23067_Blythe Isenhour_Final Grade Soil Assessment Report and Review Letter_20221222

December 22, 2022 Sent Via E-mail
Christopher J. Branch
Boulevard at 4920 Old Pineville, LLC 2100 Hastings Drive Charlotte, NC 28207 [e-mail]

Subject: Review of Final Grade Soil Assessment Report Blythe Isenhour 4290 Old Pineville Road Charlotte, Mecklenburg County
Brownfields Project Number 23067-19-060
Dear Mr. Branch: The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received and
reviewed the December 14, 2022, Final Grade Soil Assessment Report (Report) submitted by Hart &
Hickman for the above referenced Brownfields Project. The Report summarizes recent final grade soil assessment activities conducted in accordance with the approved Final Grade Soil Sampling Work Plan dated October 7, 2022.
DEQ Brownfields reviewed the Report and evaluated the analytical results using the July 2022 DEQ
Risk Calculator. The results are consistent with those provided in the Report and are below the thresholds for residential use. As such, DEQ Brownfields has determined that the Report complies with Land Use Restrictions 13.h of the Notice of Brownfields Property recorded December 10, 2021.
Be advised that this approval from the Brownfields Program does not waive any applicable requirement
to obtain any necessary permits, licenses, or certifications for the above referenced activities nor does it waive any requirement to comply with applicable law for such activities. If you have any questions, please feel free to contact me via e-mail at [e-mail].
Sincerely,
Peter L. Doorn, Brownfields Project Manager ec: Michael Bender, Boulevard at 4920 Old Pineville, LLC Ralph McGee and Haley Martin, Hart & Hickman Tracy Wahl, NC DEQ

Via Email

December 14, 2022

NCDEQ – Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attn: Mr. Peter Doorn

Re: Final Grade Soil Assessment Report
Blythe Isenhour
Old Pineville Road Towns Phase II
4920 Old Pineville Road
Charlotte, North Carolina
Brownfields Project No. 23067-19-060
H&H Project No. BOU-014

Dear Mr. Doorn:

On behalf of 4920 Old Pineville, LLC, enclosed please find a copy of the Final Grade Soil Assessment
Report prepared for the Bythe Isenhour Brownfields property (Brownfields Project No. 23067-19-060)
located in Charlotte, Mecklenburg County.

Should you have any questions or need additional information, please do not hesitate to contact me at
[phone].

Sincerely,

Hart & Hickman, PC
Ralph McGee, PG Haley Martin, PG
Project Manager Senior Project Geologist

Enclosure

cc: Mr. Michael Bender, Boulevard Real Estate Advisors (via email)
Mr. Christopher Branch, Boulevard Real Estate Advisors (via email)
i
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Boulevard Realty Estate Advisors (BOU)/BOU-014 4920 Old Pineville Rd/Final Grade/Report/23067 - Final Grade Soil Assessment - Blythe Isenhour.docx
Final Grade Soil Assessment Report
Blythe Isenhour
Old Pineville Towns Phase II
Charlotte, North Carolina
Brownfields Project No. 23067-19-060
H&H Job No. BOU-014

Table of Contents

1.0 Introduction ............................................................................................................................ 1 
2.0 Background Information....................................................................................................... 2 
2.1 Background ........................................................................................................................... 2 
2.2 Previous Assessment Activities ............................................................................................ 2 
2.3 Brownfields Activities .......................................................................................................... 5 
2.4 Debris Removal .................................................................................................................... 6 
3.0 Final Grade Soil Assessment Activities ................................................................................ 9 
3.1 Final Grade Soil Sampling Methodologies .......................................................................... 9 
3.2 Soil Sample Results ............................................................................................................ 10 
3.3 Risk Evaluation .................................................................................................................. 11 
4.0 Summary and Conclusions ................................................................................................. 13 

List of Attachments

Table 1 Summary of Final Grade Soil Analytical Results

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Final Grade Soil Sample Location Map

Appendix A Laboratory Analytical Report
Appendix B DEQ Risk Calculator

1
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
Final Grade Soil Assessment Report
Blythe Isenhour
Old Pineville Towns Phase II
Charlotte, North Carolina
Brownfields Project No. 23067-19-060
H&H Job No. BOU-014

1.0 Introduction

On behalf of Boulevard at 4920 Old Pineville, LLC (Prospective Developer or PD), Hart &
Hickman, PC (H&H) has prepared this Final Grade Soil Assessment Report for the Blythe
Isenhour Brownfields property (Brownfields Project No. 23067-19-060) located at 4920 Old
Pineville Road in Charlotte, Mecklenburg County, North Carolina (Site). A Site location map is
included as Figure 1, and the Site and surrounding area are shown on Figure 2.

The redevelopment is known as Old Pineville Towns Phase II, and is being redeveloped with for-
sale townhomes by Ryan Homes, an NVR company. The Site development plan includes
construction of forty-eight (48) individual townhome units across twelve (12) building slabs. The
proposed Site development plan is included on Figure 3.

A Brownfields Agreement between the North Carolina Department of Environmental Quality
(DEQ) and the PD was recorded on December 10, 2021. Land Use Restriction (LUR) Paragraph
13.c. generally states that physical redevelopment of the Site will be completed in accordance with
a DEQ-approved Environmental Management Plan (EMP). The EMP for the redevelopment dated
December 8, 2020 received DEQ-approval on December 23, 2020.

Requirements of the EMP include the collection of final grade soil samples upon completion of
soil disturbance activities (i.e., following completion of utility installations and final grading). In
accordance with the DEQ-approved EMP, a Final Grade Soil Assessment Work Plan (Work Plan)
was submitted to the DEQ Brownfields Program on October 7, 2022. The DEQ Brownfields
Program approved the Work Plan in a letter dated October 10, 2022. A summary of the final grade
soil sampling activities conducted in accordance with the Work Plan is provided in the following
sections.
2
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
2.0 Background Information

2.1 Background

Historically, the Site primarily consisted of land used for agricultural purposes as early as the
1930s and remained undeveloped land until the current office and warehouse buildings were
constructed in the early 1960s. Following construction of the on-Site buildings, the Site was
occupied by a general contractor business from the 1960s until the 1990s. In the late 1990s to
early 2000s, the Site was occupied by an environmental emergency response and remediation
contractor (Four Seasons Environmental). During that time, the Site was improved with a concrete
secondary containment system for above ground storage tanks (ASTs) located in the south-central
portion of the Site and a curbed concrete pad was constructed in the central portion of the Site
(Figure 2). In the mid-2000s, an abandoned railcar was staged in the northeastern portion of the
Site and remains near the northern Site boundary. The Site has been occupied by Heartwood Tree
Services since 2003. Heartwood Tree Service operations include fleet vehicle, tree service
equipment, and materials staging, fleet vehicle fueling, administrative offices, and tree clearing
debris processing activities.

2.2 Previous Assessment Activities

H&H has completed review of available environmental reports documenting assessments
previously completed at the Site. A brief summary of each assessment is provided below.

1990 UST Closure Activities
On April 27, 1990, one 3,000-gallon gasoline underground storage tank (UST) was removed from
the Site. The UST was located in the eastern portion of the Site adjacent to the storage building
(Figure 2). Upon removal of the UST from the basin, soil samples were collected from the
sidewalls and base of the excavation for analysis of total petroleum hydrocarbons as diesel-range
organics (TPH-DRO) and TPH as gasoline-range organics (TPH-GRO). Analytical results of the
closure soil samples indicated that no compounds were detected above the laboratory reporting
3
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
limits. UST removal activities and initial abatement assessment results are documented in the
Limited Site Assessment Report prepared by Aquaterra, Inc. and dated July 9, 1990.

Following the 3000-gallon UST removal, DEQ requested collection of soil samples for laboratory
analysis below the associated dispenser and product lines. In September and October 2003, soil
samples were collected and submitted for analysis of TPH-GRO. Laboratory analytical results
indicated that no compounds were detected at concentrations above the laboratory reporting limits
in the dispenser island and product line soil samples collected. The sampling activities are
documented in two letters completed by Froehling & Robertson, Inc. dated October 6, 2003 and
October 28, 2003. Based on results of the additional soil sampling activities, the DEQ UST Section
issued a No Further Action (NFA) letter for the 3000-gallon UST closure on October 29, 2003.

2001 Spill Incident
In February 2001, a tank overturned at the Site and released approximately 4,000-gallons of used
oil and water onto the ground surface west of a curbed concrete pad located in the central portion
of the Site. According to a Soil Cleanup Report prepared by MACTEC and dated June 20, 2003,
soil samples identified as 1, 2, and 3 were collected in May 2003 for laboratory analysis of TPH
as oil and grease from areas impacted by the spill. Laboratory analytical results indicated that
compound concentrations were detected above the DEQ screening criteria at the time of 250
milligrams per kilogram (mg/kg). Based on the soil sample analytical results, approximately
1,564-tons of impacted soil was excavated in the western portion of the Site and transported to the
BFI Landfill located in Concord, North Carolina. Following excavation activities, thirteen
confirmation soil samples were collected and analyzed for TPH as oil and grease to confirm
impacts were adequately removed. Analytical results indicated that no compounds were detected
at concentrations above the DEQ screening criteria in the thirteen confirmation soil samples.

July 2003 Phase I ESA
In July 2003, MACTEC performed Phase I Environmental Site Assessment (ESA) activities at the
Site. Results of the Phase I ESA identified staining near the ASTs located in the south-central
portion of the Site as an environmental concern. The ESA report also indicated that Four Seasons
Environmental staged fluids recovered from hazardous material spills and storage tanks in the
4
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
central portion of the Site. The recovered fluids were stored and mixed with sawdust for
solidifying on a curbed concrete pad located in the central portion of the Site.

Based on findings in the July 2003 Phase I ESA, MACTEC collected two soil samples for
laboratory analysis of TPH-GRO and TPH-DRO in the area of staining observed near the ASTs.
Laboratory analytical results indicated the presence of TPH-DRO and TPH-GRO concentrations
in soil sample B-1 above the DEQ screening criteria at the time. Based on the detected TPH-DRO
and TPH-GRO concentrations, MACTEC recommended the stained areas be excavated to a depth
of approximately 4 feet below ground surface (ft bgs). MACTECs findings are documented in the
Report of Regulatory File Review, Soil Sampling and Analysis report dated August 12, 2003. No
documentation for removal of the impacted soil reported by MACTEC was available for review.

October 2019 Phase I ESA
In October 2019, H&H conducted Phase I ESA activities at the Site. The results of the Phase I
ESA identified the following potential environmental concerns in connection with the Site:
 Based on review of available information, H&H was unable to obtain documentation
confirming soil impacts in the area of the ASTs, identified by MACTEC in July 2003, were
remediated to levels below DEQ screening criteria. As such, reported soil impacts in the
area of the on-Site ASTs identified by MACTEC were identified as an environmental
concern.

 H&H observed a curbed concrete pad located in the central portion of the Site used for
staging various Heartwood Tree Service equipment and materials. According to
information provided in the July 2003 MACTEC Phase I ESA report, the concrete pad was
formerly used by Four Seasons Environmental for solidification of waste fluids recovered
during responses to hazardous waste spills and from USTs prior to closure activities.
During Site reconnaissance, the concrete pad appeared to be in good condition with no
obvious evidence of drains, sumps, or significant staining or cracks. The historical use of
the concrete pad located in the central portion of the Site for solidification of waste fluids
was identified as a potential environmental concern.

5
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
 Although the 2001 tanker spill discussed above was reportedly remediated to levels below
DEQ screening criteria, the potential for residual impacts to the Site was identified as a
potential environmental concern.

 The property located adjacent to the south and topographically cross-gradient of the Site is
identified as the Old Pineville Road Brownfields Property (Brownfields Project No. 10061-
06-060, see Figure 2). According to a review of available information, ECS conducted
Phase II ESA sampling activities at the south adjacent property in March 2007. Results of
Phase II ESA activities did not identify compounds at concentrations exceeding the DEQ
screening criteria in sediment, surface water, soil, or groundwater. The potential for impact
to the Site from an undocumented release on the adjacent Old Pineville Road Brownfields
property was identified as a potential environmental concern.

In addition to the above, the Site is located in an area of Charlotte historically developed for
industrial and commercial uses. Multiple release incidents are reported on nearby off-Site
properties in available environmental databases. Additionally, properties located in the immediate
Site area have historically included automotive repair operations, a chemical manufacturing
facility, and refinery that likely used certain petroleum products and/or chlorinated solvents. The
potential for impact to the Site from potential undocumented releases on nearby off-Site properties
was identified as a potential environmental concern.

2.3 Brownfields Activities

To address potential environmental concerns associated with historical on-Site and off-Site
operations, the Site was entered into the DEQ Brownfields Program and received eligibility in a
letter dated January 13, 2020. In March 2020, H&H completed Brownfields assessment activities
at the Blythe Isenhour Brownfields property. Assessment activities included collection of soil,
groundwater, and soil gas samples for laboratory analysis. A brief summary of assessment results
is provided below:

6
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
 Results of soil samples collected at the Site did not identify constituents of concern at
concentrations above the DEQ Residential Preliminary Soil Remediation Goals (PSRGs)
or background concentrations in the case of metals.

 H&H installed and sampled four (4) temporary monitoring wells to evaluate subsurface
conditions associated with historical on-Site and nearby off-Site operations. Results of the
groundwater laboratory analytical results did not identify compounds of concern at
concentrations above the 2L Groundwater Standards.

 H&H installed and sampled six (6) temporary soil gas monitoring points within the
footprint of proposed townhome buildings to determine if compounds are present in the
subsurface at concentrations that pose potential structural vapor intrusion risks for the
planned buildings. Laboratory analytical results identified benzene (up to 31 micrograms
per cubic meter [µg/m3]), naphthalene (up to 220 µg/m3), 1,2,4-trimethylbenzene (up to
4,200 µg/m3), and 1,3,5-trimethylbenzene (up to 3,700 µg/m3) at concentrations above the
DEQ Division of Waste Management (DWM) Residential Vapor Intrusion Sub-slab and
Exterior Soil Gas Screening Levels (SGSLs).

Following completion of the Brownfields assessment activities, an EMP was prepared for the
Blythe Isenhour Brownfields property and was approved by DEQ on December 23, 2020. The
Notice of Brownfields Property was recorded on the property deed on December 10, 2021. In
accordance with the recorded Brownfields agreement and the Brownfields minimum townhomes
requirements checklist, a Vapor Intrusion Mitigation Plan (VIMP) Revision 1 was submitted for
DEQ on February 7, 2022, and received DEQ-approval in a letter dated March 3, 2022.

2.4 Debris Removal

During 2003 excavation activities associated with a surface spill from an overturned tank in the
western portion of the Site, MACTEC personnel observed wood debris during shallow (i.e., 3 to 4
ft bgs) excavation activities. On December 29, 2020, Geoscience completed gridded exploratory
trench excavation activities in the western portion of the Site to evaluate for the presence of
7
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
geotechnically unsuitable material. Results of the trenching activities identified three discrete
debris areas that appeared to be associated with historical filling activities and not related to the
former tree service operations. The debris areas are described further below:

 Area 1 – The wood debris (plywood, wood planks, etc.) located in this area appears to be
the material encountered during MACTEC excavation activities in 2003. The debris was
encountered at depths from 3-4 ft bgs and consisted of an approximately 1-1.5 ft thick layer
of buried material.
 Area 2 – Construction debris (brick and ceramic tiles) were encountered from
approximately 5 to 15 ft bgs. Wood and other organic debris was not observed in this area
of the Site.
 Area 3 – Construction debris (brick, fence posts, tree trunks, and other organic debris) were
observed at depths ranging from approximately 5 ft bgs to 9 ft bgs.

During the trench and test pit activities, H&H collected methane measurements as a cursory
evaluation for the presence of methane gas in the subsurface. Results of methane screening
activities did not identify areas with elevated concentrations of methane gas in the subsurface
during trench and excavation activities.

Approved uses included in the recorded Brownfields agreement include multi-family residential,
townhomes, office, parking, retail, recreational, and commercial. In addition, Land Use
Restriction k. included in the Brownfields agreement generally indicates that no use of the
Brownfields property may occur until debris in the western portion of the Site has been removed,
the debris removal area has been backfilled, and a work plan to conduct methane monitoring in
the area of the removed debris is provided to DEQ for approval.

On November 18, 2021, H&H prepared a Methane Sampling Work Plan in accordance with LUR
k. in the recoded Brownfields agreement, and DEQ provided approval in a letter dated November
30, 2021. In December 2021, debris located in the western portion of the Site was removed and
disposed at Republic Services in Concord, North Carolina, a lined Subtitle D Municipal Solid
Waste Landfill. In January 2022, H&H completed methane sampling activities at the Blythe
8
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
Isenhour Brownfields property. Assessment activities included collection of subsurface methane
and pressure measurements in the area of debris removal. A brief summary of assessment results
is provided below:

 Following removal of buried debris and the excavation area was backfilled with clean fill
material, the excavation area was allowed to equilibrate for a minimum of 30 days.
Following the minimum 30-day equilibration period, three (3) temporary methane gas
probes were installed within the former excavation area.

 Results of methane measurements identified trace levels of methane (up to 0.7 %) in one
methane gas probe. Methane was not measured at concentrations above the lower
explosive limit (LEL) or the DEQ Brownfields Program 30% by volume air residential use
screening criteria in soil gas measurements collected at the Site. Based on results of the
2020 Brownfields assessment activities and the 2022 soil gas methane sampling activities,
safe redevelopment of the Site will be managed in accordance with the DEQ-approved
EMP and the DEQ-approved VIMP.

The DEQ-approved EMP indicates that final grade soil assessment will be completed upon
completion of grading activities to evaluate the potential for impacts in shallow soil that will not
be beneath impervious cover at the completion of the redevelopment activities. Grading activities
and utility installation for proposed townhome buildings is complete, and contractors have
installed asphalt-paved access drives and parking areas. In accordance with the DEQ-approved
EMP, H&H prepared a Final Grade Soil Assessment Work Plan (Work Plan) for DEQ review and
approval. The Work Plan received DEQ-approval in a letter dated October 10, 2022. H&H
completed final grade soil assessment activities at the Site to evaluate the potential for impacts in
landscaped area shallow soil. A summary of the sampling activities is provided in the following
sections.
9
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
3.0 Final Grade Soil Assessment Activities

Final grade soil sampling activities were completed at the Site to evaluate the potential for impacts
in landscape area shallow soil that may pose unacceptable exposure risks to future residential
occupants. The soil sampling activities were performed in general accordance with the DEQ
Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup of Contaminated
Sites (Guidelines) dated September 2022, the DEQ-approved Work Plan, and the most recent
versions of U.S. Environmental Protection Agency (EPA) Region IV Laboratory Services and
Applied Science Division (LSASD) Field Branches Quality System and Technical Procedures
guidance.

3.1 Final Grade Soil Sampling Methodologies

To evaluate for the potential presence of impacts in unpaved areas at the Site, landscaped areas
were divided into ten (10) discrete areas (FG-1 through FG-10) and a representative final grade
soil sample was collected from each area. The ten final grade evaluation areas are shown on Figure
2 and are described below:

 Final grade area FG-1 and portions of FG-2 included the landscaped areas located in the
eastern portion of the Site along Old Pineville Road;
 Portions of final grade area FG-2 and final grade areas FG-3 through FG-6 included the
landscaped areas located in the southern portion of the Site; and
 Final grade areas FG-7 though FG-10 included the landscaped areas located in the northern
portion of the Site.

The final grade soil samples were collected by advancing a soil boring to approximately 2 feet
below the ground surface (ft bgs) utilizing a decontaminated stainless-steel hand auger and
collecting soil sample aliquots from four to five aliquot locations in each final grade area.
Continuous soil samples were collected from the center of the hand auger bucket and observed for
the presence of staining or odors and field screened for elevated volatile organic vapors using a
calibrated photo-ionization detector (PID). Field personnel did not observe the presence of
10
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
staining or odors in the sample aliquots and PID readings did not indicate the presence of organic
vapors. Soil lithology at the aliquot locations generally consisted of dry to moist clayey silt with
trace gravel. The aliquot soil sample locations for each final grade area are shown in Figure 3.

Following boring advancement, the soil sample aliquots from each area were combined and
homogenized to form one composite soil sample per area for a total of ten (10) composite final
grade soil samples (FG-1 through FG-10). Composite soil samples from each area were collected
directly into dedicated laboratory supplied sample containers and submitted to Waypoint
Analytical (Waypoint) under standard chain of custody protocols for analysis of semi-volatile
organic compounds (SVOCs) by EPA Method 8270, and Resource Conservation and Recovery
Act (RCRA) metals plus hexavalent chromium by EPA Methods 6020/7471/7199.

In addition to the composite soil samples described above, one representative grab soil sample was
collected from each section at the aliquot location that exhibited the highest PID reading. The grab
soil samples were collected from undisturbed portions of soil in the hand auger bucket and placed
directly into laboratory supplied glassware for submittal to a Waypoint under standard chain of
custody protocols for analysis of volatile organic compounds (VOCs) by EPA Method 8260.

For quality assurance and quality control purposes (QA/QC), H&H collected one duplicate
composite sample (DUP-01) from FG-9 for SVOCs and RCRA metals plus hexavalent chromium.
H&H also collected a duplicate representative grab sample from the aliquot where VOCs were
collected in the same section. A copy of the laboratory analytical report and chain of custody
record is provided in Appendix A.

Following sampling activities, the soil borings were properly abandoned and the surfaces were
repaired similar to pre-drilling conditions. Additionally, the soil boring locations were estimated
using a hand-held global positioning system (GPS) unit.

3.2 Soil Sample Results

A tabular summary of final grade soil sampling analytical results is presented in Table 1. The
laboratory analytical results were compared to the DEQ Residential and Industrial/Commercial
11
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx
Preliminary Soil Remediation Goals (PSRGs) dated July 2022. In addition to the PSRGs, metals
results were compared to published concentrations for naturally occurring metals in North Carolina
soil and Site-specific background levels.

Laboratory analytical results indicate that select VOCs were detected at concentrations above the
laboratory method detection limits in the soil samples collected at the Site. The VOCs acetone (up
to 0.108 milligrams per kilogram [mg/kg]), carbon disulfide (up to 0.003 J mg/kg), and methyl
ethyl ketone (up to 0.11 J mg/kg) were detected at concentrations above the laboratory method
detection limits, but below the DEQ Residential PSRGs. SVOCs were not detected above
laboratory method detection limits in the final grade soil samples.

As expected, several metals were detected at concentrations above laboratory method detection
limits in the final grade samples collected at the Site. Hexavalent chromium (up to 3.72 mg/kg)
was detected at a concentration above the DEQ Residential PSRG of 0.31 mg/kg in the final grade
soil samples. Remaining metals concentrations detected in the soil samples are consistent with
naturally occurring levels for the Site area.

3.3 Risk Evaluation

DEQ PSRGs are very conservative and based upon a Target Cancer Risk (TCR) of 1 x 10-6 for
potential carcinogenic effects and a Target Hazard Quotient (THQ) of 0.2 for potential non-
carcinogenic effects. Additional assessment is not typically warranted if the calculated cumulative
lifetime incremental carcinogenic risk (LICR) is 1 x 10-4 or less and the acceptable level for non-
carcinogenic risk is a calculated cumulative hazard index (HI) of 1.0 or less.

H&H utilized the DEQ Risk Calculator (July 2022) assuming residential land use scenario to
further evaluate potential cumulative risks for the direct soil contact pathway for the proposed
residential buildings. To model a hypothetical “worst-case” scenario, H&H conservatively
calculated the cumulative risks using the highest concentration of any compound detected in any
soil sample collected at the Site. The results of the risk calculations are summarized below and
are included in Appendix B.
12
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx

Land Use Scenario Calculated
Cumulative LICR
Calculated
Cumulative HI
Calculated LICR or
HI Exceeds
Acceptable Risk
Levels?
Residential 3.9 x 10-5 0.59 No

The results of the risk calculation indicate that the calculated cumulative risks do not exceed
acceptable risk levels for a residential use exposure scenario.

13
https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/boulevard realty estate advisors (bou)/bou-014 4920 old pineville rd/final grade/report/23067 - final grade soil assessment - blythe isenhour.docx

4.0 Summary and Conclusions

H&H has completed final grade soil sampling activities at the Blythe Isenhour Brownfields
property located at 4920 Old Pineville Road in Charlotte, North Carolina. The final grade soil
sampling activities were conducted in accordance with the DEQ Brownfields approved Work Plan
dated October 7, 2022. Final grade soil sampling activities included the collection of soil samples
to evaluate the potential for impacts in areas at the Site that will not be covered by demonstrably
clean fill soil, building foundations, sidewalks, or asphaltic or concrete parking areas and
driveways following redevelopment.

Laboratory analytical results indicate that several VOCs were detected at concentrations above the
laboratory method detection limits, but below the DEQ Residential PSRGs in the soil samples
collected at the Site. SVOCs were not detected at concentrations above the laboratory method
detection limits in soil samples collected at the Site.

Several metals were detected above laboratory method detection limits. Hexavalent chromium
was detected at concentrations above the DEQ Residential PSRG in select soil samples collected
at the Site. Remaining detected metals concentrations detected were within the range of naturally
occurring background concentrations and/or below the DEQ Residential PSRGs.

To evaluate potential cumulative risks for the combined soil pathway for a residential occupant at
the Site, H&H calculated cumulative risks using the highest concentrations of compounds detected
in the final grade samples. H&H utilized the DEQ risk calculator (July 2022) assuming a
residential land use scenario, based on the most conservative use the Site following redevelopment
activities. The results of the risk calculation indicate that the calculated cumulative LICR for final
grade soil samples is 3.9 x 10-5 and the cumulative HI is 0.59. Thus, the calculated risks do not
exceed acceptable risk levels for a residential use exposure scenario.

Table 1Summary of Final Grade Soil Sample Analytical ResultsBlythe Isenhour Charlotte, North CarolinaBrownfields Project No. 23067-19-060H&H Job No. BOU-014Evaluation AreaSample IDDateDepth (ft bgs)1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2Sample Type Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Range RangeUnitsVOCs (8260D)Acetone0.046NA0.108NA0.022 JNA0.032NA0.056NA14,000 210,000-- --Carbon disulfide0.002 JNA <0.0008 NA <0.0008 NA <0.0008 NA0.003 JNA160 740-- --Methyl Ethyl Ketone (MEK)<0.0008 NA0.011 JNA <0.0008 NA <0.0008 NA <0.0008 NA5,500 40,000-- --SVOCs (8270E)-- -- -- --Metals (6020B/7471B/7199)ArsenicNA1.87NA1.92NA1.29NA1.57NA1.21 0.68 3.0 3.67 - 6.47 1.0 - 18BariumNA73.0NA61.2NA65.0NA35.4NA86.4 3,100 47,000 16.8 - 48.6 50 - 1,000CadmiumNA0.0366 JNA0.0597 JNA<0.0318NA<0.0328NA0.0486 J 1.4 20 ND 1.0 - 10Chromium (total)NA42.0NA52.3NA31.0NA26.4NA29.6 NE NE 47.4 - 122 7.0 - 300Hexavalent ChromiumNA<0.181NA1.96NA3.72NA2.29NA<0.1670.31 6.5 0.415 - 0.584 NSTrivalent ChromiumNA42.0NA50.3NA27.3NA24.1NA29.6 23,000 350,000 47.0 - 121.4 NSLeadNA15.9NA13.0NA6.97NA7.21NA13.2 400 800 6.44 - 15.1 ND - 50MercuryNA0.0171 JNA0.0657NA0.0629NA0.0439NA0.0465 2.3 9.7 0.0842 - 0.139 0.03 - 0.52SeleniumNA0.575NA0.480NA0.438NA0.602NA0.375 78 1,200 0.673 - 0.988 <0.1 - 0.8SilverNA0.0448 J BNA0.0369 JNA0.0175 JNA0.00090 JNA0.0226 J 78 1,200 ND ND - 5.0Notes:2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. Aside from metals, only those compounds detected in at least one sample are shown in the table above. Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses. Bold value indicates an exceedance of the Residential PSRGs and background levels in the case of metals.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; FG = final grade; NE = not established ft bgs= feet below ground surface; NS = not specified; -- = not applicable; ND = not detected; BDL = below laboratory method detection limitsJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. B = Analyte was detected in laboratory blank. Industrial/ Commercial PSRGs (1)Site-Specific Background MetalsRegional Background Metals (2)Final Grade10/28/2022 10/28/2022 10/28/2022 10/27/2022Screening Criteria1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022.mg/kgFG-110/18/2022FG-2 FG-3 FG-4 FG-5All BDLResidential PSRGs (1)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Boulevard Realty Estate Advisors (BOU)/BOU‐014 4920 Old Pineville Rd/Final Grade/Report/Tables/Data Table_Blythe Isenhour12/12/2022Table 1 Hart & Hickman, PC
Table 1Summary of Final Grade Soil Sample Analytical ResultsBlythe Isenhour Charlotte, North CarolinaBrownfields Project No. 23067-19-060H&H Job No. BOU-014Evaluation AreaSample IDDateDepth (ft bgs)1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2Sample Type Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Range RangeUnitsVOCs (8260D)Acetone0.028NA0.053NA0.025NA0.028NA0.032NA0.054NA14,000 210,000-- --Carbon disulfide<0.0007 NA <0.0008 NA <0.0008 NA0.0009 JNA0.001 JNA <0.0008 NA160 740-- --Methyl Ethyl Ketone (MEK)<0.0007 NA <0.0008 NA <0.0008 NA <0.0008 NA <0.0008 NA0.005 JNA5,500 40,000-- --SVOCs (8270E)-- -- -- --Metals (6020B/7471B/7199)ArsenicNA0.627NA18.4NA0.827NA0.768NA0.861NA1.73 0.68 3.0 3.67 - 6.47 1.0 - 18BariumNA246NA66.8NA144NA109NA145NA56.2 3,100 47,000 16.8 - 48.6 50 - 1,000CadmiumNA0.0533 JNA0.122 JNA0.0363 JNA<0.0309NA0.0449 JNA0.0405 J 1.4 20 ND 1.0 - 10Chromium (total)NA56.7NA42.3NA57.0NA32.9NA38.6NA35.6 NE NE 47.4 - 122 7.0 - 300Hexavalent ChromiumNA <0.161NA<0.168NA<0.175NA<0.171NA<0.166NA0.266 0.31 6.5 0.415 - 0.584 NSTrivalent ChromiumNA56.7NA42.3NA57.0NA32.9NA38.6NA35.3 23,000 350,000 47.0 - 121.4 NSLeadNA12.2NA21.0NA8.04NA8.36NA8.09NA15.0 400 800 6.44 - 15.1 ND - 50MercuryNA0.0406NA0.0418NA0.0393NA0.0254 JNA0.0269 JNA0.207 2.3 9.7 0.0842 - 0.139 0.03 - 0.52SeleniumNA0.244 JNA0.382NA0.242 JNA0.343NA0.255 JNA0.402 78 1,200 0.673 - 0.988 <0.1 - 0.8SilverNA0.0311 JNA0.0234 JNA0.0171 JNA0.0226 JNA0.0357 JNA0.0332 J 78 1,200 ND ND - 5.0Notes:2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. Aside from metals, only those compounds detected in at least one sample are shown in the table above. Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses. Bold value indicates an exceedance of the Residential PSRGs and background levels in the case of metals.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; FG = final grade; NE = not established ft bgs= feet below ground surface; NS = not specified; -- = not applicable; ND = not detected; BDL = below laboratory method detection limitsJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. B = Analyte was detected in laboratory blank. ALL BDLScreening CriteriaSite-Specific Background Metals Regional Background Metals (2)Residential PSRGs (1)Industrial/ Commercial PSRGs (1)Final GradeFG-1010/28/2022FG-610/27/2022FG-710/27/2022FG-810/27/2022FG-9 / DUP-0110/28/20221) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022.mg/kghttps://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Boulevard Realty Estate Advisors (BOU)/BOU‐014 4920 Old Pineville Rd/Final Grade/Report/Tables/Data Table_Blythe Isenhour12/12/2022Table 1 Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; USGS Global Ecosystems; U.S. CensusBureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S.Department of State Humanitarian Information Unit; and NOAA NationalCenters for Environmental Information, U.S. Coastal Relief Model. Datarefreshed August, 2021.
SITE LOCATION MAP
BLYTHE ISENHOUR4920 OLD PINEVILLE ROADCHARLOTTE, NORTH CAROLINA
DATE: 10-11-22
JOB NO: BOU-014
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-014 4920 Old Pineville Rd\Figures\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE WEST, NORTH CAROLINA 2022
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
REVISION NO. 0
JOB NO. BOU-014
DATE: 10-3-22
FIGURE NO. 2
BLYTHE ISENHOUR
4920 OLD PINEVILLE ROAD
CHARLOTTE, NORTH CAROLINA
SITE MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 GeologyOLD PINEVILLE ROADNOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS, 2020.
SELF STORAGE FACILITY
(4914 OLD PINEVILLE ROAD)
OLD PINEVILLE ROAD
BROWNFIELDS PROPERTY
FORMER QUEEN CITY BOILER
BPN 10061-06-060
(4928 OLD PINEVILLE ROAD)
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
LYNX LIGHT RAIL
PARCEL BOUNDARY
LIMITS OF 2003 EXCAVATION
AREA OF FORMER
UST SYSTEM
FORMER AST
CONTAINMENT AREAFORMER CONCRETE PAD
S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-014 4920 Old Pineville Rd\Additional Brownfields Assessment\Work Plan\Figures\Figures_20211109.dwg, FIG 4, 11/10/2021 8:08:57 AM, shaynes
REVISION NO. 0
JOB NO. BOU-014
DATE: 10-3-22
FIGURE NO. 3
HEARTWOOD TREE SERVICE4920 OLD PINEVILLE ROAD
CHARLOTTE, NORTH CAROLINA
FINAL GRADE SOIL SAMPLE
LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY LINE
LYNX LIGHT RAIL
PROPOSED BUILDING FOOTPRINT
HARDSCAPED SURFACE
LANDSCAPED SURFACE
ALIQUOT SOIL SAMPLE LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 GeologyOLD PINEVILLE ROADNOTES:
1. PARCEL DATA OBTAINED FROM MECKLENBURGCOUNTY GIS 2021.
2. LANDSCAPE PLAN PROVIDED BY BOHLERENGINEERING NC, PLLC, DATED 2-17-22.
FG-6
FG-5
FG-4
FG-3
FG-2
FG-1
FG-10
FG-9
FG-8
FG-7
BIRCHAM DRIVEANSTON DR
I
V
E THORNDALE LANECLEBURNE CO
U
R
TATLANTIS LANEA
A
A
A
A
AA
A
A
A
B
B
B
B
B
B
B
B
B
B
C
C
C
C
C
C
C
C
C
C
D
D
D
D
D
D
D
D
D
E
E
E
E
E
E
D
E
E
S:\AAA-Master Projects\Boulevard Realty Estate Advisors (BOU)\BOU-014 4920 Old Pineville Rd\Final Grade\Figures\Final Grade.dwg, FIG 2, SVincent

Appendix A
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/28/2022
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-291-0024 Client Project Description: BOU-014
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/18/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 33
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2022KY90047State ProgramKentucky
12/31/2022LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2022415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202284002State ProgramSouth Carolina
02/11/202302027State ProgramTennessee
09/30/2022T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/22-291-0024
Page 2 of 33
Report Number:
Sample Summary Table
Client Project Description:
22-291-0024
BOU-014
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
10/18/2022 13:00Solids 90924 FG-1 10/18/2022 13:54
10/18/2022 13:00Solids 90924 FG-1 10/18/2022 13:54 SW-7199 WP MTN -
10/18/2022 13:00Solids 90924 FG-1 10/18/2022 13:54 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 33
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-291-0024
Report Limit
Project:BOU-014
V 90924FG-1
1.87 10/27/2022 21:416020BArsenicmg/Kg - dry 0.106
73.0 10/27/2022 21:416020BBariummg/Kg - dry 0.053
J0.0366 10/27/2022 21:416020BCadmiummg/Kg - dry 0.0322
42.0 10/27/2022 21:416020BChromiummg/Kg - dry 0.144
15.9 10/27/2022 21:416020BLeadmg/Kg - dry 0.0386
0.575 10/27/2022 21:416020BSeleniummg/Kg - dry 0.128
JB0.0448 10/27/2022 21:416020BSilvermg/Kg - dry 0.0083
J0.0171 10/20/2022 14:157471BMercury (Total)mg/Kg - dry 0.0149
0.046 10/19/2022 17:468260DAcetonemg/Kg - dry 0.002
J0.002 10/19/2022 17:468260DCarbon Disulfide mg/Kg - dry 0.0008
19.7 10/24/2022 17:39SW-DRYWT Moisture %
Page 4 of 33

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: BOU-014 Lab Report Number: 22-291-0024
Date: 10/28/2022
Metals Analyses Method 6020B Sample 91115 (UT4-10-SE-V4) Analyte: Silver
QC Batch No: L645655/L645270 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 90924 (FG-1)
Analyte: Silver QC Batch No: L645866/L645270
Target analyte(s) was identified in the method blank associated with this project, below the Method Quantitation Limit. Per laboratory protocol any associated affected sample result is flagged "B" to indicate that it was detected
in the method blank.
Sample 91115 (UT4-10-SE-V4) Analyte: Chromium
QC Batch No: L645655/L645270 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 91115 (UT4-10-SE-V4) Analyte: Lead
QC Batch No: L645655/L645270 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91115 (UT4-10-SE-V4) Analyte: Lead QC Batch No: L645866/L645270 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91115 (UT4-10-SE-V4) Analyte: Selenium QC Batch No: L645655/L645270 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Semivolatile Organic Compounds - GC/MS Method 8270E Sample 90924 (FG-1) QC Batch No: V25455/V25303 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Page 5 of 33

Page 6 of 33
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-291-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/18/2022
BOU-014
Report Date : 10/28/2022
Sample ID :
Lab No :
Sampled:FG-1
90924 Matrix:
10/18/2022 13:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.7 %Moisture 1 10/24/22 17:39 SW-DRYWTAMB
<0.181 mg/Kg - dry 0.181 0.259Chromium, Hexavalent 1 10/25/22 16:08 SW-7199SAR
1.87 mg/Kg - dry 0.106 0.311Arsenic 5 10/27/22 21:41 6020BBKN
73.0 mg/Kg - dry 0.053 0.311Barium 5 10/27/22 21:41 6020BBKN
0.0366 J mg/Kg - dry 0.0322 0.311Cadmium 5 10/27/22 21:41 6020BBKN
42.0 mg/Kg - dry 0.144 0.311
Chromium 5 10/27/22 21:41 6020BBKN
15.9 mg/Kg - dry 0.0386 0.311Lead 5 10/27/22 21:41 6020BBKN
0.0171 J mg/Kg - dry 0.0149 0.0374Mercury (Total)1 10/20/22 14:15 7471BEDV
0.575 mg/Kg - dry 0.128 0.311Selenium 5 10/27/22 21:41 6020BBKN
0.0448 JB mg/Kg - dry 0.0083 0.311Silver 5 10/27/22 21:41 6020BBKN
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 7 of 33
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-291-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/18/2022
BOU-014
Report Date : 10/28/2022
Sample ID :
Lab No :
Sampled:FG-1
90924 Matrix:
10/18/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25311 10/19/22 08:00
0.046 mg/Kg - dry 0.002 0.024Acetone 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/19/22 17:46 V25312TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/19/22 17:46 V25312TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/19/22 17:46 V25312TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/19/22 17:46 V25312TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/19/22 17:46 V25312TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/19/22 17:46 V25312TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/19/22 17:46 V25312TBL
0.002 J mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/19/22 17:46 V25312TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/19/22 17:46 V25312TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/19/22 17:46 V25312TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/19/22 17:46 V25312TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/19/22 17:46 V25312TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/19/22 17:46 V25312TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 33
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-291-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/18/2022
BOU-014
Report Date : 10/28/2022
Sample ID :
Lab No :
Sampled:FG-1
90924 Matrix:
10/18/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25311 10/19/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/19/22 17:46 V25312TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/19/22 17:46 V25312TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/19/22 17:46 V25312TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/19/22 17:46 V25312TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/19/22 17:46 V25312TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/19/22 17:46 V25312TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/19/22 17:46 V25312TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/19/22 17:46 V25312TBL
<0.017 mg/Kg - dry 0.017 0.311Ethanol 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 10/19/22 17:46 V25312TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/19/22 17:46 V25312TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 33
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-291-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/18/2022
BOU-014
Report Date : 10/28/2022
Sample ID :
Lab No :
Sampled:FG-1
90924 Matrix:
10/18/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25311 10/19/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/19/22 17:46 V25312TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/19/22 17:46 V25312TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/19/22 17:46 V25312TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/19/22 17:46 V25312TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/19/22 17:46 V25312TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/19/22 17:46 V25312TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/19/22 17:46 V25312TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 10/19/22 17:46 V25312TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/19/22 17:46 V25312TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/19/22 17:46 V25312TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/19/22 17:46 V25312TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/19/22 17:46 V25312TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 33
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-291-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/18/2022
BOU-014
Report Date : 10/28/2022
Sample ID :
Lab No :
Sampled:FG-1
90924 Matrix:
10/18/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25311 10/19/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/19/22 17:46 V25312TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/19/22 17:46 V25312TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/19/22 17:46 V25312TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/19/22 17:46 V25312TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/19/22 17:46 V25312TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/19/22 17:46 V25312TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/19/22 17:46 V25312
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/19/22 17:461 TBL V25312
Surrogate: Dibromofluoromethane 108 Limits: 84-123%10/19/22 17:461 TBL V25312
Surrogate: Toluene-d8 90.3 Limits: 76-129%10/19/22 17:461 TBL V25312
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25303 10/19/22 10:30
<0.577 mg/Kg - dry 0.577 3.29Acenaphthene 4 10/21/22 23:32 V25455JMV
<0.523 mg/Kg - dry 0.523 3.29Acenaphthylene 4 10/21/22 23:32 V25455JMV
<0.757 mg/Kg - dry 0.757 3.29Aniline 4 10/21/22 23:32 V25455JMV
<0.712 mg/Kg - dry 0.712 3.29Anthracene 4 10/21/22 23:32 V25455JMV
<0.692 mg/Kg - dry 0.692 3.29
Benzo(a)anthracene 4 10/21/22 23:32 V25455JMV
<0.732 mg/Kg - dry 0.732 3.29Benzo(a)pyrene 4 10/21/22 23:32 V25455JMV
<0.727 mg/Kg - dry 0.727 3.29Benzo(b)fluoranthene 4 10/21/22 23:32 V25455JMV
<0.677 mg/Kg - dry 0.677 3.29Benzo(g,h,i)perylene 4 10/21/22 23:32 V25455JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 33
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-291-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/18/2022
BOU-014
Report Date : 10/28/2022
Sample ID :
Lab No :
Sampled:FG-1
90924 Matrix:
10/18/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25303 10/19/22 10:30
<0.682 mg/Kg - dry 0.682 3.29Benzo(k)fluoranthene 4 10/21/22 23:32 V25455JMV
<2.89 mg/Kg - dry 2.89 9.98Benzoic Acid 4 10/21/22 23:32 V25455JMV
<0.523 mg/Kg - dry 0.523 3.29Benzyl alcohol 4 10/21/22 23:32 V25455JMV
<0.587 mg/Kg - dry 0.587 3.29Bis(2-Chloroethoxy)methane 4 10/21/22 23:32 V25455JMV
<0.533 mg/Kg - dry 0.533 3.29Bis(2-Chloroethyl)ether 4 10/21/22 23:32 V25455JMV
<0.677 mg/Kg - dry 0.677 1.64Bis(2-Chloroisopropyl)ether 4 10/21/22 23:32 V25455JMV
<0.597 mg/Kg - dry 0.597 3.29Bis(2-ethylhexyl)phthalate 4 10/21/22 23:32 V25455JMV
<0.542 mg/Kg - dry 0.542 3.294-Bromophenyl phenyl ether 4 10/21/22 23:32 V25455JMV
<0.562 mg/Kg - dry 0.562 1.64
Butyl benzyl phthalate 4 10/21/22 23:32 V25455JMV
<0.460 mg/Kg - dry 0.460 3.294-Chloro-3-methylphenol 4 10/21/22 23:32 V25455JMV
<0.557 mg/Kg - dry 0.557 1.644-Chloroaniline 4 10/21/22 23:32 V25455JMV
<0.577 mg/Kg - dry 0.577 3.292-Chloronaphthalene 4 10/21/22 23:32 V25455JMV
<0.489 mg/Kg - dry 0.489 3.292-Chlorophenol 4 10/21/22 23:32 V25455JMV
<0.627 mg/Kg - dry 0.627 4.984-Chlorophenyl phenyl ether 4 10/21/22 23:32 V25455JMV
<0.707 mg/Kg - dry 0.707 3.29Chrysene 4 10/21/22 23:32 V25455JMV
<1.15 mg/Kg - dry 1.15 3.29
Dibenz(a,h)anthracene 4 10/21/22 23:32 V25455JMV
<0.592 mg/Kg - dry 0.592 3.29Dibenzofuran 4 10/21/22 23:32 V25455JMV
<0.470 mg/Kg - dry 0.470 3.291,2-Dichlorobenzene 4 10/21/22 23:32 V25455JMV
<0.484 mg/Kg - dry 0.484 3.291,3-Dichlorobenzene 4 10/21/22 23:32 V25455JMV
<0.485 mg/Kg - dry 0.485 1.641,4-Dichlorobenzene 4 10/21/22 23:32 V25455JMV
<0.732 mg/Kg - dry 0.732 3.293,3'-Dichlorobenzidine 4 10/21/22 23:32 V25455JMV
<0.476 mg/Kg - dry 0.476 3.292,4-Dichlorophenol 4 10/21/22 23:32 V25455JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 33
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-291-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/18/2022
BOU-014
Report Date : 10/28/2022
Sample ID :
Lab No :
Sampled:FG-1
90924 Matrix:
10/18/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25303 10/19/22 10:30
<0.896 mg/Kg - dry 0.896 3.29Diethyl phthalate 4 10/21/22 23:32 V25455JMV
<0.866 mg/Kg - dry 0.866 3.29Dimethyl phthalate 4 10/21/22 23:32 V25455JMV
<0.537 mg/Kg - dry 0.537 1.642,4-Dimethylphenol 4 10/21/22 23:32 V25455JMV
<0.533 mg/Kg - dry 0.533 3.29Di-n-butyl phthalate 4 10/21/22 23:32 V25455JMV
<1.20 mg/Kg - dry 1.20 7.474,6-Dinitro-2-methylphenol 4 10/21/22 23:32 V25455JMV
<2.59 mg/Kg - dry 2.59 7.472,4-Dinitrophenol 4 10/21/22 23:32 V25455JMV
<0.480 mg/Kg - dry 0.480 3.292,4-Dinitrotoluene 4 10/21/22 23:32 V25455JMV
<0.537 mg/Kg - dry 0.537 3.292,6-Dinitrotoluene 4 10/21/22 23:32 V25455JMV
<0.712 mg/Kg - dry 0.712 1.64
Di-n-Octyl Phthalate 4 10/21/22 23:32 V25455JMV
<0.612 mg/Kg - dry 0.612 3.29Fluoranthene 4 10/21/22 23:32 V25455JMV
<0.637 mg/Kg - dry 0.637 3.29Fluorene 4 10/21/22 23:32 V25455JMV
<0.528 mg/Kg - dry 0.528 3.29Hexachlorobenzene 4 10/21/22 23:32 V25455JMV
<0.485 mg/Kg - dry 0.485 3.29Hexachlorobutadiene 4 10/21/22 23:32 V25455JMV
<0.782 mg/Kg - dry 0.782 3.29Hexachlorocyclopentadiene 4 10/21/22 23:32 V25455JMV
<0.394 mg/Kg - dry 0.394 3.29Hexachloroethane 4 10/21/22 23:32 V25455JMV
<0.891 mg/Kg - dry 0.891 3.29
Indeno(1,2,3-cd)pyrene 4 10/21/22 23:32 V25455JMV
<0.951 mg/Kg - dry 0.951 3.29Isophorone 4 10/21/22 23:32 V25455JMV
<0.528 mg/Kg - dry 0.528 3.291-Methylnaphthalene 4 10/21/22 23:32 V25455JMV
<0.498 mg/Kg - dry 0.498 3.292-Methylnaphthalene 4 10/21/22 23:32 V25455JMV
<0.483 mg/Kg - dry 0.483 3.292-Methylphenol 4 10/21/22 23:32 V25455JMV
<0.423 mg/Kg - dry 0.423 3.293&4 Methylphenol 4 10/21/22 23:32 V25455JMV
<0.717 mg/Kg - dry 0.717 3.29Naphthalene 4 10/21/22 23:32 V25455JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 33
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-291-0024
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/18/2022
BOU-014
Report Date : 10/28/2022
Sample ID :
Lab No :
Sampled:FG-1
90924 Matrix:
10/18/2022 13:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25303 10/19/22 10:30
<0.481 mg/Kg - dry 0.481 3.292-Nitroaniline 4 10/21/22 23:32 V25455JMV
<0.597 mg/Kg - dry 0.597 3.293-Nitroaniline 4 10/21/22 23:32 V25455JMV
<0.464 mg/Kg - dry 0.464 1.644-Nitroaniline 4 10/21/22 23:32 V25455JMV
<0.577 mg/Kg - dry 0.577 1.64Nitrobenzene 4 10/21/22 23:32 V25455JMV
<0.442 mg/Kg - dry 0.442 3.292-Nitrophenol 4 10/21/22 23:32 V25455JMV
<0.582 mg/Kg - dry 0.582 3.294-Nitrophenol 4 10/21/22 23:32 V25455JMV
<1.31 mg/Kg - dry 1.31 3.29N-Nitrosodimethylamine 4 10/21/22 23:32 V25455JMV
<0.901 mg/Kg - dry 0.901 3.29N-Nitrosodiphenylamine 4 10/21/22 23:32 V25455JMV
<0.587 mg/Kg - dry 0.587 3.29
N-Nitroso-di-n-propylamine 4 10/21/22 23:32 V25455JMV
<1.73 mg/Kg - dry 1.73 4.98Pentachlorophenol 4 10/21/22 23:32 V25455JMV
<1.04 mg/Kg - dry 1.04 3.29Phenanthrene 4 10/21/22 23:32 V25455JMV
<0.557 mg/Kg - dry 0.557 3.29Phenol 4 10/21/22 23:32 V25455JMV
<0.667 mg/Kg - dry 0.667 3.29Pyrene 4 10/21/22 23:32 V25455JMV
<0.394 mg/Kg - dry 0.394 1.64Pyridine 4 10/21/22 23:32 V25455JMV
<0.533 mg/Kg - dry 0.533 3.291,2,4-Trichlorobenzene 4 10/21/22 23:32 V25455JMV
<0.479 mg/Kg - dry 0.479 3.29
2,4,5-Trichlorophenol 4 10/21/22 23:32 V25455JMV
<0.480 mg/Kg - dry 0.480 3.292,4,6-Trichlorophenol 4 10/21/22 23:32 V25455JMV
8270ESurrogate: Phenol-d5 82.3 Limits: 34-121%10/21/22 23:324 JMV
Surrogate: 2-Fluorobiphenyl 92.8 Limits: 44-115%10/21/22 23:324 JMV V25455
Surrogate: 2-Fluorophenol 82.9 Limits: 35-115%10/21/22 23:324 JMV V25455
Surrogate: Nitrobenzene-d5 80.2 Limits: 37-122%10/21/22 23:324 JMV V25455
Surrogate: 4-Terphenyl-d14 98.8 Limits: 54-127%10/21/22 23:324 JMV V25455
Surrogate: 2,4,6-Tribromophenol 90.4 Limits: 39-132%10/21/22 23:324 JMV V25455
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Page 14 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Metals Analyses
6020B
L645655,L645866QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L645270
Associated Lab Samples: 90924
LRB-L645270 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/27/22 11:160.2500.0855<0.0855mg/KgArsenic
10/27/22 11:160.2500.042<0.042mg/KgBarium
10/27/22 11:160.2500.0259<0.0259mg/KgCadmium
10/27/22 11:160.2500.116<0.116mg/KgChromium
10/27/22 11:160.2500.0310<0.0310mg/KgLead
10/27/22 11:160.2500.103<0.103mg/KgSelenium
10/27/22 20:340.2500.00670.0138mg/KgSilver
LCS-L645270Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.02.442.50mg/KgArsenic 80-120
97.04.875.00mg/KgBarium 80-120
91.00.4560.500mg/KgCadmium 80-120
97.04.845.00mg/KgChromium 80-120
1012.522.50mg/KgLead 80-120
97.04.855.00mg/KgSelenium 80-120
95.00.4760.500mg/KgSilver 80-120
V 91115-MS-L645270 V 91115-MSD-L645270Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
4.23 1003.822.302.401.82mg/KgArsenic 87.0 75-125 10.1 80
37.8 85.038.04.604.8033.7mg/KgBarium 93.0 75-125 0.5 80
18.3 10819.44.604.8013.1mg/KgChromium 137*75-125 5.8 80
183 -250*1692.302.40189mg/KgLead -850*75-125 7.9 80
Page 1 of 17* QC Fail Date:10/28/2022 05:21 PM
Page 15 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Metals Analyses
6020B
L645655,L645866QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L645270
V 91115-MS-L645270 V 91115-MSD-L645270Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
3.83 72.0*3.784.604.800.358mg/KgSelenium 74.0*75-125 1.3 80
1.43 83.01.930.4600.4801.03mg/KgSilver 195*75-125 29.7 80
V 91115-PDS-L645270Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/27/22 12:1198.01.34mg/KgArsenic
10/27/22 12:111025.85mg/KgBarium
10/27/22 12:111013.74mg/KgChromium
10/27/22 21:311015.97mg/KgLead
10/27/22 12:1198.02.36mg/KgSelenium
10/27/22 12:111110.380mg/KgSilver
Page 2 of 17* QC Fail Date:10/28/2022 05:21 PM
Page 16 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V25358QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V25297
Associated Lab Samples: 90924
LRB-V25297 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/20/22 14:090.03000.0120<0.0120mg/KgMercury (Total)
LCS-V25297Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1040.4330.417mg/KgMercury (Total)80-120
V 90924-MS-V25297 V 90924-MSD-V25297Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.375 90.00.3550.4170.4170.0137mg/KgMercury (Total)85.0 80-120 5.4 20
V 90924-PDS-V25297Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
10/20/22 14:251060.220mg/KgMercury (Total)
Page 3 of 17Date:10/28/2022 05:21 PM
Page 17 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25312QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25311
Associated Lab Samples: 90924
LRB-V25311 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/19/22 12:470.0200.002<0.002mg/KgAcetone
10/19/22 12:470.0200.001<0.001mg/KgAcrolein
10/19/22 12:470.0200.0008<0.0008mg/KgAcrylonitrile
10/19/22 12:470.0050.0006<0.0006mg/KgBenzene
10/19/22 12:470.0050.0005<0.0005mg/KgBromobenzene
10/19/22 12:470.0050.0008<0.0008mg/KgBromochloromethane
10/19/22 12:470.0050.001<0.001mg/KgBromodichloromethane
10/19/22 12:470.0050.001<0.001mg/KgBromoform
10/19/22 12:470.0100.001<0.001mg/KgBromomethane
10/19/22 12:470.0050.0005<0.0005mg/Kgn-Butylbenzene
10/19/22 12:470.0050.0006<0.0006mg/Kgsec-Butyl benzene
10/19/22 12:470.0050.0005<0.0005mg/Kgtert-Butyl benzene
10/19/22 12:470.0050.0006<0.0006mg/KgCarbon Disulfide
10/19/22 12:470.0050.001<0.001mg/KgCarbon Tetrachloride
10/19/22 12:470.0050.0007<0.0007mg/KgChlorobenzene
10/19/22 12:470.0050.0009<0.0009mg/KgChlorodibromomethane
10/19/22 12:470.0100.0009<0.0009mg/KgChloroethane
10/19/22 12:470.0050.001<0.001mg/KgChloroform
10/19/22 12:470.0100.0006<0.0006mg/KgChloromethane
10/19/22 12:470.0050.0005<0.0005mg/Kg2-Chlorotoluene
10/19/22 12:470.0050.0004<0.0004mg/Kg4-Chlorotoluene
10/19/22 12:470.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
10/19/22 12:470.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
10/19/22 12:470.0050.0006<0.0006mg/Kg1,2-Dibromoethane
10/19/22 12:470.0050.0006<0.0006mg/KgDibromomethane
10/19/22 12:470.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
10/19/22 12:470.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 17Date:10/28/2022 05:21 PM
Page 18 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25312QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25311
Associated Lab Samples: 90924
LRB-V25311 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/19/22 12:470.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
10/19/22 12:470.0100.001<0.001mg/KgDichlorodifluoromethane
10/19/22 12:470.0050.0008<0.0008mg/Kg1,1-Dichloroethane
10/19/22 12:470.0050.001<0.001mg/Kg1,2-Dichloroethane
10/19/22 12:470.0050.0007<0.0007mg/Kg1,1-Dichloroethene
10/19/22 12:470.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
10/19/22 12:470.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
10/19/22 12:470.0050.0004<0.0004mg/Kg1,2-Dichloropropane
10/19/22 12:470.0050.0006<0.0006mg/Kg1,3-Dichloropropane
10/19/22 12:470.0050.001<0.001mg/Kg2,2-Dichloropropane
10/19/22 12:470.0050.0008<0.0008mg/Kg1,1-Dichloropropene
10/19/22 12:470.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
10/19/22 12:470.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
10/19/22 12:470.2500.014<0.014mg/KgEthanol
10/19/22 12:470.0050.0006<0.0006mg/KgEthylbenzene
10/19/22 12:470.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
10/19/22 12:470.0100.0008<0.0008mg/KgHexachlorobutadiene
10/19/22 12:470.0100.0007<0.0007mg/Kgn-Hexane
10/19/22 12:470.0200.0006<0.0006mg/Kg2-Hexanone
10/19/22 12:470.0050.0005<0.0005mg/KgIsopropylbenzene
10/19/22 12:470.0050.001<0.001mg/Kg4-Isopropyl toluene
10/19/22 12:470.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
10/19/22 12:470.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
10/19/22 12:470.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
10/19/22 12:470.0100.001<0.001mg/KgMethylene Chloride
10/19/22 12:470.0100.0010<0.0010mg/KgNaphthalene
10/19/22 12:470.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 17Date:10/28/2022 05:21 PM
Page 19 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25312QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25311
Associated Lab Samples: 90924
LRB-V25311 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/19/22 12:470.0050.001<0.001mg/KgStyrene
10/19/22 12:470.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
10/19/22 12:470.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
10/19/22 12:470.0050.0009<0.0009mg/KgTetrachloroethene
10/19/22 12:470.0050.0007<0.0007mg/KgToluene
10/19/22 12:470.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
10/19/22 12:470.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
10/19/22 12:470.0050.001<0.001mg/Kg1,1,1-Trichloroethane
10/19/22 12:470.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
10/19/22 12:470.0050.0009<0.0009mg/KgTrichloroethene
10/19/22 12:470.0100.002<0.002mg/KgTrichlorofluoromethane
10/19/22 12:470.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
10/19/22 12:470.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
10/19/22 12:470.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
10/19/22 12:470.0100.0005<0.0005mg/KgVinyl Acetate
10/19/22 12:470.0100.0005<0.0005mg/KgVinyl Chloride
10/19/22 12:470.0050.0005<0.0005mg/Kgo-Xylene
10/19/22 12:470.0100.001<0.001mg/Kgm,p-Xylene
10/19/22 12:474-Bromofluorobenzene (S)96.8 70-130
10/19/22 12:47Dibromofluoromethane (S)96.8 84-123
10/19/22 12:47Toluene-d8 (S)88.2 76-129
LCS-V25311 LCSD-V25311Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.111 1111120.1120.100mg/KgAcetone 29-198 0.8 20
Page 6 of 17Date:10/28/2022 05:21 PM
Page 20 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25312QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25311
LCS-V25311 LCSD-V25311Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.109 1091180.1180.100mg/KgAcrolein 70-130 7.9 20
0.110 1101030.1030.100mg/KgAcrylonitrile 65-134 6.5 20
0.052 1051080.0540.050mg/KgBenzene 74-127 3.1 20
0.042 85.290.60.0450.050mg/KgBromobenzene 73-125 6.1 20
0.055 1101160.0570.050mg/KgBromochloromethane 72-134 4.9 20
0.048 97.699.20.0490.050mg/KgBromodichloromethane 75-122 1.6 20
0.047 95.898.80.0490.050mg/KgBromoform 66-135 3.0 20
0.062 1251210.0600.050mg/KgBromomethane 20-180 3.0 20
0.042 85.689.80.0440.050mg/Kgn-Butylbenzene 65-135 4.7 20
0.042 84.887.80.0430.050mg/Kgsec-Butyl benzene 66-131 3.4 20
0.042 84.087.00.0430.050mg/Kgtert-Butyl benzene 67-132 3.5 20
0.051 1031070.0530.050mg/KgCarbon Disulfide 61-129 3.6 20
0.050 1001020.0510.050mg/KgCarbon Tetrachloride 64-143 1.7 20
0.047 94.697.80.0480.050mg/KgChlorobenzene 74-118 3.3 20
0.048 96.298.60.0490.050mg/KgChlorodibromomethane 73-122 2.4 20
0.044 88.687.60.0430.050mg/KgChloroethane 33-149 1.1 20
0.053 1071060.0530.050mg/KgChloroform 73-127 1.3 20
0.038 76.278.40.0390.050mg/KgChloromethane 45-143 2.8 20
0.043 86.489.00.0440.050mg/Kg2-Chlorotoluene 67-124 2.9 20
0.043 86.489.00.0440.050mg/Kg4-Chlorotoluene 71-126 2.9 20
0.050 1021020.0510.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.7 20
0.050 10199.20.0490.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.1 20
0.049 99.81050.0520.050mg/Kg1,2-Dibromoethane 70-132 5.4 20
0.056 1121170.0580.050mg/KgDibromomethane 74-133 4.5 20
0.044 89.495.60.0470.050mg/Kg1,2-Dichlorobenzene 72-123 6.7 20
0.045 91.891.60.0450.050mg/Kg1,3-Dichlorobenzene 71-120 0.2 20
Page 7 of 17Date:10/28/2022 05:21 PM
Page 21 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25312QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25311
LCS-V25311 LCSD-V25311Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 88.490.80.0450.050mg/Kg1,4-Dichlorobenzene 71-123 2.6 20
0.034 68.672.60.0360.050mg/KgDichlorodifluoromethane 26-146 5.6 20
0.051 10298.40.0490.050mg/Kg1,1-Dichloroethane 74-127 3.5 20
0.051 1031030.0510.050mg/Kg1,2-Dichloroethane 68-128 0.1 20
0.048 97.41020.0500.050mg/Kg1,1-Dichloroethene 67-149 4.2 20
0.051 1041020.0500.050mg/Kgcis-1,2-Dichloroethene 76-134 1.9 20
0.048 96.296.00.0480.050mg/Kgtrans-1,2-Dichloroethene 73-132 0.2 20
0.052 1041090.0540.050mg/Kg1,2-Dichloropropane 73-130 4.3 20
0.046 93.295.80.0470.050mg/Kg1,3-Dichloropropane 75-124 2.7 20
0.052 1051030.0510.050mg/Kg2,2-Dichloropropane 50-142 2.1 20
0.055 1101110.0550.050mg/Kg1,1-Dichloropropene 71-130 0.9 20
0.053 1061090.0540.050mg/Kgcis-1,3-Dichloropropene 71-125 2.2 20
0.055 1121100.0540.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.8 20
1.42 1141161.451.25mg/KgEthanol 70-130 2.0 20
0.045 90.093.60.0460.050mg/KgEthylbenzene 74-128 3.9 20
0.107 1071070.1070.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.0 20
0.045 91.694.00.0470.050mg/KgHexachlorobutadiene 64-125 2.5 20
0.052 1051120.0560.050mg/Kgn-Hexane 70-130 6.6 20
0.052 1051080.0540.050mg/Kg2-Hexanone 61-157 3.1 20
0.043 86.691.60.0450.050mg/KgIsopropylbenzene 68-126 5.6 20
0.043 86.891.60.0450.050mg/Kg4-Isopropyl toluene 68-129 5.3 20
0.051 1021040.0520.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.7 20
0.053 1071080.0540.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.9 20
0.055 1111100.0540.050mg/Kg4-Methyl-2-Pentanone 57-162 0.9 20
0.042 85.287.80.0430.050mg/KgMethylene Chloride 74-129 3.0 20
0.044 89.893.00.0460.050mg/KgNaphthalene 57-157 3.5 20
Page 8 of 17Date:10/28/2022 05:21 PM
Page 22 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25312QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25311
LCS-V25311 LCSD-V25311Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.041 83.488.40.0440.050mg/Kgn-Propylbenzene 67-130 5.8 20
0.047 94.097.40.0480.050mg/KgStyrene 77-121 3.5 20
0.046 93.698.40.0490.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 5.0 20
0.047 95.694.40.0470.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.2 20
0.051 1031060.0520.050mg/KgTetrachloroethene 68-130 2.2 20
0.052 1041060.0530.050mg/KgToluene 71-129 1.7 20
0.047 94.097.40.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 3.5 20
0.045 91.893.80.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 2.1 20
0.051 1031060.0520.050mg/Kg1,1,1-Trichloroethane 67-131 2.6 20
0.049 98.01040.0510.050mg/Kg1,1,2-Trichloroethane 70-133 5.7 20
0.050 1021060.0530.050mg/KgTrichloroethene 75-133 4.6 20
0.042 85.487.40.0430.050mg/KgTrichlorofluoromethane 44-146 2.3 20
0.043 86.693.40.0460.050mg/Kg1,2,3-Trichloropropane 60-137 7.5 20
0.041 83.887.00.0430.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.7 20
0.041 83.886.80.0430.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.5 20
0.048 97.61110.0550.050mg/KgVinyl Acetate 60-140 13.0 20
0.041 82.288.00.0440.050mg/KgVinyl Chloride 48-147 6.8 20
0.045 91.493.40.0460.050mg/Kgo-Xylene 74-126 2.1 20
0.092 92.595.80.0950.100mg/Kgm,p-Xylene 75-124 3.5 20
1011014-Bromofluorobenzene (S)70-130
10298.0Dibromofluoromethane (S)84-123
91.289.6Toluene-d8 (S)76-129
Page 9 of 17Date:10/28/2022 05:21 PM
Page 23 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25455QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25303
Associated Lab Samples: 90924
LRB-V25303 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/21/22 13:030.6600.116<0.116mg/KgAcenaphthene
10/21/22 13:030.6600.105<0.105mg/KgAcenaphthylene
10/21/22 13:030.6600.152<0.152mg/KgAniline
10/21/22 13:030.6600.143<0.143mg/KgAnthracene
10/21/22 13:030.6600.139<0.139mg/KgBenzo(a)anthracene
10/21/22 13:030.6600.147<0.147mg/KgBenzo(a)pyrene
10/21/22 13:030.6600.146<0.146mg/KgBenzo(b)fluoranthene
10/21/22 13:030.6600.136<0.136mg/KgBenzo(g,h,i)perylene
10/21/22 13:030.6600.137<0.137mg/KgBenzo(k)fluoranthene
10/21/22 13:032.000.580<0.580mg/KgBenzoic Acid
10/21/22 13:030.6600.105<0.105mg/KgBenzyl alcohol
10/21/22 13:030.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
10/21/22 13:030.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
10/21/22 13:030.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
10/21/22 13:030.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
10/21/22 13:030.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
10/21/22 13:030.3300.113<0.113mg/KgButyl benzyl phthalate
10/21/22 13:030.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
10/21/22 13:030.3300.112<0.112mg/Kg4-Chloroaniline
10/21/22 13:030.6600.116<0.116mg/Kg2-Chloronaphthalene
10/21/22 13:030.6600.098<0.098mg/Kg2-Chlorophenol
10/21/22 13:031.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
10/21/22 13:030.6600.142<0.142mg/KgChrysene
10/21/22 13:030.6600.230<0.230mg/KgDibenz(a,h)anthracene
10/21/22 13:030.6600.119<0.119mg/KgDibenzofuran
10/21/22 13:030.6600.094<0.094mg/Kg1,2-Dichlorobenzene
10/21/22 13:030.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 10 of 17Date:10/28/2022 05:21 PM
Page 24 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25455QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25303
Associated Lab Samples: 90924
LRB-V25303 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/21/22 13:030.3300.097<0.097mg/Kg1,4-Dichlorobenzene
10/21/22 13:030.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
10/21/22 13:030.6600.095<0.095mg/Kg2,4-Dichlorophenol
10/21/22 13:030.6600.180<0.180mg/KgDiethyl phthalate
10/21/22 13:030.6600.174<0.174mg/KgDimethyl phthalate
10/21/22 13:030.3300.108<0.108mg/Kg2,4-Dimethylphenol
10/21/22 13:030.6600.107<0.107mg/KgDi-n-butyl phthalate
10/21/22 13:031.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
10/21/22 13:031.500.520<0.520mg/Kg2,4-Dinitrophenol
10/21/22 13:030.6600.096<0.096mg/Kg2,4-Dinitrotoluene
10/21/22 13:030.6600.108<0.108mg/Kg2,6-Dinitrotoluene
10/21/22 13:030.3300.143<0.143mg/KgDi-n-Octyl Phthalate
10/21/22 13:030.6600.123<0.123mg/KgFluoranthene
10/21/22 13:030.6600.128<0.128mg/KgFluorene
10/21/22 13:030.6600.106<0.106mg/KgHexachlorobenzene
10/21/22 13:030.6600.097<0.097mg/KgHexachlorobutadiene
10/21/22 13:030.6600.157<0.157mg/KgHexachlorocyclopentadiene
10/21/22 13:030.6600.079<0.079mg/KgHexachloroethane
10/21/22 13:030.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
10/21/22 13:030.6600.191<0.191mg/KgIsophorone
10/21/22 13:030.6600.106<0.106mg/Kg1-Methylnaphthalene
10/21/22 13:030.6600.100<0.100mg/Kg2-Methylnaphthalene
10/21/22 13:030.6600.097<0.097mg/Kg2-Methylphenol
10/21/22 13:030.6600.084<0.084mg/Kg3&4 Methylphenol
10/21/22 13:030.6600.144<0.144mg/KgNaphthalene
10/21/22 13:030.6600.096<0.096mg/Kg2-Nitroaniline
10/21/22 13:030.6600.120<0.120mg/Kg3-Nitroaniline
Page 11 of 17Date:10/28/2022 05:21 PM
Page 25 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25455QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25303
Associated Lab Samples: 90924
LRB-V25303 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/21/22 13:030.3300.093<0.093mg/Kg4-Nitroaniline
10/21/22 13:030.3300.116<0.116mg/KgNitrobenzene
10/21/22 13:030.6600.088<0.088mg/Kg2-Nitrophenol
10/21/22 13:030.6600.117<0.117mg/Kg4-Nitrophenol
10/21/22 13:030.6600.263<0.263mg/KgN-Nitrosodimethylamine
10/21/22 13:030.6600.181<0.181mg/KgN-Nitrosodiphenylamine
10/21/22 13:030.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
10/21/22 13:031.000.347<0.347mg/KgPentachlorophenol
10/21/22 13:030.6600.208<0.208mg/KgPhenanthrene
10/21/22 13:030.6600.112<0.112mg/KgPhenol
10/21/22 13:030.6600.134<0.134mg/KgPyrene
10/21/22 13:030.3300.079<0.079mg/KgPyridine
10/21/22 13:030.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
10/21/22 13:030.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
10/21/22 13:030.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
10/21/22 13:032-Fluorobiphenyl (S)92.8 44-115
10/21/22 13:032-Fluorophenol (S)90.6 35-115
10/21/22 13:03Nitrobenzene-d5 (S)86.2 37-122
10/21/22 13:034-Terphenyl-d14 (S)102 54-127
10/21/22 13:032,4,6-Tribromophenol (S)97.2 39-132
10/21/22 13:03Phenol-d5 (S)86.4 34-121
LCS-V25303 LCSD-V25303Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.72 1031011.681.67mg/KgAcenaphthene 40-123 2.3 20
Page 12 of 17Date:10/28/2022 05:21 PM
Page 26 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25455QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25303
LCS-V25303 LCSD-V25303Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.67 10098.21.641.67mg/KgAcenaphthylene 32-132 1.8 20
2.54 1521562.611.67mg/KgAniline 12-197 2.7 20
1.71 1021061.771.67mg/KgAnthracene 47-123 3.4 20
1.70 1021021.711.67mg/KgBenzo(a)anthracene 49-126 0.5 20
2.02 1211222.041.67mg/KgBenzo(a)pyrene 45-129 0.9 20
1.86 1111131.881.67mg/KgBenzo(b)fluoranthene 45-132 1.0 20
1.77 1061071.781.67mg/KgBenzo(g,h,i)perylene 43-134 0.5 20
1.83 1101081.811.67mg/KgBenzo(k)fluoranthene 47-132 1.0 20
1.19 71.267.01.121.67mg/KgBenzoic Acid 10-83 6.0 20
1.71 1021041.741.67mg/KgBenzyl alcohol 29-122 1.7 20
1.50 89.888.61.481.67mg/KgBis(2-Chloroethoxy)methane 36-121 1.3 20
1.43 85.691.01.521.67mg/KgBis(2-Chloroethyl)ether 31-120 6.1 20
1.53 91.693.41.561.67mg/KgBis(2-Chloroisopropyl)ether 33-131 1.9 20
1.88 1131131.881.67mg/KgBis(2-ethylhexyl)phthalate 51-133 0.0 20
1.77 1061071.781.67mg/Kg4-Bromophenyl phenyl ether 46-124 0.5 20
1.85 1111111.861.67mg/KgButyl benzyl phthalate 48-132 0.5 20
1.47 88.089.81.501.67mg/Kg4-Chloro-3-methylphenol 45-122 2.0 20
1.29 77.275.41.261.67mg/Kg4-Chloroaniline 17-106 2.3 20
1.70 10299.41.661.67mg/Kg2-Chloronaphthalene 41-114 2.3 20
1.61 96.497.61.631.67mg/Kg2-Chlorophenol 34-121 1.2 20
1.71 1021021.701.67mg/Kg4-Chlorophenyl phenyl ether 45-121 0.5 20
1.79 1071071.791.67mg/KgChrysene 50-124 0.0 20
1.83 1101101.831.67mg/KgDibenz(a,h)anthracene 45-134 0.0 20
1.69 10197.61.631.67mg/KgDibenzofuran 44-120 3.6 20
1.47 88.090.41.511.67mg/Kg1,2-Dichlorobenzene 33-117 2.6 20
1.46 87.488.61.481.67mg/Kg1,3-Dichlorobenzene 30-115 1.3 20
Page 13 of 17Date:10/28/2022 05:21 PM
Page 27 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25455QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25303
LCS-V25303 LCSD-V25303Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.44 86.286.21.441.67mg/Kg1,4-Dichlorobenzene 31-115 0.0 20
1.22 73.071.81.201.67mg/Kg3,3'-Dichlorobenzidine 22-121 1.6 20
1.50 89.888.61.481.67mg/Kg2,4-Dichlorophenol 40-122 1.3 20
1.76 1051051.761.67mg/KgDiethyl phthalate 50-124 0.0 20
1.71 1021021.701.67mg/KgDimethyl phthalate 48-124 0.5 20
1.56 93.492.81.551.67mg/Kg2,4-Dimethylphenol 30-127 0.6 20
1.88 1131141.911.67mg/KgDi-n-butyl phthalate 51-128 1.5 20
1.67 1001021.701.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 1.7 20
1.72 1031011.691.67mg/Kg2,4-Dinitrophenol 27-129 1.7 20
1.82 1091081.801.67mg/Kg2,4-Dinitrotoluene 48-126 1.1 20
1.82 1091071.791.67mg/Kg2,6-Dinitrotoluene 46-124 1.6 20
1.89 1131131.891.67mg/KgDi-n-Octyl Phthalate 45-140 0.0 20
1.73 1041041.741.67mg/KgFluoranthene 50-127 0.5 20
1.74 1041021.711.67mg/KgFluorene 43-125 1.7 20
1.77 1061051.761.67mg/KgHexachlorobenzene 45-122 0.5 20
1.41 84.485.01.421.67mg/KgHexachlorobutadiene 32-123 0.7 20
1.45 86.884.41.411.67mg/KgHexachlorocyclopentadiene 32-117 2.7 20
1.37 82.083.21.391.67mg/KgHexachloroethane 28-117 1.4 20
1.78 1071061.771.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 0.5 20
1.33 79.677.81.301.67mg/KgIsophorone 30-122 2.2 20
1.46 87.484.41.411.67mg/Kg1-Methylnaphthalene 40-119 3.4 20
1.40 83.882.01.371.67mg/Kg2-Methylnaphthalene 38-122 2.1 20
1.60 95.899.41.661.67mg/Kg2-Methylphenol 32-122 3.6 20
1.42 85.086.81.451.67mg/Kg3&4 Methylphenol 34-119 2.0 20
1.41 84.482.61.381.67mg/KgNaphthalene 35-123 2.1 20
1.71 1021021.701.67mg/Kg2-Nitroaniline 44-127 0.5 20
Page 14 of 17Date:10/28/2022 05:21 PM
Page 28 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25455QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25303
LCS-V25303 LCSD-V25303Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.55 92.890.41.511.67mg/Kg3-Nitroaniline 33-119 2.6 20
1.63 97.61011.691.67mg/Kg4-Nitroaniline 63-147 3.6 20
1.42 85.084.41.411.67mg/KgNitrobenzene 34-122 0.7 20
1.44 86.284.41.411.67mg/Kg2-Nitrophenol 36-123 2.1 20
1.77 1061021.701.67mg/Kg4-Nitrophenol 30-132 4.0 20
1.17 70.076.01.271.67mg/KgN-Nitrosodimethylamine 10-146 8.1 20
2.09 1251252.091.67mg/KgN-Nitrosodiphenylamine 38-127 0.0 20
1.50 89.892.81.551.67mg/KgN-Nitroso-di-n-propylamine 36-120 3.2 20
1.85 1111141.901.67mg/KgPentachlorophenol 25-133 2.6 20
1.72 1031041.741.67mg/KgPhenanthrene 50-121 1.1 20
1.58 94.697.01.621.67mg/KgPhenol 34-121 2.5 20
1.76 1051051.751.67mg/KgPyrene 47-127 0.5 20
0.987 59.162.21.041.67mg/KgPyridine 10-80 5.2 20
1.42 85.082.01.371.67mg/Kg1,2,4-Trichlorobenzene 34-118 3.5 20
1.66 99.497.01.621.67mg/Kg2,4,5-Trichlorophenol 41-124 2.4 20
1.66 99.41011.681.67mg/Kg2,4,6-Trichlorophenol 39-126 1.1 20
97.097.62-Fluorobiphenyl (S)44-115
96.31002-Fluorophenol (S)35-115
80.879.0Nitrobenzene-d5 (S)37-122
1051074-Terphenyl-d14 (S)54-127
1061062,4,6-Tribromophenol (S)39-132
91.595.1Phenol-d5 (S)34-121
Page 15 of 17Date:10/28/2022 05:21 PM
Page 29 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L645078QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L644782
Associated Lab Samples: 90924
LRB-L644782 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
10/25/22 14:080.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L644782Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
93.03.724.00mg/KgChromium, Hexavalent 80-120
V 91121-DUP-L644782Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 10/25/22 14:4120.2*0.2610.213mg/KgChromium, Hexavalent
V 91121-MS-L644782 V 91121-MSD-L644782Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec
34.1 86.844960739.0< 1.37mg/KgChromium, Hexavalent 73.9*75-125
Page 16 of 17* QC Fail Date:10/28/2022 05:21 PM
Page 30 of 33
Quality Control Data
22-291-0024Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
Dry Weight Determination
SW-DRYWT
V25474QC Analytical Batch:
Analysis Method:
Analysis Description:
V 90435-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 10/24/22 17:391.624.524.1%Moisture
V 91441-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 10/24/22 17:390.534.134.3%Moisture
Page 17 of 17Date:10/28/2022 05:21 PM
Page 31 of 33
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-291-0024
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 1.8C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:10/18/2022 14:29:31
Special precautions or instructions included?
Comments:
Page 32 of 33
Page 33 of 33

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

11/10/2022
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-301-0015 Client Project Description: BOU-014
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/28/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 119
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2022KY90047State ProgramKentucky
12/31/2022LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2022415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
02/11/202302027State ProgramTennessee
09/30/2022T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/22-301-0015
Page 2 of 119
Report Number:
Sample Summary Table
Client Project Description:
22-301-0015
BOU-014
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
10/28/2022 09:45Solids 91761 FG-2 10/28/2022 12:40
10/28/2022 09:45Solids 91761 FG-2 10/28/2022 12:40 SW-7199 WP MTN -
10/28/2022 09:45Solids 91761 FG-2 10/28/2022 12:40 6020B WP MTN -
10/28/2022 09:55Solids 91762 FG-3 10/28/2022 12:40
10/28/2022 09:55Solids 91762 FG-3 10/28/2022 12:40 6020B WP MTN -
10/28/2022 09:55Solids 91762 FG-3 10/28/2022 12:40 SW-7199 WP MTN -
10/28/2022 11:35Solids 91763 FG-4 10/28/2022 12:40
10/28/2022 11:35Solids 91763 FG-4 10/28/2022 12:40 SW-7199 WP MTN -
10/28/2022 11:35Solids 91763 FG-4 10/28/2022 12:40 6020B WP MTN -
10/27/2022 16:05Solids 91764 FG-5 10/28/2022 12:40
10/27/2022 16:05Solids 91764 FG-5 10/28/2022 12:40 SW-7199 WP MTN -
10/27/2022 16:05Solids 91764 FG-5 10/28/2022 12:40 6020B WP MTN -
10/27/2022 16:15Solids 91765 FG-6 10/28/2022 12:40
10/27/2022 16:15Solids 91765 FG-6 10/28/2022 12:40 SW-7199 WP MTN -
10/27/2022 16:15Solids 91765 FG-6 10/28/2022 12:40 6020B WP MTN -
10/27/2022 14:00Solids 91766 FG-7 10/28/2022 12:40
10/27/2022 14:00Solids 91766 FG-7 10/28/2022 12:40 SW-7199 WP MTN -
10/27/2022 14:00Solids 91766 FG-7 10/28/2022 12:40 6020B WP MTN -
10/27/2022 13:45Solids 91767 FG-8 10/28/2022 12:40
10/27/2022 13:45Solids 91767 FG-8 10/28/2022 12:40 SW-7199 WP MTN -
10/27/2022 13:45Solids 91767 FG-8 10/28/2022 12:40 6020B WP MTN -
10/28/2022 12:00Solids 91768 FG-9 10/28/2022 12:40
10/28/2022 12:00Solids 91768 FG-9 10/28/2022 12:40 SW-7199 WP MTN -
10/28/2022 12:00Solids 91768 FG-9 10/28/2022 12:40 6020B WP MTN -
10/28/2022 11:50Solids 91769 FG-10 10/28/2022 12:40
10/28/2022 11:50Solids 91769 FG-10 10/28/2022 12:40 SW-7199 WP MTN -
10/28/2022 11:50Solids 91769 FG-10 10/28/2022 12:40 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 119
Report Number:
Sample Summary Table
Client Project Description:
22-301-0015
BOU-014
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
10/28/2022Solids 91770 DUP-01 10/28/2022 12:40
10/28/2022Solids 91770 DUP-01 10/28/2022 12:40 SW-7199 WP MTN -
10/28/2022Solids 91770 DUP-01 10/28/2022 12:40 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 4 of 119
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-301-0015
Report Limit
Project:BOU-014
V 91761FG-2
1.92 11/04/2022 21:276020BArsenicmg/Kg - dry 0.106
61.2 11/04/2022 21:276020BBariummg/Kg - dry 0.052
J0.0597 11/04/2022 21:276020BCadmiummg/Kg - dry 0.0320
52.3 11/04/2022 21:276020BChromiummg/Kg - dry 0.143
13.0 11/04/2022 21:276020BLeadmg/Kg - dry 0.0384
0.480 11/04/2022 21:276020BSeleniummg/Kg - dry 0.127
J0.0369 11/04/2022 21:276020BSilvermg/Kg - dry 0.0083
0.0657 11/02/2022 16:017471BMercury (Total)mg/Kg - dry 0.0149
0.108 10/31/2022 18:248260DAcetonemg/Kg - dry 0.002
J0.011 10/31/2022 18:248260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
1.96 11/04/2022 15:14SW-7199 Chromium, Hexavalent mg/Kg - dry 0.174
19.3 11/04/2022 11:19SW-DRYWT Moisture %
V 91762FG-3
1.29 11/04/2022 21:336020BArsenicmg/Kg - dry 0.105
65.0 11/04/2022 21:336020BBariummg/Kg - dry 0.052
31.0 11/04/2022 21:336020BChromiummg/Kg - dry 0.142
6.97 11/04/2022 21:336020BLeadmg/Kg - dry 0.0380
0.438 11/04/2022 21:336020BSeleniummg/Kg - dry 0.126
J0.0175 11/04/2022 21:336020BSilvermg/Kg - dry 0.0082
0.0629 11/02/2022 16:187471BMercury (Total)mg/Kg - dry 0.0147
J0.022 10/31/2022 18:518260DAcetonemg/Kg - dry 0.002
3.72 11/04/2022 15:25SW-7199 Chromium, Hexavalent mg/Kg - dry 0.174
18.6 11/04/2022 11:19SW-DRYWT Moisture %
V 91763FG-4
1.57 11/04/2022 21:386020BArsenicmg/Kg - dry 0.108
35.4 11/04/2022 21:386020BBariummg/Kg - dry 0.054
26.4 11/04/2022 21:386020BChromiummg/Kg - dry 0.147
7.21 11/04/2022 21:386020BLeadmg/Kg - dry 0.0392
0.602 11/04/2022 21:386020BSeleniummg/Kg - dry 0.130
J0.0090 11/04/2022 21:386020BSilvermg/Kg - dry 0.0085
0.0439 11/02/2022 16:217471BMercury (Total)mg/Kg - dry 0.0152
0.032 10/31/2022 19:188260DAcetonemg/Kg - dry 0.003
2.29 11/04/2022 15:58SW-7199 Chromium, Hexavalent mg/Kg - dry 0.179
21.1 11/04/2022 11:19SW-DRYWT Moisture %
Page 5 of 119
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-301-0015
Report Limit
Project:BOU-014
V 91764FG-5
1.21 11/04/2022 21:446020BArsenicmg/Kg - dry 0.102
86.4 11/04/2022 21:446020BBariummg/Kg - dry 0.050
J0.0486 11/04/2022 21:446020BCadmiummg/Kg - dry 0.0308
29.6 11/04/2022 21:446020BChromiummg/Kg - dry 0.138
13.2 11/04/2022 21:446020BLeadmg/Kg - dry 0.0369
0.375 11/04/2022 21:446020BSeleniummg/Kg - dry 0.122
J0.0226 11/04/2022 21:446020BSilvermg/Kg - dry 0.0080
0.0465 11/02/2022 16:237471BMercury (Total)mg/Kg - dry 0.0143
0.056 10/31/2022 19:468260DAcetonemg/Kg - dry 0.002
J0.003 10/31/2022 19:468260DCarbon Disulfide mg/Kg - dry 0.0008
16.0 11/04/2022 11:19SW-DRYWT Moisture %
V 91765FG-6
0.627 11/04/2022 21:496020BArsenicmg/Kg - dry 0.0981
246 11/04/2022 21:496020BBariummg/Kg - dry 0.049
J0.0533 11/04/2022 21:496020BCadmiummg/Kg - dry 0.0297
56.7 11/07/2022 19:066020BChromiummg/Kg - dry 0.266
12.2 11/04/2022 21:496020BLeadmg/Kg - dry 0.0355
J0.244 11/04/2022 21:496020BSeleniummg/Kg - dry 0.118
J0.0311 11/04/2022 21:496020BSilvermg/Kg - dry 0.0077
0.0406 11/02/2022 16:267471BMercury (Total)mg/Kg - dry 0.0138
0.028 10/31/2022 20:138260DAcetonemg/Kg - dry 0.002
12.9 11/04/2022 11:19SW-DRYWT Moisture %
V 91766FG-7
18.4 11/04/2022 22:036020BArsenicmg/Kg - dry 0.102
66.8 11/04/2022 22:036020BBariummg/Kg - dry 0.051
J0.122 11/04/2022 22:036020BCadmiummg/Kg - dry 0.0310
42.3 11/07/2022 19:116020BChromiummg/Kg - dry 0.277
21.0 11/04/2022 22:036020BLeadmg/Kg - dry 0.0371
0.382 11/04/2022 22:036020BSeleniummg/Kg - dry 0.123
J0.0234 11/04/2022 22:036020BSilvermg/Kg - dry 0.0080
0.0418 11/02/2022 16:287471BMercury (Total)mg/Kg - dry 0.0144
0.053 10/31/2022 20:408260DAcetonemg/Kg - dry 0.002
16.5 11/04/2022 11:19SW-DRYWT Moisture %
V 91767FG-8
0.827 11/04/2022 22:096020BArsenicmg/Kg - dry 0.104
Page 6 of 119
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-301-0015
Report Limit
Project:BOU-014
V 91767FG-8
144 11/04/2022 22:096020BBariummg/Kg - dry 0.051
J0.0363 11/04/2022 22:096020BCadmiummg/Kg - dry 0.0313
57.0 11/07/2022 19:166020BChromiummg/Kg - dry 0.280
8.04 11/04/2022 22:096020BLeadmg/Kg - dry 0.0375
J0.242 11/04/2022 22:096020BSeleniummg/Kg - dry 0.124
J0.0171 11/04/2022 22:096020BSilvermg/Kg - dry 0.0081
0.0393 11/02/2022 16:317471BMercury (Total)mg/Kg - dry 0.0145
0.025 10/31/2022 21:078260DAcetonemg/Kg - dry 0.002
17.4 11/04/2022 11:19SW-DRYWT Moisture %
V 91768FG-9
0.768 11/04/2022 22:146020BArsenicmg/Kg - dry 0.102
109 11/04/2022 22:146020BBariummg/Kg - dry 0.051
32.9 11/07/2022 19:226020BChromiummg/Kg - dry 0.277
8.36 11/04/2022 22:146020BLeadmg/Kg - dry 0.0370
0.343 11/04/2022 22:146020BSeleniummg/Kg - dry 0.123
J0.0226 11/04/2022 22:146020BSilvermg/Kg - dry 0.0080
J0.0254 11/02/2022 16:337471BMercury (Total)mg/Kg - dry 0.0144
0.028 11/01/2022 12:418260DAcetonemg/Kg - dry 0.002
J0.0009 11/01/2022 12:418260DCarbon Disulfide mg/Kg - dry 0.0008
16.4 11/04/2022 11:19SW-DRYWT Moisture %
V 91769FG-10
1.73 11/04/2022 22:196020BArsenicmg/Kg - dry 0.104
56.2 11/04/2022 22:196020BBariummg/Kg - dry 0.051
J0.0405 11/04/2022 22:196020BCadmiummg/Kg - dry 0.0315
35.6 11/07/2022 19:366020BChromiummg/Kg - dry 0.282
15.0 11/04/2022 22:196020BLeadmg/Kg - dry 0.0377
0.402 11/04/2022 22:196020BSeleniummg/Kg - dry 0.125
J0.0332 11/04/2022 22:196020BSilvermg/Kg - dry 0.0081
0.207 11/02/2022 16:367471BMercury (Total)mg/Kg - dry 0.0146
0.054 10/31/2022 22:028260DAcetonemg/Kg - dry 0.002
J0.005 10/31/2022 22:028260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
0.266 11/04/2022 17:47SW-7199 Chromium, Hexavalent mg/Kg - dry 0.173
17.8 11/04/2022 11:19SW-DRYWT Moisture %
V 91770DUP-01
0.861 11/04/2022 22:256020BArsenicmg/Kg - dry 0.101
Page 7 of 119
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-301-0015
Report Limit
Project:BOU-014
V 91770DUP-01
145 11/04/2022 22:256020BBariummg/Kg - dry 0.050
J0.0449 11/04/2022 22:256020BCadmiummg/Kg - dry 0.0305
38.6 11/07/2022 19:416020BChromiummg/Kg - dry 0.273
8.09 11/04/2022 22:256020BLeadmg/Kg - dry 0.0365
J0.255 11/04/2022 22:256020BSeleniummg/Kg - dry 0.121
J0.0357 11/04/2022 22:256020BSilvermg/Kg - dry 0.0079
J0.0269 11/02/2022 16:457471BMercury (Total)mg/Kg - dry 0.0142
0.032 10/31/2022 22:298260DAcetonemg/Kg - dry 0.002
J0.001 10/31/2022 22:298260DCarbon Disulfide mg/Kg - dry 0.0008
15.3 11/04/2022 11:19SW-DRYWT Moisture %
Page 8 of 119

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: BOU-014 Lab Report Number: 22-301-0015
Date: 11/9/2022
Metals Analyses Method 6020B Sample 91802 (COMP-5 (2-4)) Analyte: Barium
QC Batch No: L647316/L646697 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91802 (COMP-5 (2-4)) Analyte: Chromium
QC Batch No: L647584/L646697 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91802 (COMP-5 (2-4)) Analyte: Lead
QC Batch No: L647316/L646697 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 91802 (COMP-5 (2-4)) Analyte: Selenium QC Batch No: L647316/L646697 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Hexavalent Chromium by Ion Chromatography Method SW-7199 QC Batch No: L647181 Insoluble Hexavalent Chromium spike data. QC Batch No: L647184
Insoluble Hexavalent Chromium spike data. Volatile Organic Compounds - GC/MS Method 8260D Analyte: 4-Methyl-2-pentanone QC Batch No: V25789/V25731 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Analyte: Acrylonitrile
QC Batch No: V25789/V25731 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Page 9 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91761 Matrix:
10/28/2022 9:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.3 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
1.96 mg/Kg - dry 0.174 0.247Chromium, Hexavalent 1 11/04/22 15:14 SW-7199SAR
1.92 mg/Kg - dry 0.106 0.310Arsenic 5 11/04/22 21:27 6020BCPW
61.2 mg/Kg - dry 0.052 0.309Barium 5 11/04/22 21:27 6020BCPW
0.0597 J mg/Kg - dry 0.0320 0.310Cadmium 5 11/04/22 21:27 6020BCPW
52.3 mg/Kg - dry 0.143 0.309
Chromium 5 11/04/22 21:27 6020BBKN
13.0 mg/Kg - dry 0.0384 0.310Lead 5 11/04/22 21:27 6020BCPW
0.0657 mg/Kg - dry 0.0149 0.0372Mercury (Total)1 11/02/22 16:01 7471BEDV
0.480 mg/Kg - dry 0.127 0.309Selenium 5 11/04/22 21:27 6020BCPW
0.0369 J mg/Kg - dry 0.0083 0.310Silver 5 11/04/22 21:27 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91761 Matrix:
10/28/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.108 mg/Kg - dry 0.002 0.024Acetone 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/31/22 18:24 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 18:24 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 18:24 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 18:24 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 18:24 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 18:24 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 18:24 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/31/22 18:24 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 18:24 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 18:24 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/31/22 18:24 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 18:24 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 18:24 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91761 Matrix:
10/28/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 18:24 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 18:24 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 18:24 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 18:24 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 18:24 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 18:24 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/31/22 18:24 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/31/22 18:24 V25732TBL
<0.017 mg/Kg - dry 0.017 0.309Ethanol 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 18:24 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/31/22 18:24 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91761 Matrix:
10/28/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/31/22 18:24 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/31/22 18:24 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 18:24 V25732TBL
0.011 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/31/22 18:24 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 18:24 V25732TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 18:24 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 18:24 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 10/31/22 18:24 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 18:24 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 18:24 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 18:24 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 18:24 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91761 Matrix:
10/28/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 18:24 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/31/22 18:24 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 18:24 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 18:24 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 18:24 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 18:24 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 18:24 V25732
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%10/31/22 18:241 TBL V25732
Surrogate: Dibromofluoromethane 105 Limits: 84-123%10/31/22 18:241 TBL V25732
Surrogate: Toluene-d8 89.6 Limits: 76-129%10/31/22 18:241 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.143 mg/Kg - dry 0.143 0.817Acenaphthene 1 11/04/22 23:44 V25983JMV
<0.130 mg/Kg - dry 0.130 0.817Acenaphthylene 1 11/04/22 23:44 V25983JMV
<0.188 mg/Kg - dry 0.188 0.817Aniline 1 11/04/22 23:44 V25983JMV
<0.177 mg/Kg - dry 0.177 0.817Anthracene 1 11/04/22 23:44 V25983JMV
<0.172 mg/Kg - dry 0.172 0.817
Benzo(a)anthracene 1 11/04/22 23:44 V25983JMV
<0.182 mg/Kg - dry 0.182 0.817Benzo(a)pyrene 1 11/04/22 23:44 V25983JMV
<0.180 mg/Kg - dry 0.180 0.817Benzo(b)fluoranthene 1 11/04/22 23:44 V25983JMV
<0.168 mg/Kg - dry 0.168 0.817Benzo(g,h,i)perylene 1 11/04/22 23:44 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91761 Matrix:
10/28/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.169 mg/Kg - dry 0.169 0.817Benzo(k)fluoranthene 1 11/04/22 23:44 V25983JMV
<0.718 mg/Kg - dry 0.718 2.48Benzoic Acid 1 11/04/22 23:44 V25983JMV
<0.130 mg/Kg - dry 0.130 0.817Benzyl alcohol 1 11/04/22 23:44 V25983JMV
<0.146 mg/Kg - dry 0.146 0.817Bis(2-Chloroethoxy)methane 1 11/04/22 23:44 V25983JMV
<0.132 mg/Kg - dry 0.132 0.817Bis(2-Chloroethyl)ether 1 11/04/22 23:44 V25983JMV
<0.168 mg/Kg - dry 0.168 0.408Bis(2-Chloroisopropyl)ether 1 11/04/22 23:44 V25983JMV
<0.148 mg/Kg - dry 0.148 0.817Bis(2-ethylhexyl)phthalate 1 11/04/22 23:44 V25983JMV
<0.135 mg/Kg - dry 0.135 0.8174-Bromophenyl phenyl ether 1 11/04/22 23:44 V25983JMV
<0.140 mg/Kg - dry 0.140 0.408
Butyl benzyl phthalate 1 11/04/22 23:44 V25983JMV
<0.114 mg/Kg - dry 0.114 0.8174-Chloro-3-methylphenol 1 11/04/22 23:44 V25983JMV
<0.138 mg/Kg - dry 0.138 0.4084-Chloroaniline 1 11/04/22 23:44 V25983JMV
<0.143 mg/Kg - dry 0.143 0.8172-Chloronaphthalene 1 11/04/22 23:44 V25983JMV
<0.121 mg/Kg - dry 0.121 0.8172-Chlorophenol 1 11/04/22 23:44 V25983JMV
<0.156 mg/Kg - dry 0.156 1.244-Chlorophenyl phenyl ether 1 11/04/22 23:44 V25983JMV
<0.175 mg/Kg - dry 0.175 0.817Chrysene 1 11/04/22 23:44 V25983JMV
<0.285 mg/Kg - dry 0.285 0.817
Dibenz(a,h)anthracene 1 11/04/22 23:44 V25983JMV
<0.147 mg/Kg - dry 0.147 0.817Dibenzofuran 1 11/04/22 23:44 V25983JMV
<0.116 mg/Kg - dry 0.116 0.8171,2-Dichlorobenzene 1 11/04/22 23:44 V25983JMV
<0.120 mg/Kg - dry 0.120 0.8171,3-Dichlorobenzene 1 11/04/22 23:44 V25983JMV
<0.120 mg/Kg - dry 0.120 0.4081,4-Dichlorobenzene 1 11/04/22 23:44 V25983JMV
<0.182 mg/Kg - dry 0.182 0.8173,3'-Dichlorobenzidine 1 11/04/22 23:44 V25983JMV
<0.118 mg/Kg - dry 0.118 0.8172,4-Dichlorophenol 1 11/04/22 23:44 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91761 Matrix:
10/28/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.223 mg/Kg - dry 0.223 0.817Diethyl phthalate 1 11/04/22 23:44 V25983JMV
<0.215 mg/Kg - dry 0.215 0.817Dimethyl phthalate 1 11/04/22 23:44 V25983JMV
<0.133 mg/Kg - dry 0.133 0.4082,4-Dimethylphenol 1 11/04/22 23:44 V25983JMV
<0.132 mg/Kg - dry 0.132 0.817Di-n-butyl phthalate 1 11/04/22 23:44 V25983JMV
<0.297 mg/Kg - dry 0.297 1.864,6-Dinitro-2-methylphenol 1 11/04/22 23:44 V25983JMV
<0.644 mg/Kg - dry 0.644 1.862,4-Dinitrophenol 1 11/04/22 23:44 V25983JMV
<0.119 mg/Kg - dry 0.119 0.8172,4-Dinitrotoluene 1 11/04/22 23:44 V25983JMV
<0.133 mg/Kg - dry 0.133 0.8172,6-Dinitrotoluene 1 11/04/22 23:44 V25983JMV
<0.177 mg/Kg - dry 0.177 0.408
Di-n-Octyl Phthalate 1 11/04/22 23:44 V25983JMV
<0.152 mg/Kg - dry 0.152 0.817Fluoranthene 1 11/04/22 23:44 V25983JMV
<0.158 mg/Kg - dry 0.158 0.817Fluorene 1 11/04/22 23:44 V25983JMV
<0.131 mg/Kg - dry 0.131 0.817Hexachlorobenzene 1 11/04/22 23:44 V25983JMV
<0.120 mg/Kg - dry 0.120 0.817Hexachlorobutadiene 1 11/04/22 23:44 V25983JMV
<0.194 mg/Kg - dry 0.194 0.817Hexachlorocyclopentadiene 1 11/04/22 23:44 V25983JMV
<0.098 mg/Kg - dry 0.098 0.817Hexachloroethane 1 11/04/22 23:44 V25983JMV
<0.221 mg/Kg - dry 0.221 0.817
Indeno(1,2,3-cd)pyrene 1 11/04/22 23:44 V25983JMV
<0.236 mg/Kg - dry 0.236 0.817Isophorone 1 11/04/22 23:44 V25983JMV
<0.131 mg/Kg - dry 0.131 0.8171-Methylnaphthalene 1 11/04/22 23:44 V25983JMV
<0.123 mg/Kg - dry 0.123 0.8172-Methylnaphthalene 1 11/04/22 23:44 V25983JMV
<0.120 mg/Kg - dry 0.120 0.8172-Methylphenol 1 11/04/22 23:44 V25983JMV
<0.105 mg/Kg - dry 0.105 0.8173&4 Methylphenol 1 11/04/22 23:44 V25983JMV
<0.178 mg/Kg - dry 0.178 0.817Naphthalene 1 11/04/22 23:44 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-2
91761 Matrix:
10/28/2022 9:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.119 mg/Kg - dry 0.119 0.8172-Nitroaniline 1 11/04/22 23:44 V25983JMV
<0.148 mg/Kg - dry 0.148 0.8173-Nitroaniline 1 11/04/22 23:44 V25983JMV
<0.115 mg/Kg - dry 0.115 0.4084-Nitroaniline 1 11/04/22 23:44 V25983JMV
<0.143 mg/Kg - dry 0.143 0.408Nitrobenzene 1 11/04/22 23:44 V25983JMV
<0.110 mg/Kg - dry 0.110 0.8172-Nitrophenol 1 11/04/22 23:44 V25983JMV
<0.144 mg/Kg - dry 0.144 0.8174-Nitrophenol 1 11/04/22 23:44 V25983JMV
<0.325 mg/Kg - dry 0.325 0.817N-Nitrosodimethylamine 1 11/04/22 23:44 V25983JMV
<0.224 mg/Kg - dry 0.224 0.817N-Nitrosodiphenylamine 1 11/04/22 23:44 V25983JMV
<0.146 mg/Kg - dry 0.146 0.817
N-Nitroso-di-n-propylamine 1 11/04/22 23:44 V25983JMV
<0.429 mg/Kg - dry 0.429 1.24Pentachlorophenol 1 11/04/22 23:44 V25983JMV
<0.257 mg/Kg - dry 0.257 0.817Phenanthrene 1 11/04/22 23:44 V25983JMV
<0.138 mg/Kg - dry 0.138 0.817Phenol 1 11/04/22 23:44 V25983JMV
<0.166 mg/Kg - dry 0.166 0.817Pyrene 1 11/04/22 23:44 V25983JMV
<0.098 mg/Kg - dry 0.098 0.408Pyridine 1 11/04/22 23:44 V25983JMV
<0.132 mg/Kg - dry 0.132 0.8171,2,4-Trichlorobenzene 1 11/04/22 23:44 V25983JMV
<0.119 mg/Kg - dry 0.119 0.817
2,4,5-Trichlorophenol 1 11/04/22 23:44 V25983JMV
<0.119 mg/Kg - dry 0.119 0.8172,4,6-Trichlorophenol 1 11/04/22 23:44 V25983JMV
8270ESurrogate: Phenol-d5 73.9 Limits: 34-121%11/04/22 23:441 JMV
Surrogate: 2-Fluorobiphenyl 88.6 Limits: 44-115%11/04/22 23:441 JMV V25983
Surrogate: 2-Fluorophenol 75.4 Limits: 35-115%11/04/22 23:441 JMV V25983
Surrogate: Nitrobenzene-d5 81.4 Limits: 37-122%11/04/22 23:441 JMV V25983
Surrogate: 4-Terphenyl-d14 94.0 Limits: 54-127%11/04/22 23:441 JMV V25983
Surrogate: 2,4,6-Tribromophenol 68.8 Limits: 39-132%11/04/22 23:441 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91762 Matrix:
10/28/2022 9:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.6 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
3.72 mg/Kg - dry 0.174 0.248Chromium, Hexavalent 1 11/04/22 15:25 SW-7199SAR
1.29 mg/Kg - dry 0.105 0.307Arsenic 5 11/04/22 21:33 6020BCPW
65.0 mg/Kg - dry 0.052 0.307Barium 5 11/04/22 21:33 6020BCPW
<0.0318 mg/Kg - dry 0.0318 0.307Cadmium 5 11/04/22 21:33 6020BCPW
31.0 mg/Kg - dry 0.142 0.307
Chromium 5 11/04/22 21:33 6020BBKN
6.97 mg/Kg - dry 0.0380 0.307Lead 5 11/04/22 21:33 6020BCPW
0.0629 mg/Kg - dry 0.0147 0.0369Mercury (Total)1 11/02/22 16:18 7471BEDV
0.438 mg/Kg - dry 0.126 0.307Selenium 5 11/04/22 21:33 6020BCPW
0.0175 J mg/Kg - dry 0.0082 0.307Silver 5 11/04/22 21:33 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91762 Matrix:
10/28/2022 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.022 J mg/Kg - dry 0.002 0.024Acetone 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/31/22 18:51 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 18:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 18:51 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 18:51 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 18:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 18:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 18:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/31/22 18:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 18:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 18:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/31/22 18:51 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 18:51 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 18:51 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91762 Matrix:
10/28/2022 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 18:51 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 18:51 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 18:51 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 18:51 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 18:51 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 18:51 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/31/22 18:51 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/31/22 18:51 V25732TBL
<0.017 mg/Kg - dry 0.017 0.307Ethanol 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 18:51 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/31/22 18:51 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91762 Matrix:
10/28/2022 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/31/22 18:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/31/22 18:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 18:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/31/22 18:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 18:51 V25732TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 18:51 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 18:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 10/31/22 18:51 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 18:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 18:51 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 18:51 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 18:51 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91762 Matrix:
10/28/2022 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 18:51 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/31/22 18:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 18:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 18:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 18:51 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 18:51 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 18:51 V25732
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/31/22 18:511 TBL V25732
Surrogate: Dibromofluoromethane 108 Limits: 84-123%10/31/22 18:511 TBL V25732
Surrogate: Toluene-d8 89.6 Limits: 76-129%10/31/22 18:511 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.142 mg/Kg - dry 0.142 0.810Acenaphthene 1 11/05/22 00:07 V25983JMV
<0.128 mg/Kg - dry 0.128 0.810Acenaphthylene 1 11/05/22 00:07 V25983JMV
<0.186 mg/Kg - dry 0.186 0.810Aniline 1 11/05/22 00:07 V25983JMV
<0.175 mg/Kg - dry 0.175 0.810Anthracene 1 11/05/22 00:07 V25983JMV
<0.170 mg/Kg - dry 0.170 0.810
Benzo(a)anthracene 1 11/05/22 00:07 V25983JMV
<0.180 mg/Kg - dry 0.180 0.810Benzo(a)pyrene 1 11/05/22 00:07 V25983JMV
<0.179 mg/Kg - dry 0.179 0.810Benzo(b)fluoranthene 1 11/05/22 00:07 V25983JMV
<0.167 mg/Kg - dry 0.167 0.810Benzo(g,h,i)perylene 1 11/05/22 00:07 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91762 Matrix:
10/28/2022 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.168 mg/Kg - dry 0.168 0.810Benzo(k)fluoranthene 1 11/05/22 00:07 V25983JMV
<0.712 mg/Kg - dry 0.712 2.46Benzoic Acid 1 11/05/22 00:07 V25983JMV
<0.128 mg/Kg - dry 0.128 0.810Benzyl alcohol 1 11/05/22 00:07 V25983JMV
<0.144 mg/Kg - dry 0.144 0.810Bis(2-Chloroethoxy)methane 1 11/05/22 00:07 V25983JMV
<0.131 mg/Kg - dry 0.131 0.810Bis(2-Chloroethyl)ether 1 11/05/22 00:07 V25983JMV
<0.167 mg/Kg - dry 0.167 0.405Bis(2-Chloroisopropyl)ether 1 11/05/22 00:07 V25983JMV
<0.147 mg/Kg - dry 0.147 0.810Bis(2-ethylhexyl)phthalate 1 11/05/22 00:07 V25983JMV
<0.133 mg/Kg - dry 0.133 0.8104-Bromophenyl phenyl ether 1 11/05/22 00:07 V25983JMV
<0.138 mg/Kg - dry 0.138 0.405
Butyl benzyl phthalate 1 11/05/22 00:07 V25983JMV
<0.113 mg/Kg - dry 0.113 0.8104-Chloro-3-methylphenol 1 11/05/22 00:07 V25983JMV
<0.137 mg/Kg - dry 0.137 0.4054-Chloroaniline 1 11/05/22 00:07 V25983JMV
<0.142 mg/Kg - dry 0.142 0.8102-Chloronaphthalene 1 11/05/22 00:07 V25983JMV
<0.120 mg/Kg - dry 0.120 0.8102-Chlorophenol 1 11/05/22 00:07 V25983JMV
<0.154 mg/Kg - dry 0.154 1.234-Chlorophenyl phenyl ether 1 11/05/22 00:07 V25983JMV
<0.174 mg/Kg - dry 0.174 0.810Chrysene 1 11/05/22 00:07 V25983JMV
<0.282 mg/Kg - dry 0.282 0.810
Dibenz(a,h)anthracene 1 11/05/22 00:07 V25983JMV
<0.146 mg/Kg - dry 0.146 0.810Dibenzofuran 1 11/05/22 00:07 V25983JMV
<0.115 mg/Kg - dry 0.115 0.8101,2-Dichlorobenzene 1 11/05/22 00:07 V25983JMV
<0.119 mg/Kg - dry 0.119 0.8101,3-Dichlorobenzene 1 11/05/22 00:07 V25983JMV
<0.119 mg/Kg - dry 0.119 0.4051,4-Dichlorobenzene 1 11/05/22 00:07 V25983JMV
<0.180 mg/Kg - dry 0.180 0.8103,3'-Dichlorobenzidine 1 11/05/22 00:07 V25983JMV
<0.117 mg/Kg - dry 0.117 0.8102,4-Dichlorophenol 1 11/05/22 00:07 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91762 Matrix:
10/28/2022 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.221 mg/Kg - dry 0.221 0.810Diethyl phthalate 1 11/05/22 00:07 V25983JMV
<0.213 mg/Kg - dry 0.213 0.810Dimethyl phthalate 1 11/05/22 00:07 V25983JMV
<0.132 mg/Kg - dry 0.132 0.4052,4-Dimethylphenol 1 11/05/22 00:07 V25983JMV
<0.131 mg/Kg - dry 0.131 0.810Di-n-butyl phthalate 1 11/05/22 00:07 V25983JMV
<0.294 mg/Kg - dry 0.294 1.844,6-Dinitro-2-methylphenol 1 11/05/22 00:07 V25983JMV
<0.638 mg/Kg - dry 0.638 1.842,4-Dinitrophenol 1 11/05/22 00:07 V25983JMV
<0.118 mg/Kg - dry 0.118 0.8102,4-Dinitrotoluene 1 11/05/22 00:07 V25983JMV
<0.132 mg/Kg - dry 0.132 0.8102,6-Dinitrotoluene 1 11/05/22 00:07 V25983JMV
<0.175 mg/Kg - dry 0.175 0.405
Di-n-Octyl Phthalate 1 11/05/22 00:07 V25983JMV
<0.151 mg/Kg - dry 0.151 0.810Fluoranthene 1 11/05/22 00:07 V25983JMV
<0.157 mg/Kg - dry 0.157 0.810Fluorene 1 11/05/22 00:07 V25983JMV
<0.130 mg/Kg - dry 0.130 0.810Hexachlorobenzene 1 11/05/22 00:07 V25983JMV
<0.119 mg/Kg - dry 0.119 0.810Hexachlorobutadiene 1 11/05/22 00:07 V25983JMV
<0.192 mg/Kg - dry 0.192 0.810Hexachlorocyclopentadiene 1 11/05/22 00:07 V25983JMV
<0.097 mg/Kg - dry 0.097 0.810Hexachloroethane 1 11/05/22 00:07 V25983JMV
<0.219 mg/Kg - dry 0.219 0.810
Indeno(1,2,3-cd)pyrene 1 11/05/22 00:07 V25983JMV
<0.234 mg/Kg - dry 0.234 0.810Isophorone 1 11/05/22 00:07 V25983JMV
<0.130 mg/Kg - dry 0.130 0.8101-Methylnaphthalene 1 11/05/22 00:07 V25983JMV
<0.122 mg/Kg - dry 0.122 0.8102-Methylnaphthalene 1 11/05/22 00:07 V25983JMV
<0.119 mg/Kg - dry 0.119 0.8102-Methylphenol 1 11/05/22 00:07 V25983JMV
<0.104 mg/Kg - dry 0.104 0.8103&4 Methylphenol 1 11/05/22 00:07 V25983JMV
<0.176 mg/Kg - dry 0.176 0.810Naphthalene 1 11/05/22 00:07 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-3
91762 Matrix:
10/28/2022 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.118 mg/Kg - dry 0.118 0.8102-Nitroaniline 1 11/05/22 00:07 V25983JMV
<0.147 mg/Kg - dry 0.147 0.8103-Nitroaniline 1 11/05/22 00:07 V25983JMV
<0.114 mg/Kg - dry 0.114 0.4054-Nitroaniline 1 11/05/22 00:07 V25983JMV
<0.142 mg/Kg - dry 0.142 0.405Nitrobenzene 1 11/05/22 00:07 V25983JMV
<0.109 mg/Kg - dry 0.109 0.8102-Nitrophenol 1 11/05/22 00:07 V25983JMV
<0.143 mg/Kg - dry 0.143 0.8104-Nitrophenol 1 11/05/22 00:07 V25983JMV
<0.323 mg/Kg - dry 0.323 0.810N-Nitrosodimethylamine 1 11/05/22 00:07 V25983JMV
<0.222 mg/Kg - dry 0.222 0.810N-Nitrosodiphenylamine 1 11/05/22 00:07 V25983JMV
<0.144 mg/Kg - dry 0.144 0.810
N-Nitroso-di-n-propylamine 1 11/05/22 00:07 V25983JMV
<0.426 mg/Kg - dry 0.426 1.23Pentachlorophenol 1 11/05/22 00:07 V25983JMV
<0.255 mg/Kg - dry 0.255 0.810Phenanthrene 1 11/05/22 00:07 V25983JMV
<0.137 mg/Kg - dry 0.137 0.810Phenol 1 11/05/22 00:07 V25983JMV
<0.164 mg/Kg - dry 0.164 0.810Pyrene 1 11/05/22 00:07 V25983JMV
<0.097 mg/Kg - dry 0.097 0.405Pyridine 1 11/05/22 00:07 V25983JMV
<0.131 mg/Kg - dry 0.131 0.8101,2,4-Trichlorobenzene 1 11/05/22 00:07 V25983JMV
<0.118 mg/Kg - dry 0.118 0.810
2,4,5-Trichlorophenol 1 11/05/22 00:07 V25983JMV
<0.118 mg/Kg - dry 0.118 0.8102,4,6-Trichlorophenol 1 11/05/22 00:07 V25983JMV
8270ESurrogate: Phenol-d5 70.7 Limits: 34-121%11/05/22 00:071 JMV
Surrogate: 2-Fluorobiphenyl 85.0 Limits: 44-115%11/05/22 00:071 JMV V25983
Surrogate: 2-Fluorophenol 72.2 Limits: 35-115%11/05/22 00:071 JMV V25983
Surrogate: Nitrobenzene-d5 78.4 Limits: 37-122%11/05/22 00:071 JMV V25983
Surrogate: 4-Terphenyl-d14 89.2 Limits: 54-127%11/05/22 00:071 JMV V25983
Surrogate: 2,4,6-Tribromophenol 67.7 Limits: 39-132%11/05/22 00:071 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-4
91763 Matrix:
10/28/2022 11:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.1 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
2.29 mg/Kg - dry 0.179 0.256Chromium, Hexavalent 1 11/04/22 15:58 SW-7199SAR
1.57 mg/Kg - dry 0.108 0.317Arsenic 5 11/04/22 21:38 6020BCPW
35.4 mg/Kg - dry 0.054 0.316Barium 5 11/04/22 21:38 6020BCPW
<0.0328 mg/Kg - dry 0.0328 0.317Cadmium 5 11/04/22 21:38 6020BCPW
26.4 mg/Kg - dry 0.147 0.316
Chromium 5 11/04/22 21:38 6020BBKN
7.21 mg/Kg - dry 0.0392 0.317Lead 5 11/04/22 21:38 6020BCPW
0.0439 mg/Kg - dry 0.0152 0.0380Mercury (Total)1 11/02/22 16:21 7471BEDV
0.602 mg/Kg - dry 0.130 0.316Selenium 5 11/04/22 21:38 6020BCPW
0.0090 J mg/Kg - dry 0.0085 0.317Silver 5 11/04/22 21:38 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-4
91763 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.032 mg/Kg - dry 0.003 0.025Acetone 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 10/31/22 19:18 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 10/31/22 19:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 19:18 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 19:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 19:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 19:18 V25732TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 10/31/22 19:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 19:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/31/22 19:18 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 19:18 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 19:18 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-4
91763 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 19:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/31/22 19:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 19:18 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 19:18 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 19:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 19:18 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 10/31/22 19:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 19:18 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 10/31/22 19:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 10/31/22 19:18 V25732TBL
<0.017 mg/Kg - dry 0.017 0.316Ethanol 1 10/31/22 19:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 10/31/22 19:18 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-4
91763 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/31/22 19:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 19:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 10/31/22 19:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 19:18 V25732TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 19:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 19:18 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 19:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/31/22 19:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 10/31/22 19:18 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 19:18 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 19:18 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 19:18 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-4
91763 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 19:18 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 19:18 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 19:18 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 19:18 V25732
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%10/31/22 19:181 TBL V25732
Surrogate: Dibromofluoromethane 106 Limits: 84-123%10/31/22 19:181 TBL V25732
Surrogate: Toluene-d8 91.4 Limits: 76-129%10/31/22 19:181 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.147 mg/Kg - dry 0.147 0.836Acenaphthene 1 11/04/22 22:15 V25983JMV
<0.133 mg/Kg - dry 0.133 0.836Acenaphthylene 1 11/04/22 22:15 V25983JMV
<0.192 mg/Kg - dry 0.192 0.836Aniline 1 11/04/22 22:15 V25983JMV
<0.181 mg/Kg - dry 0.181 0.836Anthracene 1 11/04/22 22:15 V25983JMV
<0.176 mg/Kg - dry 0.176 0.836
Benzo(a)anthracene 1 11/04/22 22:15 V25983JMV
<0.186 mg/Kg - dry 0.186 0.836Benzo(a)pyrene 1 11/04/22 22:15 V25983JMV
<0.185 mg/Kg - dry 0.185 0.836Benzo(b)fluoranthene 1 11/04/22 22:15 V25983JMV
<0.172 mg/Kg - dry 0.172 0.836Benzo(g,h,i)perylene 1 11/04/22 22:15 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-4
91763 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.173 mg/Kg - dry 0.173 0.836Benzo(k)fluoranthene 1 11/04/22 22:15 V25983JMV
<0.735 mg/Kg - dry 0.735 2.53Benzoic Acid 1 11/04/22 22:15 V25983JMV
<0.133 mg/Kg - dry 0.133 0.836Benzyl alcohol 1 11/04/22 22:15 V25983JMV
<0.149 mg/Kg - dry 0.149 0.836Bis(2-Chloroethoxy)methane 1 11/04/22 22:15 V25983JMV
<0.135 mg/Kg - dry 0.135 0.836Bis(2-Chloroethyl)ether 1 11/04/22 22:15 V25983JMV
<0.172 mg/Kg - dry 0.172 0.418Bis(2-Chloroisopropyl)ether 1 11/04/22 22:15 V25983JMV
<0.152 mg/Kg - dry 0.152 0.836Bis(2-ethylhexyl)phthalate 1 11/04/22 22:15 V25983JMV
<0.138 mg/Kg - dry 0.138 0.8364-Bromophenyl phenyl ether 1 11/04/22 22:15 V25983JMV
<0.143 mg/Kg - dry 0.143 0.418
Butyl benzyl phthalate 1 11/04/22 22:15 V25983JMV
<0.117 mg/Kg - dry 0.117 0.8364-Chloro-3-methylphenol 1 11/04/22 22:15 V25983JMV
<0.141 mg/Kg - dry 0.141 0.4184-Chloroaniline 1 11/04/22 22:15 V25983JMV
<0.147 mg/Kg - dry 0.147 0.8362-Chloronaphthalene 1 11/04/22 22:15 V25983JMV
<0.124 mg/Kg - dry 0.124 0.8362-Chlorophenol 1 11/04/22 22:15 V25983JMV
<0.159 mg/Kg - dry 0.159 1.274-Chlorophenyl phenyl ether 1 11/04/22 22:15 V25983JMV
<0.179 mg/Kg - dry 0.179 0.836Chrysene 1 11/04/22 22:15 V25983JMV
<0.291 mg/Kg - dry 0.291 0.836
Dibenz(a,h)anthracene 1 11/04/22 22:15 V25983JMV
<0.150 mg/Kg - dry 0.150 0.836Dibenzofuran 1 11/04/22 22:15 V25983JMV
<0.119 mg/Kg - dry 0.119 0.8361,2-Dichlorobenzene 1 11/04/22 22:15 V25983JMV
<0.123 mg/Kg - dry 0.123 0.8361,3-Dichlorobenzene 1 11/04/22 22:15 V25983JMV
<0.123 mg/Kg - dry 0.123 0.4181,4-Dichlorobenzene 1 11/04/22 22:15 V25983JMV
<0.186 mg/Kg - dry 0.186 0.8363,3'-Dichlorobenzidine 1 11/04/22 22:15 V25983JMV
<0.121 mg/Kg - dry 0.121 0.8362,4-Dichlorophenol 1 11/04/22 22:15 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-4
91763 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.228 mg/Kg - dry 0.228 0.836Diethyl phthalate 1 11/04/22 22:15 V25983JMV
<0.220 mg/Kg - dry 0.220 0.836Dimethyl phthalate 1 11/04/22 22:15 V25983JMV
<0.136 mg/Kg - dry 0.136 0.4182,4-Dimethylphenol 1 11/04/22 22:15 V25983JMV
<0.135 mg/Kg - dry 0.135 0.836Di-n-butyl phthalate 1 11/04/22 22:15 V25983JMV
<0.304 mg/Kg - dry 0.304 1.904,6-Dinitro-2-methylphenol 1 11/04/22 22:15 V25983JMV
<0.659 mg/Kg - dry 0.659 1.902,4-Dinitrophenol 1 11/04/22 22:15 V25983JMV
<0.122 mg/Kg - dry 0.122 0.8362,4-Dinitrotoluene 1 11/04/22 22:15 V25983JMV
<0.136 mg/Kg - dry 0.136 0.8362,6-Dinitrotoluene 1 11/04/22 22:15 V25983JMV
<0.181 mg/Kg - dry 0.181 0.418
Di-n-Octyl Phthalate 1 11/04/22 22:15 V25983JMV
<0.155 mg/Kg - dry 0.155 0.836Fluoranthene 1 11/04/22 22:15 V25983JMV
<0.162 mg/Kg - dry 0.162 0.836Fluorene 1 11/04/22 22:15 V25983JMV
<0.134 mg/Kg - dry 0.134 0.836Hexachlorobenzene 1 11/04/22 22:15 V25983JMV
<0.123 mg/Kg - dry 0.123 0.836Hexachlorobutadiene 1 11/04/22 22:15 V25983JMV
<0.198 mg/Kg - dry 0.198 0.836Hexachlorocyclopentadiene 1 11/04/22 22:15 V25983JMV
<0.100 mg/Kg - dry 0.100 0.836Hexachloroethane 1 11/04/22 22:15 V25983JMV
<0.226 mg/Kg - dry 0.226 0.836
Indeno(1,2,3-cd)pyrene 1 11/04/22 22:15 V25983JMV
<0.242 mg/Kg - dry 0.242 0.836Isophorone 1 11/04/22 22:15 V25983JMV
<0.134 mg/Kg - dry 0.134 0.8361-Methylnaphthalene 1 11/04/22 22:15 V25983JMV
<0.126 mg/Kg - dry 0.126 0.8362-Methylnaphthalene 1 11/04/22 22:15 V25983JMV
<0.122 mg/Kg - dry 0.122 0.8362-Methylphenol 1 11/04/22 22:15 V25983JMV
<0.107 mg/Kg - dry 0.107 0.8363&4 Methylphenol 1 11/04/22 22:15 V25983JMV
<0.182 mg/Kg - dry 0.182 0.836Naphthalene 1 11/04/22 22:15 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-4
91763 Matrix:
10/28/2022 11:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.122 mg/Kg - dry 0.122 0.8362-Nitroaniline 1 11/04/22 22:15 V25983JMV
<0.152 mg/Kg - dry 0.152 0.8363-Nitroaniline 1 11/04/22 22:15 V25983JMV
<0.118 mg/Kg - dry 0.118 0.4184-Nitroaniline 1 11/04/22 22:15 V25983JMV
<0.147 mg/Kg - dry 0.147 0.418Nitrobenzene 1 11/04/22 22:15 V25983JMV
<0.112 mg/Kg - dry 0.112 0.8362-Nitrophenol 1 11/04/22 22:15 V25983JMV
<0.148 mg/Kg - dry 0.148 0.8364-Nitrophenol 1 11/04/22 22:15 V25983JMV
<0.333 mg/Kg - dry 0.333 0.836N-Nitrosodimethylamine 1 11/04/22 22:15 V25983JMV
<0.229 mg/Kg - dry 0.229 0.836N-Nitrosodiphenylamine 1 11/04/22 22:15 V25983JMV
<0.149 mg/Kg - dry 0.149 0.836
N-Nitroso-di-n-propylamine 1 11/04/22 22:15 V25983JMV
<0.439 mg/Kg - dry 0.439 1.27Pentachlorophenol 1 11/04/22 22:15 V25983JMV
<0.263 mg/Kg - dry 0.263 0.836Phenanthrene 1 11/04/22 22:15 V25983JMV
<0.141 mg/Kg - dry 0.141 0.836Phenol 1 11/04/22 22:15 V25983JMV
<0.169 mg/Kg - dry 0.169 0.836Pyrene 1 11/04/22 22:15 V25983JMV
<0.100 mg/Kg - dry 0.100 0.418Pyridine 1 11/04/22 22:15 V25983JMV
<0.135 mg/Kg - dry 0.135 0.8361,2,4-Trichlorobenzene 1 11/04/22 22:15 V25983JMV
<0.121 mg/Kg - dry 0.121 0.836
2,4,5-Trichlorophenol 1 11/04/22 22:15 V25983JMV
<0.122 mg/Kg - dry 0.122 0.8362,4,6-Trichlorophenol 1 11/04/22 22:15 V25983JMV
8270ESurrogate: Phenol-d5 73.6 Limits: 34-121%11/04/22 22:151 JMV
Surrogate: 2-Fluorobiphenyl 88.0 Limits: 44-115%11/04/22 22:151 JMV V25983
Surrogate: 2-Fluorophenol 76.0 Limits: 35-115%11/04/22 22:151 JMV V25983
Surrogate: Nitrobenzene-d5 79.6 Limits: 37-122%11/04/22 22:151 JMV V25983
Surrogate: 4-Terphenyl-d14 95.8 Limits: 54-127%11/04/22 22:151 JMV V25983
Surrogate: 2,4,6-Tribromophenol 76.0 Limits: 39-132%11/04/22 22:151 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-5
91764 Matrix:
10/27/2022 16:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.0 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
<0.167 mg/Kg - dry 0.167 0.238Chromium, Hexavalent 1 11/04/22 16:09 SW-7199SAR
1.21 mg/Kg - dry 0.102 0.298Arsenic 5 11/04/22 21:44 6020BCPW
86.4 mg/Kg - dry 0.050 0.297Barium 5 11/04/22 21:44 6020BCPW
0.0486 J mg/Kg - dry 0.0308 0.298Cadmium 5 11/04/22 21:44 6020BCPW
29.6 mg/Kg - dry 0.138 0.297
Chromium 5 11/04/22 21:44 6020BBKN
13.2 mg/Kg - dry 0.0369 0.298Lead 5 11/04/22 21:44 6020BCPW
0.0465 mg/Kg - dry 0.0143 0.0357Mercury (Total)1 11/02/22 16:23 7471BEDV
0.375 mg/Kg - dry 0.122 0.297Selenium 5 11/04/22 21:44 6020BCPW
0.0226 J mg/Kg - dry 0.0080 0.298Silver 5 11/04/22 21:44 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-5
91764 Matrix:
10/27/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.056 mg/Kg - dry 0.002 0.023Acetone 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 10/31/22 19:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 10/31/22 19:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 10/31/22 19:46 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.005Bromochloromethane 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 10/31/22 19:46 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 10/31/22 19:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 10/31/22 19:46 V25732TBL
0.003 J mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 10/31/22 19:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 10/31/22 19:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.011Chloromethane 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 10/31/22 19:46 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 10/31/22 19:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 10/31/22 19:46 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-5
91764 Matrix:
10/27/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 10/31/22 19:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 10/31/22 19:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 10/31/22 19:46 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 10/31/22 19:46 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 10/31/22 19:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 10/31/22 19:46 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 10/31/22 19:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 10/31/22 19:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 10/31/22 19:46 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 10/31/22 19:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 10/31/22 19:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 10/31/22 19:46 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.005trans-1,3-Dichloropropene 1 10/31/22 19:46 V25732TBL
<0.016 mg/Kg - dry 0.016 0.297Ethanol 1 10/31/22 19:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 10/31/22 19:46 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 19:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 10/31/22 19:46 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-5
91764 Matrix:
10/27/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 10/31/22 19:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 10/31/22 19:46 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 10/31/22 19:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 10/31/22 19:46 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 10/31/22 19:46 V25732TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 10/31/22 19:46 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 10/31/22 19:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 10/31/22 19:46 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 10/31/22 19:46 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 10/31/22 19:46 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 10/31/22 19:46 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-5
91764 Matrix:
10/27/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 10/31/22 19:46 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 10/31/22 19:46 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 10/31/22 19:46 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 10/31/22 19:46 V25732
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/31/22 19:461 TBL V25732
Surrogate: Dibromofluoromethane 106 Limits: 84-123%10/31/22 19:461 TBL V25732
Surrogate: Toluene-d8 89.6 Limits: 76-129%10/31/22 19:461 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.138 mg/Kg - dry 0.138 0.785Acenaphthene 1 11/05/22 02:45 V25983JMV
<0.125 mg/Kg - dry 0.125 0.785Acenaphthylene 1 11/05/22 02:45 V25983JMV
<0.180 mg/Kg - dry 0.180 0.785Aniline 1 11/05/22 02:45 V25983JMV
<0.170 mg/Kg - dry 0.170 0.785Anthracene 1 11/05/22 02:45 V25983JMV
<0.165 mg/Kg - dry 0.165 0.785
Benzo(a)anthracene 1 11/05/22 02:45 V25983JMV
<0.175 mg/Kg - dry 0.175 0.785Benzo(a)pyrene 1 11/05/22 02:45 V25983JMV
<0.173 mg/Kg - dry 0.173 0.785Benzo(b)fluoranthene 1 11/05/22 02:45 V25983JMV
<0.161 mg/Kg - dry 0.161 0.785Benzo(g,h,i)perylene 1 11/05/22 02:45 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-5
91764 Matrix:
10/27/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.163 mg/Kg - dry 0.163 0.785Benzo(k)fluoranthene 1 11/05/22 02:45 V25983JMV
<0.690 mg/Kg - dry 0.690 2.38Benzoic Acid 1 11/05/22 02:45 V25983JMV
<0.125 mg/Kg - dry 0.125 0.785Benzyl alcohol 1 11/05/22 02:45 V25983JMV
<0.140 mg/Kg - dry 0.140 0.785Bis(2-Chloroethoxy)methane 1 11/05/22 02:45 V25983JMV
<0.127 mg/Kg - dry 0.127 0.785Bis(2-Chloroethyl)ether 1 11/05/22 02:45 V25983JMV
<0.161 mg/Kg - dry 0.161 0.392Bis(2-Chloroisopropyl)ether 1 11/05/22 02:45 V25983JMV
<0.142 mg/Kg - dry 0.142 0.785Bis(2-ethylhexyl)phthalate 1 11/05/22 02:45 V25983JMV
<0.129 mg/Kg - dry 0.129 0.7854-Bromophenyl phenyl ether 1 11/05/22 02:45 V25983JMV
<0.134 mg/Kg - dry 0.134 0.392
Butyl benzyl phthalate 1 11/05/22 02:45 V25983JMV
<0.110 mg/Kg - dry 0.110 0.7854-Chloro-3-methylphenol 1 11/05/22 02:45 V25983JMV
<0.133 mg/Kg - dry 0.133 0.3924-Chloroaniline 1 11/05/22 02:45 V25983JMV
<0.138 mg/Kg - dry 0.138 0.7852-Chloronaphthalene 1 11/05/22 02:45 V25983JMV
<0.116 mg/Kg - dry 0.116 0.7852-Chlorophenol 1 11/05/22 02:45 V25983JMV
<0.150 mg/Kg - dry 0.150 1.194-Chlorophenyl phenyl ether 1 11/05/22 02:45 V25983JMV
<0.169 mg/Kg - dry 0.169 0.785Chrysene 1 11/05/22 02:45 V25983JMV
<0.273 mg/Kg - dry 0.273 0.785
Dibenz(a,h)anthracene 1 11/05/22 02:45 V25983JMV
<0.141 mg/Kg - dry 0.141 0.785Dibenzofuran 1 11/05/22 02:45 V25983JMV
<0.112 mg/Kg - dry 0.112 0.7851,2-Dichlorobenzene 1 11/05/22 02:45 V25983JMV
<0.115 mg/Kg - dry 0.115 0.7851,3-Dichlorobenzene 1 11/05/22 02:45 V25983JMV
<0.116 mg/Kg - dry 0.116 0.3921,4-Dichlorobenzene 1 11/05/22 02:45 V25983JMV
<0.175 mg/Kg - dry 0.175 0.7853,3'-Dichlorobenzidine 1 11/05/22 02:45 V25983JMV
<0.114 mg/Kg - dry 0.114 0.7852,4-Dichlorophenol 1 11/05/22 02:45 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-5
91764 Matrix:
10/27/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.214 mg/Kg - dry 0.214 0.785Diethyl phthalate 1 11/05/22 02:45 V25983JMV
<0.207 mg/Kg - dry 0.207 0.785Dimethyl phthalate 1 11/05/22 02:45 V25983JMV
<0.128 mg/Kg - dry 0.128 0.3922,4-Dimethylphenol 1 11/05/22 02:45 V25983JMV
<0.127 mg/Kg - dry 0.127 0.785Di-n-butyl phthalate 1 11/05/22 02:45 V25983JMV
<0.285 mg/Kg - dry 0.285 1.794,6-Dinitro-2-methylphenol 1 11/05/22 02:45 V25983JMV
<0.619 mg/Kg - dry 0.619 1.792,4-Dinitrophenol 1 11/05/22 02:45 V25983JMV
<0.115 mg/Kg - dry 0.115 0.7852,4-Dinitrotoluene 1 11/05/22 02:45 V25983JMV
<0.128 mg/Kg - dry 0.128 0.7852,6-Dinitrotoluene 1 11/05/22 02:45 V25983JMV
<0.170 mg/Kg - dry 0.170 0.392
Di-n-Octyl Phthalate 1 11/05/22 02:45 V25983JMV
<0.146 mg/Kg - dry 0.146 0.785Fluoranthene 1 11/05/22 02:45 V25983JMV
<0.152 mg/Kg - dry 0.152 0.785Fluorene 1 11/05/22 02:45 V25983JMV
<0.126 mg/Kg - dry 0.126 0.785Hexachlorobenzene 1 11/05/22 02:45 V25983JMV
<0.116 mg/Kg - dry 0.116 0.785Hexachlorobutadiene 1 11/05/22 02:45 V25983JMV
<0.186 mg/Kg - dry 0.186 0.785Hexachlorocyclopentadiene 1 11/05/22 02:45 V25983JMV
<0.094 mg/Kg - dry 0.094 0.785Hexachloroethane 1 11/05/22 02:45 V25983JMV
<0.213 mg/Kg - dry 0.213 0.785
Indeno(1,2,3-cd)pyrene 1 11/05/22 02:45 V25983JMV
<0.227 mg/Kg - dry 0.227 0.785Isophorone 1 11/05/22 02:45 V25983JMV
<0.126 mg/Kg - dry 0.126 0.7851-Methylnaphthalene 1 11/05/22 02:45 V25983JMV
<0.119 mg/Kg - dry 0.119 0.7852-Methylnaphthalene 1 11/05/22 02:45 V25983JMV
<0.115 mg/Kg - dry 0.115 0.7852-Methylphenol 1 11/05/22 02:45 V25983JMV
<0.101 mg/Kg - dry 0.101 0.7853&4 Methylphenol 1 11/05/22 02:45 V25983JMV
<0.171 mg/Kg - dry 0.171 0.785Naphthalene 1 11/05/22 02:45 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-5
91764 Matrix:
10/27/2022 16:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.115 mg/Kg - dry 0.115 0.7852-Nitroaniline 1 11/05/22 02:45 V25983JMV
<0.142 mg/Kg - dry 0.142 0.7853-Nitroaniline 1 11/05/22 02:45 V25983JMV
<0.111 mg/Kg - dry 0.111 0.3924-Nitroaniline 1 11/05/22 02:45 V25983JMV
<0.138 mg/Kg - dry 0.138 0.392Nitrobenzene 1 11/05/22 02:45 V25983JMV
<0.105 mg/Kg - dry 0.105 0.7852-Nitrophenol 1 11/05/22 02:45 V25983JMV
<0.139 mg/Kg - dry 0.139 0.7854-Nitrophenol 1 11/05/22 02:45 V25983JMV
<0.313 mg/Kg - dry 0.313 0.785N-Nitrosodimethylamine 1 11/05/22 02:45 V25983JMV
<0.215 mg/Kg - dry 0.215 0.785N-Nitrosodiphenylamine 1 11/05/22 02:45 V25983JMV
<0.140 mg/Kg - dry 0.140 0.785
N-Nitroso-di-n-propylamine 1 11/05/22 02:45 V25983JMV
<0.413 mg/Kg - dry 0.413 1.19Pentachlorophenol 1 11/05/22 02:45 V25983JMV
<0.247 mg/Kg - dry 0.247 0.785Phenanthrene 1 11/05/22 02:45 V25983JMV
<0.133 mg/Kg - dry 0.133 0.785Phenol 1 11/05/22 02:45 V25983JMV
<0.159 mg/Kg - dry 0.159 0.785Pyrene 1 11/05/22 02:45 V25983JMV
<0.094 mg/Kg - dry 0.094 0.392Pyridine 1 11/05/22 02:45 V25983JMV
<0.127 mg/Kg - dry 0.127 0.7851,2,4-Trichlorobenzene 1 11/05/22 02:45 V25983JMV
<0.114 mg/Kg - dry 0.114 0.785
2,4,5-Trichlorophenol 1 11/05/22 02:45 V25983JMV
<0.115 mg/Kg - dry 0.115 0.7852,4,6-Trichlorophenol 1 11/05/22 02:45 V25983JMV
8270ESurrogate: Phenol-d5 71.2 Limits: 34-121%11/05/22 02:451 JMV
Surrogate: 2-Fluorobiphenyl 85.0 Limits: 44-115%11/05/22 02:451 JMV V25983
Surrogate: 2-Fluorophenol 74.2 Limits: 35-115%11/05/22 02:451 JMV V25983
Surrogate: Nitrobenzene-d5 79.6 Limits: 37-122%11/05/22 02:451 JMV V25983
Surrogate: 4-Terphenyl-d14 93.4 Limits: 54-127%11/05/22 02:451 JMV V25983
Surrogate: 2,4,6-Tribromophenol 67.9 Limits: 39-132%11/05/22 02:451 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-6
91765 Matrix:
10/27/2022 16:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.9 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
<0.161 mg/Kg - dry 0.161 0.229Chromium, Hexavalent 1 11/04/22 16:19 SW-7199SAR
0.627 mg/Kg - dry 0.0981 0.287Arsenic 5 11/04/22 21:49 6020BCPW
246 mg/Kg - dry 0.049 0.287Barium 5 11/04/22 21:49 6020BCPW
0.0533 J mg/Kg - dry 0.0297 0.287Cadmium 5 11/04/22 21:49 6020BCPW
56.7 mg/Kg - dry 0.266 0.574
Chromium 10 11/07/22 19:06 6020BBKN
12.2 mg/Kg - dry 0.0355 0.287Lead 5 11/04/22 21:49 6020BCPW
0.0406 mg/Kg - dry 0.0138 0.0344Mercury (Total)1 11/02/22 16:26 7471BEDV
0.244 J mg/Kg - dry 0.118 0.287Selenium 5 11/04/22 21:49 6020BCPW
0.0311 J mg/Kg - dry 0.0077 0.287Silver 5 11/04/22 21:49 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-6
91765 Matrix:
10/27/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.028 mg/Kg - dry 0.002 0.022Acetone 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 10/31/22 20:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 10/31/22 20:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 10/31/22 20:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 10/31/22 20:13 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 10/31/22 20:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 10/31/22 20:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 10/31/22 20:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 10/31/22 20:13 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 10/31/22 20:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 10/31/22 20:13 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-6
91765 Matrix:
10/27/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 10/31/22 20:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 10/31/22 20:13 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 10/31/22 20:13 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 10/31/22 20:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 10/31/22 20:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 10/31/22 20:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 10/31/22 20:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 10/31/22 20:13 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 10/31/22 20:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 10/31/22 20:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 10/31/22 20:13 V25732TBL
<0.016 mg/Kg - dry 0.016 0.287Ethanol 1 10/31/22 20:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 10/31/22 20:13 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 20:13 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 10/31/22 20:13 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-6
91765 Matrix:
10/27/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 10/31/22 20:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 10/31/22 20:13 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 10/31/22 20:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 10/31/22 20:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 10/31/22 20:13 V25732TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 10/31/22 20:13 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 10/31/22 20:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 10/31/22 20:13 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 10/31/22 20:13 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 10/31/22 20:13 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 10/31/22 20:13 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 10/31/22 20:13 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-6
91765 Matrix:
10/27/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 10/31/22 20:13 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 10/31/22 20:13 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 10/31/22 20:13 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 10/31/22 20:13 V25732
Surrogate: 4-Bromofluorobenzene 97.6 Limits: 70-130%10/31/22 20:131 TBL V25732
Surrogate: Dibromofluoromethane 107 Limits: 84-123%10/31/22 20:131 TBL V25732
Surrogate: Toluene-d8 90.0 Limits: 76-129%10/31/22 20:131 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.133 mg/Kg - dry 0.133 0.757Acenaphthene 1 11/07/22 18:13 V25983JMV
<0.120 mg/Kg - dry 0.120 0.757Acenaphthylene 1 11/07/22 18:13 V25983JMV
<0.174 mg/Kg - dry 0.174 0.757Aniline 1 11/07/22 18:13 V25983JMV
<0.164 mg/Kg - dry 0.164 0.757Anthracene 1 11/07/22 18:13 V25983JMV
<0.159 mg/Kg - dry 0.159 0.757
Benzo(a)anthracene 1 11/07/22 18:13 V25983JMV
<0.168 mg/Kg - dry 0.168 0.757Benzo(a)pyrene 1 11/07/22 18:13 V25983JMV
<0.167 mg/Kg - dry 0.167 0.757Benzo(b)fluoranthene 1 11/07/22 18:13 V25983JMV
<0.156 mg/Kg - dry 0.156 0.757Benzo(g,h,i)perylene 1 11/07/22 18:13 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-6
91765 Matrix:
10/27/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.157 mg/Kg - dry 0.157 0.757Benzo(k)fluoranthene 1 11/07/22 18:13 V25983JMV
<0.665 mg/Kg - dry 0.665 2.30Benzoic Acid 1 11/07/22 18:13 V25983JMV
<0.120 mg/Kg - dry 0.120 0.757Benzyl alcohol 1 11/07/22 18:13 V25983JMV
<0.135 mg/Kg - dry 0.135 0.757Bis(2-Chloroethoxy)methane 1 11/07/22 18:13 V25983JMV
<0.122 mg/Kg - dry 0.122 0.757Bis(2-Chloroethyl)ether 1 11/07/22 18:13 V25983JMV
<0.156 mg/Kg - dry 0.156 0.378Bis(2-Chloroisopropyl)ether 1 11/07/22 18:13 V25983JMV
<0.137 mg/Kg - dry 0.137 0.757Bis(2-ethylhexyl)phthalate 1 11/07/22 18:13 V25983JMV
<0.125 mg/Kg - dry 0.125 0.7574-Bromophenyl phenyl ether 1 11/07/22 18:13 V25983JMV
<0.129 mg/Kg - dry 0.129 0.378
Butyl benzyl phthalate 1 11/07/22 18:13 V25983JMV
<0.106 mg/Kg - dry 0.106 0.7574-Chloro-3-methylphenol 1 11/07/22 18:13 V25983JMV
<0.128 mg/Kg - dry 0.128 0.3784-Chloroaniline 1 11/07/22 18:13 V25983JMV
<0.133 mg/Kg - dry 0.133 0.7572-Chloronaphthalene 1 11/07/22 18:13 V25983JMV
<0.112 mg/Kg - dry 0.112 0.7572-Chlorophenol 1 11/07/22 18:13 V25983JMV
<0.144 mg/Kg - dry 0.144 1.154-Chlorophenyl phenyl ether 1 11/07/22 18:13 V25983JMV
<0.163 mg/Kg - dry 0.163 0.757Chrysene 1 11/07/22 18:13 V25983JMV
<0.264 mg/Kg - dry 0.264 0.757
Dibenz(a,h)anthracene 1 11/07/22 18:13 V25983JMV
<0.136 mg/Kg - dry 0.136 0.757Dibenzofuran 1 11/07/22 18:13 V25983JMV
<0.108 mg/Kg - dry 0.108 0.7571,2-Dichlorobenzene 1 11/07/22 18:13 V25983JMV
<0.111 mg/Kg - dry 0.111 0.7571,3-Dichlorobenzene 1 11/07/22 18:13 V25983JMV
<0.111 mg/Kg - dry 0.111 0.3781,4-Dichlorobenzene 1 11/07/22 18:13 V25983JMV
<0.168 mg/Kg - dry 0.168 0.7573,3'-Dichlorobenzidine 1 11/07/22 18:13 V25983JMV
<0.109 mg/Kg - dry 0.109 0.7572,4-Dichlorophenol 1 11/07/22 18:13 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-6
91765 Matrix:
10/27/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.206 mg/Kg - dry 0.206 0.757Diethyl phthalate 1 11/07/22 18:13 V25983JMV
<0.199 mg/Kg - dry 0.199 0.757Dimethyl phthalate 1 11/07/22 18:13 V25983JMV
<0.123 mg/Kg - dry 0.123 0.3782,4-Dimethylphenol 1 11/07/22 18:13 V25983JMV
<0.122 mg/Kg - dry 0.122 0.757Di-n-butyl phthalate 1 11/07/22 18:13 V25983JMV
<0.275 mg/Kg - dry 0.275 1.724,6-Dinitro-2-methylphenol 1 11/07/22 18:13 V25983JMV
<0.597 mg/Kg - dry 0.597 1.722,4-Dinitrophenol 1 11/07/22 18:13 V25983JMV
<0.110 mg/Kg - dry 0.110 0.7572,4-Dinitrotoluene 1 11/07/22 18:13 V25983JMV
<0.123 mg/Kg - dry 0.123 0.7572,6-Dinitrotoluene 1 11/07/22 18:13 V25983JMV
<0.164 mg/Kg - dry 0.164 0.378
Di-n-Octyl Phthalate 1 11/07/22 18:13 V25983JMV
<0.141 mg/Kg - dry 0.141 0.757Fluoranthene 1 11/07/22 18:13 V25983JMV
<0.146 mg/Kg - dry 0.146 0.757Fluorene 1 11/07/22 18:13 V25983JMV
<0.121 mg/Kg - dry 0.121 0.757Hexachlorobenzene 1 11/07/22 18:13 V25983JMV
<0.112 mg/Kg - dry 0.112 0.757Hexachlorobutadiene 1 11/07/22 18:13 V25983JMV
<0.180 mg/Kg - dry 0.180 0.757Hexachlorocyclopentadiene 1 11/07/22 18:13 V25983JMV
<0.090 mg/Kg - dry 0.090 0.757Hexachloroethane 1 11/07/22 18:13 V25983JMV
<0.205 mg/Kg - dry 0.205 0.757
Indeno(1,2,3-cd)pyrene 1 11/07/22 18:13 V25983JMV
<0.219 mg/Kg - dry 0.219 0.757Isophorone 1 11/07/22 18:13 V25983JMV
<0.121 mg/Kg - dry 0.121 0.7571-Methylnaphthalene 1 11/07/22 18:13 V25983JMV
<0.114 mg/Kg - dry 0.114 0.7572-Methylnaphthalene 1 11/07/22 18:13 V25983JMV
<0.111 mg/Kg - dry 0.111 0.7572-Methylphenol 1 11/07/22 18:13 V25983JMV
<0.097 mg/Kg - dry 0.097 0.7573&4 Methylphenol 1 11/07/22 18:13 V25983JMV
<0.165 mg/Kg - dry 0.165 0.757Naphthalene 1 11/07/22 18:13 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-6
91765 Matrix:
10/27/2022 16:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.111 mg/Kg - dry 0.111 0.7572-Nitroaniline 1 11/07/22 18:13 V25983JMV
<0.137 mg/Kg - dry 0.137 0.7573-Nitroaniline 1 11/07/22 18:13 V25983JMV
<0.107 mg/Kg - dry 0.107 0.3784-Nitroaniline 1 11/07/22 18:13 V25983JMV
<0.133 mg/Kg - dry 0.133 0.378Nitrobenzene 1 11/07/22 18:13 V25983JMV
<0.101 mg/Kg - dry 0.101 0.7572-Nitrophenol 1 11/07/22 18:13 V25983JMV
<0.134 mg/Kg - dry 0.134 0.7574-Nitrophenol 1 11/07/22 18:13 V25983JMV
<0.301 mg/Kg - dry 0.301 0.757N-Nitrosodimethylamine 1 11/07/22 18:13 V25983JMV
<0.207 mg/Kg - dry 0.207 0.757N-Nitrosodiphenylamine 1 11/07/22 18:13 V25983JMV
<0.135 mg/Kg - dry 0.135 0.757
N-Nitroso-di-n-propylamine 1 11/07/22 18:13 V25983JMV
<0.398 mg/Kg - dry 0.398 1.15Pentachlorophenol 1 11/07/22 18:13 V25983JMV
<0.238 mg/Kg - dry 0.238 0.757Phenanthrene 1 11/07/22 18:13 V25983JMV
<0.128 mg/Kg - dry 0.128 0.757Phenol 1 11/07/22 18:13 V25983JMV
<0.153 mg/Kg - dry 0.153 0.757Pyrene 1 11/07/22 18:13 V25983JMV
<0.090 mg/Kg - dry 0.090 0.378Pyridine 1 11/07/22 18:13 V25983JMV
<0.122 mg/Kg - dry 0.122 0.7571,2,4-Trichlorobenzene 1 11/07/22 18:13 V25983JMV
<0.110 mg/Kg - dry 0.110 0.757
2,4,5-Trichlorophenol 1 11/07/22 18:13 V25983JMV
<0.110 mg/Kg - dry 0.110 0.7572,4,6-Trichlorophenol 1 11/07/22 18:13 V25983JMV
8270ESurrogate: Phenol-d5 70.6 Limits: 34-121%11/07/22 18:131 JMV
Surrogate: 2-Fluorobiphenyl 83.8 Limits: 44-115%11/07/22 18:131 JMV V25983
Surrogate: 2-Fluorophenol 75.4 Limits: 35-115%11/07/22 18:131 JMV V25983
Surrogate: Nitrobenzene-d5 79.6 Limits: 37-122%11/07/22 18:131 JMV V25983
Surrogate: 4-Terphenyl-d14 99.4 Limits: 54-127%11/07/22 18:131 JMV V25983
Surrogate: 2,4,6-Tribromophenol 68.2 Limits: 39-132%11/07/22 18:131 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-7
91766 Matrix:
10/27/2022 14:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.5 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
<0.168 mg/Kg - dry 0.168 0.240Chromium, Hexavalent 1 11/04/22 16:30 SW-7199SAR
18.4 mg/Kg - dry 0.102 0.299Arsenic 5 11/04/22 22:03 6020BCPW
66.8 mg/Kg - dry 0.051 0.299Barium 5 11/04/22 22:03 6020BCPW
0.122 J mg/Kg - dry 0.0310 0.299Cadmium 5 11/04/22 22:03 6020BCPW
42.3 mg/Kg - dry 0.277 0.598
Chromium 10 11/07/22 19:11 6020BBKN
21.0 mg/Kg - dry 0.0371 0.299Lead 5 11/04/22 22:03 6020BCPW
0.0418 mg/Kg - dry 0.0144 0.0359Mercury (Total)1 11/02/22 16:28 7471BEDV
0.382 mg/Kg - dry 0.123 0.299Selenium 5 11/04/22 22:03 6020BCPW
0.0234 J mg/Kg - dry 0.0080 0.299Silver 5 11/04/22 22:03 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-7
91766 Matrix:
10/27/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.053 mg/Kg - dry 0.002 0.023Acetone 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 10/31/22 20:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 10/31/22 20:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 10/31/22 20:40 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.005Bromochloromethane 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 10/31/22 20:40 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 10/31/22 20:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 10/31/22 20:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 10/31/22 20:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 10/31/22 20:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.011Chloromethane 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 10/31/22 20:40 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 10/31/22 20:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 10/31/22 20:40 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-7
91766 Matrix:
10/27/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 10/31/22 20:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 10/31/22 20:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 10/31/22 20:40 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 10/31/22 20:40 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 10/31/22 20:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 10/31/22 20:40 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 10/31/22 20:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 10/31/22 20:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 10/31/22 20:40 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 10/31/22 20:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 10/31/22 20:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 10/31/22 20:40 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.005trans-1,3-Dichloropropene 1 10/31/22 20:40 V25732TBL
<0.016 mg/Kg - dry 0.016 0.299Ethanol 1 10/31/22 20:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 10/31/22 20:40 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 20:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 10/31/22 20:40 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-7
91766 Matrix:
10/27/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 10/31/22 20:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Isopropylbenzene 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 10/31/22 20:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 10/31/22 20:40 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 10/31/22 20:40 V25732TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 10/31/22 20:40 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 10/31/22 20:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 10/31/22 20:40 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 10/31/22 20:40 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 10/31/22 20:40 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 10/31/22 20:40 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-7
91766 Matrix:
10/27/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Acetate 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 10/31/22 20:40 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 10/31/22 20:40 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 10/31/22 20:40 V25732
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%10/31/22 20:401 TBL V25732
Surrogate: Dibromofluoromethane 109 Limits: 84-123%10/31/22 20:401 TBL V25732
Surrogate: Toluene-d8 89.2 Limits: 76-129%10/31/22 20:401 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.138 mg/Kg - dry 0.138 0.791Acenaphthene 1 11/05/22 02:00 V25983JMV
<0.125 mg/Kg - dry 0.125 0.791Acenaphthylene 1 11/05/22 02:00 V25983JMV
<0.182 mg/Kg - dry 0.182 0.791Aniline 1 11/05/22 02:00 V25983JMV
<0.171 mg/Kg - dry 0.171 0.791Anthracene 1 11/05/22 02:00 V25983JMV
<0.166 mg/Kg - dry 0.166 0.791
Benzo(a)anthracene 1 11/05/22 02:00 V25983JMV
<0.176 mg/Kg - dry 0.176 0.791Benzo(a)pyrene 1 11/05/22 02:00 V25983JMV
<0.174 mg/Kg - dry 0.174 0.791Benzo(b)fluoranthene 1 11/05/22 02:00 V25983JMV
<0.162 mg/Kg - dry 0.162 0.791Benzo(g,h,i)perylene 1 11/05/22 02:00 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-7
91766 Matrix:
10/27/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.164 mg/Kg - dry 0.164 0.791Benzo(k)fluoranthene 1 11/05/22 02:00 V25983JMV
<0.694 mg/Kg - dry 0.694 2.40Benzoic Acid 1 11/05/22 02:00 V25983JMV
<0.125 mg/Kg - dry 0.125 0.791Benzyl alcohol 1 11/05/22 02:00 V25983JMV
<0.141 mg/Kg - dry 0.141 0.791Bis(2-Chloroethoxy)methane 1 11/05/22 02:00 V25983JMV
<0.128 mg/Kg - dry 0.128 0.791Bis(2-Chloroethyl)ether 1 11/05/22 02:00 V25983JMV
<0.162 mg/Kg - dry 0.162 0.395Bis(2-Chloroisopropyl)ether 1 11/05/22 02:00 V25983JMV
<0.143 mg/Kg - dry 0.143 0.791Bis(2-ethylhexyl)phthalate 1 11/05/22 02:00 V25983JMV
<0.130 mg/Kg - dry 0.130 0.7914-Bromophenyl phenyl ether 1 11/05/22 02:00 V25983JMV
<0.135 mg/Kg - dry 0.135 0.395
Butyl benzyl phthalate 1 11/05/22 02:00 V25983JMV
<0.110 mg/Kg - dry 0.110 0.7914-Chloro-3-methylphenol 1 11/05/22 02:00 V25983JMV
<0.134 mg/Kg - dry 0.134 0.3954-Chloroaniline 1 11/05/22 02:00 V25983JMV
<0.138 mg/Kg - dry 0.138 0.7912-Chloronaphthalene 1 11/05/22 02:00 V25983JMV
<0.117 mg/Kg - dry 0.117 0.7912-Chlorophenol 1 11/05/22 02:00 V25983JMV
<0.150 mg/Kg - dry 0.150 1.204-Chlorophenyl phenyl ether 1 11/05/22 02:00 V25983JMV
<0.170 mg/Kg - dry 0.170 0.791Chrysene 1 11/05/22 02:00 V25983JMV
<0.275 mg/Kg - dry 0.275 0.791
Dibenz(a,h)anthracene 1 11/05/22 02:00 V25983JMV
<0.142 mg/Kg - dry 0.142 0.791Dibenzofuran 1 11/05/22 02:00 V25983JMV
<0.113 mg/Kg - dry 0.113 0.7911,2-Dichlorobenzene 1 11/05/22 02:00 V25983JMV
<0.116 mg/Kg - dry 0.116 0.7911,3-Dichlorobenzene 1 11/05/22 02:00 V25983JMV
<0.116 mg/Kg - dry 0.116 0.3951,4-Dichlorobenzene 1 11/05/22 02:00 V25983JMV
<0.176 mg/Kg - dry 0.176 0.7913,3'-Dichlorobenzidine 1 11/05/22 02:00 V25983JMV
<0.114 mg/Kg - dry 0.114 0.7912,4-Dichlorophenol 1 11/05/22 02:00 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-7
91766 Matrix:
10/27/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.215 mg/Kg - dry 0.215 0.791Diethyl phthalate 1 11/05/22 02:00 V25983JMV
<0.208 mg/Kg - dry 0.208 0.791Dimethyl phthalate 1 11/05/22 02:00 V25983JMV
<0.129 mg/Kg - dry 0.129 0.3952,4-Dimethylphenol 1 11/05/22 02:00 V25983JMV
<0.128 mg/Kg - dry 0.128 0.791Di-n-butyl phthalate 1 11/05/22 02:00 V25983JMV
<0.287 mg/Kg - dry 0.287 1.804,6-Dinitro-2-methylphenol 1 11/05/22 02:00 V25983JMV
<0.622 mg/Kg - dry 0.622 1.802,4-Dinitrophenol 1 11/05/22 02:00 V25983JMV
<0.115 mg/Kg - dry 0.115 0.7912,4-Dinitrotoluene 1 11/05/22 02:00 V25983JMV
<0.129 mg/Kg - dry 0.129 0.7912,6-Dinitrotoluene 1 11/05/22 02:00 V25983JMV
<0.171 mg/Kg - dry 0.171 0.395
Di-n-Octyl Phthalate 1 11/05/22 02:00 V25983JMV
<0.147 mg/Kg - dry 0.147 0.791Fluoranthene 1 11/05/22 02:00 V25983JMV
<0.153 mg/Kg - dry 0.153 0.791Fluorene 1 11/05/22 02:00 V25983JMV
<0.126 mg/Kg - dry 0.126 0.791Hexachlorobenzene 1 11/05/22 02:00 V25983JMV
<0.117 mg/Kg - dry 0.117 0.791Hexachlorobutadiene 1 11/05/22 02:00 V25983JMV
<0.188 mg/Kg - dry 0.188 0.791Hexachlorocyclopentadiene 1 11/05/22 02:00 V25983JMV
<0.094 mg/Kg - dry 0.094 0.791Hexachloroethane 1 11/05/22 02:00 V25983JMV
<0.214 mg/Kg - dry 0.214 0.791
Indeno(1,2,3-cd)pyrene 1 11/05/22 02:00 V25983JMV
<0.228 mg/Kg - dry 0.228 0.791Isophorone 1 11/05/22 02:00 V25983JMV
<0.126 mg/Kg - dry 0.126 0.7911-Methylnaphthalene 1 11/05/22 02:00 V25983JMV
<0.119 mg/Kg - dry 0.119 0.7912-Methylnaphthalene 1 11/05/22 02:00 V25983JMV
<0.116 mg/Kg - dry 0.116 0.7912-Methylphenol 1 11/05/22 02:00 V25983JMV
<0.101 mg/Kg - dry 0.101 0.7913&4 Methylphenol 1 11/05/22 02:00 V25983JMV
<0.172 mg/Kg - dry 0.172 0.791Naphthalene 1 11/05/22 02:00 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-7
91766 Matrix:
10/27/2022 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.115 mg/Kg - dry 0.115 0.7912-Nitroaniline 1 11/05/22 02:00 V25983JMV
<0.143 mg/Kg - dry 0.143 0.7913-Nitroaniline 1 11/05/22 02:00 V25983JMV
<0.111 mg/Kg - dry 0.111 0.3954-Nitroaniline 1 11/05/22 02:00 V25983JMV
<0.138 mg/Kg - dry 0.138 0.395Nitrobenzene 1 11/05/22 02:00 V25983JMV
<0.106 mg/Kg - dry 0.106 0.7912-Nitrophenol 1 11/05/22 02:00 V25983JMV
<0.140 mg/Kg - dry 0.140 0.7914-Nitrophenol 1 11/05/22 02:00 V25983JMV
<0.314 mg/Kg - dry 0.314 0.791N-Nitrosodimethylamine 1 11/05/22 02:00 V25983JMV
<0.216 mg/Kg - dry 0.216 0.791N-Nitrosodiphenylamine 1 11/05/22 02:00 V25983JMV
<0.141 mg/Kg - dry 0.141 0.791
N-Nitroso-di-n-propylamine 1 11/05/22 02:00 V25983JMV
<0.415 mg/Kg - dry 0.415 1.20Pentachlorophenol 1 11/05/22 02:00 V25983JMV
<0.249 mg/Kg - dry 0.249 0.791Phenanthrene 1 11/05/22 02:00 V25983JMV
<0.134 mg/Kg - dry 0.134 0.791Phenol 1 11/05/22 02:00 V25983JMV
<0.160 mg/Kg - dry 0.160 0.791Pyrene 1 11/05/22 02:00 V25983JMV
<0.094 mg/Kg - dry 0.094 0.395Pyridine 1 11/05/22 02:00 V25983JMV
<0.128 mg/Kg - dry 0.128 0.7911,2,4-Trichlorobenzene 1 11/05/22 02:00 V25983JMV
<0.115 mg/Kg - dry 0.115 0.791
2,4,5-Trichlorophenol 1 11/05/22 02:00 V25983JMV
<0.115 mg/Kg - dry 0.115 0.7912,4,6-Trichlorophenol 1 11/05/22 02:00 V25983JMV
8270ESurrogate: Phenol-d5 65.9 Limits: 34-121%11/05/22 02:001 JMV
Surrogate: 2-Fluorobiphenyl 79.0 Limits: 44-115%11/05/22 02:001 JMV V25983
Surrogate: 2-Fluorophenol 67.7 Limits: 35-115%11/05/22 02:001 JMV V25983
Surrogate: Nitrobenzene-d5 73.7 Limits: 37-122%11/05/22 02:001 JMV V25983
Surrogate: 4-Terphenyl-d14 88.6 Limits: 54-127%11/05/22 02:001 JMV V25983
Surrogate: 2,4,6-Tribromophenol 66.5 Limits: 39-132%11/05/22 02:001 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-8
91767 Matrix:
10/27/2022 13:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.4 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
<0.175 mg/Kg - dry 0.175 0.249Chromium, Hexavalent 1 11/04/22 16:41 SW-7199SAR
0.827 mg/Kg - dry 0.104 0.303Arsenic 5 11/04/22 22:09 6020BCPW
144 mg/Kg - dry 0.051 0.302Barium 5 11/04/22 22:09 6020BCPW
0.0363 J mg/Kg - dry 0.0313 0.303Cadmium 5 11/04/22 22:09 6020BCPW
57.0 mg/Kg - dry 0.280 0.605
Chromium 10 11/07/22 19:16 6020BBKN
8.04 mg/Kg - dry 0.0375 0.303Lead 5 11/04/22 22:09 6020BCPW
0.0393 mg/Kg - dry 0.0145 0.0363Mercury (Total)1 11/02/22 16:31 7471BEDV
0.242 J mg/Kg - dry 0.124 0.302Selenium 5 11/04/22 22:09 6020BCPW
0.0171 J mg/Kg - dry 0.0081 0.303Silver 5 11/04/22 22:09 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-8
91767 Matrix:
10/27/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.025 mg/Kg - dry 0.002 0.024Acetone 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/31/22 21:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 21:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 21:07 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 21:07 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 21:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 21:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 21:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/31/22 21:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 21:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 21:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/31/22 21:07 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 21:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 21:07 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-8
91767 Matrix:
10/27/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 21:07 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 21:07 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 21:07 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 21:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 21:07 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 21:07 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 21:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/31/22 21:07 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/31/22 21:07 V25732TBL
<0.016 mg/Kg - dry 0.016 0.302Ethanol 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 21:07 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/31/22 21:07 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-8
91767 Matrix:
10/27/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/31/22 21:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/31/22 21:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 21:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/31/22 21:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 21:07 V25732TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 21:07 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 21:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 10/31/22 21:07 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 21:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 21:07 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 21:07 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 21:07 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-8
91767 Matrix:
10/27/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 21:07 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/31/22 21:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 21:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 21:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 21:07 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 21:07 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 21:07 V25732
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%10/31/22 21:071 TBL V25732
Surrogate: Dibromofluoromethane 105 Limits: 84-123%10/31/22 21:071 TBL V25732
Surrogate: Toluene-d8 90.4 Limits: 76-129%10/31/22 21:071 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.140 mg/Kg - dry 0.140 0.799Acenaphthene 1 11/05/22 01:37 V25983JMV
<0.127 mg/Kg - dry 0.127 0.799Acenaphthylene 1 11/05/22 01:37 V25983JMV
<0.184 mg/Kg - dry 0.184 0.799Aniline 1 11/05/22 01:37 V25983JMV
<0.173 mg/Kg - dry 0.173 0.799Anthracene 1 11/05/22 01:37 V25983JMV
<0.168 mg/Kg - dry 0.168 0.799
Benzo(a)anthracene 1 11/05/22 01:37 V25983JMV
<0.177 mg/Kg - dry 0.177 0.799Benzo(a)pyrene 1 11/05/22 01:37 V25983JMV
<0.176 mg/Kg - dry 0.176 0.799Benzo(b)fluoranthene 1 11/05/22 01:37 V25983JMV
<0.164 mg/Kg - dry 0.164 0.799Benzo(g,h,i)perylene 1 11/05/22 01:37 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-8
91767 Matrix:
10/27/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.165 mg/Kg - dry 0.165 0.799Benzo(k)fluoranthene 1 11/05/22 01:37 V25983JMV
<0.702 mg/Kg - dry 0.702 2.42Benzoic Acid 1 11/05/22 01:37 V25983JMV
<0.127 mg/Kg - dry 0.127 0.799Benzyl alcohol 1 11/05/22 01:37 V25983JMV
<0.142 mg/Kg - dry 0.142 0.799Bis(2-Chloroethoxy)methane 1 11/05/22 01:37 V25983JMV
<0.129 mg/Kg - dry 0.129 0.799Bis(2-Chloroethyl)ether 1 11/05/22 01:37 V25983JMV
<0.164 mg/Kg - dry 0.164 0.399Bis(2-Chloroisopropyl)ether 1 11/05/22 01:37 V25983JMV
<0.145 mg/Kg - dry 0.145 0.799Bis(2-ethylhexyl)phthalate 1 11/05/22 01:37 V25983JMV
<0.131 mg/Kg - dry 0.131 0.7994-Bromophenyl phenyl ether 1 11/05/22 01:37 V25983JMV
<0.136 mg/Kg - dry 0.136 0.399
Butyl benzyl phthalate 1 11/05/22 01:37 V25983JMV
<0.111 mg/Kg - dry 0.111 0.7994-Chloro-3-methylphenol 1 11/05/22 01:37 V25983JMV
<0.135 mg/Kg - dry 0.135 0.3994-Chloroaniline 1 11/05/22 01:37 V25983JMV
<0.140 mg/Kg - dry 0.140 0.7992-Chloronaphthalene 1 11/05/22 01:37 V25983JMV
<0.118 mg/Kg - dry 0.118 0.7992-Chlorophenol 1 11/05/22 01:37 V25983JMV
<0.152 mg/Kg - dry 0.152 1.214-Chlorophenyl phenyl ether 1 11/05/22 01:37 V25983JMV
<0.171 mg/Kg - dry 0.171 0.799Chrysene 1 11/05/22 01:37 V25983JMV
<0.278 mg/Kg - dry 0.278 0.799
Dibenz(a,h)anthracene 1 11/05/22 01:37 V25983JMV
<0.144 mg/Kg - dry 0.144 0.799Dibenzofuran 1 11/05/22 01:37 V25983JMV
<0.114 mg/Kg - dry 0.114 0.7991,2-Dichlorobenzene 1 11/05/22 01:37 V25983JMV
<0.117 mg/Kg - dry 0.117 0.7991,3-Dichlorobenzene 1 11/05/22 01:37 V25983JMV
<0.118 mg/Kg - dry 0.118 0.3991,4-Dichlorobenzene 1 11/05/22 01:37 V25983JMV
<0.177 mg/Kg - dry 0.177 0.7993,3'-Dichlorobenzidine 1 11/05/22 01:37 V25983JMV
<0.115 mg/Kg - dry 0.115 0.7992,4-Dichlorophenol 1 11/05/22 01:37 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-8
91767 Matrix:
10/27/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.217 mg/Kg - dry 0.217 0.799Diethyl phthalate 1 11/05/22 01:37 V25983JMV
<0.210 mg/Kg - dry 0.210 0.799Dimethyl phthalate 1 11/05/22 01:37 V25983JMV
<0.130 mg/Kg - dry 0.130 0.3992,4-Dimethylphenol 1 11/05/22 01:37 V25983JMV
<0.129 mg/Kg - dry 0.129 0.799Di-n-butyl phthalate 1 11/05/22 01:37 V25983JMV
<0.290 mg/Kg - dry 0.290 1.824,6-Dinitro-2-methylphenol 1 11/05/22 01:37 V25983JMV
<0.629 mg/Kg - dry 0.629 1.822,4-Dinitrophenol 1 11/05/22 01:37 V25983JMV
<0.116 mg/Kg - dry 0.116 0.7992,4-Dinitrotoluene 1 11/05/22 01:37 V25983JMV
<0.130 mg/Kg - dry 0.130 0.7992,6-Dinitrotoluene 1 11/05/22 01:37 V25983JMV
<0.173 mg/Kg - dry 0.173 0.399
Di-n-Octyl Phthalate 1 11/05/22 01:37 V25983JMV
<0.148 mg/Kg - dry 0.148 0.799Fluoranthene 1 11/05/22 01:37 V25983JMV
<0.154 mg/Kg - dry 0.154 0.799Fluorene 1 11/05/22 01:37 V25983JMV
<0.128 mg/Kg - dry 0.128 0.799Hexachlorobenzene 1 11/05/22 01:37 V25983JMV
<0.118 mg/Kg - dry 0.118 0.799Hexachlorobutadiene 1 11/05/22 01:37 V25983JMV
<0.190 mg/Kg - dry 0.190 0.799Hexachlorocyclopentadiene 1 11/05/22 01:37 V25983JMV
<0.095 mg/Kg - dry 0.095 0.799Hexachloroethane 1 11/05/22 01:37 V25983JMV
<0.216 mg/Kg - dry 0.216 0.799
Indeno(1,2,3-cd)pyrene 1 11/05/22 01:37 V25983JMV
<0.231 mg/Kg - dry 0.231 0.799Isophorone 1 11/05/22 01:37 V25983JMV
<0.128 mg/Kg - dry 0.128 0.7991-Methylnaphthalene 1 11/05/22 01:37 V25983JMV
<0.121 mg/Kg - dry 0.121 0.7992-Methylnaphthalene 1 11/05/22 01:37 V25983JMV
<0.117 mg/Kg - dry 0.117 0.7992-Methylphenol 1 11/05/22 01:37 V25983JMV
<0.102 mg/Kg - dry 0.102 0.7993&4 Methylphenol 1 11/05/22 01:37 V25983JMV
<0.174 mg/Kg - dry 0.174 0.799Naphthalene 1 11/05/22 01:37 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-8
91767 Matrix:
10/27/2022 13:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.117 mg/Kg - dry 0.117 0.7992-Nitroaniline 1 11/05/22 01:37 V25983JMV
<0.145 mg/Kg - dry 0.145 0.7993-Nitroaniline 1 11/05/22 01:37 V25983JMV
<0.112 mg/Kg - dry 0.112 0.3994-Nitroaniline 1 11/05/22 01:37 V25983JMV
<0.140 mg/Kg - dry 0.140 0.399Nitrobenzene 1 11/05/22 01:37 V25983JMV
<0.107 mg/Kg - dry 0.107 0.7992-Nitrophenol 1 11/05/22 01:37 V25983JMV
<0.141 mg/Kg - dry 0.141 0.7994-Nitrophenol 1 11/05/22 01:37 V25983JMV
<0.318 mg/Kg - dry 0.318 0.799N-Nitrosodimethylamine 1 11/05/22 01:37 V25983JMV
<0.219 mg/Kg - dry 0.219 0.799N-Nitrosodiphenylamine 1 11/05/22 01:37 V25983JMV
<0.142 mg/Kg - dry 0.142 0.799
N-Nitroso-di-n-propylamine 1 11/05/22 01:37 V25983JMV
<0.420 mg/Kg - dry 0.420 1.21Pentachlorophenol 1 11/05/22 01:37 V25983JMV
<0.251 mg/Kg - dry 0.251 0.799Phenanthrene 1 11/05/22 01:37 V25983JMV
<0.135 mg/Kg - dry 0.135 0.799Phenol 1 11/05/22 01:37 V25983JMV
<0.162 mg/Kg - dry 0.162 0.799Pyrene 1 11/05/22 01:37 V25983JMV
<0.095 mg/Kg - dry 0.095 0.399Pyridine 1 11/05/22 01:37 V25983JMV
<0.129 mg/Kg - dry 0.129 0.7991,2,4-Trichlorobenzene 1 11/05/22 01:37 V25983JMV
<0.116 mg/Kg - dry 0.116 0.799
2,4,5-Trichlorophenol 1 11/05/22 01:37 V25983JMV
<0.116 mg/Kg - dry 0.116 0.7992,4,6-Trichlorophenol 1 11/05/22 01:37 V25983JMV
8270ESurrogate: Phenol-d5 65.5 Limits: 34-121%11/05/22 01:371 JMV
Surrogate: 2-Fluorobiphenyl 77.8 Limits: 44-115%11/05/22 01:371 JMV V25983
Surrogate: 2-Fluorophenol 67.9 Limits: 35-115%11/05/22 01:371 JMV V25983
Surrogate: Nitrobenzene-d5 72.5 Limits: 37-122%11/05/22 01:371 JMV V25983
Surrogate: 4-Terphenyl-d14 84.4 Limits: 54-127%11/05/22 01:371 JMV V25983
Surrogate: 2,4,6-Tribromophenol 66.7 Limits: 39-132%11/05/22 01:371 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-9
91768 Matrix:
10/28/2022 12:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.4 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
<0.171 mg/Kg - dry 0.171 0.242Chromium, Hexavalent 1 11/04/22 16:52 SW-7199SAR
0.768 mg/Kg - dry 0.102 0.299Arsenic 5 11/04/22 22:14 6020BCPW
109 mg/Kg - dry 0.051 0.299Barium 5 11/04/22 22:14 6020BCPW
<0.0309 mg/Kg - dry 0.0309 0.299Cadmium 5 11/04/22 22:14 6020BCPW
32.9 mg/Kg - dry 0.277 0.598
Chromium 10 11/07/22 19:22 6020BBKN
8.36 mg/Kg - dry 0.0370 0.299Lead 5 11/04/22 22:14 6020BCPW
0.0254 J mg/Kg - dry 0.0144 0.0359Mercury (Total)1 11/02/22 16:33 7471BEDV
0.343 mg/Kg - dry 0.123 0.299Selenium 5 11/04/22 22:14 6020BCPW
0.0226 J mg/Kg - dry 0.0080 0.299Silver 5 11/04/22 22:14 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 66 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-9
91768 Matrix:
10/28/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
0.028 mg/Kg - dry 0.002 0.023Acetone 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 11/01/22 12:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 11/01/22 12:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 11/01/22 12:41 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.005Bromochloromethane 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 11/01/22 12:41 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 11/01/22 12:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 11/01/22 12:41 V25789TBL
0.0009 J mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 11/01/22 12:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 11/01/22 12:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.011Chloromethane 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 11/01/22 12:41 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 11/01/22 12:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 11/01/22 12:41 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-9
91768 Matrix:
10/28/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 11/01/22 12:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 11/01/22 12:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 11/01/22 12:41 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 11/01/22 12:41 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,3-Dichlorobenzene 1 11/01/22 12:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 11/01/22 12:41 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 11/01/22 12:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 11/01/22 12:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 11/01/22 12:41 V25789TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 11/01/22 12:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 11/01/22 12:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 11/01/22 12:41 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.005trans-1,3-Dichloropropene 1 11/01/22 12:41 V25789TBL
<0.016 mg/Kg - dry 0.016 0.299Ethanol 1 11/01/22 12:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 11/01/22 12:41 V25789TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 11/01/22 12:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 11/01/22 12:41 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-9
91768 Matrix:
10/28/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 11/01/22 12:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Isopropylbenzene 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 11/01/22 12:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 11/01/22 12:41 V25789TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 11/01/22 12:41 V25789TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 11/01/22 12:41 V25789TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 11/01/22 12:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 11/01/22 12:41 V25789TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 11/01/22 12:41 V25789TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 11/01/22 12:41 V25789TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 11/01/22 12:41 V25789TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-9
91768 Matrix:
10/28/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25787 11/01/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Acetate 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 11/01/22 12:41 V25789TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 11/01/22 12:41 V25789TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 11/01/22 12:41 V25789
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%11/01/22 12:411 TBL V25789
Surrogate: Dibromofluoromethane 104 Limits: 84-123%11/01/22 12:411 TBL V25789
Surrogate: Toluene-d8 89.8 Limits: 76-129%11/01/22 12:411 TBL V25789
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.138 mg/Kg - dry 0.138 0.789Acenaphthene 1 11/05/22 02:22 V25983JMV
<0.125 mg/Kg - dry 0.125 0.789Acenaphthylene 1 11/05/22 02:22 V25983JMV
<0.181 mg/Kg - dry 0.181 0.789Aniline 1 11/05/22 02:22 V25983JMV
<0.171 mg/Kg - dry 0.171 0.789Anthracene 1 11/05/22 02:22 V25983JMV
<0.166 mg/Kg - dry 0.166 0.789
Benzo(a)anthracene 1 11/05/22 02:22 V25983JMV
<0.175 mg/Kg - dry 0.175 0.789Benzo(a)pyrene 1 11/05/22 02:22 V25983JMV
<0.174 mg/Kg - dry 0.174 0.789Benzo(b)fluoranthene 1 11/05/22 02:22 V25983JMV
<0.162 mg/Kg - dry 0.162 0.789Benzo(g,h,i)perylene 1 11/05/22 02:22 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-9
91768 Matrix:
10/28/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.163 mg/Kg - dry 0.163 0.789Benzo(k)fluoranthene 1 11/05/22 02:22 V25983JMV
<0.693 mg/Kg - dry 0.693 2.39Benzoic Acid 1 11/05/22 02:22 V25983JMV
<0.125 mg/Kg - dry 0.125 0.789Benzyl alcohol 1 11/05/22 02:22 V25983JMV
<0.141 mg/Kg - dry 0.141 0.789Bis(2-Chloroethoxy)methane 1 11/05/22 02:22 V25983JMV
<0.127 mg/Kg - dry 0.127 0.789Bis(2-Chloroethyl)ether 1 11/05/22 02:22 V25983JMV
<0.162 mg/Kg - dry 0.162 0.394Bis(2-Chloroisopropyl)ether 1 11/05/22 02:22 V25983JMV
<0.143 mg/Kg - dry 0.143 0.789Bis(2-ethylhexyl)phthalate 1 11/05/22 02:22 V25983JMV
<0.130 mg/Kg - dry 0.130 0.7894-Bromophenyl phenyl ether 1 11/05/22 02:22 V25983JMV
<0.135 mg/Kg - dry 0.135 0.394
Butyl benzyl phthalate 1 11/05/22 02:22 V25983JMV
<0.110 mg/Kg - dry 0.110 0.7894-Chloro-3-methylphenol 1 11/05/22 02:22 V25983JMV
<0.133 mg/Kg - dry 0.133 0.3944-Chloroaniline 1 11/05/22 02:22 V25983JMV
<0.138 mg/Kg - dry 0.138 0.7892-Chloronaphthalene 1 11/05/22 02:22 V25983JMV
<0.117 mg/Kg - dry 0.117 0.7892-Chlorophenol 1 11/05/22 02:22 V25983JMV
<0.150 mg/Kg - dry 0.150 1.204-Chlorophenyl phenyl ether 1 11/05/22 02:22 V25983JMV
<0.169 mg/Kg - dry 0.169 0.789Chrysene 1 11/05/22 02:22 V25983JMV
<0.275 mg/Kg - dry 0.275 0.789
Dibenz(a,h)anthracene 1 11/05/22 02:22 V25983JMV
<0.142 mg/Kg - dry 0.142 0.789Dibenzofuran 1 11/05/22 02:22 V25983JMV
<0.112 mg/Kg - dry 0.112 0.7891,2-Dichlorobenzene 1 11/05/22 02:22 V25983JMV
<0.116 mg/Kg - dry 0.116 0.7891,3-Dichlorobenzene 1 11/05/22 02:22 V25983JMV
<0.116 mg/Kg - dry 0.116 0.3941,4-Dichlorobenzene 1 11/05/22 02:22 V25983JMV
<0.175 mg/Kg - dry 0.175 0.7893,3'-Dichlorobenzidine 1 11/05/22 02:22 V25983JMV
<0.114 mg/Kg - dry 0.114 0.7892,4-Dichlorophenol 1 11/05/22 02:22 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-9
91768 Matrix:
10/28/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.215 mg/Kg - dry 0.215 0.789Diethyl phthalate 1 11/05/22 02:22 V25983JMV
<0.208 mg/Kg - dry 0.208 0.789Dimethyl phthalate 1 11/05/22 02:22 V25983JMV
<0.129 mg/Kg - dry 0.129 0.3942,4-Dimethylphenol 1 11/05/22 02:22 V25983JMV
<0.127 mg/Kg - dry 0.127 0.789Di-n-butyl phthalate 1 11/05/22 02:22 V25983JMV
<0.287 mg/Kg - dry 0.287 1.794,6-Dinitro-2-methylphenol 1 11/05/22 02:22 V25983JMV
<0.622 mg/Kg - dry 0.622 1.792,4-Dinitrophenol 1 11/05/22 02:22 V25983JMV
<0.115 mg/Kg - dry 0.115 0.7892,4-Dinitrotoluene 1 11/05/22 02:22 V25983JMV
<0.129 mg/Kg - dry 0.129 0.7892,6-Dinitrotoluene 1 11/05/22 02:22 V25983JMV
<0.171 mg/Kg - dry 0.171 0.394
Di-n-Octyl Phthalate 1 11/05/22 02:22 V25983JMV
<0.147 mg/Kg - dry 0.147 0.789Fluoranthene 1 11/05/22 02:22 V25983JMV
<0.153 mg/Kg - dry 0.153 0.789Fluorene 1 11/05/22 02:22 V25983JMV
<0.126 mg/Kg - dry 0.126 0.789Hexachlorobenzene 1 11/05/22 02:22 V25983JMV
<0.116 mg/Kg - dry 0.116 0.789Hexachlorobutadiene 1 11/05/22 02:22 V25983JMV
<0.187 mg/Kg - dry 0.187 0.789Hexachlorocyclopentadiene 1 11/05/22 02:22 V25983JMV
<0.094 mg/Kg - dry 0.094 0.789Hexachloroethane 1 11/05/22 02:22 V25983JMV
<0.214 mg/Kg - dry 0.214 0.789
Indeno(1,2,3-cd)pyrene 1 11/05/22 02:22 V25983JMV
<0.228 mg/Kg - dry 0.228 0.789Isophorone 1 11/05/22 02:22 V25983JMV
<0.126 mg/Kg - dry 0.126 0.7891-Methylnaphthalene 1 11/05/22 02:22 V25983JMV
<0.119 mg/Kg - dry 0.119 0.7892-Methylnaphthalene 1 11/05/22 02:22 V25983JMV
<0.116 mg/Kg - dry 0.116 0.7892-Methylphenol 1 11/05/22 02:22 V25983JMV
<0.101 mg/Kg - dry 0.101 0.7893&4 Methylphenol 1 11/05/22 02:22 V25983JMV
<0.172 mg/Kg - dry 0.172 0.789Naphthalene 1 11/05/22 02:22 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 72 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-9
91768 Matrix:
10/28/2022 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.115 mg/Kg - dry 0.115 0.7892-Nitroaniline 1 11/05/22 02:22 V25983JMV
<0.143 mg/Kg - dry 0.143 0.7893-Nitroaniline 1 11/05/22 02:22 V25983JMV
<0.111 mg/Kg - dry 0.111 0.3944-Nitroaniline 1 11/05/22 02:22 V25983JMV
<0.138 mg/Kg - dry 0.138 0.394Nitrobenzene 1 11/05/22 02:22 V25983JMV
<0.106 mg/Kg - dry 0.106 0.7892-Nitrophenol 1 11/05/22 02:22 V25983JMV
<0.139 mg/Kg - dry 0.139 0.7894-Nitrophenol 1 11/05/22 02:22 V25983JMV
<0.314 mg/Kg - dry 0.314 0.789N-Nitrosodimethylamine 1 11/05/22 02:22 V25983JMV
<0.216 mg/Kg - dry 0.216 0.789N-Nitrosodiphenylamine 1 11/05/22 02:22 V25983JMV
<0.141 mg/Kg - dry 0.141 0.789
N-Nitroso-di-n-propylamine 1 11/05/22 02:22 V25983JMV
<0.415 mg/Kg - dry 0.415 1.20Pentachlorophenol 1 11/05/22 02:22 V25983JMV
<0.248 mg/Kg - dry 0.248 0.789Phenanthrene 1 11/05/22 02:22 V25983JMV
<0.133 mg/Kg - dry 0.133 0.789Phenol 1 11/05/22 02:22 V25983JMV
<0.160 mg/Kg - dry 0.160 0.789Pyrene 1 11/05/22 02:22 V25983JMV
<0.094 mg/Kg - dry 0.094 0.394Pyridine 1 11/05/22 02:22 V25983JMV
<0.127 mg/Kg - dry 0.127 0.7891,2,4-Trichlorobenzene 1 11/05/22 02:22 V25983JMV
<0.115 mg/Kg - dry 0.115 0.789
2,4,5-Trichlorophenol 1 11/05/22 02:22 V25983JMV
<0.115 mg/Kg - dry 0.115 0.7892,4,6-Trichlorophenol 1 11/05/22 02:22 V25983JMV
8270ESurrogate: Phenol-d5 64.9 Limits: 34-121%11/05/22 02:221 JMV
Surrogate: 2-Fluorobiphenyl 79.6 Limits: 44-115%11/05/22 02:221 JMV V25983
Surrogate: 2-Fluorophenol 65.8 Limits: 35-115%11/05/22 02:221 JMV V25983
Surrogate: Nitrobenzene-d5 73.7 Limits: 37-122%11/05/22 02:221 JMV V25983
Surrogate: 4-Terphenyl-d14 91.0 Limits: 54-127%11/05/22 02:221 JMV V25983
Surrogate: 2,4,6-Tribromophenol 59.8 Limits: 39-132%11/05/22 02:221 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-10
91769 Matrix:
10/28/2022 11:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.8 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
0.266 mg/Kg - dry 0.173 0.246Chromium, Hexavalent 1 11/04/22 17:47 SW-7199SAR
1.73 mg/Kg - dry 0.104 0.304Arsenic 5 11/04/22 22:19 6020BCPW
56.2 mg/Kg - dry 0.051 0.304Barium 5 11/04/22 22:19 6020BCPW
0.0405 J mg/Kg - dry 0.0315 0.304Cadmium 5 11/04/22 22:19 6020BCPW
35.6 mg/Kg - dry 0.282 0.608
Chromium 10 11/07/22 19:36 6020BBKN
15.0 mg/Kg - dry 0.0377 0.304Lead 5 11/04/22 22:19 6020BCPW
0.207 mg/Kg - dry 0.0146 0.0365Mercury (Total)1 11/02/22 16:36 7471BEDV
0.402 mg/Kg - dry 0.125 0.304Selenium 5 11/04/22 22:19 6020BCPW
0.0332 J mg/Kg - dry 0.0081 0.304Silver 5 11/04/22 22:19 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 74 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-10
91769 Matrix:
10/28/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.054 mg/Kg - dry 0.002 0.024Acetone 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 10/31/22 22:02 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 10/31/22 22:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 10/31/22 22:02 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 10/31/22 22:02 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 10/31/22 22:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 10/31/22 22:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 10/31/22 22:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 10/31/22 22:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 10/31/22 22:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 10/31/22 22:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 10/31/22 22:02 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 10/31/22 22:02 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 10/31/22 22:02 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 75 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-10
91769 Matrix:
10/28/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 10/31/22 22:02 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 10/31/22 22:02 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 10/31/22 22:02 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 10/31/22 22:02 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 10/31/22 22:02 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 10/31/22 22:02 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 10/31/22 22:02 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 10/31/22 22:02 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 10/31/22 22:02 V25732TBL
<0.017 mg/Kg - dry 0.017 0.304Ethanol 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 22:02 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 10/31/22 22:02 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 76 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-10
91769 Matrix:
10/28/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 10/31/22 22:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 10/31/22 22:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 10/31/22 22:02 V25732TBL
0.005 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 10/31/22 22:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 10/31/22 22:02 V25732TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 10/31/22 22:02 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 10/31/22 22:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 10/31/22 22:02 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 10/31/22 22:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 10/31/22 22:02 V25732TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 10/31/22 22:02 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 10/31/22 22:02 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 77 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-10
91769 Matrix:
10/28/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 10/31/22 22:02 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 10/31/22 22:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 10/31/22 22:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 10/31/22 22:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 10/31/22 22:02 V25732TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 10/31/22 22:02 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 10/31/22 22:02 V25732
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/31/22 22:021 TBL V25732
Surrogate: Dibromofluoromethane 107 Limits: 84-123%10/31/22 22:021 TBL V25732
Surrogate: Toluene-d8 91.2 Limits: 76-129%10/31/22 22:021 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.141 mg/Kg - dry 0.141 0.804Acenaphthene 1 11/05/22 00:30 V25983JMV
<0.127 mg/Kg - dry 0.127 0.804Acenaphthylene 1 11/05/22 00:30 V25983JMV
<0.184 mg/Kg - dry 0.184 0.804Aniline 1 11/05/22 00:30 V25983JMV
<0.173 mg/Kg - dry 0.173 0.804Anthracene 1 11/05/22 00:30 V25983JMV
<0.169 mg/Kg - dry 0.169 0.804
Benzo(a)anthracene 1 11/05/22 00:30 V25983JMV
<0.178 mg/Kg - dry 0.178 0.804Benzo(a)pyrene 1 11/05/22 00:30 V25983JMV
<0.177 mg/Kg - dry 0.177 0.804Benzo(b)fluoranthene 1 11/05/22 00:30 V25983JMV
<0.165 mg/Kg - dry 0.165 0.804Benzo(g,h,i)perylene 1 11/05/22 00:30 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 78 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-10
91769 Matrix:
10/28/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.166 mg/Kg - dry 0.166 0.804Benzo(k)fluoranthene 1 11/05/22 00:30 V25983JMV
<0.705 mg/Kg - dry 0.705 2.43Benzoic Acid 1 11/05/22 00:30 V25983JMV
<0.127 mg/Kg - dry 0.127 0.804Benzyl alcohol 1 11/05/22 00:30 V25983JMV
<0.143 mg/Kg - dry 0.143 0.804Bis(2-Chloroethoxy)methane 1 11/05/22 00:30 V25983JMV
<0.130 mg/Kg - dry 0.130 0.804Bis(2-Chloroethyl)ether 1 11/05/22 00:30 V25983JMV
<0.165 mg/Kg - dry 0.165 0.401Bis(2-Chloroisopropyl)ether 1 11/05/22 00:30 V25983JMV
<0.145 mg/Kg - dry 0.145 0.804Bis(2-ethylhexyl)phthalate 1 11/05/22 00:30 V25983JMV
<0.132 mg/Kg - dry 0.132 0.8044-Bromophenyl phenyl ether 1 11/05/22 00:30 V25983JMV
<0.137 mg/Kg - dry 0.137 0.401
Butyl benzyl phthalate 1 11/05/22 00:30 V25983JMV
<0.112 mg/Kg - dry 0.112 0.8044-Chloro-3-methylphenol 1 11/05/22 00:30 V25983JMV
<0.136 mg/Kg - dry 0.136 0.4014-Chloroaniline 1 11/05/22 00:30 V25983JMV
<0.141 mg/Kg - dry 0.141 0.8042-Chloronaphthalene 1 11/05/22 00:30 V25983JMV
<0.119 mg/Kg - dry 0.119 0.8042-Chlorophenol 1 11/05/22 00:30 V25983JMV
<0.153 mg/Kg - dry 0.153 1.224-Chlorophenyl phenyl ether 1 11/05/22 00:30 V25983JMV
<0.172 mg/Kg - dry 0.172 0.804Chrysene 1 11/05/22 00:30 V25983JMV
<0.279 mg/Kg - dry 0.279 0.804
Dibenz(a,h)anthracene 1 11/05/22 00:30 V25983JMV
<0.144 mg/Kg - dry 0.144 0.804Dibenzofuran 1 11/05/22 00:30 V25983JMV
<0.114 mg/Kg - dry 0.114 0.8041,2-Dichlorobenzene 1 11/05/22 00:30 V25983JMV
<0.118 mg/Kg - dry 0.118 0.8041,3-Dichlorobenzene 1 11/05/22 00:30 V25983JMV
<0.118 mg/Kg - dry 0.118 0.4011,4-Dichlorobenzene 1 11/05/22 00:30 V25983JMV
<0.178 mg/Kg - dry 0.178 0.8043,3'-Dichlorobenzidine 1 11/05/22 00:30 V25983JMV
<0.116 mg/Kg - dry 0.116 0.8042,4-Dichlorophenol 1 11/05/22 00:30 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 79 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-10
91769 Matrix:
10/28/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.218 mg/Kg - dry 0.218 0.804Diethyl phthalate 1 11/05/22 00:30 V25983JMV
<0.211 mg/Kg - dry 0.211 0.804Dimethyl phthalate 1 11/05/22 00:30 V25983JMV
<0.131 mg/Kg - dry 0.131 0.4012,4-Dimethylphenol 1 11/05/22 00:30 V25983JMV
<0.130 mg/Kg - dry 0.130 0.804Di-n-butyl phthalate 1 11/05/22 00:30 V25983JMV
<0.291 mg/Kg - dry 0.291 1.824,6-Dinitro-2-methylphenol 1 11/05/22 00:30 V25983JMV
<0.632 mg/Kg - dry 0.632 1.822,4-Dinitrophenol 1 11/05/22 00:30 V25983JMV
<0.117 mg/Kg - dry 0.117 0.8042,4-Dinitrotoluene 1 11/05/22 00:30 V25983JMV
<0.131 mg/Kg - dry 0.131 0.8042,6-Dinitrotoluene 1 11/05/22 00:30 V25983JMV
<0.173 mg/Kg - dry 0.173 0.401
Di-n-Octyl Phthalate 1 11/05/22 00:30 V25983JMV
<0.149 mg/Kg - dry 0.149 0.804Fluoranthene 1 11/05/22 00:30 V25983JMV
<0.155 mg/Kg - dry 0.155 0.804Fluorene 1 11/05/22 00:30 V25983JMV
<0.128 mg/Kg - dry 0.128 0.804Hexachlorobenzene 1 11/05/22 00:30 V25983JMV
<0.118 mg/Kg - dry 0.118 0.804Hexachlorobutadiene 1 11/05/22 00:30 V25983JMV
<0.190 mg/Kg - dry 0.190 0.804Hexachlorocyclopentadiene 1 11/05/22 00:30 V25983JMV
<0.096 mg/Kg - dry 0.096 0.804Hexachloroethane 1 11/05/22 00:30 V25983JMV
<0.217 mg/Kg - dry 0.217 0.804
Indeno(1,2,3-cd)pyrene 1 11/05/22 00:30 V25983JMV
<0.232 mg/Kg - dry 0.232 0.804Isophorone 1 11/05/22 00:30 V25983JMV
<0.128 mg/Kg - dry 0.128 0.8041-Methylnaphthalene 1 11/05/22 00:30 V25983JMV
<0.121 mg/Kg - dry 0.121 0.8042-Methylnaphthalene 1 11/05/22 00:30 V25983JMV
<0.118 mg/Kg - dry 0.118 0.8042-Methylphenol 1 11/05/22 00:30 V25983JMV
<0.103 mg/Kg - dry 0.103 0.8043&4 Methylphenol 1 11/05/22 00:30 V25983JMV
<0.175 mg/Kg - dry 0.175 0.804Naphthalene 1 11/05/22 00:30 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 80 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:FG-10
91769 Matrix:
10/28/2022 11:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.117 mg/Kg - dry 0.117 0.8042-Nitroaniline 1 11/05/22 00:30 V25983JMV
<0.145 mg/Kg - dry 0.145 0.8043-Nitroaniline 1 11/05/22 00:30 V25983JMV
<0.113 mg/Kg - dry 0.113 0.4014-Nitroaniline 1 11/05/22 00:30 V25983JMV
<0.141 mg/Kg - dry 0.141 0.401Nitrobenzene 1 11/05/22 00:30 V25983JMV
<0.108 mg/Kg - dry 0.108 0.8042-Nitrophenol 1 11/05/22 00:30 V25983JMV
<0.142 mg/Kg - dry 0.142 0.8044-Nitrophenol 1 11/05/22 00:30 V25983JMV
<0.319 mg/Kg - dry 0.319 0.804N-Nitrosodimethylamine 1 11/05/22 00:30 V25983JMV
<0.220 mg/Kg - dry 0.220 0.804N-Nitrosodiphenylamine 1 11/05/22 00:30 V25983JMV
<0.143 mg/Kg - dry 0.143 0.804
N-Nitroso-di-n-propylamine 1 11/05/22 00:30 V25983JMV
<0.422 mg/Kg - dry 0.422 1.22Pentachlorophenol 1 11/05/22 00:30 V25983JMV
<0.253 mg/Kg - dry 0.253 0.804Phenanthrene 1 11/05/22 00:30 V25983JMV
<0.136 mg/Kg - dry 0.136 0.804Phenol 1 11/05/22 00:30 V25983JMV
<0.163 mg/Kg - dry 0.163 0.804Pyrene 1 11/05/22 00:30 V25983JMV
<0.096 mg/Kg - dry 0.096 0.401Pyridine 1 11/05/22 00:30 V25983JMV
<0.130 mg/Kg - dry 0.130 0.8041,2,4-Trichlorobenzene 1 11/05/22 00:30 V25983JMV
<0.117 mg/Kg - dry 0.117 0.804
2,4,5-Trichlorophenol 1 11/05/22 00:30 V25983JMV
<0.117 mg/Kg - dry 0.117 0.8042,4,6-Trichlorophenol 1 11/05/22 00:30 V25983JMV
8270ESurrogate: Phenol-d5 69.8 Limits: 34-121%11/05/22 00:301 JMV
Surrogate: 2-Fluorobiphenyl 83.2 Limits: 44-115%11/05/22 00:301 JMV V25983
Surrogate: 2-Fluorophenol 71.6 Limits: 35-115%11/05/22 00:301 JMV V25983
Surrogate: Nitrobenzene-d5 78.4 Limits: 37-122%11/05/22 00:301 JMV V25983
Surrogate: 4-Terphenyl-d14 91.0 Limits: 54-127%11/05/22 00:301 JMV V25983
Surrogate: 2,4,6-Tribromophenol 62.3 Limits: 39-132%11/05/22 00:301 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 81 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:DUP-01
91770 Matrix:
10/28/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.3 %Moisture 1 11/04/22 11:19 SW-DRYWTPEB
<0.166 mg/Kg - dry 0.166 0.236Chromium, Hexavalent 1 11/04/22 18:30 SW-7199SAR
0.861 mg/Kg - dry 0.101 0.295Arsenic 5 11/04/22 22:25 6020BCPW
145 mg/Kg - dry 0.050 0.295Barium 5 11/04/22 22:25 6020BCPW
0.0449 J mg/Kg - dry 0.0305 0.295Cadmium 5 11/04/22 22:25 6020BCPW
38.6 mg/Kg - dry 0.273 0.590
Chromium 10 11/07/22 19:41 6020BBKN
8.09 mg/Kg - dry 0.0365 0.295Lead 5 11/04/22 22:25 6020BCPW
0.0269 J mg/Kg - dry 0.0142 0.0354Mercury (Total)1 11/02/22 16:45 7471BEDV
0.255 J mg/Kg - dry 0.121 0.295Selenium 5 11/04/22 22:25 6020BCPW
0.0357 J mg/Kg - dry 0.0079 0.295Silver 5 11/04/22 22:25 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 82 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:DUP-01
91770 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
0.032 mg/Kg - dry 0.002 0.023Acetone 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 10/31/22 22:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 10/31/22 22:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 10/31/22 22:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 10/31/22 22:29 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 10/31/22 22:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 10/31/22 22:29 V25732TBL
0.001 J mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 10/31/22 22:29 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 10/31/22 22:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 10/31/22 22:29 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 10/31/22 22:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 10/31/22 22:29 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 83 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:DUP-01
91770 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 10/31/22 22:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 10/31/22 22:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 10/31/22 22:29 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 10/31/22 22:29 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 10/31/22 22:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 10/31/22 22:29 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 10/31/22 22:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 10/31/22 22:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 10/31/22 22:29 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 10/31/22 22:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 10/31/22 22:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 10/31/22 22:29 V25732TBL
<0.016 mg/Kg - dry 0.016 0.295Ethanol 1 10/31/22 22:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 10/31/22 22:29 V25732TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 10/31/22 22:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 10/31/22 22:29 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 84 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:DUP-01
91770 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 10/31/22 22:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 10/31/22 22:29 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 10/31/22 22:29 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 10/31/22 22:29 V25732TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 10/31/22 22:29 V25732TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 10/31/22 22:29 V25732TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 10/31/22 22:29 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 10/31/22 22:29 V25732TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 10/31/22 22:29 V25732TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 10/31/22 22:29 V25732TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 10/31/22 22:29 V25732TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 85 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:DUP-01
91770 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V25731 10/31/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 10/31/22 22:29 V25732TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 10/31/22 22:29 V25732TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 10/31/22 22:29 V25732TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 10/31/22 22:29 V25732
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%10/31/22 22:291 TBL V25732
Surrogate: Dibromofluoromethane 109 Limits: 84-123%10/31/22 22:291 TBL V25732
Surrogate: Toluene-d8 89.0 Limits: 76-129%10/31/22 22:291 TBL V25732
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.136 mg/Kg - dry 0.136 0.780Acenaphthene 1 11/07/22 17:51 V25983JMV
<0.123 mg/Kg - dry 0.123 0.780Acenaphthylene 1 11/07/22 17:51 V25983JMV
<0.179 mg/Kg - dry 0.179 0.780Aniline 1 11/07/22 17:51 V25983JMV
<0.168 mg/Kg - dry 0.168 0.780Anthracene 1 11/07/22 17:51 V25983JMV
<0.164 mg/Kg - dry 0.164 0.780
Benzo(a)anthracene 1 11/07/22 17:51 V25983JMV
<0.173 mg/Kg - dry 0.173 0.780Benzo(a)pyrene 1 11/07/22 17:51 V25983JMV
<0.172 mg/Kg - dry 0.172 0.780Benzo(b)fluoranthene 1 11/07/22 17:51 V25983JMV
<0.160 mg/Kg - dry 0.160 0.780Benzo(g,h,i)perylene 1 11/07/22 17:51 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 86 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:DUP-01
91770 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.161 mg/Kg - dry 0.161 0.780Benzo(k)fluoranthene 1 11/07/22 17:51 V25983JMV
<0.684 mg/Kg - dry 0.684 2.36Benzoic Acid 1 11/07/22 17:51 V25983JMV
<0.123 mg/Kg - dry 0.123 0.780Benzyl alcohol 1 11/07/22 17:51 V25983JMV
<0.139 mg/Kg - dry 0.139 0.780Bis(2-Chloroethoxy)methane 1 11/07/22 17:51 V25983JMV
<0.126 mg/Kg - dry 0.126 0.780Bis(2-Chloroethyl)ether 1 11/07/22 17:51 V25983JMV
<0.160 mg/Kg - dry 0.160 0.389Bis(2-Chloroisopropyl)ether 1 11/07/22 17:51 V25983JMV
<0.141 mg/Kg - dry 0.141 0.780Bis(2-ethylhexyl)phthalate 1 11/07/22 17:51 V25983JMV
<0.128 mg/Kg - dry 0.128 0.7804-Bromophenyl phenyl ether 1 11/07/22 17:51 V25983JMV
<0.133 mg/Kg - dry 0.133 0.389
Butyl benzyl phthalate 1 11/07/22 17:51 V25983JMV
<0.109 mg/Kg - dry 0.109 0.7804-Chloro-3-methylphenol 1 11/07/22 17:51 V25983JMV
<0.132 mg/Kg - dry 0.132 0.3894-Chloroaniline 1 11/07/22 17:51 V25983JMV
<0.136 mg/Kg - dry 0.136 0.7802-Chloronaphthalene 1 11/07/22 17:51 V25983JMV
<0.116 mg/Kg - dry 0.116 0.7802-Chlorophenol 1 11/07/22 17:51 V25983JMV
<0.148 mg/Kg - dry 0.148 1.184-Chlorophenyl phenyl ether 1 11/07/22 17:51 V25983JMV
<0.167 mg/Kg - dry 0.167 0.780Chrysene 1 11/07/22 17:51 V25983JMV
<0.271 mg/Kg - dry 0.271 0.780
Dibenz(a,h)anthracene 1 11/07/22 17:51 V25983JMV
<0.140 mg/Kg - dry 0.140 0.780Dibenzofuran 1 11/07/22 17:51 V25983JMV
<0.111 mg/Kg - dry 0.111 0.7801,2-Dichlorobenzene 1 11/07/22 17:51 V25983JMV
<0.114 mg/Kg - dry 0.114 0.7801,3-Dichlorobenzene 1 11/07/22 17:51 V25983JMV
<0.115 mg/Kg - dry 0.115 0.3891,4-Dichlorobenzene 1 11/07/22 17:51 V25983JMV
<0.173 mg/Kg - dry 0.173 0.7803,3'-Dichlorobenzidine 1 11/07/22 17:51 V25983JMV
<0.113 mg/Kg - dry 0.113 0.7802,4-Dichlorophenol 1 11/07/22 17:51 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 87 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:DUP-01
91770 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.212 mg/Kg - dry 0.212 0.780Diethyl phthalate 1 11/07/22 17:51 V25983JMV
<0.205 mg/Kg - dry 0.205 0.780Dimethyl phthalate 1 11/07/22 17:51 V25983JMV
<0.127 mg/Kg - dry 0.127 0.3892,4-Dimethylphenol 1 11/07/22 17:51 V25983JMV
<0.126 mg/Kg - dry 0.126 0.780Di-n-butyl phthalate 1 11/07/22 17:51 V25983JMV
<0.283 mg/Kg - dry 0.283 1.774,6-Dinitro-2-methylphenol 1 11/07/22 17:51 V25983JMV
<0.613 mg/Kg - dry 0.613 1.772,4-Dinitrophenol 1 11/07/22 17:51 V25983JMV
<0.114 mg/Kg - dry 0.114 0.7802,4-Dinitrotoluene 1 11/07/22 17:51 V25983JMV
<0.127 mg/Kg - dry 0.127 0.7802,6-Dinitrotoluene 1 11/07/22 17:51 V25983JMV
<0.168 mg/Kg - dry 0.168 0.389
Di-n-Octyl Phthalate 1 11/07/22 17:51 V25983JMV
<0.145 mg/Kg - dry 0.145 0.780Fluoranthene 1 11/07/22 17:51 V25983JMV
<0.151 mg/Kg - dry 0.151 0.780Fluorene 1 11/07/22 17:51 V25983JMV
<0.125 mg/Kg - dry 0.125 0.780Hexachlorobenzene 1 11/07/22 17:51 V25983JMV
<0.115 mg/Kg - dry 0.115 0.780Hexachlorobutadiene 1 11/07/22 17:51 V25983JMV
<0.185 mg/Kg - dry 0.185 0.780Hexachlorocyclopentadiene 1 11/07/22 17:51 V25983JMV
<0.093 mg/Kg - dry 0.093 0.780Hexachloroethane 1 11/07/22 17:51 V25983JMV
<0.211 mg/Kg - dry 0.211 0.780
Indeno(1,2,3-cd)pyrene 1 11/07/22 17:51 V25983JMV
<0.225 mg/Kg - dry 0.225 0.780Isophorone 1 11/07/22 17:51 V25983JMV
<0.125 mg/Kg - dry 0.125 0.7801-Methylnaphthalene 1 11/07/22 17:51 V25983JMV
<0.118 mg/Kg - dry 0.118 0.7802-Methylnaphthalene 1 11/07/22 17:51 V25983JMV
<0.114 mg/Kg - dry 0.114 0.7802-Methylphenol 1 11/07/22 17:51 V25983JMV
<0.100 mg/Kg - dry 0.100 0.7803&4 Methylphenol 1 11/07/22 17:51 V25983JMV
<0.170 mg/Kg - dry 0.170 0.780Naphthalene 1 11/07/22 17:51 V25983JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 88 of 119
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-301-0015
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 10/28/2022
BOU-014
Report Date : 11/10/2022
Sample ID :
Lab No :
Sampled:DUP-01
91770 Matrix:
10/28/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V25823 11/02/22 10:35
<0.114 mg/Kg - dry 0.114 0.7802-Nitroaniline 1 11/07/22 17:51 V25983JMV
<0.141 mg/Kg - dry 0.141 0.7803-Nitroaniline 1 11/07/22 17:51 V25983JMV
<0.110 mg/Kg - dry 0.110 0.3894-Nitroaniline 1 11/07/22 17:51 V25983JMV
<0.136 mg/Kg - dry 0.136 0.389Nitrobenzene 1 11/07/22 17:51 V25983JMV
<0.104 mg/Kg - dry 0.104 0.7802-Nitrophenol 1 11/07/22 17:51 V25983JMV
<0.138 mg/Kg - dry 0.138 0.7804-Nitrophenol 1 11/07/22 17:51 V25983JMV
<0.310 mg/Kg - dry 0.310 0.780N-Nitrosodimethylamine 1 11/07/22 17:51 V25983JMV
<0.213 mg/Kg - dry 0.213 0.780N-Nitrosodiphenylamine 1 11/07/22 17:51 V25983JMV
<0.139 mg/Kg - dry 0.139 0.780
N-Nitroso-di-n-propylamine 1 11/07/22 17:51 V25983JMV
<0.409 mg/Kg - dry 0.409 1.18Pentachlorophenol 1 11/07/22 17:51 V25983JMV
<0.245 mg/Kg - dry 0.245 0.780Phenanthrene 1 11/07/22 17:51 V25983JMV
<0.132 mg/Kg - dry 0.132 0.780Phenol 1 11/07/22 17:51 V25983JMV
<0.158 mg/Kg - dry 0.158 0.780Pyrene 1 11/07/22 17:51 V25983JMV
<0.093 mg/Kg - dry 0.093 0.389Pyridine 1 11/07/22 17:51 V25983JMV
<0.126 mg/Kg - dry 0.126 0.7801,2,4-Trichlorobenzene 1 11/07/22 17:51 V25983JMV
<0.113 mg/Kg - dry 0.113 0.780
2,4,5-Trichlorophenol 1 11/07/22 17:51 V25983JMV
<0.114 mg/Kg - dry 0.114 0.7802,4,6-Trichlorophenol 1 11/07/22 17:51 V25983JMV
8270ESurrogate: Phenol-d5 69.5 Limits: 34-121%11/07/22 17:511 JMV
Surrogate: 2-Fluorobiphenyl 83.2 Limits: 44-115%11/07/22 17:511 JMV V25983
Surrogate: 2-Fluorophenol 70.4 Limits: 35-115%11/07/22 17:511 JMV V25983
Surrogate: Nitrobenzene-d5 78.4 Limits: 37-122%11/07/22 17:511 JMV V25983
Surrogate: 4-Terphenyl-d14 103 Limits: 54-127%11/07/22 17:511 JMV V25983
Surrogate: 2,4,6-Tribromophenol 61.4 Limits: 39-132%11/07/22 17:511 JMV V25983
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 89 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Metals Analyses
6020B
L647316,L647584QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L646697
Associated Lab Samples: 91761, 91762, 91763, 91764, 91765, 91766, 91767, 91768, 91769, 91770
LRB-L646697 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/04/22 20:470.2500.0855<0.0855mg/KgArsenic
11/04/22 20:470.2500.042<0.042mg/KgBarium
11/04/22 20:470.2500.0259<0.0259mg/KgCadmium
11/04/22 20:470.2500.116<0.116mg/KgChromium
11/04/22 20:470.2500.0310<0.0310mg/KgLead
11/04/22 20:470.2500.103<0.103mg/KgSelenium
11/04/22 20:470.2500.0067<0.0067mg/KgSilver
LCS-L646697Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1002.492.50mg/KgArsenic 80-120
1045.225.00mg/KgBarium 80-120
1010.5040.500mg/KgCadmium 80-120
1045.205.00mg/KgChromium 80-120
1022.562.50mg/KgLead 80-120
99.04.935.00mg/KgSelenium 80-120
1020.5110.500mg/KgSilver 80-120
V 91802-MS-L646697 V 91802-MSD-L646697Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2.77 91.03.252.442.420.564mg/KgArsenic 110 75-125 15.9 80
113 -450*1084.874.84135mg/KgBarium -550*75-125 4.5 80
0.550 1000.5410.4870.4840.0660mg/KgCadmium 97.0 75-125 1.6 80
70.5 683*44.44.874.8437.4mg/KgChromium 144*75-125 45.4 80
Page 1 of 27* QC Fail Date:11/10/2022 12:14 PM
Page 90 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Metals Analyses
6020B
L647316,L647584QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L646697
V 91802-MS-L646697 V 91802-MSD-L646697Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
14.6 186*16.92.442.4210.1mg/KgLead 279*75-125 14.6 80
2.48 48.0*2.804.874.840.133mg/KgSelenium 55.0*75-125 12.1 80
0.482 95.00.5040.4870.4840.0205mg/KgSilver 99.0 75-125 4.4 80
V 91802-PDS-L646697Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/04/22 23:1983.00.999mg/KgArsenic
11/04/22 23:1996.015.1mg/KgBarium
11/04/22 23:191000.237mg/KgCadmium
11/07/22 20:381014.20mg/KgChromium
11/04/22 23:1995.02.05mg/KgLead
11/04/22 23:1980.01.84mg/KgSelenium
11/04/22 23:1997.00.225mg/KgSilver
Page 2 of 27* QC Fail Date:11/10/2022 12:14 PM
Page 91 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V25843QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V25807
Associated Lab Samples: 91761, 91762, 91763, 91764, 91765, 91766, 91767, 91768, 91769, 91770
LRB-V25807 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/02/22 15:390.03000.0120<0.0120mg/KgMercury (Total)
LCS-V25807Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1030.4280.417mg/KgMercury (Total)80-120
V 91761-MS-V25807 V 91761-MSD-V25807Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.442 93.00.4810.4170.4170.0530mg/KgMercury (Total)103 80-120 8.4 20
V 91761-PDS-V25807Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
11/02/22 16:1399.00.233mg/KgMercury (Total)
Page 3 of 27Date:11/10/2022 12:14 PM
Page 92 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91761, 91762, 91763, 91764, 91765, 91766, 91767, 91769, 91770
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0200.002<0.002mg/KgAcetone
10/31/22 12:570.0200.001<0.001mg/KgAcrolein
10/31/22 12:570.0200.0008<0.0008mg/KgAcrylonitrile
10/31/22 12:570.0050.0006<0.0006mg/KgBenzene
10/31/22 12:570.0050.0005<0.0005mg/KgBromobenzene
10/31/22 12:570.0050.0008<0.0008mg/KgBromochloromethane
10/31/22 12:570.0050.001<0.001mg/KgBromodichloromethane
10/31/22 12:570.0050.001<0.001mg/KgBromoform
10/31/22 12:570.0100.001<0.001mg/KgBromomethane
10/31/22 12:570.0050.0005<0.0005mg/Kgn-Butylbenzene
10/31/22 12:570.0050.0006<0.0006mg/Kgsec-Butyl benzene
10/31/22 12:570.0050.0005<0.0005mg/Kgtert-Butyl benzene
10/31/22 12:570.0050.0006<0.0006mg/KgCarbon Disulfide
10/31/22 12:570.0050.001<0.001mg/KgCarbon Tetrachloride
10/31/22 12:570.0050.0007<0.0007mg/KgChlorobenzene
10/31/22 12:570.0050.0009<0.0009mg/KgChlorodibromomethane
10/31/22 12:570.0100.0009<0.0009mg/KgChloroethane
10/31/22 12:570.0050.001<0.001mg/KgChloroform
10/31/22 12:570.0100.0006<0.0006mg/KgChloromethane
10/31/22 12:570.0050.0005<0.0005mg/Kg2-Chlorotoluene
10/31/22 12:570.0050.0004<0.0004mg/Kg4-Chlorotoluene
10/31/22 12:570.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
10/31/22 12:570.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
10/31/22 12:570.0050.0006<0.0006mg/Kg1,2-Dibromoethane
10/31/22 12:570.0050.0006<0.0006mg/KgDibromomethane
10/31/22 12:570.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
10/31/22 12:570.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 27Date:11/10/2022 12:14 PM
Page 93 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91761, 91762, 91763, 91764, 91765, 91766, 91767, 91769, 91770
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
10/31/22 12:570.0100.001<0.001mg/KgDichlorodifluoromethane
10/31/22 12:570.0050.0008<0.0008mg/Kg1,1-Dichloroethane
10/31/22 12:570.0050.001<0.001mg/Kg1,2-Dichloroethane
10/31/22 12:570.0050.0007<0.0007mg/Kg1,1-Dichloroethene
10/31/22 12:570.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
10/31/22 12:570.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
10/31/22 12:570.0050.0004<0.0004mg/Kg1,2-Dichloropropane
10/31/22 12:570.0050.0006<0.0006mg/Kg1,3-Dichloropropane
10/31/22 12:570.0050.001<0.001mg/Kg2,2-Dichloropropane
10/31/22 12:570.0050.0008<0.0008mg/Kg1,1-Dichloropropene
10/31/22 12:570.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
10/31/22 12:570.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
10/31/22 12:570.2500.014<0.014mg/KgEthanol
10/31/22 12:570.0050.0006<0.0006mg/KgEthylbenzene
10/31/22 12:570.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
10/31/22 12:570.0100.0008<0.0008mg/KgHexachlorobutadiene
10/31/22 12:570.0100.0007<0.0007mg/Kgn-Hexane
10/31/22 12:570.0200.0006<0.0006mg/Kg2-Hexanone
10/31/22 12:570.0050.0005<0.0005mg/KgIsopropylbenzene
10/31/22 12:570.0050.001<0.001mg/Kg4-Isopropyl toluene
10/31/22 12:570.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
10/31/22 12:570.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
10/31/22 12:570.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
10/31/22 12:570.0100.001<0.001mg/KgMethylene Chloride
10/31/22 12:570.0100.0010<0.0010mg/KgNaphthalene
10/31/22 12:570.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 27Date:11/10/2022 12:14 PM
Page 94 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
Associated Lab Samples: 91761, 91762, 91763, 91764, 91765, 91766, 91767, 91769, 91770
LRB-V25731 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
10/31/22 12:570.0050.001<0.001mg/KgStyrene
10/31/22 12:570.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
10/31/22 12:570.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
10/31/22 12:570.0050.0009<0.0009mg/KgTetrachloroethene
10/31/22 12:570.0050.0007<0.0007mg/KgToluene
10/31/22 12:570.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
10/31/22 12:570.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
10/31/22 12:570.0050.001<0.001mg/Kg1,1,1-Trichloroethane
10/31/22 12:570.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
10/31/22 12:570.0050.0009<0.0009mg/KgTrichloroethene
10/31/22 12:570.0100.002<0.002mg/KgTrichlorofluoromethane
10/31/22 12:570.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
10/31/22 12:570.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
10/31/22 12:570.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
10/31/22 12:570.0100.0005<0.0005mg/KgVinyl Acetate
10/31/22 12:570.0100.0005<0.0005mg/KgVinyl Chloride
10/31/22 12:570.0050.0005<0.0005mg/Kgo-Xylene
10/31/22 12:570.0100.001<0.001mg/Kgm,p-Xylene
10/31/22 12:574-Bromofluorobenzene (S)101 70-130
10/31/22 12:57Dibromofluoromethane (S)97.6 84-123
10/31/22 12:57Toluene-d8 (S)93.6 76-129
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.095 95.389.60.0890.100mg/KgAcetone 29-198 6.1 20
Page 6 of 27Date:11/10/2022 12:14 PM
Page 95 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.103 1031040.1040.100mg/KgAcrolein 70-130 0.9 20
0.115 1151100.1100.100mg/KgAcrylonitrile 65-134 4.4 20
0.048 97.61000.0500.050mg/KgBenzene 74-127 2.4 20
0.043 86.091.40.0450.050mg/KgBromobenzene 73-125 6.0 20
0.054 1081070.0530.050mg/KgBromochloromethane 72-134 1.2 20
0.055 1101120.0550.050mg/KgBromodichloromethane 75-122 1.0 20
0.055 1101090.0540.050mg/KgBromoform 66-135 1.2 20
0.059 1201250.0620.050mg/KgBromomethane 20-180 4.5 20
0.040 81.089.20.0440.050mg/Kgn-Butylbenzene 65-135 9.6 20
0.041 82.290.20.0450.050mg/Kgsec-Butyl benzene 66-131 9.2 20
0.040 81.287.00.0430.050mg/Kgtert-Butyl benzene 67-132 6.8 20
0.045 91.495.60.0470.050mg/KgCarbon Disulfide 61-129 4.4 20
0.045 91.295.00.0470.050mg/KgCarbon Tetrachloride 64-143 4.0 20
0.044 88.291.80.0450.050mg/KgChlorobenzene 74-118 4.0 20
0.051 1031030.0510.050mg/KgChlorodibromomethane 73-122 0.0 20
0.049 99.41040.0510.050mg/KgChloroethane 33-149 4.3 20
0.049 98.01000.0500.050mg/KgChloroform 73-127 2.0 20
0.055 1101110.0550.050mg/KgChloromethane 45-143 0.7 20
0.040 81.886.60.0430.050mg/Kg2-Chlorotoluene 67-124 5.7 20
0.040 81.886.60.0430.050mg/Kg4-Chlorotoluene 71-126 5.7 20
0.055 1111130.0560.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.2 20
0.061 1241280.0640.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.4 20
0.055 1111130.0560.050mg/Kg1,2-Dibromoethane 70-132 1.0 20
0.054 1091150.0570.050mg/KgDibromomethane 74-133 5.1 20
0.044 89.290.60.0450.050mg/Kg1,2-Dichlorobenzene 72-123 1.5 20
0.041 83.686.40.0430.050mg/Kg1,3-Dichlorobenzene 71-120 3.2 20
Page 7 of 27Date:11/10/2022 12:14 PM
Page 96 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 84.888.00.0440.050mg/Kg1,4-Dichlorobenzene 71-123 3.7 20
0.045 91.21010.0500.050mg/KgDichlorodifluoromethane 26-146 9.8 20
0.048 96.81020.0510.050mg/Kg1,1-Dichloroethane 74-127 5.2 20
0.051 1031030.0510.050mg/Kg1,2-Dichloroethane 68-128 0.3 20
0.046 92.898.60.0490.050mg/Kg1,1-Dichloroethene 67-149 6.0 20
0.050 1021070.0530.050mg/Kgcis-1,2-Dichloroethene 76-134 5.1 20
0.048 96.81010.0500.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.2 20
0.053 1061090.0540.050mg/Kg1,2-Dichloropropane 73-130 2.4 20
0.052 1051070.0530.050mg/Kg1,3-Dichloropropane 75-124 1.8 20
0.045 91.294.40.0470.050mg/Kg2,2-Dichloropropane 50-142 3.4 20
0.043 86.894.80.0470.050mg/Kg1,1-Dichloropropene 71-130 8.8 20
0.055 1111130.0560.050mg/Kgcis-1,3-Dichloropropene 71-125 1.6 20
0.056 1131120.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.7 20
0.984 78.792.01.151.25mg/KgEthanol 70-130 15.5 20
0.044 88.490.40.0450.050mg/KgEthylbenzene 74-128 2.2 20
0.109 1091090.1090.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.0 20
0.039 79.887.40.0430.050mg/KgHexachlorobutadiene 64-125 9.0 20
0.048 96.81010.0500.050mg/Kgn-Hexane 70-130 3.8 20
0.054 1091070.0530.050mg/Kg2-Hexanone 61-157 2.2 20
0.039 79.487.00.0430.050mg/KgIsopropylbenzene 68-126 9.1 20
0.039 79.885.80.0420.050mg/Kg4-Isopropyl toluene 68-129 7.2 20
0.052 1051190.0590.050mg/KgMethyl Ethyl Ketone (MEK)63-149 12.8 20
0.057 1141170.0580.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.7 20
0.052 10491.40.0450.050mg/Kg4-Methyl-2-Pentanone 57-162 13.2 20
0.052 1051090.0540.050mg/KgMethylene Chloride 74-129 3.9 20
0.050 1021080.0530.050mg/KgNaphthalene 57-157 5.7 20
Page 8 of 27Date:11/10/2022 12:14 PM
Page 97 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25732QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25731
LCS-V25731 LCSD-V25731Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.041 83.889.60.0440.050mg/Kgn-Propylbenzene 67-130 6.6 20
0.047 94.097.60.0480.050mg/KgStyrene 77-121 3.7 20
0.045 90.691.60.0450.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.055 1101140.0570.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 3.3 20
0.046 92.696.20.0480.050mg/KgTetrachloroethene 68-130 3.8 20
0.047 94.298.20.0490.050mg/KgToluene 71-129 4.1 20
0.045 91.096.40.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 5.7 20
0.046 92.897.80.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 5.2 20
0.044 88.092.80.0460.050mg/Kg1,1,1-Trichloroethane 67-131 5.3 20
0.053 1081080.0540.050mg/Kg1,1,2-Trichloroethane 70-133 0.3 20
0.049 98.21050.0520.050mg/KgTrichloroethene 75-133 6.5 20
0.045 90.096.60.0480.050mg/KgTrichlorofluoromethane 44-146 7.0 20
0.056 1141150.0570.050mg/Kg1,2,3-Trichloropropane 60-137 0.8 20
0.041 83.887.20.0430.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.9 20
0.040 81.687.40.0430.050mg/Kg1,3,5-Trimethylbenzene 69-128 6.8 20
0.058 1171200.0590.050mg/KgVinyl Acetate 60-140 1.8 20
0.050 1011040.0520.050mg/KgVinyl Chloride 48-147 2.9 20
0.045 90.894.60.0470.050mg/Kgo-Xylene 74-126 4.0 20
0.087 87.490.90.0900.100mg/Kgm,p-Xylene 75-124 3.9 20
97.099.44-Bromofluorobenzene (S)70-130
100100Dibromofluoromethane (S)84-123
93.693.0Toluene-d8 (S)76-129
Page 9 of 27Date:11/10/2022 12:14 PM
Page 98 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
Associated Lab Samples: 91768
LRB-V25787 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/01/22 12:140.0200.002<0.002mg/KgAcetone
11/01/22 12:140.0200.001<0.001mg/KgAcrolein
11/01/22 12:140.0200.0008<0.0008mg/KgAcrylonitrile
11/01/22 12:140.0050.0006<0.0006mg/KgBenzene
11/01/22 12:140.0050.0005<0.0005mg/KgBromobenzene
11/01/22 12:140.0050.0008<0.0008mg/KgBromochloromethane
11/01/22 12:140.0050.001<0.001mg/KgBromodichloromethane
11/01/22 12:140.0050.001<0.001mg/KgBromoform
11/01/22 12:140.0100.001<0.001mg/KgBromomethane
11/01/22 12:140.0050.0005<0.0005mg/Kgn-Butylbenzene
11/01/22 12:140.0050.0006<0.0006mg/Kgsec-Butyl benzene
11/01/22 12:140.0050.0005<0.0005mg/Kgtert-Butyl benzene
11/01/22 12:140.0050.0006<0.0006mg/KgCarbon Disulfide
11/01/22 12:140.0050.001<0.001mg/KgCarbon Tetrachloride
11/01/22 12:140.0050.0007<0.0007mg/KgChlorobenzene
11/01/22 12:140.0050.0009<0.0009mg/KgChlorodibromomethane
11/01/22 12:140.0100.0009<0.0009mg/KgChloroethane
11/01/22 12:140.0050.001<0.001mg/KgChloroform
11/01/22 12:140.0100.0006<0.0006mg/KgChloromethane
11/01/22 12:140.0050.0005<0.0005mg/Kg2-Chlorotoluene
11/01/22 12:140.0050.0004<0.0004mg/Kg4-Chlorotoluene
11/01/22 12:140.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
11/01/22 12:140.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
11/01/22 12:140.0050.0006<0.0006mg/Kg1,2-Dibromoethane
11/01/22 12:140.0050.0006<0.0006mg/KgDibromomethane
11/01/22 12:140.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
11/01/22 12:140.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 10 of 27Date:11/10/2022 12:14 PM
Page 99 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
Associated Lab Samples: 91768
LRB-V25787 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/01/22 12:140.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
11/01/22 12:140.0100.001<0.001mg/KgDichlorodifluoromethane
11/01/22 12:140.0050.0008<0.0008mg/Kg1,1-Dichloroethane
11/01/22 12:140.0050.001<0.001mg/Kg1,2-Dichloroethane
11/01/22 12:140.0050.0007<0.0007mg/Kg1,1-Dichloroethene
11/01/22 12:140.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
11/01/22 12:140.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
11/01/22 12:140.0050.0004<0.0004mg/Kg1,2-Dichloropropane
11/01/22 12:140.0050.0006<0.0006mg/Kg1,3-Dichloropropane
11/01/22 12:140.0050.001<0.001mg/Kg2,2-Dichloropropane
11/01/22 12:140.0050.0008<0.0008mg/Kg1,1-Dichloropropene
11/01/22 12:140.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
11/01/22 12:140.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
11/01/22 12:140.2500.014<0.014mg/KgEthanol
11/01/22 12:140.0050.0006<0.0006mg/KgEthylbenzene
11/01/22 12:140.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
11/01/22 12:140.0100.0008<0.0008mg/KgHexachlorobutadiene
11/01/22 12:140.0100.0007<0.0007mg/Kgn-Hexane
11/01/22 12:140.0200.0006<0.0006mg/Kg2-Hexanone
11/01/22 12:140.0050.0005<0.0005mg/KgIsopropylbenzene
11/01/22 12:140.0050.001<0.001mg/Kg4-Isopropyl toluene
11/01/22 12:140.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
11/01/22 12:140.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
11/01/22 12:140.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
11/01/22 12:140.0100.001<0.001mg/KgMethylene Chloride
11/01/22 12:140.0100.0010<0.0010mg/KgNaphthalene
11/01/22 12:140.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 11 of 27Date:11/10/2022 12:14 PM
Page 100 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
Associated Lab Samples: 91768
LRB-V25787 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/01/22 12:140.0050.001<0.001mg/KgStyrene
11/01/22 12:140.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
11/01/22 12:140.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
11/01/22 12:140.0050.0009<0.0009mg/KgTetrachloroethene
11/01/22 12:140.0050.0007<0.0007mg/KgToluene
11/01/22 12:140.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
11/01/22 12:140.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
11/01/22 12:140.0050.001<0.001mg/Kg1,1,1-Trichloroethane
11/01/22 12:140.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
11/01/22 12:140.0050.0009<0.0009mg/KgTrichloroethene
11/01/22 12:140.0100.002<0.002mg/KgTrichlorofluoromethane
11/01/22 12:140.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
11/01/22 12:140.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
11/01/22 12:140.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
11/01/22 12:140.0100.0005<0.0005mg/KgVinyl Acetate
11/01/22 12:140.0100.0005<0.0005mg/KgVinyl Chloride
11/01/22 12:140.0050.0005<0.0005mg/Kgo-Xylene
11/01/22 12:140.0100.001<0.001mg/Kgm,p-Xylene
11/01/22 12:144-Bromofluorobenzene (S)103 70-130
11/01/22 12:14Dibromofluoromethane (S)98.8 84-123
11/01/22 12:14Toluene-d8 (S)91.0 76-129
LCS-V25787 LCSD-V25787Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.109 1091050.1050.100mg/KgAcetone 29-198 3.7 20
Page 12 of 27Date:11/10/2022 12:14 PM
Page 101 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
LCS-V25787 LCSD-V25787Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.120 1201190.1190.100mg/KgAcrolein 70-130 0.8 20
0.097 97.01220.1220.100mg/KgAcrylonitrile 65-134 22.8*20
0.050 1021070.0530.050mg/KgBenzene 74-127 4.8 20
0.044 89.687.80.0430.050mg/KgBromobenzene 73-125 2.0 20
0.053 1071070.0530.050mg/KgBromochloromethane 72-134 0.3 20
0.056 1121130.0560.050mg/KgBromodichloromethane 75-122 0.5 20
0.052 10495.00.0470.050mg/KgBromoform 66-135 9.2 20
0.062 1251250.0620.050mg/KgBromomethane 20-180 0.4 20
0.043 87.890.20.0450.050mg/Kgn-Butylbenzene 65-135 2.6 20
0.044 89.091.00.0450.050mg/Kgsec-Butyl benzene 66-131 2.2 20
0.044 88.688.00.0440.050mg/Kgtert-Butyl benzene 67-132 0.6 20
0.048 96.699.20.0490.050mg/KgCarbon Disulfide 61-129 2.6 20
0.048 97.01020.0510.050mg/KgCarbon Tetrachloride 64-143 5.4 20
0.047 95.692.60.0460.050mg/KgChlorobenzene 74-118 3.1 20
0.051 10396.80.0480.050mg/KgChlorodibromomethane 73-122 6.4 20
0.051 1021010.0500.050mg/KgChloroethane 33-149 1.1 20
0.051 1031010.0500.050mg/KgChloroform 73-127 1.3 20
0.056 1141150.0570.050mg/KgChloromethane 45-143 1.0 20
0.043 86.087.80.0430.050mg/Kg2-Chlorotoluene 67-124 2.0 20
0.043 86.087.80.0430.050mg/Kg4-Chlorotoluene 71-126 2.0 20
0.057 1151160.0570.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.6 20
0.053 10898.80.0490.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 8.5 20
0.054 1101020.0510.050mg/Kg1,2-Dibromoethane 70-132 7.1 20
0.054 1101080.0540.050mg/KgDibromomethane 74-133 1.1 20
0.045 90.089.60.0440.050mg/Kg1,2-Dichlorobenzene 72-123 0.4 20
0.044 88.687.60.0430.050mg/Kg1,3-Dichlorobenzene 71-120 1.1 20
Page 13 of 27* QC Fail Date:11/10/2022 12:14 PM
Page 102 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
LCS-V25787 LCSD-V25787Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.288.40.0440.050mg/Kg1,4-Dichlorobenzene 71-123 0.9 20
0.045 91.497.40.0480.050mg/KgDichlorodifluoromethane 26-146 6.3 20
0.052 1041080.0530.050mg/Kg1,1-Dichloroethane 74-127 3.5 20
0.051 1031010.0500.050mg/Kg1,2-Dichloroethane 68-128 2.1 20
0.050 1001020.0500.050mg/Kg1,1-Dichloroethene 67-149 1.7 20
0.054 1091090.0540.050mg/Kgcis-1,2-Dichloroethene 76-134 0.1 20
0.050 1021060.0530.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.2 20
0.056 1131120.0550.050mg/Kg1,2-Dichloropropane 73-130 0.8 20
0.052 10496.20.0480.050mg/Kg1,3-Dichloropropane 75-124 8.1 20
0.049 98.01020.0500.050mg/Kg2,2-Dichloropropane 50-142 3.8 20
0.046 92.698.20.0490.050mg/Kg1,1-Dichloropropene 71-130 5.8 20
0.058 1171130.0560.050mg/Kgcis-1,3-Dichloropropene 71-125 3.6 20
0.055 1101080.0540.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.0 20
1.28 1021031.291.25mg/KgEthanol 70-130 0.7 20
0.047 94.093.00.0460.050mg/KgEthylbenzene 74-128 1.0 20
0.112 1121090.1090.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 2.7 20
0.043 87.088.20.0440.050mg/KgHexachlorobutadiene 64-125 1.3 20
0.050 1021130.0560.050mg/Kgn-Hexane 70-130 10.7 20
0.058 1161080.0530.050mg/Kg2-Hexanone 61-157 7.6 20
0.043 86.688.00.0440.050mg/KgIsopropylbenzene 68-126 1.6 20
0.042 85.287.20.0430.050mg/Kg4-Isopropyl toluene 68-129 2.3 20
0.059 1191150.0570.050mg/KgMethyl Ethyl Ketone (MEK)63-149 3.5 20
0.055 1111050.0520.050mg/KgMethyl tert-butyl ether (MTBE)70-130 5.7 20
0.071 1421130.0560.050mg/Kg4-Methyl-2-Pentanone 57-162 23.3*20
0.055 1101080.0540.050mg/KgMethylene Chloride 74-129 1.8 20
0.047 94.686.60.0430.050mg/KgNaphthalene 57-157 8.8 20
Page 14 of 27* QC Fail Date:11/10/2022 12:14 PM
Page 103 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V25789QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V25787
LCS-V25787 LCSD-V25787Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.892.80.0460.050mg/Kgn-Propylbenzene 67-130 3.2 20
0.049 99.096.80.0480.050mg/KgStyrene 77-121 2.2 20
0.046 93.289.20.0440.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.3 20
0.050 10294.60.0470.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 7.1 20
0.049 99.21020.0500.050mg/KgTetrachloroethene 68-130 2.3 20
0.050 1011020.0510.050mg/KgToluene 71-129 1.1 20
0.046 92.889.00.0440.050mg/Kg1,2,3-Trichlorobenzene 68-130 4.1 20
0.048 96.492.40.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 4.2 20
0.047 95.61000.0500.050mg/Kg1,1,1-Trichloroethane 67-131 4.8 20
0.053 10798.60.0490.050mg/Kg1,1,2-Trichloroethane 70-133 8.1 20
0.052 1051050.0520.050mg/KgTrichloroethene 75-133 0.0 20
0.049 98.41050.0520.050mg/KgTrichlorofluoromethane 44-146 6.1 20
0.051 10395.60.0470.050mg/Kg1,2,3-Trichloropropane 60-137 7.2 20
0.043 87.690.20.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 2.9 20
0.044 88.689.20.0440.050mg/Kg1,3,5-Trimethylbenzene 69-128 0.6 20
0.058 1161190.0590.050mg/KgVinyl Acetate 60-140 2.8 20
0.051 1031090.0540.050mg/KgVinyl Chloride 48-147 5.8 20
0.048 97.094.80.0470.050mg/Kgo-Xylene 74-126 2.2 20
0.093 93.192.60.0920.100mg/Kgm,p-Xylene 75-124 0.5 20
1011004-Bromofluorobenzene (S)70-130
99.2101Dibromofluoromethane (S)84-123
93.892.6Toluene-d8 (S)76-129
Page 15 of 27Date:11/10/2022 12:14 PM
Page 104 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
Associated Lab Samples: 91761, 91762, 91763, 91764, 91765, 91766, 91767, 91768, 91769, 91770
LRB-V25823 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/04/22 16:380.6600.116<0.116mg/KgAcenaphthene
11/04/22 16:380.6600.105<0.105mg/KgAcenaphthylene
11/04/22 16:380.6600.152<0.152mg/KgAniline
11/04/22 16:380.6600.143<0.143mg/KgAnthracene
11/04/22 16:380.6600.139<0.139mg/KgBenzo(a)anthracene
11/04/22 16:380.6600.147<0.147mg/KgBenzo(a)pyrene
11/04/22 16:380.6600.146<0.146mg/KgBenzo(b)fluoranthene
11/04/22 16:380.6600.136<0.136mg/KgBenzo(g,h,i)perylene
11/04/22 16:380.6600.137<0.137mg/KgBenzo(k)fluoranthene
11/04/22 16:382.000.580<0.580mg/KgBenzoic Acid
11/04/22 16:380.6600.105<0.105mg/KgBenzyl alcohol
11/04/22 16:380.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
11/04/22 16:380.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
11/04/22 16:380.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
11/04/22 16:380.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
11/04/22 16:380.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
11/04/22 16:380.3300.113<0.113mg/KgButyl benzyl phthalate
11/04/22 16:380.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
11/04/22 16:380.3300.112<0.112mg/Kg4-Chloroaniline
11/04/22 16:380.6600.116<0.116mg/Kg2-Chloronaphthalene
11/04/22 16:380.6600.098<0.098mg/Kg2-Chlorophenol
11/04/22 16:381.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
11/04/22 16:380.6600.142<0.142mg/KgChrysene
11/04/22 16:380.6600.230<0.230mg/KgDibenz(a,h)anthracene
11/04/22 16:380.6600.119<0.119mg/KgDibenzofuran
11/04/22 16:380.6600.094<0.094mg/Kg1,2-Dichlorobenzene
11/04/22 16:380.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 16 of 27Date:11/10/2022 12:14 PM
Page 105 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
Associated Lab Samples: 91761, 91762, 91763, 91764, 91765, 91766, 91767, 91768, 91769, 91770
LRB-V25823 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/04/22 16:380.3300.097<0.097mg/Kg1,4-Dichlorobenzene
11/04/22 16:380.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
11/04/22 16:380.6600.095<0.095mg/Kg2,4-Dichlorophenol
11/04/22 16:380.6600.180<0.180mg/KgDiethyl phthalate
11/04/22 16:380.6600.174<0.174mg/KgDimethyl phthalate
11/04/22 16:380.3300.108<0.108mg/Kg2,4-Dimethylphenol
11/04/22 16:380.6600.107<0.107mg/KgDi-n-butyl phthalate
11/04/22 16:381.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
11/04/22 16:381.500.520<0.520mg/Kg2,4-Dinitrophenol
11/04/22 16:380.6600.096<0.096mg/Kg2,4-Dinitrotoluene
11/04/22 16:380.6600.108<0.108mg/Kg2,6-Dinitrotoluene
11/04/22 16:380.3300.143<0.143mg/KgDi-n-Octyl Phthalate
11/04/22 16:380.6600.123<0.123mg/KgFluoranthene
11/04/22 16:380.6600.128<0.128mg/KgFluorene
11/04/22 16:380.6600.106<0.106mg/KgHexachlorobenzene
11/04/22 16:380.6600.097<0.097mg/KgHexachlorobutadiene
11/04/22 16:380.6600.157<0.157mg/KgHexachlorocyclopentadiene
11/04/22 16:380.6600.079<0.079mg/KgHexachloroethane
11/04/22 16:380.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
11/04/22 16:380.6600.191<0.191mg/KgIsophorone
11/04/22 16:380.6600.106<0.106mg/Kg1-Methylnaphthalene
11/04/22 16:380.6600.100<0.100mg/Kg2-Methylnaphthalene
11/04/22 16:380.6600.097<0.097mg/Kg2-Methylphenol
11/04/22 16:380.6600.084<0.084mg/Kg3&4 Methylphenol
11/04/22 16:380.6600.144<0.144mg/KgNaphthalene
11/04/22 16:380.6600.096<0.096mg/Kg2-Nitroaniline
11/04/22 16:380.6600.120<0.120mg/Kg3-Nitroaniline
Page 17 of 27Date:11/10/2022 12:14 PM
Page 106 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
Associated Lab Samples: 91761, 91762, 91763, 91764, 91765, 91766, 91767, 91768, 91769, 91770
LRB-V25823 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
11/04/22 16:380.3300.093<0.093mg/Kg4-Nitroaniline
11/04/22 16:380.3300.116<0.116mg/KgNitrobenzene
11/04/22 16:380.6600.088<0.088mg/Kg2-Nitrophenol
11/04/22 16:380.6600.117<0.117mg/Kg4-Nitrophenol
11/04/22 16:380.6600.263<0.263mg/KgN-Nitrosodimethylamine
11/04/22 16:380.6600.181<0.181mg/KgN-Nitrosodiphenylamine
11/04/22 16:380.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
11/04/22 16:381.000.347<0.347mg/KgPentachlorophenol
11/04/22 16:380.6600.208<0.208mg/KgPhenanthrene
11/04/22 16:380.6600.112<0.112mg/KgPhenol
11/04/22 16:380.6600.134<0.134mg/KgPyrene
11/04/22 16:380.3300.079<0.079mg/KgPyridine
11/04/22 16:380.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
11/04/22 16:380.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
11/04/22 16:380.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
11/04/22 16:382-Fluorobiphenyl (S)85.0 44-115
11/04/22 16:382-Fluorophenol (S)75.3 35-115
11/04/22 16:38Nitrobenzene-d5 (S)81.4 37-122
11/04/22 16:384-Terphenyl-d14 (S)94.6 54-127
11/04/22 16:382,4,6-Tribromophenol (S)74.4 39-132
11/04/22 16:38Phenol-d5 (S)71.4 34-121
LCS-V25823Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
85.61.431.67mg/KgAcenaphthene 40-123
84.41.411.67mg/KgAcenaphthylene 32-132
Page 18 of 27Date:11/10/2022 12:14 PM
Page 107 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
LCS-V25823Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1302.171.67mg/KgAniline 12-197
91.61.531.67mg/KgAnthracene 47-123
89.81.501.67mg/KgBenzo(a)anthracene 49-126
97.61.631.67mg/KgBenzo(a)pyrene 45-129
95.21.591.67mg/KgBenzo(b)fluoranthene 45-132
86.81.451.67mg/KgBenzo(g,h,i)perylene 43-134
92.21.541.67mg/KgBenzo(k)fluoranthene 47-132
41.60.6951.67mg/KgBenzoic Acid 10-83
88.61.481.67mg/KgBenzyl alcohol 29-122
79.01.321.67mg/KgBis(2-Chloroethoxy)methane 36-121
83.21.391.67mg/KgBis(2-Chloroethyl)ether 31-120
88.01.471.67mg/KgBis(2-Chloroisopropyl)ether 33-131
96.41.611.67mg/KgBis(2-ethylhexyl)phthalate 51-133
92.21.541.67mg/Kg4-Bromophenyl phenyl ether 46-124
94.01.571.67mg/KgButyl benzyl phthalate 48-132
76.61.281.67mg/Kg4-Chloro-3-methylphenol 45-122
81.41.361.67mg/Kg4-Chloroaniline 17-106
85.61.431.67mg/Kg2-Chloronaphthalene 41-114
85.01.421.67mg/Kg2-Chlorophenol 34-121
89.21.491.67mg/Kg4-Chlorophenyl phenyl ether 45-121
89.21.491.67mg/KgChrysene 50-124
99.41.661.67mg/KgDibenz(a,h)anthracene 45-134
85.61.431.67mg/KgDibenzofuran 44-120
79.01.321.67mg/Kg1,2-Dichlorobenzene 33-117
76.61.281.67mg/Kg1,3-Dichlorobenzene 30-115
77.81.301.67mg/Kg1,4-Dichlorobenzene 31-115
76.01.271.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 19 of 27Date:11/10/2022 12:14 PM
Page 108 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
LCS-V25823Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
78.41.311.67mg/Kg2,4-Dichlorophenol 40-122
89.81.501.67mg/KgDiethyl phthalate 50-124
89.21.491.67mg/KgDimethyl phthalate 48-124
1011.691.67mg/Kg2,4-Dimethylphenol 30-127
98.21.641.67mg/KgDi-n-butyl phthalate 51-128
83.81.401.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
80.81.351.67mg/Kg2,4-Dinitrophenol 27-129
91.61.531.67mg/Kg2,4-Dinitrotoluene 48-126
89.81.501.67mg/Kg2,6-Dinitrotoluene 46-124
96.41.611.67mg/KgDi-n-Octyl Phthalate 45-140
85.01.421.67mg/KgFluoranthene 50-127
88.61.481.67mg/KgFluorene 43-125
89.81.501.67mg/KgHexachlorobenzene 45-122
75.41.261.67mg/KgHexachlorobutadiene 32-123
70.01.171.67mg/KgHexachlorocyclopentadiene 32-117
76.01.271.67mg/KgHexachloroethane 28-117
88.61.481.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
64.01.071.67mg/KgIsophorone 30-122
71.81.201.67mg/Kg1-Methylnaphthalene 40-119
71.81.201.67mg/Kg2-Methylnaphthalene 38-122
88.61.481.67mg/Kg2-Methylphenol 32-122
77.81.301.67mg/Kg3&4 Methylphenol 34-119
71.81.201.67mg/KgNaphthalene 35-123
92.21.541.67mg/Kg2-Nitroaniline 44-127
91.61.531.67mg/Kg3-Nitroaniline 33-119
91.01.521.67mg/Kg4-Nitroaniline 63-147
70.61.181.67mg/KgNitrobenzene 34-122
Page 20 of 27Date:11/10/2022 12:14 PM
Page 109 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
LCS-V25823Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
74.21.241.67mg/Kg2-Nitrophenol 36-123
92.21.541.67mg/Kg4-Nitrophenol 30-132
70.01.171.67mg/KgN-Nitrosodimethylamine 10-146
1101.831.67mg/KgN-Nitrosodiphenylamine 38-127
83.81.401.67mg/KgN-Nitroso-di-n-propylamine 36-120
1041.741.67mg/KgPentachlorophenol 25-133
90.41.511.67mg/KgPhenanthrene 50-121
80.21.341.67mg/KgPhenol 34-121
88.61.481.67mg/KgPyrene 47-127
62.81.051.67mg/KgPyridine 10-80
72.41.211.67mg/Kg1,2,4-Trichlorobenzene 34-118
85.61.431.67mg/Kg2,4,5-Trichlorophenol 41-124
86.21.441.67mg/Kg2,4,6-Trichlorophenol 39-126
87.42-Fluorobiphenyl (S)44-115
78.92-Fluorophenol (S)35-115
72.4Nitrobenzene-d5 (S)37-122
94.04-Terphenyl-d14 (S)54-127
78.02,4,6-Tribromophenol (S)39-132
74.4Phenol-d5 (S)34-121
V 91686-MS-V25823 V 91686-MSD-V25823Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.36 81.41.341.671.67<0.116mg/KgAcenaphthene 80.2 40-123 1.4 20
1.34 80.21.331.671.67<0.105mg/KgAcenaphthylene 79.6 32-132 0.7 20
1.42 85.01.421.671.67<0.152mg/KgAniline 85.0 12-197 0.0 20
Page 21 of 27Date:11/10/2022 12:14 PM
Page 110 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
V 91686-MS-V25823 V 91686-MSD-V25823Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.43 85.61.441.671.67<0.143mg/KgAnthracene 86.2 47-123 0.6 20
1.42 85.01.441.671.67<0.139mg/KgBenzo(a)anthracene 86.2 49-126 1.3 20
1.55 92.81.581.671.67<0.147mg/KgBenzo(a)pyrene 94.6 45-129 1.9 20
1.46 87.41.481.671.67<0.146mg/KgBenzo(b)fluoranthene 88.6 45-132 1.3 20
1.35 80.81.381.671.67<0.136mg/KgBenzo(g,h,i)perylene 82.6 43-134 2.1 20
1.48 88.61.501.671.67<0.137mg/KgBenzo(k)fluoranthene 89.8 47-132 1.3 20
1.22 73.01.141.671.67<0.580mg/KgBenzoic Acid 68.2 10-83 6.7 20
1.44 86.21.381.671.67<0.105mg/KgBenzyl alcohol 82.6 29-122 4.2 20
1.26 75.41.241.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 74.2 36-121 1.6 20
1.32 79.01.241.671.67<0.107mg/KgBis(2-Chloroethyl)ether 74.2 31-120 6.2 20
1.39 83.21.321.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 79.0 33-131 5.1 20
1.53 91.61.561.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 93.4 51-133 1.9 20
1.44 86.21.431.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 85.6 46-124 0.6 20
1.52 91.01.521.671.67<0.113mg/KgButyl benzyl phthalate 91.0 48-132 0.0 20
1.25 74.81.251.671.67<0.092mg/Kg4-Chloro-3-methylphenol 74.8 45-122 0.0 20
1.23 73.61.241.671.67<0.112mg/Kg4-Chloroaniline 74.2 17-106 0.8 20
1.35 80.81.351.671.67<0.116mg/Kg2-Chloronaphthalene 80.8 41-114 0.0 20
1.38 82.61.311.671.67<0.098mg/Kg2-Chlorophenol 78.4 34-121 5.2 20
1.42 85.01.401.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 83.8 45-121 1.4 20
1.46 87.41.451.671.67<0.142mg/KgChrysene 86.8 50-124 0.6 20
1.50 89.81.511.671.67<0.230mg/KgDibenz(a,h)anthracene 90.4 45-134 0.6 20
1.34 80.21.331.671.67<0.119mg/KgDibenzofuran 79.6 44-120 0.7 20
1.22 73.01.171.671.67<0.094mg/Kg1,2-Dichlorobenzene 70.0 33-117 4.1 20
1.20 71.81.141.671.67<0.097mg/Kg1,3-Dichlorobenzene 68.2 30-115 5.1 20
1.21 72.41.151.671.67<0.097mg/Kg1,4-Dichlorobenzene 68.8 31-115 5.0 20
0.795 47.60.8791.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 52.6 22-121 10.0 20
Page 22 of 27Date:11/10/2022 12:14 PM
Page 111 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
V 91686-MS-V25823 V 91686-MSD-V25823Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.27 76.01.261.671.67<0.095mg/Kg2,4-Dichlorophenol 75.4 40-122 0.7 20
1.42 85.01.431.671.67<0.180mg/KgDiethyl phthalate 85.6 50-124 0.7 20
1.42 85.01.401.671.67<0.174mg/KgDimethyl phthalate 83.8 48-124 1.4 30
1.55 92.81.571.671.67<0.108mg/Kg2,4-Dimethylphenol 94.0 30-127 1.2 20
1.54 92.21.551.671.67<0.107mg/KgDi-n-butyl phthalate 92.8 51-128 0.6 20
1.37 82.01.431.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 85.6 29-132 4.2 20
1.59 95.21.551.671.67<0.520mg/Kg2,4-Dinitrophenol 92.8 27-129 2.5 20
1.38 82.61.421.671.67<0.096mg/Kg2,4-Dinitrotoluene 85.0 48-126 2.8 20
1.37 82.01.401.671.67<0.108mg/Kg2,6-Dinitrotoluene 83.8 46-124 2.1 20
1.51 90.41.571.671.67<0.143mg/KgDi-n-Octyl Phthalate 94.0 45-140 3.8 20
1.32 79.01.341.671.67<0.123mg/KgFluoranthene 80.2 50-127 1.5 20
1.39 83.21.371.671.67<0.128mg/KgFluorene 82.0 43-125 1.4 20
1.39 83.21.411.671.67<0.106mg/KgHexachlorobenzene 84.4 45-122 1.4 20
1.18 70.61.131.671.67<0.097mg/KgHexachlorobutadiene 67.6 32-123 4.3 20
1.18 70.61.151.671.67<0.157mg/KgHexachlorocyclopentadiene 68.8 32-117 2.5 20
1.19 71.21.121.671.67<0.079mg/KgHexachloroethane 67.0 28-117 6.0 20
1.38 82.61.391.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 83.2 45-133 0.7 20
1.03 61.61.021.671.67<0.191mg/KgIsophorone 61.0 30-122 0.9 20
1.15 68.81.171.671.67<0.106mg/Kg1-Methylnaphthalene 70.0 40-119 1.7 20
1.16 69.41.161.671.67<0.100mg/Kg2-Methylnaphthalene 69.4 38-122 0.0 20
1.36 81.41.341.671.67<0.097mg/Kg2-Methylphenol 80.2 32-122 1.4 20
1.23 73.61.191.671.67<0.084mg/Kg3&4 Methylphenol 71.2 34-119 3.3 20
1.14 68.21.141.671.67<0.144mg/KgNaphthalene 68.2 35-123 0.0 20
1.47 88.01.471.671.67<0.096mg/Kg2-Nitroaniline 88.0 44-127 0.0 20
1.40 83.81.421.671.67<0.120mg/Kg3-Nitroaniline 85.0 33-119 1.4 20
1.35 80.81.411.671.67<0.093mg/Kg4-Nitroaniline 84.4 63-147 4.3 20
Page 23 of 27Date:11/10/2022 12:14 PM
Page 112 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V25983QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V25823
V 91686-MS-V25823 V 91686-MSD-V25823Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.11 66.41.101.671.67<0.116mg/KgNitrobenzene 65.8 34-122 0.9 20
1.17 70.01.171.671.67<0.088mg/Kg2-Nitrophenol 70.0 32-123 0.0 20
1.45 86.81.441.671.67<0.117mg/Kg4-Nitrophenol 86.2 30-132 0.6 20
1.11 66.41.061.671.67<0.263mg/KgN-Nitrosodimethylamine 63.4 10-146 4.6 30
1.61 96.41.661.671.67<0.181mg/KgN-Nitrosodiphenylamine 99.4 38-127 3.0 20
1.30 77.81.271.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 76.0 36-120 2.3 20
1.70 1021.751.671.67<0.347mg/KgPentachlorophenol 105 25-133 2.8 20
1.40 83.81.421.671.67<0.208mg/KgPhenanthrene 85.0 50-121 1.4 20
1.27 76.01.241.671.67<0.112mg/KgPhenol 74.2 34-121 2.3 20
1.42 85.01.451.671.67<0.134mg/KgPyrene 86.8 47-127 2.0 20
0.741 44.30.6941.671.67<0.079mg/KgPyridine 41.5 10-80 6.5 20
1.14 68.21.111.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 66.4 34-118 2.6 20
1.37 82.01.361.671.67<0.096mg/Kg2,4,5-Trichlorophenol 81.4 41-124 0.7 20
1.35 80.81.361.671.67<0.096mg/Kg2,4,6-Trichlorophenol 81.4 39-126 0.7 20
80.82-Fluorobiphenyl (S)80.2 44-115
73.32-Fluorophenol (S)70.5 35-115
68.8Nitrobenzene-d5 (S)66.4 37-122
89.84-Terphenyl-d14 (S)89.2 54-127
70.62,4,6-Tribromophenol (S)71.4 39-132
70.3Phenol-d5 (S)66.9 34-121
Page 24 of 27Date:11/10/2022 12:14 PM
Page 113 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L647181QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L646942
Associated Lab Samples: 91761, 91762, 91763, 91764, 91765, 91766, 91767, 91768
LRB-L646942 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/04/22 13:580.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L646942Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1034.114.00mg/KgChromium, Hexavalent 80-120
V 91754-DUP-L646942Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 14:300.4<0.200< 0.200mg/KgChromium, Hexavalent
V 91754-MS-L646942 V 91754-MSD-L646942Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec
36.1 90.257474140.0< 0.141mg/KgChromium, Hexavalent 77.4 75-125
Page 25 of 27Date:11/10/2022 12:14 PM
Page 114 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L647184QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L646943
Associated Lab Samples: 91769, 91770
LRB-L646943 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
11/04/22 17:250.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L646943Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
93.03.724.00mg/KgChromium, Hexavalent 80-120
V 91769-DUP-L646943Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 17:589.0<0.2000.219mg/KgChromium, Hexavalent
V 91769-MS-L646943 V 91769-MSD-L646943Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec
34.4 85.824362339.8< 1.40mg/KgChromium, Hexavalent 39.0*75-125
Page 26 of 27* QC Fail Date:11/10/2022 12:14 PM
Page 115 of 119
Quality Control Data
22-301-0015Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
BOU-014
Dry Weight Determination
SW-DRYWT
V25892QC Analytical Batch:
Analysis Method:
Analysis Description:
V 91770-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:195.716.215.3%Moisture
V 91773-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 11/04/22 11:190.519.819.7%Moisture
Page 27 of 27Date:11/10/2022 12:14 PM
Page 116 of 119
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-301-0015
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.2C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:10/28/2022 16:02:36
Special precautions or instructions included?
Comments:
Page 117 of 119
Page 118 of 119
Page 119 of 119

Appendix B
DEQ Risk Calculator

Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Prepared By:Hart & Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC 28203
Site Wide Final Grade Soil - Hypothetical Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
Blythe Isenhour
4920 Old Pineville Road, Charlotte, Mecklenburg Co.
Division of Waste Management - Brownfields Program
Brownfields Project No. 23067-19-060
July 2022
May 2022 EPA RSL Table
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: Brownfields Project No. 23067-19-060
Exposure Unit ID: Site Wide Final Grade Soil - Hypothetical Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2022Basis: May 2022 EPA RSL TableSite ID: Brownfields Project No. 23067-19-060Exposure Unit ID: Site Wide Final Grade Soil - Hypothetical Worst CaseNOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsExposure Point Concentration (mg/kg)Notes: CAS NumberChemicalFor the chemicals highlighted in blue, data entry notes are provided in the PSRG Table link on the Main MenuMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion0.108 67-64-1Acetonemg/kg18.4 7440-38-2Arsenic, Inorganicmg/kg246 7440-39-3Bariummg/kg0.122 7440-43-9Cadmium (Water)mg/kg0.003 75-15-0Carbon Disulfidemg/kg57 16065-83-1Chromium(III), Insoluble Saltsmg/kg3.72 18540-29-9Chromium(VI)mg/kg21 7439-92-1~Lead and Compoundsmg/kg0.207 7439-97-6~Mercury (elemental)mg/kg0.011 78-93-3Methyl Ethyl Ketone (2-Butanone)mg/kg0.602 7782-49-2Seleniummg/kg0.0448 7440-22-4Silvermg/kgInput Form 2ASoil Exposure Point Concentration TableDescription of Exposure Point Concentration Selection:North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: Brownfields Project No. 23067-19-060
Exposure Unit ID: Site Wide Final Grade Soil - Hypothetical Worst Case
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 3.9E-05 5.9E-01 NO
Groundwater Use* NC NC NC
Soil NC NC NC
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: Brownfields Project No. 23067-19-060
Exposure Unit ID: Site Wide Final Grade Soil - Hypothetical Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.108 0.108 0.108 1.5E-06 1.5E-06
7440-38-2 Arsenic, Inorganic 18.4 18.4 18.4 2.4E-05 3.4E-06 4.7E-10 2.7E-05 4.7E-01 5.6E-02 2.0E-05 5.3E-01
7440-39-3 Barium 246 246 246 1.6E-02 8.0E-06 1.6E-02
7440-43-9 Cadmium (Water) 0.122 0.122 0.122 1.3E-12 1.3E-12 1.6E-02 7.4E-04 2.0E-07 1.6E-02
75-15-0 Carbon Disulfide 0.003 0.003 0.003 3.8E-07 1.3E-06 1.7E-06
16065-83-1 Chromium(III), Insoluble Salts 57 57 57 4.9E-04 4.9E-04
18540-29-9 Chromium(VI) 3.72 3.72 3.72 1.2E-05 5.2E-09 1.2E-05 1.6E-02 6.0E-07 1.6E-02
7439-92-1 ~Lead and Compounds 21 21 21 <SL** <SL** <SL**
7439-97-6 ~Mercury (elemental) 0.207 0.207 0.207 1.8E-02 1.8E-02
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.011 0.011 0.011 2.3E-07 1.6E-07 4.0E-07
7782-49-2 Selenium 0.602 0.602 0.602 1.5E-03 4.9E-10 1.5E-03
7440-22-4 Silver 0.0448 0.0448 0.0448 1.1E-04 1.1E-04
Cumulative: 3.9E-05 5.9E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: July 2022
Basis: May 2022 EPA RSL Table
Site ID: Brownfields Project No. 23067-19-060
Exposure Unit ID: Site Wide Final Grade Soil - Hypothetical Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone NC NC NC NC NC NC NC NC NC NC NC
7440-38-2 Arsenic, Inorganic NC NC NC NC NC NC NC NC NC NC NC
7440-39-3 Barium NC NC NC NC NC NC NC NC NC NC NC
7440-43-9 Cadmium (Water) NC NC NC NC NC NC NC NC NC NC NC
75-15-0 Carbon Disulfide NC NC NC NC NC NC NC NC NC NC NC16065-83-1 Chromium(III), Insoluble Salts NC NC NC NC NC NC NC NC NC NC NC
18540-29-9 Chromium(VI) NC NC NC NC NC NC NC NC NC NC NC
7439-92-1 ~Lead and Compounds NC NC NC NC NC NC NC NC
7439-97-6 ~Mercury (elemental) NC NC NC NC NC NC NC NC NC NC NC
78-93-3 Methyl Ethyl Ketone (2-Butanone) NC NC NC NC NC NC NC NC NC NC NC
7782-49-2 Selenium NC NC NC NC NC NC NC NC NC NC NC
7440-22-4 Silver NC NC NC NC NC NC NC NC NC NC NC
Cumulative:NC NC
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator