/04/22 15:42 V27410JMV
<0.193 mg/Kg - dry 0.193 0.736
Dimethyl phthalate 1 12/04/22 15:42 V27410JMV
<0.120 mg/Kg - dry 0.120 0.3692,4-Dimethylphenol 1 12/04/22 15:42 V27410JMV
<0.119 mg/Kg - dry 0.119 0.736Di-n-butyl phthalate 1 12/04/22 15:42 V27410JMV
<0.267 mg/Kg - dry 0.267 1.674,6-Dinitro-2-methylphenol 1 12/04/22 15:42 V27410JMV
<0.579 mg/Kg - dry 0.579 1.672,4-Dinitrophenol 1 12/04/22 15:42 V27410JMV
<0.107 mg/Kg - dry 0.107 0.7362,4-Dinitrotoluene 1 12/04/22 15:42 V27410JMV
<0.120 mg/Kg - dry 0.120 0.7362,6-Dinitrotoluene 1 12/04/22 15:42 V27410JMV
<0.159 mg/Kg - dry 0.159 0.369
Di-n-Octyl Phthalate 1 12/04/22 15:42 V27410JMV
<0.137 mg/Kg - dry 0.137 0.736Fluoranthene 1 12/04/22 15:42 V27410JMV
<0.142 mg/Kg - dry 0.142 0.736Fluorene 1 12/04/22 15:42 V27410JMV
<0.118 mg/Kg - dry 0.118 0.736Hexachlorobenzene 1 12/04/22 15:42 V27410JMV
<0.108 mg/Kg - dry 0.108 0.736Hexachlorobutadiene 1 12/04/22 15:42 V27410JMV
<0.175 mg/Kg - dry 0.175 0.736Hexachlorocyclopentadiene 1 12/04/22 15:42 V27410JMV
<0.088 mg/Kg - dry 0.088 0.736Hexachloroethane 1 12/04/22 15:42 V27410JMV
<0.199 mg/Kg - dry 0.199 0.736Indeno(1,2,3-cd)pyrene 1 12/04/22 15:42 V27410JMV
<0.212 mg/Kg - dry 0.212 0.736Isophorone 1 12/04/22 15:42 V27410JMV
<0.118 mg/Kg - dry 0.118 0.7361-Methylnaphthalene 1 12/04/22 15:42 V27410JMV
<0.111 mg/Kg - dry 0.111 0.7362-Methylnaphthalene 1 12/04/22 15:42 V27410JMV
<0.108 mg/Kg - dry 0.108 0.7362-Methylphenol 1 12/04/22 15:42 V27410JMV
<0.094 mg/Kg - dry 0.094 0.7363&4 Methylphenol 1 12/04/22 15:42 V27410JMV
<0.160 mg/Kg - dry 0.160 0.736Naphthalene 1 12/04/22 15:42 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 28 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-2 (0-2)
94337 Matrix:
11/29/2022 14:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.107 mg/Kg - dry 0.107 0.7362-Nitroaniline 1 12/04/22 15:42 V27410JMV
<0.133 mg/Kg - dry 0.133 0.736
3-Nitroaniline 1 12/04/22 15:42 V27410JMV
<0.104 mg/Kg - dry 0.104 0.3694-Nitroaniline 1 12/04/22 15:42 V27410JMV
<0.129 mg/Kg - dry 0.129 0.369Nitrobenzene 1 12/04/22 15:42 V27410JMV
<0.099 mg/Kg - dry 0.099 0.7362-Nitrophenol 1 12/04/22 15:42 V27410JMV
<0.130 mg/Kg - dry 0.130 0.7364-Nitrophenol 1 12/04/22 15:42 V27410JMV
<0.293 mg/Kg - dry 0.293 0.736N-Nitrosodimethylamine 1 12/04/22 15:42 V27410JMV
<0.201 mg/Kg - dry 0.201 0.736N-Nitrosodiphenylamine 1 12/04/22 15:42 V27410JMV
<0.131 mg/Kg - dry 0.131 0.736
N-Nitroso-di-n-propylamine 1 12/04/22 15:42 V27410JMV
<0.386 mg/Kg - dry 0.386 1.11Pentachlorophenol 1 12/04/22 15:42 V27410JMV
<0.231 mg/Kg - dry 0.231 0.736Phenanthrene 1 12/04/22 15:42 V27410JMV
<0.124 mg/Kg - dry 0.124 0.736Phenol 1 12/04/22 15:42 V27410JMV
<0.149 mg/Kg - dry 0.149 0.736Pyrene 1 12/04/22 15:42 V27410JMV
<0.088 mg/Kg - dry 0.088 0.369Pyridine 1 12/04/22 15:42 V27410JMV
<0.119 mg/Kg - dry 0.119 0.7361,2,4-Trichlorobenzene 1 12/04/22 15:42 V27410JMV
<0.107 mg/Kg - dry 0.107 0.7362,4,5-Trichlorophenol 1 12/04/22 15:42 V27410JMV
<0.107 mg/Kg - dry 0.107 0.7362,4,6-Trichlorophenol 1 12/04/22 15:42 V27410JMV
8270ESurrogate: Phenol-d5 73.7 Limits: 34-121%12/04/22 15:421 JMV
Surrogate: 2-Fluorobiphenyl 98.8 Limits: 44-115%12/04/22 15:421 JMV V27410
Surrogate: 2-Fluorophenol 77.2 Limits: 35-115%12/04/22 15:421 JMV V27410
Surrogate: Nitrobenzene-d5 83.8 Limits: 37-122%12/04/22 15:421 JMV V27410
Surrogate: 4-Terphenyl-d14 110 Limits: 54-127%12/04/22 15:421 JMV V27410
Surrogate: 2,4,6-Tribromophenol 90.1 Limits: 39-132%12/04/22 15:421 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 29 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (0-3)
94338 Matrix:
11/29/2022 13:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.2 %Moisture 1 12/01/22 18:23 SW-DRYWTAMB
<0.168 mg/Kg - dry 0.168 0.239Chromium, Hexavalent 1 12/06/22 18:23 SW-7199SAR
1.67 mg/Kg - dry 0.163 1.19Arsenic 10 12/08/22 17:29 6020BEDV
51.9 mg/Kg - dry 1.67 11.9Barium 10 12/08/22 17:29 6020BEDV
0.183 J mg/Kg - dry 0.0787 0.597Cadmium 10 12/08/22 17:29 6020BEDV
53.7 mg/Kg - dry 0.236 1.19
Chromium 10 12/08/22 17:29 6020BEDV
49.3 mg/Kg - dry 0.174 1.19Lead 10 12/08/22 17:29 6020BEDV
0.0481 mg/Kg - dry 0.0143 0.0358Mercury (Total)1 12/05/22 13:57 7471BEDV
<0.884 mg/Kg - dry 0.884 2.39Selenium 10 12/08/22 17:29 6020BEDV
0.0638 J mg/Kg - dry 0.0560 0.597Silver 10 12/08/22 17:29 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 30 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (0-3)
94338 Matrix:
11/29/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
0.018 J mg/Kg - dry 0.002 0.023Acetone 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.023
Acrolein 1 12/01/22 14:21 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 12/01/22 14:21 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 12/01/22 14:21 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.005Bromochloromethane 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 12/01/22 14:21 V27134TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 12/01/22 14:21 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 12/01/22 14:21 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 12/01/22 14:21 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 12/01/22 14:21 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.011Chloromethane 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 12/01/22 14:21 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 12/01/22 14:21 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 12/01/22 14:21 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 31 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (0-3)
94338 Matrix:
11/29/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 12/01/22 14:21 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 12/01/22 14:21 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 12/01/22 14:21 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 12/01/22 14:21 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 12/01/22 14:21 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 12/01/22 14:21 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 12/01/22 14:21 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 12/01/22 14:21 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 12/01/22 14:21 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 12/01/22 14:21 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 12/01/22 14:21 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 12/01/22 14:21 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.005trans-1,3-Dichloropropene 1 12/01/22 14:21 V27134TBL
<0.016 mg/Kg - dry 0.016 0.298Ethanol 1 12/01/22 14:21 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 12/01/22 14:21 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 14:21 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 12/01/22 14:21 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 32 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (0-3)
94338 Matrix:
11/29/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 12/01/22 14:21 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.023
2-Hexanone 1 12/01/22 14:21 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 12/01/22 14:21 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 12/01/22 14:21 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 12/01/22 14:21 V27134TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 12/01/22 14:21 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/01/22 14:21 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 12/01/22 14:21 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/01/22 14:21 V27134TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 12/01/22 14:21 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 12/01/22 14:21 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 33 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (0-3)
94338 Matrix:
11/29/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 12/01/22 14:21 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 12/01/22 14:21 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 12/01/22 14:21 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 12/01/22 14:21 V27134
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/01/22 14:211 TBL V27134
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/01/22 14:211 TBL V27134
Surrogate: Toluene-d8 92.5 Limits: 76-129%12/01/22 14:211 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.138 mg/Kg - dry 0.138 0.788Acenaphthene 1 12/04/22 16:04 V27410JMV
<0.125 mg/Kg - dry 0.125 0.788Acenaphthylene 1 12/04/22 16:04 V27410JMV
<0.181 mg/Kg - dry 0.181 0.788Aniline 1 12/04/22 16:04 V27410JMV
<0.170 mg/Kg - dry 0.170 0.788Anthracene 1 12/04/22 16:04 V27410JMV
<0.165 mg/Kg - dry 0.165 0.788
Benzo(a)anthracene 1 12/04/22 16:04 V27410JMV
<0.175 mg/Kg - dry 0.175 0.788Benzo(a)pyrene 1 12/04/22 16:04 V27410JMV
<0.174 mg/Kg - dry 0.174 0.788Benzo(b)fluoranthene 1 12/04/22 16:04 V27410JMV
<0.162 mg/Kg - dry 0.162 0.788Benzo(g,h,i)perylene 1 12/04/22 16:04 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 34 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (0-3)
94338 Matrix:
11/29/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.163 mg/Kg - dry 0.163 0.788Benzo(k)fluoranthene 1 12/04/22 16:04 V27410JMV
<0.692 M
mg/Kg - dry 0.692 2.39
Benzoic Acid 1 12/04/22 16:04 V27410JMV
<0.125 mg/Kg - dry 0.125 0.788Benzyl alcohol 1 12/04/22 16:04 V27410JMV
<0.140 mg/Kg - dry 0.140 0.788Bis(2-Chloroethoxy)methane 1 12/04/22 16:04 V27410JMV
<0.127 mg/Kg - dry 0.127 0.788Bis(2-Chloroethyl)ether 1 12/04/22 16:04 V27410JMV
<0.162 mg/Kg - dry 0.162 0.393Bis(2-Chloroisopropyl)ether 1 12/04/22 16:04 V27410JMV
<0.143 mg/Kg - dry 0.143 0.788Bis(2-ethylhexyl)phthalate 1 12/04/22 16:04 V27410JMV
<0.130 mg/Kg - dry 0.130 0.7884-Bromophenyl phenyl ether 1 12/04/22 16:04 V27410JMV
<0.134 mg/Kg - dry 0.134 0.393
Butyl benzyl phthalate 1 12/04/22 16:04 V27410JMV
<0.110 mg/Kg - dry 0.110 0.7884-Chloro-3-methylphenol 1 12/04/22 16:04 V27410JMV
<0.133 mg/Kg - dry 0.133 0.3934-Chloroaniline 1 12/04/22 16:04 V27410JMV
<0.138 mg/Kg - dry 0.138 0.7882-Chloronaphthalene 1 12/04/22 16:04 V27410JMV
<0.117 mg/Kg - dry 0.117 0.7882-Chlorophenol 1 12/04/22 16:04 V27410JMV
<0.150 mg/Kg - dry 0.150 1.194-Chlorophenyl phenyl ether 1 12/04/22 16:04 V27410JMV
<0.169 mg/Kg - dry 0.169 0.788Chrysene 1 12/04/22 16:04 V27410JMV
<0.274 mg/Kg - dry 0.274 0.788Dibenz(a,h)anthracene 1 12/04/22 16:04 V27410JMV
<0.142 mg/Kg - dry 0.142 0.788Dibenzofuran 1 12/04/22 16:04 V27410JMV
<0.112 mg/Kg - dry 0.112 0.7881,2-Dichlorobenzene 1 12/04/22 16:04 V27410JMV
<0.116 mg/Kg - dry 0.116 0.7881,3-Dichlorobenzene 1 12/04/22 16:04 V27410JMV
<0.116 mg/Kg - dry 0.116 0.3931,4-Dichlorobenzene 1 12/04/22 16:04 V27410JMV
<0.175 mg/Kg - dry 0.175 0.7883,3'-Dichlorobenzidine 1 12/04/22 16:04 V27410JMV
<0.114 mg/Kg - dry 0.114 0.7882,4-Dichlorophenol 1 12/04/22 16:04 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 35 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (0-3)
94338 Matrix:
11/29/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.214 mg/Kg - dry 0.214 0.788Diethyl phthalate 1 12/04/22 16:04 V27410JMV
<0.207 mg/Kg - dry 0.207 0.788
Dimethyl phthalate 1 12/04/22 16:04 V27410JMV
<0.128 mg/Kg - dry 0.128 0.3932,4-Dimethylphenol 1 12/04/22 16:04 V27410JMV
<0.127 mg/Kg - dry 0.127 0.788Di-n-butyl phthalate 1 12/04/22 16:04 V27410JMV
<0.286 mg/Kg - dry 0.286 1.794,6-Dinitro-2-methylphenol 1 12/04/22 16:04 V27410JMV
<0.620 mg/Kg - dry 0.620 1.792,4-Dinitrophenol 1 12/04/22 16:04 V27410JMV
<0.115 mg/Kg - dry 0.115 0.7882,4-Dinitrotoluene 1 12/04/22 16:04 V27410JMV
<0.128 mg/Kg - dry 0.128 0.7882,6-Dinitrotoluene 1 12/04/22 16:04 V27410JMV
<0.170 mg/Kg - dry 0.170 0.393
Di-n-Octyl Phthalate 1 12/04/22 16:04 V27410JMV
<0.146 mg/Kg - dry 0.146 0.788Fluoranthene 1 12/04/22 16:04 V27410JMV
<0.152 mg/Kg - dry 0.152 0.788Fluorene 1 12/04/22 16:04 V27410JMV
<0.126 mg/Kg - dry 0.126 0.788Hexachlorobenzene 1 12/04/22 16:04 V27410JMV
<0.116 mg/Kg - dry 0.116 0.788Hexachlorobutadiene 1 12/04/22 16:04 V27410JMV
<0.187 mg/Kg - dry 0.187 0.788Hexachlorocyclopentadiene 1 12/04/22 16:04 V27410JMV
<0.094 mg/Kg - dry 0.094 0.788Hexachloroethane 1 12/04/22 16:04 V27410JMV
<0.213 mg/Kg - dry 0.213 0.788Indeno(1,2,3-cd)pyrene 1 12/04/22 16:04 V27410JMV
<0.227 mg/Kg - dry 0.227 0.788Isophorone 1 12/04/22 16:04 V27410JMV
<0.126 mg/Kg - dry 0.126 0.7881-Methylnaphthalene 1 12/04/22 16:04 V27410JMV
<0.119 mg/Kg - dry 0.119 0.7882-Methylnaphthalene 1 12/04/22 16:04 V27410JMV
<0.115 mg/Kg - dry 0.115 0.7882-Methylphenol 1 12/04/22 16:04 V27410JMV
<0.101 mg/Kg - dry 0.101 0.7883&4 Methylphenol 1 12/04/22 16:04 V27410JMV
<0.171 mg/Kg - dry 0.171 0.788Naphthalene 1 12/04/22 16:04 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 36 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (0-3)
94338 Matrix:
11/29/2022 13:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.115 mg/Kg - dry 0.115 0.7882-Nitroaniline 1 12/04/22 16:04 V27410JMV
<0.143 mg/Kg - dry 0.143 0.788
3-Nitroaniline 1 12/04/22 16:04 V27410JMV
<0.111 mg/Kg - dry 0.111 0.3934-Nitroaniline 1 12/04/22 16:04 V27410JMV
<0.138 mg/Kg - dry 0.138 0.393Nitrobenzene 1 12/04/22 16:04 V27410JMV
<0.106 mg/Kg - dry 0.106 0.7882-Nitrophenol 1 12/04/22 16:04 V27410JMV
<0.139 mg/Kg - dry 0.139 0.7884-Nitrophenol 1 12/04/22 16:04 V27410JMV
<0.313 mg/Kg - dry 0.313 0.788N-Nitrosodimethylamine 1 12/04/22 16:04 V27410JMV
<0.215 mg/Kg - dry 0.215 0.788N-Nitrosodiphenylamine 1 12/04/22 16:04 V27410JMV
<0.140 mg/Kg - dry 0.140 0.788
N-Nitroso-di-n-propylamine 1 12/04/22 16:04 V27410JMV
<0.414 mg/Kg - dry 0.414 1.19Pentachlorophenol 1 12/04/22 16:04 V27410JMV
<0.248 mg/Kg - dry 0.248 0.788Phenanthrene 1 12/04/22 16:04 V27410JMV
<0.133 mg/Kg - dry 0.133 0.788Phenol 1 12/04/22 16:04 V27410JMV
<0.159 mg/Kg - dry 0.159 0.788Pyrene 1 12/04/22 16:04 V27410JMV
<0.094 mg/Kg - dry 0.094 0.393Pyridine 1 12/04/22 16:04 V27410JMV
<0.127 mg/Kg - dry 0.127 0.7881,2,4-Trichlorobenzene 1 12/04/22 16:04 V27410JMV
<0.114 mg/Kg - dry 0.114 0.7882,4,5-Trichlorophenol 1 12/04/22 16:04 V27410JMV
<0.115 mg/Kg - dry 0.115 0.7882,4,6-Trichlorophenol 1 12/04/22 16:04 V27410JMV
8270ESurrogate: Phenol-d5 73.7 Limits: 34-121%12/04/22 16:041 JMV
Surrogate: 2-Fluorobiphenyl 95.8 Limits: 44-115%12/04/22 16:041 JMV V27410
Surrogate: 2-Fluorophenol 79.0 Limits: 35-115%12/04/22 16:041 JMV V27410
Surrogate: Nitrobenzene-d5 83.2 Limits: 37-122%12/04/22 16:041 JMV V27410
Surrogate: 4-Terphenyl-d14 110 Limits: 54-127%12/04/22 16:041 JMV V27410
Surrogate: 2,4,6-Tribromophenol 87.7 Limits: 39-132%12/04/22 16:041 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 37 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (3-6)
94339 Matrix:
11/29/2022 13:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.5 %Moisture 1 12/01/22 18:23 SW-DRYWTAMB
<0.171 mg/Kg - dry 0.171 0.243Chromium, Hexavalent 1 12/06/22 18:34 SW-7199SAR
2.96 mg/Kg - dry 0.162 1.18Arsenic 10 12/08/22 17:35 6020BEDV
79.8 mg/Kg - dry 1.66 11.8Barium 10 12/08/22 17:35 6020BEDV
0.450 J mg/Kg - dry 0.0781 0.592Cadmium 10 12/08/22 17:35 6020BEDV
49.2 mg/Kg - dry 0.234 1.18
Chromium 10 12/08/22 17:35 6020BEDV
142 mg/Kg - dry 0.173 1.18Lead 10 12/08/22 17:35 6020BEDV
0.0636 mg/Kg - dry 0.0142 0.0355Mercury (Total)1 12/05/22 14:00 7471BEDV
<0.876 mg/Kg - dry 0.876 2.37Selenium 10 12/08/22 17:35 6020BEDV
0.205 J mg/Kg - dry 0.0556 0.592Silver 10 12/08/22 17:35 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 38 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (3-6)
94339 Matrix:
11/29/2022 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
0.021 J mg/Kg - dry 0.002 0.023Acetone 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.023
Acrolein 1 12/01/22 14:49 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 12/01/22 14:49 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 12/01/22 14:49 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 12/01/22 14:49 V27134TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 12/01/22 14:49 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 12/01/22 14:49 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 12/01/22 14:49 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 12/01/22 14:49 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 12/01/22 14:49 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 12/01/22 14:49 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 12/01/22 14:49 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 39 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (3-6)
94339 Matrix:
11/29/2022 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 12/01/22 14:49 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005
1,2-Dibromoethane 1 12/01/22 14:49 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 12/01/22 14:49 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 12/01/22 14:49 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 12/01/22 14:49 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 12/01/22 14:49 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 12/01/22 14:49 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 12/01/22 14:49 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 12/01/22 14:49 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 12/01/22 14:49 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 12/01/22 14:49 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 12/01/22 14:49 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 12/01/22 14:49 V27134TBL
<0.016 mg/Kg - dry 0.016 0.295Ethanol 1 12/01/22 14:49 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 12/01/22 14:49 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 14:49 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 12/01/22 14:49 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 40 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (3-6)
94339 Matrix:
11/29/2022 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 12/01/22 14:49 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.023
2-Hexanone 1 12/01/22 14:49 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 12/01/22 14:49 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 12/01/22 14:49 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 12/01/22 14:49 V27134TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 12/01/22 14:49 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 12/01/22 14:49 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 12/01/22 14:49 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 12/01/22 14:49 V27134TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 12/01/22 14:49 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 12/01/22 14:49 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 41 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (3-6)
94339 Matrix:
11/29/2022 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005
1,3,5-Trimethylbenzene 1 12/01/22 14:49 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 12/01/22 14:49 V27134TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 12/01/22 14:49 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 12/01/22 14:49 V27134
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/01/22 14:491 TBL V27134
Surrogate: Dibromofluoromethane 98.5 Limits: 84-123%12/01/22 14:491 TBL V27134
Surrogate: Toluene-d8 93.3 Limits: 76-129%12/01/22 14:491 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.137 mg/Kg - dry 0.137 0.781Acenaphthene 1 12/04/22 16:49 V27410JMV
<0.124 mg/Kg - dry 0.124 0.781Acenaphthylene 1 12/04/22 16:49 V27410JMV
<0.179 mg/Kg - dry 0.179 0.781Aniline 1 12/04/22 16:49 V27410JMV
<0.169 mg/Kg - dry 0.169 0.781Anthracene 1 12/04/22 16:49 V27410JMV
<0.164 mg/Kg - dry 0.164 0.781
Benzo(a)anthracene 1 12/04/22 16:49 V27410JMV
<0.173 mg/Kg - dry 0.173 0.781Benzo(a)pyrene 1 12/04/22 16:49 V27410JMV
<0.172 mg/Kg - dry 0.172 0.781Benzo(b)fluoranthene 1 12/04/22 16:49 V27410JMV
<0.160 mg/Kg - dry 0.160 0.781Benzo(g,h,i)perylene 1 12/04/22 16:49 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 42 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (3-6)
94339 Matrix:
11/29/2022 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.162 mg/Kg - dry 0.162 0.781Benzo(k)fluoranthene 1 12/04/22 16:49 V27410JMV
<0.686 M
mg/Kg - dry 0.686 2.37
Benzoic Acid 1 12/04/22 16:49 V27410JMV
<0.124 mg/Kg - dry 0.124 0.781Benzyl alcohol 1 12/04/22 16:49 V27410JMV
<0.139 mg/Kg - dry 0.139 0.781Bis(2-Chloroethoxy)methane 1 12/04/22 16:49 V27410JMV
<0.126 mg/Kg - dry 0.126 0.781Bis(2-Chloroethyl)ether 1 12/04/22 16:49 V27410JMV
<0.160 mg/Kg - dry 0.160 0.390Bis(2-Chloroisopropyl)ether 1 12/04/22 16:49 V27410JMV
<0.142 mg/Kg - dry 0.142 0.781Bis(2-ethylhexyl)phthalate 1 12/04/22 16:49 V27410JMV
<0.128 mg/Kg - dry 0.128 0.7814-Bromophenyl phenyl ether 1 12/04/22 16:49 V27410JMV
<0.133 mg/Kg - dry 0.133 0.390
Butyl benzyl phthalate 1 12/04/22 16:49 V27410JMV
<0.109 mg/Kg - dry 0.109 0.7814-Chloro-3-methylphenol 1 12/04/22 16:49 V27410JMV
<0.132 mg/Kg - dry 0.132 0.3904-Chloroaniline 1 12/04/22 16:49 V27410JMV
<0.137 mg/Kg - dry 0.137 0.7812-Chloronaphthalene 1 12/04/22 16:49 V27410JMV
<0.116 mg/Kg - dry 0.116 0.7812-Chlorophenol 1 12/04/22 16:49 V27410JMV
<0.149 mg/Kg - dry 0.149 1.184-Chlorophenyl phenyl ether 1 12/04/22 16:49 V27410JMV
<0.168 mg/Kg - dry 0.168 0.781Chrysene 1 12/04/22 16:49 V27410JMV
<0.272 mg/Kg - dry 0.272 0.781Dibenz(a,h)anthracene 1 12/04/22 16:49 V27410JMV
<0.140 mg/Kg - dry 0.140 0.781Dibenzofuran 1 12/04/22 16:49 V27410JMV
<0.111 mg/Kg - dry 0.111 0.7811,2-Dichlorobenzene 1 12/04/22 16:49 V27410JMV
<0.115 mg/Kg - dry 0.115 0.7811,3-Dichlorobenzene 1 12/04/22 16:49 V27410JMV
<0.115 mg/Kg - dry 0.115 0.3901,4-Dichlorobenzene 1 12/04/22 16:49 V27410JMV
<0.173 mg/Kg - dry 0.173 0.7813,3'-Dichlorobenzidine 1 12/04/22 16:49 V27410JMV
<0.113 mg/Kg - dry 0.113 0.7812,4-Dichlorophenol 1 12/04/22 16:49 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 43 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (3-6)
94339 Matrix:
11/29/2022 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.213 mg/Kg - dry 0.213 0.781Diethyl phthalate 1 12/04/22 16:49 V27410JMV
<0.205 mg/Kg - dry 0.205 0.781
Dimethyl phthalate 1 12/04/22 16:49 V27410JMV
<0.127 mg/Kg - dry 0.127 0.3902,4-Dimethylphenol 1 12/04/22 16:49 V27410JMV
<0.126 mg/Kg - dry 0.126 0.781Di-n-butyl phthalate 1 12/04/22 16:49 V27410JMV
<0.284 mg/Kg - dry 0.284 1.784,6-Dinitro-2-methylphenol 1 12/04/22 16:49 V27410JMV
<0.615 mg/Kg - dry 0.615 1.782,4-Dinitrophenol 1 12/04/22 16:49 V27410JMV
<0.114 mg/Kg - dry 0.114 0.7812,4-Dinitrotoluene 1 12/04/22 16:49 V27410JMV
<0.127 mg/Kg - dry 0.127 0.7812,6-Dinitrotoluene 1 12/04/22 16:49 V27410JMV
<0.169 mg/Kg - dry 0.169 0.390
Di-n-Octyl Phthalate 1 12/04/22 16:49 V27410JMV
<0.145 mg/Kg - dry 0.145 0.781Fluoranthene 1 12/04/22 16:49 V27410JMV
<0.151 mg/Kg - dry 0.151 0.781Fluorene 1 12/04/22 16:49 V27410JMV
<0.125 mg/Kg - dry 0.125 0.781Hexachlorobenzene 1 12/04/22 16:49 V27410JMV
<0.115 mg/Kg - dry 0.115 0.781Hexachlorobutadiene 1 12/04/22 16:49 V27410JMV
<0.185 mg/Kg - dry 0.185 0.781Hexachlorocyclopentadiene 1 12/04/22 16:49 V27410JMV
<0.093 mg/Kg - dry 0.093 0.781Hexachloroethane 1 12/04/22 16:49 V27410JMV
<0.211 mg/Kg - dry 0.211 0.781Indeno(1,2,3-cd)pyrene 1 12/04/22 16:49 V27410JMV
<0.226 mg/Kg - dry 0.226 0.781Isophorone 1 12/04/22 16:49 V27410JMV
<0.125 mg/Kg - dry 0.125 0.7811-Methylnaphthalene 1 12/04/22 16:49 V27410JMV
<0.118 mg/Kg - dry 0.118 0.7812-Methylnaphthalene 1 12/04/22 16:49 V27410JMV
<0.114 mg/Kg - dry 0.114 0.7812-Methylphenol 1 12/04/22 16:49 V27410JMV
<0.100 mg/Kg - dry 0.100 0.7813&4 Methylphenol 1 12/04/22 16:49 V27410JMV
<0.170 mg/Kg - dry 0.170 0.781Naphthalene 1 12/04/22 16:49 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 44 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (3-6)
94339 Matrix:
11/29/2022 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.114 mg/Kg - dry 0.114 0.7812-Nitroaniline 1 12/04/22 16:49 V27410JMV
<0.142 mg/Kg - dry 0.142 0.781
3-Nitroaniline 1 12/04/22 16:49 V27410JMV
<0.110 mg/Kg - dry 0.110 0.3904-Nitroaniline 1 12/04/22 16:49 V27410JMV
<0.137 mg/Kg - dry 0.137 0.390Nitrobenzene 1 12/04/22 16:49 V27410JMV
<0.105 mg/Kg - dry 0.105 0.7812-Nitrophenol 1 12/04/22 16:49 V27410JMV
<0.138 mg/Kg - dry 0.138 0.7814-Nitrophenol 1 12/04/22 16:49 V27410JMV
<0.311 mg/Kg - dry 0.311 0.781N-Nitrosodimethylamine 1 12/04/22 16:49 V27410JMV
<0.214 mg/Kg - dry 0.214 0.781N-Nitrosodiphenylamine 1 12/04/22 16:49 V27410JMV
<0.139 mg/Kg - dry 0.139 0.781
N-Nitroso-di-n-propylamine 1 12/04/22 16:49 V27410JMV
<0.410 mg/Kg - dry 0.410 1.18Pentachlorophenol 1 12/04/22 16:49 V27410JMV
<0.246 mg/Kg - dry 0.246 0.781Phenanthrene 1 12/04/22 16:49 V27410JMV
<0.132 mg/Kg - dry 0.132 0.781Phenol 1 12/04/22 16:49 V27410JMV
<0.158 mg/Kg - dry 0.158 0.781Pyrene 1 12/04/22 16:49 V27410JMV
<0.093 mg/Kg - dry 0.093 0.390Pyridine 1 12/04/22 16:49 V27410JMV
<0.126 mg/Kg - dry 0.126 0.7811,2,4-Trichlorobenzene 1 12/04/22 16:49 V27410JMV
<0.113 mg/Kg - dry 0.113 0.7812,4,5-Trichlorophenol 1 12/04/22 16:49 V27410JMV
<0.114 mg/Kg - dry 0.114 0.7812,4,6-Trichlorophenol 1 12/04/22 16:49 V27410JMV
8270ESurrogate: Phenol-d5 70.3 Limits: 34-121%12/04/22 16:491 JMV
Surrogate: 2-Fluorobiphenyl 91.0 Limits: 44-115%12/04/22 16:491 JMV V27410
Surrogate: 2-Fluorophenol 74.2 Limits: 35-115%12/04/22 16:491 JMV V27410
Surrogate: Nitrobenzene-d5 80.8 Limits: 37-122%12/04/22 16:491 JMV V27410
Surrogate: 4-Terphenyl-d14 98.8 Limits: 54-127%12/04/22 16:491 JMV V27410
Surrogate: 2,4,6-Tribromophenol 79.3 Limits: 39-132%12/04/22 16:491 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 45 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (0-2)
94340 Matrix:
11/28/2022 13:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.8 %Moisture 1 12/01/22 18:23 SW-DRYWTAMB
<0.187 mg/Kg - dry 0.187 0.266Chromium, Hexavalent 1 12/06/22 18:45 SW-7199SAR
3.43 mg/Kg - dry 0.177 1.30Arsenic 10 12/08/22 18:00 6020BEDV
31.2 mg/Kg - dry 1.81 13.0Barium 10 12/08/22 18:00 6020BEDV
<0.0854 mg/Kg - dry 0.0854 0.648Cadmium 10 12/08/22 18:00 6020BEDV
42.6 mg/Kg - dry 0.256 1.30
Chromium 10 12/08/22 18:00 6020BEDV
9.24 mg/Kg - dry 0.189 1.30Lead 10 12/08/22 18:00 6020BEDV
0.140 mg/Kg - dry 0.0155 0.0389Mercury (Total)1 12/07/22 10:35 7471BEDV
<0.959 mg/Kg - dry 0.959 2.59Selenium 10 12/08/22 18:00 6020BEDV
<0.0608 mg/Kg - dry 0.0608 0.648Silver 10 12/08/22 18:00 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 46 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (0-2)
94340 Matrix:
11/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
0.006 J mg/Kg - dry 0.003 0.025Acetone 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.025
Acrolein 1 12/01/22 15:16 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 12/01/22 15:16 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/01/22 15:16 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/01/22 15:16 V27134TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/01/22 15:16 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/01/22 15:16 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/01/22 15:16 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/01/22 15:16 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/01/22 15:16 V27134TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/01/22 15:16 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/01/22 15:16 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/01/22 15:16 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/01/22 15:16 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/01/22 15:16 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/01/22 15:16 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 47 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (0-2)
94340 Matrix:
11/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 12/01/22 15:16 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 12/01/22 15:16 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/01/22 15:16 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/01/22 15:16 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/01/22 15:16 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/01/22 15:16 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/01/22 15:16 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/01/22 15:16 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/01/22 15:16 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 12/01/22 15:16 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/01/22 15:16 V27134TBL
<0.018 mg/Kg - dry 0.018 0.323Ethanol 1 12/01/22 15:16 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 12/01/22 15:16 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 48 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (0-2)
94340 Matrix:
11/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 12/01/22 15:16 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.025
2-Hexanone 1 12/01/22 15:16 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/01/22 15:16 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 12/01/22 15:16 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/01/22 15:16 V27134TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/01/22 15:16 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/01/22 15:16 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 15:16 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/01/22 15:16 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 12/01/22 15:16 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/01/22 15:16 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 15:16 V27134TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/01/22 15:16 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/01/22 15:16 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 49 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (0-2)
94340 Matrix:
11/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/01/22 15:16 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 12/01/22 15:16 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/01/22 15:16 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/01/22 15:16 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/01/22 15:16 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/01/22 15:16 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/01/22 15:16 V27134
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%12/01/22 15:161 TBL V27134
Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/01/22 15:161 TBL V27134
Surrogate: Toluene-d8 95.3 Limits: 76-129%12/01/22 15:161 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.150 mg/Kg - dry 0.150 0.854Acenaphthene 1 12/04/22 16:26 V27410JMV
<0.136 mg/Kg - dry 0.136 0.854Acenaphthylene 1 12/04/22 16:26 V27410JMV
<0.196 mg/Kg - dry 0.196 0.854Aniline 1 12/04/22 16:26 V27410JMV
<0.185 mg/Kg - dry 0.185 0.854Anthracene 1 12/04/22 16:26 V27410JMV
<0.180 mg/Kg - dry 0.180 0.854
Benzo(a)anthracene 1 12/04/22 16:26 V27410JMV
<0.190 mg/Kg - dry 0.190 0.854Benzo(a)pyrene 1 12/04/22 16:26 V27410JMV
<0.189 mg/Kg - dry 0.189 0.854Benzo(b)fluoranthene 1 12/04/22 16:26 V27410JMV
<0.176 mg/Kg - dry 0.176 0.854Benzo(g,h,i)perylene 1 12/04/22 16:26 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 50 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (0-2)
94340 Matrix:
11/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.177 mg/Kg - dry 0.177 0.854Benzo(k)fluoranthene 1 12/04/22 16:26 V27410JMV
<0.751 M
mg/Kg - dry 0.751 2.59
Benzoic Acid 1 12/04/22 16:26 V27410JMV
<0.136 mg/Kg - dry 0.136 0.854Benzyl alcohol 1 12/04/22 16:26 V27410JMV
<0.152 mg/Kg - dry 0.152 0.854Bis(2-Chloroethoxy)methane 1 12/04/22 16:26 V27410JMV
<0.138 mg/Kg - dry 0.138 0.854Bis(2-Chloroethyl)ether 1 12/04/22 16:26 V27410JMV
<0.176 mg/Kg - dry 0.176 0.427Bis(2-Chloroisopropyl)ether 1 12/04/22 16:26 V27410JMV
<0.155 mg/Kg - dry 0.155 0.854Bis(2-ethylhexyl)phthalate 1 12/04/22 16:26 V27410JMV
<0.141 mg/Kg - dry 0.141 0.8544-Bromophenyl phenyl ether 1 12/04/22 16:26 V27410JMV
<0.146 mg/Kg - dry 0.146 0.427
Butyl benzyl phthalate 1 12/04/22 16:26 V27410JMV
<0.119 mg/Kg - dry 0.119 0.8544-Chloro-3-methylphenol 1 12/04/22 16:26 V27410JMV
<0.145 mg/Kg - dry 0.145 0.4274-Chloroaniline 1 12/04/22 16:26 V27410JMV
<0.150 mg/Kg - dry 0.150 0.8542-Chloronaphthalene 1 12/04/22 16:26 V27410JMV
<0.127 mg/Kg - dry 0.127 0.8542-Chlorophenol 1 12/04/22 16:26 V27410JMV
<0.163 mg/Kg - dry 0.163 1.304-Chlorophenyl phenyl ether 1 12/04/22 16:26 V27410JMV
<0.183 mg/Kg - dry 0.183 0.854Chrysene 1 12/04/22 16:26 V27410JMV
<0.297 mg/Kg - dry 0.297 0.854Dibenz(a,h)anthracene 1 12/04/22 16:26 V27410JMV
<0.154 mg/Kg - dry 0.154 0.854Dibenzofuran 1 12/04/22 16:26 V27410JMV
<0.122 mg/Kg - dry 0.122 0.8541,2-Dichlorobenzene 1 12/04/22 16:26 V27410JMV
<0.126 mg/Kg - dry 0.126 0.8541,3-Dichlorobenzene 1 12/04/22 16:26 V27410JMV
<0.126 mg/Kg - dry 0.126 0.4271,4-Dichlorobenzene 1 12/04/22 16:26 V27410JMV
<0.190 mg/Kg - dry 0.190 0.8543,3'-Dichlorobenzidine 1 12/04/22 16:26 V27410JMV
<0.124 mg/Kg - dry 0.124 0.8542,4-Dichlorophenol 1 12/04/22 16:26 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 51 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (0-2)
94340 Matrix:
11/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.233 mg/Kg - dry 0.233 0.854Diethyl phthalate 1 12/04/22 16:26 V27410JMV
<0.225 mg/Kg - dry 0.225 0.854
Dimethyl phthalate 1 12/04/22 16:26 V27410JMV
<0.139 mg/Kg - dry 0.139 0.4272,4-Dimethylphenol 1 12/04/22 16:26 V27410JMV
<0.138 mg/Kg - dry 0.138 0.854Di-n-butyl phthalate 1 12/04/22 16:26 V27410JMV
<0.310 mg/Kg - dry 0.310 1.944,6-Dinitro-2-methylphenol 1 12/04/22 16:26 V27410JMV
<0.673 mg/Kg - dry 0.673 1.942,4-Dinitrophenol 1 12/04/22 16:26 V27410JMV
<0.125 mg/Kg - dry 0.125 0.8542,4-Dinitrotoluene 1 12/04/22 16:26 V27410JMV
<0.139 mg/Kg - dry 0.139 0.8542,6-Dinitrotoluene 1 12/04/22 16:26 V27410JMV
<0.185 mg/Kg - dry 0.185 0.427
Di-n-Octyl Phthalate 1 12/04/22 16:26 V27410JMV
<0.159 mg/Kg - dry 0.159 0.854Fluoranthene 1 12/04/22 16:26 V27410JMV
<0.165 mg/Kg - dry 0.165 0.854Fluorene 1 12/04/22 16:26 V27410JMV
<0.137 mg/Kg - dry 0.137 0.854Hexachlorobenzene 1 12/04/22 16:26 V27410JMV
<0.126 mg/Kg - dry 0.126 0.854Hexachlorobutadiene 1 12/04/22 16:26 V27410JMV
<0.203 mg/Kg - dry 0.203 0.854Hexachlorocyclopentadiene 1 12/04/22 16:26 V27410JMV
<0.102 mg/Kg - dry 0.102 0.854Hexachloroethane 1 12/04/22 16:26 V27410JMV
<0.231 mg/Kg - dry 0.231 0.854Indeno(1,2,3-cd)pyrene 1 12/04/22 16:26 V27410JMV
<0.247 mg/Kg - dry 0.247 0.854Isophorone 1 12/04/22 16:26 V27410JMV
<0.137 mg/Kg - dry 0.137 0.8541-Methylnaphthalene 1 12/04/22 16:26 V27410JMV
<0.129 mg/Kg - dry 0.129 0.8542-Methylnaphthalene 1 12/04/22 16:26 V27410JMV
<0.125 mg/Kg - dry 0.125 0.8542-Methylphenol 1 12/04/22 16:26 V27410JMV
<0.109 mg/Kg - dry 0.109 0.8543&4 Methylphenol 1 12/04/22 16:26 V27410JMV
<0.186 mg/Kg - dry 0.186 0.854Naphthalene 1 12/04/22 16:26 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 52 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (0-2)
94340 Matrix:
11/28/2022 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.125 mg/Kg - dry 0.125 0.8542-Nitroaniline 1 12/04/22 16:26 V27410JMV
<0.155 mg/Kg - dry 0.155 0.854
3-Nitroaniline 1 12/04/22 16:26 V27410JMV
<0.120 mg/Kg - dry 0.120 0.4274-Nitroaniline 1 12/04/22 16:26 V27410JMV
<0.150 mg/Kg - dry 0.150 0.427Nitrobenzene 1 12/04/22 16:26 V27410JMV
<0.115 mg/Kg - dry 0.115 0.8542-Nitrophenol 1 12/04/22 16:26 V27410JMV
<0.151 mg/Kg - dry 0.151 0.8544-Nitrophenol 1 12/04/22 16:26 V27410JMV
<0.340 mg/Kg - dry 0.340 0.854N-Nitrosodimethylamine 1 12/04/22 16:26 V27410JMV
<0.234 mg/Kg - dry 0.234 0.854N-Nitrosodiphenylamine 1 12/04/22 16:26 V27410JMV
<0.152 mg/Kg - dry 0.152 0.854
N-Nitroso-di-n-propylamine 1 12/04/22 16:26 V27410JMV
<0.449 mg/Kg - dry 0.449 1.30Pentachlorophenol 1 12/04/22 16:26 V27410JMV
<0.269 mg/Kg - dry 0.269 0.854Phenanthrene 1 12/04/22 16:26 V27410JMV
<0.145 mg/Kg - dry 0.145 0.854Phenol 1 12/04/22 16:26 V27410JMV
<0.173 mg/Kg - dry 0.173 0.854Pyrene 1 12/04/22 16:26 V27410JMV
<0.102 mg/Kg - dry 0.102 0.427Pyridine 1 12/04/22 16:26 V27410JMV
<0.138 mg/Kg - dry 0.138 0.8541,2,4-Trichlorobenzene 1 12/04/22 16:26 V27410JMV
<0.124 mg/Kg - dry 0.124 0.8542,4,5-Trichlorophenol 1 12/04/22 16:26 V27410JMV
<0.125 mg/Kg - dry 0.125 0.8542,4,6-Trichlorophenol 1 12/04/22 16:26 V27410JMV
8270ESurrogate: Phenol-d5 77.2 Limits: 34-121%12/04/22 16:261 JMV
Surrogate: 2-Fluorobiphenyl 91.6 Limits: 44-115%12/04/22 16:261 JMV V27410
Surrogate: 2-Fluorophenol 81.4 Limits: 35-115%12/04/22 16:261 JMV V27410
Surrogate: Nitrobenzene-d5 82.6 Limits: 37-122%12/04/22 16:261 JMV V27410
Surrogate: 4-Terphenyl-d14 113 Limits: 54-127%12/04/22 16:261 JMV V27410
Surrogate: 2,4,6-Tribromophenol 83.2 Limits: 39-132%12/04/22 16:261 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 53 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (2-4)
94341 Matrix:
11/28/2022 13:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.2 %Moisture 1 12/01/22 18:23 SW-DRYWTAMB
<0.184 mg/Kg - dry 0.184 0.262Chromium, Hexavalent 1 12/06/22 19:18 SW-7199SAR
1.87 mg/Kg - dry 0.174 1.27Arsenic 10 12/08/22 18:07 6020BEDV
20.8 mg/Kg - dry 1.78 12.7Barium 10 12/08/22 18:07 6020BEDV
<0.0837 mg/Kg - dry 0.0837 0.635Cadmium 10 12/08/22 18:07 6020BEDV
97.2 mg/Kg - dry 0.251 1.27
Chromium 10 12/08/22 18:07 6020BEDV
8.27 mg/Kg - dry 0.185 1.27Lead 10 12/08/22 18:07 6020BEDV
0.0994 mg/Kg - dry 0.0152 0.0381Mercury (Total)1 12/05/22 14:02 7471BEDV
<0.940 mg/Kg - dry 0.940 2.54Selenium 10 12/08/22 18:07 6020BEDV
<0.0596 mg/Kg - dry 0.0596 0.635Silver 10 12/08/22 18:07 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 54 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (2-4)
94341 Matrix:
11/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
0.003 J mg/Kg - dry 0.003 0.025Acetone 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.025
Acrolein 1 12/01/22 15:43 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 12/01/22 15:43 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/01/22 15:43 V27134TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/01/22 15:43 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/01/22 15:43 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/01/22 15:43 V27134TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/01/22 15:43 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/01/22 15:43 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 12/01/22 15:43 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/01/22 15:43 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/01/22 15:43 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 55 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (2-4)
94341 Matrix:
11/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 12/01/22 15:43 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 12/01/22 15:43 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/01/22 15:43 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/01/22 15:43 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/01/22 15:43 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/01/22 15:43 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/01/22 15:43 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/01/22 15:43 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 12/01/22 15:43 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/01/22 15:43 V27134TBL
<0.017 mg/Kg - dry 0.017 0.317Ethanol 1 12/01/22 15:43 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 12/01/22 15:43 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 56 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (2-4)
94341 Matrix:
11/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 12/01/22 15:43 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.025
2-Hexanone 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/01/22 15:43 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 12/01/22 15:43 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/01/22 15:43 V27134TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/01/22 15:43 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/01/22 15:43 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 15:43 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 12/01/22 15:43 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 12/01/22 15:43 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 15:43 V27134TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/01/22 15:43 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/01/22 15:43 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 57 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (2-4)
94341 Matrix:
11/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/01/22 15:43 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/01/22 15:43 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/01/22 15:43 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/01/22 15:43 V27134
Surrogate: 4-Bromofluorobenzene 98.5 Limits: 70-130%12/01/22 15:431 TBL V27134
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/01/22 15:431 TBL V27134
Surrogate: Toluene-d8 95.2 Limits: 76-129%12/01/22 15:431 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.147 mg/Kg - dry 0.147 0.837Acenaphthene 1 12/06/22 21:43 V27495JMV
<0.133 mg/Kg - dry 0.133 0.837Acenaphthylene 1 12/06/22 21:43 V27495JMV
<0.192 mg/Kg - dry 0.192 0.837Aniline 1 12/06/22 21:43 V27495JMV
<0.181 mg/Kg - dry 0.181 0.837Anthracene 1 12/06/22 21:43 V27495JMV
<0.176 mg/Kg - dry 0.176 0.837
Benzo(a)anthracene 1 12/06/22 21:43 V27495JMV
<0.186 mg/Kg - dry 0.186 0.837Benzo(a)pyrene 1 12/06/22 21:43 V27495JMV
<0.185 mg/Kg - dry 0.185 0.837Benzo(b)fluoranthene 1 12/06/22 21:43 V27495JMV
<0.172 mg/Kg - dry 0.172 0.837Benzo(g,h,i)perylene 1 12/06/22 21:43 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 58 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (2-4)
94341 Matrix:
11/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.173 mg/Kg - dry 0.173 0.837Benzo(k)fluoranthene 1 12/06/22 21:43 V27495JMV
<0.736 M
mg/Kg - dry 0.736 2.54
Benzoic Acid 1 12/06/22 21:43 V27495JMV
<0.133 mg/Kg - dry 0.133 0.837Benzyl alcohol 1 12/06/22 21:43 V27495JMV
<0.149 mg/Kg - dry 0.149 0.837Bis(2-Chloroethoxy)methane 1 12/06/22 21:43 V27495JMV
<0.135 mg/Kg - dry 0.135 0.837Bis(2-Chloroethyl)ether 1 12/06/22 21:43 V27495JMV
<0.172 mg/Kg - dry 0.172 0.418Bis(2-Chloroisopropyl)ether 1 12/06/22 21:43 V27495JMV
<0.152 mg/Kg - dry 0.152 0.837Bis(2-ethylhexyl)phthalate 1 12/06/22 21:43 V27495JMV
<0.138 mg/Kg - dry 0.138 0.8374-Bromophenyl phenyl ether 1 12/06/22 21:43 V27495JMV
<0.143 mg/Kg - dry 0.143 0.418
Butyl benzyl phthalate 1 12/06/22 21:43 V27495JMV
<0.117 mg/Kg - dry 0.117 0.8374-Chloro-3-methylphenol 1 12/06/22 21:43 V27495JMV
<0.142 mg/Kg - dry 0.142 0.4184-Chloroaniline 1 12/06/22 21:43 V27495JMV
<0.147 mg/Kg - dry 0.147 0.8372-Chloronaphthalene 1 12/06/22 21:43 V27495JMV
<0.124 mg/Kg - dry 0.124 0.8372-Chlorophenol 1 12/06/22 21:43 V27495JMV
<0.159 mg/Kg - dry 0.159 1.274-Chlorophenyl phenyl ether 1 12/06/22 21:43 V27495JMV
<0.180 mg/Kg - dry 0.180 0.837Chrysene 1 12/06/22 21:43 V27495JMV
<0.291 mg/Kg - dry 0.291 0.837Dibenz(a,h)anthracene 1 12/06/22 21:43 V27495JMV
<0.151 mg/Kg - dry 0.151 0.837Dibenzofuran 1 12/06/22 21:43 V27495JMV
<0.119 mg/Kg - dry 0.119 0.8371,2-Dichlorobenzene 1 12/06/22 21:43 V27495JMV
<0.123 mg/Kg - dry 0.123 0.8371,3-Dichlorobenzene 1 12/06/22 21:43 V27495JMV
<0.123 mg/Kg - dry 0.123 0.4181,4-Dichlorobenzene 1 12/06/22 21:43 V27495JMV
<0.186 mg/Kg - dry 0.186 0.8373,3'-Dichlorobenzidine 1 12/06/22 21:43 V27495JMV
<0.121 mg/Kg - dry 0.121 0.8372,4-Dichlorophenol 1 12/06/22 21:43 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 59 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (2-4)
94341 Matrix:
11/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.228 mg/Kg - dry 0.228 0.837Diethyl phthalate 1 12/06/22 21:43 V27495JMV
<0.220 mg/Kg - dry 0.220 0.837
Dimethyl phthalate 1 12/06/22 21:43 V27495JMV
<0.137 mg/Kg - dry 0.137 0.4182,4-Dimethylphenol 1 12/06/22 21:43 V27495JMV
<0.135 mg/Kg - dry 0.135 0.837Di-n-butyl phthalate 1 12/06/22 21:43 V27495JMV
<0.304 mg/Kg - dry 0.304 1.904,6-Dinitro-2-methylphenol 1 12/06/22 21:43 V27495JMV
<0.659 mg/Kg - dry 0.659 1.902,4-Dinitrophenol 1 12/06/22 21:43 V27495JMV
<0.122 mg/Kg - dry 0.122 0.8372,4-Dinitrotoluene 1 12/06/22 21:43 V27495JMV
<0.137 mg/Kg - dry 0.137 0.8372,6-Dinitrotoluene 1 12/06/22 21:43 V27495JMV
<0.181 mg/Kg - dry 0.181 0.418
Di-n-Octyl Phthalate 1 12/06/22 21:43 V27495JMV
<0.156 mg/Kg - dry 0.156 0.837Fluoranthene 1 12/06/22 21:43 V27495JMV
<0.162 mg/Kg - dry 0.162 0.837Fluorene 1 12/06/22 21:43 V27495JMV
<0.134 mg/Kg - dry 0.134 0.837Hexachlorobenzene 1 12/06/22 21:43 V27495JMV
<0.123 mg/Kg - dry 0.123 0.837Hexachlorobutadiene 1 12/06/22 21:43 V27495JMV
<0.199 mg/Kg - dry 0.199 0.837Hexachlorocyclopentadiene 1 12/06/22 21:43 V27495JMV
<0.100 mg/Kg - dry 0.100 0.837Hexachloroethane 1 12/06/22 21:43 V27495JMV
<0.227 mg/Kg - dry 0.227 0.837Indeno(1,2,3-cd)pyrene 1 12/06/22 21:43 V27495JMV
<0.242 mg/Kg - dry 0.242 0.837Isophorone 1 12/06/22 21:43 V27495JMV
<0.134 mg/Kg - dry 0.134 0.8371-Methylnaphthalene 1 12/06/22 21:43 V27495JMV
<0.126 mg/Kg - dry 0.126 0.8372-Methylnaphthalene 1 12/06/22 21:43 V27495JMV
<0.123 mg/Kg - dry 0.123 0.8372-Methylphenol 1 12/06/22 21:43 V27495JMV
<0.107 mg/Kg - dry 0.107 0.8373&4 Methylphenol 1 12/06/22 21:43 V27495JMV
<0.182 mg/Kg - dry 0.182 0.837Naphthalene 1 12/06/22 21:43 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 60 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (2-4)
94341 Matrix:
11/28/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.122 mg/Kg - dry 0.122 0.8372-Nitroaniline 1 12/06/22 21:43 V27495JMV
<0.152 mg/Kg - dry 0.152 0.837
3-Nitroaniline 1 12/06/22 21:43 V27495JMV
<0.118 mg/Kg - dry 0.118 0.4184-Nitroaniline 1 12/06/22 21:43 V27495JMV
<0.147 mg/Kg - dry 0.147 0.418Nitrobenzene 1 12/06/22 21:43 V27495JMV
<0.112 mg/Kg - dry 0.112 0.8372-Nitrophenol 1 12/06/22 21:43 V27495JMV
<0.148 mg/Kg - dry 0.148 0.8374-Nitrophenol 1 12/06/22 21:43 V27495JMV
<0.333 mg/Kg - dry 0.333 0.837N-Nitrosodimethylamine 1 12/06/22 21:43 V27495JMV
<0.229 mg/Kg - dry 0.229 0.837N-Nitrosodiphenylamine 1 12/06/22 21:43 V27495JMV
<0.149 mg/Kg - dry 0.149 0.837
N-Nitroso-di-n-propylamine 1 12/06/22 21:43 V27495JMV
<0.440 mg/Kg - dry 0.440 1.27Pentachlorophenol 1 12/06/22 21:43 V27495JMV
<0.263 mg/Kg - dry 0.263 0.837Phenanthrene 1 12/06/22 21:43 V27495JMV
<0.142 mg/Kg - dry 0.142 0.837Phenol 1 12/06/22 21:43 V27495JMV
<0.170 mg/Kg - dry 0.170 0.837Pyrene 1 12/06/22 21:43 V27495JMV
<0.100 mg/Kg - dry 0.100 0.418Pyridine 1 12/06/22 21:43 V27495JMV
<0.135 mg/Kg - dry 0.135 0.8371,2,4-Trichlorobenzene 1 12/06/22 21:43 V27495JMV
<0.122 mg/Kg - dry 0.122 0.8372,4,5-Trichlorophenol 1 12/06/22 21:43 V27495JMV
<0.122 mg/Kg - dry 0.122 0.8372,4,6-Trichlorophenol 1 12/06/22 21:43 V27495JMV
8270ESurrogate: Phenol-d5 67.9 Limits: 34-121%12/06/22 21:431 JMV
Surrogate: 2-Fluorobiphenyl 89.2 Limits: 44-115%12/06/22 21:431 JMV V27495
Surrogate: 2-Fluorophenol 73.9 Limits: 35-115%12/06/22 21:431 JMV V27495
Surrogate: Nitrobenzene-d5 77.2 Limits: 37-122%12/06/22 21:431 JMV V27495
Surrogate: 4-Terphenyl-d14 98.2 Limits: 54-127%12/06/22 21:431 JMV V27495
Surrogate: 2,4,6-Tribromophenol 81.1 Limits: 39-132%12/06/22 21:431 JMV V27495
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 61 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (4-6)
94342 Matrix:
11/28/2022 13:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.9 %Moisture 1 12/01/22 18:23 SW-DRYWTAMB
1.74 mg/Kg - dry 0.195 0.279Chromium, Hexavalent 1 12/06/22 19:29 SW-7199SAR
1.50 mg/Kg - dry 0.185 1.35Arsenic 10 12/08/22 18:13 6020BEDV
11.3 J mg/Kg - dry 1.89 13.5Barium 10 12/08/22 18:13 6020BEDV
<0.0890 mg/Kg - dry 0.0890 0.675Cadmium 10 12/08/22 18:13 6020BEDV
61.5 mg/Kg - dry 0.267 1.35
Chromium 10 12/08/22 18:13 6020BEDV
6.28 mg/Kg - dry 0.197 1.35Lead 10 12/08/22 18:13 6020BEDV
<0.0162 mg/Kg - dry 0.0162 0.0405Mercury (Total)1 12/02/22 14:40 7471BMMR
<1.00 mg/Kg - dry 1.00 2.70Selenium 10 12/08/22 18:13 6020BEDV
<0.0634 mg/Kg - dry 0.0634 0.675Silver 10 12/08/22 18:13 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 62 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (4-6)
94342 Matrix:
11/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.003 mg/Kg - dry 0.003 0.026Acetone 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.026
Acrolein 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 12/01/22 16:11 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/01/22 16:11 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 12/01/22 16:11 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 12/01/22 16:11 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 12/01/22 16:11 V27134TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/01/22 16:11 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/01/22 16:11 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/01/22 16:11 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/01/22 16:11 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 12/01/22 16:11 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 63 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (4-6)
94342 Matrix:
11/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 12/01/22 16:11 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 12/01/22 16:11 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 12/01/22 16:11 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/01/22 16:11 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/01/22 16:11 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/01/22 16:11 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/01/22 16:11 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/01/22 16:11 V27134TBL
<0.018 mg/Kg - dry 0.018 0.337Ethanol 1 12/01/22 16:11 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 12/01/22 16:11 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 64 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (4-6)
94342 Matrix:
11/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 12/01/22 16:11 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.026
2-Hexanone 1 12/01/22 16:11 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/01/22 16:11 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 12/01/22 16:11 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/01/22 16:11 V27134TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/01/22 16:11 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 16:11 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 12/01/22 16:11 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/01/22 16:11 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 16:11 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 12/01/22 16:11 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 12/01/22 16:11 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 65 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (4-6)
94342 Matrix:
11/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 12/01/22 16:11 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 12/01/22 16:11 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 12/01/22 16:11 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 12/01/22 16:11 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 12/01/22 16:11 V27134
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/01/22 16:111 TBL V27134
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/01/22 16:111 TBL V27134
Surrogate: Toluene-d8 92.7 Limits: 76-129%12/01/22 16:111 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.156 mg/Kg - dry 0.156 0.890Acenaphthene 1 12/04/22 11:12 V27410JMV
<0.141 mg/Kg - dry 0.141 0.890Acenaphthylene 1 12/04/22 11:12 V27410JMV
<0.205 mg/Kg - dry 0.205 0.890Aniline 1 12/04/22 11:12 V27410JMV
<0.192 mg/Kg - dry 0.192 0.890Anthracene 1 12/04/22 11:12 V27410JMV
<0.187 mg/Kg - dry 0.187 0.890
Benzo(a)anthracene 1 12/04/22 11:12 V27410JMV
<0.198 mg/Kg - dry 0.198 0.890Benzo(a)pyrene 1 12/04/22 11:12 V27410JMV
<0.197 mg/Kg - dry 0.197 0.890Benzo(b)fluoranthene 1 12/04/22 11:12 V27410JMV
<0.183 mg/Kg - dry 0.183 0.890Benzo(g,h,i)perylene 1 12/04/22 11:12 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 66 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (4-6)
94342 Matrix:
11/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.184 mg/Kg - dry 0.184 0.890Benzo(k)fluoranthene 1 12/04/22 11:12 V27410JMV
<0.782 mg/Kg - dry 0.782 2.70
Benzoic Acid 1 12/04/22 11:12 V27410JMV
<0.141 mg/Kg - dry 0.141 0.890Benzyl alcohol 1 12/04/22 11:12 V27410JMV
<0.159 mg/Kg - dry 0.159 0.890Bis(2-Chloroethoxy)methane 1 12/04/22 11:12 V27410JMV
<0.144 mg/Kg - dry 0.144 0.890Bis(2-Chloroethyl)ether 1 12/04/22 11:12 V27410JMV
<0.183 mg/Kg - dry 0.183 0.445Bis(2-Chloroisopropyl)ether 1 12/04/22 11:12 V27410JMV
<0.161 mg/Kg - dry 0.161 0.890Bis(2-ethylhexyl)phthalate 1 12/04/22 11:12 V27410JMV
<0.147 mg/Kg - dry 0.147 0.8904-Bromophenyl phenyl ether 1 12/04/22 11:12 V27410JMV
<0.152 mg/Kg - dry 0.152 0.445
Butyl benzyl phthalate 1 12/04/22 11:12 V27410JMV
<0.124 mg/Kg - dry 0.124 0.8904-Chloro-3-methylphenol 1 12/04/22 11:12 V27410JMV
<0.151 mg/Kg - dry 0.151 0.4454-Chloroaniline 1 12/04/22 11:12 V27410JMV
<0.156 mg/Kg - dry 0.156 0.8902-Chloronaphthalene 1 12/04/22 11:12 V27410JMV
<0.132 mg/Kg - dry 0.132 0.8902-Chlorophenol 1 12/04/22 11:12 V27410JMV
<0.170 mg/Kg - dry 0.170 1.354-Chlorophenyl phenyl ether 1 12/04/22 11:12 V27410JMV
<0.191 mg/Kg - dry 0.191 0.890Chrysene 1 12/04/22 11:12 V27410JMV
<0.310 mg/Kg - dry 0.310 0.890Dibenz(a,h)anthracene 1 12/04/22 11:12 V27410JMV
<0.160 mg/Kg - dry 0.160 0.890Dibenzofuran 1 12/04/22 11:12 V27410JMV
<0.127 mg/Kg - dry 0.127 0.8901,2-Dichlorobenzene 1 12/04/22 11:12 V27410JMV
<0.131 mg/Kg - dry 0.131 0.8901,3-Dichlorobenzene 1 12/04/22 11:12 V27410JMV
<0.131 mg/Kg - dry 0.131 0.4451,4-Dichlorobenzene 1 12/04/22 11:12 V27410JMV
<0.198 mg/Kg - dry 0.198 0.8903,3'-Dichlorobenzidine 1 12/04/22 11:12 V27410JMV
<0.129 mg/Kg - dry 0.129 0.8902,4-Dichlorophenol 1 12/04/22 11:12 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 67 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (4-6)
94342 Matrix:
11/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.242 mg/Kg - dry 0.242 0.890Diethyl phthalate 1 12/04/22 11:12 V27410JMV
<0.234 mg/Kg - dry 0.234 0.890
Dimethyl phthalate 1 12/04/22 11:12 V27410JMV
<0.145 mg/Kg - dry 0.145 0.4452,4-Dimethylphenol 1 12/04/22 11:12 V27410JMV
<0.144 mg/Kg - dry 0.144 0.890Di-n-butyl phthalate 1 12/04/22 11:12 V27410JMV
<0.323 mg/Kg - dry 0.323 2.024,6-Dinitro-2-methylphenol 1 12/04/22 11:12 V27410JMV
<0.701 mg/Kg - dry 0.701 2.022,4-Dinitrophenol 1 12/04/22 11:12 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8902,4-Dinitrotoluene 1 12/04/22 11:12 V27410JMV
<0.145 mg/Kg - dry 0.145 0.8902,6-Dinitrotoluene 1 12/04/22 11:12 V27410JMV
<0.192 mg/Kg - dry 0.192 0.445
Di-n-Octyl Phthalate 1 12/04/22 11:12 V27410JMV
<0.165 mg/Kg - dry 0.165 0.890Fluoranthene 1 12/04/22 11:12 V27410JMV
<0.172 mg/Kg - dry 0.172 0.890Fluorene 1 12/04/22 11:12 V27410JMV
<0.143 mg/Kg - dry 0.143 0.890Hexachlorobenzene 1 12/04/22 11:12 V27410JMV
<0.131 mg/Kg - dry 0.131 0.890Hexachlorobutadiene 1 12/04/22 11:12 V27410JMV
<0.211 mg/Kg - dry 0.211 0.890Hexachlorocyclopentadiene 1 12/04/22 11:12 V27410JMV
<0.106 mg/Kg - dry 0.106 0.890Hexachloroethane 1 12/04/22 11:12 V27410JMV
<0.241 mg/Kg - dry 0.241 0.890Indeno(1,2,3-cd)pyrene 1 12/04/22 11:12 V27410JMV
<0.257 mg/Kg - dry 0.257 0.890Isophorone 1 12/04/22 11:12 V27410JMV
<0.143 mg/Kg - dry 0.143 0.8901-Methylnaphthalene 1 12/04/22 11:12 V27410JMV
<0.134 mg/Kg - dry 0.134 0.8902-Methylnaphthalene 1 12/04/22 11:12 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8902-Methylphenol 1 12/04/22 11:12 V27410JMV
<0.114 mg/Kg - dry 0.114 0.8903&4 Methylphenol 1 12/04/22 11:12 V27410JMV
<0.194 mg/Kg - dry 0.194 0.890Naphthalene 1 12/04/22 11:12 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 68 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (4-6)
94342 Matrix:
11/28/2022 13:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.130 mg/Kg - dry 0.130 0.8902-Nitroaniline 1 12/04/22 11:12 V27410JMV
<0.161 mg/Kg - dry 0.161 0.890
3-Nitroaniline 1 12/04/22 11:12 V27410JMV
<0.125 mg/Kg - dry 0.125 0.4454-Nitroaniline 1 12/04/22 11:12 V27410JMV
<0.156 mg/Kg - dry 0.156 0.445Nitrobenzene 1 12/04/22 11:12 V27410JMV
<0.119 mg/Kg - dry 0.119 0.8902-Nitrophenol 1 12/04/22 11:12 V27410JMV
<0.157 mg/Kg - dry 0.157 0.8904-Nitrophenol 1 12/04/22 11:12 V27410JMV
<0.354 mg/Kg - dry 0.354 0.890N-Nitrosodimethylamine 1 12/04/22 11:12 V27410JMV
<0.244 mg/Kg - dry 0.244 0.890N-Nitrosodiphenylamine 1 12/04/22 11:12 V27410JMV
<0.159 mg/Kg - dry 0.159 0.890
N-Nitroso-di-n-propylamine 1 12/04/22 11:12 V27410JMV
<0.468 mg/Kg - dry 0.468 1.35Pentachlorophenol 1 12/04/22 11:12 V27410JMV
<0.280 mg/Kg - dry 0.280 0.890Phenanthrene 1 12/04/22 11:12 V27410JMV
<0.151 mg/Kg - dry 0.151 0.890Phenol 1 12/04/22 11:12 V27410JMV
<0.180 mg/Kg - dry 0.180 0.890Pyrene 1 12/04/22 11:12 V27410JMV
<0.106 mg/Kg - dry 0.106 0.445Pyridine 1 12/04/22 11:12 V27410JMV
<0.144 mg/Kg - dry 0.144 0.8901,2,4-Trichlorobenzene 1 12/04/22 11:12 V27410JMV
<0.129 mg/Kg - dry 0.129 0.8902,4,5-Trichlorophenol 1 12/04/22 11:12 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8902,4,6-Trichlorophenol 1 12/04/22 11:12 V27410JMV
8270ESurrogate: Phenol-d5 74.2 Limits: 34-121%12/04/22 11:121 JMV
Surrogate: 2-Fluorobiphenyl 92.2 Limits: 44-115%12/04/22 11:121 JMV V27410
Surrogate: 2-Fluorophenol 78.1 Limits: 35-115%12/04/22 11:121 JMV V27410
Surrogate: Nitrobenzene-d5 82.0 Limits: 37-122%12/04/22 11:121 JMV V27410
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%12/04/22 11:121 JMV V27410
Surrogate: 2,4,6-Tribromophenol 83.2 Limits: 39-132%12/04/22 11:121 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 69 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (6-8)
94343 Matrix:
11/28/2022 14:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.7 %Moisture 1 12/01/22 18:23 SW-DRYWTAMB
<0.189 mg/Kg - dry 0.189 0.269Chromium, Hexavalent 1 12/06/22 19:39 SW-7199SAR
1.06 J mg/Kg - dry 0.184 1.35Arsenic 10 12/08/22 18:20 6020BEDV
20.5 mg/Kg - dry 1.88 13.5Barium 10 12/08/22 18:20 6020BEDV
<0.0888 mg/Kg - dry 0.0888 0.673Cadmium 10 12/08/22 18:20 6020BEDV
61.4 mg/Kg - dry 0.266 1.35
Chromium 10 12/08/22 18:20 6020BEDV
7.99 mg/Kg - dry 0.197 1.35Lead 10 12/08/22 18:20 6020BEDV
<0.0162 mg/Kg - dry 0.0162 0.0404Mercury (Total)1 12/02/22 14:42 7471BMMR
<0.997 mg/Kg - dry 0.997 2.69Selenium 10 12/08/22 18:20 6020BEDV
<0.0632 mg/Kg - dry 0.0632 0.673Silver 10 12/08/22 18:20 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 70 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (6-8)
94343 Matrix:
11/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.003 mg/Kg - dry 0.003 0.026Acetone 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.026
Acrolein 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 12/01/22 16:38 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/01/22 16:38 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 12/01/22 16:38 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 12/01/22 16:38 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 12/01/22 16:38 V27134TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/01/22 16:38 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/01/22 16:38 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/01/22 16:38 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/01/22 16:38 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 12/01/22 16:38 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 71 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (6-8)
94343 Matrix:
11/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 12/01/22 16:38 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 12/01/22 16:38 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 12/01/22 16:38 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/01/22 16:38 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/01/22 16:38 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/01/22 16:38 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/01/22 16:38 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/01/22 16:38 V27134TBL
<0.018 mg/Kg - dry 0.018 0.336Ethanol 1 12/01/22 16:38 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 12/01/22 16:38 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 72 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (6-8)
94343 Matrix:
11/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 12/01/22 16:38 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.026
2-Hexanone 1 12/01/22 16:38 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/01/22 16:38 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 12/01/22 16:38 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/01/22 16:38 V27134TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/01/22 16:38 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 16:38 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 12/01/22 16:38 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/01/22 16:38 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 16:38 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 12/01/22 16:38 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 12/01/22 16:38 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 73 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (6-8)
94343 Matrix:
11/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 12/01/22 16:38 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 12/01/22 16:38 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 12/01/22 16:38 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 12/01/22 16:38 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 12/01/22 16:38 V27134
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%12/01/22 16:381 TBL V27134
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/01/22 16:381 TBL V27134
Surrogate: Toluene-d8 95.8 Limits: 76-129%12/01/22 16:381 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.156 mg/Kg - dry 0.156 0.888Acenaphthene 1 12/04/22 11:35 V27410JMV
<0.141 mg/Kg - dry 0.141 0.888Acenaphthylene 1 12/04/22 11:35 V27410JMV
<0.204 mg/Kg - dry 0.204 0.888Aniline 1 12/04/22 11:35 V27410JMV
<0.192 mg/Kg - dry 0.192 0.888Anthracene 1 12/04/22 11:35 V27410JMV
<0.187 mg/Kg - dry 0.187 0.888
Benzo(a)anthracene 1 12/04/22 11:35 V27410JMV
<0.197 mg/Kg - dry 0.197 0.888Benzo(a)pyrene 1 12/04/22 11:35 V27410JMV
<0.196 mg/Kg - dry 0.196 0.888Benzo(b)fluoranthene 1 12/04/22 11:35 V27410JMV
<0.183 mg/Kg - dry 0.183 0.888Benzo(g,h,i)perylene 1 12/04/22 11:35 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 74 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (6-8)
94343 Matrix:
11/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.184 mg/Kg - dry 0.184 0.888Benzo(k)fluoranthene 1 12/04/22 11:35 V27410JMV
<0.780 M
mg/Kg - dry 0.780 2.69
Benzoic Acid 1 12/04/22 11:35 V27410JMV
<0.141 mg/Kg - dry 0.141 0.888Benzyl alcohol 1 12/04/22 11:35 V27410JMV
<0.158 mg/Kg - dry 0.158 0.888Bis(2-Chloroethoxy)methane 1 12/04/22 11:35 V27410JMV
<0.144 mg/Kg - dry 0.144 0.888Bis(2-Chloroethyl)ether 1 12/04/22 11:35 V27410JMV
<0.183 mg/Kg - dry 0.183 0.444Bis(2-Chloroisopropyl)ether 1 12/04/22 11:35 V27410JMV
<0.161 mg/Kg - dry 0.161 0.888Bis(2-ethylhexyl)phthalate 1 12/04/22 11:35 V27410JMV
<0.146 mg/Kg - dry 0.146 0.8884-Bromophenyl phenyl ether 1 12/04/22 11:35 V27410JMV
<0.152 mg/Kg - dry 0.152 0.444
Butyl benzyl phthalate 1 12/04/22 11:35 V27410JMV
<0.124 mg/Kg - dry 0.124 0.8884-Chloro-3-methylphenol 1 12/04/22 11:35 V27410JMV
<0.150 mg/Kg - dry 0.150 0.4444-Chloroaniline 1 12/04/22 11:35 V27410JMV
<0.156 mg/Kg - dry 0.156 0.8882-Chloronaphthalene 1 12/04/22 11:35 V27410JMV
<0.132 mg/Kg - dry 0.132 0.8882-Chlorophenol 1 12/04/22 11:35 V27410JMV
<0.169 mg/Kg - dry 0.169 1.354-Chlorophenyl phenyl ether 1 12/04/22 11:35 V27410JMV
<0.191 mg/Kg - dry 0.191 0.888Chrysene 1 12/04/22 11:35 V27410JMV
<0.309 mg/Kg - dry 0.309 0.888Dibenz(a,h)anthracene 1 12/04/22 11:35 V27410JMV
<0.160 mg/Kg - dry 0.160 0.888Dibenzofuran 1 12/04/22 11:35 V27410JMV
<0.127 mg/Kg - dry 0.127 0.8881,2-Dichlorobenzene 1 12/04/22 11:35 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8881,3-Dichlorobenzene 1 12/04/22 11:35 V27410JMV
<0.131 mg/Kg - dry 0.131 0.4441,4-Dichlorobenzene 1 12/04/22 11:35 V27410JMV
<0.197 mg/Kg - dry 0.197 0.8883,3'-Dichlorobenzidine 1 12/04/22 11:35 V27410JMV
<0.128 mg/Kg - dry 0.128 0.8882,4-Dichlorophenol 1 12/04/22 11:35 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 75 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (6-8)
94343 Matrix:
11/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.242 mg/Kg - dry 0.242 0.888Diethyl phthalate 1 12/04/22 11:35 V27410JMV
<0.234 mg/Kg - dry 0.234 0.888
Dimethyl phthalate 1 12/04/22 11:35 V27410JMV
<0.145 mg/Kg - dry 0.145 0.4442,4-Dimethylphenol 1 12/04/22 11:35 V27410JMV
<0.144 mg/Kg - dry 0.144 0.888Di-n-butyl phthalate 1 12/04/22 11:35 V27410JMV
<0.323 mg/Kg - dry 0.323 2.024,6-Dinitro-2-methylphenol 1 12/04/22 11:35 V27410JMV
<0.699 mg/Kg - dry 0.699 2.022,4-Dinitrophenol 1 12/04/22 11:35 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8882,4-Dinitrotoluene 1 12/04/22 11:35 V27410JMV
<0.145 mg/Kg - dry 0.145 0.8882,6-Dinitrotoluene 1 12/04/22 11:35 V27410JMV
<0.192 mg/Kg - dry 0.192 0.444
Di-n-Octyl Phthalate 1 12/04/22 11:35 V27410JMV
<0.165 mg/Kg - dry 0.165 0.888Fluoranthene 1 12/04/22 11:35 V27410JMV
<0.172 mg/Kg - dry 0.172 0.888Fluorene 1 12/04/22 11:35 V27410JMV
<0.142 mg/Kg - dry 0.142 0.888Hexachlorobenzene 1 12/04/22 11:35 V27410JMV
<0.131 mg/Kg - dry 0.131 0.888Hexachlorobutadiene 1 12/04/22 11:35 V27410JMV
<0.211 mg/Kg - dry 0.211 0.888Hexachlorocyclopentadiene 1 12/04/22 11:35 V27410JMV
<0.106 mg/Kg - dry 0.106 0.888Hexachloroethane 1 12/04/22 11:35 V27410JMV
<0.240 mg/Kg - dry 0.240 0.888Indeno(1,2,3-cd)pyrene 1 12/04/22 11:35 V27410JMV
<0.257 mg/Kg - dry 0.257 0.888Isophorone 1 12/04/22 11:35 V27410JMV
<0.142 mg/Kg - dry 0.142 0.8881-Methylnaphthalene 1 12/04/22 11:35 V27410JMV
<0.134 mg/Kg - dry 0.134 0.8882-Methylnaphthalene 1 12/04/22 11:35 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8882-Methylphenol 1 12/04/22 11:35 V27410JMV
<0.114 mg/Kg - dry 0.114 0.8883&4 Methylphenol 1 12/04/22 11:35 V27410JMV
<0.193 mg/Kg - dry 0.193 0.888Naphthalene 1 12/04/22 11:35 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 76 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-4 (6-8)
94343 Matrix:
11/28/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.130 mg/Kg - dry 0.130 0.8882-Nitroaniline 1 12/04/22 11:35 V27410JMV
<0.161 mg/Kg - dry 0.161 0.888
3-Nitroaniline 1 12/04/22 11:35 V27410JMV
<0.125 mg/Kg - dry 0.125 0.4444-Nitroaniline 1 12/04/22 11:35 V27410JMV
<0.156 mg/Kg - dry 0.156 0.444Nitrobenzene 1 12/04/22 11:35 V27410JMV
<0.119 mg/Kg - dry 0.119 0.8882-Nitrophenol 1 12/04/22 11:35 V27410JMV
<0.157 mg/Kg - dry 0.157 0.8884-Nitrophenol 1 12/04/22 11:35 V27410JMV
<0.353 mg/Kg - dry 0.353 0.888N-Nitrosodimethylamine 1 12/04/22 11:35 V27410JMV
<0.243 mg/Kg - dry 0.243 0.888N-Nitrosodiphenylamine 1 12/04/22 11:35 V27410JMV
<0.158 mg/Kg - dry 0.158 0.888
N-Nitroso-di-n-propylamine 1 12/04/22 11:35 V27410JMV
<0.467 mg/Kg - dry 0.467 1.35Pentachlorophenol 1 12/04/22 11:35 V27410JMV
<0.279 mg/Kg - dry 0.279 0.888Phenanthrene 1 12/04/22 11:35 V27410JMV
<0.150 mg/Kg - dry 0.150 0.888Phenol 1 12/04/22 11:35 V27410JMV
<0.180 mg/Kg - dry 0.180 0.888Pyrene 1 12/04/22 11:35 V27410JMV
<0.106 mg/Kg - dry 0.106 0.444Pyridine 1 12/04/22 11:35 V27410JMV
<0.144 mg/Kg - dry 0.144 0.8881,2,4-Trichlorobenzene 1 12/04/22 11:35 V27410JMV
<0.129 mg/Kg - dry 0.129 0.8882,4,5-Trichlorophenol 1 12/04/22 11:35 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8882,4,6-Trichlorophenol 1 12/04/22 11:35 V27410JMV
8270ESurrogate: Phenol-d5 74.0 Limits: 34-121%12/04/22 11:351 JMV
Surrogate: 2-Fluorobiphenyl 93.4 Limits: 44-115%12/04/22 11:351 JMV V27410
Surrogate: 2-Fluorophenol 80.5 Limits: 35-115%12/04/22 11:351 JMV V27410
Surrogate: Nitrobenzene-d5 82.0 Limits: 37-122%12/04/22 11:351 JMV V27410
Surrogate: 4-Terphenyl-d14 103 Limits: 54-127%12/04/22 11:351 JMV V27410
Surrogate: 2,4,6-Tribromophenol 84.1 Limits: 39-132%12/04/22 11:351 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 77 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (0-2)
94344 Matrix:
11/28/2022 14:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.9 %Moisture 1 12/01/22 18:23 SW-DRYWTAMB
<0.188 mg/Kg - dry 0.188 0.267Chromium, Hexavalent 1 12/06/22 19:50 SW-7199SAR
2.66 mg/Kg - dry 0.178 1.30Arsenic 10 12/08/22 18:26 6020BEDV
18.5 mg/Kg - dry 1.82 13.0Barium 10 12/08/22 18:26 6020BEDV
<0.0856 mg/Kg - dry 0.0856 0.649Cadmium 10 12/08/22 18:26 6020BEDV
63.7 mg/Kg - dry 0.256 1.30
Chromium 10 12/08/22 18:26 6020BEDV
8.73 mg/Kg - dry 0.189 1.30Lead 10 12/08/22 18:26 6020BEDV
0.0969 mg/Kg - dry 0.0156 0.0389Mercury (Total)1 12/05/22 14:05 7471BEDV
0.968 J mg/Kg - dry 0.961 2.59Selenium 10 12/08/22 18:26 6020BEDV
<0.0609 mg/Kg - dry 0.0609 0.649Silver 10 12/08/22 18:26 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 78 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (0-2)
94344 Matrix:
11/28/2022 14:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
0.018 J mg/Kg - dry 0.003 0.025Acetone 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.025
Acrolein 1 12/01/22 17:05 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 12/01/22 17:05 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/01/22 17:05 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/01/22 17:05 V27134TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/01/22 17:05 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/01/22 17:05 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/01/22 17:05 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/01/22 17:05 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/01/22 17:05 V27134TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/01/22 17:05 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/01/22 17:05 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/01/22 17:05 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/01/22 17:05 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/01/22 17:05 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/01/22 17:05 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 79 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (0-2)
94344 Matrix:
11/28/2022 14:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 12/01/22 17:05 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 12/01/22 17:05 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/01/22 17:05 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/01/22 17:05 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/01/22 17:05 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/01/22 17:05 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/01/22 17:05 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/01/22 17:05 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/01/22 17:05 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 12/01/22 17:05 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/01/22 17:05 V27134TBL
<0.018 mg/Kg - dry 0.018 0.324Ethanol 1 12/01/22 17:05 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 12/01/22 17:05 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 80 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (0-2)
94344 Matrix:
11/28/2022 14:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 12/01/22 17:05 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.025
2-Hexanone 1 12/01/22 17:05 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/01/22 17:05 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 12/01/22 17:05 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/01/22 17:05 V27134TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/01/22 17:05 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/01/22 17:05 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 17:05 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/01/22 17:05 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 12/01/22 17:05 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/01/22 17:05 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 17:05 V27134TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/01/22 17:05 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/01/22 17:05 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 81 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (0-2)
94344 Matrix:
11/28/2022 14:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/01/22 17:05 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 12/01/22 17:05 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/01/22 17:05 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/01/22 17:05 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/01/22 17:05 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/01/22 17:05 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/01/22 17:05 V27134
Surrogate: 4-Bromofluorobenzene 95.9 Limits: 70-130%12/01/22 17:051 TBL V27134
Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/01/22 17:051 TBL V27134
Surrogate: Toluene-d8 93.7 Limits: 76-129%12/01/22 17:051 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.150 mg/Kg - dry 0.150 0.856Acenaphthene 1 12/04/22 13:27 V27410JMV
<0.136 mg/Kg - dry 0.136 0.856Acenaphthylene 1 12/04/22 13:27 V27410JMV
<0.197 mg/Kg - dry 0.197 0.856Aniline 1 12/04/22 13:27 V27410JMV
<0.185 mg/Kg - dry 0.185 0.856Anthracene 1 12/04/22 13:27 V27410JMV
<0.180 mg/Kg - dry 0.180 0.856
Benzo(a)anthracene 1 12/04/22 13:27 V27410JMV
<0.190 mg/Kg - dry 0.190 0.856Benzo(a)pyrene 1 12/04/22 13:27 V27410JMV
<0.189 mg/Kg - dry 0.189 0.856Benzo(b)fluoranthene 1 12/04/22 13:27 V27410JMV
<0.176 mg/Kg - dry 0.176 0.856Benzo(g,h,i)perylene 1 12/04/22 13:27 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 82 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (0-2)
94344 Matrix:
11/28/2022 14:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.177 mg/Kg - dry 0.177 0.856Benzo(k)fluoranthene 1 12/04/22 13:27 V27410JMV
<0.752 M
mg/Kg - dry 0.752 2.59
Benzoic Acid 1 12/04/22 13:27 V27410JMV
<0.136 mg/Kg - dry 0.136 0.856Benzyl alcohol 1 12/04/22 13:27 V27410JMV
<0.153 mg/Kg - dry 0.153 0.856Bis(2-Chloroethoxy)methane 1 12/04/22 13:27 V27410JMV
<0.138 mg/Kg - dry 0.138 0.856Bis(2-Chloroethyl)ether 1 12/04/22 13:27 V27410JMV
<0.176 mg/Kg - dry 0.176 0.428Bis(2-Chloroisopropyl)ether 1 12/04/22 13:27 V27410JMV
<0.155 mg/Kg - dry 0.155 0.856Bis(2-ethylhexyl)phthalate 1 12/04/22 13:27 V27410JMV
<0.141 mg/Kg - dry 0.141 0.8564-Bromophenyl phenyl ether 1 12/04/22 13:27 V27410JMV
<0.146 mg/Kg - dry 0.146 0.428
Butyl benzyl phthalate 1 12/04/22 13:27 V27410JMV
<0.119 mg/Kg - dry 0.119 0.8564-Chloro-3-methylphenol 1 12/04/22 13:27 V27410JMV
<0.145 mg/Kg - dry 0.145 0.4284-Chloroaniline 1 12/04/22 13:27 V27410JMV
<0.150 mg/Kg - dry 0.150 0.8562-Chloronaphthalene 1 12/04/22 13:27 V27410JMV
<0.127 mg/Kg - dry 0.127 0.8562-Chlorophenol 1 12/04/22 13:27 V27410JMV
<0.163 mg/Kg - dry 0.163 1.304-Chlorophenyl phenyl ether 1 12/04/22 13:27 V27410JMV
<0.184 mg/Kg - dry 0.184 0.856Chrysene 1 12/04/22 13:27 V27410JMV
<0.298 mg/Kg - dry 0.298 0.856Dibenz(a,h)anthracene 1 12/04/22 13:27 V27410JMV
<0.154 mg/Kg - dry 0.154 0.856Dibenzofuran 1 12/04/22 13:27 V27410JMV
<0.122 mg/Kg - dry 0.122 0.8561,2-Dichlorobenzene 1 12/04/22 13:27 V27410JMV
<0.126 mg/Kg - dry 0.126 0.8561,3-Dichlorobenzene 1 12/04/22 13:27 V27410JMV
<0.126 mg/Kg - dry 0.126 0.4281,4-Dichlorobenzene 1 12/04/22 13:27 V27410JMV
<0.190 mg/Kg - dry 0.190 0.8563,3'-Dichlorobenzidine 1 12/04/22 13:27 V27410JMV
<0.124 mg/Kg - dry 0.124 0.8562,4-Dichlorophenol 1 12/04/22 13:27 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 83 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (0-2)
94344 Matrix:
11/28/2022 14:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.233 mg/Kg - dry 0.233 0.856Diethyl phthalate 1 12/04/22 13:27 V27410JMV
<0.225 mg/Kg - dry 0.225 0.856
Dimethyl phthalate 1 12/04/22 13:27 V27410JMV
<0.140 mg/Kg - dry 0.140 0.4282,4-Dimethylphenol 1 12/04/22 13:27 V27410JMV
<0.138 mg/Kg - dry 0.138 0.856Di-n-butyl phthalate 1 12/04/22 13:27 V27410JMV
<0.311 mg/Kg - dry 0.311 1.954,6-Dinitro-2-methylphenol 1 12/04/22 13:27 V27410JMV
<0.674 mg/Kg - dry 0.674 1.952,4-Dinitrophenol 1 12/04/22 13:27 V27410JMV
<0.125 mg/Kg - dry 0.125 0.8562,4-Dinitrotoluene 1 12/04/22 13:27 V27410JMV
<0.140 mg/Kg - dry 0.140 0.8562,6-Dinitrotoluene 1 12/04/22 13:27 V27410JMV
<0.185 mg/Kg - dry 0.185 0.428
Di-n-Octyl Phthalate 1 12/04/22 13:27 V27410JMV
<0.159 mg/Kg - dry 0.159 0.856Fluoranthene 1 12/04/22 13:27 V27410JMV
<0.166 mg/Kg - dry 0.166 0.856Fluorene 1 12/04/22 13:27 V27410JMV
<0.137 mg/Kg - dry 0.137 0.856Hexachlorobenzene 1 12/04/22 13:27 V27410JMV
<0.126 mg/Kg - dry 0.126 0.856Hexachlorobutadiene 1 12/04/22 13:27 V27410JMV
<0.203 mg/Kg - dry 0.203 0.856Hexachlorocyclopentadiene 1 12/04/22 13:27 V27410JMV
<0.102 mg/Kg - dry 0.102 0.856Hexachloroethane 1 12/04/22 13:27 V27410JMV
<0.232 mg/Kg - dry 0.232 0.856Indeno(1,2,3-cd)pyrene 1 12/04/22 13:27 V27410JMV
<0.247 mg/Kg - dry 0.247 0.856Isophorone 1 12/04/22 13:27 V27410JMV
<0.137 mg/Kg - dry 0.137 0.8561-Methylnaphthalene 1 12/04/22 13:27 V27410JMV
<0.129 mg/Kg - dry 0.129 0.8562-Methylnaphthalene 1 12/04/22 13:27 V27410JMV
<0.125 mg/Kg - dry 0.125 0.8562-Methylphenol 1 12/04/22 13:27 V27410JMV
<0.110 mg/Kg - dry 0.110 0.8563&4 Methylphenol 1 12/04/22 13:27 V27410JMV
<0.186 mg/Kg - dry 0.186 0.856Naphthalene 1 12/04/22 13:27 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 84 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (0-2)
94344 Matrix:
11/28/2022 14:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.125 mg/Kg - dry 0.125 0.8562-Nitroaniline 1 12/04/22 13:27 V27410JMV
<0.155 mg/Kg - dry 0.155 0.856
3-Nitroaniline 1 12/04/22 13:27 V27410JMV
<0.121 mg/Kg - dry 0.121 0.4284-Nitroaniline 1 12/04/22 13:27 V27410JMV
<0.150 mg/Kg - dry 0.150 0.428Nitrobenzene 1 12/04/22 13:27 V27410JMV
<0.115 mg/Kg - dry 0.115 0.8562-Nitrophenol 1 12/04/22 13:27 V27410JMV
<0.151 mg/Kg - dry 0.151 0.8564-Nitrophenol 1 12/04/22 13:27 V27410JMV
<0.341 mg/Kg - dry 0.341 0.856N-Nitrosodimethylamine 1 12/04/22 13:27 V27410JMV
<0.234 mg/Kg - dry 0.234 0.856N-Nitrosodiphenylamine 1 12/04/22 13:27 V27410JMV
<0.153 mg/Kg - dry 0.153 0.856
N-Nitroso-di-n-propylamine 1 12/04/22 13:27 V27410JMV
<0.450 mg/Kg - dry 0.450 1.30Pentachlorophenol 1 12/04/22 13:27 V27410JMV
<0.269 mg/Kg - dry 0.269 0.856Phenanthrene 1 12/04/22 13:27 V27410JMV
<0.145 mg/Kg - dry 0.145 0.856Phenol 1 12/04/22 13:27 V27410JMV
<0.173 mg/Kg - dry 0.173 0.856Pyrene 1 12/04/22 13:27 V27410JMV
<0.102 mg/Kg - dry 0.102 0.428Pyridine 1 12/04/22 13:27 V27410JMV
<0.138 mg/Kg - dry 0.138 0.8561,2,4-Trichlorobenzene 1 12/04/22 13:27 V27410JMV
<0.124 mg/Kg - dry 0.124 0.8562,4,5-Trichlorophenol 1 12/04/22 13:27 V27410JMV
<0.125 mg/Kg - dry 0.125 0.8562,4,6-Trichlorophenol 1 12/04/22 13:27 V27410JMV
8270ESurrogate: Phenol-d5 75.7 Limits: 34-121%12/04/22 13:271 JMV
Surrogate: 2-Fluorobiphenyl 91.6 Limits: 44-115%12/04/22 13:271 JMV V27410
Surrogate: 2-Fluorophenol 78.4 Limits: 35-115%12/04/22 13:271 JMV V27410
Surrogate: Nitrobenzene-d5 83.8 Limits: 37-122%12/04/22 13:271 JMV V27410
Surrogate: 4-Terphenyl-d14 111 Limits: 54-127%12/04/22 13:271 JMV V27410
Surrogate: 2,4,6-Tribromophenol 81.7 Limits: 39-132%12/04/22 13:271 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 85 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (2-4)
94345 Matrix:
11/28/2022 15:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
29.2 %Moisture 1 12/01/22 18:23 SW-DRYWTAMB
<0.199 mg/Kg - dry 0.199 0.282Chromium, Hexavalent 1 12/06/22 20:01 SW-7199SAR
1.05 J mg/Kg - dry 0.194 1.41Arsenic 10 12/08/22 18:32 6020BEDV
89.8 mg/Kg - dry 1.98 14.1Barium 10 12/08/22 18:32 6020BEDV
<0.0932 mg/Kg - dry 0.0932 0.706Cadmium 10 12/08/22 18:32 6020BEDV
37.9 mg/Kg - dry 0.279 1.41
Chromium 10 12/08/22 18:32 6020BEDV
14.1 mg/Kg - dry 0.206 1.41Lead 10 12/08/22 18:32 6020BEDV
0.0363 J mg/Kg - dry 0.0169 0.0424Mercury (Total)1 12/05/22 14:07 7471BEDV
<1.05 mg/Kg - dry 1.05 2.82Selenium 10 12/08/22 18:32 6020BEDV
<0.0663 mg/Kg - dry 0.0663 0.706Silver 10 12/08/22 18:32 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 86 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (2-4)
94345 Matrix:
11/28/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
0.005 J mg/Kg - dry 0.003 0.028Acetone 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.028
Acrolein 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.028Acrylonitrile 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 12/01/22 17:33 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 12/01/22 17:33 V27134TBL
<0.002 mg/Kg - dry 0.002 0.014
Bromomethane 1 12/01/22 17:33 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 12/01/22 17:33 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 12/01/22 17:33 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 12/01/22 17:33 V27134TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 12/01/22 17:33 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.007Chlorobenzene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorodibromomethane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 12/01/22 17:33 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 12/01/22 17:33 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 12/01/22 17:33 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0074-Chlorotoluene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 12/01/22 17:33 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 87 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (2-4)
94345 Matrix:
11/28/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007
1,2-Dibromoethane 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 12/01/22 17:33 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0071,2-Dichlorobenzene 1 12/01/22 17:33 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,3-Dichlorobenzene 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,4-Dichlorobenzene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.014Dichlorodifluoromethane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007
1,2-Dichloroethane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 12/01/22 17:33 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloropropene 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 12/01/22 17:33 V27134TBL
<0.019 mg/Kg - dry 0.019 0.353Ethanol 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.070Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 12/01/22 17:33 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 88 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (2-4)
94345 Matrix:
11/28/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.014n-Hexane 1 12/01/22 17:33 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.028
2-Hexanone 1 12/01/22 17:33 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.007Isopropylbenzene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 12/01/22 17:33 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.028Methyl Ethyl Ketone (MEK)1 12/01/22 17:33 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 12/01/22 17:33 V27134TBL
<0.021 mg/Kg - dry 0.021 0.0284-Methyl-2-Pentanone 1 12/01/22 17:33 V27134TBL
<0.002 mg/Kg - dry 0.002 0.014Methylene Chloride 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.014
Naphthalene 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 12/01/22 17:33 V27134TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 12/01/22 17:33 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 12/01/22 17:33 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.007Toluene 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0141,2,3-Trichlorobenzene 1 12/01/22 17:33 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2,4-Trichlorobenzene 1 12/01/22 17:33 V27134TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 12/01/22 17:33 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 12/01/22 17:33 V27134TBL
<0.002 mg/Kg - dry 0.002 0.014Trichlorofluoromethane 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 12/01/22 17:33 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 89 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (2-4)
94345 Matrix:
11/28/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 12/01/22 17:33 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007
1,3,5-Trimethylbenzene 1 12/01/22 17:33 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.014Vinyl Acetate 1 12/01/22 17:33 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 12/01/22 17:33 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 12/01/22 17:33 V27134TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 12/01/22 17:33 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 12/01/22 17:33 V27134
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%12/01/22 17:331 TBL V27134
Surrogate: Dibromofluoromethane 99.6 Limits: 84-123%12/01/22 17:331 TBL V27134
Surrogate: Toluene-d8 93.4 Limits: 76-129%12/01/22 17:331 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.163 mg/Kg - dry 0.163 0.932Acenaphthene 1 12/04/22 11:57 V27410JMV
<0.148 mg/Kg - dry 0.148 0.932Acenaphthylene 1 12/04/22 11:57 V27410JMV
<0.214 mg/Kg - dry 0.214 0.932Aniline 1 12/04/22 11:57 V27410JMV
<0.201 mg/Kg - dry 0.201 0.932Anthracene 1 12/04/22 11:57 V27410JMV
<0.196 mg/Kg - dry 0.196 0.932
Benzo(a)anthracene 1 12/04/22 11:57 V27410JMV
<0.207 mg/Kg - dry 0.207 0.932Benzo(a)pyrene 1 12/04/22 11:57 V27410JMV
<0.206 mg/Kg - dry 0.206 0.932Benzo(b)fluoranthene 1 12/04/22 11:57 V27410JMV
<0.192 mg/Kg - dry 0.192 0.932Benzo(g,h,i)perylene 1 12/04/22 11:57 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 90 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (2-4)
94345 Matrix:
11/28/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.193 mg/Kg - dry 0.193 0.932Benzo(k)fluoranthene 1 12/04/22 11:57 V27410JMV
<0.819 M
mg/Kg - dry 0.819 2.82
Benzoic Acid 1 12/04/22 11:57 V27410JMV
<0.148 mg/Kg - dry 0.148 0.932Benzyl alcohol 1 12/04/22 11:57 V27410JMV
<0.166 mg/Kg - dry 0.166 0.932Bis(2-Chloroethoxy)methane 1 12/04/22 11:57 V27410JMV
<0.151 mg/Kg - dry 0.151 0.932Bis(2-Chloroethyl)ether 1 12/04/22 11:57 V27410JMV
<0.192 mg/Kg - dry 0.192 0.466Bis(2-Chloroisopropyl)ether 1 12/04/22 11:57 V27410JMV
<0.169 mg/Kg - dry 0.169 0.932Bis(2-ethylhexyl)phthalate 1 12/04/22 11:57 V27410JMV
<0.153 mg/Kg - dry 0.153 0.9324-Bromophenyl phenyl ether 1 12/04/22 11:57 V27410JMV
<0.159 mg/Kg - dry 0.159 0.466
Butyl benzyl phthalate 1 12/04/22 11:57 V27410JMV
<0.130 mg/Kg - dry 0.130 0.9324-Chloro-3-methylphenol 1 12/04/22 11:57 V27410JMV
<0.158 mg/Kg - dry 0.158 0.4664-Chloroaniline 1 12/04/22 11:57 V27410JMV
<0.163 mg/Kg - dry 0.163 0.9322-Chloronaphthalene 1 12/04/22 11:57 V27410JMV
<0.138 mg/Kg - dry 0.138 0.9322-Chlorophenol 1 12/04/22 11:57 V27410JMV
<0.177 mg/Kg - dry 0.177 1.414-Chlorophenyl phenyl ether 1 12/04/22 11:57 V27410JMV
<0.200 mg/Kg - dry 0.200 0.932Chrysene 1 12/04/22 11:57 V27410JMV
<0.324 mg/Kg - dry 0.324 0.932Dibenz(a,h)anthracene 1 12/04/22 11:57 V27410JMV
<0.168 mg/Kg - dry 0.168 0.932Dibenzofuran 1 12/04/22 11:57 V27410JMV
<0.133 mg/Kg - dry 0.133 0.9321,2-Dichlorobenzene 1 12/04/22 11:57 V27410JMV
<0.137 mg/Kg - dry 0.137 0.9321,3-Dichlorobenzene 1 12/04/22 11:57 V27410JMV
<0.137 mg/Kg - dry 0.137 0.4661,4-Dichlorobenzene 1 12/04/22 11:57 V27410JMV
<0.207 mg/Kg - dry 0.207 0.9323,3'-Dichlorobenzidine 1 12/04/22 11:57 V27410JMV
<0.135 mg/Kg - dry 0.135 0.9322,4-Dichlorophenol 1 12/04/22 11:57 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 91 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (2-4)
94345 Matrix:
11/28/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.254 mg/Kg - dry 0.254 0.932Diethyl phthalate 1 12/04/22 11:57 V27410JMV
<0.245 mg/Kg - dry 0.245 0.932
Dimethyl phthalate 1 12/04/22 11:57 V27410JMV
<0.152 mg/Kg - dry 0.152 0.4662,4-Dimethylphenol 1 12/04/22 11:57 V27410JMV
<0.151 mg/Kg - dry 0.151 0.932Di-n-butyl phthalate 1 12/04/22 11:57 V27410JMV
<0.338 mg/Kg - dry 0.338 2.124,6-Dinitro-2-methylphenol 1 12/04/22 11:57 V27410JMV
<0.734 mg/Kg - dry 0.734 2.122,4-Dinitrophenol 1 12/04/22 11:57 V27410JMV
<0.136 mg/Kg - dry 0.136 0.9322,4-Dinitrotoluene 1 12/04/22 11:57 V27410JMV
<0.152 mg/Kg - dry 0.152 0.9322,6-Dinitrotoluene 1 12/04/22 11:57 V27410JMV
<0.201 mg/Kg - dry 0.201 0.466
Di-n-Octyl Phthalate 1 12/04/22 11:57 V27410JMV
<0.173 mg/Kg - dry 0.173 0.932Fluoranthene 1 12/04/22 11:57 V27410JMV
<0.180 mg/Kg - dry 0.180 0.932Fluorene 1 12/04/22 11:57 V27410JMV
<0.149 mg/Kg - dry 0.149 0.932Hexachlorobenzene 1 12/04/22 11:57 V27410JMV
<0.137 mg/Kg - dry 0.137 0.932Hexachlorobutadiene 1 12/04/22 11:57 V27410JMV
<0.221 mg/Kg - dry 0.221 0.932Hexachlorocyclopentadiene 1 12/04/22 11:57 V27410JMV
<0.111 mg/Kg - dry 0.111 0.932Hexachloroethane 1 12/04/22 11:57 V27410JMV
<0.252 mg/Kg - dry 0.252 0.932Indeno(1,2,3-cd)pyrene 1 12/04/22 11:57 V27410JMV
<0.269 mg/Kg - dry 0.269 0.932Isophorone 1 12/04/22 11:57 V27410JMV
<0.149 mg/Kg - dry 0.149 0.9321-Methylnaphthalene 1 12/04/22 11:57 V27410JMV
<0.141 mg/Kg - dry 0.141 0.9322-Methylnaphthalene 1 12/04/22 11:57 V27410JMV
<0.137 mg/Kg - dry 0.137 0.9322-Methylphenol 1 12/04/22 11:57 V27410JMV
<0.119 mg/Kg - dry 0.119 0.9323&4 Methylphenol 1 12/04/22 11:57 V27410JMV
<0.203 mg/Kg - dry 0.203 0.932Naphthalene 1 12/04/22 11:57 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 92 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (2-4)
94345 Matrix:
11/28/2022 15:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.136 mg/Kg - dry 0.136 0.9322-Nitroaniline 1 12/04/22 11:57 V27410JMV
<0.169 mg/Kg - dry 0.169 0.932
3-Nitroaniline 1 12/04/22 11:57 V27410JMV
<0.131 mg/Kg - dry 0.131 0.4664-Nitroaniline 1 12/04/22 11:57 V27410JMV
<0.163 mg/Kg - dry 0.163 0.466Nitrobenzene 1 12/04/22 11:57 V27410JMV
<0.125 mg/Kg - dry 0.125 0.9322-Nitrophenol 1 12/04/22 11:57 V27410JMV
<0.165 mg/Kg - dry 0.165 0.9324-Nitrophenol 1 12/04/22 11:57 V27410JMV
<0.371 mg/Kg - dry 0.371 0.932N-Nitrosodimethylamine 1 12/04/22 11:57 V27410JMV
<0.255 mg/Kg - dry 0.255 0.932N-Nitrosodiphenylamine 1 12/04/22 11:57 V27410JMV
<0.166 mg/Kg - dry 0.166 0.932
N-Nitroso-di-n-propylamine 1 12/04/22 11:57 V27410JMV
<0.490 mg/Kg - dry 0.490 1.41Pentachlorophenol 1 12/04/22 11:57 V27410JMV
<0.293 mg/Kg - dry 0.293 0.932Phenanthrene 1 12/04/22 11:57 V27410JMV
<0.158 mg/Kg - dry 0.158 0.932Phenol 1 12/04/22 11:57 V27410JMV
<0.189 mg/Kg - dry 0.189 0.932Pyrene 1 12/04/22 11:57 V27410JMV
<0.111 mg/Kg - dry 0.111 0.466Pyridine 1 12/04/22 11:57 V27410JMV
<0.151 mg/Kg - dry 0.151 0.9321,2,4-Trichlorobenzene 1 12/04/22 11:57 V27410JMV
<0.135 mg/Kg - dry 0.135 0.9322,4,5-Trichlorophenol 1 12/04/22 11:57 V27410JMV
<0.136 mg/Kg - dry 0.136 0.9322,4,6-Trichlorophenol 1 12/04/22 11:57 V27410JMV
8270ESurrogate: Phenol-d5 70.6 Limits: 34-121%12/04/22 11:571 JMV
Surrogate: 2-Fluorobiphenyl 91.0 Limits: 44-115%12/04/22 11:571 JMV V27410
Surrogate: 2-Fluorophenol 75.1 Limits: 35-115%12/04/22 11:571 JMV V27410
Surrogate: Nitrobenzene-d5 80.7 Limits: 37-122%12/04/22 11:571 JMV V27410
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%12/04/22 11:571 JMV V27410
Surrogate: 2,4,6-Tribromophenol 80.5 Limits: 39-132%12/04/22 11:571 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 93 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (4-6)
94346 Matrix:
11/28/2022 15:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.4 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
<0.184 mg/Kg - dry 0.184 0.261Chromium, Hexavalent 1 12/07/22 11:43 SW-7199SAR
2.00 mg/Kg - dry 0.179 1.31Arsenic 10 12/08/22 18:39 6020BEDV
19.1 mg/Kg - dry 1.83 13.1Barium 10 12/08/22 18:39 6020BEDV
<0.0861 mg/Kg - dry 0.0861 0.653Cadmium 10 12/08/22 18:39 6020BEDV
46.5 mg/Kg - dry 0.258 1.31
Chromium 10 12/08/22 18:39 6020BEDV
9.01 mg/Kg - dry 0.191 1.31Lead 10 12/08/22 18:39 6020BEDV
0.0504 mg/Kg - dry 0.0157 0.0392Mercury (Total)1 12/05/22 14:10 7471BEDV
1.48 J mg/Kg - dry 0.967 2.61Selenium 10 12/08/22 18:39 6020BEDV
<0.0613 mg/Kg - dry 0.0613 0.653Silver 10 12/08/22 18:39 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 94 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (4-6)
94346 Matrix:
11/28/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.003 mg/Kg - dry 0.003 0.026Acetone 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.026
Acrolein 1 12/01/22 18:00 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 12/01/22 18:00 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/01/22 18:00 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 12/01/22 18:00 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 12/01/22 18:00 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/01/22 18:00 V27134TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/01/22 18:00 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/01/22 18:00 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/01/22 18:00 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/01/22 18:00 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 12/01/22 18:00 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 95 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (4-6)
94346 Matrix:
11/28/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 12/01/22 18:00 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/01/22 18:00 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/01/22 18:00 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/01/22 18:00 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/01/22 18:00 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/01/22 18:00 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/01/22 18:00 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/01/22 18:00 V27134TBL
<0.018 mg/Kg - dry 0.018 0.326Ethanol 1 12/01/22 18:00 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 12/01/22 18:00 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 96 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (4-6)
94346 Matrix:
11/28/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 12/01/22 18:00 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.026
2-Hexanone 1 12/01/22 18:00 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/01/22 18:00 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.026Methyl Ethyl Ketone (MEK)1 12/01/22 18:00 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/01/22 18:00 V27134TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/01/22 18:00 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 18:00 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 12/01/22 18:00 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/01/22 18:00 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 18:00 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 12/01/22 18:00 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/01/22 18:00 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 97 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (4-6)
94346 Matrix:
11/28/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 12/01/22 18:00 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 12/01/22 18:00 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 12/01/22 18:00 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 12/01/22 18:00 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 12/01/22 18:00 V27134
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/01/22 18:001 TBL V27134
Surrogate: Dibromofluoromethane 101 Limits: 84-123%12/01/22 18:001 TBL V27134
Surrogate: Toluene-d8 94.7 Limits: 76-129%12/01/22 18:001 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.151 mg/Kg - dry 0.151 0.861Acenaphthene 1 12/04/22 12:20 V27410JMV
<0.137 mg/Kg - dry 0.137 0.861Acenaphthylene 1 12/04/22 12:20 V27410JMV
<0.198 mg/Kg - dry 0.198 0.861Aniline 1 12/04/22 12:20 V27410JMV
<0.186 mg/Kg - dry 0.186 0.861Anthracene 1 12/04/22 12:20 V27410JMV
<0.181 mg/Kg - dry 0.181 0.861
Benzo(a)anthracene 1 12/04/22 12:20 V27410JMV
<0.191 mg/Kg - dry 0.191 0.861Benzo(a)pyrene 1 12/04/22 12:20 V27410JMV
<0.190 mg/Kg - dry 0.190 0.861Benzo(b)fluoranthene 1 12/04/22 12:20 V27410JMV
<0.177 mg/Kg - dry 0.177 0.861Benzo(g,h,i)perylene 1 12/04/22 12:20 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 98 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (4-6)
94346 Matrix:
11/28/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.178 mg/Kg - dry 0.178 0.861Benzo(k)fluoranthene 1 12/04/22 12:20 V27410JMV
<0.757 M
mg/Kg - dry 0.757 2.61
Benzoic Acid 1 12/04/22 12:20 V27410JMV
<0.137 mg/Kg - dry 0.137 0.861Benzyl alcohol 1 12/04/22 12:20 V27410JMV
<0.154 mg/Kg - dry 0.154 0.861Bis(2-Chloroethoxy)methane 1 12/04/22 12:20 V27410JMV
<0.139 mg/Kg - dry 0.139 0.861Bis(2-Chloroethyl)ether 1 12/04/22 12:20 V27410JMV
<0.177 mg/Kg - dry 0.177 0.430Bis(2-Chloroisopropyl)ether 1 12/04/22 12:20 V27410JMV
<0.156 mg/Kg - dry 0.156 0.861Bis(2-ethylhexyl)phthalate 1 12/04/22 12:20 V27410JMV
<0.142 mg/Kg - dry 0.142 0.8614-Bromophenyl phenyl ether 1 12/04/22 12:20 V27410JMV
<0.147 mg/Kg - dry 0.147 0.430
Butyl benzyl phthalate 1 12/04/22 12:20 V27410JMV
<0.120 mg/Kg - dry 0.120 0.8614-Chloro-3-methylphenol 1 12/04/22 12:20 V27410JMV
<0.146 mg/Kg - dry 0.146 0.4304-Chloroaniline 1 12/04/22 12:20 V27410JMV
<0.151 mg/Kg - dry 0.151 0.8612-Chloronaphthalene 1 12/04/22 12:20 V27410JMV
<0.128 mg/Kg - dry 0.128 0.8612-Chlorophenol 1 12/04/22 12:20 V27410JMV
<0.164 mg/Kg - dry 0.164 1.314-Chlorophenyl phenyl ether 1 12/04/22 12:20 V27410JMV
<0.185 mg/Kg - dry 0.185 0.861Chrysene 1 12/04/22 12:20 V27410JMV
<0.300 mg/Kg - dry 0.300 0.861Dibenz(a,h)anthracene 1 12/04/22 12:20 V27410JMV
<0.155 mg/Kg - dry 0.155 0.861Dibenzofuran 1 12/04/22 12:20 V27410JMV
<0.123 mg/Kg - dry 0.123 0.8611,2-Dichlorobenzene 1 12/04/22 12:20 V27410JMV
<0.127 mg/Kg - dry 0.127 0.8611,3-Dichlorobenzene 1 12/04/22 12:20 V27410JMV
<0.127 mg/Kg - dry 0.127 0.4301,4-Dichlorobenzene 1 12/04/22 12:20 V27410JMV
<0.191 mg/Kg - dry 0.191 0.8613,3'-Dichlorobenzidine 1 12/04/22 12:20 V27410JMV
<0.125 mg/Kg - dry 0.125 0.8612,4-Dichlorophenol 1 12/04/22 12:20 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 99 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (4-6)
94346 Matrix:
11/28/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.234 mg/Kg - dry 0.234 0.861Diethyl phthalate 1 12/04/22 12:20 V27410JMV
<0.227 mg/Kg - dry 0.227 0.861
Dimethyl phthalate 1 12/04/22 12:20 V27410JMV
<0.140 mg/Kg - dry 0.140 0.4302,4-Dimethylphenol 1 12/04/22 12:20 V27410JMV
<0.139 mg/Kg - dry 0.139 0.861Di-n-butyl phthalate 1 12/04/22 12:20 V27410JMV
<0.313 mg/Kg - dry 0.313 1.964,6-Dinitro-2-methylphenol 1 12/04/22 12:20 V27410JMV
<0.678 mg/Kg - dry 0.678 1.962,4-Dinitrophenol 1 12/04/22 12:20 V27410JMV
<0.126 mg/Kg - dry 0.126 0.8612,4-Dinitrotoluene 1 12/04/22 12:20 V27410JMV
<0.140 mg/Kg - dry 0.140 0.8612,6-Dinitrotoluene 1 12/04/22 12:20 V27410JMV
<0.186 mg/Kg - dry 0.186 0.430
Di-n-Octyl Phthalate 1 12/04/22 12:20 V27410JMV
<0.160 mg/Kg - dry 0.160 0.861Fluoranthene 1 12/04/22 12:20 V27410JMV
<0.167 mg/Kg - dry 0.167 0.861Fluorene 1 12/04/22 12:20 V27410JMV
<0.138 mg/Kg - dry 0.138 0.861Hexachlorobenzene 1 12/04/22 12:20 V27410JMV
<0.127 mg/Kg - dry 0.127 0.861Hexachlorobutadiene 1 12/04/22 12:20 V27410JMV
<0.204 mg/Kg - dry 0.204 0.861Hexachlorocyclopentadiene 1 12/04/22 12:20 V27410JMV
<0.103 mg/Kg - dry 0.103 0.861Hexachloroethane 1 12/04/22 12:20 V27410JMV
<0.233 mg/Kg - dry 0.233 0.861Indeno(1,2,3-cd)pyrene 1 12/04/22 12:20 V27410JMV
<0.249 mg/Kg - dry 0.249 0.861Isophorone 1 12/04/22 12:20 V27410JMV
<0.138 mg/Kg - dry 0.138 0.8611-Methylnaphthalene 1 12/04/22 12:20 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8612-Methylnaphthalene 1 12/04/22 12:20 V27410JMV
<0.126 mg/Kg - dry 0.126 0.8612-Methylphenol 1 12/04/22 12:20 V27410JMV
<0.110 mg/Kg - dry 0.110 0.8613&4 Methylphenol 1 12/04/22 12:20 V27410JMV
<0.187 mg/Kg - dry 0.187 0.861Naphthalene 1 12/04/22 12:20 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 100 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (4-6)
94346 Matrix:
11/28/2022 15:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.126 mg/Kg - dry 0.126 0.8612-Nitroaniline 1 12/04/22 12:20 V27410JMV
<0.156 mg/Kg - dry 0.156 0.861
3-Nitroaniline 1 12/04/22 12:20 V27410JMV
<0.121 mg/Kg - dry 0.121 0.4304-Nitroaniline 1 12/04/22 12:20 V27410JMV
<0.151 mg/Kg - dry 0.151 0.430Nitrobenzene 1 12/04/22 12:20 V27410JMV
<0.115 mg/Kg - dry 0.115 0.8612-Nitrophenol 1 12/04/22 12:20 V27410JMV
<0.152 mg/Kg - dry 0.152 0.8614-Nitrophenol 1 12/04/22 12:20 V27410JMV
<0.343 mg/Kg - dry 0.343 0.861N-Nitrosodimethylamine 1 12/04/22 12:20 V27410JMV
<0.236 mg/Kg - dry 0.236 0.861N-Nitrosodiphenylamine 1 12/04/22 12:20 V27410JMV
<0.154 mg/Kg - dry 0.154 0.861
N-Nitroso-di-n-propylamine 1 12/04/22 12:20 V27410JMV
<0.453 mg/Kg - dry 0.453 1.31Pentachlorophenol 1 12/04/22 12:20 V27410JMV
<0.271 mg/Kg - dry 0.271 0.861Phenanthrene 1 12/04/22 12:20 V27410JMV
<0.146 mg/Kg - dry 0.146 0.861Phenol 1 12/04/22 12:20 V27410JMV
<0.174 mg/Kg - dry 0.174 0.861Pyrene 1 12/04/22 12:20 V27410JMV
<0.103 mg/Kg - dry 0.103 0.430Pyridine 1 12/04/22 12:20 V27410JMV
<0.139 mg/Kg - dry 0.139 0.8611,2,4-Trichlorobenzene 1 12/04/22 12:20 V27410JMV
<0.125 mg/Kg - dry 0.125 0.8612,4,5-Trichlorophenol 1 12/04/22 12:20 V27410JMV
<0.126 mg/Kg - dry 0.126 0.8612,4,6-Trichlorophenol 1 12/04/22 12:20 V27410JMV
8270ESurrogate: Phenol-d5 71.5 Limits: 34-121%12/04/22 12:201 JMV
Surrogate: 2-Fluorobiphenyl 92.2 Limits: 44-115%12/04/22 12:201 JMV V27410
Surrogate: 2-Fluorophenol 75.4 Limits: 35-115%12/04/22 12:201 JMV V27410
Surrogate: Nitrobenzene-d5 77.2 Limits: 37-122%12/04/22 12:201 JMV V27410
Surrogate: 4-Terphenyl-d14 98.8 Limits: 54-127%12/04/22 12:201 JMV V27410
Surrogate: 2,4,6-Tribromophenol 79.9 Limits: 39-132%12/04/22 12:201 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 101 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (6-8)
94347 Matrix:
11/28/2022 15:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.9 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
<0.190 mg/Kg - dry 0.190 0.269Chromium, Hexavalent 1 12/07/22 12:49 SW-7199SAR
1.97 mg/Kg - dry 0.185 1.35Arsenic 10 12/08/22 18:45 6020BEDV
41.3 mg/Kg - dry 1.89 13.5Barium 10 12/08/22 18:45 6020BEDV
<0.0890 mg/Kg - dry 0.0890 0.675Cadmium 10 12/08/22 18:45 6020BEDV
60.3 mg/Kg - dry 0.267 1.35
Chromium 10 12/08/22 18:45 6020BEDV
6.10 mg/Kg - dry 0.197 1.35Lead 10 12/08/22 18:45 6020BEDV
<0.0162 mg/Kg - dry 0.0162 0.0405Mercury (Total)1 12/02/22 14:56 7471BMMR
1.27 J mg/Kg - dry 1.00 2.70Selenium 10 12/08/22 18:45 6020BEDV
<0.0634 mg/Kg - dry 0.0634 0.675Silver 10 12/08/22 18:45 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 102 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (6-8)
94347 Matrix:
11/28/2022 15:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.003 mg/Kg - dry 0.003 0.026Acetone 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.026
Acrolein 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 12/01/22 18:28 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/01/22 18:28 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 12/01/22 18:28 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 12/01/22 18:28 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 12/01/22 18:28 V27134TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/01/22 18:28 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/01/22 18:28 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/01/22 18:28 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/01/22 18:28 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 12/01/22 18:28 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 103 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (6-8)
94347 Matrix:
11/28/2022 15:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 12/01/22 18:28 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 12/01/22 18:28 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 12/01/22 18:28 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/01/22 18:28 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/01/22 18:28 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/01/22 18:28 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/01/22 18:28 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/01/22 18:28 V27134TBL
<0.018 mg/Kg - dry 0.018 0.337Ethanol 1 12/01/22 18:28 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 12/01/22 18:28 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 104 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (6-8)
94347 Matrix:
11/28/2022 15:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 12/01/22 18:28 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.026
2-Hexanone 1 12/01/22 18:28 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/01/22 18:28 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 12/01/22 18:28 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/01/22 18:28 V27134TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/01/22 18:28 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 18:28 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 12/01/22 18:28 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/01/22 18:28 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 18:28 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 12/01/22 18:28 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 12/01/22 18:28 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 105 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (6-8)
94347 Matrix:
11/28/2022 15:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 12/01/22 18:28 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 12/01/22 18:28 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 12/01/22 18:28 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 12/01/22 18:28 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 12/01/22 18:28 V27134
Surrogate: 4-Bromofluorobenzene 96.0 Limits: 70-130%12/01/22 18:281 TBL V27134
Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/01/22 18:281 TBL V27134
Surrogate: Toluene-d8 95.1 Limits: 76-129%12/01/22 18:281 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.156 mg/Kg - dry 0.156 0.890Acenaphthene 1 12/04/22 12:42 V27410JMV
<0.141 mg/Kg - dry 0.141 0.890Acenaphthylene 1 12/04/22 12:42 V27410JMV
<0.205 mg/Kg - dry 0.205 0.890Aniline 1 12/04/22 12:42 V27410JMV
<0.192 mg/Kg - dry 0.192 0.890Anthracene 1 12/04/22 12:42 V27410JMV
<0.187 mg/Kg - dry 0.187 0.890
Benzo(a)anthracene 1 12/04/22 12:42 V27410JMV
<0.198 mg/Kg - dry 0.198 0.890Benzo(a)pyrene 1 12/04/22 12:42 V27410JMV
<0.197 mg/Kg - dry 0.197 0.890Benzo(b)fluoranthene 1 12/04/22 12:42 V27410JMV
<0.183 mg/Kg - dry 0.183 0.890Benzo(g,h,i)perylene 1 12/04/22 12:42 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 106 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (6-8)
94347 Matrix:
11/28/2022 15:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.184 mg/Kg - dry 0.184 0.890Benzo(k)fluoranthene 1 12/04/22 12:42 V27410JMV
<0.782 M
mg/Kg - dry 0.782 2.70
Benzoic Acid 1 12/04/22 12:42 V27410JMV
<0.141 mg/Kg - dry 0.141 0.890Benzyl alcohol 1 12/04/22 12:42 V27410JMV
<0.159 mg/Kg - dry 0.159 0.890Bis(2-Chloroethoxy)methane 1 12/04/22 12:42 V27410JMV
<0.144 mg/Kg - dry 0.144 0.890Bis(2-Chloroethyl)ether 1 12/04/22 12:42 V27410JMV
<0.183 mg/Kg - dry 0.183 0.445Bis(2-Chloroisopropyl)ether 1 12/04/22 12:42 V27410JMV
<0.161 mg/Kg - dry 0.161 0.890Bis(2-ethylhexyl)phthalate 1 12/04/22 12:42 V27410JMV
<0.147 mg/Kg - dry 0.147 0.8904-Bromophenyl phenyl ether 1 12/04/22 12:42 V27410JMV
<0.152 mg/Kg - dry 0.152 0.445
Butyl benzyl phthalate 1 12/04/22 12:42 V27410JMV
<0.124 mg/Kg - dry 0.124 0.8904-Chloro-3-methylphenol 1 12/04/22 12:42 V27410JMV
<0.151 mg/Kg - dry 0.151 0.4454-Chloroaniline 1 12/04/22 12:42 V27410JMV
<0.156 mg/Kg - dry 0.156 0.8902-Chloronaphthalene 1 12/04/22 12:42 V27410JMV
<0.132 mg/Kg - dry 0.132 0.8902-Chlorophenol 1 12/04/22 12:42 V27410JMV
<0.170 mg/Kg - dry 0.170 1.354-Chlorophenyl phenyl ether 1 12/04/22 12:42 V27410JMV
<0.191 mg/Kg - dry 0.191 0.890Chrysene 1 12/04/22 12:42 V27410JMV
<0.310 mg/Kg - dry 0.310 0.890Dibenz(a,h)anthracene 1 12/04/22 12:42 V27410JMV
<0.160 mg/Kg - dry 0.160 0.890Dibenzofuran 1 12/04/22 12:42 V27410JMV
<0.127 mg/Kg - dry 0.127 0.8901,2-Dichlorobenzene 1 12/04/22 12:42 V27410JMV
<0.131 mg/Kg - dry 0.131 0.8901,3-Dichlorobenzene 1 12/04/22 12:42 V27410JMV
<0.131 mg/Kg - dry 0.131 0.4451,4-Dichlorobenzene 1 12/04/22 12:42 V27410JMV
<0.198 mg/Kg - dry 0.198 0.8903,3'-Dichlorobenzidine 1 12/04/22 12:42 V27410JMV
<0.129 mg/Kg - dry 0.129 0.8902,4-Dichlorophenol 1 12/04/22 12:42 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 107 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (6-8)
94347 Matrix:
11/28/2022 15:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.242 mg/Kg - dry 0.242 0.890Diethyl phthalate 1 12/04/22 12:42 V27410JMV
<0.234 mg/Kg - dry 0.234 0.890
Dimethyl phthalate 1 12/04/22 12:42 V27410JMV
<0.145 mg/Kg - dry 0.145 0.4452,4-Dimethylphenol 1 12/04/22 12:42 V27410JMV
<0.144 mg/Kg - dry 0.144 0.890Di-n-butyl phthalate 1 12/04/22 12:42 V27410JMV
<0.323 mg/Kg - dry 0.323 2.024,6-Dinitro-2-methylphenol 1 12/04/22 12:42 V27410JMV
<0.701 mg/Kg - dry 0.701 2.022,4-Dinitrophenol 1 12/04/22 12:42 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8902,4-Dinitrotoluene 1 12/04/22 12:42 V27410JMV
<0.145 mg/Kg - dry 0.145 0.8902,6-Dinitrotoluene 1 12/04/22 12:42 V27410JMV
<0.192 mg/Kg - dry 0.192 0.445
Di-n-Octyl Phthalate 1 12/04/22 12:42 V27410JMV
<0.165 mg/Kg - dry 0.165 0.890Fluoranthene 1 12/04/22 12:42 V27410JMV
<0.172 mg/Kg - dry 0.172 0.890Fluorene 1 12/04/22 12:42 V27410JMV
<0.143 mg/Kg - dry 0.143 0.890Hexachlorobenzene 1 12/04/22 12:42 V27410JMV
<0.131 mg/Kg - dry 0.131 0.890Hexachlorobutadiene 1 12/04/22 12:42 V27410JMV
<0.211 mg/Kg - dry 0.211 0.890Hexachlorocyclopentadiene 1 12/04/22 12:42 V27410JMV
<0.106 mg/Kg - dry 0.106 0.890Hexachloroethane 1 12/04/22 12:42 V27410JMV
<0.241 mg/Kg - dry 0.241 0.890Indeno(1,2,3-cd)pyrene 1 12/04/22 12:42 V27410JMV
<0.257 mg/Kg - dry 0.257 0.890Isophorone 1 12/04/22 12:42 V27410JMV
<0.143 mg/Kg - dry 0.143 0.8901-Methylnaphthalene 1 12/04/22 12:42 V27410JMV
<0.134 mg/Kg - dry 0.134 0.8902-Methylnaphthalene 1 12/04/22 12:42 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8902-Methylphenol 1 12/04/22 12:42 V27410JMV
<0.114 mg/Kg - dry 0.114 0.8903&4 Methylphenol 1 12/04/22 12:42 V27410JMV
<0.194 mg/Kg - dry 0.194 0.890Naphthalene 1 12/04/22 12:42 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 108 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5 (6-8)
94347 Matrix:
11/28/2022 15:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.130 mg/Kg - dry 0.130 0.8902-Nitroaniline 1 12/04/22 12:42 V27410JMV
<0.161 mg/Kg - dry 0.161 0.890
3-Nitroaniline 1 12/04/22 12:42 V27410JMV
<0.125 mg/Kg - dry 0.125 0.4454-Nitroaniline 1 12/04/22 12:42 V27410JMV
<0.156 mg/Kg - dry 0.156 0.445Nitrobenzene 1 12/04/22 12:42 V27410JMV
<0.119 mg/Kg - dry 0.119 0.8902-Nitrophenol 1 12/04/22 12:42 V27410JMV
<0.157 mg/Kg - dry 0.157 0.8904-Nitrophenol 1 12/04/22 12:42 V27410JMV
<0.354 mg/Kg - dry 0.354 0.890N-Nitrosodimethylamine 1 12/04/22 12:42 V27410JMV
<0.244 mg/Kg - dry 0.244 0.890N-Nitrosodiphenylamine 1 12/04/22 12:42 V27410JMV
<0.159 mg/Kg - dry 0.159 0.890
N-Nitroso-di-n-propylamine 1 12/04/22 12:42 V27410JMV
<0.468 mg/Kg - dry 0.468 1.35Pentachlorophenol 1 12/04/22 12:42 V27410JMV
<0.280 mg/Kg - dry 0.280 0.890Phenanthrene 1 12/04/22 12:42 V27410JMV
<0.151 mg/Kg - dry 0.151 0.890Phenol 1 12/04/22 12:42 V27410JMV
<0.180 mg/Kg - dry 0.180 0.890Pyrene 1 12/04/22 12:42 V27410JMV
<0.106 mg/Kg - dry 0.106 0.445Pyridine 1 12/04/22 12:42 V27410JMV
<0.144 mg/Kg - dry 0.144 0.8901,2,4-Trichlorobenzene 1 12/04/22 12:42 V27410JMV
<0.129 mg/Kg - dry 0.129 0.8902,4,5-Trichlorophenol 1 12/04/22 12:42 V27410JMV
<0.130 mg/Kg - dry 0.130 0.8902,4,6-Trichlorophenol 1 12/04/22 12:42 V27410JMV
8270ESurrogate: Phenol-d5 74.6 Limits: 34-121%12/04/22 12:421 JMV
Surrogate: 2-Fluorobiphenyl 95.8 Limits: 44-115%12/04/22 12:421 JMV V27410
Surrogate: 2-Fluorophenol 78.7 Limits: 35-115%12/04/22 12:421 JMV V27410
Surrogate: Nitrobenzene-d5 80.8 Limits: 37-122%12/04/22 12:421 JMV V27410
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%12/04/22 12:421 JMV V27410
Surrogate: 2,4,6-Tribromophenol 83.5 Limits: 39-132%12/04/22 12:421 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 109 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5A (0-2)
94348 Matrix:
11/29/2022 9:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
29.0 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 110 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5A (0-2)
94348 Matrix:
11/29/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
0.008 J mg/Kg - dry 0.003 0.028Acetone 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.028
Acrolein 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.028Acrylonitrile 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 12/01/22 18:55 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 12/01/22 18:55 V27134TBL
<0.002 mg/Kg - dry 0.002 0.014
Bromomethane 1 12/01/22 18:55 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 12/01/22 18:55 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 12/01/22 18:55 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 12/01/22 18:55 V27134TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 12/01/22 18:55 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.007Chlorobenzene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Chlorodibromomethane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 12/01/22 18:55 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 12/01/22 18:55 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 12/01/22 18:55 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0074-Chlorotoluene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 12/01/22 18:55 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 111 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5A (0-2)
94348 Matrix:
11/29/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007
1,2-Dibromoethane 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 12/01/22 18:55 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0071,2-Dichlorobenzene 1 12/01/22 18:55 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,3-Dichlorobenzene 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,4-Dichlorobenzene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.014Dichlorodifluoromethane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007
1,2-Dichloroethane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 12/01/22 18:55 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloropropene 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 12/01/22 18:55 V27134TBL
<0.019 mg/Kg - dry 0.019 0.352Ethanol 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.070Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 12/01/22 18:55 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 112 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5A (0-2)
94348 Matrix:
11/29/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.014n-Hexane 1 12/01/22 18:55 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.028
2-Hexanone 1 12/01/22 18:55 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.007Isopropylbenzene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 12/01/22 18:55 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.028Methyl Ethyl Ketone (MEK)1 12/01/22 18:55 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 12/01/22 18:55 V27134TBL
<0.021 mg/Kg - dry 0.021 0.0284-Methyl-2-Pentanone 1 12/01/22 18:55 V27134TBL
<0.002 mg/Kg - dry 0.002 0.014Methylene Chloride 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.014
Naphthalene 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 12/01/22 18:55 V27134TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 12/01/22 18:55 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 12/01/22 18:55 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.007Toluene 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0141,2,3-Trichlorobenzene 1 12/01/22 18:55 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2,4-Trichlorobenzene 1 12/01/22 18:55 V27134TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 12/01/22 18:55 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 12/01/22 18:55 V27134TBL
<0.002 mg/Kg - dry 0.002 0.014Trichlorofluoromethane 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 12/01/22 18:55 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 113 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5A (0-2)
94348 Matrix:
11/29/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 12/01/22 18:55 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.007
1,3,5-Trimethylbenzene 1 12/01/22 18:55 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.014Vinyl Acetate 1 12/01/22 18:55 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 12/01/22 18:55 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 12/01/22 18:55 V27134TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 12/01/22 18:55 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 12/01/22 18:55 V27134
Surrogate: 4-Bromofluorobenzene 98.5 Limits: 70-130%12/01/22 18:551 TBL V27134
Surrogate: Dibromofluoromethane 104 Limits: 84-123%12/01/22 18:551 TBL V27134
Surrogate: Toluene-d8 93.0 Limits: 76-129%12/01/22 18:551 TBL V27134
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 114 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5A (6-8)
94349 Matrix:
11/29/2022 9:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.4 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 115 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5A (6-8)
94349 Matrix:
11/29/2022 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.002 mg/Kg - dry 0.002 0.024Acetone 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 12/01/22 19:22 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/01/22 19:22 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/01/22 19:22 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/01/22 19:22 V27134TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/01/22 19:22 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/01/22 19:22 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/01/22 19:22 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 12/01/22 19:22 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/01/22 19:22 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/01/22 19:22 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 12/01/22 19:22 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/01/22 19:22 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/01/22 19:22 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 116 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5A (6-8)
94349 Matrix:
11/29/2022 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/01/22 19:22 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/01/22 19:22 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/01/22 19:22 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/01/22 19:22 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/01/22 19:22 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/01/22 19:22 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/01/22 19:22 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 12/01/22 19:22 V27134TBL
<0.017 mg/Kg - dry 0.017 0.306Ethanol 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 19:22 V27134TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 12/01/22 19:22 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 117 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5A (6-8)
94349 Matrix:
11/29/2022 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 12/01/22 19:22 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 12/01/22 19:22 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/01/22 19:22 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 12/01/22 19:22 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/01/22 19:22 V27134TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/01/22 19:22 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 19:22 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 12/01/22 19:22 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/01/22 19:22 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 19:22 V27134TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/01/22 19:22 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/01/22 19:22 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 118 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-5A (6-8)
94349 Matrix:
11/29/2022 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/01/22 19:22 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 12/01/22 19:22 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/01/22 19:22 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/01/22 19:22 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/01/22 19:22 V27134TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/01/22 19:22 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/01/22 19:22 V27134
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%12/01/22 19:221 TBL V27134
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/01/22 19:221 TBL V27134
Surrogate: Toluene-d8 95.0 Limits: 76-129%12/01/22 19:221 TBL V27134
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 119 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-Dup
94350 Matrix:
11/28/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.1 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
<0.198 mg/Kg - dry 0.198 0.282Chromium, Hexavalent 1 12/07/22 12:59 SW-7199SAR
0.967 J mg/Kg - dry 0.191 1.39Arsenic 10 12/08/22 18:51 6020BEDV
19.7 mg/Kg - dry 1.95 13.9Barium 10 12/08/22 18:51 6020BEDV
<0.0917 mg/Kg - dry 0.0917 0.695Cadmium 10 12/08/22 18:51 6020BEDV
97.5 mg/Kg - dry 0.275 1.39
Chromium 10 12/08/22 18:51 6020BEDV
8.55 mg/Kg - dry 0.203 1.39Lead 10 12/08/22 18:51 6020BEDV
<0.0167 mg/Kg - dry 0.0167 0.0417Mercury (Total)1 12/02/22 14:59 7471BMMR
<1.03 mg/Kg - dry 1.03 2.78Selenium 10 12/08/22 18:51 6020BEDV
<0.0653 mg/Kg - dry 0.0653 0.695Silver 10 12/08/22 18:51 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 120 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-Dup
94350 Matrix:
11/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.003 mg/Kg - dry 0.003 0.027Acetone 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.027
Acrolein 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/01/22 19:50 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/01/22 19:50 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 12/01/22 19:50 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 12/01/22 19:50 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 12/01/22 19:50 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 12/01/22 19:50 V27134TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/01/22 19:50 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/01/22 19:50 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 12/01/22 19:50 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/01/22 19:50 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 12/01/22 19:50 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 121 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-Dup
94350 Matrix:
11/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 12/01/22 19:50 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/01/22 19:50 V27134TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/01/22 19:50 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006cis-1,3-Dichloropropene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/01/22 19:50 V27134TBL
<0.019 mg/Kg - dry 0.019 0.347Ethanol 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 12/01/22 19:50 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 122 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-Dup
94350 Matrix:
11/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 12/01/22 19:50 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.027
2-Hexanone 1 12/01/22 19:50 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/01/22 19:50 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 12/01/22 19:50 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 12/01/22 19:50 V27134TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 12/01/22 19:50 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006n-Propylbenzene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/01/22 19:50 V27134TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 19:50 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,3-Trichlorobenzene 1 12/01/22 19:50 V27134TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 12/01/22 19:50 V27134TBL
<0.002 mg/Kg - dry 0.002 0.0061,1,1-Trichloroethane 1 12/01/22 19:50 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 19:50 V27134TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.0061,2,3-Trichloropropane 1 12/01/22 19:50 V27134TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 123 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-Dup
94350 Matrix:
11/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 12/01/22 19:50 V27134TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,3,5-Trimethylbenzene 1 12/01/22 19:50 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 12/01/22 19:50 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 12/01/22 19:50 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 12/01/22 19:50 V27134TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 12/01/22 19:50 V27134TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 12/01/22 19:50 V27134
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%12/01/22 19:501 TBL V27134
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/01/22 19:501 TBL V27134
Surrogate: Toluene-d8 94.5 Limits: 76-129%12/01/22 19:501 TBL V27134
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.161 mg/Kg - dry 0.161 0.917Acenaphthene 1 12/04/22 13:05 V27410JMV
<0.146 mg/Kg - dry 0.146 0.917Acenaphthylene 1 12/04/22 13:05 V27410JMV
<0.211 mg/Kg - dry 0.211 0.917Aniline 1 12/04/22 13:05 V27410JMV
<0.198 mg/Kg - dry 0.198 0.917Anthracene 1 12/04/22 13:05 V27410JMV
<0.193 mg/Kg - dry 0.193 0.917
Benzo(a)anthracene 1 12/04/22 13:05 V27410JMV
<0.204 mg/Kg - dry 0.204 0.917Benzo(a)pyrene 1 12/04/22 13:05 V27410JMV
<0.203 mg/Kg - dry 0.203 0.917Benzo(b)fluoranthene 1 12/04/22 13:05 V27410JMV
<0.189 mg/Kg - dry 0.189 0.917Benzo(g,h,i)perylene 1 12/04/22 13:05 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 124 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-Dup
94350 Matrix:
11/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.190 mg/Kg - dry 0.190 0.917Benzo(k)fluoranthene 1 12/04/22 13:05 V27410JMV
<0.806 M
mg/Kg - dry 0.806 2.78
Benzoic Acid 1 12/04/22 13:05 V27410JMV
<0.146 mg/Kg - dry 0.146 0.917Benzyl alcohol 1 12/04/22 13:05 V27410JMV
<0.164 mg/Kg - dry 0.164 0.917Bis(2-Chloroethoxy)methane 1 12/04/22 13:05 V27410JMV
<0.148 mg/Kg - dry 0.148 0.917Bis(2-Chloroethyl)ether 1 12/04/22 13:05 V27410JMV
<0.189 mg/Kg - dry 0.189 0.458Bis(2-Chloroisopropyl)ether 1 12/04/22 13:05 V27410JMV
<0.166 mg/Kg - dry 0.166 0.917Bis(2-ethylhexyl)phthalate 1 12/04/22 13:05 V27410JMV
<0.151 mg/Kg - dry 0.151 0.9174-Bromophenyl phenyl ether 1 12/04/22 13:05 V27410JMV
<0.157 mg/Kg - dry 0.157 0.458
Butyl benzyl phthalate 1 12/04/22 13:05 V27410JMV
<0.128 mg/Kg - dry 0.128 0.9174-Chloro-3-methylphenol 1 12/04/22 13:05 V27410JMV
<0.155 mg/Kg - dry 0.155 0.4584-Chloroaniline 1 12/04/22 13:05 V27410JMV
<0.161 mg/Kg - dry 0.161 0.9172-Chloronaphthalene 1 12/04/22 13:05 V27410JMV
<0.136 mg/Kg - dry 0.136 0.9172-Chlorophenol 1 12/04/22 13:05 V27410JMV
<0.175 mg/Kg - dry 0.175 1.394-Chlorophenyl phenyl ether 1 12/04/22 13:05 V27410JMV
<0.197 mg/Kg - dry 0.197 0.917Chrysene 1 12/04/22 13:05 V27410JMV
<0.319 mg/Kg - dry 0.319 0.917Dibenz(a,h)anthracene 1 12/04/22 13:05 V27410JMV
<0.165 mg/Kg - dry 0.165 0.917Dibenzofuran 1 12/04/22 13:05 V27410JMV
<0.131 mg/Kg - dry 0.131 0.9171,2-Dichlorobenzene 1 12/04/22 13:05 V27410JMV
<0.135 mg/Kg - dry 0.135 0.9171,3-Dichlorobenzene 1 12/04/22 13:05 V27410JMV
<0.135 mg/Kg - dry 0.135 0.4581,4-Dichlorobenzene 1 12/04/22 13:05 V27410JMV
<0.204 mg/Kg - dry 0.204 0.9173,3'-Dichlorobenzidine 1 12/04/22 13:05 V27410JMV
<0.133 mg/Kg - dry 0.133 0.9172,4-Dichlorophenol 1 12/04/22 13:05 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 125 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-Dup
94350 Matrix:
11/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.250 mg/Kg - dry 0.250 0.917Diethyl phthalate 1 12/04/22 13:05 V27410JMV
<0.242 mg/Kg - dry 0.242 0.917
Dimethyl phthalate 1 12/04/22 13:05 V27410JMV
<0.150 mg/Kg - dry 0.150 0.4582,4-Dimethylphenol 1 12/04/22 13:05 V27410JMV
<0.148 mg/Kg - dry 0.148 0.917Di-n-butyl phthalate 1 12/04/22 13:05 V27410JMV
<0.333 mg/Kg - dry 0.333 2.094,6-Dinitro-2-methylphenol 1 12/04/22 13:05 V27410JMV
<0.723 mg/Kg - dry 0.723 2.092,4-Dinitrophenol 1 12/04/22 13:05 V27410JMV
<0.134 mg/Kg - dry 0.134 0.9172,4-Dinitrotoluene 1 12/04/22 13:05 V27410JMV
<0.150 mg/Kg - dry 0.150 0.9172,6-Dinitrotoluene 1 12/04/22 13:05 V27410JMV
<0.198 mg/Kg - dry 0.198 0.458
Di-n-Octyl Phthalate 1 12/04/22 13:05 V27410JMV
<0.171 mg/Kg - dry 0.171 0.917Fluoranthene 1 12/04/22 13:05 V27410JMV
<0.178 mg/Kg - dry 0.178 0.917Fluorene 1 12/04/22 13:05 V27410JMV
<0.147 mg/Kg - dry 0.147 0.917Hexachlorobenzene 1 12/04/22 13:05 V27410JMV
<0.135 mg/Kg - dry 0.135 0.917Hexachlorobutadiene 1 12/04/22 13:05 V27410JMV
<0.218 mg/Kg - dry 0.218 0.917Hexachlorocyclopentadiene 1 12/04/22 13:05 V27410JMV
<0.110 mg/Kg - dry 0.110 0.917Hexachloroethane 1 12/04/22 13:05 V27410JMV
<0.248 mg/Kg - dry 0.248 0.917Indeno(1,2,3-cd)pyrene 1 12/04/22 13:05 V27410JMV
<0.265 mg/Kg - dry 0.265 0.917Isophorone 1 12/04/22 13:05 V27410JMV
<0.147 mg/Kg - dry 0.147 0.9171-Methylnaphthalene 1 12/04/22 13:05 V27410JMV
<0.139 mg/Kg - dry 0.139 0.9172-Methylnaphthalene 1 12/04/22 13:05 V27410JMV
<0.134 mg/Kg - dry 0.134 0.9172-Methylphenol 1 12/04/22 13:05 V27410JMV
<0.118 mg/Kg - dry 0.118 0.9173&4 Methylphenol 1 12/04/22 13:05 V27410JMV
<0.200 mg/Kg - dry 0.200 0.917Naphthalene 1 12/04/22 13:05 V27410JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 126 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-Dup
94350 Matrix:
11/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27192 12/02/22 10:40
<0.134 mg/Kg - dry 0.134 0.9172-Nitroaniline 1 12/04/22 13:05 V27410JMV
<0.166 mg/Kg - dry 0.166 0.917
3-Nitroaniline 1 12/04/22 13:05 V27410JMV
<0.129 mg/Kg - dry 0.129 0.4584-Nitroaniline 1 12/04/22 13:05 V27410JMV
<0.161 mg/Kg - dry 0.161 0.458Nitrobenzene 1 12/04/22 13:05 V27410JMV
<0.123 mg/Kg - dry 0.123 0.9172-Nitrophenol 1 12/04/22 13:05 V27410JMV
<0.162 mg/Kg - dry 0.162 0.9174-Nitrophenol 1 12/04/22 13:05 V27410JMV
<0.365 mg/Kg - dry 0.365 0.917N-Nitrosodimethylamine 1 12/04/22 13:05 V27410JMV
<0.251 mg/Kg - dry 0.251 0.917N-Nitrosodiphenylamine 1 12/04/22 13:05 V27410JMV
<0.164 mg/Kg - dry 0.164 0.917
N-Nitroso-di-n-propylamine 1 12/04/22 13:05 V27410JMV
<0.482 mg/Kg - dry 0.482 1.39Pentachlorophenol 1 12/04/22 13:05 V27410JMV
<0.289 mg/Kg - dry 0.289 0.917Phenanthrene 1 12/04/22 13:05 V27410JMV
<0.155 mg/Kg - dry 0.155 0.917Phenol 1 12/04/22 13:05 V27410JMV
<0.186 mg/Kg - dry 0.186 0.917Pyrene 1 12/04/22 13:05 V27410JMV
<0.110 mg/Kg - dry 0.110 0.458Pyridine 1 12/04/22 13:05 V27410JMV
<0.148 mg/Kg - dry 0.148 0.9171,2,4-Trichlorobenzene 1 12/04/22 13:05 V27410JMV
<0.133 mg/Kg - dry 0.133 0.9172,4,5-Trichlorophenol 1 12/04/22 13:05 V27410JMV
<0.134 mg/Kg - dry 0.134 0.9172,4,6-Trichlorophenol 1 12/04/22 13:05 V27410JMV
8270ESurrogate: Phenol-d5 74.2 Limits: 34-121%12/04/22 13:051 JMV
Surrogate: 2-Fluorobiphenyl 95.2 Limits: 44-115%12/04/22 13:051 JMV V27410
Surrogate: 2-Fluorophenol 78.7 Limits: 35-115%12/04/22 13:051 JMV V27410
Surrogate: Nitrobenzene-d5 81.4 Limits: 37-122%12/04/22 13:051 JMV V27410
Surrogate: 4-Terphenyl-d14 100 Limits: 54-127%12/04/22 13:051 JMV V27410
Surrogate: 2,4,6-Tribromophenol 81.1 Limits: 39-132%12/04/22 13:051 JMV V27410
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 127 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-01 (0-2)
94351 Matrix:
11/28/2022 12:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.1 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 128 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-01 (0-2)
94351 Matrix:
11/28/2022 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/01/22 20:17 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,2-Dichloroethene 1 12/01/22 20:17 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 20:17 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 20:17 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 12/01/22 20:17 V27134TBL
Surrogate: 4-Bromofluorobenzene 96.5 Limits: 70-130%12/01/22 20:171 TBL V27134
Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/01/22 20:171 TBL V27134
Surrogate: Toluene-d8 93.2 Limits: 76-129%12/01/22 20:171 TBL V27134
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 129 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-01 (4-6)
94352 Matrix:
11/28/2022 12:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.6 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 130 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-01 (4-6)
94352 Matrix:
11/28/2022 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/01/22 20:45 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,2-Dichloroethene 1 12/01/22 20:45 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 20:45 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 20:45 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 12/01/22 20:45 V27134TBL
Surrogate: 4-Bromofluorobenzene 98.9 Limits: 70-130%12/01/22 20:451 TBL V27134
Surrogate: Dibromofluoromethane 100 Limits: 84-123%12/01/22 20:451 TBL V27134
Surrogate: Toluene-d8 94.3 Limits: 76-129%12/01/22 20:451 TBL V27134
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 131 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-02 (2-4)
94353 Matrix:
11/28/2022 12:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.8 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 132 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-02 (2-4)
94353 Matrix:
11/28/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/01/22 21:12 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,2-Dichloroethene 1 12/01/22 21:12 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 21:12 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 21:12 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/01/22 21:12 V27134TBL
Surrogate: 4-Bromofluorobenzene 99.0 Limits: 70-130%12/01/22 21:121 TBL V27134
Surrogate: Dibromofluoromethane 99.7 Limits: 84-123%12/01/22 21:121 TBL V27134
Surrogate: Toluene-d8 93.8 Limits: 76-129%12/01/22 21:121 TBL V27134
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 133 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-02 (4-6)
94354 Matrix:
11/28/2022 12:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.1 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 134 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-02 (4-6)
94354 Matrix:
11/28/2022 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/01/22 21:39 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,2-Dichloroethene 1 12/01/22 21:39 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 21:39 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 21:39 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/01/22 21:39 V27134TBL
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/01/22 21:391 TBL V27134
Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/01/22 21:391 TBL V27134
Surrogate: Toluene-d8 95.1 Limits: 76-129%12/01/22 21:391 TBL V27134
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 135 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-03 (2-4)
94355 Matrix:
11/28/2022 11:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.0 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 136 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-03 (2-4)
94355 Matrix:
11/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27133 12/01/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/01/22 22:07 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,2-Dichloroethene 1 12/01/22 22:07 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 22:07 V27134TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 22:07 V27134TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/01/22 22:07 V27134TBL
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%12/01/22 22:071 TBL V27134
Surrogate: Dibromofluoromethane 101 Limits: 84-123%12/01/22 22:071 TBL V27134
Surrogate: Toluene-d8 93.2 Limits: 76-129%12/01/22 22:071 TBL V27134
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 137 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-03 (4-6)
94356 Matrix:
11/28/2022 11:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.1 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 138 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-03 (4-6)
94356 Matrix:
11/28/2022 11:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27135 12/01/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/01/22 22:34 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,2-Dichloroethene 1 12/01/22 22:34 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 22:34 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 22:34 V27136TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/01/22 22:34 V27136TBL
Surrogate: 4-Bromofluorobenzene 96.5 Limits: 70-130%12/01/22 22:341 TBL V27136
Surrogate: Dibromofluoromethane 100 Limits: 84-123%12/01/22 22:341 TBL V27136
Surrogate: Toluene-d8 94.6 Limits: 76-129%12/01/22 22:341 TBL V27136
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 139 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-04 (0-2)
94357 Matrix:
11/28/2022 11:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.2 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 140 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-04 (0-2)
94357 Matrix:
11/28/2022 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27135 12/01/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/01/22 23:02 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,2-Dichloroethene 1 12/01/22 23:02 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 23:02 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 23:02 V27136TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/01/22 23:02 V27136TBL
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/01/22 23:021 TBL V27136
Surrogate: Dibromofluoromethane 101 Limits: 84-123%12/01/22 23:021 TBL V27136
Surrogate: Toluene-d8 94.0 Limits: 76-129%12/01/22 23:021 TBL V27136
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 141 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-04 (6-8)
94358 Matrix:
11/28/2022 12:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
29.0 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 142 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-04 (6-8)
94358 Matrix:
11/28/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27135 12/01/22 08:00
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 12/01/22 23:29 V27136TBL
<0.001 mg/Kg - dry 0.001 0.007
trans-1,2-Dichloroethene 1 12/01/22 23:29 V27136TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 12/01/22 23:29 V27136TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 12/01/22 23:29 V27136TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 12/01/22 23:29 V27136TBL
Surrogate: 4-Bromofluorobenzene 99.7 Limits: 70-130%12/01/22 23:291 TBL V27136
Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/01/22 23:291 TBL V27136
Surrogate: Toluene-d8 93.3 Limits: 76-129%12/01/22 23:291 TBL V27136
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 143 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-05 (2-4)
94359 Matrix:
11/28/2022 10:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.6 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 144 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-05 (2-4)
94359 Matrix:
11/28/2022 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27135 12/01/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/01/22 23:57 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,2-Dichloroethene 1 12/01/22 23:57 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/01/22 23:57 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/01/22 23:57 V27136TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/01/22 23:57 V27136TBL
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%12/01/22 23:571 TBL V27136
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/01/22 23:571 TBL V27136
Surrogate: Toluene-d8 94.7 Limits: 76-129%12/01/22 23:571 TBL V27136
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 145 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-05 (4-6)
94360 Matrix:
11/28/2022 10:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.5 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 146 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-05 (4-6)
94360 Matrix:
11/28/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27135 12/01/22 08:00
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/02/22 00:24 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,2-Dichloroethene 1 12/02/22 00:24 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/02/22 00:24 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/02/22 00:24 V27136TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 12/02/22 00:24 V27136TBL
Surrogate: 4-Bromofluorobenzene 98.9 Limits: 70-130%12/02/22 00:241 TBL V27136
Surrogate: Dibromofluoromethane 102 Limits: 84-123%12/02/22 00:241 TBL V27136
Surrogate: Toluene-d8 93.6 Limits: 76-129%12/02/22 00:241 TBL V27136
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 147 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-DUP
94361 Matrix:
11/28/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.5 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 148 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:BF-SB-DUP
94361 Matrix:
11/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27135 12/01/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 12/02/22 00:51 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006
trans-1,2-Dichloroethene 1 12/02/22 00:51 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/02/22 00:51 V27136TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/02/22 00:51 V27136TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/02/22 00:51 V27136TBL
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/02/22 00:511 TBL V27136
Surrogate: Dibromofluoromethane 105 Limits: 84-123%12/02/22 00:511 TBL V27136
Surrogate: Toluene-d8 93.4 Limits: 76-129%12/02/22 00:511 TBL V27136
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 149 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2A
94362 Matrix:
11/29/2022 12:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
10.9 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
20.1 mg/Kg - dry 0.0347 0.281Lead 5 12/13/22 21:33 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 150 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2A
94362 Matrix:
11/29/2022 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.130 mg/Kg - dry 0.130 0.741Acenaphthene 1 12/06/22 22:05 V27495JMV
<0.117 mg/Kg - dry 0.117 0.741
Acenaphthylene 1 12/06/22 22:05 V27495JMV
<0.170 mg/Kg - dry 0.170 0.741Aniline 1 12/06/22 22:05 V27495JMV
<0.160 mg/Kg - dry 0.160 0.741Anthracene 1 12/06/22 22:05 V27495JMV
<0.156 mg/Kg - dry 0.156 0.741Benzo(a)anthracene 1 12/06/22 22:05 V27495JMV
<0.164 mg/Kg - dry 0.164 0.741Benzo(a)pyrene 1 12/06/22 22:05 V27495JMV
0.168 J mg/Kg - dry 0.163 0.741Benzo(b)fluoranthene 1 12/06/22 22:05 V27495JMV
<0.152 mg/Kg - dry 0.152 0.741Benzo(g,h,i)perylene 1 12/06/22 22:05 V27495JMV
<0.153 mg/Kg - dry 0.153 0.741
Benzo(k)fluoranthene 1 12/06/22 22:05 V27495JMV
<0.650 M mg/Kg - dry 0.650 2.24Benzoic Acid 1 12/06/22 22:05 V27495JMV
<0.117 mg/Kg - dry 0.117 0.741Benzyl alcohol 1 12/06/22 22:05 V27495JMV
<0.132 mg/Kg - dry 0.132 0.741Bis(2-Chloroethoxy)methane 1 12/06/22 22:05 V27495JMV
<0.120 mg/Kg - dry 0.120 0.741Bis(2-Chloroethyl)ether 1 12/06/22 22:05 V27495JMV
<0.152 mg/Kg - dry 0.152 0.370Bis(2-Chloroisopropyl)ether 1 12/06/22 22:05 V27495JMV
<0.134 mg/Kg - dry 0.134 0.741Bis(2-ethylhexyl)phthalate 1 12/06/22 22:05 V27495JMV
<0.122 mg/Kg - dry 0.122 0.7414-Bromophenyl phenyl ether 1 12/06/22 22:05 V27495JMV
<0.126 mg/Kg - dry 0.126 0.370Butyl benzyl phthalate 1 12/06/22 22:05 V27495JMV
<0.103 mg/Kg - dry 0.103 0.7414-Chloro-3-methylphenol 1 12/06/22 22:05 V27495JMV
<0.125 mg/Kg - dry 0.125 0.3704-Chloroaniline 1 12/06/22 22:05 V27495JMV
<0.130 mg/Kg - dry 0.130 0.7412-Chloronaphthalene 1 12/06/22 22:05 V27495JMV
<0.110 mg/Kg - dry 0.110 0.7412-Chlorophenol 1 12/06/22 22:05 V27495JMV
<0.141 mg/Kg - dry 0.141 1.124-Chlorophenyl phenyl ether 1 12/06/22 22:05 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 151 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2A
94362 Matrix:
11/29/2022 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.159 mg/Kg - dry 0.159 0.741Chrysene 1 12/06/22 22:05 V27495JMV
<0.258 mg/Kg - dry 0.258 0.741
Dibenz(a,h)anthracene 1 12/06/22 22:05 V27495JMV
<0.133 mg/Kg - dry 0.133 0.741Dibenzofuran 1 12/06/22 22:05 V27495JMV
<0.106 mg/Kg - dry 0.106 0.7411,2-Dichlorobenzene 1 12/06/22 22:05 V27495JMV
<0.109 mg/Kg - dry 0.109 0.7411,3-Dichlorobenzene 1 12/06/22 22:05 V27495JMV
<0.109 mg/Kg - dry 0.109 0.3701,4-Dichlorobenzene 1 12/06/22 22:05 V27495JMV
<0.164 mg/Kg - dry 0.164 0.7413,3'-Dichlorobenzidine 1 12/06/22 22:05 V27495JMV
<0.107 mg/Kg - dry 0.107 0.7412,4-Dichlorophenol 1 12/06/22 22:05 V27495JMV
<0.202 mg/Kg - dry 0.202 0.741
Diethyl phthalate 1 12/06/22 22:05 V27495JMV
<0.195 mg/Kg - dry 0.195 0.741Dimethyl phthalate 1 12/06/22 22:05 V27495JMV
<0.121 mg/Kg - dry 0.121 0.3702,4-Dimethylphenol 1 12/06/22 22:05 V27495JMV
<0.120 mg/Kg - dry 0.120 0.741Di-n-butyl phthalate 1 12/06/22 22:05 V27495JMV
<0.269 mg/Kg - dry 0.269 1.684,6-Dinitro-2-methylphenol 1 12/06/22 22:05 V27495JMV
<0.583 mg/Kg - dry 0.583 1.682,4-Dinitrophenol 1 12/06/22 22:05 V27495JMV
<0.108 mg/Kg - dry 0.108 0.7412,4-Dinitrotoluene 1 12/06/22 22:05 V27495JMV
<0.121 mg/Kg - dry 0.121 0.7412,6-Dinitrotoluene 1 12/06/22 22:05 V27495JMV
<0.160 mg/Kg - dry 0.160 0.370Di-n-Octyl Phthalate 1 12/06/22 22:05 V27495JMV
<0.138 mg/Kg - dry 0.138 0.741Fluoranthene 1 12/06/22 22:05 V27495JMV
<0.143 mg/Kg - dry 0.143 0.741Fluorene 1 12/06/22 22:05 V27495JMV
<0.118 mg/Kg - dry 0.118 0.741Hexachlorobenzene 1 12/06/22 22:05 V27495JMV
<0.109 mg/Kg - dry 0.109 0.741Hexachlorobutadiene 1 12/06/22 22:05 V27495JMV
<0.176 mg/Kg - dry 0.176 0.741Hexachlorocyclopentadiene 1 12/06/22 22:05 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 152 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2A
94362 Matrix:
11/29/2022 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.089 mg/Kg - dry 0.089 0.741Hexachloroethane 1 12/06/22 22:05 V27495JMV
<0.200 mg/Kg - dry 0.200 0.741
Indeno(1,2,3-cd)pyrene 1 12/06/22 22:05 V27495JMV
<0.214 mg/Kg - dry 0.214 0.741Isophorone 1 12/06/22 22:05 V27495JMV
<0.118 mg/Kg - dry 0.118 0.7411-Methylnaphthalene 1 12/06/22 22:05 V27495JMV
<0.112 mg/Kg - dry 0.112 0.7412-Methylnaphthalene 1 12/06/22 22:05 V27495JMV
<0.108 mg/Kg - dry 0.108 0.7412-Methylphenol 1 12/06/22 22:05 V27495JMV
<0.095 mg/Kg - dry 0.095 0.7413&4 Methylphenol 1 12/06/22 22:05 V27495JMV
<0.161 mg/Kg - dry 0.161 0.741Naphthalene 1 12/06/22 22:05 V27495JMV
<0.108 mg/Kg - dry 0.108 0.741
2-Nitroaniline 1 12/06/22 22:05 V27495JMV
<0.134 mg/Kg - dry 0.134 0.7413-Nitroaniline 1 12/06/22 22:05 V27495JMV
<0.104 mg/Kg - dry 0.104 0.3704-Nitroaniline 1 12/06/22 22:05 V27495JMV
<0.130 mg/Kg - dry 0.130 0.370Nitrobenzene 1 12/06/22 22:05 V27495JMV
<0.099 mg/Kg - dry 0.099 0.7412-Nitrophenol 1 12/06/22 22:05 V27495JMV
<0.131 mg/Kg - dry 0.131 0.7414-Nitrophenol 1 12/06/22 22:05 V27495JMV
<0.295 mg/Kg - dry 0.295 0.741N-Nitrosodimethylamine 1 12/06/22 22:05 V27495JMV
<0.203 mg/Kg - dry 0.203 0.741N-Nitrosodiphenylamine 1 12/06/22 22:05 V27495JMV
<0.132 mg/Kg - dry 0.132 0.741N-Nitroso-di-n-propylamine 1 12/06/22 22:05 V27495JMV
<0.389 mg/Kg - dry 0.389 1.12Pentachlorophenol 1 12/06/22 22:05 V27495JMV
<0.233 mg/Kg - dry 0.233 0.741Phenanthrene 1 12/06/22 22:05 V27495JMV
<0.125 mg/Kg - dry 0.125 0.741Phenol 1 12/06/22 22:05 V27495JMV
<0.150 mg/Kg - dry 0.150 0.741Pyrene 1 12/06/22 22:05 V27495JMV
<0.088 mg/Kg - dry 0.088 0.370Pyridine 1 12/06/22 22:05 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 153 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2A
94362 Matrix:
11/29/2022 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.120 mg/Kg - dry 0.120 0.7411,2,4-Trichlorobenzene 1 12/06/22 22:05 V27495JMV
<0.108 mg/Kg - dry 0.108 0.741
2,4,5-Trichlorophenol 1 12/06/22 22:05 V27495JMV
<0.108 mg/Kg - dry 0.108 0.7412,4,6-Trichlorophenol 1 12/06/22 22:05 V27495JMV
8270ESurrogate: Phenol-d5 76.0 Limits: 34-121%12/06/22 22:051 JMV
Surrogate: 2-Fluorobiphenyl 101 Limits: 44-115%12/06/22 22:051 JMV V27495
Surrogate: 2-Fluorophenol 81.1 Limits: 35-115%12/06/22 22:051 JMV V27495
Surrogate: Nitrobenzene-d5 89.2 Limits: 37-122%12/06/22 22:051 JMV V27495
Surrogate: 4-Terphenyl-d14 103 Limits: 54-127%12/06/22 22:051 JMV V27495
Surrogate: 2,4,6-Tribromophenol 85.9 Limits: 39-132%12/06/22 22:051 JMV V27495
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 154 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2B
94363 Matrix:
11/29/2022 12:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.87 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
490 mg/Kg - dry 1.38 11.1Lead 200 12/13/22 21:39 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 155 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2B
94363 Matrix:
11/29/2022 12:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.128 mg/Kg - dry 0.128 0.732Acenaphthene 1 12/06/22 22:28 V27495JMV
<0.116 mg/Kg - dry 0.116 0.732
Acenaphthylene 1 12/06/22 22:28 V27495JMV
<0.168 mg/Kg - dry 0.168 0.732Aniline 1 12/06/22 22:28 V27495JMV
<0.158 mg/Kg - dry 0.158 0.732Anthracene 1 12/06/22 22:28 V27495JMV
0.359 J mg/Kg - dry 0.154 0.732Benzo(a)anthracene 1 12/06/22 22:28 V27495JMV
0.523 J mg/Kg - dry 0.163 0.732Benzo(a)pyrene 1 12/06/22 22:28 V27495JMV
0.685 J mg/Kg - dry 0.161 0.732Benzo(b)fluoranthene 1 12/06/22 22:28 V27495JMV
0.356 J mg/Kg - dry 0.150 0.732Benzo(g,h,i)perylene 1 12/06/22 22:28 V27495JMV
0.183 J
mg/Kg - dry 0.152 0.732
Benzo(k)fluoranthene 1 12/06/22 22:28 V27495JMV
<0.643 M mg/Kg - dry 0.643 2.22Benzoic Acid 1 12/06/22 22:28 V27495JMV
<0.116 mg/Kg - dry 0.116 0.732Benzyl alcohol 1 12/06/22 22:28 V27495JMV
<0.130 mg/Kg - dry 0.130 0.732Bis(2-Chloroethoxy)methane 1 12/06/22 22:28 V27495JMV
<0.118 mg/Kg - dry 0.118 0.732Bis(2-Chloroethyl)ether 1 12/06/22 22:28 V27495JMV
<0.150 mg/Kg - dry 0.150 0.366Bis(2-Chloroisopropyl)ether 1 12/06/22 22:28 V27495JMV
<0.133 mg/Kg - dry 0.133 0.732Bis(2-ethylhexyl)phthalate 1 12/06/22 22:28 V27495JMV
<0.120 mg/Kg - dry 0.120 0.7324-Bromophenyl phenyl ether 1 12/06/22 22:28 V27495JMV
<0.125 mg/Kg - dry 0.125 0.366Butyl benzyl phthalate 1 12/06/22 22:28 V27495JMV
<0.102 mg/Kg - dry 0.102 0.7324-Chloro-3-methylphenol 1 12/06/22 22:28 V27495JMV
<0.124 mg/Kg - dry 0.124 0.3664-Chloroaniline 1 12/06/22 22:28 V27495JMV
<0.128 mg/Kg - dry 0.128 0.7322-Chloronaphthalene 1 12/06/22 22:28 V27495JMV
<0.108 mg/Kg - dry 0.108 0.7322-Chlorophenol 1 12/06/22 22:28 V27495JMV
<0.139 mg/Kg - dry 0.139 1.114-Chlorophenyl phenyl ether 1 12/06/22 22:28 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 156 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2B
94363 Matrix:
11/29/2022 12:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
0.353 J mg/Kg - dry 0.157 0.732Chrysene 1 12/06/22 22:28 V27495JMV
<0.255 mg/Kg - dry 0.255 0.732
Dibenz(a,h)anthracene 1 12/06/22 22:28 V27495JMV
<0.132 mg/Kg - dry 0.132 0.732Dibenzofuran 1 12/06/22 22:28 V27495JMV
<0.104 mg/Kg - dry 0.104 0.7321,2-Dichlorobenzene 1 12/06/22 22:28 V27495JMV
<0.107 mg/Kg - dry 0.107 0.7321,3-Dichlorobenzene 1 12/06/22 22:28 V27495JMV
<0.108 mg/Kg - dry 0.108 0.3661,4-Dichlorobenzene 1 12/06/22 22:28 V27495JMV
<0.163 mg/Kg - dry 0.163 0.7323,3'-Dichlorobenzidine 1 12/06/22 22:28 V27495JMV
<0.106 mg/Kg - dry 0.106 0.7322,4-Dichlorophenol 1 12/06/22 22:28 V27495JMV
<0.199 mg/Kg - dry 0.199 0.732
Diethyl phthalate 1 12/06/22 22:28 V27495JMV
<0.193 mg/Kg - dry 0.193 0.732Dimethyl phthalate 1 12/06/22 22:28 V27495JMV
<0.119 mg/Kg - dry 0.119 0.3662,4-Dimethylphenol 1 12/06/22 22:28 V27495JMV
<0.118 mg/Kg - dry 0.118 0.732Di-n-butyl phthalate 1 12/06/22 22:28 V27495JMV
<0.266 mg/Kg - dry 0.266 1.664,6-Dinitro-2-methylphenol 1 12/06/22 22:28 V27495JMV
<0.576 mg/Kg - dry 0.576 1.662,4-Dinitrophenol 1 12/06/22 22:28 V27495JMV
<0.107 mg/Kg - dry 0.107 0.7322,4-Dinitrotoluene 1 12/06/22 22:28 V27495JMV
<0.119 mg/Kg - dry 0.119 0.7322,6-Dinitrotoluene 1 12/06/22 22:28 V27495JMV
<0.158 mg/Kg - dry 0.158 0.366Di-n-Octyl Phthalate 1 12/06/22 22:28 V27495JMV
0.469 J mg/Kg - dry 0.136 0.732Fluoranthene 1 12/06/22 22:28 V27495JMV
<0.142 mg/Kg - dry 0.142 0.732Fluorene 1 12/06/22 22:28 V27495JMV
<0.117 mg/Kg - dry 0.117 0.732Hexachlorobenzene 1 12/06/22 22:28 V27495JMV
<0.108 mg/Kg - dry 0.108 0.732Hexachlorobutadiene 1 12/06/22 22:28 V27495JMV
<0.174 mg/Kg - dry 0.174 0.732Hexachlorocyclopentadiene 1 12/06/22 22:28 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 157 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2B
94363 Matrix:
11/29/2022 12:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.087 mg/Kg - dry 0.087 0.732Hexachloroethane 1 12/06/22 22:28 V27495JMV
0.372 J
mg/Kg - dry 0.198 0.732
Indeno(1,2,3-cd)pyrene 1 12/06/22 22:28 V27495JMV
<0.211 mg/Kg - dry 0.211 0.732Isophorone 1 12/06/22 22:28 V27495JMV
<0.117 mg/Kg - dry 0.117 0.7321-Methylnaphthalene 1 12/06/22 22:28 V27495JMV
<0.110 mg/Kg - dry 0.110 0.7322-Methylnaphthalene 1 12/06/22 22:28 V27495JMV
<0.107 mg/Kg - dry 0.107 0.7322-Methylphenol 1 12/06/22 22:28 V27495JMV
<0.094 mg/Kg - dry 0.094 0.7323&4 Methylphenol 1 12/06/22 22:28 V27495JMV
<0.159 mg/Kg - dry 0.159 0.732Naphthalene 1 12/06/22 22:28 V27495JMV
<0.107 mg/Kg - dry 0.107 0.732
2-Nitroaniline 1 12/06/22 22:28 V27495JMV
<0.133 mg/Kg - dry 0.133 0.7323-Nitroaniline 1 12/06/22 22:28 V27495JMV
<0.103 mg/Kg - dry 0.103 0.3664-Nitroaniline 1 12/06/22 22:28 V27495JMV
<0.128 mg/Kg - dry 0.128 0.366Nitrobenzene 1 12/06/22 22:28 V27495JMV
<0.098 mg/Kg - dry 0.098 0.7322-Nitrophenol 1 12/06/22 22:28 V27495JMV
<0.129 mg/Kg - dry 0.129 0.7324-Nitrophenol 1 12/06/22 22:28 V27495JMV
<0.291 mg/Kg - dry 0.291 0.732N-Nitrosodimethylamine 1 12/06/22 22:28 V27495JMV
<0.200 mg/Kg - dry 0.200 0.732N-Nitrosodiphenylamine 1 12/06/22 22:28 V27495JMV
<0.130 mg/Kg - dry 0.130 0.732N-Nitroso-di-n-propylamine 1 12/06/22 22:28 V27495JMV
<0.384 mg/Kg - dry 0.384 1.11Pentachlorophenol 1 12/06/22 22:28 V27495JMV
<0.230 mg/Kg - dry 0.230 0.732Phenanthrene 1 12/06/22 22:28 V27495JMV
<0.124 mg/Kg - dry 0.124 0.732Phenol 1 12/06/22 22:28 V27495JMV
0.482 J mg/Kg - dry 0.148 0.732Pyrene 1 12/06/22 22:28 V27495JMV
<0.087 mg/Kg - dry 0.087 0.366Pyridine 1 12/06/22 22:28 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 158 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2B
94363 Matrix:
11/29/2022 12:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.118 mg/Kg - dry 0.118 0.7321,2,4-Trichlorobenzene 1 12/06/22 22:28 V27495JMV
<0.106 mg/Kg - dry 0.106 0.732
2,4,5-Trichlorophenol 1 12/06/22 22:28 V27495JMV
<0.107 mg/Kg - dry 0.107 0.7322,4,6-Trichlorophenol 1 12/06/22 22:28 V27495JMV
8270ESurrogate: Phenol-d5 67.0 Limits: 34-121%12/06/22 22:281 JMV
Surrogate: 2-Fluorobiphenyl 86.2 Limits: 44-115%12/06/22 22:281 JMV V27495
Surrogate: 2-Fluorophenol 48.9 Limits: 35-115%12/06/22 22:281 JMV V27495
Surrogate: Nitrobenzene-d5 72.5 Limits: 37-122%12/06/22 22:281 JMV V27495
Surrogate: 4-Terphenyl-d14 102 Limits: 54-127%12/06/22 22:281 JMV V27495
Surrogate: 2,4,6-Tribromophenol 56.5 Limits: 39-132%12/06/22 22:281 JMV V27495
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 159 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2C
94364 Matrix:
11/29/2022 11:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.1 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
125 mg/Kg - dry 0.150 1.21Lead 20 12/13/22 21:43 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 160 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2C
94364 Matrix:
11/29/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.139 mg/Kg - dry 0.139 0.797Acenaphthene 1 12/06/22 22:50 V27495JMV
<0.126 mg/Kg - dry 0.126 0.797
Acenaphthylene 1 12/06/22 22:50 V27495JMV
<0.183 mg/Kg - dry 0.183 0.797Aniline 1 12/06/22 22:50 V27495JMV
<0.172 mg/Kg - dry 0.172 0.797Anthracene 1 12/06/22 22:50 V27495JMV
<0.167 mg/Kg - dry 0.167 0.797Benzo(a)anthracene 1 12/06/22 22:50 V27495JMV
<0.177 mg/Kg - dry 0.177 0.797Benzo(a)pyrene 1 12/06/22 22:50 V27495JMV
<0.176 mg/Kg - dry 0.176 0.797Benzo(b)fluoranthene 1 12/06/22 22:50 V27495JMV
<0.164 mg/Kg - dry 0.164 0.797Benzo(g,h,i)perylene 1 12/06/22 22:50 V27495JMV
<0.165 mg/Kg - dry 0.165 0.797
Benzo(k)fluoranthene 1 12/06/22 22:50 V27495JMV
<0.699 M mg/Kg - dry 0.699 2.41Benzoic Acid 1 12/06/22 22:50 V27495JMV
<0.126 mg/Kg - dry 0.126 0.797Benzyl alcohol 1 12/06/22 22:50 V27495JMV
<0.142 mg/Kg - dry 0.142 0.797Bis(2-Chloroethoxy)methane 1 12/06/22 22:50 V27495JMV
<0.129 mg/Kg - dry 0.129 0.797Bis(2-Chloroethyl)ether 1 12/06/22 22:50 V27495JMV
<0.164 mg/Kg - dry 0.164 0.398Bis(2-Chloroisopropyl)ether 1 12/06/22 22:50 V27495JMV
<0.144 mg/Kg - dry 0.144 0.797Bis(2-ethylhexyl)phthalate 1 12/06/22 22:50 V27495JMV
<0.131 mg/Kg - dry 0.131 0.7974-Bromophenyl phenyl ether 1 12/06/22 22:50 V27495JMV
<0.136 mg/Kg - dry 0.136 0.398Butyl benzyl phthalate 1 12/06/22 22:50 V27495JMV
<0.111 mg/Kg - dry 0.111 0.7974-Chloro-3-methylphenol 1 12/06/22 22:50 V27495JMV
<0.135 mg/Kg - dry 0.135 0.3984-Chloroaniline 1 12/06/22 22:50 V27495JMV
<0.139 mg/Kg - dry 0.139 0.7972-Chloronaphthalene 1 12/06/22 22:50 V27495JMV
<0.118 mg/Kg - dry 0.118 0.7972-Chlorophenol 1 12/06/22 22:50 V27495JMV
<0.151 mg/Kg - dry 0.151 1.214-Chlorophenyl phenyl ether 1 12/06/22 22:50 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 161 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2C
94364 Matrix:
11/29/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.171 mg/Kg - dry 0.171 0.797Chrysene 1 12/06/22 22:50 V27495JMV
<0.277 mg/Kg - dry 0.277 0.797
Dibenz(a,h)anthracene 1 12/06/22 22:50 V27495JMV
<0.143 mg/Kg - dry 0.143 0.797Dibenzofuran 1 12/06/22 22:50 V27495JMV
<0.113 mg/Kg - dry 0.113 0.7971,2-Dichlorobenzene 1 12/06/22 22:50 V27495JMV
<0.117 mg/Kg - dry 0.117 0.7971,3-Dichlorobenzene 1 12/06/22 22:50 V27495JMV
<0.117 mg/Kg - dry 0.117 0.3981,4-Dichlorobenzene 1 12/06/22 22:50 V27495JMV
<0.177 mg/Kg - dry 0.177 0.7973,3'-Dichlorobenzidine 1 12/06/22 22:50 V27495JMV
<0.115 mg/Kg - dry 0.115 0.7972,4-Dichlorophenol 1 12/06/22 22:50 V27495JMV
<0.217 mg/Kg - dry 0.217 0.797
Diethyl phthalate 1 12/06/22 22:50 V27495JMV
<0.209 mg/Kg - dry 0.209 0.797Dimethyl phthalate 1 12/06/22 22:50 V27495JMV
<0.130 mg/Kg - dry 0.130 0.3982,4-Dimethylphenol 1 12/06/22 22:50 V27495JMV
<0.129 mg/Kg - dry 0.129 0.797Di-n-butyl phthalate 1 12/06/22 22:50 V27495JMV
<0.289 mg/Kg - dry 0.289 1.814,6-Dinitro-2-methylphenol 1 12/06/22 22:50 V27495JMV
<0.627 mg/Kg - dry 0.627 1.812,4-Dinitrophenol 1 12/06/22 22:50 V27495JMV
<0.116 mg/Kg - dry 0.116 0.7972,4-Dinitrotoluene 1 12/06/22 22:50 V27495JMV
<0.130 mg/Kg - dry 0.130 0.7972,6-Dinitrotoluene 1 12/06/22 22:50 V27495JMV
<0.172 mg/Kg - dry 0.172 0.398Di-n-Octyl Phthalate 1 12/06/22 22:50 V27495JMV
<0.148 mg/Kg - dry 0.148 0.797Fluoranthene 1 12/06/22 22:50 V27495JMV
<0.154 mg/Kg - dry 0.154 0.797Fluorene 1 12/06/22 22:50 V27495JMV
<0.127 mg/Kg - dry 0.127 0.797Hexachlorobenzene 1 12/06/22 22:50 V27495JMV
<0.117 mg/Kg - dry 0.117 0.797Hexachlorobutadiene 1 12/06/22 22:50 V27495JMV
<0.189 mg/Kg - dry 0.189 0.797Hexachlorocyclopentadiene 1 12/06/22 22:50 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 162 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2C
94364 Matrix:
11/29/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.095 mg/Kg - dry 0.095 0.797Hexachloroethane 1 12/06/22 22:50 V27495JMV
<0.215 mg/Kg - dry 0.215 0.797
Indeno(1,2,3-cd)pyrene 1 12/06/22 22:50 V27495JMV
<0.230 mg/Kg - dry 0.230 0.797Isophorone 1 12/06/22 22:50 V27495JMV
<0.127 mg/Kg - dry 0.127 0.7971-Methylnaphthalene 1 12/06/22 22:50 V27495JMV
<0.120 mg/Kg - dry 0.120 0.7972-Methylnaphthalene 1 12/06/22 22:50 V27495JMV
<0.117 mg/Kg - dry 0.117 0.7972-Methylphenol 1 12/06/22 22:50 V27495JMV
<0.102 mg/Kg - dry 0.102 0.7973&4 Methylphenol 1 12/06/22 22:50 V27495JMV
<0.173 mg/Kg - dry 0.173 0.797Naphthalene 1 12/06/22 22:50 V27495JMV
<0.116 mg/Kg - dry 0.116 0.797
2-Nitroaniline 1 12/06/22 22:50 V27495JMV
<0.144 mg/Kg - dry 0.144 0.7973-Nitroaniline 1 12/06/22 22:50 V27495JMV
<0.112 mg/Kg - dry 0.112 0.3984-Nitroaniline 1 12/06/22 22:50 V27495JMV
<0.139 mg/Kg - dry 0.139 0.398Nitrobenzene 1 12/06/22 22:50 V27495JMV
<0.107 mg/Kg - dry 0.107 0.7972-Nitrophenol 1 12/06/22 22:50 V27495JMV
<0.141 mg/Kg - dry 0.141 0.7974-Nitrophenol 1 12/06/22 22:50 V27495JMV
<0.317 mg/Kg - dry 0.317 0.797N-Nitrosodimethylamine 1 12/06/22 22:50 V27495JMV
<0.218 mg/Kg - dry 0.218 0.797N-Nitrosodiphenylamine 1 12/06/22 22:50 V27495JMV
<0.142 mg/Kg - dry 0.142 0.797N-Nitroso-di-n-propylamine 1 12/06/22 22:50 V27495JMV
<0.418 mg/Kg - dry 0.418 1.21Pentachlorophenol 1 12/06/22 22:50 V27495JMV
<0.250 mg/Kg - dry 0.250 0.797Phenanthrene 1 12/06/22 22:50 V27495JMV
<0.135 mg/Kg - dry 0.135 0.797Phenol 1 12/06/22 22:50 V27495JMV
<0.161 mg/Kg - dry 0.161 0.797Pyrene 1 12/06/22 22:50 V27495JMV
<0.095 mg/Kg - dry 0.095 0.398Pyridine 1 12/06/22 22:50 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 163 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2C
94364 Matrix:
11/29/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.129 mg/Kg - dry 0.129 0.7971,2,4-Trichlorobenzene 1 12/06/22 22:50 V27495JMV
<0.116 mg/Kg - dry 0.116 0.797
2,4,5-Trichlorophenol 1 12/06/22 22:50 V27495JMV
<0.116 mg/Kg - dry 0.116 0.7972,4,6-Trichlorophenol 1 12/06/22 22:50 V27495JMV
8270ESurrogate: Phenol-d5 71.9 Limits: 34-121%12/06/22 22:501 JMV
Surrogate: 2-Fluorobiphenyl 91.6 Limits: 44-115%12/06/22 22:501 JMV V27495
Surrogate: 2-Fluorophenol 78.7 Limits: 35-115%12/06/22 22:501 JMV V27495
Surrogate: Nitrobenzene-d5 82.0 Limits: 37-122%12/06/22 22:501 JMV V27495
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%12/06/22 22:501 JMV V27495
Surrogate: 2,4,6-Tribromophenol 81.7 Limits: 39-132%12/06/22 22:501 JMV V27495
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 164 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2D
94365 Matrix:
11/29/2022 11:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.5 %Moisture 1 12/02/22 12:17 SW-DRYWTAMB
35.1 mg/Kg - dry 0.0389 0.314Lead 5 12/08/22 19:00 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 165 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2D
94365 Matrix:
11/29/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.145 mg/Kg - dry 0.145 0.830Acenaphthene 1 12/06/22 23:12 V27495JMV
<0.132 mg/Kg - dry 0.132 0.830
Acenaphthylene 1 12/06/22 23:12 V27495JMV
<0.191 mg/Kg - dry 0.191 0.830Aniline 1 12/06/22 23:12 V27495JMV
<0.179 mg/Kg - dry 0.179 0.830Anthracene 1 12/06/22 23:12 V27495JMV
<0.174 mg/Kg - dry 0.174 0.830Benzo(a)anthracene 1 12/06/22 23:12 V27495JMV
<0.184 mg/Kg - dry 0.184 0.830Benzo(a)pyrene 1 12/06/22 23:12 V27495JMV
<0.183 mg/Kg - dry 0.183 0.830Benzo(b)fluoranthene 1 12/06/22 23:12 V27495JMV
<0.171 mg/Kg - dry 0.171 0.830Benzo(g,h,i)perylene 1 12/06/22 23:12 V27495JMV
<0.172 mg/Kg - dry 0.172 0.830
Benzo(k)fluoranthene 1 12/06/22 23:12 V27495JMV
<0.729 M mg/Kg - dry 0.729 2.52Benzoic Acid 1 12/06/22 23:12 V27495JMV
<0.132 mg/Kg - dry 0.132 0.830Benzyl alcohol 1 12/06/22 23:12 V27495JMV
<0.148 mg/Kg - dry 0.148 0.830Bis(2-Chloroethoxy)methane 1 12/06/22 23:12 V27495JMV
<0.134 mg/Kg - dry 0.134 0.830Bis(2-Chloroethyl)ether 1 12/06/22 23:12 V27495JMV
<0.171 mg/Kg - dry 0.171 0.415Bis(2-Chloroisopropyl)ether 1 12/06/22 23:12 V27495JMV
<0.150 mg/Kg - dry 0.150 0.830Bis(2-ethylhexyl)phthalate 1 12/06/22 23:12 V27495JMV
<0.137 mg/Kg - dry 0.137 0.8304-Bromophenyl phenyl ether 1 12/06/22 23:12 V27495JMV
<0.142 mg/Kg - dry 0.142 0.415Butyl benzyl phthalate 1 12/06/22 23:12 V27495JMV
<0.116 mg/Kg - dry 0.116 0.8304-Chloro-3-methylphenol 1 12/06/22 23:12 V27495JMV
<0.140 mg/Kg - dry 0.140 0.4154-Chloroaniline 1 12/06/22 23:12 V27495JMV
<0.145 mg/Kg - dry 0.145 0.8302-Chloronaphthalene 1 12/06/22 23:12 V27495JMV
<0.123 mg/Kg - dry 0.123 0.8302-Chlorophenol 1 12/06/22 23:12 V27495JMV
<0.158 mg/Kg - dry 0.158 1.264-Chlorophenyl phenyl ether 1 12/06/22 23:12 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 166 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2D
94365 Matrix:
11/29/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.178 mg/Kg - dry 0.178 0.830Chrysene 1 12/06/22 23:12 V27495JMV
<0.289 mg/Kg - dry 0.289 0.830
Dibenz(a,h)anthracene 1 12/06/22 23:12 V27495JMV
<0.149 mg/Kg - dry 0.149 0.830Dibenzofuran 1 12/06/22 23:12 V27495JMV
<0.118 mg/Kg - dry 0.118 0.8301,2-Dichlorobenzene 1 12/06/22 23:12 V27495JMV
<0.122 mg/Kg - dry 0.122 0.8301,3-Dichlorobenzene 1 12/06/22 23:12 V27495JMV
<0.122 mg/Kg - dry 0.122 0.4151,4-Dichlorobenzene 1 12/06/22 23:12 V27495JMV
<0.184 mg/Kg - dry 0.184 0.8303,3'-Dichlorobenzidine 1 12/06/22 23:12 V27495JMV
<0.120 mg/Kg - dry 0.120 0.8302,4-Dichlorophenol 1 12/06/22 23:12 V27495JMV
<0.226 mg/Kg - dry 0.226 0.830
Diethyl phthalate 1 12/06/22 23:12 V27495JMV
<0.218 mg/Kg - dry 0.218 0.830Dimethyl phthalate 1 12/06/22 23:12 V27495JMV
<0.135 mg/Kg - dry 0.135 0.4152,4-Dimethylphenol 1 12/06/22 23:12 V27495JMV
<0.134 mg/Kg - dry 0.134 0.830Di-n-butyl phthalate 1 12/06/22 23:12 V27495JMV
<0.301 mg/Kg - dry 0.301 1.894,6-Dinitro-2-methylphenol 1 12/06/22 23:12 V27495JMV
<0.654 mg/Kg - dry 0.654 1.892,4-Dinitrophenol 1 12/06/22 23:12 V27495JMV
<0.121 mg/Kg - dry 0.121 0.8302,4-Dinitrotoluene 1 12/06/22 23:12 V27495JMV
<0.135 mg/Kg - dry 0.135 0.8302,6-Dinitrotoluene 1 12/06/22 23:12 V27495JMV
<0.179 mg/Kg - dry 0.179 0.415Di-n-Octyl Phthalate 1 12/06/22 23:12 V27495JMV
<0.154 mg/Kg - dry 0.154 0.830Fluoranthene 1 12/06/22 23:12 V27495JMV
<0.161 mg/Kg - dry 0.161 0.830Fluorene 1 12/06/22 23:12 V27495JMV
<0.133 mg/Kg - dry 0.133 0.830Hexachlorobenzene 1 12/06/22 23:12 V27495JMV
<0.122 mg/Kg - dry 0.122 0.830Hexachlorobutadiene 1 12/06/22 23:12 V27495JMV
<0.197 mg/Kg - dry 0.197 0.830Hexachlorocyclopentadiene 1 12/06/22 23:12 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 167 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2D
94365 Matrix:
11/29/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.099 mg/Kg - dry 0.099 0.830Hexachloroethane 1 12/06/22 23:12 V27495JMV
<0.225 mg/Kg - dry 0.225 0.830
Indeno(1,2,3-cd)pyrene 1 12/06/22 23:12 V27495JMV
<0.240 mg/Kg - dry 0.240 0.830Isophorone 1 12/06/22 23:12 V27495JMV
<0.133 mg/Kg - dry 0.133 0.8301-Methylnaphthalene 1 12/06/22 23:12 V27495JMV
<0.125 mg/Kg - dry 0.125 0.8302-Methylnaphthalene 1 12/06/22 23:12 V27495JMV
<0.122 mg/Kg - dry 0.122 0.8302-Methylphenol 1 12/06/22 23:12 V27495JMV
<0.106 mg/Kg - dry 0.106 0.8303&4 Methylphenol 1 12/06/22 23:12 V27495JMV
<0.181 mg/Kg - dry 0.181 0.830Naphthalene 1 12/06/22 23:12 V27495JMV
<0.121 mg/Kg - dry 0.121 0.830
2-Nitroaniline 1 12/06/22 23:12 V27495JMV
<0.150 mg/Kg - dry 0.150 0.8303-Nitroaniline 1 12/06/22 23:12 V27495JMV
<0.117 mg/Kg - dry 0.117 0.4154-Nitroaniline 1 12/06/22 23:12 V27495JMV
<0.145 mg/Kg - dry 0.145 0.415Nitrobenzene 1 12/06/22 23:12 V27495JMV
<0.111 mg/Kg - dry 0.111 0.8302-Nitrophenol 1 12/06/22 23:12 V27495JMV
<0.147 mg/Kg - dry 0.147 0.8304-Nitrophenol 1 12/06/22 23:12 V27495JMV
<0.330 mg/Kg - dry 0.330 0.830N-Nitrosodimethylamine 1 12/06/22 23:12 V27495JMV
<0.227 mg/Kg - dry 0.227 0.830N-Nitrosodiphenylamine 1 12/06/22 23:12 V27495JMV
<0.148 mg/Kg - dry 0.148 0.830N-Nitroso-di-n-propylamine 1 12/06/22 23:12 V27495JMV
<0.436 mg/Kg - dry 0.436 1.26Pentachlorophenol 1 12/06/22 23:12 V27495JMV
<0.261 mg/Kg - dry 0.261 0.830Phenanthrene 1 12/06/22 23:12 V27495JMV
<0.140 mg/Kg - dry 0.140 0.830Phenol 1 12/06/22 23:12 V27495JMV
<0.168 mg/Kg - dry 0.168 0.830Pyrene 1 12/06/22 23:12 V27495JMV
<0.099 mg/Kg - dry 0.099 0.415Pyridine 1 12/06/22 23:12 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 168 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2D
94365 Matrix:
11/29/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.134 mg/Kg - dry 0.134 0.8301,2,4-Trichlorobenzene 1 12/06/22 23:12 V27495JMV
<0.121 mg/Kg - dry 0.121 0.830
2,4,5-Trichlorophenol 1 12/06/22 23:12 V27495JMV
<0.121 mg/Kg - dry 0.121 0.8302,4,6-Trichlorophenol 1 12/06/22 23:12 V27495JMV
8270ESurrogate: Phenol-d5 73.3 Limits: 34-121%12/06/22 23:121 JMV
Surrogate: 2-Fluorobiphenyl 95.8 Limits: 44-115%12/06/22 23:121 JMV V27495
Surrogate: 2-Fluorophenol 73.9 Limits: 35-115%12/06/22 23:121 JMV V27495
Surrogate: Nitrobenzene-d5 80.8 Limits: 37-122%12/06/22 23:121 JMV V27495
Surrogate: 4-Terphenyl-d14 108 Limits: 54-127%12/06/22 23:121 JMV V27495
Surrogate: 2,4,6-Tribromophenol 89.8 Limits: 39-132%12/06/22 23:121 JMV V27495
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 169 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2E
94366 Matrix:
11/29/2022 12:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.15 %Moisture 1 12/02/22 12:44 SW-DRYWTAMB
37.5 mg/Kg - dry 0.0341 0.275Lead 5 12/08/22 19:07 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 170 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2E
94366 Matrix:
11/29/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.127 mg/Kg - dry 0.127 0.726Acenaphthene 1 12/06/22 23:35 V27495JMV
0.301 J
mg/Kg - dry 0.115 0.726
Acenaphthylene 1 12/06/22 23:35 V27495JMV
<0.167 mg/Kg - dry 0.167 0.726Aniline 1 12/06/22 23:35 V27495JMV
1.68 mg/Kg - dry 0.157 0.726Anthracene 1 12/06/22 23:35 V27495JMV
6.44 mg/Kg - dry 0.152 0.726Benzo(a)anthracene 1 12/06/22 23:35 V27495JMV
6.32 mg/Kg - dry 0.161 0.726Benzo(a)pyrene 1 12/06/22 23:35 V27495JMV
8.65 mg/Kg - dry 0.642 2.91Benzo(b)fluoranthene 4 12/09/22 01:07 V27495JMV
3.15 mg/Kg - dry 0.149 0.726Benzo(g,h,i)perylene 1 12/06/22 23:35 V27495JMV
3.05 mg/Kg - dry 0.150 0.726
Benzo(k)fluoranthene 1 12/06/22 23:35 V27495JMV
<0.638 M mg/Kg - dry 0.638 2.20Benzoic Acid 1 12/06/22 23:35 V27495JMV
<0.115 mg/Kg - dry 0.115 0.726Benzyl alcohol 1 12/06/22 23:35 V27495JMV
<0.129 mg/Kg - dry 0.129 0.726Bis(2-Chloroethoxy)methane 1 12/06/22 23:35 V27495JMV
<0.117 mg/Kg - dry 0.117 0.726Bis(2-Chloroethyl)ether 1 12/06/22 23:35 V27495JMV
<0.149 mg/Kg - dry 0.149 0.363Bis(2-Chloroisopropyl)ether 1 12/06/22 23:35 V27495JMV
<0.132 mg/Kg - dry 0.132 0.726Bis(2-ethylhexyl)phthalate 1 12/06/22 23:35 V27495JMV
<0.119 mg/Kg - dry 0.119 0.7264-Bromophenyl phenyl ether 1 12/06/22 23:35 V27495JMV
<0.124 mg/Kg - dry 0.124 0.363Butyl benzyl phthalate 1 12/06/22 23:35 V27495JMV
<0.101 mg/Kg - dry 0.101 0.7264-Chloro-3-methylphenol 1 12/06/22 23:35 V27495JMV
<0.123 mg/Kg - dry 0.123 0.3634-Chloroaniline 1 12/06/22 23:35 V27495JMV
<0.127 mg/Kg - dry 0.127 0.7262-Chloronaphthalene 1 12/06/22 23:35 V27495JMV
<0.108 mg/Kg - dry 0.108 0.7262-Chlorophenol 1 12/06/22 23:35 V27495JMV
<0.138 mg/Kg - dry 0.138 1.104-Chlorophenyl phenyl ether 1 12/06/22 23:35 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 171 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2E
94366 Matrix:
11/29/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
5.67 mg/Kg - dry 0.156 0.726Chrysene 1 12/06/22 23:35 V27495JMV
0.361 J
mg/Kg - dry 0.253 0.726
Dibenz(a,h)anthracene 1 12/06/22 23:35 V27495JMV
0.178 J mg/Kg - dry 0.130 0.726Dibenzofuran 1 12/06/22 23:35 V27495JMV
<0.103 mg/Kg - dry 0.103 0.7261,2-Dichlorobenzene 1 12/06/22 23:35 V27495JMV
<0.107 mg/Kg - dry 0.107 0.7261,3-Dichlorobenzene 1 12/06/22 23:35 V27495JMV
<0.107 mg/Kg - dry 0.107 0.3631,4-Dichlorobenzene 1 12/06/22 23:35 V27495JMV
<0.161 mg/Kg - dry 0.161 0.7263,3'-Dichlorobenzidine 1 12/06/22 23:35 V27495JMV
<0.105 mg/Kg - dry 0.105 0.7262,4-Dichlorophenol 1 12/06/22 23:35 V27495JMV
<0.198 mg/Kg - dry 0.198 0.726
Diethyl phthalate 1 12/06/22 23:35 V27495JMV
<0.191 mg/Kg - dry 0.191 0.726Dimethyl phthalate 1 12/06/22 23:35 V27495JMV
<0.118 mg/Kg - dry 0.118 0.3632,4-Dimethylphenol 1 12/06/22 23:35 V27495JMV
<0.117 mg/Kg - dry 0.117 0.726Di-n-butyl phthalate 1 12/06/22 23:35 V27495JMV
<0.264 mg/Kg - dry 0.264 1.654,6-Dinitro-2-methylphenol 1 12/06/22 23:35 V27495JMV
<0.572 mg/Kg - dry 0.572 1.652,4-Dinitrophenol 1 12/06/22 23:35 V27495JMV
<0.106 mg/Kg - dry 0.106 0.7262,4-Dinitrotoluene 1 12/06/22 23:35 V27495JMV
<0.118 mg/Kg - dry 0.118 0.7262,6-Dinitrotoluene 1 12/06/22 23:35 V27495JMV
<0.157 mg/Kg - dry 0.157 0.363Di-n-Octyl Phthalate 1 12/06/22 23:35 V27495JMV
12.4 mg/Kg - dry 0.541 2.91Fluoranthene 4 12/09/22 01:07 V27495JMV
0.258 J mg/Kg - dry 0.140 0.726Fluorene 1 12/06/22 23:35 V27495JMV
<0.116 mg/Kg - dry 0.116 0.726Hexachlorobenzene 1 12/06/22 23:35 V27495JMV
<0.107 mg/Kg - dry 0.107 0.726Hexachlorobutadiene 1 12/06/22 23:35 V27495JMV
<0.172 mg/Kg - dry 0.172 0.726Hexachlorocyclopentadiene 1 12/06/22 23:35 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 172 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2E
94366 Matrix:
11/29/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.087 mg/Kg - dry 0.087 0.726Hexachloroethane 1 12/06/22 23:35 V27495JMV
3.80 mg/Kg - dry 0.197 0.726
Indeno(1,2,3-cd)pyrene 1 12/06/22 23:35 V27495JMV
<0.210 mg/Kg - dry 0.210 0.726Isophorone 1 12/06/22 23:35 V27495JMV
<0.116 mg/Kg - dry 0.116 0.7261-Methylnaphthalene 1 12/06/22 23:35 V27495JMV
<0.110 mg/Kg - dry 0.110 0.7262-Methylnaphthalene 1 12/06/22 23:35 V27495JMV
<0.106 mg/Kg - dry 0.106 0.7262-Methylphenol 1 12/06/22 23:35 V27495JMV
<0.093 mg/Kg - dry 0.093 0.7263&4 Methylphenol 1 12/06/22 23:35 V27495JMV
0.176 J mg/Kg - dry 0.158 0.726Naphthalene 1 12/06/22 23:35 V27495JMV
<0.106 mg/Kg - dry 0.106 0.726
2-Nitroaniline 1 12/06/22 23:35 V27495JMV
<0.132 mg/Kg - dry 0.132 0.7263-Nitroaniline 1 12/06/22 23:35 V27495JMV
<0.102 mg/Kg - dry 0.102 0.3634-Nitroaniline 1 12/06/22 23:35 V27495JMV
<0.127 mg/Kg - dry 0.127 0.363Nitrobenzene 1 12/06/22 23:35 V27495JMV
<0.097 mg/Kg - dry 0.097 0.7262-Nitrophenol 1 12/06/22 23:35 V27495JMV
<0.128 mg/Kg - dry 0.128 0.7264-Nitrophenol 1 12/06/22 23:35 V27495JMV
<0.289 mg/Kg - dry 0.289 0.726N-Nitrosodimethylamine 1 12/06/22 23:35 V27495JMV
<0.199 mg/Kg - dry 0.199 0.726N-Nitrosodiphenylamine 1 12/06/22 23:35 V27495JMV
<0.129 mg/Kg - dry 0.129 0.726N-Nitroso-di-n-propylamine 1 12/06/22 23:35 V27495JMV
<0.381 mg/Kg - dry 0.381 1.10Pentachlorophenol 1 12/06/22 23:35 V27495JMV
4.01 mg/Kg - dry 0.228 0.726Phenanthrene 1 12/06/22 23:35 V27495JMV
0.559 J mg/Kg - dry 0.123 0.726Phenol 1 12/06/22 23:35 V27495JMV
11.1 mg/Kg - dry 0.589 2.91Pyrene 4 12/09/22 01:07 V27495JMV
<0.087 mg/Kg - dry 0.087 0.363Pyridine 1 12/06/22 23:35 V27495JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 173 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2E
94366 Matrix:
11/29/2022 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27278 12/05/22 11:00
<0.117 mg/Kg - dry 0.117 0.7261,2,4-Trichlorobenzene 1 12/06/22 23:35 V27495JMV
<0.105 mg/Kg - dry 0.105 0.726
2,4,5-Trichlorophenol 1 12/06/22 23:35 V27495JMV
<0.106 mg/Kg - dry 0.106 0.7262,4,6-Trichlorophenol 1 12/06/22 23:35 V27495JMV
8270ESurrogate: Phenol-d5 50.2 Limits: 34-121%12/06/22 23:351 JMV
Surrogate: 2-Fluorobiphenyl 67.7 Limits: 44-115%12/06/22 23:351 JMV V27495
Surrogate: 2-Fluorophenol 52.0 Limits: 35-115%12/06/22 23:351 JMV V27495
Surrogate: Nitrobenzene-d5 61.1 Limits: 37-122%12/06/22 23:351 JMV V27495
Surrogate: 4-Terphenyl-d14 68.9 Limits: 54-127%12/06/22 23:351 JMV V27495
Surrogate: 2,4,6-Tribromophenol 58.0 Limits: 39-132%12/06/22 23:351 JMV V27495
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 174 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-2 (0-2)
95246 Matrix:
11/29/2022 14:15
TCLP
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
LeachateTCLP Metals Extraction 1 12/12/22 17:03 SW-1311LMZ
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
SW-3010A
6010D Prep Batch(es):V27679 12/12/22 11:04
0.060 mg/L 0.008 0.030TCLP Lead 1 12/13/22 14:47 V27698EDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 175 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:EX-3 (3-6)
95247 Matrix:
11/29/2022 13:25
TCLP
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
LeachateTCLP Metals Extraction 1 12/12/22 17:03 SW-1311LMZ
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
SW-3010A
6010D Prep Batch(es):V27679 12/12/22 11:04
0.074 mg/L 0.008 0.030TCLP Lead 1 12/13/22 14:54 V27698EDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 176 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2B
95652 Matrix:
11/29/2022 12:25
TCLP
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
LeachateTCLP Metals Extraction 1 12/20/22 16:12 SW-1311LMZ
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
SW-3010A
6010D Prep Batch(es):V28065 12/20/22 12:00
0.166 mg/L 0.008 0.030TCLP Lead 1 12/20/22 18:48 V28095EDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 177 of 220
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-334-0100
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 11/30/2022
TCR-003
Report Date : 12/21/2022
Sample ID :
Lab No :
Sampled:COMP-2C
95653 Matrix:
11/29/2022 11:35
TCLP
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
LeachateTCLP Metals Extraction 1 12/20/22 16:12 SW-1311LMZ
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
SW-3010A
6010D Prep Batch(es):V28065 12/20/22 12:00
0.020 J mg/L 0.008 0.030TCLP Lead 1 12/20/22 19:01 V28095EDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 178 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Metals Analysis (TCLP)
6010D
V27698QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3010A
QC Prep:V27679
Associated Lab Samples: 95246, 95247
LRB-V27679 Matrix: TCLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/13/22 13:570.0300.008<0.008mg/LTCLP Lead
LCS-V27679Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.00.4820.500mg/LTCLP Lead 80-120
V 95240-MS-V27679 V 95240-MSD-V27679Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2.86 96.02.820.5000.5002.38mg/LTCLP Lead 88.0 75-125 1.4 20
V 95240-PDS-V27679Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/13/22 14:3898.02.39mg/LTCLP Lead
Page 1 of 39Date:12/21/2022 01:43 PM
Page 179 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Metals Analysis (TCLP)
6010D
V28095QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3010A
QC Prep:V28065
Associated Lab Samples: 95652, 95653
LRB-V28065 Matrix: TCLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/20/22 17:550.0300.008<0.008mg/LTCLP Lead
LCS-V28065Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1070.5370.500mg/LTCLP Lead 80-120
V 96037-MS-V28065 V 96037-MSD-V28065Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.55 92.01.580.5000.5001.09mg/LTCLP Lead 98.0 75-125 1.9 20
V 96037-PDS-V28065Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/20/22 18:261021.83mg/LTCLP Lead
Page 2 of 39Date:12/21/2022 01:43 PM
Page 180 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Metals Analyses
6020B
L653746QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L651943
Associated Lab Samples: 94362, 94363, 94364, 94365, 94366
LRB-L651943 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/13/22 21:150.2500.0310<0.0310mg/KgLead
LCS-L651943Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
99.02.472.50mg/KgLead 80-120
V 94366-MS-L651943 V 94366-MSD-L651943Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
34.8 66.0*34.12.392.4233.2mg/KgLead 38.0*75-125 2.0 80
V 94366-PDS-L651943Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/13/22 22:051022.06mg/KgLead
Page 3 of 39* QC Fail Date:12/21/2022 01:43 PM
Page 181 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Metals Analyses
6020B
V27539,V27628QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V27451
Associated Lab Samples: 94336, 94337, 94338, 94339, 94340, 94341, 94342, 94343, 94344, 94345, 94346, 94347, 94350
LRB-V27451 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/08/22 17:541.000.137<0.137mg/KgArsenic
12/08/22 17:5410.01.40<1.40mg/KgBarium
12/08/22 17:540.5000.0660<0.0660mg/KgCadmium
12/08/22 17:541.000.198<0.198mg/KgChromium
12/08/22 17:541.000.146<0.146mg/KgLead
12/08/22 17:542.000.741<0.741mg/KgSelenium
12/08/22 17:540.5000.0470<0.0470mg/KgSilver
LCS-V27451Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.011.812.5mg/KgArsenic 80-120
97.012.112.5mg/KgBarium 80-120
10112.612.5mg/KgCadmium 80-120
98.012.312.5mg/KgChromium 80-120
10012.512.5mg/KgLead 80-120
97.012.112.5mg/KgSelenium 80-120
97.04.865.00mg/KgSilver 80-120
V 94337-MS-V27451 V 94337-MSD-V27451Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
25.6 94.025.712.512.513.8mg/KgArsenic 95.0 75-125 0.3 20
192 256*19112.512.5160mg/KgBarium 248*75-125 0.5 20
31.4 12231.812.512.516.1mg/KgCadmium 126*75-125 1.2 20
85.9 26.0*78.712.512.582.6mg/KgChromium -31*75-125 8.7 20
Page 4 of 39* QC Fail Date:12/21/2022 01:43 PM
Page 182 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Metals Analyses
6020B
V27539,V27628QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V27451
V 94337-MS-V27451 V 94337-MSD-V27451Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
3210 6720*300012.512.52370mg/KgLead 5040*75-125 6.7 20
13.0 93.013.312.512.51.33mg/KgSelenium 96.0 75-125 2.2 20
9.53 1089.615.005.004.14mg/KgSilver 109 75-125 0.8 20
V 94337-PDS-V27451Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/08/22 17:1610119.6mg/KgArsenic
12/08/22 17:1610294.5mg/KgBarium
12/08/22 17:1699.020.4mg/KgCadmium
12/08/22 17:1698.052.7mg/KgChromium
12/09/22 23:091171460mg/KgLead
12/08/22 17:1610013.1mg/KgSelenium
12/08/22 17:1698.014.2mg/KgSilver
Page 5 of 39* QC Fail Date:12/21/2022 01:43 PM
Page 183 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V27185QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V27161
Associated Lab Samples: 94342, 94343, 94347, 94350
LRB-V27161 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/02/22 13:500.03000.0120<0.0120mg/KgMercury (Total)
LCS-V27161Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
99.00.4130.417mg/KgMercury (Total)80-120
V 94534-MS-V27161 V 94534-MSD-V27161Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.411 99.00.4160.4170.417<0.0120mg/KgMercury (Total)100 80-120 1.2 20
V 94534-PDS-V27161Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/02/22 14:061010.210mg/KgMercury (Total)
Page 6 of 39Date:12/21/2022 01:43 PM
Page 184 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V27259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V27204
Associated Lab Samples: 94337, 94338, 94339, 94341, 94344, 94345, 94346
LRB-V27204 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/05/22 13:180.03000.0120<0.0120mg/KgMercury (Total)
LCS-V27204Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1030.4290.417mg/KgMercury (Total)80-120
V 94204-MS-V27204 V 94204-MSD-V27204Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.665 90.00.6810.4170.4170.289mg/KgMercury (Total)94.0 80-120 2.3 20
V 94204-PDS-V27204Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/05/22 13:3699.00.350mg/KgMercury (Total)
Page 7 of 39Date:12/21/2022 01:43 PM
Page 185 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V27259QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V27234
Associated Lab Samples: 94336
LRB-V27234 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/05/22 14:150.03000.0120<0.0120mg/KgMercury (Total)
LCS-V27234Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1010.4190.417mg/KgMercury (Total)80-120
V 94752-MS-V27234 V 94752-MSD-V27234Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.411 99.00.4050.4170.417<0.0120mg/KgMercury (Total)97.0 80-120 1.4 20
V 94752-PDS-V27234Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/05/22 14:3793.00.194mg/KgMercury (Total)
Page 8 of 39Date:12/21/2022 01:43 PM
Page 186 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V27401QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V27292
Associated Lab Samples: 94340
LRB-V27292 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/07/22 10:290.03000.0120<0.0120mg/KgMercury (Total)
LCS-V27292Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1060.4410.417mg/KgMercury (Total)80-120
V 94340-MS-V27292 V 94340-MSD-V27292Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.508 96.00.5310.4170.4170.108mg/KgMercury (Total)102 80-120 4.4 20
V 94340-PDS-V27292Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/07/22 10:461050.276mg/KgMercury (Total)
Page 9 of 39Date:12/21/2022 01:43 PM
Page 187 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27134QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27133
Associated Lab Samples: 94336, 94337, 94338, 94339, 94340, 94341, 94342, 94343, 94344, 94345, 94346, 94347, 94348, 94349, 94350,
94351, 94352, 94353, 94354, 94355
LRB-V27133 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/01/22 12:590.0200.002<0.002mg/KgAcetone
12/01/22 12:590.0200.001<0.001mg/KgAcrolein
12/01/22 12:590.0200.0008<0.0008mg/KgAcrylonitrile
12/01/22 12:590.0050.0006<0.0006mg/KgBenzene
12/01/22 12:590.0050.0005<0.0005mg/KgBromobenzene
12/01/22 12:590.0050.0008<0.0008mg/KgBromochloromethane
12/01/22 12:590.0050.001<0.001mg/KgBromodichloromethane
12/01/22 12:590.0050.001<0.001mg/KgBromoform
12/01/22 12:590.0100.001<0.001mg/KgBromomethane
12/01/22 12:590.0050.0005<0.0005mg/Kgn-Butylbenzene
12/01/22 12:590.0050.0006<0.0006mg/Kgsec-Butyl benzene
12/01/22 12:590.0050.0005<0.0005mg/Kgtert-Butyl benzene
12/01/22 12:590.0050.0006<0.0006mg/KgCarbon Disulfide
12/01/22 12:590.0050.001<0.001mg/KgCarbon Tetrachloride
12/01/22 12:590.0050.0007<0.0007mg/KgChlorobenzene
12/01/22 12:590.0050.0009<0.0009mg/KgChlorodibromomethane
12/01/22 12:590.0100.0009<0.0009mg/KgChloroethane
12/01/22 12:590.0050.001<0.001mg/KgChloroform
12/01/22 12:590.0100.0006<0.0006mg/KgChloromethane
12/01/22 12:590.0050.0005<0.0005mg/Kg2-Chlorotoluene
12/01/22 12:590.0050.0004<0.0004mg/Kg4-Chlorotoluene
12/01/22 12:590.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
12/01/22 12:590.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
12/01/22 12:590.0050.0006<0.0006mg/Kg1,2-Dibromoethane
12/01/22 12:590.0050.0006<0.0006mg/KgDibromomethane
12/01/22 12:590.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
12/01/22 12:590.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 10 of 39Date:12/21/2022 01:43 PM
Page 188 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27134QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27133
Associated Lab Samples: 94336, 94337, 94338, 94339, 94340, 94341, 94342, 94343, 94344, 94345, 94346, 94347, 94348, 94349, 94350,
94351, 94352, 94353, 94354, 94355
LRB-V27133 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/01/22 12:590.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
12/01/22 12:590.0100.001<0.001mg/KgDichlorodifluoromethane
12/01/22 12:590.0050.0008<0.0008mg/Kg1,1-Dichloroethane
12/01/22 12:590.0050.001<0.001mg/Kg1,2-Dichloroethane
12/01/22 12:590.0050.0007<0.0007mg/Kg1,1-Dichloroethene
12/01/22 12:590.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
12/01/22 12:590.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
12/01/22 12:590.0050.0004<0.0004mg/Kg1,2-Dichloropropane
12/01/22 12:590.0050.0006<0.0006mg/Kg1,3-Dichloropropane
12/01/22 12:590.0050.001<0.001mg/Kg2,2-Dichloropropane
12/01/22 12:590.0050.0008<0.0008mg/Kg1,1-Dichloropropene
12/01/22 12:590.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
12/01/22 12:590.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
12/01/22 12:590.2500.014<0.014mg/KgEthanol
12/01/22 12:590.0050.0006<0.0006mg/KgEthylbenzene
12/01/22 12:590.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
12/01/22 12:590.0100.0008<0.0008mg/KgHexachlorobutadiene
12/01/22 12:590.0100.0007<0.0007mg/Kgn-Hexane
12/01/22 12:590.0200.0006<0.0006mg/Kg2-Hexanone
12/01/22 12:590.0050.0005<0.0005mg/KgIsopropylbenzene
12/01/22 12:590.0050.001<0.001mg/Kg4-Isopropyl toluene
12/01/22 12:590.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
12/01/22 12:590.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
12/01/22 12:590.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
12/01/22 12:590.0100.001<0.001mg/KgMethylene Chloride
12/01/22 12:590.0100.0010<0.0010mg/KgNaphthalene
12/01/22 12:590.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 11 of 39Date:12/21/2022 01:43 PM
Page 189 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27134QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27133
Associated Lab Samples: 94336, 94337, 94338, 94339, 94340, 94341, 94342, 94343, 94344, 94345, 94346, 94347, 94348, 94349, 94350,
94351, 94352, 94353, 94354, 94355
LRB-V27133 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/01/22 12:590.0050.001<0.001mg/KgStyrene
12/01/22 12:590.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
12/01/22 12:590.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
12/01/22 12:590.0050.0009<0.0009mg/KgTetrachloroethene
12/01/22 12:590.0050.0007<0.0007mg/KgToluene
12/01/22 12:590.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
12/01/22 12:590.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
12/01/22 12:590.0050.001<0.001mg/Kg1,1,1-Trichloroethane
12/01/22 12:590.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
12/01/22 12:590.0050.0009<0.0009mg/KgTrichloroethene
12/01/22 12:590.0100.002<0.002mg/KgTrichlorofluoromethane
12/01/22 12:590.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
12/01/22 12:590.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
12/01/22 12:590.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
12/01/22 12:590.0100.0005<0.0005mg/KgVinyl Acetate
12/01/22 12:590.0100.0005<0.0005mg/KgVinyl Chloride
12/01/22 12:590.0050.0005<0.0005mg/Kgo-Xylene
12/01/22 12:590.0100.001<0.001mg/Kgm,p-Xylene
12/01/22 12:594-Bromofluorobenzene (S)99.8 70-130
12/01/22 12:59Dibromofluoromethane (S)101 84-123
12/01/22 12:59Toluene-d8 (S)95.2 76-129
LCS-V27133 LCSD-V27133Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.079 79.283.80.0830.100mg/KgAcetone 29-198 5.6 20
Page 12 of 39Date:12/21/2022 01:43 PM
Page 190 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27134QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27133
LCS-V27133 LCSD-V27133Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.090 90.892.20.0920.100mg/KgAcrolein 70-130 1.5 20
0.093 93.894.00.0940.100mg/KgAcrylonitrile 65-134 0.2 20
0.052 1041060.0530.050mg/KgBenzene 74-127 1.8 20
0.049 99.496.80.0480.050mg/KgBromobenzene 73-125 2.6 20
0.056 1131190.0590.050mg/KgBromochloromethane 72-134 5.1 20
0.053 1071060.0530.050mg/KgBromodichloromethane 75-122 1.1 20
0.041 83.489.80.0440.050mg/KgBromoform 66-135 7.3 20
0.053 1081020.0500.050mg/KgBromomethane 20-180 5.7 20
0.047 94.897.80.0480.050mg/Kgn-Butylbenzene 65-135 3.1 20
0.048 97.898.40.0490.050mg/Kgsec-Butyl benzene 66-131 0.6 20
0.048 96.21010.0500.050mg/Kgtert-Butyl benzene 67-132 4.8 20
0.051 1041090.0540.050mg/KgCarbon Disulfide 61-129 4.8 20
0.057 1141190.0590.050mg/KgCarbon Tetrachloride 64-143 4.1 20
0.049 98.61020.0510.050mg/KgChlorobenzene 74-118 3.7 20
0.054 1081120.0550.050mg/KgChlorodibromomethane 73-122 3.4 20
0.046 92.491.00.0450.050mg/KgChloroethane 33-149 1.5 20
0.052 1051070.0530.050mg/KgChloroform 73-127 2.2 20
0.040 80.287.20.0430.050mg/KgChloromethane 45-143 8.3 20
0.048 97.297.80.0480.050mg/Kg2-Chlorotoluene 67-124 0.6 20
0.048 97.297.80.0480.050mg/Kg4-Chlorotoluene 71-126 0.6 20
0.041 83.685.60.0420.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.3 20
0.047 94.894.40.0470.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 0.4 20
0.052 1041020.0510.050mg/Kg1,2-Dibromoethane 70-132 2.1 20
0.051 1031120.0560.050mg/KgDibromomethane 74-133 8.5 20
0.047 95.293.80.0460.050mg/Kg1,2-Dichlorobenzene 72-123 1.4 20
0.046 92.493.80.0460.050mg/Kg1,3-Dichlorobenzene 71-120 1.5 20
Page 13 of 39Date:12/21/2022 01:43 PM
Page 191 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27134QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27133
LCS-V27133 LCSD-V27133Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 88.891.00.0450.050mg/Kg1,4-Dichlorobenzene 71-123 2.4 20
0.048 96.21020.0500.050mg/KgDichlorodifluoromethane 26-146 5.6 20
0.048 97.498.60.0490.050mg/Kg1,1-Dichloroethane 74-127 1.2 20
0.049 98.896.00.0480.050mg/Kg1,2-Dichloroethane 68-128 2.8 20
0.049 98.61010.0500.050mg/Kg1,1-Dichloroethene 67-149 2.2 20
0.051 1041020.0500.050mg/Kgcis-1,2-Dichloroethene 76-134 2.1 20
0.050 1011060.0530.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.4 20
0.048 97.699.20.0490.050mg/Kg1,2-Dichloropropane 73-130 1.6 20
0.047 95.697.40.0480.050mg/Kg1,3-Dichloropropane 75-124 1.8 20
0.052 1041060.0530.050mg/Kg2,2-Dichloropropane 50-142 1.9 20
0.053 1071080.0540.050mg/Kg1,1-Dichloropropene 71-130 1.4 20
0.052 1051050.0520.050mg/Kgcis-1,3-Dichloropropene 71-125 0.7 20
0.054 1081070.0530.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.9 20
0.989 79.179.70.9971.25mg/KgEthanol 70-130 0.8 20
0.047 95.097.40.0480.050mg/KgEthylbenzene 74-128 2.4 20
0.094 94.993.30.0930.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.7 20
0.040 81.083.40.0410.050mg/KgHexachlorobutadiene 64-125 2.9 20
0.060 1211200.0600.050mg/Kgn-Hexane 70-130 0.9 20
0.037 74.280.80.0400.050mg/Kg2-Hexanone 61-157 8.5 20
0.049 98.099.00.0490.050mg/KgIsopropylbenzene 68-126 1.0 20
0.048 97.498.00.0490.050mg/Kg4-Isopropyl toluene 68-129 0.6 20
0.036 73.670.40.0350.050mg/KgMethyl Ethyl Ketone (MEK)63-149 4.4 20
0.050 1021030.0510.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.5 20
0.038 77.678.00.0390.050mg/Kg4-Methyl-2-Pentanone 57-162 0.5 20
0.042 85.486.20.0430.050mg/KgMethylene Chloride 74-129 0.9 20
0.048 96.497.00.0480.050mg/KgNaphthalene 57-157 0.6 20
Page 14 of 39Date:12/21/2022 01:43 PM
Page 192 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27134QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27133
LCS-V27133 LCSD-V27133Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.047 94.498.20.0490.050mg/Kgn-Propylbenzene 67-130 3.9 20
0.050 1011040.0510.050mg/KgStyrene 77-121 2.9 20
0.049 99.01030.0510.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 3.5 20
0.045 90.092.80.0460.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.0 20
0.048 96.01030.0510.050mg/KgTetrachloroethene 68-130 6.6 20
0.049 99.01010.0500.050mg/KgToluene 71-129 1.8 20
0.046 92.489.20.0440.050mg/Kg1,2,3-Trichlorobenzene 68-130 3.5 20
0.047 94.493.20.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.2 20
0.053 1071070.0530.050mg/Kg1,1,1-Trichloroethane 67-131 0.0 20
0.051 1021020.0500.050mg/Kg1,1,2-Trichloroethane 70-133 0.7 20
0.055 1111110.0550.050mg/KgTrichloroethene 75-133 0.1 20
0.048 96.01010.0500.050mg/KgTrichlorofluoromethane 44-146 5.0 20
0.043 87.887.00.0430.050mg/Kg1,2,3-Trichloropropane 60-137 0.9 20
0.046 93.496.00.0480.050mg/Kg1,2,4-Trimethylbenzene 69-129 2.7 20
0.049 98.61030.0510.050mg/Kg1,3,5-Trimethylbenzene 69-128 4.3 20
0.057 1151160.0580.050mg/KgVinyl Acetate 60-140 0.8 20
0.047 94.899.80.0490.050mg/KgVinyl Chloride 48-147 5.1 20
0.048 97.41010.0500.050mg/Kgo-Xylene 74-126 3.8 20
0.095 95.81010.1010.100mg/Kgm,p-Xylene 75-124 5.2 20
99.697.64-Bromofluorobenzene (S)70-130
99.098.2Dibromofluoromethane (S)84-123
95.895.6Toluene-d8 (S)76-129
Page 15 of 39Date:12/21/2022 01:43 PM
Page 193 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27136QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27135
Associated Lab Samples: 94356, 94357, 94358, 94359, 94360, 94361
LRB-V27135 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/01/22 12:590.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
12/01/22 12:590.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
12/01/22 12:590.0050.0009<0.0009mg/KgTetrachloroethene
12/01/22 12:590.0050.0009<0.0009mg/KgTrichloroethene
12/01/22 12:590.0100.0005<0.0005mg/KgVinyl Chloride
12/01/22 12:594-Bromofluorobenzene (S)99.8 70-130
12/01/22 12:59Dibromofluoromethane (S)101 84-123
12/01/22 12:59Toluene-d8 (S)95.2 76-129
LCS-V27135 LCSD-V27135Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1041020.0500.050mg/Kgcis-1,2-Dichloroethene 76-134 2.1 20
0.050 1011060.0530.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.4 20
0.048 96.01030.0510.050mg/KgTetrachloroethene 68-130 6.6 20
0.055 1111110.0550.050mg/KgTrichloroethene 75-133 0.1 20
0.047 94.899.80.0490.050mg/KgVinyl Chloride 48-147 5.1 20
99.697.64-Bromofluorobenzene (S)70-130
99.098.2Dibromofluoromethane (S)84-123
95.895.6Toluene-d8 (S)76-129
Page 16 of 39Date:12/21/2022 01:43 PM
Page 194 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27410QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27192
Associated Lab Samples: 94336, 94337, 94338, 94339, 94340, 94342, 94343, 94344, 94345, 94346, 94347, 94350
LRB-V27192 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/04/22 10:280.6600.116<0.116mg/KgAcenaphthene
12/04/22 10:280.6600.105<0.105mg/KgAcenaphthylene
12/04/22 10:280.6600.152<0.152mg/KgAniline
12/04/22 10:280.6600.143<0.143mg/KgAnthracene
12/04/22 10:280.6600.139<0.139mg/KgBenzo(a)anthracene
12/04/22 10:280.6600.147<0.147mg/KgBenzo(a)pyrene
12/04/22 10:280.6600.146<0.146mg/KgBenzo(b)fluoranthene
12/04/22 10:280.6600.136<0.136mg/KgBenzo(g,h,i)perylene
12/04/22 10:280.6600.137<0.137mg/KgBenzo(k)fluoranthene
12/04/22 10:282.000.580<0.580mg/KgBenzoic Acid
12/04/22 10:280.6600.105<0.105mg/KgBenzyl alcohol
12/04/22 10:280.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
12/04/22 10:280.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
12/04/22 10:280.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
12/04/22 10:280.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
12/04/22 10:280.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
12/04/22 10:280.3300.113<0.113mg/KgButyl benzyl phthalate
12/04/22 10:280.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
12/04/22 10:280.3300.112<0.112mg/Kg4-Chloroaniline
12/04/22 10:280.6600.116<0.116mg/Kg2-Chloronaphthalene
12/04/22 10:280.6600.098<0.098mg/Kg2-Chlorophenol
12/04/22 10:281.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
12/04/22 10:280.6600.142<0.142mg/KgChrysene
12/04/22 10:280.6600.230<0.230mg/KgDibenz(a,h)anthracene
12/04/22 10:280.6600.119<0.119mg/KgDibenzofuran
12/04/22 10:280.6600.094<0.094mg/Kg1,2-Dichlorobenzene
12/04/22 10:280.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 17 of 39Date:12/21/2022 01:43 PM
Page 195 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27410QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27192
Associated Lab Samples: 94336, 94337, 94338, 94339, 94340, 94342, 94343, 94344, 94345, 94346, 94347, 94350
LRB-V27192 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/04/22 10:280.3300.097<0.097mg/Kg1,4-Dichlorobenzene
12/04/22 10:280.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
12/04/22 10:280.6600.095<0.095mg/Kg2,4-Dichlorophenol
12/04/22 10:280.6600.180<0.180mg/KgDiethyl phthalate
12/04/22 10:280.6600.174<0.174mg/KgDimethyl phthalate
12/04/22 10:280.3300.108<0.108mg/Kg2,4-Dimethylphenol
12/04/22 10:280.6600.107<0.107mg/KgDi-n-butyl phthalate
12/04/22 10:281.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
12/04/22 10:281.500.520<0.520mg/Kg2,4-Dinitrophenol
12/04/22 10:280.6600.096<0.096mg/Kg2,4-Dinitrotoluene
12/04/22 10:280.6600.108<0.108mg/Kg2,6-Dinitrotoluene
12/04/22 10:280.3300.143<0.143mg/KgDi-n-Octyl Phthalate
12/04/22 10:280.6600.123<0.123mg/KgFluoranthene
12/04/22 10:280.6600.128<0.128mg/KgFluorene
12/04/22 10:280.6600.106<0.106mg/KgHexachlorobenzene
12/04/22 10:280.6600.097<0.097mg/KgHexachlorobutadiene
12/04/22 10:280.6600.157<0.157mg/KgHexachlorocyclopentadiene
12/04/22 10:280.6600.079<0.079mg/KgHexachloroethane
12/04/22 10:280.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
12/04/22 10:280.6600.191<0.191mg/KgIsophorone
12/04/22 10:280.6600.106<0.106mg/Kg1-Methylnaphthalene
12/04/22 10:280.6600.100<0.100mg/Kg2-Methylnaphthalene
12/04/22 10:280.6600.097<0.097mg/Kg2-Methylphenol
12/04/22 10:280.6600.084<0.084mg/Kg3&4 Methylphenol
12/04/22 10:280.6600.144<0.144mg/KgNaphthalene
12/04/22 10:280.6600.096<0.096mg/Kg2-Nitroaniline
12/04/22 10:280.6600.120<0.120mg/Kg3-Nitroaniline
Page 18 of 39Date:12/21/2022 01:43 PM
Page 196 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27410QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27192
Associated Lab Samples: 94336, 94337, 94338, 94339, 94340, 94342, 94343, 94344, 94345, 94346, 94347, 94350
LRB-V27192 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/04/22 10:280.3300.093<0.093mg/Kg4-Nitroaniline
12/04/22 10:280.3300.116<0.116mg/KgNitrobenzene
12/04/22 10:280.6600.088<0.088mg/Kg2-Nitrophenol
12/04/22 10:280.6600.117<0.117mg/Kg4-Nitrophenol
12/04/22 10:280.6600.263<0.263mg/KgN-Nitrosodimethylamine
12/04/22 10:280.6600.181<0.181mg/KgN-Nitrosodiphenylamine
12/04/22 10:280.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
12/04/22 10:281.000.347<0.347mg/KgPentachlorophenol
12/04/22 10:280.6600.208<0.208mg/KgPhenanthrene
12/04/22 10:280.6600.112<0.112mg/KgPhenol
12/04/22 10:280.6600.134<0.134mg/KgPyrene
12/04/22 10:280.3300.079<0.079mg/KgPyridine
12/04/22 10:280.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
12/04/22 10:280.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
12/04/22 10:280.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
12/04/22 10:282-Fluorobiphenyl (S)90.4 44-115
12/04/22 10:282-Fluorophenol (S)76.8 35-115
12/04/22 10:28Nitrobenzene-d5 (S)77.2 37-122
12/04/22 10:284-Terphenyl-d14 (S)103 54-127
12/04/22 10:282,4,6-Tribromophenol (S)77.1 39-132
12/04/22 10:28Phenol-d5 (S)72.0 34-121
LCS-V27192Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.01.421.67mg/KgAcenaphthene 40-123
88.01.471.67mg/KgAcenaphthylene 32-132
Page 19 of 39Date:12/21/2022 01:43 PM
Page 197 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27410QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27192
LCS-V27192Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1011.691.67mg/KgAniline 12-197
94.01.571.67mg/KgAnthracene 47-123
95.81.601.67mg/KgBenzo(a)anthracene 49-126
1141.901.67mg/KgBenzo(a)pyrene 45-129
1141.901.67mg/KgBenzo(b)fluoranthene 45-132
1041.741.67mg/KgBenzo(g,h,i)perylene 43-134
1071.791.67mg/KgBenzo(k)fluoranthene 47-132
0.0*<0.5801.67mg/KgBenzoic Acid 10-83
80.21.341.67mg/KgBenzyl alcohol 29-122
79.01.321.67mg/KgBis(2-Chloroethoxy)methane 36-121
88.61.481.67mg/KgBis(2-Chloroethyl)ether 31-120
83.21.391.67mg/KgBis(2-Chloroisopropyl)ether 33-131
92.81.551.67mg/KgBis(2-ethylhexyl)phthalate 51-133
97.01.621.67mg/Kg4-Bromophenyl phenyl ether 46-124
94.01.571.67mg/KgButyl benzyl phthalate 48-132
73.01.221.67mg/Kg4-Chloro-3-methylphenol 45-122
70.01.171.67mg/Kg4-Chloroaniline 17-106
89.81.501.67mg/Kg2-Chloronaphthalene 41-114
85.61.431.67mg/Kg2-Chlorophenol 34-121
93.41.561.67mg/Kg4-Chlorophenyl phenyl ether 45-121
94.01.571.67mg/KgChrysene 50-124
1131.891.67mg/KgDibenz(a,h)anthracene 45-134
88.61.481.67mg/KgDibenzofuran 44-120
76.61.281.67mg/Kg1,2-Dichlorobenzene 33-117
73.61.231.67mg/Kg1,3-Dichlorobenzene 30-115
73.01.221.67mg/Kg1,4-Dichlorobenzene 31-115
64.01.071.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 20 of 39* QC Fail Date:12/21/2022 01:43 PM
Page 198 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27410QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27192
LCS-V27192Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
77.81.301.67mg/Kg2,4-Dichlorophenol 40-122
91.01.521.67mg/KgDiethyl phthalate 50-124
89.21.491.67mg/KgDimethyl phthalate 48-124
99.41.661.67mg/Kg2,4-Dimethylphenol 30-127
1011.691.67mg/KgDi-n-butyl phthalate 51-128
83.21.391.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
58.00.9701.67mg/Kg2,4-Dinitrophenol 27-129
89.21.491.67mg/Kg2,4-Dinitrotoluene 48-126
88.61.481.67mg/Kg2,6-Dinitrotoluene 46-124
1011.681.67mg/KgDi-n-Octyl Phthalate 45-140
88.61.481.67mg/KgFluoranthene 50-127
91.61.531.67mg/KgFluorene 43-125
1001.671.67mg/KgHexachlorobenzene 45-122
76.01.271.67mg/KgHexachlorobutadiene 32-123
83.81.401.67mg/KgHexachlorocyclopentadiene 32-117
74.81.251.67mg/KgHexachloroethane 28-117
1031.721.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
59.81.001.67mg/KgIsophorone 30-122
74.21.241.67mg/Kg1-Methylnaphthalene 40-119
74.21.241.67mg/Kg2-Methylnaphthalene 38-122
84.41.411.67mg/Kg2-Methylphenol 32-122
74.81.251.67mg/Kg3&4 Methylphenol 34-119
74.21.241.67mg/KgNaphthalene 35-123
85.61.431.67mg/Kg2-Nitroaniline 44-127
83.21.391.67mg/Kg3-Nitroaniline 33-119
90.41.511.67mg/Kg4-Nitroaniline 63-147
70.61.181.67mg/KgNitrobenzene 34-122
Page 21 of 39Date:12/21/2022 01:43 PM
Page 199 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27410QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27192
LCS-V27192Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
70.01.171.67mg/Kg2-Nitrophenol 36-123
1021.711.67mg/Kg4-Nitrophenol 30-132
63.41.061.67mg/KgN-Nitrosodimethylamine 10-146
1111.861.67mg/KgN-Nitrosodiphenylamine 38-127
77.81.301.67mg/KgN-Nitroso-di-n-propylamine 36-120
1161.941.67mg/KgPentachlorophenol 25-133
94.61.581.67mg/KgPhenanthrene 50-121
85.01.421.67mg/KgPhenol 34-121
92.21.541.67mg/KgPyrene 47-127
49.50.8281.67mg/KgPyridine 10-80
72.41.211.67mg/Kg1,2,4-Trichlorobenzene 34-118
88.61.481.67mg/Kg2,4,5-Trichlorophenol 41-124
89.21.491.67mg/Kg2,4,6-Trichlorophenol 39-126
91.02-Fluorobiphenyl (S)44-115
75.32-Fluorophenol (S)35-115
70.6Nitrobenzene-d5 (S)37-122
1014-Terphenyl-d14 (S)54-127
87.62,4,6-Tribromophenol (S)39-132
71.1Phenol-d5 (S)34-121
V 94281-MS-V27192 V 94281-MSD-V27192Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.47 88.01.541.671.67<0.116mg/KgAcenaphthene 92.2 40-123 4.6 20
1.49 89.21.521.671.67<0.105mg/KgAcenaphthylene 91.0 32-132 1.9 20
1.82 1091.801.671.67<0.152mg/KgAniline 108 12-197 1.1 20
Page 22 of 39Date:12/21/2022 01:43 PM
Page 200 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27410QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27192
V 94281-MS-V27192 V 94281-MSD-V27192Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.63 97.61.611.671.67<0.143mg/KgAnthracene 96.4 47-123 1.2 20
1.62 88.11.691.671.670.148mg/KgBenzo(a)anthracene 92.3 49-126 4.2 20
1.86 1022.021.671.670.150mg/KgBenzo(a)pyrene 112 45-129 8.2 20
1.87 1011.951.671.670.178mg/KgBenzo(b)fluoranthene 106 45-132 4.1 20
1.68 1011.881.671.67<0.136mg/KgBenzo(g,h,i)perylene 113 43-134 11.2 20
1.74 1041.801.671.67<0.137mg/KgBenzo(k)fluoranthene 108 47-132 3.3 20
<0.580 0.0*<0.5801.671.67<0.580mg/KgBenzoic Acid 0.0 10-83 0.0 20
1.47 88.01.481.671.67<0.105mg/KgBenzyl alcohol 88.6 29-122 0.6 20
1.37 82.01.421.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 85.0 36-121 3.5 20
1.48 88.61.541.671.67<0.107mg/KgBis(2-Chloroethyl)ether 92.2 31-120 3.9 20
1.50 89.81.501.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 89.8 33-131 0.0 20
1.63 97.61.741.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 104 51-133 6.5 20
1.63 97.61.751.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 105 46-124 7.1 20
1.63 97.61.751.671.67<0.113mg/KgButyl benzyl phthalate 105 48-132 7.1 20
1.20 71.81.331.671.67<0.092mg/Kg4-Chloro-3-methylphenol 79.6 45-122 10.2 20
1.15 68.81.201.671.67<0.112mg/Kg4-Chloroaniline 71.8 17-106 4.2 20
1.62 97.01.571.671.67<0.116mg/Kg2-Chloronaphthalene 94.0 41-114 3.1 20
1.58 94.61.641.671.67<0.098mg/Kg2-Chlorophenol 98.2 34-121 3.7 20
1.55 92.81.671.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 100 45-121 7.4 20
1.62 97.01.711.671.67<0.142mg/KgChrysene 102 50-124 5.4 20
1.69 1012.031.671.67<0.230mg/KgDibenz(a,h)anthracene 122 45-134 18.2 20
1.48 88.61.541.671.67<0.119mg/KgDibenzofuran 92.2 44-120 3.9 20
1.39 83.21.431.671.67<0.094mg/Kg1,2-Dichlorobenzene 85.6 33-117 2.8 20
1.35 80.81.401.671.67<0.097mg/Kg1,3-Dichlorobenzene 83.8 30-115 3.6 20
1.32 79.01.371.671.67<0.097mg/Kg1,4-Dichlorobenzene 82.0 31-115 3.7 20
1.23 73.61.261.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 75.4 22-121 2.4 20
Page 23 of 39Date:12/21/2022 01:43 PM
Page 201 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27410QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27192
V 94281-MS-V27192 V 94281-MSD-V27192Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.38 82.61.451.671.67<0.095mg/Kg2,4-Dichlorophenol 86.8 40-122 4.9 20
1.50 89.81.601.671.67<0.180mg/KgDiethyl phthalate 95.8 50-124 6.4 20
1.54 92.21.531.671.67<0.174mg/KgDimethyl phthalate 91.6 48-124 0.6 30
1.75 1051.841.671.67<0.108mg/Kg2,4-Dimethylphenol 110 30-127 5.0 20
1.72 1031.651.671.67<0.107mg/KgDi-n-butyl phthalate 98.8 51-128 4.1 20
1.33 79.61.411.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 84.4 29-132 5.8 20
0.978 58.50.9431.671.67<0.520mg/Kg2,4-Dinitrophenol 56.4 27-129 3.6 20
1.51 90.41.581.671.67<0.096mg/Kg2,4-Dinitrotoluene 94.6 48-126 4.5 20
1.46 87.41.561.671.67<0.108mg/Kg2,6-Dinitrotoluene 93.4 46-124 6.6 20
1.82 1091.841.671.67<0.143mg/KgDi-n-Octyl Phthalate 110 45-140 1.0 20
1.57 80.81.521.671.670.219mg/KgFluoranthene 77.9 50-127 3.2 20
1.53 91.61.641.671.67<0.128mg/KgFluorene 98.2 43-125 6.9 20
1.66 99.41.771.671.67<0.106mg/KgHexachlorobenzene 106 45-122 6.4 20
1.35 80.81.461.671.67<0.097mg/KgHexachlorobutadiene 87.4 32-123 7.8 20
1.18 70.61.011.671.67<0.157mg/KgHexachlorocyclopentadiene 60.4 32-117 15.5 20
1.35 80.81.381.671.67<0.079mg/KgHexachloroethane 82.6 28-117 2.1 20
1.59 95.21.921.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 115 45-133 18.8 20
1.04 62.21.091.671.67<0.191mg/KgIsophorone 65.2 30-122 4.6 20
1.18 70.61.271.671.67<0.106mg/Kg1-Methylnaphthalene 76.0 40-119 7.3 20
1.24 74.21.301.671.67<0.100mg/Kg2-Methylnaphthalene 77.8 38-122 4.7 20
1.51 90.41.561.671.67<0.097mg/Kg2-Methylphenol 93.4 32-122 3.2 20
1.31 78.41.351.671.67<0.084mg/Kg3&4 Methylphenol 80.8 34-119 3.0 20
1.31 78.41.381.671.67<0.144mg/KgNaphthalene 82.6 35-123 5.2 20
1.48 88.61.481.671.67<0.096mg/Kg2-Nitroaniline 88.6 44-127 0.0 20
1.40 83.81.441.671.67<0.120mg/Kg3-Nitroaniline 86.2 33-119 2.8 20
1.49 89.21.591.671.67<0.093mg/Kg4-Nitroaniline 95.2 63-147 6.4 20
Page 24 of 39Date:12/21/2022 01:43 PM
Page 202 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27410QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27192
V 94281-MS-V27192 V 94281-MSD-V27192Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.22 73.01.251.671.67<0.116mg/KgNitrobenzene 74.8 34-122 2.4 20
1.25 74.81.311.671.67<0.088mg/Kg2-Nitrophenol 78.4 32-123 4.6 20
2.06 1231.791.671.67<0.117mg/Kg4-Nitrophenol 107 30-132 14.0 20
1.17 70.01.271.671.67<0.263mg/KgN-Nitrosodimethylamine 76.0 10-146 8.1 30
1.88 1132.031.671.67<0.181mg/KgN-Nitrosodiphenylamine 122 38-127 7.6 20
1.37 82.01.401.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 83.8 36-120 2.1 20
2.01 1202.041.671.67<0.347mg/KgPentachlorophenol 122 25-133 1.4 20
1.61 96.41.641.671.67<0.208mg/KgPhenanthrene 98.2 50-121 1.8 20
1.51 90.41.601.671.67<0.112mg/KgPhenol 95.8 34-121 5.7 20
1.61 79.71.781.671.670.278mg/KgPyrene 89.9 47-127 10.0 20
0.978 58.51.091.671.67<0.079mg/KgPyridine 65.2 10-80 10.8 20
1.31 78.41.321.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 79.0 34-118 0.7 20
1.58 94.61.611.671.67<0.096mg/Kg2,4,5-Trichlorophenol 96.4 41-124 1.8 20
1.60 95.81.601.671.67<0.096mg/Kg2,4,6-Trichlorophenol 95.8 39-126 0.0 20
96.42-Fluorobiphenyl (S)96.4 44-115
80.72-Fluorophenol (S)82.0 35-115
73.0Nitrobenzene-d5 (S)73.0 37-122
1024-Terphenyl-d14 (S)106 54-127
87.92,4,6-Tribromophenol (S)91.0 39-132
75.9Phenol-d5 (S)79.6 34-121
Page 25 of 39Date:12/21/2022 01:43 PM
Page 203 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27495QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27278
Associated Lab Samples: 94341, 94362, 94363, 94364, 94365, 94366
LRB-V27278 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/06/22 16:510.6600.116<0.116mg/KgAcenaphthene
12/06/22 16:510.6600.105<0.105mg/KgAcenaphthylene
12/06/22 16:510.6600.152<0.152mg/KgAniline
12/06/22 16:510.6600.143<0.143mg/KgAnthracene
12/06/22 16:510.6600.139<0.139mg/KgBenzo(a)anthracene
12/06/22 16:510.6600.147<0.147mg/KgBenzo(a)pyrene
12/06/22 16:510.6600.146<0.146mg/KgBenzo(b)fluoranthene
12/06/22 16:510.6600.136<0.136mg/KgBenzo(g,h,i)perylene
12/06/22 16:510.6600.137<0.137mg/KgBenzo(k)fluoranthene
12/06/22 16:512.000.580<0.580mg/KgBenzoic Acid
12/06/22 16:510.6600.105<0.105mg/KgBenzyl alcohol
12/06/22 16:510.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
12/06/22 16:510.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
12/06/22 16:510.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
12/06/22 16:510.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
12/06/22 16:510.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
12/06/22 16:510.3300.113<0.113mg/KgButyl benzyl phthalate
12/06/22 16:510.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
12/06/22 16:510.3300.112<0.112mg/Kg4-Chloroaniline
12/06/22 16:510.6600.116<0.116mg/Kg2-Chloronaphthalene
12/06/22 16:510.6600.098<0.098mg/Kg2-Chlorophenol
12/06/22 16:511.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
12/06/22 16:510.6600.142<0.142mg/KgChrysene
12/06/22 16:510.6600.230<0.230mg/KgDibenz(a,h)anthracene
12/06/22 16:510.6600.119<0.119mg/KgDibenzofuran
12/06/22 16:510.6600.094<0.094mg/Kg1,2-Dichlorobenzene
12/06/22 16:510.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 26 of 39Date:12/21/2022 01:43 PM
Page 204 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27495QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27278
Associated Lab Samples: 94341, 94362, 94363, 94364, 94365, 94366
LRB-V27278 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/06/22 16:510.3300.097<0.097mg/Kg1,4-Dichlorobenzene
12/06/22 16:510.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
12/06/22 16:510.6600.095<0.095mg/Kg2,4-Dichlorophenol
12/06/22 16:510.6600.180<0.180mg/KgDiethyl phthalate
12/06/22 16:510.6600.174<0.174mg/KgDimethyl phthalate
12/06/22 16:510.3300.108<0.108mg/Kg2,4-Dimethylphenol
12/06/22 16:510.6600.107<0.107mg/KgDi-n-butyl phthalate
12/06/22 16:511.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
12/06/22 16:511.500.520<0.520mg/Kg2,4-Dinitrophenol
12/06/22 16:510.6600.096<0.096mg/Kg2,4-Dinitrotoluene
12/06/22 16:510.6600.108<0.108mg/Kg2,6-Dinitrotoluene
12/06/22 16:510.3300.143<0.143mg/KgDi-n-Octyl Phthalate
12/06/22 16:510.6600.123<0.123mg/KgFluoranthene
12/06/22 16:510.6600.128<0.128mg/KgFluorene
12/06/22 16:510.6600.106<0.106mg/KgHexachlorobenzene
12/06/22 16:510.6600.097<0.097mg/KgHexachlorobutadiene
12/06/22 16:510.6600.157<0.157mg/KgHexachlorocyclopentadiene
12/06/22 16:510.6600.079<0.079mg/KgHexachloroethane
12/06/22 16:510.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
12/06/22 16:510.6600.191<0.191mg/KgIsophorone
12/06/22 16:510.6600.106<0.106mg/Kg1-Methylnaphthalene
12/06/22 16:510.6600.100<0.100mg/Kg2-Methylnaphthalene
12/06/22 16:510.6600.097<0.097mg/Kg2-Methylphenol
12/06/22 16:510.6600.084<0.084mg/Kg3&4 Methylphenol
12/06/22 16:510.6600.144<0.144mg/KgNaphthalene
12/06/22 16:510.6600.096<0.096mg/Kg2-Nitroaniline
12/06/22 16:510.6600.120<0.120mg/Kg3-Nitroaniline
Page 27 of 39Date:12/21/2022 01:43 PM
Page 205 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27495QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27278
Associated Lab Samples: 94341, 94362, 94363, 94364, 94365, 94366
LRB-V27278 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/06/22 16:510.3300.093<0.093mg/Kg4-Nitroaniline
12/06/22 16:510.3300.116<0.116mg/KgNitrobenzene
12/06/22 16:510.6600.088<0.088mg/Kg2-Nitrophenol
12/06/22 16:510.6600.117<0.117mg/Kg4-Nitrophenol
12/06/22 16:510.6600.263<0.263mg/KgN-Nitrosodimethylamine
12/06/22 16:510.6600.181<0.181mg/KgN-Nitrosodiphenylamine
12/06/22 16:510.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
12/06/22 16:511.000.347<0.347mg/KgPentachlorophenol
12/06/22 16:510.6600.208<0.208mg/KgPhenanthrene
12/06/22 16:510.6600.112<0.112mg/KgPhenol
12/06/22 16:510.6600.134<0.134mg/KgPyrene
12/06/22 16:510.3300.079<0.079mg/KgPyridine
12/06/22 16:510.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
12/06/22 16:510.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
12/06/22 16:510.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
12/06/22 16:512-Fluorobiphenyl (S)83.8 44-115
12/06/22 16:512-Fluorophenol (S)72.3 35-115
12/06/22 16:51Nitrobenzene-d5 (S)75.4 37-122
12/06/22 16:514-Terphenyl-d14 (S)104 54-127
12/06/22 16:512,4,6-Tribromophenol (S)75.9 39-132
12/06/22 16:51Phenol-d5 (S)68.1 34-121
LCS-V27278Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
87.41.461.67mg/KgAcenaphthene 40-123
88.61.481.67mg/KgAcenaphthylene 32-132
Page 28 of 39Date:12/21/2022 01:43 PM
Page 206 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27495QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27278
LCS-V27278Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1071.791.67mg/KgAniline 12-197
94.61.581.67mg/KgAnthracene 47-123
94.61.581.67mg/KgBenzo(a)anthracene 49-126
1131.881.67mg/KgBenzo(a)pyrene 45-129
1051.751.67mg/KgBenzo(b)fluoranthene 45-132
1061.771.67mg/KgBenzo(g,h,i)perylene 43-134
1081.811.67mg/KgBenzo(k)fluoranthene 47-132
0.0*<0.5801.67mg/KgBenzoic Acid 10-83
80.21.341.67mg/KgBenzyl alcohol 29-122
76.61.281.67mg/KgBis(2-Chloroethoxy)methane 36-121
82.01.371.67mg/KgBis(2-Chloroethyl)ether 31-120
79.61.331.67mg/KgBis(2-Chloroisopropyl)ether 33-131
95.81.601.67mg/KgBis(2-ethylhexyl)phthalate 51-133
97.01.621.67mg/Kg4-Bromophenyl phenyl ether 46-124
98.21.641.67mg/KgButyl benzyl phthalate 48-132
76.01.271.67mg/Kg4-Chloro-3-methylphenol 45-122
68.21.141.67mg/Kg4-Chloroaniline 17-106
90.41.511.67mg/Kg2-Chloronaphthalene 41-114
83.21.391.67mg/Kg2-Chlorophenol 34-121
89.21.491.67mg/Kg4-Chlorophenyl phenyl ether 45-121
92.81.551.67mg/KgChrysene 50-124
1161.941.67mg/KgDibenz(a,h)anthracene 45-134
83.81.401.67mg/KgDibenzofuran 44-120
74.81.251.67mg/Kg1,2-Dichlorobenzene 33-117
73.01.221.67mg/Kg1,3-Dichlorobenzene 30-115
74.81.251.67mg/Kg1,4-Dichlorobenzene 31-115
58.90.9851.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 29 of 39* QC Fail Date:12/21/2022 01:43 PM
Page 207 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27495QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27278
LCS-V27278Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
77.81.301.67mg/Kg2,4-Dichlorophenol 40-122
86.81.451.67mg/KgDiethyl phthalate 50-124
92.21.541.67mg/KgDimethyl phthalate 48-124
95.21.591.67mg/Kg2,4-Dimethylphenol 30-127
1041.731.67mg/KgDi-n-butyl phthalate 51-128
85.01.421.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
64.61.081.67mg/Kg2,4-Dinitrophenol 27-129
85.01.421.67mg/Kg2,4-Dinitrotoluene 48-126
92.81.551.67mg/Kg2,6-Dinitrotoluene 46-124
1001.671.67mg/KgDi-n-Octyl Phthalate 45-140
91.01.521.67mg/KgFluoranthene 50-127
86.81.451.67mg/KgFluorene 43-125
1021.701.67mg/KgHexachlorobenzene 45-122
74.81.251.67mg/KgHexachlorobutadiene 32-123
86.21.441.67mg/KgHexachlorocyclopentadiene 32-117
73.61.231.67mg/KgHexachloroethane 28-117
1061.771.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
57.00.9531.67mg/KgIsophorone 30-122
73.01.221.67mg/Kg1-Methylnaphthalene 40-119
73.61.231.67mg/Kg2-Methylnaphthalene 38-122
84.41.411.67mg/Kg2-Methylphenol 32-122
75.41.261.67mg/Kg3&4 Methylphenol 34-119
73.01.221.67mg/KgNaphthalene 35-123
89.21.491.67mg/Kg2-Nitroaniline 44-127
83.81.401.67mg/Kg3-Nitroaniline 33-119
88.01.471.67mg/Kg4-Nitroaniline 63-147
67.01.121.67mg/KgNitrobenzene 34-122
Page 30 of 39Date:12/21/2022 01:43 PM
Page 208 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27495QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27278
LCS-V27278Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
67.61.131.67mg/Kg2-Nitrophenol 36-123
95.81.601.67mg/Kg4-Nitrophenol 30-132
60.41.011.67mg/KgN-Nitrosodimethylamine 10-146
1131.891.67mg/KgN-Nitrosodiphenylamine 38-127
77.81.301.67mg/KgN-Nitroso-di-n-propylamine 36-120
1191.991.67mg/KgPentachlorophenol 25-133
94.61.581.67mg/KgPhenanthrene 50-121
85.01.421.67mg/KgPhenol 34-121
93.41.561.67mg/KgPyrene 47-127
47.30.7901.67mg/KgPyridine 10-80
71.81.201.67mg/Kg1,2,4-Trichlorobenzene 34-118
92.21.541.67mg/Kg2,4,5-Trichlorophenol 41-124
92.81.551.67mg/Kg2,4,6-Trichlorophenol 39-126
93.42-Fluorobiphenyl (S)44-115
73.82-Fluorophenol (S)35-115
68.2Nitrobenzene-d5 (S)37-122
1034-Terphenyl-d14 (S)54-127
85.52,4,6-Tribromophenol (S)39-132
71.4Phenol-d5 (S)34-121
V 94691-MS-V27278 V 94691-MSD-V27278Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.44 86.21.511.671.67<0.116mg/KgAcenaphthene 90.4 40-123 4.7 20
1.45 86.81.501.671.67<0.105mg/KgAcenaphthylene 89.8 32-132 3.3 20
2.63 1571.221.671.67<0.152mg/KgAniline 73.0 12-197 73.2*20
Page 31 of 39* QC Fail Date:12/21/2022 01:43 PM
Page 209 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27495QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27278
V 94691-MS-V27278 V 94691-MSD-V27278Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.59 95.21.661.671.67<0.143mg/KgAnthracene 99.4 47-123 4.3 20
1.57 94.01.591.671.67<0.139mg/KgBenzo(a)anthracene 95.2 49-126 1.2 20
1.84 1101.941.671.67<0.147mg/KgBenzo(a)pyrene 116 45-129 5.2 20
1.78 1071.861.671.67<0.146mg/KgBenzo(b)fluoranthene 111 45-132 4.3 20
1.78 1071.731.671.67<0.136mg/KgBenzo(g,h,i)perylene 104 43-134 2.8 20
1.76 1051.881.671.67<0.137mg/KgBenzo(k)fluoranthene 113 47-132 6.5 20
1.24 74.21.311.671.67<0.580mg/KgBenzoic Acid 78.4 10-83 5.4 20
1.38 82.61.421.671.67<0.105mg/KgBenzyl alcohol 85.0 29-122 2.8 20
1.23 73.61.371.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 82.0 36-121 10.7 20
2.40 144*1.491.671.67<0.107mg/KgBis(2-Chloroethyl)ether 89.2 31-120 46.7*20
1.32 79.01.361.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 81.4 33-131 2.9 20
1.83 1101.831.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 110 51-133 0.0 20
1.63 97.61.701.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 102 46-124 4.2 20
1.69 1011.681.671.67<0.113mg/KgButyl benzyl phthalate 101 48-132 0.5 20
1.31 78.41.281.671.67<0.092mg/Kg4-Chloro-3-methylphenol 76.6 45-122 2.3 20
1.02 61.01.081.671.67<0.112mg/Kg4-Chloroaniline 64.6 17-106 5.7 20
1.60 95.81.501.671.67<0.116mg/Kg2-Chloronaphthalene 89.8 41-114 6.4 20
1.37 82.01.441.671.67<0.098mg/Kg2-Chlorophenol 86.2 34-121 4.9 20
1.56 93.41.591.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 95.2 45-121 1.9 20
1.56 93.41.631.671.67<0.142mg/KgChrysene 97.6 50-124 4.3 20
2.00 1201.891.671.67<0.230mg/KgDibenz(a,h)anthracene 113 45-134 5.6 20
1.45 86.81.521.671.67<0.119mg/KgDibenzofuran 91.0 44-120 4.7 20
1.26 75.41.321.671.67<0.094mg/Kg1,2-Dichlorobenzene 79.0 33-117 4.6 20
1.22 73.01.271.671.67<0.097mg/Kg1,3-Dichlorobenzene 76.0 30-115 4.0 20
1.21 72.41.261.671.67<0.097mg/Kg1,4-Dichlorobenzene 75.4 31-115 4.0 20
1.02 61.01.121.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 67.0 22-121 9.3 20
Page 32 of 39* QC Fail Date:12/21/2022 01:43 PM
Page 210 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27495QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27278
V 94691-MS-V27278 V 94691-MSD-V27278Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.32 79.01.401.671.67<0.095mg/Kg2,4-Dichlorophenol 83.8 40-122 5.8 20
1.54 92.21.551.671.67<0.180mg/KgDiethyl phthalate 92.8 50-124 0.6 20
1.50 89.81.521.671.67<0.174mg/KgDimethyl phthalate 91.0 48-124 1.3 30
1.65 98.81.871.671.67<0.108mg/Kg2,4-Dimethylphenol 112 30-127 12.5 20
1.62 97.01.741.671.67<0.107mg/KgDi-n-butyl phthalate 104 51-128 7.1 20
1.49 89.21.581.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 94.6 29-132 5.8 20
1.66 99.41.711.671.67<0.520mg/Kg2,4-Dinitrophenol 102 27-129 2.9 20
1.46 87.41.511.671.67<0.096mg/Kg2,4-Dinitrotoluene 90.4 48-126 3.3 20
1.49 89.21.531.671.67<0.108mg/Kg2,6-Dinitrotoluene 91.6 46-124 2.6 20
1.77 1061.801.671.67<0.143mg/KgDi-n-Octyl Phthalate 108 45-140 1.6 20
1.37 82.01.451.671.67<0.123mg/KgFluoranthene 86.8 50-127 5.6 20
1.55 92.81.551.671.67<0.128mg/KgFluorene 92.8 43-125 0.0 20
1.66 99.41.731.671.67<0.106mg/KgHexachlorobenzene 104 45-122 4.1 20
1.27 76.01.351.671.67<0.097mg/KgHexachlorobutadiene 80.8 32-123 6.1 20
0.878 52.50.6921.671.67<0.157mg/KgHexachlorocyclopentadiene 41.4 32-117 23.6*20
1.23 73.61.321.671.67<0.079mg/KgHexachloroethane 79.0 28-117 7.0 20
1.79 1071.731.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 104 45-133 3.4 20
0.994 59.51.091.671.67<0.191mg/KgIsophorone 65.2 30-122 9.2 20
1.30 77.81.311.671.67<0.106mg/Kg1-Methylnaphthalene 78.4 40-119 0.7 20
1.33 79.61.311.671.67<0.100mg/Kg2-Methylnaphthalene 78.4 38-122 1.5 20
1.40 83.81.431.671.67<0.097mg/Kg2-Methylphenol 85.6 32-122 2.1 20
1.27 76.01.251.671.67<0.084mg/Kg3&4 Methylphenol 74.8 34-119 1.5 20
1.21 72.41.311.671.67<0.144mg/KgNaphthalene 78.4 35-123 7.9 20
1.56 93.41.531.671.67<0.096mg/Kg2-Nitroaniline 91.6 44-127 1.9 20
1.34 80.21.401.671.67<0.120mg/Kg3-Nitroaniline 83.8 33-119 4.3 20
1.44 86.21.491.671.67<0.093mg/Kg4-Nitroaniline 89.2 63-147 3.4 20
Page 33 of 39* QC Fail Date:12/21/2022 01:43 PM
Page 211 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27495QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27278
V 94691-MS-V27278 V 94691-MSD-V27278Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.14 68.21.221.671.67<0.116mg/KgNitrobenzene 73.0 34-122 6.7 20
1.15 68.81.351.671.67<0.088mg/Kg2-Nitrophenol 80.8 32-123 16.0 20
1.77 1061.741.671.67<0.117mg/Kg4-Nitrophenol 104 30-132 1.7 20
0.836 50.00.8991.671.67<0.263mg/KgN-Nitrosodimethylamine 53.8 10-146 7.2 30
1.86 1111.981.671.67<0.181mg/KgN-Nitrosodiphenylamine 119 38-127 6.2 20
1.28 76.61.341.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 80.2 36-120 4.5 20
2.14 1282.201.671.67<0.347mg/KgPentachlorophenol 132 25-133 2.7 20
1.56 93.41.641.671.67<0.208mg/KgPhenanthrene 98.2 50-121 5.0 20
1.28 76.61.341.671.67<0.112mg/KgPhenol 80.2 34-121 4.5 20
1.57 94.01.531.671.67<0.134mg/KgPyrene 91.6 47-127 2.5 20
0.742 44.40.7501.671.67<0.079mg/KgPyridine 44.9 10-80 1.0 20
1.21 72.41.291.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 77.2 34-118 6.4 20
1.62 97.01.471.671.67<0.096mg/Kg2,4,5-Trichlorophenol 88.0 41-124 9.7 20
1.63 97.61.491.671.67<0.096mg/Kg2,4,6-Trichlorophenol 89.2 39-126 8.9 20
98.22-Fluorobiphenyl (S)86.8 44-115
69.62-Fluorophenol (S)71.8 35-115
70.6Nitrobenzene-d5 (S)76.0 37-122
1024-Terphenyl-d14 (S)97.6 54-127
90.92,4,6-Tribromophenol (S)85.9 39-132
66.0Phenol-d5 (S)66.7 34-121
Page 34 of 39Date:12/21/2022 01:43 PM
Page 212 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L651985QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L651698
Associated Lab Samples: 94336, 94337, 94338, 94339, 94340, 94341, 94342, 94343, 94344, 94345
LRB-L651698 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/06/22 17:070.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L651698Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
99.03.964.00mg/KgChromium, Hexavalent 80-120
V 94336-DUP-L651698Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/06/22 17:392.4<0.202< 0.202mg/KgChromium, Hexavalent
V 94336-MS-L651698Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
30.7 77.339.7< 0.145mg/KgChromium, Hexavalent 75-125
Page 35 of 39Date:12/21/2022 01:43 PM
Page 213 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L652184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L651699
Associated Lab Samples: 94346, 94347, 94350
LRB-L651699 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/07/22 11:220.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L651699Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1054.194.00mg/KgChromium, Hexavalent 80-120
V 94346-DUP-L651699Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/07/22 12:160.0<0.200< 0.200mg/KgChromium, Hexavalent
V 94346-MS-L651699Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
38.6 98.939.0< 0.141mg/KgChromium, Hexavalent 75-125
Page 36 of 39Date:12/21/2022 01:43 PM
Page 214 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
Dry Weight Determination
SW-DRYWT
V27130QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94012-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/01/22 18:238.026.228.4%Moisture
V 94111-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/01/22 18:238.712.013.1%Moisture
Page 37 of 39Date:12/21/2022 01:43 PM
Page 215 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
Dry Weight Determination
SW-DRYWT
V27169QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94346-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/02/22 12:172.522.823.4%Moisture
V 94363-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/02/22 12:177.110.69.87%Moisture
Page 38 of 39Date:12/21/2022 01:43 PM
Page 216 of 220
Quality Control Data
22-334-0100Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-003
Dry Weight Determination
SW-DRYWT
V27170QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94092-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/02/22 12:440.331.030.9%Moisture
V 94093-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/02/22 12:4410.526.929.9%Moisture
Page 39 of 39Date:12/21/2022 01:43 PM
Page 217 of 220
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-334-0100
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.5 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:11/30/2022 14:09:44
Special precautions or instructions included?
Comments:
Page 218 of 220
Page 219 of 220
Page 220 of 220

Appendix D

DEQ Risk Calculators
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Shallow Soil Evaluation Area COMP-2 - Hypothetical Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
Former Press Club Cleaners
South Boulevard and Hartford Avenue, Charlotte, Meck. Co.
Division of Waste Management - Brownfields Program
25101-21-060
July 2022
May 2022 EPA RSL Table
Prepared By:Hart & Hickman, PC
2923 South Tryon Street, Suite 100, Charlotte, NC
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Shallow Soil Evaluation Area COMP-2 - Hypothetical Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Shallow Soil Evaluation Area COMP-2 - Hypothetical Worst Case
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes: CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
2.7 7440-38-2 Arsenic, Inorganic mg/kg
92.3 7440-39-3 Barium mg/kg
1.07 7440-43-9 Cadmium (Diet)mg/kg
44.56 16065-83-1 Chromium(III), Insoluble Salts mg/kg
1.67 18540-29-9 Chromium(VI)mg/kg
0.0043 J 100-41-4 Ethylbenzene mg/kg
0.178 J 132-64-9 ~Dibenzofuran mg/kg
490 7439-92-1 ~Lead and Compounds mg/kg
0.11 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
0.0459 J 78-93-3 Methyl Ethyl Ketone (2-Butanone)mg/kg
0.559 J 108-95-2 Phenol mg/kg
1.68 120-12-7 ~Anthracene mg/kg
6.44 56-55-3 ~Benz[a]anthracene mg/kg
6.32 50-32-8 ~Benzo[a]pyrene mg/kg
8.65 205-99-2 ~Benzo[b]fluoranthene mg/kg
3.05 207-08-9 ~Benzo[k]fluoranthene mg/kg
7.12 218-01-9 ~Chrysene mg/kg
0.361 J 53-70-3 ~Dibenz[a,h]anthracene mg/kg
14.3 206-44-0 ~Fluoranthene mg/kg
0.258 J 86-73-7 ~Fluorene mg/kg
3.8 193-39-5 ~Indeno[1,2,3-cd]pyrene mg/kg
0.176 J 91-20-3 ~Naphthalene mg/kg
11.1 129-00-0 ~Pyrene mg/kg
0.5 J 7782-49-2 Selenium mg/kg
0.4 J 7440-22-4 Silver mg/kg
0.0085 108-88-3 Toluene mg/kg
0.0037 J 95-63-6 Trimethylbenzene, 1,2,4-mg/kg
0.0191 1330-20-7 Xylenes mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Shallow Soil Evaluation Area COMP-2 - Hypothetical Worst Case
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 8.5E-05 6.2E-01 NO
Groundwater Use* NC NC NC
Soil 5.3E-06 4.7E-02 NO
Groundwater Use* NC NC NC
Construction Worker Soil 1.1E-06 9.0E-01 NO
Soil 4.7E-05 3.4E-01 NO
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Shallow Soil Evaluation Area COMP-2 - Hypothetical Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated Non-
Carcinogenic
Hazard
Quotient
7440-38-2 Arsenic, Inorganic 2.7 2.7 2.7 3.5E-06 4.9E-07 7.0E-11 4.0E-06 6.9E-02 8.2E-03 2.9E-06 7.7E-02
7440-39-3 Barium 92.3 92.3 92.3 5.9E-03 3.0E-06 5.9E-03
7440-43-9 Cadmium (Diet) 1.07 1.07 1.07 1.2E-11 1.2E-11 1.4E-01 1.3E-02 1.7E-06 1.5E-01
16065-83-1 Chromium(III), Insoluble Salts 44.56 44.56 44.56 3.8E-04 3.8E-04
18540-29-9 Chromium(VI) 1.67 1.67 1.67 5.5E-06 2.3E-09 5.5E-06 7.1E-03 2.7E-07 7.1E-03
100-41-4 Ethylbenzene 0.0043 0.0043 0.0043 6.8E-11 6.3E-10 7.0E-10 1.1E-06 6.8E-07 1.8E-06
132-64-9 ~Dibenzofuran 0.178 0.178 0.178 2.3E-03 2.3E-03
7439-92-1 ~Lead and Compounds 490 490 490 >SL** >SL** >SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.11 0.11 0.11 4.7E-03 5.9E-09 4.7E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.0459 0.0459 0.0459 9.8E-07 6.8E-07 1.7E-06
108-95-2 Phenol 0.559 0.559 0.559 2.4E-05 5.7E-06 4.5E-11 2.9E-05
120-12-7 ~Anthracene 1.68 1.68 1.68 7.2E-05 2.2E-05 9.4E-05
56-55-3 ~Benz[a]anthracene 6.44 6.44 6.44 4.2E-06 1.4E-06 8.1E-08 5.7E-06
50-32-8 ~Benzo[a]pyrene 6.32 6.32 6.32 4.1E-05 1.4E-05 6.3E-11 5.5E-05 2.7E-01 8.3E-02 5.1E-05 3.5E-01
205-99-2 ~Benzo[b]fluoranthene 8.65 8.65 8.65 5.6E-06 1.9E-06 8.6E-12 7.5E-06
207-08-9 ~Benzo[k]fluoranthene 3.05 3.05 3.05 2.0E-07 6.6E-08 3.0E-13 2.7E-07
218-01-9 ~Chrysene 7.12 7.12 7.12 4.6E-08 1.6E-08 7.1E-14 6.2E-08
53-70-3 ~Dibenz[a,h]anthracene 0.361 0.361 0.361 2.4E-06 7.9E-07 3.6E-12 3.1E-06
206-44-0 ~Fluoranthene 14.3 14.3 14.3 4.6E-03 1.4E-03 6.0E-03
86-73-7 ~Fluorene 0.258 0.258 0.258 8.2E-05 2.5E-05 1.1E-04
193-39-5 ~Indeno[1,2,3-cd]pyrene 3.8 3.8 3.8 2.5E-06 8.3E-07 3.8E-12 3.3E-06
91-20-3 ~Naphthalene 0.176 0.176 0.176 3.0E-08 1.1E-08 4.3E-08 8.5E-08 1.1E-04 3.5E-05 1.1E-03 1.3E-03
129-00-0 ~Pyrene 11.1 11.1 11.1 4.7E-03 1.5E-03 6.2E-03
7782-49-2 Selenium 0.5 0.5 0.5 1.3E-03 4.0E-10 1.3E-03
7440-22-4 Silver 0.4 0.4 0.4 1.0E-03 1.0E-03
108-88-3 Toluene 0.0085 0.0085 0.0085 1.4E-06 3.6E-07 1.7E-06
95-63-6 Trimethylbenzene, 1,2,4- 0.0037 0.0037 0.0037 4.7E-06 7.0E-06 1.2E-05
1330-20-7 Xylenes 0.0191 0.0191 0.0191 1.2E-06 3.0E-05 3.1E-05
Cumulative: 8.5E-05 6.2E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Shallow Soil Evaluation Area COMP-2 - Hypothetical Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
7440-38-2 Arsenic, Inorganic 2.7 2.7 2.7 7.4E-07 1.6E-07 1.6E-11 9.0E-07 4.6E-03 9.8E-04 6.9E-07 5.6E-03
7440-39-3 Barium 92.3 92.3 92.3 4.0E-04 7.1E-07 4.0E-04
7440-43-9 Cadmium (Diet) 1.07 1.07 1.07 2.6E-12 2.6E-12 9.2E-03 1.6E-03 4.1E-07 1.1E-02
16065-83-1 Chromium(III), Insoluble Salts 44.56 44.56 44.56 2.5E-05 2.5E-05
18540-29-9 Chromium(VI) 1.67 1.67 1.67 2.6E-07 1.9E-10 2.6E-07 4.8E-04 6.4E-08 4.8E-04
100-41-4 Ethylbenzene 0.0043 0.0043 0.0043 1.4E-11 1.5E-10 1.6E-10 7.4E-08 1.6E-07 2.4E-07
132-64-9 ~Dibenzofuran 0.178 0.178 0.178 1.5E-04 1.5E-04
7439-92-1 ~Lead and Compounds 490 490 490 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.11 0.11 0.11 3.1E-04 1.4E-09 3.1E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.0459 0.0459 0.0459 6.5E-08 1.6E-07 2.3E-07
108-95-2 Phenol 0.559 0.559 0.559 1.6E-06 6.8E-07 1.1E-11 2.3E-06
120-12-7 ~Anthracene 1.68 1.68 1.68 4.8E-06 2.6E-06 7.4E-06
56-55-3 ~Benz[a]anthracene 6.44 6.44 6.44 2.0E-07 1.1E-07 6.7E-09 3.1E-07
50-32-8 ~Benzo[a]pyrene 6.32 6.32 6.32 1.9E-06 1.1E-06 5.2E-12 3.0E-06 1.8E-02 9.9E-03 1.2E-05 2.8E-02
205-99-2 ~Benzo[b]fluoranthene 8.65 8.65 8.65 2.6E-07 1.5E-07 7.1E-13 4.1E-07
207-08-9 ~Benzo[k]fluoranthene 3.05 3.05 3.05 9.3E-09 5.1E-09 2.5E-14 1.4E-08
218-01-9 ~Chrysene 7.12 7.12 7.12 2.2E-09 1.2E-09 5.9E-15 3.4E-09
53-70-3 ~Dibenz[a,h]anthracene 0.361 0.361 0.361 1.1E-07 6.1E-08 3.0E-13 1.7E-07
206-44-0 ~Fluoranthene 14.3 14.3 14.3 3.1E-04 1.7E-04 4.7E-0486-73-7 ~Fluorene 0.258 0.258 0.258 5.5E-06 3.0E-06 8.6E-06
193-39-5 ~Indeno[1,2,3-cd]pyrene 3.8 3.8 3.8 1.2E-07 6.4E-08 3.1E-13 1.8E-07
91-20-3 ~Naphthalene 0.176 0.176 0.176 6.5E-09 3.6E-09 9.9E-09 2.0E-08 7.5E-06 4.1E-06 2.7E-04 2.8E-04
129-00-0 ~Pyrene 11.1 11.1 11.1 3.2E-04 1.7E-04 4.9E-04
7782-49-2 Selenium 0.5 0.5 0.5 8.6E-05 9.6E-11 8.6E-05
7440-22-4 Silver 0.4 0.4 0.4 6.8E-05 6.8E-05
108-88-3 Toluene 0.0085 0.0085 0.0085 9.1E-08 8.5E-08 1.8E-07
95-63-6 Trimethylbenzene, 1,2,4- 0.0037 0.0037 0.0037 3.2E-07 1.7E-06 2.0E-06
1330-20-7 Xylenes 0.0191 0.0191 0.0191 8.2E-08 7.1E-06 7.2E-06
Cumulative: 5.3E-06 4.7E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Shallow Soil Evaluation Area COMP-2 - Hypothetical Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
7440-38-2 Arsenic, Inorganic 2.7 2.7 2.7 9.8E-08 1.6E-08 3.6E-08 1.5E-07 1.6E-02 2.6E-03 4.0E-02 5.9E-02
7440-39-3 Barium 92.3 92.3 92.3 1.4E-03 4.1E-03 5.5E-03
7440-43-9 Cadmium (Diet) 1.07 1.07 1.07 5.9E-09 5.9E-09 6.3E-03 8.1E-04 2.4E-02 3.1E-02
16065-83-1 Chromium(III), Insoluble Salts 44.56 44.56 44.56 8.8E-05 2.0E-03 2.1E-03
18540-29-9 Chromium(VI) 1.67 1.67 1.67 3.4E-08 4.3E-07 4.7E-07 9.8E-04 1.3E-03 2.2E-03
100-41-4 Ethylbenzene 0.0043 0.0043 0.0043 1.9E-12 2.8E-11 2.9E-11 2.5E-07 8.9E-08 3.4E-07
132-64-9 ~Dibenzofuran 0.178 0.178 0.178 1.3E-04 1.3E-04
7439-92-1 ~Lead and Compounds 490 490 490 <SL** <SL** <SL**7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.11 0.11 0.11 1.6E-04 8.2E-05 2.4E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.0459 0.0459 0.0459 6.8E-08 4.0E-06 4.1E-06
108-95-2 Phenol 0.559 0.559 0.559 2.7E-06 8.8E-07 6.3E-07 4.3E-06
120-12-7 ~Anthracene 1.68 1.68 1.68 5.0E-06 2.1E-06 7.0E-06
56-55-3 ~Benz[a]anthracene 6.44 6.44 6.44 2.6E-08 1.1E-08 2.5E-09 3.9E-08
50-32-8 ~Benzo[a]pyrene 6.32 6.32 6.32 2.6E-07 1.1E-07 1.2E-08 3.7E-07 6.2E-02 2.6E-02 7.1E-01 8.0E-01
205-99-2 ~Benzo[b]fluoranthene 8.65 8.65 8.65 3.5E-08 1.5E-08 1.6E-09 5.1E-08
207-08-9 ~Benzo[k]fluoranthene 3.05 3.05 3.05 1.2E-09 5.1E-10 5.6E-11 1.8E-09
218-01-9 ~Chrysene 7.12 7.12 7.12 2.9E-10 1.2E-10 1.3E-11 4.2E-10
53-70-3 ~Dibenz[a,h]anthracene 0.361 0.361 0.361 1.5E-08 6.1E-09 6.7E-10 2.1E-08
206-44-0 ~Fluoranthene 14.3 14.3 14.3 4.2E-04 1.8E-04 6.0E-04
86-73-7 ~Fluorene 0.258 0.258 0.258 1.9E-06 7.9E-07 2.7E-06
193-39-5 ~Indeno[1,2,3-cd]pyrene 3.8 3.8 3.8 1.5E-08 6.4E-09 7.0E-10 2.2E-08
91-20-3 ~Naphthalene 0.176 0.176 0.176 8.5E-10 3.6E-10 1.9E-09 3.1E-09 8.6E-07 3.6E-07 1.4E-03 1.4E-03
129-00-0 ~Pyrene 11.1 11.1 11.1 1.1E-04 4.5E-05 1.5E-04
7782-49-2 Selenium 0.5 0.5 0.5 2.9E-04 5.6E-06 3.0E-04
7440-22-4 Silver 0.4 0.4 0.4 2.4E-04 2.4E-04108-88-3 Toluene 0.0085 0.0085 0.0085 3.1E-08 4.2E-07 4.5E-07
95-63-6 Trimethylbenzene, 1,2,4- 0.0037 0.0037 0.0037 2.7E-07 2.5E-06 2.8E-06
1330-20-7 Xylenes 0.0191 0.0191 0.0191 1.4E-07 8.8E-06 9.0E-06
Cumulative: 1.1E-06 9.0E-01
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg
for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Recreator/Trespasser Soil Output Form 2F
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Shallow Soil Evaluation Area COMP-2 - Hypothetical Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
Receptor Type: Trespasser
CAS # Chemical Name:
Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
7440-38-2 Arsenic, Inorganic 2.7 2.7 2.7 1.9E-06 2.7E-07 3.2E-12 2.2E-06 3.8E-02 4.6E-03 1.4E-07 4.3E-02
7440-39-3 Barium 92.3 92.3 92.3 3.3E-03 1.4E-07 3.3E-03
7440-43-9 Cadmium (Diet) 1.07 1.07 1.07 5.4E-13 5.4E-13 7.6E-02 7.2E-03 8.0E-08 8.3E-02
16065-83-1 Chromium(III), Insoluble Salts 44.56 44.56 44.56 2.1E-04 2.1E-04
18540-29-9 Chromium(VI) 1.67 1.67 1.67 3.0E-06 1.1E-10 3.0E-06 4.0E-03 1.3E-08 4.0E-03
100-41-4 Ethylbenzene 0.0043 0.0043 0.0043 3.8E-11 2.9E-11 6.7E-11 6.1E-07 3.2E-08 6.4E-07
132-64-9 ~Dibenzofuran 0.178 0.178 0.178 1.3E-03 1.3E-03
7439-92-1 ~Lead and Compounds 490 490 490 >SL** >SL** >SL**7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.11 0.11 0.11 2.6E-03 2.8E-10 2.6E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.0459 0.0459 0.0459 5.4E-07 3.1E-08 5.8E-07
108-95-2 Phenol 0.559 0.559 0.559 1.3E-05 3.1E-06 2.1E-12 1.6E-05
120-12-7 ~Anthracene 1.68 1.68 1.68 4.0E-05 1.2E-05 5.2E-05
56-55-3 ~Benz[a]anthracene 6.44 6.44 6.44 2.3E-06 7.8E-07 3.8E-09 3.1E-06
50-32-8 ~Benzo[a]pyrene 6.32 6.32 6.32 2.3E-05 7.7E-06 2.9E-12 3.1E-05 1.5E-01 4.6E-02 2.4E-06 2.0E-01
205-99-2 ~Benzo[b]fluoranthene 8.65 8.65 8.65 3.1E-06 1.1E-06 4.0E-13 4.2E-06
207-08-9 ~Benzo[k]fluoranthene 3.05 3.05 3.05 1.1E-07 3.7E-08 1.4E-14 1.5E-07
218-01-9 ~Chrysene 7.12 7.12 7.12 2.6E-08 8.6E-09 3.3E-15 3.5E-08
53-70-3 ~Dibenz[a,h]anthracene 0.361 0.361 0.361 1.3E-06 4.4E-07 1.7E-13 1.8E-06
206-44-0 ~Fluoranthene 14.3 14.3 14.3 2.5E-03 7.9E-04 3.3E-03
86-73-7 ~Fluorene 0.258 0.258 0.258 4.6E-05 1.4E-05 6.0E-05
193-39-5 ~Indeno[1,2,3-cd]pyrene 3.8 3.8 3.8 1.4E-06 4.6E-07 1.8E-13 1.8E-06
91-20-3 ~Naphthalene 0.176 0.176 0.176 1.7E-08 6.2E-09 2.0E-09 2.5E-08 6.3E-05 1.9E-05 5.3E-05 1.3E-04
129-00-0 ~Pyrene 11.1 11.1 11.1 2.6E-03 8.1E-04 3.4E-03
7782-49-2 Selenium 0.5 0.5 0.5 7.1E-04 1.9E-11 7.1E-04
7440-22-4 Silver 0.4 0.4 0.4 5.7E-04 5.7E-04108-88-3 Toluene 0.0085 0.0085 0.0085 7.6E-07 1.7E-08 7.7E-07
95-63-6 Trimethylbenzene, 1,2,4- 0.0037 0.0037 0.0037 2.6E-06 3.3E-07 3.0E-06
1330-20-7 Xylenes 0.0191 0.0191 0.0191 6.8E-07 1.4E-06 2.1E-06
Cumulative: 4.7E-05 3.4E-01
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400
mg/kg for residential soil.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
In Situ Evaluation Area EX-2
North Carolina Department of Environmental Quality
Risk Calculator
Former Press Club Cleaners
South Boulevard and Hartford Avenue, Charlotte, Meck. Co.
Division of Waste Management - Brownfields Program
25101-21-060
July 2022
May 2022 EPA RSL Table
Prepared By:Hart & Hickman, PC
2923 South Tryon Street, Suite 100, Charlotte, NC
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: In Situ Evaluation Area EX-2
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: In Situ Evaluation Area EX-2
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes: CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
0.011 J 67-64-1 Acetone mg/kg
15.4 7440-38-2 Arsenic, Inorganic mg/kg
178 7440-39-3 Barium mg/kg
17.9 7440-43-9 Cadmium (Diet)mg/kg
92.1 16065-83-1 Chromium(III), Insoluble Salts mg/kg
0.001 J 110-54-3 Hexane, N-mg/kg
2640 7439-92-1 ~Lead and Compounds mg/kg
0.194 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
1.48 J 7782-49-2 Selenium mg/kg
4.62 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: In Situ Evaluation Area EX-2
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 2.3E-05 3.0E+00 YES
Groundwater Use* NC NC NC
Soil 5.1E-06 2.1E-01 NO
Groundwater Use* NC NC NC
Construction Worker Soil 9.5E-07 8.8E-01 NO
Soil 1.3E-05 1.7E+00 YES
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: In Situ Evaluation Area EX-2
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.011 0.011 0.011 1.6E-07 1.6E-07
7440-38-2 Arsenic, Inorganic 15.4 15.4 15.4 2.0E-05 2.8E-06 4.0E-10 2.3E-05 3.9E-01 4.7E-02 1.7E-05 4.4E-01
7440-39-3 Barium 178 178 178 1.1E-02 5.8E-06 1.1E-02
7440-43-9 Cadmium (Diet) 17.9 17.9 17.9 1.9E-10 1.9E-10 2.3E+00 2.2E-01 2.9E-05 2.5E+00
16065-83-1 Chromium(III), Insoluble Salts 92.1 92.1 92.1 7.9E-04 7.9E-04
110-54-3 Hexane, N- 0.001 0.001 0.001 4.4E-07 4.4E-07
7439-92-1 ~Lead and Compounds 2640 2640 2640 >SL** >SL** >SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.194 0.194 0.194 8.3E-03 1.0E-08 8.3E-03
7782-49-2 Selenium 1.48 1.48 1.48 3.8E-03 1.2E-09 3.8E-03
7440-22-4 Silver 4.62 4.62 4.62 1.2E-02 1.2E-02
Cumulative: 2.3E-05 3.0E+00
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: In Situ Evaluation Area EX-2
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.011 0.011 0.011 1.0E-08 1.0E-08
7440-38-2 Arsenic, Inorganic 15.4 15.4 15.4 4.2E-06 9.0E-07 9.1E-11 5.1E-06 2.6E-02 5.6E-03 4.0E-06 3.2E-02
7440-39-3 Barium 178 178 178 7.6E-04 1.4E-06 7.6E-04
7440-43-9 Cadmium (Diet) 17.9 17.9 17.9 4.4E-11 4.4E-11 1.5E-01 2.6E-02 6.9E-06 1.8E-01
16065-83-1 Chromium(III), Insoluble Salts 92.1 92.1 92.1 5.3E-05 5.3E-05
110-54-3 Hexane, N- 0.001 0.001 0.001 1.0E-07 1.0E-07
7439-92-1 ~Lead and Compounds 2640 2640 2640 >SL** >SL** >SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.194 0.194 0.194 5.5E-04 2.5E-09 5.5E-04
7782-49-2 Selenium 1.48 1.48 1.48 2.5E-04 2.8E-10 2.5E-04
7440-22-4 Silver 4.62 4.62 4.62 7.9E-04 7.9E-04
Cumulative: 5.1E-06 2.1E-01
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: In Situ Evaluation Area EX-2
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.011 0.011 0.011 3.2E-08 3.2E-08
7440-38-2 Arsenic, Inorganic 15.4 15.4 15.4 5.6E-07 9.0E-08 2.0E-07 8.5E-07 9.1E-02 1.5E-02 2.3E-01 3.4E-01
7440-39-3 Barium 178 178 178 2.6E-03 8.0E-03 1.1E-02
7440-43-9 Cadmium (Diet) 17.9 17.9 17.9 9.9E-08 9.9E-08 1.1E-01 1.4E-02 4.0E-01 5.2E-01
16065-83-1 Chromium(III), Insoluble Salts 92.1 92.1 92.1 1.8E-04 4.1E-03 4.3E-03
110-54-3 Hexane, N- 0.001 0.001 0.001 9.8E-09 6.4E-07 6.5E-07
7439-92-1 ~Lead and Compounds 2640 2640 2640 >SL** >SL** >SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.194 0.194 0.194 2.9E-04 1.5E-04 4.3E-04
7782-49-2 Selenium 1.48 1.48 1.48 8.7E-04 1.7E-05 8.9E-04
7440-22-4 Silver 4.62 4.62 4.62 2.7E-03 2.7E-03
Cumulative: 9.5E-07 8.8E-01
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg
for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Recreator/Trespasser Soil Output Form 2F
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: In Situ Evaluation Area EX-2
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
Receptor Type: Trespasser
CAS # Chemical Name:
Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.011 0.011 0.011 8.7E-08 8.7E-08
7440-38-2 Arsenic, Inorganic 15.4 15.4 15.4 1.1E-05 1.6E-06 1.8E-11 1.3E-05 2.2E-01 2.6E-02 7.7E-07 2.5E-01
7440-39-3 Barium 178 178 178 6.3E-03 2.7E-07 6.3E-03
7440-43-9 Cadmium (Diet) 17.9 17.9 17.9 9.0E-12 9.0E-12 1.3E+00 1.2E-01 1.3E-06 1.4E+00
16065-83-1 Chromium(III), Insoluble Salts 92.1 92.1 92.1 4.4E-04 4.4E-04
110-54-3 Hexane, N- 0.001 0.001 0.001 2.0E-08 2.0E-08
7439-92-1 ~Lead and Compounds 2640 2640 2640 >SL** >SL** >SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.194 0.194 0.194 4.6E-03 4.9E-10 4.6E-03
7782-49-2 Selenium 1.48 1.48 1.48 2.1E-03 5.6E-11 2.1E-03
7440-22-4 Silver 4.62 4.62 4.62 6.6E-03 6.6E-03
Cumulative: 1.3E-05 1.7E+00
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400
mg/kg for residential soil.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Export Sections EX-1, EX-3, EX-4, and EX-5 - Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
Former Press Club Cleaners
South Boulevard and Hartford Avenue, Charlotte, Meck. Co.
Division of Waste Management - Brownfields Program
25101-21-060
July 2022
May 2022 EPA RSL Table
Prepared By:Hart & Hickman, PC
2923 South Tryon Street, Suite 100, Charlotte, NC
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Export Sections EX-1, EX-3, EX-4, and EX-5 - Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Export Sections EX-1, EX-3, EX-4, and EX-5 - Worst Case
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes: CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
0.021 J 67-64-1 Acetone mg/kg
3.43 7440-38-2 Arsenic, Inorganic mg/kg
89.8 7440-39-3 Barium mg/kg
0.45 J 7440-43-9 Cadmium (Diet)mg/kg
97.2 16065-83-1 Chromium(III), Insoluble Salts mg/kg
1.74 18540-29-9 Chromium(VI)mg/kg
142 7439-92-1 ~Lead and Compounds mg/kg
0.14 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
1.48 J 7782-49-2 Selenium mg/kg
0.205 J 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Export Sections EX-1, EX-3, EX-4, and EX-5 - Worst Case
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 1.1E-05 1.9E-01 NO
Groundwater Use* NC NC NC
Soil 1.4E-06 1.3E-02 NO
Groundwater Use* NC NC NC
Construction Worker Soil 6.8E-07 1.0E-01 NO
Soil 6.0E-06 1.0E-01 NO
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Export Sections EX-1, EX-3, EX-4, and EX-5 - Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.021 0.021 0.021 3.0E-07 3.0E-07
7440-38-2 Arsenic, Inorganic 3.43 3.43 3.43 4.4E-06 6.2E-07 8.9E-11 5.1E-06 8.8E-02 1.0E-02 3.7E-06 9.8E-02
7440-39-3 Barium 89.8 89.8 89.8 5.7E-03 2.9E-06 5.7E-03
7440-43-9 Cadmium (Diet) 0.45 0.45 0.45 4.9E-12 4.9E-12 5.8E-02 5.5E-03 7.3E-07 6.3E-02
16065-83-1 Chromium(III), Insoluble Salts 97.2 97.2 97.2 8.3E-04 8.3E-04
18540-29-9 Chromium(VI) 1.74 1.74 1.74 5.7E-06 2.4E-09 5.7E-06 7.4E-03 2.8E-07 7.4E-03
7439-92-1 ~Lead and Compounds 142 142 142 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.14 0.14 0.14 6.0E-03 7.5E-09 6.0E-03
7782-49-2 Selenium 1.48 1.48 1.48 3.8E-03 1.2E-09 3.8E-03
7440-22-4 Silver 0.205 0.205 0.205 5.2E-04 5.2E-04
Cumulative: 1.1E-05 1.9E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Export Sections EX-1, EX-3, EX-4, and EX-5 - Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.021 0.021 0.021 2.0E-08 2.0E-08
7440-38-2 Arsenic, Inorganic 3.43 3.43 3.43 9.4E-07 2.0E-07 2.0E-11 1.1E-06 5.9E-03 1.2E-03 8.8E-07 7.1E-03
7440-39-3 Barium 89.8 89.8 89.8 3.8E-04 6.9E-07 3.9E-04
7440-43-9 Cadmium (Diet) 0.45 0.45 0.45 1.1E-12 1.1E-12 3.9E-03 6.5E-04 1.7E-07 4.5E-03
16065-83-1 Chromium(III), Insoluble Salts 97.2 97.2 97.2 5.5E-05 5.5E-05
18540-29-9 Chromium(VI) 1.74 1.74 1.74 2.7E-07 2.0E-10 2.7E-07 5.0E-04 6.7E-08 5.0E-04
7439-92-1 ~Lead and Compounds 142 142 142 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.14 0.14 0.14 4.0E-04 1.8E-09 4.0E-04
7782-49-2 Selenium 1.48 1.48 1.48 2.5E-04 2.8E-10 2.5E-04
7440-22-4 Silver 0.205 0.205 0.205 3.5E-05 3.5E-05
Cumulative: 1.4E-06 1.3E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Export Sections EX-1, EX-3, EX-4, and EX-5 - Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.021 0.021 0.021 6.2E-08 6.2E-08
7440-38-2 Arsenic, Inorganic 3.43 3.43 3.43 1.2E-07 2.0E-08 4.5E-08 1.9E-07 2.0E-02 3.2E-03 5.1E-02 7.5E-02
7440-39-3 Barium 89.8 89.8 89.8 1.3E-03 4.0E-03 5.4E-03
7440-43-9 Cadmium (Diet) 0.45 0.45 0.45 2.5E-09 2.5E-09 2.7E-03 3.4E-04 1.0E-02 1.3E-02
16065-83-1 Chromium(III), Insoluble Salts 97.2 97.2 97.2 1.9E-04 4.4E-03 4.6E-03
18540-29-9 Chromium(VI) 1.74 1.74 1.74 3.5E-08 4.5E-07 4.8E-07 1.0E-03 1.3E-03 2.3E-03
7439-92-1 ~Lead and Compounds 142 142 142 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.14 0.14 0.14 2.1E-04 1.0E-04 3.1E-04
7782-49-2 Selenium 1.48 1.48 1.48 8.7E-04 1.7E-05 8.9E-04
7440-22-4 Silver 0.205 0.205 0.205 1.2E-04 1.2E-04
Cumulative: 6.8E-07 1.0E-01
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg
for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Recreator/Trespasser Soil Output Form 2F
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: 25101-21-060
Exposure Unit ID: Export Sections EX-1, EX-3, EX-4, and EX-5 - Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
Receptor Type: Trespasser
CAS # Chemical Name:
Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.021 0.021 0.021 1.7E-07 1.7E-07
7440-38-2 Arsenic, Inorganic 3.43 3.43 3.43 2.5E-06 3.5E-07 4.1E-12 2.8E-06 4.9E-02 5.8E-03 1.7E-07 5.5E-02
7440-39-3 Barium 89.8 89.8 89.8 3.2E-03 1.3E-07 3.2E-03
7440-43-9 Cadmium (Diet) 0.45 0.45 0.45 2.3E-13 2.3E-13 3.2E-02 3.0E-03 3.4E-08 3.5E-02
16065-83-1 Chromium(III), Insoluble Salts 97.2 97.2 97.2 4.6E-04 4.6E-04
18540-29-9 Chromium(VI) 1.74 1.74 1.74 3.2E-06 1.1E-10 3.2E-06 4.1E-03 1.3E-08 4.1E-03
7439-92-1 ~Lead and Compounds 142 142 142 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.14 0.14 0.14 3.3E-03 3.5E-10 3.3E-03
7782-49-2 Selenium 1.48 1.48 1.48 2.1E-03 5.6E-11 2.1E-03
7440-22-4 Silver 0.205 0.205 0.205 2.9E-04 2.9E-04
Cumulative: 6.0E-06 1.0E-01
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400
mg/kg for residential soil.
North Carolina DEQ Risk Calculator

Appendix E

Comparison of Detected Metals in Uncontaminated Export to LCID Background Data
Appendix E
Comparison of Detected Metals in Uncontaminated Export to LCID Background Data
Former Press Club Cleaners
Charlotte, North Carolina
Brownfields Project No. 25101-21-060
H&H Job No. TCR-003
Former Press Club Cleaners
(25101-21-060)2
Reeve’s LCID
(60S-LCID)3
Old 27 LCID
(36A-LCID)4
Range
VOCs (8260D)
Acetone 25 14,000 210,000 --0.021J NA NA
n-Hexane 55 160 740 --0.001 J NA NA
SVOCs (8270E)-- -- -- -- ALL BDL NA NA
Metals (6020B/6010/7471B/7199)
Arsenic 5.8 0.68 3.0 1.0 - 18 3.43 3.0 2.7
Barium 580 3,100 47,000 50 - 1,000 89.8 150 220
Cadmium 3.0 1.4 20 1.0 - 10 0.450 J 0.13 J <0.051
Chromium (Total) NE NE NE 7.0 - 300 97.2 58 90
Chromium (III)360,000 23,000 350,000 NS 97.2 57.76 90
Chromium (VI) 3.8 0.31 6.5 NS 1.74 0.43 J 2.0
Lead 270 400 800 ND - 50 142 29 18
Mercury 1.0 2.3 9.7 0.03 - 0.52 0.140 0.097 0.074
Selenium 2.1 78 1,200 <0.1 - 0.8 1.48 J 6.4 4.1
Silver 3.4 78 1,200 ND - 5.0 0.205 J 0.54 J <0.071
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022.
2) Highest detected concentrations for in situ soil samples EX-1, EX-3, EX-4, and EX-5 collected by Hart & Hickman, PC (H&H) on November 28 and 29, 2022.
3) Reeve's LCID data were obtained from Table 2 of the Soil Management Options Letter prepared for DEQ by H&H on August 7, 2020.
4) Old 27 LCID data were obtained from Table 2 of the Background Soil Assessment Report prepared for DEQ by H&H on May 11, 2021.
Compound concentrations reported to the laboratory method detection limits.
Compound concentrations are reported in milligrams per kilograms (mg/kg).
Bold indicates concentration exceeds Residential PSRGs and background metals concentrations.
ND = not detected; NA = not analyzed; -- = not applicable; NS = not specified; BDL = below laboratory method detection limits
J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.
Regional Background Metals
(2)
Constituent
PSRGs
Protection of Groundwater (1)
(mg/kg)
Residential (1)
(mg/kg)
Industrial/Commercial (1)
(mg/kg)
Highest Concentration at
Receiving Site (mg/kg)
Highest Concentration for
Proposed Beneficial Fill Export
(mg/kg)
Highest Concentration at
Receiving Site (mg/kg)
File:https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Trammell Crow Residential - TCR/TCR-003 Press Club Cleaners/Brownfields/In Situ/Report/Data Tables_Press Club Cleaners Data Tables_Press Club Cleaners
Appendix E (Page 1 of 1)
Hart & Hickman, PC