25036_Clariant Corp_Brownfields Assessment Report_20220517

BROWNFIELDS ASSESSMENT REPORT & RECEPTOR SURVEY

CLARIANT CORPORATION SITE
4000 MONROE ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
BROWNFIELDS PROJECT ID. 25036-21-060

ECS PROJECT NO. 49:12929-D
PREPARED FOR
PARKSIDE PARTNERS

May 17, 2022
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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

TABLE OF CONTENTS
1.0 PROJECT INFORMATION ................................................................................................................... 1
2.0 PREVIOUS INVESTIGATIONS .............................................................................................................. 4
3.0 OBJECTIVE OF THE ASSESSMENT ...................................................................................................... 4
4.0 FIELD ACTIVITIES ............................................................................................................................... 5
4.1 Utility Locate ..................................................................................................................................... 5
4.2 Monitoring Well Evaluation .............................................................................................................. 5
4.3 Soil Samples ....................................................................................................................................... 5
4.4 Indoor Air Samples ............................................................................................................................ 6
4.5 Sub-Slab Soil Gas Samples ................................................................................................................. 6
5.0 RESULTS............................................................................................................................................. 7
5.1 Monitoring Well Evaluation Results .................................................................................................. 7
5.2 Soil Boring Soil Analysis ..................................................................................................................... 8
5.3 Indoor Air Analysis ............................................................................................................................ 8
5.4 Sub-Slab Soil Gas Soil Analysis ........................................................................................................... 9
5.5 Brownfields Receptor Survey ............................................................................................................ 9
5.6 Investigative Derived Waste ............................................................................................................. 9
6.0 CONCLUSIONS AND DISCUSSION .................................................................................................... 10
7.0 DEVIATIONS FROM WORK PLAN ..................................................................................................... 11

FIGURES

Figure 1 USGS Topographic Map
Figure 2 Groundwater Sample Locations Map
Figure 3 Sub-Slab Soil Gas Sample Locations Map
Figure 4 Soil Sample Locations Map
Figure 5 Indoor Air Sample Locations Map

TABLES

Table 1 Summary of Soil Samples Analytical Results
Table 2 Summary of Indoor Air Samples Analytical Results
Table 3 Summary of Sub-Slab Soil Gas Samples Analytical Results

APPENDICIES

Appendix A Field Sampling Notes
Appendix B Laboratory Analytical Reports and Chains-of-Custody
Appendix C Safety Data Sheets
Appendix D NCDEQ Risk Calculator Output
Appendix E Brownfields Receptor Survey Form and Figures
Appendix F Floor Plans
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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

1.0 PROJECT INFORMATION

The subject property is located at 4000 Monroe Road in Charlotte, Mecklenburg County, North Carolina
(Figure 1). According to the Mecklenburg County Online Geographic Information Systems website, the
subject property is identified as Parcel Identification Number (PIN) 15904612 and was owned by Clariant
Corporation (Demerger)/Alisa Bradshaw. The approximately 9.799-acre subject property was developed
with Clariant Corporation, a specialty chemical company. The subject property is developed with an
approximate 92,780-square foot building that is subdivided into Buildings 1-4 that were reportedly
constructed in 1956; an approximate 75,606-square foot building designated as Building 5 that was
reportedly constructed in 1956; an approximately 391-square foot building designated as Building 6 that
was reportedly constructed in 1994; and an approximate 100-aquare foot structure designated as Building
7. ECS previously completed a Phase I Environmental Site Assessment (ESA) on the property for Parkside
Partners/4000 Monroe, LLC, as documented in the report dated January 15, 2021, ECS Project Number
49:12929. The ESA identified the following recognized environmental conditions (RECs):
• Based on a history of industrial and fueling operations of this facility, the use of chemicals, and
the potential for an undocumented release that could impact the subject property, ECS
considered the historic and current use of the site to represent a REC.
• ECS considered the potential for a release from the wastewater treatment activities in Building 6
which was constructed in 1996 and associated piping to represent a REC.
• Based on the lack of closure documentation and the potential for an undocumented release at
the subject property to impact subsurface conditions, ECS considered four former 4,000-gallon
gasoline underground storage tanks (USTs) to represent a REC.
• ECS considered the potential for additional orphan USTs associated with the former gasoline
station on the northwestern portion of the property that operated from around 1962 to 1993 to
represent a REC.
• Based on distance, measured groundwater flow towards the subject property, and documented
impacts to groundwater above regulatory standards, ECS considered the incident associated with
the former gasoline station that operated on the northeast adjoining property from around 1983-
2005 to represent a REC.
• Based on measured groundwater flow towards the subject property and documented impacts to
groundwater in close proximity to the subject property, ECS considered the potential for
chlorinated solvents to have migrated from the east adjoining Takatori facility to represent a REC.
• ECS considers the documented tetrachloroethene (PCE) impacts in groundwater above regulatory
standards during a Phase II ESA at the north adjacent property in 2019 to represent a REC.
• Based on length of service from approximately 1969 to 1994 and the potential for an
undocumented release that could impact the subject property, ECS considers the former
operation of the north adjacent dry-cleaning facility to represent a REC.

In an effort to determine if the subject property had been adversely affected by the identified RECs, ECS
conducted an initial limited environmental assessment at the site as detailed in ECS’s Report of
Environmental Assessment Services (ECS Project No.: 49:12929-A, submitted March 12, 2021).

This initial limited environmental assessment included the following:

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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

• ECS observed the performance of a ground penetrating radar (GPR) survey of the area where a
former gasoline station and three 550-gallon underground storage tanks (USTs) were located in
the northwest corner of the subject property. The results of the GPR survey did not indicate the
presence of any remaining USTs in this area.
• 17 borings (GW-1 through GW-17) were advanced at the site at the locations shown on Figure 2
for the collection of groundwater samples. Refusal was encountered in borings GW-11 (18 feet
below ground surface or ft-bgs) and GW-15 (12 ft-bgs) prior to encountering groundwater.
Groundwater samples were collected from the remaining borings. Review of the laboratory
analytical results for the groundwater samples collected indicated one or more volatile organic
compounds (VOCs) in the samples collected from borings GW-1, GW-2, GW-4 through GW-7, GW-
12, GW-13, GW-16, and GW-17 at concentrations greater than the laboratory method detection
limits. Benzene in the sample collected from GW-13, methyl tert-butyl ether in the samples
collected from GW-12 and GW-13, and tetrachloroethene (also known as perchloroethene or PCE)
in the samples collected from GW-1, GW-2, GW-5, GW-13, GW-16, and GW-17 were detected at
concentrations greater than the North Carolina 2L Groundwater Quality Standards (NC2LGWQS).
In addition, the concentrations of benzene in the sample collected from GW-13 and PCE in the
samples collected from GW-2, GW-5, GW-13, and GW-17 were detected greater than the NCDEQ
Non-Residential Groundwater Vapor Intrusion Screening Level (VISL). Based on the anticipated
groundwater flow direction and the compound concentrations detected in the groundwater
samples collected, it appears the groundwater impacts may have originated from off-site sources.
• 12 sub-slab soil gas sample points (SG-A through SG-K) were installed beneath the interior of the
structures on the subject site. The approximate locations of these soil gas samples are shown on
Figure 3. Review of the laboratory analytical results for the samples collected from the sub-slab
sample points indicated several VOCs at concentrations greater than the laboratory method
detection limits in each of the sub-slab samples collected as part of this investigation. The
concentration of chloroform detected in the SG-A sample was present greater than its NCDEQ
Non-Residential Sub-Slab and Exterior Soil Gas VISL. Chloroform is present in municipally supplied
water and is often detected due to leaks in municipal water lines. As chloroform was detected at
a concentration greater than its VISL in the SG-A sample and more than five compounds with non-
cancer effects were detected at concentrations greater than the laboratory method reporting
limits in each of the sub-slab soil gas samples collected as part of this investigation, ECS input the
laboratory analytical results of each sub-slab soil gas sample collected in to the NCDEQ Risk
Calculator. Based on the results of the NCDEQ Risk Calculator, the concentrations in the sub-slab
soil gas samples did not exceed the risk thresholds.

Based upon the results above, Parkside Partners/4000 Monroe, LLC requested additional assessment
activities. ECS prepared a proposal (ECS Proposal No.: 49:23603P, approved April 8, 2021) for the
collection of soil samples, additional groundwater samples, and additional sub-slab soil gas samples. In
addition, ECS was requested to include the collection of groundwater elevation data for the estimation of
groundwater flow direction beneath the site.

ECS submitted the Report of Additional Environmental Assessment Services (ECS Project No. 49:12929-B)
on May 6, 2021, documenting the additional assessment services. This additional environmental
assessment included the following:

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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

• Eight soil borings (B-1 through B-4, SB-1A, SB-2A, SB-13A, and SB-18) were advanced at the site
for the collection of soil samples for laboratory analysis. The locations of the soil borings are
indicated on Figure 4. Review of the laboratory analytical results for the soil samples collected
did not indicate compounds at concentrations greater than the laboratory method reporting
limits in any of the soil samples collected at the site.
• Three temporary monitoring wells (GW-5A, GW-16A, and GW-17A) were installed along the
northern property boundary to further assess site groundwater. In addition, between May 10 and
11, 2021, temporary monitoring wells GW-1A, GW-2A, GW-13A, and GW-18 were installed in soil
borings SB-1A, SB-2A, SB-13A, and SB-18, respectively. The locations of the temporary monitoring
wells are shown on Figure 2. Review of the laboratory analytical results for the groundwater
samples collected indicated concentrations of PCE in the GW-1A, GW-2A, GW-13A, GW-17A, and
GW-18 samples at concentrations greater than its NC2LGWQS, including the concentrations in the
GW-13A and GW-17A samples which were greater than its Non-Residential Groundwater VISL.
Groundwater sampling points GW-13A and GW- 17A were located along the eastern and
northeastern property boundaries, respectively, of the site. The PCE concentrations detected in
groundwater decreased in the samples collected from the eastern and northeastern property
boundaries toward the interior of the site. In addition, 2-butanone (GW-1A and GW-2A samples),
chloroform (GW-17A sample), chloromethane (GW-13A), and methyl tert-butyl ether (GW-13A
and GW-17A) were detected at concentrations greater than the laboratory method reporting
limits, but less than their respective NC2LGWQS and Non-Residential Groundwater VISL.
• Six sub-slab soil gas sample points (SG-L through SG-Q) were installed in the interior of the
structures of the subject site. The approximate locations of these soil gas samples are shown on
Figure 3. Review of the laboratory analytical results for the samples collected from the sub-slab
sample points indicated several VOCs at concentrations greater than the laboratory method
detection limits in each of the sub-slab samples collected as part of this investigation. Only the
concentrations of chloroform detected in the SG-L sample and PCE in SG-O sample were present
greater than their respective NCDEQ Non-Residential Sub-Slab and Exterior Soil Gas VISLs in the
sub-slab samples collected as part of this assessment. In light of the sub-slab vapor results, ECS
input the laboratory analytical results of each sub-slab soil gas sample collected in to the NCDEQ
Risk Calculator. Based on the results of the NCDEQ Risk Calculator, the concentrations in the sub-
slab soil gas samples did not exceed the risk thresholds for nonresidential use.

Based on the environmental assessment data collected and the planned redevelopment of the site, a
Brownfields Property Application (BPA) was submitted to the NCDEQ, on April 28, 2021, along with the
above referenced assessment services reports. On September 10, 2021, the NCDEQ Brownfields Program
submitted a Letter of Eligibility and established the Brownfields Project Number as 25036-21-060. On
September 30, 2021, the property was purchased by 4000 Monroe LLC c/o Parkside Partners.

On November 4, 2021, ECS presented a Brownfields Kickoff Meeting that summarized the site, previous
assessment activities and results, was well as the proposed site redevelopment activities during a Teams
meeting on, with Parkside Partners, their environmental attorney, and the assigned NCDEQ Brownfields
Project Manager (Mr. Peter Doorn). As a result of the kickoff meeting, in a January 6, 2022, email, Mr.
Doorn requested for additional assessment activities to address potential data gaps, as identified by the
NCDEQ, and requested the status of a previously documented monitoring well that was reportedly located
near the southeast property corner. Generally, the additional assessment activities included the
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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

collection and laboratory analysis of additional soil, sub-slab soil gas, and indoor air, as well as completing
a Brownfields receptor survey.

Based upon the January 6, 2022, email from the NCDEQ Brownfields Project Manager, ECS prepared a
Work Plan (ECS Project No. 49:12929-C) and submitted to NCDEQ Brownfields on February 1, 2022. The
Work Plan was approved by NCDEQ Brownfields via email on February 2, 2022.

2.0 PREVIOUS INVESTIGATIONS

ECS previously conducted multiple environmental assessments at the site. Previous assessment activities
conducted on the various parcels include the following:

• Phase I ESA, prepared by ECS and dated January 15, 2021 (ECS Project No.: 49:12929).
• Report of Environmental Assessment Services by ECS and dated March 12, 2021 (ECS Project No.:
49:12929-A. The assessment activities are described above in Section 1.0.
• Report of Additional Environmental Assessment Services by ECS and dated May 26, 2021 (ECS
Project No.: 49:12929-B. The assessment activities are described above in Section 1.0.

3.0 OBJECTIVE OF THE ASSESSMENT

The objective of the assessment was to address the data gaps identified by the BF Program in their January
6, 2022, email by conducting the following sampling activities:

• Conduct a reconnaissance of the southeastern portion of the subject property in an effort to
evaluate if a monitoring well reported to be that area from an offsite investigation, remained.
• The advancement of three soil borings to depths of up to two feet bgs and collection of a soil
sample from each boring.
• The collection of seven additional indoor air samples.
• The collection of seven additional sub-slab soil gas samples.
• Completion of a Brownfields Receptor Survey.

The indoor air and sub-slab soil gas samples collected were submitted for laboratory analysis of VOCs by
EPA Method TO-15.

The soil samples collected were submitted for laboratory analysis of VOCs by EPA Method 8260, semi-
volatile organic compounds (SVOCs) by EPA Method 8270, RCRA Metals by EPA Method 6010/7471, and
hexavalent chromium by EPA Method 7199 and were selected from the interval exhibiting the highest
photoionization detector (PID) reading in each boring.

The sampling activities were conducted in general accordance with the Brownfields Assessment Work
Plan (Work Plan) prepared by ECS (ECS Project No. 49:12929-C) dated February 1, 2022, and approved by
the NCDEQ Brownfields Program via email on February 2, 2022. This assessment was also conducted in
general accordance with the North Carolina Division of Waste Management’s (NCDWM) Inactive
Hazardous Site Program’s Guidelines for Assessment and Cleanup (Revised October 2015).

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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

4.0 FIELD ACTIVITIES
4.1 Utility Locate

Prior to commencing with field activities, ECS contacted North Carolina One-Call to locate/mark public
utilities at the site. Required separation distances between subsurface activities and marked utilities
(typically 30-inches) were maintained during the field activities. In addition, ECS contracted with Priority
Underground Locating Services to clear the boring areas of private utilities.

4.2 Monitoring Well Evaluation

On February 25, 2022, ECS personnel conducted a reconnaissance of the southeastern portion of the site
in an effort to try to locate a monitoring well that was reportedly in this area. The area is indicated on
Figure 2. This monitoring well was previously identified as ZMW-1 and was associated with the Former
Rea Construction East Plant site (NCDEQ Groundwater Incident #12783), which was located offsite to the
southeast.

4.3 Soil Samples

Number and Sample Location

In general accordance with the Work Plan, ECS advanced three soil borings via decontaminated hand auger
at three locations (SB-1, SB-2, and SB-3) to depths of up to two feet bgs at the locations shown on Figure 4.

Sample Collection

On February 25, 2022, ECS collected two aliquots from each boring. Each aliquot was placed in a re-
sealable plastic bag which was promptly sealed after soil was placed within. ECS used a PID to screen for
volatile organic vapors in one of the aliquots associated with each boring. One soil sample from borings
SB-1 through SB-3 were collected over the zero to two feet bgs interval. Copies of the field sampling
notes are included in Appendix A.

Sample Analysis

Following sample collection, the sample containers were placed on ice in a cooler and maintained under
chain-of-custody until delivered to Pace Analytical Services, LLC (Pace), a North Carolina certified
laboratory located in Huntersville, North Carolina. Chain-of-custody protocol was utilized throughout the
collection and transport of the samples. As previously stated, the soil samples collected were submitted
for laboratory analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, RCRA Metals by EPA
Method 6010/7471, and hexavalent chromium by EPA Method 7199. The laboratory reporting limits were
reported at or below the applicable NCDEQ Preliminary Soil Remediation Goals (PSRGs) for residential soil,
industrial/commercial soil, and protection of groundwater. Additionally, concentrations detected below
the laboratory reporting limit (RL) and above the laboratory method detection limit were reported by the
laboratory were flagged with a J-flag qualifier, indicating the reported concentrations were estimates.

For quality assurance/quality control (QA/QC) purposes, one duplicate soil sample (DUP-1) was collected
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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

from the same location as SB-1 and analyzed for the same compounds as the record sample.

4.4 Indoor Air Samples

Number and Sample Location

In general accordance with the approved Work Plan, ECS collected seven indoor air samples at the
approximate locations shown on Figure 5. The indoor air samples were identified as IA-1 through IA-7.

Sample Collection

On April 19, 2022, the samples were collected using an individually certified 6-liter (L) Summa canister
equipped with an 8-hour flow restrictor. The samples were collected by placing the intake for the Summa
canister at a height of approximately 5 feet above the floor during sampling. Copies of the field sampling
notes are included in Appendix A.

ECS checked and noted the vacuum on each Summa Canister before initiating the sampling procedure.
The sampling procedure was terminated when the vacuum reading was approximately five inches of
mercury.

Sample Analysis

Following sample collection, the sample containers were repackaged and delivered to Con-Test Analytical
Laboratory (Con-Test), an analytical laboratory located in East Longmeadow, Massachusetts. Chain-of-
custody protocol was utilized throughout the collection and transport of the samples. As previously
stated, the indoor air samples collected were submitted for laboratory analysis of VOCs by EPA Method
TO-15. The laboratory reporting limits were reported at or below the applicable North Carolina Residential
and Non-Residential VISLs. Additionally, concentrations detected below the laboratory reporting limit (RL)
and above the laboratory method detection limit were reported by the laboratory were flagged with a J-
flag qualifier, indicating the reported concentrations were estimates.

Initially, for QA/QC purposes, one duplicate indoor air sample and one ambient, outdoor air sample were
to be collected as part of the indoor air sampling assessment; however, these samples were not collected.
The absence of these samples does not appear to have jeopardized the findings.

4.5 Sub-Slab Soil Gas Samples

Number and Sample Location

In accordance with the approved Work Plan, ECS collected seven sub-slab soil gas samples (SS-1 through
SS-7) at the approximate locations shown on Figure 3. The sub-slab soil gas samples were collected
adjacent to, but after, the collection of the above referenced indoor air samples.

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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

Sample Collection

The sub-slab soil gas samples were collected using VaporPins® within the existing floor slab. On April 20,
2022, ECS installed VaporPins® using a hammer drill to penetrate through the concrete slab. Once the
concrete slab was penetrated, a new VaporPin® with a new silicon sleeve was inserted in the concrete
slab in general conformance with manufacturer’s recommendations (Vapor Pin Enterprises, Inc.). The
VaporPin® setup was allowed to equilibrate for at least 20 minutes prior to leak testing.

Prior to collecting the sub-slab soil gas samples, laboratory grade helium gas was used as a QA/QC
measure to confirm the integrity of the probe seal at each sample location. A shroud that encloses the
fittings and sample train was placed over each newly installed vapor point and filled with helium. The
sample tubing and tracer gas tubing was placed through the shroud wall via rubber grommets. During the
purging stage, the cylinder was flooded with laboratory grade helium via the hose placed through the
shroud wall. A Model MGD-2002 Multi-Gas Leak detector was connected to the probe tube and the air
stream being purged was measured for helium. A helium concentration of less than ten percent helium
detected within the shroud was considered acceptable. During leak check activities, helium
concentrations remained above 10 percent in air by volume in each shroud and below 10 percent of the
concentration of Helium inside of the shroud in each sample train. In addition to the leak check, a shut-
in test was conducted to assess for leaks in the fittings and regulator. Copies of the field sampling notes
are included in Appendix A.

Following purging, the vapor point was connected to a batch certified 1-liter Summa canister, which was
used to collect the sample. The Summa canister was fitted with a five-minute flow regulator. ECS checked
and noted the vacuum on each Summa Canister before initiating the sampling procedure. The sampling
procedure was terminated when the vacuum reading was approximately five inches of mercury.

Sample Analysis

Following sample collection, the sample containers were repackaged and delivered to Con-Test. Chain-of-
custody protocol was utilized throughout the collection and transport of the samples. As previously
stated, the soil samples collected were submitted for laboratory analysis of VOCs by EPA Method TO-15.
The laboratory reporting limits were reported at or below the applicable North Carolina Residential and
Non-Residential VISLs. Additionally, concentrations detected below the laboratory reporting limit (RL) and
above the laboratory method detection limit were reported by the laboratory were flagged with a J-flag
qualifier, indicating the reported concentrations were estimates.

For QA/QC purposes, one duplicate soil sample (DUP) was collected from the same location as SS-1 and
analyzed for the same compounds as the record sample.

5.0 RESULTS
5.1 Monitoring Well Evaluation Results

As stated previously, ECS personnel examined the area shown on Figure 2 for the presence of the reported
monitoring well ZMW-1. No evidence of the monitoring well was noted by ECS. Based upon records
reviewed by ECS, monitoring well ZMW-1 was last sampled in August of 2003, with no analyzed
compounds being reported at concentrations greater than the laboratory method reporting limits.
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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022
5.2 Soil Boring Soil Analysis
Constituents of concern were not detected in any soil samples at concentrations greater than the
industrial/commercial PSRGS. PCE was detected in the SB-2 soil sample at an estimated concentration
greater than its Protection of Groundwater PSRG, but less than its Residential and Industrial/Commercial
PSRGs. Four SVOCs were detected in the SB-2 soil sample at estimated concentrations greater than the
laboratory method detection limits, but less than their respective PSRGs. Additional VOCs and SVOCs
were not detected at concentrations greater than the laboratory method reporting limits in any of the
samples collected.
Arsenic in the SB-3 soil sample and hexavalent chromium in the SB-1, SB-2, and SB-3 soil samples were
detected at concentrations greater than its Residential PSRGs, but less than its Protection of Groundwater
and Industrial/Commercial PSRGs. Additional metals were detected in each of the samples collected at
concentrations greater than the laboratory method reporting limits, but less than their respective PSRGs.
A summary of the soil sample analytical results is included as Table 1 and the laboratory report is included
as Appendix B.
Quality Control
Laboratory results of duplicate soil sample (DUP-1) that was collected as a duplicate of soil sample SB-1 and
analyzed for VOCs, SVOCs, and RCRA metals plus hexavalent chromium using EPA Method 8260, 8270,
6020/7471, and 7199 were similar to those detected in SB-1. A Level II QA/QC package was requested
from the laboratory.
The results are summarized in Table 1 and the laboratory report is included as Appendix B.
5.3 Indoor Air Analysis
Review of the laboratory analytical results for the indoor air samples indicated concentrations of seven
compounds in one or more of the IA-1, IA-2, IA-4, IA-5, IA-6, and IA-7 indoor air samples greater than their
respective Residential VISL; with concentrations of 1,4-dichlorobenzene in the IA-2 indoor air sample, and
ethyl acetate in the IA-5, IA-6, and IA-7 indoor air samples detected at concentrations greater than their
respective Non-Residential VISLs.
In light of the indoor air sample results, ECS input the laboratory analytical results of the indoor air samples
in to the NCDEQ Risk Calculator. Based on the results of the NCDEQ Risk Calculator, the concentrations in
the IA-1 through IA-4 indoor air samples did not exceed the risk thresholds. However, the concentrations
in the IA-5, IA-6, IA-7 indoor air samples did exceed the risk threshold for Residential classification, with
the concentrations in the IA-5 and IA-6 indoor air samples also exceeding the risk thresholds for the Non-
Resident Worker classification. These exceedances are likely attributable to the use of ethyl acetate in
the current laboratory operations as opposed to a subsurface release (See Appendix C for Safety Data
Sheets (SDSs) documenting the onsite use of ethyl acetate). If the ethyl acetate results are removed from
the from the risk calculators, the results of the IA-5 and IA-6 indoor air samples do not exceed the risk
thresholds for Resident or Non-Residential Works classifications. Output from the results of the NCDEQ
Risk Calculator are presented in Appendix D.
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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

Additional compounds were detected in each sample collected at concentrations greater than the
laboratory method detection limit, but less than their respective VISLs.

A summary of the indoor air sample analytical results is included as Table 2 and the laboratory report is
included as Appendix B.

5.4 Sub-Slab Soil Gas Soil Analysis

Review of the laboratory analytical results for the sub-slab soil gas samples indicated concentrations of
chloroform in the SS-1 sub-slab soil gas sample, dichlorofluoromethane in the SS-7 sub-slab soil gas
sample, and PCE in the SS-1, SS-5, SS-6, and SS-7 sub-slab soil gas samples at concentrations greater than
their respective Residential VISLs, but less than their respective Non-Residential VISLs. Additional
compounds were detected in each of the sub-slab soil gas samples collected at concentrations greater
than the laboratory method detection limits, but less than their respective Residential and Non-
Residential VISLs

In light of the sub-slab soil gas sample results, ECS input the laboratory analytical results of the sub-slab
soil gas samples in to the NCDEQ Risk Calculator. Based on the results of the NCDEQ Risk Calculator, the
concentrations in each of the sub-slab soil gas samples did not exceed the Residential or Non-Residential
risk thresholds. Output from the results of the NCDEQ Risk Calculator are presented in Appendix D.

A summary of the sub-slab soil gas sample analytical results is included as Table 3 and the laboratory report
is included as Appendix B.

Quality Control

One duplicate sub-slab soil gas sample (DUP) was collected as a duplicate of sub-slab soil gas sample SS-1
and analyzed for VOCs using EPA Method TO-15. The compounds detected in the duplicate sample were
similar to those detected in SS-1. A Level II QA/QC package was requested from the laboratory.

The results are summarized in Table 3 and the laboratory report is included as Appendix B.

5.5 Brownfields Receptor Survey

ECS performed a Brownfields Receptor Survey. The results of the Brownfields Receptor Survey identified
an inactive water supply well located approximately 1,000 feet to the north of the subject site located at
640 Vinewood Place. The nearest residence to the subject site is located approximately 525 feet
northwest at 613 Mayview Drive. A property with a basement was identified approximately 890 feet
northwest of the subject property at 645 Mayview Drive. Underground utilities were noted in the vicinity
of the site at the locations identified on the figure included in Appendix E. Also, the Brownfields Receptor
Survey form is included in Appendix E.

5.6 Investigative Derived Waste

In accordance with the approved Work Plan, Investigative Derived Waste (IDW) generated from the soil
borings (i.e., soil cuttings) were thinly spread onsite in the vicinity of the boring location. IDW generated
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Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

during the installation and sampling of the monitoring wells (i.e., soil cuttings, development water, and
purge water) was placed onsite in the vicinity of the monitoring well location.

6.0 CONCLUSIONS AND DISCUSSION

Based on the results of the sampling presented above, as well as the receptor survey conducted for the
site, ECS has the following conclusions:

• Based on the results of the Brownfields Receptor Survey, an inactive water supply well located
approximately 1,000 feet to the north of the subject site located at 640 Vinewood Place. The
nearest residence to the subject site is located approximately 525 feet northwest at 613 Mayview
Drive. A property with a basement was identified approximately 890 feet northwest of the subject
property at 645 Mayview Drive. Also, the Brownfields Receptor Survey form is included in
Appendix E.
• The monitoring well ZMW-1 was not located during ECS’ reconnaissance of the reported location
of the monitoring well. Therefore, it is estimated that this well was abandoned.
• Constituents of concern were not detected at concentrations greater than the
Industrial/Commercial PSRGS in any of the soil samples collected as part of this assessment.
• Seven compounds in one or more of the IA-1, IA-2, IA-4, IA-5, IA-6, and IA-7 indoor air samples
were detected at concentrations greater than their respective Residential VISLs, but less than
their respective Non-Residential VISLs. Concentrations of 1,4-dichlorobenzene in the IA-2 indoor
air sample, and ethyl acetate in the IA-5, IA-6, and IA-7 indoor air samples were detected at
concentrations greater than their respective Non-Residential VISLs. As noted below, the primary
constituents of concern, PCE and trichloroethene (TCE), were not detected at concentrations
greater than the Residential VISLs.
• The results of the NCDEQ Risk Calculator for the indoor air samples indicated the concentrations
in the IA-5, IA-6, and IA-7 indoor air samples did exceed the risk threshold for Residential
classification, with the concentrations in the IA-5 and IA-6 indoor air samples also exceeding the
risk thresholds for the Non-Resident Worker classification.
• ECS removed the ethyl acetate concentrations from the calculators of the IA-5 and IA-6 indoor air
samples because ethyl acetate is documented to be used in the buildings within which the
samples were collected. The results of the new calculations did not indicate exceedances of either
the Residential or Non-Residential Worker risk thresholds for the IA-5 and IA-6 indoor air samples.
Output from the results of the NCDEQ Risk Calculator are presented in Appendix D.
• Ethyl acetate is used in paints as an activator or hardener. A small laboratory used to study paint
products is located in the general areas from which indoor air samples IA-5 and IA-6 were
collected. Based upon Safety Data Sheets (SDSs) obtained from Clariant Corporation/Colorant
Solutions, ethyl acetate is used in the laboratory activities. The SDSs are included in Appendix C.
• The locations of indoor air samples IA-5, IA-6, and IA-7 and sub-slab soil gas samples SS-5, SS-6,
and SS-7 overlain on floor plans of the first floor of Buildings 2, 3, and 4 are included in Appendix
F. The laboratory is located on the first floor of Building 3, with office space associated with the
laboratory located on the second floor of Building 3. Buildings 2 and 4 are currently vacant. The
laboratory is scheduled to vacate the site on September 10, 2022.
• Review of the laboratory analytical results for the sub-slab soil gas samples indicated
concentrations of chloroform in the SS-1 sub-slab soil gas sample, dichlorofluoromethane in the
11
Brownfields Assessment Report & Receptor Survey
Clariant Corporation Site
Brownfields Project Number 25036-21-060
ECS Project No. 49:12929-D
May 17, 2022

SS-7 sub-slab soil gas sample, and PCE in the SS-1, SS-5, SS-6, and SS-7 sub-slab soil gas samples
at concentrations greater than their respective Residential VISLs, but less than their respective
Non-Residential VISLs.
• The results of the NCDEQ Risk Calculator for the sub-slab soil gas samples indicated the
concentrations in each of the sub-slab soil gas samples did not exceed the risk thresholds for
Residential and Non-Residential Worker classifications.
• PCE and TCE, the constituents of concern, were not detected in the sub-slab soil gas samples at
concentrations greater than their respective Non-Residential VISLs. Additionally, detected levels
of PCE and TCE were less than their respective Residential VISLs.
• Based on the samples collected, the results of the indoor samples IA-5, IA-6, and IA-7 are the only
samples that exceed the proposed future site use (i.e., commercial, office, etc.). However, the
exceedances of the three indoor air samples appear to be due to the use of VOCs by the existing
site laboratory, particularly the use of ethyl acetate, and not the result of indoor air intrusion from
site soils and/or groundwater. This is supported by the facts that (i) the current laboratory
operations use ethyl acetate and (ii) the detected sub-slab soil gas concentrations of ethyl acetate
were either below the laboratory method reporting limit or significantly lower than the ethyl
acetate concentrations detected in the indoor air samples.
• Currently the lab is scheduled to cease operation (September 10, 2022) prior to the anticipated
occupancy by future tenants (in approximately March 2023), with demolition of portions of the
existing structure scheduled to begin in mid-November 2022. The scheduled demolition of the
structure, along with the extended time period after laboratory use and future occupancy, is
expected to allow for the current indoor VOCs to dissipate prior to occupancy of the new tenants.

7.0 DEVIATIONS FROM WORK PLAN

There were no deviations from the approved Work Plan with the exception of a duplicate indoor air
sample was not collected and an ambient background air sample was not collected concurrently with the
indoor air samples. Based on a review of the indoor air sample results verses the results of the other site
samples, specifically the sub-slab soil gas results, the exclusion of these two samples do not appear to
have jeopardized the conclusions presented in this report.

FIGURES
FIGURE 1
USGS TOPOGRAPHIC MAP
CLARIANT CORPORATION SITE
4000 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
BROWNFIELD PROJECT ID: 25306-21-060
ECS PROJECT NO. 49:12929-D
SOURCE:
USGS 7.5’ TOPOGRAPHIC MAP
CHARLOTTE WEST, NC 2019
SCALE:
AS SHOWN
SITE
LOCATION
FIGURE 2
GROUNDWATER SAMPLE LOCATIONS MAP
CLARIANT CORPORATION SITE
4000 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
BROWNFIELD PROJECT ID: 25306-21-060
ECS PROJECT NO. 49:12929-D
SOURCE:
CHARLOTTE MECKLENBURG POLARIS GIS WEBSITE
ACCESSED JANUARY 19, 2021
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE PREVIOUS GROUNDWATER SAMPLE LOCATION
GW-1
GW-2
GW-3 GW-4 GW-
5/5A
GW-6
GW-
16/16A
GW-
17/17A
GW-8
GW-7
GW-9
GW-10
GW-11 GW-15
GW-14
GW-
13/13-A
GW-12
GW-2A
GW-18
GW-1A
AREA INSPECTED FOR
REPORTED MONITORING
WELL
FIGURE 3
SUB-SLAB SOIL GAS SAMPLE LOCATIONS MAP
CLARIANT CORPORATION SITE
4000 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
BROWNFIELD PROJECT ID: 25306-21-060
ECS PROJECT NO. 49:12929-D
SOURCE:
CHARLOTTE MECKLENBURG POLARIS GIS WEBSITE
ACCESSED JANUARY 19, 2021
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
APPROXIMATE SUB-SLAB SOIL GAS SAMPLE LOCATION
Former Gasoline
Station and Three 550-
gallon USTs removed
SG-K
SG-J
SG-I
SG-G
SG-F
SG-E
SG-H
SG-D
SG-B
SG-C
SG-A
LEGEND
SG-M
SG-Q
SG-P
SG-O
SG-L
SG-N
SS-1
SS-2
SS-3
SS-4
SS-5
SS-6SS-7
FIGURE 4
SOIL SAMPLE LOCATIONS MAP
CLARIANT CORPORATION SITE
4000 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
BROWNFIELD PROJECT ID: 25306-21-060
ECS PROJECT NO. 49:12929-D
SOURCE:
CHARLOTTE MECKLENBURG POLARIS GIS WEBSITE
ACCESSED JANUARY 19, 2021
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
APPROXIMATE SOIL SAMPLE LOCATION
APPROXIMATE BACKGROUND SOIL SAMPLE LOCATION
SB-2A
SB-13A
SB-18
LEGEND
B-1
B-2
B-3B-4
SB-1A
SB-1
SB-2
SB-3
FIGURE 5
INDOOR AIR SAMPLE LOCATIONS MAP
CLARIANT CORPORATION SITE
4000 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
BROWNFIELD PROJECT ID: 25306-21-060
ECS PROJECT NO. 49:12929-D
SOURCE:
CHARLOTTE MECKLENBURG POLARIS GIS WEBSITE
ACCESSED JANUARY 19, 2021
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
APPROXIMATE SUB-SLAB SOIL GAS SAMPLE LOCATION
LEGEND
IA-1
IA-2
IA-3
IA-4
IA-5
IA-6
IA-7
TABLES
Table 1
Summary of Soil Samples Analytical Results
Clariant Corporation Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
Brownfields Project ID: 25306-21-060
ECS Project No.: 49:12929-D
VOCs by EPA
Method 8260 SVOCs by EPA Method 8270 RCRA Metals by EPA Methods 6010/7471/7199
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Protection of Groundwater PSRG 0.0063 1.2 670 NE 440 5.8 580 3.0 NE 360,000 3.8 270 1.0 2.1 3.4
Residential PSRG 1.7 1.1 480 NE 360 0.68 3,100 1.4 NE 23,000 0.31 400 4.7 78 78
Industrial/Commercial PSRG 82 21 6,000 NE 4,500 3.0 47,000 20 NE 350,000 6.5 800 70 1,200 1,200
SB-1 02/25/22 0.0' - 2.0'<0.0057 <0.38 <0.38 <0.38 <0.38 <3.3 29.0 <1.1 4.0 3.3 0.656 9.5 0.043 J <4.4 <1.1
DUP-1*02/25/22 0.0' - 2.0'<0.0056 <0.38 <0.38 <0.38 <0.38 <3.4 34.3 <1.1 7.1 6.8 0.348 J 12.7 0.039 J <4.6 <1.1
SB-2 02/25/22 0.0' - 2.0'0.0067 J 0.15 J 0.22 J 0.14 J 0.19 J <3.6 33.1 <1.2 12.8 11.7 1.11 23.0 0.068 J <4.8 <1.2
SB-3 02/25/22 0.0' - 2.0'<0.0073 <0.39 <0.39 <0.39 <0.39 2.6 J 86.7 <1.1 16.1 13.8 2.31 16.9 0.036 J <4.6 <1.1
Notes:
All results presented in milligrams per kilogram (mg/kg)
Compounds not shown were not detected
VOCs = Volatile Organic Compounds
SVOCs = Semi-voaltile Organic Compounds
PSRGs = Preliminary Soil Remediation Goals (January 2022)
* = DUP-1 is a duplicate sample of the SB-1 record sample
VALUE = concentration greater than the laboratory method reporting limit
VALUE = concentration greater than the Protection of Groundwater PSRG
VALUE = concentration greater than the Residential PSRG
Sample ID Sample
Date
Sample Depth
(x to y ft bgs)
Table 2
Summary of Indoor Air Samples Analytical Results
Clariant Corporation Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
Brownfields Project ID: 25306-21-060
ECS Project No.: 49:12929-D
VOCs by EPA Method TO-15
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Residential VISL NE 0.36 1,000 0.47 0.12 19 0.26 21 NE 15 1.1 NE 83 150 42 100 630 0.083 8.3 1,000 0.42 NE 1,000 13 13 21
Non-Residential VISL NE 1.6 4,400 2.0 0.53 79 1.1 88 NE 61 4.9 NE 350 610 180 530 2,600 0.36 35 4,400 1.8 NE 4,400 53 53 88
IA-1 04/19/22 9.5 0.33 1.2 J 0.47 <0.17 1.1 0.89 2.3 6.4 2.0 0.17 <0.17 0.16 1.3 J 1.4 J 0.78 J <0.14 0.32 0.26 0.80 <0.19 3.2 0.64 J 0.19 <0.17 0.83
IA-2 04/19/22 10 0.30 3.0 J 0.42 <0.17 1.1 1.1 2.3 6.8 3.5 0.12 J <0.17 0.19 1.3 J 1.3 J <1.2 0.17 0.25 0.20 J 0.54 <0.19 2.8 0.61 J 0.13 J <0.17 0.53
IA-3 04/19/22 9.6 0.24 2.0 J 0.45 <0.17 1.3 <0.21 2.5 6.3 10 0.15 J <0.17 0.30 1.3 J 0.84 J <1.2 0.17 <0.18 <0.24 0.63 <0.19 6.1 0.65 J 0.13 J <0.17 0.62
IA-4 04/19/22 10 0.23 1.8 J 0.48 <0.17 1.1 <0.21 2.4 6.6 20 0.13 J <0.17 <0.14 1.6 J 1.5 J 0.88 J <0.14 <0.18 <0.24 0.45 <0.19 1.9 0.61 J 0.15 J <0.17 0.62
IA-5 04/19/22 14 0.25 1.6 J 0.49 <0.17 1.2 <0.21 2.5 23 430 1.3 0.16 J 0.55 7.6 5.3 0.87 J <0.14 <0.18 0.25 0.74 <0.19 2.8 0.60 J 0.61 0.19 7.2
IA-6 04/19/22 33 0.26 2.2 J 0.48 0.29 1.2 <0.21 0.32 50 1,800 3.9 0.38 <0.14 <4.9 13 0.82 J <0.14 <0.18 0.67 1.0 0.32 4.1 0.69 J 1.7 0.37 22.2
IA-7 04/19/22 17 0.26 <4.1 0.44 0.40 1.3 0.62 6.2 33 220 1.6 0.38 <0.14 <4.9 10 0.71 J <0.14 <0.18 <0.24 0.88 <0.19 7.8 0.62 J 1.6 0.40 1.68
Notes:
All results presented in micrograms per cubic meter (µg/m3)
Compounds not shown were not detected
VOCs = Volatile Organic Compounds
Residential VISLs = NCDEQ Residential Indoor Air Instrusion Screening Levels (January 2022)
Non-Residential VISLs = NCDEQ Non-Residential Sub-Slab Vapor Instrusion Screening Levels (January 2022)
NE = Not established
VALUE = concentration greater than the laboratory method reporting limit
VALUE = concentration greater than the Residential VISL
VALUE = concentration greater than the Non-Residential VISL
Sample ID Sample
Date
Table 3Summary of Sub-Slab Soil Gas Samples Analytical Results
Clariant Corporation Site4000 Monroe Road
Charlotte, Mecklenburg County, North CarolinaBrownfields Project ID: 25306-21-060
ECS Project No.: 49:12929-D
VOCs by EPA Method TO-15
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Residential VISL NE 12 2.5 35 35,000 4,900 16 4.1 630 42,000 700 1,400 19 NE 490 37 2,800 4,900 210 1,400 3,400 21,000 2.8 21,000 7,000 280 14,000 35,000 35,000 14 NE 35,000 420 420 700
Non-Residential VISL NE 160 33 440 440,000 61,000 61,000 53 7,900 530,000 8,800 18,000 250 NE 6,100 490 35,000 61,000 2,600 18,000 53,000 260,000 36 260,000 88,000 3,500 180,000 440,000 440,000 180 NE 440,000 5,300 5,300 8,800
SS-1 04/20/22 53 <0.64 <1.3 <0.78 6.6 J 3.0 J <1.3 26 0.77 J 4.1 2.3 <0.79 <7.2 81 <7.2 3.4 <0.82 <28 <0.82 8.1 J <6.9 <0.82 <1.0 <14 0.55 J 520 <5.9 2.0 <1.1 <1.1 2.8 J <6.1 <0.98 <0.98 21.8
DUP 04/20/22 61 <0.64 <1.3 <0.78 <24 3.8 J <1.3 33 <0.83 4.5 3.3 <0.79 <7.2 100 <7.2 4.2 <0.82 6.1 J <0.82 10 J <6.9 <0.82 <1.0 <14 0.66 J 670 <5.9 2.4 <1.1 0.73 J 2.7 J <6.1 1.1 <0.98 26.6
SS-2 04/20/22 57 <0.64 <1.3 <0.78 <24 18 <1.3 <0.98 <0.83 6.3 <0.99 <0.79 <7.2 130 <7.2 3.9 <0.82 <28 <0.82 8.7 J <6.9 <0.82 <1.0 <14 <0.85 2.9 <5.9 2.2 <1.1 <1.1 4.0 J 7.0 0.98 <0.98 27.1
SS-3 04/20/22 57 <0.64 <1.3 <0.78 <24 1.4 J <1.3 <0.98 <0.83 4.2 15 <0.79 <7.2 80 4.0 J 5.7 <0.82 6.9 J <0.82 24 3.3 J <0.82 <1.0 <14 0.51 J 29 1.3 J 2.2 <1.1 <1.1 1.9 J <6.1 1.2 <0.98 36.0SS-4 04/20/22 240 4.6 <1.3 <0.78 16 J <6.2 <1.3 <0.98 1.1 3.5 3.4 <0.79 <7.2 150 73 11 2.5 9.2 J <0.82 10 J <6.9 <0.82 1.9 <14 <0.85 79 <5.9 18 <1.1 <1.1 4.0 J <6.1 1.0 <0.98 39.0
SS-5 04/20/22 240 <0.64 <1.3 <0.78 30 13 <1.3 <0.98 0.90 8.8 3.0 <0.79 11 240 14 8.7 <0.82 6.3 J <0.82 23 <6.9 <0.82 <1.0 <14 1.0 440 <5.9 2.9 <1.1 <1.1 2.4 J 2.0 J 1.6 0.53 J 50.0
SS-6 04/20/22 570 <0.64 <1.3 1.4 16 J 6.2 <1.3 1.2 3.5 9.6 4.9 <0.79 <7.2 260 120 6.8 <0.82 7.1 J <0.82 24 <6.9 <0.82 <1.0 <14 1.1 940 3.0 J 3.7 23 <1.1 3.7 J 2.8 J 1.5 <0.98 43.0
SS-7 04/20/22 130 <0.64 <1.3 <0.78 6.4 J 2.3 J <1.3 <0.98 <0.83 3.7 2,000 <0.79 <7.2 160 19 5.5 <0.82 5.9 J <0.82 19 J <6.9 5.8 <1.0 <14 0.72 J 1,100 <5.9 4.0 <1.1 <1.1 11 <6.1 1.2 <0.98 32.0
Notes:
All results presented in micrograms per cubic meter (µg/m3)
Compounds not shown were not detected
VOCs = Volatile Organic Compounds
Residential VISLs = NCDEQ Residential Sub-Slab Vapor Instrusion Screening Levels (January 2022)
Non-Residential VISLs = NCDEQ Non-Residential Sub-Slab Vapor Instrusion Screening Levels (January 2022)
NE = Not established
* = DUP is a duplicate sample of the SS-1 record sample
VALUE = concentration greater than the laboratory method reporting limit
VALUE = concentration greater than the Residential VISL
VALUE = concentration greater than the Non-Residential VISL
Sample ID Sample
Date

APPENDIX A

APPENDIX B
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
April 28, 2022
Scott Young
ECS Southeast - Charlotte, NC
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project Location: 4000 Monroe Rd.
Client Job Number:
Project Number: 12929
Laboratory Work Order Number: 22D1698
Enclosed are results of analyses for samples as received by the laboratory on April 22, 2022. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
4/28/2022ECS Southeast - Charlotte, NC
1812 Center Park Drive, Suite D
Charlotte, NC 28217
ATTN: Scott Young
12929
22D1698
The results of analyses performed on the following samples submitted to Con-Test, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
4000 Monroe Rd.
SS-1 22D1698-01 Sub Slab -
EPA TO-15
SS-2 22D1698-02 Sub Slab -
EPA TO-15
SS-3 22D1698-03 Sub Slab -
EPA TO-15
SS-4 22D1698-04 Sub Slab -
EPA TO-15
SS-5 22D1698-05 Sub Slab -
EPA TO-15
SS-6 22D1698-06 Sub Slab -
EPA TO-15
SS-7 22D1698-07 Sub Slab -
EPA TO-15
Dup 22D1698-08 Sub Slab -
EPA TO-15
Page 2 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not
detected" for all samples in this batch for this compound and bias is on the high side.
Analyte & Samples(s) Qualified:
L-01
Benzyl chloride
B307102-BS1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
Vinyl Acetate
22D1698-08[Dup], B307102-BLK1, B307102-BS1, B307102-DUP1, S070925-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
Benzyl chloride
B307102-BS1, S070925-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since
sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-36
1,2,4-Trichlorobenzene, Benzyl chloride
B306974-BS1, B307102-BS1, S070889-CCV1, S070925-CCV1
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 3 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-1
Sample ID: 22D1698-01
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.3
Sampled: 4/20/2022 13:32
Canister ID: 3101
Flow Controller ID: 4289
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 22 8.0 4/27/22 4:30 BRF53 4194.8 11
Benzene ND 0.20 4/27/22 4:30 BRFND40.640.15 0.48
Benzyl chloride ND 0.40 4/27/22 4:30 BRFND42.10.18 0.91
Bromodichloromethane ND 0.20 4/27/22 4:30 BRFND41.30.14 0.94
Bromoform ND 0.20 4/27/22 4:30 BRFND42.10.14 1.4
Bromomethane ND 0.20 4/27/22 4:30 BRFND40.780.13 0.52
1,3-Butadiene ND 0.20 4/27/22 4:30 BRFND40.440.17 0.37
2-Butanone (MEK)2.2 8.0 4/27/22 4:30 BRFJ6.6 4242.1 6.3
Carbon Disulfide 0.96 2.0 4/27/22 4:30 BRFJ3.0 46.20.18 0.58
Carbon Tetrachloride ND 0.20 4/27/22 4:30 BRFND41.30.16 1.0
Chlorobenzene ND 0.20 4/27/22 4:30 BRFND40.920.13 0.61
Chloroethane ND 0.20 4/27/22 4:30 BRFND40.530.18 0.47
Chloroform 5.4 0.20 4/27/22 4:30 BRF26 40.980.19 0.93
Chloromethane 0.37 0.40 4/27/22 4:30 BRFJ0.77 40.830.16 0.33
Cyclohexane 1.2 0.20 4/27/22 4:30 BRF4.1 40.690.12 0.42
Dibromochloromethane ND 0.20 4/27/22 4:30 BRFND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 4/27/22 4:30 BRFND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 4/27/22 4:30 BRFND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 4/27/22 4:30 BRFND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 4/27/22 4:30 BRFND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)0.47 0.20 4/27/22 4:30 BRF2.3 40.990.20 0.97
1,1-Dichloroethane ND 0.20 4/27/22 4:30 BRFND40.810.17 0.71
1,2-Dichloroethane ND 0.20 4/27/22 4:30 BRFND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 4/27/22 4:30 BRFND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 4/27/22 4:30 BRFND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 4/27/22 4:30 BRFND40.790.16 0.62
1,2-Dichloropropane ND 0.20 4/27/22 4:30 BRFND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 4/27/22 4:30 BRFND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 4/27/22 4:30 BRFND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 4/27/22 4:30 BRFND41.40.20 1.4
1,4-Dioxane ND 2.0 4/27/22 4:30 BRFND47.20.17 0.60
Ethanol 43 8.0 4/27/22 4:30 BRF81 4153.5 6.6
Ethyl Acetate ND 2.0 4/27/22 4:30 BRFND47.21.0 3.6
Ethylbenzene 0.78 0.20 4/27/22 4:30 BRF3.4 40.870.12 0.51
4-Ethyltoluene ND 0.20 4/27/22 4:30 BRFND40.980.12 0.60
Heptane ND 0.20 4/27/22 4:30 BRFND40.820.13 0.52
Hexachlorobutadiene ND 0.20 4/27/22 4:30 BRFND42.10.16 1.8
Hexane ND 8.0 4/27/22 4:30 BRFND4281.0 3.7
2-Hexanone (MBK)ND 0.20 4/27/22 4:30 BRFND40.820.10 0.41
Isopropanol 3.3 8.0 4/27/22 4:30 BRFJ8.1 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 4/27/22 4:30 BRFND40.720.15 0.56
Methylene Chloride ND 2.0 4/27/22 4:30 BRFND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 4/27/22 4:30 BRFND40.820.11 0.44
Naphthalene ND 0.20 4/27/22 4:30 BRFND41.00.15 0.79
Propene ND 8.0 4/27/22 4:30 BRFND4141.8 3.0
Styrene 0.13 0.20 4/27/22 4:30 BRFJ0.55 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 4/27/22 4:30 BRFND41.40.11 0.74
Page 4 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-1
Sample ID: 22D1698-01
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.3
Sampled: 4/20/2022 13:32
Canister ID: 3101
Flow Controller ID: 4289
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 77 0.20 4/27/22 4:30 BRF520 41.40.15 1.0
Tetrahydrofuran ND 2.0 4/27/22 4:30 BRFND45.90.33 0.97
Toluene 0.53 0.20 4/27/22 4:30 BRF2.0 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 4/27/22 4:30 BRFND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 4/27/22 4:30 BRFND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 4/27/22 4:30 BRFND41.10.14 0.77
Trichloroethylene ND 0.20 4/27/22 4:30 BRFND41.10.13 0.72
Trichlorofluoromethane (Freon 11)0.50 0.80 4/27/22 4:30 BRFJ2.8 44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 4/27/22 4:30 BRFND46.10.22 1.7
1,2,4-Trimethylbenzene ND 0.20 4/27/22 4:30 BRFND40.980.088 0.43
1,3,5-Trimethylbenzene ND 0.20 4/27/22 4:30 BRFND40.980.11 0.52
Vinyl Acetate ND 4.0 4/27/22 4:30 BRFND4141.1 3.8
Vinyl Chloride ND 0.20 4/27/22 4:30 BRFND40.510.18 0.46
m&p-Xylene 3.4 0.40 4/27/22 4:30 BRF15 41.70.22 0.97
o-Xylene 1.6 0.20 4/27/22 4:30 BRF6.8 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)106 4/27/22 4:3070-130
Page 5 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-2
Sample ID: 22D1698-02
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.0
Sampled: 4/20/2022 14:01
Canister ID: 2563
Flow Controller ID: 4097
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 24 8.0 4/27/22 5:01 BRF57 4194.8 11
Benzene ND 0.20 4/27/22 5:01 BRFND40.640.15 0.48
Benzyl chloride ND 0.40 4/27/22 5:01 BRFND42.10.18 0.91
Bromodichloromethane ND 0.20 4/27/22 5:01 BRFND41.30.14 0.94
Bromoform ND 0.20 4/27/22 5:01 BRFND42.10.14 1.4
Bromomethane ND 0.20 4/27/22 5:01 BRFND40.780.13 0.52
1,3-Butadiene ND 0.20 4/27/22 5:01 BRFND40.440.17 0.37
2-Butanone (MEK)ND 8.0 4/27/22 5:01 BRFND4242.1 6.3
Carbon Disulfide 5.9 2.0 4/27/22 5:01 BRF18 46.20.18 0.58
Carbon Tetrachloride ND 0.20 4/27/22 5:01 BRFND41.30.16 1.0
Chlorobenzene ND 0.20 4/27/22 5:01 BRFND40.920.13 0.61
Chloroethane ND 0.20 4/27/22 5:01 BRFND40.530.18 0.47
Chloroform ND 0.20 4/27/22 5:01 BRFND40.980.19 0.93
Chloromethane ND 0.40 4/27/22 5:01 BRFND40.830.16 0.33
Cyclohexane 1.8 0.20 4/27/22 5:01 BRF6.3 40.690.12 0.42
Dibromochloromethane ND 0.20 4/27/22 5:01 BRFND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 4/27/22 5:01 BRFND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 4/27/22 5:01 BRFND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 4/27/22 5:01 BRFND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 4/27/22 5:01 BRFND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)ND 0.20 4/27/22 5:01 BRFND40.990.20 0.97
1,1-Dichloroethane ND 0.20 4/27/22 5:01 BRFND40.810.17 0.71
1,2-Dichloroethane ND 0.20 4/27/22 5:01 BRFND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 4/27/22 5:01 BRFND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 4/27/22 5:01 BRFND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 4/27/22 5:01 BRFND40.790.16 0.62
1,2-Dichloropropane ND 0.20 4/27/22 5:01 BRFND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 4/27/22 5:01 BRFND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 4/27/22 5:01 BRFND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 4/27/22 5:01 BRFND41.40.20 1.4
1,4-Dioxane ND 2.0 4/27/22 5:01 BRFND47.20.17 0.60
Ethanol 72 8.0 4/27/22 5:01 BRF130 4153.5 6.6
Ethyl Acetate ND 2.0 4/27/22 5:01 BRFND47.21.0 3.6
Ethylbenzene 0.90 0.20 4/27/22 5:01 BRF3.9 40.870.12 0.51
4-Ethyltoluene ND 0.20 4/27/22 5:01 BRFND40.980.12 0.60
Heptane ND 0.20 4/27/22 5:01 BRFND40.820.13 0.52
Hexachlorobutadiene ND 0.20 4/27/22 5:01 BRFND42.10.16 1.8
Hexane ND 8.0 4/27/22 5:01 BRFND4281.0 3.7
2-Hexanone (MBK)ND 0.20 4/27/22 5:01 BRFND40.820.10 0.41
Isopropanol 3.6 8.0 4/27/22 5:01 BRFJ8.7 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 4/27/22 5:01 BRFND40.720.15 0.56
Methylene Chloride ND 2.0 4/27/22 5:01 BRFND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 4/27/22 5:01 BRFND40.820.11 0.44
Naphthalene ND 0.20 4/27/22 5:01 BRFND41.00.15 0.79
Propene ND 8.0 4/27/22 5:01 BRFND4141.8 3.0
Styrene ND 0.20 4/27/22 5:01 BRFND40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 4/27/22 5:01 BRFND41.40.11 0.74
Page 6 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-2
Sample ID: 22D1698-02
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.0
Sampled: 4/20/2022 14:01
Canister ID: 2563
Flow Controller ID: 4097
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.43 0.20 4/27/22 5:01 BRF2.9 41.40.15 1.0
Tetrahydrofuran ND 2.0 4/27/22 5:01 BRFND45.90.33 0.97
Toluene 0.57 0.20 4/27/22 5:01 BRF2.2 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 4/27/22 5:01 BRFND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 4/27/22 5:01 BRFND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 4/27/22 5:01 BRFND41.10.14 0.77
Trichloroethylene ND 0.20 4/27/22 5:01 BRFND41.10.13 0.72
Trichlorofluoromethane (Freon 11)0.70 0.80 4/27/22 5:01 BRFJ4.0 44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.91 0.80 4/27/22 5:01 BRF7.0 46.10.22 1.7
1,2,4-Trimethylbenzene 0.20 0.20 4/27/22 5:01 BRF0.98 40.980.088 0.43
1,3,5-Trimethylbenzene ND 0.20 4/27/22 5:01 BRFND40.980.11 0.52
Vinyl Acetate ND 4.0 4/27/22 5:01 BRFND4141.1 3.8
Vinyl Chloride ND 0.20 4/27/22 5:01 BRFND40.510.18 0.46
m&p-Xylene 4.3 0.40 4/27/22 5:01 BRF19 41.70.22 0.97
o-Xylene 1.9 0.20 4/27/22 5:01 BRF8.1 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)108 4/27/22 5:0170-130
Page 7 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-3
Sample ID: 22D1698-03
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.7
Sampled: 4/20/2022 14:33
Canister ID: 2788
Flow Controller ID: 4117
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 24 8.0 4/27/22 6:02 BRF57 4194.8 11
Benzene ND 0.20 4/27/22 6:02 BRFND40.640.15 0.48
Benzyl chloride ND 0.40 4/27/22 6:02 BRFND42.10.18 0.91
Bromodichloromethane ND 0.20 4/27/22 6:02 BRFND41.30.14 0.94
Bromoform ND 0.20 4/27/22 6:02 BRFND42.10.14 1.4
Bromomethane ND 0.20 4/27/22 6:02 BRFND40.780.13 0.52
1,3-Butadiene ND 0.20 4/27/22 6:02 BRFND40.440.17 0.37
2-Butanone (MEK)ND 8.0 4/27/22 6:02 BRFND4242.1 6.3
Carbon Disulfide 0.45 2.0 4/27/22 6:02 BRFJ1.4 46.20.18 0.58
Carbon Tetrachloride ND 0.20 4/27/22 6:02 BRFND41.30.16 1.0
Chlorobenzene ND 0.20 4/27/22 6:02 BRFND40.920.13 0.61
Chloroethane ND 0.20 4/27/22 6:02 BRFND40.530.18 0.47
Chloroform ND 0.20 4/27/22 6:02 BRFND40.980.19 0.93
Chloromethane ND 0.40 4/27/22 6:02 BRFND40.830.16 0.33
Cyclohexane 1.2 0.20 4/27/22 6:02 BRF4.2 40.690.12 0.42
Dibromochloromethane ND 0.20 4/27/22 6:02 BRFND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 4/27/22 6:02 BRFND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 4/27/22 6:02 BRFND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 4/27/22 6:02 BRFND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 4/27/22 6:02 BRFND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)3.1 0.20 4/27/22 6:02 BRF15 40.990.20 0.97
1,1-Dichloroethane ND 0.20 4/27/22 6:02 BRFND40.810.17 0.71
1,2-Dichloroethane ND 0.20 4/27/22 6:02 BRFND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 4/27/22 6:02 BRFND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 4/27/22 6:02 BRFND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 4/27/22 6:02 BRFND40.790.16 0.62
1,2-Dichloropropane ND 0.20 4/27/22 6:02 BRFND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 4/27/22 6:02 BRFND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 4/27/22 6:02 BRFND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 4/27/22 6:02 BRFND41.40.20 1.4
1,4-Dioxane ND 2.0 4/27/22 6:02 BRFND47.20.17 0.60
Ethanol 42 8.0 4/27/22 6:02 BRF80 4153.5 6.6
Ethyl Acetate 1.1 2.0 4/27/22 6:02 BRFJ4.0 47.21.0 3.6
Ethylbenzene 1.3 0.20 4/27/22 6:02 BRF5.7 40.870.12 0.51
4-Ethyltoluene ND 0.20 4/27/22 6:02 BRFND40.980.12 0.60
Heptane ND 0.20 4/27/22 6:02 BRFND40.820.13 0.52
Hexachlorobutadiene ND 0.20 4/27/22 6:02 BRFND42.10.16 1.8
Hexane 2.0 8.0 4/27/22 6:02 BRFJ6.9 4281.0 3.7
2-Hexanone (MBK)ND 0.20 4/27/22 6:02 BRFND40.820.10 0.41
Isopropanol 9.8 8.0 4/27/22 6:02 BRF24 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 4/27/22 6:02 BRFND40.720.15 0.56
Methylene Chloride 0.95 2.0 4/27/22 6:02 BRFJ3.3 46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 4/27/22 6:02 BRFND40.820.11 0.44
Naphthalene ND 0.20 4/27/22 6:02 BRFND41.00.15 0.79
Propene ND 8.0 4/27/22 6:02 BRFND4141.8 3.0
Styrene 0.12 0.20 4/27/22 6:02 BRFJ0.51 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 4/27/22 6:02 BRFND41.40.11 0.74
Page 8 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-3
Sample ID: 22D1698-03
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.7
Sampled: 4/20/2022 14:33
Canister ID: 2788
Flow Controller ID: 4117
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 4.2 0.20 4/27/22 6:02 BRF29 41.40.15 1.0
Tetrahydrofuran 0.42 2.0 4/27/22 6:02 BRFJ1.3 45.90.33 0.97
Toluene 0.57 0.20 4/27/22 6:02 BRF2.2 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 4/27/22 6:02 BRFND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 4/27/22 6:02 BRFND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 4/27/22 6:02 BRFND41.10.14 0.77
Trichloroethylene ND 0.20 4/27/22 6:02 BRFND41.10.13 0.72
Trichlorofluoromethane (Freon 11)0.34 0.80 4/27/22 6:02 BRFJ1.9 44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 4/27/22 6:02 BRFND46.10.22 1.7
1,2,4-Trimethylbenzene 0.24 0.20 4/27/22 6:02 BRF1.2 40.980.088 0.43
1,3,5-Trimethylbenzene ND 0.20 4/27/22 6:02 BRFND40.980.11 0.52
Vinyl Acetate ND 4.0 4/27/22 6:02 BRFND4141.1 3.8
Vinyl Chloride ND 0.20 4/27/22 6:02 BRFND40.510.18 0.46
m&p-Xylene 5.8 0.40 4/27/22 6:02 BRF25 41.70.22 0.97
o-Xylene 2.5 0.20 4/27/22 6:02 BRF11 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)106 4/27/22 6:0270-130
Page 9 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-4
Sample ID: 22D1698-04
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.1
Sampled: 4/20/2022 15:02
Canister ID: 2291
Flow Controller ID: 4118
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 100 8.0 4/27/22 6:32 BRF240 4194.8 11
Benzene 1.4 0.20 4/27/22 6:32 BRF4.6 40.640.15 0.48
Benzyl chloride ND 0.40 4/27/22 6:32 BRFND42.10.18 0.91
Bromodichloromethane ND 0.20 4/27/22 6:32 BRFND41.30.14 0.94
Bromoform ND 0.20 4/27/22 6:32 BRFND42.10.14 1.4
Bromomethane ND 0.20 4/27/22 6:32 BRFND40.780.13 0.52
1,3-Butadiene ND 0.20 4/27/22 6:32 BRFND40.440.17 0.37
2-Butanone (MEK)5.6 8.0 4/27/22 6:32 BRFJ16 4242.1 6.3
Carbon Disulfide ND 2.0 4/27/22 6:32 BRFND46.20.18 0.58
Carbon Tetrachloride ND 0.20 4/27/22 6:32 BRFND41.30.16 1.0
Chlorobenzene ND 0.20 4/27/22 6:32 BRFND40.920.13 0.61
Chloroethane ND 0.20 4/27/22 6:32 BRFND40.530.18 0.47
Chloroform ND 0.20 4/27/22 6:32 BRFND40.980.19 0.93
Chloromethane 0.52 0.40 4/27/22 6:32 BRF1.1 40.830.16 0.33
Cyclohexane 1.0 0.20 4/27/22 6:32 BRF3.5 40.690.12 0.42
Dibromochloromethane ND 0.20 4/27/22 6:32 BRFND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 4/27/22 6:32 BRFND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 4/27/22 6:32 BRFND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 4/27/22 6:32 BRFND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 4/27/22 6:32 BRFND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)0.68 0.20 4/27/22 6:32 BRF3.4 40.990.20 0.97
1,1-Dichloroethane ND 0.20 4/27/22 6:32 BRFND40.810.17 0.71
1,2-Dichloroethane ND 0.20 4/27/22 6:32 BRFND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 4/27/22 6:32 BRFND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 4/27/22 6:32 BRFND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 4/27/22 6:32 BRFND40.790.16 0.62
1,2-Dichloropropane ND 0.20 4/27/22 6:32 BRFND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 4/27/22 6:32 BRFND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 4/27/22 6:32 BRFND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 4/27/22 6:32 BRFND41.40.20 1.4
1,4-Dioxane ND 2.0 4/27/22 6:32 BRFND47.20.17 0.60
Ethanol 78 8.0 4/27/22 6:32 BRF150 4153.5 6.6
Ethyl Acetate 20 2.0 4/27/22 6:32 BRF73 47.21.0 3.6
Ethylbenzene 2.5 0.20 4/27/22 6:32 BRF11 40.870.12 0.51
4-Ethyltoluene ND 0.20 4/27/22 6:32 BRFND40.980.12 0.60
Heptane 0.62 0.20 4/27/22 6:32 BRF2.5 40.820.13 0.52
Hexachlorobutadiene ND 0.20 4/27/22 6:32 BRFND42.10.16 1.8
Hexane 2.6 8.0 4/27/22 6:32 BRFJ9.2 4281.0 3.7
2-Hexanone (MBK)ND 0.20 4/27/22 6:32 BRFND40.820.10 0.41
Isopropanol 4.2 8.0 4/27/22 6:32 BRFJ10 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 4/27/22 6:32 BRFND40.720.15 0.56
Methylene Chloride ND 2.0 4/27/22 6:32 BRFND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 4/27/22 6:32 BRFND40.820.11 0.44
Naphthalene 0.37 0.20 4/27/22 6:32 BRF1.9 41.00.15 0.79
Propene ND 8.0 4/27/22 6:32 BRFND4141.8 3.0
Styrene ND 0.20 4/27/22 6:32 BRFND40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 4/27/22 6:32 BRFND41.40.11 0.74
Page 10 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-4
Sample ID: 22D1698-04
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.1
Sampled: 4/20/2022 15:02
Canister ID: 2291
Flow Controller ID: 4118
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 12 0.20 4/27/22 6:32 BRF79 41.40.15 1.0
Tetrahydrofuran ND 2.0 4/27/22 6:32 BRFND45.90.33 0.97
Toluene 4.9 0.20 4/27/22 6:32 BRF18 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 4/27/22 6:32 BRFND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 4/27/22 6:32 BRFND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 4/27/22 6:32 BRFND41.10.14 0.77
Trichloroethylene ND 0.20 4/27/22 6:32 BRFND41.10.13 0.72
Trichlorofluoromethane (Freon 11)0.72 0.80 4/27/22 6:32 BRFJ4.0 44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 4/27/22 6:32 BRFND46.10.22 1.7
1,2,4-Trimethylbenzene 0.20 0.20 4/27/22 6:32 BRF1.0 40.980.088 0.43
1,3,5-Trimethylbenzene ND 0.20 4/27/22 6:32 BRFND40.980.11 0.52
Vinyl Acetate ND 4.0 4/27/22 6:32 BRFND4141.1 3.8
Vinyl Chloride ND 0.20 4/27/22 6:32 BRFND40.510.18 0.46
m&p-Xylene 6.2 0.40 4/27/22 6:32 BRF27 41.70.22 0.97
o-Xylene 2.7 0.20 4/27/22 6:32 BRF12 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)107 4/27/22 6:3270-130
Page 11 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-5
Sample ID: 22D1698-05
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.7
Sampled: 4/20/2022 15:31
Canister ID: 3411
Flow Controller ID: 4346
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 100 8.0 4/27/22 7:02 BRF240 4194.8 11
Benzene ND 0.20 4/27/22 7:02 BRFND40.640.15 0.48
Benzyl chloride ND 0.40 4/27/22 7:02 BRFND42.10.18 0.91
Bromodichloromethane ND 0.20 4/27/22 7:02 BRFND41.30.14 0.94
Bromoform ND 0.20 4/27/22 7:02 BRFND42.10.14 1.4
Bromomethane ND 0.20 4/27/22 7:02 BRFND40.780.13 0.52
1,3-Butadiene ND 0.20 4/27/22 7:02 BRFND40.440.17 0.37
2-Butanone (MEK)10 8.0 4/27/22 7:02 BRF30 4242.1 6.3
Carbon Disulfide 4.3 2.0 4/27/22 7:02 BRF13 46.20.18 0.58
Carbon Tetrachloride ND 0.20 4/27/22 7:02 BRFND41.30.16 1.0
Chlorobenzene ND 0.20 4/27/22 7:02 BRFND40.920.13 0.61
Chloroethane ND 0.20 4/27/22 7:02 BRFND40.530.18 0.47
Chloroform ND 0.20 4/27/22 7:02 BRFND40.980.19 0.93
Chloromethane 0.44 0.40 4/27/22 7:02 BRF0.90 40.830.16 0.33
Cyclohexane 2.5 0.20 4/27/22 7:02 BRF8.8 40.690.12 0.42
Dibromochloromethane ND 0.20 4/27/22 7:02 BRFND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 4/27/22 7:02 BRFND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 4/27/22 7:02 BRFND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 4/27/22 7:02 BRFND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 4/27/22 7:02 BRFND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)0.62 0.20 4/27/22 7:02 BRF3.0 40.990.20 0.97
1,1-Dichloroethane ND 0.20 4/27/22 7:02 BRFND40.810.17 0.71
1,2-Dichloroethane ND 0.20 4/27/22 7:02 BRFND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 4/27/22 7:02 BRFND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 4/27/22 7:02 BRFND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 4/27/22 7:02 BRFND40.790.16 0.62
1,2-Dichloropropane ND 0.20 4/27/22 7:02 BRFND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 4/27/22 7:02 BRFND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 4/27/22 7:02 BRFND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 4/27/22 7:02 BRFND41.40.20 1.4
1,4-Dioxane 3.0 2.0 4/27/22 7:02 BRF11 47.20.17 0.60
Ethanol 120 8.0 4/27/22 7:02 BRF240 4153.5 6.6
Ethyl Acetate 3.8 2.0 4/27/22 7:02 BRF14 47.21.0 3.6
Ethylbenzene 2.0 0.20 4/27/22 7:02 BRF8.7 40.870.12 0.51
4-Ethyltoluene ND 0.20 4/27/22 7:02 BRFND40.980.12 0.60
Heptane ND 0.20 4/27/22 7:02 BRFND40.820.13 0.52
Hexachlorobutadiene ND 0.20 4/27/22 7:02 BRFND42.10.16 1.8
Hexane 1.8 8.0 4/27/22 7:02 BRFJ6.3 4281.0 3.7
2-Hexanone (MBK)ND 0.20 4/27/22 7:02 BRFND40.820.10 0.41
Isopropanol 9.3 8.0 4/27/22 7:02 BRF23 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 4/27/22 7:02 BRFND40.720.15 0.56
Methylene Chloride ND 2.0 4/27/22 7:02 BRFND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 4/27/22 7:02 BRFND40.820.11 0.44
Naphthalene ND 0.20 4/27/22 7:02 BRFND41.00.15 0.79
Propene ND 8.0 4/27/22 7:02 BRFND4141.8 3.0
Styrene 0.24 0.20 4/27/22 7:02 BRF1.0 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 4/27/22 7:02 BRFND41.40.11 0.74
Page 12 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-5
Sample ID: 22D1698-05
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.7
Sampled: 4/20/2022 15:31
Canister ID: 3411
Flow Controller ID: 4346
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 65 0.20 4/27/22 7:02 BRF440 41.40.15 1.0
Tetrahydrofuran ND 2.0 4/27/22 7:02 BRFND45.90.33 0.97
Toluene 0.76 0.20 4/27/22 7:02 BRF2.9 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 4/27/22 7:02 BRFND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 4/27/22 7:02 BRFND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 4/27/22 7:02 BRFND41.10.14 0.77
Trichloroethylene ND 0.20 4/27/22 7:02 BRFND41.10.13 0.72
Trichlorofluoromethane (Freon 11)0.44 0.80 4/27/22 7:02 BRFJ2.4 44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.26 0.80 4/27/22 7:02 BRFJ2.0 46.10.22 1.7
1,2,4-Trimethylbenzene 0.33 0.20 4/27/22 7:02 BRF1.6 40.980.088 0.43
1,3,5-Trimethylbenzene 0.11 0.20 4/27/22 7:02 BRFJ0.53 40.980.11 0.52
Vinyl Acetate ND 4.0 4/27/22 7:02 BRFND4141.1 3.8
Vinyl Chloride ND 0.20 4/27/22 7:02 BRFND40.510.18 0.46
m&p-Xylene 8.0 0.40 4/27/22 7:02 BRF35 41.70.22 0.97
o-Xylene 3.4 0.20 4/27/22 7:02 BRF15 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)104 4/27/22 7:0270-130
Page 13 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-6
Sample ID: 22D1698-06
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.0
Sampled: 4/20/2022 15:52
Canister ID: 1334
Flow Controller ID: 4328
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 240 40 4/27/22 19:51 BRF570 20952457
Benzene ND 0.20 4/27/22 7:32 BRFND40.640.15 0.48
Benzyl chloride ND 0.40 4/27/22 7:32 BRFND42.10.18 0.91
Bromodichloromethane ND 0.20 4/27/22 7:32 BRFND41.30.14 0.94
Bromoform ND 0.20 4/27/22 7:32 BRFND42.10.14 1.4
Bromomethane 0.37 0.20 4/27/22 7:32 BRF1.4 40.780.13 0.52
1,3-Butadiene ND 0.20 4/27/22 7:32 BRFND40.440.17 0.37
2-Butanone (MEK)5.5 8.0 4/27/22 7:32 BRFJ16 4242.1 6.3
Carbon Disulfide 2.0 2.0 4/27/22 7:32 BRF6.2 46.20.18 0.58
Carbon Tetrachloride ND 0.20 4/27/22 7:32 BRFND41.30.16 1.0
Chlorobenzene ND 0.20 4/27/22 7:32 BRFND40.920.13 0.61
Chloroethane ND 0.20 4/27/22 7:32 BRFND40.530.18 0.47
Chloroform 0.24 0.20 4/27/22 7:32 BRF1.2 40.980.19 0.93
Chloromethane 1.7 0.40 4/27/22 7:32 BRF3.5 40.830.16 0.33
Cyclohexane 2.8 0.20 4/27/22 7:32 BRF9.6 40.690.12 0.42
Dibromochloromethane ND 0.20 4/27/22 7:32 BRFND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 4/27/22 7:32 BRFND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 4/27/22 7:32 BRFND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 4/27/22 7:32 BRFND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 4/27/22 7:32 BRFND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)0.99 0.20 4/27/22 7:32 BRF4.9 40.990.20 0.97
1,1-Dichloroethane ND 0.20 4/27/22 7:32 BRFND40.810.17 0.71
1,2-Dichloroethane ND 0.20 4/27/22 7:32 BRFND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 4/27/22 7:32 BRFND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 4/27/22 7:32 BRFND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 4/27/22 7:32 BRFND40.790.16 0.62
1,2-Dichloropropane ND 0.20 4/27/22 7:32 BRFND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 4/27/22 7:32 BRFND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 4/27/22 7:32 BRFND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 4/27/22 7:32 BRFND41.40.20 1.4
1,4-Dioxane ND 2.0 4/27/22 7:32 BRFND47.20.17 0.60
Ethanol 140 8.0 4/27/22 7:32 BRF260 4153.5 6.6
Ethyl Acetate 33 2.0 4/27/22 7:32 BRF120 47.21.0 3.6
Ethylbenzene 1.6 0.20 4/27/22 7:32 BRF6.8 40.870.12 0.51
4-Ethyltoluene ND 0.20 4/27/22 7:32 BRFND40.980.12 0.60
Heptane ND 0.20 4/27/22 7:32 BRFND40.820.13 0.52
Hexachlorobutadiene ND 0.20 4/27/22 7:32 BRFND42.10.16 1.8
Hexane 2.0 8.0 4/27/22 7:32 BRFJ7.1 4281.0 3.7
2-Hexanone (MBK)ND 0.20 4/27/22 7:32 BRFND40.820.10 0.41
Isopropanol 9.7 8.0 4/27/22 7:32 BRF24 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 4/27/22 7:32 BRFND40.720.15 0.56
Methylene Chloride ND 2.0 4/27/22 7:32 BRFND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 4/27/22 7:32 BRFND40.820.11 0.44
Naphthalene ND 0.20 4/27/22 7:32 BRFND41.00.15 0.79
Propene ND 8.0 4/27/22 7:32 BRFND4141.8 3.0
Styrene 0.27 0.20 4/27/22 7:32 BRF1.1 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 4/27/22 7:32 BRFND41.40.11 0.74
Page 14 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-6
Sample ID: 22D1698-06
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.0
Sampled: 4/20/2022 15:52
Canister ID: 1334
Flow Controller ID: 4328
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 140 0.20 4/27/22 7:32 BRF940 41.40.15 1.0
Tetrahydrofuran 1.0 2.0 4/27/22 7:32 BRFJ3.0 45.90.33 0.97
Toluene 0.99 0.20 4/27/22 7:32 BRF3.7 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 4/27/22 7:32 BRFND41.50.19 1.4
1,1,1-Trichloroethane 4.3 0.20 4/27/22 7:32 BRF23 41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 4/27/22 7:32 BRFND41.10.14 0.77
Trichloroethylene ND 0.20 4/27/22 7:32 BRFND41.10.13 0.72
Trichlorofluoromethane (Freon 11)0.65 0.80 4/27/22 7:32 BRFJ3.7 44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.36 0.80 4/27/22 7:32 BRFJ2.8 46.10.22 1.7
1,2,4-Trimethylbenzene 0.31 0.20 4/27/22 7:32 BRF1.5 40.980.088 0.43
1,3,5-Trimethylbenzene ND 0.20 4/27/22 7:32 BRFND40.980.11 0.52
Vinyl Acetate ND 4.0 4/27/22 7:32 BRFND4141.1 3.8
Vinyl Chloride ND 0.20 4/27/22 7:32 BRFND40.510.18 0.46
m&p-Xylene 7.0 0.40 4/27/22 7:32 BRF30 41.70.22 0.97
o-Xylene 3.0 0.20 4/27/22 7:32 BRF13 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)103 4/27/22 19:5170-130
4-Bromofluorobenzene (1)105 4/27/22 7:3270-130
Page 15 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-7
Sample ID: 22D1698-07
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.1
Sampled: 4/20/2022 16:09
Canister ID: 3427
Flow Controller ID: 4340
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 56 8.0 4/27/22 8:03 BRF130 4194.8 11
Benzene ND 0.20 4/27/22 8:03 BRFND40.640.15 0.48
Benzyl chloride ND 0.40 4/27/22 8:03 BRFND42.10.18 0.91
Bromodichloromethane ND 0.20 4/27/22 8:03 BRFND41.30.14 0.94
Bromoform ND 0.20 4/27/22 8:03 BRFND42.10.14 1.4
Bromomethane ND 0.20 4/27/22 8:03 BRFND40.780.13 0.52
1,3-Butadiene ND 0.20 4/27/22 8:03 BRFND40.440.17 0.37
2-Butanone (MEK)2.2 8.0 4/27/22 8:03 BRFJ6.4 4242.1 6.3
Carbon Disulfide 0.75 2.0 4/27/22 8:03 BRFJ2.3 46.20.18 0.58
Carbon Tetrachloride ND 0.20 4/27/22 8:03 BRFND41.30.16 1.0
Chlorobenzene ND 0.20 4/27/22 8:03 BRFND40.920.13 0.61
Chloroethane ND 0.20 4/27/22 8:03 BRFND40.530.18 0.47
Chloroform ND 0.20 4/27/22 8:03 BRFND40.980.19 0.93
Chloromethane ND 0.40 4/27/22 8:03 BRFND40.830.16 0.33
Cyclohexane 1.1 0.20 4/27/22 8:03 BRF3.7 40.690.12 0.42
Dibromochloromethane ND 0.20 4/27/22 8:03 BRFND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 4/27/22 8:03 BRFND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 4/27/22 8:03 BRFND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 4/27/22 8:03 BRFND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 4/27/22 8:03 BRFND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)400 1.0 4/27/22 20:22 BRF2000 204.90.98 4.8
1,1-Dichloroethane ND 0.20 4/27/22 8:03 BRFND40.810.17 0.71
1,2-Dichloroethane ND 0.20 4/27/22 8:03 BRFND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 4/27/22 8:03 BRFND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 4/27/22 8:03 BRFND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 4/27/22 8:03 BRFND40.790.16 0.62
1,2-Dichloropropane ND 0.20 4/27/22 8:03 BRFND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 4/27/22 8:03 BRFND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 4/27/22 8:03 BRFND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 4/27/22 8:03 BRFND41.40.20 1.4
1,4-Dioxane ND 2.0 4/27/22 8:03 BRFND47.20.17 0.60
Ethanol 84 8.0 4/27/22 8:03 BRF160 4153.5 6.6
Ethyl Acetate 5.4 2.0 4/27/22 8:03 BRF19 47.21.0 3.6
Ethylbenzene 1.3 0.20 4/27/22 8:03 BRF5.5 40.870.12 0.51
4-Ethyltoluene ND 0.20 4/27/22 8:03 BRFND40.980.12 0.60
Heptane ND 0.20 4/27/22 8:03 BRFND40.820.13 0.52
Hexachlorobutadiene ND 0.20 4/27/22 8:03 BRFND42.10.16 1.8
Hexane 1.7 8.0 4/27/22 8:03 BRFJ5.9 4281.0 3.7
2-Hexanone (MBK)ND 0.20 4/27/22 8:03 BRFND40.820.10 0.41
Isopropanol 7.9 8.0 4/27/22 8:03 BRFJ19 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 4/27/22 8:03 BRFND40.720.15 0.56
Methylene Chloride ND 2.0 4/27/22 8:03 BRFND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)1.4 0.20 4/27/22 8:03 BRF5.8 40.820.11 0.44
Naphthalene ND 0.20 4/27/22 8:03 BRFND41.00.15 0.79
Propene ND 8.0 4/27/22 8:03 BRFND4141.8 3.0
Styrene 0.17 0.20 4/27/22 8:03 BRFJ0.72 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 4/27/22 8:03 BRFND41.40.11 0.74
Page 16 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: SS-7
Sample ID: 22D1698-07
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.1
Sampled: 4/20/2022 16:09
Canister ID: 3427
Flow Controller ID: 4340
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 160 0.20 4/27/22 8:03 BRF1100 41.40.15 1.0
Tetrahydrofuran ND 2.0 4/27/22 8:03 BRFND45.90.33 0.97
Toluene 1.1 0.20 4/27/22 8:03 BRF4.0 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 4/27/22 8:03 BRFND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 4/27/22 8:03 BRFND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 4/27/22 8:03 BRFND41.10.14 0.77
Trichloroethylene ND 0.20 4/27/22 8:03 BRFND41.10.13 0.72
Trichlorofluoromethane (Freon 11)1.9 0.80 4/27/22 8:03 BRF11 44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 4/27/22 8:03 BRFND46.10.22 1.7
1,2,4-Trimethylbenzene 0.24 0.20 4/27/22 8:03 BRF1.2 40.980.088 0.43
1,3,5-Trimethylbenzene ND 0.20 4/27/22 8:03 BRFND40.980.11 0.52
Vinyl Acetate ND 4.0 4/27/22 8:03 BRFND4141.1 3.8
Vinyl Chloride ND 0.20 4/27/22 8:03 BRFND40.510.18 0.46
m&p-Xylene 5.1 0.40 4/27/22 8:03 BRF22 41.70.22 0.97
o-Xylene 2.3 0.20 4/27/22 8:03 BRF10 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)97.0 4/27/22 20:2270-130
4-Bromofluorobenzene (1)109 4/27/22 8:0370-130
Page 17 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: Dup
Sample ID: 22D1698-08
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.2
Sampled: 4/20/2022 13:32
Canister ID: 2492
Flow Controller ID: 4289
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 26 8.0 4/27/22 18:50 BRF61 4194.8 11
Benzene ND 0.20 4/27/22 18:50 BRFND40.640.15 0.48
Benzyl chloride ND 0.40 4/27/22 18:50 BRFND42.10.18 0.91
Bromodichloromethane ND 0.20 4/27/22 18:50 BRFND41.30.14 0.94
Bromoform ND 0.20 4/27/22 18:50 BRFND42.10.14 1.4
Bromomethane ND 0.20 4/27/22 18:50 BRFND40.780.13 0.52
1,3-Butadiene ND 0.20 4/27/22 18:50 BRFND40.440.17 0.37
2-Butanone (MEK)ND 8.0 4/27/22 18:50 BRFND4242.1 6.3
Carbon Disulfide 1.2 2.0 4/27/22 18:50 BRFJ3.8 46.20.18 0.58
Carbon Tetrachloride ND 0.20 4/27/22 18:50 BRFND41.30.16 1.0
Chlorobenzene ND 0.20 4/27/22 18:50 BRFND40.920.13 0.61
Chloroethane ND 0.20 4/27/22 18:50 BRFND40.530.18 0.47
Chloroform 6.7 0.20 4/27/22 18:50 BRF33 40.980.19 0.93
Chloromethane ND 0.40 4/27/22 18:50 BRFND40.830.16 0.33
Cyclohexane 1.3 0.20 4/27/22 18:50 BRF4.5 40.690.12 0.42
Dibromochloromethane ND 0.20 4/27/22 18:50 BRFND41.70.13 1.1
1,2-Dibromoethane (EDB)ND 0.20 4/27/22 18:50 BRFND41.50.12 0.93
1,2-Dichlorobenzene ND 0.20 4/27/22 18:50 BRFND41.20.11 0.69
1,3-Dichlorobenzene ND 0.20 4/27/22 18:50 BRFND41.20.11 0.67
1,4-Dichlorobenzene ND 0.20 4/27/22 18:50 BRFND41.20.13 0.79
Dichlorodifluoromethane (Freon 12)0.67 0.20 4/27/22 18:50 BRF3.3 40.990.20 0.97
1,1-Dichloroethane ND 0.20 4/27/22 18:50 BRFND40.810.17 0.71
1,2-Dichloroethane ND 0.20 4/27/22 18:50 BRFND40.810.18 0.73
1,1-Dichloroethylene ND 0.20 4/27/22 18:50 BRFND40.790.15 0.60
cis-1,2-Dichloroethylene ND 0.20 4/27/22 18:50 BRFND40.790.15 0.58
trans-1,2-Dichloroethylene ND 0.20 4/27/22 18:50 BRFND40.790.16 0.62
1,2-Dichloropropane ND 0.20 4/27/22 18:50 BRFND40.920.11 0.50
cis-1,3-Dichloropropene ND 0.20 4/27/22 18:50 BRFND40.910.10 0.47
trans-1,3-Dichloropropene ND 0.20 4/27/22 18:50 BRFND40.910.10 0.46
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 4/27/22 18:50 BRFND41.40.20 1.4
1,4-Dioxane ND 2.0 4/27/22 18:50 BRFND47.20.17 0.60
Ethanol 55 8.0 4/27/22 18:50 BRF100 4153.5 6.6
Ethyl Acetate ND 2.0 4/27/22 18:50 BRFND47.21.0 3.6
Ethylbenzene 0.96 0.20 4/27/22 18:50 BRF4.2 40.870.12 0.51
4-Ethyltoluene ND 0.20 4/27/22 18:50 BRFND40.980.12 0.60
Heptane ND 0.20 4/27/22 18:50 BRFND40.820.13 0.52
Hexachlorobutadiene ND 0.20 4/27/22 18:50 BRFND42.10.16 1.8
Hexane 1.7 8.0 4/27/22 18:50 BRFJ6.1 4281.0 3.7
2-Hexanone (MBK)ND 0.20 4/27/22 18:50 BRFND40.820.10 0.41
Isopropanol 4.2 8.0 4/27/22 18:50 BRFJ10 4201.4 3.4
Methyl tert-Butyl Ether (MTBE)ND 0.20 4/27/22 18:50 BRFND40.720.15 0.56
Methylene Chloride ND 2.0 4/27/22 18:50 BRFND46.90.93 3.2
4-Methyl-2-pentanone (MIBK)ND 0.20 4/27/22 18:50 BRFND40.820.11 0.44
Naphthalene ND 0.20 4/27/22 18:50 BRFND41.00.15 0.79
Propene ND 8.0 4/27/22 18:50 BRFND4141.8 3.0
Styrene 0.16 0.20 4/27/22 18:50 BRFJ0.66 40.850.11 0.45
1,1,2,2-Tetrachloroethane ND 0.20 4/27/22 18:50 BRFND41.40.11 0.74
Page 18 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1698Sample Description/Location:
Field Sample #: Dup
Sample ID: 22D1698-08
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.2
Sampled: 4/20/2022 13:32
Canister ID: 2492
Flow Controller ID: 4289
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 98 0.20 4/27/22 18:50 BRF670 41.40.15 1.0
Tetrahydrofuran ND 2.0 4/27/22 18:50 BRFND45.90.33 0.97
Toluene 0.63 0.20 4/27/22 18:50 BRF2.4 40.750.11 0.43
1,2,4-Trichlorobenzene ND 0.20 4/27/22 18:50 BRFND41.50.19 1.4
1,1,1-Trichloroethane ND 0.20 4/27/22 18:50 BRFND41.10.16 0.86
1,1,2-Trichloroethane ND 0.20 4/27/22 18:50 BRFND41.10.14 0.77
Trichloroethylene 0.14 0.20 4/27/22 18:50 BRFJ0.73 41.10.13 0.72
Trichlorofluoromethane (Freon 11)0.47 0.80 4/27/22 18:50 BRFJ2.7 44.50.24 1.3
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 4/27/22 18:50 BRFND46.10.22 1.7
1,2,4-Trimethylbenzene 0.22 0.20 4/27/22 18:50 BRF1.1 40.980.088 0.43
1,3,5-Trimethylbenzene ND 0.20 4/27/22 18:50 BRFND40.980.11 0.52
Vinyl Acetate ND 4.0 4/27/22 18:50 BRFV-05 ND 4141.1 3.8
Vinyl Chloride ND 0.20 4/27/22 18:50 BRFND40.510.18 0.46
m&p-Xylene 4.2 0.40 4/27/22 18:50 BRF18 41.70.22 0.97
o-Xylene 2.0 0.20 4/27/22 18:50 BRF8.6 40.870.10 0.44
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)104 4/27/22 18:5070-130
Page 19 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
22D1698-01 [SS-1]B306974 1.5 1 N/A 1000 200 75 04/26/22
22D1698-02 [SS-2]B306974 1.5 1 N/A 1000 200 75 04/26/22
22D1698-03 [SS-3]B306974 1.5 1 N/A 1000 200 75 04/26/22
22D1698-04 [SS-4]B306974 1.5 1 N/A 1000 200 75 04/26/22
22D1698-05 [SS-5]B306974 1.5 1 N/A 1000 200 75 04/26/22
22D1698-06 [SS-6]B306974 1.5 1 N/A 1000 200 75 04/26/22
22D1698-07 [SS-7]B306974 1.5 1 N/A 1000 200 75 04/26/22
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
22D1698-06RE1 [SS-6]B307102 1.5 1 N/A 1000 200 15 04/27/22
22D1698-07RE1 [SS-7]B307102 1.5 1 N/A 1000 200 15 04/27/22
22D1698-08 [Dup]B307102 1.5 1 N/A 1000 200 75 04/27/22
Page 20 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B306974 - TO-15 Prep
Blank (B306974-BLK1)Prepared & Analyzed: 04/26/22
0.80NDAcetone
0.020NDBenzene
0.040NDBenzyl chloride
0.020NDBromodichloromethane
0.020NDBromoform
0.020NDBromomethane
0.020ND1,3-Butadiene
0.80ND2-Butanone (MEK)
0.20NDCarbon Disulfide
0.020NDCarbon Tetrachloride
0.020NDChlorobenzene
0.020NDChloroethane
0.020NDChloroform
0.040NDChloromethane
0.020NDCyclohexane
0.020NDDibromochloromethane
0.020ND1,2-Dibromoethane (EDB)
0.020ND1,2-Dichlorobenzene
0.020ND1,3-Dichlorobenzene
0.020ND1,4-Dichlorobenzene
0.020NDDichlorodifluoromethane (Freon 12)
0.020ND1,1-Dichloroethane
0.020ND1,2-Dichloroethane
0.020ND1,1-Dichloroethylene
0.020NDcis-1,2-Dichloroethylene
0.020NDtrans-1,2-Dichloroethylene
0.020ND1,2-Dichloropropane
0.020NDcis-1,3-Dichloropropene
0.020NDtrans-1,3-Dichloropropene
0.020ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.20ND1,4-Dioxane
0.80NDEthanol
0.20NDEthyl Acetate
0.020NDEthylbenzene
0.020ND4-Ethyltoluene
0.020NDHeptane
0.020NDHexachlorobutadiene
0.80NDHexane
0.020ND2-Hexanone (MBK)
0.80NDIsopropanol
0.020NDMethyl tert-Butyl Ether (MTBE)
0.20NDMethylene Chloride
0.020ND4-Methyl-2-pentanone (MIBK)
0.020NDNaphthalene
0.80NDPropene
0.020NDStyrene
Page 21 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B306974 - TO-15 Prep
Blank (B306974-BLK1)Prepared & Analyzed: 04/26/22
0.020ND1,1,2,2-Tetrachloroethane
0.020NDTetrachloroethylene
0.20NDTetrahydrofuran
0.020NDToluene
0.020ND1,2,4-Trichlorobenzene
0.020ND1,1,1-Trichloroethane
0.020ND1,1,2-Trichloroethane
0.020NDTrichloroethylene
0.080NDTrichlorofluoromethane (Freon 11)
0.080ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.020ND1,2,4-Trimethylbenzene
0.020ND1,3,5-Trimethylbenzene
0.40NDVinyl Acetate
0.020NDVinyl Chloride
0.040NDm&p-Xylene
0.020NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1018.07
LCS (B306974-BS1)Prepared & Analyzed: 04/26/22
5.00 70-13090.14.50Acetone
5.00 70-13085.34.27Benzene
5.00 V-3670-1301145.71Benzyl chloride
5.00 70-13083.74.18Bromodichloromethane
5.00 70-13099.34.96Bromoform
5.00 70-1301035.13Bromomethane
5.00 70-13094.34.711,3-Butadiene
5.00 70-13086.34.322-Butanone (MEK)
5.00 70-13097.24.86Carbon Disulfide
5.00 70-13088.44.42Carbon Tetrachloride
5.00 70-13091.34.57Chlorobenzene
5.00 70-1301015.04Chloroethane
5.00 70-1301025.08Chloroform
5.00 70-13090.54.53Chloromethane
5.00 70-13090.64.53Cyclohexane
5.00 70-13094.44.72Dibromochloromethane
5.00 70-13093.44.671,2-Dibromoethane (EDB)
5.00 70-1301025.111,2-Dichlorobenzene
5.00 70-1301105.491,3-Dichlorobenzene
5.00 70-1301105.521,4-Dichlorobenzene
5.00 70-13097.94.90Dichlorodifluoromethane (Freon 12)
5.00 70-1301005.021,1-Dichloroethane
5.00 70-13093.84.691,2-Dichloroethane
5.00 70-13095.44.771,1-Dichloroethylene
5.00 70-13096.24.81cis-1,2-Dichloroethylene
5.00 70-13097.74.88trans-1,2-Dichloroethylene
5.00 70-13081.24.061,2-Dichloropropane
Page 22 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B306974 - TO-15 Prep
LCS (B306974-BS1)Prepared & Analyzed: 04/26/22
5.00 70-13085.84.29cis-1,3-Dichloropropene
5.00 70-13087.94.40trans-1,3-Dichloropropene
5.00 70-13095.14.751,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
5.00 70-13096.64.831,4-Dioxane
5.00 70-13090.04.50Ethanol
5.00 70-13092.44.62Ethyl Acetate
5.00 70-13089.14.46Ethylbenzene
5.00 70-13095.84.794-Ethyltoluene
5.00 70-13084.64.23Heptane
5.00 70-13093.54.68Hexachlorobutadiene
5.00 70-13092.14.61Hexane
5.00 70-13088.44.422-Hexanone (MBK)
5.00 70-13079.43.97Isopropanol
5.00 70-13098.94.94Methyl tert-Butyl Ether (MTBE)
5.00 70-13088.34.42Methylene Chloride
5.00 70-13082.04.104-Methyl-2-pentanone (MIBK)
5.00 70-13092.64.63Naphthalene
5.00 70-13088.54.42Propene
5.00 70-13097.64.88Styrene
5.00 70-13088.74.431,1,2,2-Tetrachloroethane
5.00 70-13093.94.70Tetrachloroethylene
5.00 70-13089.34.46Tetrahydrofuran
5.00 70-13089.04.45Toluene
5.00 V-3670-1301145.681,2,4-Trichlorobenzene
5.00 70-13085.54.271,1,1-Trichloroethane
5.00 70-13092.44.621,1,2-Trichloroethane
5.00 70-13088.54.43Trichloroethylene
5.00 70-1301025.11Trichlorofluoromethane (Freon 11)
5.00 70-13094.94.751,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-13095.54.781,2,4-Trimethylbenzene
5.00 70-1301015.031,3,5-Trimethylbenzene
5.00 70-13081.64.08Vinyl Acetate
5.00 70-13098.24.91Vinyl Chloride
10.0 70-13095.29.52m&p-Xylene
5.00 70-13094.64.73o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1088.63
Page 23 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B306974 - TO-15 Prep
Duplicate (B306974-DUP1)Prepared: 04/26/22 Analyzed: 04/27/22 Source: 22D1698-02
8.0 24 250.066424Acetone1957
0.20 ND 25NDBenzene0.64ND
0.40 ND 25NDBenzyl chloride 2.1ND
0.20 ND 25NDBromodichloromethane1.3ND
0.20 ND 25NDBromoform2.1ND
0.20 ND 25NDBromomethane0.78ND
0.20 ND 25ND1,3-Butadiene 0.44ND
8.0 ND 25ND2-Butanone (MEK)24ND
2.0 5.9 253.846.2Carbon Disulfide 6.219
0.20 ND 25NDCarbon Tetrachloride 1.3ND
0.20 ND 25NDChlorobenzene0.92ND
0.20 ND 25NDChloroethane0.53ND
0.20 ND 25NDChloroform0.98ND
0.40 ND 25NDChloromethane0.83ND
0.20 1.8 254.261.7Cyclohexane 0.696.0
0.20 ND 25NDDibromochloromethane1.7ND
0.20 ND 25ND1,2-Dibromoethane (EDB)1.5ND
0.20 ND 25ND1,2-Dichlorobenzene 1.2ND
0.20 ND 25ND1,3-Dichlorobenzene 1.2ND
0.20 ND 25ND1,4-Dichlorobenzene 1.2ND
0.20 ND 25NDDichlorodifluoromethane (Freon 12)0.99ND
0.20 ND 25ND1,1-Dichloroethane 0.81ND
0.20 ND 25ND1,2-Dichloroethane 0.81ND
0.20 ND 25ND1,1-Dichloroethylene 0.79ND
0.20 ND 25NDcis-1,2-Dichloroethylene 0.79ND
0.20 ND 25NDtrans-1,2-Dichloroethylene 0.79ND
0.20 ND 25ND1,2-Dichloropropane 0.92ND
0.20 ND 25NDcis-1,3-Dichloropropene 0.91ND
0.20 ND 25NDtrans-1,3-Dichloropropene 0.91ND
0.20 ND 25ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
1.4ND
2.0 ND 25ND1,4-Dioxane 7.2ND
8.0 72 251.0072Ethanol15140
2.0 ND 25NDEthyl Acetate 7.2ND
0.20 0.90 253.060.93Ethylbenzene 0.874.0
0.20 ND 25ND4-Ethyltoluene 0.98ND
0.20 ND 25NDHeptane0.82ND
0.20 ND 25NDHexachlorobutadiene2.1ND
8.0 ND 25NDHexane28ND
0.20 ND 25ND2-Hexanone (MBK)0.82ND
8.0 3.6 25 J0.7853.6Isopropanol 208.8
0.20 ND 25NDMethyl tert-Butyl Ether (MTBE)0.72ND
2.0 ND 25NDMethylene Chloride 6.9ND
0.20 ND 25ND4-Methyl-2-pentanone (MIBK)0.82ND
0.20 ND 25NDNaphthalene1.0ND
8.0 ND 25NDPropene14ND
0.20 ND 25NDStyrene0.85ND
Page 24 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B306974 - TO-15 Prep
Duplicate (B306974-DUP1)Prepared: 04/26/22 Analyzed: 04/27/22 Source: 22D1698-02
0.20 ND 25ND1,1,2,2-Tetrachloroethane 1.4ND
0.20 0.43 256.280.46Tetrachloroethylene 1.43.1
2.0 ND 25NDTetrahydrofuran5.9ND
0.20 0.57 253.440.59Toluene 0.752.2
0.20 ND 25ND1,2,4-Trichlorobenzene 1.5ND
0.20 ND 25ND1,1,1-Trichloroethane 1.1ND
0.20 ND 25ND1,1,2-Trichloroethane 1.1ND
0.20 ND 25NDTrichloroethylene1.1ND
0.80 0.70 25 J2.800.72Trichlorofluoromethane (Freon 11)4.54.1
0.80 0.91 250.4400.911,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
6.17.0
0.20 0.20 250.000.201,2,4-Trimethylbenzene 0.980.98
0.20 ND 25ND1,3,5-Trimethylbenzene 0.98ND
4.0 ND 25NDVinyl Acetate 14ND
0.20 ND 25NDVinyl Chloride 0.51ND
0.40 4.3 250.09324.3m&p-Xylene 1.719
0.20 1.9 252.551.9o-Xylene 0.878.3
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1078.56
Batch B307102 - TO-15 Prep
Blank (B307102-BLK1)Prepared & Analyzed: 04/27/22
0.80NDAcetone
0.020NDBenzene
0.040NDBenzyl chloride
0.020NDBromodichloromethane
0.020NDBromoform
0.020NDBromomethane
0.020ND1,3-Butadiene
0.80ND2-Butanone (MEK)
0.20NDCarbon Disulfide
0.020NDCarbon Tetrachloride
0.020NDChlorobenzene
0.020NDChloroethane
0.020NDChloroform
0.040NDChloromethane
0.020NDCyclohexane
0.020NDDibromochloromethane
0.020ND1,2-Dibromoethane (EDB)
0.020ND1,2-Dichlorobenzene
0.020ND1,3-Dichlorobenzene
0.020ND1,4-Dichlorobenzene
0.020NDDichlorodifluoromethane (Freon 12)
0.020ND1,1-Dichloroethane
0.020ND1,2-Dichloroethane
0.020ND1,1-Dichloroethylene
0.020NDcis-1,2-Dichloroethylene
Page 25 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B307102 - TO-15 Prep
Blank (B307102-BLK1)Prepared & Analyzed: 04/27/22
0.020NDtrans-1,2-Dichloroethylene
0.020ND1,2-Dichloropropane
0.020NDcis-1,3-Dichloropropene
0.020NDtrans-1,3-Dichloropropene
0.020ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.20ND1,4-Dioxane
0.80NDEthanol
0.20NDEthyl Acetate
0.020NDEthylbenzene
0.020ND4-Ethyltoluene
0.020NDHeptane
0.020NDHexachlorobutadiene
0.80NDHexane
0.020ND2-Hexanone (MBK)
0.80NDIsopropanol
0.020NDMethyl tert-Butyl Ether (MTBE)
0.20NDMethylene Chloride
0.020ND4-Methyl-2-pentanone (MIBK)
0.020NDNaphthalene
0.80NDPropene
0.020NDStyrene
0.020ND1,1,2,2-Tetrachloroethane
0.020NDTetrachloroethylene
0.20NDTetrahydrofuran
0.020NDToluene
0.020ND1,2,4-Trichlorobenzene
0.020ND1,1,1-Trichloroethane
0.020ND1,1,2-Trichloroethane
0.020NDTrichloroethylene
0.080NDTrichlorofluoromethane (Freon 11)
0.080ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.020ND1,2,4-Trimethylbenzene
0.020ND1,3,5-Trimethylbenzene
0.40 V-05NDVinyl Acetate
0.020NDVinyl Chloride
0.040NDm&p-Xylene
0.020NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)98.87.90
Page 26 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B307102 - TO-15 Prep
LCS (B307102-BS1)Prepared & Analyzed: 04/27/22
5.00 70-13096.64.83Acetone
5.00 70-13091.04.55Benzene
5.00 L-01,
V-20,
70-1301366.82Benzyl chloride *
5.00 70-13088.04.40Bromodichloromethane
5.00 70-1301045.21Bromoform
5.00 70-1301095.46Bromomethane
5.00 70-13099.95.001,3-Butadiene
5.00 70-13095.34.772-Butanone (MEK)
5.00 70-1301055.23Carbon Disulfide
5.00 70-13093.14.65Carbon Tetrachloride
5.00 70-13098.44.92Chlorobenzene
5.00 70-1301065.30Chloroethane
5.00 70-1301075.36Chloroform
5.00 70-13096.74.84Chloromethane
5.00 70-13096.94.84Cyclohexane
5.00 70-13099.95.00Dibromochloromethane
5.00 70-1301005.011,2-Dibromoethane (EDB)
5.00 70-1301135.641,2-Dichlorobenzene
5.00 70-1301185.921,3-Dichlorobenzene
5.00 70-1301155.751,4-Dichlorobenzene
5.00 70-1301055.23Dichlorodifluoromethane (Freon 12)
5.00 70-1301055.251,1-Dichloroethane
5.00 70-1301005.011,2-Dichloroethane
5.00 70-1301025.121,1-Dichloroethylene
5.00 70-1301025.10cis-1,2-Dichloroethylene
5.00 70-1301025.12trans-1,2-Dichloroethylene
5.00 70-13087.04.351,2-Dichloropropane
5.00 70-13089.94.50cis-1,3-Dichloropropene
5.00 70-13093.84.69trans-1,3-Dichloropropene
5.00 70-1301015.041,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
5.00 70-1301055.231,4-Dioxane
5.00 70-13092.24.61Ethanol
5.00 70-1301025.09Ethyl Acetate
5.00 70-13096.04.80Ethylbenzene
5.00 70-1301065.284-Ethyltoluene
5.00 70-13090.84.54Heptane
5.00 70-1301035.14Hexachlorobutadiene
5.00 70-13096.74.84Hexane
5.00 70-13091.84.592-Hexanone (MBK)
5.00 70-13086.54.32Isopropanol
5.00 70-1301055.26Methyl tert-Butyl Ether (MTBE)
5.00 70-13091.84.59Methylene Chloride
5.00 70-13088.34.424-Methyl-2-pentanone (MIBK)
5.00 70-13097.64.88Naphthalene
5.00 70-13094.34.71Propene
Page 27 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B307102 - TO-15 Prep
LCS (B307102-BS1)Prepared & Analyzed: 04/27/22
5.00 70-1301065.28Styrene
5.00 70-13095.34.761,1,2,2-Tetrachloroethane
5.00 70-1301015.06Tetrachloroethylene
5.00 70-13096.74.84Tetrahydrofuran
5.00 70-13095.14.75Toluene
5.00 V-3670-1301175.851,2,4-Trichlorobenzene
5.00 70-13090.74.531,1,1-Trichloroethane
5.00 70-13098.44.921,1,2-Trichloroethane
5.00 70-13092.94.64Trichloroethylene
5.00 70-1301085.42Trichlorofluoromethane (Freon 11)
5.00 70-1301155.751,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-1301065.311,2,4-Trimethylbenzene
5.00 70-1301095.441,3,5-Trimethylbenzene
5.00 V-0570-13077.13.86Vinyl Acetate
5.00 70-1301045.20Vinyl Chloride
10.0 70-13010210.2m&p-Xylene
5.00 70-1301015.07o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1088.65
Duplicate (B307102-DUP1)Prepared & Analyzed: 04/27/22 Source: 22D1698-08
8.0 26 250.56525Acetone1960
0.20 ND 25NDBenzene0.64ND
0.40 ND 25NDBenzyl chloride 2.1ND
0.20 ND 25NDBromodichloromethane1.3ND
0.20 ND 25NDBromoform2.1ND
0.20 ND 25NDBromomethane0.78ND
0.20 ND 25ND1,3-Butadiene 0.44ND
8.0 ND 25 J2.22-Butanone (MEK)246.5
2.0 1.2 25 J0.6541.2Carbon Disulfide 6.23.8
0.20 ND 25NDCarbon Tetrachloride 1.3ND
0.20 ND 25NDChlorobenzene0.92ND
0.20 ND 25NDChloroethane0.53ND
0.20 6.7 250.7776.7Chloroform 0.9833
0.40 ND 25NDChloromethane0.83ND
0.20 1.3 251.221.3Cyclohexane 0.694.5
0.20 ND 25NDDibromochloromethane1.7ND
0.20 ND 25ND1,2-Dibromoethane (EDB)1.5ND
0.20 ND 25ND1,2-Dichlorobenzene 1.2ND
0.20 ND 25ND1,3-Dichlorobenzene 1.2ND
0.20 ND 25ND1,4-Dichlorobenzene 1.2ND
0.20 0.67 255.250.70Dichlorodifluoromethane (Freon 12)0.993.5
0.20 ND 25ND1,1-Dichloroethane 0.81ND
0.20 ND 25ND1,2-Dichloroethane 0.81ND
0.20 ND 25ND1,1-Dichloroethylene 0.79ND
0.20 ND 25NDcis-1,2-Dichloroethylene 0.79ND
0.20 ND 25NDtrans-1,2-Dichloroethylene 0.79ND
Page 28 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B307102 - TO-15 Prep
Duplicate (B307102-DUP1)Prepared & Analyzed: 04/27/22 Source: 22D1698-08
0.20 ND 25ND1,2-Dichloropropane 0.92ND
0.20 ND 25NDcis-1,3-Dichloropropene 0.91ND
0.20 ND 25NDtrans-1,3-Dichloropropene 0.91ND
0.20 ND 25ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
1.4ND
2.0 ND 25ND1,4-Dioxane 7.2ND
8.0 55 250.38155Ethanol15100
2.0 ND 25NDEthyl Acetate 7.2ND
0.20 0.96 251.650.98Ethylbenzene 0.874.3
0.20 ND 25ND4-Ethyltoluene 0.98ND
0.20 ND 25NDHeptane0.82ND
0.20 ND 25NDHexachlorobutadiene2.1ND
8.0 1.7 25 J4.771.8Hexane 286.4
0.20 ND 25ND2-Hexanone (MBK)0.82ND
8.0 4.2 25 J0.2874.2Isopropanol 2010
0.20 ND 25NDMethyl tert-Butyl Ether (MTBE)0.72ND
2.0 ND 25NDMethylene Chloride 6.9ND
0.20 ND 25ND4-Methyl-2-pentanone (MIBK)0.82ND
0.20 ND 25NDNaphthalene1.0ND
8.0 ND 25NDPropene14ND
0.20 0.16 25 J7.410.17Styrene 0.850.72
0.20 ND 25ND1,1,2,2-Tetrachloroethane 1.4ND
0.20 98 250.37499Tetrachloroethylene1.4670
2.0 ND 25NDTetrahydrofuran5.9ND
0.20 0.63 251.930.62Toluene 0.752.3
0.20 ND 25ND1,2,4-Trichlorobenzene 1.5ND
0.20 ND 25ND1,1,1-Trichloroethane 1.1ND
0.20 ND 25ND1,1,2-Trichloroethane 1.1ND
0.20 0.14 25 J8.450.15Trichloroethylene 1.10.80
0.80 0.47 25 J1.710.46Trichlorofluoromethane (Freon 11)4.52.6
0.80 ND 25ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
6.1ND
0.20 0.22 256.900.241,2,4-Trimethylbenzene 0.981.2
0.20 ND 25ND1,3,5-Trimethylbenzene 0.98ND
4.0 ND 25 V-05NDVinyl Acetate 14ND
0.20 ND 25NDVinyl Chloride 0.51ND
0.40 4.2 252.094.3m&p-Xylene 1.718
0.20 2.0 250.4022.0o-Xylene 0.878.7
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1038.20
Page 29 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Note: Blank Subtraction is not performed unless otherwise noted
*QC result is outside of established limits.
†Wide recovery limits established for difficult compound.
‡Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramµg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not
affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high
side.
L-01
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data
validation is not affected since sample result was "not detected" for this compound.
V-36
Page 30 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYST
Thomas P. HniteckiTPH
Raisa A. PetraitisRAP
PDF Management StationSTATION
Kerry K. McGeeKKM
Brittany R. FiskBRF
Page 31 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S069304-ICV1 )Lab File ID: K22A075019.D Analyzed: 03/16/22 23:55
Bromochloromethane (1)104138 2.987 102745 2.987 60 - 140101 0.0000 +/-0.50
1,4-Difluorobenzene (1)315817 3.584 303801 3.579 60 - 140104 0.0050 +/-0.50
Chlorobenzene-d5 (1)233658 5.159 223280 5.159 60 - 140105 0.0000 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S070889-CCV1 )Lab File ID: K22A116004.D Analyzed: 04/26/22 09:00
Bromochloromethane (1)97154 2.992 102745 2.987 60 - 14095 0.0050 +/-0.50
1,4-Difluorobenzene (1)323453 3.584 303801 3.579 60 - 140106 0.0050 +/-0.50
Chlorobenzene-d5 (1)241568 5.159 223280 5.159 60 - 140108 0.0000 +/-0.50
LCS (B306974-BS1 )Lab File ID: K22A116005.D Analyzed: 04/26/22 09:31
Bromochloromethane (1)95505 2.991 97154 2.992 60 - 14098 -0.0010 +/-0.50
1,4-Difluorobenzene (1)326455 3.584 323453 3.584 60 - 140101 0.0000 +/-0.50
Chlorobenzene-d5 (1)238868 5.159 241568 5.159 60 - 14099 0.0000 +/-0.50
Blank (B306974-BLK1 )Lab File ID: K22A116008.D Analyzed: 04/26/22 11:24
Bromochloromethane (1)93530 2.992 97154 2.992 60 - 14096 0.0000 +/-0.50
1,4-Difluorobenzene (1)297714 3.584 323453 3.584 60 - 14092 0.0000 +/-0.50
Chlorobenzene-d5 (1)225983 5.159 241568 5.159 60 - 14094 0.0000 +/-0.50
SS-1 (22D1698-01 )Lab File ID: K22A116038.D Analyzed: 04/27/22 04:30
Bromochloromethane (1)91306 2.992 97154 2.992 60 - 14094 0.0000 +/-0.50
1,4-Difluorobenzene (1)313860 3.584 323453 3.584 60 - 14097 0.0000 +/-0.50
Chlorobenzene-d5 (1)231103 5.159 241568 5.159 60 - 14096 0.0000 +/-0.50
SS-2 (22D1698-02 )Lab File ID: K22A116039.D Analyzed: 04/27/22 05:01
Bromochloromethane (1)91421 2.992 97154 2.992 60 - 14094 0.0000 +/-0.50
1,4-Difluorobenzene (1)296991 3.584 323453 3.584 60 - 14092 0.0000 +/-0.50
Chlorobenzene-d5 (1)227489 5.159 241568 5.159 60 - 14094 0.0000 +/-0.50
Duplicate (B306974-DUP1 )Lab File ID: K22A116040.D Analyzed: 04/27/22 05:31
Bromochloromethane (1)91778 2.992 97154 2.992 60 - 14094 0.0000 +/-0.50
1,4-Difluorobenzene (1)295021 3.584 323453 3.584 60 - 14091 0.0000 +/-0.50
Chlorobenzene-d5 (1)225590 5.159 241568 5.159 60 - 14093 0.0000 +/-0.50
SS-3 (22D1698-03 )Lab File ID: K22A116041.D Analyzed: 04/27/22 06:02
Bromochloromethane (1)93513 2.992 97154 2.992 60 - 14096 0.0000 +/-0.50
1,4-Difluorobenzene (1)306768 3.584 323453 3.584 60 - 14095 0.0000 +/-0.50
Chlorobenzene-d5 (1)233284 5.159 241568 5.159 60 - 14097 0.0000 +/-0.50
Page 32 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SS-4 (22D1698-04 )Lab File ID: K22A116042.D Analyzed: 04/27/22 06:32
Bromochloromethane (1)90358 2.996 97154 2.992 60 - 14093 0.0040 +/-0.50
1,4-Difluorobenzene (1)294607 3.589 323453 3.584 60 - 14091 0.0050 +/-0.50
Chlorobenzene-d5 (1)226048 5.159 241568 5.159 60 - 14094 0.0000 +/-0.50
SS-5 (22D1698-05 )Lab File ID: K22A116043.D Analyzed: 04/27/22 07:02
Bromochloromethane (1)91615 2.996 97154 2.992 60 - 14094 0.0040 +/-0.50
1,4-Difluorobenzene (1)302447 3.584 323453 3.584 60 - 14094 0.0000 +/-0.50
Chlorobenzene-d5 (1)239199 5.159 241568 5.159 60 - 14099 0.0000 +/-0.50
SS-6 (22D1698-06 )Lab File ID: K22A116044.D Analyzed: 04/27/22 07:32
Bromochloromethane (1)92258 2.996 97154 2.992 60 - 14095 0.0040 +/-0.50
1,4-Difluorobenzene (1)314922 3.588 323453 3.584 60 - 14097 0.0040 +/-0.50
Chlorobenzene-d5 (1)233794 5.159 241568 5.159 60 - 14097 0.0000 +/-0.50
SS-7 (22D1698-07 )Lab File ID: K22A116045.D Analyzed: 04/27/22 08:03
Bromochloromethane (1)93688 2.996 97154 2.992 60 - 14096 0.0040 +/-0.50
1,4-Difluorobenzene (1)305412 3.588 323453 3.584 60 - 14094 0.0040 +/-0.50
Chlorobenzene-d5 (1)247846 5.159 241568 5.159 60 - 140103 0.0000 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S070925-CCV1 )Lab File ID: K22A117004.D Analyzed: 04/27/22 11:56
Bromochloromethane (1)95483 2.992 102745 2.987 60 - 14093 0.0050 +/-0.50
1,4-Difluorobenzene (1)326692 3.584 303801 3.579 60 - 140108 0.0050 +/-0.50
Chlorobenzene-d5 (1)240375 5.159 223280 5.159 60 - 140108 0.0000 +/-0.50
LCS (B307102-BS1 )Lab File ID: K22A117005.D Analyzed: 04/27/22 12:27
Bromochloromethane (1)95373 2.992 95483 2.992 60 - 140100 0.0000 +/-0.50
1,4-Difluorobenzene (1)328630 3.584 326692 3.584 60 - 140101 0.0000 +/-0.50
Chlorobenzene-d5 (1)238104 5.159 240375 5.159 60 - 14099 0.0000 +/-0.50
Blank (B307102-BLK1 )Lab File ID: K22A117008.D Analyzed: 04/27/22 14:15
Bromochloromethane (1)94259 2.992 95483 2.992 60 - 14099 0.0000 +/-0.50
1,4-Difluorobenzene (1)301627 3.584 326692 3.584 60 - 14092 0.0000 +/-0.50
Chlorobenzene-d5 (1)228891 5.159 240375 5.159 60 - 14095 0.0000 +/-0.50
Dup (22D1698-08 )Lab File ID: K22A117016.D Analyzed: 04/27/22 18:50
Bromochloromethane (1)96696 2.996 95483 2.992 60 - 140101 0.0040 +/-0.50
1,4-Difluorobenzene (1)323273 3.584 326692 3.584 60 - 14099 0.0000 +/-0.50
Chlorobenzene-d5 (1)242782 5.159 240375 5.159 60 - 140101 0.0000 +/-0.50
Page 33 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Duplicate (B307102-DUP1 )Lab File ID: K22A117017.D Analyzed: 04/27/22 19:20
Bromochloromethane (1)96051 2.996 95483 2.992 60 - 140101 0.0040 +/-0.50
1,4-Difluorobenzene (1)320993 3.588 326692 3.584 60 - 14098 0.0040 +/-0.50
Chlorobenzene-d5 (1)237539 5.159 240375 5.159 60 - 14099 0.0000 +/-0.50
SS-6 (22D1698-06RE1 )Lab File ID: K22A117018.D Analyzed: 04/27/22 19:51
Bromochloromethane (1)94197 2.996 95483 2.992 60 - 14099 0.0040 +/-0.50
1,4-Difluorobenzene (1)312746 3.588 326692 3.584 60 - 14096 0.0040 +/-0.50
Chlorobenzene-d5 (1)224243 5.163 240375 5.159 60 - 14093 0.0040 +/-0.50
SS-7 (22D1698-07RE1 )Lab File ID: K22A117019.D Analyzed: 04/27/22 20:22
Bromochloromethane (1)96210 2.996 95483 2.992 60 - 140101 0.0040 +/-0.50
1,4-Difluorobenzene (1)312081 3.588 326692 3.584 60 - 14096 0.0040 +/-0.50
Chlorobenzene-d5 (1)238554 5.159 240375 5.159 60 - 14099 0.0000 +/-0.50
Page 34 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S070889-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.927056A -7.3 304.63 1.0005655.00Acetone
0.6016825A -4.9 304.75 0.63275915.00Benzene
0.558266A 26.3 306.31 0.44216445.00Benzyl chloride
0.4207498A -6.1 304.69 0.44785535.00Bromodichloromethane
0.5780501A 9.1 305.44 0.53002115.00Bromoform
0.6436626A 13.3 305.66 0.56819065.00Bromomethane
0.5239023A 6.1 305.30 0.49389165.001,3-Butadiene
1.047047A -8.4 304.58 1.1427965.002-Butanone (MEK)
2.174346A 4.1 305.17 2.0889415.00Carbon Disulfide
0.360223A 0.7 305.03 0.35787875.00Carbon Tetrachloride
0.7411511A 1.4 305.07 0.73082645.00Chlorobenzene
0.3944912A 5.8 305.29 0.37271415.00Chloroethane
1.335414A 10.8 305.54 1.2054345.00Chloroform
0.590617A 1.1 305.05 0.58407155.00Chloromethane
0.2455553A -0.6 304.96 0.24707665.00Cyclohexane
0.5608889A 4.5 305.23 0.53660835.00Dibromochloromethane
0.4873493A 3.7 305.19 0.46991195.001,2-Dibromoethane (EDB)
0.6135382A 13.1 305.65 0.54259785.001,2-Dichlorobenzene
0.6597894A 18.0 305.92 0.55904685.001,3-Dichlorobenzene
0.5386011A 11.2 305.56 0.48421685.001,4-Dichlorobenzene
1.519188A 5.7 305.28 1.4366615.00Dichlorodifluoromethane (Freon 12)
1.054211A 6.2 305.31 0.99287285.001,1-Dichloroethane
0.7768944A 2.2 305.11 0.76016775.001,2-Dichloroethane
1.04512A 2.0 305.10 1.0249615.001,1-Dichloroethylene
0.8506412A 4.1 305.20 0.81706385.00cis-1,2-Dichloroethylene
0.8763818A 6.1 305.30 0.82618555.00trans-1,2-Dichloroethylene
0.2320906A -8.0 304.60 0.25221315.001,2-Dichloropropane
0.3947553A -2.2 304.88 0.40368315.00cis-1,3-Dichloropropene
0.2769763A -1.7 304.91 0.28179515.00trans-1,3-Dichloropropene
1.72592A 9.9 305.49 1.5704175.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.126866A 1.5 305.06 0.12504885.001,4-Dioxane
0.2202853A -6.1 304.69 0.23459935.00Ethanol
0.1727237A -3.9 304.80 0.1796975.00Ethyl Acetate
1.152524A -1.2 304.94 1.1663635.00Ethylbenzene
1.167989A 7.0 305.35 1.0916415.004-Ethyltoluene
0.2258776A -4.6 304.76 0.23675525.00Heptane
0.3967943A 3.1 305.16 0.38473725.00Hexachlorobutadiene
0.6149248L -2.0 304.90 0.61131925.00Hexane
Page 35 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S070889-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.4998079A -5.6 304.72 0.52939375.002-Hexanone (MBK)
1.220775A -0.9 304.95 1.2321385.00Isopropanol
1.507512A 7.4 305.37 1.4032345.00Methyl tert-Butyl Ether (MTBE)
0.7417337A -4.2 304.79 0.7746185.00Methylene Chloride
9.122067E-02A -11.9 304.40 0.10352975.004-Methyl-2-pentanone (MIBK)
0.8632667A -4.8 304.76 0.90681415.00Naphthalene
0.4648126A -2.2 304.88 0.47538415.00Propene
0.6810703A 9.9 305.50 0.6196185.00Styrene
0.739853A -3.3 304.84 0.76502585.001,1,2,2-Tetrachloroethane
0.420208A 4.4 305.22 0.40258465.00Tetrachloroethylene
0.6004158A -3.0 304.85 0.61895225.00Tetrahydrofuran
0.9408531A -1.9 304.91 0.95897385.00Toluene
0.3443171A 19.2 305.96 0.28888655.001,2,4-Trichlorobenzene
0.3961107A -1.0 304.94 0.39993535.001,1,1-Trichloroethane
0.3363359A 0.7 305.04 0.33398865.001,1,2-Trichloroethane
0.2622897A -1.6 304.91 0.26654695.00Trichloroethylene
1.519205A 11.5 305.57 1.3626215.00Trichlorofluoromethane (Freon 11)
1.534356A 17.4 305.85 1.3073015.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
0.9776527A 7.4 305.37 0.91020485.001,2,4-Trimethylbenzene
1.041893A 11.8 305.60 0.93205925.001,3,5-Trimethylbenzene
1.353875A -8.0 304.65 1.4714225.00Vinyl Acetate
0.7098009A 6.0 305.30 0.6697665.00Vinyl Chloride
1.036167A 5.0 3010.5 0.987220410.0m&p-Xylene
0.9378792A 4.1 305.21 0.9007275.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 36 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S070925-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.9708786A -3.0 304.85 1.0005655.00Acetone
0.619343A -2.1 304.89 0.63275915.00Benzene
0.6386222A 44.4 *307.22 0.44216445.00Benzyl chloride
0.4225142A -5.7 304.71 0.44785535.00Bromodichloromethane
0.5974931A 12.7 305.62 0.53002115.00Bromoform
0.6725721A 18.4 305.92 0.56819065.00Bromomethane
0.5546705A 12.3 305.61 0.49389165.001,3-Butadiene
1.061969A -7.1 304.64 1.1427965.002-Butanone (MEK)
2.319927A 11.1 305.52 2.0889415.00Carbon Disulfide
0.3647717A 1.9 305.09 0.35787875.00Carbon Tetrachloride
0.7645121A 4.6 305.23 0.73082645.00Chlorobenzene
0.417733A 12.1 305.60 0.37271415.00Chloroethane
1.408703A 16.9 305.84 1.2054345.00Chloroform
0.6059634A 3.7 305.18 0.58407155.00Chloromethane
0.2533959A 2.6 305.12 0.24707665.00Cyclohexane
0.5723657A 6.7 305.33 0.53660835.00Dibromochloromethane
0.5054236A 7.6 305.38 0.46991195.001,2-Dibromoethane (EDB)
0.6551497A 20.7 306.04 0.54259785.001,2-Dichlorobenzene
0.7021695A 25.6 306.29 0.55904685.001,3-Dichlorobenzene
0.5663884A 17.0 305.85 0.48421685.001,4-Dichlorobenzene
1.586745A 10.4 305.52 1.4366615.00Dichlorodifluoromethane (Freon 12)
1.121473A 13.0 305.64 0.99287285.001,1-Dichloroethane
0.8104814A 6.6 305.33 0.76016775.001,2-Dichloroethane
1.119579A 9.2 305.46 1.0249615.001,1-Dichloroethylene
0.8993433A 10.1 305.50 0.81706385.00cis-1,2-Dichloroethylene
0.910671A 10.2 305.51 0.82618555.00trans-1,2-Dichloroethylene
0.2313421A -8.3 304.58 0.25221315.001,2-Dichloropropane
0.402341A -0.3 304.98 0.40368315.00cis-1,3-Dichloropropene
0.2865721A 1.7 305.08 0.28179515.00trans-1,3-Dichloropropene
1.769815A 12.7 305.63 1.5704175.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.1302168A 4.1 305.20 0.12504885.001,4-Dioxane
0.241333A 2.9 305.14 0.23459935.00Ethanol
0.1809579A 0.7 305.03 0.1796975.00Ethyl Acetate
1.201489A 3.0 305.15 1.1663635.00Ethylbenzene
1.234697A 13.1 305.66 1.0916415.004-Ethyltoluene
0.2321844A -1.9 304.90 0.23675525.00Heptane
0.4222269A 9.7 305.49 0.38473725.00Hexachlorobutadiene
0.6448226L 2.5 305.12 0.61131925.00Hexane
Page 37 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S070925-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.523502A -1.1 304.94 0.52939375.002-Hexanone (MBK)
1.306955A 6.1 305.30 1.2321385.00Isopropanol
1.57778A 12.4 305.62 1.4032345.00Methyl tert-Butyl Ether (MTBE)
0.7747222A 0.01 305.00 0.7746185.00Methylene Chloride
9.036034E-02A -12.7 304.36 0.10352975.004-Methyl-2-pentanone (MIBK)
0.910098A 0.4 305.02 0.90681415.00Naphthalene
0.4918321A 3.5 305.17 0.47538415.00Propene
0.7058771A 13.9 305.70 0.6196185.00Styrene
0.7796751A 1.9 305.10 0.76502585.001,1,2,2-Tetrachloroethane
0.4361851A 8.3 305.42 0.40258465.00Tetrachloroethylene
0.6448562A 4.2 305.21 0.61895225.00Tetrahydrofuran
0.9707033A 1.2 305.06 0.95897385.00Toluene
0.3455201A 19.6 305.98 0.28888655.001,2,4-Trichlorobenzene
0.412288A 3.1 305.15 0.39993535.001,1,1-Trichloroethane
0.3455401A 3.5 305.17 0.33398865.001,1,2-Trichloroethane
0.2683825A 0.7 305.03 0.26654695.00Trichloroethylene
1.554103A 14.1 305.70 1.3626215.00Trichlorofluoromethane (Freon 11)
1.597017A 22.2 306.09 1.3073015.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
1.031668A 13.3 305.67 0.91020485.001,2,4-Trimethylbenzene
1.086922A 16.6 305.84 0.93205925.001,3,5-Trimethylbenzene
0.9927128A -32.5 *303.41 1.4714225.00Vinyl Acetate
0.7492014A 11.9 305.59 0.6697665.00Vinyl Chloride
1.083487A 9.8 3010.9 0.987220410.0m&p-Xylene
0.9749699A 8.2 305.41 0.9007275.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 38 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,ME,NHAcetone
AIHA,FL,NJ,NY,ME,NH,VABenzene
AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride
AIHA,NJ,NY,ME,NH,VABromodichloromethane
AIHA,NJ,NY,ME,NH,VABromoform
AIHA,FL,NJ,NY,ME,NHBromomethane
AIHA,NJ,NY,ME,NH,VA1,3-Butadiene
AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
AIHA,NJ,NY,ME,NH,VACarbon Disulfide
AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride
AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene
AIHA,FL,NJ,NY,ME,NH,VAChloroethane
AIHA,FL,NJ,NY,ME,NH,VAChloroform
AIHA,FL,NJ,NY,ME,NH,VAChloromethane
AIHA,NJ,NY,ME,NH,VACyclohexane
AIHA,NY,ME,NHDibromochloromethane
AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
AIHA,NY,ME,NHtrans-1,3-Dichloropropene
AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,ME,NH,VA1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,ME,NH,VAHeptane
AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene
AIHA,FL,NJ,NY,ME,NH,VAHexane
AIHA2-Hexanone (MBK)
AIHA,NY,ME,NHIsopropanol
AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride
AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
AIHAPropene
AIHA,FL,NJ,NY,ME,NH,VAStyrene
AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
Page 39 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,ME,NH,VAToluene
AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene
AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride
AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene
AIHA,FL,NJ,NY,ME,NH,VAo-Xylene
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2024
M-MA100Massachusetts DEPMA 06/30/2022
PH-0165Connecticut Department of Publilc HealthCT 12/31/2022
10899 NELAPNew York State Department of HealthNY 04/1/2023
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2023
LAO00373Rhode Island Department of HealthRI 12/30/2022
652North Carolina Div. of Water QualityNC 12/31/2022
MA007 NELAPNew Jersey DEPNJ 06/30/2022
E871027 NELAPFlorida Department of HealthFL 06/30/2022
LL720741Vermont Department of Health Lead LaboratoryVT 07/30/2022
MA00100State of MaineME 06/9/2023
460217Commonwealth of VirginiaVA 12/14/2022
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2022
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2022
25703North Carolina Department of HealthNC-DW 07/31/2022
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2022
9100Dept. of Env, Great Lakes, and EnergyMI 09/6/2022
Page 40 of 43
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Page 43 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
April 28, 2022
Scott Young
ECS Southeast - Charlotte, NC
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project Location: 4000 Monroe Rd.
Client Job Number:
Project Number: 12929
Laboratory Work Order Number: 22D1699
Enclosed are results of analyses for samples as received by the laboratory on April 22, 2022. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
4/28/2022ECS Southeast - Charlotte, NC
1812 Center Park Drive, Suite D
Charlotte, NC 28217
ATTN: Scott Young
12929
22D1699
The results of analyses performed on the following samples submitted to Con-Test, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
4000 Monroe Rd.
IA-1 22D1699-01 Indoor air -
EPA TO-15
IA-2 22D1699-02 Indoor air -
EPA TO-15
IA-3 22D1699-03 Indoor air -
EPA TO-15
IA-4 22D1699-04 Indoor air -
EPA TO-15
IA-5 22D1699-05 Indoor air -
EPA TO-15
IA-6 22D1699-06 Indoor air -
EPA TO-15
IA-7 22D1699-07 Indoor air -
EPA TO-15
Unused Can#1504/Unused Reg#4642 22D1699-08 Air -
Unused Can#1319/Unused Reg#4642 22D1699-09 Air -
Page 2 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since
sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-36
1,2,4-Trichlorobenzene, Benzyl chloride
B306974-BS1, S070889-CCV1
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 3 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-1
Sample ID: 22D1699-01
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -8
Receipt Vacuum(in Hg): -9
Sampled: 4/19/2022 18:30
Canister ID: 1881
Flow Controller ID: 3582
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 4.0 1.4 4/26/22 15:32 BRF9.5 0.6983.30.84 2.0
Benzene 0.10 0.035 4/26/22 15:32 BRF0.33 0.6980.110.026 0.084
Benzyl chloride ND 0.070 4/26/22 15:32 BRFND0.6980.360.031 0.16
Bromodichloromethane ND 0.035 4/26/22 15:32 BRFND0.6980.230.024 0.16
Bromoform ND 0.035 4/26/22 15:32 BRFND0.6980.360.024 0.25
Bromomethane ND 0.035 4/26/22 15:32 BRFND0.6980.140.023 0.090
1,3-Butadiene ND 0.035 4/26/22 15:32 BRFND0.6980.0770.029 0.065
2-Butanone (MEK)0.40 1.4 4/26/22 15:32 BRFJ1.2 0.6984.10.37 1.1
Carbon Disulfide ND 0.35 4/26/22 15:32 BRFND0.6981.10.032 0.10
Carbon Tetrachloride 0.075 0.035 4/26/22 15:32 BRF0.47 0.6980.220.028 0.17
Chlorobenzene ND 0.035 4/26/22 15:32 BRFND0.6980.160.023 0.11
Chloroethane ND 0.035 4/26/22 15:32 BRFND0.6980.0920.031 0.082
Chloroform ND 0.035 4/26/22 15:32 BRFND0.6980.170.033 0.16
Chloromethane 0.55 0.070 4/26/22 15:32 BRF1.1 0.6980.140.028 0.057
Cyclohexane ND 0.035 4/26/22 15:32 BRFND0.6980.120.021 0.073
Dibromochloromethane ND 0.035 4/26/22 15:32 BRFND0.6980.300.023 0.20
1,2-Dibromoethane (EDB)ND 0.035 4/26/22 15:32 BRFND0.6980.270.021 0.16
1,2-Dichlorobenzene ND 0.035 4/26/22 15:32 BRFND0.6980.210.020 0.12
1,3-Dichlorobenzene ND 0.035 4/26/22 15:32 BRFND0.6980.210.019 0.12
1,4-Dichlorobenzene 0.15 0.035 4/26/22 15:32 BRF0.89 0.6980.210.023 0.14
Dichlorodifluoromethane (Freon 12)0.47 0.035 4/26/22 15:32 BRF2.3 0.6980.170.034 0.17
1,1-Dichloroethane ND 0.035 4/26/22 15:32 BRFND0.6980.140.030 0.12
1,2-Dichloroethane ND 0.035 4/26/22 15:32 BRFND0.6980.140.032 0.13
1,1-Dichloroethylene ND 0.035 4/26/22 15:32 BRFND0.6980.140.027 0.11
cis-1,2-Dichloroethylene ND 0.035 4/26/22 15:32 BRFND0.6980.140.025 0.10
trans-1,2-Dichloroethylene ND 0.035 4/26/22 15:32 BRFND0.6980.140.027 0.11
1,2-Dichloropropane ND 0.035 4/26/22 15:32 BRFND0.6980.160.019 0.087
cis-1,3-Dichloropropene ND 0.035 4/26/22 15:32 BRFND0.6980.160.018 0.082
trans-1,3-Dichloropropene ND 0.035 4/26/22 15:32 BRFND0.6980.160.018 0.081
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.035 4/26/22 15:32 BRFND0.6980.240.034 0.24
1,4-Dioxane ND 0.35 4/26/22 15:32 BRFND0.6981.30.029 0.10
Ethanol 3.4 1.4 4/26/22 15:32 BRF6.4 0.6982.60.62 1.2
Ethyl Acetate 0.55 0.35 4/26/22 15:32 BRF2.0 0.6981.30.18 0.64
Ethylbenzene 0.040 0.035 4/26/22 15:32 BRF0.17 0.6980.150.020 0.088
4-Ethyltoluene ND 0.035 4/26/22 15:32 BRFND0.6980.170.021 0.11
Heptane 0.040 0.035 4/26/22 15:32 BRF0.16 0.6980.140.022 0.091
Hexachlorobutadiene ND 0.035 4/26/22 15:32 BRFND0.6980.370.029 0.31
Hexane 0.38 1.4 4/26/22 15:32 BRFJ1.3 0.6984.90.18 0.64
2-Hexanone (MBK)ND 0.035 4/26/22 15:32 BRFND0.6980.140.017 0.071
Isopropanol 0.58 1.4 4/26/22 15:32 BRFJ1.4 0.6983.40.24 0.59
Methyl tert-Butyl Ether (MTBE)ND 0.035 4/26/22 15:32 BRFND0.6980.130.027 0.097
Methylene Chloride 0.22 0.35 4/26/22 15:32 BRFJ0.78 0.6981.20.16 0.56
4-Methyl-2-pentanone (MIBK)ND 0.035 4/26/22 15:32 BRFND0.6980.140.019 0.076
Naphthalene 0.061 0.035 4/26/22 15:32 BRF0.32 0.6980.180.026 0.14
Propene ND 1.4 4/26/22 15:32 BRFND0.6982.40.31 0.53
Styrene ND 0.035 4/26/22 15:32 BRFND0.6980.150.018 0.078
1,1,2,2-Tetrachloroethane ND 0.035 4/26/22 15:32 BRFND0.6980.240.019 0.13
Page 4 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-1
Sample ID: 22D1699-01
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -8
Receipt Vacuum(in Hg): -9
Sampled: 4/19/2022 18:30
Canister ID: 1881
Flow Controller ID: 3582
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.039 0.035 4/26/22 15:32 BRF0.26 0.6980.240.027 0.18
Tetrahydrofuran ND 0.35 4/26/22 15:32 BRFND0.6981.00.057 0.17
Toluene 0.21 0.035 4/26/22 15:32 BRF0.80 0.6980.130.020 0.075
1,2,4-Trichlorobenzene ND 0.035 4/26/22 15:32 BRFND0.6980.260.032 0.24
1,1,1-Trichloroethane ND 0.035 4/26/22 15:32 BRFND0.6980.190.027 0.15
1,1,2-Trichloroethane ND 0.035 4/26/22 15:32 BRFND0.6980.190.025 0.13
Trichloroethylene ND 0.035 4/26/22 15:32 BRFND0.6980.190.024 0.13
Trichlorofluoromethane (Freon 11)0.58 0.14 4/26/22 15:32 BRF3.2 0.6980.780.041 0.23
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.083 0.14 4/26/22 15:32 BRFJ0.64 0.6981.10.039 0.30
1,2,4-Trimethylbenzene 0.038 0.035 4/26/22 15:32 BRF0.19 0.6980.170.015 0.076
1,3,5-Trimethylbenzene ND 0.035 4/26/22 15:32 BRFND0.6980.170.018 0.091
Vinyl Acetate ND 0.70 4/26/22 15:32 BRFND0.6982.50.19 0.66
Vinyl Chloride ND 0.035 4/26/22 15:32 BRFND0.6980.0890.031 0.080
m&p-Xylene 0.13 0.070 4/26/22 15:32 BRF0.55 0.6980.300.039 0.17
o-Xylene 0.065 0.035 4/26/22 15:32 BRF0.28 0.6980.150.018 0.078
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)104 4/26/22 15:3270-130
Page 5 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-2
Sample ID: 22D1699-02
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -7
Receipt Vacuum(in Hg): -9
Sampled: 4/19/2022 18:25
Canister ID: 2171
Flow Controller ID: 3173
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 4.4 1.4 4/26/22 16:40 BRF10 0.6983.30.84 2.0
Benzene 0.093 0.035 4/26/22 16:40 BRF0.30 0.6980.110.026 0.084
Benzyl chloride ND 0.070 4/26/22 16:40 BRFND0.6980.360.031 0.16
Bromodichloromethane ND 0.035 4/26/22 16:40 BRFND0.6980.230.024 0.16
Bromoform ND 0.035 4/26/22 16:40 BRFND0.6980.360.024 0.25
Bromomethane ND 0.035 4/26/22 16:40 BRFND0.6980.140.023 0.090
1,3-Butadiene ND 0.035 4/26/22 16:40 BRFND0.6980.0770.029 0.065
2-Butanone (MEK)1.0 1.4 4/26/22 16:40 BRFJ3.0 0.6984.10.37 1.1
Carbon Disulfide ND 0.35 4/26/22 16:40 BRFND0.6981.10.032 0.10
Carbon Tetrachloride 0.067 0.035 4/26/22 16:40 BRF0.42 0.6980.220.028 0.17
Chlorobenzene ND 0.035 4/26/22 16:40 BRFND0.6980.160.023 0.11
Chloroethane ND 0.035 4/26/22 16:40 BRFND0.6980.0920.031 0.082
Chloroform ND 0.035 4/26/22 16:40 BRFND0.6980.170.033 0.16
Chloromethane 0.54 0.070 4/26/22 16:40 BRF1.1 0.6980.140.028 0.057
Cyclohexane ND 0.035 4/26/22 16:40 BRFND0.6980.120.021 0.073
Dibromochloromethane ND 0.035 4/26/22 16:40 BRFND0.6980.300.023 0.20
1,2-Dibromoethane (EDB)ND 0.035 4/26/22 16:40 BRFND0.6980.270.021 0.16
1,2-Dichlorobenzene ND 0.035 4/26/22 16:40 BRFND0.6980.210.020 0.12
1,3-Dichlorobenzene ND 0.035 4/26/22 16:40 BRFND0.6980.210.019 0.12
1,4-Dichlorobenzene 0.18 0.035 4/26/22 16:40 BRF1.1 0.6980.210.023 0.14
Dichlorodifluoromethane (Freon 12)0.47 0.035 4/26/22 16:40 BRF2.3 0.6980.170.034 0.17
1,1-Dichloroethane ND 0.035 4/26/22 16:40 BRFND0.6980.140.030 0.12
1,2-Dichloroethane ND 0.035 4/26/22 16:40 BRFND0.6980.140.032 0.13
1,1-Dichloroethylene ND 0.035 4/26/22 16:40 BRFND0.6980.140.027 0.11
cis-1,2-Dichloroethylene ND 0.035 4/26/22 16:40 BRFND0.6980.140.025 0.10
trans-1,2-Dichloroethylene ND 0.035 4/26/22 16:40 BRFND0.6980.140.027 0.11
1,2-Dichloropropane ND 0.035 4/26/22 16:40 BRFND0.6980.160.019 0.087
cis-1,3-Dichloropropene ND 0.035 4/26/22 16:40 BRFND0.6980.160.018 0.082
trans-1,3-Dichloropropene ND 0.035 4/26/22 16:40 BRFND0.6980.160.018 0.081
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.035 4/26/22 16:40 BRFND0.6980.240.034 0.24
1,4-Dioxane ND 0.35 4/26/22 16:40 BRFND0.6981.30.029 0.10
Ethanol 3.6 1.4 4/26/22 16:40 BRF6.8 0.6982.60.62 1.2
Ethyl Acetate 0.96 0.35 4/26/22 16:40 BRF3.5 0.6981.30.18 0.64
Ethylbenzene 0.028 0.035 4/26/22 16:40 BRFJ0.12 0.6980.150.020 0.088
4-Ethyltoluene ND 0.035 4/26/22 16:40 BRFND0.6980.170.021 0.11
Heptane 0.047 0.035 4/26/22 16:40 BRF0.19 0.6980.140.022 0.091
Hexachlorobutadiene ND 0.035 4/26/22 16:40 BRFND0.6980.370.029 0.31
Hexane 0.37 1.4 4/26/22 16:40 BRFJ1.3 0.6984.90.18 0.64
2-Hexanone (MBK)ND 0.035 4/26/22 16:40 BRFND0.6980.140.017 0.071
Isopropanol 0.53 1.4 4/26/22 16:40 BRFJ1.3 0.6983.40.24 0.59
Methyl tert-Butyl Ether (MTBE)ND 0.035 4/26/22 16:40 BRFND0.6980.130.027 0.097
Methylene Chloride ND 0.35 4/26/22 16:40 BRFND0.6981.20.16 0.56
4-Methyl-2-pentanone (MIBK)0.040 0.035 4/26/22 16:40 BRF0.17 0.6980.140.019 0.076
Naphthalene 0.048 0.035 4/26/22 16:40 BRF0.25 0.6980.180.026 0.14
Propene ND 1.4 4/26/22 16:40 BRFND0.6982.40.31 0.53
Styrene ND 0.035 4/26/22 16:40 BRFND0.6980.150.018 0.078
1,1,2,2-Tetrachloroethane ND 0.035 4/26/22 16:40 BRFND0.6980.240.019 0.13
Page 6 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-2
Sample ID: 22D1699-02
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -7
Receipt Vacuum(in Hg): -9
Sampled: 4/19/2022 18:25
Canister ID: 2171
Flow Controller ID: 3173
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.029 0.035 4/26/22 16:40 BRFJ0.20 0.6980.240.027 0.18
Tetrahydrofuran ND 0.35 4/26/22 16:40 BRFND0.6981.00.057 0.17
Toluene 0.14 0.035 4/26/22 16:40 BRF0.54 0.6980.130.020 0.075
1,2,4-Trichlorobenzene ND 0.035 4/26/22 16:40 BRFND0.6980.260.032 0.24
1,1,1-Trichloroethane ND 0.035 4/26/22 16:40 BRFND0.6980.190.027 0.15
1,1,2-Trichloroethane ND 0.035 4/26/22 16:40 BRFND0.6980.190.025 0.13
Trichloroethylene ND 0.035 4/26/22 16:40 BRFND0.6980.190.024 0.13
Trichlorofluoromethane (Freon 11)0.50 0.14 4/26/22 16:40 BRF2.8 0.6980.780.041 0.23
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.080 0.14 4/26/22 16:40 BRFJ0.61 0.6981.10.039 0.30
1,2,4-Trimethylbenzene 0.027 0.035 4/26/22 16:40 BRFJ0.13 0.6980.170.015 0.076
1,3,5-Trimethylbenzene ND 0.035 4/26/22 16:40 BRFND0.6980.170.018 0.091
Vinyl Acetate ND 0.70 4/26/22 16:40 BRFND0.6982.50.19 0.66
Vinyl Chloride ND 0.035 4/26/22 16:40 BRFND0.6980.0890.031 0.080
m&p-Xylene 0.079 0.070 4/26/22 16:40 BRF0.34 0.6980.300.039 0.17
o-Xylene 0.044 0.035 4/26/22 16:40 BRF0.19 0.6980.150.018 0.078
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 4/26/22 16:4070-130
Page 7 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-3
Sample ID: 22D1699-03
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -8
Receipt Vacuum(in Hg): -9.4
Sampled: 4/19/2022 18:53
Canister ID: 1995
Flow Controller ID: 3643
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 4.1 1.4 4/26/22 17:47 BRF9.6 0.6983.30.84 2.0
Benzene 0.076 0.035 4/26/22 17:47 BRF0.24 0.6980.110.026 0.084
Benzyl chloride ND 0.070 4/26/22 17:47 BRFND0.6980.360.031 0.16
Bromodichloromethane ND 0.035 4/26/22 17:47 BRFND0.6980.230.024 0.16
Bromoform ND 0.035 4/26/22 17:47 BRFND0.6980.360.024 0.25
Bromomethane ND 0.035 4/26/22 17:47 BRFND0.6980.140.023 0.090
1,3-Butadiene ND 0.035 4/26/22 17:47 BRFND0.6980.0770.029 0.065
2-Butanone (MEK)0.69 1.4 4/26/22 17:47 BRFJ2.0 0.6984.10.37 1.1
Carbon Disulfide ND 0.35 4/26/22 17:47 BRFND0.6981.10.032 0.10
Carbon Tetrachloride 0.071 0.035 4/26/22 17:47 BRF0.45 0.6980.220.028 0.17
Chlorobenzene ND 0.035 4/26/22 17:47 BRFND0.6980.160.023 0.11
Chloroethane ND 0.035 4/26/22 17:47 BRFND0.6980.0920.031 0.082
Chloroform ND 0.035 4/26/22 17:47 BRFND0.6980.170.033 0.16
Chloromethane 0.62 0.070 4/26/22 17:47 BRF1.3 0.6980.140.028 0.057
Cyclohexane ND 0.035 4/26/22 17:47 BRFND0.6980.120.021 0.073
Dibromochloromethane ND 0.035 4/26/22 17:47 BRFND0.6980.300.023 0.20
1,2-Dibromoethane (EDB)ND 0.035 4/26/22 17:47 BRFND0.6980.270.021 0.16
1,2-Dichlorobenzene ND 0.035 4/26/22 17:47 BRFND0.6980.210.020 0.12
1,3-Dichlorobenzene ND 0.035 4/26/22 17:47 BRFND0.6980.210.019 0.12
1,4-Dichlorobenzene ND 0.035 4/26/22 17:47 BRFND0.6980.210.023 0.14
Dichlorodifluoromethane (Freon 12)0.50 0.035 4/26/22 17:47 BRF2.5 0.6980.170.034 0.17
1,1-Dichloroethane ND 0.035 4/26/22 17:47 BRFND0.6980.140.030 0.12
1,2-Dichloroethane ND 0.035 4/26/22 17:47 BRFND0.6980.140.032 0.13
1,1-Dichloroethylene ND 0.035 4/26/22 17:47 BRFND0.6980.140.027 0.11
cis-1,2-Dichloroethylene ND 0.035 4/26/22 17:47 BRFND0.6980.140.025 0.10
trans-1,2-Dichloroethylene ND 0.035 4/26/22 17:47 BRFND0.6980.140.027 0.11
1,2-Dichloropropane ND 0.035 4/26/22 17:47 BRFND0.6980.160.019 0.087
cis-1,3-Dichloropropene ND 0.035 4/26/22 17:47 BRFND0.6980.160.018 0.082
trans-1,3-Dichloropropene ND 0.035 4/26/22 17:47 BRFND0.6980.160.018 0.081
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.035 4/26/22 17:47 BRFND0.6980.240.034 0.24
1,4-Dioxane ND 0.35 4/26/22 17:47 BRFND0.6981.30.029 0.10
Ethanol 3.3 1.4 4/26/22 17:47 BRF6.3 0.6982.60.62 1.2
Ethyl Acetate 2.8 0.35 4/26/22 17:47 BRF10 0.6981.30.18 0.64
Ethylbenzene 0.033 0.035 4/26/22 17:47 BRFJ0.15 0.6980.150.020 0.088
4-Ethyltoluene ND 0.035 4/26/22 17:47 BRFND0.6980.170.021 0.11
Heptane 0.073 0.035 4/26/22 17:47 BRF0.30 0.6980.140.022 0.091
Hexachlorobutadiene ND 0.035 4/26/22 17:47 BRFND0.6980.370.029 0.31
Hexane 0.37 1.4 4/26/22 17:47 BRFJ1.3 0.6984.90.18 0.64
2-Hexanone (MBK)ND 0.035 4/26/22 17:47 BRFND0.6980.140.017 0.071
Isopropanol 0.34 1.4 4/26/22 17:47 BRFJ0.84 0.6983.40.24 0.59
Methyl tert-Butyl Ether (MTBE)ND 0.035 4/26/22 17:47 BRFND0.6980.130.027 0.097
Methylene Chloride ND 0.35 4/26/22 17:47 BRFND0.6981.20.16 0.56
4-Methyl-2-pentanone (MIBK)0.041 0.035 4/26/22 17:47 BRF0.17 0.6980.140.019 0.076
Naphthalene ND 0.035 4/26/22 17:47 BRFND0.6980.180.026 0.14
Propene ND 1.4 4/26/22 17:47 BRFND0.6982.40.31 0.53
Styrene ND 0.035 4/26/22 17:47 BRFND0.6980.150.018 0.078
1,1,2,2-Tetrachloroethane ND 0.035 4/26/22 17:47 BRFND0.6980.240.019 0.13
Page 8 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-3
Sample ID: 22D1699-03
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -8
Receipt Vacuum(in Hg): -9.4
Sampled: 4/19/2022 18:53
Canister ID: 1995
Flow Controller ID: 3643
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.035 4/26/22 17:47 BRFND0.6980.240.027 0.18
Tetrahydrofuran ND 0.35 4/26/22 17:47 BRFND0.6981.00.057 0.17
Toluene 0.17 0.035 4/26/22 17:47 BRF0.63 0.6980.130.020 0.075
1,2,4-Trichlorobenzene ND 0.035 4/26/22 17:47 BRFND0.6980.260.032 0.24
1,1,1-Trichloroethane ND 0.035 4/26/22 17:47 BRFND0.6980.190.027 0.15
1,1,2-Trichloroethane ND 0.035 4/26/22 17:47 BRFND0.6980.190.025 0.13
Trichloroethylene ND 0.035 4/26/22 17:47 BRFND0.6980.190.024 0.13
Trichlorofluoromethane (Freon 11)1.1 0.14 4/26/22 17:47 BRF6.1 0.6980.780.041 0.23
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.084 0.14 4/26/22 17:47 BRFJ0.65 0.6981.10.039 0.30
1,2,4-Trimethylbenzene 0.027 0.035 4/26/22 17:47 BRFJ0.13 0.6980.170.015 0.076
1,3,5-Trimethylbenzene ND 0.035 4/26/22 17:47 BRFND0.6980.170.018 0.091
Vinyl Acetate ND 0.70 4/26/22 17:47 BRFND0.6982.50.19 0.66
Vinyl Chloride ND 0.035 4/26/22 17:47 BRFND0.6980.0890.031 0.080
m&p-Xylene 0.10 0.070 4/26/22 17:47 BRF0.45 0.6980.300.039 0.17
o-Xylene 0.039 0.035 4/26/22 17:47 BRF0.17 0.6980.150.018 0.078
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)104 4/26/22 17:4770-130
Page 9 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-4
Sample ID: 22D1699-04
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -7
Receipt Vacuum(in Hg): -8.2
Sampled: 4/19/2022 19:00
Canister ID: 2182
Flow Controller ID: 3550
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 4.3 1.4 4/26/22 19:23 BRF10 0.6983.30.84 2.0
Benzene 0.071 0.035 4/26/22 19:23 BRF0.23 0.6980.110.026 0.084
Benzyl chloride ND 0.070 4/26/22 19:23 BRFND0.6980.360.031 0.16
Bromodichloromethane ND 0.035 4/26/22 19:23 BRFND0.6980.230.024 0.16
Bromoform ND 0.035 4/26/22 19:23 BRFND0.6980.360.024 0.25
Bromomethane ND 0.035 4/26/22 19:23 BRFND0.6980.140.023 0.090
1,3-Butadiene ND 0.035 4/26/22 19:23 BRFND0.6980.0770.029 0.065
2-Butanone (MEK)0.60 1.4 4/26/22 19:23 BRFJ1.8 0.6984.10.37 1.1
Carbon Disulfide ND 0.35 4/26/22 19:23 BRFND0.6981.10.032 0.10
Carbon Tetrachloride 0.077 0.035 4/26/22 19:23 BRF0.48 0.6980.220.028 0.17
Chlorobenzene ND 0.035 4/26/22 19:23 BRFND0.6980.160.023 0.11
Chloroethane ND 0.035 4/26/22 19:23 BRFND0.6980.0920.031 0.082
Chloroform ND 0.035 4/26/22 19:23 BRFND0.6980.170.033 0.16
Chloromethane 0.55 0.070 4/26/22 19:23 BRF1.1 0.6980.140.028 0.057
Cyclohexane ND 0.035 4/26/22 19:23 BRFND0.6980.120.021 0.073
Dibromochloromethane ND 0.035 4/26/22 19:23 BRFND0.6980.300.023 0.20
1,2-Dibromoethane (EDB)ND 0.035 4/26/22 19:23 BRFND0.6980.270.021 0.16
1,2-Dichlorobenzene ND 0.035 4/26/22 19:23 BRFND0.6980.210.020 0.12
1,3-Dichlorobenzene ND 0.035 4/26/22 19:23 BRFND0.6980.210.019 0.12
1,4-Dichlorobenzene ND 0.035 4/26/22 19:23 BRFND0.6980.210.023 0.14
Dichlorodifluoromethane (Freon 12)0.49 0.035 4/26/22 19:23 BRF2.4 0.6980.170.034 0.17
1,1-Dichloroethane ND 0.035 4/26/22 19:23 BRFND0.6980.140.030 0.12
1,2-Dichloroethane ND 0.035 4/26/22 19:23 BRFND0.6980.140.032 0.13
1,1-Dichloroethylene ND 0.035 4/26/22 19:23 BRFND0.6980.140.027 0.11
cis-1,2-Dichloroethylene ND 0.035 4/26/22 19:23 BRFND0.6980.140.025 0.10
trans-1,2-Dichloroethylene ND 0.035 4/26/22 19:23 BRFND0.6980.140.027 0.11
1,2-Dichloropropane ND 0.035 4/26/22 19:23 BRFND0.6980.160.019 0.087
cis-1,3-Dichloropropene ND 0.035 4/26/22 19:23 BRFND0.6980.160.018 0.082
trans-1,3-Dichloropropene ND 0.035 4/26/22 19:23 BRFND0.6980.160.018 0.081
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.035 4/26/22 19:23 BRFND0.6980.240.034 0.24
1,4-Dioxane ND 0.35 4/26/22 19:23 BRFND0.6981.30.029 0.10
Ethanol 3.5 1.4 4/26/22 19:23 BRF6.6 0.6982.60.62 1.2
Ethyl Acetate 5.5 0.35 4/26/22 19:23 BRF20 0.6981.30.18 0.64
Ethylbenzene 0.031 0.035 4/26/22 19:23 BRFJ0.13 0.6980.150.020 0.088
4-Ethyltoluene ND 0.035 4/26/22 19:23 BRFND0.6980.170.021 0.11
Heptane ND 0.035 4/26/22 19:23 BRFND0.6980.140.022 0.091
Hexachlorobutadiene ND 0.035 4/26/22 19:23 BRFND0.6980.370.029 0.31
Hexane 0.46 1.4 4/26/22 19:23 BRFJ1.6 0.6984.90.18 0.64
2-Hexanone (MBK)ND 0.035 4/26/22 19:23 BRFND0.6980.140.017 0.071
Isopropanol 0.59 1.4 4/26/22 19:23 BRFJ1.5 0.6983.40.24 0.59
Methyl tert-Butyl Ether (MTBE)ND 0.035 4/26/22 19:23 BRFND0.6980.130.027 0.097
Methylene Chloride 0.25 0.35 4/26/22 19:23 BRFJ0.88 0.6981.20.16 0.56
4-Methyl-2-pentanone (MIBK)ND 0.035 4/26/22 19:23 BRFND0.6980.140.019 0.076
Naphthalene ND 0.035 4/26/22 19:23 BRFND0.6980.180.026 0.14
Propene ND 1.4 4/26/22 19:23 BRFND0.6982.40.31 0.53
Styrene ND 0.035 4/26/22 19:23 BRFND0.6980.150.018 0.078
1,1,2,2-Tetrachloroethane ND 0.035 4/26/22 19:23 BRFND0.6980.240.019 0.13
Page 10 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-4
Sample ID: 22D1699-04
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -7
Receipt Vacuum(in Hg): -8.2
Sampled: 4/19/2022 19:00
Canister ID: 2182
Flow Controller ID: 3550
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.035 4/26/22 19:23 BRFND0.6980.240.027 0.18
Tetrahydrofuran ND 0.35 4/26/22 19:23 BRFND0.6981.00.057 0.17
Toluene 0.12 0.035 4/26/22 19:23 BRF0.45 0.6980.130.020 0.075
1,2,4-Trichlorobenzene ND 0.035 4/26/22 19:23 BRFND0.6980.260.032 0.24
1,1,1-Trichloroethane ND 0.035 4/26/22 19:23 BRFND0.6980.190.027 0.15
1,1,2-Trichloroethane ND 0.035 4/26/22 19:23 BRFND0.6980.190.025 0.13
Trichloroethylene ND 0.035 4/26/22 19:23 BRFND0.6980.190.024 0.13
Trichlorofluoromethane (Freon 11)0.34 0.14 4/26/22 19:23 BRF1.9 0.6980.780.041 0.23
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.080 0.14 4/26/22 19:23 BRFJ0.61 0.6981.10.039 0.30
1,2,4-Trimethylbenzene 0.030 0.035 4/26/22 19:23 BRFJ0.15 0.6980.170.015 0.076
1,3,5-Trimethylbenzene ND 0.035 4/26/22 19:23 BRFND0.6980.170.018 0.091
Vinyl Acetate ND 0.70 4/26/22 19:23 BRFND0.6982.50.19 0.66
Vinyl Chloride ND 0.035 4/26/22 19:23 BRFND0.6980.0890.031 0.080
m&p-Xylene 0.11 0.070 4/26/22 19:23 BRF0.46 0.6980.300.039 0.17
o-Xylene 0.037 0.035 4/26/22 19:23 BRF0.16 0.6980.150.018 0.078
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 4/26/22 19:2370-130
Page 11 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-5
Sample ID: 22D1699-05
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -9
Receipt Vacuum(in Hg): -9.6
Sampled: 4/19/2022 19:05
Canister ID: 1814
Flow Controller ID: 3629
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 5.9 1.4 4/26/22 20:33 BRF14 0.6983.30.84 2.0
Benzene 0.077 0.035 4/26/22 20:33 BRF0.25 0.6980.110.026 0.084
Benzyl chloride ND 0.070 4/26/22 20:33 BRFND0.6980.360.031 0.16
Bromodichloromethane ND 0.035 4/26/22 20:33 BRFND0.6980.230.024 0.16
Bromoform ND 0.035 4/26/22 20:33 BRFND0.6980.360.024 0.25
Bromomethane ND 0.035 4/26/22 20:33 BRFND0.6980.140.023 0.090
1,3-Butadiene ND 0.035 4/26/22 20:33 BRFND0.6980.0770.029 0.065
2-Butanone (MEK)0.54 1.4 4/26/22 20:33 BRFJ1.6 0.6984.10.37 1.1
Carbon Disulfide ND 0.35 4/26/22 20:33 BRFND0.6981.10.032 0.10
Carbon Tetrachloride 0.077 0.035 4/26/22 20:33 BRF0.49 0.6980.220.028 0.17
Chlorobenzene ND 0.035 4/26/22 20:33 BRFND0.6980.160.023 0.11
Chloroethane ND 0.035 4/26/22 20:33 BRFND0.6980.0920.031 0.082
Chloroform ND 0.035 4/26/22 20:33 BRFND0.6980.170.033 0.16
Chloromethane 0.57 0.070 4/26/22 20:33 BRF1.2 0.6980.140.028 0.057
Cyclohexane ND 0.035 4/26/22 20:33 BRFND0.6980.120.021 0.073
Dibromochloromethane ND 0.035 4/26/22 20:33 BRFND0.6980.300.023 0.20
1,2-Dibromoethane (EDB)ND 0.035 4/26/22 20:33 BRFND0.6980.270.021 0.16
1,2-Dichlorobenzene ND 0.035 4/26/22 20:33 BRFND0.6980.210.020 0.12
1,3-Dichlorobenzene ND 0.035 4/26/22 20:33 BRFND0.6980.210.019 0.12
1,4-Dichlorobenzene ND 0.035 4/26/22 20:33 BRFND0.6980.210.023 0.14
Dichlorodifluoromethane (Freon 12)0.51 0.035 4/26/22 20:33 BRF2.5 0.6980.170.034 0.17
1,1-Dichloroethane ND 0.035 4/26/22 20:33 BRFND0.6980.140.030 0.12
1,2-Dichloroethane ND 0.035 4/26/22 20:33 BRFND0.6980.140.032 0.13
1,1-Dichloroethylene ND 0.035 4/26/22 20:33 BRFND0.6980.140.027 0.11
cis-1,2-Dichloroethylene ND 0.035 4/26/22 20:33 BRFND0.6980.140.025 0.10
trans-1,2-Dichloroethylene ND 0.035 4/26/22 20:33 BRFND0.6980.140.027 0.11
1,2-Dichloropropane ND 0.035 4/26/22 20:33 BRFND0.6980.160.019 0.087
cis-1,3-Dichloropropene ND 0.035 4/26/22 20:33 BRFND0.6980.160.018 0.082
trans-1,3-Dichloropropene ND 0.035 4/26/22 20:33 BRFND0.6980.160.018 0.081
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.035 4/26/22 20:33 BRFND0.6980.240.034 0.24
1,4-Dioxane ND 0.35 4/26/22 20:33 BRFND0.6981.30.029 0.10
Ethanol 12 1.4 4/26/22 20:33 BRF23 0.6982.60.62 1.2
Ethyl Acetate 120 5.0 4/26/22 21:05 BRF430 10182.5 9.1
Ethylbenzene 0.30 0.035 4/26/22 20:33 BRF1.3 0.6980.150.020 0.088
4-Ethyltoluene 0.033 0.035 4/26/22 20:33 BRFJ0.16 0.6980.170.021 0.11
Heptane 0.13 0.035 4/26/22 20:33 BRF0.55 0.6980.140.022 0.091
Hexachlorobutadiene ND 0.035 4/26/22 20:33 BRFND0.6980.370.029 0.31
Hexane 2.2 1.4 4/26/22 20:33 BRF7.6 0.6984.90.18 0.64
2-Hexanone (MBK)ND 0.035 4/26/22 20:33 BRFND0.6980.140.017 0.071
Isopropanol 2.2 1.4 4/26/22 20:33 BRF5.3 0.6983.40.24 0.59
Methyl tert-Butyl Ether (MTBE)ND 0.035 4/26/22 20:33 BRFND0.6980.130.027 0.097
Methylene Chloride 0.25 0.35 4/26/22 20:33 BRFJ0.87 0.6981.20.16 0.56
4-Methyl-2-pentanone (MIBK)ND 0.035 4/26/22 20:33 BRFND0.6980.140.019 0.076
Naphthalene ND 0.035 4/26/22 20:33 BRFND0.6980.180.026 0.14
Propene ND 1.4 4/26/22 20:33 BRFND0.6982.40.31 0.53
Styrene ND 0.035 4/26/22 20:33 BRFND0.6980.150.018 0.078
1,1,2,2-Tetrachloroethane ND 0.035 4/26/22 20:33 BRFND0.6980.240.019 0.13
Page 12 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-5
Sample ID: 22D1699-05
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -9
Receipt Vacuum(in Hg): -9.6
Sampled: 4/19/2022 19:05
Canister ID: 1814
Flow Controller ID: 3629
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.036 0.035 4/26/22 20:33 BRF0.25 0.6980.240.027 0.18
Tetrahydrofuran ND 0.35 4/26/22 20:33 BRFND0.6981.00.057 0.17
Toluene 0.20 0.035 4/26/22 20:33 BRF0.74 0.6980.130.020 0.075
1,2,4-Trichlorobenzene ND 0.035 4/26/22 20:33 BRFND0.6980.260.032 0.24
1,1,1-Trichloroethane ND 0.035 4/26/22 20:33 BRFND0.6980.190.027 0.15
1,1,2-Trichloroethane ND 0.035 4/26/22 20:33 BRFND0.6980.190.025 0.13
Trichloroethylene ND 0.035 4/26/22 20:33 BRFND0.6980.190.024 0.13
Trichlorofluoromethane (Freon 11)0.50 0.14 4/26/22 20:33 BRF2.8 0.6980.780.041 0.23
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.078 0.14 4/26/22 20:33 BRFJ0.60 0.6981.10.039 0.30
1,2,4-Trimethylbenzene 0.12 0.035 4/26/22 20:33 BRF0.61 0.6980.170.015 0.076
1,3,5-Trimethylbenzene 0.038 0.035 4/26/22 20:33 BRF0.19 0.6980.170.018 0.091
Vinyl Acetate ND 0.70 4/26/22 20:33 BRFND0.6982.50.19 0.66
Vinyl Chloride ND 0.035 4/26/22 20:33 BRFND0.6980.0890.031 0.080
m&p-Xylene 1.3 0.070 4/26/22 20:33 BRF5.5 0.6980.300.039 0.17
o-Xylene 0.39 0.035 4/26/22 20:33 BRF1.7 0.6980.150.018 0.078
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)101 4/26/22 21:0570-130
4-Bromofluorobenzene (1)105 4/26/22 20:3370-130
Page 13 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-6
Sample ID: 22D1699-06
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -10
Receipt Vacuum(in Hg): -10.6
Sampled: 4/19/2022 19:09
Canister ID: 1304
Flow Controller ID: 3554
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 14 1.4 4/26/22 21:42 BRF33 0.6983.30.84 2.0
Benzene 0.080 0.035 4/26/22 21:42 BRF0.26 0.6980.110.026 0.084
Benzyl chloride ND 0.070 4/26/22 21:42 BRFND0.6980.360.031 0.16
Bromodichloromethane ND 0.035 4/26/22 21:42 BRFND0.6980.230.024 0.16
Bromoform ND 0.035 4/26/22 21:42 BRFND0.6980.360.024 0.25
Bromomethane ND 0.035 4/26/22 21:42 BRFND0.6980.140.023 0.090
1,3-Butadiene ND 0.035 4/26/22 21:42 BRFND0.6980.0770.029 0.065
2-Butanone (MEK)0.74 1.4 4/26/22 21:42 BRFJ2.2 0.6984.10.37 1.1
Carbon Disulfide ND 0.35 4/26/22 21:42 BRFND0.6981.10.032 0.10
Carbon Tetrachloride 0.076 0.035 4/26/22 21:42 BRF0.48 0.6980.220.028 0.17
Chlorobenzene ND 0.035 4/26/22 21:42 BRFND0.6980.160.023 0.11
Chloroethane ND 0.035 4/26/22 21:42 BRFND0.6980.0920.031 0.082
Chloroform 0.059 0.035 4/26/22 21:42 BRF0.29 0.6980.170.033 0.16
Chloromethane 0.57 0.070 4/26/22 21:42 BRF1.2 0.6980.140.028 0.057
Cyclohexane ND 0.035 4/26/22 21:42 BRFND0.6980.120.021 0.073
Dibromochloromethane ND 0.035 4/26/22 21:42 BRFND0.6980.300.023 0.20
1,2-Dibromoethane (EDB)ND 0.035 4/26/22 21:42 BRFND0.6980.270.021 0.16
1,2-Dichlorobenzene ND 0.035 4/26/22 21:42 BRFND0.6980.210.020 0.12
1,3-Dichlorobenzene ND 0.035 4/26/22 21:42 BRFND0.6980.210.019 0.12
1,4-Dichlorobenzene ND 0.035 4/26/22 21:42 BRFND0.6980.210.023 0.14
Dichlorodifluoromethane (Freon 12)0.065 0.035 4/26/22 21:42 BRF0.32 0.6980.170.034 0.17
1,1-Dichloroethane ND 0.035 4/26/22 21:42 BRFND0.6980.140.030 0.12
1,2-Dichloroethane ND 0.035 4/26/22 21:42 BRFND0.6980.140.032 0.13
1,1-Dichloroethylene ND 0.035 4/26/22 21:42 BRFND0.6980.140.027 0.11
cis-1,2-Dichloroethylene ND 0.035 4/26/22 21:42 BRFND0.6980.140.025 0.10
trans-1,2-Dichloroethylene ND 0.035 4/26/22 21:42 BRFND0.6980.140.027 0.11
1,2-Dichloropropane ND 0.035 4/26/22 21:42 BRFND0.6980.160.019 0.087
cis-1,3-Dichloropropene ND 0.035 4/26/22 21:42 BRFND0.6980.160.018 0.082
trans-1,3-Dichloropropene ND 0.035 4/26/22 21:42 BRFND0.6980.160.018 0.081
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.035 4/26/22 21:42 BRFND0.6980.240.034 0.24
1,4-Dioxane ND 0.35 4/26/22 21:42 BRFND0.6981.30.029 0.10
Ethanol 26 1.4 4/26/22 21:42 BRF50 0.6982.60.62 1.2
Ethyl Acetate 500 5.0 4/26/22 22:14 BRF1800 10182.5 9.1
Ethylbenzene 0.90 0.035 4/26/22 21:42 BRF3.9 0.6980.150.020 0.088
4-Ethyltoluene 0.077 0.035 4/26/22 21:42 BRF0.38 0.6980.170.021 0.11
Heptane ND 0.035 4/26/22 21:42 BRFND0.6980.140.022 0.091
Hexachlorobutadiene ND 0.035 4/26/22 21:42 BRFND0.6980.370.029 0.31
Hexane ND 1.4 4/26/22 21:42 BRFND0.6984.90.18 0.64
2-Hexanone (MBK)ND 0.035 4/26/22 21:42 BRFND0.6980.140.017 0.071
Isopropanol 5.2 1.4 4/26/22 21:42 BRF13 0.6983.40.24 0.59
Methyl tert-Butyl Ether (MTBE)ND 0.035 4/26/22 21:42 BRFND0.6980.130.027 0.097
Methylene Chloride 0.24 0.35 4/26/22 21:42 BRFJ0.82 0.6981.20.16 0.56
4-Methyl-2-pentanone (MIBK)ND 0.035 4/26/22 21:42 BRFND0.6980.140.019 0.076
Naphthalene ND 0.035 4/26/22 21:42 BRFND0.6980.180.026 0.14
Propene ND 1.4 4/26/22 21:42 BRFND0.6982.40.31 0.53
Styrene ND 0.035 4/26/22 21:42 BRFND0.6980.150.018 0.078
1,1,2,2-Tetrachloroethane ND 0.035 4/26/22 21:42 BRFND0.6980.240.019 0.13
Page 14 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-6
Sample ID: 22D1699-06
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -10
Receipt Vacuum(in Hg): -10.6
Sampled: 4/19/2022 19:09
Canister ID: 1304
Flow Controller ID: 3554
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.098 0.035 4/26/22 21:42 BRF0.67 0.6980.240.027 0.18
Tetrahydrofuran ND 0.35 4/26/22 21:42 BRFND0.6981.00.057 0.17
Toluene 0.27 0.035 4/26/22 21:42 BRF1.0 0.6980.130.020 0.075
1,2,4-Trichlorobenzene ND 0.035 4/26/22 21:42 BRFND0.6980.260.032 0.24
1,1,1-Trichloroethane ND 0.035 4/26/22 21:42 BRFND0.6980.190.027 0.15
1,1,2-Trichloroethane ND 0.035 4/26/22 21:42 BRFND0.6980.190.025 0.13
Trichloroethylene 0.059 0.035 4/26/22 21:42 BRF0.32 0.6980.190.024 0.13
Trichlorofluoromethane (Freon 11)0.73 0.14 4/26/22 21:42 BRF4.1 0.6980.780.041 0.23
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.090 0.14 4/26/22 21:42 BRFJ0.69 0.6981.10.039 0.30
1,2,4-Trimethylbenzene 0.34 0.035 4/26/22 21:42 BRF1.7 0.6980.170.015 0.076
1,3,5-Trimethylbenzene 0.075 0.035 4/26/22 21:42 BRF0.37 0.6980.170.018 0.091
Vinyl Acetate ND 0.70 4/26/22 21:42 BRFND0.6982.50.19 0.66
Vinyl Chloride ND 0.035 4/26/22 21:42 BRFND0.6980.0890.031 0.080
m&p-Xylene 3.8 0.070 4/26/22 21:42 BRF17 0.6980.300.039 0.17
o-Xylene 1.2 0.035 4/26/22 21:42 BRF5.2 0.6980.150.018 0.078
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)103 4/26/22 22:1470-130
4-Bromofluorobenzene (1)110 4/26/22 21:4270-130
Page 15 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-7
Sample ID: 22D1699-07
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -8
Receipt Vacuum(in Hg): -8.5
Sampled: 4/19/2022 19:12
Canister ID: 1624
Flow Controller ID: 3158
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 7.0 1.4 4/26/22 22:51 BRF17 0.6983.30.84 2.0
Benzene 0.081 0.035 4/26/22 22:51 BRF0.26 0.6980.110.026 0.084
Benzyl chloride ND 0.070 4/26/22 22:51 BRFND0.6980.360.031 0.16
Bromodichloromethane ND 0.035 4/26/22 22:51 BRFND0.6980.230.024 0.16
Bromoform ND 0.035 4/26/22 22:51 BRFND0.6980.360.024 0.25
Bromomethane ND 0.035 4/26/22 22:51 BRFND0.6980.140.023 0.090
1,3-Butadiene ND 0.035 4/26/22 22:51 BRFND0.6980.0770.029 0.065
2-Butanone (MEK)ND 1.4 4/26/22 22:51 BRFND0.6984.10.37 1.1
Carbon Disulfide ND 0.35 4/26/22 22:51 BRFND0.6981.10.032 0.10
Carbon Tetrachloride 0.070 0.035 4/26/22 22:51 BRF0.44 0.6980.220.028 0.17
Chlorobenzene ND 0.035 4/26/22 22:51 BRFND0.6980.160.023 0.11
Chloroethane ND 0.035 4/26/22 22:51 BRFND0.6980.0920.031 0.082
Chloroform 0.081 0.035 4/26/22 22:51 BRF0.40 0.6980.170.033 0.16
Chloromethane 0.65 0.070 4/26/22 22:51 BRF1.3 0.6980.140.028 0.057
Cyclohexane ND 0.035 4/26/22 22:51 BRFND0.6980.120.021 0.073
Dibromochloromethane ND 0.035 4/26/22 22:51 BRFND0.6980.300.023 0.20
1,2-Dibromoethane (EDB)ND 0.035 4/26/22 22:51 BRFND0.6980.270.021 0.16
1,2-Dichlorobenzene ND 0.035 4/26/22 22:51 BRFND0.6980.210.020 0.12
1,3-Dichlorobenzene ND 0.035 4/26/22 22:51 BRFND0.6980.210.019 0.12
1,4-Dichlorobenzene 0.10 0.035 4/26/22 22:51 BRF0.62 0.6980.210.023 0.14
Dichlorodifluoromethane (Freon 12)1.3 0.035 4/26/22 22:51 BRF6.2 0.6980.170.034 0.17
1,1-Dichloroethane ND 0.035 4/26/22 22:51 BRFND0.6980.140.030 0.12
1,2-Dichloroethane ND 0.035 4/26/22 22:51 BRFND0.6980.140.032 0.13
1,1-Dichloroethylene ND 0.035 4/26/22 22:51 BRFND0.6980.140.027 0.11
cis-1,2-Dichloroethylene ND 0.035 4/26/22 22:51 BRFND0.6980.140.025 0.10
trans-1,2-Dichloroethylene ND 0.035 4/26/22 22:51 BRFND0.6980.140.027 0.11
1,2-Dichloropropane ND 0.035 4/26/22 22:51 BRFND0.6980.160.019 0.087
cis-1,3-Dichloropropene ND 0.035 4/26/22 22:51 BRFND0.6980.160.018 0.082
trans-1,3-Dichloropropene ND 0.035 4/26/22 22:51 BRFND0.6980.160.018 0.081
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.035 4/26/22 22:51 BRFND0.6980.240.034 0.24
1,4-Dioxane ND 0.35 4/26/22 22:51 BRFND0.6981.30.029 0.10
Ethanol 18 1.4 4/26/22 22:51 BRF33 0.6982.60.62 1.2
Ethyl Acetate 61 5.0 4/26/22 23:24 BRF220 10182.5 9.1
Ethylbenzene 0.37 0.035 4/26/22 22:51 BRF1.6 0.6980.150.020 0.088
4-Ethyltoluene 0.077 0.035 4/26/22 22:51 BRF0.38 0.6980.170.021 0.11
Heptane ND 0.035 4/26/22 22:51 BRFND0.6980.140.022 0.091
Hexachlorobutadiene ND 0.035 4/26/22 22:51 BRFND0.6980.370.029 0.31
Hexane ND 1.4 4/26/22 22:51 BRFND0.6984.90.18 0.64
2-Hexanone (MBK)ND 0.035 4/26/22 22:51 BRFND0.6980.140.017 0.071
Isopropanol 4.1 1.4 4/26/22 22:51 BRF10.0 0.6983.40.24 0.59
Methyl tert-Butyl Ether (MTBE)ND 0.035 4/26/22 22:51 BRFND0.6980.130.027 0.097
Methylene Chloride 0.20 0.35 4/26/22 22:51 BRFJ0.71 0.6981.20.16 0.56
4-Methyl-2-pentanone (MIBK)ND 0.035 4/26/22 22:51 BRFND0.6980.140.019 0.076
Naphthalene ND 0.035 4/26/22 22:51 BRFND0.6980.180.026 0.14
Propene ND 1.4 4/26/22 22:51 BRFND0.6982.40.31 0.53
Styrene ND 0.035 4/26/22 22:51 BRFND0.6980.150.018 0.078
1,1,2,2-Tetrachloroethane ND 0.035 4/26/22 22:51 BRFND0.6980.240.019 0.13
Page 16 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 4000 Monroe Rd.
Date Received: 4/22/2022
Work Order: 22D1699Sample Description/Location:
Field Sample #: IA-7
Sample ID: 22D1699-07
Sample Matrix: Indoor air
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -8
Receipt Vacuum(in Hg): -8.5
Sampled: 4/19/2022 19:12
Canister ID: 1624
Flow Controller ID: 3158
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 8 hr
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.035 4/26/22 22:51 BRFND0.6980.240.027 0.18
Tetrahydrofuran ND 0.35 4/26/22 22:51 BRFND0.6981.00.057 0.17
Toluene 0.23 0.035 4/26/22 22:51 BRF0.88 0.6980.130.020 0.075
1,2,4-Trichlorobenzene ND 0.035 4/26/22 22:51 BRFND0.6980.260.032 0.24
1,1,1-Trichloroethane ND 0.035 4/26/22 22:51 BRFND0.6980.190.027 0.15
1,1,2-Trichloroethane ND 0.035 4/26/22 22:51 BRFND0.6980.190.025 0.13
Trichloroethylene ND 0.035 4/26/22 22:51 BRFND0.6980.190.024 0.13
Trichlorofluoromethane (Freon 11)1.4 0.14 4/26/22 22:51 BRF7.8 0.6980.780.041 0.23
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.081 0.14 4/26/22 22:51 BRFJ0.62 0.6981.10.039 0.30
1,2,4-Trimethylbenzene 0.33 0.035 4/26/22 22:51 BRF1.6 0.6980.170.015 0.076
1,3,5-Trimethylbenzene 0.081 0.035 4/26/22 22:51 BRF0.40 0.6980.170.018 0.091
Vinyl Acetate ND 0.70 4/26/22 22:51 BRFND0.6982.50.19 0.66
Vinyl Chloride ND 0.035 4/26/22 22:51 BRFND0.6980.0890.031 0.080
m&p-Xylene 1.3 0.070 4/26/22 22:51 BRF5.5 0.6980.300.039 0.17
o-Xylene 0.38 0.035 4/26/22 22:51 BRF1.7 0.6980.150.018 0.078
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)102 4/26/22 23:2470-130
4-Bromofluorobenzene (1)105 4/26/22 22:5170-130
Page 17 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
22D1699-01 [IA-1]B306974 1.5 1 N/A 1000 200 430 04/26/22
22D1699-02 [IA-2]B306974 1.5 1 N/A 1000 200 430 04/26/22
22D1699-03 [IA-3]B306974 1.5 1 N/A 1000 200 430 04/26/22
22D1699-04 [IA-4]B306974 1.5 1 N/A 1000 200 430 04/26/22
22D1699-05 [IA-5]B306974 1.5 1 N/A 1000 200 430 04/26/22
22D1699-05RE1 [IA-5]B306974 1.5 1 N/A 1000 200 30 04/26/22
22D1699-06 [IA-6]B306974 1.5 1 N/A 1000 200 430 04/26/22
22D1699-06RE1 [IA-6]B306974 1.5 1 N/A 1000 200 30 04/26/22
22D1699-07 [IA-7]B306974 1.5 1 N/A 1000 200 430 04/26/22
22D1699-07RE1 [IA-7]B306974 1.5 1 N/A 1000 200 30 04/26/22
Page 18 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B306974 - TO-15 Prep
Blank (B306974-BLK1)Prepared & Analyzed: 04/26/22
0.80NDAcetone
0.020NDBenzene
0.040NDBenzyl chloride
0.020NDBromodichloromethane
0.020NDBromoform
0.020NDBromomethane
0.020ND1,3-Butadiene
0.80ND2-Butanone (MEK)
0.20NDCarbon Disulfide
0.020NDCarbon Tetrachloride
0.020NDChlorobenzene
0.020NDChloroethane
0.020NDChloroform
0.040NDChloromethane
0.020NDCyclohexane
0.020NDDibromochloromethane
0.020ND1,2-Dibromoethane (EDB)
0.020ND1,2-Dichlorobenzene
0.020ND1,3-Dichlorobenzene
0.020ND1,4-Dichlorobenzene
0.020NDDichlorodifluoromethane (Freon 12)
0.020ND1,1-Dichloroethane
0.020ND1,2-Dichloroethane
0.020ND1,1-Dichloroethylene
0.020NDcis-1,2-Dichloroethylene
0.020NDtrans-1,2-Dichloroethylene
0.020ND1,2-Dichloropropane
0.020NDcis-1,3-Dichloropropene
0.020NDtrans-1,3-Dichloropropene
0.020ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.20ND1,4-Dioxane
0.80NDEthanol
0.20NDEthyl Acetate
0.020NDEthylbenzene
0.020ND4-Ethyltoluene
0.020NDHeptane
0.020NDHexachlorobutadiene
0.80NDHexane
0.020ND2-Hexanone (MBK)
0.80NDIsopropanol
0.020NDMethyl tert-Butyl Ether (MTBE)
0.20NDMethylene Chloride
0.020ND4-Methyl-2-pentanone (MIBK)
0.020NDNaphthalene
0.80NDPropene
0.020NDStyrene
Page 19 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B306974 - TO-15 Prep
Blank (B306974-BLK1)Prepared & Analyzed: 04/26/22
0.020ND1,1,2,2-Tetrachloroethane
0.020NDTetrachloroethylene
0.20NDTetrahydrofuran
0.020NDToluene
0.020ND1,2,4-Trichlorobenzene
0.020ND1,1,1-Trichloroethane
0.020ND1,1,2-Trichloroethane
0.020NDTrichloroethylene
0.080NDTrichlorofluoromethane (Freon 11)
0.080ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.020ND1,2,4-Trimethylbenzene
0.020ND1,3,5-Trimethylbenzene
0.40NDVinyl Acetate
0.020NDVinyl Chloride
0.040NDm&p-Xylene
0.020NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1018.07
LCS (B306974-BS1)Prepared & Analyzed: 04/26/22
5.00 70-13090.14.50Acetone
5.00 70-13085.34.27Benzene
5.00 V-3670-1301145.71Benzyl chloride
5.00 70-13083.74.18Bromodichloromethane
5.00 70-13099.34.96Bromoform
5.00 70-1301035.13Bromomethane
5.00 70-13094.34.711,3-Butadiene
5.00 70-13086.34.322-Butanone (MEK)
5.00 70-13097.24.86Carbon Disulfide
5.00 70-13088.44.42Carbon Tetrachloride
5.00 70-13091.34.57Chlorobenzene
5.00 70-1301015.04Chloroethane
5.00 70-1301025.08Chloroform
5.00 70-13090.54.53Chloromethane
5.00 70-13090.64.53Cyclohexane
5.00 70-13094.44.72Dibromochloromethane
5.00 70-13093.44.671,2-Dibromoethane (EDB)
5.00 70-1301025.111,2-Dichlorobenzene
5.00 70-1301105.491,3-Dichlorobenzene
5.00 70-1301105.521,4-Dichlorobenzene
5.00 70-13097.94.90Dichlorodifluoromethane (Freon 12)
5.00 70-1301005.021,1-Dichloroethane
5.00 70-13093.84.691,2-Dichloroethane
5.00 70-13095.44.771,1-Dichloroethylene
5.00 70-13096.24.81cis-1,2-Dichloroethylene
5.00 70-13097.74.88trans-1,2-Dichloroethylene
5.00 70-13081.24.061,2-Dichloropropane
Page 20 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B306974 - TO-15 Prep
LCS (B306974-BS1)Prepared & Analyzed: 04/26/22
5.00 70-13085.84.29cis-1,3-Dichloropropene
5.00 70-13087.94.40trans-1,3-Dichloropropene
5.00 70-13095.14.751,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
5.00 70-13096.64.831,4-Dioxane
5.00 70-13090.04.50Ethanol
5.00 70-13092.44.62Ethyl Acetate
5.00 70-13089.14.46Ethylbenzene
5.00 70-13095.84.794-Ethyltoluene
5.00 70-13084.64.23Heptane
5.00 70-13093.54.68Hexachlorobutadiene
5.00 70-13092.14.61Hexane
5.00 70-13088.44.422-Hexanone (MBK)
5.00 70-13079.43.97Isopropanol
5.00 70-13098.94.94Methyl tert-Butyl Ether (MTBE)
5.00 70-13088.34.42Methylene Chloride
5.00 70-13082.04.104-Methyl-2-pentanone (MIBK)
5.00 70-13092.64.63Naphthalene
5.00 70-13088.54.42Propene
5.00 70-13097.64.88Styrene
5.00 70-13088.74.431,1,2,2-Tetrachloroethane
5.00 70-13093.94.70Tetrachloroethylene
5.00 70-13089.34.46Tetrahydrofuran
5.00 70-13089.04.45Toluene
5.00 V-3670-1301145.681,2,4-Trichlorobenzene
5.00 70-13085.54.271,1,1-Trichloroethane
5.00 70-13092.44.621,1,2-Trichloroethane
5.00 70-13088.54.43Trichloroethylene
5.00 70-1301025.11Trichlorofluoromethane (Freon 11)
5.00 70-13094.94.751,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-13095.54.781,2,4-Trimethylbenzene
5.00 70-1301015.031,3,5-Trimethylbenzene
5.00 70-13081.64.08Vinyl Acetate
5.00 70-13098.24.91Vinyl Chloride
10.0 70-13095.29.52m&p-Xylene
5.00 70-13094.64.73o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1088.63
Page 21 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Note: Blank Subtraction is not performed unless otherwise noted
*QC result is outside of established limits.
†Wide recovery limits established for difficult compound.
‡Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramµg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data
validation is not affected since sample result was "not detected" for this compound.
V-36
ANALYST
Thomas P. HniteckiTPH
Raisa A. PetraitisRAP
PDF Management StationSTATION
Kerry K. McGeeKKM
Brittany R. FiskBRF
Page 22 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S069304-ICV1 )Lab File ID: K22A075019.D Analyzed: 03/16/22 23:55
Bromochloromethane (1)104138 2.987 102745 2.987 60 - 140101 0.0000 +/-0.50
1,4-Difluorobenzene (1)315817 3.584 303801 3.579 60 - 140104 0.0050 +/-0.50
Chlorobenzene-d5 (1)233658 5.159 223280 5.159 60 - 140105 0.0000 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S070889-CCV1 )Lab File ID: K22A116004.D Analyzed: 04/26/22 09:00
Bromochloromethane (1)97154 2.992 102745 2.987 60 - 14095 0.0050 +/-0.50
1,4-Difluorobenzene (1)323453 3.584 303801 3.579 60 - 140106 0.0050 +/-0.50
Chlorobenzene-d5 (1)241568 5.159 223280 5.159 60 - 140108 0.0000 +/-0.50
LCS (B306974-BS1 )Lab File ID: K22A116005.D Analyzed: 04/26/22 09:31
Bromochloromethane (1)95505 2.991 97154 2.992 60 - 14098 -0.0010 +/-0.50
1,4-Difluorobenzene (1)326455 3.584 323453 3.584 60 - 140101 0.0000 +/-0.50
Chlorobenzene-d5 (1)238868 5.159 241568 5.159 60 - 14099 0.0000 +/-0.50
Blank (B306974-BLK1 )Lab File ID: K22A116008.D Analyzed: 04/26/22 11:24
Bromochloromethane (1)93530 2.992 97154 2.992 60 - 14096 0.0000 +/-0.50
1,4-Difluorobenzene (1)297714 3.584 323453 3.584 60 - 14092 0.0000 +/-0.50
Chlorobenzene-d5 (1)225983 5.159 241568 5.159 60 - 14094 0.0000 +/-0.50
IA-1 (22D1699-01 )Lab File ID: K22A116015.D Analyzed: 04/26/22 15:32
Bromochloromethane (1)93890 2.996 97154 2.992 60 - 14097 0.0040 +/-0.50
1,4-Difluorobenzene (1)294565 3.588 323453 3.584 60 - 14091 0.0040 +/-0.50
Chlorobenzene-d5 (1)232183 5.163 241568 5.159 60 - 14096 0.0040 +/-0.50
IA-2 (22D1699-02 )Lab File ID: K22A116017.D Analyzed: 04/26/22 16:40
Bromochloromethane (1)95526 2.996 97154 2.992 60 - 14098 0.0040 +/-0.50
1,4-Difluorobenzene (1)309054 3.588 323453 3.584 60 - 14096 0.0040 +/-0.50
Chlorobenzene-d5 (1)238233 5.163 241568 5.159 60 - 14099 0.0040 +/-0.50
IA-3 (22D1699-03 )Lab File ID: K22A116019.D Analyzed: 04/26/22 17:47
Bromochloromethane (1)93117 2.996 97154 2.992 60 - 14096 0.0040 +/-0.50
1,4-Difluorobenzene (1)294015 3.584 323453 3.584 60 - 14091 0.0000 +/-0.50
Chlorobenzene-d5 (1)230379 5.159 241568 5.159 60 - 14095 0.0000 +/-0.50
IA-4 (22D1699-04 )Lab File ID: K22A116022.D Analyzed: 04/26/22 19:23
Bromochloromethane (1)92129 2.992 97154 2.992 60 - 14095 0.0000 +/-0.50
1,4-Difluorobenzene (1)291828 3.584 323453 3.584 60 - 14090 0.0000 +/-0.50
Chlorobenzene-d5 (1)225994 5.159 241568 5.159 60 - 14094 0.0000 +/-0.50
Page 23 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
IA-5 (22D1699-05 )Lab File ID: K22A116024.D Analyzed: 04/26/22 20:33
Bromochloromethane (1)92182 2.996 97154 2.992 60 - 14095 0.0040 +/-0.50
1,4-Difluorobenzene (1)294926 3.584 323453 3.584 60 - 14091 0.0000 +/-0.50
Chlorobenzene-d5 (1)233728 5.159 241568 5.159 60 - 14097 0.0000 +/-0.50
IA-5 (22D1699-05RE1 )Lab File ID: K22A116025.D Analyzed: 04/26/22 21:05
Bromochloromethane (1)91589 2.992 97154 2.992 60 - 14094 0.0000 +/-0.50
1,4-Difluorobenzene (1)288367 3.584 323453 3.584 60 - 14089 0.0000 +/-0.50
Chlorobenzene-d5 (1)221265 5.163 241568 5.159 60 - 14092 0.0040 +/-0.50
IA-6 (22D1699-06 )Lab File ID: K22A116026.D Analyzed: 04/26/22 21:42
Bromochloromethane (1)90300 2.996 97154 2.992 60 - 14093 0.0040 +/-0.50
1,4-Difluorobenzene (1)291895 3.584 323453 3.584 60 - 14090 0.0000 +/-0.50
Chlorobenzene-d5 (1)228164 5.159 241568 5.159 60 - 14094 0.0000 +/-0.50
IA-6 (22D1699-06RE1 )Lab File ID: K22A116027.D Analyzed: 04/26/22 22:14
Bromochloromethane (1)90889 2.992 97154 2.992 60 - 14094 0.0000 +/-0.50
1,4-Difluorobenzene (1)287428 3.584 323453 3.584 60 - 14089 0.0000 +/-0.50
Chlorobenzene-d5 (1)218037 5.159 241568 5.159 60 - 14090 0.0000 +/-0.50
IA-7 (22D1699-07 )Lab File ID: K22A116028.D Analyzed: 04/26/22 22:51
Bromochloromethane (1)92092 2.996 97154 2.992 60 - 14095 0.0040 +/-0.50
1,4-Difluorobenzene (1)289156 3.584 323453 3.584 60 - 14089 0.0000 +/-0.50
Chlorobenzene-d5 (1)226408 5.159 241568 5.159 60 - 14094 0.0000 +/-0.50
IA-7 (22D1699-07RE1 )Lab File ID: K22A116029.D Analyzed: 04/26/22 23:24
Bromochloromethane (1)91451 2.996 97154 2.992 60 - 14094 0.0040 +/-0.50
1,4-Difluorobenzene (1)289553 3.588 323453 3.584 60 - 14090 0.0040 +/-0.50
Chlorobenzene-d5 (1)217778 5.159 241568 5.159 60 - 14090 0.0000 +/-0.50
Page 24 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S070889-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.927056A -7.3 304.63 1.0005655.00Acetone
0.6016825A -4.9 304.75 0.63275915.00Benzene
0.558266A 26.3 306.31 0.44216445.00Benzyl chloride
0.4207498A -6.1 304.69 0.44785535.00Bromodichloromethane
0.5780501A 9.1 305.44 0.53002115.00Bromoform
0.6436626A 13.3 305.66 0.56819065.00Bromomethane
0.5239023A 6.1 305.30 0.49389165.001,3-Butadiene
1.047047A -8.4 304.58 1.1427965.002-Butanone (MEK)
2.174346A 4.1 305.17 2.0889415.00Carbon Disulfide
0.360223A 0.7 305.03 0.35787875.00Carbon Tetrachloride
0.7411511A 1.4 305.07 0.73082645.00Chlorobenzene
0.3944912A 5.8 305.29 0.37271415.00Chloroethane
1.335414A 10.8 305.54 1.2054345.00Chloroform
0.590617A 1.1 305.05 0.58407155.00Chloromethane
0.2455553A -0.6 304.96 0.24707665.00Cyclohexane
0.5608889A 4.5 305.23 0.53660835.00Dibromochloromethane
0.4873493A 3.7 305.19 0.46991195.001,2-Dibromoethane (EDB)
0.6135382A 13.1 305.65 0.54259785.001,2-Dichlorobenzene
0.6597894A 18.0 305.92 0.55904685.001,3-Dichlorobenzene
0.5386011A 11.2 305.56 0.48421685.001,4-Dichlorobenzene
1.519188A 5.7 305.28 1.4366615.00Dichlorodifluoromethane (Freon 12)
1.054211A 6.2 305.31 0.99287285.001,1-Dichloroethane
0.7768944A 2.2 305.11 0.76016775.001,2-Dichloroethane
1.04512A 2.0 305.10 1.0249615.001,1-Dichloroethylene
0.8506412A 4.1 305.20 0.81706385.00cis-1,2-Dichloroethylene
0.8763818A 6.1 305.30 0.82618555.00trans-1,2-Dichloroethylene
0.2320906A -8.0 304.60 0.25221315.001,2-Dichloropropane
0.3947553A -2.2 304.88 0.40368315.00cis-1,3-Dichloropropene
0.2769763A -1.7 304.91 0.28179515.00trans-1,3-Dichloropropene
1.72592A 9.9 305.49 1.5704175.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.126866A 1.5 305.06 0.12504885.001,4-Dioxane
0.2202853A -6.1 304.69 0.23459935.00Ethanol
0.1727237A -3.9 304.80 0.1796975.00Ethyl Acetate
1.152524A -1.2 304.94 1.1663635.00Ethylbenzene
1.167989A 7.0 305.35 1.0916415.004-Ethyltoluene
0.2258776A -4.6 304.76 0.23675525.00Heptane
0.3967943A 3.1 305.16 0.38473725.00Hexachlorobutadiene
0.6149248L -2.0 304.90 0.61131925.00Hexane
Page 25 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S070889-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.4998079A -5.6 304.72 0.52939375.002-Hexanone (MBK)
1.220775A -0.9 304.95 1.2321385.00Isopropanol
1.507512A 7.4 305.37 1.4032345.00Methyl tert-Butyl Ether (MTBE)
0.7417337A -4.2 304.79 0.7746185.00Methylene Chloride
9.122067E-02A -11.9 304.40 0.10352975.004-Methyl-2-pentanone (MIBK)
0.8632667A -4.8 304.76 0.90681415.00Naphthalene
0.4648126A -2.2 304.88 0.47538415.00Propene
0.6810703A 9.9 305.50 0.6196185.00Styrene
0.739853A -3.3 304.84 0.76502585.001,1,2,2-Tetrachloroethane
0.420208A 4.4 305.22 0.40258465.00Tetrachloroethylene
0.6004158A -3.0 304.85 0.61895225.00Tetrahydrofuran
0.9408531A -1.9 304.91 0.95897385.00Toluene
0.3443171A 19.2 305.96 0.28888655.001,2,4-Trichlorobenzene
0.3961107A -1.0 304.94 0.39993535.001,1,1-Trichloroethane
0.3363359A 0.7 305.04 0.33398865.001,1,2-Trichloroethane
0.2622897A -1.6 304.91 0.26654695.00Trichloroethylene
1.519205A 11.5 305.57 1.3626215.00Trichlorofluoromethane (Freon 11)
1.534356A 17.4 305.85 1.3073015.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
0.9776527A 7.4 305.37 0.91020485.001,2,4-Trimethylbenzene
1.041893A 11.8 305.60 0.93205925.001,3,5-Trimethylbenzene
1.353875A -8.0 304.65 1.4714225.00Vinyl Acetate
0.7098009A 6.0 305.30 0.6697665.00Vinyl Chloride
1.036167A 5.0 3010.5 0.987220410.0m&p-Xylene
0.9378792A 4.1 305.21 0.9007275.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 26 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,ME,NHAcetone
AIHA,FL,NJ,NY,ME,NH,VABenzene
AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride
AIHA,NJ,NY,ME,NH,VABromodichloromethane
AIHA,NJ,NY,ME,NH,VABromoform
AIHA,FL,NJ,NY,ME,NHBromomethane
AIHA,NJ,NY,ME,NH,VA1,3-Butadiene
AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
AIHA,NJ,NY,ME,NH,VACarbon Disulfide
AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride
AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene
AIHA,FL,NJ,NY,ME,NH,VAChloroethane
AIHA,FL,NJ,NY,ME,NH,VAChloroform
AIHA,FL,NJ,NY,ME,NH,VAChloromethane
AIHA,NJ,NY,ME,NH,VACyclohexane
AIHA,NY,ME,NHDibromochloromethane
AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
AIHA,NY,ME,NHtrans-1,3-Dichloropropene
AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,ME,NH,VA1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,ME,NH,VAHeptane
AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene
AIHA,FL,NJ,NY,ME,NH,VAHexane
AIHA2-Hexanone (MBK)
AIHA,NY,ME,NHIsopropanol
AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride
AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
AIHAPropene
AIHA,FL,NJ,NY,ME,NH,VAStyrene
AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
Page 27 of 31
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,ME,NH,VAToluene
AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene
AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride
AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene
AIHA,FL,NJ,NY,ME,NH,VAo-Xylene
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2024
M-MA100Massachusetts DEPMA 06/30/2022
PH-0165Connecticut Department of Publilc HealthCT 12/31/2022
10899 NELAPNew York State Department of HealthNY 04/1/2023
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2023
LAO00373Rhode Island Department of HealthRI 12/30/2022
652North Carolina Div. of Water QualityNC 12/31/2022
MA007 NELAPNew Jersey DEPNJ 06/30/2022
E871027 NELAPFlorida Department of HealthFL 06/30/2022
LL720741Vermont Department of Health Lead LaboratoryVT 07/30/2022
MA00100State of MaineME 06/9/2023
460217Commonwealth of VirginiaVA 12/14/2022
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2022
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2022
25703North Carolina Department of HealthNC-DW 07/31/2022
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2022
9100Dept. of Env, Great Lakes, and EnergyMI 09/6/2022
Page 28 of 31
Page 29 of 31
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Page 31 of 31
#=CL#
March 11, 2022
LIMS USE: FR - SCOTT YOUNG
LIMS OBJECT ID: 92590340
92590340
Project:
Pace Project No.:
RE:
Scott Young
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
Monroe Road Project
Dear Scott Young:
Enclosed are the analytical results for sample(s) received by the laboratory on February 25, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 60
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92590340
Monroe Road Project
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 60
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92590340
Monroe Road Project
Lab ID Sample ID Matrix Date Collected Date Received
92590340001 SB-1 Solid 02/25/22 11:40 02/25/22 14:35
92590340002 SB-2 Solid 02/25/22 12:00 02/25/22 14:35
92590340003 SB-3 Solid 02/25/22 12:20 02/25/22 14:35
92590340004 DUP-1 Solid 02/25/22 00:00 02/25/22 14:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 60
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92590340
Monroe Road Project
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92590340001 SB-1 EPA 6010D 7 PASI-GAKH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92590340002 SB-2 EPA 6010D 7 PASI-GAKH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92590340003 SB-3 EPA 6010D 7 PASI-GAKH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92590340004 DUP-1 EPA 6010D 7 PASI-GAKH
EPA 7471B 1 PASI-GAVB
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 60
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92590340
Monroe Road Project
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92590340001 SB-1
Barium 29.0 mg/kg 03/03/22 20:061.1EPA 6010D
Chromium 4.0 mg/kg 03/03/22 20:061.1EPA 6010D
Lead 9.5 mg/kg 03/03/22 20:062.8EPA 6010D
Mercury 0.043J mg/kg 03/02/22 09:510.27EPA 7471B
Percent Moisture 13.0 %02/25/22 17:48 N20.10SW-846
92590340002 SB-2
Barium 33.1 mg/kg 03/03/22 20:101.2EPA 6010D
Chromium 12.8 mg/kg 03/03/22 20:101.2EPA 6010D
Lead 23.0 mg/kg 03/03/22 20:103.0EPA 6010D
Mercury 0.068J mg/kg 03/02/22 09:590.27EPA 7471B
Benzo(b)fluoranthene 0.15J mg/kg 03/03/22 11:520.42EPA 8270E
Fluoranthene 0.22J mg/kg 03/03/22 11:520.42EPA 8270E
Phenanthrene 0.14J mg/kg 03/03/22 11:520.42EPA 8270E
Pyrene 0.19J mg/kg 03/03/22 11:520.42EPA 8270E
Tetrachloroethene 0.0067J mg/kg 03/01/22 01:420.0067EPA 8260D
Percent Moisture 20.1 %02/25/22 17:48 N20.10SW-846
92590340003 SB-3
Arsenic 2.6J mg/kg 03/03/22 20:153.4EPA 6010D
Barium 86.7 mg/kg 03/03/22 20:151.1EPA 6010D
Chromium 16.1 mg/kg 03/03/22 20:151.1EPA 6010D
Lead 16.9 mg/kg 03/03/22 20:152.9EPA 6010D
Mercury 0.036J mg/kg 03/02/22 10:010.27EPA 7471B
Percent Moisture 14.7 %02/25/22 17:48 N20.10SW-846
92590340004 DUP-1
Barium 34.3 mg/kg 03/03/22 20:201.1EPA 6010D
Chromium 7.1 mg/kg 03/03/22 20:201.1EPA 6010D
Lead 12.7 mg/kg 03/03/22 20:202.9EPA 6010D
Mercury 0.039J mg/kg 03/02/22 10:040.26EPA 7471B
Percent Moisture 12.5 %02/25/22 17:48 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-1 Lab ID:92590340001 Collected:02/25/22 11:40 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 03/03/22 20:06 7440-38-202/28/22 10:213.3 2.4 1
Barium 29.0 mg/kg 03/03/22 20:06 7440-39-302/28/22 10:211.1 0.29 1
Cadmium ND mg/kg 03/03/22 20:06 7440-43-902/28/22 10:211.1 0.33 1
Chromium 4.0 mg/kg 03/03/22 20:06 7440-47-302/28/22 10:211.1 1.0 1
Lead 9.5 mg/kg 03/03/22 20:06 7439-92-102/28/22 10:212.8 1.7 1
Selenium ND mg/kg 03/03/22 20:06 7782-49-202/28/22 10:214.4 4.1 1
Silver ND mg/kg 03/03/22 20:06 7440-22-402/28/22 10:211.1 0.45 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.043J mg/kg 03/02/22 09:51 7439-97-603/01/22 14:300.27 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 03/03/22 11:25 83-32-903/02/22 16:130.38 0.14 1
Acenaphthylene ND mg/kg 03/03/22 11:25 208-96-803/02/22 16:130.38 0.14 1
Aniline ND mg/kg 03/03/22 11:25 62-53-303/02/22 16:130.38 0.15 1
Anthracene ND mg/kg 03/03/22 11:25 120-12-703/02/22 16:130.38 0.13 1
Benzo(a)anthracene ND mg/kg 03/03/22 11:25 56-55-303/02/22 16:130.38 0.13 1
Benzo(a)pyrene ND mg/kg 03/03/22 11:25 50-32-803/02/22 16:130.38 0.13 1
Benzo(b)fluoranthene ND mg/kg 03/03/22 11:25 205-99-203/02/22 16:130.38 0.13 1
Benzo(g,h,i)perylene ND mg/kg 03/03/22 11:25 191-24-203/02/22 16:130.38 0.15 1
Benzo(k)fluoranthene ND mg/kg 03/03/22 11:25 207-08-903/02/22 16:130.38 0.14 1
Benzoic Acid ND mg/kg 03/03/22 11:25 65-85-003/02/22 16:131.9 0.83 1
Benzyl alcohol ND mg/kg 03/03/22 11:25 100-51-603/02/22 16:130.77 0.29 1
4-Bromophenylphenyl ether ND mg/kg 03/03/22 11:25 101-55-303/02/22 16:130.38 0.15 1
Butylbenzylphthalate ND mg/kg 03/03/22 11:25 85-68-703/02/22 16:130.38 0.16 1
4-Chloro-3-methylphenol ND mg/kg 03/03/22 11:25 59-50-703/02/22 16:130.77 0.27 1
4-Chloroaniline ND mg/kg 03/03/22 11:25 106-47-8 IL03/02/22 16:130.77 0.30 1
bis(2-Chloroethoxy)methane ND mg/kg 03/03/22 11:25 111-91-103/02/22 16:130.38 0.16 1
bis(2-Chloroethyl) ether ND mg/kg 03/03/22 11:25 111-44-403/02/22 16:130.38 0.14 1
2-Chloronaphthalene ND mg/kg 03/03/22 11:25 91-58-703/02/22 16:130.38 0.15 1
2-Chlorophenol ND mg/kg 03/03/22 11:25 95-57-803/02/22 16:130.38 0.14 1
4-Chlorophenylphenyl ether ND mg/kg 03/03/22 11:25 7005-72-303/02/22 16:130.38 0.14 1
Chrysene ND mg/kg 03/03/22 11:25 218-01-903/02/22 16:130.38 0.14 1
Dibenz(a,h)anthracene ND mg/kg 03/03/22 11:25 53-70-303/02/22 16:130.38 0.15 1
Dibenzofuran ND mg/kg 03/03/22 11:25 132-64-903/02/22 16:130.38 0.14 1
1,2-Dichlorobenzene ND mg/kg 03/03/22 11:25 95-50-103/02/22 16:130.38 0.14 1
1,3-Dichlorobenzene ND mg/kg 03/03/22 11:25 541-73-103/02/22 16:130.38 0.14 1
1,4-Dichlorobenzene ND mg/kg 03/03/22 11:25 106-46-703/02/22 16:130.38 0.15 1
3,3'-Dichlorobenzidine ND mg/kg 03/03/22 11:25 91-94-1 IL03/02/22 16:130.77 0.26 1
2,4-Dichlorophenol ND mg/kg 03/03/22 11:25 120-83-203/02/22 16:130.38 0.15 1
Diethylphthalate ND mg/kg 03/03/22 11:25 84-66-203/02/22 16:130.38 0.14 1
2,4-Dimethylphenol ND mg/kg 03/03/22 11:25 105-67-903/02/22 16:130.38 0.16 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-1 Lab ID:92590340001 Collected:02/25/22 11:40 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 03/03/22 11:25 131-11-303/02/22 16:130.38 0.14 1
Di-n-butylphthalate ND mg/kg 03/03/22 11:25 84-74-203/02/22 16:130.38 0.13 1
4,6-Dinitro-2-methylphenol ND mg/kg 03/03/22 11:25 534-52-103/02/22 16:130.77 0.36 1
2,4-Dinitrophenol ND mg/kg 03/03/22 11:25 51-28-503/02/22 16:131.9 1.2 1
2,4-Dinitrotoluene ND mg/kg 03/03/22 11:25 121-14-203/02/22 16:130.38 0.15 1
2,6-Dinitrotoluene ND mg/kg 03/03/22 11:25 606-20-203/02/22 16:130.38 0.14 1
Di-n-octylphthalate ND mg/kg 03/03/22 11:25 117-84-003/02/22 16:130.38 0.15 1
bis(2-Ethylhexyl)phthalate ND mg/kg 03/03/22 11:25 117-81-703/02/22 16:130.38 0.15 1
Fluoranthene ND mg/kg 03/03/22 11:25 206-44-003/02/22 16:130.38 0.13 1
Fluorene ND mg/kg 03/03/22 11:25 86-73-703/02/22 16:130.38 0.14 1
Hexachloro-1,3-butadiene ND mg/kg 03/03/22 11:25 87-68-3 v103/02/22 16:130.38 0.17 1
Hexachlorobenzene ND mg/kg 03/03/22 11:25 118-74-103/02/22 16:130.38 0.15 1
Hexachlorocyclopentadiene ND mg/kg 03/03/22 11:25 77-47-403/02/22 16:130.38 0.22 1
Hexachloroethane ND mg/kg 03/03/22 11:25 67-72-103/02/22 16:130.38 0.15 1
Indeno(1,2,3-cd)pyrene ND mg/kg 03/03/22 11:25 193-39-503/02/22 16:130.38 0.15 1
Isophorone ND mg/kg 03/03/22 11:25 78-59-103/02/22 16:130.38 0.17 1
1-Methylnaphthalene ND mg/kg 03/03/22 11:25 90-12-003/02/22 16:130.38 0.14 1
2-Methylnaphthalene ND mg/kg 03/03/22 11:25 91-57-603/02/22 16:130.38 0.15 1
2-Methylphenol(o-Cresol)ND mg/kg 03/03/22 11:25 95-48-703/02/22 16:130.38 0.16 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 03/03/22 11:25 15831-10-403/02/22 16:130.38 0.15 1
Naphthalene ND mg/kg 03/03/22 11:25 91-20-303/02/22 16:130.38 0.13 1
2-Nitroaniline ND mg/kg 03/03/22 11:25 88-74-403/02/22 16:131.9 0.31 1
3-Nitroaniline ND mg/kg 03/03/22 11:25 99-09-2 IL03/02/22 16:131.9 0.30 1
4-Nitroaniline ND mg/kg 03/03/22 11:25 100-01-603/02/22 16:130.77 0.29 1
Nitrobenzene ND mg/kg 03/03/22 11:25 98-95-303/02/22 16:130.38 0.18 1
2-Nitrophenol ND mg/kg 03/03/22 11:25 88-75-503/02/22 16:130.38 0.17 1
4-Nitrophenol ND mg/kg 03/03/22 11:25 100-02-703/02/22 16:131.9 0.74 1
N-Nitrosodimethylamine ND mg/kg 03/03/22 11:25 62-75-903/02/22 16:130.38 0.13 1
N-Nitroso-di-n-propylamine ND mg/kg 03/03/22 11:25 621-64-703/02/22 16:130.38 0.14 1
N-Nitrosodiphenylamine ND mg/kg 03/03/22 11:25 86-30-603/02/22 16:130.38 0.14 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 03/03/22 11:25 108-60-1 v103/02/22 16:130.38 0.18 1
Pentachlorophenol ND mg/kg 03/03/22 11:25 87-86-5 v203/02/22 16:130.77 0.38 1
Phenanthrene ND mg/kg 03/03/22 11:25 85-01-803/02/22 16:130.38 0.13 1
Phenol ND mg/kg 03/03/22 11:25 108-95-203/02/22 16:130.38 0.17 1
Pyrene ND mg/kg 03/03/22 11:25 129-00-003/02/22 16:130.38 0.16 1
Pyridine ND mg/kg 03/03/22 11:25 110-86-103/02/22 16:130.38 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 03/03/22 11:25 120-82-103/02/22 16:130.38 0.15 1
2,4,5-Trichlorophenol ND mg/kg 03/03/22 11:25 95-95-403/02/22 16:130.38 0.18 1
2,4,6-Trichlorophenol ND mg/kg 03/03/22 11:25 88-06-203/02/22 16:130.38 0.16 1
Surrogates
Nitrobenzene-d5 (S)74 %03/03/22 11:25 4165-60-003/02/22 16:1321-130 1
2-Fluorobiphenyl (S)63 %03/03/22 11:25 321-60-803/02/22 16:1319-130 1
Terphenyl-d14 (S)102 %03/03/22 11:25 1718-51-003/02/22 16:1315-130 1
Phenol-d6 (S)63 %03/03/22 11:25 13127-88-303/02/22 16:1318-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-1 Lab ID:92590340001 Collected:02/25/22 11:40 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)57 %03/03/22 11:25 367-12-403/02/22 16:1318-130 1
2,4,6-Tribromophenol (S)73 %03/03/22 11:25 118-79-603/02/22 16:1318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 03/01/22 01:23 67-64-102/25/22 21:030.11 0.037 1
Benzene ND mg/kg 03/01/22 01:23 71-43-202/25/22 21:030.0057 0.0023 1
Bromobenzene ND mg/kg 03/01/22 01:23 108-86-102/25/22 21:030.0057 0.0019 1
Bromochloromethane ND mg/kg 03/01/22 01:23 74-97-502/25/22 21:030.0057 0.0017 1
Bromodichloromethane ND mg/kg 03/01/22 01:23 75-27-402/25/22 21:030.0057 0.0022 1
Bromoform ND mg/kg 03/01/22 01:23 75-25-202/25/22 21:030.0057 0.0020 1
Bromomethane ND mg/kg 03/01/22 01:23 74-83-9 v202/25/22 21:030.011 0.0090 1
2-Butanone (MEK)ND mg/kg 03/01/22 01:23 78-93-302/25/22 21:030.11 0.027 1
n-Butylbenzene ND mg/kg 03/01/22 01:23 104-51-802/25/22 21:030.0057 0.0027 1
sec-Butylbenzene ND mg/kg 03/01/22 01:23 135-98-802/25/22 21:030.0057 0.0025 1
tert-Butylbenzene ND mg/kg 03/01/22 01:23 98-06-602/25/22 21:030.0057 0.0020 1
Carbon tetrachloride ND mg/kg 03/01/22 01:23 56-23-502/25/22 21:030.0057 0.0021 1
Chlorobenzene ND mg/kg 03/01/22 01:23 108-90-702/25/22 21:030.0057 0.0011 1
Chloroethane ND mg/kg 03/01/22 01:23 75-00-302/25/22 21:030.011 0.0044 1
Chloroform ND mg/kg 03/01/22 01:23 67-66-302/25/22 21:030.0057 0.0035 1
Chloromethane ND mg/kg 03/01/22 01:23 74-87-302/25/22 21:030.011 0.0048 1
2-Chlorotoluene ND mg/kg 03/01/22 01:23 95-49-802/25/22 21:030.0057 0.0020 1
4-Chlorotoluene ND mg/kg 03/01/22 01:23 106-43-402/25/22 21:030.0057 0.0010 1
1,2-Dibromo-3-chloropropane ND mg/kg 03/01/22 01:23 96-12-802/25/22 21:030.0057 0.0022 1
Dibromochloromethane ND mg/kg 03/01/22 01:23 124-48-102/25/22 21:030.0057 0.0032 1
1,2-Dibromoethane (EDB)ND mg/kg 03/01/22 01:23 106-93-402/25/22 21:030.0057 0.0025 1
Dibromomethane ND mg/kg 03/01/22 01:23 74-95-302/25/22 21:030.0057 0.0012 1
1,2-Dichlorobenzene ND mg/kg 03/01/22 01:23 95-50-102/25/22 21:030.0057 0.0021 1
1,3-Dichlorobenzene ND mg/kg 03/01/22 01:23 541-73-102/25/22 21:030.0057 0.0018 1
1,4-Dichlorobenzene ND mg/kg 03/01/22 01:23 106-46-702/25/22 21:030.0057 0.0015 1
Dichlorodifluoromethane ND mg/kg 03/01/22 01:23 75-71-802/25/22 21:030.011 0.0025 1
1,1-Dichloroethane ND mg/kg 03/01/22 01:23 75-34-302/25/22 21:030.0057 0.0024 1
1,2-Dichloroethane ND mg/kg 03/01/22 01:23 107-06-202/25/22 21:030.0057 0.0038 1
1,1-Dichloroethene ND mg/kg 03/01/22 01:23 75-35-402/25/22 21:030.0057 0.0024 1
cis-1,2-Dichloroethene ND mg/kg 03/01/22 01:23 156-59-202/25/22 21:030.0057 0.0020 1
trans-1,2-Dichloroethene ND mg/kg 03/01/22 01:23 156-60-502/25/22 21:030.0057 0.0020 1
1,2-Dichloropropane ND mg/kg 03/01/22 01:23 78-87-502/25/22 21:030.0057 0.0017 1
1,3-Dichloropropane ND mg/kg 03/01/22 01:23 142-28-902/25/22 21:030.0057 0.0018 1
2,2-Dichloropropane ND mg/kg 03/01/22 01:23 594-20-702/25/22 21:030.0057 0.0019 1
1,1-Dichloropropene ND mg/kg 03/01/22 01:23 563-58-602/25/22 21:030.0057 0.0027 1
cis-1,3-Dichloropropene ND mg/kg 03/01/22 01:23 10061-01-502/25/22 21:030.0057 0.0016 1
trans-1,3-Dichloropropene ND mg/kg 03/01/22 01:23 10061-02-602/25/22 21:030.0057 0.0020 1
Diisopropyl ether ND mg/kg 03/01/22 01:23 108-20-302/25/22 21:030.0057 0.0015 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-1 Lab ID:92590340001 Collected:02/25/22 11:40 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 03/01/22 01:23 100-41-402/25/22 21:030.0057 0.0027 1
Hexachloro-1,3-butadiene ND mg/kg 03/01/22 01:23 87-68-302/25/22 21:030.011 0.0094 1
2-Hexanone ND mg/kg 03/01/22 01:23 591-78-602/25/22 21:030.057 0.0055 1
Isopropylbenzene (Cumene)ND mg/kg 03/01/22 01:23 98-82-802/25/22 21:030.0057 0.0019 1
p-Isopropyltoluene ND mg/kg 03/01/22 01:23 99-87-602/25/22 21:030.0057 0.0028 1
Methylene Chloride ND mg/kg 03/01/22 01:23 75-09-202/25/22 21:030.023 0.016 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 03/01/22 01:23 108-10-102/25/22 21:030.057 0.0055 1
Methyl-tert-butyl ether ND mg/kg 03/01/22 01:23 1634-04-402/25/22 21:030.0057 0.0021 1
Naphthalene ND mg/kg 03/01/22 01:23 91-20-302/25/22 21:030.0057 0.0030 1
n-Propylbenzene ND mg/kg 03/01/22 01:23 103-65-102/25/22 21:030.0057 0.0020 1
Styrene ND mg/kg 03/01/22 01:23 100-42-502/25/22 21:030.0057 0.0015 1
1,1,1,2-Tetrachloroethane ND mg/kg 03/01/22 01:23 630-20-602/25/22 21:030.0057 0.0022 1
1,1,2,2-Tetrachloroethane ND mg/kg 03/01/22 01:23 79-34-502/25/22 21:030.0057 0.0015 1
Tetrachloroethene ND mg/kg 03/01/22 01:23 127-18-402/25/22 21:030.0057 0.0018 1
Toluene ND mg/kg 03/01/22 01:23 108-88-302/25/22 21:030.0057 0.0016 1
1,2,3-Trichlorobenzene ND mg/kg 03/01/22 01:23 87-61-602/25/22 21:030.0057 0.0046 1
1,2,4-Trichlorobenzene ND mg/kg 03/01/22 01:23 120-82-102/25/22 21:030.0057 0.0048 1
1,1,1-Trichloroethane ND mg/kg 03/01/22 01:23 71-55-602/25/22 21:030.0057 0.0030 1
1,1,2-Trichloroethane ND mg/kg 03/01/22 01:23 79-00-502/25/22 21:030.0057 0.0019 1
Trichloroethene ND mg/kg 03/01/22 01:23 79-01-602/25/22 21:030.0057 0.0015 1
Trichlorofluoromethane ND mg/kg 03/01/22 01:23 75-69-402/25/22 21:030.0057 0.0031 1
1,2,3-Trichloropropane ND mg/kg 03/01/22 01:23 96-18-402/25/22 21:030.0057 0.0029 1
1,2,4-Trimethylbenzene ND mg/kg 03/01/22 01:23 95-63-602/25/22 21:030.0057 0.0016 1
1,3,5-Trimethylbenzene ND mg/kg 03/01/22 01:23 108-67-802/25/22 21:030.0057 0.0019 1
Vinyl acetate ND mg/kg 03/01/22 01:23 108-05-402/25/22 21:030.057 0.0042 1
Vinyl chloride ND mg/kg 03/01/22 01:23 75-01-402/25/22 21:030.011 0.0029 1
Xylene (Total)ND mg/kg 03/01/22 01:23 1330-20-702/25/22 21:030.011 0.0033 1
m&p-Xylene ND mg/kg 03/01/22 01:23 179601-23-102/25/22 21:030.011 0.0039 1
o-Xylene ND mg/kg 03/01/22 01:23 95-47-602/25/22 21:030.0057 0.0025 1
Surrogates
Toluene-d8 (S)99 %03/01/22 01:23 2037-26-502/25/22 21:0370-130 1
4-Bromofluorobenzene (S)96 %03/01/22 01:23 460-00-402/25/22 21:0369-134 1
1,2-Dichloroethane-d4 (S)94 %03/01/22 01:23 17060-07-002/25/22 21:0370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.0 %02/25/22 17:48 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-2 Lab ID:92590340002 Collected:02/25/22 12:00 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 03/03/22 20:10 7440-38-202/28/22 10:213.6 2.6 1
Barium 33.1 mg/kg 03/03/22 20:10 7440-39-302/28/22 10:211.2 0.32 1
Cadmium ND mg/kg 03/03/22 20:10 7440-43-902/28/22 10:211.2 0.36 1
Chromium 12.8 mg/kg 03/03/22 20:10 7440-47-302/28/22 10:211.2 1.1 1
Lead 23.0 mg/kg 03/03/22 20:10 7439-92-102/28/22 10:213.0 1.9 1
Selenium ND mg/kg 03/03/22 20:10 7782-49-202/28/22 10:214.8 4.5 1
Silver ND mg/kg 03/03/22 20:10 7440-22-402/28/22 10:211.2 0.49 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.068J mg/kg 03/02/22 09:59 7439-97-603/01/22 14:300.27 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 03/03/22 11:52 83-32-903/02/22 16:130.42 0.15 1
Acenaphthylene ND mg/kg 03/03/22 11:52 208-96-803/02/22 16:130.42 0.15 1
Aniline ND mg/kg 03/03/22 11:52 62-53-303/02/22 16:130.42 0.16 1
Anthracene ND mg/kg 03/03/22 11:52 120-12-703/02/22 16:130.42 0.14 1
Benzo(a)anthracene ND mg/kg 03/03/22 11:52 56-55-303/02/22 16:130.42 0.14 1
Benzo(a)pyrene ND mg/kg 03/03/22 11:52 50-32-803/02/22 16:130.42 0.14 1
Benzo(b)fluoranthene 0.15J mg/kg 03/03/22 11:52 205-99-203/02/22 16:130.42 0.14 1
Benzo(g,h,i)perylene ND mg/kg 03/03/22 11:52 191-24-203/02/22 16:130.42 0.16 1
Benzo(k)fluoranthene ND mg/kg 03/03/22 11:52 207-08-903/02/22 16:130.42 0.15 1
Benzoic Acid ND mg/kg 03/03/22 11:52 65-85-003/02/22 16:132.1 0.90 1
Benzyl alcohol ND mg/kg 03/03/22 11:52 100-51-603/02/22 16:130.83 0.32 1
4-Bromophenylphenyl ether ND mg/kg 03/03/22 11:52 101-55-303/02/22 16:130.42 0.16 1
Butylbenzylphthalate ND mg/kg 03/03/22 11:52 85-68-703/02/22 16:130.42 0.18 1
4-Chloro-3-methylphenol ND mg/kg 03/03/22 11:52 59-50-703/02/22 16:130.83 0.29 1
4-Chloroaniline ND mg/kg 03/03/22 11:52 106-47-8 IL03/02/22 16:130.83 0.33 1
bis(2-Chloroethoxy)methane ND mg/kg 03/03/22 11:52 111-91-103/02/22 16:130.42 0.17 1
bis(2-Chloroethyl) ether ND mg/kg 03/03/22 11:52 111-44-403/02/22 16:130.42 0.16 1
2-Chloronaphthalene ND mg/kg 03/03/22 11:52 91-58-703/02/22 16:130.42 0.17 1
2-Chlorophenol ND mg/kg 03/03/22 11:52 95-57-803/02/22 16:130.42 0.16 1
4-Chlorophenylphenyl ether ND mg/kg 03/03/22 11:52 7005-72-303/02/22 16:130.42 0.16 1
Chrysene ND mg/kg 03/03/22 11:52 218-01-903/02/22 16:130.42 0.15 1
Dibenz(a,h)anthracene ND mg/kg 03/03/22 11:52 53-70-303/02/22 16:130.42 0.16 1
Dibenzofuran ND mg/kg 03/03/22 11:52 132-64-903/02/22 16:130.42 0.15 1
1,2-Dichlorobenzene ND mg/kg 03/03/22 11:52 95-50-103/02/22 16:130.42 0.15 1
1,3-Dichlorobenzene ND mg/kg 03/03/22 11:52 541-73-103/02/22 16:130.42 0.15 1
1,4-Dichlorobenzene ND mg/kg 03/03/22 11:52 106-46-703/02/22 16:130.42 0.16 1
3,3'-Dichlorobenzidine ND mg/kg 03/03/22 11:52 91-94-1 IL03/02/22 16:130.83 0.28 1
2,4-Dichlorophenol ND mg/kg 03/03/22 11:52 120-83-203/02/22 16:130.42 0.16 1
Diethylphthalate ND mg/kg 03/03/22 11:52 84-66-203/02/22 16:130.42 0.15 1
2,4-Dimethylphenol ND mg/kg 03/03/22 11:52 105-67-903/02/22 16:130.42 0.17 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-2 Lab ID:92590340002 Collected:02/25/22 12:00 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 03/03/22 11:52 131-11-303/02/22 16:130.42 0.15 1
Di-n-butylphthalate ND mg/kg 03/03/22 11:52 84-74-203/02/22 16:130.42 0.14 1
4,6-Dinitro-2-methylphenol ND mg/kg 03/03/22 11:52 534-52-103/02/22 16:130.83 0.39 1
2,4-Dinitrophenol ND mg/kg 03/03/22 11:52 51-28-503/02/22 16:132.1 1.3 1
2,4-Dinitrotoluene ND mg/kg 03/03/22 11:52 121-14-203/02/22 16:130.42 0.16 1
2,6-Dinitrotoluene ND mg/kg 03/03/22 11:52 606-20-203/02/22 16:130.42 0.15 1
Di-n-octylphthalate ND mg/kg 03/03/22 11:52 117-84-003/02/22 16:130.42 0.16 1
bis(2-Ethylhexyl)phthalate ND mg/kg 03/03/22 11:52 117-81-703/02/22 16:130.42 0.16 1
Fluoranthene 0.22J mg/kg 03/03/22 11:52 206-44-003/02/22 16:130.42 0.14 1
Fluorene ND mg/kg 03/03/22 11:52 86-73-703/02/22 16:130.42 0.15 1
Hexachloro-1,3-butadiene ND mg/kg 03/03/22 11:52 87-68-3 v103/02/22 16:130.42 0.18 1
Hexachlorobenzene ND mg/kg 03/03/22 11:52 118-74-103/02/22 16:130.42 0.16 1
Hexachlorocyclopentadiene ND mg/kg 03/03/22 11:52 77-47-403/02/22 16:130.42 0.24 1
Hexachloroethane ND mg/kg 03/03/22 11:52 67-72-103/02/22 16:130.42 0.16 1
Indeno(1,2,3-cd)pyrene ND mg/kg 03/03/22 11:52 193-39-503/02/22 16:130.42 0.16 1
Isophorone ND mg/kg 03/03/22 11:52 78-59-103/02/22 16:130.42 0.19 1
1-Methylnaphthalene ND mg/kg 03/03/22 11:52 90-12-003/02/22 16:130.42 0.15 1
2-Methylnaphthalene ND mg/kg 03/03/22 11:52 91-57-603/02/22 16:130.42 0.17 1
2-Methylphenol(o-Cresol)ND mg/kg 03/03/22 11:52 95-48-703/02/22 16:130.42 0.17 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 03/03/22 11:52 15831-10-403/02/22 16:130.42 0.17 1
Naphthalene ND mg/kg 03/03/22 11:52 91-20-303/02/22 16:130.42 0.14 1
2-Nitroaniline ND mg/kg 03/03/22 11:52 88-74-403/02/22 16:132.1 0.34 1
3-Nitroaniline ND mg/kg 03/03/22 11:52 99-09-2 IL03/02/22 16:132.1 0.33 1
4-Nitroaniline ND mg/kg 03/03/22 11:52 100-01-603/02/22 16:130.83 0.32 1
Nitrobenzene ND mg/kg 03/03/22 11:52 98-95-303/02/22 16:130.42 0.19 1
2-Nitrophenol ND mg/kg 03/03/22 11:52 88-75-503/02/22 16:130.42 0.18 1
4-Nitrophenol ND mg/kg 03/03/22 11:52 100-02-703/02/22 16:132.1 0.81 1
N-Nitrosodimethylamine ND mg/kg 03/03/22 11:52 62-75-903/02/22 16:130.42 0.14 1
N-Nitroso-di-n-propylamine ND mg/kg 03/03/22 11:52 621-64-703/02/22 16:130.42 0.16 1
N-Nitrosodiphenylamine ND mg/kg 03/03/22 11:52 86-30-603/02/22 16:130.42 0.15 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 03/03/22 11:52 108-60-1 v103/02/22 16:130.42 0.20 1
Pentachlorophenol ND mg/kg 03/03/22 11:52 87-86-5 v203/02/22 16:130.83 0.41 1
Phenanthrene 0.14J mg/kg 03/03/22 11:52 85-01-803/02/22 16:130.42 0.14 1
Phenol ND mg/kg 03/03/22 11:52 108-95-203/02/22 16:130.42 0.19 1
Pyrene 0.19J mg/kg 03/03/22 11:52 129-00-003/02/22 16:130.42 0.17 1
Pyridine ND mg/kg 03/03/22 11:52 110-86-103/02/22 16:130.42 0.13 1
1,2,4-Trichlorobenzene ND mg/kg 03/03/22 11:52 120-82-103/02/22 16:130.42 0.16 1
2,4,5-Trichlorophenol ND mg/kg 03/03/22 11:52 95-95-403/02/22 16:130.42 0.19 1
2,4,6-Trichlorophenol ND mg/kg 03/03/22 11:52 88-06-203/02/22 16:130.42 0.17 1
Surrogates
Nitrobenzene-d5 (S)59 %03/03/22 11:52 4165-60-003/02/22 16:1321-130 1
2-Fluorobiphenyl (S)49 %03/03/22 11:52 321-60-803/02/22 16:1319-130 1
Terphenyl-d14 (S)82 %03/03/22 11:52 1718-51-003/02/22 16:1315-130 1
Phenol-d6 (S)50 %03/03/22 11:52 13127-88-303/02/22 16:1318-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-2 Lab ID:92590340002 Collected:02/25/22 12:00 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)44 %03/03/22 11:52 367-12-403/02/22 16:1318-130 1
2,4,6-Tribromophenol (S)62 %03/03/22 11:52 118-79-603/02/22 16:1318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 03/01/22 01:42 67-64-102/25/22 21:030.13 0.043 1
Benzene ND mg/kg 03/01/22 01:42 71-43-202/25/22 21:030.0067 0.0027 1
Bromobenzene ND mg/kg 03/01/22 01:42 108-86-102/25/22 21:030.0067 0.0022 1
Bromochloromethane ND mg/kg 03/01/22 01:42 74-97-502/25/22 21:030.0067 0.0020 1
Bromodichloromethane ND mg/kg 03/01/22 01:42 75-27-402/25/22 21:030.0067 0.0026 1
Bromoform ND mg/kg 03/01/22 01:42 75-25-202/25/22 21:030.0067 0.0024 1
Bromomethane ND mg/kg 03/01/22 01:42 74-83-9 v202/25/22 21:030.013 0.011 1
2-Butanone (MEK)ND mg/kg 03/01/22 01:42 78-93-302/25/22 21:030.13 0.032 1
n-Butylbenzene ND mg/kg 03/01/22 01:42 104-51-802/25/22 21:030.0067 0.0032 1
sec-Butylbenzene ND mg/kg 03/01/22 01:42 135-98-802/25/22 21:030.0067 0.0030 1
tert-Butylbenzene ND mg/kg 03/01/22 01:42 98-06-602/25/22 21:030.0067 0.0024 1
Carbon tetrachloride ND mg/kg 03/01/22 01:42 56-23-502/25/22 21:030.0067 0.0025 1
Chlorobenzene ND mg/kg 03/01/22 01:42 108-90-702/25/22 21:030.0067 0.0013 1
Chloroethane ND mg/kg 03/01/22 01:42 75-00-302/25/22 21:030.013 0.0052 1
Chloroform ND mg/kg 03/01/22 01:42 67-66-302/25/22 21:030.0067 0.0041 1
Chloromethane ND mg/kg 03/01/22 01:42 74-87-302/25/22 21:030.013 0.0057 1
2-Chlorotoluene ND mg/kg 03/01/22 01:42 95-49-802/25/22 21:030.0067 0.0024 1
4-Chlorotoluene ND mg/kg 03/01/22 01:42 106-43-402/25/22 21:030.0067 0.0012 1
1,2-Dibromo-3-chloropropane ND mg/kg 03/01/22 01:42 96-12-802/25/22 21:030.0067 0.0026 1
Dibromochloromethane ND mg/kg 03/01/22 01:42 124-48-102/25/22 21:030.0067 0.0038 1
1,2-Dibromoethane (EDB)ND mg/kg 03/01/22 01:42 106-93-402/25/22 21:030.0067 0.0030 1
Dibromomethane ND mg/kg 03/01/22 01:42 74-95-302/25/22 21:030.0067 0.0014 1
1,2-Dichlorobenzene ND mg/kg 03/01/22 01:42 95-50-102/25/22 21:030.0067 0.0024 1
1,3-Dichlorobenzene ND mg/kg 03/01/22 01:42 541-73-102/25/22 21:030.0067 0.0021 1
1,4-Dichlorobenzene ND mg/kg 03/01/22 01:42 106-46-702/25/22 21:030.0067 0.0018 1
Dichlorodifluoromethane ND mg/kg 03/01/22 01:42 75-71-802/25/22 21:030.013 0.0029 1
1,1-Dichloroethane ND mg/kg 03/01/22 01:42 75-34-302/25/22 21:030.0067 0.0028 1
1,2-Dichloroethane ND mg/kg 03/01/22 01:42 107-06-202/25/22 21:030.0067 0.0045 1
1,1-Dichloroethene ND mg/kg 03/01/22 01:42 75-35-402/25/22 21:030.0067 0.0028 1
cis-1,2-Dichloroethene ND mg/kg 03/01/22 01:42 156-59-202/25/22 21:030.0067 0.0023 1
trans-1,2-Dichloroethene ND mg/kg 03/01/22 01:42 156-60-502/25/22 21:030.0067 0.0024 1
1,2-Dichloropropane ND mg/kg 03/01/22 01:42 78-87-502/25/22 21:030.0067 0.0020 1
1,3-Dichloropropane ND mg/kg 03/01/22 01:42 142-28-902/25/22 21:030.0067 0.0021 1
2,2-Dichloropropane ND mg/kg 03/01/22 01:42 594-20-702/25/22 21:030.0067 0.0022 1
1,1-Dichloropropene ND mg/kg 03/01/22 01:42 563-58-602/25/22 21:030.0067 0.0032 1
cis-1,3-Dichloropropene ND mg/kg 03/01/22 01:42 10061-01-502/25/22 21:030.0067 0.0018 1
trans-1,3-Dichloropropene ND mg/kg 03/01/22 01:42 10061-02-602/25/22 21:030.0067 0.0023 1
Diisopropyl ether ND mg/kg 03/01/22 01:42 108-20-302/25/22 21:030.0067 0.0018 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-2 Lab ID:92590340002 Collected:02/25/22 12:00 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 03/01/22 01:42 100-41-402/25/22 21:030.0067 0.0031 1
Hexachloro-1,3-butadiene ND mg/kg 03/01/22 01:42 87-68-302/25/22 21:030.013 0.011 1
2-Hexanone ND mg/kg 03/01/22 01:42 591-78-602/25/22 21:030.067 0.0065 1
Isopropylbenzene (Cumene)ND mg/kg 03/01/22 01:42 98-82-802/25/22 21:030.0067 0.0023 1
p-Isopropyltoluene ND mg/kg 03/01/22 01:42 99-87-602/25/22 21:030.0067 0.0033 1
Methylene Chloride ND mg/kg 03/01/22 01:42 75-09-202/25/22 21:030.027 0.018 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 03/01/22 01:42 108-10-102/25/22 21:030.067 0.0065 1
Methyl-tert-butyl ether ND mg/kg 03/01/22 01:42 1634-04-402/25/22 21:030.0067 0.0025 1
Naphthalene ND mg/kg 03/01/22 01:42 91-20-302/25/22 21:030.0067 0.0036 1
n-Propylbenzene ND mg/kg 03/01/22 01:42 103-65-102/25/22 21:030.0067 0.0024 1
Styrene ND mg/kg 03/01/22 01:42 100-42-502/25/22 21:030.0067 0.0018 1
1,1,1,2-Tetrachloroethane ND mg/kg 03/01/22 01:42 630-20-602/25/22 21:030.0067 0.0026 1
1,1,2,2-Tetrachloroethane ND mg/kg 03/01/22 01:42 79-34-502/25/22 21:030.0067 0.0018 1
Tetrachloroethene 0.0067J mg/kg 03/01/22 01:42 127-18-402/25/22 21:030.0067 0.0021 1
Toluene ND mg/kg 03/01/22 01:42 108-88-302/25/22 21:030.0067 0.0019 1
1,2,3-Trichlorobenzene ND mg/kg 03/01/22 01:42 87-61-602/25/22 21:030.0067 0.0055 1
1,2,4-Trichlorobenzene ND mg/kg 03/01/22 01:42 120-82-102/25/22 21:030.0067 0.0057 1
1,1,1-Trichloroethane ND mg/kg 03/01/22 01:42 71-55-602/25/22 21:030.0067 0.0035 1
1,1,2-Trichloroethane ND mg/kg 03/01/22 01:42 79-00-502/25/22 21:030.0067 0.0022 1
Trichloroethene ND mg/kg 03/01/22 01:42 79-01-602/25/22 21:030.0067 0.0017 1
Trichlorofluoromethane ND mg/kg 03/01/22 01:42 75-69-402/25/22 21:030.0067 0.0037 1
1,2,3-Trichloropropane ND mg/kg 03/01/22 01:42 96-18-402/25/22 21:030.0067 0.0034 1
1,2,4-Trimethylbenzene ND mg/kg 03/01/22 01:42 95-63-602/25/22 21:030.0067 0.0018 1
1,3,5-Trimethylbenzene ND mg/kg 03/01/22 01:42 108-67-802/25/22 21:030.0067 0.0023 1
Vinyl acetate ND mg/kg 03/01/22 01:42 108-05-402/25/22 21:030.067 0.0049 1
Vinyl chloride ND mg/kg 03/01/22 01:42 75-01-402/25/22 21:030.013 0.0034 1
Xylene (Total)ND mg/kg 03/01/22 01:42 1330-20-702/25/22 21:030.013 0.0038 1
m&p-Xylene ND mg/kg 03/01/22 01:42 179601-23-102/25/22 21:030.013 0.0046 1
o-Xylene ND mg/kg 03/01/22 01:42 95-47-602/25/22 21:030.0067 0.0030 1
Surrogates
Toluene-d8 (S)99 %03/01/22 01:42 2037-26-502/25/22 21:0370-130 1
4-Bromofluorobenzene (S)97 %03/01/22 01:42 460-00-402/25/22 21:0369-134 1
1,2-Dichloroethane-d4 (S)92 %03/01/22 01:42 17060-07-002/25/22 21:0370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.1 %02/25/22 17:48 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-3 Lab ID:92590340003 Collected:02/25/22 12:20 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic 2.6J mg/kg 03/03/22 20:15 7440-38-202/28/22 10:213.4 2.5 1
Barium 86.7 mg/kg 03/03/22 20:15 7440-39-302/28/22 10:211.1 0.31 1
Cadmium ND mg/kg 03/03/22 20:15 7440-43-902/28/22 10:211.1 0.34 1
Chromium 16.1 mg/kg 03/03/22 20:15 7440-47-302/28/22 10:211.1 1.0 1
Lead 16.9 mg/kg 03/03/22 20:15 7439-92-102/28/22 10:212.9 1.8 1
Selenium ND mg/kg 03/03/22 20:15 7782-49-202/28/22 10:214.6 4.3 1
Silver ND mg/kg 03/03/22 20:15 7440-22-402/28/22 10:211.1 0.47 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.036J mg/kg 03/02/22 10:01 7439-97-603/01/22 14:300.27 0.013 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 03/03/22 12:19 83-32-903/02/22 16:130.39 0.14 1
Acenaphthylene ND mg/kg 03/03/22 12:19 208-96-803/02/22 16:130.39 0.14 1
Aniline ND mg/kg 03/03/22 12:19 62-53-303/02/22 16:130.39 0.15 1
Anthracene ND mg/kg 03/03/22 12:19 120-12-703/02/22 16:130.39 0.13 1
Benzo(a)anthracene ND mg/kg 03/03/22 12:19 56-55-303/02/22 16:130.39 0.13 1
Benzo(a)pyrene ND mg/kg 03/03/22 12:19 50-32-803/02/22 16:130.39 0.14 1
Benzo(b)fluoranthene ND mg/kg 03/03/22 12:19 205-99-203/02/22 16:130.39 0.13 1
Benzo(g,h,i)perylene ND mg/kg 03/03/22 12:19 191-24-203/02/22 16:130.39 0.15 1
Benzo(k)fluoranthene ND mg/kg 03/03/22 12:19 207-08-903/02/22 16:130.39 0.14 1
Benzoic Acid ND mg/kg 03/03/22 12:19 65-85-003/02/22 16:132.0 0.85 1
Benzyl alcohol ND mg/kg 03/03/22 12:19 100-51-603/02/22 16:130.79 0.30 1
4-Bromophenylphenyl ether ND mg/kg 03/03/22 12:19 101-55-303/02/22 16:130.39 0.15 1
Butylbenzylphthalate ND mg/kg 03/03/22 12:19 85-68-703/02/22 16:130.39 0.17 1
4-Chloro-3-methylphenol ND mg/kg 03/03/22 12:19 59-50-703/02/22 16:130.79 0.28 1
4-Chloroaniline ND mg/kg 03/03/22 12:19 106-47-8 IL03/02/22 16:130.79 0.31 1
bis(2-Chloroethoxy)methane ND mg/kg 03/03/22 12:19 111-91-103/02/22 16:130.39 0.16 1
bis(2-Chloroethyl) ether ND mg/kg 03/03/22 12:19 111-44-403/02/22 16:130.39 0.15 1
2-Chloronaphthalene ND mg/kg 03/03/22 12:19 91-58-703/02/22 16:130.39 0.16 1
2-Chlorophenol ND mg/kg 03/03/22 12:19 95-57-803/02/22 16:130.39 0.15 1
4-Chlorophenylphenyl ether ND mg/kg 03/03/22 12:19 7005-72-303/02/22 16:130.39 0.15 1
Chrysene ND mg/kg 03/03/22 12:19 218-01-903/02/22 16:130.39 0.14 1
Dibenz(a,h)anthracene ND mg/kg 03/03/22 12:19 53-70-303/02/22 16:130.39 0.15 1
Dibenzofuran ND mg/kg 03/03/22 12:19 132-64-903/02/22 16:130.39 0.14 1
1,2-Dichlorobenzene ND mg/kg 03/03/22 12:19 95-50-103/02/22 16:130.39 0.14 1
1,3-Dichlorobenzene ND mg/kg 03/03/22 12:19 541-73-103/02/22 16:130.39 0.14 1
1,4-Dichlorobenzene ND mg/kg 03/03/22 12:19 106-46-703/02/22 16:130.39 0.15 1
3,3'-Dichlorobenzidine ND mg/kg 03/03/22 12:19 91-94-1 IL03/02/22 16:130.79 0.27 1
2,4-Dichlorophenol ND mg/kg 03/03/22 12:19 120-83-203/02/22 16:130.39 0.15 1
Diethylphthalate ND mg/kg 03/03/22 12:19 84-66-203/02/22 16:130.39 0.14 1
2,4-Dimethylphenol ND mg/kg 03/03/22 12:19 105-67-903/02/22 16:130.39 0.16 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-3 Lab ID:92590340003 Collected:02/25/22 12:20 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 03/03/22 12:19 131-11-303/02/22 16:130.39 0.14 1
Di-n-butylphthalate ND mg/kg 03/03/22 12:19 84-74-203/02/22 16:130.39 0.13 1
4,6-Dinitro-2-methylphenol ND mg/kg 03/03/22 12:19 534-52-103/02/22 16:130.79 0.37 1
2,4-Dinitrophenol ND mg/kg 03/03/22 12:19 51-28-503/02/22 16:132.0 1.2 1
2,4-Dinitrotoluene ND mg/kg 03/03/22 12:19 121-14-203/02/22 16:130.39 0.15 1
2,6-Dinitrotoluene ND mg/kg 03/03/22 12:19 606-20-203/02/22 16:130.39 0.14 1
Di-n-octylphthalate ND mg/kg 03/03/22 12:19 117-84-003/02/22 16:130.39 0.16 1
bis(2-Ethylhexyl)phthalate ND mg/kg 03/03/22 12:19 117-81-703/02/22 16:130.39 0.15 1
Fluoranthene ND mg/kg 03/03/22 12:19 206-44-003/02/22 16:130.39 0.13 1
Fluorene ND mg/kg 03/03/22 12:19 86-73-703/02/22 16:130.39 0.14 1
Hexachloro-1,3-butadiene ND mg/kg 03/03/22 12:19 87-68-3 v103/02/22 16:130.39 0.17 1
Hexachlorobenzene ND mg/kg 03/03/22 12:19 118-74-103/02/22 16:130.39 0.15 1
Hexachlorocyclopentadiene ND mg/kg 03/03/22 12:19 77-47-403/02/22 16:130.39 0.23 1
Hexachloroethane ND mg/kg 03/03/22 12:19 67-72-103/02/22 16:130.39 0.15 1
Indeno(1,2,3-cd)pyrene ND mg/kg 03/03/22 12:19 193-39-503/02/22 16:130.39 0.16 1
Isophorone ND mg/kg 03/03/22 12:19 78-59-103/02/22 16:130.39 0.18 1
1-Methylnaphthalene ND mg/kg 03/03/22 12:19 90-12-003/02/22 16:130.39 0.14 1
2-Methylnaphthalene ND mg/kg 03/03/22 12:19 91-57-603/02/22 16:130.39 0.16 1
2-Methylphenol(o-Cresol)ND mg/kg 03/03/22 12:19 95-48-703/02/22 16:130.39 0.16 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 03/03/22 12:19 15831-10-403/02/22 16:130.39 0.16 1
Naphthalene ND mg/kg 03/03/22 12:19 91-20-303/02/22 16:130.39 0.13 1
2-Nitroaniline ND mg/kg 03/03/22 12:19 88-74-403/02/22 16:132.0 0.32 1
3-Nitroaniline ND mg/kg 03/03/22 12:19 99-09-2 IL03/02/22 16:132.0 0.31 1
4-Nitroaniline ND mg/kg 03/03/22 12:19 100-01-603/02/22 16:130.79 0.30 1
Nitrobenzene ND mg/kg 03/03/22 12:19 98-95-303/02/22 16:130.39 0.18 1
2-Nitrophenol ND mg/kg 03/03/22 12:19 88-75-503/02/22 16:130.39 0.17 1
4-Nitrophenol ND mg/kg 03/03/22 12:19 100-02-703/02/22 16:132.0 0.76 1
N-Nitrosodimethylamine ND mg/kg 03/03/22 12:19 62-75-903/02/22 16:130.39 0.13 1
N-Nitroso-di-n-propylamine ND mg/kg 03/03/22 12:19 621-64-703/02/22 16:130.39 0.15 1
N-Nitrosodiphenylamine ND mg/kg 03/03/22 12:19 86-30-603/02/22 16:130.39 0.14 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 03/03/22 12:19 108-60-1 v103/02/22 16:130.39 0.19 1
Pentachlorophenol ND mg/kg 03/03/22 12:19 87-86-5 v203/02/22 16:130.79 0.39 1
Phenanthrene ND mg/kg 03/03/22 12:19 85-01-803/02/22 16:130.39 0.13 1
Phenol ND mg/kg 03/03/22 12:19 108-95-203/02/22 16:130.39 0.18 1
Pyrene ND mg/kg 03/03/22 12:19 129-00-003/02/22 16:130.39 0.16 1
Pyridine ND mg/kg 03/03/22 12:19 110-86-103/02/22 16:130.39 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 03/03/22 12:19 120-82-103/02/22 16:130.39 0.16 1
2,4,5-Trichlorophenol ND mg/kg 03/03/22 12:19 95-95-403/02/22 16:130.39 0.18 1
2,4,6-Trichlorophenol ND mg/kg 03/03/22 12:19 88-06-203/02/22 16:130.39 0.16 1
Surrogates
Nitrobenzene-d5 (S)49 %03/03/22 12:19 4165-60-003/02/22 16:1321-130 1
2-Fluorobiphenyl (S)45 %03/03/22 12:19 321-60-803/02/22 16:1319-130 1
Terphenyl-d14 (S)89 %03/03/22 12:19 1718-51-003/02/22 16:1315-130 1
Phenol-d6 (S)51 %03/03/22 12:19 13127-88-303/02/22 16:1318-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-3 Lab ID:92590340003 Collected:02/25/22 12:20 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)40 %03/03/22 12:19 367-12-403/02/22 16:1318-130 1
2,4,6-Tribromophenol (S)59 %03/03/22 12:19 118-79-603/02/22 16:1318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 03/01/22 02:01 67-64-102/25/22 21:030.15 0.047 1
Benzene ND mg/kg 03/01/22 02:01 71-43-202/25/22 21:030.0073 0.0029 1
Bromobenzene ND mg/kg 03/01/22 02:01 108-86-102/25/22 21:030.0073 0.0024 1
Bromochloromethane ND mg/kg 03/01/22 02:01 74-97-502/25/22 21:030.0073 0.0022 1
Bromodichloromethane ND mg/kg 03/01/22 02:01 75-27-402/25/22 21:030.0073 0.0028 1
Bromoform ND mg/kg 03/01/22 02:01 75-25-202/25/22 21:030.0073 0.0026 1
Bromomethane ND mg/kg 03/01/22 02:01 74-83-9 v202/25/22 21:030.015 0.012 1
2-Butanone (MEK)ND mg/kg 03/01/22 02:01 78-93-302/25/22 21:030.15 0.035 1
n-Butylbenzene ND mg/kg 03/01/22 02:01 104-51-802/25/22 21:030.0073 0.0034 1
sec-Butylbenzene ND mg/kg 03/01/22 02:01 135-98-802/25/22 21:030.0073 0.0032 1
tert-Butylbenzene ND mg/kg 03/01/22 02:01 98-06-602/25/22 21:030.0073 0.0026 1
Carbon tetrachloride ND mg/kg 03/01/22 02:01 56-23-502/25/22 21:030.0073 0.0027 1
Chlorobenzene ND mg/kg 03/01/22 02:01 108-90-702/25/22 21:030.0073 0.0014 1
Chloroethane ND mg/kg 03/01/22 02:01 75-00-302/25/22 21:030.015 0.0056 1
Chloroform ND mg/kg 03/01/22 02:01 67-66-302/25/22 21:030.0073 0.0044 1
Chloromethane ND mg/kg 03/01/22 02:01 74-87-302/25/22 21:030.015 0.0061 1
2-Chlorotoluene ND mg/kg 03/01/22 02:01 95-49-802/25/22 21:030.0073 0.0026 1
4-Chlorotoluene ND mg/kg 03/01/22 02:01 106-43-402/25/22 21:030.0073 0.0013 1
1,2-Dibromo-3-chloropropane ND mg/kg 03/01/22 02:01 96-12-802/25/22 21:030.0073 0.0028 1
Dibromochloromethane ND mg/kg 03/01/22 02:01 124-48-102/25/22 21:030.0073 0.0041 1
1,2-Dibromoethane (EDB)ND mg/kg 03/01/22 02:01 106-93-402/25/22 21:030.0073 0.0032 1
Dibromomethane ND mg/kg 03/01/22 02:01 74-95-302/25/22 21:030.0073 0.0016 1
1,2-Dichlorobenzene ND mg/kg 03/01/22 02:01 95-50-102/25/22 21:030.0073 0.0026 1
1,3-Dichlorobenzene ND mg/kg 03/01/22 02:01 541-73-102/25/22 21:030.0073 0.0023 1
1,4-Dichlorobenzene ND mg/kg 03/01/22 02:01 106-46-702/25/22 21:030.0073 0.0019 1
Dichlorodifluoromethane ND mg/kg 03/01/22 02:01 75-71-802/25/22 21:030.015 0.0032 1
1,1-Dichloroethane ND mg/kg 03/01/22 02:01 75-34-302/25/22 21:030.0073 0.0030 1
1,2-Dichloroethane ND mg/kg 03/01/22 02:01 107-06-202/25/22 21:030.0073 0.0048 1
1,1-Dichloroethene ND mg/kg 03/01/22 02:01 75-35-402/25/22 21:030.0073 0.0030 1
cis-1,2-Dichloroethene ND mg/kg 03/01/22 02:01 156-59-202/25/22 21:030.0073 0.0025 1
trans-1,2-Dichloroethene ND mg/kg 03/01/22 02:01 156-60-502/25/22 21:030.0073 0.0025 1
1,2-Dichloropropane ND mg/kg 03/01/22 02:01 78-87-502/25/22 21:030.0073 0.0022 1
1,3-Dichloropropane ND mg/kg 03/01/22 02:01 142-28-902/25/22 21:030.0073 0.0023 1
2,2-Dichloropropane ND mg/kg 03/01/22 02:01 594-20-702/25/22 21:030.0073 0.0024 1
1,1-Dichloropropene ND mg/kg 03/01/22 02:01 563-58-602/25/22 21:030.0073 0.0035 1
cis-1,3-Dichloropropene ND mg/kg 03/01/22 02:01 10061-01-502/25/22 21:030.0073 0.0020 1
trans-1,3-Dichloropropene ND mg/kg 03/01/22 02:01 10061-02-602/25/22 21:030.0073 0.0025 1
Diisopropyl ether ND mg/kg 03/01/22 02:01 108-20-302/25/22 21:030.0073 0.0020 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:SB-3 Lab ID:92590340003 Collected:02/25/22 12:20 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 03/01/22 02:01 100-41-402/25/22 21:030.0073 0.0034 1
Hexachloro-1,3-butadiene ND mg/kg 03/01/22 02:01 87-68-302/25/22 21:030.015 0.012 1
2-Hexanone ND mg/kg 03/01/22 02:01 591-78-602/25/22 21:030.073 0.0070 1
Isopropylbenzene (Cumene)ND mg/kg 03/01/22 02:01 98-82-802/25/22 21:030.0073 0.0025 1
p-Isopropyltoluene ND mg/kg 03/01/22 02:01 99-87-602/25/22 21:030.0073 0.0036 1
Methylene Chloride ND mg/kg 03/01/22 02:01 75-09-202/25/22 21:030.029 0.020 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 03/01/22 02:01 108-10-102/25/22 21:030.073 0.0070 1
Methyl-tert-butyl ether ND mg/kg 03/01/22 02:01 1634-04-402/25/22 21:030.0073 0.0027 1
Naphthalene ND mg/kg 03/01/22 02:01 91-20-302/25/22 21:030.0073 0.0038 1
n-Propylbenzene ND mg/kg 03/01/22 02:01 103-65-102/25/22 21:030.0073 0.0026 1
Styrene ND mg/kg 03/01/22 02:01 100-42-502/25/22 21:030.0073 0.0019 1
1,1,1,2-Tetrachloroethane ND mg/kg 03/01/22 02:01 630-20-602/25/22 21:030.0073 0.0028 1
1,1,2,2-Tetrachloroethane ND mg/kg 03/01/22 02:01 79-34-502/25/22 21:030.0073 0.0019 1
Tetrachloroethene ND mg/kg 03/01/22 02:01 127-18-402/25/22 21:030.0073 0.0023 1
Toluene ND mg/kg 03/01/22 02:01 108-88-302/25/22 21:030.0073 0.0021 1
1,2,3-Trichlorobenzene ND mg/kg 03/01/22 02:01 87-61-602/25/22 21:030.0073 0.0059 1
1,2,4-Trichlorobenzene ND mg/kg 03/01/22 02:01 120-82-102/25/22 21:030.0073 0.0061 1
1,1,1-Trichloroethane ND mg/kg 03/01/22 02:01 71-55-602/25/22 21:030.0073 0.0038 1
1,1,2-Trichloroethane ND mg/kg 03/01/22 02:01 79-00-502/25/22 21:030.0073 0.0024 1
Trichloroethene ND mg/kg 03/01/22 02:01 79-01-602/25/22 21:030.0073 0.0019 1
Trichlorofluoromethane ND mg/kg 03/01/22 02:01 75-69-402/25/22 21:030.0073 0.0040 1
1,2,3-Trichloropropane ND mg/kg 03/01/22 02:01 96-18-402/25/22 21:030.0073 0.0037 1
1,2,4-Trimethylbenzene ND mg/kg 03/01/22 02:01 95-63-602/25/22 21:030.0073 0.0020 1
1,3,5-Trimethylbenzene ND mg/kg 03/01/22 02:01 108-67-802/25/22 21:030.0073 0.0024 1
Vinyl acetate ND mg/kg 03/01/22 02:01 108-05-402/25/22 21:030.073 0.0053 1
Vinyl chloride ND mg/kg 03/01/22 02:01 75-01-402/25/22 21:030.015 0.0037 1
Xylene (Total)ND mg/kg 03/01/22 02:01 1330-20-702/25/22 21:030.015 0.0042 1
m&p-Xylene ND mg/kg 03/01/22 02:01 179601-23-102/25/22 21:030.015 0.0050 1
o-Xylene ND mg/kg 03/01/22 02:01 95-47-602/25/22 21:030.0073 0.0032 1
Surrogates
Toluene-d8 (S)99 %03/01/22 02:01 2037-26-502/25/22 21:0370-130 1
4-Bromofluorobenzene (S)97 %03/01/22 02:01 460-00-402/25/22 21:0369-134 1
1,2-Dichloroethane-d4 (S)94 %03/01/22 02:01 17060-07-002/25/22 21:0370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.7 %02/25/22 17:48 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:DUP-1 Lab ID:92590340004 Collected:02/25/22 00:00 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 03/03/22 20:20 7440-38-202/28/22 10:213.4 2.4 1
Barium 34.3 mg/kg 03/03/22 20:20 7440-39-302/28/22 10:211.1 0.30 1
Cadmium ND mg/kg 03/03/22 20:20 7440-43-902/28/22 10:211.1 0.34 1
Chromium 7.1 mg/kg 03/03/22 20:20 7440-47-302/28/22 10:211.1 1.0 1
Lead 12.7 mg/kg 03/03/22 20:20 7439-92-102/28/22 10:212.9 1.8 1
Selenium ND mg/kg 03/03/22 20:20 7782-49-202/28/22 10:214.6 4.3 1
Silver ND mg/kg 03/03/22 20:20 7440-22-402/28/22 10:211.1 0.47 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury 0.039J mg/kg 03/02/22 10:04 7439-97-603/01/22 14:300.26 0.012 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 03/03/22 12:46 83-32-903/02/22 16:130.38 0.13 1
Acenaphthylene ND mg/kg 03/03/22 12:46 208-96-803/02/22 16:130.38 0.13 1
Aniline ND mg/kg 03/03/22 12:46 62-53-303/02/22 16:130.38 0.15 1
Anthracene ND mg/kg 03/03/22 12:46 120-12-703/02/22 16:130.38 0.12 1
Benzo(a)anthracene ND mg/kg 03/03/22 12:46 56-55-303/02/22 16:130.38 0.13 1
Benzo(a)pyrene ND mg/kg 03/03/22 12:46 50-32-803/02/22 16:130.38 0.13 1
Benzo(b)fluoranthene ND mg/kg 03/03/22 12:46 205-99-203/02/22 16:130.38 0.13 1
Benzo(g,h,i)perylene ND mg/kg 03/03/22 12:46 191-24-203/02/22 16:130.38 0.15 1
Benzo(k)fluoranthene ND mg/kg 03/03/22 12:46 207-08-903/02/22 16:130.38 0.13 1
Benzoic Acid ND mg/kg 03/03/22 12:46 65-85-003/02/22 16:131.9 0.81 1
Benzyl alcohol ND mg/kg 03/03/22 12:46 100-51-603/02/22 16:130.75 0.29 1
4-Bromophenylphenyl ether ND mg/kg 03/03/22 12:46 101-55-303/02/22 16:130.38 0.15 1
Butylbenzylphthalate ND mg/kg 03/03/22 12:46 85-68-703/02/22 16:130.38 0.16 1
4-Chloro-3-methylphenol ND mg/kg 03/03/22 12:46 59-50-703/02/22 16:130.75 0.27 1
4-Chloroaniline ND mg/kg 03/03/22 12:46 106-47-8 IL03/02/22 16:130.75 0.30 1
bis(2-Chloroethoxy)methane ND mg/kg 03/03/22 12:46 111-91-103/02/22 16:130.38 0.16 1
bis(2-Chloroethyl) ether ND mg/kg 03/03/22 12:46 111-44-403/02/22 16:130.38 0.14 1
2-Chloronaphthalene ND mg/kg 03/03/22 12:46 91-58-703/02/22 16:130.38 0.15 1
2-Chlorophenol ND mg/kg 03/03/22 12:46 95-57-803/02/22 16:130.38 0.14 1
4-Chlorophenylphenyl ether ND mg/kg 03/03/22 12:46 7005-72-303/02/22 16:130.38 0.14 1
Chrysene ND mg/kg 03/03/22 12:46 218-01-903/02/22 16:130.38 0.14 1
Dibenz(a,h)anthracene ND mg/kg 03/03/22 12:46 53-70-303/02/22 16:130.38 0.15 1
Dibenzofuran ND mg/kg 03/03/22 12:46 132-64-903/02/22 16:130.38 0.14 1
1,2-Dichlorobenzene ND mg/kg 03/03/22 12:46 95-50-103/02/22 16:130.38 0.14 1
1,3-Dichlorobenzene ND mg/kg 03/03/22 12:46 541-73-103/02/22 16:130.38 0.13 1
1,4-Dichlorobenzene ND mg/kg 03/03/22 12:46 106-46-703/02/22 16:130.38 0.14 1
3,3'-Dichlorobenzidine ND mg/kg 03/03/22 12:46 91-94-1 IL03/02/22 16:130.75 0.25 1
2,4-Dichlorophenol ND mg/kg 03/03/22 12:46 120-83-203/02/22 16:130.38 0.15 1
Diethylphthalate ND mg/kg 03/03/22 12:46 84-66-203/02/22 16:130.38 0.14 1
2,4-Dimethylphenol ND mg/kg 03/03/22 12:46 105-67-903/02/22 16:130.38 0.16 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:DUP-1 Lab ID:92590340004 Collected:02/25/22 00:00 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 03/03/22 12:46 131-11-303/02/22 16:130.38 0.14 1
Di-n-butylphthalate ND mg/kg 03/03/22 12:46 84-74-203/02/22 16:130.38 0.13 1
4,6-Dinitro-2-methylphenol ND mg/kg 03/03/22 12:46 534-52-103/02/22 16:130.75 0.35 1
2,4-Dinitrophenol ND mg/kg 03/03/22 12:46 51-28-503/02/22 16:131.9 1.2 1
2,4-Dinitrotoluene ND mg/kg 03/03/22 12:46 121-14-203/02/22 16:130.38 0.15 1
2,6-Dinitrotoluene ND mg/kg 03/03/22 12:46 606-20-203/02/22 16:130.38 0.14 1
Di-n-octylphthalate ND mg/kg 03/03/22 12:46 117-84-003/02/22 16:130.38 0.15 1
bis(2-Ethylhexyl)phthalate ND mg/kg 03/03/22 12:46 117-81-703/02/22 16:130.38 0.15 1
Fluoranthene ND mg/kg 03/03/22 12:46 206-44-003/02/22 16:130.38 0.13 1
Fluorene ND mg/kg 03/03/22 12:46 86-73-703/02/22 16:130.38 0.13 1
Hexachloro-1,3-butadiene ND mg/kg 03/03/22 12:46 87-68-3 v103/02/22 16:130.38 0.16 1
Hexachlorobenzene ND mg/kg 03/03/22 12:46 118-74-103/02/22 16:130.38 0.15 1
Hexachlorocyclopentadiene ND mg/kg 03/03/22 12:46 77-47-403/02/22 16:130.38 0.22 1
Hexachloroethane ND mg/kg 03/03/22 12:46 67-72-103/02/22 16:130.38 0.14 1
Indeno(1,2,3-cd)pyrene ND mg/kg 03/03/22 12:46 193-39-503/02/22 16:130.38 0.15 1
Isophorone ND mg/kg 03/03/22 12:46 78-59-103/02/22 16:130.38 0.17 1
1-Methylnaphthalene ND mg/kg 03/03/22 12:46 90-12-003/02/22 16:130.38 0.13 1
2-Methylnaphthalene ND mg/kg 03/03/22 12:46 91-57-603/02/22 16:130.38 0.15 1
2-Methylphenol(o-Cresol)ND mg/kg 03/03/22 12:46 95-48-703/02/22 16:130.38 0.15 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 03/03/22 12:46 15831-10-403/02/22 16:130.38 0.15 1
Naphthalene ND mg/kg 03/03/22 12:46 91-20-303/02/22 16:130.38 0.13 1
2-Nitroaniline ND mg/kg 03/03/22 12:46 88-74-403/02/22 16:131.9 0.31 1
3-Nitroaniline ND mg/kg 03/03/22 12:46 99-09-2 IL03/02/22 16:131.9 0.30 1
4-Nitroaniline ND mg/kg 03/03/22 12:46 100-01-603/02/22 16:130.75 0.29 1
Nitrobenzene ND mg/kg 03/03/22 12:46 98-95-303/02/22 16:130.38 0.17 1
2-Nitrophenol ND mg/kg 03/03/22 12:46 88-75-503/02/22 16:130.38 0.16 1
4-Nitrophenol ND mg/kg 03/03/22 12:46 100-02-703/02/22 16:131.9 0.73 1
N-Nitrosodimethylamine ND mg/kg 03/03/22 12:46 62-75-903/02/22 16:130.38 0.13 1
N-Nitroso-di-n-propylamine ND mg/kg 03/03/22 12:46 621-64-703/02/22 16:130.38 0.14 1
N-Nitrosodiphenylamine ND mg/kg 03/03/22 12:46 86-30-603/02/22 16:130.38 0.13 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 03/03/22 12:46 108-60-1 v103/02/22 16:130.38 0.18 1
Pentachlorophenol ND mg/kg 03/03/22 12:46 87-86-5 v203/02/22 16:130.75 0.37 1
Phenanthrene ND mg/kg 03/03/22 12:46 85-01-803/02/22 16:130.38 0.12 1
Phenol ND mg/kg 03/03/22 12:46 108-95-203/02/22 16:130.38 0.17 1
Pyrene ND mg/kg 03/03/22 12:46 129-00-003/02/22 16:130.38 0.15 1
Pyridine ND mg/kg 03/03/22 12:46 110-86-103/02/22 16:130.38 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 03/03/22 12:46 120-82-103/02/22 16:130.38 0.15 1
2,4,5-Trichlorophenol ND mg/kg 03/03/22 12:46 95-95-403/02/22 16:130.38 0.17 1
2,4,6-Trichlorophenol ND mg/kg 03/03/22 12:46 88-06-203/02/22 16:130.38 0.16 1
Surrogates
Nitrobenzene-d5 (S)63 %03/03/22 12:46 4165-60-003/02/22 16:1321-130 1
2-Fluorobiphenyl (S)51 %03/03/22 12:46 321-60-803/02/22 16:1319-130 1
Terphenyl-d14 (S)86 %03/03/22 12:46 1718-51-003/02/22 16:1315-130 1
Phenol-d6 (S)53 %03/03/22 12:46 13127-88-303/02/22 16:1318-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:DUP-1 Lab ID:92590340004 Collected:02/25/22 00:00 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)47 %03/03/22 12:46 367-12-403/02/22 16:1318-130 1
2,4,6-Tribromophenol (S)60 %03/03/22 12:46 118-79-603/02/22 16:1318-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 03/01/22 02:19 67-64-102/25/22 21:030.11 0.036 1
Benzene ND mg/kg 03/01/22 02:19 71-43-202/25/22 21:030.0056 0.0022 1
Bromobenzene ND mg/kg 03/01/22 02:19 108-86-102/25/22 21:030.0056 0.0018 1
Bromochloromethane ND mg/kg 03/01/22 02:19 74-97-502/25/22 21:030.0056 0.0017 1
Bromodichloromethane ND mg/kg 03/01/22 02:19 75-27-402/25/22 21:030.0056 0.0022 1
Bromoform ND mg/kg 03/01/22 02:19 75-25-202/25/22 21:030.0056 0.0020 1
Bromomethane ND mg/kg 03/01/22 02:19 74-83-9 v202/25/22 21:030.011 0.0089 1
2-Butanone (MEK)ND mg/kg 03/01/22 02:19 78-93-302/25/22 21:030.11 0.027 1
n-Butylbenzene ND mg/kg 03/01/22 02:19 104-51-802/25/22 21:030.0056 0.0027 1
sec-Butylbenzene ND mg/kg 03/01/22 02:19 135-98-802/25/22 21:030.0056 0.0025 1
tert-Butylbenzene ND mg/kg 03/01/22 02:19 98-06-602/25/22 21:030.0056 0.0020 1
Carbon tetrachloride ND mg/kg 03/01/22 02:19 56-23-502/25/22 21:030.0056 0.0021 1
Chlorobenzene ND mg/kg 03/01/22 02:19 108-90-702/25/22 21:030.0056 0.0011 1
Chloroethane ND mg/kg 03/01/22 02:19 75-00-302/25/22 21:030.011 0.0043 1
Chloroform ND mg/kg 03/01/22 02:19 67-66-302/25/22 21:030.0056 0.0034 1
Chloromethane ND mg/kg 03/01/22 02:19 74-87-302/25/22 21:030.011 0.0047 1
2-Chlorotoluene ND mg/kg 03/01/22 02:19 95-49-802/25/22 21:030.0056 0.0020 1
4-Chlorotoluene ND mg/kg 03/01/22 02:19 106-43-402/25/22 21:030.0056 0.0010 1
1,2-Dibromo-3-chloropropane ND mg/kg 03/01/22 02:19 96-12-802/25/22 21:030.0056 0.0022 1
Dibromochloromethane ND mg/kg 03/01/22 02:19 124-48-102/25/22 21:030.0056 0.0032 1
1,2-Dibromoethane (EDB)ND mg/kg 03/01/22 02:19 106-93-402/25/22 21:030.0056 0.0025 1
Dibromomethane ND mg/kg 03/01/22 02:19 74-95-302/25/22 21:030.0056 0.0012 1
1,2-Dichlorobenzene ND mg/kg 03/01/22 02:19 95-50-102/25/22 21:030.0056 0.0020 1
1,3-Dichlorobenzene ND mg/kg 03/01/22 02:19 541-73-102/25/22 21:030.0056 0.0017 1
1,4-Dichlorobenzene ND mg/kg 03/01/22 02:19 106-46-702/25/22 21:030.0056 0.0015 1
Dichlorodifluoromethane ND mg/kg 03/01/22 02:19 75-71-802/25/22 21:030.011 0.0024 1
1,1-Dichloroethane ND mg/kg 03/01/22 02:19 75-34-302/25/22 21:030.0056 0.0023 1
1,2-Dichloroethane ND mg/kg 03/01/22 02:19 107-06-202/25/22 21:030.0056 0.0037 1
1,1-Dichloroethene ND mg/kg 03/01/22 02:19 75-35-402/25/22 21:030.0056 0.0023 1
cis-1,2-Dichloroethene ND mg/kg 03/01/22 02:19 156-59-202/25/22 21:030.0056 0.0019 1
trans-1,2-Dichloroethene ND mg/kg 03/01/22 02:19 156-60-502/25/22 21:030.0056 0.0020 1
1,2-Dichloropropane ND mg/kg 03/01/22 02:19 78-87-502/25/22 21:030.0056 0.0017 1
1,3-Dichloropropane ND mg/kg 03/01/22 02:19 142-28-902/25/22 21:030.0056 0.0018 1
2,2-Dichloropropane ND mg/kg 03/01/22 02:19 594-20-702/25/22 21:030.0056 0.0018 1
1,1-Dichloropropene ND mg/kg 03/01/22 02:19 563-58-602/25/22 21:030.0056 0.0027 1
cis-1,3-Dichloropropene ND mg/kg 03/01/22 02:19 10061-01-502/25/22 21:030.0056 0.0015 1
trans-1,3-Dichloropropene ND mg/kg 03/01/22 02:19 10061-02-602/25/22 21:030.0056 0.0019 1
Diisopropyl ether ND mg/kg 03/01/22 02:19 108-20-302/25/22 21:030.0056 0.0015 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 60
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590340
Monroe Road Project
Sample:DUP-1 Lab ID:92590340004 Collected:02/25/22 00:00 Received:02/25/22 14:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 03/01/22 02:19 100-41-402/25/22 21:030.0056 0.0026 1
Hexachloro-1,3-butadiene ND mg/kg 03/01/22 02:19 87-68-302/25/22 21:030.011 0.0092 1
2-Hexanone ND mg/kg 03/01/22 02:19 591-78-602/25/22 21:030.056 0.0054 1
Isopropylbenzene (Cumene)ND mg/kg 03/01/22 02:19 98-82-802/25/22 21:030.0056 0.0019 1
p-Isopropyltoluene ND mg/kg 03/01/22 02:19 99-87-602/25/22 21:030.0056 0.0028 1
Methylene Chloride ND mg/kg 03/01/22 02:19 75-09-202/25/22 21:030.023 0.015 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 03/01/22 02:19 108-10-102/25/22 21:030.056 0.0054 1
Methyl-tert-butyl ether ND mg/kg 03/01/22 02:19 1634-04-402/25/22 21:030.0056 0.0021 1
Naphthalene ND mg/kg 03/01/22 02:19 91-20-302/25/22 21:030.0056 0.0030 1
n-Propylbenzene ND mg/kg 03/01/22 02:19 103-65-102/25/22 21:030.0056 0.0020 1
Styrene ND mg/kg 03/01/22 02:19 100-42-502/25/22 21:030.0056 0.0015 1
1,1,1,2-Tetrachloroethane ND mg/kg 03/01/22 02:19 630-20-602/25/22 21:030.0056 0.0022 1
1,1,2,2-Tetrachloroethane ND mg/kg 03/01/22 02:19 79-34-502/25/22 21:030.0056 0.0015 1
Tetrachloroethene ND mg/kg 03/01/22 02:19 127-18-402/25/22 21:030.0056 0.0018 1
Toluene ND mg/kg 03/01/22 02:19 108-88-302/25/22 21:030.0056 0.0016 1
1,2,3-Trichlorobenzene ND mg/kg 03/01/22 02:19 87-61-602/25/22 21:030.0056 0.0045 1
1,2,4-Trichlorobenzene ND mg/kg 03/01/22 02:19 120-82-102/25/22 21:030.0056 0.0047 1
1,1,1-Trichloroethane ND mg/kg 03/01/22 02:19 71-55-602/25/22 21:030.0056 0.0029 1
1,1,2-Trichloroethane ND mg/kg 03/01/22 02:19 79-00-502/25/22 21:030.0056 0.0019 1
Trichloroethene ND mg/kg 03/01/22 02:19 79-01-602/25/22 21:030.0056 0.0015 1
Trichlorofluoromethane ND mg/kg 03/01/22 02:19 75-69-402/25/22 21:030.0056 0.0031 1
1,2,3-Trichloropropane ND mg/kg 03/01/22 02:19 96-18-402/25/22 21:030.0056 0.0028 1
1,2,4-Trimethylbenzene ND mg/kg 03/01/22 02:19 95-63-602/25/22 21:030.0056 0.0015 1
1,3,5-Trimethylbenzene ND mg/kg 03/01/22 02:19 108-67-802/25/22 21:030.0056 0.0019 1
Vinyl acetate ND mg/kg 03/01/22 02:19 108-05-402/25/22 21:030.056 0.0041 1
Vinyl chloride ND mg/kg 03/01/22 02:19 75-01-402/25/22 21:030.011 0.0029 1
Xylene (Total)ND mg/kg 03/01/22 02:19 1330-20-702/25/22 21:030.011 0.0032 1
m&p-Xylene ND mg/kg 03/01/22 02:19 179601-23-102/25/22 21:030.011 0.0038 1
o-Xylene ND mg/kg 03/01/22 02:19 95-47-602/25/22 21:030.0056 0.0025 1
Surrogates
Toluene-d8 (S)99 %03/01/22 02:19 2037-26-502/25/22 21:0370-130 1
4-Bromofluorobenzene (S)98 %03/01/22 02:19 460-00-402/25/22 21:0369-134 1
1,2-Dichloroethane-d4 (S)91 %03/01/22 02:19 17060-07-002/25/22 21:0370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.5 %02/25/22 17:48 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
681269
EPA 3050B
EPA 6010D
6010D ATL
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3564068
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 3.0 03/03/22 14:292.1
Barium mg/kg ND 1.0 03/03/22 14:290.27
Cadmium mg/kg ND 1.0 03/03/22 14:290.30
Chromium mg/kg ND 1.0 03/03/22 14:290.91
Lead mg/kg ND 2.5 03/03/22 14:291.6
Selenium mg/kg ND 4.0 03/03/22 14:293.7
Silver mg/kg ND 1.0 03/03/22 14:290.41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3564069LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 99.2100 99 80-120
Barium mg/kg 104100 104 80-120
Cadmium mg/kg 98.1100 98 80-120
Chromium mg/kg 106100 106 80-120
Lead mg/kg 102100 102 80-120
Selenium mg/kg 96.7100 97 80-120
Silver mg/kg 96.3100 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3564070MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92589911002
3564071
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 125 92 75-12593 1 201252.8J 118 119
Barium mg/kg 125 99 75-125108 7 2012543.7 168 179
Cadmium mg/kg 125 96 75-12598 2 20125ND120122
Chromium mg/kg 125 101 75-125101 0 201259.5 136 135
Lead mg/kg 125 95 75-125110 12 2012527.8 147 166
Selenium mg/kg 125 92 75-12592 0 20125ND115115
Silver mg/kg 125 95 75-12597 2 20125ND118121
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
681614
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3565556
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.24 03/02/22 09:250.012
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3565557LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.380.33 115 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3565558MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92589911001
3565559
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.45 117 75-125119 4 200.430.043J 0.58 0.55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
681117
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3563560
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 02/28/22 23:310.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 02/28/22 23:310.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 02/28/22 23:310.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 02/28/22 23:310.0017
1,1-Dichloroethane mg/kg ND 0.0050 02/28/22 23:310.0021
1,1-Dichloroethene mg/kg ND 0.0050 02/28/22 23:310.0021
1,1-Dichloropropene mg/kg ND 0.0050 02/28/22 23:310.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 02/28/22 23:310.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 02/28/22 23:310.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 02/28/22 23:310.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 02/28/22 23:310.0014
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 02/28/22 23:310.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 02/28/22 23:310.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 02/28/22 23:310.0018
1,2-Dichloroethane mg/kg ND 0.0050 02/28/22 23:310.0033
1,2-Dichloropropane mg/kg ND 0.0050 02/28/22 23:310.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 02/28/22 23:310.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 02/28/22 23:310.0016
1,3-Dichloropropane mg/kg ND 0.0050 02/28/22 23:310.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 02/28/22 23:310.0013
2,2-Dichloropropane mg/kg ND 0.0050 02/28/22 23:310.0016
2-Butanone (MEK)mg/kg ND 0.10 02/28/22 23:310.024
2-Chlorotoluene mg/kg ND 0.0050 02/28/22 23:310.0018
2-Hexanone mg/kg ND 0.050 02/28/22 23:310.0048
4-Chlorotoluene mg/kg ND 0.0050 02/28/22 23:310.00088
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 02/28/22 23:310.0048
Acetone mg/kg ND 0.10 02/28/22 23:310.032
Benzene mg/kg ND 0.0050 02/28/22 23:310.0020
Bromobenzene mg/kg ND 0.0050 02/28/22 23:310.0016
Bromochloromethane mg/kg ND 0.0050 02/28/22 23:310.0015
Bromodichloromethane mg/kg ND 0.0050 02/28/22 23:310.0019
Bromoform mg/kg ND 0.0050 02/28/22 23:310.0018
Bromomethane mg/kg ND 0.010 v202/28/22 23:310.0079
Carbon tetrachloride mg/kg ND 0.0050 02/28/22 23:310.0019
Chlorobenzene mg/kg ND 0.0050 02/28/22 23:310.00096
Chloroethane mg/kg ND 0.010 02/28/22 23:310.0039
Chloroform mg/kg ND 0.0050 02/28/22 23:310.0030
Chloromethane mg/kg ND 0.010 02/28/22 23:310.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 02/28/22 23:310.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 02/28/22 23:310.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3563560
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 02/28/22 23:310.0028
Dibromomethane mg/kg ND 0.0050 02/28/22 23:310.0011
Dichlorodifluoromethane mg/kg ND 0.010 02/28/22 23:310.0022
Diisopropyl ether mg/kg ND 0.0050 02/28/22 23:310.0014
Ethylbenzene mg/kg ND 0.0050 02/28/22 23:310.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 02/28/22 23:310.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 02/28/22 23:310.0017
m&p-Xylene mg/kg ND 0.010 02/28/22 23:310.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 02/28/22 23:310.0019
Methylene Chloride mg/kg ND 0.020 02/28/22 23:310.014
n-Butylbenzene mg/kg ND 0.0050 02/28/22 23:310.0024
n-Propylbenzene mg/kg ND 0.0050 02/28/22 23:310.0018
Naphthalene mg/kg ND 0.0050 02/28/22 23:310.0026
o-Xylene mg/kg ND 0.0050 02/28/22 23:310.0022
p-Isopropyltoluene mg/kg ND 0.0050 02/28/22 23:310.0025
sec-Butylbenzene mg/kg ND 0.0050 02/28/22 23:310.0022
Styrene mg/kg ND 0.0050 02/28/22 23:310.0013
tert-Butylbenzene mg/kg ND 0.0050 02/28/22 23:310.0018
Tetrachloroethene mg/kg ND 0.0050 02/28/22 23:310.0016
Toluene mg/kg ND 0.0050 02/28/22 23:310.0014
trans-1,2-Dichloroethene mg/kg ND 0.0050 02/28/22 23:310.0018
trans-1,3-Dichloropropene mg/kg ND 0.0050 02/28/22 23:310.0017
Trichloroethene mg/kg ND 0.0050 02/28/22 23:310.0013
Trichlorofluoromethane mg/kg ND 0.0050 02/28/22 23:310.0028
Vinyl acetate mg/kg ND 0.050 02/28/22 23:310.0036
Vinyl chloride mg/kg ND 0.010 02/28/22 23:310.0025
Xylene (Total)mg/kg ND 0.010 02/28/22 23:310.0028
1,2-Dichloroethane-d4 (S)%95 70-130 02/28/22 23:31
4-Bromofluorobenzene (S)%97 69-134 02/28/22 23:31
Toluene-d8 (S)%98 70-130 02/28/22 23:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3563561LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.21.2 95 70-130
1,1,1-Trichloroethane mg/kg 1.11.2 89 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.11.2 91 70-130
1,1,2-Trichloroethane mg/kg 1.21.2 95 70-130
1,1-Dichloroethane mg/kg 1.11.2 87 70-130
1,1-Dichloroethene mg/kg 1.01.2 84 70-130
1,1-Dichloropropene mg/kg 1.11.2 90 70-130
1,2,3-Trichlorobenzene mg/kg 1.21.2 98 65-130
1,2,3-Trichloropropane mg/kg 1.11.2 89 70-130
1,2,4-Trichlorobenzene mg/kg 1.21.2 97 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3563561LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.11.2 91 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.11.2 91 70-130
1,2-Dibromoethane (EDB)mg/kg 1.11.2 89 70-130
1,2-Dichlorobenzene mg/kg 1.11.2 92 70-130
1,2-Dichloroethane mg/kg 1.01.2 80 63-130
1,2-Dichloropropane mg/kg 1.11.2 91 70-130
1,3,5-Trimethylbenzene mg/kg 1.21.2 93 70-130
1,3-Dichlorobenzene mg/kg 1.11.2 92 70-130
1,3-Dichloropropane mg/kg 1.11.2 85 70-130
1,4-Dichlorobenzene mg/kg 1.11.2 88 70-130
2,2-Dichloropropane mg/kg 1.11.2 84 66-130
2-Butanone (MEK)mg/kg 2.22.5 87 70-130
2-Chlorotoluene mg/kg 1.11.2 89 70-130
2-Hexanone mg/kg 2.32.5 92 70-130
4-Chlorotoluene mg/kg 1.11.2 87 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.42.5 95 70-130
Acetone mg/kg 2.12.5 83 69-130
Benzene mg/kg 1.11.2 87 70-130
Bromobenzene mg/kg 1.21.2 95 70-130
Bromochloromethane mg/kg 1.31.2 100 70-130
Bromodichloromethane mg/kg 1.21.2 92 69-130
Bromoform mg/kg 1.31.2 105 70-130
Bromomethane mg/kg 1.1 v31.2 84 52-130
Carbon tetrachloride mg/kg 1.21.2 92 70-130
Chlorobenzene mg/kg 1.11.2 89 70-130
Chloroethane mg/kg 1.21.2 94 65-130
Chloroform mg/kg 1.11.2 89 70-130
Chloromethane mg/kg 0.991.2 79 55-130
cis-1,2-Dichloroethene mg/kg 1.11.2 88 70-130
cis-1,3-Dichloropropene mg/kg 1.21.2 93 70-130
Dibromochloromethane mg/kg 1.11.2 90 70-130
Dibromomethane mg/kg 1.21.2 100 70-130
Dichlorodifluoromethane mg/kg 0.991.2 79 45-156
Diisopropyl ether mg/kg 1.11.2 84 70-130
Ethylbenzene mg/kg 1.01.2 84 70-130
Hexachloro-1,3-butadiene mg/kg 1.31.2 102 66-130
Isopropylbenzene (Cumene)mg/kg 1.21.2 95 70-130
m&p-Xylene mg/kg 2.22.5 89 70-130
Methyl-tert-butyl ether mg/kg 1.11.2 88 70-130
Methylene Chloride mg/kg 1.01.2 83 65-130
n-Butylbenzene mg/kg 1.11.2 90 67-130
n-Propylbenzene mg/kg 1.11.2 90 70-130
Naphthalene mg/kg 1.21.2 95 70-130
o-Xylene mg/kg 1.21.2 93 70-130
p-Isopropyltoluene mg/kg 1.21.2 94 67-130
sec-Butylbenzene mg/kg 1.11.2 91 69-130
Styrene mg/kg 1.21.2 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3563561LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.21.2 92 67-130
Tetrachloroethene mg/kg 1.11.2 88 70-130
Toluene mg/kg 1.11.2 89 70-130
trans-1,2-Dichloroethene mg/kg 1.11.2 87 70-130
trans-1,3-Dichloropropene mg/kg 1.21.2 93 68-130
Trichloroethene mg/kg 1.11.2 90 70-130
Trichlorofluoromethane mg/kg 1.01.2 82 70-130
Vinyl acetate mg/kg 2.42.5 95 70-130
Vinyl chloride mg/kg 1.11.2 84 61-130
Xylene (Total)mg/kg 3.43.8 90 70-130
1,2-Dichloroethane-d4 (S)%83 70-130
4-Bromofluorobenzene (S)%96 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3563562MATRIX SPIKE SAMPLE:
MSSpike
Result
92590319005
1,1,1,2-Tetrachloroethane mg/kg 1.21.2 101 70-131ND
1,1,1-Trichloroethane mg/kg 1.01.2 91 65-133ND
1,1,2,2-Tetrachloroethane mg/kg 1.01.2 91 66-130ND
1,1,2-Trichloroethane mg/kg 1.11.2 95 66-133ND
1,1-Dichloroethane mg/kg 1.01.2 88 65-130ND
1,1-Dichloroethene mg/kg 0.951.2 83 10-158ND
1,1-Dichloropropene mg/kg 1.01.2 89 68-133ND
1,2,3-Trichlorobenzene mg/kg 1.01.2 87 27-138ND
1,2,3-Trichloropropane mg/kg 0.931.2 81 67-130ND
1,2,4-Trichlorobenzene mg/kg 1.01.2 91 51-134ND
1,2,4-Trimethylbenzene mg/kg 1.01.2 89 63-136ND
1,2-Dibromo-3-chloropropane mg/kg 0.951.2 82 32-130ND
1,2-Dibromoethane (EDB)mg/kg 1.11.2 92 70-130ND
1,2-Dichlorobenzene mg/kg 1.11.2 94 69-130ND
1,2-Dichloroethane mg/kg 0.961.2 83 59-130ND
1,2-Dichloropropane mg/kg 1.11.2 96 70-130ND
1,3,5-Trimethylbenzene mg/kg 1.11.2 91 65-137ND
1,3-Dichlorobenzene mg/kg 1.01.2 89 70-130ND
1,3-Dichloropropane mg/kg 1.01.2 91 70-130ND
1,4-Dichlorobenzene mg/kg 1.01.2 90 68-130ND
2,2-Dichloropropane mg/kg 0.501.2 44 32-130ND
2-Butanone (MEK)mg/kg 1.82.3 77 10-136ND
2-Chlorotoluene mg/kg 1.01.2 89 69-141ND
2-Hexanone mg/kg 1.92.3 84 10-144ND
4-Chlorotoluene mg/kg 0.991.2 86 70-132ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.92.3 85 25-143ND
Acetone mg/kg 1.62.3 66 10-130111J ug/kg
Benzene mg/kg 1.11.2 93 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3563562MATRIX SPIKE SAMPLE:
MSSpike
Result
92590319005
Bromobenzene mg/kg 1.11.2 97 70-130ND
Bromochloromethane mg/kg 1.11.2 94 69-134ND
Bromodichloromethane mg/kg 1.01.2 91 64-130ND
Bromoform mg/kg 1.11.2 95 62-130ND
Bromomethane mg/kg 0.84 v31.2 73 20-176ND
Carbon tetrachloride mg/kg 1.11.2 97 65-140ND
Chlorobenzene mg/kg 1.11.2 97 70-130ND
Chloroethane mg/kg 0.511.2 44 10-130ND
Chloroform mg/kg 1.01.2 91 63-130ND
Chloromethane mg/kg 1.11.2 93 58-130ND
cis-1,2-Dichloroethene mg/kg 1.11.2 92 66-130ND
cis-1,3-Dichloropropene mg/kg 0.941.2 82 67-130ND
Dibromochloromethane mg/kg 1.01.2 88 67-130ND
Dibromomethane mg/kg 1.21.2 102 63-131ND
Dichlorodifluoromethane mg/kg 0.991.2 86 44-180ND
Diisopropyl ether mg/kg 0.971.2 84 63-130ND
Ethylbenzene mg/kg 1.01.2 90 66-130ND
Hexachloro-1,3-butadiene mg/kg 0.971.2 84 64-150ND
Isopropylbenzene (Cumene)mg/kg 1.21.2 101 69-135ND
m&p-Xylene mg/kg 2.22.3 94 60-133ND
Methyl-tert-butyl ether mg/kg 0.981.2 85 65-130ND
Methylene Chloride mg/kg 0.951.2 82 61-130ND
n-Butylbenzene mg/kg 0.891.2 77 65-140ND
n-Propylbenzene mg/kg 1.01.2 87 67-140ND
Naphthalene mg/kg 1.01.2 90 15-145ND
o-Xylene mg/kg 1.11.2 98 66-133ND
p-Isopropyltoluene mg/kg 1.01.2 88 56-147ND
sec-Butylbenzene mg/kg 1.01.2 89 65-139ND
Styrene mg/kg 1.21.2 100 70-132ND
tert-Butylbenzene mg/kg 1.11.2 94 62-135ND
Tetrachloroethene mg/kg 1.01.2 87 70-135ND
Toluene mg/kg 1.11.2 94 67-130ND
trans-1,2-Dichloroethene mg/kg 0.951.2 82 69-130ND
trans-1,3-Dichloropropene mg/kg 0.911.2 79 62-130ND
Trichloroethene mg/kg 1.11.2 95 70-135ND
Trichlorofluoromethane mg/kg 0.541.2 47 10-130ND
Vinyl acetate mg/kg 1.82.3 78 53-130ND
Vinyl chloride mg/kg 1.01.2 88 61-148ND
Xylene (Total)mg/kg 3.33.4 95 63-132ND
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%97 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92590319006
3563563SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND v230ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92590319006
3563563SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9492
4-Bromofluorobenzene (S)%9697
Toluene-d8 (S)%9998
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
681992
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3567276
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 03/03/22 08:140.13
1,2-Dichlorobenzene mg/kg ND 0.33 03/03/22 08:140.12
1,3-Dichlorobenzene mg/kg ND 0.33 03/03/22 08:140.12
1,4-Dichlorobenzene mg/kg ND 0.33 03/03/22 08:140.13
1-Methylnaphthalene mg/kg ND 0.33 03/03/22 08:140.12
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 03/03/22 08:140.16
2,4,5-Trichlorophenol mg/kg ND 0.33 03/03/22 08:140.15
2,4,6-Trichlorophenol mg/kg ND 0.33 03/03/22 08:140.14
2,4-Dichlorophenol mg/kg ND 0.33 03/03/22 08:140.13
2,4-Dimethylphenol mg/kg ND 0.33 03/03/22 08:140.14
2,4-Dinitrophenol mg/kg ND 1.6 03/03/22 08:141.0
2,4-Dinitrotoluene mg/kg ND 0.33 03/03/22 08:140.13
2,6-Dinitrotoluene mg/kg ND 0.33 03/03/22 08:140.12
2-Chloronaphthalene mg/kg ND 0.33 03/03/22 08:140.13
2-Chlorophenol mg/kg ND 0.33 03/03/22 08:140.12
2-Methylnaphthalene mg/kg ND 0.33 03/03/22 08:140.13
2-Methylphenol(o-Cresol)mg/kg ND 0.33 03/03/22 08:140.13
2-Nitroaniline mg/kg ND 1.6 03/03/22 08:140.27
2-Nitrophenol mg/kg ND 0.33 03/03/22 08:140.14
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 03/03/22 08:140.13
3,3'-Dichlorobenzidine mg/kg ND 0.66 IL03/03/22 08:140.22
3-Nitroaniline mg/kg ND 1.6 03/03/22 08:140.26
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 03/03/22 08:140.31
4-Bromophenylphenyl ether mg/kg ND 0.33 03/03/22 08:140.13
4-Chloro-3-methylphenol mg/kg ND 0.66 03/03/22 08:140.23
4-Chloroaniline mg/kg ND 0.66 03/03/22 08:140.26
4-Chlorophenylphenyl ether mg/kg ND 0.33 03/03/22 08:140.12
4-Nitroaniline mg/kg ND 0.66 03/03/22 08:140.25
4-Nitrophenol mg/kg ND 1.6 03/03/22 08:140.64
Acenaphthene mg/kg ND 0.33 03/03/22 08:140.12
Acenaphthylene mg/kg ND 0.33 03/03/22 08:140.12
Aniline mg/kg ND 0.33 03/03/22 08:140.13
Anthracene mg/kg ND 0.33 03/03/22 08:140.11
Benzo(a)anthracene mg/kg ND 0.33 03/03/22 08:140.11
Benzo(a)pyrene mg/kg ND 0.33 03/03/22 08:140.11
Benzo(b)fluoranthene mg/kg ND 0.33 03/03/22 08:140.11
Benzo(g,h,i)perylene mg/kg ND 0.33 03/03/22 08:140.13
Benzo(k)fluoranthene mg/kg ND 0.33 03/03/22 08:140.12
Benzoic Acid mg/kg ND 1.6 03/03/22 08:140.71
Benzyl alcohol mg/kg ND 0.66 03/03/22 08:140.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3567276
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane mg/kg ND 0.33 03/03/22 08:140.14
bis(2-Chloroethyl) ether mg/kg ND 0.33 03/03/22 08:140.12
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 03/03/22 08:140.13
Butylbenzylphthalate mg/kg ND 0.33 03/03/22 08:140.14
Chrysene mg/kg ND 0.33 03/03/22 08:140.12
Di-n-butylphthalate mg/kg ND 0.33 03/03/22 08:140.11
Di-n-octylphthalate mg/kg ND 0.33 03/03/22 08:140.13
Dibenz(a,h)anthracene mg/kg ND 0.33 03/03/22 08:140.13
Dibenzofuran mg/kg ND 0.33 03/03/22 08:140.12
Diethylphthalate mg/kg ND 0.33 03/03/22 08:140.12
Dimethylphthalate mg/kg ND 0.33 03/03/22 08:140.12
Fluoranthene mg/kg ND 0.33 03/03/22 08:140.11
Fluorene mg/kg ND 0.33 03/03/22 08:140.12
Hexachloro-1,3-butadiene mg/kg ND 0.33 03/03/22 08:140.14
Hexachlorobenzene mg/kg ND 0.33 03/03/22 08:140.13
Hexachlorocyclopentadiene mg/kg ND 0.33 v203/03/22 08:140.19
Hexachloroethane mg/kg ND 0.33 03/03/22 08:140.13
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 03/03/22 08:140.13
Isophorone mg/kg ND 0.33 03/03/22 08:140.15
N-Nitroso-di-n-propylamine mg/kg ND 0.33 03/03/22 08:140.12
N-Nitrosodimethylamine mg/kg ND 0.33 03/03/22 08:140.11
N-Nitrosodiphenylamine mg/kg ND 0.33 03/03/22 08:140.12
Naphthalene mg/kg ND 0.33 03/03/22 08:140.11
Nitrobenzene mg/kg ND 0.33 03/03/22 08:140.15
Pentachlorophenol mg/kg ND 0.66 03/03/22 08:140.32
Phenanthrene mg/kg ND 0.33 03/03/22 08:140.11
Phenol mg/kg ND 0.33 03/03/22 08:140.15
Pyrene mg/kg ND 0.33 03/03/22 08:140.13
Pyridine mg/kg ND 0.33 03/03/22 08:140.10
2,4,6-Tribromophenol (S)%82 18-130 03/03/22 08:14
2-Fluorobiphenyl (S)%69 19-130 03/03/22 08:14
2-Fluorophenol (S)%71 18-130 03/03/22 08:14
Nitrobenzene-d5 (S)%71 21-130 03/03/22 08:14
Phenol-d6 (S)%73 18-130 03/03/22 08:14
Terphenyl-d14 (S)%107 15-130 03/03/22 08:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3567277LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.21.7 75 47-130
1,2-Dichlorobenzene mg/kg 1.21.7 71 49-130
1,3-Dichlorobenzene mg/kg 1.21.7 71 48-130
1,4-Dichlorobenzene mg/kg 1.21.7 70 49-130
1-Methylnaphthalene mg/kg 1.31.7 77 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3567277LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.21.7 74 38-130
2,4,5-Trichlorophenol mg/kg 1.41.7 86 49-130
2,4,6-Trichlorophenol mg/kg 1.41.7 84 50-130
2,4-Dichlorophenol mg/kg 1.41.7 82 51-130
2,4-Dimethylphenol mg/kg 1.31.7 77 53-130
2,4-Dinitrophenol mg/kg 6.18.3 73 39-130
2,4-Dinitrotoluene mg/kg 1.51.7 91 53-130
2,6-Dinitrotoluene mg/kg 1.51.7 90 55-130
2-Chloronaphthalene mg/kg 1.31.7 80 48-130
2-Chlorophenol mg/kg 1.21.7 73 54-130
2-Methylnaphthalene mg/kg 1.31.7 77 57-130
2-Methylphenol(o-Cresol)mg/kg 1.31.7 78 50-130
2-Nitroaniline mg/kg 2.63.3 79 49-130
2-Nitrophenol mg/kg 1.31.7 81 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.31.7 80 50-130
3,3'-Dichlorobenzidine mg/kg 2.6 IL3.3 79 47-130
3-Nitroaniline mg/kg 2.83.3 85 45-130
4,6-Dinitro-2-methylphenol mg/kg 2.83.3 83 50-142
4-Bromophenylphenyl ether mg/kg 1.31.7 81 55-130
4-Chloro-3-methylphenol mg/kg 2.73.3 82 52-130
4-Chloroaniline mg/kg 2.43.3 73 49-130
4-Chlorophenylphenyl ether mg/kg 1.31.7 80 53-130
4-Nitroaniline mg/kg 2.73.3 81 51-130
4-Nitrophenol mg/kg 7.18.3 85 40-130
Acenaphthene mg/kg 1.41.7 82 56-130
Acenaphthylene mg/kg 1.31.7 81 58-130
Aniline mg/kg 1.11.7 67 44-130
Anthracene mg/kg 1.41.7 82 60-130
Benzo(a)anthracene mg/kg 1.41.7 86 59-130
Benzo(a)pyrene mg/kg 1.61.7 94 57-130
Benzo(b)fluoranthene mg/kg 1.51.7 91 54-130
Benzo(g,h,i)perylene mg/kg 1.51.7 92 59-130
Benzo(k)fluoranthene mg/kg 1.61.7 95 54-130
Benzoic Acid mg/kg 5.08.3 61 19-130
Benzyl alcohol mg/kg 2.53.3 76 50-130
bis(2-Chloroethoxy)methane mg/kg 1.31.7 76 55-130
bis(2-Chloroethyl) ether mg/kg 1.21.7 72 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.51.7 93 58-130
Butylbenzylphthalate mg/kg 1.61.7 96 46-138
Chrysene mg/kg 1.51.7 89 57-130
Di-n-butylphthalate mg/kg 1.41.7 84 57-130
Di-n-octylphthalate mg/kg 1.61.7 95 57-130
Dibenz(a,h)anthracene mg/kg 1.51.7 91 60-130
Dibenzofuran mg/kg 1.41.7 84 54-130
Diethylphthalate mg/kg 1.41.7 83 55-130
Dimethylphthalate mg/kg 1.41.7 84 57-130
Fluoranthene mg/kg 1.41.7 85 57-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3567277LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.41.7 84 56-130
Hexachloro-1,3-butadiene mg/kg 1.11.7 67 41-130
Hexachlorobenzene mg/kg 1.41.7 86 53-130
Hexachlorocyclopentadiene mg/kg 0.79 v31.7 48 23-130
Hexachloroethane mg/kg 1.21.7 70 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.41.7 87 61-130
Isophorone mg/kg 1.21.7 75 49-130
N-Nitroso-di-n-propylamine mg/kg 1.21.7 75 52-130
N-Nitrosodimethylamine mg/kg 1.21.7 70 45-130
N-Nitrosodiphenylamine mg/kg 1.31.7 78 56-130
Naphthalene mg/kg 1.21.7 71 56-130
Nitrobenzene mg/kg 1.21.7 73 50-130
Pentachlorophenol mg/kg 2.83.3 86 33-130
Phenanthrene mg/kg 1.41.7 86 60-130
Phenol mg/kg 1.41.7 84 54-130
Pyrene mg/kg 1.51.7 90 61-130
Pyridine mg/kg 0.981.7 59 35-130
2,4,6-Tribromophenol (S)%98 18-130
2-Fluorobiphenyl (S)%73 19-130
2-Fluorophenol (S)%72 18-130
Nitrobenzene-d5 (S)%71 21-130
Phenol-d6 (S)%73 18-130
Terphenyl-d14 (S)%101 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3567278MATRIX SPIKE SAMPLE:
MSSpike
Result
92590280001
1,2,4-Trichlorobenzene mg/kg 1.12.2 49 22-130ND
1,2-Dichlorobenzene mg/kg 1.02.2 46 23-130ND
1,3-Dichlorobenzene mg/kg 0.982.2 45 26-130ND
1,4-Dichlorobenzene mg/kg 0.982.2 45 27-130ND
1-Methylnaphthalene mg/kg 1.22.2 56 30-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.02.2 48 30-130ND
2,4,5-Trichlorophenol mg/kg 1.82.2 81 26-130ND
2,4,6-Trichlorophenol mg/kg 1.62.2 74 23-130ND
2,4-Dichlorophenol mg/kg 1.22.2 57 29-130ND
2,4-Dimethylphenol mg/kg 1.12.2 51 13-130ND
2,4-Dinitrophenol mg/kg 9.110.9 83 10-131ND
2,4-Dinitrotoluene mg/kg 2.12.2 97 28-130ND
2,6-Dinitrotoluene mg/kg 2.02.2 92 36-130ND
2-Chloronaphthalene mg/kg 1.32.2 60 27-130ND
2-Chlorophenol mg/kg 1.02.2 48 29-130ND
2-Methylnaphthalene mg/kg 1.22.2 55 29-130ND
2-Methylphenol(o-Cresol)mg/kg 1.12.2 51 20-130ND
2-Nitroaniline mg/kg 3.44.3 79 29-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3567278MATRIX SPIKE SAMPLE:
MSSpike
Result
92590280001
2-Nitrophenol mg/kg 1.22.2 56 26-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.22.2 53 10-176ND
3,3'-Dichlorobenzidine mg/kg 3.8 IL4.3 87 15-130ND
3-Nitroaniline mg/kg 3.74.3 85 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 4.04.3 92 15-132ND
4-Bromophenylphenyl ether mg/kg 1.72.2 79 35-130ND
4-Chloro-3-methylphenol mg/kg 3.24.3 74 30-130ND
4-Chloroaniline mg/kg 2.44.3 55 28-130ND
4-Chlorophenylphenyl ether mg/kg 1.62.2 75 32-130ND
4-Nitroaniline mg/kg 3.94.3 89 30-130ND
4-Nitrophenol mg/kg 9.810.9 90 17-130ND
Acenaphthene mg/kg 1.52.2 71 29-130ND
Acenaphthylene mg/kg 1.52.2 70 31-130ND
Aniline mg/kg 0.872.2 40 10-130ND
Anthracene mg/kg 1.92.2 85 33-130ND
Benzo(a)anthracene mg/kg 2.02.2 91 32-130ND
Benzo(a)pyrene mg/kg 2.12.2 97 32-130ND
Benzo(b)fluoranthene mg/kg 2.12.2 97 33-130ND
Benzo(g,h,i)perylene mg/kg 2.12.2 95 28-130ND
Benzo(k)fluoranthene mg/kg 2.22.2 100 31-130ND
Benzoic Acid mg/kg 2.810.9 25 10-130ND
Benzyl alcohol mg/kg 2.34.3 53 31-130ND
bis(2-Chloroethoxy)methane mg/kg 1.12.2 52 30-130ND
bis(2-Chloroethyl) ether mg/kg 1.0 M12.2 47 68-130ND
bis(2-Ethylhexyl)phthalate mg/kg 2.12.2 95 40-130ND
Butylbenzylphthalate mg/kg 2.12.2 98 40-130ND
Chrysene mg/kg 2.12.2 95 30-130ND
Di-n-butylphthalate mg/kg 1.92.2 87 41-130ND
Di-n-octylphthalate mg/kg 2.12.2 97 42-130ND
Dibenz(a,h)anthracene mg/kg 2.02.2 92 27-130ND
Dibenzofuran mg/kg 1.72.2 76 32-130ND
Diethylphthalate mg/kg 1.92.2 88 40-130ND
Dimethylphthalate mg/kg 1.92.2 86 37-130ND
Fluoranthene mg/kg 2.12.2 94 26-130ND
Fluorene mg/kg 1.82.2 80 31-130ND
Hexachloro-1,3-butadiene mg/kg 0.892.2 41 20-130ND
Hexachlorobenzene mg/kg 1.92.2 87 29-130ND
Hexachlorocyclopentadiene mg/kg 0.63 v32.2 29 10-130ND
Hexachloroethane mg/kg 0.932.2 42 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 2.02.2 94 28-130ND
Isophorone mg/kg 1.32.2 58 32-130ND
N-Nitroso-di-n-propylamine mg/kg 1.12.2 53 31-130ND
N-Nitrosodimethylamine mg/kg 0.972.2 44 20-130ND
N-Nitrosodiphenylamine mg/kg 1.82.2 81 32-130ND
Naphthalene mg/kg 1.02.2 48 30-130ND
Nitrobenzene mg/kg 1.12.2 50 25-130ND
Pentachlorophenol mg/kg 4.04.3 93 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3567278MATRIX SPIKE SAMPLE:
MSSpike
Result
92590280001
Phenanthrene mg/kg 1.92.2 89 34-130ND
Phenol mg/kg 1.22.2 55 14-130ND
Pyrene mg/kg 2.12.2 95 31-130ND
Pyridine mg/kg 0.792.2 36 10-130ND
2,4,6-Tribromophenol (S)%98 18-130
2-Fluorobiphenyl (S)%50 19-130
2-Fluorophenol (S)%44 18-130
Nitrobenzene-d5 (S)%48 21-130
Phenol-d6 (S)%48 18-130
Terphenyl-d14 (S)%97 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92590280002
3567279SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
1-Methylnaphthalene mg/kg ND 30ND
2,2'-Oxybis(1-chloropropane)mg/kg ND v130ND
2,4,5-Trichlorophenol mg/kg ND 30ND
2,4,6-Trichlorophenol mg/kg ND 30ND
2,4-Dichlorophenol mg/kg ND 30ND
2,4-Dimethylphenol mg/kg ND 30ND
2,4-Dinitrophenol mg/kg ND 30ND
2,4-Dinitrotoluene mg/kg ND 30ND
2,6-Dinitrotoluene mg/kg ND 30ND
2-Chloronaphthalene mg/kg ND 30ND
2-Chlorophenol mg/kg ND 30ND
2-Methylnaphthalene mg/kg ND 30ND
2-Methylphenol(o-Cresol)mg/kg ND 30ND
2-Nitroaniline mg/kg ND 30ND
2-Nitrophenol mg/kg ND 30ND
3&4-Methylphenol(m&p Cresol)mg/kg ND 30ND
3,3'-Dichlorobenzidine mg/kg ND IL30ND
3-Nitroaniline mg/kg ND IL30ND
4,6-Dinitro-2-methylphenol mg/kg ND 30ND
4-Bromophenylphenyl ether mg/kg ND 30ND
4-Chloro-3-methylphenol mg/kg ND 30ND
4-Chloroaniline mg/kg ND IL30ND
4-Chlorophenylphenyl ether mg/kg ND 30ND
4-Nitroaniline mg/kg ND 30ND
4-Nitrophenol mg/kg ND 30ND
Acenaphthene mg/kg ND 30ND
Acenaphthylene mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92590280002
3567279SAMPLE DUPLICATE:
Aniline mg/kg ND 30ND
Anthracene mg/kg ND 30ND
Benzo(a)anthracene mg/kg 0.15J 30264J ug/kg
Benzo(a)pyrene mg/kg 0.16J 30261J ug/kg
Benzo(b)fluoranthene mg/kg 0.22J 30366J ug/kg
Benzo(g,h,i)perylene mg/kg ND 30158J ug/kg
Benzo(k)fluoranthene mg/kg ND 30147J ug/kg
Benzoic Acid mg/kg ND 30ND
Benzyl alcohol mg/kg ND 30ND
bis(2-Chloroethoxy)methane mg/kg ND 30ND
bis(2-Chloroethyl) ether mg/kg ND 30ND
bis(2-Ethylhexyl)phthalate mg/kg ND 30ND
Butylbenzylphthalate mg/kg ND 30ND
Chrysene mg/kg 0.20J 30302J ug/kg
Di-n-butylphthalate mg/kg ND 30ND
Di-n-octylphthalate mg/kg ND 30ND
Dibenz(a,h)anthracene mg/kg ND 30ND
Dibenzofuran mg/kg ND 30ND
Diethylphthalate mg/kg ND 30ND
Dimethylphthalate mg/kg ND 30ND
Fluoranthene mg/kg 0.34J 30550 ug/kg
Fluorene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND v130ND
Hexachlorobenzene mg/kg ND 30ND
Hexachlorocyclopentadiene mg/kg ND 30ND
Hexachloroethane mg/kg ND 30ND
Indeno(1,2,3-cd)pyrene mg/kg ND 30ND
Isophorone mg/kg ND 30ND
N-Nitroso-di-n-propylamine mg/kg ND 30ND
N-Nitrosodimethylamine mg/kg ND 30ND
N-Nitrosodiphenylamine mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
Nitrobenzene mg/kg ND 30ND
Pentachlorophenol mg/kg ND v230ND
Phenanthrene mg/kg 0.17J 30252J ug/kg
Phenol mg/kg ND 30ND
Pyrene mg/kg 0.30J 30507 ug/kg
Pyridine mg/kg ND 30ND
2,4,6-Tribromophenol (S)%6477
2-Fluorobiphenyl (S)%4365
2-Fluorophenol (S)%4365
Nitrobenzene-d5 (S)%5072
Phenol-d6 (S)%5172
Terphenyl-d14 (S)%84106
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 60
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590340
Monroe Road Project
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
681105
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92590340001, 92590340002, 92590340003, 92590340004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92590123025
3563533SAMPLE DUPLICATE:
Percent Moisture %19.8 N212520.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92590302004
3563534SAMPLE DUPLICATE:
Percent Moisture %23.7 N242524.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 38 of 60
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92590340
Monroe Road Project
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
WORKORDER QUALIFIERS
WO: 92590340
Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees
Celsius.[1]
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in theassociated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 60
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92590340
Monroe Road Project
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92590340001 681269 681329SB-1 EPA 3050B EPA 6010D
92590340002 681269 681329SB-2 EPA 3050B EPA 6010D
92590340003 681269 681329SB-3 EPA 3050B EPA 6010D
92590340004 681269 681329DUP-1 EPA 3050B EPA 6010D
92590340001 681614 681821SB-1 EPA 7471B EPA 7471B
92590340002 681614 681821SB-2 EPA 7471B EPA 7471B
92590340003 681614 681821SB-3 EPA 7471B EPA 7471B
92590340004 681614 681821DUP-1 EPA 7471B EPA 7471B
92590340001 681992 682125SB-1 EPA 3546 EPA 8270E
92590340002 681992 682125SB-2 EPA 3546 EPA 8270E
92590340003 681992 682125SB-3 EPA 3546 EPA 8270E
92590340004 681992 682125DUP-1 EPA 3546 EPA 8270E
92590340001 681117 681353SB-1 EPA 5035A/5030B EPA 8260D
92590340002 681117 681353SB-2 EPA 5035A/5030B EPA 8260D
92590340003 681117 681353SB-3 EPA 5035A/5030B EPA 8260D
92590340004 681117 681353DUP-1 EPA 5035A/5030B EPA 8260D
92590340001 681105SB-1 SW-846
92590340002 681105SB-2 SW-846
92590340003 681105SB-3 SW-846
92590340004 681105DUP-1 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 04:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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ANALYTICAL REPORT
Eurofins Lancaster Laboratories Env, LLC
2425 New Holland Pike
Lancaster, PA 17601
Tel: [phone]
Laboratory Job ID: 410-74568-1
Client Project/Site: 92590340
For:
Pace Analytical Services, LLC
9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078
Attn: Angela Baioni
Authorized for release by:
3/11/2022 7:53:15 AM
Nicole Brown, Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Analytical test results meet all requirements of the associated regulatory program (e.g., NELAC (TNI), DoD,
and ISO 17025) unless otherwise noted under the individual analysis. Data qualifiers are applied to note
exceptions. Noncompliant quality control (QC) is further explained in narrative comments.
· QC results that exceed the upper limits and are associated with non-detect samples are qualified but further
narration is not required since the bias is high and does not change a non-detect result. Further narration is
also not required with QC blank detection when the associated sample concentration is non-detect or more
than ten times the level in the blank.
· Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD is performed, unless otherwise
specified in the method.
· Surrogate and/or isotope dilution analyte recoveries (if applicable) which are outside of the QC window are
confirmed unless attributed to a dilution or otherwise noted in the narrative.
Regulated compliance samples (e.g. SDWA, NPDES) must comply with the associated agency
requirements/permits.
Measurement uncertainty values, as applicable, are available upon request.
Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or
microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of
the bulk of material involved, the test results will be meaningless. If you have questions regarding the proper
techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity,
however, unless sampling has been performed by a member of our staff. Times are local to the area of activity.
Parameters listed in the 40 CFR Part 136 Table II as "analyze immediately" and tested in the laboratory are not
performed within 15 minutes of collection.
This report shall not be reproduced except in full, without the written approval of the laboratory.
WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results
for the sample as submitted. The foregoing express warranty is exclusive and is given in lieu of all other
warranties, expressed or implied, except as otherwise agreed. We disclaim any other warranties, expressed or
implied, including a warranty of fitness for particular purpose and warranty of merchantability. In no event shall
Eurofins Lancaster Laboratories Environmental, LLC be liable for indirect, special, consequential, or incidental
damages including, but not limited to, damages for loss of profit or goodwill regardless of (A) the negligence
(either sole or concurrent) of Eurofins Lancaster Laboratories Environmental and (B) whether Eurofins
Lancaster Laboratories Environmental has been informed of the possibility of such damages. We accept no
legal responsibility for the purposes for which the client uses the test results. Except as otherwise agreed, no
purchase order or other order for work shall be accepted by Eurofins Lancaster Laboratories Environmental
which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster
Laboratories Environmental hereby objects to any conflicting terms contained in any acceptance or order
submitted by client.
Nicole Brown
Project Manager
3/11/2022 7:53:15 AM
Client: Pace Analytical Services, LLC
Project/Site: 92590340
Laboratory Job ID: 410-74568-1
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Table of Contents
Client: Pace Analytical Services, LLC
Project/Site: 92590340
Laboratory Job ID: 410-74568-1
Page 3 of 17 Eurofins Lancaster Laboratories Env, LLC3/11/2022
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
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Definitions/Glossary
Job ID: 410-74568-1Client: Pace Analytical Services, LLC
Project/Site: 92590340
Qualifiers
HPLC/IC
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
1C Result is from the primary column on a dual-column method.
2C Result is from the confirmation column on a dual-column method.
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Lancaster Laboratories Env, LLC
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Case Narrative
Client: Pace Analytical Services, LLC Job ID: 410-74568-1
Project/Site: 92590340
Job ID: 410-74568-1
Laboratory: Eurofins Lancaster Laboratories Env, LLC
Narrative
Job Narrative
410-74568-1
Receipt
The samples were received on 3/2/2022 10:44 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 1.7°C
HPLC/IC
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
General Chemistry
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Eurofins Lancaster Laboratories Env, LLCPage 5 of 17 3/11/2022
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Detection Summary
Job ID: 410-74568-1Client: Pace Analytical Services, LLC
Project/Site: 92590340
Client Sample ID: SB-1 / 92590340001 Lab Sample ID: 410-74568-1
☼Cr (VI)
RL
0.489 mg/Kg
MDL
0.171
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10.656 7199
Client Sample ID: SB-2 / 92590340002 Lab Sample ID: 410-74568-2
☼Cr (VI)
RL
0.511 mg/Kg
MDL
0.179
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.11 7199
Client Sample ID: SB-3 / 92590340003 Lab Sample ID: 410-74568-3
☼Cr (VI)
RL
0.477 mg/Kg
MDL
0.167
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA12.31 7199
Client Sample ID: DUP-1 / 92590340004 Lab Sample ID: 410-74568-4
☼Cr (VI)
RL
0.531 mg/Kg
MDL
0.186
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.348 7199
Eurofins Lancaster Laboratories Env, LLC
This Detection Summary does not include radiochemical test results.
Page 6 of 17 3/11/2022
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Client Sample Results
Job ID: 410-74568-1Client: Pace Analytical Services, LLC
Project/Site: 92590340
Lab Sample ID: 410-74568-1Client Sample ID: SB-1 / 92590340001
Matrix: SolidDate Collected: 02/25/22 11:40
Date Received: 03/02/22 10:44
General Chemistry
RL MDL
Percent Moisture 18.0 1.0 1.0 %03/02/22 20:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 410-74568-1Client Sample ID: SB-1 / 92590340001
Matrix: SolidDate Collected: 02/25/22 11:40
Percent Solids: 82.0Date Received: 03/02/22 10:44
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Cr (VI)0.656 0.489 0.171 mg/Kg ☼03/09/22 13:17 03/10/22 20:15 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 410-74568-2Client Sample ID: SB-2 / 92590340002
Matrix: SolidDate Collected: 02/25/22 12:00
Date Received: 03/02/22 10:44
General Chemistry
RL MDL
Percent Moisture 19.2 1.0 1.0 %03/02/22 20:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 410-74568-2Client Sample ID: SB-2 / 92590340002
Matrix: SolidDate Collected: 02/25/22 12:00
Percent Solids: 80.8Date Received: 03/02/22 10:44
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Cr (VI)1.11 0.511 0.179 mg/Kg ☼03/09/22 13:17 03/10/22 20:36 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 410-74568-3Client Sample ID: SB-3 / 92590340003
Matrix: SolidDate Collected: 02/25/22 12:20
Date Received: 03/02/22 10:44
General Chemistry
RL MDL
Percent Moisture 17.4 1.0 1.0 %03/02/22 20:39 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 410-74568-3Client Sample ID: SB-3 / 92590340003
Matrix: SolidDate Collected: 02/25/22 12:20
Percent Solids: 82.6Date Received: 03/02/22 10:44
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Cr (VI)2.31 0.477 0.167 mg/Kg ☼03/09/22 13:17 03/10/22 20:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Lab Sample ID: 410-74568-4Client Sample ID: DUP-1 / 92590340004
Matrix: SolidDate Collected: 02/25/22 00:00
Date Received: 03/02/22 10:44
General Chemistry
RL MDL
Percent Moisture 24.1 1.0 1.0 %03/02/22 22:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins Lancaster Laboratories Env, LLC
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Client Sample Results
Job ID: 410-74568-1Client: Pace Analytical Services, LLC
Project/Site: 92590340
Lab Sample ID: 410-74568-4Client Sample ID: DUP-1 / 92590340004
Matrix: SolidDate Collected: 02/25/22 00:00
Percent Solids: 75.9Date Received: 03/02/22 10:44
Method: 7199 - Chromium, Hexavalent (IC)
RL MDL
Cr (VI)0.348 J 0.531 0.186 mg/Kg ☼03/09/22 13:17 03/10/22 20:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
Eurofins Lancaster Laboratories Env, LLC
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QC Sample Results
Job ID: 410-74568-1Client: Pace Analytical Services, LLC
Project/Site: 92590340
Method: 7199 - Chromium, Hexavalent (IC)
Client Sample ID: Method BlankLab Sample ID: MB 410-231755/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 232552 Prep Batch: 231755
RL MDL
Cr (VI)ND 0.400 0.140 mg/Kg 03/09/22 13:17 03/10/22 17:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-231755/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 232552 Prep Batch: 231755
Cr (VI)5.00 4.561 mg/Kg 91 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCSI 410-231755/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 232552 Prep Batch: 231755
Cr (VI)862 794.3 mg/Kg 92 80 -120
Analyte
LCSI LCSI
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Eurofins Lancaster Laboratories Env, LLC
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QC Association Summary
Job ID: 410-74568-1Client: Pace Analytical Services, LLC
Project/Site: 92590340
HPLC/IC
Prep Batch: 231755
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A410-74568-1 SB-1 / 92590340001 Total/NA
Solid 3060A410-74568-2 SB-2 / 92590340002 Total/NA
Solid 3060A410-74568-3 SB-3 / 92590340003 Total/NA
Solid 3060A410-74568-4 DUP-1 / 92590340004 Total/NA
Solid 3060AMB 410-231755/1-A Method Blank Total/NA
Solid 3060ALCS 410-231755/2-A Lab Control Sample Total/NA
Solid 3060ALCSI 410-231755/3-A Lab Control Sample Total/NA
Analysis Batch: 232552
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7199 231755410-74568-1 SB-1 / 92590340001 Total/NA
Solid 7199 231755410-74568-1 SB-1 / 92590340001 Total/NA
Solid 7199 231755410-74568-2 SB-2 / 92590340002 Total/NA
Solid 7199 231755410-74568-2 SB-2 / 92590340002 Total/NA
Solid 7199 231755410-74568-3 SB-3 / 92590340003 Total/NA
Solid 7199 231755410-74568-3 SB-3 / 92590340003 Total/NA
Solid 7199 231755410-74568-4 DUP-1 / 92590340004 Total/NA
Solid 7199 231755410-74568-4 DUP-1 / 92590340004 Total/NA
Solid 7199 231755MB 410-231755/1-A Method Blank Total/NA
Solid 7199 231755LCS 410-231755/2-A Lab Control Sample Total/NA
Solid 7199 231755LCSI 410-231755/3-A Lab Control Sample Total/NA
General Chemistry
Analysis Batch: 229421
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture410-74568-1 SB-1 / 92590340001 Total/NA
Solid Moisture410-74568-2 SB-2 / 92590340002 Total/NA
Solid Moisture410-74568-3 SB-3 / 92590340003 Total/NA
Solid Moisture410-74568-4 DUP-1 / 92590340004 Total/NA
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Lab Chronicle
Client: Pace Analytical Services, LLC Job ID: 410-74568-1
Project/Site: 92590340
Client Sample ID: SB-1 / 92590340001 Lab Sample ID: 410-74568-1
Matrix: SolidDate Collected: 02/25/22 11:40
Date Received: 03/02/22 10:44
Analysis Moisture 03/02/22 20:39 OEL41229421 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: SB-1 / 92590340001 Lab Sample ID: 410-74568-1
Matrix: SolidDate Collected: 02/25/22 11:40
Percent Solids: 82.0Date Received: 03/02/22 10:44
Prep 3060A 03/09/22 13:17 L4QM231755 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 7199 1 232552 03/10/22 20:15 Z7CH ELLETotal/NA
Prep 3060A 231755 03/09/22 13:17 L4QM ELLETotal/NA
Analysis 7199 1 232552 03/10/22 20:22 Z7CH ELLETotal/NA
Client Sample ID: SB-2 / 92590340002 Lab Sample ID: 410-74568-2
Matrix: SolidDate Collected: 02/25/22 12:00
Date Received: 03/02/22 10:44
Analysis Moisture 03/02/22 20:39 OEL41229421 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: SB-2 / 92590340002 Lab Sample ID: 410-74568-2
Matrix: SolidDate Collected: 02/25/22 12:00
Percent Solids: 80.8Date Received: 03/02/22 10:44
Prep 3060A 03/09/22 13:17 L4QM231755 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 7199 1 232552 03/10/22 20:29 Z7CH ELLETotal/NA
Prep 3060A 231755 03/09/22 13:17 L4QM ELLETotal/NA
Analysis 7199 1 232552 03/10/22 20:36 Z7CH ELLETotal/NA
Client Sample ID: SB-3 / 92590340003 Lab Sample ID: 410-74568-3
Matrix: SolidDate Collected: 02/25/22 12:20
Date Received: 03/02/22 10:44
Analysis Moisture 03/02/22 20:39 OEL41229421 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: SB-3 / 92590340003 Lab Sample ID: 410-74568-3
Matrix: SolidDate Collected: 02/25/22 12:20
Percent Solids: 82.6Date Received: 03/02/22 10:44
Prep 3060A 03/09/22 13:17 L4QM231755 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 7199 1 232552 03/10/22 20:43 Z7CH ELLETotal/NA
Prep 3060A 231755 03/09/22 13:17 L4QM ELLETotal/NA
Analysis 7199 1 232552 03/10/22 20:50 Z7CH ELLETotal/NA
Eurofins Lancaster Laboratories Env, LLC
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Lab Chronicle
Client: Pace Analytical Services, LLC Job ID: 410-74568-1
Project/Site: 92590340
Client Sample ID: DUP-1 / 92590340004 Lab Sample ID: 410-74568-4
Matrix: SolidDate Collected: 02/25/22 00:00
Date Received: 03/02/22 10:44
Analysis Moisture 03/02/22 22:00 OEL41229421 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Client Sample ID: DUP-1 / 92590340004 Lab Sample ID: 410-74568-4
Matrix: SolidDate Collected: 02/25/22 00:00
Percent Solids: 75.9Date Received: 03/02/22 10:44
Prep 3060A 03/09/22 13:17 L4QM231755 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 7199 1 232552 03/10/22 20:57 Z7CH ELLETotal/NA
Prep 3060A 231755 03/09/22 13:17 L4QM ELLETotal/NA
Analysis 7199 1 232552 03/10/22 21:04 Z7CH ELLETotal/NA
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Lancaster Laboratories Env, LLC
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Accreditation/Certification Summary
Client: Pace Analytical Services, LLC Job ID: 410-74568-1
Project/Site: 92590340
Laboratory: Eurofins Lancaster Laboratories Env, LLC
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 521 12-31-22
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
Moisture Solid Percent Moisture
Eurofins Lancaster Laboratories Env, LLC
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Method Summary
Job ID: 410-74568-1Client: Pace Analytical Services, LLC
Project/Site: 92590340
Method Method Description LaboratoryProtocol
SW8467199Chromium, Hexavalent (IC)ELLE
EPAMoisturePercent Moisture ELLE
SW8463060AAlkaline Digestion (Chromium, Hexavalent)ELLE
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Lancaster Laboratories Env, LLC
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Sample Summary
Client: Pace Analytical Services, LLC Job ID: 410-74568-1
Project/Site: 92590340
Lab Sample ID Client Sample ID Matrix Collected Received
410-74568-1 SB-1 / 92590340001 Solid 02/25/22 11:40 03/02/22 10:44
410-74568-2 SB-2 / 92590340002 Solid 02/25/22 12:00 03/02/22 10:44
410-74568-3 SB-3 / 92590340003 Solid 02/25/22 12:20 03/02/22 10:44
410-74568-4 DUP-1 / 92590340004 Solid 02/25/22 00:00 03/02/22 10:44
Eurofins Lancaster Laboratories Env, LLCPage 15 of 17 3/11/2022
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Login Sample Receipt Checklist
Client: Pace Analytical Services, LLC Job Number: 410-74568-1
Login Number: 74568
Question Answer Comment
Creator: McCaskey, Jonathan
List Source: Eurofins Lancaster Laboratories Env, LLC
List Number: 1
N/AThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
FalseIs the Field Sampler's name present on COC?Received project as a subcontract.
N/ASample custody seals are intact.
Eurofins Lancaster Laboratories Env, LLC
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APPENDIX C

Univar USA Inc Safety Data Sheet

SDS No:
Version No:
Order No:

3075 Highland Pkwy, Ste 200, Downers Grove, IL 60515
[phone]

Emergency Assistance
For emergency assistance involving chemicals call
Chemtrec - [phone]
002 2015-06-05
SAFETY DATA SHEET

1. Identification

Product identifier: - CYCLOHEXANONE
Other means of identification
SDS number: 000100000090
Recommended use and restriction on use
Recommended use: Not available.
Restrictions on use: Not known.
Emergency telephone number:For emergency assistance Involving chemicals
call CHEMTREC day or night at: 1-800-424-9300. CHEMTREC INTERNATIONAL Tel# [phone]
2. Hazard(s) identification

Hazard classification
Health hazards
Acute toxicity (Dermal) Category 3

Skin corrosion/irritation Category 2

Hazard symbol

Signal word Danger

Label elements
Univar
3075 Highland Pkwy STE 200
Downers Grove, IL 60515
425-889-3400
UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 2/13

Hazard statement Flammable liquid and vapor.
Aspiration hazard if swallowed - can enter lungs and cause damage.
Harmful if swallowed.
Harmful if inhaled.
Harmful in contact with skin.
Causes skin and eye irritation.
May cause respiratory irritation.

Precautionary statement

Prevention Wear protective gloves/protective clothing/eye protection/face protection.
Wash thoroughly after handling. Do not get in eyes, on skin, or on clothing.
Avoid breathing vapors. Keep away from heat/sparks/open flames/hot
surfaces. No smoking. Ground/bond container and receiving equipment.
Take precautionary measures against static discharge.

Response IF ON SKIN: Wash with plenty of water. If skin irritation occurs: Get medical
advice/attention. Call a POISON CENTER/doctor if you feel unwell. Specific
treatment (see this label). Remove/Take off immediately all contaminated
clothing. Wash contaminated clothing before reuse.

Storage Store in a closed container. Keep container tightly closed. Store in a well-
ventilated place. Store in a dry place. Store locked up.

Disposal Dispose of contents/container to an appropriate treatment and disposal
facility in accordance with applicable laws and regulations, and product
characteristics at time of disposal.
Other hazards which do not
result in GHS classification
None.

3. Composition/information on ingredients

UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 3/13

Substances
Chemical identity Common name
and synonyms CAS number Content in percent (%)*
Cyclohexanone 108-94-1 100%
* All concentrations are percent by weight unless ingredient is a gas. Gas concentrations are in percent by volume.
Composition comments: The components are not hazardous or are below required disclosure
limits.

4. First-aid measures

General information: CAUTION! First aid personnel must be aware of own risk during rescue!
Ingestion: Do NOT induce vomiting. Never give liquid to an unconscious person. Get
medical attention immediately.
Inhalation: Move to fresh air. Get medical attention immediately.
Skin contact: Immediately flush with plenty of water for at least 15 minutes while
removing contaminated clothing and shoes.
Eye contact: If in eyes, hold eyes open, flood with water for at least 15 minutes and see
a doctor.
Most important symptoms/effects, acute and delayed
Symptoms: No data available.

Indication of immediate medical attention and special treatment needed
Treatment: No data available.
5. Fire-fighting measures

General fire hazards: No data available.
Suitable (and unsuitable) extinguishing media

Suitable extinguishing
media:
Extinguish with foam, carbon dioxide or dry powder.
Unsuitable extinguishing
media:
No data available.
Specific hazards arising from the
chemical:
Vapors may travel considerable distance to a source of ignition and flash
back.
Special protective equipment and precautions for firefighters
Special fire fighting
procedures:
No data available.
UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 4/13

Special protective equipment for
fire-fighters:
No data available.
6. Accidental release measures

Personal precautions, protective
equipment and emergency
procedures:

Use personal protective equipment. Keep unauthorized personnel away.
Methods and material for
containment and cleaning up:
All equipment used when handling the product must be grounded.
Eliminate sources of ignition. Absorb spillage with non-combustible,
absorbent material. Dike for later disposal.
7. Handling and storage

Precautions for safe handling:

Use personal protective equipment as required. Eliminate all sources of
ignition. Container must be kept tightly closed. Ground/bond container
and receiving equipment. Use only with adequate ventilation.
Conditions for safe storage,
including any
incompatibilities:
No data available.
8. Exposure controls/personal protection

Control parameters
Occupational exposure limits
Chemical identity Type Exposure Limit values Source
Cyclohexanone TWA 20 ppm US. ACGIH Threshold Limit Values (03
2013)
STEL 50 ppm US. ACGIH Threshold Limit Values (03
2013)
REL 25 ppm 100
mg/m3
US. NIOSH: Pocket Guide to Chemical
Hazards (2010)
PEL 50 ppm 200
mg/m3
US. OSHA Table Z-1 Limits for Air
Contaminants (29 CFR 1910.1000)
(02 2006)
TWA 25 ppm 100
mg/m3
US. OSHA Table Z-1-A (29 CFR
1910.1000) (1989)
TWA 25 ppm 100
mg/m3
US. Tennessee. OELs. Occupational
Exposure Limits, Table Z1A (06 2008)
ST ESL 480
µg/m3
US. Texas. Effects Screening Levels
(Texas Commission on Environmental
UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 5/13

Quality) (02 2013)
AN ESL 80 µg/m3 US. Texas. Effects Screening Levels
(Texas Commission on Environmental
Quality) (02 2013)
AN ESL 20 ppb US. Texas. Effects Screening Levels
(Texas Commission on Environmental
Quality) (02 2013)
ST ESL 120 ppb US. Texas. Effects Screening Levels
(Texas Commission on Environmental
Quality) (02 2013)
TWA PEL 25 ppm 100
mg/m3
US. California Code of Regulations,
Title 8, Section 5155. Airborne
Contaminants (02 2012)
Biological limit values
Chemical identity Exposure Limit values Source
Cyclohexanone (1,2-
Cyclohexanediol, with
hydrolysis: Sampling
time: End of shift at
end of work week.)
80 mg/l (Urine) ACGIH BEL (03 2013)
Cyclohexanone
(Cyclohexanol, with
hydrolysis: Sampling
time: End of shift.)
8 mg/l (Urine) ACGIH BEL (03 2013)
Appropriate engineering
controls
No data available.
Individual protection measures, such as personal protective equipment
General information: Use personal protective equipment as required. Always observe good
personal hygiene measures, such as washing after handling the
material and before eating, drinking, and/or smoking. Routinely wash
work clothing to remove contaminants. Discard contaminated
footwear that cannot be cleaned. Practice good housekeeping.
Eye/face protection: Wear face shield if there is risk of splashes. Wear approved safety
goggles.
Skin protection
Hand protection: Chemical resistant gloves
Other: No data available.
UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 6/13

Respiratory protection: Wear suitable respiratory protection.
Hygiene measures: No data available.
9. Physical and chemical properties

Physical state: Liquid
Form: No data available.
Color: No data available.
Odor: No data available.
Odor threshold: No data available.
pH: 6.6
Melting point/freezing point: -26 °C
Initial boiling point and boiling range: 153 - 156 °C
Flash Point: 43 °C
Evaporation rate: No data available.
Flammability (solid, gas): No data available.
Upper/lower limit on flammability or explosive limits
Flammability limit - upper (%): No data available.
Flammability limit - lower (%): No data available.
Explosive limit - upper (%): No data available.
Explosive limit - lower (%): No data available.
Vapor pressure: No data available.
Vapor density: No data available.
Relative density: No data available.
Solubility(ies)
Solubility in water: No data available.
Solubility (other): No data available.
Partition coefficient (n-octanol/water): No data available.
Auto-ignition temperature: No data available.
Decomposition temperature: No data available.
Viscosity: No data available.

UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 7/13

10. Stability and reactivity
Reactivity: No data available.
Chemical stability: No data available.
Possibility of hazardous
reactions: No data available.
Conditions to avoid: No data available.
Incompatible materials: No data available.
Hazardous decomposition
products:
No data available.
11. Toxicological information

Symptoms related to the physical, chemical and toxicological characteristics
Ingestion: No data available.
Inhalation: No data available.
Skin contact: No data available.
Eye contact: No data available.
Information on toxicological effects
Acute toxicity (list all possible routes of exposure)
Oral
Product: No data available.
Specified substance(s):
Cyclohexanone ALD 50 (Rat): 1,890 mg/kg (, No ) 2 (reliable with restrictions)
Dermal
Product: ATEmix (): 794 mg/kg

Inhalation
Product: No data available.
Specified substance(s):
Cyclohexanone LC 50 (Rat, ): > 6.2 mg/l (, No) 2 (reliable with restrictions)
Repeated dose toxicity
Product: No data available.
Skin corrosion/irritation
Product: No data available.
Serious eye damage/eye irritation
Product: No data available.
Respiratory or skin sensitization
Product: No data available.
Carcinogenicity
Product: No data available.
UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 8/13

IARC Monographs on the Evaluation of Carcinogenic Risks to Humans:
No carcinogenic components identified

US. National Toxicology Program (NTP) Report on Carcinogens:
No carcinogenic components identified
US. OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050):
No carcinogenic components identified
Germ cell mutagenicity
In vitro
Product: No data available.
In vivo
Product: No data available.
Reproductive toxicity
Product: No data available.
Specific target organ toxicity - single exposure
Product: No data available.
Specific target organ toxicity - repeated exposure
Product: No data available.
Aspiration hazard
Product: No data available.
Other effects: No data available.

12. Ecological information

Ecotoxicity:
Acute hazards to the aquatic environment:
Fish
Product: No data available.
Specified substance(s):
Cyclohexanone LC 50 (Fathead minnow (Pimephales promelas), 96 h): 481 - 578 mg/l
Mortality LC 50 (Fathead minnow (Pimephales promelas), 96 h): 630 mg/l
Mortality LC 50 (Fathead minnow (Pimephales promelas), 96 h): 696 - 770
mg/l Mortality LC 50 (Carp (Leuciscus idus melanotus), 48 h): 536 mg/l
Mortality LC 50 (Carp (Leuciscus idus melanotus), 48 h): 752 mg/l Mortality
Aquatic invertebrates
Product: No data available.
Specified substance(s):
Cyclohexanone LC 50 (Water flea (Daphnia magna), 24 h): 800 mg/l Mortality
Chronic hazards to the aquatic environment:
Fish
UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 9/13

Product: No data available.
Aquatic invertebrates
Product: No data available.
Toxicity to Aquatic Plants
Product: No data available.
Persistence and degradability
Biodegradation
Product: No data available.
BOD/COD ratio
Product: No data available.
Bioaccumulative potential
Bioconcentration factor (BCF)
Product: No data available.
Partition coefficient n-octanol / water (log Kow)
Product: No data available.
Specified substance(s):
Cyclohexanone Log Kow: 0.81
Mobility in soil: No data available.
Known or predicted distribution to environmental compartments
Cyclohexanone No data available.

13. Disposal considerations

Disposal instructions: No data available.
Contaminated packaging: No data available.
14. Transport information
DOT
UN number: UN 1915
UN proper shipping name: Cyclohexanone
Transport hazard class(es)
Class: 3
Label(s): 3
Packing group: III
Marine Pollutant: Not regulated.
UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 10/13

Special precautions for user: –
IMDG
UN number: UN 1915
UN proper shipping name: CYCLOHEXANONE
Transport hazard class(es)
Class: 3
Label(s): 3
EmS No.: F-E, S-D
Packing group: III
Marine Pollutant: Not regulated.
Special precautions for user: –
IATA
UN number: UN 1915
Proper Shipping Name: Cyclohexanone
Transport hazard class(es):
Class: 3
Label(s): 3
Packing group: III
Environmental hazards Not regulated.
Special precautions for user: –
Other information
Passenger and cargo aircraft: Allowed.
Cargo aircraft only: Allowed.
15. Regulatory information
US federal regulationsUS. OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050)
None present or none present in regulated quantities.
CERCLA Hazardous Substance List (40 CFR 302.4):
Cyclohexanone Reportable quantity: 5000 lbs.
Superfund amendments and reauthorization act of 1986 (SARA)
Hazard categories
Not listed.
UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 11/13

SARA 302 Extremely hazardous substance
None present or none present in regulated quantities.
SARA 304 Emergency release notification
Chemical identity RQ
Cyclohexanone 5000 lbs.
SARA 311/312 Hazardous chemical
Chemical identity Threshold Planning Quantity
Cyclohexanone 500 lbs
SARA 313 (TRI reporting)
None present or none present in regulated quantities.
Clean Water Act Section 311 Hazardous Substances (40 CFR 117.3)
None present or none present in regulated quantities.
Clean Air Act (CAA) Section 112(r) Accidental Release Prevention (40 CFR 68.130):
None present or none present in regulated quantities.
US state regulations
US. California Proposition 65
No ingredient regulated by CA Prop 65 present.
US. New Jersey Worker and Community Right-to-Know Act
Cyclohexanone Listed
US. Massachusetts RTK - Substance List
Cyclohexanone Listed
US. Pennsylvania RTK - Hazardous Substances
Cyclohexanone Listed
US. Rhode Island RTK
Cyclohexanone Listed
UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 12/13

Inventory Status:Australia AICS: Not in compliance with the inventory.
Canada DSL Inventory List: Not in compliance with the inventory.
EU EINECS List: On or in compliance with the inventory
EU ELINCS List: Not in compliance with the inventory.
Japan (ENCS) List: Not in compliance with the inventory.
EU No Longer Polymers List: Not in compliance with the inventory.
China Inv. Existing Chemical Substances: Not in compliance with the inventory.
Korea Existing Chemicals Inv. (KECI): Not in compliance with the inventory.
Canada NDSL Inventory: Not in compliance with the inventory.
Philippines PICCS: Not in compliance with the inventory.
US TSCA Inventory: On or in compliance with the inventory
New Zealand Inventory of Chemicals: Not in compliance with the inventory.
Japan ISHL Listing: Not in compliance with the inventory.
Japan Pharmacopoeia Listing: Not in compliance with the inventory.
16.Other information, including date of preparation or last revision
HMIS Hazard ID
Health 2
Flammability 2
Physical hazards 0
PERSONAL PROTECTION E
Hazard rating: 0 - Minimal; 1 - Slight; 2 - Moderate; 3 - Serious; 4 - Severe; *Chronic health
effect
NFPA Hazard ID

Flammability
Health
Reactivity
Special hazard.
Hazard rating: 0 - Minimal; 1 - Slight; 2 - Moderate; 3 - Serious; 4 - Severe
Issue date: 06/05/2015
Revision date: No data available.
Version #: 1.1
Further information: No data available.

2
0

2

E - Safety Glasses, Gloves & Dust Respirator
UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:
Version: 1.1
Revision date: 06/05/2015

SDS_US - 000100000090 13/13

UNIVAR USA INC.SDS NO:10000090
ISSUE DATE:2015-06-05 VERSION:002 2015-06-05
Annotation:

Univar USA Inc Safety Data Sheet
For Additional Information contact SDS Coordinator during business hours, Pacific time: [phone]

Notice
Univar USA Inc. (”Univar”) expressly disclaims all express or implied warranties of merchantability and fitness for
a particular purpose, with respect to the product or information provided herein, and shall under no
circumstances be liable for incidental or consequential damages.
Do not use ingredient information and/or ingredient percentages in this SDS as a product specification. For
product specification information refer to a product specification sheet and/or a certificate of analysis. These
can be obtained from your local Univar sales office.

All information appearing herein is based upon data obtained from the manufacturer and/or recognized
technical sources. While the information is believed to be accurate, Univar makes no representations as to its
accuracy or sufficiency. Conditions of use are beyond Univar's control and therefore users are responsible to
verify this data under their own operating conditions to determine whether the product is suitable for their
particular purposes and they assume all risks of their use, handling, and disposal of the product, or from the
publication or use of, or reliance upon, information contained herein.

This information relates only to the product designated herein, and does not relate to its use in combination
with any other material or in any other process

SAFETY DATA SHEET

Ethanol 99% Page 1

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

SECTION 1. IDENTIFICATION
Identification of the
company:
Colorants Solutions USA LLC
4000 Monroe Road
Charlotte, NC, 28205
Telephone No.: [phone]

Information of the substance/preparation:
Product Stewardship, [phone] Emergency tel. number: [phone] CHEMTREC

Trade name: Ethanol 99%
Material number: 301712

CAS number: 64-17-5

Chemical family: Ethanol

SECTION 2. HAZARDS IDENTIFICATION
GHS classification in accordance with the OSHA Hazard Communication Standard (29 CFR
1910.1200)
Flammable liquids

: Category 2
Eye irritation

: Category 2A
GHS label elements
Hazard pictograms

:

Signal word

: Danger

Hazard statements

: H225 Highly flammable liquid and vapour.
H319 Causes serious eye irritation.

Precautionary statements

: Prevention:
P210 Keep away from heat/ sparks/ open flames/ hot surfaces.
No smoking.
P233 Keep container tightly closed.
P240 Ground/bond container and receiving equipment.
P241 Use explosion-proof electrical/ ventilating/ lighting
equipment.
P242 Use only non-sparking tools.
P243 Take precautionary measures against static discharge.
P264 Wash skin thoroughly after handling.
P280 Wear protective gloves/ eye protection/ face protection.

SAFETY DATA SHEET

Ethanol 99% Page 2

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

Response:
P303 + P361 + P353 IF ON SKIN (or hair): Take off immediately
all contaminated clothing. Rinse skin with water/ shower.
P305 + P351 + P338 IF IN EYES: Rinse cautiously with water
for several minutes. Remove contact lenses, if present and easy
to do. Continue rinsing.
P337 + P313 If eye irritation persists: Get medical advice/
attention.
P370 + P378 In case of fire: Use dry sand, dry chemical or
alcohol-resistant foam to extinguish.
Storage:
P403 + P235 Store in a well-ventilated place. Keep cool.
Disposal:
P501 Dispose of contents/ container to an approved waste
disposal plant.

Other hazards
None known.
SECTION 3. COMPOSITION/INFORMATION ON INGREDIENTS
Substance / Mixture

: Substance
Substance name

: Ethanol

CAS-No.

: 64-17-5

Components
Chemical name CAS-No. Concentration (% w/w)
Ethanol 64-17-5 >= 90 - <= 100
Actual concentration is withheld as a trade secret

SECTION 4. FIRST AID MEASURES
General advice

: Remove/ Take off immediately all contaminated clothing.
Get medical advice/ attention if you feel unwell.
Show this safety data sheet to the doctor in attendance.

If inhaled

: If inhaled, remove to fresh air.
If symptoms persist, call a physician.

In case of skin contact

: In case of contact, immediately flush skin with soap and plenty
of water.

In case of eye contact

: Rinse immediately with plenty of water, also under the eyelids,
for at least 15 minutes.
If easy to do, remove contact lens, if worn.
If eye irritation persists, consult a specialist.

SAFETY DATA SHEET

Ethanol 99% Page 3

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

If swallowed

: Immediately give large quantities of water to drink.
If symptoms persist, call a physician.

Most important symptoms
and effects, both acute and
delayed

: The possible risks known are those derived from the labelling
(see section 2).

Notes to physician

: Treat symptomatically.
SECTION 5. FIREFIGHTING MEASURES
Suitable extinguishing media

: Use water spray, alcohol-resistant foam, dry chemical or
carbon dioxide.

Unsuitable extinguishing
media

: High volume water jet

Specific hazards during
firefighting

: In case of fire hazardous decomposition products may be
produced such as:
Flammable gases/vapours
Carbon monoxide
Carbon dioxide (CO2)
Combustion gases of organic materials must in principle be
graded as inhalation poisons.

Further information : Wear suitable protective equipment.
Evacuate endangered area, seal off area.

SECTION 6. ACCIDENTAL RELEASE MEASURES
Personal precautions,
protective equipment and
emergency procedures

: Use personal protective equipment.
Remove all sources of ignition.
Ensure adequate ventilation.

Environmental precautions

: Do not flush into surface water or sanitary sewer system.

Methods and materials for
containment and cleaning up

: Soak up with inert absorbent material (e.g. sand, silica gel,
acid binder, universal binder, sawdust).
Dispose of absorbed material in accordance with the
regulations.
Ventilate the area.

SECTION 7. HANDLING AND STORAGE
Advice on protection against
fire and explosion

: Vapours may form explosive mixtures with air.
Keep away from heat and sources of ignition.
Take precautionary measures against static discharges.
Use only explosion-proof equipment.
Vapours are heavier than air and may spread along floors.

SAFETY DATA SHEET

Ethanol 99% Page 4

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

When transferring from one container to another apply
earthing measures and use conductive hose material.

Advice on safe handling

: Avoid inhalation, ingestion and contact with skin and eyes.
Provide adequate ventilation.

Conditions for safe storage

: Keep containers tightly closed in a cool, well-ventilated place.
Keep away from heat and sources of ignition.

Further information on
storage conditions

: Keep containers tightly closed in a cool, well-ventilated place.
Handle and open container with care.

Materials to avoid

: Keep away from oxidizing agents.

Further information on
storage stability

: no data available
SECTION 8. EXPOSURE CONTROLS/PERSONAL PROTECTION
Components with workplace control parameters
Components CAS-No. Value type
(Form of
exposure)
Control
parameters /
Permissible
concentration
Basis
Ethanol 64-17-5 STEL 1,000 ppm ACGIH
TWA 1,000 ppm
1,900 mg/m3
NIOSH REL
TWA 1,000 ppm
1,900 mg/m3
OSHA Z-1
TWA 1,000 ppm
1,900 mg/m3
OSHA P0
Personal protective equipment
Respiratory protection

: Breathing apparatus needed only when aerosol or mist is
formed.
Filter A (organic gases and vapours) to standard DIN EN 141

Hand protection
Remarks : Protective gloves

Material : butyl-rubber
Break through time : > 480 min
Glove thickness : 0.7 mm
The choice of an appropriate glove does not only depend on
its material but also on other quality features and is different
from one producer to the other. Take note of the information
given by the producer concerning permeability and break
through times, and of special workplace conditions
(mechanical strain, duration of contact).

Eye protection

: Safety glasses with side-shields

SAFETY DATA SHEET

Ethanol 99% Page 5

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

Skin and body protection

: Choose body protection according to the amount and
concentration of the dangerous substance at the work place.
Flame retardant antistatic protective clothing.

Protective measures

: Avoid contact with the skin and the eyes.
Do not breathe vapours, aerosols.
Follow the skin protection plan.
Wash face, hands and any exposed skin thoroughly after
handling.

Hygiene measures

: Take off immediately all contaminated clothing.
Preventive skin protection (protective ointment for the skin)
Wash hands before breaks and at the end of workday.

SECTION 9. PHYSICAL AND CHEMICAL PROPERTIES
Appearance

: liquid

Colour

: colourless

Odour

: alcohol-like

pH

: 7.0 (68 °F / 20 °C)
Concentration: 10 g/l

Melting point

: ca. -175 °F / -115 °C

Boiling point

: ca. 172 °F / 78 °C

Flash point

: ca. 54 °F / 12 °C

Upper explosion limit / upper
flammability limit

: 19 %(V)

Lower explosion limit / Lower
flammability limit

: 3.4 %(V)

Relative density

: 0.793 (68 °F / 20 °C)

Density

: 0.789 g/cm3 (68 °F / 20 °C)

Solubility(ies)
Water solubility

: completely miscible (68 °F / 20 °C)

Partition coefficient: n-
octanol/water

: log Pow: ca. -0.32

SAFETY DATA SHEET

Ethanol 99% Page 6

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

Auto-ignition temperature

: ca. 797 °F / 425 °C

Viscosity
Viscosity, dynamic

: ca. 1.2 mPa.s (68 °F / 20 °C)

Molecular weight

: 46.07 g/mol

SECTION 10. STABILITY AND REACTIVITY
Reactivity

: See section 10.3. "Possibility of hazardous reactions"

Chemical stability

: Stable under normal conditions.

Possibility of hazardous
reactions

: Reactions with strong oxidising agents.
Reactions with alkali metals.
Reactions with earth alkali metals.
Reaction with Sulfuric acid
Reaction with nitric acid.
Aluminium

Conditions to avoid

: Keep away from heat.
Keep away from open flames, hot surfaces and sources of
ignition.

Incompatible materials

: Strong oxidizing agents

Hazardous decomposition
products
: Carbon monoxide and carbon dioxide

SECTION 11. TOXICOLOGICAL INFORMATION
Acute toxicity
Components:
Ethanol:
Acute oral toxicity

: LD50 (Rat, male and female): 10,470 mg/kg
Method: OECD Test Guideline 401
GLP: no

Acute inhalation toxicity

: LC50 (Rat, male and female): 124.7 mg/l
Exposure time: 4 h
Test atmosphere: vapour
Method: OECD Test Guideline 403
GLP: no

Acute dermal toxicity

: LD50 (Rabbit): > 2,000 mg/kg
Method: OECD Test Guideline 402
Assessment: The substance or mixture has no acute dermal
toxicity

SAFETY DATA SHEET

Ethanol 99% Page 7

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

Skin corrosion/irritation
Product:
Method: OECD Test Guideline 404
Result: No skin irritation

Components:
Ethanol:
Species: Rabbit
Exposure time: 24 h
Method: OECD Test Guideline 404
Result: No skin irritation
GLP: yes

Serious eye damage/eye irritation
Product:
Result: irritating

Components:
Ethanol:
Species: Rabbit
Result: Irritating to eyes.
Method: OECD Test Guideline 405
GLP: No information available.

Respiratory or skin sensitisation
Product:
Method: OECD Test Guideline 406
Result: non-sensitizing

Components:
Ethanol:
Exposure routes: Dermal
Species: Mouse
Method: Other
Result: Not a skin sensitizer.
GLP: No information available.

Germ cell mutagenicity
Components:
Ethanol:
Genotoxicity in vitro

: Test Type: Ames test
Test system: Salmonella typhimurium
Metabolic activation: with and without metabolic activation
Method: OECD Test Guideline 471

SAFETY DATA SHEET

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Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

Result: negative
GLP: No information available.

Test Type: In vitro mammalian cell gene mutation test
Test system: mouse lymphoma cells
Metabolic activation: with and without metabolic activation
Method: OECD Test Guideline 476
Result: negative
GLP: No information available.

Test Type: Chromosome aberration test in vitro
Test system: Human lymphocytes
Method: OECD Test Guideline 473
Result: negative
GLP: No information available.

Genotoxicity in vivo

: Test Type: In vivo micronucleus test
Species: Rat (male)
Strain: Other
Cell type: Bone marrow
Application Route: Drinking water
Method: OECD Test Guideline 474
Result: negative
GLP: No information available.

Germ cell mutagenicity -
Assessment

: It is concluded that the product is not mutagenic based on
evaluation of several mutagenicity tests.

Carcinogenicity
Components:
Ethanol:
Species: Mouse, (female)
Application Route: Drinking water
Exposure time: 105 weeks
Dose: 0, 2.5 and 5% in drinking wate
Group: yes
4,400 mg/kg bw/day
Method: OPPTS 870.4200
GLP: yes

Carcinogenicity -
Assessment

: Not classifiable as a human carcinogen.

IARC

Group 1: Carcinogenic to humans

Ethanol

64-17-5

OSHA

No component of this product present at levels greater than or
equal to 0.1% is on OSHA’s list of regulated carcinogens.

NTP

No component of this product present at levels greater than or
equal to 0.1% is identified as a known or anticipated carcinogen

SAFETY DATA SHEET

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Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

by NTP.

Reproductive toxicity
Components:
Ethanol:
Effects on fertility

: Test Type: Two-generation study
Species: Mouse, male and female
Strain: CD1
Application Route: Drinking water
Dose: 5, 10 and 15% v/v in water
Duration of Single Treatment: 126 d
General Toxicity - Parent: NOAEL: 15 %
General Toxicity F1: NOAEL: 10 %
General Toxicity F2: NOAEL: < 15 %
Method: OECD Test Guideline 416
GLP: No information available.

Effects on foetal
development

: Test Type: Pre-natal
Species: Rat, female
Strain: Sprague-Dawley
Application Route: Inhalation
Dose: 10000, 16000, 20000 ppm nom.
Duration of Single Treatment: 19 d
Frequency of Treatment: 1 daily
General Toxicity Maternal: NOAEL: 16,000 ppm
Teratogenicity: NOAEL: 20,000 ppm
Method: OECD Test Guideline 414
GLP: No information available.

Reproductive toxicity -
Assessment

: No reproductive toxicity to be expected.
No teratogenic effects to be expected.

STOT - single exposure
Components:
Ethanol:
Assessment: The substance or mixture is not classified as specific target organ toxicant, single
exposure.

STOT - repeated exposure
Components:
Ethanol:
Remarks: no data available

SAFETY DATA SHEET

Ethanol 99% Page 10

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

Repeated dose toxicity
Components:
Ethanol:
Species: Rat, male and female
LOAEL: ca. 3200 mg/kg
Application Route: oral (gavage)
Exposure time: 7 weeks or 14 weeks
Number of exposures: twice daily, 7 days a week
Dose: 5, 10, 20 ml/kg
Group: yes
Method: OECD Test Guideline 408
GLP: No information available.

Species: Rat, male
NOEL: > 20 mg/l
Application Route: inhalation (vapour)
Exposure time: 3, 6, 9, 26 day groups
Number of exposures: continuous
Dose: >20 mg/l
Group: yes
Method: Other
GLP: No information available.

Aspiration toxicity
Components:
Ethanol:
No aspiration toxicity classification

SECTION 12. ECOLOGICAL INFORMATION
Ecotoxicity
Components:
Ethanol:
Toxicity to fish

: LC50 (Pimephales promelas (fathead minnow)): 15,300 mg/l
End point: mortality
Exposure time: 96 h
Test Type: flow-through test
Analytical monitoring: yes
Method: Other
GLP: No information available.

LC50 (Oncorhynchus mykiss (rainbow trout)): 11,200 mg/l
End point: mortality
Exposure time: 24 h
Test Type: flow-through test
Analytical monitoring: no
Method: Other
GLP: No information available.

SAFETY DATA SHEET

Ethanol 99% Page 11

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

Toxicity to daphnia and other
aquatic invertebrates

: LC50 (Ceriodaphnia dubia (water flea)): 5,012 mg/l
End point: mortality
Exposure time: 48 h
Test Type: static test
Analytical monitoring: no
Method: Other
GLP: No information available.

EC50 (Daphnia magna (Water flea)): > 10,000 mg/l
End point: Immobilization
Exposure time: 48 h
Method: DIN 38412
GLP: no

Toxicity to algae/aquatic
plants

: EC50 (Chlorella vulgaris (Fresh water algae)): 275 mg/l
Exposure time: 72 h
Test Type: static test
Method: OECD Test Guideline 201

EC10 (Chlorella vulgaris (Fresh water algae)): 11.5 mg/l
Exposure time: 72 h
Test Type: static test
Method: OECD Test Guideline 201

Toxicity to fish (Chronic
toxicity)

: NOEC (Danio rerio (zebra fish)): 250 mg/l
End point: Other
Exposure time: 120 h
Test Type: semi-static test
Method: OECD Test Guideline 212
GLP: No information available.

Toxicity to daphnia and other
aquatic invertebrates
(Chronic toxicity)

: Remarks: no data available

Toxicity to microorganisms

: EC50 (Natural microorganism): 5,800 mg/l
Exposure time: 4 h
Test Type: static test

Toxicity to soil dwelling
organisms

: Remarks: Not applicable

Plant toxicity

: Remarks: Not applicable

Sediment toxicity

: Remarks: Not applicable

Toxicity to terrestrial
organisms

: Remarks: Not applicable

SAFETY DATA SHEET

Ethanol 99% Page 12

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

Persistence and degradability
Components:
Ethanol:
Biodegradability

: aerobic
Result: Readily biodegradable.
Biodegradation: 84 %
Exposure time: 20 d

Bioaccumulative potential
Components:
Ethanol:
Bioaccumulation

: Bioconcentration factor (BCF): 0.66
Method: calculated
Remarks: Does not bioaccumulate.

Partition coefficient: n-
octanol/water

: log Pow: -0.35 (75 °F / 24 °C)
pH: 7.4
Method: OECD Test Guideline 107

Mobility in soil
Components:
Ethanol:
Distribution among
environmental compartments

: adsorption
Medium: water - soil
Remarks: Not expected to adsorb on soil.

Other adverse effects
Components:
Ethanol:
Results of PBT and vPvB
assessment

: This substance is not considered to be persistent,
bioaccumulating and toxic (PBT).

Additional ecological
information

: The product should not be allowed to enter drains, water
courses or the soil.

SECTION 13. DISPOSAL CONSIDERATIONS
Disposal methods
Waste from residues : Product should be taken to a suitable and authorized waste
disposal site in accordance with relevant regulations and if
necessary after consultation with the waste disposal operator
and/or the competent Authorities

Contaminated packaging

: Packaging that cannot be cleaned should be disposed of as
product waste

SAFETY DATA SHEET

Ethanol 99% Page 13

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

SECTION 14. TRANSPORT INFORMATION

DOT Regulation:
UN/NA-number: UN 1170
Proper shipping name: Ethanol solutions

Primary hazard class: 3
Packing group: II
Emergency Response
Guide:
127

IATA
UN/ID number: UN 1170
Proper shipping name: Ethanol solution

Primary risk: 3
Packing group: II
Remarks: Shipment permitted
IMDG
UN no.: UN 1170
Proper shipping name: Ethanol solution

Primary risk: 3
Packing group: II
EmS: F-E S-D

SECTION 15. REGULATORY INFORMATION
CERCLA Reportable Quantity
This material does not contain any components with a CERCLA RQ.
SARA 304 Extremely Hazardous Substances Reportable Quantity
This material does not contain any components with a section 304 EHS RQ.
SARA 302 Extremely Hazardous Substances Threshold Planning Quantity
This material does not contain any components with a section 302 EHS TPQ.
SARA 311/312 Hazards

: Flammable (gases, aerosols, liquids, or solids)
Serious eye damage or eye irritation

SARA 313

: This material does not contain any chemical components with
known CAS numbers that exceed the threshold (De Minimis)
reporting levels established by SARA Title III, Section 313.

US State Regulations
Massachusetts Right To Know
Ethanol 64-17-5
Pennsylvania Right To Know

SAFETY DATA SHEET

Ethanol 99% Page 14

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

Ethanol 64-17-5
Pennsylvania Right To Know
Ethanol 64-17-5
Maine Chemicals of High Concern
Product does not contain any listed chemicals
Vermont Chemicals of High Concern
Product does not contain any listed chemicals
Washington Chemicals of High Concern
Product does not contain any listed chemicals
New Jersey Right To Know
Ethanol 64-17-5
California Prop. 65
WARNING: This product can expose you to chemicals including Ethanol, which is/are known to
the State of California to cause cancer and birth defects or other reproductive harm. For more
information go to www.P65Warnings.ca.gov.
California Permissible Exposure Limits for Chemical Contaminants
Ethanol 64-17-5
The components of this product are reported in the following inventories:
TSCA

: All chemical substances in this product are either listed on the
TSCA Inventory or are in compliance with a TSCA Inventory
exemption., All components are compliant with the TSCA
Inventory Notification (Active) rule.

TSCA list
TSCA - 5(a) Significant New Use Rule List of Chemicals: No substances are subject to a
Significant New Use Rule.

US. Toxic Substances Control Act (TSCA) Section 12(b) Export Notification (40 CFR 707, Subpt
D): No substances are subject to TSCA 12(b) export notification requirements.

SECTION 16. OTHER INFORMATION
Further information

SAFETY DATA SHEET

Ethanol 99% Page 15

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

NFPA 704:

Full text of other abbreviations
ACGIH : USA. ACGIH Threshold Limit Values (TLV)
NIOSH REL : USA. NIOSH Recommended Exposure Limits
OSHA P0 : USA. OSHA - TABLE Z-1 Limits for Air Contaminants -
1910.1000
OSHA Z-1 : USA. Occupational Exposure Limits (OSHA) - Table Z-1
Limits for Air Contaminants
ACGIH / STEL : Short-term exposure limit
NIOSH REL / TWA : Time-weighted average concentration for up to a 10-hour
workday during a 40-hour workweek
OSHA P0 / TWA : 8-hour time weighted average
OSHA Z-1 / TWA : 8-hour time weighted average

AIIC - Australian Inventory of Industrial Chemicals; ASTM - American Society for the Testing of
Materials; bw - Body weight; CERCLA - Comprehensive Environmental Response,
Compensation, and Liability Act; CMR - Carcinogen, Mutagen or Reproductive Toxicant; DIN -
Standard of the German Institute for Standardisation; DOT - Department of Transportation; DSL -
Domestic Substances List (Canada); ECx - Concentration associated with x% response; EHS -
Extremely Hazardous Substance; ELx - Loading rate associated with x% response; EmS -
Emergency Schedule; ENCS - Existing and New Chemical Substances (Japan); ErCx -
Concentration associated with x% growth rate response; ERG - Emergency Response Guide;
GHS - Globally Harmonized System; GLP - Good Laboratory Practice; HMIS - Hazardous
Materials Identification System; IARC - International Agency for Research on Cancer; IATA -
International Air Transport Association; IBC - International Code for the Construction and
Equipment of Ships carrying Dangerous Chemicals in Bulk; IC50 - Half maximal inhibitory
concentration; ICAO - International Civil Aviation Organization; IECSC - Inventory of Existing
Chemical Substances in China; IMDG - International Maritime Dangerous Goods; IMO -
International Maritime Organization; ISHL - Industrial Safety and Health Law (Japan); ISO -
International Organisation for Standardization; KECI - Korea Existing Chemicals Inventory; LC50
- Lethal Concentration to 50 % of a test population; LD50 - Lethal Dose to 50% of a test
population (Median Lethal Dose); MARPOL - International Convention for the Prevention of
Pollution from Ships; MSHA - Mine Safety and Health Administration; n.o.s. - Not Otherwise
Specified; NFPA - National Fire Protection Association; NO(A)EC - No Observed (Adverse) Effect
2
3
0

Flammability

Instability
Special hazard

Health

SAFETY DATA SHEET

Ethanol 99% Page 16

Substance key: 000000662972 Revision Date: 03/09/2021
Version : 1 - 0 / USA Date of printing :07/29/2021

Concentration; NO(A)EL - No Observed (Adverse) Effect Level; NOELR - No Observable Effect
Loading Rate; NTP - National Toxicology Program; NZIoC - New Zealand Inventory of Chemicals;
OECD - Organization for Economic Co-operation and Development; OPPTS - Office of Chemical
Safety and Pollution Prevention; PBT - Persistent, Bioaccumulative and Toxic substance; PICCS
- Philippines Inventory of Chemicals and Chemical Substances; (Q)SAR - (Quantitative) Structure
Activity Relationship; RCRA - Resource Conservation and Recovery Act; REACH - Regulation
(EC) No 1907/2006 of the European Parliament and of the Council concerning the Registration,
Evaluation, Authorisation and Restriction of Chemicals; RQ - Reportable Quantity; SADT - Self-
Accelerating Decomposition Temperature; SARA - Superfund Amendments and Reauthorization
Act; SDS - Safety Data Sheet; TCSI - Taiwan Chemical Substance Inventory; TSCA - Toxic
Substances Control Act (United States); UN - United Nations; UNRTDG - United Nations
Recommendations on the Transport of Dangerous Goods; vPvB - Very Persistent and Very
Bioaccumulative

Revision Date : 03/09/2021

This information corresponds to the present state of our knowledge and is intended as a general
description of our products and their possible applications. Clariant makes no warranties, express
or implied, as to the information’s accuracy, adequacy, sufficiency or freedom from defect and
assumes no liability in connection with any use of this information. Any user of this product is
responsible for determining the suitability of Clariant's products for its particular application. NO
EXPRESS OR IMPLIED WARRANTY IS MADE OF THE MERCHANTABILITY, SUITABILITY,
FITNESS FOR A PARTICULAR PURPOSE OR OTHERWISE OF ANY PRODUCT OR
SERVICE. Nothing included in this information waives any of Clariant’s General Terms and
Conditions of Sale, which control unless it agrees otherwise in writing. Any existing
intellectual/industrial property rights must be observed. Due to possible changes in our products
and applicable national and international regulations and laws, the status of our products could
change. Material Safety Data Sheets providing safety precautions, that should be observed when
handling or storing Clariant products, are available upon request and are provided in compliance
with applicable law. You should obtain and review the applicable Material Safety Data Sheet
information before handling any of these products. For additional information, please contact
Clariant.

US / EN

Univar USA Inc Safety Data Sheet

SDS No:
Version No:
Order No:

3075 Highland Pkwy, Ste 200, Downers Grove, IL 60515
[phone]

Emergency Assistance
For emergency assistance involving chemicals call
Chemtrec - [phone]
SAFETY DATA SHEET

1. Identification

Product identifier: GLYCOL ETHER EB ACETATE
Other means of identification
SDS number: 000100000493
Recommended use and restriction on use
Recommended use: Not available.
Restrictions on use: Not known.
Emergency telephone number:For emergency assistance Involving chemicals
call CHEMTREC day or night at: 1-800-424-9300. CHEMTREC INTERNATIONAL Tel# [phone]
2. Hazard(s) identification

Hazard classification
Physical hazards
Flammable liquids Category 4
Health hazards
Acute toxicity (Dermal) Category 4

Hazard symbol

Signal word Warning

Label elements
Univar
3075 Highland Pkwy STE 200
Downers Grove, IL 60515
425-889-3400
UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:
Version: 1.0
Revision date: 05/19/2015

SDS_US - 000100000493 2/11

Hazard statement Combustible liquid.
Causes eye irritation.
Harmful in contact with skin.
May be harmful if swallowed.

Precautionary statement

Prevention Wear protective gloves/protective clothing/eye protection/face protection.

Response IF ON SKIN: Wash with plenty of water. Call a POISON CENTER/doctor if you
feel unwell. Specific measures (see this label). Wash contaminated clothing
before reuse. In case of fire: Use … to extinguish.

Storage Store in a closed container. Keep container tightly closed. Store in well-
ventilated place.

Disposal Dispose of contents/container to an appropriate treatment and disposal
facility in accordance with applicable laws and regulations, and product
characteristics at time of disposal.
Other hazards which do not
result in GHS classification
None.

3. Composition/information on ingredients

Substances
Chemical identity Common name
and synonyms CAS number Content in percent (%)*
2-Butoxyethyl acetate 112-07-2 100%
* All concentrations are percent by weight unless ingredient is a gas. Gas concentrations are in percent by volume.
Composition comments: The components are not hazardous or are below required disclosure
UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:
Version: 1.0
Revision date: 05/19/2015

SDS_US - 000100000493 3/11

limits.

4. First-aid measures
Ingestion: Do NOT induce vomiting. Never give liquid to an unconscious person. Get
medical attention.
Inhalation: Move to fresh air. If breathing is difficult, give oxygen. Perform artificial
respiration if breathing has stopped.
Skin contact: Immediately flush with plenty of water for at least 15 minutes while
removing contaminated clothing and shoes.
Eye contact: If in eyes, hold eyes open, flood with water for at least 15 minutes and see
a doctor.
Most important symptoms/effects, acute and delayed
Symptoms: No data available.

Indication of immediate medical attention and special treatment needed
Treatment: No data available.
5. Fire-fighting measures

General fire hazards: No data available.
Suitable (and unsuitable) extinguishing media

Suitable extinguishing
media:
Use: Water spray, fog, CO2, dry chemical, or alcohol resistant foam.
Unsuitable extinguishing
media:
No data available.
Specific hazards arising from the
chemical:
No data available.
Special protective equipment and precautions for firefighters
Special fire fighting
procedures:
No data available.
Special protective equipment for
fire-fighters:
No data available.
6. Accidental release measures
UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:
Version: 1.0
Revision date: 05/19/2015

SDS_US - 000100000493 4/11

Personal precautions, protective
equipment and emergency
procedures:

No data available.
Methods and material for
containment and cleaning up:
All equipment used when handling the product must be grounded.
Eliminate sources of ignition. Absorb spillage with non-combustible,
absorbent material. Dike for later disposal.
7. Handling and storage

Precautions for safe handling:

Keep away from heat, sparks and open flame. Avoid contact with eyes,
skin, and clothing. Avoid breathing mists or vapors. Use only with
adequate ventilation.
Conditions for safe storage,
including any
incompatibilities:
No data available.
8. Exposure controls/personal protection

Control parameters
Occupational exposure limits
Chemical identity Type Exposure Limit values Source
2-Butoxyethyl acetate TWA 20 ppm US. ACGIH Threshold Limit Values (03
2013)
REL 5 ppm 33 mg/m3 US. NIOSH: Pocket Guide to Chemical
Hazards (2010)
ST ESL 310
µg/m3
US. Texas. Effects Screening Levels
(Texas Commission on Environmental
Quality) (02 2013)
AN ESL 31 µg/m3 US. Texas. Effects Screening Levels
(Texas Commission on Environmental
Quality) (02 2013)
ST ESL 50 ppb US. Texas. Effects Screening Levels
(Texas Commission on Environmental
Quality) (02 2013)
AN ESL 5 ppb US. Texas. Effects Screening Levels
(Texas Commission on Environmental
Quality) (02 2013)
Appropriate engineering
controls
No data available.
UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:
Version: 1.0
Revision date: 05/19/2015

SDS_US - 000100000493 5/11

Individual protection measures, such as personal protective equipment
General information: No data available.
Eye/face protection: No data available.
Skin protection
Hand protection: No data available.
Other: No data available.
Respiratory protection: No data available.
Hygiene measures: No data available.
9. Physical and chemical properties

Physical state: Liquid
Form: No data available.
Color: No data available.
Odor: No data available.
Odor threshold: No data available.
pH: No data available.
Melting point/freezing point: -64.6 °C
Initial boiling point and boiling range: 186 °C
Flash Point: 71 °C
Evaporation rate: No data available.
Flammability (solid, gas): No data available.
Upper/lower limit on flammability or explosive limits
Flammability limit - upper (%): No data available.
Flammability limit - lower (%): No data available.
Explosive limit - upper (%): No data available.
Explosive limit - lower (%): No data available.
Vapor pressure: No data available.
Vapor density: No data available.
Relative density: No data available.
Solubility(ies)
Solubility in water: No data available.
Solubility (other): No data available.
Partition coefficient (n-octanol/water): No data available.
UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:
Version: 1.0
Revision date: 05/19/2015

SDS_US - 000100000493 6/11

Auto-ignition temperature: No data available.
Decomposition temperature: No data available.
Viscosity: No data available.

10. Stability and reactivity

Reactivity: No data available.
Chemical stability: No data available.
Possibility of hazardous
reactions: No data available.
Conditions to avoid: No data available.
Incompatible materials: No data available.
Hazardous decomposition
products:
No data available.
11. Toxicological information

Symptoms related to the physical, chemical and toxicological characteristics
Ingestion: No data available.
Inhalation: No data available.
Skin contact: No data available.
Eye contact: No data available.
Information on toxicological effects
Acute toxicity (list all possible routes of exposure)
Oral
Product: No data available.
Specified substance(s):
2-Butoxyethyl acetate LD 100 (Rabbit): Approximate 987 mg/kg (, No ) 2 (reliable with restrictions)
Dermal
Product: ATEmix (): 1,580 mg/kg

Inhalation
Product: No data available.
Specified substance(s):
2-Butoxyethyl acetate Inhalation hazard test (IHT) (Rat, ): 3.68 mg/l (, No) 2 (reliable with
restrictions) Inhalation hazard test (IHT) (Rat, ): 3.91 mg/l (, No) 2 (reliable
with restrictions)
Repeated dose toxicity
Product: No data available.
Skin corrosion/irritation
UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:
Version: 1.0
Revision date: 05/19/2015

SDS_US - 000100000493 7/11

Product: No data available.
Serious eye damage/eye irritation
Product: No data available.
Respiratory or skin sensitization
Product: No data available.
Carcinogenicity
Product: No data available.
IARC Monographs on the Evaluation of Carcinogenic Risks to Humans:
No carcinogenic components identified

US. National Toxicology Program (NTP) Report on Carcinogens:
No carcinogenic components identified
US. OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050):
No carcinogenic components identified
Germ cell mutagenicity
In vitro
Product: No data available.
In vivo
Product: No data available.
Reproductive toxicity
Product: No data available.
Specific target organ toxicity - single exposure
Product: No data available.
Specific target organ toxicity - repeated exposure
Product: No data available.
Aspiration hazard
Product: No data available.
Other effects: No data available.

12. Ecological information

Ecotoxicity:
Acute hazards to the aquatic environment:
Fish Product: No data available.
Aquatic invertebrates
Product: No data available.
Chronic hazards to the aquatic environment:
Fish
Product: No data available.
UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:
Version: 1.0
Revision date: 05/19/2015

SDS_US - 000100000493 8/11

Aquatic invertebrates
Product: No data available.
Toxicity to Aquatic Plants
Product: No data available.
Persistence and degradability
Biodegradation
Product: No data available.
BOD/COD ratio
Product: No data available.
Bioaccumulative potential
Bioconcentration factor (BCF)
Product: No data available.
Partition coefficient n-octanol / water (log Kow)
Product: No data available.
Mobility in soil: No data available.
Known or predicted distribution to environmental compartments
2-Butoxyethyl acetate No data available.

13. Disposal considerations

Disposal instructions: No data available.
Contaminated packaging: No data available.
14. Transport information
DOT
UN number: NA 1993
UN proper shipping name: Combustible liquid, n.o.s.
Transport hazard class(es)
Class: CBL
Label(s): NONE
Packing group: III
Marine Pollutant: Not regulated.
Special precautions for user: –
NOT D.O.T. REGULATED FOR DOMESTIC GROUND TRANSPORTATION IN NON BULK CONTAINERSNot regulated for US domestic
ground transportation.
15. Regulatory information

UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:
Version: 1.0
Revision date: 05/19/2015

SDS_US - 000100000493 9/11

US federal regulationsUS. OSHA Specifically Regulated Substances (29 CFR 1910.1001-1050)
None present or none present in regulated quantities.
CERCLA Hazardous Substance List (40 CFR 302.4):
Superfund amendments and reauthorization act of 1986 (SARA)
Hazard categories
Not listed.
SARA 302 Extremely hazardous substance
None present or none present in regulated quantities.
SARA 304 Emergency release notification
Chemical identity RQ
2-Butoxyethyl acetate
SARA 311/312 Hazardous chemical
Chemical identity Threshold Planning Quantity
2-Butoxyethyl acetate 500 lbs
SARA 313 (TRI reporting)
Chemical identity
Reporting
threshold for
other users
Reporting threshold for
manufacturing and processing
2-Butoxyethyl acetate 10000 lbs 25000 lbs.
Clean Water Act Section 311 Hazardous Substances (40 CFR 117.3)
None present or none present in regulated quantities.
Clean Air Act (CAA) Section 112(r) Accidental Release Prevention (40 CFR 68.130):
None present or none present in regulated quantities.
US state regulations
US. California Proposition 65
WARNING: This product contains a chemical known to the State of California to cause birth defects or other
reproductive harm.
Ethanol, 2-ethoxy- Developmental toxin.
Ethanol, 2-ethoxy- Male reproductive toxin.
US. New Jersey Worker and Community Right-to-Know Act
2-Butoxyethyl acetate Listed
US. Massachusetts RTK - Substance List
No ingredient regulated by MA Right-to-Know Law present.
US. Pennsylvania RTK - Hazardous Substances
2-Butoxyethyl acetate Listed
US. Rhode Island RTK
2-Butoxyethyl acetate Listed
UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:
Version: 1.0
Revision date: 05/19/2015

SDS_US - 000100000493 10/11

Inventory Status:Australia AICS: Not in compliance with the inventory.
Canada DSL Inventory List: Not in compliance with the inventory.
EU EINECS List: On or in compliance with the inventory
EU ELINCS List: Not in compliance with the inventory.
Japan (ENCS) List: Not in compliance with the inventory.
EU No Longer Polymers List: Not in compliance with the inventory.
China Inv. Existing Chemical Substances: Not in compliance with the inventory.
Korea Existing Chemicals Inv. (KECI): Not in compliance with the inventory.
Canada NDSL Inventory: Not in compliance with the inventory.
Philippines PICCS: Not in compliance with the inventory.
US TSCA Inventory: On or in compliance with the inventory
New Zealand Inventory of Chemicals: Not in compliance with the inventory.
Japan ISHL Listing: Not in compliance with the inventory.
Japan Pharmacopoeia Listing: Not in compliance with the inventory.
16.Other information, including date of preparation or last revision
HMIS Hazard ID
Health * 1
Flammability 2
Physical hazards 0
PERSONAL PROTECTION B
Hazard rating: 0 - Minimal; 1 - Slight; 2 - Moderate; 3 - Serious; 4 - Severe; *Chronic health
effect
NFPA Hazard ID

Flammability
Health
Reactivity
Special hazard.
Hazard rating: 0 - Minimal; 1 - Slight; 2 - Moderate; 3 - Serious; 4 - Severe
Issue date: 05/19/2015
Revision date: No data available.
Version #: 1.0
Further information: No data available.

2
0

1

B - Safety Glasses & Gloves
UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:
Version: 1.0
Revision date: 05/19/2015

SDS_US - 000100000493 11/11

UNIVAR USA INC.SDS NO:10000493
ISSUE DATE:2015-05-19 VERSION:001 2015-05-19
Annotation:

Univar USA Inc Safety Data Sheet
For Additional Information contact SDS Coordinator during business hours, Pacific time: [phone]

Notice
Univar USA Inc. (”Univar”) expressly disclaims all express or implied warranties of merchantability and fitness for
a particular purpose, with respect to the product or information provided herein, and shall under no
circumstances be liable for incidental or consequential damages.
Do not use ingredient information and/or ingredient percentages in this SDS as a product specification. For
product specification information refer to a product specification sheet and/or a certificate of analysis. These
can be obtained from your local Univar sales office.

All information appearing herein is based upon data obtained from the manufacturer and/or recognized
technical sources. While the information is believed to be accurate, Univar makes no representations as to its
accuracy or sufficiency. Conditions of use are beyond Univar's control and therefore users are responsible to
verify this data under their own operating conditions to determine whether the product is suitable for their
particular purposes and they assume all risks of their use, handling, and disposal of the product, or from the
publication or use of, or reliance upon, information contained herein.

This information relates only to the product designated herein, and does not relate to its use in combination
with any other material or in any other process
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1. IDENTIFICATION OF THE SUBSTANCE/MIXTURE AND OF THE COMPANY/UNDERTAKING

Trade name : SDA3C/200PF/IPA/140500
CAS Number: : 64-17-5
Chemical characterization : Ethyl Alcohol
Chemical name : Ethyl Alcohol
Synonyms : 200 Proof Ethyl Alcohol, Anhydrous, Denatured Ethanol

Identified uses : For excipient use only; Manufacture of pharmaceutical
mixtures; Other consumer uses

Prohibited uses : Active pharmaceutical ingredient (API); Beverages; Tobacco;
Cannabis Applications; Use in Injectables in Pharmaceuticals
Applications; Direct Food additives

Company Address Company Telephone
Equistar Chemicals, LP
LyondellBasell Tower, Suite 300
1221 McKinney St.
P.O. Box 2583
Houston Texas 77252-2583

Customer Service 888 777-0232
[e-mail]

Emergency telephone number
CHEMTREC USA 800-424-9300
EQUISTAR 800-245-4532

E-mail address
Responsible/issuing person
: [e-mail]

2. HAZARDS IDENTIFICATION
GHS Classification
Flammable liquids Category 2
Eye irritation Category 2A
Specific target organ toxicity - single exposure Category 3

Label elements
Hazard symbols :

Signal word : Danger

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Hazard Statements : H225 Highly flammable liquid and vapour.
H319 Causes serious eye irritation.
H335 + H336 May cause respiratory irritation, and
drowsiness or dizziness.

Precautionary
Statements
: Prevention
P210 Keep away from heat/sparks/open flames/hot surfaces.
No smoking.
P233 Keep container tightly closed.
P240 Ground and bond container and receiving equipment.
P241 Use explosion-proof electrical/ ventilating/ lighting
equipment.
P242 Use non-sparking tools.
P243 Take action to prevent static discharges.
P280 Wear protective gloves/ protective clothing.
P264 Wash skin thoroughly after handling.
P261 Avoid breathing vapours.
P271 Use only outdoors or in a well-ventilated area.

Response
P370 + P378 In case of fire: Use alcohol-resistant foam,
carbon dioxide or dry sand for extinction.
P303 + P361 + P353 IF ON SKIN (or hair): Take off
immediately all contaminated clothing. Rinse skin with water
or shower.
P305 + P351 + P338 IF IN EYES: Rinse cautiously with
water for several minutes. Remove contact lenses, if present
and easy to do. Continue rinsing.
P337 + P313 If eye irritation persists: Get medical advice/
attention.
P304 + P340 IF INHALED: Remove victim to fresh air and
keep at rest in a position comfortable for breathing.
P312 Call a POISON CENTER/doctor if you feel unwell.

Storage
P403 + P235 Store in a well-ventilated place. Keep cool.
P405 Store locked up.

Disposal
P501 Dispose of contents/ container to an approved waste
disposal plant.

Other hazards
Hazards Not Otherwise Classified (HNOC)
Prolonged or repeated contact may cause skin to become dry or cracked.

3. COMPOSITION/INFORMATION ON INGREDIENTS
Mixtures
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Components
Chemical name CAS-No. Weight %

Ethyl alcohol 64-17-5 95.3 %
Isopropyl Alcohol 67-63-0 4.7 %

4. FIRST AID MEASURES
General advice : Consult a physician/doctor if necessary.
Take proper precautions to ensure your own health and safety
before attempting rescue and providing first aid.
Show this material safety data sheet to the doctor in
attendance.
Do not leave the victim unattended.

If inhaled : Remove person to fresh air. If signs/symptoms continue, get
medical attention.
Give oxygen or artificial respiration as needed.

In case of skin contact : Immediately flush affected area with plenty of water while
removing contaminated clothing. Wash contaminated clothing
before reuse. If irritation persists, get medical attention.

In case of eye contact : Thoroughly flush the eyes with large amounts of clean low-
pressure water for at least 15 minutes, occasionally lifting the
upper and lower eyelids. If irritation persists, seek medical
attention.
Remove contact lenses.
Do not use eye ointment unless directed to by a physician.

If swallowed : Do not induce vomiting. Risk of damage to lungs exceeds
poisoning risk.
Drink plenty of water.
If vomiting does occur, have victim lean forward to reduce risk
of aspiration.
If victim is drowsy or unconscious, place on the left side with
head down.
Never give anything by mouth to an unconscious person.
Obtain emergency room treatment immediately.

Notes to physician
Symptoms : Ingestion of the liquid or exposure to high airborne
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concentrations can cause central nervous system (CNS) effects
ranging from excitation, dizziness, drowsiness, and headache
to deep anesthesia, respiratory arrest, and death in cases of
severe over-exposure.
Repeated or prolonged contact with skin may cause defatting
and drying of the skin which may result in dermatitis.

Hazards : May be harmful if swallowed and enters airways.
Causes serious eye irritation.
May cause respiratory irritation.
May cause drowsiness or dizziness.

Treatment : Treat symptomatically.
Treatment of overexposure should be directed at the control of
symptoms and the clinical condition of the patient.
There is no specific antidote.
Gastric lavage can be used if done shortly after ingestion. GI
decontamination with charcoal is not effective unless other toxic
co-ingestants are involved.

5. FIRE-FIGHTING MEASURES
Suitable extinguishing media : SMALL FIRE: Use dry chemicals, CO2, water spray or alcohol-
resistant foam
LARGE FIRE: Use water spray, water fog or alcohol-resistant
foam

Specific hazards during fire
fighting
: Extremely flammable well below ambient temperatures.
Vapor forms explosive mixture with air and may cause a flash
fire.
Eliminate all sources of ignition.
Prevent entry into waterways, sewers, basements or confined
areas.
Ethanol vapors are heavier than air and may travel a
considerable distance to a source of ignition and flash back.
Alcohols burn with a pale blue flame which may be extremely
hard to see under normal lighting conditions. Personnel may
only be able to feel the heat of the fire without seeing flames.
Extreme caution must be exercised in fighting alcohol fires.
When exposed to ignition source in air, vapors can burn in
open or explode if confined.
Fight fire from maximum distance or use unmanned hose
holders or monitor nozzles.
Heat may build enough pressure to rupture closed
containers/spreading fire/increasing risk of burns/injuries.
Cool containers with flooding quantities of water until well after
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fire is out.
Withdraw immediately in case of rising sound from venting
safety devices or discoloration of tank.
Always stay away from tanks engulfed in fire.
Move containers from fire area if it can be done without risk.
Prevent fire extinguishing water from contaminating surface
water or the ground water system.
When fighting a fire, notify environmental authorities if liquid
enters sewers or public waters.
Fire residues and contaminated fire extinguishing water must
be disposed of in accordance with local regulations.

Special protective equipment
for fire-fighters
: Wear positive pressure self-contained breathing apparatus
(SCBA).
Structural firefighter’s protective clothing will only provide
limited protection.

6. ACCIDENTAL RELEASE MEASURES
Personal precautions : Clean-up to be performed only by trained and properly
equipped personnel.
Wear recommended personal protective equipment.
Eliminate all sources of ignition.
Ensure adequate ventilation.
Evacuate personnel to safe areas.

Environmental precautions : If necessary, all contaminated waste water must be treated in a
municipal or industrial wastewater treatment plant before
release to surface water.

Chemical removal by air and water pollution control devices
must meet the minimum efficiency requirements needed to
reduce exposures to an acceptable level.
The discharge of treatment plant effluent to rivers and oceans
must achieve the dilution ratio needed to reduce exposures to
an acceptable level.
The size and capacity of wastewater treatment plants must
meet the minimum requirements needed to reduce exposures
to an acceptable level.
Waste management practices such as incineration, recycling,
reuse must be enforced as needed to reduce exposures to an
acceptable level.

External treatment and disposal of waste should comply with
applicable local and/or national regulations.
The maximum allowable site tonnage and the days of use
should be below the number needed to maintain exposures at
an acceptable level.

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Methods for containment /
Methods for cleaning up
: Highly flammable liquid and vapour.
Eliminate all sources of ignition.
All equipment used when handling this product must be
grounded.
Do not touch or walk through spilled material.
Stop leak if you can do it without risk.
Prevent entry into waterways, sewers, basements or confined
areas.
A vapor suppressing foam may be used to reduce vapors.
Absorb or cover with dry earth, sand or other non-combustible
material and transfer to containers.
Use clean non-sparking tools to collect absorbed material.
For large spills:
Contain spill with dike to prevent entry into sewers or
waterways.
Water spray may reduce vapor; but may not prevent ignition in
closed spaces.

7. Handling and storage
Precautions for safe handling
Advice on safe handling : Wear recommended personal protective equipment.
Eliminate all sources of ignition.
Use only in area provided with appropriate exhaust ventilation.
Take necessary action to avoid static electricity discharge
(which might cause ignition of organic vapors).
Use only non-sparking tools.
Avoid contact with incompatible agents.
Open and handle container with care.
Keep in properly labeled containers.
Metal containers involved in the transfer of this material
should be grounded and bonded. Keep containers tightly
closed and in a well-ventilated place. Store away from
oxidizers and other combustible material by a distance of at
least 20 feet. Metal containers used to store this material
should be grounded.
Ensure all equipment is electrically grounded before beginning
transfer operations.
Handle empty containers with care; vapor/residue may be
extremely flammable.
Do not pressurize or expose empty containers to open flame,
sparks, or heat.
Isolate, vent, drain, wash and purge systems or equipment
before maintenance or repair.
Observe precautions pertaining to confined space entry.

Advice on protection against
fire and explosion
: Take precautionary measures against static discharges.
Keep away from heat and sources of ignition.
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Fire-fighting class : Highly flammable liquid and vapour.

Conditions for safe storage, including any incompatibilities
Requirements for storage
areas and containers
: Flammable materials should be stored in a separate safety
storage cabinet or room.
Store only in tightly closed, properly vented containers away
from heat, sparks, open flame and strong oxidizing agents.
Store this product in a dry location where it can be protected
from the elements.
Keep in a well-ventilated place.
Metal containers involved in the transfer of this material
should be grounded and bonded. Keep containers tightly
closed and in a well-ventilated place. Store away from
oxidizers and other combustible material by a distance of at
least 20 feet. Metal containers used to store this material
should be grounded.
Ensure that all relevant regulations regarding explosive
atmosphere, and handling and storage facilities of flammable
products are followed.
Store closed drums with bung in up position.

Specific end use(s)
: See Section 1.

8. EXPOSURE CONTROLS/PERSONAL PROTECTION
Control parameters

Ingredients with workplace control parameters

Occupational Exposure Limits

Components CAS-No. Type Limit Value Basis
Revision Date
Additional
Information
Ethyl alcohol 64-17-5 STEL 1,000 ppm US (ACGIH)
2012

Ethyl alcohol 64-17-5 IDLH

3,300 ppm

NIOSH
September 2007

Remarks: 10% LEL

Ethyl alcohol 64-17-5 TWA

1,000 ppm
1,900 mg/m3

US (OSHA)
June 23, 2006

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Isopropyl Alcohol 67-63-0 STEL 400 ppm US (ACGIH)
2012

Isopropyl Alcohol 67-63-0 TWA 200 ppm US (ACGIH)
2012

Isopropyl Alcohol 67-63-0 IDLH

2,000 ppm

NIOSH
September 2007

Remarks: 10% LEL

Isopropyl Alcohol 67-63-0 TWA

400 ppm
980 mg/m3

US (OSHA)
June 23, 2006

Consult local authorities for acceptable exposure limits.

Biological Exposure Indices

Components CAS-No. Control
parameters
Biological
specimen
Sampling
time
Concentration Basis
Isopropyl
Alcohol
67-63-0 Acetone urine end of shift
at end of
workweek
40 mg/l ACGIH_BEI
S
Remarks: background, nonspecific.

Exposure controls
Engineering measures
General room or local exhaust ventilation is usually required to meet exposure limit(s).
Electrical equipment should be grounded and conform to applicable electrical code.

Personal protective equipment
Respiratory protection : When workers are facing concentrations above the exposure
limit they must use appropriate certified respirators.

Hand protection : Wear chemical resistant gloves such as:
Glove material butyl rubber; material thickness .5mm; break
through time ≥ 480 min. Gloves must be replaced after 8
hours of wear.

Glove material fluoroelastomer; material thickness 0.4 mm;
break through time ≥ 480 min. Gloves must be replaced after
8 hours of wear.
Gloves should be discarded and replaced if there is any
indication of degradation or chemical breakthrough.

Eye and face protection : Use splash goggles when eye contact due to splashing or
spraying liquid is possible.

Skin and body protection : When skin contact is possible, protective clothing including
gloves, apron, sleeves, boots, head and face protection
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should be worn.

Hygiene measures : Selection of appropriate personal protective equipment should
be based on an evaluation of the performance characteristics
of the protective equipment relative to the task(s) to be
performed, conditions present, duration of use, and the
hazards and/or potential hazards that may be encountered
during use.
Emergency eye wash fountains and safety showers should be
available in the immediate vicinity of any potential exposure.
Use good personal hygiene practices.
Wash hands before eating, drinking, smoking, or using toilet
facilities.
Take off contaminated clothing and wash before reuse.

9. PHYSICAL AND CHEMICAL PROPERTIES
Appearance : liquid
Color : Colorless liquid/invisible vapor.

Odor : Sweet.
Alcohol-like.

Odor Threshold : No Data Available.

Flash point : 13 - 16 °C
Method: ASTM D 56

Lower explosion limit : 3.3 vol%

Upper explosion limit : 19 vol%

Flammability (solid, gas) : Not applicable

Oxidizing properties : The substance or mixture is not classified as oxidizing.

Autoignition temperature : 363 °C
at 1,013 hPa

Decomposition temperature : not determined

Melting point/freezing point : -114.1 °C

Boiling point/boiling range : 78.5 °C

Vapor pressure : 59.45 hPa
at 20 °C

Density : 0.789 g/cm3
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at 20 °C

Water solubility : completely soluble

Partition coefficient: n-
octanol/water
: log Pow: -0.35
at 20 °C

Viscosity, dynamic : No Data Available.

Viscosity, kinematic : 1.08 mm2/s
at 40 °C

Relative vapor density : 1.6
(Air = 1.0)

Explosive properties : Not explosive

Other Information : No additional information available.

10. STABILITY AND REACTIVITY
Reactivity : Will not occur.

Chemical stability : Stable under recommended storage conditions.

Hazardous reactions : Not expected to occur.

Conditions to avoid : Avoid contact with strong oxidizers, excessive heat, sparks or
open flame.

Materials to avoid : Contact with acetyl chloride or other oxidizing agents may
result in a violent reaction.

Hazardous decomposition
products
: Not expected to decompose under normal conditions.

Thermal decomposition : Carbon monoxide is expected to be the primary hazardous
combustion product.

11. TOXICOLOGICAL INFORMATION
Product Summary : The below given information is based on the assessment of
the product including impurities.

Acute toxicity

Acute oral toxicity : Based on acute toxicity values, not classified.
Short term overexposure May cause drunkenness, depression
of the central nervous system and death.

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: LD50: > 5,000 mg/kg
Species: Rat

Acute inhalation toxicity : Based on acute toxicity values, not classified.
Short term overexposure may cause irritation of eyes, nose
and throat and central nervous system (CNS) effects such as
headache, dizziness, drowsiness and an inability to
concentrate.

: LC50: > 20 mg/l
Species: Rat

Acute dermal toxicity : Based on acute toxicity values, not classified.

: LD50: > 5,000 mg/kg
Species: Rabbit

Method: Acute toxicity estimate

Skin corrosion/irritation : Based on skin irritation values, not classified.

Serious eye damage/eye
irritation
: Classified
Causes serious eye irritation.

Respiratory or skin
sensitization
: Respiratory sensitization
Not classified
No study available.

: Skin sensitization
Not classified
No adverse effect observed.

Chronic toxicity

Component Name NTP IARC OSHA
Ethyl alcohol 1 Present

Carcinogenicity : Not classified
Ethanol possesses properties that indicate a carcinogenicity
hazard for human health but these are manifest only at doses
associated with consumption of alcoholic beverages.
In the context of an industrial chemical, these hazards do not
warrant concern as these are not likely to result from the
manufacture and use of ethanol and ethanol containing
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products.

Germ cell mutagenicity : Not classified
No adverse effect observed.

Reproductive toxicity
Effects on fertility /
Effects on or via lactation
: Not classified
Ethanol possesses properties that indicate a lactation hazard
for human health but these are manifest only at doses
associated with consumption of alcoholic beverages.
In the context of an industrial chemical, these hazards do not
warrant concern as these are not likely to result from the
manufacture and use of ethanol and ethanol containing
products.

Effects on Development : Not classified
Ethanol possesses properties that indicate a developmental
hazard for human health but these are manifest only at doses
associated with consumption of alcoholic beverages.
In the context of an industrial chemical, these hazards do not
warrant concern as these are not likely to result from the
manufacture and use of ethanol and ethanol containing
products.

Target Organ Systemic
Toxicant - Single exposure
: Classified, May cause respiratory irritation., May cause
drowsiness or dizziness.

: Target Organs: Respiratory system, Central nervous system

Target Organ Systemic
Toxicant - Repeated
exposure
: Based on repeated exposure toxicity values, not classified.,
Repeated exposure to high oral doses may damage the liver.

Aspiration hazard : Not classified
May be harmful if swallowed and enters airways.

12. Ecological information
Ecotoxicology Assessment
Short-term (acute) aquatic
hazard
: Based on acute aquatic toxicity values, not classified.

Long-term (chronic)
aquatic hazard
: Not classified, based on readily biodegradability and low acute
toxicity.

Toxicity to fish : Test substance: Based on Ethanol
Low acute toxicity to fish
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Toxicity to daphnia and
other aquatic invertebrates
: Test substance: Based on Ethanol
Low acute toxicity to aquatic invertebrates.

Toxicity to algae : Test substance: Based on Ethanol
Low toxicity to algae.

Toxicity to bacteria : Test substance: Based on Ethanol
Low toxicity to bacteria.

Toxicity to fish (Chronic
toxicity)
: No Data Available.

Toxicity to daphnia and
other aquatic invertebrates
(Chronic toxicity)
: Test substance: Based on Ethanol
Low chronic toxicity to aquatic invertebrates.

Persistence and degradability

Biodegradability : Biodegradation: 74 %
Test substance: Based on Ethanol
Rapidly degradable.
(After 5 days in a ready biodegradability test)

Stability in soil
ethyl alcohol : Low potential for soil adsorption expected

Bioaccumulative potential

Bioaccumulation : This material is not expected to bioaccumulate.

Mobility in soil

Distribution among environmental compartments
propan-2-ol : Type: Stability in water
Not expected to hydrolyze readily.

Type: Stability in soil
Low potential for soil adsorption expected

Other adverse effects

Environmental fate and
pathways
: No additional information available.

Other information

SAFETY DATA SHEET
SDA3C/200PF/IPA/140500 Gen. Variant: SDS_US_GHS
Version 1.4 Revision Date 11/22/2019 Print Date 02/10/2020 SDS No.: 840

14 / 18

Additional ecological
information
: No additional information available.

13. Disposal considerations
Waste treatment methods
Product : Contaminated products/soil/water may be Resource
Conservation and Recovery Act (RCRA) hazardous
waste/Occupational Safety and Health Administration (OSHA)
hazardous material due to low flash point (see 40 Code of
Federal Regulations (CFR) 261 and 29 CFR 1910).
Comply with applicable local, state or international regulations
concerning solid or hazardous waste disposal and/or
container disposal.

14. TRANSPORT INFORMATION

CFR_ROAD
UN number : 1170
Description of the goods : ETHANOL SOLUTIONS
Class : 3
Packing group : II
Labels : 3

Marine pollutant : no

CFR_RAIL
UN number : 1170
Description of the goods : ETHANOL SOLUTIONS
Class : 3
Packing group : II
Labels : 3

Marine pollutant : no

IMDG
UN number : 1170
Description of the goods : ETHANOL SOLUTIONS
Class : 3
Packing group : II
Labels : 3
EmS Number 1 : F-E
EmS Number 2 : S-D

Marine pollutant : no

SAFETY DATA SHEET
SDA3C/200PF/IPA/140500 Gen. Variant: SDS_US_GHS
Version 1.4 Revision Date 11/22/2019 Print Date 02/10/2020 SDS No.: 840

15 / 18

BLG (MARPOL Annex II)
Description of the goods : ETHYL ALCOHOL
Pollution category : Z
Ship type : NONE

IATA
UN number : 1170
Description of the goods : ETHANOL SOLUTION
Class : 3
Packing group : II
Labels : 3

For further information see Title 49, Code of Federal Regulations, parts 172 and 173.

15. REGULATORY INFORMATION

TSCA 12b

No substances are subject to TSCA 12(b) export notification requirements.

Significant New Use Rules (SNUR)

No substances are subject to a Significant New Use Rule.

SARA 302/304

This product contains no known chemicals regulated under SARA 302/304.

SARA 311/312

Based upon available information, this material is classified as the following health and/or physical
hazards according to Section 311 & 312:

Flammable (gases, aerosols, liquids, or solids)
Serious eye damage or eye irritation
Specific target organ toxicity (single or repeated
exposure)

SARA 313

This product contains the following chemicals subject to the reporting requirements of SARA Title III,
Section 313 and 40 CFR 372:

Component CASRN Reporting Threshold

Isopropyl Alcohol 67-63-0 1.0%

SAFETY DATA SHEET
SDA3C/200PF/IPA/140500 Gen. Variant: SDS_US_GHS
Version 1.4 Revision Date 11/22/2019 Print Date 02/10/2020 SDS No.: 840

16 / 18

State Reporting

This material contains the following chemical substance at very low levels which is regulated under
California Proposition 65. However, it is the responsibility of the California business owner to develop
his or her own regulatory compliance plan. Contact Product Safety for further information at
[e-mail].

Substance CASRN Type of Toxicity
Carcinogen Developmental Repro-Male Repro-
Female
Acetaldehyde 75-07-0 X

This product contains the following chemicals regulated by New Jersey's Worker and Community
Right to Know Act:

64-17-5 Ethyl alcohol
67-63-0 Isopropyl Alcohol

This product contains the following chemicals regulated by Massachusetts' Right to Know Law:

64-17-5 Ethyl alcohol
75-07-0 Acetaldehyde
67-63-0 Isopropyl Alcohol

This product contains the following chemicals regulated by Pennsylvania's Right to Know Act:

64-17-5 Ethyl alcohol
67-63-0 Isopropyl Alcohol

Other international regulations
Global Inventory Status
The ingredients of this product are compliant with the following chemical inventory requirements or
exemptions.
*Additional Explanatory Status Statements follow the table, as necessary.

Country/Region Inventory Status Description
Australia AICS Compliant
Canada DSL Compliant
China IECSC Compliant
Europe REACH See REACH Compliance Statement
Japan ENCS Compliant
Korea KECI Compliant
New Zealand NZIoC Compliant
Philippines PICCS Compliant
United States of America TSCA Compliant
Taiwan TCSCA Compliant

REACh status
SAFETY DATA SHEET
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Version 1.4 Revision Date 11/22/2019 Print Date 02/10/2020 SDS No.: 840

17 / 18

If the product has been purchased from any company of the LyondellBasell group of companies
registered in the European Union, we confirm that all substances in this preparation have been
registered under REACh, in accordance with the deadlines set forth in REACh. (Regulation (EU) No.
1907/2006)

Contact [e-mail] for additional global inventory information.

16. OTHER INFORMATION

Material safety datasheet sections which have been updated:

Revised Section(s): 15 16

HMIS Classification : Health Hazard: 2
Flammability: 3
Physical hazards: 0

NFPA Classification : Health Hazard: 2
Fire Hazard: 3
Instability: 0

Further information

HMIS rating scale (0 = minimal hazard; 4 = severe hazard)
NFPA rating scale (0 = minimal hazard; 4 = severe hazard)

Disclaimer
Information in this document is accurate to the best of our knowledge at the date of publication.
The document is designed to provide users general information for safe handling, use,
processing, storage, transportation, disposal and release and does not c onstitute any warranty
or quality specification, either express or implied, including any warranty of merchantability or
fitness for any particular purpose. Users shall determine whether the product is suitable for
their use and can be used safely and legally.

In addition to any prohibitions of use specifically noted in this document, LyondellBasell may
0

3
2
2 3 0

SAFETY DATA SHEET
SDA3C/200PF/IPA/140500 Gen. Variant: SDS_US_GHS
Version 1.4 Revision Date 11/22/2019 Print Date 02/10/2020 SDS No.: 840

18 / 18

Disclaimer
further prohibit or restrict the sale of its products into certain applications. For further
information, please contact a LyondellBasell representative or visit the LyondellBasell website
at: https://www.lyondellbasell.com/en/products-technology/product-safety-stewardship/
The Trade Name referenced in section 1 is a trademark owned or used by the LyondellBasell
family of companies.

Numerical Data Presentation
The presentation of numerical data, such as that used for physical and chemical properties and
toxicological values, is expressed using a comma (,) to separate digits into groups of three and
a period (.) as the decimal marker. For example, 1,234.56 mg/kg = 1 234,56 mg/kg.

Language Translations
The information presented in this document has been translated from English by a vendor
LyondellBasell believes to be reliable. LyondellBasell and its vendor have made a good-faith
effort to verify the accuracy of the translation, but assume no liability or other responsibility for
any errors that may have occurred. Please refer to our web site (www.lyondellbasell.com) for
the original document written in English.

End of Material Safety Data Sheet

APPENDIX D
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: IA-1
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 9.5E-06 2.1E-01 NO
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 2.2E-06 4.9E-02 NO
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: IA-2
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 9.2E-06 2.0E-01 NO
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 2.1E-06 4.7E-02 NO
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: IA-3
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 1.8E-06 2.0E-01 NO
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 4.0E-07 4.8E-02 NO
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: IA-4
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 1.8E-06 3.4E-01 NO
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 4.1E-07 8.1E-02 NO
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: IA-5 w/o ethyl acetate
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 2.9E-06 1.8E-01 NO
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 6.7E-07 4.2E-02 NO
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: IA-5
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 2.9E-06 6.1E+00 YES
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 6.7E-07 1.4E+00 YES
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: IA-6 w/o ethyl acetate
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 8.3E-06 5.1E-01 NO
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 1.9E-06 1.2E-01 NO
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: IA-6
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 8.3E-06 2.5E+01 YES
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 1.9E-06 6.0E+00 YES
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: IA-7
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 8.8E-06 3.2E+00 YES
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air 2.0E-06 7.6E-01 NO
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SS-1
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 7.9E-06 3.9E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 6.0E-07 3.1E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SS-2
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.1E-07 1.3E-02 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 8.6E-09 1.0E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SS-3
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.3E-07 3.8E-02 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.8E-08 3.0E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SS-4
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.6E-06 1.2E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.2E-07 9.8E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SS-5
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.0E-06 3.5E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.6E-07 2.8E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SS-6
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 3.7E-06 7.6E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.8E-07 6.1E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SS-7
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 3.2E-06 8.1E-01 NO
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.4E-07 6.4E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
APPENDIX E
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site:Clariant Corporation Site
Address:4000 Monroe Road
City:Charlotte
County:Mecklenburg
Brownfields Project Number: 25036-21-060
Property and Building Characteristics
a. Provide occupancy and use information.
75,606 square foot, single-story office building, built in 1956
92,780 square foot, two-story office building, built in 1956
391 square foot, single-story mechanical building, built in 1994
75,606 sq. ft. single-story building constructed of concrete block
92,780 sq. ft. two-story building constructed of cement brick
391 sq. ft. single-story building constructed of concrete block
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
Concrete slab for all buildings, other foundation info unknown
75,606 sq ft and 92,780 sq ft buildings have forced air - ducted
391 sq ft buildings has none
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
No subslab ventilation systems in place. It is not known if moisture barriers are in place.
50
NASize of Property (acres)
% of property that is wooded/brush
9.892
5
10
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and
design considerations (e.g. positive pressure?).
0
35
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information
requested below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ
Brownfield’s Project Manager (PM).
Current Usage Proposed UsageSurface Conditions
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed.
If numerous buildings are on-site, consult with your PM as only information on specific buildings may be needed.
b. Describe the construction of the building including materials (e.g. wood frame, block), type and size of openings (e.g.
windows, bay doors), and height (number of stories).
% of property that is covered by buildings
Rev. 09/2015 Page 1 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
West
South
East
N NA NA
Y 525'NW
Y 890'NW
Utilities
Is there a septic system on-site? (Y or N) ___N______
Please provide the utility providers for the subject property
a. Natural Gas ____PNG______________
b. Sewer ____City of Charlotte__________
c. Electricity ___Duke Energy______________
d. Other
For surrounding properties, please complete the following table with available information.
Y
Y
NA
Y
Y
Y
N
Zoning/Land Use Proposed Usage Current Use/Occupant
DirectionDistance
(ft)Address
Same
Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding
areas. If specific receptors are present, please provide addresses of the facilities.
Commerical, then Residential Further
Commerical
Railroad, then Commercial Further
Commercial
For the subject property, please provide a map of known buried utilities. If available, include depth to top, construction
material, and diameter of the utilities. In addition, please provide the following information on utility providers. If additional
assessment is required, the public utility locators should be contacted. This information can then be added to a site map.
Y/N *
Is a school or daycare center within 1,000 ft of the Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses.
Distance
(ft)
613 Mayview Dr.
645 Mayview Dr.
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject
property.
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
Same
Same
Same
Is there a basement within 1,000 ft of the Property?
NA
Is there a residence within 1,000 ft of the Property?
Utility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is a sanitary sewer within 100 ft of the Property boundary?
Rev. 09/2015 Page 2 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public ___Y____ Private ______
Charlotte Water
N NA NA NA
Y 1000'NA 640 Vinewood Place
N NA NA NA
Surface Water & Wetlands
Are there surface water features on the
property? (If yes, please complete a. to d.)
Provide Information regarding Surface Water
and Wetlands
Distance
(ft)Direction Address
No
a. Is the water body naturally developed or
man-made?
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a
windshield survey within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation
wells may be present. Information from applicable databases can and should be utilized; however, should not be utilized in
lieu of the windshield survey. If multiple wells are present within the requested radius, please provide a map of the well
locations. If needed, please attach a separate table to list all wells. Please note, the PM may opt for a more extensive water
supply well survey if needed.
If Private, please provide details of the water supply source (i.e. well location, well construction, etc.). If public, please include
the water providers name.
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property
b d?Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity
of the Property.
b. List the uses of the water body.
c. What is the source of the water for the
water body?
d. What is the nature of the bottom of the
water body (e.g., rocky or concrete bottom,
drainage ways or impoundments)
If no on-site surface water features, what is the
nearest surface water body?
Are there any wetlands present on the property?
If no wetlands on-site, are wetlands suspected
on adjoining properties?
Rev. 09/2015 Page 3 of 3
FIGURE A
RECEPTOR SURVEY UTILTIES MAP
CLARIANT CORPORATION SITE
4000 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
BROWNFIELD PROJECT ID: 25306-21-060
ECS PROJECT NO. 49:12929-D
SOURCE:
CHARLOTTE MECKLENBURG POLARIS GIS WEBSITE
ACCESSED JANUARY 19, 2021
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE MUNICPAL WATER LINE LOCATION
APPROXIMATE NATURAL GAS LINE LOCATION
APPROXIMATE COMMUNICATIONS LINE LOCATION
FIGURE B
RECEPTOR SURVEY WATER SUPPLY WELL MAP
CLARIANT CORPORATION SITE
4000 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
BROWNFIELD PROJECT ID: 25306-21-060
ECS PROJECT NO. 49:12929-D
SOURCE:
CHARLOTTE MECKLENBURG POLARIS GIS WEBSITE
ACCESSED MAY 12, 2022
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
INACTIVE WATER SUPPLY WELL
1,500 ft.

APPENDIX F

BUILDING 2 FLOOR 1 PLAN MAP
CLARIANT CORPORATION SITE4000 MONROE ROADCHARLOTTE, NORTH CAROLINABROWNFIELD PROJECT ID: 25306-21-060
ECS PROJECT NO. 49:12929-D
SOURCE:PARSIDE PARTNERS
SCALE:NOT TO SCALE
LEGEND
SS-5/IA-5
APPROXIMATE SUB-SLAB SOIL GAS INDOOR AIR SAMPLE LOCATION
BUILDING 3 FLOOR 1 PLAN MAP
CLARIANT CORPORATION SITE4000 MONROE ROADCHARLOTTE, NORTH CAROLINABROWNFIELD PROJECT ID: 25306-21-060
ECS PROJECT NO. 49:12929-D
APPROXIMATE SUB-SLAB SOIL GAS INDOOR AIR SAMPLE LOCATION
LEGEND
SS-6/IA-6
SOURCE:PARSIDE PARTNERS
SCALE:NOT TO SCALE
LEGEND
BUILDING 4 FLOOR 1 PLAN MAP
CLARIANT CORPORATION SITE4000 MONROE ROADCHARLOTTE, NORTH CAROLINABROWNFIELD PROJECT ID: 25306-21-060
ECS PROJECT NO. 49:12929-D
APPROXIMATE SUB-SLAB SOIL GAS INDOOR AIR SAMPLE LOCATION
SS-7/IA-7
SOURCE:PARSIDE PARTNERS
SCALE:NOT TO SCALE