20050 Rite Aid CNE B3 Soil Export email and tables 20221220

From:Andrew Besu
To:Minnich, Carolyn
Cc:Scott Carr; Matt Ingalls
Subject:RE: [External] CAMP North End In-situ Soil Sampling Request
Date:Tuesday, December 20, 2022 10:08:20 AM
Attachments:image005.pngCNE B3 In-Situ Data Summary Package.pdf
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Hi Carolyn,

H&H completed in-situ soil characterization activities on December 12, 2022 for approximately 3,100
CYs of soil that will be generated by the PD during upcoming grading activities for redevelopment of
Building 3 (B3) at the CAMP North End/Rite Aid Brownfields Property (BPN 20050-16-060). The soil
characterization activities were completed in general accordance with the DEQ approved
environmental management plan (EMP) and scope of work proposed in the December 8, 2022 email
below. Based on soil sampling data discussed below, the PD is requesting approval to export
approximately 2,450 CYs of soil from the CS-2 though CS-5 evaluation areas to Old 27 LCID Landfill
(120 Tate Street, Mt. Holly, North Carolina). Included in the attached data summary package are
figures depicting the work area, a summary of in-situ soil analytical data, and the laboratory
analytical report.

As noted on the attached Figure 3, the B3 excavation area was divided into five (5) areas (CS-1
through CS-5), with each area comprised of between 500 CYs to 650 CYs of soil. H&H advance
three(3) soil borings in each of the five (5) soil evaluation areas using a decontaminated stainless
steel hand auger to the proposed grading cut depths of 2 ft bgs (CS-1) or 4 ft bgs (CS-2 through CS-
5). The soil borings were observed for visual and olfactory evidence of impacts, and screened for the
presence of volatile organic vapors with a calibrated photoionization detector (PID). A grab sample
was collected from each characterization area for analysis of volatile organic compounds (VOCs) by
EPA Method 8260 from undisturbed portions of the aliquot exhibiting the highest potential for
impact based on field screening results. The three (3) aliquots in each area where then homogenized
for a composite sample for analysis of semi-VOCs (SVOCs) by EPA Method 8270, and RCRA metals
plus hexavalent chromium by EPA Methods 6020/7179/7199. In addition to the five (5) soil samples
discussed above, H&H collected a duplicate sample from one of the five soil samples for the same
analyses as the parent sample for quality assurance/quality control (QA/QC) purposes. The soil
samples were placed in dedicated laboratory supplied sample containers, labeled with the sample
identification, date, and requested analyses and placed in a laboratory supplied cooler with ice. The
samples were then delivered to Waypoint Analytical under standard chain of custody protocols for
the analyses described above.

Soil analytical results were compared to the DEQ Preliminary Soil Remediation Goals (PSRGs) dated
July 2022, Site-specific background metals concentrations, and background metals concentrations at
the Old 27 LCID Landfill. As summarized in the attached Table 1, laboratory analytical results
indicate estimated trace levels of the VOCs acetone and methylene chloride in each of the samples
at a concentrations above the laboratory method detection limit, but well below their respective
PSRGs. The VOC n-hexane was detected at an estimated concentration of 0.001 J mg/kg in soil
samples CS-3, CS-4, and CS-DUP, well below the most stringent protection of groundwater PSRG of
55 mg/kg. The polycyclic aromatic hydrocarbons (PAHs) benzo(a)anthracene (0.261 J mg/kg),
benzo(b)fluoranthene (0.326 J mg/kg) chrysene (0.230 J mg/kg), fluoranthene (0.486 J mg/kg), and
pyrene (0.402 J mg/kg) were detected above laboratory method detection limits but below PSRGs in
sample CS-1. Additionally, the compound benzo(a)pyrene (0.236 J mg/kg) was detected in sample
CS-1 above the Residential PSRG of 0.11 mg/kg and protection of groundwater PSRG of 0.12 mg/kg.
As anticipated, metals were detected in each of the samples. The metal arsenic was detected at
concentrations above the Residential PSRGs of 0.68 mg/kg in each sample. Additionally, the metal
hexavalent chromium was detected above of the Residential PSRG of 0.31 mg/kg in soil samples CS-2
(0.654 mg/kg) and CS-DUP (0.365 mg/kg). However, the detected concentrations of arsenic and
hexavalent chromium are consistent with background levels at the Site and the Old 27 LCID Landfill.

As such, H&H is requesting your approval to export soils represented by samples CS-2 through CS-5
to the Old 27 LCID landfill. Soil represented by sample CS-1 will be managed on-site or exported to
the Republic CMS Landfill in Concord, North Carolina in accordance with the EMP.

Thank you for your assistance with this project and we appreciate your prompt review and approval
to transport the soils from B3 within the CS-2 through CS-5 evaluation areas.

Andrew

Andrew Besu, Environmental Redevelopment ManagerHart & Hickman, PC2923 S Tryon Street, Suite 100 · Charlotte, NC 28203Direct: 704-887-4618 · Mobile: [phone]www.harthickman.com

From: Minnich, Carolyn <[e-mail]>
Sent: Thursday, December 8, 2022 1:32 PM
To: Andrew Besu <[e-mail]>
Cc: Scott Carr <[e-mail]>; Matt Ingalls <[e-mail]>
Subject: RE: [External] CAMP North End In-situ Soil Sampling Request

Good afternoon. The scope of work you have outlined is in accordance with with the EMP revised on
3/28/2019) and with current best practices in the brownfields program. Just a reminder, the final
data will need to be sumarized and compared with Old 27 LCID site specific data. Summary report
will need certified lab reports and sealed by NC PE or PG.

It’s a quick turn around, not much time for error.
I’ll be out of the office on 12/15 & 16 (Picking up son at college and next day he has shoulder
surgery).

CFM

Carolyn Minnich
Brownfields Project ManagerDivision of Waste ManagementDepartment of Environmental Quality 704 661 0330 office/mobile
[e-mail]

1646 Mail Service Center
Raleigh, NC 27699-1646

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Andrew Besu <[e-mail]>
Sent: Thursday, December 8, 2022 12:44 PM
To: Minnich, Carolyn <[e-mail]>
Cc: Scott Carr <[e-mail]>; Matt Ingalls <[e-mail]>
Subject: [External] CAMP North End In-situ Soil Sampling Request

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
attachment to Report Spam.

Hi Carolyn,

On behalf of Scott Carr (CAMP North End/Rite Aid Brownfields Property, BPN 20050-16-060), we are
seeking approval via this work plan summary email to conduct soil characterization activities for
redevelopment activities for the Building 3 (B3) redevelopment proposed in the central portion of
the Site (see attached Site Location Map -Figure 1). During renovation activities of Building 3, the
contractor anticipates generating approximately 3,100 CYs of soil to be exported off-Site. The
purpose of the characterization will be to determine export/disposal options for excavated soil.
Based on timing, Scott would like to send the soil to the Old 27 land clearing and inert debris (LCID)
landfill located in Mount Holly, NC, if acceptable, based on the results of the proposed soil
characterization activities as described below.

H&H met on-Site this week with the construction contractor and determined the following
information regarding the proposed B3 project.

• there is not enough room on-site to manage the soil to be generated during the pending B3
construction activities without handling the soil multiple times;
• contractors want to initiate grading activities next Wednesday 12/14; and
• the depths of the excavation will range from 2 to 4 ft below the ground surface (bgs),
estimated volumes, and the boundary of the excavation(s) are as depicted on the attached Sample
Location Map - Figure 2.

Please note, grading is anticipated to begin Wednesday 12/14 and H&H has tentatively scheduled
soil characterization field activities on Monday 12/12. H&H proposes to complete in-situ soil
characterization using an approach similar as to what is described in the DEQ approved In-situ Soil
Characterization Work Plan completed for CIP roadway improvement at the Site dated September 4,
2019. As noted on the attached Figure 2, we propose dividing the B3 excavation area into five (5)
areas (CS-1 through CS-5), with each area comprised of between 500 CYs to 650 CYs of soil. In each
of the five areas, H&H proposes to collect three (3) aliquot soil samples with a decontaminated
stainless steel hand auger for the following analysis:

one grab sample per area (5 areas total) collected from the “worst case” aliquot and analyzed
for VOCs by EPA Method 8260; and
one composite sample per area (5 areas total) collected and analyzed for SVOCs by EPA
Method 8270 and RCRA Metals by EPA Methods 6020/7471 (plus Cr VI by EPA Method 7199).

In addition to the five (5) soil samples discussed above, H&H proposes to collect a duplicate sample
from one of the five soil samples for analysis of VOCs by EPA Method 8260, SVOCs by EPA Method
8270, and RCRA Metals by EPA Methods 6020/7471 (plus Cr VI by EPA Method 7199) for quality
assurance/quality control (QA/QC) purposes. H&H will submit the soil samples to a NC-certified
laboratory under a chain of custody. Upon receipt of the data, H&H will generate an email soil
transfer request which includes a summary of soil characterization activities and table comparing soil
characterization results to DEQ preliminary soil remediation goals (PSRGs) and Old 27 background
metals concentrations. Additionally, H&H will submit a letter report separate from the email
transfer request for documentation purposes. H&H will share this data with DEQ to determine
disposal options for each of the excavation areas (C1-C5).

We appreciate your prompt review of this proposed work plan. Please feel free to reach out to me
or Matt Ingalls should you have any questions.

Thanks,
Andrew

Andrew Besu, Environmental Redevelopment ManagerHart & Hickman, PC2923 S Tryon Street, Suite 100 · Charlotte, NC 28203Direct: 704-887-4618 · Mobile: [phone]www.harthickman.com

Table 1Summary of In-situ Soil Analytical Data Camp North EndRite Aid Brownfields Site Brownfields Project No. 20050-16-060 H&H Project: ATL-007Evaluation AreaSample IDSample Type Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite GrabDepth (ft bgs) 0-4 2-4 0-4 2-4 0-4 2-4 0-4 2-4 0-4 2-4DateUnitsRange MeanVOCs by EPA 8260AcetoneNA0.015 JNA0.004 JNA0.003 JNA0.011 JNA0.005 JNA0.005 J14,000 210,000 25 -- ---- --n-HexaneNA <0.0009 NA <0.0009 NA0.001 JNA0.001 JNA0.001 JNA <0.0010130540 55-- ---- --Methylene ChlorideNA0.003 JNA0.005 JNA0.005 JNA0.004 JNA0.004 JNA0.004 J58650 0.025-- ---- --SVOCs by 8270 Benzo(a)anthracene0.261 JNA <0.179 NA <0.178 NA <0.181 NA <0.182 NA <0.202 NA1.1210.35--------Benzo(a)pyrene0.236 JNA <0.189 NA <0.189 NA <0.192 NA <0.192 NA <0.214 NA0.11 2.10.12--------Benzo(b)fluoranthene0.326 JNA <0.188 NA <0.187 NA <0.190 NA <0.191 NA <0.213 NA1.1211.2--------Chrysene0.230 JNA <0.182 NA <0.182 NA <0.185 NA <0.186 NA <0.207 NA110 2,100 36--------Fluoranthene0.486 JNA <0.158 NA <0.158 NA <0.160 NA <0.161 NA <0.179 NA480 6,000 670--------Pyrene0.402 JNA<0.172 NA<0.172 NA<0.175 NA<0.175 NA<0.195 NA360 4,500 440---- -- --Metals by 6020/7199/7471Arsenic1.71 JNA1.62 JNA1.63 JNA1.99 JNA1.01 JNA2.16 JNA0.68 3.05.81.0 - 18 4.8<2.35 - 5.251.2 - 2.7Barium27.9NA79.0NA64.5NA39NA82.2NA26.6 JNA3,100 47,000 58050 - 1,000 356--64 - 220Cadmium<0.176 NA<0.170 NA<0.170 NA<0.173 NA<0.173 NA<0.193 NA1.4203.01.0 - 10 4.3<1.12 - 1.64<0.045 - <0.051Chromium39.9NA65.7NA71.4NA33.6NA17.6NA92.4NANENENE7.0 - 300 6523.4 - 70.737 - 90Chromium (III)39.9NA65.046NA71.035NA33.404NA17.6NA92.4NA24,000 350,000 360,000NSNS23.4 - 70.736.7 - 89.7Chromium (VI)<0.188 NA0.654NA0.365NA0.196 JNA <0.187 NA <0.205 NA0.31 6.53.8NSNS<2.35 - 2.18 J<0.27 - 2.0Lead9.77NA7.93NA13.3NA8.09NA6.71NA13.6NA400 800270ND - 50 1613.3 - 53.46.6 - 18Mercury (Total)0.0179 JNA0.0164 JNA0.0175 JNA <0.0157 NA <0.0157 NA0.0204 JNA2.39.7NE0.03 - 0.52 0.121<0.108 - 0.3030.032 J - 0.074Selenium<1.97NA<1.91NA<1.90NA<1.93NA<1.94NA<2.16NA78 1,200 2.1<0.1 - 0.8 0.42<2.41 - 7.771.2 J - 4.1Silver<0.125 NA<0.121 NA<0.121 NA<0.123 NA<0.123 NA<0.137 NA78 1,200 3.4ND - 5.0 NS--<0.062 - <0.071Notes:1) NC Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022 and based uponcarcinogenic total risk of 1.0 x 10-6 and non-carcinogenic target hazard quotient of 0.2.2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.Cd and Ag concentrations were taken from Southeastern & Conterminous U.S. soils.3)Range of site-specific metal background concentrations collected by H&H at the Rite Aid Brownfields site on November 16, 2016 (excluding soil sample SSB-10).4) Range of Old 27 LCID landfill import site background metal concentrations collected by H&H on December 17, 2020.With the exception of metals, only constituents detected in at least one sample are shown.Bold indicates exceedance of Residential PSRG and background concentrations.Gray shading indicates an exceedance of Protection of Groundwater PSRG and background concentrations.Laboratory analytical methods are shown in parentheses.Compound concentrations are reported to the laboratory method detection limits.VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic Compounds; ft bgs = feet below ground surfaceNE = Not Established; NS = Not Specified; NA = Not Analyzed; -- = Not Applicable; LCID = land-clearing and inert debris landfillJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.Old 27 LCID Range of Background Metal Concentrations (4)Health Based PSRGs (1) ResidentialIndustrial/ CommercialArea-Specific Background Metal Concentrations (2)CS-3CS-4CS-5Site-Specific Background Metal Concentrations (3)Building 312/12/202212/12/202212/12/202212/12/2022CS-1CS-2/CS-DUPProtection of Groundwater0-212/12/2022mg/kghttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/ATCO LLC - ATC/ATL-007 Woodward Ave Multi-Family/In-Situ Soil Sampling 12.12.2022/Table 3 -Summary of In-situ Soil Analytical DataTable 1Hart & Hickman, PC
TITLE
PROJECT
SITE LOCATION MAP
CAMP NORTH END
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
6-14-19 0
1ATL-006
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NC 1967
REVISED/INSPECTED 1988
AND
DERITA, NC 1993
SITE
RAMP REVISED PER 8/20/2018ON SITE MTG AND SHOP DWGS.
ROOF ACCESS DELETED PER OWNER DIRECTION
CAMP NORTH END
- MULTI-FAMILY
BUILDINGS
ATCO
110 RAZADES WAY
CHARLOTTE NC
1020123
OVERALL SITE PLAN
N/A
LDI
LDI
LDI
CA1-03
8/3/2022 2:26 PM CASSIDY FRANKLIN \\CHFILES\PROJECTS\_2020\1020123\CAD\EXHIBITS\1020123_PLN_OVRL.DWG
KEY MAP
SEAL
SHEET NUMBER
SHEET TITLE
LANDDESIGN PROJ.#
SCALE
PROJECT
NORTH
NO.DESCRIPTION DATE
REVISION / ISSUANCE
ORIGINAL SHEET SIZE: 24" X 36"
VERT:
HORZ:
CHECKED BY:
DRAWN BY:
DESIGNED BY:
223 NORTH GRAHAM STREET
CHARLOTTE, NC 28202
704.333.0325
WWW.LANDDESIGN.COM
NC ENG. FIRM LICENSE # C-0658
05/31/2022
1 03.21.2022PERMIT SET
2 05.31.2022REVISION 1
0
1"=60'
30'60'120'
N. GRAHAM ST.
(NCDOT MAINTAI
N
E
D
)
CAMP ROAD
KESWICK AVE.(LDUUMUDD-2020-00023)PROP. MUTLI-FAMILY PROP. PARKING GARAGE PROP. ADAPTIVE RE-USE
(MIXED-USE)PROP. ADAPTIVE RE-USE
(MIXED-USE)
PROP. R/W FROM FUTURE
SYLVANIA AVE.
PROP. SUE FROM FUTURE
SYLVANIA AVE.
20' SYLVANIA SETBACK
NORFOLK SOUTHERN SETBACK
0
1"=60'
30'60'120'
PROP. MOVE-IN & TRASH LOADING
AREA (±1,045 SQ. FT)
22.0' MULTI-MODAL LANES
16.0' PEDESTRIAN AMENITY ZONE
8.0' PEDESTRIAN AMENITY ZONE
22.0' MULTI-MODAL LANES
16.0' PEDESTRIAN AMENITY ZONE
20.0' MULTI-MODAL LANES
4.0' PEDESTRIAN AMENITY ZONE
EX. TYPE II MODIFIED
DRIVEWAY TO REMAIN
ON-STREET PARKING SPACES
TO BE CONSTRUCTED PER
CLDSM 50.09CPROP. TRANSFORMER (TYP.)
24.0' TRAVEL LANES
8.0' PARKING LANE
6.0' PEDESTRIAN WALKWAY
8.0' PARKING LANE
6.0' PEDESTRIAN WALKWAY
ACCESSIBLE PARKING & SIGNAGE TO
BE CONSTRUCTED PER CLDSM 50.10A
PROP. 1,393 SQ. FT. OF
COMMERCIAL SPACE
20.0' TRAVEL LANES
24.0' TRAVEL LANES
EX. BUILDING 3A
TO REMAIN
EX. BUILDING 7
TO REMAIN
EX. BUILDING 4, 5A, & 5B
TO REMAIN
EX. CONCRETE LOADING DOCK WITHIN NORFOLK
SOUTHERN RIGHT-OF-WAY TO REMAIN
ON-STREET PARKING SPACES
TO BE CONSTRUCTED PER
CLDSM 50.09D
PROP. TIE-IN TO EXISTING
RAILROAD CROSSING
CONNECTIO
N

DWOO
N
ER
F

4
NORFOLK SOUTHERN RAILROAD
71' RIGHT OF WAY
RAZADES WAY
PROP. ELEVATED INTERSECTION
SEE SHEET C4-02 FOR DETAILS
LEGEND
PROP. ASPHALT
PROP. CONCRETE
20' SETBACK
CAMP ROADPROP. SHORT TERM BIKE
PARKING (8 SPACES)
PROP. SHORT TERM BIKE
PARKING (4 SPACES)
PROP. SHORT TERM BIKE
PARKING (10 SPACES)
PROP. LONG TERM BIKE
PARKING (78 SPACES)
PROP. SHORT TERM BIKE
PARKING (4 SPACES)
PROP. PARKING LOT
WITH 12 SPACES (2 ADA)
PROP. 61 ON-STREET
PARKING SPACES (5 ADA)
PROP. 201 CAMP ROAD TRASH & RECYCLING
TO BE STORED INTERNALLY AND ROLLED OUT
TO BUILDING 12 FOR COLLECTION
PROP. TRANSFORMER (TYP.)
PROP. SHORT TERM BIKE
PARKING (8 SPACES)
EX. BUILDING 12
TO REMAIN
EX. BUILDING 3B TO
REMAIN
(LDUUMUDD-2018-00034)EX. BU
ILD
ING

9TO REMA
IN
EX. BUILDING 1B TO REMAIN
(LDUUMUDD-2018-00018)
EX. BUILDING 1B TO REMAIN
(LDUUMUDD-2018-00018)EX. BUILDING 1A TO REMAIN
(LDUUMUDD-2018-00018)PHASE 1PHASE 2PROP. CAMP NORTH END CIP RAILROAD CROSSING
PENDING NORFOLK SOUTHERN RAILWAY
APPROVAL.REFER TO NEEL SCHAFFER PLANS FOR
PRELIMINARY DESIGN DETAILS.
EX. CAMP ROAD TEMPORARY CROSSING CURRENTLY
IN PLACE ON SITE, AS SHOWN
PROP. CAMP NORTH END CIP RAILROAD CROSSING PENDING
NORFOLK SOUTHERN RAILWAY APPROVAL. REFER TO NEEL
SCHAFFER PLANS FOR PRELIMINARY DESIGN DETAILS.
EXISTING 27.50' TEMPORARY KESWICK CROSSING
CURRENTLY IN PLACE ON SITE, AS SHOWN
PROP. CAMP NORTH END CIP RAILROAD
CROSSING PENDING NORFOLK SOUTHERN
RAILWAY APPROVAL/REFER TO NEEL SCHAFFER
PLANS FOR PRELIMINARY DESIGN DETAILS.
NO TEMPORARY CROSSING TO BE
CONSTRUCTED WITH CIP
8.0' PEDESTRIAN AMENITY ZONE
7.5' AMENITY ZONE
PROP. 10' X 25' LOADING SPACE
KESWICK AVE.(LDUUMUDD-2018-00018)SYLVANIA
AVE
.
(CDOT
MA
INTA
INED

-
SDRU
-2018
-0000
6
)CAMP ROAD(SDRU-2018-00006)STAT
E
S
VI
L
L
E
A
V
E.(NCDO
T
M
A
I
N
T
AI
N
E
D -
S
D
R
U-
2
0
1
8-
0
0
0
0
6
)
FUTURE NORFOLK SOUTHERN
CROSSING PER APPROVED CIP
PROP. ELEVATED INTERSECTION
SEE SHEET C4-03 FOR DETAILS
PROP. SHORT TERM BIKE
PARKING (4 SPACES)
PROP. TRANSFORMER (TYP.)
EX. 6' SIDEWALK
EX. 8' PLANTING STRIP PROP. SHORT TERM BIKE
PARKING (4 SPACES)
PROP. SHORT TERM BIKE
PARKING (4 SPACES)
4' TRANSITION ZONE FOR
MULTI-FAMILY BUILDING
PROP. TRANSFORMER (TYP.)
PROP. ± 33 LF OF RETAINING WALL.
SEE STRUCTURAL PLANS FOR
DETAILS
CONNECTION 6
CONNECTION GPROP. TRANSFORMERS (2)
22.0' MULTI-MODAL LANES
16.0' PEDESTRIAN AMENITY ZONE
16.0' PEDESTRIAN AMENITY ZONE
22.0' MULTI-MODAL LANES
PROPOSED
MULTIFAMILY
PROP. RAISED PLANTER (TYP.)
PROP. SHORT TERM BIKE
PARKING (4 SPACES)
54' PUBLIC
ACCESS EASMENT
SSSSSSSSSSSSSSSSWWWWWWWWW
WWWWWWWWW
GASGASGASGASGASGAS FOFOFOFOFOFOFOFOFOFOFOUGEUGEUGEUGEUGEUGEUGE UGE UGE
PA
PA PA
EX. 701 KESWICK
AVE. TO REMAIN
(LDUUMUDD-2020-00066)
755
756
754
753
752
751
750
749748
749
749
748
748
750
748
749749749750751752751750749749 749
FFE: 752.75
FFE: 749.50
FFE: 749.50
TC:749.26
BC: 748.76
748.60 EG
748.43 EG748.69 FG
752.56 EX. TW
751.30 EX. BW
752.50 EX. TW
748.98 EX. BW
752.50 EX. TW
748.56 EX. BW
748.82 EG
747.88 EX. TC
747.49 EX. BC
747.74 EG
748.95 EG
748.69 EG
748.73 EG
748.93 EG
749.47 EG
749.62 EG750.22 BP749.86 EG
749.52 EG
749.48 EG
748.66 EG
748.17 EG
747.95 EG
PA
PA
PA
PA1.0%1.0%1.0%MATCH EXISTING
TP 748.07
PA
PA
748.07 FG
PA PA PA PA
748.48 FG 748.35 FG
TC:748.70
BC: 748.20
TC:748.77
BC: 748.27 748.62 FG
748.28 FG
748.40 FG
749.48 FG
TC:749.01
BC: 748.51 748.86 FG
748.52 FG
748.64 FG
TC:749.28
BC: 748.78
749.13 FG
748.79 FG
748.91 FG
TC:749.53
BC: 749.03 749.38 FG
TC:749.54
BC: 749.04
749.54 FG
TC:749.68
BC: 749.18
749.53 FG
749.19 FG
749.36 FG
TC:749.61
BC: 749.11
749.45 FG
TC:749.63
BC: 749.13
749.24 FG
TC:749.45
BC: 748.95 749.29 FG
TC:749.44
BC: 748.94
749.14 FG
748.72 FG
749.06 FG
749.01 FG
TC:749.25
BC: 748.75
PROP. DI-01
RIM: 748.15
PROP. DI-05
RIM: 748.52
PROP. DI-03
RIM: 748.09
PROP. DI-06
RIM: 747.73
PROP. CB-08
RIM: 747.92
PROP. DI-04
RIM: 747.78
PROP. DI-07
RIM: 747.52
PROP. SDMH-11
RIM: 752.84
PROP. DI-10
RIM: 748.81
749.48 FG
749.48 FG
749.48 FG
749.48 FG
749.48 FG
749.48 FG
749.36 FG
749.54 FG
749.45 FG
749.48 FG
749.48 FG
749.47 FG
749.50 FG
749.50 FG
749.48 FG
TC:749.10
BC: 748.60
TC:749.28
BC: 748.78
749.27 FG
749.48 FG
749.46 FG
749.46 FG
TC:749.34
BC: 748.84
TC:749.54
BC: 748.94
748.30 FG
748.26 FG 748.31 FG
748.35 FG
748.34 FG
TC:748.73
BC: 748.23
TC:749.50
BC: 749.00 TC:749.17
BC: 748.67
TC:749.05
BC: 748.55
TC:748.93
BC: 748.43 TC:748.81
BC: 748.31 TC:748.72
BC: 748.22
TC:748.56
BC: 748.06 TC:748.44
BC: 747.94
TC:748.32
BC: 747.82
TC:748.32
BC: 747.82
TC:748.07
BC: 747.57
TC:747.97
BC: 747.47
3.13%3.13%
3.13%3.13%
3.13%3.13%
4.75%
1.50%
1.00%
749.34 FG
1.50%
749.30 FG1.09%0.86%1.18%1.12%0.53%749.53 FG 749.45 FG 749.40 FG
749.48 FG
749.35 FG 749.34 FG
749.33 FG
749.32 FG
749.09 FG
749.46 FG749.46 FG749.46 FG
749.48 FG
749.62 FG
749.67 FG749.55 FG
748.99 FG
748.90 FG748.85 FG
749.13 FG749.26 FG
749.18 FG
748.92 FG
748.53 FG
748.52 FG 748.40 FG
748.34 FG 748.40 FG 748.16 FG748.30 FG
TC:748.15
BC: 747.65
748.38 EX. BS1.50%1.50%1.50%0.50%
TC:747.96
BC: 747.46
748.32 FG
748.20 FG
MATCH EX. GRADE3.13%3.13%3.13%3.13%3.13%3.13%752.73 FG 752.73 FG 752.73 FG752.71 FG
752.57 EX. TW
751.30 EX. BW
0.70%
2.18%
0.50%
749.27 BP
TC:749.41
BC: 748.91
TC:748.77
BC: 748.27
748.61 FG 748.90 FG
TC:749.06
BC: 748.56
749.07 FG
TC:749.22
BC: 748.72
748.78 FG
TC:748.93
BC: 748.43
748.65 FG
TC:748.81
BC: 748.31
748.56 FG
TC:748.72
BC: 748.22
0.50%0.50%
748.40 FG
TC:748.56
BC: 748.06
748.29 FG
TC:748.44
BC: 747.94
748.16 FG
TC:748.32
BC: 747.82
748.05 FG
TC:748.21
BC: 747.71
747.92 FG
TC:748.07
BC: 747.57
747.81 FG
TC:747.97
BC: 747.47
747.80 FG
TC:747.96
BC: 747.46
748.50 FG 3:13:13:13:13:13:1
3:1
3:1
749.02 EG
PROP. DI-09
RIM: 748.81
PROP. DI-02
RIM: 748.15
PA
PA
PA
748.29 FG
749.40 TS
748.40 BS
MATCH EX. GRADE
749.32 FG
749.12 BS
752.62 TS
748.84 BS
752.34 TS
749.18 FG
748.96 BS
752.46 TS
EX. 748.69 BS
749.69 FG
749.85 FG
749.92 FG
749.78 FG
749.53 FG
749.25 FG
749.02 FG
1.5% MAX
1.5% MAX
1.5% MAX
CAMP NORTH END
- MULTI-FAMILY
BUILDINGS
ATCO
115 RAZADES WAY
CHARLOTTE NC
1021272
GRADING PLAN
N/A
LDI
LDI
LDI
CB4-00
9/6/2022 9:38 AM CASSIDY FRANKLIN \\CHFILES\PROJECTS\_2021\1021272\CAD\DOCUMENTATION\1021272_PLN_GRAD.DWG
KEY MAP
SEAL
SHEET NUMBER
SHEET TITLE
LANDDESIGN PROJ.#
SCALE
PROJECT
NORTH
NO.DESCRIPTION DATE
REVISION / ISSUANCE
ORIGINAL SHEET SIZE: 24" X 36"
VERT:
HORZ:
CHECKED BY:
DRAWN BY:
DESIGNED BY:
223 NORTH GRAHAM STREET
CHARLOTTE, NC 28202
704.333.0325
WWW.LANDDESIGN.COM
NC ENG. FIRM LICENSE # C-0658
09/06/2022
1 03.21.2022PERMIT SET
2 05.31.2022REVISION 1
3 08.11.2022REVISION 3
4 09.06.2022REVISION 4
RAZADES WAY
EX. BUILDING 3A
TO REMAIN
EX. BUILDING 3A
TO REMAIN
EX. MULTI-FAMILY
TO REMAIN
(LDUUMUDD-2020-00066)
EX. PARKING DECK
TO REMAIN
(LDUUMUDD-2020-00066)
PROPOSED
MULTI-FAMILY
EX. BUILDING 3B
TO REMAIN
CONNECTION 6
CAMP ROAD(LDUUMUDD-2020-00066)GENERAL NOTE:
CONTRACTOR TO DIFFER TO LANDSCAPE DRAWINGS FOR DETAILS
ON TOP 10" OF PLANTER BED AND PLANTED AREA SOIL
PREPARATION.
ALL DROP INLETS WITHIN CONNECTION G & CONNECTION 6 TRAVEL
LANES TO BE TRAFFIC BEARING PER NCDOT STD. DETAIL 840.35
ALL CONCRETE FINISHES AND FINAL MATERIAL TO BE DESIGNATED
ON NBWLA L3.1.10 & L3.1.20
CONTRACTOR TO AERATE SOIL BED PREPARATION PER NBWLA
DRAWINGS WITHIN 7 DAYS OF LANDSCAPER APPLICABLE PLANTER
BED INSTALL
0
1"=
10'20'40'
20'CONNECTION GPROP. INTERNAL GRADE
TRANSITION FROM 752.80' FFE
TO 749.50' FFE
EX. EDGE OF PARKING LOT
PAVEMENT TO REMAIN
PROP. SEAT WALL. SEE NBWLA SHEET
L3.5.19 DETAILS 1& 2 FOR SPECIFICATIONS
CONTRACTOR TO REFER TO NWBLA DRAWING
SPECIFICATIONS FOR ALL GRADING,
MATERIAL, AND SOIL SPECIFICATIONS FOR
PLANTER AREAS AND BEDS
CONTRACTOR TO AERATE SOIL BED
PREPARATION PER NBWLA DRAWINGS WITHIN
7 DAYS OF LANDSCAPER APPLICABLE
PLANTER BED INSTALL

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

12/19/2022
Hart & Hickman (Charlotte) Shannon Switch
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-346-0011 Client Project Description: ATL-006
Dear Shannon Switch:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 12/12/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 74
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/28/202340750State ProgramAlabama
02/07/202388-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
02/18/2023C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2022KY90047State ProgramKentucky
12/31/2022LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2022415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
02/11/202302027State ProgramTennessee
09/30/2022T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/22-346-0011
Page 2 of 74
Report Number:
Sample Summary Table
Client Project Description:
22-346-0011
ATL-006
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
12/12/2022 11:00Solids 95295 CS-1 12/12/2022 12:09
12/12/2022 11:00Solids 95295 CS-1 12/12/2022 12:09 SW-7199 WP MTN -
12/12/2022 10:10Solids 95296 CS-2 12/12/2022 12:09
12/12/2022 10:10Solids 95296 CS-2 12/12/2022 12:09 SW-7199 WP MTN -
12/12/2022 10:45Solids 95297 CS-3 12/12/2022 12:09
12/12/2022 10:45Solids 95297 CS-3 12/12/2022 12:09 SW-7199 WP MTN -
12/12/2022 11:05Solids 95298 CS-4 12/12/2022 12:09
12/12/2022 11:05Solids 95298 CS-4 12/12/2022 12:09 SW-7199 WP MTN -
12/12/2022 10:25Solids 95299 CS-5 12/12/2022 12:09
12/12/2022 10:25Solids 95299 CS-5 12/12/2022 12:09 SW-7199 WP MTN -
12/12/2022Solids 95300 CS-DUP 12/12/2022 12:09
12/12/2022Solids 95300 CS-DUP 12/12/2022 12:09 SW-7199 WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 74
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-346-0011
Report Limit
Project:ATL-006
V 95295CS-1
J1.71 12/15/2022 16:326020BArsenicmg/Kg - dry 0.365
27.9 12/15/2022 16:326020BBariummg/Kg - dry 3.72
39.9 12/15/2022 16:326020BChromiummg/Kg - dry 0.528
9.77 12/15/2022 16:326020BLeadmg/Kg - dry 0.389
J0.0179 12/16/2022 10:237471BMercury (Total)mg/Kg - dry 0.0160
J0.015 12/13/2022 14:528260DAcetonemg/Kg - dry 0.003
J0.003 12/13/2022 14:528260DMethylene Chloride mg/Kg - dry 0.001
J0.261 12/15/2022 17:028270EBenzo(a)anthracene mg/Kg - dry 0.185
J0.236 12/15/2022 17:028270EBenzo(a)pyrene mg/Kg - dry 0.196
J0.326 12/15/2022 17:028270EBenzo(b)fluoranthene mg/Kg - dry 0.194
J0.230 12/15/2022 17:028270EChrysenemg/Kg - dry 0.189
J0.486 12/15/2022 17:028270EFluoranthenemg/Kg - dry 0.164
J0.402 12/15/2022 17:028270EPyrenemg/Kg - dry 0.178
25.0 12/13/2022 18:01SW-DRYWT Moisture %
V 95296CS-2
J1.62 12/15/2022 17:176020BArsenicmg/Kg - dry 0.353
79.0 12/15/2022 17:176020BBariummg/Kg - dry 3.60
65.7 12/15/2022 17:176020BChromiummg/Kg - dry 0.510
7.93 12/15/2022 17:176020BLeadmg/Kg - dry 0.376
J0.0164 12/16/2022 10:267471BMercury (Total)mg/Kg - dry 0.0155
J0.004 12/13/2022 15:198260DAcetonemg/Kg - dry 0.003
J0.005 12/13/2022 15:198260DMethylene Chloride mg/Kg - dry 0.001
0.654 12/19/2022 10:24SW-7199 Chromium, Hexavalent mg/Kg - dry 0.185
22.4 12/13/2022 18:01SW-DRYWT Moisture %
V 95297CS-3
J1.99 12/15/2022 17:236020BArsenicmg/Kg - dry 0.358
39.0 12/15/2022 17:236020BBariummg/Kg - dry 3.65
33.6 12/15/2022 17:236020BChromiummg/Kg - dry 0.517
8.09 12/15/2022 17:236020BLeadmg/Kg - dry 0.382
J0.011 12/13/2022 15:478260DAcetonemg/Kg - dry 0.003
J0.001 12/13/2022 15:478260Dn-Hexane mg/Kg - dry 0.0009
J0.004 12/13/2022 15:478260DMethylene Chloride mg/Kg - dry 0.001
J0.196 12/19/2022 10:35SW-7199 Chromium, Hexavalent mg/Kg - dry 0.188
23.5 12/13/2022 18:01SW-DRYWT Moisture %
Page 4 of 74
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-346-0011
Report Limit
Project:ATL-006
V 95298CS-4
J1.01 12/15/2022 17:296020BArsenicmg/Kg - dry 0.360
82.2 12/15/2022 17:296020BBariummg/Kg - dry 3.66
17.6 12/15/2022 17:296020BChromiummg/Kg - dry 0.519
6.71 12/15/2022 17:296020BLeadmg/Kg - dry 0.383
J0.005 12/13/2022 16:148260DAcetonemg/Kg - dry 0.003
J0.001 12/13/2022 16:148260Dn-Hexane mg/Kg - dry 0.0009
J0.004 12/13/2022 16:148260DMethylene Chloride mg/Kg - dry 0.001
23.8 12/13/2022 18:01SW-DRYWT Moisture %
V 95299CS-5
J2.16 12/15/2022 17:366020BArsenicmg/Kg - dry 0.400
J26.6 12/15/2022 17:366020BBariummg/Kg - dry 4.07
92.4 12/15/2022 17:366020BChromiummg/Kg - dry 0.578
13.6 12/15/2022 17:366020BLeadmg/Kg - dry 0.426
J0.0204 12/16/2022 10:407471BMercury (Total)mg/Kg - dry 0.0175
J0.005 12/13/2022 16:428260DAcetonemg/Kg - dry 0.003
J0.004 12/13/2022 16:428260DMethylene Chloride mg/Kg - dry 0.002
31.5 12/13/2022 18:01SW-DRYWT Moisture %
V 95300CS-DUP
J1.63 12/15/2022 17:426020BArsenicmg/Kg - dry 0.353
64.5 12/15/2022 17:426020BBariummg/Kg - dry 3.59
71.4 12/15/2022 17:426020BChromiummg/Kg - dry 0.509
13.3 12/15/2022 17:426020BLeadmg/Kg - dry 0.376
J0.0175 12/16/2022 10:427471BMercury (Total)mg/Kg - dry 0.0154
J0.003 12/13/2022 17:098260DAcetonemg/Kg - dry 0.003
J0.001 12/13/2022 17:098260Dn-Hexane mg/Kg - dry 0.0008
J0.005 12/13/2022 17:098260DMethylene Chloride mg/Kg - dry 0.001
0.365 12/16/2022 18:47SW-7199 Chromium, Hexavalent mg/Kg - dry 0.185
22.3 12/13/2022 18:01SW-DRYWT Moisture %
Page 5 of 74

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: ATL-006 Lab Report Number: 22-346-0011
Date: 12/19/2022
Metals Analyses Method 6020B Sample 95295 (CS-1) QC Batch No: V27907/V27811
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 95296 (CS-2) QC Batch No: V27907/V27811
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 95297 (CS-3) QC Batch No: V27907/V27811
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 95298 (CS-4) QC Batch No: V27907/V27811
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 95299 (CS-5) QC Batch No: V27907/V27811
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample 95300 (CS-DUP) QC Batch No: V27907/V27811
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 95295 (CS-1) Analyte: Barium
QC Batch No: V27907/V27811 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 95295 (CS-1)
Analyte: Barium QC Batch No: V27907/V27811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 95295 (CS-1) Analyte: Chromium
QC Batch No: V27907/V27811 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Semivolatile Organic Compounds - GC/MS Method 8270E
Page 6 of 74

Analyte: Benzoic Acid
QC Batch No: V27890/V27785 This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low bias.
This target analyte was flagged for recoveries outside QC limits in the associated LCS. Data for this analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for a low
bias.
Analyte: Dibenz(a,h)anthracene QC Batch No: V27890/V27785
LCS is above range. LCSD result is within limits.

Page 7 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-1
95295 Matrix:
12/12/2022 11:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.0 %Moisture 1 12/13/22 18:01 SW-DRYWTAMB
<0.188 mg/Kg - dry 0.188 0.266Chromium, Hexavalent 1 12/19/22 09:41 SW-7199SAR
1.71 J mg/Kg - dry 0.365 2.67Arsenic 20 12/15/22 16:32 6020BEDV
27.9 mg/Kg - dry 3.72 26.7Barium 20 12/15/22 16:32 6020BEDV
<0.176 mg/Kg - dry 0.176 1.33Cadmium 20 12/15/22 16:32 6020BEDV
39.9 mg/Kg - dry 0.528 2.67
Chromium 20 12/15/22 16:32 6020BEDV
9.77 mg/Kg - dry 0.389 2.67Lead 20 12/15/22 16:32 6020BEDV
0.0179 J mg/Kg - dry 0.0160 0.0400Mercury (Total)1 12/16/22 10:23 7471BEDV
<1.97 mg/Kg - dry 1.97 5.33Selenium 20 12/15/22 16:32 6020BEDV
<0.125 mg/Kg - dry 0.125 1.33Silver 20 12/15/22 16:32 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 8 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-1
95295 Matrix:
12/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
0.015 J mg/Kg - dry 0.003 0.026Acetone 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 12/13/22 14:52 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/13/22 14:52 V27717TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 12/13/22 14:52 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 12/13/22 14:52 V27717TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/13/22 14:52 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/13/22 14:52 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/13/22 14:52 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/13/22 14:52 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 12/13/22 14:52 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 9 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-1
95295 Matrix:
12/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 12/13/22 14:52 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/13/22 14:52 V27717TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/13/22 14:52 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/13/22 14:52 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/13/22 14:52 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/13/22 14:52 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/13/22 14:52 V27717TBL
<0.018 mg/Kg - dry 0.018 0.333Ethanol 1 12/13/22 14:52 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.066Ethyl Tertiary Butyl Ether (ETBE)1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 12/13/22 14:52 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 10 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-1
95295 Matrix:
12/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 12/13/22 14:52 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 12/13/22 14:52 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/13/22 14:52 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 12/13/22 14:52 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/13/22 14:52 V27717TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 12/13/22 14:52 V27717TBL
0.003 J mg/Kg - dry 0.001 0.013Methylene Chloride 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/13/22 14:52 V27717TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/13/22 14:52 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 12/13/22 14:52 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/13/22 14:52 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/13/22 14:52 V27717TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 12/13/22 14:52 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 12/13/22 14:52 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 11 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-1
95295 Matrix:
12/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/13/22 14:52 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 12/13/22 14:52 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 12/13/22 14:52 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 12/13/22 14:52 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 12/13/22 14:52 V27717
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%12/13/22 14:521 TBL V27717
Surrogate: Dibromofluoromethane 101 Limits: 84-123%12/13/22 14:521 TBL V27717
Surrogate: Toluene-d8 96.4 Limits: 76-129%12/13/22 14:521 TBL V27717
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.154 mg/Kg - dry 0.154 0.881Acenaphthene 1 12/15/22 17:02 V27890JMV
<0.140 mg/Kg - dry 0.140 0.881Acenaphthylene 1 12/15/22 17:02 V27890JMV
<0.202 mg/Kg - dry 0.202 0.881Aniline 1 12/15/22 17:02 V27890JMV
<0.190 mg/Kg - dry 0.190 0.881Anthracene 1 12/15/22 17:02 V27890JMV
0.261 J
mg/Kg - dry 0.185 0.881
Benzo(a)anthracene 1 12/15/22 17:02 V27890JMV
0.236 J mg/Kg - dry 0.196 0.881Benzo(a)pyrene 1 12/15/22 17:02 V27890JMV
0.326 J mg/Kg - dry 0.194 0.881Benzo(b)fluoranthene 1 12/15/22 17:02 V27890JMV
<0.181 mg/Kg - dry 0.181 0.881Benzo(g,h,i)perylene 1 12/15/22 17:02 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 12 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-1
95295 Matrix:
12/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.182 mg/Kg - dry 0.182 0.881Benzo(k)fluoranthene 1 12/15/22 17:02 V27890JMV
<0.773 M mg/Kg - dry 0.773 2.67Benzoic Acid 1 12/15/22 17:02 V27890JMV
<0.140 mg/Kg - dry 0.140 0.881Benzyl alcohol 1 12/15/22 17:02 V27890JMV
<0.157 mg/Kg - dry 0.157 0.881Bis(2-Chloroethoxy)methane 1 12/15/22 17:02 V27890JMV
<0.142 mg/Kg - dry 0.142 0.881Bis(2-Chloroethyl)ether 1 12/15/22 17:02 V27890JMV
<0.181 mg/Kg - dry 0.181 0.441Bis(2-Chloroisopropyl)ether 1 12/15/22 17:02 V27890JMV
<0.160 mg/Kg - dry 0.160 0.881Bis(2-ethylhexyl)phthalate 1 12/15/22 17:02 V27890JMV
<0.145 mg/Kg - dry 0.145 0.8814-Bromophenyl phenyl ether 1 12/15/22 17:02 V27890JMV
<0.150 mg/Kg - dry 0.150 0.441
Butyl benzyl phthalate 1 12/15/22 17:02 V27890JMV
<0.123 mg/Kg - dry 0.123 0.8814-Chloro-3-methylphenol 1 12/15/22 17:02 V27890JMV
<0.149 mg/Kg - dry 0.149 0.4414-Chloroaniline 1 12/15/22 17:02 V27890JMV
<0.154 mg/Kg - dry 0.154 0.8812-Chloronaphthalene 1 12/15/22 17:02 V27890JMV
<0.131 mg/Kg - dry 0.131 0.8812-Chlorophenol 1 12/15/22 17:02 V27890JMV
<0.168 mg/Kg - dry 0.168 1.334-Chlorophenyl phenyl ether 1 12/15/22 17:02 V27890JMV
0.230 J mg/Kg - dry 0.189 0.881Chrysene 1 12/15/22 17:02 V27890JMV
<0.306 mg/Kg - dry 0.306 0.881
Dibenz(a,h)anthracene 1 12/15/22 17:02 V27890JMV
<0.158 mg/Kg - dry 0.158 0.881Dibenzofuran 1 12/15/22 17:02 V27890JMV
<0.126 mg/Kg - dry 0.126 0.8811,2-Dichlorobenzene 1 12/15/22 17:02 V27890JMV
<0.129 mg/Kg - dry 0.129 0.8811,3-Dichlorobenzene 1 12/15/22 17:02 V27890JMV
<0.130 mg/Kg - dry 0.130 0.4411,4-Dichlorobenzene 1 12/15/22 17:02 V27890JMV
<0.196 mg/Kg - dry 0.196 0.8813,3'-Dichlorobenzidine 1 12/15/22 17:02 V27890JMV
<0.127 mg/Kg - dry 0.127 0.8812,4-Dichlorophenol 1 12/15/22 17:02 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 13 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-1
95295 Matrix:
12/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.240 mg/Kg - dry 0.240 0.881Diethyl phthalate 1 12/15/22 17:02 V27890JMV
<0.232 mg/Kg - dry 0.232 0.881Dimethyl phthalate 1 12/15/22 17:02 V27890JMV
<0.144 mg/Kg - dry 0.144 0.4412,4-Dimethylphenol 1 12/15/22 17:02 V27890JMV
<0.142 mg/Kg - dry 0.142 0.881Di-n-butyl phthalate 1 12/15/22 17:02 V27890JMV
<0.320 mg/Kg - dry 0.320 2.004,6-Dinitro-2-methylphenol 1 12/15/22 17:02 V27890JMV
<0.693 mg/Kg - dry 0.693 2.002,4-Dinitrophenol 1 12/15/22 17:02 V27890JMV
<0.128 mg/Kg - dry 0.128 0.8812,4-Dinitrotoluene 1 12/15/22 17:02 V27890JMV
<0.144 mg/Kg - dry 0.144 0.8812,6-Dinitrotoluene 1 12/15/22 17:02 V27890JMV
<0.190 mg/Kg - dry 0.190 0.441
Di-n-Octyl Phthalate 1 12/15/22 17:02 V27890JMV
0.486 J mg/Kg - dry 0.164 0.881Fluoranthene 1 12/15/22 17:02 V27890JMV
<0.170 mg/Kg - dry 0.170 0.881Fluorene 1 12/15/22 17:02 V27890JMV
<0.141 mg/Kg - dry 0.141 0.881Hexachlorobenzene 1 12/15/22 17:02 V27890JMV
<0.130 mg/Kg - dry 0.130 0.881Hexachlorobutadiene 1 12/15/22 17:02 V27890JMV
<0.209 mg/Kg - dry 0.209 0.881Hexachlorocyclopentadiene 1 12/15/22 17:02 V27890JMV
<0.105 mg/Kg - dry 0.105 0.881Hexachloroethane 1 12/15/22 17:02 V27890JMV
<0.238 mg/Kg - dry 0.238 0.881
Indeno(1,2,3-cd)pyrene 1 12/15/22 17:02 V27890JMV
<0.254 mg/Kg - dry 0.254 0.881Isophorone 1 12/15/22 17:02 V27890JMV
<0.141 mg/Kg - dry 0.141 0.8811-Methylnaphthalene 1 12/15/22 17:02 V27890JMV
<0.133 mg/Kg - dry 0.133 0.8812-Methylnaphthalene 1 12/15/22 17:02 V27890JMV
<0.129 mg/Kg - dry 0.129 0.8812-Methylphenol 1 12/15/22 17:02 V27890JMV
<0.113 mg/Kg - dry 0.113 0.8813&4 Methylphenol 1 12/15/22 17:02 V27890JMV
<0.192 mg/Kg - dry 0.192 0.881Naphthalene 1 12/15/22 17:02 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 14 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-1
95295 Matrix:
12/12/2022 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.129 mg/Kg - dry 0.129 0.8812-Nitroaniline 1 12/15/22 17:02 V27890JMV
<0.160 mg/Kg - dry 0.160 0.8813-Nitroaniline 1 12/15/22 17:02 V27890JMV
<0.124 mg/Kg - dry 0.124 0.4414-Nitroaniline 1 12/15/22 17:02 V27890JMV
<0.154 mg/Kg - dry 0.154 0.441Nitrobenzene 1 12/15/22 17:02 V27890JMV
<0.118 mg/Kg - dry 0.118 0.8812-Nitrophenol 1 12/15/22 17:02 V27890JMV
<0.156 mg/Kg - dry 0.156 0.8814-Nitrophenol 1 12/15/22 17:02 V27890JMV
<0.350 mg/Kg - dry 0.350 0.881N-Nitrosodimethylamine 1 12/15/22 17:02 V27890JMV
<0.241 mg/Kg - dry 0.241 0.881N-Nitrosodiphenylamine 1 12/15/22 17:02 V27890JMV
<0.157 mg/Kg - dry 0.157 0.881
N-Nitroso-di-n-propylamine 1 12/15/22 17:02 V27890JMV
<0.462 mg/Kg - dry 0.462 1.33Pentachlorophenol 1 12/15/22 17:02 V27890JMV
<0.277 mg/Kg - dry 0.277 0.881Phenanthrene 1 12/15/22 17:02 V27890JMV
<0.149 mg/Kg - dry 0.149 0.881Phenol 1 12/15/22 17:02 V27890JMV
0.402 J mg/Kg - dry 0.178 0.881Pyrene 1 12/15/22 17:02 V27890JMV
<0.105 mg/Kg - dry 0.105 0.441Pyridine 1 12/15/22 17:02 V27890JMV
<0.142 mg/Kg - dry 0.142 0.8811,2,4-Trichlorobenzene 1 12/15/22 17:02 V27890JMV
<0.128 mg/Kg - dry 0.128 0.881
2,4,5-Trichlorophenol 1 12/15/22 17:02 V27890JMV
<0.128 mg/Kg - dry 0.128 0.8812,4,6-Trichlorophenol 1 12/15/22 17:02 V27890JMV
8270ESurrogate: Phenol-d5 72.5 Limits: 34-121%12/15/22 17:021 JMV
Surrogate: 2-Fluorobiphenyl 91.6 Limits: 44-115%12/15/22 17:021 JMV V27890
Surrogate: 2-Fluorophenol 76.6 Limits: 35-115%12/15/22 17:021 JMV V27890
Surrogate: Nitrobenzene-d5 80.8 Limits: 37-122%12/15/22 17:021 JMV V27890
Surrogate: 4-Terphenyl-d14 107 Limits: 54-127%12/15/22 17:021 JMV V27890
Surrogate: 2,4,6-Tribromophenol 77.5 Limits: 39-132%12/15/22 17:021 JMV V27890
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 15 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-2
95296 Matrix:
12/12/2022 10:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.4 %Moisture 1 12/13/22 18:01 SW-DRYWTAMB
0.654 mg/Kg - dry 0.185 0.264Chromium, Hexavalent 1 12/19/22 10:24 SW-7199SAR
1.62 J mg/Kg - dry 0.353 2.58Arsenic 20 12/15/22 17:17 6020BEDV
79.0 mg/Kg - dry 3.60 25.8Barium 20 12/15/22 17:17 6020BEDV
<0.170 mg/Kg - dry 0.170 1.29Cadmium 20 12/15/22 17:17 6020BEDV
65.7 mg/Kg - dry 0.510 2.58
Chromium 20 12/15/22 17:17 6020BEDV
7.93 mg/Kg - dry 0.376 2.58Lead 20 12/15/22 17:17 6020BEDV
0.0164 J mg/Kg - dry 0.0155 0.0387Mercury (Total)1 12/16/22 10:26 7471BEDV
<1.91 mg/Kg - dry 1.91 5.15Selenium 20 12/15/22 17:17 6020BEDV
<0.121 mg/Kg - dry 0.121 1.29Silver 20 12/15/22 17:17 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 16 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-2
95296 Matrix:
12/12/2022 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
0.004 J mg/Kg - dry 0.003 0.025Acetone 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 12/13/22 15:19 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 12/13/22 15:19 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/13/22 15:19 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/13/22 15:19 V27717TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/13/22 15:19 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/13/22 15:19 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/13/22 15:19 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/13/22 15:19 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/13/22 15:19 V27717TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/13/22 15:19 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/13/22 15:19 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/13/22 15:19 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/13/22 15:19 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/13/22 15:19 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/13/22 15:19 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 17 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-2
95296 Matrix:
12/12/2022 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 12/13/22 15:19 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 12/13/22 15:19 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/13/22 15:19 V27717TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/13/22 15:19 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/13/22 15:19 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/13/22 15:19 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/13/22 15:19 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/13/22 15:19 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/13/22 15:19 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 12/13/22 15:19 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/13/22 15:19 V27717TBL
<0.018 mg/Kg - dry 0.018 0.322Ethanol 1 12/13/22 15:19 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 12/13/22 15:19 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 18 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-2
95296 Matrix:
12/12/2022 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0009 mg/Kg - dry 0.0009 0.012n-Hexane 1 12/13/22 15:19 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 12/13/22 15:19 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/13/22 15:19 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 12/13/22 15:19 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/13/22 15:19 V27717TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 12/13/22 15:19 V27717TBL
0.005 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/13/22 15:19 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/13/22 15:19 V27717TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/13/22 15:19 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/13/22 15:19 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 12/13/22 15:19 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/13/22 15:19 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/13/22 15:19 V27717TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/13/22 15:19 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/13/22 15:19 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 19 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-2
95296 Matrix:
12/12/2022 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/13/22 15:19 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/13/22 15:19 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/13/22 15:19 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/13/22 15:19 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/13/22 15:19 V27717TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/13/22 15:19 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/13/22 15:19 V27717
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%12/13/22 15:191 TBL V27717
Surrogate: Dibromofluoromethane 98.1 Limits: 84-123%12/13/22 15:191 TBL V27717
Surrogate: Toluene-d8 90.7 Limits: 76-129%12/13/22 15:191 TBL V27717
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.149 mg/Kg - dry 0.149 0.850Acenaphthene 1 12/15/22 11:57 V27890JMV
<0.135 mg/Kg - dry 0.135 0.850Acenaphthylene 1 12/15/22 11:57 V27890JMV
<0.195 mg/Kg - dry 0.195 0.850Aniline 1 12/15/22 11:57 V27890JMV
<0.184 mg/Kg - dry 0.184 0.850Anthracene 1 12/15/22 11:57 V27890JMV
<0.179 mg/Kg - dry 0.179 0.850
Benzo(a)anthracene 1 12/15/22 11:57 V27890JMV
<0.189 mg/Kg - dry 0.189 0.850Benzo(a)pyrene 1 12/15/22 11:57 V27890JMV
<0.188 mg/Kg - dry 0.188 0.850Benzo(b)fluoranthene 1 12/15/22 11:57 V27890JMV
<0.175 mg/Kg - dry 0.175 0.850Benzo(g,h,i)perylene 1 12/15/22 11:57 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 20 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-2
95296 Matrix:
12/12/2022 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.176 mg/Kg - dry 0.176 0.850Benzo(k)fluoranthene 1 12/15/22 11:57 V27890JMV
<0.747 M mg/Kg - dry 0.747 2.58Benzoic Acid 1 12/15/22 11:57 V27890JMV
<0.135 mg/Kg - dry 0.135 0.850Benzyl alcohol 1 12/15/22 11:57 V27890JMV
<0.152 mg/Kg - dry 0.152 0.850Bis(2-Chloroethoxy)methane 1 12/15/22 11:57 V27890JMV
<0.137 mg/Kg - dry 0.137 0.850Bis(2-Chloroethyl)ether 1 12/15/22 11:57 V27890JMV
<0.175 mg/Kg - dry 0.175 0.425Bis(2-Chloroisopropyl)ether 1 12/15/22 11:57 V27890JMV
<0.154 mg/Kg - dry 0.154 0.850Bis(2-ethylhexyl)phthalate 1 12/15/22 11:57 V27890JMV
<0.140 mg/Kg - dry 0.140 0.8504-Bromophenyl phenyl ether 1 12/15/22 11:57 V27890JMV
<0.145 mg/Kg - dry 0.145 0.425
Butyl benzyl phthalate 1 12/15/22 11:57 V27890JMV
<0.119 mg/Kg - dry 0.119 0.8504-Chloro-3-methylphenol 1 12/15/22 11:57 V27890JMV
<0.144 mg/Kg - dry 0.144 0.4254-Chloroaniline 1 12/15/22 11:57 V27890JMV
<0.149 mg/Kg - dry 0.149 0.8502-Chloronaphthalene 1 12/15/22 11:57 V27890JMV
<0.126 mg/Kg - dry 0.126 0.8502-Chlorophenol 1 12/15/22 11:57 V27890JMV
<0.162 mg/Kg - dry 0.162 1.294-Chlorophenyl phenyl ether 1 12/15/22 11:57 V27890JMV
<0.182 mg/Kg - dry 0.182 0.850Chrysene 1 12/15/22 11:57 V27890JMV
<0.296 mg/Kg - dry 0.296 0.850
Dibenz(a,h)anthracene 1 12/15/22 11:57 V27890JMV
<0.153 mg/Kg - dry 0.153 0.850Dibenzofuran 1 12/15/22 11:57 V27890JMV
<0.121 mg/Kg - dry 0.121 0.8501,2-Dichlorobenzene 1 12/15/22 11:57 V27890JMV
<0.125 mg/Kg - dry 0.125 0.8501,3-Dichlorobenzene 1 12/15/22 11:57 V27890JMV
<0.125 mg/Kg - dry 0.125 0.4251,4-Dichlorobenzene 1 12/15/22 11:57 V27890JMV
<0.189 mg/Kg - dry 0.189 0.8503,3'-Dichlorobenzidine 1 12/15/22 11:57 V27890JMV
<0.123 mg/Kg - dry 0.123 0.8502,4-Dichlorophenol 1 12/15/22 11:57 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 21 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-2
95296 Matrix:
12/12/2022 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.231 mg/Kg - dry 0.231 0.850Diethyl phthalate 1 12/15/22 11:57 V27890JMV
<0.224 mg/Kg - dry 0.224 0.850Dimethyl phthalate 1 12/15/22 11:57 V27890JMV
<0.139 mg/Kg - dry 0.139 0.4252,4-Dimethylphenol 1 12/15/22 11:57 V27890JMV
<0.137 mg/Kg - dry 0.137 0.850Di-n-butyl phthalate 1 12/15/22 11:57 V27890JMV
<0.309 mg/Kg - dry 0.309 1.934,6-Dinitro-2-methylphenol 1 12/15/22 11:57 V27890JMV
<0.670 mg/Kg - dry 0.670 1.932,4-Dinitrophenol 1 12/15/22 11:57 V27890JMV
<0.124 mg/Kg - dry 0.124 0.8502,4-Dinitrotoluene 1 12/15/22 11:57 V27890JMV
<0.139 mg/Kg - dry 0.139 0.8502,6-Dinitrotoluene 1 12/15/22 11:57 V27890JMV
<0.184 mg/Kg - dry 0.184 0.425
Di-n-Octyl Phthalate 1 12/15/22 11:57 V27890JMV
<0.158 mg/Kg - dry 0.158 0.850Fluoranthene 1 12/15/22 11:57 V27890JMV
<0.164 mg/Kg - dry 0.164 0.850Fluorene 1 12/15/22 11:57 V27890JMV
<0.136 mg/Kg - dry 0.136 0.850Hexachlorobenzene 1 12/15/22 11:57 V27890JMV
<0.125 mg/Kg - dry 0.125 0.850Hexachlorobutadiene 1 12/15/22 11:57 V27890JMV
<0.202 mg/Kg - dry 0.202 0.850Hexachlorocyclopentadiene 1 12/15/22 11:57 V27890JMV
<0.102 mg/Kg - dry 0.102 0.850Hexachloroethane 1 12/15/22 11:57 V27890JMV
<0.230 mg/Kg - dry 0.230 0.850
Indeno(1,2,3-cd)pyrene 1 12/15/22 11:57 V27890JMV
<0.246 mg/Kg - dry 0.246 0.850Isophorone 1 12/15/22 11:57 V27890JMV
<0.136 mg/Kg - dry 0.136 0.8501-Methylnaphthalene 1 12/15/22 11:57 V27890JMV
<0.128 mg/Kg - dry 0.128 0.8502-Methylnaphthalene 1 12/15/22 11:57 V27890JMV
<0.125 mg/Kg - dry 0.125 0.8502-Methylphenol 1 12/15/22 11:57 V27890JMV
<0.109 mg/Kg - dry 0.109 0.8503&4 Methylphenol 1 12/15/22 11:57 V27890JMV
<0.185 mg/Kg - dry 0.185 0.850Naphthalene 1 12/15/22 11:57 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 22 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-2
95296 Matrix:
12/12/2022 10:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.124 mg/Kg - dry 0.124 0.8502-Nitroaniline 1 12/15/22 11:57 V27890JMV
<0.154 mg/Kg - dry 0.154 0.8503-Nitroaniline 1 12/15/22 11:57 V27890JMV
<0.120 mg/Kg - dry 0.120 0.4254-Nitroaniline 1 12/15/22 11:57 V27890JMV
<0.149 mg/Kg - dry 0.149 0.425Nitrobenzene 1 12/15/22 11:57 V27890JMV
<0.114 mg/Kg - dry 0.114 0.8502-Nitrophenol 1 12/15/22 11:57 V27890JMV
<0.150 mg/Kg - dry 0.150 0.8504-Nitrophenol 1 12/15/22 11:57 V27890JMV
<0.338 mg/Kg - dry 0.338 0.850N-Nitrosodimethylamine 1 12/15/22 11:57 V27890JMV
<0.233 mg/Kg - dry 0.233 0.850N-Nitrosodiphenylamine 1 12/15/22 11:57 V27890JMV
<0.152 mg/Kg - dry 0.152 0.850
N-Nitroso-di-n-propylamine 1 12/15/22 11:57 V27890JMV
<0.447 mg/Kg - dry 0.447 1.29Pentachlorophenol 1 12/15/22 11:57 V27890JMV
<0.268 mg/Kg - dry 0.268 0.850Phenanthrene 1 12/15/22 11:57 V27890JMV
<0.144 mg/Kg - dry 0.144 0.850Phenol 1 12/15/22 11:57 V27890JMV
<0.172 mg/Kg - dry 0.172 0.850Pyrene 1 12/15/22 11:57 V27890JMV
<0.102 mg/Kg - dry 0.102 0.425Pyridine 1 12/15/22 11:57 V27890JMV
<0.137 mg/Kg - dry 0.137 0.8501,2,4-Trichlorobenzene 1 12/15/22 11:57 V27890JMV
<0.123 mg/Kg - dry 0.123 0.850
2,4,5-Trichlorophenol 1 12/15/22 11:57 V27890JMV
<0.124 mg/Kg - dry 0.124 0.8502,4,6-Trichlorophenol 1 12/15/22 11:57 V27890JMV
8270ESurrogate: Phenol-d5 71.2 Limits: 34-121%12/15/22 11:571 JMV
Surrogate: 2-Fluorobiphenyl 94.0 Limits: 44-115%12/15/22 11:571 JMV V27890
Surrogate: 2-Fluorophenol 75.4 Limits: 35-115%12/15/22 11:571 JMV V27890
Surrogate: Nitrobenzene-d5 80.8 Limits: 37-122%12/15/22 11:571 JMV V27890
Surrogate: 4-Terphenyl-d14 105 Limits: 54-127%12/15/22 11:571 JMV V27890
Surrogate: 2,4,6-Tribromophenol 85.6 Limits: 39-132%12/15/22 11:571 JMV V27890
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 23 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-3
95297 Matrix:
12/12/2022 10:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.5 %Moisture 1 12/13/22 18:01 SW-DRYWTAMB
0.196 J mg/Kg - dry 0.188 0.267Chromium, Hexavalent 1 12/19/22 10:35 SW-7199SAR
1.99 J mg/Kg - dry 0.358 2.61Arsenic 20 12/15/22 17:23 6020BEDV
39.0 mg/Kg - dry 3.65 26.1Barium 20 12/15/22 17:23 6020BEDV
<0.173 mg/Kg - dry 0.173 1.31Cadmium 20 12/15/22 17:23 6020BEDV
33.6 mg/Kg - dry 0.517 2.61
Chromium 20 12/15/22 17:23 6020BEDV
8.09 mg/Kg - dry 0.382 2.61Lead 20 12/15/22 17:23 6020BEDV
<0.0157 mg/Kg - dry 0.0157 0.0392Mercury (Total)1 12/16/22 10:29 7471BEDV
<1.93 mg/Kg - dry 1.93 5.23Selenium 20 12/15/22 17:23 6020BEDV
<0.123 mg/Kg - dry 0.123 1.31Silver 20 12/15/22 17:23 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 24 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-3
95297 Matrix:
12/12/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
0.011 J mg/Kg - dry 0.003 0.026Acetone 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 12/13/22 15:47 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 12/13/22 15:47 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/13/22 15:47 V27717TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 12/13/22 15:47 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 12/13/22 15:47 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/13/22 15:47 V27717TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/13/22 15:47 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/13/22 15:47 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/13/22 15:47 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/13/22 15:47 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 12/13/22 15:47 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 25 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-3
95297 Matrix:
12/12/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 12/13/22 15:47 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/13/22 15:47 V27717TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/13/22 15:47 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/13/22 15:47 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/13/22 15:47 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/13/22 15:47 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/13/22 15:47 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/13/22 15:47 V27717TBL
<0.018 mg/Kg - dry 0.018 0.326Ethanol 1 12/13/22 15:47 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 12/13/22 15:47 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 26 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-3
95297 Matrix:
12/12/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
0.001 J mg/Kg - dry 0.0009 0.013n-Hexane 1 12/13/22 15:47 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 12/13/22 15:47 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/13/22 15:47 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.026Methyl Ethyl Ketone (MEK)1 12/13/22 15:47 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/13/22 15:47 V27717TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 12/13/22 15:47 V27717TBL
0.004 J mg/Kg - dry 0.001 0.013Methylene Chloride 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/13/22 15:47 V27717TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/13/22 15:47 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 12/13/22 15:47 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/13/22 15:47 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/13/22 15:47 V27717TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 12/13/22 15:47 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/13/22 15:47 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 27 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-3
95297 Matrix:
12/12/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/13/22 15:47 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 12/13/22 15:47 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 12/13/22 15:47 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 12/13/22 15:47 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 12/13/22 15:47 V27717
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 70-130%12/13/22 15:471 TBL V27717
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/13/22 15:471 TBL V27717
Surrogate: Toluene-d8 93.9 Limits: 76-129%12/13/22 15:471 TBL V27717
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.151 mg/Kg - dry 0.151 0.864Acenaphthene 1 12/15/22 12:19 V27890JMV
<0.137 mg/Kg - dry 0.137 0.864Acenaphthylene 1 12/15/22 12:19 V27890JMV
<0.198 mg/Kg - dry 0.198 0.864Aniline 1 12/15/22 12:19 V27890JMV
<0.186 mg/Kg - dry 0.186 0.864Anthracene 1 12/15/22 12:19 V27890JMV
<0.181 mg/Kg - dry 0.181 0.864
Benzo(a)anthracene 1 12/15/22 12:19 V27890JMV
<0.192 mg/Kg - dry 0.192 0.864Benzo(a)pyrene 1 12/15/22 12:19 V27890JMV
<0.190 mg/Kg - dry 0.190 0.864Benzo(b)fluoranthene 1 12/15/22 12:19 V27890JMV
<0.177 mg/Kg - dry 0.177 0.864Benzo(g,h,i)perylene 1 12/15/22 12:19 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 28 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-3
95297 Matrix:
12/12/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.179 mg/Kg - dry 0.179 0.864Benzo(k)fluoranthene 1 12/15/22 12:19 V27890JMV
<0.758 M mg/Kg - dry 0.758 2.61Benzoic Acid 1 12/15/22 12:19 V27890JMV
<0.137 mg/Kg - dry 0.137 0.864Benzyl alcohol 1 12/15/22 12:19 V27890JMV
<0.154 mg/Kg - dry 0.154 0.864Bis(2-Chloroethoxy)methane 1 12/15/22 12:19 V27890JMV
<0.139 mg/Kg - dry 0.139 0.864Bis(2-Chloroethyl)ether 1 12/15/22 12:19 V27890JMV
<0.177 mg/Kg - dry 0.177 0.431Bis(2-Chloroisopropyl)ether 1 12/15/22 12:19 V27890JMV
<0.156 mg/Kg - dry 0.156 0.864Bis(2-ethylhexyl)phthalate 1 12/15/22 12:19 V27890JMV
<0.142 mg/Kg - dry 0.142 0.8644-Bromophenyl phenyl ether 1 12/15/22 12:19 V27890JMV
<0.147 mg/Kg - dry 0.147 0.431
Butyl benzyl phthalate 1 12/15/22 12:19 V27890JMV
<0.120 mg/Kg - dry 0.120 0.8644-Chloro-3-methylphenol 1 12/15/22 12:19 V27890JMV
<0.146 mg/Kg - dry 0.146 0.4314-Chloroaniline 1 12/15/22 12:19 V27890JMV
<0.151 mg/Kg - dry 0.151 0.8642-Chloronaphthalene 1 12/15/22 12:19 V27890JMV
<0.128 mg/Kg - dry 0.128 0.8642-Chlorophenol 1 12/15/22 12:19 V27890JMV
<0.164 mg/Kg - dry 0.164 1.314-Chlorophenyl phenyl ether 1 12/15/22 12:19 V27890JMV
<0.185 mg/Kg - dry 0.185 0.864Chrysene 1 12/15/22 12:19 V27890JMV
<0.300 mg/Kg - dry 0.300 0.864
Dibenz(a,h)anthracene 1 12/15/22 12:19 V27890JMV
<0.155 mg/Kg - dry 0.155 0.864Dibenzofuran 1 12/15/22 12:19 V27890JMV
<0.123 mg/Kg - dry 0.123 0.8641,2-Dichlorobenzene 1 12/15/22 12:19 V27890JMV
<0.127 mg/Kg - dry 0.127 0.8641,3-Dichlorobenzene 1 12/15/22 12:19 V27890JMV
<0.127 mg/Kg - dry 0.127 0.4311,4-Dichlorobenzene 1 12/15/22 12:19 V27890JMV
<0.192 mg/Kg - dry 0.192 0.8643,3'-Dichlorobenzidine 1 12/15/22 12:19 V27890JMV
<0.125 mg/Kg - dry 0.125 0.8642,4-Dichlorophenol 1 12/15/22 12:19 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 29 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-3
95297 Matrix:
12/12/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.235 mg/Kg - dry 0.235 0.864Diethyl phthalate 1 12/15/22 12:19 V27890JMV
<0.227 mg/Kg - dry 0.227 0.864Dimethyl phthalate 1 12/15/22 12:19 V27890JMV
<0.141 mg/Kg - dry 0.141 0.4312,4-Dimethylphenol 1 12/15/22 12:19 V27890JMV
<0.139 mg/Kg - dry 0.139 0.864Di-n-butyl phthalate 1 12/15/22 12:19 V27890JMV
<0.313 mg/Kg - dry 0.313 1.964,6-Dinitro-2-methylphenol 1 12/15/22 12:19 V27890JMV
<0.679 mg/Kg - dry 0.679 1.962,4-Dinitrophenol 1 12/15/22 12:19 V27890JMV
<0.126 mg/Kg - dry 0.126 0.8642,4-Dinitrotoluene 1 12/15/22 12:19 V27890JMV
<0.141 mg/Kg - dry 0.141 0.8642,6-Dinitrotoluene 1 12/15/22 12:19 V27890JMV
<0.186 mg/Kg - dry 0.186 0.431
Di-n-Octyl Phthalate 1 12/15/22 12:19 V27890JMV
<0.160 mg/Kg - dry 0.160 0.864Fluoranthene 1 12/15/22 12:19 V27890JMV
<0.167 mg/Kg - dry 0.167 0.864Fluorene 1 12/15/22 12:19 V27890JMV
<0.138 mg/Kg - dry 0.138 0.864Hexachlorobenzene 1 12/15/22 12:19 V27890JMV
<0.127 mg/Kg - dry 0.127 0.864Hexachlorobutadiene 1 12/15/22 12:19 V27890JMV
<0.205 mg/Kg - dry 0.205 0.864Hexachlorocyclopentadiene 1 12/15/22 12:19 V27890JMV
<0.103 mg/Kg - dry 0.103 0.864Hexachloroethane 1 12/15/22 12:19 V27890JMV
<0.233 mg/Kg - dry 0.233 0.864
Indeno(1,2,3-cd)pyrene 1 12/15/22 12:19 V27890JMV
<0.249 mg/Kg - dry 0.249 0.864Isophorone 1 12/15/22 12:19 V27890JMV
<0.138 mg/Kg - dry 0.138 0.8641-Methylnaphthalene 1 12/15/22 12:19 V27890JMV
<0.130 mg/Kg - dry 0.130 0.8642-Methylnaphthalene 1 12/15/22 12:19 V27890JMV
<0.126 mg/Kg - dry 0.126 0.8642-Methylphenol 1 12/15/22 12:19 V27890JMV
<0.111 mg/Kg - dry 0.111 0.8643&4 Methylphenol 1 12/15/22 12:19 V27890JMV
<0.188 mg/Kg - dry 0.188 0.864Naphthalene 1 12/15/22 12:19 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 30 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-3
95297 Matrix:
12/12/2022 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.126 mg/Kg - dry 0.126 0.8642-Nitroaniline 1 12/15/22 12:19 V27890JMV
<0.156 mg/Kg - dry 0.156 0.8643-Nitroaniline 1 12/15/22 12:19 V27890JMV
<0.121 mg/Kg - dry 0.121 0.4314-Nitroaniline 1 12/15/22 12:19 V27890JMV
<0.151 mg/Kg - dry 0.151 0.431Nitrobenzene 1 12/15/22 12:19 V27890JMV
<0.116 mg/Kg - dry 0.116 0.8642-Nitrophenol 1 12/15/22 12:19 V27890JMV
<0.152 mg/Kg - dry 0.152 0.8644-Nitrophenol 1 12/15/22 12:19 V27890JMV
<0.343 mg/Kg - dry 0.343 0.864N-Nitrosodimethylamine 1 12/15/22 12:19 V27890JMV
<0.236 mg/Kg - dry 0.236 0.864N-Nitrosodiphenylamine 1 12/15/22 12:19 V27890JMV
<0.154 mg/Kg - dry 0.154 0.864
N-Nitroso-di-n-propylamine 1 12/15/22 12:19 V27890JMV
<0.453 mg/Kg - dry 0.453 1.31Pentachlorophenol 1 12/15/22 12:19 V27890JMV
<0.271 mg/Kg - dry 0.271 0.864Phenanthrene 1 12/15/22 12:19 V27890JMV
<0.146 mg/Kg - dry 0.146 0.864Phenol 1 12/15/22 12:19 V27890JMV
<0.175 mg/Kg - dry 0.175 0.864Pyrene 1 12/15/22 12:19 V27890JMV
<0.103 mg/Kg - dry 0.103 0.431Pyridine 1 12/15/22 12:19 V27890JMV
<0.139 mg/Kg - dry 0.139 0.8641,2,4-Trichlorobenzene 1 12/15/22 12:19 V27890JMV
<0.125 mg/Kg - dry 0.125 0.864
2,4,5-Trichlorophenol 1 12/15/22 12:19 V27890JMV
<0.126 mg/Kg - dry 0.126 0.8642,4,6-Trichlorophenol 1 12/15/22 12:19 V27890JMV
8270ESurrogate: Phenol-d5 73.1 Limits: 34-121%12/15/22 12:191 JMV
Surrogate: 2-Fluorobiphenyl 91.6 Limits: 44-115%12/15/22 12:191 JMV V27890
Surrogate: 2-Fluorophenol 74.6 Limits: 35-115%12/15/22 12:191 JMV V27890
Surrogate: Nitrobenzene-d5 80.2 Limits: 37-122%12/15/22 12:191 JMV V27890
Surrogate: 4-Terphenyl-d14 106 Limits: 54-127%12/15/22 12:191 JMV V27890
Surrogate: 2,4,6-Tribromophenol 78.1 Limits: 39-132%12/15/22 12:191 JMV V27890
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 31 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-4
95298 Matrix:
12/12/2022 11:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
23.8 %Moisture 1 12/13/22 18:01 SW-DRYWTAMB
<0.187 mg/Kg - dry 0.187 0.266Chromium, Hexavalent 1 12/19/22 10:46 SW-7199SAR
1.01 J mg/Kg - dry 0.360 2.62Arsenic 20 12/15/22 17:29 6020BEDV
82.2 mg/Kg - dry 3.66 26.2Barium 20 12/15/22 17:29 6020BEDV
<0.173 mg/Kg - dry 0.173 1.31Cadmium 20 12/15/22 17:29 6020BEDV
17.6 mg/Kg - dry 0.519 2.62
Chromium 20 12/15/22 17:29 6020BEDV
6.71 mg/Kg - dry 0.383 2.62Lead 20 12/15/22 17:29 6020BEDV
<0.0157 mg/Kg - dry 0.0157 0.0394Mercury (Total)1 12/16/22 10:37 7471BEDV
<1.94 mg/Kg - dry 1.94 5.25Selenium 20 12/15/22 17:29 6020BEDV
<0.123 mg/Kg - dry 0.123 1.31Silver 20 12/15/22 17:29 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 32 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-4
95298 Matrix:
12/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
0.005 J mg/Kg - dry 0.003 0.026Acetone 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 12/13/22 16:14 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 12/13/22 16:14 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/13/22 16:14 V27717TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 12/13/22 16:14 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 12/13/22 16:14 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/13/22 16:14 V27717TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/13/22 16:14 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/13/22 16:14 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/13/22 16:14 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/13/22 16:14 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 12/13/22 16:14 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 33 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-4
95298 Matrix:
12/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 12/13/22 16:14 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/13/22 16:14 V27717TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/13/22 16:14 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/13/22 16:14 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/13/22 16:14 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/13/22 16:14 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/13/22 16:14 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/13/22 16:14 V27717TBL
<0.018 mg/Kg - dry 0.018 0.328Ethanol 1 12/13/22 16:14 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 12/13/22 16:14 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 34 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-4
95298 Matrix:
12/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
0.001 J mg/Kg - dry 0.0009 0.013n-Hexane 1 12/13/22 16:14 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 12/13/22 16:14 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/13/22 16:14 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 12/13/22 16:14 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/13/22 16:14 V27717TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 12/13/22 16:14 V27717TBL
0.004 J mg/Kg - dry 0.001 0.013Methylene Chloride 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/13/22 16:14 V27717TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/13/22 16:14 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 12/13/22 16:14 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/13/22 16:14 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/13/22 16:14 V27717TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 12/13/22 16:14 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/13/22 16:14 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 35 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-4
95298 Matrix:
12/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/13/22 16:14 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 12/13/22 16:14 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 12/13/22 16:14 V27717TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 12/13/22 16:14 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 12/13/22 16:14 V27717
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%12/13/22 16:141 TBL V27717
Surrogate: Dibromofluoromethane 103 Limits: 84-123%12/13/22 16:141 TBL V27717
Surrogate: Toluene-d8 95.0 Limits: 76-129%12/13/22 16:141 TBL V27717
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.152 mg/Kg - dry 0.152 0.867Acenaphthene 1 12/15/22 12:42 V27890JMV
<0.137 mg/Kg - dry 0.137 0.867Acenaphthylene 1 12/15/22 12:42 V27890JMV
<0.199 mg/Kg - dry 0.199 0.867Aniline 1 12/15/22 12:42 V27890JMV
<0.187 mg/Kg - dry 0.187 0.867Anthracene 1 12/15/22 12:42 V27890JMV
<0.182 mg/Kg - dry 0.182 0.867
Benzo(a)anthracene 1 12/15/22 12:42 V27890JMV
<0.192 mg/Kg - dry 0.192 0.867Benzo(a)pyrene 1 12/15/22 12:42 V27890JMV
<0.191 mg/Kg - dry 0.191 0.867Benzo(b)fluoranthene 1 12/15/22 12:42 V27890JMV
<0.178 mg/Kg - dry 0.178 0.867Benzo(g,h,i)perylene 1 12/15/22 12:42 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 36 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-4
95298 Matrix:
12/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.179 mg/Kg - dry 0.179 0.867Benzo(k)fluoranthene 1 12/15/22 12:42 V27890JMV
<0.761 M mg/Kg - dry 0.761 2.62Benzoic Acid 1 12/15/22 12:42 V27890JMV
<0.137 mg/Kg - dry 0.137 0.867Benzyl alcohol 1 12/15/22 12:42 V27890JMV
<0.154 mg/Kg - dry 0.154 0.867Bis(2-Chloroethoxy)methane 1 12/15/22 12:42 V27890JMV
<0.140 mg/Kg - dry 0.140 0.867Bis(2-Chloroethyl)ether 1 12/15/22 12:42 V27890JMV
<0.178 mg/Kg - dry 0.178 0.434Bis(2-Chloroisopropyl)ether 1 12/15/22 12:42 V27890JMV
<0.157 mg/Kg - dry 0.157 0.867Bis(2-ethylhexyl)phthalate 1 12/15/22 12:42 V27890JMV
<0.143 mg/Kg - dry 0.143 0.8674-Bromophenyl phenyl ether 1 12/15/22 12:42 V27890JMV
<0.148 mg/Kg - dry 0.148 0.434
Butyl benzyl phthalate 1 12/15/22 12:42 V27890JMV
<0.121 mg/Kg - dry 0.121 0.8674-Chloro-3-methylphenol 1 12/15/22 12:42 V27890JMV
<0.146 mg/Kg - dry 0.146 0.4344-Chloroaniline 1 12/15/22 12:42 V27890JMV
<0.152 mg/Kg - dry 0.152 0.8672-Chloronaphthalene 1 12/15/22 12:42 V27890JMV
<0.129 mg/Kg - dry 0.129 0.8672-Chlorophenol 1 12/15/22 12:42 V27890JMV
<0.165 mg/Kg - dry 0.165 1.314-Chlorophenyl phenyl ether 1 12/15/22 12:42 V27890JMV
<0.186 mg/Kg - dry 0.186 0.867Chrysene 1 12/15/22 12:42 V27890JMV
<0.301 mg/Kg - dry 0.301 0.867
Dibenz(a,h)anthracene 1 12/15/22 12:42 V27890JMV
<0.156 mg/Kg - dry 0.156 0.867Dibenzofuran 1 12/15/22 12:42 V27890JMV
<0.124 mg/Kg - dry 0.124 0.8671,2-Dichlorobenzene 1 12/15/22 12:42 V27890JMV
<0.127 mg/Kg - dry 0.127 0.8671,3-Dichlorobenzene 1 12/15/22 12:42 V27890JMV
<0.128 mg/Kg - dry 0.128 0.4341,4-Dichlorobenzene 1 12/15/22 12:42 V27890JMV
<0.192 mg/Kg - dry 0.192 0.8673,3'-Dichlorobenzidine 1 12/15/22 12:42 V27890JMV
<0.125 mg/Kg - dry 0.125 0.8672,4-Dichlorophenol 1 12/15/22 12:42 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 37 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-4
95298 Matrix:
12/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.236 mg/Kg - dry 0.236 0.867Diethyl phthalate 1 12/15/22 12:42 V27890JMV
<0.228 mg/Kg - dry 0.228 0.867Dimethyl phthalate 1 12/15/22 12:42 V27890JMV
<0.141 mg/Kg - dry 0.141 0.4342,4-Dimethylphenol 1 12/15/22 12:42 V27890JMV
<0.140 mg/Kg - dry 0.140 0.867Di-n-butyl phthalate 1 12/15/22 12:42 V27890JMV
<0.314 mg/Kg - dry 0.314 1.974,6-Dinitro-2-methylphenol 1 12/15/22 12:42 V27890JMV
<0.682 mg/Kg - dry 0.682 1.972,4-Dinitrophenol 1 12/15/22 12:42 V27890JMV
<0.126 mg/Kg - dry 0.126 0.8672,4-Dinitrotoluene 1 12/15/22 12:42 V27890JMV
<0.141 mg/Kg - dry 0.141 0.8672,6-Dinitrotoluene 1 12/15/22 12:42 V27890JMV
<0.187 mg/Kg - dry 0.187 0.434
Di-n-Octyl Phthalate 1 12/15/22 12:42 V27890JMV
<0.161 mg/Kg - dry 0.161 0.867Fluoranthene 1 12/15/22 12:42 V27890JMV
<0.167 mg/Kg - dry 0.167 0.867Fluorene 1 12/15/22 12:42 V27890JMV
<0.139 mg/Kg - dry 0.139 0.867Hexachlorobenzene 1 12/15/22 12:42 V27890JMV
<0.128 mg/Kg - dry 0.128 0.867Hexachlorobutadiene 1 12/15/22 12:42 V27890JMV
<0.206 mg/Kg - dry 0.206 0.867Hexachlorocyclopentadiene 1 12/15/22 12:42 V27890JMV
<0.104 mg/Kg - dry 0.104 0.867Hexachloroethane 1 12/15/22 12:42 V27890JMV
<0.234 mg/Kg - dry 0.234 0.867
Indeno(1,2,3-cd)pyrene 1 12/15/22 12:42 V27890JMV
<0.250 mg/Kg - dry 0.250 0.867Isophorone 1 12/15/22 12:42 V27890JMV
<0.139 mg/Kg - dry 0.139 0.8671-Methylnaphthalene 1 12/15/22 12:42 V27890JMV
<0.131 mg/Kg - dry 0.131 0.8672-Methylnaphthalene 1 12/15/22 12:42 V27890JMV
<0.127 mg/Kg - dry 0.127 0.8672-Methylphenol 1 12/15/22 12:42 V27890JMV
<0.111 mg/Kg - dry 0.111 0.8673&4 Methylphenol 1 12/15/22 12:42 V27890JMV
<0.188 mg/Kg - dry 0.188 0.867Naphthalene 1 12/15/22 12:42 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 38 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-4
95298 Matrix:
12/12/2022 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.127 mg/Kg - dry 0.127 0.8672-Nitroaniline 1 12/15/22 12:42 V27890JMV
<0.157 mg/Kg - dry 0.157 0.8673-Nitroaniline 1 12/15/22 12:42 V27890JMV
<0.122 mg/Kg - dry 0.122 0.4344-Nitroaniline 1 12/15/22 12:42 V27890JMV
<0.152 mg/Kg - dry 0.152 0.434Nitrobenzene 1 12/15/22 12:42 V27890JMV
<0.116 mg/Kg - dry 0.116 0.8672-Nitrophenol 1 12/15/22 12:42 V27890JMV
<0.153 mg/Kg - dry 0.153 0.8674-Nitrophenol 1 12/15/22 12:42 V27890JMV
<0.345 mg/Kg - dry 0.345 0.867N-Nitrosodimethylamine 1 12/15/22 12:42 V27890JMV
<0.237 mg/Kg - dry 0.237 0.867N-Nitrosodiphenylamine 1 12/15/22 12:42 V27890JMV
<0.154 mg/Kg - dry 0.154 0.867
N-Nitroso-di-n-propylamine 1 12/15/22 12:42 V27890JMV
<0.455 mg/Kg - dry 0.455 1.31Pentachlorophenol 1 12/15/22 12:42 V27890JMV
<0.272 mg/Kg - dry 0.272 0.867Phenanthrene 1 12/15/22 12:42 V27890JMV
<0.146 mg/Kg - dry 0.146 0.867Phenol 1 12/15/22 12:42 V27890JMV
<0.175 mg/Kg - dry 0.175 0.867Pyrene 1 12/15/22 12:42 V27890JMV
<0.104 mg/Kg - dry 0.104 0.434Pyridine 1 12/15/22 12:42 V27890JMV
<0.140 mg/Kg - dry 0.140 0.8671,2,4-Trichlorobenzene 1 12/15/22 12:42 V27890JMV
<0.126 mg/Kg - dry 0.126 0.867
2,4,5-Trichlorophenol 1 12/15/22 12:42 V27890JMV
<0.126 mg/Kg - dry 0.126 0.8672,4,6-Trichlorophenol 1 12/15/22 12:42 V27890JMV
8270ESurrogate: Phenol-d5 65.0 Limits: 34-121%12/15/22 12:421 JMV
Surrogate: 2-Fluorobiphenyl 89.8 Limits: 44-115%12/15/22 12:421 JMV V27890
Surrogate: 2-Fluorophenol 69.2 Limits: 35-115%12/15/22 12:421 JMV V27890
Surrogate: Nitrobenzene-d5 74.3 Limits: 37-122%12/15/22 12:421 JMV V27890
Surrogate: 4-Terphenyl-d14 92.8 Limits: 54-127%12/15/22 12:421 JMV V27890
Surrogate: 2,4,6-Tribromophenol 74.6 Limits: 39-132%12/15/22 12:421 JMV V27890
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 39 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-5
95299 Matrix:
12/12/2022 10:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
31.5 %Moisture 1 12/13/22 18:01 SW-DRYWTAMB
<0.205 mg/Kg - dry 0.205 0.291Chromium, Hexavalent 1 12/19/22 10:57 SW-7199SAR
2.16 J mg/Kg - dry 0.400 2.92Arsenic 20 12/15/22 17:36 6020BEDV
26.6 J mg/Kg - dry 4.07 29.2Barium 20 12/15/22 17:36 6020BEDV
<0.193 mg/Kg - dry 0.193 1.46Cadmium 20 12/15/22 17:36 6020BEDV
92.4 mg/Kg - dry 0.578 2.92
Chromium 20 12/15/22 17:36 6020BEDV
13.6 mg/Kg - dry 0.426 2.92Lead 20 12/15/22 17:36 6020BEDV
0.0204 J mg/Kg - dry 0.0175 0.0438Mercury (Total)1 12/16/22 10:40 7471BEDV
<2.16 mg/Kg - dry 2.16 5.84Selenium 20 12/15/22 17:36 6020BEDV
<0.137 mg/Kg - dry 0.137 1.46Silver 20 12/15/22 17:36 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 40 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-5
95299 Matrix:
12/12/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
0.005 J mg/Kg - dry 0.003 0.029Acetone 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.029Acrolein 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.029Acrylonitrile 1 12/13/22 16:42 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.007Benzene 1 12/13/22 16:42 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.007Bromobenzene 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007Bromochloromethane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007Bromodichloromethane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007Bromoform 1 12/13/22 16:42 V27717TBL
<0.002 mg/Kg - dry 0.002 0.014
Bromomethane 1 12/13/22 16:42 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.007n-Butylbenzene 1 12/13/22 16:42 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.007sec-Butyl benzene 1 12/13/22 16:42 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.007tert-Butyl benzene 1 12/13/22 16:42 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.007Carbon Disulfide 1 12/13/22 16:42 V27717TBL
<0.002 mg/Kg - dry 0.002 0.007Carbon Tetrachloride 1 12/13/22 16:42 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.007Chlorobenzene 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007
Chlorodibromomethane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.014Chloroethane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007Chloroform 1 12/13/22 16:42 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.014Chloromethane 1 12/13/22 16:42 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0072-Chlorotoluene 1 12/13/22 16:42 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0074-Chlorotoluene 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007Di-Isopropyl Ether (DIPE)1 12/13/22 16:42 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 41 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-5
95299 Matrix:
12/12/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0141,2-Dibromo-3-Chloropropane 1 12/13/22 16:42 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,2-Dibromoethane 1 12/13/22 16:42 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.007Dibromomethane 1 12/13/22 16:42 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,2-Dichlorobenzene 1 12/13/22 16:42 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,3-Dichlorobenzene 1 12/13/22 16:42 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0071,4-Dichlorobenzene 1 12/13/22 16:42 V27717TBL
<0.002 mg/Kg - dry 0.002 0.014Dichlorodifluoromethane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethane 1 12/13/22 16:42 V27717TBL
<0.002 mg/Kg - dry 0.002 0.007
1,2-Dichloroethane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0071,1-Dichloroethene 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007cis-1,2-Dichloroethene 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,2-Dichloroethene 1 12/13/22 16:42 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0071,2-Dichloropropane 1 12/13/22 16:42 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3-Dichloropropane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0072,2-Dichloropropane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007
1,1-Dichloropropene 1 12/13/22 16:42 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.007cis-1,3-Dichloropropene 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007trans-1,3-Dichloropropene 1 12/13/22 16:42 V27717TBL
<0.020 mg/Kg - dry 0.020 0.364Ethanol 1 12/13/22 16:42 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.007Ethylbenzene 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.072Ethyl Tertiary Butyl Ether (ETBE)1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.014Hexachlorobutadiene 1 12/13/22 16:42 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 42 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-5
95299 Matrix:
12/12/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0010 mg/Kg - dry 0.0010 0.014n-Hexane 1 12/13/22 16:42 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0292-Hexanone 1 12/13/22 16:42 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.007Isopropylbenzene 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0074-Isopropyl toluene 1 12/13/22 16:42 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.029Methyl Ethyl Ketone (MEK)1 12/13/22 16:42 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.007Methyl tert-butyl ether (MTBE)1 12/13/22 16:42 V27717TBL
<0.021 mg/Kg - dry 0.021 0.0294-Methyl-2-Pentanone 1 12/13/22 16:42 V27717TBL
0.004 J mg/Kg - dry 0.002 0.014Methylene Chloride 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.014
Naphthalene 1 12/13/22 16:42 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.007n-Propylbenzene 1 12/13/22 16:42 V27717TBL
<0.002 mg/Kg - dry 0.002 0.007Styrene 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0071,1,1,2-Tetrachloroethane 1 12/13/22 16:42 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0071,1,2,2-Tetrachloroethane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007Tetrachloroethene 1 12/13/22 16:42 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.007Toluene 1 12/13/22 16:42 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.014
1,2,3-Trichlorobenzene 1 12/13/22 16:42 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0141,2,4-Trichlorobenzene 1 12/13/22 16:42 V27717TBL
<0.002 mg/Kg - dry 0.002 0.0071,1,1-Trichloroethane 1 12/13/22 16:42 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0071,1,2-Trichloroethane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.007Trichloroethene 1 12/13/22 16:42 V27717TBL
<0.003 mg/Kg - dry 0.003 0.014Trichlorofluoromethane 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0071,2,3-Trichloropropane 1 12/13/22 16:42 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 43 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-5
95299 Matrix:
12/12/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.0071,2,4-Trimethylbenzene 1 12/13/22 16:42 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0071,3,5-Trimethylbenzene 1 12/13/22 16:42 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Acetate 1 12/13/22 16:42 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.014Vinyl Chloride 1 12/13/22 16:42 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.007o-Xylene 1 12/13/22 16:42 V27717TBL
<0.001 mg/Kg - dry 0.001 0.014m,p-Xylene 1 12/13/22 16:42 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.007Xylene (Total)1 12/13/22 16:42 V27717
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%12/13/22 16:421 TBL V27717
Surrogate: Dibromofluoromethane 101 Limits: 84-123%12/13/22 16:421 TBL V27717
Surrogate: Toluene-d8 94.2 Limits: 76-129%12/13/22 16:421 TBL V27717
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.169 mg/Kg - dry 0.169 0.964Acenaphthene 1 12/15/22 13:04 V27890JMV
<0.153 mg/Kg - dry 0.153 0.964Acenaphthylene 1 12/15/22 13:04 V27890JMV
<0.221 mg/Kg - dry 0.221 0.964Aniline 1 12/15/22 13:04 V27890JMV
<0.208 mg/Kg - dry 0.208 0.964Anthracene 1 12/15/22 13:04 V27890JMV
<0.202 mg/Kg - dry 0.202 0.964
Benzo(a)anthracene 1 12/15/22 13:04 V27890JMV
<0.214 mg/Kg - dry 0.214 0.964Benzo(a)pyrene 1 12/15/22 13:04 V27890JMV
<0.213 mg/Kg - dry 0.213 0.964Benzo(b)fluoranthene 1 12/15/22 13:04 V27890JMV
<0.198 mg/Kg - dry 0.198 0.964Benzo(g,h,i)perylene 1 12/15/22 13:04 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 44 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-5
95299 Matrix:
12/12/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.200 mg/Kg - dry 0.200 0.964Benzo(k)fluoranthene 1 12/15/22 13:04 V27890JMV
<0.846 M mg/Kg - dry 0.846 2.92Benzoic Acid 1 12/15/22 13:04 V27890JMV
<0.153 mg/Kg - dry 0.153 0.964Benzyl alcohol 1 12/15/22 13:04 V27890JMV
<0.172 mg/Kg - dry 0.172 0.964Bis(2-Chloroethoxy)methane 1 12/15/22 13:04 V27890JMV
<0.156 mg/Kg - dry 0.156 0.964Bis(2-Chloroethyl)ether 1 12/15/22 13:04 V27890JMV
<0.198 mg/Kg - dry 0.198 0.481Bis(2-Chloroisopropyl)ether 1 12/15/22 13:04 V27890JMV
<0.175 mg/Kg - dry 0.175 0.964Bis(2-ethylhexyl)phthalate 1 12/15/22 13:04 V27890JMV
<0.159 mg/Kg - dry 0.159 0.9644-Bromophenyl phenyl ether 1 12/15/22 13:04 V27890JMV
<0.164 mg/Kg - dry 0.164 0.481
Butyl benzyl phthalate 1 12/15/22 13:04 V27890JMV
<0.135 mg/Kg - dry 0.135 0.9644-Chloro-3-methylphenol 1 12/15/22 13:04 V27890JMV
<0.163 mg/Kg - dry 0.163 0.4814-Chloroaniline 1 12/15/22 13:04 V27890JMV
<0.169 mg/Kg - dry 0.169 0.9642-Chloronaphthalene 1 12/15/22 13:04 V27890JMV
<0.143 mg/Kg - dry 0.143 0.9642-Chlorophenol 1 12/15/22 13:04 V27890JMV
<0.183 mg/Kg - dry 0.183 1.464-Chlorophenyl phenyl ether 1 12/15/22 13:04 V27890JMV
<0.207 mg/Kg - dry 0.207 0.964Chrysene 1 12/15/22 13:04 V27890JMV
<0.335 mg/Kg - dry 0.335 0.964
Dibenz(a,h)anthracene 1 12/15/22 13:04 V27890JMV
<0.173 mg/Kg - dry 0.173 0.964Dibenzofuran 1 12/15/22 13:04 V27890JMV
<0.137 mg/Kg - dry 0.137 0.9641,2-Dichlorobenzene 1 12/15/22 13:04 V27890JMV
<0.142 mg/Kg - dry 0.142 0.9641,3-Dichlorobenzene 1 12/15/22 13:04 V27890JMV
<0.142 mg/Kg - dry 0.142 0.4811,4-Dichlorobenzene 1 12/15/22 13:04 V27890JMV
<0.214 mg/Kg - dry 0.214 0.9643,3'-Dichlorobenzidine 1 12/15/22 13:04 V27890JMV
<0.140 mg/Kg - dry 0.140 0.9642,4-Dichlorophenol 1 12/15/22 13:04 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 45 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-5
95299 Matrix:
12/12/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.262 mg/Kg - dry 0.262 0.964Diethyl phthalate 1 12/15/22 13:04 V27890JMV
<0.254 mg/Kg - dry 0.254 0.964Dimethyl phthalate 1 12/15/22 13:04 V27890JMV
<0.157 mg/Kg - dry 0.157 0.4812,4-Dimethylphenol 1 12/15/22 13:04 V27890JMV
<0.156 mg/Kg - dry 0.156 0.964Di-n-butyl phthalate 1 12/15/22 13:04 V27890JMV
<0.350 mg/Kg - dry 0.350 2.194,6-Dinitro-2-methylphenol 1 12/15/22 13:04 V27890JMV
<0.759 mg/Kg - dry 0.759 2.192,4-Dinitrophenol 1 12/15/22 13:04 V27890JMV
<0.141 mg/Kg - dry 0.141 0.9642,4-Dinitrotoluene 1 12/15/22 13:04 V27890JMV
<0.157 mg/Kg - dry 0.157 0.9642,6-Dinitrotoluene 1 12/15/22 13:04 V27890JMV
<0.208 mg/Kg - dry 0.208 0.481
Di-n-Octyl Phthalate 1 12/15/22 13:04 V27890JMV
<0.179 mg/Kg - dry 0.179 0.964Fluoranthene 1 12/15/22 13:04 V27890JMV
<0.186 mg/Kg - dry 0.186 0.964Fluorene 1 12/15/22 13:04 V27890JMV
<0.154 mg/Kg - dry 0.154 0.964Hexachlorobenzene 1 12/15/22 13:04 V27890JMV
<0.142 mg/Kg - dry 0.142 0.964Hexachlorobutadiene 1 12/15/22 13:04 V27890JMV
<0.229 mg/Kg - dry 0.229 0.964Hexachlorocyclopentadiene 1 12/15/22 13:04 V27890JMV
<0.115 mg/Kg - dry 0.115 0.964Hexachloroethane 1 12/15/22 13:04 V27890JMV
<0.261 mg/Kg - dry 0.261 0.964
Indeno(1,2,3-cd)pyrene 1 12/15/22 13:04 V27890JMV
<0.278 mg/Kg - dry 0.278 0.964Isophorone 1 12/15/22 13:04 V27890JMV
<0.154 mg/Kg - dry 0.154 0.9641-Methylnaphthalene 1 12/15/22 13:04 V27890JMV
<0.145 mg/Kg - dry 0.145 0.9642-Methylnaphthalene 1 12/15/22 13:04 V27890JMV
<0.141 mg/Kg - dry 0.141 0.9642-Methylphenol 1 12/15/22 13:04 V27890JMV
<0.124 mg/Kg - dry 0.124 0.9643&4 Methylphenol 1 12/15/22 13:04 V27890JMV
<0.210 mg/Kg - dry 0.210 0.964Naphthalene 1 12/15/22 13:04 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 46 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-5
95299 Matrix:
12/12/2022 10:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.141 mg/Kg - dry 0.141 0.9642-Nitroaniline 1 12/15/22 13:04 V27890JMV
<0.175 mg/Kg - dry 0.175 0.9643-Nitroaniline 1 12/15/22 13:04 V27890JMV
<0.136 mg/Kg - dry 0.136 0.4814-Nitroaniline 1 12/15/22 13:04 V27890JMV
<0.169 mg/Kg - dry 0.169 0.481Nitrobenzene 1 12/15/22 13:04 V27890JMV
<0.129 mg/Kg - dry 0.129 0.9642-Nitrophenol 1 12/15/22 13:04 V27890JMV
<0.170 mg/Kg - dry 0.170 0.9644-Nitrophenol 1 12/15/22 13:04 V27890JMV
<0.383 mg/Kg - dry 0.383 0.964N-Nitrosodimethylamine 1 12/15/22 13:04 V27890JMV
<0.264 mg/Kg - dry 0.264 0.964N-Nitrosodiphenylamine 1 12/15/22 13:04 V27890JMV
<0.172 mg/Kg - dry 0.172 0.964
N-Nitroso-di-n-propylamine 1 12/15/22 13:04 V27890JMV
<0.506 mg/Kg - dry 0.506 1.46Pentachlorophenol 1 12/15/22 13:04 V27890JMV
<0.303 mg/Kg - dry 0.303 0.964Phenanthrene 1 12/15/22 13:04 V27890JMV
<0.163 mg/Kg - dry 0.163 0.964Phenol 1 12/15/22 13:04 V27890JMV
<0.195 mg/Kg - dry 0.195 0.964Pyrene 1 12/15/22 13:04 V27890JMV
<0.115 mg/Kg - dry 0.115 0.481Pyridine 1 12/15/22 13:04 V27890JMV
<0.156 mg/Kg - dry 0.156 0.9641,2,4-Trichlorobenzene 1 12/15/22 13:04 V27890JMV
<0.140 mg/Kg - dry 0.140 0.964
2,4,5-Trichlorophenol 1 12/15/22 13:04 V27890JMV
<0.141 mg/Kg - dry 0.141 0.9642,4,6-Trichlorophenol 1 12/15/22 13:04 V27890JMV
8270ESurrogate: Phenol-d5 66.5 Limits: 34-121%12/15/22 13:041 JMV
Surrogate: 2-Fluorobiphenyl 89.2 Limits: 44-115%12/15/22 13:041 JMV V27890
Surrogate: 2-Fluorophenol 73.4 Limits: 35-115%12/15/22 13:041 JMV V27890
Surrogate: Nitrobenzene-d5 77.8 Limits: 37-122%12/15/22 13:041 JMV V27890
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%12/15/22 13:041 JMV V27890
Surrogate: 2,4,6-Tribromophenol 75.7 Limits: 39-132%12/15/22 13:041 JMV V27890
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 47 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-DUP
95300 Matrix:
12/12/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.3 %Moisture 1 12/13/22 18:01 SW-DRYWTAMB
0.365 mg/Kg - dry 0.185 0.263Chromium, Hexavalent 1 12/16/22 18:47 SW-7199SAR
1.63 J mg/Kg - dry 0.353 2.57Arsenic 20 12/15/22 17:42 6020BEDV
64.5 mg/Kg - dry 3.59 25.7Barium 20 12/15/22 17:42 6020BEDV
<0.170 mg/Kg - dry 0.170 1.29Cadmium 20 12/15/22 17:42 6020BEDV
71.4 mg/Kg - dry 0.509 2.57
Chromium 20 12/15/22 17:42 6020BEDV
13.3 mg/Kg - dry 0.376 2.57Lead 20 12/15/22 17:42 6020BEDV
0.0175 J mg/Kg - dry 0.0154 0.0386Mercury (Total)1 12/16/22 10:42 7471BEDV
<1.90 mg/Kg - dry 1.90 5.15Selenium 20 12/15/22 17:42 6020BEDV
<0.121 mg/Kg - dry 0.121 1.29Silver 20 12/15/22 17:42 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 48 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-DUP
95300 Matrix:
12/12/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
0.003 J mg/Kg - dry 0.003 0.025Acetone 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 12/13/22 17:09 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 12/13/22 17:09 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 12/13/22 17:09 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 12/13/22 17:09 V27717TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 12/13/22 17:09 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 12/13/22 17:09 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 12/13/22 17:09 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 12/13/22 17:09 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 12/13/22 17:09 V27717TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 12/13/22 17:09 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 12/13/22 17:09 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 12/13/22 17:09 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 12/13/22 17:09 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 12/13/22 17:09 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 12/13/22 17:09 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 49 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-DUP
95300 Matrix:
12/12/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 12/13/22 17:09 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 12/13/22 17:09 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 12/13/22 17:09 V27717TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 12/13/22 17:09 V27717TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 12/13/22 17:09 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 12/13/22 17:09 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 12/13/22 17:09 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 12/13/22 17:09 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 12/13/22 17:09 V27717TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 12/13/22 17:09 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 12/13/22 17:09 V27717TBL
<0.018 mg/Kg - dry 0.018 0.321Ethanol 1 12/13/22 17:09 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 12/13/22 17:09 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 50 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-DUP
95300 Matrix:
12/12/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 12/13/22 17:09 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 12/13/22 17:09 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 12/13/22 17:09 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 12/13/22 17:09 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 12/13/22 17:09 V27717TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 12/13/22 17:09 V27717TBL
0.005 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 12/13/22 17:09 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 12/13/22 17:09 V27717TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 12/13/22 17:09 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 12/13/22 17:09 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 12/13/22 17:09 V27717TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 12/13/22 17:09 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 12/13/22 17:09 V27717TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 12/13/22 17:09 V27717TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 12/13/22 17:09 V27717TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 51 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-DUP
95300 Matrix:
12/12/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V27716 12/13/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 12/13/22 17:09 V27717TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 12/13/22 17:09 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 12/13/22 17:09 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 12/13/22 17:09 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 12/13/22 17:09 V27717TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 12/13/22 17:09 V27717TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 12/13/22 17:09 V27717
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 70-130%12/13/22 17:091 TBL V27717
Surrogate: Dibromofluoromethane 97.7 Limits: 84-123%12/13/22 17:091 TBL V27717
Surrogate: Toluene-d8 93.7 Limits: 76-129%12/13/22 17:091 TBL V27717
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.149 mg/Kg - dry 0.149 0.849Acenaphthene 1 12/15/22 13:27 V27890JMV
<0.135 mg/Kg - dry 0.135 0.849Acenaphthylene 1 12/15/22 13:27 V27890JMV
<0.195 mg/Kg - dry 0.195 0.849Aniline 1 12/15/22 13:27 V27890JMV
<0.184 mg/Kg - dry 0.184 0.849Anthracene 1 12/15/22 13:27 V27890JMV
<0.178 mg/Kg - dry 0.178 0.849
Benzo(a)anthracene 1 12/15/22 13:27 V27890JMV
<0.189 mg/Kg - dry 0.189 0.849Benzo(a)pyrene 1 12/15/22 13:27 V27890JMV
<0.187 mg/Kg - dry 0.187 0.849Benzo(b)fluoranthene 1 12/15/22 13:27 V27890JMV
<0.175 mg/Kg - dry 0.175 0.849Benzo(g,h,i)perylene 1 12/15/22 13:27 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 52 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-DUP
95300 Matrix:
12/12/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.176 mg/Kg - dry 0.176 0.849Benzo(k)fluoranthene 1 12/15/22 13:27 V27890JMV
<0.746 M mg/Kg - dry 0.746 2.57Benzoic Acid 1 12/15/22 13:27 V27890JMV
<0.135 mg/Kg - dry 0.135 0.849Benzyl alcohol 1 12/15/22 13:27 V27890JMV
<0.151 mg/Kg - dry 0.151 0.849Bis(2-Chloroethoxy)methane 1 12/15/22 13:27 V27890JMV
<0.137 mg/Kg - dry 0.137 0.849Bis(2-Chloroethyl)ether 1 12/15/22 13:27 V27890JMV
<0.175 mg/Kg - dry 0.175 0.424Bis(2-Chloroisopropyl)ether 1 12/15/22 13:27 V27890JMV
<0.154 mg/Kg - dry 0.154 0.849Bis(2-ethylhexyl)phthalate 1 12/15/22 13:27 V27890JMV
<0.140 mg/Kg - dry 0.140 0.8494-Bromophenyl phenyl ether 1 12/15/22 13:27 V27890JMV
<0.145 mg/Kg - dry 0.145 0.424
Butyl benzyl phthalate 1 12/15/22 13:27 V27890JMV
<0.118 mg/Kg - dry 0.118 0.8494-Chloro-3-methylphenol 1 12/15/22 13:27 V27890JMV
<0.144 mg/Kg - dry 0.144 0.4244-Chloroaniline 1 12/15/22 13:27 V27890JMV
<0.149 mg/Kg - dry 0.149 0.8492-Chloronaphthalene 1 12/15/22 13:27 V27890JMV
<0.126 mg/Kg - dry 0.126 0.8492-Chlorophenol 1 12/15/22 13:27 V27890JMV
<0.162 mg/Kg - dry 0.162 1.294-Chlorophenyl phenyl ether 1 12/15/22 13:27 V27890JMV
<0.182 mg/Kg - dry 0.182 0.849Chrysene 1 12/15/22 13:27 V27890JMV
<0.296 mg/Kg - dry 0.296 0.849
Dibenz(a,h)anthracene 1 12/15/22 13:27 V27890JMV
<0.153 mg/Kg - dry 0.153 0.849Dibenzofuran 1 12/15/22 13:27 V27890JMV
<0.121 mg/Kg - dry 0.121 0.8491,2-Dichlorobenzene 1 12/15/22 13:27 V27890JMV
<0.125 mg/Kg - dry 0.125 0.8491,3-Dichlorobenzene 1 12/15/22 13:27 V27890JMV
<0.125 mg/Kg - dry 0.125 0.4241,4-Dichlorobenzene 1 12/15/22 13:27 V27890JMV
<0.189 mg/Kg - dry 0.189 0.8493,3'-Dichlorobenzidine 1 12/15/22 13:27 V27890JMV
<0.123 mg/Kg - dry 0.123 0.8492,4-Dichlorophenol 1 12/15/22 13:27 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 53 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-DUP
95300 Matrix:
12/12/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.231 mg/Kg - dry 0.231 0.849Diethyl phthalate 1 12/15/22 13:27 V27890JMV
<0.223 mg/Kg - dry 0.223 0.849Dimethyl phthalate 1 12/15/22 13:27 V27890JMV
<0.138 mg/Kg - dry 0.138 0.4242,4-Dimethylphenol 1 12/15/22 13:27 V27890JMV
<0.137 mg/Kg - dry 0.137 0.849Di-n-butyl phthalate 1 12/15/22 13:27 V27890JMV
<0.308 mg/Kg - dry 0.308 1.934,6-Dinitro-2-methylphenol 1 12/15/22 13:27 V27890JMV
<0.669 mg/Kg - dry 0.669 1.932,4-Dinitrophenol 1 12/15/22 13:27 V27890JMV
<0.124 mg/Kg - dry 0.124 0.8492,4-Dinitrotoluene 1 12/15/22 13:27 V27890JMV
<0.138 mg/Kg - dry 0.138 0.8492,6-Dinitrotoluene 1 12/15/22 13:27 V27890JMV
<0.184 mg/Kg - dry 0.184 0.424
Di-n-Octyl Phthalate 1 12/15/22 13:27 V27890JMV
<0.158 mg/Kg - dry 0.158 0.849Fluoranthene 1 12/15/22 13:27 V27890JMV
<0.164 mg/Kg - dry 0.164 0.849Fluorene 1 12/15/22 13:27 V27890JMV
<0.136 mg/Kg - dry 0.136 0.849Hexachlorobenzene 1 12/15/22 13:27 V27890JMV
<0.125 mg/Kg - dry 0.125 0.849Hexachlorobutadiene 1 12/15/22 13:27 V27890JMV
<0.202 mg/Kg - dry 0.202 0.849Hexachlorocyclopentadiene 1 12/15/22 13:27 V27890JMV
<0.101 mg/Kg - dry 0.101 0.849Hexachloroethane 1 12/15/22 13:27 V27890JMV
<0.230 mg/Kg - dry 0.230 0.849
Indeno(1,2,3-cd)pyrene 1 12/15/22 13:27 V27890JMV
<0.245 mg/Kg - dry 0.245 0.849Isophorone 1 12/15/22 13:27 V27890JMV
<0.136 mg/Kg - dry 0.136 0.8491-Methylnaphthalene 1 12/15/22 13:27 V27890JMV
<0.128 mg/Kg - dry 0.128 0.8492-Methylnaphthalene 1 12/15/22 13:27 V27890JMV
<0.124 mg/Kg - dry 0.124 0.8492-Methylphenol 1 12/15/22 13:27 V27890JMV
<0.109 mg/Kg - dry 0.109 0.8493&4 Methylphenol 1 12/15/22 13:27 V27890JMV
<0.185 mg/Kg - dry 0.185 0.849Naphthalene 1 12/15/22 13:27 V27890JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLMinimum valueM
Page 54 of 74
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-346-0011
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Shannon Switch
Charlotte
Received : 12/12/2022
ATL-006
Report Date : 12/19/2022
Sample ID :
Lab No :
Sampled:CS-DUP
95300 Matrix:
12/12/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V27785 12/14/22 10:40
<0.124 mg/Kg - dry 0.124 0.8492-Nitroaniline 1 12/15/22 13:27 V27890JMV
<0.154 mg/Kg - dry 0.154 0.8493-Nitroaniline 1 12/15/22 13:27 V27890JMV
<0.120 mg/Kg - dry 0.120 0.4244-Nitroaniline 1 12/15/22 13:27 V27890JMV
<0.149 mg/Kg - dry 0.149 0.424Nitrobenzene 1 12/15/22 13:27 V27890JMV
<0.114 mg/Kg - dry 0.114 0.8492-Nitrophenol 1 12/15/22 13:27 V27890JMV
<0.150 mg/Kg - dry 0.150 0.8494-Nitrophenol 1 12/15/22 13:27 V27890JMV
<0.338 mg/Kg - dry 0.338 0.849N-Nitrosodimethylamine 1 12/15/22 13:27 V27890JMV
<0.232 mg/Kg - dry 0.232 0.849N-Nitrosodiphenylamine 1 12/15/22 13:27 V27890JMV
<0.151 mg/Kg - dry 0.151 0.849
N-Nitroso-di-n-propylamine 1 12/15/22 13:27 V27890JMV
<0.446 mg/Kg - dry 0.446 1.29Pentachlorophenol 1 12/15/22 13:27 V27890JMV
<0.267 mg/Kg - dry 0.267 0.849Phenanthrene 1 12/15/22 13:27 V27890JMV
<0.144 mg/Kg - dry 0.144 0.849Phenol 1 12/15/22 13:27 V27890JMV
<0.172 mg/Kg - dry 0.172 0.849Pyrene 1 12/15/22 13:27 V27890JMV
<0.101 mg/Kg - dry 0.101 0.424Pyridine 1 12/15/22 13:27 V27890JMV
<0.137 mg/Kg - dry 0.137 0.8491,2,4-Trichlorobenzene 1 12/15/22 13:27 V27890JMV
<0.123 mg/Kg - dry 0.123 0.849
2,4,5-Trichlorophenol 1 12/15/22 13:27 V27890JMV
<0.124 mg/Kg - dry 0.124 0.8492,4,6-Trichlorophenol 1 12/15/22 13:27 V27890JMV
8270ESurrogate: Phenol-d5 73.7 Limits: 34-121%12/15/22 13:271 JMV
Surrogate: 2-Fluorobiphenyl 104 Limits: 44-115%12/15/22 13:271 JMV V27890
Surrogate: 2-Fluorophenol 79.9 Limits: 35-115%12/15/22 13:271 JMV V27890
Surrogate: Nitrobenzene-d5 89.2 Limits: 37-122%12/15/22 13:271 JMV V27890
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%12/15/22 13:271 JMV V27890
Surrogate: 2,4,6-Tribromophenol 85.9 Limits: 39-132%12/15/22 13:271 JMV V27890
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 55 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Metals Analyses
6020B
V27907QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V27811
Associated Lab Samples: 95295, 95296, 95297, 95298, 95299, 95300
LRB-V27811 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/15/22 16:192.000.274<0.274mg/KgArsenic
12/15/22 16:1920.02.79<2.79mg/KgBarium
12/15/22 16:191.000.132<0.132mg/KgCadmium
12/15/22 16:192.000.396<0.396mg/KgChromium
12/15/22 16:192.000.292<0.292mg/KgLead
12/15/22 16:194.001.48<1.48mg/KgSelenium
12/15/22 16:191.000.0940<0.0940mg/KgSilver
LCS-V27811Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
97.012.112.5mg/KgArsenic 80-120
98.012.212.5mg/KgBarium 80-120
98.012.212.5mg/KgCadmium 80-120
97.012.112.5mg/KgChromium 80-120
10012.512.5mg/KgLead 80-120
10212.812.5mg/KgSelenium 80-120
93.04.645.00mg/KgSilver 80-120
V 95295-MS-V27811 V 95295-MSD-V27811Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
11.8 84.011.712.512.51.28mg/KgArsenic 83.0 75-125 0.8 20
49.6 230*72.012.512.520.9mg/KgBarium 409*75-125 36.8*20
12.0 96.012.412.512.5<0.132mg/KgCadmium 99.0 75-125 3.2 20
41.3 91.036.912.512.529.9mg/KgChromium 56.0*75-125 11.2 20
Page 1 of 17* QC Fail Date:12/19/2022 03:33 PM
Page 56 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Metals Analyses
6020B
V27907QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V27811
V 95295-MS-V27811 V 95295-MSD-V27811Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
18.8 92.020.812.512.57.33mg/KgLead 108 75-125 10.1 20
11.9 95.013.112.512.5<1.48mg/KgSelenium 105 75-125 9.6 20
4.56 91.04.645.005.00<0.0940mg/KgSilver 93.0 75-125 1.7 20
V 95295-PDS-V27811Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/15/22 16:5195.024.5mg/KgArsenic
12/15/22 16:5110637.7mg/KgBarium
12/15/22 16:5197.024.1mg/KgCadmium
12/15/22 16:5196.038.4mg/KgChromium
12/15/22 16:5196.027.4mg/KgLead
12/15/22 16:5195.023.6mg/KgSelenium
12/15/22 16:5197.024.2mg/KgSilver
Page 2 of 17Date:12/19/2022 03:33 PM
Page 57 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V27927QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V27863
Associated Lab Samples: 95295, 95296, 95297, 95298, 95299, 95300
LRB-V27863 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/16/22 10:030.03000.0120<0.0120mg/KgMercury (Total)
LCS-V27863Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1010.4190.417mg/KgMercury (Total)80-120
V 95665-MS-V27863 V 95665-MSD-V27863Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.425 1020.4280.4170.417<0.0120mg/KgMercury (Total)103 80-120 0.7 20
V 95665-PDS-V27863Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
12/16/22 10:1889.00.186mg/KgMercury (Total)
Page 3 of 17Date:12/19/2022 03:33 PM
Page 58 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27716
Associated Lab Samples: 95295, 95296, 95297, 95298, 95299, 95300
LRB-V27716 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/13/22 14:240.0200.002<0.002mg/KgAcetone
12/13/22 14:240.0200.001<0.001mg/KgAcrolein
12/13/22 14:240.0200.0008<0.0008mg/KgAcrylonitrile
12/13/22 14:240.0050.0006<0.0006mg/KgBenzene
12/13/22 14:240.0050.0005<0.0005mg/KgBromobenzene
12/13/22 14:240.0050.0008<0.0008mg/KgBromochloromethane
12/13/22 14:240.0050.001<0.001mg/KgBromodichloromethane
12/13/22 14:240.0050.001<0.001mg/KgBromoform
12/13/22 14:240.0100.001<0.001mg/KgBromomethane
12/13/22 14:240.0050.0005<0.0005mg/Kgn-Butylbenzene
12/13/22 14:240.0050.0006<0.0006mg/Kgsec-Butyl benzene
12/13/22 14:240.0050.0005<0.0005mg/Kgtert-Butyl benzene
12/13/22 14:240.0050.0006<0.0006mg/KgCarbon Disulfide
12/13/22 14:240.0050.001<0.001mg/KgCarbon Tetrachloride
12/13/22 14:240.0050.0007<0.0007mg/KgChlorobenzene
12/13/22 14:240.0050.0009<0.0009mg/KgChlorodibromomethane
12/13/22 14:240.0100.0009<0.0009mg/KgChloroethane
12/13/22 14:240.0050.001<0.001mg/KgChloroform
12/13/22 14:240.0100.0006<0.0006mg/KgChloromethane
12/13/22 14:240.0050.0005<0.0005mg/Kg2-Chlorotoluene
12/13/22 14:240.0050.0004<0.0004mg/Kg4-Chlorotoluene
12/13/22 14:240.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
12/13/22 14:240.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
12/13/22 14:240.0050.0006<0.0006mg/Kg1,2-Dibromoethane
12/13/22 14:240.0050.0006<0.0006mg/KgDibromomethane
12/13/22 14:240.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
12/13/22 14:240.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 17Date:12/19/2022 03:33 PM
Page 59 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27716
Associated Lab Samples: 95295, 95296, 95297, 95298, 95299, 95300
LRB-V27716 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/13/22 14:240.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
12/13/22 14:240.0100.001<0.001mg/KgDichlorodifluoromethane
12/13/22 14:240.0050.0008<0.0008mg/Kg1,1-Dichloroethane
12/13/22 14:240.0050.001<0.001mg/Kg1,2-Dichloroethane
12/13/22 14:240.0050.0007<0.0007mg/Kg1,1-Dichloroethene
12/13/22 14:240.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
12/13/22 14:240.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
12/13/22 14:240.0050.0004<0.0004mg/Kg1,2-Dichloropropane
12/13/22 14:240.0050.0006<0.0006mg/Kg1,3-Dichloropropane
12/13/22 14:240.0050.001<0.001mg/Kg2,2-Dichloropropane
12/13/22 14:240.0050.0008<0.0008mg/Kg1,1-Dichloropropene
12/13/22 14:240.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
12/13/22 14:240.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
12/13/22 14:240.2500.014<0.014mg/KgEthanol
12/13/22 14:240.0050.0006<0.0006mg/KgEthylbenzene
12/13/22 14:240.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
12/13/22 14:240.0100.0008<0.0008mg/KgHexachlorobutadiene
12/13/22 14:240.0100.0007<0.0007mg/Kgn-Hexane
12/13/22 14:240.0200.0006<0.0006mg/Kg2-Hexanone
12/13/22 14:240.0050.0005<0.0005mg/KgIsopropylbenzene
12/13/22 14:240.0050.001<0.001mg/Kg4-Isopropyl toluene
12/13/22 14:240.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
12/13/22 14:240.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
12/13/22 14:240.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
12/13/22 14:240.0100.001<0.001mg/KgMethylene Chloride
12/13/22 14:240.0100.0010<0.0010mg/KgNaphthalene
12/13/22 14:240.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 17Date:12/19/2022 03:33 PM
Page 60 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27716
Associated Lab Samples: 95295, 95296, 95297, 95298, 95299, 95300
LRB-V27716 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/13/22 14:240.0050.001<0.001mg/KgStyrene
12/13/22 14:240.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
12/13/22 14:240.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
12/13/22 14:240.0050.0009<0.0009mg/KgTetrachloroethene
12/13/22 14:240.0050.0007<0.0007mg/KgToluene
12/13/22 14:240.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
12/13/22 14:240.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
12/13/22 14:240.0050.001<0.001mg/Kg1,1,1-Trichloroethane
12/13/22 14:240.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
12/13/22 14:240.0050.0009<0.0009mg/KgTrichloroethene
12/13/22 14:240.0100.002<0.002mg/KgTrichlorofluoromethane
12/13/22 14:240.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
12/13/22 14:240.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
12/13/22 14:240.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
12/13/22 14:240.0100.0005<0.0005mg/KgVinyl Acetate
12/13/22 14:240.0100.0005<0.0005mg/KgVinyl Chloride
12/13/22 14:240.0050.0005<0.0005mg/Kgo-Xylene
12/13/22 14:240.0100.001<0.001mg/Kgm,p-Xylene
12/13/22 14:244-Bromofluorobenzene (S)98.8 70-130
12/13/22 14:24Dibromofluoromethane (S)100 84-123
12/13/22 14:24Toluene-d8 (S)94.2 76-129
LCS-V27716 LCSD-V27716Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.112 1121070.1070.100mg/KgAcetone 29-198 4.5 20
Page 6 of 17Date:12/19/2022 03:33 PM
Page 61 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27716
LCS-V27716 LCSD-V27716Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.093.40.0930.100mg/KgAcrolein 70-130 3.7 20
0.104 10499.00.0990.100mg/KgAcrylonitrile 65-134 4.9 20
0.048 96.696.60.0480.050mg/KgBenzene 74-127 0.0 20
0.043 87.890.40.0450.050mg/KgBromobenzene 73-125 2.9 20
0.050 1021000.0500.050mg/KgBromochloromethane 72-134 1.1 20
0.048 97.096.60.0480.050mg/KgBromodichloromethane 75-122 0.4 20
0.047 95.690.40.0450.050mg/KgBromoform 66-135 5.5 20
0.034 68.479.80.0390.050mg/KgBromomethane 20-180 15.3 20
0.043 87.090.60.0450.050mg/Kgn-Butylbenzene 65-135 4.0 20
0.041 82.887.80.0430.050mg/Kgsec-Butyl benzene 66-131 5.8 20
0.042 84.487.60.0430.050mg/Kgtert-Butyl benzene 67-132 3.7 20
0.048 97.699.60.0490.050mg/KgCarbon Disulfide 61-129 2.0 20
0.047 94.496.60.0480.050mg/KgCarbon Tetrachloride 64-143 2.3 20
0.047 94.289.00.0440.050mg/KgChlorobenzene 74-118 5.6 20
0.049 98.492.60.0460.050mg/KgChlorodibromomethane 73-122 6.0 20
0.049 98.299.80.0490.050mg/KgChloroethane 33-149 1.6 20
0.049 98.297.60.0480.050mg/KgChloroform 73-127 0.6 20
0.038 77.281.60.0400.050mg/KgChloromethane 45-143 5.5 20
0.042 85.089.80.0440.050mg/Kg2-Chlorotoluene 67-124 5.4 20
0.042 85.296.00.0480.050mg/Kg4-Chlorotoluene 71-126 11.9 20
0.048 96.092.20.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159 4.0 20
0.048 97.896.00.0480.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.8 20
0.047 94.696.40.0480.050mg/Kg1,2-Dibromoethane 70-132 1.8 20
0.049 98.81000.0500.050mg/KgDibromomethane 74-133 1.2 20
0.045 90.891.00.0450.050mg/Kg1,2-Dichlorobenzene 72-123 0.2 20
0.043 86.688.00.0440.050mg/Kg1,3-Dichlorobenzene 71-120 1.6 20
Page 7 of 17Date:12/19/2022 03:33 PM
Page 62 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27716
LCS-V27716 LCSD-V27716Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 88.289.60.0440.050mg/Kg1,4-Dichlorobenzene 71-123 1.5 20
0.043 86.687.00.0430.050mg/KgDichlorodifluoromethane 26-146 0.4 20
0.047 95.694.60.0470.050mg/Kg1,1-Dichloroethane 74-127 1.0 20
0.049 99.095.40.0470.050mg/Kg1,2-Dichloroethane 68-128 3.7 20
0.046 93.094.20.0470.050mg/Kg1,1-Dichloroethene 67-149 1.2 20
0.047 95.896.20.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 0.4 20
0.047 95.696.60.0480.050mg/Kgtrans-1,2-Dichloroethene 73-132 1.0 20
0.050 10196.20.0480.050mg/Kg1,2-Dichloropropane 73-130 5.0 20
0.047 95.091.40.0450.050mg/Kg1,3-Dichloropropane 75-124 3.8 20
0.046 92.094.80.0470.050mg/Kg2,2-Dichloropropane 50-142 2.9 20
0.045 91.094.80.0470.050mg/Kg1,1-Dichloropropene 71-130 4.0 20
0.052 10598.60.0490.050mg/Kgcis-1,3-Dichloropropene 71-125 6.4 20
0.052 1051010.0500.050mg/Kgtrans-1,3-Dichloropropene 68-123 3.8 20
1.46 1171051.311.25mg/KgEthanol 70-130 10.8 20
0.045 90.489.40.0440.050mg/KgEthylbenzene 74-128 1.1 20
0.098 98.094.80.0940.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 3.3 20
0.044 89.090.20.0450.050mg/KgHexachlorobutadiene 64-125 1.3 20
0.046 92.090.00.0450.050mg/Kgn-Hexane 70-130 2.1 20
0.048 97.687.20.0430.050mg/Kg2-Hexanone 61-157 11.2 20
0.041 83.689.20.0440.050mg/KgIsopropylbenzene 68-126 6.4 20
0.042 85.289.40.0440.050mg/Kg4-Isopropyl toluene 68-129 4.8 20
0.044 89.484.20.0420.050mg/KgMethyl Ethyl Ketone (MEK)63-149 5.9 20
0.048 96.494.80.0470.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.6 20
0.052 10498.00.0490.050mg/Kg4-Methyl-2-Pentanone 57-162 6.1 20
0.044 89.285.40.0420.050mg/KgMethylene Chloride 74-129 4.3 20
0.046 93.892.40.0460.050mg/KgNaphthalene 57-157 1.5 20
Page 8 of 17Date:12/19/2022 03:33 PM
Page 63 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V27717QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V27716
LCS-V27716 LCSD-V27716Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.041 83.287.00.0430.050mg/Kgn-Propylbenzene 67-130 4.4 20
0.047 94.691.20.0450.050mg/KgStyrene 77-121 3.6 20
0.047 94.089.00.0440.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 5.4 20
0.043 86.686.60.0430.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.0 20
0.044 88.292.60.0460.050mg/KgTetrachloroethene 68-130 4.8 20
0.047 95.496.20.0480.050mg/KgToluene 71-129 0.8 20
0.047 94.693.20.0460.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.4 20
0.047 95.694.60.0470.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.0 20
0.045 91.896.40.0480.050mg/Kg1,1,1-Trichloroethane 67-131 4.8 20
0.047 94.889.40.0440.050mg/Kg1,1,2-Trichloroethane 70-133 5.8 20
0.048 97.495.40.0470.050mg/KgTrichloroethene 75-133 2.0 20
0.044 89.491.40.0450.050mg/KgTrichlorofluoromethane 44-146 2.2 20
0.044 88.691.40.0450.050mg/Kg1,2,3-Trichloropropane 60-137 3.1 20
0.042 85.690.20.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 5.2 20
0.041 83.686.80.0430.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.7 20
0.052 10594.00.0470.050mg/KgVinyl Acetate 60-140 11.0 20
0.042 85.687.20.0430.050mg/KgVinyl Chloride 48-147 1.8 20
0.046 92.090.40.0450.050mg/Kgo-Xylene 74-126 1.7 20
0.092 92.290.40.0900.100mg/Kgm,p-Xylene 75-124 1.9 20
96.098.44-Bromofluorobenzene (S)70-130
99.897.8Dibromofluoromethane (S)84-123
97.095.4Toluene-d8 (S)76-129
Page 9 of 17Date:12/19/2022 03:33 PM
Page 64 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27890QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27785
Associated Lab Samples: 95295, 95296, 95297, 95298, 95299, 95300
LRB-V27785 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/15/22 10:490.6600.116<0.116mg/KgAcenaphthene
12/15/22 10:490.6600.105<0.105mg/KgAcenaphthylene
12/15/22 10:490.6600.152<0.152mg/KgAniline
12/15/22 10:490.6600.143<0.143mg/KgAnthracene
12/15/22 10:490.6600.139<0.139mg/KgBenzo(a)anthracene
12/15/22 10:490.6600.147<0.147mg/KgBenzo(a)pyrene
12/15/22 10:490.6600.146<0.146mg/KgBenzo(b)fluoranthene
12/15/22 10:490.6600.136<0.136mg/KgBenzo(g,h,i)perylene
12/15/22 10:490.6600.137<0.137mg/KgBenzo(k)fluoranthene
12/15/22 10:492.000.580<0.580mg/KgBenzoic Acid
12/15/22 10:490.6600.105<0.105mg/KgBenzyl alcohol
12/15/22 10:490.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
12/15/22 10:490.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
12/15/22 10:490.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
12/15/22 10:490.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
12/15/22 10:490.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
12/15/22 10:490.3300.113<0.113mg/KgButyl benzyl phthalate
12/15/22 10:490.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
12/15/22 10:490.3300.112<0.112mg/Kg4-Chloroaniline
12/15/22 10:490.6600.116<0.116mg/Kg2-Chloronaphthalene
12/15/22 10:490.6600.098<0.098mg/Kg2-Chlorophenol
12/15/22 10:491.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
12/15/22 10:490.6600.142<0.142mg/KgChrysene
12/15/22 10:490.6600.230<0.230mg/KgDibenz(a,h)anthracene
12/15/22 10:490.6600.119<0.119mg/KgDibenzofuran
12/15/22 10:490.6600.094<0.094mg/Kg1,2-Dichlorobenzene
12/15/22 10:490.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 10 of 17Date:12/19/2022 03:33 PM
Page 65 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27890QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27785
Associated Lab Samples: 95295, 95296, 95297, 95298, 95299, 95300
LRB-V27785 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/15/22 10:490.3300.097<0.097mg/Kg1,4-Dichlorobenzene
12/15/22 10:490.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
12/15/22 10:490.6600.095<0.095mg/Kg2,4-Dichlorophenol
12/15/22 10:490.6600.180<0.180mg/KgDiethyl phthalate
12/15/22 10:490.6600.174<0.174mg/KgDimethyl phthalate
12/15/22 10:490.3300.108<0.108mg/Kg2,4-Dimethylphenol
12/15/22 10:490.6600.107<0.107mg/KgDi-n-butyl phthalate
12/15/22 10:491.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
12/15/22 10:491.500.520<0.520mg/Kg2,4-Dinitrophenol
12/15/22 10:490.6600.096<0.096mg/Kg2,4-Dinitrotoluene
12/15/22 10:490.6600.108<0.108mg/Kg2,6-Dinitrotoluene
12/15/22 10:490.3300.143<0.143mg/KgDi-n-Octyl Phthalate
12/15/22 10:490.6600.123<0.123mg/KgFluoranthene
12/15/22 10:490.6600.128<0.128mg/KgFluorene
12/15/22 10:490.6600.106<0.106mg/KgHexachlorobenzene
12/15/22 10:490.6600.097<0.097mg/KgHexachlorobutadiene
12/15/22 10:490.6600.157<0.157mg/KgHexachlorocyclopentadiene
12/15/22 10:490.6600.079<0.079mg/KgHexachloroethane
12/15/22 10:490.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
12/15/22 10:490.6600.191<0.191mg/KgIsophorone
12/15/22 10:490.6600.106<0.106mg/Kg1-Methylnaphthalene
12/15/22 10:490.6600.100<0.100mg/Kg2-Methylnaphthalene
12/15/22 10:490.6600.097<0.097mg/Kg2-Methylphenol
12/15/22 10:490.6600.084<0.084mg/Kg3&4 Methylphenol
12/15/22 10:490.6600.144<0.144mg/KgNaphthalene
12/15/22 10:490.6600.096<0.096mg/Kg2-Nitroaniline
12/15/22 10:490.6600.120<0.120mg/Kg3-Nitroaniline
Page 11 of 17Date:12/19/2022 03:33 PM
Page 66 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27890QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27785
Associated Lab Samples: 95295, 95296, 95297, 95298, 95299, 95300
LRB-V27785 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
12/15/22 10:490.3300.093<0.093mg/Kg4-Nitroaniline
12/15/22 10:490.3300.116<0.116mg/KgNitrobenzene
12/15/22 10:490.6600.088<0.088mg/Kg2-Nitrophenol
12/15/22 10:490.6600.117<0.117mg/Kg4-Nitrophenol
12/15/22 10:490.6600.263<0.263mg/KgN-Nitrosodimethylamine
12/15/22 10:490.6600.181<0.181mg/KgN-Nitrosodiphenylamine
12/15/22 10:490.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
12/15/22 10:491.000.347<0.347mg/KgPentachlorophenol
12/15/22 10:490.6600.208<0.208mg/KgPhenanthrene
12/15/22 10:490.6600.112<0.112mg/KgPhenol
12/15/22 10:490.6600.134<0.134mg/KgPyrene
12/15/22 10:490.3300.079<0.079mg/KgPyridine
12/15/22 10:490.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
12/15/22 10:490.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
12/15/22 10:490.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
12/15/22 10:492-Fluorobiphenyl (S)94.0 44-115
12/15/22 10:492-Fluorophenol (S)78.6 35-115
12/15/22 10:49Nitrobenzene-d5 (S)79.0 37-122
12/15/22 10:494-Terphenyl-d14 (S)108 54-127
12/15/22 10:492,4,6-Tribromophenol (S)80.1 39-132
12/15/22 10:49Phenol-d5 (S)75.3 34-121
LCS-V27785 LCSD-V27785Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.46 87.489.81.501.67mg/KgAcenaphthene 40-123 2.7 20
Page 12 of 17Date:12/19/2022 03:33 PM
Page 67 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27890QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27785
LCS-V27785 LCSD-V27785Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.51 90.491.01.521.67mg/KgAcenaphthylene 32-132 0.6 20
2.03 1221232.051.67mg/KgAniline 12-197 0.9 20
1.69 1011011.681.67mg/KgAnthracene 47-123 0.5 20
1.71 1021021.711.67mg/KgBenzo(a)anthracene 49-126 0.0 20
2.07 1241292.151.67mg/KgBenzo(a)pyrene 45-129 3.7 20
2.03 1221232.051.67mg/KgBenzo(b)fluoranthene 45-132 0.9 20
1.88 1131191.991.67mg/KgBenzo(g,h,i)perylene 43-134 5.6 20
1.99 1191272.121.67mg/KgBenzo(k)fluoranthene 47-132 6.3 20
<0.580 0.0*0.0*<0.5801.67mg/KgBenzoic Acid 10-83 0.0 20
1.40 83.883.21.391.67mg/KgBenzyl alcohol 29-122 0.7 20
1.35 80.880.21.341.67mg/KgBis(2-Chloroethoxy)methane 36-121 0.7 20
1.30 77.880.81.351.67mg/KgBis(2-Chloroethyl)ether 31-120 3.7 20
1.44 86.283.21.391.67mg/KgBis(2-Chloroisopropyl)ether 33-131 3.5 20
1.80 1081071.781.67mg/KgBis(2-ethylhexyl)phthalate 51-133 1.1 20
1.73 1041041.741.67mg/Kg4-Bromophenyl phenyl ether 46-124 0.5 20
1.77 1061021.701.67mg/KgButyl benzyl phthalate 48-132 4.0 20
1.27 76.076.01.271.67mg/Kg4-Chloro-3-methylphenol 45-122 0.0 20
1.30 77.874.81.251.67mg/Kg4-Chloroaniline 17-106 3.9 20
1.57 94.094.61.581.67mg/Kg2-Chloronaphthalene 41-114 0.6 20
1.46 87.489.21.491.67mg/Kg2-Chlorophenol 34-121 2.0 20
1.52 91.095.81.601.67mg/Kg4-Chlorophenyl phenyl ether 45-121 5.1 20
1.70 1021011.681.67mg/KgChrysene 50-124 1.1 20
2.17 130138*2.301.67mg/KgDibenz(a,h)anthracene 45-134 5.8 20
1.46 87.491.61.531.67mg/KgDibenzofuran 44-120 4.6 20
1.39 83.281.41.361.67mg/Kg1,2-Dichlorobenzene 33-117 2.1 20
1.26 75.479.01.321.67mg/Kg1,3-Dichlorobenzene 30-115 4.6 20
Page 13 of 17* QC Fail Date:12/19/2022 03:33 PM
Page 68 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27890QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27785
LCS-V27785 LCSD-V27785Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.28 76.679.01.321.67mg/Kg1,4-Dichlorobenzene 31-115 3.0 20
1.24 74.270.01.171.67mg/Kg3,3'-Dichlorobenzidine 22-121 5.8 20
1.43 85.683.21.391.67mg/Kg2,4-Dichlorophenol 40-122 2.8 20
1.54 92.295.21.591.67mg/KgDiethyl phthalate 50-124 3.1 20
1.60 95.894.61.581.67mg/KgDimethyl phthalate 48-124 1.2 20
1.71 1021051.761.67mg/Kg2,4-Dimethylphenol 30-127 2.8 20
1.83 1101101.841.67mg/KgDi-n-butyl phthalate 51-128 0.5 20
1.42 85.078.41.311.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 8.0 20
1.01 60.456.10.9371.67mg/Kg2,4-Dinitrophenol 27-129 7.4 20
1.54 92.295.21.591.67mg/Kg2,4-Dinitrotoluene 48-126 3.1 20
1.54 92.293.41.561.67mg/Kg2,6-Dinitrotoluene 46-124 1.2 20
1.85 1111262.101.67mg/KgDi-n-Octyl Phthalate 45-140 12.6 20
1.56 93.494.01.571.67mg/KgFluoranthene 50-127 0.6 20
1.49 89.292.81.551.67mg/KgFluorene 43-125 3.9 20
1.75 1051051.761.67mg/KgHexachlorobenzene 45-122 0.5 20
1.30 77.879.01.321.67mg/KgHexachlorobutadiene 32-123 1.5 20
1.21 72.479.01.321.67mg/KgHexachlorocyclopentadiene 32-117 8.6 20
1.35 80.877.81.301.67mg/KgHexachloroethane 28-117 3.7 20
1.89 1131181.971.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 4.1 20
1.00 59.859.20.9901.67mg/KgIsophorone 30-122 1.0 20
1.30 77.877.21.291.67mg/Kg1-Methylnaphthalene 40-119 0.7 20
1.29 77.275.41.261.67mg/Kg2-Methylnaphthalene 38-122 2.3 20
1.53 91.687.41.461.67mg/Kg2-Methylphenol 32-122 4.6 20
1.37 82.079.61.331.67mg/Kg3&4 Methylphenol 34-119 2.9 20
1.29 77.277.21.291.67mg/KgNaphthalene 35-123 0.0 20
1.55 92.889.81.501.67mg/Kg2-Nitroaniline 44-127 3.2 20
Page 14 of 17Date:12/19/2022 03:33 PM
Page 69 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V27890QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V27785
LCS-V27785 LCSD-V27785Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.48 88.686.81.451.67mg/Kg3-Nitroaniline 33-119 2.0 20
1.61 96.497.61.631.67mg/Kg4-Nitroaniline 63-147 1.2 20
1.23 73.671.81.201.67mg/KgNitrobenzene 34-122 2.4 20
1.27 76.074.21.241.67mg/Kg2-Nitrophenol 36-123 2.3 20
1.63 97.697.61.631.67mg/Kg4-Nitrophenol 30-132 0.0 20
1.11 66.466.41.111.67mg/KgN-Nitrosodimethylamine 10-146 0.0 20
1.96 1171141.901.67mg/KgN-Nitrosodiphenylamine 38-127 3.1 20
1.38 82.680.81.351.67mg/KgN-Nitroso-di-n-propylamine 36-120 2.1 20
2.01 1201181.971.67mg/KgPentachlorophenol 25-133 2.0 20
1.65 98.81011.681.67mg/KgPhenanthrene 50-121 1.8 20
1.43 85.689.81.501.67mg/KgPhenol 34-121 4.7 20
1.73 1041041.741.67mg/KgPyrene 47-127 0.5 20
0.881 52.753.70.8981.67mg/KgPyridine 10-80 1.9 20
1.27 76.076.61.281.67mg/Kg1,2,4-Trichlorobenzene 34-118 0.7 20
1.55 92.891.01.521.67mg/Kg2,4,5-Trichlorophenol 41-124 1.9 20
1.52 91.097.01.621.67mg/Kg2,4,6-Trichlorophenol 39-126 6.3 20
93.498.82-Fluorobiphenyl (S)44-115
75.678.02-Fluorophenol (S)35-115
74.871.8Nitrobenzene-d5 (S)37-122
1101114-Terphenyl-d14 (S)54-127
86.491.22,4,6-Tribromophenol (S)39-132
69.974.7Phenol-d5 (S)34-121
Page 15 of 17Date:12/19/2022 03:33 PM
Page 70 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L654576QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L653975
Associated Lab Samples: 95295, 95296, 95297, 95298, 95299, 95300
LRB-L653975 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
12/19/22 09:190.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L653975Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1044.174.00mg/KgChromium, Hexavalent 80-120
V 95295-DUP-L653975Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/19/22 09:511.4<0.203< 0.203mg/KgChromium, Hexavalent
V 95295-MS-L653975Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
38.4 92.541.5< 0.141mg/KgChromium, Hexavalent 75-125
Page 16 of 17Date:12/19/2022 03:33 PM
Page 71 of 74
Quality Control Data
22-346-0011Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
ATL-006
Dry Weight Determination
SW-DRYWT
V27711QC Analytical Batch:
Analysis Method:
Analysis Description:
V 95297-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/13/22 18:015.222.323.5%Moisture
V 95404-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 12/13/22 18:015.817.516.5%Moisture
Page 17 of 17Date:12/19/2022 03:33 PM
Page 72 of 74
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-346-0011
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 1.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:12/12/2022 15:34:53
Special precautions or instructions included?
Comments:
Page 73 of 74
Page 74 of 74