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HomeMy WebLinkAbout24028_National Linen_PIIR_20201020ENVIRONMENTAL SITE ASSESSMENT REPORT NATIONAL LINEN PROPERTY BROWNFIELDS PROJECT NO. 24028-20-065 (Version 1.0) Prepared for: NC Department of Environmental Quality Division of Waste Management Brownfields Program 217 W Jones St. Raleigh, NC 27699 Prepared by: Aptus Management, PLLC 109 Amber Court Carrboro, NC 27510 NC Firm Engineering License # P-1130 John Gallagher, P.E., RSM ,`��it�zit=rtai�,�� "• O\A Roz 4QFESS%� SEAL 024199 13 Poo GAIlk 11-`%,,*' October 20, 2020 Table of Contents 1 EXECUTIVE SUMMARY..........................................................................................................................1 2 INTRODUCTION..................................................................................................................................... 2 2.1 Site Location, Address and Acreage.............................................................................................. 2 2.2 History of the Property................................................................................................................. 2 2.3 National Linen Site Redevelopment Plan......................................................................................3 2.4 Prior Assessment Findings............................................................................................................ 3 2.5 Data Gaps To Be Filled..................................................................................................................4 3 SOIL GAS ASSESSMENT SUMMARY.......................................................................................................4 3.1 Non -Residential Site Use and VI Risk............................................................................................4 3.2 Residential Site Use and VI Risk....................................................................................................5 4 SUMMARY OF SOIL AND GROUNDWATER SAMPLING ACTIVITIES.......................................................5 4.1 Soil Sampling.................................................................................................................................5 4.2 Groundwater Sampling................................................................................................................. 6 4.3 Groundwater Elevation Measurements.......................................................................................7 5 SUMMARY OF LABORATORY TEST RESULTS.........................................................................................8 5.1 Soil Testing Results........................................................................................................................8 5.2 Groundwater Testing Results........................................................................................................8 6 QUALITY ASSURANCE/ QUALITY CONTROL...........................................................................................8 7 INVESTIGATION DERIVED WASTE MANAGEMENT................................................................................9 8 SUMMARY OF FINDINGS AND RECOMMENDATIONS...........................................................................9 8.1 Assessment Findings.....................................................................................................................9 8.1.1 Soil Gas Testing and VI Risks.................................................................................................9 8.1.2 Soil Testing............................................................................................................................9 8.1.3 Groundwater Testing............................................................................................................9 8.2 Recommendations Regarding RECs and Data Gaps....................................................................10 8.2.1 Possible Vapor Intrusion Risk..............................................................................................10 8.2.2 Site -Wide Soil Conditions....................................................................................................10 8.2.3 Site -Wide Groundwater Conditions....................................................................................10 8.2.4 Confirmation of Groundwater Flow Direction....................................................................10 8.2.5 Possible Localized Impacts..................................................................................................10 8.2.6 Possible Offsite Releases.....................................................................................................11 Figures Tables Appendix A — RDHEC Soil Gas Assessment Appendix B — Site Photos Appendix C — Instrument Calibration Appendix D — Boring Logs Appendix E — Laboratory Reports Site Assessment Report National Linen 1 EXECUTIVE SUMMARY October 20, 2020 Page 1 The National Linen site is located at 1315 South 5t" Avenue in Wilmington. The 2.6-acre site consists of the three parcels. The largest parcel is zoned UMX-Urban Mixed Use and was home to the former National Linen industrial laundry facility from circa 1950 until 2010. For the last ten years, the site was used as a storage warehouse. The main parcel is improved with a 43,000-sq-ft building, which was home to the laundry. The two smaller out -parcels are unused and unimproved and zoned Light Industrial. This report provides the assessment finding for soil gas, soil, and groundwater testing conducted at the National Laundry site. Testing focused on the largest parcel, which was home to the laundry. There are no known concerns associated with the two smaller out - parcels, and therefore no testing was conducted on either out -parcel. Samples were collected from across the property to address data gaps and provide information on possible recognized environmental conditions (i.e., contamination). The assessment was also intended to help guide due diligence, identify the land use restrictions and mitigation measures needed to safely redevelop the property, and provide suitable information for a Brownfields Agreement with North Carolina's Department of Environmental Quality (DEQ). The assessment was thorough and complete and conducted in general accordance with DEQ guidelines. It included seven soil boring sampling locations and seven temporary groundwater well sampling locations. Soil and groundwater samples were analyzed for volatile organic compounds (VOCs), semi -volatile organic compounds (SVOCs) and RCRA metals. Soil gas testing was conducted to evaluate possible vapor intrusion (VI) risk and included soil gas samples collected from seven locations at the laundry that were analyzed by US EPA Method TO-15. Only limited, low-level contamination was found at National Linen. Soil and groundwater had no measurable contamination above DEQ standards or guidelines for both commercial and residential site use. Soil gas testing showed no unacceptable VI risk for commercial redevelopment of the property, which is intended. For possible residential site use, which is not the current redevelopment plan, further assessment of potential VI risks is warranted, but only if residential development is planned. The redevelopment of the National Linen site was deemed eligible to participate in the Brownfields Program on June 30, 2020. Fifth Street Investors, LLC and Raleigh Restoration Group, LLC are co -Prospective Developers. The current redevelopment plan for the site is as a commercial brewery and retail food hall. However, other types of commercial redevelopment options are possible and residential development will be requested as an allowable future site use. The Brownfields Program was established under the Brownfields Property Reuse Act of 1997 [NCGS 130A310.30 et seq.]. This statute authorizes DEQ to work with prospective developers (provided they did not cause or contribute to site contamination) to promote the redevelopment of urban infill properties, old industrial sites, and other types of underutilized, environmentally impaired real estate. Site Assessment Report National Linen 2 INTRODUCTION 2.1 Site Location, Address and Acreage October 20, 2020 Page 2 National Linen is located at 1315 South 5t" Avenue in Wilmington. Location maps and site map showing the areas investigated are attached as Figures 1, 2 and 3, respectively. The 2.6-acre site consists of the three parcels listed below. The largest parcel is zoned UMX-Urban Mixed Use and was home to the former National Linen laundry facility and improved with a 43,000-sq-ft building. The two smaller lots are unused and unimproved and zoned Light Industrial. Parcel ID Address Parcel No. Acreage 1 1315 South 5t" Ave R05413-040-002-000 1.90 2 Unassigned R05413-041-005-000 0.56 3 Unassigned R05413-041-006-000 0.14 The site is in a mixed commercial and residential area of Wilmington. It bound on the north by The Longshoreman's Union and residences followed by Kidder Street, on the east by South 5t" Avenue followed by The Rusty Nail Bar and Maverick America, on the south by Martin Street and a rail line followed by Shannon's Auto Service, GMC Air Conditioning and Heating Equipment, and a residence (from west to east), and on the west by residences and South 7t" Street. Since development in the early 1900's, the surrounding area has been a mix of industrial, commercial, and residential buildings. 2.2 History of the Property Parcel 1 of the site was developed first as Wilmington Linen Service circa 1950 and then was owned by National Linen and affiliated entities until 2011. There were additions to the laundry facility building in the 1960's and 1970's. Current improvements total about 43,000-sq-ft. Parcels 2 and 3, located to the east of South 6th Street, are wooded and have been undeveloped since 1915 at the latest. The property was purchased by Fifth Street Investors, LLC, the current site owner, in 2011 from National Services Industries. During their ownership, there were reportedly no ongoing laundry operations. The building on Parcel 1 was utilized as a storage space for Tribute Construction, Inc., a movie set, and as temporary storage space for Mayflower Transportation. Tribute Construction stored only building materials for residential construction and Mayflower stored furniture in the building under a short-term lease. Parcels 2 and 3 remained vacant and unused by Fifth Street Investors, LLC. The redevelopment of the National Linen site was deemed eligible to participate in the Brownfields Program on June 30, 2020. Fifth Street Investors, LLC and Raleigh Restoration Group, LLC are co -Prospective Developers. The North Carolina Brownfields Program was established under the Brownfields Property Reuse Act of 1997 [NCGS 130A310.30 et seq.]. This statute authorizes DEQ to work with prospective developers (provided they did not cause or contribute to site contamination) to promote the redevelopment of urban infill properties, old industrial sites, and other types of underutilized, environmentally impaired real estate. Site Assessment Report National Linen 2.3 National Linen Site Redevelopment Plan October 20, 2020 Page 3 The current redevelopment plan for the site is as commercial brewery and retail food hall. However, other types of commercial redevelopment options are possible. The brewery/food hall plan is modeled on the successful re -purposing of the Stone's Warehouse Brownfields Property (BPN 20044-16-092) in downtown Raleigh. The co -Prospective Developer will request that residential redevelopment be an allowed land use under the Brownfields Agreement, notwithstanding that is not the current plan for the property's reuse. 2.4 Prior Assessment Findinqs ECS Southeast, LLP (ECS) prepared a Phase I Environmental Site Assessment (ESA) on June 3, 2019 for the National Linen property. Based on their findings, which included a summary of earlier work, ECS reported that from 1950 until the 1960's there were two 5,000-gallon heating oil underground storage tanks (USTs) onsite, which were reportedly replaced with two 10,000-gallon heating oil USTs. There was also one 6,000-gallon gasoline UST. One of the 10,000-gallon USTs was reportedly closed in place in 1991 and filled with sand. The other two USTs were removed in 1993 and received a Notice of No Further Action (NFA) in 1999 for residual groundwater contamination. Two 10,000-gallon heating oil aboveground storage tanks (ASTs), which remain on the exterior southeastern side of the building by the boiler room, were reportedly installed in 1986 and likely taken out of service circa 2010. ESC also noted a large out -of -service boiler, miscellaneous drums, tanks, hydraulic lifts, compressors, and some remnants of equipment from the former laundry operations (e.g., overhead piping, duct work, etc.). Besides the records associated with the USTs and ASTs, the National Linen site is not otherwise listed as a disposal site, release or environmental incident location by federal, state, or local authorities. Based on their Phase I ESA, ECS concluded the following were recognized environmental conditions (RECs). All RECs were associated with Parcel 1 and the past use as an industrial laundry. • A 10,000-gallon closed -in -place UST on the southeastern side of the building because no formal closure information was available. • Two out -of -service ASTs, although there was no direct evidence that a release had occurred from the tanks or ancillary piping systems. • Interior hydraulic lift remnants, tanks, compressors, and drum storage. ECS concluded further that these RECs have the potential to impact subsurface conditions and cause a vapor intrusion concern. ECS recommended additional assessment but did not specify further. ECS identified no RECs with respect to Parcels 2 and 3. In addition, they identified no offsite incidents or releases expected to result in an onsite contamination at the National Linen property. Site Assessment Report October 20, 2020 National Linen Page 4 ECS did not identify the past possible use of National Laundry as a dry-cleaning facility as an REC, even though dry cleaning was noted on a 1951 Sanborn Fire Insurance Map (but not on other Sanborn maps nor was this noted elsewhere in the Phase I ESA). In addition, ECS did not identify the boiler equipment as an REC. Therefore, in addition to the RECs listed above noted by ECS, we consider the possibility that the site operated historically as a dry cleaner to be an REC. Also, we consider the out -of -service boiler and ancillary equipment in the boiler room area to be an REC. 2.5 Data Gaps To Be Filled At National Linen only limited prior Phase II -type assessment work has been completed and what was done focused on testing in and around the USTs that were taken out of service and either removed or, in the case of one tank, closed -in -place. Otherwise, the other RECs noted above have not been assessed. Therefore, the assessment was designed to fill data gaps regarding the possible nature and extent of contamination and other pertinent information, including: • Possible vapor intrusion risk • Site -wide soil conditions • Site -wide groundwater conditions • Confirmation of groundwater flow direction • Possible localized impacts where USTs were located, near ASTs and other equipment, and in the boiler room area • Possible offsite releases causing onsite contamination No RECs or other potential concerns were identified associated with the two smaller out - parcels located to the east of the former laundry facility. Consequently, no assessment sampling was conducted there. 3 SOIL GAS ASSESSMENT SUMMARY Aptus retained RDH Environmental Consulting (RDHEC) to complete a soil gas assessment at National Linen and evaluate possible vapor VI risks. The RDHEC report is included by reference here and provided in Appendix A. RDHEC conducted soil gas sampling on September 10, 2020. At total of nine soil gas samples at eight locations, plus a duplicate sample, were collected, including beneath the boiler room, and in laundry process areas and storage locations within the building. The soil gas samples were analyzed by USEPA Method TO-15 for the full analyte list. A total of 24 analytes were detected. The results were compared to the DEQ's February 2018 list of Non -Residential and Residential VI Soil Gas Screening Levels (SGSLs) and evaluated further using DEQ's Risk Calculator. 3.1 Non -Residential Site Use and VI Risk The reported concentrations of detected analytes were well below their respective Non - Residential SGSLs. In addition, concentrations of the detected analytes was entered into the DEQ Risk Calculator to determine the Non -Residential Soil Gas to Indoor Air risk. This showed no unacceptable cancer risk or non -cancer hazard risk. Site Assessment Report National Linen October 20, 2020 Page 5 As a result, RDHEC concluded that no unacceptable VI risks exist, the VI pathway at the existing building is incomplete, and no further investigation or mitigation is necessary for commercial redevelopment. Aptus concurs with these findings. 3.2 Residential Site Use and VI Risk While the current redevelopment plan does not include residential use, residential use may, nevertheless, be an allowed future land use pursuant to a Brownfields Agreement entered into by the Prospective Developer and DEQ. Therefore, RDHEC also evaluated possible VI risk for residential use. For this, they compared the soil gas assessment results against Residential SGSLs. Only three analytes — chloroform, dichlorodifluoromethane (Freon 12) and trichloroethylene (TCE) — exceeded their Residential SGSLs. RDHEC also evaluated possible VI risk for residential use using the DEQ Risk Calculator to determine the Resident Soil Gas to Indoor Air risk. This showed acceptable cumulative cancer risk, but the non -cancer hazard risk was greater than 1.0, primarily from Freon 12 and TCE. We do not have an explanation for the possible presence of Freon 12, a refrigerant with no known use at the facility. RDHEC noted that the presence of low-level TCE (and PCE at levels below the Residential SGSL) could be from possible solvent use or historical dry-cleaning operations, notwithstanding no indication of gross pollution conditions were found. As a result, RDHEC concluded that in the event of future residential site use, which is not the current redevelopment plan, further assessment of potential VI risks was warranted. Aptus concurs with these findings. 4 SUMMARY OF SOIL AND GROUNDWATER SAMPLING ACTIVITIES 4.1 Soil Sampling On September 11, 2020, Tom Proctor of Proctor Environmental Services, Inc. (PES) conducted the assessment sampling. The site was walked to verify parcel locations, property boundaries, and proposed sample locations. The soil boring locations were marked and are shown in Figure 4; photographs of the site can be seen in Appendix B. A total of seven borings were advanced for soil sample collection using a GeoProbe. Extracted soil was visually inspected for staining (none was observed) and screened with a photoionization device (PID) for evidence of VOC emissions. The PID, a MiniRae 3000, Unit Number 21706, was rented from Pine Environmental Services, and calibrated by a certified technician. A calibration certificate for the unit is provided in Appendix C. Boring logs summarizing the soil conditions, PID readings, and sample collection intervals are provided in Appendix D. PID readings were collected directly from the soil core removed from the boring soon after collection. As the plastic -encased soil sample cores were removed from the boring, they were marked for depth -intervals at each end and laid on the ground, on either plastic sheeting or cardboard. The driller used a GeoProbe razor -knife to slice a small section from the plastic liner tube so soil could be examined and PID readings collected. The field technician inserted a field -decontaminated probe rod into the soil sample core at approximately one -foot intervals to create a hole and subsequently inserted the PID probe Site Assessment Report October 20, 2020 National Linen Page 6 into the hole to collect a PID reading from the extracted soil. This Kwik-Screening Process (KSP) allows for numerous PID readings in a short period of time to determine if an interval of extracted soil exhibits indications of adverse impact without leaving the soil exposed to atmospheric conditions over an extended period. Representative portions of the soil were collected into plastic Ziplock baggies, labeled with the boring number and depth interval, and allowed to equilibrate for approximately 15 minutes before then collecting a "baggie PID reading" by puncturing the baggie and inserting the PID probe. Finally, a "borehole PID reading" was collected by inserting the PID probe into the top of the borehole after its completion and after removing the sampling equipment. PID readings were recorded in the field notes and are summarized below. The "Borehole PID Reading" column refers to the reading collected by inserting the PID into the completed borehole after sampling equipment was removed. Soil Boring Sampling Summary Boring VOc Boring No. DPT Refusal? Termination In -Situ KSP Baggie PID Borehole Sample" (ft. bls) PID (ppm) (ppm) PID (ppm) Depth (ft. bls TW-1 S No 9 <1 <1 <1 None TW-2S No 15 <1 <1 <1 3.5 TW-3S No 15 <1 <1 <1 3.5 TW-4S No 15 <1 <1 <1 3.5 TW-5S No 15 <1 <1 <1 3.5 TW-6S No 15 <1 <1 <1 3.5 TW-7S No 15 <1 <1 <1 3.5 Discrete samples were collected for VOC analyses and three-point composite samples were the collected for SVOCs and metals analysis. Composite samples consisted of the residual soil left in the vicinity of the VOC sample and then a similar amount of soil collected approximately one foot deeper and one foot shallower from the VOC sample interval. The three-part composite samples were placed in a Ziplock baggies, thoroughly mixed and then immediately placed into the laboratory glassware and placed in an ice - filled cooler. Soil samples were transported under chain -of -custody to Waypoint Laboratories in Charlotte analysis for VOCs by Method 8260B, SVOCs by Method 8270, and RCRA metals. The two soil samples exhibiting the highest concentration of total chromium, TW- 2S and TW-7S, were also analyzed for Cr6+ by Method 7196A. The laboratory was instructed that their detection limits should, if possible, be less than the IHSB Preliminary Soil Remediation Goals (PSRGs). 4.2 Groundwater Sampling Seven temporary wells were constructed and sampled on September 11, 2020 in accordance with DEQ procedures in the locations shown in Figure 4. Site Assessment Report October 20, 2020 National Linen Page 7 Well ID Boring Depth (ft) Approximate Depth to Water (ft) Screen Interval (ft) TW-1 9 3.69 4' - 9' TW-2 15 6.61 5'-15' TW-3 15 6.73 5-15' TW-4 15 5.91 5-15' TW-5 15 6.22 5-15' TW-6 15 7.33 5-15' TW-7 15 6.03 5'-15' GeoProbe borings were advanced to approximately five (5) feet below the expected groundwater depth or 5 to 7 feet bls, and then ten feet of PVC screen and riser pipe were installed and then backfilled with filter sand and topped with a temporary bentonite seal. New polyethylene tubing and a peristaltic pump was used to slowly pump groundwater until the purged water became clearer, then a YSI multiparameter instrument was used to measure temperature, dissolved oxygen, conductivity, specific conductance, and pH to verify that representative samples are collected (Table 2). After developing the wells, groundwater samples were collected beginning with three HCl- preserved 40-ml vials (for VOC analysis), proceeding to two, one -liter unpreserved glass bottles (for SVOC analysis), and finishing with one 250-ml HNO3-preserved plastic bottle for metals analysis. This process resulted in the clearest possible samples for the metals analysis. Samples were unfiltered. A duplicate QA/QC groundwater sample and a trip blank for VOC analysis was collected. The groundwater samples were shipped under chain -of -custody to Waypoint. They were analyzed for VOCs by Method 8260B, SVOCs by Method 8270, RCRA metals and Cr6+. The laboratory was instructed that detection limits, if possible, needed to be less than the NC Groundwater Quality Standards and IHSB residential VISLs. 4.3 Groundwater Elevation Measurements The location of six of the seven temporary wells (excluding TW-3, which was not needed to establish groundwater flow direction) were field surveyed relative to a fixed landmark; the top of casing elevation was surveyed and referenced to an arbitrary datum. The depth to groundwater was subtracted from the top of casing to determine the static water level elevation. The survey data and water level measurements are summarized on Tables 4 and 5. Based on survey and depth to groundwater measurements, as shown in Figure 5, the groundwater flow direction is generally towards the south/southwest, which is consistent with the area's topography. (Mr. Proctor is not a registered land surveyor and the field survey was to determine general groundwater flow direction.) Site Assessment Report October 20, 2020 National Linen Page 8 5 SUMMARY OF LABORATORY TEST RESULTS 5.1 Soil Testing Results The soil laboratory test results are summarized in Table 1 and a copy of the laboratory report is provided in Appendix E. Most constituents were reported as not detected (i.e., below the laboratory detection limits). The few low-level detections measured were well below PSRGs for both commercial and residential site use. Perhaps most importantly, no contamination in soil attributable to dry-cleaning solvents was found. Methylene chloride, a common laboratory relict, was detected at low estimated concentrations indicated by the "J" flag. Four common SVOCs often found in urban fill (benzo(a)pyrene, benzo(b)fluoranthene, fluoranthene, and pyrene) were detected in a single sample from the boring TW-7, but at low estimated concentrations below PSRGs. Chromium (total) and lead were detected but below PSRGs. Chromium 6+ was reported as non -detected in the two samples that were analyzed. The detection limit for chromium 6+ was below the commercial PSRG (although slightly above the residential PSRG). 5.2 Groundwater Testina Results The groundwater analytical results are summarized in Table 3 and a copy of the laboratory report is provided in Appendix E. No contamination above NC Groundwater Quality Standards or vapor intrusion screening levels were reported. The laboratory reported low levels VOCs (chloromethane, chloroform, methylene chloride and tetrachloroethylene) at "J" estimated values. No TCE was reported above laboratory detection limits. No SVOCs were reported in any samples above reporting detection limits. Barium, a natural mineral, was detected but below its groundwater standard. 6 QUALITY ASSURANCE/ QUALITY CONTROL Standard DEQ quality assurance/quality control (QA/QC) procedures were followed. Sampling equipment, including the water -level probe, were decontaminated using Liquinox° detergent and deionized water prior to and between each use. Sampling personnel wore disposable nitrile gloves. New polyethylene tubing was used at each groundwater sampling point. Samples were collected into laboratory -provided glassware or specified containers to ensure sufficient sample volume for analyses. Samples were shipped overnight by courier to the laboratory in ice -filled coolers under chain -of -custody protocols. QA/AC samples were submitted to the laboratory. Specifically, one duplicate groundwater sample (Dupe-W from TMW-6) and one water trip blank were submitted for VOC analysis. Neither the duplicate sample nor trip blank had detectable concentrations of VOCs over laboratory reporting limits. Records of equipment calibration and well gauging, purging, and sampling data were maintained by field personnel at each sample location. The laboratory analytical reports, chain -of -custody records and field notes were evaluated to ensure that the reported results are valid, accurate and sufficient to meet quality objectives. Accuracy has been evaluated through reviewing laboratory -spiked recoveries and precision has been evaluated through the assessment of duplicate results. Site Assessment Report October 20, 2020 National Linen Page 9 7 INVESTIGATION DERIVED WASTE MANAGEMENT The small quantities of groundwater and soil IDW generated during sampling was placed back into the boring or spread around the boring location as no indications of adverse impacts were encountered. 8 SUMMARY OF FINDINGS AND RECOMMENDATIONS 8.1 Assessment Findings This report provides the assessment finding for soil gas, soil, and groundwater testing. Samples were collected from across the property and intended to address data gaps and provide information on possible RECs at National Linen. The assessment was also intended to help guide due diligence, identify the land use restrictions and mitigation measures needed to safely redevelop the property, and provide suitable information for a Brownfields Agreement that the Prospective Developer intends to enter into with DEQ. As discussed above and summarized in more detail below, only limited, low-level contamination was found at National Linen. Soil and groundwater had no measurable contamination above DEQ standards or guidelines applicable to both commercial and residential site use. Soil gas testing showed no unacceptable VI risk for commercial redevelopment of the property, which is the intended plan for National Linen. For residential site use, which is not the current redevelopment plan, further assessment of potential VI risks should be conducted. 8.1.1 Soil Gas Testing and VI Risks Low-level contamination was reported in soil gas samples, but below Non -Residential SGSLs. RDHEC concluded that no unacceptable VI risks exist, and no further investigation or mitigation is necessary for commercial redevelopment. For possible, residential site use, which is not the current redevelopment plan, further assessment of potential VI risks should be conducted. Aptus concurs with these findings. 8.1.2 Soil Testing No VOCs, SVOCs or metals were detected in soil at concentrations that exceeded their most stringent regulatory guidelines, which depending on the analyte, is either the IHSB residential health -based or protection of groundwater PSRGs. Most constituents tested were reported as non -detected. Based on these assessment findings, there were no VOCs, SVOCs or metal contaminants in soil that are expected to pose an unacceptable risk for redevelopment of the National Linen site. 8.1.3 Groundwater Testing No VOCs, SVOCs or metals were detected in groundwater at concentrations above their NC Groundwater Quality Standards or DEQ vapor intrusion screening levels for residential and commercial site use. Most analytes were reported as non -detected. Only four VOCs (chloromethane, methylene chloride, chloroform and tetrachloroethylene) were reported as being detected in groundwater. In each case, they were reported as estimated concentrations, as indicated by the "J" flags in the laboratory report. None of Site Assessment Report October 20, 2020 National Linen Page 10 the estimated levels of these analytes exceeded their North Carolina Groundwater Quality Standards or vapor intrusion screening levels. Also based on the groundwater test results, there does not appear to be onsite contamination at National Linen that originated from offsite upgradient sources. The most upgradient well, TW-2, located at the northeast corner of the site, was contaminant -free and the other onsite wells, including those with low-level impacts, do not appear to be impacted by a possible offsite source. 8.2 Recommendations Regarding RECs and Data Gaps Among other objectives of this assessment, as discussed above, the work was intended to provide information to fill certain data gaps, help direct safe redevelopment of the National Linen property and for the site Brownfields Agreement. 8.2.1 Possible Vapor Intrusion Risk No unacceptable VI risks appear to exist for commercial use and, therefore, no further VI investigation or mitigation is recommended for that development scenario. For possible residential site use, which is not the current redevelopment plan, further assessment of potential VI risks is warranted, but only if residential development is planned. 8.2.2 Site -Wide Soil Conditions Across the site, no VOCs, SVOCs or metals were detected in soil at concentrations that exceeded their most stringent regulatory guidelines, which depending on the analyte, is either the IHSB residential health -based or protection of groundwater PSRGs. Most constituents tested were reported as non -detected. Therefore, no further investigation of soil conditions is recommended. 8.2.3 Site -Wide Groundwater Conditions Across the site, no VOCs, SVOCs or metals were detected in groundwater at concentrations above their NC Groundwater Quality Standards or DEQ vapor intrusion screening levels for residential and commercial site use. Most analytes were reported as non -detected. Therefore, no further investigation of groundwater conditions is recommended. 8.2.4 Confirmation of Groundwater Flow Direction Groundwater flow is generally to the southwest following the area topography. No further assessment of groundwater flow direction is recommended. 8.2.5 Possible Localized Impacts The assessment included soil, groundwater and soil gas sampling throughout the site including near where USTs were located, the remaining ASTs and other equipment, and in the boiler room area. Like our findings on the site -wide conditions, virtually no contamination was found in soil and groundwater attributable to possible localized onsite sources. Therefore, no further investigation of soil or groundwater conditions is recommended with respect to possible onsite sources. Site Assessment Report National Linen 8.2.6 Possible Offsite Releases October 20, 2020 Page 11 Based on the groundwater test results, there does not appear to be onsite contamination at National Linen that originated from an offsite upgradient source. The most upgradient well, TW-2, located at the northeast corner of the site, was contaminant -free and the other onsite wells, including those with low-level impacts, do not appear to be contaminated by possible offsite sources. Therefore, no further investigation of possible offsite upgradient contaminant sources is recommended. Figures or ti 11 i � f Aptus Management, PLLC TOPOGRAPHICAL SITE MAP FORMER NATIONAL LINEN FACILITY 1315 SOUTH 5TH AVENUE WILMINGTON, NEW HANOVER COUNTY, NC 28401 NCBF PROJECT NO: 24028-20-065 DRAWN BY: DATE: OCT 2020 DRAFTING CHECK BY: JOB NO: 2009.00 BYGINEER CHECK CAD # 2009-00-02 APPROVED , BY: DWG NO: 2 REFERENCE: IMAGERY SOURCE - USGS 7.5 Minute Wilmington NC Quadrangle 2019, 5-Foot Contours, North American Datum of 1983 (NAD83), World Geodetic System 1984 (WGS84) L-.0 J (iC) H --LLL 4s � I � j I ;61- + I I i — Lr 311 I I I � u v (_40 — jjs x DRAWN BY: �` DATE: OCT 2020 SITE MAP WITH PARCEL OVERLAYS DRAFTING CHECK JOB N0: 2009.00 Aptus Management, PLLC FORMER NATIONAL LINEN FACILITY 1315 WILMINGTON, SOUTH 5TH AVENUE NEW HANOVER COUNTY, NC 28401 BYGINEER CHECK CAD # 2009-00-03 NCBF PROJECT NO: 24028-20-065 APPROVED BY: DWG NO: 3 REFERENCE: IMAGERY SOURCE - New Hanover County GIS Parcel Map ® TW-1 _ 1 TW- TW i44_. . y , r 1 W-6 TW-3 ®TW-2 = :� ®TW-7 — LEGEND: ® Well Location and I D# 1" = 50' Figure 4 — Soil Boring and Basemap Source: Site Map with Overlay Provided by Clearscapes Architecture & Art, 9/21/20 Temporary Well Location Map ft 1' I Well Location and ID# 1"=50' Figure 5 - Groundwater Flow Basemap Source: Site Map with Overlay Provided by Clearscapes Architecture & Art, 9/21/20 Direction Map, 9/11/19 Former National Linen Facility 1315 South 5t" Avenue Wilmington, New Hanover County, North Carolina ctl APTUS Management, PLLC NCBF Project No. 24028-20-065 Tables r Table 1 Soil Sample Analytical Results Former National Linen Facility 1315 South 5th Avenue Wilmington, New Hanover County, North Carolina Brownfield Project Number: 24028-20-065 IHSB IHSB Industrial Sample ID Protection of TW-1S TW-2S TW-3S TW-4S TW-5S TW-6S TW-7S Residential Health Based Commercial Health Based Groundwater VOC Sample Depth (ft bgs)* PSRG (mg/Kg) 2.5' 3.5 3.5' 3.5' 3.5' 3.5 4' PSRG (irri PSRG (irri VOCs by 8260B Methylene Chloride 58 650 0.025 NS 0.0052 0.0032 J 0.0035 J 0.0030 J 0.0031 J 0.0035 J SVOCs by 8270D Benzo(a)pyrene BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.038 J Benzo(b)fluoranthene BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.046 J Fluoranthene BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.053 J Pyrene BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.047 J Metals by 601 OD Chromium* No PSRG No PSRG 360,000 NS 1.7 1.5 1.3 BRL 1.4 2.1 Chromium VI by Method 7196 0.31 6.5 No PSRG NA <0.45 NA NA NA NA <0.53 Lead 400 800 270 NS 3.8 1.4 BRL BRL 1.6 8.7 NOTES: I concentrations are in mg/Kg or parts per million (ppm) NS - No Sample collected from this location *VOC samples were collected from discrete depths. SVOC and Metals samples were composited from aliquots collected from the VOC sample depth intervals and within one (1) foot on either side of it ** The two soil samples exhibiting the highest total chromium concentrations, TW-2S and TW-7S, were also analyzed by the laboratory for Chromium VI by Method 7196A NA - Sample not analyzed for that constituent ft bgs - feet below ground surface Bolded concentrations indicate constituent detected in excess of laboratory reporting limit Bolded and Shaded concentrations exceed at least one IHSB PSRG Table 2 Summary of Groundwater Field Parameters Former National Linen Facility 1315 South 5th Avenue Wilmington, New Hanover County, North Carolina Brownfield Project Number: 24028-20-065 Well ID °C DO (mg/L) SC (mS/m) pH ORP (mV) TW-1 @1442 16.9 9.75 620 6.44 -85 @1444 16.0 9.52 628 6.45 -87 @1446 16.0 9.42 634 6.45 -103 @1448 16.0 9.44 665 6.46 -107 TW-2 @1245 19.3 0.43 440 6.31 -113 @1247 19.5 0.51 431 6.43 -165 @1250 19.7 0.47 420 6.45 -192 @1252 19.7 0.46 417 6.46 -203 TW-3 @1650 13.6 3.31 1145 6.73 -154 @1652 13.8 3.42 1142 6.78 -155 @1654 13.7 3.37 1147 6.69 -151 @1656 13.9 3.39 1140 6.80 -159 TW-4 @1050 16.3 9.75 629 6.40 -85 @1053 16.2 9.52 628 6.45 -87 @1055 16.3 9.42 634 6.46 -103 @1058 16.2 9.44 663 6.47 -107 TW-5 @1120 17.3 0.43 440 6.31 -113 @1123 17.4 0.51 431 6.43 -165 @1125 17.3 0.47 420 6.45 -192 @1127 17.6 0.46 417 6.46 -203 TW-6 @1155 13.6 3.31 1145 6.73 -154 @1158 13.8 3.42 1142 6.78 -155 @1159 13.7 3.37 1147 6.69 -151 @1201 13.9 3.39 1 1140 6.80 -159 TW-7 @1320 13.6 3.31 1145 6.73 -154 @1322 13.8 3.42 1142 6.78 -155 @1323 13.7 3.37 1147 6.69 -151 1326 1 13.9 3.39 1140 6.80 -159 NOTES: (Samples collected on 9/11/20 IDO - Dissolved Oxygen (in milligrams per liter or mg/L) ISC - Specific Conductance (in milliSeimens/meter) IpH - measured in Standard Units JORP - Oxygen Reducing Potential (in millivolts) Table 3 Groundwater Sample Analytical Results Former National Linen Facility 1315 South 5th Avenue Wilmington, New Hanover County, North Carolina Brownfield Project Number: 24028-20-065 NC Non- North Carolina Sample ID NC Residential TW 1 W TW-2W TW-3W TW-4W TW-5W TW-6W Dupe (TW-6W) TW-7W VI Screening Residential VI Screening Groundwater QualityLevels Screened Interval (ft bgs) Levels (uglL) 4 - 9 5' - 15' 5' -15' 5' -15' S' 15' 5' -15' 5' - 15' 5' - 15' (ug/L) Standard (ug/L) VOCs by 8260B Chloromethane 52 220 3 BRL BRL 0.34 J BRL 0.37 J BRL BRL BRL Methylene Chloride 940 4000 5 BRL BRL BRL 0.67 J BRL BRL BRL BRL Chloroform 8.1 36 70 BRL BRL BRL BRL BRL BRL BRL 0.23 J Tetrachloroethylene 12 48 1 BRL BRL BRL BRL BRL BRL BRL 0.27 J SVOCs by 8270D ND ND ND ND ND ND ND ND Metals by 6010D Barium NV NV 700 BRL BRL 0.023 BRL BRL BRL NA BRL NOTES: II concentrations are in ug/L or parts per billion (ppb) Dupe - Duplicate sample of groundwater at location TW-6W ND - No constituent detected in excess of its laboratory reporting limit NV - Constituent not volatile Bolded concentrations indicate constituent detected in excess of laboratory reporting limit Bolded and Shaded concentrations exceed NC Groundwater Quality Standard Table 4 Monitoring Well Water Level Elevations Former National Linen Facility 1315 South 5th Avenue Wilmington, New Hanover County, North Carolina Brownfield Project Number: 24028-20-065 Instrument Top of Casing Well ID + Reading Mid Reading - Reading Distance (ft) Degrees Heighth Elevation (ft) TW-1 6.54 5.26 4.01 105.26 100.00 253 150 TW-2 6.95 6.36 5.78 98.90 117 88 TW-7 9.72 8.23 6.76 97.03 296 69 TW-4 5.05 4.83 4.62 104.83 100.00 43 0 TW-5 5.18 4.88 4.59 99.95 59 260 TW-6 5.14 4.74 4.34 100.09 80 168 NOTES: ITW - Temporary Monitoring Well ID I IWell survey was not conducted by a RLS and is not intended to be used for any purpose other than determining groundwater flow direction. I (Wells TW-1, TW-2 and TW-7 were surveyed separately from wells TW-4 through TW-6. Separate flow directions were determined for each well set, as shown on Figure _. I IAII depths recorded in feet below TOC (Top of Casing). I Depths to groundwater in permanent wells were measured on September 11, 2020. Table 5 Monitoring Well Water Level Elevations Former National Linen Facility 1315 South 5th Avenue Wilmington, New Hanover County, North Carolina Brownfield Project Number: 24028-20-065 ' Static Water Level Elevation(ft) Well ID Top of Casing Elevation (ft) Depth to Water (ft) TW-1 100.00 3.69 96.31 TW-2 98.90 6.61 92.29 TW-7 97.03 6.03 91.00 TW-4 100.00 5.91 94.09 TW-5 99.95 6.22 93.73 TW-6 100.09 7.33 92.76 NOTES: (Well survey was not conducted by a RLS and is not intended to be used for any purpose other than determining groundwater flow direction. hells TW-1, TW-2 and TW-7 were surveyed separately from wells TW-4 through TW-6. Separate flow directions were determined for each well set. ITW - Temporary Monitoring Well ID kll depths recorded in feet below TOC (Top of Casing). (Depths to groundwater were measured on September 11, 2020 prior to well abandonment. Appendices Appendix A - RDHEC Soil Gas Assessment DF R� Environmental Consulting October 12, 2020 Mr. John Gallagher, P.E., RSM President, Managing Director Aptus Management, PLLC 109 Amber Court Carrboro, North Carolina 27510 4012 Ridgebrook Bluffs Dr. Raleigh, NC 27603 (919)389-7747 info@rdhec.com Subject: VAPOR INTRUSION SOIL GAS SAMPLING REPORT— FORMER NATIONAL LINEN SITE 1315 SOUTH 5TH AVENUE — WILMINGTON, NEW HANOVER COUNTY, NORTH CAROLINA NCBP PROJECT NO. 24028-20-065 RDHEC PROJECT NO. 1907.00 Dear Mr. Gallagher: RDH Environmental Consulting (RDHEC) is pleased to provide the enclosed report for the vapor intrusion (VI) sampling that was conducted at the above -referenced site on September 10, 2020. The project was performed in accordance with the terms and conditions of RDHEC Proposal No. P2992 dated August 29, 2020, which was authorized by your email on this date. The VI assessment was comprehensive and targeted locations throughout the former laundry facility. The work was completed in general accordance with current NC Brownfields Program VI guidance. The assessment indicated low-level detections of 24 contaminants when analyzed for the full -list of EPA Method TO-15 laboratory analytes. Comparisons of the maximum detected sample concentrations to the February 2018 North Carolina VI screening levels for soil gas at commercial properties, as well as via the NCDEQ Risk Calculator, showed no unacceptable VI risk exists for commercial use of the site. Consequently, it is RDHEC's opinion that no further assessment or mitigation is warranted. When the results were compared to the more stringent screening levels for residential use, the maximum detections of three contaminants were found to exceed their screening levels. While the redevelopment plans are currently for commercial purposes, further assessment of potential VI risks should be conducted should redevelopment plans change to residential site use. If you have any questions regarding the report or associated documentation, please feel free to contact me at (919) 389-7747 at your convenience. Sincerely, RDHYNVIRQNMfNTA `CONSULTING r- - .-1 - - % Robert D. Hill, P.E. Principal Consultant Enclosure Nflt/r," r�- 201 7 j� 7 tIN :,.`N/ t��tfN! I {Ntttttyt TABLE OF CONTENTS 1.0 EXECUTIVE SUMMARY............................................................................................ 1 2.0 INTRODUCTION...................................................................................................... 2 3.0 TESTING SUMMARY................................................................................................ 2 PROBE LOCATIONS/PLACEMENT (9/10/2020)............................................................................. 2 SAMPLING(9/10/2020).......................................................................................................... 3 4.0 SOIL GAS SAMPLING RESULTS.................................................................................. 4 5.0 CONCLUSIONS/RECOMMENDATIONS...................................................................... 5 6.0 CLOSING................................................................................................................ 6 TABLES Table 1 Vapor Intrusion Soil Gas Sampling Form (9/10/2020) Table 2 Comparison of Lab Results to Non -Residential Soil Gas Screening Levels (NRSGSLs) (DETECTIONS ONLY) Table 3 Comparison of Lab Results to Residential Soil Gas Screening Levels (RSGSLs) (DETECTIONS ONLY) DRAWINGS 1 Site Location Map 2 Topographical Site Map 3 Site Map with Parcel Overlays 4 Soil Gas Sampling Locations 5 Soil Gas Sampling Locations (w/Tabulated RSGSL Exceedances) APPENDICES Appendix A Photographs Appendix B NCDWM Non -Residential Vapor Intrusion Screening Levels Table (February 2018) Appendix C NCDWM Residential Vapor Intrusion Screening Levels Table (February 2018) Appendix D Laboratory Report and Chain of Custody Form Appendix E NCDEQ Risk Calculator Results (Resident Soil Gas to Indoor Air pathway for Vapor Intrusion) 1.0 EXECUTIVE SUMMARY Pursuant to NC Brownfields Program (NCBP) Project No: 24028-20-065, RDHEC conducted vapor intrusion (VI) sampling on September 10, 2020 at the former National Linen site located at 1315 South 51" Avenue in Wilmington, New Hanover County, North Carolina (see Drawing 1— Site Location Map, Drawing 2 — Topographical Site Map, and Drawing 3 — Site Map with Parcel Overlays, attached). The sampling was performed to provide the North Carolina Division of Environmental Quality (NCDEQ) Division of Waste Management (NCDWM) Brownfields Program an assessment of VI conditions prior to development of the site. Current plans are to repurpose the site to commercial use as a brewery and restaurant. The project involved installation of sub -slab probes (Vapor Pins) in the existing concrete slab to evaluate soil gas beneath various segments of the floor plan (boiler room, laundry process areas, and storage locations). Testing was conducted later the same day, after allowing each probe location to equilibrate for at least two hours. The sampling involved collection of nine (9) soil gas canister samples across eight (8) locations in the building footprint (one of the locations, SG-5, included a duplicate sample), in accordance with DWM VI guidance. Table 1 summarizes the canister sampling details, including boring/slab specifics, shut-in test vacuum, and pre- and post -sampling leak check observations for each location tested. The soil gas sampling locations are shown in Drawing 4. Photographs from the sampling are referenced in Appendix A. The results of the laboratory EPA Method TO-15 analyses were compared to the NCDEQ's February 2018 list of Non -Residential and Residential VI Soil Gas Screening Levels (NRSGSLs and RSGSLs, attached in Appendices B and C, respectively) following receipt of the laboratory report (Appendix D). A total of 24 analytes were detected across the nine analyses. Non -Residential Site Use and VI Risk The concentrations of each detected analyte were well below the respective NRSGSLs (three detected analytes had no NRSGSL). These results are provided in Table 2 (attached). In addition, concentrations of each of the detected analytes was entered into the NCDEQ Risk Calculator to determine the Non -Residential Soil Gas to Indoor Air risk (see Appendix E). This showed both acceptable cumulative cancer risk and non -cancer hazard risk. These VI testing results, coupled with the recent soil and groundwater site assessment by Proctor Environmental Services (PES), indicate that no unacceptable VI risks exist, the VI pathway at the existing building is incomplete, and no further investigation or mitigation is necessary for commercial redevelopment. Vapor Intrusion Soil Gas Sampling Report Former National Linen Site Wilmington, North Carolina Residential Site Use and VI Risk October 12, 2020 Page 2 While the current redevelopment plan does not include residential use, residential use may, nevertheless, be an allowed future land use pursuant to a Brownfields Agreement entered into with the prospective developer and DEQ. Therefore, we evaluated possible VI risk for residential use. For this, we compared the VI assessment results against RSGSLs — see Table 3. Three analytes — chloroform, dichlorodifluoromethane (Freon 12) and trichloroethylene (TCE) — exceeded their RSGSLs. These results are provided on Drawing 5 for reference. After discounting the presence of chloroform as a VI contaminant (due to chlorinated municipal water use), concentrations of detected analytes were entered into the NCDEQ Risk Calculator to determine the Resident Soil Gas to Indoor Air risk (see Appendix Q. This showed acceptable cumulative cancer risk but a non- cancer hazard risk greater than 1.0, primarily from Freon 12 and TCE. We do not have an explanation for the possible presence of Freon 12, a refrigerant not known to have been used at the facility. The presence of low-level TCE (and PCE at levels below the RSGSL) could be from possible historical use of the site as a dry cleaner facility. In the event of future residential site use, which is not the current redevelopment plan, RDHEC recommends further assessment of potential VI risks. 2.0 INTRODUCTION The site is comprised of three parcels across approximately 2.58 acres zoned for urban mixed - use redevelopment. One of the parcels (1315 S 5th Avenue) is a paved lot occupied by an approximately 43,000 square foot building, which is currently vacant. The other two eastern parcels across S 6th Street consist of wooded, undeveloped land. Aptus requested PES to perform soil and groundwater sampling, and RDHEC to conduct sub -slab soil gas sampling to assess site conditions. This report summarizes RDHEC's VI testing, including sampling, laboratory results and conclusions. 3.0 TESTING SUMMARY Sampling Probe Locations/Placement (9/10/2020) Shortly after arrival at 10:30 am, the probe/sampling point locations were marked and documented using a measuring wheel. A portable generator provided power for a hammer drill that was used to bore 5/8-inch holes in the concrete slab. Vapor Pins fitted with silicone sleeves were secured into each boring using a special tool and rubber hammer, then capped. The building has concrete floor slabs throughout. Each of the probes were placed into the concrete floor and compacted sands were found beneath each boring location. Additional details regarding boring ��TL7 Vapor Intrusion Soil Gas Sampling Report Former National Linen Site Wilmington, North Carolina October 12, 2020 Page 3 depth and slab thickness are provided in Table 1. The eight sample locations are shown to scale on Drawing 4. Following completion of installation at 2:30 pm, the probe locations were left to equilibrate for two hours prior to sampling. Meteorological conditions from the time of probe placement through sampling included clear/ partly cloudy skies and slight winds with periodic gusts from 5 to 10 mph. Temperatures ranged from 80 °F at the time of arrival to a high of 90 °F in the afternoon (average 81.6 °F), with relative humidity ranging from 77 to 99% (average 92%). These data are from a nearby personal weather station (station ID Historic Downtown Wilmington - KNCWILM1158) located approximately 1.1 miles north- northwest of the site on Castle Street. According to the weather station, barometric pressure was nearly constant, ranging between 30.08 to 30.16 inches during the testing (average 30.12 inches). The last rain event at the site occurred two days prior to the testing date (0.68 inches on Tuesday, September 8t"). Thus, there was no significant precipitation within 12 hours prior to (or during) the sampling event to induce pressure gradients that might affect soil V1. Sampling (9/10/2020) RDHEC began the sampling later that afternoon at 4:30 pm at the boiler room location. Sampling continued until 8 pm. The samples were collected using 1/4-inch rigid Teflon tubing and 1-L Summa canisters. Small 1- to 2-inch pieces of 1/4-inch and 3/8- inch silicone tubing were employed to make connections to the various valves and fittings of the sampling trains. Tubing was connected to the barbed fittings of the Vapor Pins, routed through a plastic shroud (which was placed over each probe site) and the opposite ends connected to 3-way valves and 60-milliliter (mQ syringes to form a sampling train for each probe location. Shut-in tests were performed to ensure air tight conditions at each location. Once the sampling train was deemed leak -free, the probe tubing was purged of three dead volumes using a 60-mL syringe and leak checked while the shroud was filled with helium. With 2.0 feet of 1/4-Inch tubing (inner diameter of 0.177 inches), three dead volumes equaled 29 mL. (Note — 120 to 180 mLs were slowly purged using the syringe to allow for sufficient volume for the helium leak check, described below). The helium concentrations within the shroud were measured and noted using a MGD-2002 leak detector. The purged soil gas was collected into a 0.5-L Tedlar bag via the 3-way valve. After purging, the Tedlar bag was removed and the contents monitored for helium levels. A successful leak check was deemed when the purged soil gas contained less than 10% of the initial shroud concentration of helium. Each of the purged helium concentrations were between 0 and 150 ppm (0.02%). Therefore leak -free conditions were achieved and no adjustments were necessary. Each of soil gas samples was collected using 1-L canisters fitted with 15- to 30-min flow regulators. The SG-5 sample location employed an inline tee and a single flow regulator to collect Vapor Intrusion Soil Gas Sampling Report Former National Linen Site Wilmington, North Carolina October 12, 2020 Page 4 a duplicate sample for quality assurance purposes, in accordance with Brownfields Program guidance, for a total of nine (9) soil gas samples/analyses across eight (8) sample locations. Following completion of the sampling, post -sampling leak checks were performed again at each location using helium. After a successful post -sampling leak check, the probe tubing and Vapor Pins were removed from each location and the probe borings were sealed with grout. Quality assurance results (shut-in test vacuum levels and pre- and post -testing leak check shroud and purge helium concentrations) are included in Table 1. Laboratory analysis request forms were then completed for laboratory analysis using EPA Compendium Method TO-15 "Determination of Volatile Organic Compounds (VOCs) in Air Collected in Specially -Prepared Canisters and Analyzed by Gas Chromatography/Mass Spectrometry (GC/MS)" and the canisters were placed back in the laboratory packaging for return shipment. The full -list of TO-15 analytes was requested for low-level analysis. Since post - sampling leak checks were conducted, helium analysis by the laboratory was not required. Samples were taken to FeclEx the next day for shipment under proper chain of custody. 4.0 SOIL GAS SAMPLING RESULTS Laboratory results for the soil gas analyses are summarized in Table 2, attached. Of the 24 analytes that resulted in detectable quantities, three (3) of the compounds did not have a listed NRSGSL. The levels for the detected compounds were compared to the current (February 2018) table of the NCDWM non-resident soil gas screening levels (NRSGSLs) for sub -slab and exterior soil gas VI at commercial sites. None of the analytes exceeded its respective NRSGSL. Each concentration was minimal and well below the corresponding NRSGSL for the contaminants, ranging from 0.003% to 26.1% of the respective screening levels. Fifteen (15) of the 21 analytes with a screening level were less than 1% of the NRSGSL. Although none of the detected analytes exceeded commercial NRSGSLs, a risk analysis was performed using the DEQ Risk Calculator. The guidance for soil gas data evaluation and screening states, "If soil gas concentrations do NOT EXCEED the SGSLs, typically no further investigation is necessary and the VI pathway may be considered incomplete if the investigator is confident in the CSM and the data collected are adequate to evaluate the VI pathway. The SGSLs are expected to be conservative due to a generic default attenuation factor." The soil and groundwater assessment results provided by Proctor Environmental Services (PES) showed almost no contamination in subsurface soil or groundwater. This also suggests site conditions will pose no unacceptable VI risk. The PES soil samples indicated no VOC concerns, and what was detected was well below the NC Preliminary Soil Remediation Goals (PSRGs). ��� Vapor Intrusion Soil Gas Sampling Report Former National Linen Site Wilmington, North Carolina October 12, 2020 Page 5 No groundwater samples collected under the building footprint showed impacts. One groundwater sample presented low-level J-Flag hits for chloromethanes and PCE outside the southwest corner of the building. PCE measured at this location was 0.27 ug/L, which is below the 15A NCAC 02L .0202 groundwater quality standard of 0.7 ug/L Residential Site Use and VI Risk While the current redevelopment plan does not include residential use, residential use may, nevertheless, be an allowed future land use pursuant to a Brownfields Agreement entered into with the prospective developer and DEQ. Therefore, we evaluated possible VI risk for residential use. For this, we compared the VI assessment results against residential soil gas screening levels (RSGSLs) — see Table 3. Three analytes — chloroform, dichlorodifluoromethane (Freon 12) and trichloroethylene (TCE) — exceeded their RSGSLs. These results are provided on Drawing 5 for reference. After discounting the presence of chloroform as a VI contaminant (due to chlorinated municipal water use), concentrations of detected analytes were entered into the NCDEQ Risk Calculator to determine the Resident Soil Gas to Indoor Air risk (see Appendix Q. This showed acceptable cumulative cancer risk but a non -cancer hazard risk greater than 1.0, primarily from Freon 12 and TCE. We do not have an explanation for the possible presence of Freon 12, a refrigerant not known to have been used at the facility. The presence of low-level TCE (and PCE also at low levels) could be from possible historical use of the site as a dry cleaner facility. In the event of future residential site use, which is not the current redevelopment plan, further assessment of VI risks should be considered. 5.0 CONCLUSIONS/RECOMMENDATIONS Based on the prior Phase I ESAs, the known concerns at the National Linen site are from onsite petroleum releases, none of which resulted in onsite groundwater contamination based on soil and groundwater sampling conducted by PES on September 11, 2020. Additionally, dry cleaning may have been conducted based on a 1951 Sanborn map that showed "Dry Cleaning" at the site, although two Phase I reports did not cite dry cleaning as a recognized environmental concern (REC). The results from this soil gas investigation show that sub -slab soil gas concentrations are below NCDWM SGSLs for non-residential use (i.e., minimal VI risk since the levels of site COCs were less than 27% of the NRSGSLs). Similarly, a risk analysis was also performed using the DEQ Risk Calculator showed no unacceptable VI risks for commercial site use. On this basis, it is RDHEC's opinion that no unacceptable VI risk exists for commercial use and no further assessment or mitigation is warranted. Vapor Intrusion Soil Gas Sampling Report Former National Linen Site Wilmington, North Carolina October 12, 2020 Page 6 If the site is to be used for residential purposes, there may be a risk of VI due to cumulative hazards of non -carcinogens primarily associated with Freon 12 and TCE (see Table 3 and Drawing S). In the event of future residential site use, which is not the current redevelopment plan, further assessment of potential VI risks should be conducted. 6.0 CLOSING Thank you for allowing RDHEC to be of assistance with your VI testing needs. If you should have questions regarding this submittal or associated documentation, please feel free to contact us at (919) 389-7747 at your convenience. Sincerely, RDH ENVIRONMENTAL CONSULTING Robert D. Hill, PE Principal Consulting Engineer Attachments cc: T. Proctor — PES ��� RDFr \1 Environmental Consulting 4012 Ridgebrook Bluffs Dr. I Raleigh, NC 27603 (919) 389-7747 1 info@rdhec.com TABLES TABLE 1 - VAPOR INTRUSION SOIL GAS SAMPLING FORM (9/10/2020) NATIONAL LINEN - WILMINGTON, NC NCBP PROJECT NO. 24028-20-06S RDHEC PROJECT NO. 2009.00 Flow Initial Final Slab Thickness Probe Sample Canister ID Controller Shut -In Pre -Hood Pre -He Leak Check Sample Canister Sample Canister Post Hood Post He Leak Check Date Area (inches) Depth ID (BC) ID Test (" Hg) Init He Purge Pass? Start Time Pressure End Pressure Init He Purge Pass? (inches) (%) (ppm) (<10%)* Time N (ppm) ( <30%) (FC) („ Hg) („ Hg) 9/10/2020 Boiler Room (S) 5.75 15 SG-1 2096 4353 -21.5 45.2 0 y 1631 -30 1640 -5 52.5 0 y 9/10/2020 Storage (SE) 5 12 SG-2 2112 4354 -25 50.4 0 y 1654 -30 1703 -5 48.4 0 y 9/10/2020 Storage(E) 5.75 12 SG-3 2235 4321 -21.5 49.4 25 y 1720 -30 1729 -5 45.8 0 y 9/10/2020 Storage (SW) 5.75 12 SG-4 2257 4337 -23 51.7 25 y 1746 -30 1755 -5 44.8 0 y 9/10/2020 Laundry Area (SE) 5.75 11.5 SG-5 2103 4211 -15 63.9 50 y 1808 -30 1817 -5 40.4 25 y 9/10/2020 Laundry Area (SE) 5.75 11.5 SG-5 DUP 2326 4211 -15 63.9 50 y 1808 -30 1817 -5 40.4 25 y 9/10/2020 Laundry Area 4.5 12 SG-6 2312 4253 -21.5 43.6 25 y 1830 -30 1839 -5 43.1 25 y (NE) 9/10/2020 Laundry Area 5.5 12 SG-7 2099 4348 -23 44.5 0 y 1856 -29 1905 -5 64.3 150 y (SW) 9/10/2020 Laundry Area 5.5 12 SG-8 2240 4347 -24 49.5 0 y 1920 -30 1929 -5 55 0 y (NW) NOTES: * NCDEQ Guidance considers a leak at 10% of hood helium concentration. 1% = 10,000 ppm Leak % = purge concentration (ppm) hood concentration (%) x 10,000 (ppm / %) TABLE 2 - COMPARISON OF LAB RESULTS TO NON-RESIDENTIAL SOIL GAS SCREENING LEVELS (NRSGSLs ) VAPOR INTRUSION SOIL GAS SAMPLING (9/10/2020) NATIONAL LINEN - WILMINGTON, INC NCBP PROJECT NO. 24028-20-065 RDHEC PROJECT NO. 2009.00 Residential SAMPLING LOCATION Parameter Soil Gas % of NRSGSL Screening SG-1 SG-2 SG-3 SG-4 SG-5 DUP SG-5 SG-6 SG-7 SG-8 of Max Levels Boiler Room(5) Storage (SE) Storage(E) Storage (SW) Laundry Area (SE) Laundry Area (SE) Laundry Area [NE) Laundry Area (SW) Laundry Area (NW) Detected iNRqrqLsi Sampling Date/Time ug/m3 9/10/2020 911012020 911012020 911012020 911012020 911012020 911012020 911012020 9/10/2020 Analyte 4:40 PM 5.03 PM 5.29 PM 5:55 PM 6.17 PM 6.17 PM 6.39 PM 7:05 PM 7:29 PM Acetone 2.70E+06 62 470 790 240 250 250 98 67 73 0.03% Benzene 1.60E+03 3.6 5.3 2.9 1.2 1.5 1.5 0.93 1.4 0.66 0.33% 2-Butanone(MEK) 4.40E+05 101 61 32 121 111 111 12J 8.11 6.1J 0.01% Chloroform 5.30E+02 6.2 4.5 1.1 50 130 130 1.9 12 1.0 24.53% Dichlorodifluoromethane (Freon 12) 8.80E+03 7.2 1200 130 43 19 19 7.0 79 12 13.64% 1,4-Dioxane 2.50E+03 ND (2.0) 8.8 ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) ND (2.0) NO (2.0) 0.35% Ethanol 260 1700 490 140 110 110 38 100 63 Ethyl Acetate 6.10E+03 ND (4.3) 39 ND (4.3) ND (4.3) ND (4.3) ND (4.3) ND (4.3) ND (4.3) ND (4.3) 0.64% Ethylbenzene 4.90E+03 17 13 9.7 8.2 11 14 7.9 4.7 6.1 0.35% 4-Ethyltoluene 30 6.7 6.2 6.8 9.8 9.8 8.1 ND (0.30) 5.3 Heptane 3.50E+04 5.2 4.2 3.3 2.1 1.9 1.8 ND (0.35) 1.7 ND (0.35) 0.01% Hexane 6.10E+04 ND (1.3) ND (1.3) 3.51 ND (1.3) ND (1.3) ND (1.3) ND (1.3) ND (1.3) ND (1.3) 0.57% Isopropanol 1.80E+04 7.61 73 240 30 34 34 13J 5.71 8.81 1.33% 4-Methyl-2-pentanone (MIBK) 2.60E+05 ND (0.43) 32 17 ND (0.43) ND (0.43) ND (0.43) ND (0.43) ND (0.43) ND (0.43) 0.01% Naphthalene 2.60E+02 ND (0.59) 5.7 3.4 6.3 13 3.7 3.9 3.7 3.2 5.00% Styrene 8.80E+04 1.3 2.3 0.751 ND (0.24) ND (0.24) ND (0.24) ND (0.24) ND (0.24) ND (0.24) 0.00% Tetrachloroethylene 3.50E+03 51 9.2 5.6 65 19 19 12 15 7.6 1.86% Toluene 4.40E+05 56 40 30 18 28 28 15 16 10 0.01% Trichloroethylene 1.80E+02 2.8 11 6.0 0.45 1 47 45 5.1 0.92 1 ND (0.40) 26.11% Trichlorofluoromethane 1.11 1.31 1.31 1.31 1.11 1.21 1.3J 1.41 1.91 1,2,4-Trimethylbenzene 5.30E+03 ND (0.22) ND (0.22) ND (0.22) ND (0.22) 38 ND (0.22) 36 ND (0.22) ND (0.22) 0.72% 1,3,5-Trimethylbenzene 5.30E+03 8.8 6.1 5.7 6.9 8.7 8.6 7.6 3.5 5.1 0.17% Xylene, m&p 8.80E+03 71 43 39 35 58 59 36 21 28 0.81% X lene, o- 8.80E+03 27 17 16 15 24 24 16 8.7 12 0.31% NOTES: 1. ND = Not detected above the lab reporting limits shown in parenthesis. 2. NT = Not tested. 3. -= No IHSB Residential or Non -Residential screening limits limits. 4. Red Shaded values exceed the IHSB Non -Residential Soil -Gas Screening Limits. S. IHSB Residential/Non-Residential screening limits displayed for Xylenes are for the summation of all isomers and not for the individual isomer. Cells for individual isomers might not be in italics, and/or shaded when the summation (total amount of all isomers) exceeds the limits for these parameters. User discretion is advised when interpreting these results. TABLE 3 - COMPARISON OF LAB RESULTS TO RESIDENTIAL SOIL GAS SCREENING LEVELS (RSGSLs ) VAPOR INTRUSION SOIL GAS SAMPLING (9/10/2020) NATIONAL LINEN - WILMINGTON, NC NCBP PROJECT NO. 24028-20-065 RDHEC PROJECT NO. 2009.00 Residential SAMPLING LOCATION Soil Gas Parameter Screening % of RSGSL Levels SG-1 SG-2 SG-3 SG-4 SG-5 DUP SG-5 SG-6 SG-7 SG-8 of Max (RSGSLs) Boiler Room(5) Storage (SE) Storage(E) Storage (SW) Laundry Area (SE) Laundry Area (SE) Laundry Area [NE) Laundry Area (SW) Laundry Area (NW) Detected Sampling Opte/Time ug/m' 9/10/2020 911012020 911012020 911012020 911012020 911012020 911012020 911012020 9/10/2020 Analyte 4:40 PM 5.03 PM 5.29 PM 5:55 PM 6.17 PM 6.17 PM 6.39 PM 7:05 PM 7:29 PM Acetone 220000 62 470 790 240 250 250 98 67 73 0.36% Benzene 120 3.6 5.3 2.9 1.2 1.5 1.5 0.93 1.4 0.66 4.42% 2-Butanone(MEK) 35000 101 61 32 12J 111 111 12J 8.11 6.1J 0.17% Chloroform 41 6.2 4.5 1.1 50 130 130 1.9 12 1.0 317.07% Dichlorodifluoromethane (Freon 12) 700 7.2 1200 130 43 19 19 7.0 79 12 171.43% 1,4-Dioxane 190 NO (2.0) 8.8 NO (2.0) NO (2.0) NO (2.0) NO (2.0) NO (2.0) NO (2.0) NO (2.0) 4.63% Ethanol 260 1700 490 140 110 110 38 100 63 Ethyl Acetate 490 NO (4.3) 39 NO (4.3) NO (4.3) NO (4.3) NO (4.3) ND (4.3) NO (4.3) NO (4.3) 7.96% Ethylbenzene 370 17 13 9.7 8.2 11 14 7.9 4.7 6.1 4.59% 4-Ethyltoluene 30 6.7 6.2 6.8 9.8 9.8 8.1 NO (0.30) 5.3 Heptane 2800 5.2 4.2 3.3 2.1 1.9 1.8 ND (0.35) 1.7 NO (0.35) 0.19% Hexane 4900 NO (1.3) NO (1.3) 3.51 NO (1.3) NO (1.3) NO (1.3) ND (1.3) NO (1.3) NO (1.3) 7.14% Isopropanol 1400 7.61 73 240 30 34 34 13 J 5.71 8.8 J 17.14% 4-Methyl-2-pentanone (MIBK) 21000 NO (0.43) 32 17 NO (0.43) NO (0.43) NO (0.43) ND (0.43) NO (0.43) NO (0.43) 0.15% Naphthalene 21 NO (0.59) 5.7 3.4 6.3 13 3.7 3.9 3.7 3.2 61.90% Styrene 7000 1.3 2.3 0.751 ND (0.24) NO (0.24) NO (0.24) NO (0.24) NO (0.24) NO (0.24) 0.03% Tetrachloroethylene 280 51 9.2 5.6 65 19 19 12 15 7.6 23.21% Toluene 35000 56 40 30 18 28 28 15 16 10 0.16% Trichloroethylene 14 2.8 11 6.0 0.451 47 45 5.1 0.921 NO (0.40) 335.71% Trichlorofluoromethane 1.11 1.31 1.31 1.31 1.11 1.21 1.3J 1.41 1.91 1,2,4-Trimethylbenzene 420 ND (0.22) ND (0.22) ND (0.22) ND (0.22) 38 NO (0.22) 36 ND (0.22) NO (0.22) 9.05% 1,3,5-Trimethylbenzene 420 8.8 6.1 5.7 6.9 8.7 8.6 7.6 3.5 5.1 2.10% Xylene, m&p 700 71 43 39 35 58 59 36 21 28 10.14% X lene, o- 700 27 17 16 15 24 24 16 8.7 12 3.86% NOTES: 1. NO = Not detected above the lab reporting limits shown in parenthesis. 2. NT = Not tested. 3. -= No IHSB Residential or Non -Residential screening limits limits. 4. Yellow Shaded values exceed the IHSB Residential Soil -Gas Screening Limits. S. Red Shaded values exceed the IHSB Non -Residential Soil -Gas Screening Limits. 6. IHSB Residential/Non-Residential screening limits displayed for Xylenes are for the summation of all isomers and not for the individual isomer. Cells for RDFr \1 Environmental Consulting 4012 Ridgebrook Bluffs Dr. I Raleigh, NC 27603 (919) 389-7747 1 info@rdhec.com DRAWINGS 11 I �N: 1 1pr, mid;lb �• �� or 1 7 _ i �:.. t ' 0 iSi ••1 ., - 1 A 1 R � # i � T • t s P il 0 -ANft r L, P. ■ in ' 1 R. DRAWN BY: DATE: OCT 2020 ��L TOPOGRAPHICAL SITE MAP DRAFTING CHECK fir, �" JOB N0: 2009.00 FORMER NATIONAL LINEN FACILITY 1315 SOUTH 5TH AVENUE BY: BYGINEER CHECK CAD # 2009-00-02 Environmental Consulting WILMINGTON, NEW HANOVER COUNTY, NC 28401 4012 Ridgehrook Bluffs Dr. i Raleigh, NC 27603 NCBF PROJECT NO: 24028-20-065 APPROVED (919) 389-7747 1 info@rdhec.com BY: 4�_ DWG NO: 2 REFERENCE: IMAGERY SOURCE - USGS 7.5 Minute Wilmington NC Quadrangle 2019, 5-Foot Contours, North American Datum of 1983 (NAD83), World Geodetic System 1984 (WGS84) C\jO CD O N p 00 O O O0 U po-cn Ln .., ICY w o — �Kidder� Li } I I ,a , M I I� a .. �� E �r a .. (.D z5-: 0- a- 5-1 0m c�m wM Qm I I 00 N Z g o _ > z Z I O Z > 00 — a J w Q O N O W Q J w �z200 F Z — -- - Z 2 ~ z ON w Q��wO Lv Z IY W Z W O O m C m Z Z_ d I _J m a � N to 3 O v — 0 _ - rtir�_a { -- R— .+, z e r ; m Z v O Ln w I C ° ac '_ I I jj; (APPROXIMATE) m v, � , W 0 30 60 > N z W SCALE: 1 "= 60 FT W Of W LL- W Of 0 0 ;t _;t N O 0 4� 0 N 00 0 •+ U N 1 � - "m 0 0 o 0 i IRONING &-LAUNDRY- SORTING o r-----.. z z 1 1 w 1 1 Z W LLJ > ---� SG-8 SG-6 :I i Z Q.. a.. �.. d.. j, ------- ----- ---------------- .-.------ .--.-.-.---- .-.-.---- .---- .-.-.----- .-. ------ .-.---- .®--- .--------- i 0 m o m W m Q m ry ' STORAGE MAIN LAUNDRY AREA W/VENTS AND EXHAUST HOODS o ---i ..,. ' :........x............................ ' 1 SG-3 00 N Z • 1 �® 0 cn 1 z J a 1 f ! j D Q w OI + W 1 i 1---SG 7 ........ ..:............................•---. ------------ SG-5 I ----- / . � I < w z= I w � 00 1 1 ♦DUP z �zQoo W � � z J N H = Q> O y 1 1 1 1 = z= 0 z a y 1 R i 1 o z Q = Q- LA w y 1 1 1 1 a cCi)zo=w 0 v Q � n z �LLJ a 0c/) ow zo m m �SG-2 v o .................................................: BOILER STORAGE z z o ROOM o t....................... SG-4..................; r a h.. i SG-1 z ................. STORAGE .................. : -r ® - Lu > n= i- -P_ my m p O 3 H .......�::1:�7::Sv'-'till'A'-F•::::.:�::::.3SSSS•CIS•`...�'S:::«-0:5:.:3�:i•.-.L22SS• � � � � �i aj v1 i i �-m D 2 L m a W u 1 U {D p e o LA LEGEND N m n uj _ SG-1 ® SOIL GAS SAMPLE LOCATION + _ _ 0 m 0 � � SG-5/ SOIL GAS SAMPLE LOCATION .r 0 (APPROXIMATE) 30 U WITH N o W ypUp DUPLICATE CANISTER SCALE: 1 "= 30 FT W ow� L1J L� W lY Ln O o N o 0 -+ RSGSLs Sample Location/ID C) O i Analyte (ug/m3) SG-2 SG-4 SG-5 SG-5 DUP O O i Chloroform 41 50 130 130 0 N IRON.ING.&.-LAUNDRY- SORTfNG.......... Dichlorodifluoromethane (Freon 12) 7DD 12DD p O ............................*................ Trichloroethylene 14 47 45 c_j Y Y r7 1 I U C) i ' _.. SG-8 SG-6 i i ' a . z a . Li> CD. a . ......--------------- ®------------------------------------------- ......................-®-------- --.-.1 O m 0 m W 0] Q 0] N ' STORAGE MAIN LAUNDRY AREA W/VENTS AND EXHAUST H ODS .. .........A................................................................................................, :: 1 � co N Z . _ 1 ® � o ; ; cn z z O a _ l E Z o y ;-...-...' SG-7 .............. ..-..-.. -. SG-5/ ; I aw�wo C� y ti 1 DUP o,xzQoCD y F . -�1 ..* i C9 J J 2 zN � w ~ u y 1 1 1 1 J J Ln C, a_ of z= o oz a y 1 1 1 1 } o Z � m Q V1 a y 1 1 1 1 tail LLJ o= w z Q g `0 r I KJ _ 0 =) z J m ro a Lu SG-2 OfZ cn m = o o m m C) C .................................................. BOILER STORAGE z Z `" c ROOM o cc .......................� ................ ... i SG-1 oge .... .............STORAGE .................. i -r ® Lu 1_ 0 2 o o a Lu V �- �y d t W CC o LEGEND ' i N _ m n } CK cu _ SG-1 ® SOIL GAS SAMPLE LOCATION SG-5/ SOIL GAS SAMPLE LOCATION y (APPROXIMATE) 0 15 30 t > r W U z WITH N yDUP DUPLICATE CANISTER SCALE: 1 "= 30 FT Lu � — W LL. W RDFr \1 Environmental Consulting 4012 Ridgebrook Bluffs Dr. I Raleigh, NC 27603 (919) 389-7747 1 info@rdhec.com APPENDIX A PHOTOGRAPHS (Click hyperlinks below to view photos online) 2020-09-10 National Linen Soil Gas Assessment RDFr \1 Environmental Consulting 4012 Ridgebrook Bluffs Dr. I Raleigh, NC 27603 (919) 389-7747 1 info@rdhec.com APPENDIX B NCDWM NON-RESIDENTIAL VAPOR INTRUSION SCREENING LEVELS TABLE (FEBRUARY 2018) North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.0E-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.0E-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 30560-19-1 Acephate 75-07-0 Acetaldehyde 2.9E+03 7.9E+02 N 5.6E+00 C 7.9E+00 N 7.9E+00 N Yes 34256-82-1 Acetochlor 67-64-1 Acetone 1.9E+07 2.7E+06 N 2.7E+04 N 2.7E+04 N 2.7E+04 N Yes 75-86-5 Acetone Cyanohydrin Not Volatile Not Volatile 1.8E+00 N 1.8E+00 N 1.8E+00 N Yes 75-05-8 Acetonitrile 3.7E+04 5.3E+03 N 5.3E+01 N 5.3E+01 N 5.3E+01 N Yes 98-86-2 Acetophenone 53-96-3 Acetylaminofluorene, 2- Not Volatile Not Volatile 9.4E-03 C 9.4E-02 C 9.4E-01 C 107-02-8 Acrolein 3.5E+00 1.8E+00 N 1.8E-02 N 1.8E-02 N 1.8E-02 N Yes 79-06-1 Acrylamide Not Volatile Not Volatile 1.2E-01 C 1.2E+00 C 5.3E+00 N Yes 79-10-7 Acrylic Acid 5.8E+04 8.8E+01 N 8.8E-01 N 8.8E-01 N 8.8E-01 N Yes 107-13-1 Acrylonitrile 3.1E+02 1.8E+02 N 1.8E-01 C 1.8E+00 N 1.8E+00 N Yes 111-69-3 Adiponitrile Not Volatile Not Volatile 5.3E+00 N 5.3E+00 N 5.3E+00 N Yes 15972-60-8 Alachlor 116-06-3 Aldicarb 1646-88-4 Aldicarb Sulfone 1646-87-3 Aldicarb sulfoxide 309-00-2 Aldrin 1.4E+01 2.5E+00 C 2.5E-03 C 2.5E-02 C 2.5E-01 C 107-18-6 Allyl Alcohol 4.3E+02 8.8E+00 N 8.8E-02 N 8.8E-02 N 8.8E-02 N Yes 107-05-1 Allyl Chloride 1.9E+00 8.8E+01 N 8.8E-01 N 8.8E-01 N 8.8E-01 N Yes 7429-90-5 Aluminum Not Volatile Not Volatile 4.4E+00 N 4.4E+00 N 4.4E+00 N Yes 20859-73-8 Aluminum Phosphide 834-12-8 Ametryn 92-67-1 Aminobiphenyl, 4- Not Volatile Not Volatile 2.0E-03 C 2.0E-02 C 2.0E-01 C 591-27-5 Aminophenol, m- 95-55-6 Aminophenol, o- 123-30-8 Aminophenol,p- 33089-61-1 Amitraz 766441-7 Ammonia 6.7E+05 4.4E+04 N 4.4E+02 N 4.4E+02 N 4.4E+02 N Yes 7773-06-0 Ammonium Sulfamate 75-85-4 Amyl Alcohol,tert- 4.7E+03 2.6E+02 N 2.6E+00 N 2.6E+00 N 2.6E+00 N Yes 62-53-3 Aniline Not Volatile Not Volatile 8.8E-01 N 8.8E-01 N 8.8E-01 N Yes 84-65-1 Anthraquinone, 9,10- 7440-36-0 Anfimony (metallic) 1314-60-9 Anfimony Pentoxide 1332-81-6 Anfimony Tetroxide 1309-64-4 Antimony Trioxide Not Volatile Not Volatile 1.8E-01 N 1.8E-01 N I 1.8E-01 N Yes 7440-38-2 Arsenic, Inorganic Not Volatile Not Volatile 2.9E-03 C 1.3E-02 N 1.3E-02 N Yes 778442-1 Arsine Not Volatile Not Volatile 4.4E-02 N 4.4E-02 N 4.4E-02 N Yes 3337-71-1 Asulam 1912-24-9 Atrazine 492-80-8 Auramine Not Volatile Not Volatile 4.9E-02 C 4.9E-01 C 4.9E+00 C 65195-55-3 Avermectm Bl 86-50-0 Azinphos-methyl Not Volatile Not Volatile 8.8E+00 N 8.8E+00 N 8.8E+00 N Yes 103-33-3 Azobenzene 7.2E+03 4.0E+02 C 4.0E-01 C 4.0E+00 C 4.0E+01 C 123-77-3 Azodicarbonamide Not Volatile Not Volatile 6.1E-03 N 6.1E-03 N 6.1E-03 N Yes 7440-39-3 Barium Not Volatile Not Volatile 4.4E-01 N 4.4E-01 N 4.4E-01 N Yes 186140-1 Benfluralin 17804-35-2 Benomyl 83055-99-6 Bensulfuron-methyl 25057-89-0 Bemazon 100-52-7 Benzaldehyde 7143-2 Benzene 6.9E+01 1.6E+03 C 1.6E+00 C 1.6E+01 C 2.6E+01 N Yes 6369-59-1 Benzenediamine-2-methyl sulfate, 1,4- 108-98-5 Benzenethiol 92-87-5 Benzidine Not Volatile Not Volatile 1.8E-04 C 1.8E-03 C 1.8E-02 C 65-85-0 Benzoic Acid 98-07-7 Benzotrichloride 100-51-6 Benzyl Alcohol 100-44-7 Benzyl Chloride 5.2E+01 8.8E+01 N 2.5E-01 C 8.8E-01 N 8.8E-01 N Yes 744041-7 Beryllium and compounds Not Volatile Not Volatile 5.1E-03 C 1.8E-02 N 1.8E-02 N Yes 42576-02-3 Bifenox 82657-04-3 Biphenthrin 92-52-4 Biphenyl, 1,1'- 2.8E+01 3.5E+01 N 3.5E-01 N 3.5E-01 N 3.5E-01 N Yes 108-60-1 Bis(2-chloro-1-methylethyl) ether 111-91-1 Bis(2-chloroethoxy)methane 111-44-4 Bis(2-chloroethyl)ether 5.3E+02 3.7E+01 C 3.7E-02 C 3.7E-01 C 3.7E+00 C 542-88-1 Bis(chloromethyl)ether 1.1E-02 2.0E-01 C 2.0E-04 C 2.0E-03 C 2.0E-02 C 80-05-7 Bisphenol A 744042-8 Boron And Berates Only Not Volatile Not Volatile 1.8E+01 N 1.8E+01 N 1.8E+01 N Yes 10294-34-5 Boron Trichloride 2.3E+01 1.8E+03 N 1.8E+01 N 1.8E+01 N 1.8E+01 N Yes 7637-07-2 Boron Trifluoride 1.1E+03 N 1.1E+01 N 1.1E+01 N 1.1E+01 N Yes 1554145-4 Bromate 107-04-0 Bromo-2-chloroethane, 1- 5.5E+00 2.0E+01 C 2.0E-02 C 2.0E-01 C 2.0E+00 C Page 1 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.oE-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.oE-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.oE-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 1073-06-9 Bromo-3-fluorobenzene,1- 460-00-4 Bromo-4-fluorobenzene,1- 108-86-1 Bromobenzene 5.2E+02 5.3E+03 N 5.3E+01 N 5.3E+01 N 5.3E+01 N Yes 74-97-5 Bromochloromethane 5.9E+02 3.5E+03 N 3.5E+01 N 3.5E+01 N 3.5E+01 N Yes 75-27-4 Bromodichloromethane 3.8E+01 3.3E+02 C 3.3E-01 C 3.3E+00 C 3.3E+01 C 75-25-2 Bromoform 5.1E+03 1.1E+04 C 1.1E+01 C 1.1E+02 C 1.1E+03 C 74-83-9 Bromomethane 1.5E+01 4.4E+02 N 4.4E+00 N 4.4E+00 N 4.4E+00 N Yes 2104-96-3 Bromophos 106-94-5 Bromopropane, 1- 2.9E+02 8.8E+03 N 8.8E+01 N 8.8E+01 N 8.8E+01 N Yes 1689-84-5 Bromoxynil 1689-99-2 Bromoxynil Octanoate 106-99-0 Butadiene, 1,3- 5.8E-01 1.8E+02 N 4.1E-01 C 1.8E+00 N 1.8E+00 N Yes 94-82-6 Butanoic acid, 4-(2,4-dichlorophenoxy)- 71-36-3 Butanol, N- 78-92-2 Butyl alcohol, sec- 7.1E+07 2.6E+06 N 2.6E+04 N 2.6E+04 N 2.6E+04 N Yes 200841-5 Butylate 25013-16-5 Butylated hydroxyanisole Not Volatile Not Volatile 2.2E+02 C 2.2E+03 C 2.2E+04 C 128-37-0 Butylated hydroxytoluene 104-51-8 Butylbenzene, n- 135-98-8 Butylbenzene,sec- 98-06-6 Butylbenzene, tert- 75-60-5 Cacodylic Acid 744043-9 Cadmium (Diet) Not Volatile Not Volatile 6.8E-03 C 8.8E-03 N 8.8E-03 N Yes 744043-9 Cadmium (Water) Not Volatile Not Volatile 6.8E-03 C 8.8E-03 N 8.8E-03 N Yes 105-60-2 Caprolactam Not Volatile Not Volatile 1.9E+00 N 1.9E+00 N 1.9E+00 N Yes 2425-06-1 Captafol Not Volatile Not Volatile 2.9E-01 C 2.9E+00 C 2.9E+O1 C 133-06-2 Captan Not Volatile Not Volatile 1.9E+01 C 1.9E+02 C 1.9E+03 C 63-25-2 Carbaryl 1563-66-2 Carbofaran 75-15-0 Carbon Disulfide 1.0E+03 6.1E+04 N 6.1E+02 N 6.1E+02 N 6.1E+02 N Yes 56-23-5 Carbon Tetrachloride 1.8E+01 2.0E+03 C 2.0E+00 C 2.0E+01 C 8.8E+01 N Yes 463-58-1 Carbonyl Sulfide 3.5E+00 8.8E+03 N 8.8E+01 N 8.8E+01 N 8.8E+01 N Yes 55285-14-8 Carbosulfan 5234-68-4 Carboxin 1306-38-3 Ceric oxide Not Volatile Not Volatile 7.9E-01 N 7.9E-01 N 7.9E-01 N Yes 302-17-0 Chloral Hydrate 133-90-4 Chloramben 118-75-2 Chloranil 12789-03-6 Chlordane 3.1E+02 6.1E+01 N 1.2E-01 C 6.1E-01 N 6.1E-01 N Yes 143-50-0 Chlordecone (Kepone) Not Volatile Not Volatile 2.7E-03 C 2.7E-02 C 2.7E-01 C 470-90-6 Chlorfenvinphos 90982-32-4 Chlorhnuron, Ethyl- 7782-50-5 Chlorine 2.7E-01 1.3E+01 N 1.3E-01 N 1.3E-01 N 1.3E-01 N Yes 10049-04-4 Chlorine Dioxide 1.1E-01 1.8E+01 N 1.8E-01 N 1.8E-01 N 1.8E-01 N Yes 7758-19-2 Chlorite (Sodium Salt) 75-68-3 Chloro-1,l-difluoroethane, 1- 1.8E+04 4.4E+06 N 4.4E+04 N 4.4E+04 N 4.4E+04 N Yes 126-99-8 Chloro-1,3-butadiene, 2- 1.8E-01 4.1E+01 C 4.1E-02 C 4.1E-01 C 4.1E+00 C Yes 3165-93-3 Chloro-2-methylaniline HCI, 4- 95-69-2 Chloro-2-methylaniline, 4- Not Volatile Not Volatile 1.6E-01 C 1.6E+00 C 1.6E+01 C 107-20-0 Chloroacetaldehyde, 2- 79-11-8 Chloroacetic Acid 532-27-4 Chloroacetophenone, 2- Not Volatile Not Volatile 2.6E-02 N 2.6E-02 N 2.6E-02 N Yes 10647-8 Chloroaniline, p- 108-90-7 Chlorobenzene 3.4E+02 4.4E+03 N 4.4E+O1 N 4.4E+O1 N 4.4E+O1 N Yes 98-66-8 Chlorobenzene sulfonic acid, p- 510-15-6 Chlorobenzilate Not Volatile Not Volatile 4.oE-01 C 4.0E+00 C 4.0E+01 C 74-11-3 Chlorobenzoic Acid, p- 98-56-6 Chlorobenzotrifluoride,4- 1.9E+02 2.6E+04 N 2.6E+02 N 2.6E+02 N 2.6E+02 N Yes 109-69-3 Chlorobutane, 1- 7545-6 Chlorodifluoromethane 2.6E+04 4.4E+06 N 4.4E+04 N 4.4E+04 N 4.4E+04 N Yes 107-07-3 Chloroethanol, 2- 67-66-3 Chloroform 3.6E+O1 5.3E+02 C 5.3E-01 C 5.3E+00 C 5.3E+01 C Yes 74-87-3 Chloromethane 2.2E+02 7.9E+03 N 7.9E+O1 N 7.9E+O1 N 7.9E+O1 N Yes 107-30-2 Chloromethyl Methyl Ether 1.4E+01 1.8E+01 C 1.8E-02 C 1.8E-01 C 1.8E+00 C 88-73-3 Chloronitrobenzene, o- Not Volatile Not Volatile 8.8E-03 N 8.8E-03 N 8.8E-03 N Yes 100-00-5 Chloronitrobenzene, p- Not Volatile Not Volatile 1.8E+00 N 1.8E+00 N 1.8E+00 N Yes 95-57-8 Chlorophenol, 2- 76-06-2 Chloropicrin 4.2E+00 3.5E+01 N 3.5E-01 N 3.5E-01 N 3.5E-01 N Yes 189745-6 Chlorothalonil Not Volatile Not Volatile 1.4E+O1 C 1.4E+02 C 1.4E+03 C 9549-8 Chlorotoluene, o- 10643-4 Chlorotoluene,p- 54749-90-5 Chlorozotocin Not Volatile Not Volatile 1.8E-04 C 1.8E-03 C 1.8E-02 C 101-21-3 Chlorpropham Page 2 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.oE-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.oE-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.oE-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 2921-88-2 Chlorpyrifos 5598-13-0 Chlorpyrifos Methyl 64902-72-3 Chlorsulfaron 1861-32-1 Chlorthal-dimethyl 60238-56-4 Chlorthiophos 16065-83-1 Chromium(IH), Insoluble Salts 18540-29-9 Chromium(VI) Not Volatile Not Volatile 1.5E-04 C 1.5E-03 C 1.5E-02 C Yes 744047-3 Chromium, Total 74115-24-5 Clofentezine 744048-4 Cobalt Not Volatile Not Volatile 1.4E-03 C 5.3E-03 N 5.3E-03 N Yes 800745-2 Coke Oven Emissions 4.4E-01 2.0E+01 C 2.0E-02 C 2.oE-01 C 2.0E+00 C 7440-50-8 Copper 108-39-4 Cresol, m- Not Volatile Not Volatile 5.3E+02 N 5.3E+02 N 5.3E+02 N Yes 9548-7 Cresol, o- Not Volatile Not Volatile 5.3E+02 N 5.3E+02 N 5.3E+02 N Yes 106-44-5 Cresol, p- Not Volatile Not Volatile 5.3E+02 N 5.3E+02 N 5.3E+02 N Yes 59-50-7 Cresol, p-chloro-m- 1319-77-3 Cresols Not Volatile Not Volatile 5.3E+02 N 5.3E+02 N 5.3E+02 N Yes 123-73-9 Crotonaldehyde, trans- 98-82-8 Cumene 7.5E+02 3.5E+04 N 3.5E+02 N 3.5E+02 N 3.5E+02 N Yes 135-20-6 Cupferron Not Volatile Not Volatile 1.9E-01 C 1.9E+00 C 1.9E+01 C 2172546-2 Cyanazine Cyanides 592-01-8 -Calcium Cyanide 544-92-3 -Copper Cyanide 57-12-5 -Cyanide (CN-) 1.7E+02 7.0E+01 N 7AE-01 N 7AE-01 N 7AE-01 N Yes 460-19-5 -Cyanogen 506-68-3 -Cyanogen Bromide 506-77-4 -Cyanogen Chloride 74-90-8 -Hydrogen Cyanide 1.3E+02 7.0E+01 N 7AE-01 N 7AE-01 N 7AE-01 N Yes 151-50-8 -Potassium Cyanide 506-61-6 -Potassium Silver Cyanide 506-64-9 -Silver Cyanide 143-33-9 -Sodium Cyanide E1790664 -Thiocyanates 463-56-9 -Thiocyanic Acid 557-21-1 -Zinc Cyanide 110-82-7 Cyclohexane 8.6E+02 5.3E+05 N 5.3E+03 N 5.3E+03 N 5.3E+03 N Yes 87-84-3 Cyclohexane, 1,2,3,4,5-pentabromo-6- chloro- 108-94-1 Cyclohexanone 1.7E+06 6.1E+04 N 6.1E+02 N 6.1E+02 N 6.1E+02 N Yes 110-83-8 Cyclohexee 4.7E+02 8.8E+04 N 8.8E+02 N 8.8E+02 N 8.8E+02 N Yes 108-91-8 Cyclohexylamine 68359-37-5 Cyfluthrm 68085-85-8 Cyhalothrin 52315-07-8 Cypennethrin 66215-27-8 Cyromazine 72-54-8 DDD, p,p'- (DDD) Not Volatile Not Volatile 1.8E-01 C 1.8E+00 C 1.8E+01 C 72-55-9 DDE, p,p'- 7.4E+02 1.3E+02 C 1.3E-01 C 1.3E+00 C 1.3E+01 C 50-29-3 DDT Not Volatile Not Volatile 1.3E-01 C 1.3E+00 C 1.3E+01 C 75-99-0 Dalapon 1596-84-5 Daminozide Not Volatile Not Volatile 2.4E+00 C 2.4E+O1 C 2.4E+02 C 1163-19-5 Decabromodiphenyl ether, 2,2',3,3',4,4',5,5',6,6'- (BDE-209) 806548-3 Demeton 103-23-1 Di(2-ethylhexyl)adipate 2303-16-4 Diallate 33341-5 Diazinon 132-65-0 Dibenzothiophene 96-12-8 Dibromo-3-chloropropane, 1,2- 3.4E+00 2.0E+00 C 2.0E-03 C 2.0E-02 C 1.8E-01 N Yes 108-36-1 Dibromobenzene, 1,3- 106-37-6 Dibromobenzene, 1,4- 12448-1 Dibromochloromethane 106-93-4 Dibromoethane, 1,2- 7.7E+00 2.0E+01 C 2.0E-02 C 2.oE-01 C 2.0E+00 C Yes 74-95-3 Dibromomethane (Methylene Bromide) 1.0E+02 3.5E+02 N 3.5E+00 N 3.5E+00 N 3.5E+00 N Yes E1790660 Dibutyltin Compounds 1918-00-9 Dicamba 76441-0 Dichloro-2-butene, 1,4- 8.4E-02 2.9E+00 C 2.9E-03 C 2.9E-02 C 2.9E-01 C 1476-11-5 Dichloro-2-butene, cis-1,4- 1.1E+00 2.9E+00 C 2.9E-03 C 2.9E-02 C 2.9E-01 C 110-57-6 Dichloro-2-butene, trans-1,4- 1.1E+00 2.9E+00 C 2.9E-03 C 2.9E-02 C 2.9E-01 C 7943-6 Dichloroacetic Acid 95-50-1 Dichlorobenzene, 1,2- 2.2E+03 1.8E+04 N 1.8E+02 N 1.8E+02 N 1.8E+02 N Yes 106-46-7 Dichlorobenzene, 1,4- 1.1E+02 1.1E+03 C 1.1E+00 C 1.1E+O1 C 1.1E+02 C Yes 91-94-1 Dichlorobenzidine, 3,3'- Not Volatile Not Volatile 3.6E-02 C 3.6E-01 C 3.6E+00 C Page 3 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.0E-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.0E-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 90-98-2 Dichlorobenzophenone, 4,4'- 75-71-8 Dichlorodifluoromethane 6.2E+00 8.8E+03 N 8.8E+01 N 8.8E+01 N 8.8E+01 N Yes 75-34-3 Dichloroethane, 1,1- 3.3E+02 7.7E+03 C 7.7E+00 C 7.7E+O1 C 7.7E+02 C 107-06-2 Dichloroethane, 1,2- 9.8E+01 4.7E+02 C 4.7E-01 C 4.7E+00 C 6.1E+00 N Yes 75-35-4 Dichloroethylene, 1,1- 1.6E+02 1.8E+04 N 1.8E+02 N 1.8E+02 N 1.8E+02 N Yes 156-59-2 Dichloroethylene, 1,2-cis- 156-60-5 Dichloroethylene, 1,2-trans- 120-83-2 Dichlorophenol, 2,4- 94-75-7 Dichlorophenoxy Acetic Acid, 2,4- 78-87-5 Dichloropropane, 1,2- 3.0E+01 3.5E+02 N 3.3E+00 C 3.5E+00 N 3.5E+00 N Yes 142-28-9 Dichloropropane, 1,3- 616-23-9 Dichloropropanol, 2,3- 542-75-6 Dichloropropene, 1,3- 1.2E+02 1.8E+03 N 3.1E+00 C 1.8E+01 N 1.8E+01 N Yes 62-73-7 Dichlorvos Not Volatile Not Volatile 1.5E-01 C 4.4E-01 N 4.4E-01 N Yes 141-66-2 Dicrotophos 77-73-6 Dicyclopentadiene 1.0E-01 2.6E+01 N 2.6E-01 N 2.6E-01 N 2.6E-01 N Yes 60-57-1 Dieldrin Not Volatile Not Volatile 2.7E-03 C 2.7E-02 C 2.7E-01 C E17136615 Diesel Engine Exhaust Not Volatile Not Volatile 4.1E-02 C 4.1E-01 C 4.1E+00 C Yes 11142-2 Diethanolamine Not Volatile Not Volatile 1.8E-01 N 1.8E-01 N 1.8E-01 N Yes 112-34-5 Diethylene Glycol Monobutyl Ether Not Volatile Not Volatile 8.8E-02 N 8.8E-02 N 8.8E-02 N Yes 111-90-0 Diethylene Glycol Monoethyl Ether Not Volatile Not Volatile 2.6E-01 N 2.6E-01 N 2.6E-01 N Yes 617-84-5 Diethylformamide 56-53-1 Diethylstilbestrol Not Volatile Not Volatile 1.2E-04 C 1.2E-03 C 1.2E-02 C 4322248-6 Difenzoquat 35367-38-5 Diflubenzuron 75-37-6 Difluoroethane, 1,1- 4.2E+04 3.5E+06 N 3.5E+04 N 3.5E+04 N 3.5E+04 N Yes 42045-1 Difluoropropane, 2,2- 1.3E+03 2.6E+06 N 2.6E+04 N 2.6E+04 N 2.6E+04 N Yes 94-58-6 Dihydrosafrole 1.9E+04 9.4E+02 C 9.4E-01 C 9.4E+00 C 9.4E+O1 C 108-20-3 Diisopropyl Ether 5.9E+03 6.1E+04 N 6.1E+02 N 6.1E+02 N 6.1E+02 N Yes 1445-75-6 Diisopropyl Methylphosphonate 55290-64-7 Dimethipin 60-51-5 Dimethoate 119-90-4 Dimethoxybenzidine,3,3'- 756-79-6 Dimethyl methylphosphonate 60-11-7 D methylamino azobenzene [p-] Not Volatile Not Volatile 9.4E-03 C 9.4E-02 C 9.4E-01 C 21436-96-4 Dimethylaniline HCI, 2,4- 95-68-1 Dimethylaniline, 2,4- 121-69-7 Dimethylaniline, N,N- 119-93-7 Dimethylbenzidine, 3,3'- 68-12-2 Dimethylformamide 8.7E+06 2.6E+03 N 2.6E+01 N 2.6E+01 N 2.6E+01 N Yes 57-14-7 Dimethylhydrazine, 1,1- 3.3E+00 1.8E-01 N 1.8E-03 N 1.8E-03 N 1.8E-03 N Yes 540-73-8 Dimethylhydrazine, 1,2- 2.7E+02 7.7E-02 C 7.7E-05 C 7.7E-04 C 7.7E-03 C 105-67-9 Dimethylphenol, 2,4- 576-26-1 Dimethylphenol, 2,6- 95-65-8 Dimethylphenol, 3,4- 513-37-1 Dimethylvinylchloride 1.9E+02 9.4E+02 C 9.4E-01 C 9.4E+00 C 9.4E+O1 C 534-52-1 Dinitro-o-cresol, 4,6- 131-89-5 Dinitro-o-cyclohexyl Phenol, 4,6- 528-29-0 Dinitrobenzene,l,2- 99-65-0 Dinitrobenzene,l,3- 100-25-4 Dinitrobenzene,l,4- 51-28-5 Dinitrophenol, 2,4- E1615210 Dinitrotoluene Mixture, 2,4/2,6- 121-14-2 Dinitrotoluene, 2,4- Not Volatile Not Volatile 1.4E-01 C 1.4E+00 C 1.4E+01 C 606-20-2 Dinitrotoluene, 2,6- 35572-78-2 Dinitrotoluene, 2-Amino4,6- 19406-51-0 Dinitrotoluene, 4-Amino-2,6- 25321-14-6 Dinitrotoluene, Technical grade 88-85-7 Dinoseb 123-91-1 Dioxane, 1,4- 1.3E+05 2.5E+03 C 2.5E+00 C 2.5E+01 C 2.6E+01 N Yes Dioxins -Hexachlorodibenzo-p-dioxin, Mixture Not Volatile Not Volatile 9.4E-06 C 9.4E-05 C 9.4E-04 C 1746-01-6 -TCDD, 2,3,7,8- 1.6E-03 3.2E-04 C 3.2E-07 C 3.2E-06 C 3.2E-05 C Yes 957-51-7 Diphenamid 101-84-8 Diphenyl Ether 3.1E+01 3.5E+01 N 3.5E-01 N 3.5E-01 N 3.5E-01 N Yes 127-63-9 Diphenyl Sulfone 122-39-4 Diphenylamine 122-66-7 Diphenylhydrazine, 1,2- Not Volatile Not Volatile 5.6E-02 C 5.6E-01 C 5.6E+00 C 85-00-7 Diquat 1937-37-7 Direct Black 38 Not Volatile Not Volatile 8.8E-05 C 8.8E-04 C 8.8E-03 C 260246-2 Direct Blue 6 Not Volatile Not Volatile 8.8E-05 C 8.8E-04 C 8.8E-03 C 16071-86-6 Direct Brown 95 Not Volatile Not Volatile 8.8E-05 C 8.8E-04 C 8.8E-03 C 298-04-4 Disulfoton Page 4 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.0E-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.0E-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 505-29-3 Dithiane, 1,4- 330-54-1 Diuron 2439-10-3 Dodine 759-94-4 EPTC 115-29-7 Endosulfan 145-73-3 Endothall 72-20-8 Endrin 106-89-8 Epichlorohydrin 7.0E+02 8.8E+01 N 8.8E-01 N 8.8E-01 N 8.8E-01 N Yes 106-88-7 Epoxybutane,l,2- 2.4E+03 1.8E+03 N 1.8E+01 N 1.8E+01 N 1.8E+01 N Yes 111-77-3 Ethanol, 2-(2-methoxyethoxy)- 16672-87-0 Ethephon 563-12-2 Ethion 111-15-9 Ethoxyethanol Acetate, 2- 4.0E+05 5.3E+03 N 5.3E+01 N 5.3E+01 N 5.3E+01 N Yes 110-80-5 Ethoxyethanol, 2- 9.1E+06 1.8E+04 N 1.8E+02 N 1.8E+02 N 1.8E+02 N Yes 141-78-6 Ethyl Acetate 1.1E+04 6.1E+03 N 6.1E+01 N 6.1E+01 N 6.1E+01 N Yes 140-88-5 Ethyl Acrylate 5.1E+02 7.0E+02 N 7.0E+00 N 7.0E+00 N 7.0E+00 N Yes 75-00-3 Ethyl Chloride (Chloroethane) 1.9E+04 8.8E+05 N 8.8E+03 N 8.8E+03 N 8.8E+03 N Yes 60-29-7 Ethyl Ether 97-63-2 Ethyl Methacrylate 1.1E+04 2.6E+04 N 2.6E+02 N 2.6E+02 N 2.6E+02 N Yes 2104-64-5 Ethyl-p-nitrophenyl Phosphonate 10041-4 Ethylbenzene 1.5E+02 4.9E+03 C 4.9E+00 C 4.9E+O1 C 4.9E+02 C Yes 109-78-4 Ethylene Cyanohydrin 107-15-3 Ethylene Dianne 107-21-1 Ethylene Glycol Not Volatile Not Volatile 3.5E+02 N 3.5E+02 N 3.5E+02 N Yes 111-76-2 Ethylene Glycol Monobutyl Ether Not Volatile Not Volatile 1.4E+03 N 1.4E+03 N 1.4E+03 N Yes 75-21-8 Ethylene Oxide 6.8E+00 4.1E+00 C 4.1E-03 C 4.1E-02 C 4.1E-01 C Yes 9645-7 Ethylene Thiourea Not Volatile Not Volatile 9.4E-01 C 9.4E+00 C 9.4E+O1 C 151-56-4 Ethyleneimine 1.3E+01 6.5E-01 C 6.5E-04 C 6.5E-03 C 6.5E-02 C 84-72-0 Ethylphthalyl Ethyl Glycolate 22224-92-6 Fenamiphos 3951541-8 Fenpropathrin 51630-58-1 Fenvalerate 2164-17-2 Fluometuron 1698448-8 Fluoride Not Volatile Not Volatile 1.1E+01 N 1.1E+01 N 1.1E+01 N Yes 778241-4 Fluorine (Soluble Fluoride) Not Volatile Not Volatile 1.1E+01 N 1.1E+01 N 1.1E+01 N Yes 59756-60-4 Fluridone 56425-91-3 Flurprimidol 85509-19-9 Flusilazole 66332-96-5 Flutolanil 69409-94-5 Fluvalinate 133-07-3 Folpet 72178-02-0 Fomesafen 944-22-9 Fonofos 50-00-0 Formaldehyde 6.2E+05 8.6E+02 N 9.4E-01 C 8.6E+00 N 8.6E+00 N Yes 64-18-6 Formic Acid 3.8E+04 2.6E+O1 N 2.6E-01 N 2.6E-01 N 2.6E-01 N Yes 39148-24-8 Fosetyl-AL Furans 132-64-9 -Dibenzofuran 110-00-9 -Furan 109-99-9 -Tetrahydrofaran 6.1E+05 1.8E+05 N 1.8E+03 N 1.8E+03 N 1.8E+03 N Yes 6745-8 Furazolidone 98-01-1 Furfural 2.8E+05 4.4E+03 N 4.4E+01 N 4.4E+01 N 4.4E+01 N Yes 531-82-8 Furium Not Volatile Not Volatile 2.9E-02 C 2.9E-01 C 2.9E+00 C 60568-05-0 Furmecyclox Not Volatile Not Volatile 1.4E+00 C 1.4E+01 C 1.4E+02 C 77182-82-2 Glufosinate, Ammonium 111-30-8 Glutaraldehyde Not Volatile Not Volatile 7.0E-02 N 7.0E-02 N 7.0E-02 N Yes 765-34-4 Glycidyl 4.2E+04 8.8E+01 N 8.8E-01 N 8.8E-01 N 8.8E-01 N Yes 1071-83-6 Glyphosate 113-00-8 Guanidine 50-01-1 Guanidine Chloride 506-93-4 Guanidine Nitrate 6980640-2 Haloxyfop, Methyl 76-44-8 Heptachlor 7.8E+00 9.4E+00 C 9.4E-03 C 9.4E-02 C 9.4E-01 C 1024-57-3 Heptachlor Epoxide 5.5E+01 4.7E+00 C 4.7E-03 C 4.7E-02 C 4.7E-01 C 111-71-7 Heptanal,n- 2.4E+02 2.6E+02 N 2.6E+00 N 2.6E+00 N 2.6E+00 N Yes 142-82-5 Heptane, N- 4.3E+00 3.5E+04 N 3.5E+02 N 3.5E+02 N 3.5E+02 N Yes 87-82-1 Hexabromobenzene 6863149-2 Hexabromodiphenyl ether, 2,2',4,4',5,5'- (BDE-153) 118-74-1 Hexachlorobenzene 3.8E+00 2.7E+01 C 2.7E-02 C 2.7E-01 C 2.7E+00 C 87-68-3 Hexachlorobutadiene 1.3E+01 5.6E+02 C 5.6E-01 C 5.6E+00 C 5.6E+O1 C 319-84-6 Hexachlorocyclohexane, Alpha- Not Volatile Not Volatile 6.8E-03 C 6.8E-02 C 6.8E-01 C 319-85-7 Hexachlorocyclohexane, Beta- Not Volatile Not Volatile 2.3E-02 C 2.3E-01 C 2.3E+00 C Page 5 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.oE-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.oE-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.oE-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 58-89-9 Hexachlorocyclohexane, Gamma- (Lindane) Not Volatile Not Volatile 4.0E-02 C 4.oE-01 C 4.0E+00 C 608-73-1 Hexachlorocyclohexane, Technical Not Volatile Not Volatile 2.4E-02 C 2.4E-01 C 2.4E+00 C 7747-4 Hexachlorocyclopentadiene 1.6E-01 1.8E+01 N 1.8E-01 N 1.8E-01 N 1.8E-01 N Yes 67-72-1 Hexachloroethane 7.0E+01 1.1E+03 C 1.1E+00 C 1.1E+01 C 2.6E+01 N Yes 70-30-4 Hexachlorophene 121-82-4 Hexahydro- 1,3,5 -trinitro- 1,3,5 -triazine (RDX) 822-06-0 Hexamethylene Diisocyanate, 1,6- 4.5E+00 8.8E-01 N 8.8E-03 N 8.8E-03 N 8.8E-03 N Yes 680-31-9 Hexamethylphosphoramide 110-54-3 Hexane, N- 8.3E+00 6.1E+04 N 6.1E+02 N 6.1E+02 N 6.1E+02 N Yes 124-04-9 Hexanedioic Acid 591-78-6 Hexanone,2- 6.9E+03 2.6E+03 N 2.6E+O1 N 2.6E+O1 N 2.6E+O1 N Yes 51235-04-2 Hexazinone 78587-05-0 Hexythiazox 67485-29-4 Hydramethylnon 302-01-2 Hydrazine 1.0E+03 2.5E+00 C 2.5E-03 C 2.5E-02 C 2.6E-02 N Yes 10034-93-2 Hydrazine Sulfate Not Volatile Not Volatile 2.5E-03 C 2.5E-02 C 2.5E-01 C 7647-01-0 Hydrogen Chloride 2.1E-07 1.8E+03 N 1.8E+01 N 1.8E+01 N 1.8E+01 N Yes 7664-39-3 Hydrogen Fluoride 2.9E+03 1.2E+03 N 1.2E+01 N 1.2E+01 N 1.2E+01 N Yes 7783-06-4 Hydrogen Sulfide 5.0E+00 1.8E+02 N 1.8E+00 N 1.8E+00 N 1.8E+00 N Yes 123-31-9 Hydroquinone 35554-44-0 Imazalil 81335-37-7 Imazaquin 81335-77-5 Imazethapyr 7553-56-2 Iodine 36734-19-7 Iprodione 7439-89-6 Iron 78-83-1 Isobutyl Alcohol 78-59-1 Isophorone Not Volatile Not Volatile 1.8E+03 N 1.8E+03 N 1.8E+03 N Yes 33820-53-0 Isopropalin 67-63-0 Isopropanol 5.3E+05 1.8E+04 N 1.8E+02 N 1.8E+02 N 1.8E+02 N Yes 1832-54-8 Isopropyl Methyl Phosphonic Acid 82558-50-7 Isoxaben E1737665 JP-7 6.4E+02 2.6E+04 N 2.6E+02 N 2.6E+02 N 2.6E+02 N Yes 77501-63-4 Lactofen 78-97-7 Lactonitrile Lead Compounds 7446-27-7 -Lead Phosphate Not Volatile Not Volatile 1.0E+00 C 1.0E+01 C 1.0E+02 C 301-04-2 -Lead acetate Not Volatile Not Volatile 1.0E+00 C 1.0E+01 C 1.0E+02 C 7439-92-1 Lead and Compounds Not Volatile Not Volatile 1.5E-01 N 1.5E-01 N 1.5E-01 N Yes 1335-32-6 -Lead subacetate Not Volatile Not Volatile 1.0E+00 C 1.0E+01 C 1.0E+02 C 78-00-2 -Tetraethyl Lead 541-25-3 Lewisite 330-55-2 Linuron 7439-93-2 Lithium 94-74-6 MCPA 94-81-5 MCPB 93-65-2 MCPP 121-75-5 Malathion 108-31-6 Maleic Anhydride Not Volatile Not Volatile 6.1E-01 N 6.1E-01 N 6.1E-01 N Yes 123-33-1 Maleic Hydrazide 109-77-3 Malononitrile 8018-01-7 Mancozeb 12427-38-2 Maneb 7439-96-5 Manganese (Diet) Not Volatile Not Volatile 4.4E-02 N 4.4E-02 N 4.4E-02 N Yes 7439-96-5 Manganese (Non -diet) Not Volatile Not Volatile 4.4E-02 N 4.4E-02 N 4.4E-02 N Yes 950-10-7 Mephosfolan 24307-26-4 Mepiquat Chloride 149-30-4 Mercaptobenzothiazole,2- Mercury Compounds 7487 94 7 --Mercuric Chloride (and other Mercury salts) Not Volatile Not Volatile 2.6E-01 N 2.6E-01 N 2.6E-01 N Yes 7439-97-6 -Mercury (elemental) 7.5E-01 2.6E+O1 N 2.6E-01 N 2.6E-01 N 2.6E-01 N Yes 22967-92-6 -Methyl Mercury 62-38-4 -Phenyhnercuric Acetate 150-50-5 Merphos 7848-8 Merphos Oxide 57837-19-1 Metalaxyl 126-98-7 Methacrylonitrile 2.6E+03 2.6E+03 N 2.6E+01 N 2.6E+01 N 2.6E+01 N Yes 10265-92-6 Methamidophos 67-56-1 Methanol 9.4E+07 1.8E+06 N 1.8E+04 N 1.8E+04 N 1.8E+04 N Yes 950-37-8 Methidathion 16752-77-5 Methomyl Page 6 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.0E-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.0E-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 99-59-2 Methoxy-5-nitroaniline, 2- Not Volatile Not Volatile 8.8E-01 C 8.8E+00 C 8.8E+01 C 7243-5 Methoxychlor 11049-6 Methoxyethanol Acetate, 2- 6.9E+04 8.8E+01 N 8.8E-01 N 8.8E-01 N 8.8E-01 N Yes 109-86-4 Methoxyethanol,2- 1.3E+06 1.8E+03 N 1.8E+01 N 1.8E+01 N 1.8E+01 N Yes 79-20-9 Methyl Acetate 96-33-3 Methyl Acrylate 2.2E+03 1.8E+03 N 1.8E+01 N 1.8E+01 N 1.8E+01 N Yes 78-93-3 Methyl Ethyl Ketone (2-Butanone) 1.9E+06 4.4E+05 N 4.4E+03 N 4.4E+03 N 4.4E+03 N Yes 60-34-4 Methyl Hydrazine 1.4E+02 1.8E+00 N 1.2E-02 C 1.8E-02 N 1.8E-02 N Yes 108-10-1 Methyl Isobutyl Ketone (4-methyl-2- pentanone) 4,7E+05 2.6E+05 N 2.6E+03 N 2.6E+03 N 2.6E+03 N Yes 624-83-9 Methyl Isocyanate 2.3E+01 8.8E+01 N 8.8E-01 N 8.8E-01 N 8.8E-01 N Yes 80-62-6 Methyl Methacrylate 4.7E+04 6.1E+04 N 6.1E+02 N 6.1E+02 N 6.1E+02 N Yes 298-00-0 Methyl Parathion 993-13-5 Methyl Phosphonic Acid 25013-15-4 Methyl Styrene (Mixed Isomers) 3.3E+02 3.5E+03 N 3.5E+01 N 3.5E+01 N 3.5E+01 N Yes 66-27-3 Methyl methanesulfonate Not Volatile Not Volatile 4.4E-01 C 4.4E+00 C 4.4E+O1 C 1634-04-4 Methyl tert-Butyl Ether (MTBE) 2.0E+04 4.7E+04 C 4.7E+01 C 4.7E+02 C 2.6E+03 N Yes 61545-2 Methyl-1,4-benzenediamine dihydrochloride, 2- 108-11-2 Methyl-2-Pentanol, 4- 1.4E+06 2.6E+05 N 2.6E+03 N 2.6E+03 N 2.6E+03 N Yes 99-55-8 Methyl-5-Nitroaniline, 2- 70-25-7 Methyl-N-nitro-N-nitrosoguanidine, N- Not Volatile Not Volatile 5.1E-03 C 5.1E-02 C 5.1E-01 C 636-21-5 Methylaniline Hydrochloride, 2- Not Volatile Not Volatile 3.3E-01 C 3.3E+00 C 3.3E+01 C 124-58-3 Methylarsonic acid 74612-12-7 Methylbenzene,I 4-diamine monohydrochloride, 2- 615-50-9 Methylbenzene-1,4-diamine sulfate, 2- 5649-5 Methylcholanthrene, 3- Not Volatile Not Volatile 1.9E-03 C 1.9E-02 C 1.9E-01 C 75-09-2 Methylene Chloride 4.0E+03 5.3E+04 N 5.3E+02 N 5.3E+02 N 5.3E+02 N Yes 101-14-4 Methylene-bis(2-chloroaniline), 4,4'- Not Volatile Not Volatile 2.9E-02 C 2.9E-01 C 2.9E+00 C 101-61-1 Methylene-bis(N,N-dimethyl) Aniline, 4,4'- Not Volatile Not Volatile 9.4E-01 C 9.4E+00 C 9.4E+O1 C 101-77-9 Methylenebisbenzenamine, 4,4'- Not Volatile Not Volatile 2.7E-02 C 2.7E-01 C 2.7E+00 C Yes 101-68-8 Methylenediphenyl Diisocyanate Not Volatile Not Volatile 5.3E-01 N 5.3E-01 N 5.3E-01 N Yes 98-83-9 Methylstyrene, Alpha- 5121845-2 Metolachlor 21087-64-9 Metribuzin 74223-64-6 Metsulf iron -methyl 8012-95-1 Mineral oils 2385-85-5 Mirex 7.3E-01 2.4E+00 C 2.4E-03 C 2.4E-02 C 2.4E-01 C 2212-67-1 Molinate 7439-98-7 Molybdenum 10599-90-3 Monochloramine 100-61-8 Monomethylaniline 88671-89-0 Myclobutanil 74-31-7 N,M-Diphenyl-1,4-benzenediamine 300-76-5 Naled 64742-95-6 Naphtha, High Flash Aromatic (HFAN) 4.9E+03 8.8E+03 N 8.8E+01 N 8.8E+01 N 8.8E+01 N Yes 91-59-8 Naphthylamine, 2- 15299-99-7 Napropamide 373-02-4 Nickel Acetate Not Volatile Not Volatile 1.2E-02 N 1.2E-02 N 1.2E-02 N Yes 3333-67-3 Nickel Carbonate Not Volatile Not Volatile 1.2E-02 N 1.2E-02 N 1.2E-02 N Yes 13463-39-3 Nickel Carbonyl 6.0E-04 1.2E+00 N 1.2E-02 N 1.2E-02 N 1.2E-02 N Yes 1205448-7 Nickel Hydroxide Not Volatile Not Volatile 1.2E-02 N 1.2E-02 N 1.2E-02 N Yes 1313-99-1 Nickel Oxide Not Volatile Not Volatile 1.8E-02 N 1.8E-02 N 1.8E-02 N Yes E715532 Nickel Refinery Dust Not Volatile Not Volatile 1.2E-02 N 1.2E-02 N 1.2E-02 N Yes 7440-02-0 Nickel Soluble Salts Not Volatile Not Volatile 4.7E-02 C 7.9E-02 N 7.9E-02 N Yes 12035-72-2 Nickel Subsulfide Not Volatile Not Volatile 1.2E-02 N 1.2E-02 N 1.2E-02 N Yes 1271-28-9 Nickelocene Not Volatile Not Volatile 1.2E-02 N 1.2E-02 N 1.2E-02 N Yes 14797-55-8 Nitrate E701177 Nitrate +Nitrite (as N) 14797-65-0 Nitrite 88-74-4 Nitroaniline, 2- Not Volatile Not Volatile 4.4E-02 N 4.4E-02 N 4.4E-02 N Yes 100-01-6 Nitroaniline, 4- Not Volatile Not Volatile 5.3E+00 N 5.3E+00 N 5.3E+00 N Yes 98-95-3 Nitrobenzene 3.1E+03 3.1E+02 C 3.1E-01 C 3.1E+00 C 7.9E+00 N Yes 9004-70-0 Nitrocellulose 67-20-9 Nitrofurantoin 59-87-0 Nitrofurazone Not Volatile Not Volatile 3.3E-02 C 3.3E-01 C 3.3E+00 C 55-63-0 Nitroglycerin 556-88-7 Nitroguanidine 75-52-5 Nitromethane 3.7E+03 4.4E+02 N 1.4E+00 C 4.4E+00 N 4.4E+00 N Yes 7946-9 Nitropropane, 2- 9.3E+00 4.5E+00 C 4.5E-03 C 4.5E-02 C 4.5E-01 C Yes 759-73-9 Nitroso-N-ethylurea, N- Not Volatile Not Volatile 1.6E-03 C 1.6E-02 C 1.6E-01 C Page 7 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.0E-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.0E-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 684-93-5 Nitroso-N-methylurea, N- Not Volatile Not Volatile 3.6E-04 C 3.6E-03 C 3.6E-02 C 924-16-3 Nitroso-di-N-butylamine, N- 1.4E+02 7.7E+00 C 7.7E-03 C 7.7E-02 C 7.7E-01 C 621-64-7 Nitroso-di-N-propylamine, N- Not Volatile Not Volatile 6.1E-03 C 6.1E-02 C 6.1E-01 C 1116-54-7 Nitrosodiethanolamine, N- Not Volatile Not Volatile 1.5E-02 C 1.5E-01 C 1.5E+00 C 55-18-5 Nitrosodiethylamine, N- Not Volatile Not Volatile 2.9E-04 C 2.9E-03 C 2.9E-02 C 62-75-9 Nitrosodimethylamine, N- 1.2E+02 8.8E-01 C 8.8E-04 C 8.8E-03 C 3.5E-02 N Yes 86-30-6 Nitrosodiphenylamine, N- Not Volatile Not Volatile 4.7E+00 C 4.7E+O1 C 4.7E+02 C 10595-95-6 Nitrosomethylethylamine, N- 3.3E+02 1.9E+00 C 1.9E-03 C 1.9E-02 C 1.9E-01 C 59-89-2 Nitrosomorpholine [N-] Not Volatile Not Volatile 6.5E-03 C 6.5E-02 C 6.5E-01 C 100-75-4 Nitrosopiperidine [N-] Not Volatile Not Volatile 4.5E-03 C 4.5E-02 C 4.5E-01 C 930-55-2 Nitrosopyrrolidine, N- Not Volatile Not Volatile 2.0E-02 C 2.0E-01 C 2.0E+00 C 99-08-1 Nitrotoluene, m- 88-72-2 Nitrotoluene, o- 99-99-0 Nitrotoluene, p- 111-84-2 Nonane, n- 1.3E-01 1.8E+03 N 1.8E+01 N 1.8E+01 N 1.8E+01 N Yes 27314-13-2 Norflurazon 32536-52-0 Octabromodiphenyl Ether 269141-0 Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX) 152-16-9 Octamethylpyrophosphoramide 19044-88-3 Oryzalin 19666-30-9 Oxadiazon 23135-22-0 Oxamyl 42874-03-3 Oxytluorfen 76738-62-0 Paclobutrazol 191042-5 Paraquat Dichloride 56-38-2 Parathion 1114-71-2 Pebulate 4048742-1 Pendimethalin 32534-81-9 Pentabromodiphenyl Ether 60348-60-9 Pentabromodiphenyl ether, 2,2',4,4',5- (BDE-99) 608-93-5 Pentachlorobenzene 76-01-7 Pentachloroethane 82-68-8 Pentachloronitrobenzene 87-86-5 Pentachlorophenol Not Volatile Not Volatile 2.4E+00 C 2.4E+01 C 2.4E+02 C 78-11-5 Pentaerythritol tenar itrate (PETN) 109-66-0 Pentane,n- 1.7E+01 8.8E+04 N 8.8E+02 N 8.8E+02 N 8.8E+02 N Yes Perchlorates 7790-98-9 -Ammonium Perchlorate 7791-03-9 -Lithium Perchlorate 14797-73-0 -Perchlorate and Perchlorate Salts 7778-74-7 -Potassium Perchlorate 7601-89-0 -Sodium Perchlorate 375-73-5 Perfluorobutane sulfuric acid (PFBS) 45187-15-3 Perfluorobutanesulfonate 52645-53-1 Permethrin 62-44-2 Phenacetin Not Volatile Not Volatile 1.9E+01 C 1.9E+02 C 1.9E+03 C 13684-63-4 Phenmedipham 108-95-2 Phenol Not Volatile Not Volatile 1.8E+02 N 1.8E+02 N 1.8E+02 N Yes 114-26-1 Phenol, 2-(I-methylethoxy)-, methylcarbamate 92-84-2 Phenothiazine 103-72-0 Phenyl Isothiocyanate 10845-2 Phenylenediam ne, m- 95-54-5 Phenylenediamine, o- 106-50-3 Phenylenediamine, p- 9043-7 Phenylphenol, 2- 298-02-2 Phorate 75-44-5 Phosgene 3.8E-01 2.6E+01 N 2.6E-01 N 2.6E-01 N 2.6E-01 N Yes 732-11-6 Phosmet Phosphates, Inorganic 13776-88-0 -Aluminum metaphosphate 68333-79-9 -Ammonium polyphosphate 7790-76-3 -Calcium pyrophosphate 7783-28-0 -Diammonium phosphate 7757-93-9 -Dicalcium phosphate 7782-75-4 -Dimagnesium phosphate 7758-11-4 -Dipotassium phosphate 7558-79-4 -Disodium phosphate 13530-50-2 -Monoaluminum phosphate 7722-76-1 -Monoammonium phosphate 7758-23-8 -Monocalcium phosphate 7757-86-0 -Monomagnesium phosphate Page 8 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.oE-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.oE-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.oE-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 7778-77-0 -Monopotassium phosphate 7558-80-7 -Monosodium phosphate 8017-16-1 -Polyphosphoric acid 13845-36-8 -Potassium tripolyphosphate 7758-16-9 -Sodium acid pyrophosphate 7785-88-8 Sodium aluminum phosphate (acidic) 10279-59-1 --Sodium aluminum phosphate (anhydrous) 10305-76-7 -Sodium aluminum phosphate (tetrahydrate) 10124-56-8 -Sodium hexametaphosphate 68915-31-1 -Sodium polyphosphate 7785-84-4 -Sodium trimetaphosphate 7758-29-4 -Sodium tripolyphosphate 7320-34-5 -Tetrapotassium phosphate 7722-88-5 -Tetrasodium pyrophosphate 15136-87-5 -Trialuminum sodium tetra decahydrogenoctaorthophosphate (dehydrate) 7758-87-4 -Tricalcium phosphate 7757-87-1 -Trimagnesium phosphate 7778-53-2 -Tripotassium phosphate 7601-54-9 -Trisodeum phosphate 7803-51-2 Phosphine 2.6E-01 2.6E+O1 N 2.6E-01 N 2.6E-01 N 2.6E-01 N Yes 7664-38-2 Phosphoric Acid Not Volatile Not Volatile 8.8E+00 N 8.8E+00 N 8.8E+00 N Yes 7723-14-0 Phosphorus, White Phthalates 117-81-7 -Bis(2-ethylhexyl)phthalate Not Volatile Not Volatile 5.1E+00 C 5.1E+01 C 5.1E+02 C 85-68-7 -Butyl Benzyl Phthalate 85-70-1 -Butylphthalyl Butylglycolate 84-74-2 -Dibutyl Phthalate 84-66-2 -Diethyl Phthalate 120-61-6 -Dimethylterephthalate 117-84-0 -Octyl Phthalate, de-N- 100-21-0 -Phthalic Acid, P- 85-44-9 -Phthalic Anhydride Not Volatile Not Volatile 1.8E+01 N 1.8E+01 N 1.8E+01 N Yes 1918-02-1 Picloram 96-91-3 Picramic Acid (2-Amino-4,6- dinitrophenol) 88-89-1 Picric Acid (2,4,6-Trinitrophenol) 29232-93-7 Pirimiphos, Methyl 59536-65-1 Polybrominated Biphenyls Not Volatile Not Volatile 1.4E-03 C 1.4E-02 C 1.4E-01 C Polychlorinated Biphenyls (PCBs) 12674-11-2 -Aroclor1016 7.5E+02 6.1E+02 C 6.1E-01 C 6.1E+00 C 6.1E+01 C 11104-28-2 -Aroclor1221 2.3E+01 2.2E+01 C 2.2E-02 C 2.2E-01 C 2.2E+00 C 11141-16-5 -Aroclor1232 7.2E+00 2.2E+01 C 2.2E-02 C 2.2E-01 C 2.2E+00 C 53469-21-9 -Aroclor1242 1.5E+01 2.2E+01 C 2.2E-02 C 2.2E-01 C 2.2E+00 C 12672-29-6 -Aroclor1248 1.2E+01 2.2E+01 C 2.2E-02 C 2.2E-01 C 2.2E+00 C 11097-69-1 -Aroclor1254 1.9E+01 2.2E+01 C 2.2E-02 C 2.2E-01 C 2.2E+00 C 11096-82-5 -Aroclor1260 1.6E+01 2.2E+01 C 2.2E-02 C 2.2E-01 C 2.2E+00 C 1112642-4 -Aroclor5460 39635-31-9 --Heptachlorobiphenyl, 2,3,3',4,4',5,5'- (PCB 189) 5.4E+01 1.1E+01 C 1.1E-02 C 1.1E-01 C 1.1E+00 C Yes 52663-72-6 --Hexachlorobiphenyl, 2,3',4,4',5,5'- (PCB 167) 4,0E+01 1.1E+01 C 1.1E-02 C 1.1E-01 C 1.1E+00 C Yes 69782-90-7 --Hexachlorobiphenyl, 2,3,3',4,4',5'- (PCB 157) 1.7E+01 1.1E+01 C 1.1E-02 C 1.1E-01 C 1.1E+00 C Yes 38380-08-4 --Hexachlorobiphenyl, 2,3,3',4,4',5- (PCB 156) 1.9E+01 1.1E+01 C 1.1E-02 C 1.1E-01 C 1.1E+00 C Yes 32774-16-6 --Hexachlorobiphenyl, 3,3',4,4',5,5'- (PCB 169) 4,0E-02 1.1E-02 C 1.1E-05 C 1.1E-04 C 1.1E-03 C Yes 65510-44-3 --Pentachlorobiph1nn3),2',3,4,4',5-(PCB 1.4E+01 1.1E+01 C 1.1E-02 C 1.1E-01 C 1.1E+00 C Yes 31508-00-6 --Pentachlorobiphlly8),2,3',4,4',5-(PCB 9.5E+00 1.1E+01 C 1.1E-02 C 1.1E-01 C 1.1E+00 C Yes 32598-14-4 --Pentachlorobiph105) 2,3,3',4,4'-(PCB 9.6E+00 1.1E+01 C 1.1E-02 C 1.1E-01 C 1.1E+00 C Yes 74472-37-0 --Pentachlorobiph114) 23,4,4',5-(PCB 3.0E+01 1.1E+01 C 1.1E-02 C 1.1E-01 C 1.1E+00 C Yes 57465-28-8 --Pentachlorobiph1nny6), 3,3',4,4',5- (PCB 4,2E-03 3.2E-03 C 3.2E-06 C 3.2E-05 C 3.2E-04 C Yes 1336-36-3 Polychlorinated Biphenyls (high risk) 1.3E+01 2.2E+01 C 2.2E-02 C 2.2E-01 C 2.2E+00 C Page 9 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.oE-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.oE-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.oE-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 1336-36-3 -Polychlorinated Biphenyls (low risk) 7.2E+01 1.2E+02 C 1.2E-01 C 1.2E+00 C 1.2E+01 C 1336-36-3 -Polychlorinated Biphenyls (lowest risk) 3.6E+02 6.1E+02 C 6.1E-01 C 6.1E+00 C 6.1E+01 C 32598-13-3 --Tetrachlorobiphenyl, 3,3',4,4'- (PCB 77) Not Volatile Not Volatile 3.2E-03 C 3.2E-02 C 3.2E-01 C Yes 70362-50-4 --Tetrachlorobiph8e1)1, 3,4,4',5- (PCB 1.2E+00 1.1E+00 C 1.1E-03 C 1.1E-02 C 1.1E-01 C Yes 9016-87-9 Polymeric Methylene Diphenyl Dusocyanate (PMDI) Not Volatile Not Volatile 5.3E-01 N 5.3E-01 N 5.3E-01 N Yes Polynuclear Aromatic Hydrocarbons (PAHs) 83-32-9 -Acenaphthene 120-12-7 -Anthracene 56-55-3 -Benz[a]anthracene 4.2E+03 2.0E+02 C 2.oE-01 C 2.0E+00 C 2.0E+01 C 205-82-3 -Benzoo)fluoranthene Not Volatile Not Volatile 1.1E-01 C 1.1E+00 C 1.1E+01 C 50-32-8 -Benzo[a]pyrene Not Volatile Not Volatile 1.8E-03 N 1.8E-03 N 1.8E-03 N Yes 205-99-2 -Benzo[b]fluoranthene Not Volatile Not Volatile 2.oE-01 C 2.0E+00 C 2.0E+01 C 207-08-9 -Benzo[k]fluoranthene Not Volatile Not Volatile 2.0E+00 C 2.0E+01 C 2.0E+02 C 91-58-7 -Chloronaphthalene, Beta- 218-01-9 -Chrysene Not Volatile Not Volatile 2.0E+01 C 2.0E+02 C 2.0E+03 C 53-70-3 -Dibenz[a,h]anthracene Not Volatile Not Volatile 2.0E-02 C 2.oE-01 C 2.0E+00 C 192-65-4 -Dibenzo(a,e)pyrene Not Volatile Not Volatile 1.1E-02 C 1.1E-01 C 1.1E+00 C 57-97-6 -Dimethylbenz(a)anthracene, 7,12- Not Volatile Not Volatile 1.7E-04 C 1.7E-03 C 1.7E-02 C 206-44-0 -Fluoranthene 86-73-7 -Fluorene 193-39-5 -Indeno[l,2,3-cd]pyrene Not Volatile Not Volatile 2.oE-01 C 2.0E+00 C 2.0E+01 C 90-12-0 -Methylnaphthalene, 1- 91-57-6 -Methylnaphthalene, 2- 91-20-3 -Naphthalene 1.5E+02 2.6E+02 N 3.6E-01 C 2.6E+00 N 2.6E+00 N Yes 57835-92-4 -Nitropyrene, 4- Not Volatile Not Volatile 1.1E-01 C 1.1E+00 C 1.1E+01 C 129-00-0 -Pyrene 2942049-3 Potassium Perfluorobutane Sulfonate 67747-09-5 Prochloraz 26399-36-0 Profluralin 1610-18-0 Prometon 7287-19-6 Prometryn 1918-16-7 Propachlor 709-98-8 Propanil 2312-35-8 Propargite 107-19-7 Propargyl Alcohol 13940-2 Propazgie 12242-9 Propham 60207-90-1 Propiconazole 123-38-6 Propionaldehyde 2.3E+03 7.0E+02 N 7.0E+00 N 7.0E+00 N 7.0E+00 N Yes 103-65-1 Propyl benzene 2.0E+03 8.8E+04 N 8.8E+02 N 8.8E+02 N 8.8E+02 N Yes 115-07-1 Propylene 3.3E+02 2.6E+05 N 2.6E+03 N 2.6E+03 N 2.6E+03 N Yes 57-55-6 Propylene Glycol 642343-4 Propylene Glycol Dinitrate Not Volatile Not Volatile 2.4E-01 N 2.4E-01 N 2.4E-01 N Yes 107-98-2 Propylene Glycol Monomethyl Ether 4.7E+07 1.8E+05 N 1.8E+03 N 1.8E+03 N 1.8E+03 N Yes 75-56-9 Propylene Oxide 9.2E+03 2.6E+03 N 3.3E+00 C 2.6E+O1 N 2.6E+O1 N Yes 23950-58-5 Propyzamide 110-86-1 Pyridine 13593-03-8 Quinalphos 91-22-5 Quinoline 76578-14-8 Quizalofop-ethyl E715557 Refractory Ceramic Fibers Not Volatile Not Volatile 2.6E+01 N 2.6E+01 N 2.6E+01 N Yes 10453-86-8 Resmethrin 299-84-3 Runnel 83-79-4 Rotenone 94-59-7 Safrole Not Volatile Not Volatile 1.9E-01 C 1.9E+00 C 1.9E+01 C 7783-00-8 Selenious Acid 778249-2 Selenium Not Volatile Not Volatile 1.8E+01 N 1.8E+01 N 1.8E+01 N Yes 7446-34-6 Selenium Sulfide Not Volatile Not Volatile 1.8E+01 N 1.8E+01 N 1.8E+01 N Yes 74051-80-2 Sethoxydim 7631-86-9 Silica (crystalline, respirable) Not Volatile Not Volatile 2.6E+00 N 2.6E+00 N 2.6E+00 N Yes 7440-22-4 Silver 122-34-9 Simazine 62476-59-9 Sodium Acifluorfen 26628-22-8 Sodium Azide 148-18-5 1 Sodium Diethyldithiocarbamate 768149-4 Sodium Fluoride Not Volatile Not Volatile 1.1E+01 N 1.1E+01 N 1.1E+01 N Yes 62-74-8 Sodium Fluoroacetate 13718-26-8 Sodium Metavanadate Page 10 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.0E-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.0E-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 1347245-2 Sodium Tungstate 10213-10-2 Sodium Tungstate Dihydrate 961-11-5 Stirofos (Tetrachlomvinphos) 7440-24-6 Strontium, Stable 57-24-9 Strychnine 10042-5 Styrene 7.8E+03 8.8E+04 N 8.8E+02 N 8.8E+02 N 8.8E+02 N Yes NA Styrene-Acrylonitrile (SAN) Trimer 126-33-0 Sulfolane Not Volatile Not Volatile 1.8E+00 N 1.8E+00 N 1.8E+00 N Yes 80-07-9 Sulfonylbis(4-chlorobenzene), 1,1'- 7446-11-9 Sulfur Trioxide 8.8E+01 N 8.8E-01 N 8.8E-01 N 8.8E-01 N Yes 7664-93-9 Sulfuric Acid Not Volatile Not Volatile 8.8E-01 N 8.8E-01 N 8.8E-01 N Yes 140-57-8 Sulfurous acid, 2-chloroethyl 2-[4-(1,1- dimethylethyl)phenoxy]-1-methylethyl ester Not Volatile Not Volatile 1.7E+00 C 1.7E+01 C 1.7E+02 C 21564-17-0 TCMTB 34014-18-1 Tebuthiuron 3383-96-8 Temephos 5902-51-2 Terbacil 13071-79-9 Terbufos 886-50-0 Terbutryn 543643-1 Tetrabromodiphenyl ether, 2,2',4,4'- (BDE-47) 95-94-3 Tetrachlorobenzene,1,2,4,5- 630-20-6 Tetrachloroethane, 1,1,1,2- 1.6E+02 1.7E+03 C 1.7E+00 C 1.7E+01 C 1.7E+02 C 79-34-5 Tetrachloroethane, 1,1,2,2- 1.4E+02 2.1E+02 C 2.1E-01 C 2.1E+00 C 2.1E+01 C 127-18-4 Tetrachloroethylene 4.8E+01 3.5E+03 N 3.5E+01 N 3.5E+01 N 3.5E+01 N Yes 58-90-2 Tetrachlorophenol,2,3,4,6- 5216-25-1 Tetrachlorotoluene,p- alpha, alpha, alpha- 3689-24-5 Tetraethyl Dithiopyrophosphate 811-97-2 Tetrafluoroethane, 1,1,1,2- 3.4E+04 7.0E+06 N 7.0E+04 N 7.0E+04 N 7.0E+04 N Yes 47945-8 Tetryl (Trinitrophenylmethylnitramine) 1314-32-5 Thallic Oxide 1010245-1 Thallium (1) Nitrate 7440-28-0 Thallium (Soluble Salts) 563-68-8 Thallium Acetate 6533-73-9 Thallium Carbonate 7791-12-0 Thallium Chloride 12039-52-0 Thallium Selenite 7446-18-6 Thallium Sulfate 79277-27-3 Thifensulfuron-methyl 28249-77-6 Thiobencarb 11148-8 Thiodiglycol 39196-18-4 Thiofanox 23564-05-8 Thiophanate, Methyl 137-26-8 Thiram 7440-31-5 Tin 755045-0 Titanium Tetrachloride 8.8E+00 N 8.8E-02 N 8.8E-02 N 8.8E-02 N Yes 108-88-3 Toluene 1.6E+04 4.4E+05 N 4.4E+03 N 4.4E+03 N 4.4E+03 N Yes 584-84-9 Toluene-2,4-diisocyanate 1.5E+01 7.0E-01 N 7.0E-03 N 7.0E-03 N 7.0E-03 N Yes 95-70-5 Toluene-2,5-diamine 91-08-7 Toluene-2,6-diisocyanate 1.5E+01 7.0E-01 N 7.0E-03 N 7.0E-03 N 7.0E-03 N Yes 99-94-5 Toluic Acid, p- 95-53-4 Toluidine, o- (Methylaniline, 2-) Not Volatile Not Volatile 2.4E-01 C 2.4E+00 C 2.4E+O1 C 10649-0 Toluidine,p- E1790670 Total Petroleum Hydrocarbons (Aliphatic High) E1790666 Total Petroleum Hydrocarbons (Aliphatic Low) 7,1E+00 5.3E+04 N 5.3E+02 N 5.3E+02 N 5.3E+02 N Yes E1790668 Total Petroleum Hydrocarbons (Aliphatic Medium) 6.3E-01 8.8E+03 N 8.8E+01 N 8.8E+01 N 8.8E+01 N Yes E1790676 Total Petroleum Hydrocarbons (Aromatic High) E1790672 Total Petroleum Hydrocarbons (Aromatic Low) 1.2E+02 2.6E+03 N 2.6E+O1 N 2.6E+O1 N 2.6E+O1 N Yes E1790674 Total Petroleum Hydrocarbons (Aromatic Medium) 1.3E+02 2.6E+02 N 2.6E+00 N 2.6E+00 N 2.6E+00 N Yes 8001-35-2 Toxaphene Not Volatile Not Volatile 3.8E-02 C 3.8E-01 C 3.8E+00 C 66841-25-6 Tralomethrin 688-73-3 Tri-n-butyltin 102-76-1 Triacetin 4312143-3 Triadimefon 2303-17-5 Triallate Page 11 of 12 North Carolina Department of Environmental Quality Non -Residential Vapor Intrusion Screening Levels Not To Be Used for Structures Frequented or Occupied By Children February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level s (SGSL) ug/m TCR=1.0E-05 THQ=0.2 Basis IASL (A) u m3 TCR=1.0E-06 THQ=0.2 Basis IASL (B) u m3 TCR=1.0E-05 THQ=0.2 Basis 2 IASL (C) u ms TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non -Cancer Effect?' 82097-50-5 Triasulfuron 10120048-0 Tribenuron-methyl 615-54-3 Tribromobenzene, 1,2,4- 118-79-6 Tribromophenol, 2,4,6- 126-73-8 Tributyl Phosphate E1790678 Tributylfin Compounds 56-35-9 Tributylfin Oxide 76-13-1 Tichloro-1,2,2-trifluoroethane, 1,1,2- 2.0E+02 4.4E+05 N 4.4E+03 N 4.4E+03 N 4.4E+03 N Yes 76-03-9 Trichloroacefic Acid 33663-50-2 Trichloroaniline HC1, 2,4,6- 634-93-5 Trichloroaniline, 2,4,6- 87-61-6 Trichlorobenzene, 1,2,3- 120-82-1 Trichlorobenzene, 1,2,4- 3.0E+01 1.8E+02 N 1.8E+00 N 1.8E+00 N 1.8E+00 N Yes 71-55-6 Trichloroethane, 1,1,1- 6.2E+03 4.4E+05 N 4.4E+03 N 4.4E+03 N 4.4E+03 N Yes 79-00-5 Trichloroethane, 1,1,2- 5.2E+00 1.8E+01 N 1.8E-01 N 1.8E-01 N 1.8E-01 N Yes 79-01-6 Trichloroethylene 4.4E+00 1.8E+02 N 1.8E+00 N 1.8E+00 N 1.8E+00 N Yes 75-69-4 Trichlorofluoromethane 95-95-4 Trichlorophenol, 2,4,5- 88-06-2 Trichlorophenol, 2,4,6- Not Volatile Not Volatile 4.0E+00 C 4.0E+01 C 4.0E+02 C 93-76-5 Trichlorophenoxyacefic Acid,2,4,5- 93-72-1 Trichlorophenoxypropionic acid,-2,4,5 598-77-6 Trichloropropane, 1,1,2- 96-18-4 Trichloropropane, 1,2,3- 1.9E+01 2.6E+O1 N 2.6E-01 N 2.6E-01 N 2.6E-01 N Yes 96-19-5 Trichloropropee, 1,2,3- 3.7E-01 2.6E+O1 N 2.6E-01 N 2.6E-01 N 2.6E-01 N Yes 1330-78-5 Tricresyl Phosphate (TCP) 58138-08-2 Tridiphane 121-44-8 Triethylamine 1.0E+03 6.1E+02 N 6.1E+00 N 6.1E+00 N 6.1E+00 N Yes 112-27-6 Triethylene Glycol 42046-2 Trifluoroethane, 1,1,1- 5.6E+02 1.8E+06 N 1.8E+04 N 1.8E+04 N 1.8E+04 N Yes 1582-09-8 Trifluralin 512-56-1 Trimethyl Phosphate 526-73-8 Trimethylbenzene, 1,2,3- 2.9E+02 5.3E+03 N 5.3E+01 N 5.3E+01 N 5.3E+01 N Yes 95-63-6 Trimethylbenzene, 1,2,4- 2.1E+02 5.3E+03 N 5.3E+01 N 5.3E+01 N 5.3E+01 N Yes 108-67-8 Trimethylbenzene, 1,3,5- 1.5E+02 5.3E+03 N 5.3E+01 N 5.3E+01 N 5.3E+01 N Yes 25167-70-8 Trimethylpentene, 2,4,4- 99-35-4 Trinitrobenzene, 1,3,5- 118-96-7 Trinitrotoluene, 2,4,6- 791-28-6 Triphenylphosphine Oxide 13674-87-8 Tris(1,3-Dichloro-2-propyl) Phosphate 13674-84-5 Tris(1-chloro-2-propyl)phosphate 126-72-7 Tris(2,3-dibromopropyl)phosphate 2.1E+02 1.9E+01 C 1.9E-02 C 1.9E-01 C 1.9E+00 C 115-96-8 Tris(2-chloroethyl)phosphate 7842-2 Tris(2-ethylhexyl)phosphate 7440-33-7 Tungsten E715565 Uranium (Soluble Salts) Not Volatile Not Volatile 3.5E-02 N 3.5E-02 N 3.5E-02 N Yes 51-79-6 Urethane Not Volatile Not Volatile 4.2E-02 C 4.2E-01 C 4.2E+00 C 1314-62-1 Vanadium Pentoxide Not Volatile Not Volatile 1.5E-03 C 6.1E-03 N 6.1E-03 N Yes 7440-62-2 Vanadium and Compounds Not Volatile Not Volatile 8.8E-02 N 8.8E-02 N 8.8E-02 N Yes 1929-77-7 Vemolate 50471-44-8 Vinclozolin 108-05-4 Vinyl Acetate 8.4E+03 1.8E+04 N 1.8E+02 N 1.8E+02 N 1.8E+02 N Yes 593-60-2 Vinyl Bromide 5.2E+00 2.6E+02 N 3.8E-01 C 2.6E+00 N 2.6E+00 N Yes 75-01-4 Vinyl Chloride 2.5E+01 2.8E+03 C 2.8E+00 C 2.8E+01 C 8.8E+01 N Yes 81-81-2 Warfarin 10642-3 Xylene,P- 3.1E+02 8.8E+03 N 8.8E+01 N 8.8E+01 N 8.8E+01 N Yes 108-38-3 Xylene, m- 3.0E+02 8.8E+03 N 8.8E+01 N 8.8E+01 N 8.8E+01 N Yes 9547-6 Xylene, o- 4.1E+02 8.8E+03 N 8.8E+01 N 8.8E+01 N 8.8E+01 N Yes 1330-20-7 Xylenes 3.2E+02 8.8E+03 N 8.8E+01 N 8.8E+01 N 8.8E+01 N Yes 1314-84-7 Zinc Phosphide 7440-66-6 Zinc and Compounds 12122-67-7 Zineb 7440-67-7 Zirconium 1) TCR = Target Cancer Risk; THQ=Target Hazard Quotient; C= Carcinogenic; N = Non -Carcinogenic 2) Indoor Air/Crawlspace Screening Levels at target risk 1.0E-04 (IASL C) to be used if only one carcinogen is present. 3) If more than five compounds with non -cancer effects are present risk should be evaluated using NCDEQ Risk Calculator. Page 12 of 12 RDFr \1 Environmental Consulting 4012 Ridgebrook Bluffs Dr. I Raleigh, NC 27603 (919) 389-7747 1 info@rdhec.com APPENDIX C NCDWM RESIDENTIAL VAPOR INTRUSION SCREENING LEVELS TABLE (FEBRUARY 2018) North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/m' TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/ms TCR=1.0E-06 THQ=0.2 Basis IASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' 30560-19-1 Acephate 75-07-0 Acetaldehyde 6.9E+02 6.3E+01 N 1.3E+00 C 1.9E+00 N 1.9E+00 N Yes 34256-82-1 Acetochlor 67-64-1 Acetone 4.5E+06 2.2E+05 N 6.5E+03 N 6.5E+03 N 6.5E+03 N Yes 75-86-5 Acetone Cyanohydrin Not Volatile Not Volatile 4.2E-01 N 4.2E-01 N 4.2E-01 N Yes 75-05-8 Acemnitrile 8.9E+03 4.2E+02 N 1.3E+01 N 1.3E+01 N 1.3E+01 N Yes 98-86-2 Acetophenone 53-96-3 Acetylaminofluorene, 2- Not Volatile Not Volatile 2.2E-03 C 2.2E-02 C 2.2E-01 C 107-02-8 Acrolein 8.4E-01 1.4E-01 N 4.2E-03 N 4.2E-03 N 4.2E-03 N Yes 79-06-1 Acrylamide Not Volatile Not Volatile 1.0E-02 C 1.0E-01 C 1.0E+00 C Yes 79-10-7 Acrylic Acid 1.4E+04 7.0E+00 N 2.1E-01 N 2.1E-01 N 2.1E-01 N Yes 107-13-1 Acrylonitrile 7.3E+01 1.4E+01 C 4.1E-02 C 4.1E-01 C 4.2E-01 N Yes 111-69-3 Adiponitrile Not Volatile Not Volatile 1.3E+00 N 1.3E+00 N 1.3E+00 N Yes 15972-60-8 Alachlor 116-06-3 Aldicarb 1646-88-4 Aldicarb Sulfone 1646-87-3 Aldicarb sulfoxide 309-00-2 Aldrin 3.2E+00 1.9E-01 C 5.7E-04 C 5.7E-03 C 5.7E-02 C 107-18-6 Allyl Alcohol 1.0E+02 7.0E-01 N 2.1E-02 N 2.1E-02 N 2.1E-02 N Yes 107-05-1 Allyl Chloride 4.6E-01 7.0E+00 N 2.1E-01 N 2.1E-01 N 2.1E-01 N Yes 7429-90-5 Aluminum Not Volatile Not Volatile 1.0E+00 N 1.0E+00 N 1.0E+00 N Yes 20859-73-8 Aluminum Phosphide 834-12-8 Ametryn 92-67-1 Aminobiphenyl, 4- Not Volatile Not Volatile 4.7E-04 C 4.7E-03 C 4.7E-02 C 591-27-5 Aminophenol, m- 95-55-6 Aminophenol, o- 123-30-8 Aminophenol,p- 33089-61-1 Amitraz 766441-7 Ammonia 1.6E+05 3.5E+03 N 1.0E+02 N 1.0E+02 N 1.0E+02 N Yes 7773-06-0 Ammonium Sulfamate 75-854 Amyl Alcohol, tert- 1.1E+03 2.1E+01 N 6.3E-01 N 6.3E-01 N 6.3E-01 N Yes 62-53-3 Aniline Not Volatile Not Volatile 2.1E-01 N 2.1E-01 N 2.1E-01 N Yes 84-65-1 Anthmquinone, 9,10- 7440-36-0 Antimony (metallic) 1314-60-9 Antimony Pentoxide 1332-81-6 Antimony Tetroxide 1309-644 Antimony Trioxide Not Volatile Not Volatile 4.2E-02 N 4.2E-02 N 4.2E-02 N Yes 7440-38-2 Arsenic, Inorganic Not Volatile Not Volatile 6.5E-04 C 3.1E-03 N 3.1E-03 N Yes 778442-1 Arsine Not Volatile Not Volatile 1.0E-02 N 1.0E-02 N 1.0E-02 N Yes 3337-71-1 Asulam 1912-24-9 Atrazine 492-80-8 Auramine Not Volatile Not Volatile 1.1E-02 C 1.1E-01 C 1.1E+00 C 65195-55-3 AvermectinB1 86-50-0 Azinphos-methyl Not Volatile Not Volatile 2.1E+00 N 2.1E+00 N 2.1E+00 N Yes 103-33-3 Azobenzene 1.6E+03 3.0E+01 C 9.1E-02 C 9.1E-01 C 9.1E+00 C 123-77-3 Azodicarbonamide Not Volatile Not Volatile 1.5E-03 N 1.5E-03 N 1.5E-03 N Yes 7440-39-3 Barium Not Volatile Not Volatile 1.0E-01 N 1.0E-01 N 1.0E-01 N Yes 186140-1 Benfluralin 17804-35-2 Benomyl 83055-99-6 Bensulfuron-methyl 25057-89-0 Bemazon 100-52-7 Benzaldehyde 7143-2 Benzene 1.6E+01 1.2E+02 C 3.6E-01 C 3.6E+00 C 6.3E+00 N Yes 6369-59-1 Benzenediamine-2-methyl sulfate, 1,4 108-98-5 Benzenethiol 92-87-5 Benzidine Not Volatile Not Volatile 1.5E-05 C 1.5E-04 C 1.5E-03 C 65-85-0 Benzoic Acid 98-07-7 Benzotrichloride 100-51-6 Benzyl Alcohol 100-44-7 Benzyl Chloride 1.2E+01 7.0E+00 N 5.7E-02 C 2.1E-01 N 2.1E-01 N Yes 744041-7 Beryllium and compounds Not Volatile Not Volatile 1.2E-03 C 4.2E-03 N 4.2E-03 N Yes 42576-02-3 Bifenox 82657-04-3 Biphenthrin 92-524 Biphenyl, 1,1'- 6.6E+00 2.8E+00 N 8.3E-02 N 8.3E-02 N 8.3E-02 N Yes 108-60-1 Bis(2-chloro-1-methylethyl) ether 111-91-1 Bis(2-chloroethoxy)methane 111-44-4 Bis(2-chloroethyl)ether 1.2E+02 2.8E+00 C 8.5E-03 C 8.5E-02 C 8.5E-01 C 542-88-1 Bis(chloromethyl)ether 2.5E-03 1.5E-02 C 4.5E-05 C 4.5E-04 C 4.5E-03 C 80-05-7 Bisphenol A 744042-8 Boron And Bomtes Only Not Volatile Not Volatile 4.2E+00 N 4.2E+00 N 4.2E+00 N Yes 10294-34-5 Boron Trichloride 5.6E+00 1.4E+02 N 4.2E+00 N 4.2E+00 N 4.2E+00 N Yes 7637-07-2 Boron Trifluoride 9.0E+01 N 2.7E+00 N 2.7E+00 N 2.7E+00 N Yes 15541-45-4 Bromate 107-04-0 Bromo-2-chloroethane, 1- 1.3E+00 1.6E+00 C 4.7E-03 C 4.7E-02 C 4.7E-01 C 1073-06-9 Bromo-3-fluorobenzene,1- 460-00-4 Bromo-4-fluorobenzene, 1- 108-86-1 Bromobenzene 1.2E+02 4.2E+02 N 1.3E+01 N 1.3E+01 N 1.3E+01 N Yes 74-97-5 Bromochloromethane 1.4E+02 2 .5E+175-274 8.3E+00N 8.3E+00 N 8.3E+00 Yes Bromodichloromethane 8.8E+00 C 7.6E-02 C 7.6E-01 C 7.6E+00 C 75-25-2 Bromoform 1.2E+03 8.5E+02 C 2.6E+00 C 2.6E+01 C 2.6E+02 C Page 1 0£ 11 North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/m' TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/ms TCR=1.0E-06 THQ=0.2 Basis IASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' 74-83-9 Bromomethane 3.5E+00 3.5E+01 N 1.0E+00 N 1.0E+00 N 1.0E+00 N Yes 2104-96-3 Bromophos 106-94-5 1 Bromopropane, 1- 7.0E+01 7.0E+02 N 2.1E+01 N 2.1E+01 N 2.1E+01 N Yes 1689-84-5 Bromoxynil 1689-99-2 BromoxynilOctanoate 106-99-0 Butadiene, 1,3- 1.4E-01 1.4E+01 N 9.4E-02 C 4.2E-01 N 4.2E-01 N Yes 94-82-6 Butanoic acid, 4-(2,4- dichlorophenoxy)- 71-36-3 Butanol, N- 78-92-2 Butyl alcohol, sec- 1.7E+07 2.1E+05 N 6.3E+03 N 6.3E+03 N 6.3E+03 N Yes 200841-5 Butylate 25013-16-5 Butylated hydroxyanisole Not Volatile Not Volatile 4.9E+01 C 4.9E+02 C 4.9E+03 C 128-37-0 Butylated hydroxytoluene 104-51-8 Butylbemmne, n- 135-98-8 Butylbenzene, sec- 98-06-6 Butylbenzene,tert- 75-60-5 Cacodylic Acid 744043-9 Cadmium (Diet) Not Volatile Not Volatile 1.6E-03 C 2.1E-03 N 2.1E-03 N Yes 744043-9 Cadmium (Water) Not Volatile Not Volatile 1.6E-03 C 2.1E-03 N 2.1E-03 N Yes 105-60-2 Caprolactam Not Volatile Not Volatile 4.6E-01 N 4.6E-01 N 4.6E-01 N Yes 2425-06-1 Captafol Not Volatile Not Volatile 6.5E-02 C 6.5E-01 C 6.5E+00 C 133-06-2 Captan Not Volatile Not Volatile 4.3E+00 C 4.3E+01 C 4.3E+02 C 63-25-2 Carbaryl 1563-66-2 Carbofuran 75-15-0 Carbon Disulfide 2.5E+02 4.9E+03 N 1.5E+02 N 1.5E+02 N 1.5E+02 N Yes 56-23-5 Carbon Tetrachloride 4.1E+00 1.6E+02 C 4.7E-01 C 4.7E+00 C 2.1E+01 N Yes 463-58-1 Carbonyl Sulfide 8.4E-01 7.0E+02 N 2.1E+01 N 2.1E+01 N 2.1E+01 N Yes 55285-14-8 Carbosulfan 5234-684 Carboxin 1306-38-3 Ceric oxide Not Volatile Not Volatile 1.9E-01 N 1.9E-01 N 1.9E-01 N Yes 302-17-0 Chloral Hydrate 133-90-4 Chloramben 118-75-2 Chloranil 12789-03-6 Chlordane 7.3E+01 4.9E+00 N 2.8E-02 C 1.5E-01 N 1.5E-01 N Yes 143-50-0 Chlordecone (Kepone) Not Volatile Not Volatile 6.1E-04 C 6.1E-03 C 6.1E-02 C 470-90-6 Chlorfenvinphos 90982-32-4 Chlorimuron, Ethyl- 7782-50-5 Chlorine 6.5E-02 1.0E+00 N 3.1E-02 N 3.1E-02 N 3.1E-02 N Yes 10049-04-4 Chlorine Dioxide 2.5E-02 1.4E+00 N 4.2E-02 N 4.2E-02 N 4.2E-02 N Yes 7758-19-2 Chlorite (Sodium Salt) 75-68-3 Chloro-1,l-difluoroethane, 1- 4.3E+03 3.5E+05 N 1.0E+04 N 1.0E+04 N 1.0E+04 N Yes 126-99-8 Chloro-1,3-butadiene,2- 4.1E-02 3.1E+00 C 9.4E-03 C 9.4E-02 C 9.4E-01 C Yes 3165-93-3 Chloro-2-methylmiline HCl, 4- 95-69-2 Chloro-2-methylaniline, 4- Not Volatile Not Volatile 3.6E-02 C 3.6E-01 C 3.6E+00 C 107-20-0 Chloroacetaldehyde, 2- 79-11-8 Chloroacetic Acid 532-27-4 Chloroacetophenone, 2- Not Volatile Not Volatile 6.3E-03 N 6.3E-03 N 6.3E-03 N Yes 106-47-8 Chloromiline, p- 108-90-7 Chlorobenzene 8.2E+01 3.5E+02 N 1.0E+01 N 1.0E+01 N 1.0E+01 N Yes 98-66-8 Chlorobemmne sulfonic acid, p- 510-15-6 Chlorobenzilate Not Volatile Not Volatile 9.1E-02 C 9.1E-01 C 9.1E+00 C 74-11-3 Chlorobenzoic Acid, p- 98-56-6 Chlorobenzotrifluoride, 4- 4.4E+O1 2.1E+03 N 6.3E+01 N 6.3E+01 N 6.3E+01 N Yes 109-69-3 Chlorobutane, 1- 7545-6 Chlorodifluoromethane 6.3E+03 3.5E+05 N 1.0E+04 N 1.0E+04 N 1.0E+04 N Yes 107-07-3 Chloroethanol, 2- 67-66-3 Chloroform 8.1E+00 4.1E+01 C 1.2E-01 C 1.2E+00 C 1.2E+01 C Yes 74-87-3 Chloromethane 5.2E+01 6.3E+02 N 1.9E+01 N 1.9E+01 N 1.9E+01 N Yes 107-30-2 Chloromethyl Methyl Ether 3.3E+00 1.4E+00 C 4.1E-03 C 4.1E-02 C 4.1E-01 C 88-73-3 Chloronitrobenzene, o- Not Volatile Not Volatile 2.1E-03 N 2.1E-03 N 2.1E-03 N Yes 100-00-5 Chloronitrobenzene, p- Not Volatile Not Volatile 4.2E-01 N 4.2E-01 N 4.2E-01 N Yes 95-57-8 Chlorophenol, 2- 76-06-2 Chloropicrin 1.0E+00 2.8E+00 N 8.3E-02 N 8.3E-02 N 8.3E-02 N Yes 189745-6 Chlorothalonil Not Volatile Not Volatile 3.2E+00 C 3.2E+01 C 3.2E+02 C 9549-8 Chlorotoluene, o- 106-43-4 Chlorotoluene, p- 54749-90-5 Chlorozotocin Not Volatile Not Volatile 4.1E-05 C 4.1E-04 C 4.1E-03 C 101-21-3 Chlorpropham 2921-88-2 Chlorpyrifos 5598-13-0 Chlorpyrifos Methyl 64902-72-3 Chlorsulfuron 1861-32-1 Chlorthal-dimethyl 60238-56-4 Chlorthiophos 16065-83-1 Chromium(III), Insoluble Salts 18540-29-9 Chromium(VI) Not Volatile Not Volatile 1.2E-05 C 1.2E-04 C 1.2E-03 C Yes 744047-3 Chromium, Total 74115-24-5 Clofentezine 7440484 Cobalt Not Volatile Not Volatile 3.1E-04 C 1.3E-03 N 1.3E-03 N Yes 800745-2 Coke Oven Emissions 3.6E-02 5.5E-01 C 1.6E-03 C 1.6E-02 C 1.6E-01 C 7440-50-8 Copper 108-39-4 Cresol, m- Not Volatile I Not Volatile 1.3E+02 N 1.3E+02 N 1.3E+02 N Yes Page 2 of 11 North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/m' TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/ms TCR=1.0E-06 THQ=0.2 Basis IASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' 9548-7 Cresol, o- Not Volatile Not Volatile 1.3E+02 N 1.3E+02 N 1.3E+02 N Yes 106-44-5 Cresol, p- Not Volatile Not Volatile 1.3E+02 N 1.3E+02 N 1.3E+02 N Yes 59-50-7 1 Cresol, p-chloro-m- 1319-77-3 Cresols Not Volatile Not Volatile 1.3E+02 N 1.3E+02 N 1.3E+02 N Yes 123-73-9 Crotonaldehyde,trans- 98-82-8 Cumene 1.8E+02 2.8E+03 N 8.3E+01 N 8.3E+01 N 8.3E+01 N Yes 135-20-6 Cupfermn Not Volatile Not Volatile 4.5E-02 C 4.5E-01 C 4.5E+00 C 21725-46-2 Cyanazine Cyanides 592-01-8 -Calcium Cyanide 544-92-3 -Copper Cyanide 57-12-5 -Cyanide (CN-) 4.0E+01 5.6E+00 N 1.7E-01 N 1.7E-01 N 1.7E-01 N Yes 460-19-5 -Cyanogen 506-68-3 -Cyanogen Bromide 506-77-4 -Cyanogen Chloride 74-90-8 -Hydrogen Cyanide 3.1E+01 5.6E+00 N 1.7E-01 N 1.7E-01 N 1.7E-01 N Yes 151-50-8 -Potassium Cyanide 506-61-6 -Potassium Silver Cyanide 506-64-9 -Silver Cyanide 143-33-9 -Sodium Cyanide E1790664 -Thiocyanates 463-56-9 -Thiocyanic Acid 557-21-1 -Zinc Cyanide 110-82-7 Cyclohexane 2.0E+02 4.2E+04 N 1.3E+03 N 1.3E+03 N 1.3E+03 N Yes 87-84-3 Cyclohexane, 1,2,3,4,5-pentabromo-6 chloro- 108-94-1 Cyclohexanone 4.0E+05 4.9E+03 N 1.5E+02 N 1.5E+02 N 1.5E+02 N Yes 110-83-8 Cyclohexee 1.1E+02 7.0E+03 N 2.1E+02 N 2.1E+02 N 2.1E+02 N Yes 108-91-8 Cyclohexylamine 68359-37-5 Cyfluthrin 68085-85-8 Cyhalothrin 52315-07-8 Cypemrethrin 66215-27-8 Cyromazine 72-54-8 DDD, p,p'-(DDD) Not Volatile Not Volatile 4.1E-02 C 4.1E-01 C 4.1E+00 C 72-55-9 DDE, p,p'- 1.7E+02 9.6E+00 C 2.9E-02 C 2.9E-01 C 2.9E+00 C 50-29-3 DDT Not Volatile Not Volatile 2.9E-02 C 2.9E-01 C 2.9E+00 C 75-99-0 Dalapon 1596-84-5 Daminozide Not Volatile Not Volatile 5.5E-01 C 5.5E+00 C 5.5E+01 C 1163-19-5 Decabromodiphenyl ether, 2,2',3,3',4,4',5,5',6,6'- (BDE-209) 806548-3 Demeton 103-23-1 Di(2-ethylhexyl)adipate 2303-164 Diallate 333-41-5 Diazinon 132-65-0 Dibenzothiophene 96-12-8 Dibromo-3-chloropropme, 1,2- 2.8E-01 5.6E-02 C 1.7E-04 C 1.7E-03 C 1.7E-02 C Yes 108-36-1 Dibromobenzene,l,3- 106-37-6 Dibromobenzene,l,4- 124-48-1 Dibromochloromethane 106-93-4 Dibromoethane, 1,2- 1.8E+00 1.6E+00 C 4.7E-03 C 4.7E-02 C 4.7E-01 C Yes 74-95-3 Dibromomethane (Methylene Bromide) 2.5E+01 2.8E+01 N 8.3E-01 N 8.3E-01 N 8.3E-01 N Yes E1790660 Dibutyltin Compounds 1918-00-9 Dicamba 764-41-0 Dichloro-2-butene, 1,4- 1.9E-02 2.2E-01 C 6.7E-04 C 6.7E-03 C 6.7E-02 C 1476-11-5 Dichloro-2-butene, cis-1,4- 2.5E-01 2.2E-01 C 6.7E-04 C 6.7E-03 C 6.7E-02 C 110-57-6 Dichloro-2-butene, trans-1,4- 2.5E-01 2.2E-01 C 6.7E-04 C 6.7E-03 C 6.7E-02 C 7943-6 Dichloroacetic Acid 95-50-1 Dichlorobenzene, 1,2- 5.3E+02 1.4E+03 N 4.2E+01 N 4.2E+01 N 4.2E+01 N Yes 106-46-7 Dichlorobenzene, 1,4- 2.6E+O1 8.5E+01 C 2.6E-01 C 2.6E+00 C 2.6E+01 C Yes 91-94-1 Dichlorobenzidine, 3,3'- Not Volatile Not Volatile 8.3E-03 C 8.3E-02 C 8.3E-01 C 90-98-2 Dichlorobenzophenone, 4,4'- 75-71-8 Dichlorodifluoromethane 1.5E+00 7.0E+02 N 2.1E+01 N 2.1E+01 N 2.1E+01 N Yes 75-34-3 Dichloroethane, 1,1- 7.6E+O1 5.8E+02 C 1.8E+00 C 1.8E+01 C 1.8E+02 C 107-06-2 Dichloroethane, 1,2- 2.2E+01 3.6E+O1 C 1.1E-01 C 1.1E+00 C 1.5E+00 N Yes 75-354 Dichloroethylene, 1,1- 3.9E+01 1.4E+03 N 4.2E+01 N 4.2E+01 N 4.2E+01 N Yes 156-59-2 Dichloroethylene, 1,2-cis- 156-60-5 Dichloroethylene, 1,2-trans- 120-83-2 Dichlorophenol,2,4- 94-75-7 Dichlorophenoxy Acetic Acid, 2,4- 78-87-5 Dichloropropane, 1,2- 7.2E+00 2.8E+01 N 7.6E-01 C 8.3E-01 N 8.3E-01 N Yes 142-28-9 Dichloropropane, 1,3- 616-23-9 Dichloropropanol, 2,3- 542-75-6 Dichloropropee, 1,3- 2.9E+01 1.4E+02 N 7.0E-01 C 4.2E+00 N 4.2E+00 N Yes 62-73-7 Dichlorvos Not Volatile Not Volatile 3.4E-02 C 1.0E-01 N 1.0E-01 N Yes 141-66-2 Dicrotophos 77-73-6 Dicyclopentadiene 2.4E-02 2.1E+00 N 6.3E-02 N 6.3E-02 N 6.3E-02 N Yes 60-57-1 Dieldrin Not Volatile Not Volatile 6.1E-04 C 6.1E-03 C 6.1E-02 C E17136615 Diesel Engine Exhaust Not Volatile Not Volatile 9.4E-03 C 9.4E-02 C 9.4E-01 C Yes 111-42-2 Diethanolamine Not Volatile Not Volatile 4.2E-02 N 4.2E-02 N 4.2E-02 N Yes 112-34-5 Dethylene Glycol Monobutyl Ether Not Volatile Not Volatile 2.1E-02 N 2.1E-02 N 2.1E-02 N Yes Page 3 of 11 North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/m' TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/ms TCR=1.0E-06 THQ=0.2 Basis IASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' 111-90-0 Diethylene Glycol Monoethyl Ether Not Volatile Not Volatile 6.3E-02 N 6.3E-02 N 6.3E-02 N Yes 617-84-5 Diethylfomramide 56-53-1 1 Diethylstilbestrol Not Volatile Not Volatile 2.8E-05 C 2.8E-04 C 2.8E-03 C 43222-48-6 Difenzoquat 35367-38-5 Diflubenzuron 75-37-6 Difluoroethane, 1,1- 1.0E+04 2.8E+05 N 8.3E+03 N 8.3E+03 N 8.3E+03 N Yes 420-45-1 Diflucropropane, 2,2- 3.0E+02 2.1E+05 N 6.3E+03 N 6.3E+03 N 6.3E+03 N Yes 94-58-6 Dihydrosafrole 4.3E+03 7.2E+01 C 2.2E-01 C 2.2E+00 C 2.2E+01 C 108-20-3 Diisopropyl Ether 1.4E+03 4.9E+03 N 1.5E+02 N 1.5E+02 N 1.5E+02 N Yes 1445-75-6 Diisopropyl Methylphosphonate 55290-64-7 Dimethipin 60-51-5 Dimethoate 119-90-4 Dimethoxybenzidine,3,3'- 756-79-6 Dimethyl methylphosphonate 60-11-7 Dimethylamino azobenzene rp-1 Not Volatile Not Volatile 2.2E-03 C 2.2E-02 C 2.2E-01 C 21436-96-4 Dimethylaniline 140, 2,4- 95-68-1 Dimethylaniline, 2,4- 121-69-7 Dimethylaniline, N,N- 119-93-7 Dimethylbenzidine, 3,3'- 68-12-2 Dimethylformamide 2.1E+06 2.1E+02 N 6.3E+00 N 6.3E+00 N 6.3E+00 N Yes 57-14-7 Dimethylhydrazine, 1,1- 7.9E-01 1.4E-02 N 4.2E-04 N 4.2E-04 N 4.2E-04 N Yes 540-73-8 Dimethylhydrazine, 1,2- 6.2E+01 5.8E-03 C 1.8E-05 C 1.8E-04 C 1.8E-03 C 105-67-9 Dimethylphenol, 2,4- 576-26-1 Dimethylphenol, 2,6- 95-65-8 Dimethylphenol, 3,4- 513-37-1 Dimethylvinylchloride 4.5E+01 7.2E+01 C 2.2E-01 C 2.2E+00 C 2.2E+01 C 534-52-1 Dinitro-o-cresol, 4,6- 131-89-5 Dinitro-o-cyclohexyl Phenol,4,6- 528-29-0 Dinitrobenzene,l,2- 99-65-0 Dinitrobenzene,l,3- 100-25-4 Dinitrobenzene,l,4- 51-28-5 Dinitrophenol, 2,4- E1615210 Dinitrotoluene Mixture, 2,4/2,6- 121-14-2 Dinitrotoluene, 2,4- Not Volatile Not Volatile 3.2E-02 C 3.2E-01 C 3.2E+00 C 606-20-2 Dinitrotoluene, 2,6- 35572-78-2 Dinitrotoluene, 2-Amino-4,6- 19406-51-0 Dinitrotoluene, 4-Amino-2,6- 25321-14-6 Dinitrotoluene, Technical grade 88-85-7 Dinoseb 123-91-1 Dioxane, 1,4- 2.9E+04 1.9E+02 C 5.6E-01 C 5.6E+00 C 6.3E+00 N Yes Dioxins -Hexachlorodibenzo-p-dioxin, Mixture Not Volatile Not Volatile 2.2E-06 C 2.2E-05 C 2.2E-04 C 1746-01-6 -TCDD, 2,3,7,8- 3.6E-04 2.5E-05 C 7.4E-08 C 7.4E-07 C 7.4E-06 C Yes 957-51-7 Diphenamid 101-84-8 Diphenyl Ether 7.3E+00 2.8E+00 N 8.3E-02 N 8.3E-02 N 8.3E-02 N Yes 127-63-9 Diphenyl Sulfone 122-39-4 Diphenylamine 122-66-7 Diphenylhydrazine, 1,2- Not Volatile Not Volatile 1.3E-02 C 1.3E-01 C 1.3E+00 C 85-00-7 Diquat 1937-37-7 Direct Black 38 Not Volatile Not Volatile 2.0E-05 C 2.0E-04 C 2.0E-03 C 260246-2 Direct Blue 6 Not Volatile Not Volatile 2.0E-05 C 2.0E-04 C 2.0E-03 C 16071-86-6 Direct Brown 95 Not Volatile Not Volatile 2.0E-05 C 2.0E-04 C 2.0E-03 C 298-04-4 Disulfoton 505-29-3 Dithiane, 1,4- 330-54-1 Diuron 2439-10-3 Dodine 759-94-4 EPTC 115-29-7 Endosulfan 145-73-3 Endothall 72-20-8 Endrin 106-89-8 Epichlorohydrin 1.7E+02 7.0E+00 N 2.1E-01 N 2.1E-01 N 2.1E-01 N Yes 106-88-7 Epoxybutane, 1,2- 5.7E+02 1.4E+02 N 4.2E+00 N 4.2E+00 N 4.2E+00 N Yes 111-77-3 Ethanol, 2-(2-methoxyethoxy)- 16672-87-0 Ethephon 563-12-2 Ethion 111-15-9 Ethoxyethanol Acetate, 2- 9.6E+04 4.2E+02 N 1.3E+01 N 1.3E+01 N 1.3E+01 N Yes 110-80-5 Ethoxyethanol, 2- 2.2E+06 1.4E+03 N 4.2E+01 N 4.2E+01 N 4.2E+01 N Yes 141-78-6 Ethyl Acetate 2.7E+03 4.9E+02 N 1.5E+01 N 1.5E+01 N 1.5E+01 N Yes 140-88-5 Ethyl Acrylate 1.2E+02 5.6E+O1 N 1.7E+00 N 1.7E+00 N 1.7E+00 N Yes 75-00-3 Ethyl Chloride(Chloroethane) 4.6E+03 7.0E+04 N 2.1E+03 N 2.1E+03 N 2.1E+03 N Yes 60-29-7 Ethyl Ether 97-63-2 Ethyl Methacrylate 2.7E+03 2.1E+03 N 6.3E+01 N 6.3E+01 N 6.3E+01 N Yes 2104-64-5 Ethyl-p-nitrophenyl Phosphonate 100-41-4 Ethylbenzene 3.5E+01 3.7E+02 C 1.1E+00 C l.lE+01 C 1.1E+02 C Yes 109-78-4 Ethylene Cyanohydrin 107-15-3 Ethylene Diamine 107-21-1 Ethylene Glycol Not Volatile Not Volatile 8.3E+01 N 8.3E+01 N 8.3E+01 N Yes 111-76-2 Ethylene Glycol Monobutyl Ether Not Volatile Not Volatile 3.3E+02 N 3.3E+02 N 3.3E+02 N Yes 75-21-8 Ethylene Oxide 5.6E-01 1.1E-01 C 3.4E-04 C 3.4E-03 C 3.4E-02 C Yes 96-45-7 Ethylene Thiourea Not Volatile Not Volatile 2.2E-01 C 2.2E+00 C 2.2E+01 C Page 4 of 11 North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/mm TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/mm TCR=1.0E-06 THQ=0.2 Basis IASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' 151-56-4 Ethyleneimine 3.0E+00 4.9E-02 C 1.5E-04 C 1.5E-03 C 1.5E-02 C 84-72-0 Ethylphthalyl Ethyl Glycolate 22224-92-6 1 Fenamiphos 39515-41-8 Fenpropathrin 51630-58-1 Fenvalemte 2164-17-2 Fluometuron 16984-48-8 Fluoride Not Volatile Not Volatile 2.7E+00 N 2.7E+00 N 2.7E+00 N Yes 7782414 Fluorine (Soluble Fluoride) Not Volatile Not Volatile 2.7E+00 N 2.7E+00 N 2.7E+00 N Yes 59756-60-4 Fluridone 56425-91-3 Flurimmidol 85509-19-9 Flusilazole 66332-96-5 Flutolanil 69409-94-5 Fluvalinate 133-07-3 Folpet 72178-02-0 Fomesafen 944-22-9 Fowles 50-00-0 Formaldehyde 1.5E+05 6.8E+01 N 2.2E-01 C 2.0E+00 N 2.0E+00 N Yes 64-18-6 Formic Acid 9.2E+03 2.1E+00 N 6.3E-02 N 6.3E-02 N 6.3E-02 N Yes 39148-24-8 Fosetyl-AL Forms 132-64-9 -Dibenzofuran 110-00-9 -Furan 109-99-9 -Tehuhydrofurm 1.4E+05 1.4E+04 N 4.2E+02 N 4.2E+02 N 4.2E+02 N Yes 6745-8 Fum olidone 98-01-1 Furfural 6.8E+04 3.5E+02 N 1.0E+01 N 1.0E+01 N 1.0E+01 N Yes 531-82-8 Furium Not Volatile Not Volatile 6.5E-03 C 6.5E-02 C 6.5E-01 C 60568-05-0 Furmecyclox Not Volatile Not Volatile 3.3E-01 C 3.3E+00 C 3.3E+01 C 77182-82-2 Glufosinate, Ammonium 111-30-8 Glutaraldehyde Not Volatile Not Volatile 1.7E-02 N 1.7E-02 N 1.7E-02 N Yes 765-34-4 Glycidyl 1.0E+04 7.0E+00 N 2.1E-01 N 2.1E-01 N 2.1E-01 N Yes 1071-83-6 Glyphosate 113-00-8 Guanidine 50-01-1 Guanidine Chloride 506-93-4 Guanidine Nitrate 69806-40-2 Haloxyfop, Methyl 7644-8 Heptachlor 1.8E+00 7.2E-01 C 2.2E-03 C 2.2E-02 C 2.2E-01 C 1024-57-3 Heptachlor Epoxide 1.3E+01 3.6E-01 C 1.1E-03 C 1.1E-02 C 1.1E-01 C 111-71-7 Heptanal,n- 5.7E+01 2.1E+01 N 6.3E-01 N 6.3E-01 N 6.3E-01 N Yes 142-82-5 Heptane,N- 1.0E+00 2.8E+03 N 8.3E+01 N 8.3E+01 N 8.3E+01 N Yes 87-82-1 Hexabromobenzene 68631-49-2 Hexabromodiphenyl ether, 2,2',4,4',5,5'- (BDE-153) 118-74-1 Hexachlorobemmne 8.8E-01 2.0E+00 C 6.1E-03 C 6.1E-02 C 6.1E-01 C 87-68-3 Hexachlorobutadiene 3.0E+00 4.3E+01 C 1.3E-01 C 1.3E+00 C 1.3E+01 C 319-84-6 Hexachlorocyclohexane, Alpha- Not Volatile Not Volatile 1.6E-03 C 1.6E-02 C 1.6E-01 C 319-85-7 Hexachlorocyclohexane, Beta- Not Volatile Not Volatile 5.3E-03 C 5.3E-02 C 5.3E-01 C 58-89-9 Hexachlorocyclohexane, Gamma- (Lindane) Not Volatile Not Volatile 9.1E-03 C 9.1E-02 C 9.1E-01 C 608-73-1 Hexachlorocyclohexane, Technical Not Volatile Not Volatile 5.5E-03 C 5.5E-02 C 5.5E-01 C 77474 Hexachlorocyclopentadiene 3.8E-02 1.4E+00 N 4.2E-02 N 4.2E-02 N 4.2E-02 N Yes 67-72-1 Hexachloroethane 1.6E+01 8.5E+01 C 2.6E-01 C 2.6E+00 C 6.3E+00 N Yes 70-304 Hexachlorophene 121-82-4 Hexahydro-1,3,5-trinitro-1,3,5- triazine (RDJ) 822-06-0 Hexamethylene Diisocyanate, 1,6- 1.1E+00 7.0E-02 N 2.1E-03 N 2.1E-03 N 2.1E-03 N Yes 680-31-9 Hexamethylphosphoramide 110-54-3 Hexane, N- 2.0E+00 4.9E+03 N 1.5E+02 N 1.5E+02 N 1.5E+02 N Yes 124-04-9 Hexanedioic Acid 591-78-6 Hexamme,2- 1.6E+03 2.1E+02 N 6.3E+00 N 6.3E+00 N 6.3E+00 N Yes 51235-04-2 Hexazinone 78587-05-0 Hexythiazox 67485-29-4 Hydramethylnon 302-01-2 Hydrazine 2.3E+02 1.9E-01 C 5.7E-04 C 5.7E-03 C 6.3E-03 N Yes 10034-93-2 Hydrazine Sulfate Not Volatile Not Volatile 5.7E-04 C 5.7E-03 C 5.7E-02 C 7647-01-0 Hydrogen Chloride 5.0E-08 1.4E+02 N 4.2E+00 N 4.2E+00 N 4.2E+00 N Yes 7664-39-3 Hydrogen Fluoride 6.9E+02 9.7E+01 N 2.9E+00 N 2.9E+00 N 2.9E+00 N Yes 7783-064 Hydrogen Sulfide 1.2E+00 1.4E+01 N 4.2E-01 N 4.2E-01 N 4.2E-01 N Yes 123-31-9 Hydroquinone 35554-44-0 hnazalil 81335-37-7 hnazaquin 81335-77-5 hnazethapyr 7553-56-2 Iodine 36734-19-7 Iprodione 7439-89-6 Iron 78-83-1 Isobutyl Alcohol 78-59-1 Isophorone Not Volatile Not Volatile 4.2E+02 N 4.2E+02 N 4.2E+02 N Yes 33820-53-0 Isopropalin 67-63-0 Isopropanol 1.3E+05 1.4E+03 N 4.2E+01 N 4.2E+01 N 4.2E+01 N Yes 1832-54-8 Isopropyl Methyl Phosphonic Acid 82558-50-7 Isoxaben E173766, JP-7 1.5E+02 2.1E+03 N 6.3E+01 N 6.3E+01 N 6.3E+01 N Yes Page 5 of 11 North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/m' TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/ms TCR=1.0E-06 THQ=0.2 Basis IASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' 77501-63-4 Lactofen 78-97-7 Lactonitrile Lead Compounds 7446-27-7 -Lead Phosphate Not Volatile Not Volatile 2.3E-01 C 2.3E+00 C 2.3E+01 C 301-04-2 -Lead acetate Not Volatile Not Volatile 2.3E-01 C 2.3E+00 C 2.3E+01 C 7439-92-1 -Lead and Compounds Not Volatile Not Volatile 1.5E-01 N 1.5E-01 N 1.5E-01 N Yes 1335-32-6 Lead subacetate Not Volatile Not Volatile 2.3E-01 C 2.3E+00 C 2.3E+01 C 78-00-2 -Tetraethyl Lead 541-25-3 Lewisite 330-55-2 Linuron 7439-93-2 Lithium 94-74-6 MCPA 94-81-5 MCPB 93-65-2 MCPP 121-75-5 Malathion 108-31-6 Maleic Anhydride Not Volatile Not Volatile 1.5E-01 N 1.5E-01 N 1.5E-01 N Yes 123-33-1 Maleic Hydrazide 109-77-3 Malononitrile 8018-01-7 Mancozeb 12427-38-2 Maneb 7439-96-5 Manganese (Diet) Not Volatile Not Volatile 1.0E-02 N 1.0E-02 N 1.0E-02 N Yes 7439-96-5 Manganese (Non -diet) Not Volatile Not Volatile 1.0E-02 N 1.0E-02 N 1.0E-02 N Yes 950-10-7 Mephosfolan 24307-26-4 Mepiquat Chloride 149-30-4 Mercaptobenzothiazole, 2- Mercury Compounds 7487-94-7 -Mercuric Chloride (and other Mercury salts) Not Volatile Not Volatile 6.3E-02 N 6.3E-02 N 6.3E-02 N Yes 7439-97-6 -Mercury(elemental) 1.8E-01 2.1E+00 N 6.3E-02 N 6.3E-02 N 6.3E-02 N Yes 22967-92-6 -Methyl Mercury 62-384 -Phenylmercuric Acetate 150-50-5 Merphos 7848-8 Merphos Oxide 57837-19-1 Metalaxyl 126-98-7 Metbacrylonitrile 6.2E+02 2.1E+02 N 6.3E+00 N 6.3E+00 N 6.3E+00 N Yes 10265-92-6 Methamidophos 67-56-1 Methanol 2.2E+07 1.4E+05 N 4.2E+03 N 4.2E+03 N 4.2E+03 N Yes 950-37-8 Methidathion 16752-77-5 Methomyl 99-59-2 Metboxy-5-nitromiline, 2- Not Volatile Not Volatile 2.0E-01 C 2.0E+00 C 2.0E+01 C 7243-5 Methoxychlor 110-49-6 Metboxyethanol Acetate, 2- 1.6E+04 7.0E+00 N 2.1E-01 N 2.1E-01 N 2.1E-01 N Yes 109-86-4 Metboxyethanol, 2- 3.1E+05 1.4E+02 N 4.2E+00 N 4.2E+00 N 4.2E+00 N Yes 79-20-9 Methyl Acetate 96-33-3 Methyl Acrylate 5.1E+02 1.4E+02 N 4.2E+00 N 4.2E+00 N 4.2E+00 N Yes 78-93-3 Methyl Ethyl Ketone (2-Butanone) 4.5E+05 3.5E+04 N 1.0E+03 N 1.0E+03 N 1.0E+03 N Yes 60-344 Methyl Hydrazine 3.4E+O1 1.4E-01 N 2.8E-03 C 4.2E-03 N 4.2E-03 N Yes 108-10-1 Methyl Isobutyl Ketone(4-methyl-2- pentanone) 1.1E+05 2.1E+04 N 6.3E+02 N 6.3E+02 N 6.3E+02 N Yes 624-83-9 Methyl lsocyanate 5.5E+00 7.0E+00 N 2.1E-01 N 2.1E-01 N 2.1E-01 N Yes 80-62-6 Methyl Metbacrylate 1.1E+04 4.9E+03 N 1.5E+02 N 1.5E+02 N 1.5E+02 N Yes 298-00-0 Methyl Parathion 993-13-5 Methyl Phosphonic Acid 25013-15-4 Methyl Styrene (Mixed Isomers) 7.8E+01 2.8E+02 N 8.3E+00 N 8.3E+00 N 8.3E+00 N Yes 66-27-3 Methyl methmesulfonate Not Volatile Not Volatile 1.0E-01 C 1.0E+00 C 1.0E+01 C 1634-044 Methyl tert-Butyl Ether(MTBE) 4.5E+03 3.6E+03 C 1.1E+01 C 1.1E+02 C 6.3E+02 N Yes 615-45-2 Methyl-1,4-benzenediamine dihydrochloride, 2- 108-11-2 Methyl-2-Pentmol, 4- 3.4E+05 2.1E+04 N 6.3E+02 N 6.3E+02 N 6.3E+02 N Yes 99-55-8 Methyl-S-Nitromiline, 2- 70-25-7 Methyl-N-nitro-N-nitrosoguanidine, N- Not Volatile Not Volatile 1.2E-03 C 1.2E-02 C 1.2E-01 C 636-21-5 Methylaniline Hydrochloride, 2- Not Volatile Not Volatile 7.6E-02 C 7.6E-01 C 7.6E+00 C 124-58-3 Methylarsonic acid 74612-12-7 Methylbenzene, 1 4-diamine monohydrochloride, 2- 615-50-9 Methylbenzene-1,4-diamine sulfate, 2 5649-5 Methylcholanthrene, 3- Not Volatile Not Volatile 1.6E-04 C 1.6E-03 C 1.6E-02 C 75-09-2 Methylene Chloride 9.4E+02 4.2E+03 N 1.0E+02 C 1.3E+02 N 1.3E+02 N Yes 101-14-4 Methylene-bis(2-chloromiline), 4,4'- Not Volatile Not Volatile 2.4E-03 C 2.4E-02 C 2.4E-01 C 101-61-1 Methylene-bis(N,N-dimethyl) Aniline, 4,4'- Not Volatile Not Volatile 2.2E-01 C 2.2E+00 C 2.2E+01 C 101-77-9 Methylenebisbemmnamine, 4,4'- Not Volatile Not Volatile 6.1E-03 C 6.1E-02 C 6.1E-01 C Yes 101-68-8 Methylenediphenyl Diisocyanate Not Volatile Not Volatile 1.3E-01 N 1.3E-01 N 1.3E-01 N Yes 98-83-9 Methylstyrene, Alpha- 51218-45-2 Metolachlor 21087-64-9 Metribuzin 74223-64-6 Metsulfuron-methyl 8012-95-1 Mineral oils Page 6 of 11 North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/m' TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/ms TCR=1.0E-06 THQ=0.2 Basis NASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' 2385-85-5 Mirex 1.7E-01 1.8E-01 C 5.5E-04 C 5.5E-03 C 5.5E-02 C 2212-67-1 Molinate 7439-98-7 1 Molybdenum 10599-90-3 Monochlommine 100-61-8 Monomethylaniline 88671-89-0 Myclobutanil 74-31-7 N,N'-Dipheny1-1,4-benzenediamine 300-76-5 Naled 64742-95-6 Naphtha, High Flash Aromatic (HFAN) 1.2E+03 7.0E+02 N 2.1E+01 N 2.1E+01 N 2.1E+01 N Yes 91-59-8 Naphthylamine, 2- 15299-99-7 Napropamide 373-02-4 Nickel Acetate Not Volatile Not Volatile 2.9E-03 N 2.9E-03 N 2.9E-03 N Yes 3333-67-3 Nickel Carbonate Not Volatile Not Volatile 2.9E-03 N 2.9E-03 N 2.9E-03 N Yes 13463-39-3 Nickel Carbonyl 1.4E-04 9.7E-02 N 2.9E-03 N 2.9E-03 N 2.9E-03 N Yes 12054-48-7 Nickel Hydroxide Not Volatile Not Volatile 2.9E-03 N 2.9E-03 N 2.9E-03 N Yes 1313-99-1 Nickel Oxide Not Volatile Not Volatile 4.2E-03 N 4.2E-03 N 4.2E-03 N Yes E715532 Nickel Refinery Dust Not Volatile Not Volatile 2.9E-03 N 2.9E-03 N 2.9E-03 N Yes 7440-02-0 Nickel Soluble Salts Not Volatile Not Volatile 1.1E-02 C 1.9E-02 N 1.9E-02 N Yes 12035-72-2 Nickel Subsulfide Not Volatile Not Volatile 2.9E-03 N 2.9E-03 N 2.9E-03 N Yes 1271-28-9 Nickelocene Not Volatile Not Volatile 2.9E-03 N 2.9E-03 N 2.9E-03 N Yes 14797-55-8 Nitrate E701177 Nitrate + Nitrite (as N) 14797-65-0 Nitrite 88-744 Nitroaniline, 2- Not Volatile Not Volatile 1.0E-02 N 1.0E-02 N 1.0E-02 N Yes 100-01-6 Nitroaniline, 4- Not Volatile Not Volatile 1.3E+00 N 1.3E+00 N 1.3E+00 N Yes 98-95-3 Nitrobenzene 7.2E+02 2.3E+01 C 7.0E-02 C 7.0E-01 C 1.9E+00 N Yes 9004-70-0 Nitrocellulose 67-20-9 Nitrofurantoin 59-87-0 Nitrofurazone Not Volatile Not Volatile 7.6E-03 C 7.6E-02 C 7.6E-01 C 55-63-0 Nitroglycerin 556-88-7 Nitroguanidine 75-52-5 Nitromethane 8.9E+02 3.5E+01 N 3.2E-01 C 1.0E+00 N 1.0E+00 N Yes 7946-9 Nitropropane,2- 2.1E+00 3.5E-01 C 1.0E-03 C 1.0E-02 C 1.0E-01 C Yes 759-73-9 Nitroso-N-ethylurea, N- Not Volatile Not Volatile 1.3E-04 C 1.3E-03 C 1.3E-02 C 684-93-5 Nitroso-N-methylurea, N- Not Volatile Not Volatile 3.0E-05 C 3.0E-04 C 3.0E-03 C 924-16-3 Nitroso-di-N-butylamine, N- 3.3E+01 5.8E-01 C 1.8E-03 C 1.8E-02 C 1.8E-01 C 621-64-7 Nitroso-di-N-propylamine, N- Not Volatile Not Volatile 1.4E-03 C 1.4E-02 C 1.4E-01 C 1116-54-7 Nitrosodiethanolamine, N- Not Volatile Not Volatile 3.5E-03 C 3.5E-02 C 3.5E-01 C 55-18-5 Nitrosodiethylamine, N- Not Volatile Not Volatile 2.4E-05 C 2.4E-04 C 2.4E-03 C 62-75-9 Nitrosodimethylamine, N- 9.7E+00 2.4E-02 C 7.2E-05 C 7.2E-04 C 7.2E-03 C Yes 86-30-6 Nitrosodiphenylamine, N- Not Volatile Not Volatile 1.1E+00 C 1.1E+01 C 1.1E+02 C 10595-95-6 Nitrosomethylethylamine, N- 7.6E+O1 1.5E-01 C 4.5E-04 C 4.5E-03 C 4.5E-02 C 59-89-2 Nitrosomorpholine jN-j Not Volatile Not Volatile 1.5E-03 C 1.5E-02 C 1.5E-01 C 100-75-4 Nitrosopiperidine jN-) Not Volatile Not Volatile 1.0E-03 C 1.0E-02 C 1.0E-01 C 930-55-2 Nitrosopyrrolidine, N- Not Volatile Not Volatile 4.6E-03 C 4.6E-02 C 4.6E-01 C 99-08-1 Nitrotoluene, m- 88-72-2 Nitrotoluene,o- 99-99-0 Nitrotoluene, p- 111-84-2 Nonane, n- 3.0E-02 1.4E+02 N 4.2E+00 N 4.2E+00 N 4.2E+00 N Yes 27314-13-2 Norfiurazon 32536-52-0 Octabromodiphenyl Ether 269141-0 Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (BA4X) 152-16-9 Octamethylpyrophosphoramide 19044-88-3 Oryzalin 19666-30-9 Oxadiazon 23135-22-0 Oxamyl 42874-03-3 Oxyfiuorfen 76738-62-0 Paclobutrazol 191042-5 Paraquat Dichloride 56-38-2 Parathion 1114-71-2 Pebulate 40487-42-1 Pendimethalin 32534-81-9 Pentabromodiphenyl Ether 60348-60-9 Pentabromodiphenyl ether, 2,2',4,4',5- (BDE-99) 608-93-5 Pentachlorobenzene 76-01-7 Pentachloroethane 82-68-8 Pentachloronitrobenzene 87-86-5 Pentachlorophenol Not Volatile Not Volatile 5.5E-01 C 5.5E+00 C 5.5E+01 C 78-11-5 Pentaerythritol tetranitrate (PETN ) 109-66-0 Pentane, n- 4.1E+00 7.0E+03 N 2.1E+02 N 2.1E+02 N 2.1E+02 N Yes Perchlorates 7790-98-9 -Ammonium Perchlorate 7791-03-9 -Lithium Perchlorate 14797-73-0 -Perchlorate and Perchlorate Salts 7778-74-7 -Potassium Perchlorate 7601-89-0 -Sodium Perchlorate 375-73-5 Perfiuorobutane sulfonic acid (PFBS) Page 7 of 11 North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/ms TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/ms TCR=1.0E-06 THQ=0.2 Basis IASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' 45187-15-3 Perfluorobutanesulfonate 52645-53-1 Permethrin 6244-2 Phenacetin Not Volatile Not Volatile 4.5E+00 C 4.5E+01 C 4.5E+02 C 13684-63-4 Phenmedipham 108-95-2 Phenol Not Volatile Not Volatile 4.2E+01 N 4.2E+01 N 4.2E+01 N Yes 114-26-1 Phenol, 2-(I-methylethoxy)-, methylcarbamate 92-84-2 Phenothi-ine 103-72-0 Phenyl lsothiocyanate 108-45-2 Phenylenediamine, m- 95-54-5 Phenylenediamine, o- 106-50-3 Phenylenediamine,p- 90-43-7 Phenylphenol,2- 298-02-2 Phorate 7544-5 Phosgene 9.2E-02 2.1E+00 N 6.3E-02 N 6.3E-02 N 6.3E-02 N Yes 732-11-6 Phosmet Phosphates, Inorganic 13776-88-0 -Aluminum metaphosphate 68333-79-9 -Ammonium polyphosphate 7790-76-3 -Calcium pyrophosphate 7783-28-0 -Diammonium phosphate 7757-93-9 -Dicalcium phosphate 7782-754 -Dimagnesium phosphate 7758-114 -Dipotassium phosphate 7558-794 -Disodium phosphate 13530-50-2 -Monoaluminum phosphate 7722-76-1 -Monoammonium phosphate 7758-23-8 -Monocalcium phosphate 7757-86-0 -Monomagnesium phosphate 7778-77-0 -Monopotassium phosphate 7558-80-7 -Monosodium phosphate 8017-16-1 -Polyphosphoric acid 13845-36-8 -Potassium tripolyphosphate 7758-16-9 -Sodium acid pyrophosphate 7785 88 8 -Sodium aluminum phosphate (acidic) 10279-59-1 -Sodium aluminum phosphate (anhydrous) 10305-76-7 -Sodium aluminum phosphate (tetrahydrate) 10124-56-8 -Sodium hexametaphosphate 68915-31-1 -Sodium polyphosphate 7785-844 -Sodium trimetaphosphate 7758-294 -Sodium tripolyphosphate 7320-34-5 -Tetrapotassium phosphate 7722-88-5 -Tetmsodium pyrophosphate 15136-87-5 -Trialuminum sodium tetra decahydrogenoctaorthophosphate (dihydrate) 7758-874 -Tricalcium phosphate 7757-87-1 -Trimagnesium phosphate 7778-53-2 -Tripotassium phosphate 7601-54-9 -Trisodium phosphate 7803-51-2 Phosphine 6.3E-02 2.1E+00 N 6.3E-02 N 6.3E-02 N 6.3E-02 N Yes 7664-38-2 Phosphoric Acid Not Volatile Not Volatile 2.1E+00 N 2.1E+00 N 2.1E+00 N Yes 7723-14-0 Phosphorus, White Phthalates 117-81-7 -Bis(2-ethylhexyl)phthalate Not Volatile Not Volatile 1.2E+00 C 1.2E+01 C 1.2E+02 C 85-68-7 -Butyl Benzyl Phthalate 85-70-1 -Butylphthalyl Butylglycolate 84-74-2 -Dibutyl Phthalate 84-66-2 -Diethyl Phthalate 120-61-6 -Dimethylterephthalate 117-84-0 -Octyl Phthalate, di-N- 100-21-0 -Phthalic Acid, P- 8544-9 -Phthalic Anhydride Not Volatile Not Volatile 4.2E+00 N 4.2E+00 N 4.2E+00 N Yes 1918-02-1 Picloram 96-91-3 Picmmic Acid (2-Amino-4,6- dinitrophenol) 88-89-1 Picric Acid(2,4,6-Trinitrophenol) 29232-93-7 Pirimiphos, Methyl 59536-65-1 Polybrominated Biphenyls Not Volatile Not Volatile 3.3E-04 C 3.3E-03 C 3.3E-02 C Polychlorinated Biphenyls (PCBs) 12674-11-2 -Aroclor 1016 1.7E+02 4.7E+01 C 1.4E-01 C 1.4E+00 C 1.4E+O1 C 11104-28-2 -Aroclor 1221 5.3E+00 1.6E+00 C 4.9E-03 C 4.9E-02 C 4.9E-01 C 11141-16-5 -Aroclor 1232 1.6E+00 1.6E+00 C 4.9E-03 C 4.9E-02 C 4.9E-01 C 53469-21-9 -Aroclor 1242 3.5E+00 1.6E+00 C 4.9E-03 C 4.9E-02 C 4.9E-01 C 12672-29-6 -Aroclor 1248 2.7E+00 1.6E+00 C 4.9E-03 C 4.9E-02 C 4.9E-01 C 11097-69-1 -Aroclor 1254 4.3E+00 1.6E+00 C 4.9E-03 C 4.9E-02 C 4.9E-01 C 11096-82-5 -Aroclor 1260 3.6E+00 1.6E+00 C 4.9E-03 C 4.9E-02 C 4.9E-01 C 11126-42-4 -Aroclor 5460 Page 8 0£ 11 North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/ms TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/ms TCR=1.0E-06 THQ=0.2 Basis IASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' 39635-31-9 -Heptuhlorobiphenyl, 2,3,3',4,4',5,5'- (PCB 189) 1.2E+01 8.5E-01 C 2.6E-03 C 2.6E-02 C 2.6E-01 C Yes 52663-72-6 -Hexachlorobiphenyl,2,3',4,4',5,5'- (PCB 167) 9.1E+00 8.5E-01 C 2.6E-03 C 2.6E-02 C 2.6E-01 C Yes 69782-90-7 -Hexachlorobiphenyl, 2,3,3',4,4',5'- (PCB 157) 3.9E+00 8.5E-01 C 2.6E-03 C 2.6E-02 C 2.6E-01 C Yes 38380-08-4 -Hexachlorobiphenyl, 2,3,3',4,4',5- (PCB 156) 4.4E+00 8.5E-01 C 2.6E-03 C 2.6E-02 C 2.6E-01 C Yes 32774-16-6 -Hexachlorobiphenyl, 3,3',4,4',5,5'- (PCB 169) 9.1E-03 8.5E-04 C 2.6E-06 C 2.6E-05 C 2.6E-04 C Yes 65510-44-3 -Pentachlorobiphenyl, 2',3,4,4',5- (PCB 123) 3.3E+00 8.5E-01 C 2.6E-03 C 2.6E-02 C 2.6E-01 C Yes 31508-00-6 -Pentachlorobiphenyl, 2,3',4,4',5- (PCB 118) 2.2E+00 8.5E-01 C 2.6E-03 C 2.6E-02 C 2.6E-01 C Yes 32598-14-4 -Pentachlorobiphenyl, 2,3,3',4,4'- (PCB 105) 2.2E+00 8.5E-01 C 2.6E-03 C 2.6E-02 C 2.6E-01 C Yes 74472-37-0 -Pentachlorobiphenyl, 2,3,4,4',5- (PCB 114) 6.8E+00 8.5E-01 C 2.6E-03 C 2.6E-02 C 2.6E-01 C Yes 57465-28-8 -Pentachlorobiphenyl, 3,3',4,4',5- (PCB 126) 9.5E-04 2.5E-04 C 7.4E-07 C 7.4E-06 C 7.4E-05 C Yes 1336-36-3 -Polychlorinated Biphenyls (high 2.9E+00 1.6E+00 C 4.9E-03 C 4.9E-02 C 4.9E-01 C 1336-36-3 -Polychlorinated ) Biphenyls (low 1.7E+01 9.4E+00 C 2.8E-02 C 2.8E-01 C 2.8E+00 C 1336-36-3 -Polychlorinated Biphenyls (lowest risk) 8.3E+01 4.7E+01 C 1.4E-01 C 1.4E+00 C 1.4E+O1 C 32598-13-3 -Tetruhlorobiphenyl, 3,3',4,4'- (PCB 77) Not Volatile Not Volatile 7.4E-04 C 7.4E-03 C 7.4E-02 C Yes 70362-50-4 -Tetruhlorobiph8e1) 1, 3,4,4',5- (PCB 2.8E-01 8.5E-02 C 2.6E-04 C 2.6E-03 C 2.6E-02 C Yes 9016-87-9 Polymeric Methylene Diphenyl Diisocyanate (PMDI) Not Volatile Not Volatile 1.3E-01 N 1.3E-01 N 1.3E-01 N Yes Polynuclear Aromatic Hydrocarbons (PAHs) 83-32-9 -Acenaphthene 120-12-7 -Anthracene 56-55-3 -Benzra)anthracene 3.4E+02 5.6E+00 C 1.7E-02 C 1.7E-01 C 1.7E+00 C 205-82-3 -Benzo(i)flumanthene Not Volatile Not Volatile 2.6E-02 C 2.6E-01 C 2.6E+00 C 50-32-8 -Benzora)pyrene Not Volatile Not Volatile 4.2E-04 N 4.2E-04 N 4.2E-04 N Yes 205-99-2 -Benzorb)fluoranthene Not Volatile Not Volatile 1.7E-02 C 1.7E-01 C 1.7E+00 C 207-08-9 -Benzork)fluoranthene Not Volatile Not Volatile 1.7E-01 C 1.7E+00 C 1.7E+01 C 91-58-7 -Chloronaphthalene, Beta- 218-01-9 -Chrysene Not Volatile Not Volatile 1.7E+00 C 1.7E+01 C 1.7E+02 C 53-70-3 -Dibenzra,h)anthmcene Not Volatile Not Volatile 1.7E-03 C 1.7E-02 C 1.7E-01 C 192-65-4 -Dibenzo(a,e)pyrene Not Volatile Not Volatile 2.6E-03 C 2.6E-02 C 2.6E-01 C 57-97-6 -Dimethylbenz(a)anthmcene, 7,12- Not Volatile Not Volatile 1.4E-05 C 1.4E-04 C 1.4E-03 C 206-44-0 -Fluoranthene 86-73-7 -Flumene 193-39-5 -Indenor1,2,3-cd)pyrene Not Volatile Not Volatile 1.7E-02 C 1.7E-01 C 1.7E+00 C 90-12-0 -Methylnaphthalene, 1- 91-57-6 -Methylnaphthalene, 2- 91-20-3 -Naphthalene 3.5E+01 2.1E+01 N 8.3E-02 C 6.3E-01 N 6.3E-01 N Yes 57835-92-4 -Nitropyrene, 4- Not Volatile Not Volatile 2.6E-02 C 2.6E-01 C 2.6E+00 C 129-00-0 -Pyrene 29420-49-3 Potassium Perflumobutane Sulfonate 67747-09-5 Prochloraz 26399-36-0 Profluralin 1610-18-0 Prometon 7287-19-6 Prometryn 1918-16-7 Propachlor 709-98-8 Propanil 2312-35-8 Prolawgite 107-19-7 Propargyl Alcohol 139-40-2 Propazine 122-42-9 Propham 60207-90-1 Propiconazole 123-38-6 Propionaldehyde 5.6E+02 5.6E+01 N 1.7E+00 N 1.7E+00 N 1.7E+00 N Yes 103-65-1 Propyl benzene 4.9E+02 7.0E+03 N 2.1E+02 N 2.1E+02 N 2.1E+02 N Yes 115-07-1 Propylene 7.8E+01 2.1E+04 N 6.3E+02 N 6.3E+02 N 6.3E+02 N Yes 57-55-6 Propylene Glycol 6423434 Propylene Glycol Dinitrate Not Volatile Not Volatile 5.6E-02 N 5.6E-02 N 5.6E-02 N Yes 107-98-2 Propylene Glycol Monomethyl Ether 1.1E+07 1.4E+04 N 4.2E+02 N 4.2E+02 N 4.2E+02 N Yes 75-56-9 Propylene Oxide 2.2E+03 2.1E+02 N 7.6E-01 C 6.3E+00 N 6.3E+00 N Yes 23950-58-5 Propyzamide 110-86-1 Pyridine 13593-03-8 Quinalphos 91-22-5 Quinoline 76578-14-8 Quizalofop-ethyl E715557 Refractory Ceramic Fibers Not Volatile Not Volatile 6.3E+00 N 6.3E+00 N 6.3E+00 N Yes Page of 11 North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/ms TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/ms TCR=1.0E-06 THQ=0.2 Basis IASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' 10453-86-8 Resmethrin 299-84-3 Runnel 83-794 Rotenone 94-59-7 Safrole Not Volatile Not Volatile 1.6E-02 C 1.6E-01 C 1.6E+00 C 7783-00-8 Seleniou Acid 778249-2 Selenium Not Volatile Not Volatile 4.2E+00 N 4.2E+00 N 4.2E+00 N Yes 7446-34-6 Selenium Sulfide Not Volatile Not Volatile 4.2E+00 N 4.2E+00 N 4.2E+00 N Yes 74051-80-2 Sethoxydim 7631-86-9 Silica (crystalline, respirable) Not Volatile Not Volatile 6.3E-01 N 6.3E-01 N 6.3E-01 N Yes 7440-224 Silver 122-34-9 Simazine 62476-59-9 Sodium Acifluorfen 26628-22-8 Sodium Azide 148-18-5 Sodium Diethyldithiocarbamate 7681494 Sodium Fluoride Not Volatile Not Volatile 2.7E+00 N 2.7E+00 N 2.7E+00 N Yes 62-74-8 Sodium Fluoroacetate 13718-26-8 Sodium Metavanadate 13472-45-2 1 Sodium Tungstate 10213-10-2 Sodium Tungstate Dihydmte 961-11-5 Stirofos (Tetrachlorovinphos) 7440-24-6 Strontium, Stable 57-24-9 Strychnine 100-42-5 Styrene 1.9E+03 7.0E+03 N 2.1E+02 N 2.1E+02 N 2.1E+02 N Yes NA Styrene-Acrylonitrile (SAN) Trimer 126-33-0 Sulfolane Not Volatile Not Volatile 4.2E-01 N 4.2E-01 N 4.2E-01 N Yes 80-07-9 Sulfonylbis(4-chlorobenzene), 1,1'- 7446-11-9 Sulfur Trioxide 7.0E+00 N 2.1E-01 N 2.1E-01 N 2.1E-01 N Yes 7664-93-9 Sulfuric Acid Not Volatile Not Volatile 2.1E-01 N 2.1E-01 N 2.1E-01 N Yes 140-57-8 Sulfurous acid, 2-chloroethyl 2-[4- (1,1-dimethylethyl)phenoxy]-1- methylethyl ester Not Volatile Not Volatile 4.0E-01 C 4.0E+00 C 4.0E+01 C 21564-17-0 TCMTB 34014-18-1 Tebuthiumn 3383-96-8 Temephos 5902-51-2 Terbacil 13071-79-9 Terbufos 886-50-0 Terbutryn 543643-1 Tetmbromodiphenyl ether, 2,2',4,4'- (BDE47) 95-94-3 Tetrachlorobenzene, 1,2,4,5- 630-20-6 Tetrachloroethane, 1,1,1,2- 3.7E+01 1.3E+02 C 3.8E-01 C 3.8E+00 C 3.8E+01 C 79-34-5 Tetrachloroethane, 1,1,2,2- 3.2E+01 1.6E+01 C 4.8E-02 C 4.8E-01 C 4.8E+00 C 127-18-4 Tetrachloroethylene 1.2E+01 2.8E+02 N 8.3E+00 N 8.3E+00 N 8.3E+00 N Yes 58-90-2 Tetrachlorophenol, 2,3,4,6- 5216-25-1 Tetrachlorotoluene, p- alpha, alpha, alpha- 3689-24-5 Tetraethyl Dithiopyrophosphate 811-97-2 Tetrafluoroethane, 1,1,1,2- 8.2E+03 5.6E+05 N 1.7E+04 N 1.7E+04 N 1.7E+04 N Yes 479-45-8 Tetryl (Trinitmphenylmethylnitramine) 1314-32-5 Thallic Oxide 10102-45-1 Thallium (I) Nitrate 7440-28-0 Thallium (Soluble Salts) 563-68-8 Thallium Acetate 6533-73-9 Thallium Carbonate 7791-12-0 Thallium Chloride 12039-52-0 Thallium Selenite 7446-18-6 Thallium Sulfate 79277-27-3 Thifensulfuron-methyl 28249-77-6 Thiobencarb 111-48-8 Thiodiglycol 39196-18-4 Thiofanox 23564-05-8 Thiophanate, Methyl 137-26-8 Thiram 7440-31-5 Tin 755045-0 Titanium Tetrachloride 7.0E-01 N 2.1E-02 N 2.1E-02 N 2.1E-02 N Yes 108-88-3 Toluene 3.8E+03 3.5E+04 N 1.0E+03 N 1.0E+03 N 1.0E+03 N Yes 584-84-9 Toluene-2,4-diisocyanate 3.7E+00 5.6E-02 N 1.7E-03 N 1.7E-03 N 1.7E-03 N Yes 95-70-5 Toluene-2,5-diamine 91-08-7 Toluene-2,6-diisocyanate 3.7E+00 5.6E-02 N 1.7E-03 N 1.7E-03 N 1.7E-03 N Yes 99-94-5 Toluic Acid, p- 95-534 Toluidine, o- (Methylaniline, 2-) Not Volatile Not Volatile 5.5E-02 C 5.5E-01 C 5.5E+00 C 106-49-0 Toluidine,p- E1790670 Total Petroleum Hydrocarbons (Aliphatic High) E1790666 Total Petroleum Hydrocarbons (Aliphatic Low) 1.7E+00 4.2E+03 N 1.3E+02 N 1.3E+02 N 1.3E+02 N Yes E1790668 Total Petroleum Hydrocarbons (Aliphatic Medium) 1.5E-01 7.0E+02 N 2.1E+01 N 2.1E+01 N 2.1E+01 N Yes E1790676 Total Petroleum Hydrocarbons (Aromatic High) Page 10 oft I North Carolina Department of Environmental Quality Residential Vapor Intrusion Screening Levels February 2018 (based on November 2017 USEPA Regional Screening Tables) CAS # Chemical Name: Ground Water Screening Level (GWSL) ug/L TCR=1.0E-05 THQ=0.2 Sub -slab and Exterior Soil Gas Screening Level (SGSL) ug/m' TCR=1.0E-05 THQ=0.2 Basis IASL (A) ug/ms TCR=1.0E-06 THQ=0.2 Basis IASL (B) ng/m TCR=1.0E-05 THQ=0.2 Basis z IASL (C) ug/m TCR=1.0E-04 THQ=0.2 Basis Does Chemical Have a Non- Cancer Effect?' E1790672 Total Petroleum Hydrocarbons (Aromatic Low) 2.8E+01 2.1E+02 N 6.3E+00 N 6.3E+00 N 6.3E+00 N Yes E1790674 Total Petroleum Hydrocarbons (Aromatic Medium) 3.2E+01 2.1E+01 N 6.3E-01 N 6.3E-01 N 6.3E-01 N Yes 8001-35-2 Toxaphene Not Volatile Not Volatile 8.8E-03 C 8.8E-02 C 8.8E-01 C 66841-25-6 Tmlomethrin 688-73-3 Tri-n-butyltin 102-76-1 Triacetin 43121-43-3 Triadimefon 2303-17-5 Triallate 82097-50-5 Triasulfuron 101200-48-0 Tribenuron-methyl 615-54-3 Tribromobenzene, 1,2,4- 118-79-6 Tribromophenol, 2,4,6- 126-73-8 Tributyl Phosphate E1790678 Tributyltin Compounds 56-35-9 Tributyltin Oxide 76-13-1 Trichloro-1,2,2-trifluoroethme, 1,1,2- 4.8E+01 3.5E+04 N 1.0E+03 N 1.0E+03 N 1.0E+03 N Yes 76-03-9 Trichloroacetic Acid 33663-50-2 Trichloroaniline HCI, 2,4,6- 634-93-5 Trichloroaniline, 2,4,6- 87-61-6 Trichlorobemmne, 1,2,3- 120-82-1 Trichlorobenzene, 1,2,4- 7.2E+00 1.4E+01 N 4.2E-01 N 4.2E-01 N 4.2E-01 N Yes 71-55-6 Trichloroethane, 1,1,1- 1.5E+03 3.5E+04 N 1.0E+03 N 1.0E+03 N 1.0E+03 N Yes 79-00-5 Trichloroethane, 1,1,2- 1.2E+00 1.4E+00 N 4.2E-02 N 4.2E-02 N 4.2E-02 N Yes 79-01-6 Trichloroethylene 1.0E+00 1.4E+01 N 4.2E-01 N 4.2E-01 N 4.2E-01 N Yes 75-694 Trichlorofluoromethane 95-954 Trichlorophenol, 2,4,5- 88-06-2 Trichlorophenol, 2,4,6- Not Volatile Not Volatile 9.1E-01 C 9.1E+00 C 9.1E+01 C 93-76-5 Trichlorophenoxyacetic Acid, 2,4,5- 93-72-1 Trichlorophenoxypropionic acid, - 2,4,5 598-77-6 Trichloropropane, 1,1,2- 96-184 Trichloropropane, 1,2,3- 4.5E+00 2.1E+00 N 6.3E-02 N 6.3E-02 N 6.3E-02 N Yes 96-19-5 Trichloropropee, 1,2,3- 8.7E-02 2.1E+00 N 6.3E-02 N 6.3E-02 N 6.3E-02 N Yes 1330-78-5 Tricresyl Phosphate (TCP) 58138-08-2 Tridiphane 121-44-8 Triethylamine 2.4E+02 4.9E+01 N 1.5E+00 N 1.5E+00 N 1.5E+00 N Yes 112-27-6 Triethylene Glycol 420-46-2 Trifluoroethane, 1,1,1- 1.3E+02 1.4E+05 N 4.2E+03 N 4.2E+03 N 4.2E+03 N Yes 1582-09-8 Triflumlin 512-56-1 Trimethyl Phosphate 526-73-8 Trimethylbenzene, 1,2,3- 7.0E+01 4.2E+02 N 1.3E+01 N 1.3E+01 N 1.3E+01 N Yes 95-63-6 Trimethylbenzene, 1,2,4- 5.0E+01 4.2E+02 N 1.3E+01 N 1.3E+01 N 1.3E+01 N Yes 108-67-8 Trimethylbenzene, 1,3,5- 3.5E+01 4.2E+02 N 1.3E+01 N 1.3E+01 N 1.3E+01 N Yes 25167-70-8 Trimethylpentene, 2,4,4- 99-354 Trinitrobenzene, 1,3,5- 118-96-7 Trinitrotoluene, 2,4,6- 791-28-6 Triphenylphosphine Oxide 13674-87-8 Tris(1,3-Dichloro-2-propyl) Phosphate 13674-84-5 Tris(1-chloro-2-propyl)phosphate 126-72-7 Tris(2,3-dibromopropyl)phosphate 4.8E+01 1.4E+00 C 4.3E-03 C 4.3E-02 C 4.3E-01 C 115-96-8 Tris(2-chloroethyl)phosphate 7842-2 Tris(2-ethylhexyl)phosphate 7440-33-7 Tungsten E715565 Uranium (Soluble Salts) Not Volatile Not Volatile 8.3E-03 N 8.3E-03 N 8.3E-03 N Yes 51-79-6 Urethane Not Volatile Not Volatile 3.5E-03 C 3.5E-02 C 3.5E-01 C 1314-62-1 Vanadium Pentoxide Not Volatile Not Volatile 3.4E-04 C 1.5E-03 N 1.5E-03 N Yes 7440-62-2 Vanadium and Compounds Not Volatile Not Volatile 2.1E-02 N 2.1E-02 N 2.1E-02 N Yes 1929-77-7 Vemolate 50471-44-8 Vinclozolin 108-05-4 Vinyl Acetate 2.0E+03 1.4E+03 N 4.2E+01 N 4.2E+01 N 4.2E+01 N Yes 593-60-2 Vinyl Bromide 1.2E+00 2.1E+01 N 8.8E-02 C 6.3E-01 N 6.3E-01 N Yes 75-014 Vinyl Chloride 1.5E+00 5.6E+O1 C 1.7E-01 C 1.7E+00 C 1.7E+01 C Yes 81-81-2 Warfarin 106-42-3 Xylene, P- 7.4E+01 7.0E+02 N 2.1E+01 N 2.1E+01 N 2.1E+01 N Yes 108-38-3 Xylene,m- 7.1E+01 7.0E+02 N 2.1E+01 N 2.1E+01 N 2.1E+01 N Yes 9547-6 Xylene,o- 9.8E+01 7.0E+02 N 2.1E+01 N 2.1E+01 N 2.1E+01 N Yes 1330-20-7 Xylenes 7.7E+01 7.0E+02 N 2.1E+01 N 2.1E+01 N 2.1E+01 N Yes 1314-84-7 Zinc Phosphide 7440-66-6 Zinc and Compounds 12122-67-7 Zineb 7440-67-7 Zirconium 1) TCR = Target Cancer Risk; THQ=Target Hazard Quotient; C= Carcinogenic; N = Non -Carcinogenic 2) Indoor A r/Crawlspace Screening Levels at target risk 1.0E-04 (IASL C) to be used if only one carcinogen is present. 3) If more than five compounds with non -cancer effects are present risk should be evaluated using NCDEQ Risk Calculator. Page 11 oft I RDFr \1 Environmental Consulting 4012 Ridgebrook Bluffs Dr. I Raleigh, NC 27603 (919) 389-7747 1 info@rdhec.com APPENDIX D LABORATORY REPORT AND CHAIN OF CUSTODY FORM icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 September 25, 2020 Robert Hill RDH Environmental Consulting 4012 Ridgebrook Bluffs Drive Raleigh, NC 27603 Project Location: Wilmington, NC Client Job Number: Project Number: 2009.00 Laboratory Work Order Number: 20I1007 Enclosed are results of analyses for samples received by the laboratory on September 11, 2020. If you have any questions concerning this report, please feel free to contact me. Sincerely, I,&, �. A�� Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 RDH Environmental Consulting REPORT DATE: 9/25/2020 4012 Ridgebrook Bluffs Drive Raleigh, NC 27603 PURCHASE ORDER NUMBER: ATTN: Robert Hill PROJECT NUMBER: 2009.00 ANALYTICAL SUMMARY WORK ORDER NUMBER: 20I1007 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Wilmington, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB SG-l/Boiler Room (S) 20I1007-01 Air EPA TO-15 SG-2/Storage (SE) 20I1007-02 Air EPA TO-15 SG-3/Storage (E) 20I1007-03 Air EPA TO-15 SG-4/Storage (SW) 20I1007-04 Air EPA TO-15 SG-5/Laundry Area (SE) 20I1007-05 Air EPA TO-15 SG-5 DUP/LaundryArea (SE) 20I1007-06 Air EPA TO-15 SG-6/Laundry Area (NE) 20I1007-07 Air EPA TO-15 SG-7/Laundry Area (SW) 20I1007-08 Air EPA TO-15 SG-8/Laundry Area (NW) 20I1007-09 Air EPA TO-15 SG-9/Ironing/Sorting (NW) 20I1007-10 Air Unused Can/Reg #2300/4134 20I1007-11 Air Unused Can/Reg #2116/4355 20I1007-12 Air Page 2 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. d� Lisa A. Worthington Technical Representative Page 3 of 35 icon-tes w . ANALYTICAL LABORATORY Project Location: Wilmington, NC Date Received: 9/11/2020 Field Sample #: SG-1/Boiler Room (S) Sample ID: 20I1007-01 Sample Matrix: Air Sampled: 9/10/2020 16:40 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Work Order: 20I1007 Sub Description/Location: Initial Vacuum(in Hg): -30 Canister ID: 2096 Final Vacuum(in Hg): -5 Canister Size: 1 liter Receipt Vacuum(in Hg): -6.2 Flow Controller ID: -6.2 Flow Controller Type: Fixed -Orifice Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results ILL MDL Dilution Analyzed Analyst Acetone 26 8.0 4.8 62 19 11 4 9/22/20 22:40 BRF Benzene 1.1 0.20 0.058 3.6 0.64 0.19 4 9/22/20 22:40 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/22/20 22:40 BRF Bromodichloromethane ND 0.20 0.056 ND 1.3 0.37 4 9/22/20 22:40 BRF Bromoform ND 0.20 0.069 ND 2.1 0.71 4 9/22/20 22:40 BRF Bromomethane ND 0.20 0.11 ND 0.78 0.41 4 9/22/20 22:40 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 9/22/20 22:40 BRF 2-Butanone (MEK) 3.4 8.0 0.66 J 10 24 2.0 4 9/22/20 22:40 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/22/20 22:40 BRF Carbon Tetrachloride ND 0.20 0.053 ND 1.3 0.33 4 9/22/20 22:40 BRF Chlorobenzene ND 0.20 0.048 ND 0.92 0.22 4 9/22/20 22:40 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 9/22/20 22:40 BRF Chloroform 1.3 0.20 0.048 6.2 0.98 0.24 4 9/22/20 22:40 BRF Chloromethane ND 0.40 0.15 ND 0.83 0.32 4 9/22/20 22:40 BRF Cyclohexane ND 0.20 0.098 ND 0.69 0.34 4 9/22/20 22:40 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/22/20 22:40 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.052 ND 1.5 0.40 4 9/22/20 22:40 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/22/20 22:40 BRF 1,3-Dichlorobenzene ND 0.20 0.073 ND 1.2 0.44 4 9/22/20 22:40 BRF 1,4-Dichlorobenzene ND 0.20 0.045 ND 1.2 0.27 4 9/22/20 22:40 BRF Dichlorodifluoromethane (Freon 12) 1.5 0.20 0.063 7.2 0.99 0.31 4 9/22/20 22:40 BRF 1, 1 -Dichloroethane ND 0.20 0.063 ND 0.81 0.25 4 9/22/20 22:40 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/22/20 22:40 BRF 1, 1 -Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 9/22/20 22:40 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/22/20 22:40 BRF trans-1,2-Dichloroethylene ND 0.20 0.059 ND 0.79 0.23 4 9/22/20 22:40 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/22/20 22:40 BRF cis- 1,3-Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/22/20 22:40 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.067 ND 0.91 0.30 4 9/22/20 22:40 BRF 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 9/22/20 22:40 BRF 1,4-Dioxane ND 2.0 0.56 ND 7.2 2.0 4 9/22/20 22:40 BRF Ethanol 140 8.0 2.4 260 15 4.6 4 9/22/20 22:40 BRF Ethyl Acetate ND 2.0 1.2 ND 7.2 4.3 4 9/22/20 22:40 BRF Ethylbenzene 3.8 0.20 0.042 17 0.87 0.18 4 9/22/20 22:40 BRF 4-Ethyltoluene 2.0 0.20 0.062 10 0.98 0.30 4 9/22/20 22:40 BRF Heptane 1.3 0.20 0.086 5.2 0.82 0.35 4 9/22/20 22:40 BRF Hexachlorobutadiene ND 0.20 0.088 ND 2.1 0.94 4 9/22/20 22:40 BRF Hexane ND 8.0 0.36 ND 28 1.3 4 9/22/20 22:40 BRF 2-Hexanone (MBK) ND 0.20 0.11 ND 0.82 0.46 4 9/22/20 22:40 BRF Isopropanol 3.1 8.0 1.8 J 7.6 20 4.5 4 9/22/20 22:40 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/22/20 22:40 BRF Methylene Chloride ND 2.0 0.46 ND 6.9 1.6 4 9/22/20 22:40 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 9/22/20 22:40 BRF Naphthalene ND 0.20 0.11 ND 1.0 0.59 4 9/22/20 22:40 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/22/20 22:40 BRF Styrene 0.30 0.20 0.057 1.3 0.85 0.24 4 9/22/20 22:40 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.053 ND 1.4 0.37 4 9/22/20 22:40 BRF Page 4 of 35 icon-tes w . ANALYTICAL LABORATORY Project Location: Wilmington, NC Date Received: 9/11/2020 Field Sample #: SG-1/Boiler Room (S) Sample ID: 20I1007-01 Sample Matrix: Air Sampled: 9/ 10/2020 16:40 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2096 Canister Size: 1 liter Flow Controller ID: -6.2 Sample Type: 10 min Work Order: 20I1007 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -6.2 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 7.5 0.20 0.065 51 1.4 0.44 4 9/22/20 22:40 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/22/20 22:40 BRF Toluene 15 0.20 0.058 56 0.75 0.22 4 9/22/20 22:40 BRF 1,2,4-Trichlorobenzene ND 0.20 0.12 ND 1.5 0.91 4 9/22/20 22:40 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.065 ND 1.1 0.36 4 9/22/20 22:40 BRF 1,1,2-Trichloroethane ND 0.20 0.073 ND 1.1 0.40 4 9/22/20 22:40 BRF Trichloroethylene 0.52 0.20 0.074 2.8 1.1 0.40 4 9/22/20 22:40 BRF Trichlorofluoromethane (Freon 11) 0.20 0.80 0.15 J 1.1 4.5 0.85 4 9/22/20 22:40 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 9/22/20 22:40 BRF 1,2,4-Trimethylbenzene ND 0.20 0.046 ND 0.98 0.22 4 9/22/20 22:40 BRF 1,3,5-Trimethylbenzene 1.8 0.20 0.052 8.8 0.98 0.26 4 9/22/20 22:40 BRF Vinyl Acetate ND 4.0 0.56 ND 14 2.0 4 9/22/20 22:40 BRF Vinyl Chloride ND 0.20 0.11 ND 0.51 0.29 4 9/22/20 22:40 BRF m&p-Xylene 16 0.40 0.070 71 1.7 0.30 4 9/22/20 22:40 BRF o-Xylene 6.2 0.20 0.054 27 0.87 0.23 4 9/22/20 22:40 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 102 % REC Limits 70-130 9/22/20 22:40 Page 5 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wilmington, NC Sample Description/Location: Work Order: 20I1007 Date Received: 9/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SG-2/Storage (SE) Canister ID: 2112 Final Vacuum(in Hg): -5 Sample ID: 20I1007-02 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.6 Sample Matrix: Air Flow Controller ID: -4.6 Flow Controller Type: Fixed -Orifice Sampled: 9/10/2020 17:03 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 200 8.0 4.8 470 19 11 4 9/22/20 23:20 BRF Benzene 1.7 0.20 0.058 5.3 0.64 0.19 4 9/22/20 23:20 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/22/20 23:20 BRF Bromodichloromethane ND 0.20 0.056 ND 1.3 0.37 4 9/22/20 23:20 BRF Bromoform ND 0.20 0.069 ND 2.1 0.71 4 9/22/20 23:20 BRF Bromomethane ND 0.20 0.11 ND 0.78 0.41 4 9/22/20 23:20 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 9/22/20 23:20 BRF 2-Butanone (MEK) 21 8.0 0.66 61 24 2.0 4 9/22/20 23:20 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/22/20 23:20 BRF Carbon Tetrachloride ND 0.20 0.053 ND 1.3 0.33 4 9/22/20 23:20 BRF Chlorobenzene ND 0.20 0.048 ND 0.92 0.22 4 9/22/20 23:20 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 9/22/20 23:20 BRF Chloroform 0.92 0.20 0.048 4.5 0.98 0.24 4 9/22/20 23:20 BRF Chloromethane ND 0.40 0.15 ND 0.83 0.32 4 9/22/20 23:20 BRF Cyclohexane ND 0.20 0.098 ND 0.69 0.34 4 9/22/20 23:20 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/22/20 23:20 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.052 ND 1.5 0.40 4 9/22/20 23:20 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/22/20 23:20 BRF 1,3-Dichlorobenzene ND 0.20 0.073 ND 1.2 0.44 4 9/22/20 23:20 BRF 1,4-Dichlorobenzene ND 0.20 0.045 ND 1.2 0.27 4 9/22/20 23:20 BRF Dichlorodifluoromethane (Freon 12) 250 1.0 0.31 1200 4.9 1.6 20 9/23/20 0:00 BRF 1,1-Dichloroethane ND 0.20 0.063 ND 0.81 0.25 4 9/22/20 23:20 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/22/20 23:20 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 9/22/20 23:20 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/22/20 23:20 BRF trans-1,2-Dichloroethylene ND 0.20 0.059 ND 0.79 0.23 4 9/22/20 23:20 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/22/20 23:20 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/22/20 23:20 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.067 ND 0.91 0.30 4 9/22/20 23:20 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 9/22/20 23:20 BRF 1,4-Dioxane 2.4 2.0 0.56 8.8 7.2 2.0 4 9/22/20 23:20 BRF Ethanol 880 40 12 1700 75 23 20 9/23/20 0:00 BRF Ethyl Acetate 11 2.0 1.2 39 7.2 4.3 4 9/22/20 23:20 BRF Ethylbenzene 3.0 0.20 0.042 13 0.87 0.18 4 9/22/20 23:20 BRF 4-Ethyltoluene 1.4 0.20 0.062 6.7 0.98 0.30 4 9/22/20 23:20 BRF Heptane 1.0 0.20 0.086 4.2 0.82 0.35 4 9/22/20 23:20 BRF Hexachlorobutadiene ND 0.20 0.088 ND 2.1 0.94 4 9/22/20 23:20 BRF Hexane ND 8.0 0.36 ND 28 1.3 4 9/22/20 23:20 BRF 2-Hexanone (MBK) ND 0.20 0.11 ND 0.82 0.46 4 9/22/20 23:20 BRF Isopropanol 30 8.0 1.8 73 20 4.5 4 9/22/20 23:20 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/22/20 23:20 BRF Methylene Chloride ND 2.0 0.46 ND 6.9 1.6 4 9/22/20 23:20 BRF 4-Methyl-2-pentanone (MIBK) 7.8 0.20 0.10 32 0.82 0.43 4 9/22/20 23:20 BRF Naphthalene 1.1 0.20 0.11 5.7 1.0 0.59 4 9/22/20 23:20 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/22/20 23:20 BRF Styrene 0.54 0.20 0.057 2.3 0.85 0.24 4 9/22/20 23:20 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.053 ND 1.4 0.37 4 9/22/20 23:20 BRF Page 6 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wilmington, NC Sample Description/Location: Work Order: 20I1007 Date Received: 9/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SG-2/Storage (SE) Canister ID: 2112 Final Vacuum(in Hg): -5 Sample ID: 20I1007-02 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.6 Sample Matrix: Air Flow Controller ID: -4.6 Flow Controller Type: Fixed -Orifice Sampled: 9/10/2020 17:03 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 1.4 0.20 0.065 9.2 1.4 0.44 4 9/22/20 23:20 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/22/20 23:20 BRF Toluene 11 0.20 0.058 40 0.75 0.22 4 9/22/20 23:20 BRF 1,2,4-Trichlorobenzene ND 0.20 0.12 ND 1.5 0.91 4 9/22/20 23:20 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.065 ND 1.1 0.36 4 9/22/20 23:20 BRF 1,1,2-Trichloroethane ND 0.20 0.073 ND 1.1 0.40 4 9/22/20 23:20 BRF Trichloroethylene 2.0 0.20 0.074 11 1.1 0.40 4 9/22/20 23:20 BRF Trichlorofluoromethane (Freon 11) 0.22 0.80 0.15 J 1.3 4.5 0.85 4 9/22/20 23:20 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 9/22/20 23:20 BRF 1,2,4-Trimethylbenzene ND 0.20 0.046 ND 0.98 0.22 4 9/22/20 23:20 BRF 1,3,5-Trimethylbenzene 1.2 0.20 0.052 6.1 0.98 0.26 4 9/22/20 23:20 BRF Vinyl Acetate ND 4.0 0.56 ND 14 2.0 4 9/22/20 23:20 BRF Vinyl Chloride ND 0.20 0.11 ND 0.51 0.29 4 9/22/20 23:20 BRF m&p-Xylene 10 0.40 0.070 43 1.7 0.30 4 9/22/20 23:20 BRF o-Xylene 3.9 0.20 0.054 17 0.87 0.23 4 9/22/20 23:20 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 101 70-130 9/23/20 0:00 4-Bromofluorobenzene (1) 103 70-130 9/22/20 23:20 Page 7 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wilmington, NC Sample Description/Location: Work Order: 20I1007 Date Received: 9/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SG-3/Storage (E) Canister ID: 2235 Final Vacuum(in Hg): -5 Sample ID: 20I1007-03 Canister Size: 1 liter Receipt Vacuum(in Hg): -5 Sample Matrix: Air Flow Controller ID: -5 Flow Controller Type: Fixed -Orifice Sampled: 9/10/2020 17:29 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 330 20 12 790 48 29 10 9/23/20 1:21 BRF Benzene 0.90 0.20 0.058 2.9 0.64 0.19 4 9/23/20 0:41 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/23/20 0:41 BRF Bromodichloromethane ND 0.20 0.056 ND 1.3 0.37 4 9/23/20 0:41 BRF Bromoform ND 0.20 0.069 ND 2.1 0.71 4 9/23/20 0:41 BRF Bromomethane ND 0.20 0.11 ND 0.78 0.41 4 9/23/20 0:41 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 9/23/20 0:41 BRF 2-Butanone (MEK) 11 8.0 0.66 32 24 2.0 4 9/23/20 0:41 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/23/20 0:41 BRF Carbon Tetrachloride ND 0.20 0.053 ND 1.3 0.33 4 9/23/20 0:41 BRF Chlorobenzene ND 0.20 0.048 ND 0.92 0.22 4 9/23/20 0:41 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 9/23/20 0:41 BRF Chloroform 0.23 0.20 0.048 1.1 0.98 0.24 4 9/23/20 0:41 BRF Chloromethane ND 0.40 0.15 ND 0.83 0.32 4 9/23/20 0:41 BRF Cyclohexane ND 0.20 0.098 ND 0.69 0.34 4 9/23/20 0:41 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/23/20 0:41 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.052 ND 1.5 0.40 4 9/23/20 0:41 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/23/20 0:41 BRF 1,3-Dichlorobenzene ND 0.20 0.073 ND 1.2 0.44 4 9/23/20 0:41 BRF 1,4-Dichlorobenzene ND 0.20 0.045 ND 1.2 0.27 4 9/23/20 0:41 BRF Dichlorodifluoromethane (Freon 12) 26 0.20 0.063 130 0.99 0.31 4 9/23/20 0:41 BRF 1,1-Dichloroethane ND 0.20 0.063 ND 0.81 0.25 4 9/23/20 0:41 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/23/20 0:41 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 9/23/20 0:41 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/23/20 0:41 BRF trans-1,2-Dichloroethylene ND 0.20 0.059 ND 0.79 0.23 4 9/23/20 0:41 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/23/20 0:41 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/23/20 0:41 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.067 ND 0.91 0.30 4 9/23/20 0:41 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 9/23/20 0:41 BRF 1,4-Dioxane ND 2.0 0.56 ND 7.2 2.0 4 9/23/20 0:41 BRF Ethanol 260 20 6.1 490 38 11 10 9/23/20 1:21 BRF Ethyl Acetate ND 2.0 1.2 ND 7.2 4.3 4 9/23/20 0:41 BRF Ethylbenzene 2.2 0.20 0.042 9.7 0.87 0.18 4 9/23/20 0:41 BRF 4-Ethyltoluene 1.3 0.20 0.062 6.2 0.98 0.30 4 9/23/20 0:41 BRF Heptane 0.80 0.20 0.086 3.3 0.82 0.35 4 9/23/20 0:41 BRF Hexachlorobutadiene ND 0.20 0.088 ND 2.1 0.94 4 9/23/20 0:41 BRF Hexane 0.98 8.0 0.36 J 3.5 28 1.3 4 9/23/20 0:41 BRF 2-Hexanone (MBK) ND 0.20 0.11 ND 0.82 0.46 4 9/23/20 0:41 BRF Isopropanol 96 8.0 1.8 240 20 4.5 4 9/23/20 0:41 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/23/20 0:41 BRF Methylene Chloride ND 2.0 0.46 ND 6.9 1.6 4 9/23/20 0:41 BRF 4-Methyl-2-pentanone (MIBK) 4.1 0.20 0.10 17 0.82 0.43 4 9/23/20 0:41 BRF Naphthalene 0.66 0.20 0.11 3.4 1.0 0.59 4 9/23/20 0:41 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/23/20 0:41 BRF Styrene 0.18 0.20 0.057 J 0.75 0.85 0.24 4 9/23/20 0:41 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.053 ND 1.4 0.37 4 9/23/20 0:41 BRF Page 8 of 35 icon-tes w . ANALYTICAL LABORATORY Project Location: Wilmington, NC Date Received: 9/11/2020 Field Sample #: SG-3/Storage (E) Sample ID: 20I1007-03 Sample Matrix: Air Sampled: 9/ 10/2020 17:29 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2235 Canister Size: 1 liter Flow Controller ID: -5 Sample Type: 10 min Work Order: 20I1007 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.82 0.20 0.065 5.6 1.4 0.44 4 9/23/20 0:41 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/23/20 0:41 BRF Toluene 8.0 0.20 0.058 30 0.75 0.22 4 9/23/20 0:41 BRF 1,2,4-Trichlorobenzene ND 0.20 0.12 ND 1.5 0.91 4 9/23/20 0:41 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.065 ND 1.1 0.36 4 9/23/20 0:41 BRF 1,1,2-Trichloroethane ND 0.20 0.073 ND 1.1 0.40 4 9/23/20 0:41 BRF Trichloroethylene 1.1 0.20 0.074 6.0 1.1 0.40 4 9/23/20 0:41 BRF Trichlorofluoromethane (Freon 11) 0.24 0.80 0.15 J 1.3 4.5 0.85 4 9/23/20 0:41 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 9/23/20 0:41 BRF 1,2,4-Trimethylbenzene ND 0.20 0.046 ND 0.98 0.22 4 9/23/20 0:41 BRF 1,3,5-Trimethylbenzene 1.2 0.20 0.052 5.7 0.98 0.26 4 9/23/20 0:41 BRF Vinyl Acetate ND 4.0 0.56 ND 14 2.0 4 9/23/20 0:41 BRF Vinyl Chloride ND 0.20 0.11 ND 0.51 0.29 4 9/23/20 0:41 BRF m&p-Xylene 9.0 0.40 0.070 39 1.7 0.30 4 9/23/20 0:41 BRF o-Xylene 3.7 0.20 0.054 16 0.87 0.23 4 9/23/20 0:41 BRF Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 99.0 70-130 101 70-130 9/23/20 1:21 9/23/20 0:41 Page 9 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wilmington, NC Sample Description/Location: Work Order: 20I1007 Date Received: 9/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SG-4/Storage (SW) Canister ID: 2257 Final Vacuum(in Hg): -5 Sample ID: 20I1007-04 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Air Flow Controller ID: -5.2 Flow Controller Type: Fixed -Orifice Sampled: 9/10/2020 17:55 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 99 8.0 4.8 240 19 11 4 9/23/20 2:02 BRF Benzene 0.36 0.20 0.058 1.2 0.64 0.19 4 9/23/20 2:02 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/23/20 2:02 BRF Bromodichloromethane ND 0.20 0.056 ND 1.3 0.37 4 9/23/20 2:02 BRF Bromoform ND 0.20 0.069 ND 2.1 0.71 4 9/23/20 2:02 BRF Bromomethane ND 0.20 0.11 ND 0.78 0.41 4 9/23/20 2:02 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 9/23/20 2:02 BRF 2-Butanone (MEK) 4.2 8.0 0.66 J 12 24 2.0 4 9/23/20 2:02 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/23/20 2:02 BRF Carbon Tetrachloride ND 0.20 0.053 ND 1.3 0.33 4 9/23/20 2:02 BRF Chlorobenzene ND 0.20 0.048 ND 0.92 0.22 4 9/23/20 2:02 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 9/23/20 2:02 BRF Chloroform 10 0.20 0.048 50 0.98 0.24 4 9/23/20 2:02 BRF Chloromethane ND 0.40 0.15 ND 0.83 0.32 4 9/23/20 2:02 BRF Cyclohexane ND 0.20 0.098 ND 0.69 0.34 4 9/23/20 2:02 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/23/20 2:02 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.052 ND 1.5 0.40 4 9/23/20 2:02 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/23/20 2:02 BRF 1,3-Dichlorobenzene ND 0.20 0.073 ND 1.2 0.44 4 9/23/20 2:02 BRF 1,4-Dichlorobenzene ND 0.20 0.045 ND 1.2 0.27 4 9/23/20 2:02 BRF Dichlorodifluoromethane (Freon 12) 8.7 0.20 0.063 43 0.99 0.31 4 9/23/20 2:02 BRF 1,1-Dichloroethane ND 0.20 0.063 ND 0.81 0.25 4 9/23/20 2:02 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/23/20 2:02 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 9/23/20 2:02 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/23/20 2:02 BRF trans-1,2-Dichloroethylene ND 0.20 0.059 ND 0.79 0.23 4 9/23/20 2:02 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/23/20 2:02 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/23/20 2:02 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.067 ND 0.91 0.30 4 9/23/20 2:02 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 9/23/20 2:02 BRF 1,4-Dioxane ND 2.0 0.56 ND 7.2 2.0 4 9/23/20 2:02 BRF Ethanol 74 8.0 2.4 140 15 4.6 4 9/23/20 2:02 BRF Ethyl Acetate ND 2.0 1.2 ND 7.2 4.3 4 9/23/20 2:02 BRF Ethylbenzene 1.9 0.20 0.042 8.2 0.87 0.18 4 9/23/20 2:02 BRF 4-Ethyltoluene 1.4 0.20 0.062 6.8 0.98 0.30 4 9/23/20 2:02 BRF Heptane 0.52 0.20 0.086 2.1 0.82 0.35 4 9/23/20 2:02 BRF Hexachlorobutadiene ND 0.20 0.088 ND 2.1 0.94 4 9/23/20 2:02 BRF Hexane ND 8.0 0.36 ND 28 1.3 4 9/23/20 2:02 BRF 2-Hexanone (MBK) ND 0.20 0.11 ND 0.82 0.46 4 9/23/20 2:02 BRF Isopropanol 12 8.0 1.8 30 20 4.5 4 9/23/20 2:02 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/23/20 2:02 BRF Methylene Chloride ND 2.0 0.46 ND 6.9 1.6 4 9/23/20 2:02 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 9/23/20 2:02 BRF Naphthalene 1.2 0.20 0.11 6.3 1.0 0.59 4 9/23/20 2:02 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/23/20 2:02 BRF Styrene ND 0.20 0.057 ND 0.85 0.24 4 9/23/20 2:02 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.053 ND 1.4 0.37 4 9/23/20 2:02 BRF Page 10 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wilmington, NC Sample Description/Location: Work Order: 20I1007 Date Received: 9/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SG-4/Storage (SW) Canister ID: 2257 Final Vacuum(in Hg): -5 Sample ID: 20I1007-04 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Air Flow Controller ID: -5.2 Flow Controller Type: Fixed -Orifice Sampled: 9/10/2020 17:55 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene 9.6 0.20 0.065 65 1.4 0.44 4 9/23/20 2:02 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/23/20 2:02 BRF Toluene 4.7 0.20 0.058 18 0.75 0.22 4 9/23/20 2:02 BRF 1,2,4-Trichlorobenzene ND 0.20 0.12 ND 1.5 0.91 4 9/23/20 2:02 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.065 ND 1.1 0.36 4 9/23/20 2:02 BRF 1,1,2-Trichloroethane ND 0.20 0.073 ND 1.1 0.40 4 9/23/20 2:02 BRF Trichloroethylene 0.084 0.20 0.074 J 0.45 1.1 0.40 4 9/23/20 2:02 BRF Trichlorofluoromethane (Freon 11) 0.23 0.80 0.15 J 1.3 4.5 0.85 4 9/23/20 2:02 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 9/23/20 2:02 BRF 1,2,4-Trimethylbenzene ND 0.20 0.046 ND 0.98 0.22 4 9/23/20 2:02 BRF 1,3,5-Trimethylbenzene 1.4 0.20 0.052 6.9 0.98 0.26 4 9/23/20 2:02 BRF Vinyl Acetate ND 4.0 0.56 ND 14 2.0 4 9/23/20 2:02 BRF Vinyl Chloride ND 0.20 0.11 ND 0.51 0.29 4 9/23/20 2:02 BRF m&p-Xylene 8.1 0.40 0.070 35 1.7 0.30 4 9/23/20 2:02 BRF o-Xylene 3.4 0.20 0.054 15 0.87 0.23 4 9/23/20 2:02 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 99.3 70-130 9/23/20 2:02 Page 11 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wilmington, NC Sample Description/Location: Work Order: 20I1007 Date Received: 9/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SG-5/Laundry Area (SE) Canister ID: 2103 Final Vacuum(in Hg): -5 Sample ID: 20I1007-05 Canister Size: 1 liter Receipt Vacuum(in Hg): -6.8 Sample Matrix: Air Flow Controller ID: -6.8 Flow Controller Type: Fixed -Orifice Sampled: 9/10/2020 18:17 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 110 8.0 4.8 250 19 11 4 9/23/20 2:43 BRF Benzene 0.46 0.20 0.058 1.5 0.64 0.19 4 9/23/20 2:43 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/23/20 2:43 BRF Bromodichloromethane ND 0.20 0.056 ND 1.3 0.37 4 9/23/20 2:43 BRF Bromoform ND 0.20 0.069 ND 2.1 0.71 4 9/23/20 2:43 BRF Bromomethane ND 0.20 0.11 ND 0.78 0.41 4 9/23/20 2:43 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 9/23/20 2:43 BRF 2-Butanone (MEK) 3.8 8.0 0.66 J 11 24 2.0 4 9/23/20 2:43 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/23/20 2:43 BRF Carbon Tetrachloride ND 0.20 0.053 ND 1.3 0.33 4 9/23/20 2:43 BRF Chlorobenzene ND 0.20 0.048 ND 0.92 0.22 4 9/23/20 2:43 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 9/23/20 2:43 BRF Chloroform 26 0.20 0.048 130 0.98 0.24 4 9/23/20 2:43 BRF Chloromethane ND 0.40 0.15 ND 0.83 0.32 4 9/23/20 2:43 BRF Cyclohexane ND 0.20 0.098 ND 0.69 0.34 4 9/23/20 2:43 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/23/20 2:43 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.052 ND 1.5 0.40 4 9/23/20 2:43 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/23/20 2:43 BRF 1,3-Dichlorobenzene ND 0.20 0.073 ND 1.2 0.44 4 9/23/20 2:43 BRF 1,4-Dichlorobenzene ND 0.20 0.045 ND 1.2 0.27 4 9/23/20 2:43 BRF Dichlorodifluoromethane (Freon 12) 3.8 0.20 0.063 19 0.99 0.31 4 9/23/20 2:43 BRF 1,1-Dichloroethane ND 0.20 0.063 ND 0.81 0.25 4 9/23/20 2:43 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/23/20 2:43 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 9/23/20 2:43 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/23/20 2:43 BRF trans-1,2-Dichloroethylene ND 0.20 0.059 ND 0.79 0.23 4 9/23/20 2:43 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/23/20 2:43 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/23/20 2:43 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.067 ND 0.91 0.30 4 9/23/20 2:43 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 9/23/20 2:43 BRF 1,4-Dioxane ND 2.0 0.56 ND 7.2 2.0 4 9/23/20 2:43 BRF Ethanol 61 8.0 2.4 110 15 4.6 4 9/23/20 2:43 BRF Ethyl Acetate ND 2.0 1.2 ND 7.2 4.3 4 9/23/20 2:43 BRF Ethylbenzene 3.1 0.20 0.042 14 0.87 0.18 4 9/23/20 2:43 BRF 4-Ethyltoluene 2.0 0.20 0.062 9.8 0.98 0.30 4 9/23/20 2:43 BRF Heptane 0.45 0.20 0.086 1.8 0.82 0.35 4 9/23/20 2:43 BRF Hexachlorobutadiene ND 0.20 0.088 ND 2.1 0.94 4 9/23/20 2:43 BRF Hexane ND 8.0 0.36 ND 28 1.3 4 9/23/20 2:43 BRF 2-Hexanone (MBK) ND 0.20 0.11 ND 0.82 0.46 4 9/23/20 2:43 BRF Isopropanol 14 8.0 1.8 34 20 4.5 4 9/23/20 2:43 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/23/20 2:43 BRF Methylene Chloride ND 2.0 0.46 ND 6.9 1.6 4 9/23/20 2:43 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 9/23/20 2:43 BRF Naphthalene 0.71 0.20 0.11 3.7 1.0 0.59 4 9/23/20 2:43 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/23/20 2:43 BRF Styrene ND 0.20 0.057 ND 0.85 0.24 4 9/23/20 2:43 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.053 ND 1.4 0.37 4 9/23/20 2:43 BRF Page 12 of 35 icon-tes w . ANALYTICAL LABORATORY Project Location: Wilmington, NC Date Received: 9/11/2020 Field Sample #: SG-5/Laundry Area (SE) Sample ID: 20I1007-05 Sample Matrix: Air Sampled: 9/ 10/2020 18:17 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2103 Canister Size: 1 liter Flow Controller ID: -6.8 Sample Type: 10 min Work Order: 20I1007 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -6.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 2.8 0.20 0.065 19 1.4 0.44 4 9/23/20 2:43 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/23/20 2:43 BRF Toluene 7.3 0.20 0.058 28 0.75 0.22 4 9/23/20 2:43 BRF 1,2,4-Trichlorobenzene ND 0.20 0.12 ND 1.5 0.91 4 9/23/20 2:43 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.065 ND 1.1 0.36 4 9/23/20 2:43 BRF 1,1,2-Trichloroethane ND 0.20 0.073 ND 1.1 0.40 4 9/23/20 2:43 BRF Trichloroethylene 8.4 0.20 0.074 45 1.1 0.40 4 9/23/20 2:43 BRF Trichlorofluoromethane (Freon 11) 0.22 0.80 0.15 J 1.2 4.5 0.85 4 9/23/20 2:43 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 9/23/20 2:43 BRF 1,2,4-Trimethylbenzene ND 0.20 0.046 ND 0.98 0.22 4 9/23/20 2:43 BRF 1,3,5-Trimethylbenzene 1.8 0.20 0.052 8.6 0.98 0.26 4 9/23/20 2:43 BRF Vinyl Acetate ND 4.0 0.56 ND 14 2.0 4 9/23/20 2:43 BRF Vinyl Chloride ND 0.20 0.11 ND 0.51 0.29 4 9/23/20 2:43 BRF m&p-Xylene 14 0.40 0.070 59 1.7 0.30 4 9/23/20 2:43 BRF o-Xylene 5.5 0.20 0.054 24 0.87 0.23 4 9/23/20 2:43 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 99.0 % REC Limits 70-130 9/23/20 2:43 Page 13 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wilmington, NC Sample Description/Location: Work Order: 20I1007 Date Received: 9/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SG-5 DUP/Laundry Area (SE) Canister ID: 2326 Final Vacuum(in Hg): -5 Sample ID: 20I1007-06 Canister Size: 1 liter Receipt Vacuum(in Hg): -6.8 Sample Matrix: Air Flow Controller ID: -6.8 Flow Controller Type: Fixed -Orifice Sampled: 9/10/2020 18:17 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 100 8.0 4.8 250 19 11 4 9/23/20 3:24 BRF Benzene 0.46 0.20 0.058 1.5 0.64 0.19 4 9/23/20 3:24 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/23/20 3:24 BRF Bromodichloromethane ND 0.20 0.056 ND 1.3 0.37 4 9/23/20 3:24 BRF Bromoform ND 0.20 0.069 ND 2.1 0.71 4 9/23/20 3:24 BRF Bromomethane ND 0.20 0.11 ND 0.78 0.41 4 9/23/20 3:24 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 9/23/20 3:24 BRF 2-Butanone (MEK) 3.8 8.0 0.66 J 11 24 2.0 4 9/23/20 3:24 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/23/20 3:24 BRF Carbon Tetrachloride ND 0.20 0.053 ND 1.3 0.33 4 9/23/20 3:24 BRF Chlorobenzene ND 0.20 0.048 ND 0.92 0.22 4 9/23/20 3:24 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 9/23/20 3:24 BRF Chloroform 26 0.20 0.048 130 0.98 0.24 4 9/23/20 3:24 BRF Chloromethane ND 0.40 0.15 ND 0.83 0.32 4 9/23/20 3:24 BRF Cyclohexane ND 0.20 0.098 ND 0.69 0.34 4 9/23/20 3:24 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/23/20 3:24 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.052 ND 1.5 0.40 4 9/23/20 3:24 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/23/20 3:24 BRF 1,3-Dichlorobenzene ND 0.20 0.073 ND 1.2 0.44 4 9/23/20 3:24 BRF 1,4-Dichlorobenzene ND 0.20 0.045 ND 1.2 0.27 4 9/23/20 3:24 BRF Dichlorodifluoromethane (Freon 12) 3.8 0.20 0.063 19 0.99 0.31 4 9/23/20 3:24 BRF 1,1-Dichloroethane ND 0.20 0.063 ND 0.81 0.25 4 9/23/20 3:24 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/23/20 3:24 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 9/23/20 3:24 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/23/20 3:24 BRF trans-1,2-Dichloroethylene ND 0.20 0.059 ND 0.79 0.23 4 9/23/20 3:24 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/23/20 3:24 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/23/20 3:24 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.067 ND 0.91 0.30 4 9/23/20 3:24 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 9/23/20 3:24 BRF 1,4-Dioxane ND 2.0 0.56 ND 7.2 2.0 4 9/23/20 3:24 BRF Ethanol 60 8.0 2.4 110 15 4.6 4 9/23/20 3:24 BRF Ethyl Acetate ND 2.0 1.2 ND 7.2 4.3 4 9/23/20 3:24 BRF Ethylbenzene 2.4 0.20 0.042 11 0.87 0.18 4 9/23/20 3:24 BRF 4-Ethyltoluene 2.0 0.20 0.062 9.8 0.98 0.30 4 9/23/20 3:24 BRF Heptane 0.46 0.20 0.086 1.9 0.82 0.35 4 9/23/20 3:24 BRF Hexachlorobutadiene ND 0.20 0.088 ND 2.1 0.94 4 9/23/20 3:24 BRF Hexane ND 8.0 0.36 ND 28 1.3 4 9/23/20 3:24 BRF 2-Hexanone (MBK) ND 0.20 0.11 ND 0.82 0.46 4 9/23/20 3:24 BRF Isopropanol 14 8.0 1.8 34 20 4.5 4 9/23/20 3:24 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/23/20 3:24 BRF Methylene Chloride ND 2.0 0.46 ND 6.9 1.6 4 9/23/20 3:24 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 9/23/20 3:24 BRF Naphthalene 2.5 0.20 0.11 13 1.0 0.59 4 9/23/20 3:24 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/23/20 3:24 BRF Styrene ND 0.20 0.057 ND 0.85 0.24 4 9/23/20 3:24 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.053 ND 1.4 0.37 4 9/23/20 3:24 BRF Page 14 of 35 icon-tes w . ANALYTICAL LABORATORY Project Location: Wilmington, NC Date Received: 9/11/2020 Field Sample #: SG-5 DUP/Laundry Area (SE) Sample ID: 20I1007-06 Sample Matrix: Air Sampled: 9/ 10/2020 18:17 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2326 Canister Size: 1 liter Flow Controller ID: -6.8 Sample Type: 10 min Work Order: 20I1007 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -6.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 2.9 0.20 0.065 19 1.4 0.44 4 9/23/20 3:24 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/23/20 3:24 BRF Toluene 7.4 0.20 0.058 28 0.75 0.22 4 9/23/20 3:24 BRF 1,2,4-Trichlorobenzene ND 0.20 0.12 ND 1.5 0.91 4 9/23/20 3:24 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.065 ND 1.1 0.36 4 9/23/20 3:24 BRF 1,1,2-Trichloroethane ND 0.20 0.073 ND 1.1 0.40 4 9/23/20 3:24 BRF Trichloroethylene 8.7 0.20 0.074 47 1.1 0.40 4 9/23/20 3:24 BRF Trichlorofluoromethane (Freon 11) 0.20 0.80 0.15 J 1.1 4.5 0.85 4 9/23/20 3:24 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 9/23/20 3:24 BRF 1,2,4-Trimethylbenzene 7.8 0.20 0.046 38 0.98 0.22 4 9/23/20 3:24 BRF 1,3,5-Trimethylbenzene 1.8 0.20 0.052 8.7 0.98 0.26 4 9/23/20 3:24 BRF Vinyl Acetate ND 4.0 0.56 ND 14 2.0 4 9/23/20 3:24 BRF Vinyl Chloride ND 0.20 0.11 ND 0.51 0.29 4 9/23/20 3:24 BRF m&p-Xylene 13 0.40 0.070 58 1.7 0.30 4 9/23/20 3:24 BRF o-Xylene 5.6 0.20 0.054 24 0.87 0.23 4 9/23/20 3:24 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 96.8 % REC Limits 70-130 9/23/20 3:24 Page 15 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wilmington, NC Sample Description/Location: Work Order: 20I1007 Date Received: 9/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SG-6/Laundry Area (NE) Canister ID: 2312 Final Vacuum(in Hg): -5 Sample ID: 20I1007-07 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.9 Sample Matrix: Air Flow Controller ID: -5.9 Flow Controller Type: Fixed -Orifice Sampled: 9/10/2020 18:39 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 41 8.0 4.8 98 19 11 4 9/23/20 4:44 BRF Benzene 0.29 0.20 0.058 0.93 0.64 0.19 4 9/23/20 4:44 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/23/20 4:44 BRF Bromodichloromethane ND 0.20 0.056 ND 1.3 0.37 4 9/23/20 4:44 BRF Bromoform ND 0.20 0.069 ND 2.1 0.71 4 9/23/20 4:44 BRF Bromomethane ND 0.20 0.11 ND 0.78 0.41 4 9/23/20 4:44 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 9/23/20 4:44 BRF 2-Butanone (MEK) 4.0 8.0 0.66 J 12 24 2.0 4 9/23/20 4:44 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/23/20 4:44 BRF Carbon Tetrachloride ND 0.20 0.053 ND 1.3 0.33 4 9/23/20 4:44 BRF Chlorobenzene ND 0.20 0.048 ND 0.92 0.22 4 9/23/20 4:44 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 9/23/20 4:44 BRF Chloroform 0.39 0.20 0.048 1.9 0.98 0.24 4 9/23/20 4:44 BRF Chloromethane ND 0.40 0.15 ND 0.83 0.32 4 9/23/20 4:44 BRF Cyclohexane ND 0.20 0.098 ND 0.69 0.34 4 9/23/20 4:44 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/23/20 4:44 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.052 ND 1.5 0.40 4 9/23/20 4:44 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/23/20 4:44 BRF 1,3-Dichlorobenzene ND 0.20 0.073 ND 1.2 0.44 4 9/23/20 4:44 BRF 1,4-Dichlorobenzene ND 0.20 0.045 ND 1.2 0.27 4 9/23/20 4:44 BRF Dichlorodifluoromethane (Freon 12) 1.4 0.20 0.063 7.0 0.99 0.31 4 9/23/20 4:44 BRF 1,1-Dichloroethane ND 0.20 0.063 ND 0.81 0.25 4 9/23/20 4:44 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/23/20 4:44 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 9/23/20 4:44 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/23/20 4:44 BRF trans-1,2-Dichloroethylene ND 0.20 0.059 ND 0.79 0.23 4 9/23/20 4:44 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/23/20 4:44 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/23/20 4:44 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.067 ND 0.91 0.30 4 9/23/20 4:44 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 9/23/20 4:44 BRF 1,4-Dioxane ND 2.0 0.56 ND 7.2 2.0 4 9/23/20 4:44 BRF Ethanol 20 8.0 2.4 38 15 4.6 4 9/23/20 4:44 BRF Ethyl Acetate ND 2.0 1.2 ND 7.2 4.3 4 9/23/20 4:44 BRF Ethylbenzene 1.8 0.20 0.042 7.9 0.87 0.18 4 9/23/20 4:44 BRF 4-Ethyltoluene 1.6 0.20 0.062 8.1 0.98 0.30 4 9/23/20 4:44 BRF Heptane ND 0.20 0.086 ND 0.82 0.35 4 9/23/20 4:44 BRF Hexachlorobutadiene ND 0.20 0.088 ND 2.1 0.94 4 9/23/20 4:44 BRF Hexane ND 8.0 0.36 ND 28 1.3 4 9/23/20 4:44 BRF 2-Hexanone (MBK) ND 0.20 0.11 ND 0.82 0.46 4 9/23/20 4:44 BRF Isopropanol 5.3 8.0 1.8 J 13 20 4.5 4 9/23/20 4:44 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/23/20 4:44 BRF Methylene Chloride ND 2.0 0.46 ND 6.9 1.6 4 9/23/20 4:44 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 9/23/20 4:44 BRF Naphthalene 0.75 0.20 0.11 3.9 1.0 0.59 4 9/23/20 4:44 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/23/20 4:44 BRF Styrene ND 0.20 0.057 ND 0.85 0.24 4 9/23/20 4:44 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.053 ND 1.4 0.37 4 9/23/20 4:44 BRF Page 16 of 35 icon-tes w . ANALYTICAL LABORATORY Project Location: Wilmington, NC Date Received: 9/11/2020 Field Sample #: SG-6/Laundry Area (NE) Sample ID: 20I1007-07 Sample Matrix: Air Sampled: 9/ 10/2020 18:39 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2312 Canister Size: 1 liter Flow Controller ID: -5.9 Sample Type: 10 min Work Order: 20I1007 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.9 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 1.7 0.20 0.065 12 1.4 0.44 4 9/23/20 4:44 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/23/20 4:44 BRF Toluene 3.9 0.20 0.058 15 0.75 0.22 4 9/23/20 4:44 BRF 1,2,4-Trichlorobenzene ND 0.20 0.12 ND 1.5 0.91 4 9/23/20 4:44 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.065 ND 1.1 0.36 4 9/23/20 4:44 BRF 1,1,2-Trichloroethane ND 0.20 0.073 ND 1.1 0.40 4 9/23/20 4:44 BRF Trichloroethylene 0.94 0.20 0.074 5.1 1.1 0.40 4 9/23/20 4:44 BRF Trichlorofluoromethane (Freon 11) 0.22 0.80 0.15 J 1.3 4.5 0.85 4 9/23/20 4:44 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 9/23/20 4:44 BRF 1,2,4-Trimethylbenzene 7.4 0.20 0.046 36 0.98 0.22 4 9/23/20 4:44 BRF 1,3,5-Trimethylbenzene 1.5 0.20 0.052 7.6 0.98 0.26 4 9/23/20 4:44 BRF Vinyl Acetate ND 4.0 0.56 ND 14 2.0 4 9/23/20 4:44 BRF Vinyl Chloride ND 0.20 0.11 ND 0.51 0.29 4 9/23/20 4:44 BRF m&p-Xylene 8.3 0.40 0.070 36 1.7 0.30 4 9/23/20 4:44 BRF o-Xylene 3.7 0.20 0.054 16 0.87 0.23 4 9/23/20 4:44 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 97.0 % REC Limits 70-130 9/23/20 4:44 Page 17 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wilmington, NC Sample Description/Location: Work Order: 20I1007 Date Received: 9/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: SG-7/Laundry Area (SW) Canister ID: 2099 Final Vacuum(in Hg): -5 Sample ID: 20I1007-08 Canister Size: 1 liter Receipt Vacuum(in Hg): -6.3 Sample Matrix: Air Flow Controller ID: -6.3 Flow Controller Type: Fixed -Orifice Sampled: 9/10/2020 19:05 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 28 8.0 4.8 67 19 11 4 9/23/20 5:25 BRF Benzene 0.43 0.20 0.058 1.4 0.64 0.19 4 9/23/20 5:25 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/23/20 5:25 BRF Bromodichloromethane ND 0.20 0.056 ND 1.3 0.37 4 9/23/20 5:25 BRF Bromoform ND 0.20 0.069 ND 2.1 0.71 4 9/23/20 5:25 BRF Bromomethane ND 0.20 0.11 ND 0.78 0.41 4 9/23/20 5:25 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 9/23/20 5:25 BRF 2-Butanone (MEK) 2.7 8.0 0.66 J 8.1 24 2.0 4 9/23/20 5:25 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/23/20 5:25 BRF Carbon Tetrachloride ND 0.20 0.053 ND 1.3 0.33 4 9/23/20 5:25 BRF Chlorobenzene ND 0.20 0.048 ND 0.92 0.22 4 9/23/20 5:25 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 9/23/20 5:25 BRF Chloroform 2.4 0.20 0.048 12 0.98 0.24 4 9/23/20 5:25 BRF Chloromethane ND 0.40 0.15 ND 0.83 0.32 4 9/23/20 5:25 BRF Cyclohexane ND 0.20 0.098 ND 0.69 0.34 4 9/23/20 5:25 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/23/20 5:25 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.052 ND 1.5 0.40 4 9/23/20 5:25 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/23/20 5:25 BRF 1,3-Dichlorobenzene ND 0.20 0.073 ND 1.2 0.44 4 9/23/20 5:25 BRF 1,4-Dichlorobenzene ND 0.20 0.045 ND 1.2 0.27 4 9/23/20 5:25 BRF Dichlorodifluoromethane (Freon 12) 16 0.20 0.063 79 0.99 0.31 4 9/23/20 5:25 BRF 1,1-Dichloroethane ND 0.20 0.063 ND 0.81 0.25 4 9/23/20 5:25 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/23/20 5:25 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 9/23/20 5:25 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/23/20 5:25 BRF trans-1,2-Dichloroethylene ND 0.20 0.059 ND 0.79 0.23 4 9/23/20 5:25 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/23/20 5:25 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/23/20 5:25 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.067 ND 0.91 0.30 4 9/23/20 5:25 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 9/23/20 5:25 BRF 1,4-Dioxane ND 2.0 0.56 ND 7.2 2.0 4 9/23/20 5:25 BRF Ethanol 55 8.0 2.4 100 15 4.6 4 9/23/20 5:25 BRF Ethyl Acetate ND 2.0 1.2 ND 7.2 4.3 4 9/23/20 5:25 BRF Ethylbenzene 1.1 0.20 0.042 4.7 0.87 0.18 4 9/23/20 5:25 BRF 4-Ethyltoluene ND 0.20 0.062 ND 0.98 0.30 4 9/23/20 5:25 BRF Heptane 0.42 0.20 0.086 1.7 0.82 0.35 4 9/23/20 5:25 BRF Hexachlorobutadiene ND 0.20 0.088 ND 2.1 0.94 4 9/23/20 5:25 BRF Hexane ND 8.0 0.36 ND 28 1.3 4 9/23/20 5:25 BRF 2-Hexanone (MBK) ND 0.20 0.11 ND 0.82 0.46 4 9/23/20 5:25 BRF Isopropanol 2.3 8.0 1.8 J 5.7 20 4.5 4 9/23/20 5:25 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/23/20 5:25 BRF Methylene Chloride ND 2.0 0.46 ND 6.9 1.6 4 9/23/20 5:25 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 9/23/20 5:25 BRF Naphthalene 0.70 0.20 0.11 3.7 1.0 0.59 4 9/23/20 5:25 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/23/20 5:25 BRF Styrene ND 0.20 0.057 ND 0.85 0.24 4 9/23/20 5:25 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.053 ND 1.4 0.37 4 9/23/20 5:25 BRF Page 18 of 35 icon-tes w . ANALYTICAL LABORATORY Project Location: Wilmington, NC Date Received: 9/11/2020 Field Sample #: SG-7/Laundry Area (SW) Sample ID: 20I1007-08 Sample Matrix: Air Sampled: 9/ 10/2020 19:05 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2099 Canister Size: 1 liter Flow Controller ID: -6.3 Sample Type: 10 min Work Order: 20I1007 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -6.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 2.2 0.20 0.065 15 1.4 0.44 4 9/23/20 5:25 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/23/20 5:25 BRF Toluene 4.3 0.20 0.058 16 0.75 0.22 4 9/23/20 5:25 BRF 1,2,4-Trichlorobenzene ND 0.20 0.12 ND 1.5 0.91 4 9/23/20 5:25 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.065 ND 1.1 0.36 4 9/23/20 5:25 BRF 1,1,2-Trichloroethane ND 0.20 0.073 ND 1.1 0.40 4 9/23/20 5:25 BRF Trichloroethylene 0.17 0.20 0.074 J 0.92 1.1 0.40 4 9/23/20 5:25 BRF Trichlorofluoromethane (Freon 11) 0.24 0.80 0.15 J 1.4 4.5 0.85 4 9/23/20 5:25 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 9/23/20 5:25 BRF 1,2,4-Trimethylbenzene ND 0.20 0.046 ND 0.98 0.22 4 9/23/20 5:25 BRF 1,3,5-Trimethylbenzene 0.72 0.20 0.052 3.5 0.98 0.26 4 9/23/20 5:25 BRF Vinyl Acetate ND 4.0 0.56 ND 14 2.0 4 9/23/20 5:25 BRF Vinyl Chloride ND 0.20 0.11 ND 0.51 0.29 4 9/23/20 5:25 BRF m&p-Xylene 4.9 0.40 0.070 21 1.7 0.30 4 9/23/20 5:25 BRF o-Xylene 2.0 0.20 0.054 8.7 0.87 0.23 4 9/23/20 5:25 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 97.3 % REC Limits 70-130 9/23/20 5:25 Page 19 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Wilmington, NC Sample Description/Location: Work Order: 20I1007 Date Received: 9/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SG-8/Laundry Area (NW) Canister ID: 2240 Final Vacuum(in Hg): -5 Sample ID: 20I1007-09 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.8 Sample Matrix: Air Flow Controller ID: -5.8 Flow Controller Type: Fixed -Orifice Sampled: 9/10/2020 19:29 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 31 8.0 4.8 73 19 11 4 9/23/20 6:06 BRF Benzene 0.21 0.20 0.058 0.66 0.64 0.19 4 9/23/20 6:06 BRF Benzyl chloride ND 0.20 0.090 ND 1.0 0.47 4 9/23/20 6:06 BRF Bromodichloromethane ND 0.20 0.056 ND 1.3 0.37 4 9/23/20 6:06 BRF Bromoform ND 0.20 0.069 ND 2.1 0.71 4 9/23/20 6:06 BRF Bromomethane ND 0.20 0.11 ND 0.78 0.41 4 9/23/20 6:06 BRF 1,3-Butadiene ND 0.20 0.15 ND 0.44 0.32 4 9/23/20 6:06 BRF 2-Butanone (MEK) 2.1 8.0 0.66 J 6.1 24 2.0 4 9/23/20 6:06 BRF Carbon Disulfide ND 2.0 0.51 ND 6.2 1.6 4 9/23/20 6:06 BRF Carbon Tetrachloride ND 0.20 0.053 ND 1.3 0.33 4 9/23/20 6:06 BRF Chlorobenzene ND 0.20 0.048 ND 0.92 0.22 4 9/23/20 6:06 BRF Chloroethane ND 0.20 0.20 ND 0.53 0.52 4 9/23/20 6:06 BRF Chloroform 0.21 0.20 0.048 1.0 0.98 0.24 4 9/23/20 6:06 BRF Chloromethane ND 0.40 0.15 ND 0.83 0.32 4 9/23/20 6:06 BRF Cyclohexane ND 0.20 0.098 ND 0.69 0.34 4 9/23/20 6:06 BRF Dibromochloromethane ND 0.20 0.067 ND 1.7 0.57 4 9/23/20 6:06 BRF 1,2-Dibromoethane (EDB) ND 0.20 0.052 ND 1.5 0.40 4 9/23/20 6:06 BRF 1,2-Dichlorobenzene ND 0.20 0.074 ND 1.2 0.44 4 9/23/20 6:06 BRF 1,3-Dichlorobenzene ND 0.20 0.073 ND 1.2 0.44 4 9/23/20 6:06 BRF 1,4-Dichlorobenzene ND 0.20 0.045 ND 1.2 0.27 4 9/23/20 6:06 BRF Dichlorodifluoromethane (Freon 12) 2.5 0.20 0.063 12 0.99 0.31 4 9/23/20 6:06 BRF 1,1-Dichloroethane ND 0.20 0.063 ND 0.81 0.25 4 9/23/20 6:06 BRF 1,2-Dichloroethane ND 0.20 0.073 ND 0.81 0.30 4 9/23/20 6:06 BRF 1,1-Dichloroethylene ND 0.20 0.11 ND 0.79 0.43 4 9/23/20 6:06 BRF cis-1,2-Dichloroethylene ND 0.20 0.068 ND 0.79 0.27 4 9/23/20 6:06 BRF trans-1,2-Dichloroethylene ND 0.20 0.059 ND 0.79 0.23 4 9/23/20 6:06 BRF 1,2-Dichloropropane ND 0.20 0.072 ND 0.92 0.33 4 9/23/20 6:06 BRF cis- 1,3 -Dichloropropene ND 0.20 0.093 ND 0.91 0.42 4 9/23/20 6:06 BRF trans- 1, 3 -Dichloropropene ND 0.20 0.067 ND 0.91 0.30 4 9/23/20 6:06 BRF 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.11 ND 1.4 0.79 4 9/23/20 6:06 BRF 1,4-Dioxane ND 2.0 0.56 ND 7.2 2.0 4 9/23/20 6:06 BRF Ethanol 33 8.0 2.4 63 15 4.6 4 9/23/20 6:06 BRF Ethyl Acetate ND 2.0 1.2 ND 7.2 4.3 4 9/23/20 6:06 BRF Ethylbenzene 1.4 0.20 0.042 6.1 0.87 0.18 4 9/23/20 6:06 BRF 4-Ethyltoluene 1.1 0.20 0.062 5.3 0.98 0.30 4 9/23/20 6:06 BRF Heptane ND 0.20 0.086 ND 0.82 0.35 4 9/23/20 6:06 BRF Hexachlorobutadiene ND 0.20 0.088 ND 2.1 0.94 4 9/23/20 6:06 BRF Hexane ND 8.0 0.36 ND 28 1.3 4 9/23/20 6:06 BRF 2-Hexanone (MBK) ND 0.20 0.11 ND 0.82 0.46 4 9/23/20 6:06 BRF Isopropanol 3.6 8.0 1.8 J 8.8 20 4.5 4 9/23/20 6:06 BRF Methyl tert-Butyl Ether (MTBE) ND 0.20 0.080 ND 0.72 0.29 4 9/23/20 6:06 BRF Methylene Chloride ND 2.0 0.46 ND 6.9 1.6 4 9/23/20 6:06 BRF 4-Methyl-2-pentanone (MIBK) ND 0.20 0.10 ND 0.82 0.43 4 9/23/20 6:06 BRF Naphthalene 0.61 0.20 0.11 3.2 1.0 0.59 4 9/23/20 6:06 BRF Propene ND 8.0 0.67 ND 14 1.2 4 9/23/20 6:06 BRF Styrene ND 0.20 0.057 ND 0.85 0.24 4 9/23/20 6:06 BRF 1,1,2,2-Tetrachloroethane ND 0.20 0.053 ND 1.4 0.37 4 9/23/20 6:06 BRF Page 20 of 35 icon-tes w . ANALYTICAL LABORATORY Project Location: Wilmington, NC Date Received: 9/11/2020 Field Sample #: SG-8/Laundry Area (NW) Sample ID: 20I1007-09 Sample Matrix: Air Sampled: 9/ 10/2020 19:29 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2240 Canister Size: 1 liter Flow Controller ID: -5.8 Sample Type: 10 min Work Order: 20I1007 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 1.1 0.20 0.065 7.6 1.4 0.44 4 9/23/20 6:06 BRF Tetrahydrofuran ND 2.0 0.49 ND 5.9 1.5 4 9/23/20 6:06 BRF Toluene 2.8 0.20 0.058 10 0.75 0.22 4 9/23/20 6:06 BRF 1,2,4-Trichlorobenzene ND 0.20 0.12 ND 1.5 0.91 4 9/23/20 6:06 BRF 1, 1, 1 -Trichloroethane ND 0.20 0.065 ND 1.1 0.36 4 9/23/20 6:06 BRF 1,1,2-Trichloroethane ND 0.20 0.073 ND 1.1 0.40 4 9/23/20 6:06 BRF Trichloroethylene ND 0.20 0.074 ND 1.1 0.40 4 9/23/20 6:06 BRF Trichlorofluoromethane (Freon 11) 0.34 0.80 0.15 J 1.9 4.5 0.85 4 9/23/20 6:06 BRF 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.15 ND 6.1 1.2 4 9/23/20 6:06 BRF 1,2,4-Trimethylbenzene ND 0.20 0.046 ND 0.98 0.22 4 9/23/20 6:06 BRF 1,3,5-Trimethylbenzene 1.0 0.20 0.052 5.1 0.98 0.26 4 9/23/20 6:06 BRF Vinyl Acetate ND 4.0 0.56 ND 14 2.0 4 9/23/20 6:06 BRF Vinyl Chloride ND 0.20 0.11 ND 0.51 0.29 4 9/23/20 6:06 BRF m&p-Xylene 6.5 0.40 0.070 28 1.7 0.30 4 9/23/20 6:06 BRF o-Xylene 2.7 0.20 0.054 12 0.87 0.23 4 9/23/20 6:06 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 96.5 % REC Limits 70-130 9/23/20 6:06 Page 21 of 35 icon-tes w . ANALYTICAL LABORATORY Prep Method: TO-15 Prep -EPA TO-15 Lab Number [Field ID] 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Pre-Dil Pre-Dil Default Pressure Pre Initial Final Injection Batch Dilution Dilution mL mL mL Actual Injection mL Date 20I1007-01 [SG- 1 /Boiler Room (S)] B267103 1.5 1 N/A 1000 400 150 09/22/20 2011007-02 [SG-2/Storage (SE)] B267103 1.5 1 N/A 1000 400 150 09/22/20 20I1007-02RE1 [SG-2/Storage (SE)] B267103 1.5 1 N/A 1000 400 30 09/22/20 2011007-03[SG-3/Storage(E)] B267103 1.5 1 N/A 1000 400 150 09/22/20 2011007-03RE1 [SG-3/Storage (E)] B267103 1.5 1 N/A 1000 400 60 09/22/20 2011007-04[SG-4/Storage(SW)] B267103 1.5 1 N/A 1000 400 150 09/22/20 2011007-05 [SG-5/Laundry Area (SE)] B267103 1.5 1 N/A 1000 400 150 09/22/20 2011007-06 [SG-5 DUP/Laundry Area (SE)] B267103 1.5 1 N/A 1000 400 150 09/22/20 2011007-07 [SG-6/Laundry Area (NE)] B267103 1.5 1 N/A 1000 400 150 09/22/20 2011007-08 [SG-7/Laundry Area (SW)] B267103 1.5 1 N/A 1000 400 150 09/22/20 20I1007-09 [SG-8/Laundry Area (NW)] B267103 1.5 1 N/A 1000 400 150 09/22/20 Page 22 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD malyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B267103 - TO-15 Prep Blank (B267103-BLKl) Prepared & Analyzed: 09/22/20 Acetone ND 0.80 Benzene ND 0.020 Benzyl chloride ND 0.020 Bromodichloromethane ND 0.020 Bromoform ND 0.020 Bromomethane ND 0.020 113-Butadiene ND 0.020 2-Butanone (MEK) ND 0.80 Carbon Disulfide ND 0.20 Carbon Tetrachloride ND 0.020 Chlorobenzene ND 0.020 Chloroethane ND 0.020 Chloroform ND 0.020 Chloromethane ND 0.040 Cyclohexane ND 0.020 Dibromochloromethane ND 0.020 1,2-Dibromoethane (EDB) ND 0.020 1,2-Dichlorobenzene ND 0.020 1,3-Dichlorobenzene ND 0.020 114-Dichlorobenzene ND 0.020 Dichlorodifluoromethane (Freon 12) ND 0.020 1,1-Dichloroethane ND 0.020 1,2-Dichloroethane ND 0.020 1,1-Dichloroethylene ND 0.020 cis-1,2-Dichloroethylene ND 0.020 trans-1,2-Dichloroethylene ND 0.020 1,2-Dichloropropane ND 0.020 cis- 1,3 -Dichloropropene ND 0.020 trans- l,3-Dichloropropene ND 0.020 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.020 (Freon 114) 114-Dioxane ND 0.20 Ethanol ND 0.80 Ethyl Acetate ND 0.20 Ethylbenzene ND 0.020 4-Ethyltoluene ND 0.020 Heptane ND 0.020 Hexachlorobutadiene ND 0.020 Hexane ND 0.80 2-Hexanone (MBK) ND 0.020 Isopropanol ND 0.80 Methyl tert-Butyl Ether (MTBE) ND 0.020 Methylene Chloride ND 0.20 4-Methyl-2-pentanone (MIBK) ND 0.020 Naphthalene ND 0.020 Propene ND 0.80 Styrene ND 0.020 Page 23 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B267103 - TO-15 Prep Blank (B267103-BLKI) Prepared & Analyzed: 09/22/20 1,1,2,2-Tetrachloroethane ND 0.020 Tetrachloroethylene 0.0072 0.020 J Tetrahydrofuran ND 0.20 Toluene ND 0.020 1,2,4-Trichlorobenzene ND 0.020 1, 1, 1 -Trichloroethane ND 0.020 1,1,2-Trichloroethane ND 0.020 Trichloroethylene ND 0.020 Trichlorofluoromethane (Freon 11) ND 0.080 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.080 113) 1,2,4-Trimethylbenzene ND 0.020 1,3,5-Trimethylbenzene ND 0.020 Vinyl Acetate ND 0.40 Vinyl Chloride ND 0.020 m&p-Xylene ND 0.040 o-Xylene ND 0.020 Surrogate: 4-Bromofluorobenzene (1) LCS (B267103-BSI) 7.15 8.00 89.4 Prepared & Analyzed: 09/22/20 70-130 Acetone 4.45 5.00 89.0 70-130 Benzene 4.69 5.00 93.8 70-130 Benzyl chloride 5.61 5.00 112 70-130 Bromodichloromethane 4.72 5.00 94.4 70-130 Bromoform 5.32 5.00 106 70-130 Bromomethane 4.05 5.00 81.0 70-130 1,3-Butadiene 3.61 5.00 72.3 70-130 2-Butanone (MEK) 4.55 5.00 91.0 70-130 Carbon Disulfide 4.18 5.00 83.7 70-130 Carbon Tetrachloride 4.89 5.00 97.8 70-130 Chlorobenzene 4.92 5.00 98.5 70-130 Chloroethane 3.73 5.00 74.5 70-130 Chloroform 3.97 5.00 79.4 70-130 Chloromethane 3.70 5.00 74.1 70-130 Cyclohexane 4.14 5.00 82.8 70-130 Dibromochloromethane 5.48 5.00 110 70-130 1,2-Dibromoethane (EDB) 4.68 5.00 93.5 70-130 1,2-Dichlorobenzene 5.57 5.00 111 70-130 1,3-Dichlorobenzene 5.61 5.00 112 70-130 1,4-Dichlorobenzene 5.37 5.00 107 70-130 Dichlorodifluoromethane (Freon 12) 4.22 5.00 84.4 70-130 1,1-Dichloroethane 4.21 5.00 84.2 70-130 1,2-Dichloroethane 3.92 5.00 78.5 70-130 1,1-Dichloroethylene 4.05 5.00 81.0 70-130 cis-1,2-Dichloroethylene 3.76 5.00 75.3 70-130 trans-1,2-Dichloroethylene 4.06 5.00 81.1 70-130 1,2-Dichloropropane 4.63 5.00 92.6 70-130 Page 24 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B267103 - TO-15 Prep LCS (B267103-BS1) Prepared & Analyzed: 09/22/20 cis-1,3-Dichloropropene 4.21 5.00 84.2 70-130 trans-1,3-Dichloropropene 4.59 5.00 91.8 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 3.91 5.00 78.2 70-130 (Freon 114) 1,4-Dioxane 5.06 5.00 101 70-130 Ethanol 4.45 5.00 88.9 70-130 Ethyl Acetate 3.93 5.00 78.7 70-130 Ethylbenzene 4.74 5.00 94.9 70-130 4-Ethyltoluene 5.21 5.00 104 70-130 Heptane 4.64 5.00 92.8 70-130 Hexachlorobutadiene 4.68 5.00 93.6 70-130 Hexane 4.48 5.00 89.6 70-130 2-Hexanone (MBK) 5.53 5.00 ill 70-130 Isopropanol 4.10 5.00 81.9 70-130 Methyl tert-Butyl Ether (MTBE) 3.91 5.00 78.2 70-130 Methylene Chloride 3.81 5.00 76.2 70-130 4-Methyl-2-pentanone (MIBK) 5.41 5.00 108 70-130 Naphthalene 6.27 5.00 125 70-130 Propene 4.09 5.00 81.8 70-130 Styrene 4.83 5.00 96.5 70-130 1,1,2,2-Tetrachloroethane 5.26 5.00 105 70-130 Tetrachloroethylene 4.37 5.00 87.4 70-130 Tetrahydrofuran 4.13 5.00 82.6 70-130 Toluene 4.70 5.00 94.1 70-130 1,2,4-Trichlorobenzene 5.75 5.00 115 70-130 1, 1, 1 -Trichloroethane 4.32 5.00 86.5 70-130 1,1,2-Trichloroethane 4.66 5.00 93.2 70-130 Trichloroethylene 4.42 5.00 88.4 70-130 Trichlorofluoromethane (Freon 11) 4.72 5.00 94.4 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 4.15 5.00 83.0 70-130 113) 1,2,4-Trimethylbenzene 5.25 5.00 105 70-130 1,3,5-Trimethylbenzene 5.05 5.00 101 70-130 Vinyl Acetate 3.66 5.00 73.1 70-130 Vinyl Chloride 3.90 5.00 78.1 70-130 m&p-Xylene 9.91 10.0 99.1 70-130 o-Xylene 4.93 5.00 98.5 70-130 Surrogate: 4-Bromofluorobenzene (1) 7.64 8.00 95.4 70-130 Page 25 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 ` TEL. 413/525-2332 Note: Blank Subtraction is not performed unless otherwise noted FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). ANALYST RLF Rebecca Faust KKM Kerry K. McGee BRF Brittany R. Fisk Page 26 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (S050606-ICV1) Lab File ID: G2020617.13 Analyzed: 07/24/20 19:18 Bromochloromethane (1) 517660 8.515 520641 8.521 99 60 - 140 -0.0060 +/-0.50 1,4-Difluorobenzene (1) 1364277 10.295 1344293 10.295 101 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 1228652 14.673 1216922 14.672 101 60-140 0.0010 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S052675-CCV1) Lab File ID: G2026604.13 Analyzed: 09/22/20 09:49 Bromochloromethane (1) 498253 8.521 520641 8.521 96 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 1052683 10.295 1344293 10.295 78 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 894140 14.672 1216922 14.672 73 60-140 0.0000 +/-0.50 LCS (B267103-BS1 ) Lab File ID: G2026605.13 Analyzed: 09/22/20 10:28 Bromochloromethane (1) 504480 8.521 498253 8.521 101 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 1069005 10.295 1052683 10.295 102 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 944020 14.673 894140 14.672 106 60-140 0.0010 +/-0.50 Blank (B267103-BLK1) Lab File ID: G2026608.13 Analyzed: 09/22/20 12:40 Bromochloromethane (1) 510416 8.521 498253 8.521 102 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 1018900 10.295 1052683 10.295 97 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 919004 14.666 894140 14.672 103 60-140 -0.0060 +/-0.50 SG-1/Boiler Room (S) (20I1007-01) Lab File ID: G2026623.13 Analyzed: 09/22/20 22:40 Bromochloromethane (1) 603703 8.515 498253 8.521 121 60 - 140 -0.0060 +/-0.50 1,4-Difluorobenzene(1) 1303911 10.295 1052683 10.295 124 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 1198142 14.667 894140 14.672 134 60-140 -0.0050 +/-0.50 SG-2/Storage (SE) (2011007-02) Lab File ID: G2026624.13 Analyzed: 09/22/20 23:20 Bromochloromethane (1) 615930 8.515 498253 8.521 124 60 - 140 -0.0060 +/-0.50 1,4-Difluorobenzene(1) 1320813 10.295 1052683 10.295 125 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 1207873 14.673 894140 14.672 135 60-140 0.0010 +/-0.50 SG-2/Storage (SE) (2011007-02RE1) Lab File ID: G2026625.1) Analyzed: 09/23/20 00:00 Bromochloromethane (1) 614184 8.515 498253 8.521 123 60 - 140 -0.0060 +/-0.50 1,4-Difluorobenzene(1) 1301109 10.295 1052683 10.295 124 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 1169723 14.672 894140 14.672 131 60-140 0.0000 +/-0.50 SG-3/Storage (E) (20I1007-03) Lab File ID: G2026626.13 Analyzed: 09/23/20 00:41 Bromochloromethane (1) 608235 8.515 498253 8.521 122 60 - 140 -0.0060 +/-0.50 1,4-Difluorobenzene(1) 1265102 10.295 1052683 10.295 120 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 1142859 14.673 894140 14.672 128 60-140 0.0010 +/-0.50 Page 27 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q SG-3/Storage (E) (20I1007-03RE1) Lab File ID: G2026627.D Analyzed: 09/23/20 01:21 Bromochloromethane (1) 613827 8.521 498253 8.521 123 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 1284426 10.295 1052683 10.295 122 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 1148337 14.673 894140 14.672 128 60-140 0.0010 +/-0.50 SG4/Storage (SW) (20I1007-04) Lab File ID: G2026628.D Analyzed: 09/23/20 02:02 Bromochloromethane (1) 604265 8.515 498253 8.521 121 60 - 140 -0.0060 +/-0.50 1,4-Difluorobenzene (1) 1276591 10.295 1052683 10.295 121 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 1162625 14.667 894140 14.672 130 60-140 -0.0050 +/-0.50 SG-5/Laundry Area (SE) (20I1007-05) Lab File ID: G2026629.D Analyzed: 09/23/20 02:43 Bromochloromethane (1) 593617 8.521 498253 8.521 119 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 1256551 10.295 1052683 10.295 119 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 1133996 14.673 894140 14.672 127 60-140 0.0010 +/-0.50 SG-5 DUP/Laundry Area (SE) (20I1007-06) Lab File ID: G2026630.D Analyzed: 09/23/20 03:24 Bromochloromethane (1) 594510 8.521 498253 8.521 119 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 1232452 10.295 1052683 10.295 117 60-140 0.0000 +/-0.50 Chlorobenzene-d5 (1) 1118248 14.672 894140 14.672 125 60-140 0.0000 +/-0.50 SG-6/Laundry Area (NE) (20I 1007-07) Lab File ID: G2026632.D Analyzed: 09/23/20 04:44 Bromochloromethane (1) 510827 8.521 498253 8.521 103 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 1034557 10.295 1052683 10.295 98 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 942125 14.673 894140 14.672 105 60-140 0.0010 +/-0.50 SG-7/Laundry Area (SW) (20I1007-08) Lab File ID: G2026633.D Analyzed: 09/23/20 05:25 Bromochloromethane (1) 492931 8.521 498253 8.521 99 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 1025301 10.295 1052683 10.295 97 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 945540 14.673 894140 14.672 106 60-140 0.0010 +/-0.50 SG-8/Laundry Area (NW) (2011007-09) Lab File ID: G2026634.1) Analyzed: 09/23/20 06:06 Bromochloromethane (1) 500825 8.521 498253 8.521 101 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 1022786 10.295 1052683 10.295 97 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 943087 14.666 894140 14.672 105 60-140 -0.0060 +/-0.50 Page 28 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S052675-CCV 1 COMPOUND TYPE. CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 4.41 1.053555 0.9289899 -11.8 30 Benzene A 5.00 4.75 0.8318195 0.8379123 0.7 30 Benzyl chloride A 5.00 5.70 0.9744539 1.110307 13.9 30 Bromodichloromethane A 5.00 4.72 0.6722987 0.6353168 -5.5 30 Bromoform A 5.00 5.62 0.4697758 0.5282197 12.4 30 Bromomethane A 5.00 4.00 0.4868206 0.3890907 -20.1 30 1,3-Butadiene A 5.00 3.63 0.5501589 0.399418 -27.4 30 2-Butanone(MEK) A 5.00 4.36 1.617461 1.411964 -12.7 30 Carbon Disulfide A 5.00 4.10 1.939703 1.589149 -18.1 30 Carbon Tetrachloride A 5.00 5.00 0.5586121 0.5586366 0.004 30 Chlorobenzene A 5.00 5.22 0.8038151 0.8389272 4.4 30 Chloroethane A 5.00 3.63 0.3279605 0.2383303 -27.3 30 Chloroform A 5.00 3.96 1.550025 1.22815 -20.8 30 Chloromethane A 5.00 3.77 0.6810125 0.5133296 -24.6 30 Cyclohexane A 5.00 4.25 0.3964233 0.3370527 -15.0 30 Dibromochloromethane A 5.00 5.69 0.576644 0.6564896 13.8 30 1,2-Dibromoethane(EDB) A 5.00 4.86 0.5831203 0.5668428 -2.8 30 1,2-Dichlorobenzene A 5.00 5.67 0.61554 0.6980777 13.4 30 1,3-Dichlorobenzene A 5.00 5.72 0.6695671 0.7659758 14.4 30 1,4-Dichlorobenzene A 5.00 5.51 0.6878458 0.7585192 10.3 30 Dichlorodifluoromethane (Freon 12) A 5.00 4.13 1.51727 1.254367 -17.3 30 1,1-Dichloroethane A 5.00 4.15 1.343108 1.114027 -17.1 30 1,2-Dichloroethane A 5.00 3.90 1.077518 0.8415484 -21.9 30 1,1-Dichloroethylene A 5.00 4.10 1.184388 0.970238 -18.1 30 cis-1,2-Dichloroethylene A 5.00 3.78 1.085884 0.8204539 -24.4 30 trans-1,2-Dichloroethylene A 5.00 4.03 1.061368 0.8553502 -19.4 30 1,2-Dichloropropane A 5.00 4.71 0.3607611 0.3396532 -5.9 30 cis-1,3-Dichloropropene A 5.00 4.46 0.5752596 0.5130327 -10.8 30 trans- l,3-Dichloropropene A 5.00 4.54 0.4864319 0.4419686 -9.1 30 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1 A 5.00 4.13 1.409476 1.165368 -17.3 30 1,4-Dioxane A 5.00 4.72 0.1646065 0.1552528 -5.7 30 Ethanol A 5.00 3.76 0.1738083 0.1306292 -24.8 30 Ethyl Acetate A 5.00 4.15 0.2615225 0.2172422 -16.9 30 Ethylbenzene A 5.00 4.99 1.439572 1.437287 -0.2 30 4-Ethyltoluene A 5.00 5.50 1.384056 1.52282 10.0 30 Heptane A 5.00 4.82 0.3047774 0.2934916 -3.7 30 Hexachlorobutadiene A 5.00 4.95 0.3462355 0.3429244 -1.0 30 Hexane A 5.00 4.50 1.064145 0.8427718 -10.0 30 Page 29 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S052675-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone(MBK) A 5.00 5.61 0.7811532 0.8763227 12.2 30 Isopropanol A 5.00 4.33 1.148999 0.9946818 -13.4 30 Methyl tert-Butyl Ether (MTBE) A 5.00 3.94 1.954358 1.53934 -21.2 30 Methylene Chloride A 5.00 3.83 1.022002 0.7826771 -23.4 30 4-Methyl-2-pentanone (MI13K) A 5.00 5.51 0.7709494 0.8501613 10.3 30 Naphthalene A 5.00 5.68 1.085833 1.234371 13.7 30 Propene A 5.00 4.18 0.6831069 0.571716 -16.3 30 Styrene A 5.00 5.10 0.7957025 0.8123131 2.1 30 1,1,2,2-Tetrachloroethane A 5.00 5.38 0.831055 0.8933491 7.5 30 Tetrachloroethylene A 5.00 4.64 0.4300822 0.3986633 -7.3 30 Tetrahydroforan A 5.00 4.01 0.3072743 0.2465254 -19.8 30 Toluene A 5.00 4.92 1.113036 1.09474 -1.6 30 1,2,4-Trichlorobenzene A 5.00 5.74 0.3844426 0.4415344 14.9 30 1, 1, 1 -Trichloroethane A 5.00 4.74 0.5985351 0.5673123 -5.2 30 1,1,2-Trichloroethane A 5.00 4.89 0.3937739 0.3848435 -2.3 30 Trichloroethylene A 5.00 4.49 0.3942249 0.3538706 -10.2 30 Trichlorofluoromethane (Freon 11) A 5.00 4.68 1.21703 1.1398 -6.3 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 4.18 1.272717 1.064943 -16.3 30 1,2,4-Trimethylbenzene A 5.00 5.51 1.131143 1.247477 10.3 30 1,3,5-Trimethylbenzene A 5.00 5.40 1.197527 1.293711 8.0 30 Vinyl Acetate A 5.00 3.58 2.43106 1.741573 -28.4 30 Vinyl Chloride A 5.00 3.86 0.6541511 0.5048648 -22.8 30 m&p-Xylene A 10.0 10.5 1.091281 1.144152 4.8 30 o-Xylene A 5.00 5.20 1.128079 1.172352 3.9 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 30 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte EPA TO-15 in Air Acetone Benzene Benzyl chloride Bromodichloromethane Bromoform Bromomethane 1,3-Butadiene 2-Butanone (MEK) Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Cyclohexane Dibromochloromethane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane (Freon 12) 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethylene cis-1,2-Dichloroethylene trans- l,2-Dichloro ethylene 1,2-Dichloropropane cis- 1,3 -Dichloropropene trans- 1, 3 -Dichloropropene 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 1,4-Dioxane Ethanol Ethyl Acetate Ethylbenzene 4-Ethyltoluene Heptane Hexachlorobutadiene Hexane 2-Hexanone (MBK) Isopropanol Methyl tart -Butyl Ether (MTBE) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Naphthalene Propene Styrene 1,1,2,2-Tetrachloroethane Certifications AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,Nf E,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA, FL,NJ,NY,ME,NH, VA AIHA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH NY,ME,NH AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA Page 31 of 35 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications EPA TO-15 in Air Tetrachloroethylene AIHA,FL,NJ,NY,ME,NH,VA Tetrahydrofuran AIHA Toluene AIHA,FL,NJ,NYM E,NH,VA 1,2,4-Trichlorobenzene AIHA,NJ,NY,ME,NH,VA 1, 1, 1 -Trichloroethane AIHA,FL,NJ,NY,ME,NH,VA 1,1,2-Trichloroethane AIHA,FL,NJ,NY,ME,NH,VA Trichloroethylene AIHA,FL,NJ,NY,ME,NH,VA Trichlorofluoromethane (Freon 11) AIHA,NY,ME,NH 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) AIHA,NJ,NY,ME,NH,VA 1,2,4-Trimethylbenzene AIHA,NJ,NY,ME,NH 1,3,5-Trimethylbenzene AIHA,NJ,NY,ME,NH Vinyl Acetate AIHA,FLNJ,NY,ME,NH,VA Vinyl Chloride AIHA,FLNJ,NY,ME,NH,VA m&p-Xylene AIHA,FL,NJ,NY,ME,NH,VA o-Xylene AIHA,FL,NJ,NY,ME,NH,VA The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2017 100033 03/l/2022 MA Massachusetts DEP M-MA100 06/30/2021 CT Connecticut Department of Publilc Health PH-0567 09/30/2021 NY New York State Department of Health 10899 NELAP 04/1/2021 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2021 RI Rhode Island Department of Health LA000112 12/30/2020 NC North Carolina Div. of Water Quality 652 12/31/2020 NJ New Jersey DEP MA007 NELAP 06/30/2021 FL Florida Department of Health E871027 NELAP 06/30/2021 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2021 ME State of Maine 2011028 06/9/2021 VA Commonwealth of Virginia 460217 12/14/2020 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2021 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2021 NC-DW North Carolina Department of Health 25703 07/31/2021 PA Commonwealth of Pennsylvania DEP 68-05812 06/30/2021 MI Dept. of Env, Great Lakes, and Energy 9100 10/1/2020 Page 32 of 35 ZLLL]6 w contesE[abs tom Doc # 379 Rev-0 5/8l2D15 ( �} CO fl EES��>hone: 413.525-2332 CHAIN Ohtt oif F CUSTODY RECORD (Borth Carrsaj 39 Spruce Street ���� n Tax: 413.525-6405 Easy Longmeadow, MA 01029 Email: infoocontestiabs.com 7-paFEWWWRIPPMy ,Q FQ-Day [f RUH Environmental Consuttm Address: 4012 Ridgebrook Bluffs Dr., Raleigh NC 27603 Phone: (919)389.7747 vay I_I 3-Day ❑ ANALYSIS REQUESTED National Linen 2-Da -' Project Location: y 4 Day ❑ W WRmington, NC t _ Project Number. 2Q09.Q0 Formal: PDF ❑✓ EXCEL Q Project Manai Can -Test Bid: Invoice Recipie Semp1111 By: Con -Test work Order# Page 1 of 1 # of Containers 10 a Preservation Code ' Container Code S O Field Filtered O Lab to Filter o v Kerry McGee Other: NC SG srs EDD r Order # 2009028 _ d a Enhanced Data package Required:^' Rob Hitl ` - a O Feld Filtered Email To: fob rdheg.com a O Rob Hill Fax To #' v ! j .. �' lab to Filter Ctient Sample ID / Driptton esc Beginning Ending Composite u LLLLI Date/Time Date/Tsme l E SG-1 /Boller Room (S) [BC 2096, FC 4353] 9/1012020 9!€0l2020 1631 164o SG-2 / Storage ISE) [BC 2112, FC 4354) 9l10l2020 9/10/2,020 M 1654 1703 -3D SG-31Siorpge(E)[BC2235,FC4321]9/10l2020 9lm7202o172D 30 1729 - 5G-4 / Storage (SW) 16C 2257, FC 43371 9/1012020 9/10/2020 ao 1746 1755 A U x _� - � NDTF 1: SG-5 / Laundry Area (SE) (8C 2103, FC 4211] 9lt0/2020 9/14312020 1808 181), A U X All samples are sub-s}ab wllected beneath slab foundations, unknown level of -30 SG-5 DUP / Laundry Area (SE) [BC 2326, rC 4211) 9/10/2020 9/10/2020 1808 1B17 A U X -contamination, if any. An Inf lal diluunn Is recommended to gauge range, -3o SG-6I Laundry Area (NE) [BC 2312, FC 4253] -+9/1 D/2020 9110l2020 'Mat X Codes; GW = Ground Water WW - Waste Water OW = Drinking Water A = A€r 5 = Soil/Solid SL - Sludge O - Other(please define) 1830 1839 A U % .30 -5 a Preservation Codes: SG-71 Laundry Area (SW) [BE 2099, FC 4348] 9110/202D 9/10/2020 I = iced 1856 t90i A U X -39 -5 H = HCI, SG-8 / Laundry Area (NW) [I" 224or FC 4347] 9/10/2020 9110/2020 M - Methano( 1920 1929 A U X -30 -5 N - Nitric Acid $G-[B €r2126, FC 432 9/10/2020 9/10/2020 - 5 = SDIfUFIC Acid (NW) (8C 2126, FC 4320] ",1 .oc1 A O X Please email results in PDF and Excel EDD format with units in ug/m]i with NC iNSB / Brownfields RESIDENTIAL SOIL GAS screenRlg levels included) by: v eived by: (signature} (Q O W inquished by: (signature} W eived by; (signaturey Cl) C31 QIl 1:11?3p -30 _s B = Sodium Bisulfate X = Sodium Hydroxide T - Sodium Thiosulfate Please use the following Codes to indicate possible sample concentration within O - Other (please the Conc Codecdumn above: define) H - High; M - Medium; L - Low; C - Clean; U - Unknown s Contat_„ ner Codes: Program lnfarmation c � slas Amber class 2L GWPC 1) MC O UST P = Plastic SW51 O SWS Landfill O Trust Fund ST = Sterile a -IHSB Orphaned landfilt REC = Via[ 1H5B (RESIDFNTIAL SGJ S = Summa Canister MSC[ O State Lead T = Ted lar Bag Ot a MC Brownflelds Program O - Other (please deffnel NELAC and A1HA-LAP, LLC Accredited 3UND TIME (BUSINESS DAYS) STARTS AT 9:00 AM THE DAY AFTER SAMPLE RECEIPT UNLESS THERE ARE NS ON THIS CHAIN. 1F THIS FORM IS NOT FILLED OUT COMPLETELY OR IS INCORRECT, TURNAROUND TIME START UNTIL ALL QUESTIONS HAVE BEEN ANSWERED. PLEASE BE CAREFUL NOT TO CONTAMINATE THIS DOCUMENT 9/18/2020 Track your package or shipment with FedEx Tracking IMPORTANT! FedE x is closely Monitoring the Remnants of Sally and Wildfires. Learn More N&X 715C,267S91 b �\, * Delivered Friday 9/1 S/2020 at 10.-53 am DFLIVERLD Signature not required GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM TO R�I�ioh, NG lJS - 1_AS1 :L0N6VAL At11UtiN,-MA LDS Multiple -piece Shipment 3 Piece shipment TRACKING NUMBER SHIPPER CITY, D.ESTJNAT10N/REC€PIENT STATE SHED PATE STRTDS, ,. ..,.DELIVERY DATE CITY, STATE 'i �5U �'3607 r�JR('A'Vi,NC 9,` 3;2020 9;�1I%2l)20' k=ASI L0NGv]EAr)1'-;VV,MA 77 507 13629 DNRi i`F2iv1, NC 911 1 1 i2020 a 9 i 5'2U20 FAS1 LONGM EADCW, MA 771502 b7>91 b DURi 4.j (M, !V 9! i i 12020 -9,1812G20 LAST LONGM AGJlu, MA Shipment Facts TRACKING NUMBER 7 i 5,)2673(,16 MASTER TRACKING NUMBER TOTAL PIECES S SERVICE F eel-x'Grourid WEIGHT 15 Il�s; F S kt�s TOTAL SHIPMENT WEIGHT REFERENCE 2G[i 00 Nat'l t_.w 1. `v`i 0=, irr: DIMENSIONS M),1 7x10 in TERMS SI t ppef PACKAGING STANDARD TRANSIT SHIP DATE �ckac;c � f, j C i 5 2a^C; r i g!11; 2020 https:llwww,fedex.com/apps/fedextrack/?action=track&tracknumbers=771502673916&locale=en_US&cntry_code=us Page 34 of 35 I Haye Not Confirmed Sample Container Numbers With Lab Staff Before C: 4:11 n amn bE md"'Plow tw Relinquishing Over ANALYTICAL LABOF�A-r�iiY Samples Do. c,#.278 Rev 6 2Q17. Air Media Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State True or False Client Received By {� Date Time How were the samples In Cooler On Ice No Ice received? In Box e Ambient Melted Ice Were samples within Temperature By Gun # Actual Temp - Compliance? 2-6°C By Blank # Actual Temp - Was Custody Seal Intact? V—(A Were Samples Tampered with? Was COG Relinquished ? 7 Does Chain Agree With Samples? Are there any loose caps/valves on any samples? j= Is COG in ink/ Legible? i Did COG Include all Client 7 Analysis -7 Sampler Name - i Pertinent Information? Project 1 Are Sample Labels filled out and legible? Are there Rushes? Samples are received within holding time? Proper Media Used? --I Are there Trip Blanks? 1�7 I D's 1 Who was notified? �C Collection DatesfTimes Individually Certified Cans? 17— Is there enough Volume? MCA- sec i = - C� � c-0 v ' Oo�� Pape 35 of 35 1 RDFr \1 Environmental Consulting 4012 Ridgebrook Bluffs Dr. I Raleigh, NC 27603 (919) 389-7747 1 info@rdhec.com APPENDIX E NCDEQ RISK CALCULATOR RESULTS (RESIDENT SOIL GAS TO INDOOR AIR PATHWAY FOR VAPOR INTRUSION) Risk for Individual Pathways rim Version Date: July 2020 Basis: May 2020 EPA RSL Table 7 Site ID: 24028-20-065 Exposure Unit ID: DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway Risk Carcinogenic Hazard Index Risk exceeded`., Resident Soil 0.0E+00 0.0E+00 NO NC Groundwater Use* NC NC Non -Residential Worker Soil 0.0E+00 0.0E+00 NO Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS Receptor Pathway CarcinogenicRisk Hazard Index Risk exceeded? Resident Groundwater to Indoor Air 0.0E+00 0.0E+00 NO Soil Gas to Indoor Air 4.1E-05 1.4E+00 YES Indoor Air 0.0E+00 0.0E+00 NO Non -Residential Worker Groundwater to Indoor Air 0.0E+00 0.0E+00 NO Soil Gas to Indoor Air 3.1E-06 1.1E-01 NO Indoor Air 0.0E+00 0.0E+00 NO CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 21, at Receptor? NM Source Groundwater Exceedence of 21, at Receptor? NM Surface Water Source Soil Exceedence of 2B at Receptor? NM Source Groundwater Exceedence of 2B at Receptor? NM Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not complete North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Soil Gas to Indoor Air 1 Version Date: July 2020 Basis: May 2020 EPA RSL Table Site ID: 24028-20-065 Exposure Unit ID: Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m3 CAS # Chemical Name: Soil Gas Concentration s (ug/m) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 790 7.9 2.7E+04 5.8E-05 71-43-2 Benzene 5.3 0.053 1.6E+00 2.6E+01 3.4E-08 4.0E-04 67-66-3 Chloroform 130 1.3 5.3E-01 8.6E+01 2.4E-06 3.0E-03 75-71-8 Dichlorodifluoromethane 1200 12 8.8E+01 2.7E-02 123-91-1 Dioxane, 1,4- 8.8 0.088 2.5E+00 2.6E+01 3.6E-08 6.7E-04 141-78-6 Ethyl Acetate 39 0.39 6.1E+01 1.3E-03 100-41-4 Eth lbenzene 17 0.17 4.9E+00 8.8E+02 3.5E-08 3.9E-05 142-82-5 Heptane, N- 5.2 0.052 3.5E+02 3.0E-05 110-54-3 Hexane, N- 3.5 0.035 6.1E+02 1.1E-05 67-63-0 Iso ro anol 240 2.4 1.8E+02 2.7E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone) 61 0.61 4.4E+03 2.8E-05 108-10-1 Methyl Isobutyl Ketone (4-meth 1-2- entanone) 32 0.32 2.6E+03 2.4E-05 91-20-3 -Naphthalene 13 0.13 3.6E-01 2.6E+00 3.6E-07 9.9E-03 100-42-5 Styrene 2.3 0.023 8.8E+02 5.3E-06 127-18-4 Tetrachloroeth lene 65 0.65 4.7E+01 3.5E+01 1.4E-08 3.7E-03 108-88-3 Toluene 56 0.56 4.4E+03 2.6E-05 79-01-6 Trichloroeth lene 47 0.47 3.0E+00 1.8E+00 1.6E-07 5.4E-02 95-63-6 Trimeth lbenzene, 1,2,4- 38 0.38 5.3E+01 1.4E-03 108-67-8 Trimeth lbenzene, 1,3,5- 8.8 0.088 5.3E+01 3.3E-04 10642-3 X lene, P- 71 0.71 8.8E+01 1.6E-03 108-38-3 X lene, m- 71 0.71 8.8E+01 1.6E-03 9547-6 X lene, o- 27 0.27 8.8E+01 6.2E-04 Cumulative: I 3.1E-06 I 1.1E-01 North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: July 2020 Basis: Mav 2020 EPA RSL Table Site ID: 24028-20-065 Exposure Unit ID: Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m3 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m) Target Indoor Air Conc. for Carcinogens @ TCR = 1 E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 790 23.7 6.5E+03 7.3E-04 71-43-2 Benzene 5.3 0.159 3.6E-01 6.3E+00 4.4E-07 5.1E-03 67-66-3 Chloroform 130 3.9 1.2E-01 2.0E+01 3.2E-05 3.8E-02 75-71-8 Dichlorodifluoromethane 1200 36 2.1E+01 3.5E-01 123-91-1 Dioxane, 1,4- 8.8 0.264 5.6E-01 6.3E+00 4.7E-07 8.4E-03 141-78-6 Ethyl Acetate 39 1.17 1.5E+01 1.6E-02 100-41-4 Eth lbenzene 17 0.51 1.1E+00 2.1E+02 4.5E-07 4.9E-04 142-82-5 He tane, N- 5.2 0.156 8.3E+01 3.7E-04 110-54-3 Hexane, N- 3.5 0.105 1.5E+02 1.4E-04 67-63-0 Iso ro anol 240 7.2 4.2E+01 3.5E-02 78-93-3 Methyl Ethyl Ketone (2-Butanone) 61 1.83 1.0E+03 3.5E-04 108-10-1 Methyl Isobutyl Ketone (4-meth 1-2- entanone) 32 0.96 6.3E+02 3.1E-04 91-20-3 -Naphthalene 13 0.39 1 8.3E-02 6.3E-01 4.7E-06 1.2E-01 10042-5 Styrene 2.3 0.069 2.1E+02 6.6E-05 127-18-4 Tetrachloroeth lene 65 1.95 1.1E+01 8.3E+00 1.8E-07 4.7E-02 108-88-3 Toluene 56 1.68 1.0E+03 3.2E-04 79-01-6 Trichloroeth lene 47 1.41 4.8E-01 4.2E-01 2.9E-06 6.8E-01 95-63-6 Trimeth lbenzene, 1,2,4- 38 1.14 1.3E+01 1.8E-02 108-67-8 Trimeth lbenzene, 1,3,5- 8.8 0.264 1.3E+01 4.2E-03 10642-3 X lene,P- 71 2.13 2.1E+01 2.0E-02 108-38-3 X lene, m- 71 2.13 2.1E+01 2.0E-02 95-47-6 Xylene, o- 27 0.81 2.1E+01 7.8E-03 Cumulative: I 4.1E-05 I 1.4E+00 North Carolina DEQ Risk Calculator Risk for Individual Pathways rim Version Date: July 2020 Basis: May 2020 EPA RSL Table 7 Site ID: 24028-20-065 Exposure Unit ID: DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway Risk Carcinogenic Hazard Index Risk exceeded`., Resident Soil 0.0E+00 0.0E+00 NO NC Groundwater Use* NC NC Non -Residential Worker Soil 0.0E+00 0.0E+00 NO Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS Receptor Pathway CarcinogenicRisk Hazard Index Risk exceeded? Resident Groundwater to Indoor Air 0.0E+00 0.0E+00 NO Soil Gas to Indoor Air 8.2E-06 8.9E-01 NO Indoor Air 0.0E+00 0.0E+00 NO Non -Residential Worker Groundwater to Indoor Air 0.0E+00 0.0E+00 NO Soil Gas to Indoor Air 5.6E-07 7.1E-02 NO Indoor Air 0.0E+00 0.0E+00 NO CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 21, at Receptor? NM Source Groundwater Exceedence of 21, at Receptor? NM Surface Water Source Soil Exceedence of 2B at Receptor? NM Source Groundwater Exceedence of 2B at Receptor? NM Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not complete North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Soil Gas to Indoor Air 1 Version Date: July 2020 Basis: May 2020 EPA RSL Table Site ID: 24028-20-065 Exposure Unit ID: Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m3 CAS # Chemical Name: Soil Gas Concentration s (ug/m) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 250 2.5 2.7E+04 1.8E-05 71-43-2 Benzene 1.5 0.015 1.6E+00 2.6E+01 9.5E-09 1.1E-04 67-66-3 Chloroform 5.3E-01 8.6E+01 75-71-8 Dichlorodifluoromethane 19 0.19 8.8E+01 4.3E-04 123-91-1 Dioxane, 1,4- 2.5E+00 2.6E+01 141-78-6 Ethyl Acetate 6.1E+01 100-41-4 Eth lbenzene 14 0.14 4.9E+00 8.8E+02 2.9E-08 3.2E-05 142-82-5 Heptane, N- 1.9 0.019 3.5E+02 1.1E-05 110-54-3 Hexane, N- 3.5 0.035 6.1E+02 1.1E-05 67-63-0 Iso ro anol 34 1 0.34 1.8E+02 3.9E-04 78-93-3 Methyl Ethyl Ketone (2-Butanone) 11 0.11 4.4E+03 5.0E-06 108-10-1 Methyl Isobutyl Ketone (4-meth 1-2- entanone) 2.6E+03 91-20-3 -Naphthalene 13 0.13 3.6E-01 2.6E+00 3.6E-07 9.9E-03 100-42-5 Styrene 8.8E+02 127-18-4 Tetrachloroeth lene 19 0.19 4.7E+01 3.5E+01 4.0E-09 1.1E-03 108-88-3 Toluene 28 0.28 4.4E+03 1.3E-05 79-01-6 Trichloroeth lene 47 0.47 3.0E+00 1.8E+00 1.6E-07 5.4E-02 95-63-6 Trimeth lbenzene, 1,2,4- 38 0.38 5.3E+01 1.4E-03 108-67-8 Trimeth lbenzene, 1,3,5- 8.7 0.087 5.3E+01 3.3E-04 106-42-3 X lene, P- 59 0.59 8.8E+01 1.3E-03 108-38-3 1 X lene, m- 59 0.59 8.8E+01 1.3E-03 9547-6 1 X lene, o- 1 24 0.24 8.8E+01 5.5E-04 Cumulative: I 5.6E-07 I 7.1E-02 North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: July 2020 Basis: Mav 2020 EPA RSL Table Site ID: 24028-20-065 Exposure Unit ID: Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m3 CAS # Chemical Name: Soil Gas Concentration 3 (ug/m) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ T'HQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 250 7.5 6.5E+03 2.3E-04 71-43-2 Benzene 1.5 0.045 3.6E-01 6.3E+00 1.3E-07 1.4E-03 67-66-3 Chloroform 1.2E-01 2.0E+01 75-71-8 Dichlorodifluoromethane 19 0.57 2.1E+01 5.5E-03 123-91-1 Dioxane, 1,4- 5.6E-01 6.3E+00 141-78-6 Ethyl Acetate 1.5E+01 100-41-4 Eth lbenzene 14 0.42 1 1.1E+00 2.1E+02 3.7E-07 4.0E-04 142-82-5 Heptane, N- 1.9 0.057 8.3E+01 1.4E-04 110-54-3 Hexane, N- 3.5 0.105 1.5E+02 1.4E-04 67-63-0 Iso ro anol 34 1.02 4.2E+01 4.9E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone) 11 0.33 1.0E+03 6.3E-05 108-10-1 Methyl Isobutyl Ketone (4-meth 1-2- entanone) 6.3E+02 91-20-3 -Naphthalene 13 0.39 8.3E-02 6.3E-01 4.7E-06 1.2E-01 100-42-5 Styrene 2.1E+02 127-18-4 Tetrachloroeth lene 19 1 0.57 1.1E+01 8.3E+00 5.3E-08 1.4E-02 108-88-3 Toluene 28 0.84 1.0E+03 1.6E-04 79-01-6 Trichloroeth lene 47 1.41 4.8E-01 4.2E-01 2.9E-06 6.8E-01 95-63-6 Trimeth lbenzene, 1,2,4- 38 1.14 1.3E+01 1.8E-02 108-67-8 Trimeth lbenzene, 1,3,5- 8.7 0.261 1.3E+01 4.2E-03 10642-3 X lene, P- 59 1.77 2.1E+01 1.7E-02 108-38-3 X lene, m- 59 1.77 2.1E+01 1.7E-02 95-47-6 Xylene, o- 24 0.72 2.1E+01 6.9E-03 Cumulative: I 8.2E-06 I 8.9E-01 North Carolina DEQ Risk Calculator Risk for Individual Pathways rim Version Date: July 2020 Basis: May 2020 EPA RSL Table 7 Site ID: 24028-20-065 Exposure Unit ID: DIRECT CONTACT SOIL AND WATER CALCULATORS Receptor Pathway Carcinogenic Hazard Index Risk exceeded? Resident Soil 0.0E+00 0.0E+00 NO NC Groundwater Use* NC NC Non -Residential Worker Soil 0.0E+00 0.0E+00 NO Groundwater Use* NC NC NC Construction Worker Soil NC NC NC Recreator/Trespasser Soil NC NC NC Surface Water* NC NC NC VAPOR INTRUSION CALCULATORS no Receptor Pathway CarcinogenicRisk Hazard Index Risk exceeded? Resident Groundwater to Indoor Air 0.0E+00 0.0E+00 NO Soil Gas to Indoor Air 4.0E-06 6.4E-01 NO Indoor Air 0.0E+00 0.0E+00 NO Non -Residential Worker Groundwater to Indoor Air 0.0E+00 0.0E+00 NO Soil Gas to Indoor Air 2.9E-07 5.1E-02 NO Indoor Air 0.0E+00 0.0E+00 NO CONTAMINANT MIGRATION CALCULATORS Pathway Source Target Receptor Concentrations Exceeded? Groundwater Source Soil Exceedence of 21, at Receptor? NM Source Groundwater Exceedence of 21, at Receptor? NM Surface Water Source Soil Exceedence of 2B at Receptor? NM Source Groundwater Exceedence of 2B at Receptor? NM Notes: 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk -based closure. 3. NM = Not Modeled 4. NC = Pathway not complete North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Soil Gas to Indoor Air 1 Version Date: July 2020 Basis: May 2020 EPA RSL Table Site ID: 24028-20-065 Exposure Unit ID: Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m3 CAS # Chemical Name: Soil Gas Concentration s (ug/m) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 470 4.7 2.7E+04 3.5E-05 71-43-2 Benzene 5.3 0.053 1.6E+00 2.6E+01 3.4E-08 4.0E-04 67-66-3 Chloroform 5.3E-01 8.6E+01 75-71-8 Dichlorodifluoromethane 1200 12 8.8E+01 2.7E-02 123-91-1 Dioxane, 1,4- 8.8 0.088 2.5E+00 2.6E+01 3.6E-08 6.7E-04 141-78-6 Ethyl Acetate 39 0.39 6.1E+01 1.3E-03 100-41-4 Eth lbenzene 13 0.13 4.9E+00 8.8E+02 2.7E-08 3.0E-05 142-82-5 Heptane, N- 4.2 0.042 3.5E+02 2.4E-05 110-54-3 Hexane, N- 6.1E+02 67-63-0 Iso ro anol 73 0.73 1.8E+02 8.3E-04 78-93-3 Methyl Ethyl Ketone (2-Butanone) 61 0.61 4.4E+03 2.8E-05 108-10-1 Methyl Isobutyl Ketone (4-meth 1-2- entanone) 32 0.32 2.6E+03 2.4E-05 91-20-3 -Naphthalene 5.7 0.057 3.6E-01 2.6E+00 1.6E-07 4.3E-03 100-42-5 Styrene 2.3 0.023 8.8E+02 5.3E-06 127-18-4 Tetrachloroeth lene 9.2 0.092 4.7E+01 3.5E+01 2.0E-09 5.3E-04 108-88-3 Toluene 40 0.4 4.4E+03 1.8E-05 79-01-6 Trichloroeth lene 11 0.11 3.0E+00 1.8E+00 3.7E-08 1.3E-02 95-63-6 Trimeth lbenzene, 1,2,4- 5.3E+01 108-67-8 Trimeth lbenzene, 1,3,5- 6.1 0.061 5.3E+01 2.3E-04 10642-3 X lene,P- 43 0.43 8.8E+01 9.8E-04 108-38-3 X lene, m- 43 0.43 8.8E+01 9.8E-04 9547-6 X lene, o- 17 0.17 8.8E+01 3.9E-04 Cumulative: I 2.9E-07 I 5.1E-02 North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: July 2020 Basis: Mav 2020 EPA RSL Table Site ID: 24028-20-065 Exposure Unit ID: Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m3 CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m) Target Indoor Air Conc. for Carcinogens @ TCR = 1 E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 470 14.1 6.5E+03 4.4E-04 71-43-2 Benzene 5.3 0.159 3.6E-01 6.3E+00 4.4E-07 5.1E-03 67-66-3 Chloroform 1.2E-01 2.0E+01 75-71-8 Dichlorodifluoromethane 1200 36 2.1E+01 3.5E-01 123-91-1 Dioxane, 1,4- 8.8 0.264 5.6E-01 6.3E+00 4.7E-07 8.4E-03 141-78-6 Ethyl Acetate 39 1.17 1.5E+01 1.6E-02 100-41-4 Eth lbenzene 13 0.39 1 1.1E+00 2.1E+02 3.5E-07 3.7E-04 142-82-5 He tane, N- 4.2 0.126 8.3E+01 3.0E-04 110-54-3 Hexane, N- 1.5E+02 67-63-0 Iso ro anol 73 2.19 4.2E+01 1.1E-02 78-93-3 Methyl Ethyl Ketone (2-Butanone) 61 1.83 1.0E+03 3.5E-04 108-10-1 Methyl Isobutyl Ketone (4-meth 1-2- entanone) 32 0.96 6.3E+02 3.1E-04 91-20-3 -Naphthalene 5.7 0.171 8.3E-02 6.3E-01 2.1E-06 5.5E-02 100-42-5 Styrene 2.3 0.069 2.1E+02 6.6E-05 127-18-4 Tetrachloroeth lene 9.2 0.276 1.1E+01 8.3E+00 2.6E-08 6.6E-03 108-88-3 Toluene 40 1.2 1.0E+03 2.3E-04 79-01-6 Trichloroeth lene 11 0.33 4.8E-01 4.2E-01 6.9E-07 1.6E-01 95-63-6 Trimeth lbenzene, 1,2,4- 1.3E+01 108-67-8 Trimeth lbenzene, 1,3,5- 6.1 0.183 1.3E+01 2.9E-03 10642-3 X lene, P- 43 1.29 2.1E+01 1.2E-02 108-38-3 X lene, m- 43 1.29 2.1E+01 1.2E-02 9547-6 Were, o- 17 0.51 2.1E+01 4.9E-03 Cumulative: I 4.0E-06 I 6.4E-Ol North Carolina DEQ Risk Calculator Appendix B - Site Photos NATIONAL LINEN - PHOTO LOG Photograph 1: Building Exterior & Entrance jI �-7 �-m WRL - . , •t i Photograph 2: Building Interior Page 1 NATIONAL LINEN - PHOTO LOG `FRiil�%-'% -AWIIIII Photograph 4: Interior— Building Supplies Page 2 0 WOW Jr. Wig.. NATIONAL LINEN - PHOTO LOG Photograph 9 - Building Interior Photograph 10 - Building Interior Page 5 Appendix C - Instrument Calibration i p� INSTRUMENT CALIBRATION REPORT Pine Environmental Services LLC 530 Pylon Drive Raleigh, NC 27606 Phone: (919) 713-0008 Pine Environmental Services, Inc. o Instrument ID 21706 Description MiniRAE 3000 Calibrated 9/9/202012:43:16PM Manufacturer Rae Systems State Certified Model Number MiniRAE 3000 Status Pass Serial Number/ Lot 592-908279 Temp °C 24 Number Location North Carolina Humidity % 52 Department Calibration Specifications Group # I Range Ace % 0.0000 Group Name lsobutylene Reading Ace % 3.0000 Stated Accy Pet of Reading Plus/Minus 0.0 Nom In Val / In Val In Type Out Val Out Tvpe FndAs LftAs Dev% Pass/Fail 100.0 / 100.0 PPM I00.0 PPM 92.8 100.1 0.10% Pass Test Instruments Used During the Calibration As Of Cal Entry Date Serial Number / Next Cal Date / Test Standard ID Description Manufacturer Model Number Lot Number Last Cal Date/ Expiration Date Opened Date NC ISO 100 NC ISO 100 Pine 31721 9/4/2.023 GBJ-248-100-3 GBJ-248-100-3 Environmental Services, Inc. Notes about this calibration Calibration Result Calibration Successful Who Calibrated Blaine Bunch All instruments are calibrated by Pine Environmental Services LLC according to the manufacturer's specifications, but it is the customer's responsibility to calibrate and maintain this unit in accordance with the manufacturer's specifications and/or the customer's own specific needs. Notify Pine Environmental Services LLC of any defect within 24 hours of receipt of equipin ent Please call 800-301-9663 for Technical Assistance Pine Environmental Services LLC Windsor Industrial Park, 92 North Main Street, Bldg 20, Windsor, NJ 08561, 800-301-9663 www.pine-environmental.com Appendix D - Boring Logs f'-' LOG OF BORING: TW-1 PROCTOR 5113 Yachtsman Ct PESENVIRONMENTAL Raleigh, NC 27615 , SERVICES, INC. Ph: (919) 630-0721 Page: 1 of 1 Site Name: National Linen Drilling/Boring Method: GeoProbe Total Boring Depth (ft): 9 Project Number: R331 Sampling Method: DPT Temp Well Depth (ft): 9 Location: Wilmington, NC Subcontractor/Drillers: Regional Probing Screen Depth (ft): 4' - 9' Date Started: 9/11/2020 Driller : Larry Opper Approx. DTW (ft): 3.69' Date Completed: 9/11/2020 Monitoring Equipment: PID PES Field Staff: To Proctor Sampling SOIL DESCRIPTION (color, texture, moisture, comments etc.) Construction Details a w Interval, Odors a 0 Asphalt and Stone Base a o 0 i i 0 0 i i 3.69' 5 Tan, brown, orange and gray mottled silty fine sand and/or fill material --- 5 z 0 --- 0 0 0 u ' 10 10 0 0 1s 15 20 20 25 25 30 TD = 16 ft. 30 COMMENTS: in - indicates inches N/A - indicates not applicable to this boring DTW - Depth to Water at Time of GeoProbe ft - indicates depth in feet ppm - indicates parts per million ♦ Approximate Static Water Level ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling The shaded area represents the sample interval submitted to the laboratory f'-' LOG OF BORING: TW-2 PROCTOR 5113 Yachtsman Ct PESENVIRONMENTAL Raleigh, NC 27615 , SERVICES, INC. Ph: (919) 630-0721 Page: 1 of 1 Site Name: National Linen Drilling/Boring Method: GeoProbe Total Boring Depth (ft): 15 Project Number: R331 Sampling Method: DPT Temp Well Depth (ft): 15 Location: Wilmington, NC Subcontractor/Drillers: Regional Probing Screen Depth (ft): 5'- 15' Date Started: 9/11/2020 Driller: Larry Opper Approx. DTW (ft): 6.61' Date Completed: 9/11/2020 Monitoring Equipment: PID PES Field Staff: To Proctor Sampling g R ° SOIL DESCRIPTION (color, texture, moisture, comments etc.) Construction Details a w Interval, Odors A F, �° w a 0 Asphalt and Stone Base a o 0 i i u W 5 0 5 z U 6.61' Tan, brown, orange and gray mottled silty fine sand and/or fill material --- 10 --- 10 15 ; --- ; 15 20 20 25 i i 25 30 Temp well installed in soil boring B-7 as original location encountered probe refusal at 9' bls TD = 9 ft. 30 COMMENTS: in - indicates inches N/A - indicates not applicable to this boring DTW - Depth to Water at Time of GeoProbe ft - indicates depth in feet ppm - indicates parts per million ♦ Approximate Static Water Level ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling The shaded area represents the sample interval submitted to the laboratory f'-' LOG OF BORING: TW-3 PROCTOR 5113 Yachtsman ct PESENVIRONMENTAL Raleigh, NC 27615 , SERVICES, INC. Ph: (919) 630-0721 Page: 1 of 1 Site Name: National Linen Drilling/Boring Method: GeoProbe Total Boring Depth (ft): 15 Project Number: R331 Sampling Method: DPT Temp Well Depth (ft): 15 Location: Wilmington, NC Subcontractor/Drillers: Regional Probing Screen Depth (ft): 5' - 15' Date Started: 9/11/2020 Driller : Larry Opper Approx. DTW (ft): 6.73' Date Completed: 9/11/2020 Monitoring Equipment: PID PES Field Staff: To Proctor Sampling g R ° SOIL DESCRIPTION (color, texture, moisture, comments etc.) Construction Details a w Interval, Odors A F, �° w a 0 Asphalt and Stone Base a o 0 i i u W 5 0 --- 5 z U --- 6.73' Tan, brown, orange and gray mottled silty fine sand and/or fill material --- 10 --- 10 15 ; --- ; 15 20 20 25 i i 25 30 TD = 12 ft. 30 COMMENTS: in - indicates inches N/A - indicates not applicable to this boring DTW - Depth to Water at Time of GeoProbe ft - indicates depth in feet ppm - indicates parts per million ♦ Approximate Static Water Level ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling The shaded area represents the sample interval submitted to the laboratory f'-' LOG OF BORING: TW-4 PROCTOR 5113 Yachtsman ct PESENVIRONMENTAL Raleigh, NC 27615 , SERVICES, INC. Ph: (919) 630-0721 Page: 1 of 1 Site Name: National Linen Drilling/Boring Method: GeoProbe Total Boring Depth (ft): 15 Project Number: R331 Sampling Method: DPT Temp Well Depth (ft): 15 Location: Wilmington, NC Subcontractor/Drillers: Regional Probing Screen Depth (ft): 5'- 15' Date Started: 9/11/2020 Driller: Larry Opper Approx. DTW (ft): 5.91' Date Completed: 9/11/2020 Monitoring Equipment: PID PES Field Staff: To Proctor Sampling g R ° SOIL DESCRIPTION (color, texture, moisture, comments etc.) Construction Details a w Interval, Odors A F, �° w a 0 Asphalt and Stone Base a 0 u W 5 5 z U 0 i --- i 5.91, Tan, brown, orange and gray mottled silty fine sand and/or fill material --- 10 --- 10 15 ; --- ; 15 20 20 25 i i 25 30 TD = 12 ft. 30 COMMENTS: in - indicates inches N/A - indicates not applicable to this boring DTW - Depth to Water at Time of GeoProbe ft - indicates depth in feet ppm - indicates parts per million ♦ Approximate Static Water Level ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling The shaded area represents the sample interval submitted to the laboratory f'-' LOG OF BORING: TW-5 PROCTOR 5113 Yachtsman ct PESENVIRONMENTAL Raleigh, NC 27615 , SERVICES, INC. Ph: (919) 630-0721 Page: 1 of 1 Site Name: National Linen Drilling/Boring Method: GeoProbe Total Boring Depth (ft): 15 Project Number: R331 Sampling Method: DPT Temp Well Depth (ft): 15 Location: Wilmington, NC Subcontractor/Drillers: Regional Probing Screen Depth (ft): 5'- 15' Date Started: 9/11/2020 Driller: Larry Opper Approx. DTW (ft): 6.22' Date Completed: 9/11/2020 Monitoring Equipment: PID PES Field Staff: To Proctor Sampling g R ° SOIL DESCRIPTION (color, texture, moisture, comments etc.) Construction Details a w Interval, Odors A F, �° w a 0 Asphalt and Stone Base a 0 u W 5 0 --- 5 z U 6.22 Tan, brown, orange and gray mottled silty fine sand and/or fill material --- 10 --- 10 15 ; --- ; 15 20 20 25 i i 25 30 TD = 12 ft. 30 COMMENTS: in - indicates inches N/A - indicates not applicable to this boring DTW - Depth to Water at Time of GeoProbe ft - indicates depth in feet ppm - indicates parts per million ♦ Approximate Static Water Level ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling The shaded area represents the sample interval submitted to the laboratory f'-' LOG OF BORING: TW-6 PROCTOR 5113 Yachtsman Ct PESENVIRONMENTAL Raleigh, NC 27615 , SERVICES, INC. Ph: (919) 630-0721 Page: 1 of 1 Site Name: National Linen Drilling/Boring Method: GeoProbe Total Boring Depth (ft): 15 Project Number: R331 Sampling Method: DPT Temp Well Depth (ft): 15 Location: Wilmington, NC Subcontractor/Drillers: Regional Probing Screen Depth (ft): 5' - 15' Date Started: 9/11/2020 Driller : Larry Opper Approx. DTW (ft): 7.33' Date Completed: 9/11/2020 Monitoring Equipment: PID PES Field Staff: To Proctor Sampling g R ° SOIL DESCRIPTION (color, texture, moisture, comments etc.) Construction Details a w Interval, Odors A F, �° w a 0 Asphalt and Stone Base a 0 u W 5 0 --- 5 z U 0 Tan, brown, orange and gray mottled silty fine sand and/or fill material --- 7.33' 10 i --- i 10 15 ; --- ; 15 20 20 25 i i i 25 30 TD = 12 ft. 30 COMMENTS: in - indicates inches N/A - indicates not applicable to this boring DTW - Depth to Water at Time of GeoProbe ft - indicates depth in feet ppm - indicates parts per million ♦ Approximate Static Water Level ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling The shaded area represents the sample interval submitted to the laboratory f'-' LOG OF BORING: TW-7 PROCTOR 5113 Yachtsman ct PESENVIRONMENTAL Raleigh, NC 27615 , SERVICES, INC. Ph: (919) 630-0721 Page: 1 of 1 Site Name: National Linen Drilling/Boring Method: GeoProbe Total Boring Depth (ft): 15 Project Number: R331 Sampling Method: DPT Temp Well Depth (ft): 15 Location: Wilmington, NC Subcontractor/Drillers: Regional Probing Screen Depth (ft): 5'- 15' Date Started: 9/11/2020 Driller: Larry Opper Approx. DTW (ft): 6.03' Date Completed: 9/11/2020 Monitoring Equipment: PID PES Field Staff: To Proctor Sampling g R ° SOIL DESCRIPTION (color, texture, moisture, comments etc.) Construction Details a w Interval, Odors A F, �° w a 0 Asphalt and Stone Base a 0 u W 5 0 --- 5 z U 6.03' Tan, brown, orange and gray mottled silty fine sand and/or fill material ___ 10 --- 10 15 ; --- ; 15 20 20 25 i i 25 30 TD = 12 ft. 30 COMMENTS: in - indicates inches N/A - indicates not applicable to this boring DTW - Depth to Water at Time of GeoProbe ft - indicates depth in feet ppm - indicates parts per million ♦ Approximate Static Water Level ft-bgs - indicates feet below ground surface TD - Total Depth of Boring for Sampling The shaded area represents the sample interval submitted to the laboratory Appendix E - Laboratory Reports Case Narrative Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: National Linen Lab Submittal Date: 09/15/2020 Work Order: 0090162 10/13/20 14:08 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL a,j Angela D. Overcash Senior Project Manager Data Qualifiers Key Reference: CCVH CCV result is above control limits but within method parameters. Result is considered estimated. D RPD value outside of the control limits. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. M Matrix spike outside of the control limits. MI Matrix spike outside of the control limits. Matrix interference suspected. SE Surrogate recovery outside of the QC limits due to emulsion. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 93 Way� nt poiAICAL NALYT Sample Receipt Summary 10/13/2020 Work Order: 0090162 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received TW-1W 0090162-01 Water 09/11/20 13:40 09/15/20 12:00 TW-2W 0090162-02 Water 09/11/20 14:30 09/15/20 12:00 TW-3W 0090162-03 Water 09/11/20 13:00 09/15/20 12:00 TW-4W 0090162-04 Water 09/11/20 13:50 09/15/20 12:00 TW-5W 0090162-05 Water 09/11/20 14:40 09/15/20 12:00 TW-6W 0090162-06 Water 09/11/20 16:10 09/15/20 12:00 TW-7W 0090162-07 Water 09/11/20 17:00 09/15/20 12:00 TW-2S 0090162-08 Solid 09/11/20 14:30 09/15/20 12:00 TW-3S 0090162-09 Solid 09/11/20 13:00 09/15/20 12:00 TW-4S 0090162-10 Solid 09/11/20 13:50 09/15/20 12:00 TW-5S 0090162-11 Solid 09/11/20 14:40 09/15/20 12:00 TW-6S 0090162-12 Solid 09/11/20 16:10 09/15/20 12:00 TW-7S 0090162-13 Solid 09/11/20 17:00 09/15/20 12:00 Dupe 0090162-14 Water 09/11/20 0:00 09/15/20 12:00 Trip Blank 0090162-15 Water 09/11/20 0:00 09/15/20 12:00 Samples were received in good condition at 2.2 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 93 WayPAoi nt . NALYTICAL Summary of Detections 10,131620 Work Order: 00902 Waypoint ID Client ID Parameter Method Result Units 0090162-03 TW-3W Barium `6010D 0.023 mg/L 0090162-03 TW-3W Chloromethane 8260D 0.34 J ug/L 0090162-04 TW-4W Methylene Chloride 8260D 0.67 J ug/L 0090162-05 TW-5W Chloromethane 8260D 0.37 J ug/L 0090162-07 TW-7W Chloroform 8260D 0.23 J ug/L 0090162-07 TW-7W Tetrachloroethylene 8260D 0.27 J ug/L 0090162-08 TW-2S Chromium '6010D 1.7 mg/kg dry 0090162-08 TW-2S Lead `6010D 3.8 mg/kg dry 0090162-08 TW-2S Methylene Chloride 8260D 0.0052 mg/kg dry 0090162-09 TW-3S Chromium '6010D 1.5 mg/kg dry 0090162-09 TW-3S Lead `6010D 1.4 mg/kg dry 0090162-09 TW-3S Methylene Chloride 8260D 0.0032 J mg/kg dry 0090162-10 TW-4S Chromium "6010D 1.3 mg/kg dry 0090162-10 TW-4S Methylene Chloride 8260D 0.0035 J mg/kg dry 0090162-11 TW-5S Methylene Chloride 8260D 0.0030 J mg/kg dry 0090162-12 TW-6S Chromium "6010D 1.4 mg/kg dry 0090162-12 TW-6S Lead '6010D 1.6 mg/kg dry 0090162-12 TW-6S Methylene Chloride 8260D 0.0031 .1 mg/kg dry 0090162-13 TW-7S Benzo(a)pyrene 8270E 0.038 J mg/kg dry 0090162-13 TW-7S Benzo(b)fluoranthene 8270E 0.046 J mg/kg dry 0090162-13 TW-7S Fluoranthene 8270E 0.053 J mg/kg dry 0090162-13 TW-7S Pyrene 8270E 0.047 J mg/kg dry 0090162-13 TW-7S Chromium "6010D 2.1 mg/kg dry 0090162-13 TW-7S Lead '6010D 8.7 mg/kg dry 0090162-13 TW-7S Methylene Chloride 8260D 0.0035 .1 mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-1 W Attn: Tom Proctor Sample ID: 0090162-01 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 3.0 1 8270E 9/17/20 17:13 JMV P010794 1,2-Dichlorobenzene BRL ug/L 10 2.4 1 8270E 9/17/20 17:13 JMV P010794 1,3-Dichlorobenzene BRL ug/L 10 3.9 1 8270E 9/17/20 17:13 JMV P010794 1,4-Dichlorobenzene BRL ug/L 10 4.1 1 8270E 9/17/20 17:13 JMV P010794 1-Methyl naphthalene BRL ug/L 10 1.1 1 8270E 9/17/20 17:13 JMV P010794 2,4,5-Trichlorophenol BRL ug/L 20 3.6 1 8270E 9/17/20 17:13 JMV P010794 2,4,6-Trichlorophenol BRL ug/L 20 4.5 1 8270E 9/17/20 17:13 JMV P010794 2,4-Dichlorophenol BRL ug/L 10 2.6 1 8270E 9/17/20 17:13 JMV P010794 2,4-Dimethylphenol BRL ug/L 10 4.9 1 8270E 9/17/20 17:13 JMV P010794 2,4-Dinitrophenol BRL ug/L 50 12 1 8270E 9/17/20 17:13 JMV P010794 2,4-Dinitrotoluene BRL ug/L 10 4.2 1 8270E 9/17/20 17:13 JMV P010794 2,6-Dinitrotoluene BRL ug/L 20 3.9 1 8270E 9/17/20 17:13 JMV P010794 2-Chloronaphthalene BRL ug/L 20 4.7 1 8270E 9/17/20 17:13 JMV P010794 2-Chlorophenol BRL ug/L 10 2.7 1 8270E 9/17/20 17:13 JMV P010794 2-Methyl naphthalene BRL ug/L 10 1.2 1 8270E 9/17/20 17:13 JMV P010794 2-Methylphenol BRL ug/L 10 2.4 1 8270E 9/17/20 17:13 JMV P010794 2-Nitroaniline BRL ug/L 10 4.1 1 8270E 9/17/20 17:13 JMV P010794 2-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 17:13 JMV P010794 3,3'-Dichlorobenzidine BRL ug/L 10 3.9 1 8270E 9/17/20 17:13 JMV P010794 3/4-Methyl phenol BRL ug/L 10 2.5 1 8270E 9/17/20 17:13 JMV P010794 3-Nitroaniline BRL ug/L 10 3.8 1 8270E 9/17/20 17:13 JMV P010794 4,6-Dinitro-2-methylphenol BRL ug/L 50 11 1 8270E 9/17/20 17:13 JMV P010794 4-Bromophenyl phenyl ether BRL ug/L 20 4.4 1 8270E 9/17/20 17:13 JMV P010794 4-Chloro-3-methylphenol BRL ug/L 10 2.9 1 8270E 9/17/20 17:13 JMV P010794 4-Chloroaniline BRL ug/L 10 3.5 1 8270E 9/17/20 17:13 JMV P010794 4-Chlorophenyl phenyl ether BRL ug/L 20 4.7 1 8270E 9/17/20 17:13 JMV P010794 4-Nitroaniline BRL ug/L 10 4.1 1 8270E 9/17/20 17:13 JMV P010794 4-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 17:13 JMV P010794 Acenaphthene BRL ug/L 10 0.76 1 8270E 9/17/20 17:13 JMV P010794 Acenaphthylene BRL ug/L 20 0.60 1 8270E 9/17/20 17:13 JMV P010794 Aniline BRL ug/L 50 12 1 8270E 9/17/20 17:13 JMV P010794 Anthracene BRL ug/L 10 0.47 1 8270E 9/17/20 17:13 JMV P010794 Azobenzene BRL ug/L 10 3.2 1 8270E 9/17/20 17:13 JMV P010794 Benzo(a)anthracene BRL ug/L 10 0.74 1 8270E 9/17/20 17:13 JMV P010794 Benzo(a)pyrene BRL ug/L 10 0.44 1 8270E 9/17/20 17:13 JMV P010794 Benzo(b)fluoranthene BRL ug/L 10 0.87 1 8270E 9/17/20 17:13 JMV P010794 Benzo(g,hJ)perylene BRL ug/L 10 0.98 1 8270E 9/17/20 17:13 JMV P010794 Benzo(k)fluoranthene BRL ug/L 10 0.81 1 8270E 9/17/20 17:13 JMV P010794 Benzoic Acid BRL ug/L 100 19 1 8270E 9/17/20 17:13 JMV P010794 Benzyl alcohol BRL ug/L 10 2.5 1 8270E 9/17/20 17:13 JMV P010794 bis(2-Chloroethoxy)methane BRL ug/L 10 3.8 1 8270E 9/17/20 17:13 JMV P010794 Bis(2-Chloroethyl)ether BRL ug/L 10 2.6 1 8270E 9/17/20 17:13 JMV P010794 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-1 W Attn: Tom Proctor Sample ID: 0090162-01 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Bis(2-chloroisopropyl)ether BRL ug/L 10 2.8 1 8270E 9/17/20 17:13 JMV P010794 Bis(2-Ethylhexyl)phthaIate BRL ug/L 10 3.7 1 8270E 9/17/20 17:13 JMV P010794 Butyl benzyl phthalate BRL ug/L 10 2.9 1 8270E 9/17/20 17:13 JMV P010794 Chrysene BRL ug/L 10 0.98 1 8270E 9/17/20 17:13 JMV P010794 Dibenzo(a,h)anthracene BRL ug/L 20 1.6 1 8270E 9/17/20 17:13 JMV P010794 Dibenzofuran BRL ug/L 20 4.2 1 8270E 9/17/20 17:13 JMV P010794 Diethyl phthalate BRL ug/L 20 4.2 1 8270E 9/17/20 17:13 JMV P010794 Dimethyl phthalate BRL ug/L 10 4.1 1 8270E 9/17/20 17:13 JMV P010794 Di-n-butyl phthalate BRL ug/L 10 4.3 1 8270E 9/17/20 17:13 JMV P010794 Di-n-octyl phthalate BRL ug/L 10 4.5 1 8270E 9/17/20 17:13 JMV P010794 Fluoranthene BRL ug/L 10 0.57 1 8270E 9/17/20 17:13 JMV P010794 Fluorene BRL ug/L 10 0.46 1 8270E 9/17/20 17:13 JMV P010794 Hexachlorobenzene BRL ug/L 20 3.9 1 8270E 9/17/20 17:13 JMV P010794 Hexachlorobutadiene BRL ug/L 20 4.5 1 8270E 9/17/20 17:13 JMV P010794 Hexachlorocyclopentadiene BRL ug/L 20 7.3 1 8270E 9/17/20 17:13 JMV P010794 Hexachloroethane BRL ug/L 10 3.7 1 8270E 9/17/20 17:13 JMV P010794 Indeno(1,2,3-cd)pyrene BRL ug/L 10 0.75 1 8270E 9/17/20 17:13 JMV P010794 Isophorone BRL ug/L 10 4.1 1 8270E 9/17/20 17:13 JMV P010794 Naphthalene BRL ug/L 10 1.3 1 8270E 9/17/20 17:13 JMV P010794 Nitrobenzene BRL ug/L 10 3.8 1 8270E 9/17/20 17:13 JMV P010794 N-Nitroso-di-n-propylamine BRL ug/L 20 3.3 1 8270E 9/17/20 17:13 JMV P010794 N-Nitrosodiphenylamine BRL ug/L 20 4.4 1 8270E 9/17/20 17:13 JMV P010794 Pentachlorophenol BRL ug/L 50 11 1 8270E 9/17/20 17:13 JMV P010794 Phenanthrene BRL ug/L 10 0.40 1 8270E 9/17/20 17:13 JMV P010794 Phenol BRL ug/L 10 1.4 1 8270E 9/17/20 17:13 JMV P010794 Pyrene BRL ug/L 10 0.67 1 8270E 9/17/20 17:13 JMV P010794 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 11 % 43-140 SE 2-Fluorobiphenyl 13 % 44-119 SE 2-Fluorophenol 6 % 19-119 SE Nitrobenzene-d5 10 % 44-120 SE Phenol-d5 4 % 11-52 SE Terphenyl-d14 15 % 50-134 SE Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 9/19/20 1:10 JLB P010844 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 9/19/20 1:10 JLB P010844 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 9/19/20 1:10 JLB P010844 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 9/19/20 1:10 JLB P010844 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 9/19/20 1:10 JLB P010844 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 9/19/20 1:10 JLB P010844 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 9/19/20 1:10 JLB P010844 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 9/19/20 1:10 JLB P010844 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 9/19/20 1:10 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-1 W Attn: Tom Proctor Sample ID: 0090162-01 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 9/19/20 1:10 JLB P010844 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 9/19/20 1:10 JLB P010844 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 9/19/20 1:10 JLB P010844 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 9/19/20 1:10 JLB P010844 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 9/19/20 1:10 JLB P010844 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 9/19/20 1:10 JLB P010844 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 9/19/20 1:10 JLB P010844 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 9/19/20 1:10 JLB P010844 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 9/19/20 1:10 JLB P010844 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 9/19/20 1:10 JLB P010844 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 9/19/20 1:10 JLB P010844 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 9/19/20 1:10 JLB P010844 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 9/19/20 1:10 JLB P010844 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 9/19/20 1:10 JLB P010844 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 9/19/20 1:10 JLB P010844 Acetone BRL ug/L 5.0 0.31 1 8260D 9/19/20 1:10 JLB P010844 Acrolein BRL ug/L 20 0.20 1 8260D 9/19/20 1:10 JLB P010844 Acrylonitrile BRL ug/L 20 0.20 1 8260D 9/19/20 1:10 JLB P010844 Benzene BRL ug/L 0.50 0.048 1 8260D 9/19/20 1:10 JLB P010844 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 9/19/20 1:10 JLB P010844 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 9/19/20 1:10 JLB P010844 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 9/19/20 1:10 JLB P010844 Bromoform BRL ug/L 1.0 0.040 1 8260D 9/19/20 1:10 JLB P010844 Bromomethane BRL ug/L 1.0 0.18 1 8260D 9/19/20 1:10 JLB P010844 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 9/19/20 1:10 JLB P010844 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 9/19/20 1:10 JLB P010844 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 9/19/20 1:10 JLB P010844 Chloroethane BRL ug/L 0.50 0.22 1 8260D 9/19/20 1:10 JLB P010844 Chloroform BRL ug/L 0.50 0.076 1 8260D 9/19/20 1:10 JLB P010844 Chloromethane BRL ug/L 0.50 0.079 1 8260D 9/19/20 1:10 JLB P010844 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 9/19/20 1:10 JLB P010844 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 9/19/20 1:10 JLB P010844 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 9/19/20 1:10 JLB P010844 Dibromomethane BRL ug/L 0.50 0.065 1 8260D 9/19/20 1:10 JLB P010844 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 9/19/20 1:10 JLB P010844 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 9/19/20 1:10 JLB P010844 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 9/19/20 1:10 JLB P010844 Isopropyl Ether BRL ug/L 5.0 0.96 1 8260D 9/19/20 1:10 JLB P010844 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 9/19/20 1:10 JLB P010844 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 9/19/20 1:10 JLB P010844 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 9/19/20 1:10 JLB P010844 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260D 9/19/20 1:10 JLB P010844 Methyl Isobutyl Ketone BRL ug/L 5.0 1.0 1 8260D 9/19/20 1:10 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-1 W Attn: Tom Proctor Sample ID: 0090162-01 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methylene Chloride BRL ug/L 1.0 0.083 1 8260D 9/19/20 1:10 JLB P010844 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 9/19/20 1:10 JLB P010844 Naphthalene BRL ug/L 1.0 0.30 1 8260D 9/19/20 1:10 JLB P010844 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 9/19/20 1:10 JLB P010844 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 9/19/20 1:10 JLB P010844 o-Xylene BRL ug/L 0.50 0.044 1 8260D 9/19/20 1:10 JLB P010844 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 9/19/20 1:10 JLB P010844 Styrene BRL ug/L 0.50 0.047 1 8260D 9/19/20 1:10 JLB P010844 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 9/19/20 1:10 JLB P010844 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260D 9/19/20 1:10 JLB P010844 Toluene BRL ug/L 0.50 0.044 1 8260D 9/19/20 1:10 JLB P010844 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 9/19/20 1:10 JLB P010844 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 9/19/20 1:10 JLB P010844 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 9/19/20 1:10 JLB P010844 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 9/19/20 1:10 JLB P010844 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 9/19/20 1:10 JLB P010844 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 9/19/20 1:10 JLB P010844 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 9/19/20 1:10 JLB P010844 Surrogate Recovery Control Limits 4-Bromofluorobenzene 104 % 80-124 Dibromofluoromethane 104 % 75-129 Toluene-d8 97 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-2W Attn: Tom Proctor Sample ID: 0090162-02 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 14:30 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 3.0 1 8270E 9/17/20 17:35 JMV P010794 1,2-Dichlorobenzene BRL ug/L 10 2.4 1 8270E 9/17/20 17:35 JMV P010794 1,3-Dichlorobenzene BRL ug/L 10 3.9 1 8270E 9/17/20 17:35 JMV P010794 1,4-Dichlorobenzene BRL ug/L 10 4.1 1 8270E 9/17/20 17:35 JMV P010794 1-Methyl naphthalene BRL ug/L 10 1.1 1 8270E 9/17/20 17:35 JMV P010794 2,4,5-Trichlorophenol BRL ug/L 20 3.6 1 8270E 9/17/20 17:35 JMV P010794 2,4,6-Trichlorophenol BRL ug/L 20 4.5 1 8270E 9/17/20 17:35 JMV P010794 2,4-Dichlorophenol BRL ug/L 10 2.6 1 8270E 9/17/20 17:35 JMV P010794 2,4-Dimethylphenol BRL ug/L 10 4.9 1 8270E 9/17/20 17:35 JMV P010794 2,4-Dinitrophenol BRL ug/L 50 12 1 8270E 9/17/20 17:35 JMV P010794 2,4-Dinitrotoluene BRL ug/L 10 4.2 1 8270E 9/17/20 17:35 JMV P010794 2,6-Dinitrotoluene BRL ug/L 20 3.9 1 8270E 9/17/20 17:35 JMV P010794 2-Chloronaphthalene BRL ug/L 20 4.7 1 8270E 9/17/20 17:35 JMV P010794 2-Chlorophenol BRL ug/L 10 2.7 1 8270E 9/17/20 17:35 JMV P010794 2-Methyl naphthalene BRL ug/L 10 1.2 1 8270E 9/17/20 17:35 JMV P010794 2-Methylphenol BRL ug/L 10 2.4 1 8270E 9/17/20 17:35 JMV P010794 2-Nitroaniline BRL ug/L 10 4.1 1 8270E 9/17/20 17:35 JMV P010794 2-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 17:35 JMV P010794 3,3'-Dichlorobenzidine BRL ug/L 10 3.9 1 8270E 9/17/20 17:35 JMV P010794 3/4-Methyl phenol BRL ug/L 10 2.5 1 8270E 9/17/20 17:35 JMV P010794 3-Nitroaniline BRL ug/L 10 3.8 1 8270E 9/17/20 17:35 JMV P010794 4,6-Dinitro-2-methylphenol BRL ug/L 50 11 1 8270E 9/17/20 17:35 JMV P010794 4-Bromophenyl phenyl ether BRL ug/L 20 4.4 1 8270E 9/17/20 17:35 JMV P010794 4-Chloro-3-methylphenol BRL ug/L 10 2.9 1 8270E 9/17/20 17:35 JMV P010794 4-Chloroaniline BRL ug/L 10 3.5 1 8270E 9/17/20 17:35 JMV P010794 4-Chlorophenyl phenyl ether BRL ug/L 20 4.7 1 8270E 9/17/20 17:35 JMV P010794 4-Nitroaniline BRL ug/L 10 4.1 1 8270E 9/17/20 17:35 JMV P010794 4-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 17:35 JMV P010794 Acenaphthene BRL ug/L 10 0.76 1 8270E 9/17/20 17:35 JMV P010794 Acenaphthylene BRL ug/L 20 0.60 1 8270E 9/17/20 17:35 JMV P010794 Aniline BRL ug/L 50 12 1 8270E 9/17/20 17:35 JMV P010794 Anthracene BRL ug/L 10 0.47 1 8270E 9/17/20 17:35 JMV P010794 Azobenzene BRL ug/L 10 3.2 1 8270E 9/17/20 17:35 JMV P010794 Benzo(a)anthracene BRL ug/L 10 0.74 1 8270E 9/17/20 17:35 JMV P010794 Benzo(a)pyrene BRL ug/L 10 0.44 1 8270E 9/17/20 17:35 JMV P010794 Benzo(b)fluoranthene BRL ug/L 10 0.87 1 8270E 9/17/20 17:35 JMV P010794 Benzo(g,hJ)perylene BRL ug/L 10 0.98 1 8270E 9/17/20 17:35 JMV P010794 Benzo(k)fluoranthene BRL ug/L 10 0.81 1 8270E 9/17/20 17:35 JMV P010794 Benzoic Acid BRL ug/L 100 19 1 8270E 9/17/20 17:35 JMV P010794 Benzyl alcohol BRL ug/L 10 2.5 1 8270E 9/17/20 17:35 JMV P010794 bis(2-Chloroethoxy)methane BRL ug/L 10 3.8 1 8270E 9/17/20 17:35 JMV P010794 Bis(2-Chloroethyl)ether BRL ug/L 10 2.6 1 8270E 9/17/20 17:35 JMV P010794 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-2W Attn: Tom Proctor Sample ID: 0090162-02 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 14:30 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Bis(2-chloroisopropyl)ether BRL ug/L 10 2.8 1 8270E 9/17/20 17:35 JMV P010794 Bis(2-Ethylhexyl)phthaIate BRL ug/L 10 3.7 1 8270E 9/17/20 17:35 JMV P010794 Butyl benzyl phthalate BRL ug/L 10 2.9 1 8270E 9/17/20 17:35 JMV P010794 Chrysene BRL ug/L 10 0.98 1 8270E 9/17/20 17:35 JMV P010794 Dibenzo(a,h)anthracene BRL ug/L 20 1.6 1 8270E 9/17/20 17:35 JMV P010794 Dibenzofuran BRL ug/L 20 4.2 1 8270E 9/17/20 17:35 JMV P010794 Diethyl phthalate BRL ug/L 20 4.2 1 8270E 9/17/20 17:35 JMV P010794 Dimethyl phthalate BRL ug/L 10 4.1 1 8270E 9/17/20 17:35 JMV P010794 Di-n-butyl phthalate BRL ug/L 10 4.3 1 8270E 9/17/20 17:35 JMV P010794 Di-n-octyl phthalate BRL ug/L 10 4.5 1 8270E 9/17/20 17:35 JMV P010794 Fluoranthene BRL ug/L 10 0.57 1 8270E 9/17/20 17:35 JMV P010794 Fluorene BRL ug/L 10 0.46 1 8270E 9/17/20 17:35 JMV P010794 Hexachlorobenzene BRL ug/L 20 3.9 1 8270E 9/17/20 17:35 JMV P010794 Hexachlorobutadiene BRL ug/L 20 4.5 1 8270E 9/17/20 17:35 JMV P010794 Hexachlorocyclopentadiene BRL ug/L 20 7.3 1 8270E 9/17/20 17:35 JMV P010794 Hexachloroethane BRL ug/L 10 3.7 1 8270E 9/17/20 17:35 JMV P010794 Indeno(1,2,3-cd)pyrene BRL ug/L 10 0.75 1 8270E 9/17/20 17:35 JMV P010794 Isophorone BRL ug/L 10 4.1 1 8270E 9/17/20 17:35 JMV P010794 Naphthalene BRL ug/L 10 1.3 1 8270E 9/17/20 17:35 JMV P010794 Nitrobenzene BRL ug/L 10 3.8 1 8270E 9/17/20 17:35 JMV P010794 N-Nitroso-di-n-propylamine BRL ug/L 20 3.3 1 8270E 9/17/20 17:35 JMV P010794 N-Nitrosodiphenylamine BRL ug/L 20 4.4 1 8270E 9/17/20 17:35 JMV P010794 Pentachlorophenol BRL ug/L 50 11 1 8270E 9/17/20 17:35 JMV P010794 Phenanthrene BRL ug/L 10 0.40 1 8270E 9/17/20 17:35 JMV P010794 Phenol BRL ug/L 10 1.4 1 8270E 9/17/20 17:35 JMV P010794 Pyrene BRL ug/L 10 0.67 1 8270E 9/17/20 17:35 JMV P010794 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 76 % 43-140 2-Fluorobiphenyl 55 % 44-119 2-Fluorophenol 26 % 19-119 Nitrobenzene-d5 45 % 44-120 Phenol-d5 17 % 11-52 Terphenyl-d14 70 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 9/18/20 21:56 JLB P010844 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 9/18/20 21:56 JLB P010844 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 9/18/20 21:56 JLB P010844 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 21:56 JLB P010844 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 9/18/20 21:56 JLB P010844 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 9/18/20 21:56 JLB P010844 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 9/18/20 21:56 JLB P010844 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 9/18/20 21:56 JLB P010844 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 9/18/20 21:56 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-2W Attn: Tom Proctor Sample ID: 0090162-02 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 14:30 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 9/18/20 21:56 JLB P010844 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 21:56 JLB P010844 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 9/18/20 21:56 JLB P010844 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 9/18/20 21:56 JLB P010844 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 21:56 JLB P010844 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 21:56 JLB P010844 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 9/18/20 21:56 JLB P010844 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 21:56 JLB P010844 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 21:56 JLB P010844 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 9/18/20 21:56 JLB P010844 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 9/18/20 21:56 JLB P010844 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 9/18/20 21:56 JLB P010844 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 9/18/20 21:56 JLB P010844 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 9/18/20 21:56 JLB P010844 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 9/18/20 21:56 JLB P010844 Acetone BRL ug/L 5.0 0.31 1 8260D 9/18/20 21:56 JLB P010844 Acrolein BRL ug/L 20 0.20 1 8260D 9/18/20 21:56 JLB P010844 Acrylonitrile BRL ug/L 20 0.20 1 8260D 9/18/20 21:56 JLB P010844 Benzene BRL ug/L 0.50 0.048 1 8260D 9/18/20 21:56 JLB P010844 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 9/18/20 21:56 JLB P010844 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 9/18/20 21:56 JLB P010844 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 21:56 JLB P010844 Bromoform BRL ug/L 1.0 0.040 1 8260D 9/18/20 21:56 JLB P010844 Bromomethane BRL ug/L 1.0 0.18 1 8260D 9/18/20 21:56 JLB P010844 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 9/18/20 21:56 JLB P010844 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 9/18/20 21:56 JLB P010844 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 9/18/20 21:56 JLB P010844 Chloroethane BRL ug/L 0.50 0.22 1 8260D 9/18/20 21:56 JLB P010844 Chloroform BRL ug/L 0.50 0.076 1 8260D 9/18/20 21:56 JLB P010844 Chloromethane BRL ug/L 0.50 0.079 1 8260D 9/18/20 21:56 JLB P010844 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 9/18/20 21:56 JLB P010844 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 9/18/20 21:56 JLB P010844 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 9/18/20 21:56 JLB P010844 Dibromomethane BRL ug/L 0.50 0.065 1 8260D 9/18/20 21:56 JLB P010844 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 9/18/20 21:56 JLB P010844 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 9/18/20 21:56 JLB P010844 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 9/18/20 21:56 JLB P010844 Isopropyl Ether BRL ug/L 5.0 0.96 1 8260D 9/18/20 21:56 JLB P010844 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 9/18/20 21:56 JLB P010844 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 9/18/20 21:56 JLB P010844 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 9/18/20 21:56 JLB P010844 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260D 9/18/20 21:56 JLB P010844 Methyl Isobutyl Ketone BRL ug/L 5.0 1.0 1 8260D 9/18/20 21:56 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-2W Attn: Tom Proctor Sample ID: 0090162-02 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 14:30 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methylene Chloride BRL ug/L 1.0 0.083 1 8260D 9/18/20 21:56 JLB P010844 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 9/18/20 21:56 JLB P010844 Naphthalene BRL ug/L 1.0 0.30 1 8260D 9/18/20 21:56 JLB P010844 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 9/18/20 21:56 JLB P010844 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 9/18/20 21:56 JLB P010844 o-Xylene BRL ug/L 0.50 0.044 1 8260D 9/18/20 21:56 JLB P010844 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 21:56 JLB P010844 Styrene BRL ug/L 0.50 0.047 1 8260D 9/18/20 21:56 JLB P010844 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 9/18/20 21:56 JLB P010844 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260D 9/18/20 21:56 JLB P010844 Toluene BRL ug/L 0.50 0.044 1 8260D 9/18/20 21:56 JLB P010844 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 9/18/20 21:56 JLB P010844 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 9/18/20 21:56 JLB P010844 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 9/18/20 21:56 JLB P010844 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 21:56 JLB P010844 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 9/18/20 21:56 JLB P010844 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 9/18/20 21:56 JLB P010844 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 9/18/20 21:56 JLB P010844 Surrogate Recovery Control Limits 4-Bromofluorobenzene 104 % 80-124 Dibromofluoromethane 103 % 75-129 Toluene-d8 98 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-3W Attn: Tom Proctor Sample ID: 0090162-03 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 3.0 1 8270E 9/17/20 17:58 JMV P010794 1,2-Dichlorobenzene BRL ug/L 10 2.4 1 8270E 9/17/20 17:58 JMV P010794 1,3-Dichlorobenzene BRL ug/L 10 3.9 1 8270E 9/17/20 17:58 JMV P010794 1,4-Dichlorobenzene BRL ug/L 10 4.1 1 8270E 9/17/20 17:58 JMV P010794 1-Methyl naphthalene BRL ug/L 10 1.1 1 8270E 9/17/20 17:58 JMV P010794 2,4,5-Trichlorophenol BRL ug/L 20 3.6 1 8270E 9/17/20 17:58 JMV P010794 2,4,6-Trichlorophenol BRL ug/L 20 4.5 1 8270E 9/17/20 17:58 JMV P010794 2,4-Dichlorophenol BRL ug/L 10 2.6 1 8270E 9/17/20 17:58 JMV P010794 2,4-Dimethylphenol BRL ug/L 10 4.9 1 8270E 9/17/20 17:58 JMV P010794 2,4-Dinitrophenol BRL ug/L 50 12 1 8270E 9/17/20 17:58 JMV P010794 2,4-Dinitrotoluene BRL ug/L 10 4.2 1 8270E 9/17/20 17:58 JMV P010794 2,6-Dinitrotoluene BRL ug/L 20 3.9 1 8270E 9/17/20 17:58 JMV P010794 2-Chloronaphthalene BRL ug/L 20 4.7 1 8270E 9/17/20 17:58 JMV P010794 2-Chlorophenol BRL ug/L 10 2.7 1 8270E 9/17/20 17:58 JMV P010794 2-Methyl naphthalene BRL ug/L 10 1.2 1 8270E 9/17/20 17:58 JMV P010794 2-Methylphenol BRL ug/L 10 2.4 1 8270E 9/17/20 17:58 JMV P010794 2-Nitroaniline BRL ug/L 10 4.1 1 8270E 9/17/20 17:58 JMV P010794 2-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 17:58 JMV P010794 3,3'-Dichlorobenzidine BRL ug/L 10 3.9 1 8270E 9/17/20 17:58 JMV P010794 3/4-Methyl phenol BRL ug/L 10 2.5 1 8270E 9/17/20 17:58 JMV P010794 3-Nitroaniline BRL ug/L 10 3.8 1 8270E 9/17/20 17:58 JMV P010794 4,6-Dinitro-2-methylphenol BRL ug/L 50 11 1 8270E 9/17/20 17:58 JMV P010794 4-Bromophenyl phenyl ether BRL ug/L 20 4.4 1 8270E 9/17/20 17:58 JMV P010794 4-Chloro-3-methylphenol BRL ug/L 10 2.9 1 8270E 9/17/20 17:58 JMV P010794 4-Chloroaniline BRL ug/L 10 3.5 1 8270E 9/17/20 17:58 JMV P010794 4-Chlorophenyl phenyl ether BRL ug/L 20 4.7 1 8270E 9/17/20 17:58 JMV P010794 4-Nitroaniline BRL ug/L 10 4.1 1 8270E 9/17/20 17:58 JMV P010794 4-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 17:58 JMV P010794 Acenaphthene BRL ug/L 10 0.76 1 8270E 9/17/20 17:58 JMV P010794 Acenaphthylene BRL ug/L 20 0.60 1 8270E 9/17/20 17:58 JMV P010794 Aniline BRL ug/L 50 12 1 8270E 9/17/20 17:58 JMV P010794 Anthracene BRL ug/L 10 0.47 1 8270E 9/17/20 17:58 JMV P010794 Azobenzene BRL ug/L 10 3.2 1 8270E 9/17/20 17:58 JMV P010794 Benzo(a)anthracene BRL ug/L 10 0.74 1 8270E 9/17/20 17:58 JMV P010794 Benzo(a)pyrene BRL ug/L 10 0.44 1 8270E 9/17/20 17:58 JMV P010794 Benzo(b)fluoranthene BRL ug/L 10 0.87 1 8270E 9/17/20 17:58 JMV P010794 Benzo(g,hJ)perylene BRL ug/L 10 0.98 1 8270E 9/17/20 17:58 JMV P010794 Benzo(k)fluoranthene BRL ug/L 10 0.81 1 8270E 9/17/20 17:58 JMV P010794 Benzoic Acid BRL ug/L 100 19 1 8270E 9/17/20 17:58 JMV P010794 Benzyl alcohol BRL ug/L 10 2.5 1 8270E 9/17/20 17:58 JMV P010794 bis(2-Chloroethoxy)methane BRL ug/L 10 3.8 1 8270E 9/17/20 17:58 JMV P010794 Bis(2-Chloroethyl)ether BRL ug/L 10 2.6 1 8270E 9/17/20 17:58 JMV P010794 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-3W Attn: Tom Proctor Sample ID: 0090162-03 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Bis(2-chloroisopropyl)ether BRL ug/L 10 2.8 1 8270E 9/17/20 17:58 JMV P010794 Bis(2-Ethylhexyl)phthaIate BRL ug/L 10 3.7 1 8270E 9/17/20 17:58 JMV P010794 Butyl benzyl phthalate BRL ug/L 10 2.9 1 8270E 9/17/20 17:58 JMV P010794 Chrysene BRL ug/L 10 0.98 1 8270E 9/17/20 17:58 JMV P010794 Dibenzo(a,h)anthracene BRL ug/L 20 1.6 1 8270E 9/17/20 17:58 JMV P010794 Dibenzofuran BRL ug/L 20 4.2 1 8270E 9/17/20 17:58 JMV P010794 Diethyl phthalate BRL ug/L 20 4.2 1 8270E 9/17/20 17:58 JMV P010794 Dimethyl phthalate BRL ug/L 10 4.1 1 8270E 9/17/20 17:58 JMV P010794 Di-n-butyl phthalate BRL ug/L 10 4.3 1 8270E 9/17/20 17:58 JMV P010794 Di-n-octyl phthalate BRL ug/L 10 4.5 1 8270E 9/17/20 17:58 JMV P010794 Fluoranthene BRL ug/L 10 0.57 1 8270E 9/17/20 17:58 JMV P010794 Fluorene BRL ug/L 10 0.46 1 8270E 9/17/20 17:58 JMV P010794 Hexachlorobenzene BRL ug/L 20 3.9 1 8270E 9/17/20 17:58 JMV P010794 Hexachlorobutadiene BRL ug/L 20 4.5 1 8270E 9/17/20 17:58 JMV P010794 Hexachlorocyclopentadiene BRL ug/L 20 7.3 1 8270E 9/17/20 17:58 JMV P010794 Hexachloroethane BRL ug/L 10 3.7 1 8270E 9/17/20 17:58 JMV P010794 Indeno(1,2,3-cd)pyrene BRL ug/L 10 0.75 1 8270E 9/17/20 17:58 JMV P010794 Isophorone BRL ug/L 10 4.1 1 8270E 9/17/20 17:58 JMV P010794 Naphthalene BRL ug/L 10 1.3 1 8270E 9/17/20 17:58 JMV P010794 Nitrobenzene BRL ug/L 10 3.8 1 8270E 9/17/20 17:58 JMV P010794 N-Nitroso-di-n-propylamine BRL ug/L 20 3.3 1 8270E 9/17/20 17:58 JMV P010794 N-Nitrosodiphenylamine BRL ug/L 20 4.4 1 8270E 9/17/20 17:58 JMV P010794 Pentachlorophenol BRL ug/L 50 11 1 8270E 9/17/20 17:58 JMV P010794 Phenanthrene BRL ug/L 10 0.40 1 8270E 9/17/20 17:58 JMV P010794 Phenol BRL ug/L 10 1.4 1 8270E 9/17/20 17:58 JMV P010794 Pyrene BRL ug/L 10 0.67 1 8270E 9/17/20 17:58 JMV P010794 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 88 % 43-140 2-Fluorobiphenyl 61 % 44-119 2-Fluorophenol 33 % 19-119 Nitrobenzene-d5 53 % 44-120 Phenol-d5 22 % 11-52 Terphenyl-d14 77 % 50-134 Total Metals Mercury BRL mg/L 0.00020 0.000034 1 *7470A 9/18/20 15:30 EDV P010809 Arsenic BRL mg/L 0.020 0.0074 1 *601OD 9/18/20 19:59 JAB P010799 Barium 0.023 mg/L 0.010 0.0016 1 *6010D 9/18/20 19:59 JAB P010799 Cadmium BRL mg/L 0.0020 0.00040 1 *601OD 9/18/20 19:59 JAB P010799 Chromium BRL mg/L 0.010 0.0020 1 *601OD 9/18/20 19:59 JAB P010799 Lead BRL mg/L 0.0050 0.0025 1 *601OD 9/18/20 19:59 JAB P010799 Selenium BRL mg/L 0.030 0.010 1 *601OD 9/18/20 19:59 JAB P010799 Silver BRL mg/L 0.0050 0.00070 1 *601OD 9/18/20 19:59 JAB P010799 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-3W Attn: Tom Proctor Sample ID: 0090162-03 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 9/18/20 22:24 JLB P010844 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 9/18/20 22:24 JLB P010844 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 9/18/20 22:24 JLB P010844 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 22:24 JLB P010844 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 9/18/20 22:24 JLB P010844 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 9/18/20 22:24 JLB P010844 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 9/18/20 22:24 JLB P010844 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 9/18/20 22:24 JLB P010844 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 9/18/20 22:24 JLB P010844 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 9/18/20 22:24 JLB P010844 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 22:24 JLB P010844 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 9/18/20 22:24 JLB P010844 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 9/18/20 22:24 JLB P010844 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 22:24 JLB P010844 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 22:24 JLB P010844 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 9/18/20 22:24 JLB P010844 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 22:24 JLB P010844 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 22:24 JLB P010844 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 9/18/20 22:24 JLB P010844 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 9/18/20 22:24 JLB P010844 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 9/18/20 22:24 JLB P010844 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 9/18/20 22:24 JLB P010844 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 9/18/20 22:24 JLB P010844 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 9/18/20 22:24 JLB P010844 Acetone BRL ug/L 5.0 0.31 1 8260D 9/18/20 22:24 JLB P010844 Acrolein BRL ug/L 20 0.20 1 8260D 9/18/20 22:24 JLB P010844 Acrylonitrile BRL ug/L 20 0.20 1 8260D 9/18/20 22:24 JLB P010844 Benzene BRL ug/L 0.50 0.048 1 8260D 9/18/20 22:24 JLB P010844 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 9/18/20 22:24 JLB P010844 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 9/18/20 22:24 JLB P010844 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 22:24 JLB P010844 Bromoform BRL ug/L 1.0 0.040 1 8260D 9/18/20 22:24 JLB P010844 Bromomethane BRL ug/L 1.0 0.18 1 8260D 9/18/20 22:24 JLB P010844 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 9/18/20 22:24 JLB P010844 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 9/18/20 22:24 JLB P010844 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 9/18/20 22:24 JLB P010844 Chloroethane BRL ug/L 0.50 0.22 1 8260D 9/18/20 22:24 JLB P010844 Chloroform BRL ug/L 0.50 0.076 1 8260D 9/18/20 22:24 JLB P010844 Chloromethane 0.34 J ug/L 0.50 0.079 1 8260D 9/18/20 22:24 JLB P010844 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 9/18/20 22:24 JLB P010844 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 9/18/20 22:24 JLB P010844 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 9/18/20 22:24 JLB P010844 Dibromomethane BRL ug/L 0.50 0.065 1 8260D 9/18/20 22:24 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-3W Attn: Tom Proctor Sample ID: 0090162-03 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 9/18/20 22:24 JLB P010844 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 9/18/20 22:24 JLB P010844 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 9/18/20 22:24 JLB P010844 Isopropyl Ether BRL ug/L 5.0 0.96 1 8260D 9/18/20 22:24 JLB P010844 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 9/18/20 22:24 JLB P010844 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 9/18/20 22:24 JLB P010844 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 9/18/20 22:24 JLB P010844 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260D 9/18/20 22:24 JLB P010844 Methyl Isobutyl Ketone BRL ug/L 5.0 1.0 1 8260D 9/18/20 22:24 JLB P010844 Methylene Chloride BRL ug/L 1.0 0.083 1 8260D 9/18/20 22:24 JLB P010844 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 9/18/20 22:24 JLB P010844 Naphthalene BRL ug/L 1.0 0.30 1 8260D 9/18/20 22:24 JLB P010844 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 9/18/20 22:24 JLB P010844 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 9/18/20 22:24 JLB P010844 o-Xylene BRL ug/L 0.50 0.044 1 8260D 9/18/20 22:24 JLB P010844 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 22:24 JLB P010844 Styrene BRL ug/L 0.50 0.047 1 8260D 9/18/20 22:24 JLB P010844 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 9/18/20 22:24 JLB P010844 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260D 9/18/20 22:24 JLB P010844 Toluene BRL ug/L 0.50 0.044 1 8260D 9/18/20 22:24 JLB P010844 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 9/18/20 22:24 JLB P010844 trans- 1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 9/18/20 22:24 JLB P010844 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 9/18/20 22:24 JLB P010844 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 22:24 JLB P010844 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 9/18/20 22:24 JLB P010844 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 9/18/20 22:24 JLB P010844 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 9/18/20 22:24 JLB P010844 Surrogate Recovery Control Limits 4-Bromofluorobenzene 104 % 80-124 Dibromofluoromethane 103 % 75-129 Toluene-d8 98 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-4W Attn: Tom Proctor Sample ID: 0090162-04 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:50 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 3.0 1 8270E 9/17/20 18:21 JMV P010794 1,2-Dichlorobenzene BRL ug/L 10 2.5 1 8270E 9/17/20 18:21 JMV P010794 1,3-Dichlorobenzene BRL ug/L 10 4.0 1 8270E 9/17/20 18:21 JMV P010794 1,4-Dichlorobenzene BRL ug/L 10 4.2 1 8270E 9/17/20 18:21 JMV P010794 1-Methyl naphthalene BRL ug/L 10 1.1 1 8270E 9/17/20 18:21 JMV P010794 2,4,5-Trichlorophenol BRL ug/L 21 3.7 1 8270E 9/17/20 18:21 JMV P010794 2,4,6-Trichlorophenol BRL ug/L 21 4.7 1 8270E 9/17/20 18:21 JMV P010794 2,4-Dichlorophenol BRL ug/L 10 2.7 1 8270E 9/17/20 18:21 JMV P010794 2,4-Dimethylphenol BRL ug/L 10 5.0 1 8270E 9/17/20 18:21 JMV P010794 2,4-Dinitrophenol BRL ug/L 52 12 1 8270E 9/17/20 18:21 JMV P010794 2,4-Dinitrotoluene BRL ug/L 10 4.3 1 8270E 9/17/20 18:21 JMV P010794 2,6-Dinitrotoluene BRL ug/L 21 4.0 1 8270E 9/17/20 18:21 JMV P010794 2-Chloronaphthalene BRL ug/L 21 4.8 1 8270E 9/17/20 18:21 JMV P010794 2-Chlorophenol BRL ug/L 10 2.8 1 8270E 9/17/20 18:21 JMV P010794 2-Methyl naphthalene BRL ug/L 10 1.2 1 8270E 9/17/20 18:21 JMV P010794 2-Methylphenol BRL ug/L 10 2.5 1 8270E 9/17/20 18:21 JMV P010794 2-Nitroaniline BRL ug/L 10 4.2 1 8270E 9/17/20 18:21 JMV P010794 2-Nitrophenol BRL ug/L 10 2.7 1 8270E 9/17/20 18:21 JMV P010794 3,3'-Dichlorobenzidine BRL ug/L 10 4.0 1 8270E 9/17/20 18:21 JMV P010794 3/4-Methyl phenol BRL ug/L 10 2.5 1 8270E 9/17/20 18:21 JMV P010794 3-Nitroaniline BRL ug/L 10 3.9 1 8270E 9/17/20 18:21 JMV P010794 4,6-Dinitro-2-methylphenol BRL ug/L 52 12 1 8270E 9/17/20 18:21 JMV P010794 4-Bromophenyl phenyl ether BRL ug/L 21 4.5 1 8270E 9/17/20 18:21 JMV P010794 4-Chloro-3-methylphenol BRL ug/L 10 3.0 1 8270E 9/17/20 18:21 JMV P010794 4-Chloroaniline BRL ug/L 10 3.6 1 8270E 9/17/20 18:21 JMV P010794 4-Chlorophenyl phenyl ether BRL ug/L 21 4.8 1 8270E 9/17/20 18:21 JMV P010794 4-Nitroaniline BRL ug/L 10 4.3 1 8270E 9/17/20 18:21 JMV P010794 4-Nitrophenol BRL ug/L 10 2.7 1 8270E 9/17/20 18:21 JMV P010794 Acenaphthene BRL ug/L 10 0.79 1 8270E 9/17/20 18:21 JMV P010794 Acenaphthylene BRL ug/L 21 0.61 1 8270E 9/17/20 18:21 JMV P010794 Aniline BRL ug/L 52 12 1 8270E 9/17/20 18:21 JMV P010794 Anthracene BRL ug/L 10 0.49 1 8270E 9/17/20 18:21 JMV P010794 Azobenzene BRL ug/L 10 3.3 1 8270E 9/17/20 18:21 JMV P010794 Benzo(a)anthracene BRL ug/L 10 0.77 1 8270E 9/17/20 18:21 JMV P010794 Benzo(a)pyrene BRL ug/L 10 0.46 1 8270E 9/17/20 18:21 JMV P010794 Benzo(b)fluoranthene BRL ug/L 10 0.90 1 8270E 9/17/20 18:21 JMV P010794 Benzo(g,hJ)perylene BRL ug/L 10 1.0 1 8270E 9/17/20 18:21 JMV P010794 Benzo(k)fluoranthene BRL ug/L 10 0.84 1 8270E 9/17/20 18:21 JMV P010794 Benzoic Acid BRL ug/L 100 20 1 8270E 9/17/20 18:21 JMV P010794 Benzyl alcohol BRL ug/L 10 2.6 1 8270E 9/17/20 18:21 JMV P010794 bis(2-Chloroethoxy)methane BRL ug/L 10 3.9 1 8270E 9/17/20 18:21 JMV P010794 Bis(2-Chloroethyl)ether BRL ug/L 10 2.7 1 8270E 9/17/20 18:21 JMV P010794 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-4W Attn: Tom Proctor Sample ID: 0090162-04 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:50 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Bis(2-chloroisopropyl)ether BRL ug/L 10 2.9 1 8270E 9/17/20 18:21 JMV P010794 Bis(2-Ethylhexyl)phthaIate BRL ug/L 10 3.8 1 8270E 9/17/20 18:21 JMV P010794 Butyl benzyl phthalate BRL ug/L 10 3.0 1 8270E 9/17/20 18:21 JMV P010794 Chrysene BRL ug/L 10 1.0 1 8270E 9/17/20 18:21 JMV P010794 Dibenzo(a,h)anthracene BRL ug/L 21 1.6 1 8270E 9/17/20 18:21 JMV P010794 Dibenzofuran BRL ug/L 21 4.3 1 8270E 9/17/20 18:21 JMV P010794 Diethyl phthalate BRL ug/L 21 4.3 1 8270E 9/17/20 18:21 JMV P010794 Dimethyl phthalate BRL ug/L 10 4.2 1 8270E 9/17/20 18:21 JMV P010794 Di-n-butyl phthalate BRL ug/L 10 4.5 1 8270E 9/17/20 18:21 JMV P010794 Di-n-octyl phthalate BRL ug/L 10 4.6 1 8270E 9/17/20 18:21 JMV P010794 Fluoranthene BRL ug/L 10 0.59 1 8270E 9/17/20 18:21 JMV P010794 Fluorene BRL ug/L 10 0.47 1 8270E 9/17/20 18:21 JMV P010794 Hexachlorobenzene BRL ug/L 21 4.0 1 8270E 9/17/20 18:21 JMV P010794 Hexachlorobutadiene BRL ug/L 21 4.6 1 8270E 9/17/20 18:21 JMV P010794 Hexachlorocyclopentadiene BRL ug/L 21 7.5 1 8270E 9/17/20 18:21 JMV P010794 Hexachloroethane BRL ug/L 10 3.8 1 8270E 9/17/20 18:21 JMV P010794 Indeno(1,2,3-cd)pyrene BRL ug/L 10 0.77 1 8270E 9/17/20 18:21 JMV P010794 Isophorone BRL ug/L 10 4.2 1 8270E 9/17/20 18:21 JMV P010794 Naphthalene BRL ug/L 10 1.3 1 8270E 9/17/20 18:21 JMV P010794 Nitrobenzene BRL ug/L 10 4.0 1 8270E 9/17/20 18:21 JMV P010794 N-Nitroso-di-n-propylamine BRL ug/L 21 3.4 1 8270E 9/17/20 18:21 JMV P010794 N-Nitrosodiphenylamine BRL ug/L 21 4.6 1 8270E 9/17/20 18:21 JMV P010794 Pentachlorophenol BRL ug/L 52 11 1 8270E 9/17/20 18:21 JMV P010794 Phenanthrene BRL ug/L 10 0.42 1 8270E 9/17/20 18:21 JMV P010794 Phenol BRL ug/L 10 1.4 1 8270E 9/17/20 18:21 JMV P010794 Pyrene BRL ug/L 10 0.69 1 8270E 9/17/20 18:21 JMV P010794 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 92 % 43-140 2-Fluorobiphenyl 60 % 44-119 2-Fluorophenol 31 % 19-119 Nitrobenzene-d5 49 % 44-120 Phenol-d5 22 % 11-52 Terphenyl-d14 78 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 9/18/20 22:52 JLB P010844 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 9/18/20 22:52 JLB P010844 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 9/18/20 22:52 JLB P010844 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 22:52 JLB P010844 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 9/18/20 22:52 JLB P010844 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 9/18/20 22:52 JLB P010844 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 9/18/20 22:52 JLB P010844 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 9/18/20 22:52 JLB P010844 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 9/18/20 22:52 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-4W Attn: Tom Proctor Sample ID: 0090162-04 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:50 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 9/18/20 22:52 JLB P010844 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 22:52 JLB P010844 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 9/18/20 22:52 JLB P010844 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 9/18/20 22:52 JLB P010844 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 22:52 JLB P010844 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 22:52 JLB P010844 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 9/18/20 22:52 JLB P010844 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 22:52 JLB P010844 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 22:52 JLB P010844 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 9/18/20 22:52 JLB P010844 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 9/18/20 22:52 JLB P010844 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 9/18/20 22:52 JLB P010844 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 9/18/20 22:52 JLB P010844 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 9/18/20 22:52 JLB P010844 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 9/18/20 22:52 JLB P010844 Acetone BRL ug/L 5.0 0.31 1 8260D 9/18/20 22:52 JLB P010844 Acrolein BRL ug/L 20 0.20 1 8260D 9/18/20 22:52 JLB P010844 Acrylonitrile BRL ug/L 20 0.20 1 8260D 9/18/20 22:52 JLB P010844 Benzene BRL ug/L 0.50 0.048 1 8260D 9/18/20 22:52 JLB P010844 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 9/18/20 22:52 JLB P010844 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 9/18/20 22:52 JLB P010844 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 22:52 JLB P010844 Bromoform BRL ug/L 1.0 0.040 1 8260D 9/18/20 22:52 JLB P010844 Bromomethane BRL ug/L 1.0 0.18 1 8260D 9/18/20 22:52 JLB P010844 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 9/18/20 22:52 JLB P010844 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 9/18/20 22:52 JLB P010844 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 9/18/20 22:52 JLB P010844 Chloroethane BRL ug/L 0.50 0.22 1 8260D 9/18/20 22:52 JLB P010844 Chloroform BRL ug/L 0.50 0.076 1 8260D 9/18/20 22:52 JLB P010844 Chloromethane BRL ug/L 0.50 0.079 1 8260D 9/18/20 22:52 JLB P010844 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 9/18/20 22:52 JLB P010844 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 9/18/20 22:52 JLB P010844 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 9/18/20 22:52 JLB P010844 Dibromomethane BRL ug/L 0.50 0.065 1 8260D 9/18/20 22:52 JLB P010844 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 9/18/20 22:52 JLB P010844 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 9/18/20 22:52 JLB P010844 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 9/18/20 22:52 JLB P010844 Isopropyl Ether BRL ug/L 5.0 0.96 1 8260D 9/18/20 22:52 JLB P010844 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 9/18/20 22:52 JLB P010844 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 9/18/20 22:52 JLB P010844 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 9/18/20 22:52 JLB P010844 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260D 9/18/20 22:52 JLB P010844 Methyl Isobutyl Ketone BRL ug/L 5.0 1.0 1 8260D 9/18/20 22:52 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 0f 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-4W Attn: Tom Proctor Sample ID: 0090162-04 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 13:50 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methylene Chloride 0.67 J ug/L 1.0 0.083 1 8260D 9/18/20 22:52 JLB P010844 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 9/18/20 22:52 JLB P010844 Naphthalene BRL ug/L 1.0 0.30 1 8260D 9/18/20 22:52 JLB P010844 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 9/18/20 22:52 JLB P010844 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 9/18/20 22:52 JLB P010844 o-Xylene BRL ug/L 0.50 0.044 1 8260D 9/18/20 22:52 JLB P010844 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 22:52 JLB P010844 Styrene BRL ug/L 0.50 0.047 1 8260D 9/18/20 22:52 JLB P010844 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 9/18/20 22:52 JLB P010844 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260D 9/18/20 22:52 JLB P010844 Toluene BRL ug/L 0.50 0.044 1 8260D 9/18/20 22:52 JLB P010844 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 9/18/20 22:52 JLB P010844 trans- 1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 9/18/20 22:52 JLB P010844 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 9/18/20 22:52 JLB P010844 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 22:52 JLB P010844 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 9/18/20 22:52 JLB P010844 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 9/18/20 22:52 JLB P010844 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 9/18/20 22:52 JLB P010844 Surrogate Recovery Control Limits 4-Bromofluorobenzene 106 % 80-124 Dibromofluoromethane 104 % 75-129 Toluene-d8 97 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-5W Attn: Tom Proctor Sample ID: 0090162-05 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 14:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 3.0 1 8270E 9/17/20 19:51 JMV P010794 1,2-Dichlorobenzene BRL ug/L 10 2.5 1 8270E 9/17/20 19:51 JMV P010794 1,3-Dichlorobenzene BRL ug/L 10 3.9 1 8270E 9/17/20 19:51 JMV P010794 1,4-Dichlorobenzene BRL ug/L 10 4.2 1 8270E 9/17/20 19:51 JMV P010794 1-Methyl naphthalene BRL ug/L 10 1.1 1 8270E 9/17/20 19:51 JMV P010794 2,4,5-Trichlorophenol BRL ug/L 20 3.7 1 8270E 9/17/20 19:51 JMV P010794 2,4,6-Trichlorophenol BRL ug/L 20 4.6 1 8270E 9/17/20 19:51 JMV P010794 2,4-Dichlorophenol BRL ug/L 10 2.7 1 8270E 9/17/20 19:51 JMV P010794 2,4-Dimethylphenol BRL ug/L 10 4.9 1 8270E 9/17/20 19:51 JMV P010794 2,4-Dinitrophenol BRL ug/L 51 12 1 8270E 9/17/20 19:51 JMV P010794 2,4-Dinitrotoluene BRL ug/L 10 4.2 1 8270E 9/17/20 19:51 JMV P010794 2,6-Dinitrotoluene BRL ug/L 20 4.0 1 8270E 9/17/20 19:51 JMV P010794 2-Chloronaphthalene BRL ug/L 20 4.7 1 8270E 9/17/20 19:51 JMV P010794 2-Chlorophenol BRL ug/L 10 2.7 1 8270E 9/17/20 19:51 JMV P010794 2-Methyl naphthalene BRL ug/L 10 1.2 1 8270E 9/17/20 19:51 JMV P010794 2-Methylphenol BRL ug/L 10 2.5 1 8270E 9/17/20 19:51 JMV P010794 2-Nitroaniline BRL ug/L 10 4.1 1 8270E 9/17/20 19:51 JMV P010794 2-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 19:51 JMV P010794 3,3'-Dichlorobenzidine BRL ug/L 10 4.0 1 8270E 9/17/20 19:51 JMV P010794 3/4-Methyl phenol BRL ug/L 10 2.5 1 8270E 9/17/20 19:51 JMV P010794 3-Nitroaniline BRL ug/L 10 3.8 1 8270E 9/17/20 19:51 JMV P010794 4,6-Dinitro-2-methylphenol BRL ug/L 51 11 1 8270E 9/17/20 19:51 JMV P010794 4-Bromophenyl phenyl ether BRL ug/L 20 4.4 1 8270E 9/17/20 19:51 JMV P010794 4-Chloro-3-methylphenol BRL ug/L 10 3.0 1 8270E 9/17/20 19:51 JMV P010794 4-Chloroaniline BRL ug/L 10 3.5 1 8270E 9/17/20 19:51 JMV P010794 4-Chlorophenyl phenyl ether BRL ug/L 20 4.7 1 8270E 9/17/20 19:51 JMV P010794 4-Nitroaniline BRL ug/L 10 4.2 1 8270E 9/17/20 19:51 JMV P010794 4-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 19:51 JMV P010794 Acenaphthene BRL ug/L 10 0.77 1 8270E 9/17/20 19:51 JMV P010794 Acenaphthylene BRL ug/L 20 0.60 1 8270E 9/17/20 19:51 JMV P010794 Aniline BRL ug/L 51 12 1 8270E 9/17/20 19:51 JMV P010794 Anthracene BRL ug/L 10 0.48 1 8270E 9/17/20 19:51 JMV P010794 Azobenzene BRL ug/L 10 3.2 1 8270E 9/17/20 19:51 JMV P010794 Benzo(a)anthracene BRL ug/L 10 0.75 1 8270E 9/17/20 19:51 JMV P010794 Benzo(a)pyrene BRL ug/L 10 0.45 1 8270E 9/17/20 19:51 JMV P010794 Benzo(b)fluoranthene BRL ug/L 10 0.88 1 8270E 9/17/20 19:51 JMV P010794 Benzo(g,hJ)perylene BRL ug/L 10 0.99 1 8270E 9/17/20 19:51 JMV P010794 Benzo(k)fluoranthene BRL ug/L 10 0.82 1 8270E 9/17/20 19:51 JMV P010794 Benzoic Acid BRL ug/L 100 19 1 8270E 9/17/20 19:51 JMV P010794 Benzyl alcohol BRL ug/L 10 2.5 1 8270E 9/17/20 19:51 JMV P010794 bis(2-Chloroethoxy)methane BRL ug/L 10 3.8 1 8270E 9/17/20 19:51 JMV P010794 Bis(2-Chloroethyl)ether BRL ug/L 10 2.6 1 8270E 9/17/20 19:51 JMV P010794 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-5W Attn: Tom Proctor Sample ID: 0090162-05 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 14:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Bis(2-chloroisopropyl)ether BRL ug/L 10 2.8 1 8270E 9/17/20 19:51 JMV P010794 Bis(2-Ethylhexyl)phthaIate BRL ug/L 10 3.8 1 8270E 9/17/20 19:51 JMV P010794 Butyl benzyl phthalate BRL ug/L 10 3.0 1 8270E 9/17/20 19:51 JMV P010794 Chrysene BRL ug/L 10 0.99 1 8270E 9/17/20 19:51 JMV P010794 Dibenzo(a,h)anthracene BRL ug/L 20 1.6 1 8270E 9/17/20 19:51 JMV P010794 Dibenzofuran BRL ug/L 20 4.2 1 8270E 9/17/20 19:51 JMV P010794 Diethyl phthalate BRL ug/L 20 4.2 1 8270E 9/17/20 19:51 JMV P010794 Dimethyl phthalate BRL ug/L 10 4.1 1 8270E 9/17/20 19:51 JMV P010794 Di-n-butyl phthalate BRL ug/L 10 4.4 1 8270E 9/17/20 19:51 JMV P010794 Di-n-octyl phthalate BRL ug/L 10 4.6 1 8270E 9/17/20 19:51 JMV P010794 Fluoranthene BRL ug/L 10 0.57 1 8270E 9/17/20 19:51 JMV P010794 Fluorene BRL ug/L 10 0.46 1 8270E 9/17/20 19:51 JMV P010794 Hexachlorobenzene BRL ug/L 20 3.9 1 8270E 9/17/20 19:51 JMV P010794 Hexachlorobutadiene BRL ug/L 20 4.5 1 8270E 9/17/20 19:51 JMV P010794 Hexachlorocyclopentadiene BRL ug/L 20 7.3 1 8270E 9/17/20 19:51 JMV P010794 Hexachloroethane BRL ug/L 10 3.8 1 8270E 9/17/20 19:51 JMV P010794 Indeno(1,2,3-cd)pyrene BRL ug/L 10 0.76 1 8270E 9/17/20 19:51 JMV P010794 Isophorone BRL ug/L 10 4.1 1 8270E 9/17/20 19:51 JMV P010794 Naphthalene BRL ug/L 10 1.3 1 8270E 9/17/20 19:51 JMV P010794 Nitrobenzene BRL ug/L 10 3.9 1 8270E 9/17/20 19:51 JMV P010794 N-Nitroso-di-n-propylamine BRL ug/L 20 3.3 1 8270E 9/17/20 19:51 JMV P010794 N-Nitrosodiphenylamine BRL ug/L 20 4.5 1 8270E 9/17/20 19:51 JMV P010794 Pentachlorophenol BRL ug/L 51 11 1 8270E 9/17/20 19:51 JMV P010794 Phenanthrene BRL ug/L 10 0.41 1 8270E 9/17/20 19:51 JMV P010794 Phenol BRL ug/L 10 1.4 1 8270E 9/17/20 19:51 JMV P010794 Pyrene BRL ug/L 10 0.68 1 8270E 9/17/20 19:51 JMV P010794 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 119 % 43-140 2-Fluorobiphenyl 76 % 44-119 2-Fluorophenol 43 % 19-119 Nitrobenzene-d5 65 % 44-120 Phenol-d5 32 % 11-52 Terphenyl-d14 93 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 9/18/20 23:19 JLB P010844 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 9/18/20 23:19 JLB P010844 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 9/18/20 23:19 JLB P010844 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 23:19 JLB P010844 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 9/18/20 23:19 JLB P010844 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 9/18/20 23:19 JLB P010844 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 9/18/20 23:19 JLB P010844 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 9/18/20 23:19 JLB P010844 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 9/18/20 23:19 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-5W Attn: Tom Proctor Sample ID: 0090162-05 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 14:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 9/18/20 23:19 JLB P010844 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 23:19 JLB P010844 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 9/18/20 23:19 JLB P010844 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 9/18/20 23:19 JLB P010844 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 23:19 JLB P010844 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 23:19 JLB P010844 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 9/18/20 23:19 JLB P010844 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 23:19 JLB P010844 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 23:19 JLB P010844 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 9/18/20 23:19 JLB P010844 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 9/18/20 23:19 JLB P010844 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 9/18/20 23:19 JLB P010844 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 9/18/20 23:19 JLB P010844 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 9/18/20 23:19 JLB P010844 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 9/18/20 23:19 JLB P010844 Acetone BRL ug/L 5.0 0.31 1 8260D 9/18/20 23:19 JLB P010844 Acrolein BRL ug/L 20 0.20 1 8260D 9/18/20 23:19 JLB P010844 Acrylonitrile BRL ug/L 20 0.20 1 8260D 9/18/20 23:19 JLB P010844 Benzene BRL ug/L 0.50 0.048 1 8260D 9/18/20 23:19 JLB P010844 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 9/18/20 23:19 JLB P010844 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 9/18/20 23:19 JLB P010844 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 23:19 JLB P010844 Bromoform BRL ug/L 1.0 0.040 1 8260D 9/18/20 23:19 JLB P010844 Bromomethane BRL ug/L 1.0 0.18 1 8260D 9/18/20 23:19 JLB P010844 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 9/18/20 23:19 JLB P010844 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 9/18/20 23:19 JLB P010844 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 9/18/20 23:19 JLB P010844 Chloroethane BRL ug/L 0.50 0.22 1 8260D 9/18/20 23:19 JLB P010844 Chloroform BRL ug/L 0.50 0.076 1 8260D 9/18/20 23:19 JLB P010844 Chloromethane 0.37 J ug/L 0.50 0.079 1 8260D 9/18/20 23:19 JLB P010844 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 9/18/20 23:19 JLB P010844 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 9/18/20 23:19 JLB P010844 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 9/18/20 23:19 JLB P010844 Dibromomethane BRL ug/L 0.50 0.065 1 8260D 9/18/20 23:19 JLB P010844 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 9/18/20 23:19 JLB P010844 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 9/18/20 23:19 JLB P010844 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 9/18/20 23:19 JLB P010844 Isopropyl Ether BRL ug/L 5.0 0.96 1 8260D 9/18/20 23:19 JLB P010844 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 9/18/20 23:19 JLB P010844 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 9/18/20 23:19 JLB P010844 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 9/18/20 23:19 JLB P010844 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260D 9/18/20 23:19 JLB P010844 Methyl Isobutyl Ketone BRL ug/L 5.0 1.0 1 8260D 9/18/20 23:19 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 0f 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-5W Attn: Tom Proctor Sample ID: 0090162-05 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 14:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methylene Chloride BRL ug/L 1.0 0.083 1 8260D 9/18/20 23:19 JLB P010844 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 9/18/20 23:19 JLB P010844 Naphthalene BRL ug/L 1.0 0.30 1 8260D 9/18/20 23:19 JLB P010844 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 9/18/20 23:19 JLB P010844 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 9/18/20 23:19 JLB P010844 o-Xylene BRL ug/L 0.50 0.044 1 8260D 9/18/20 23:19 JLB P010844 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 23:19 JLB P010844 Styrene BRL ug/L 0.50 0.047 1 8260D 9/18/20 23:19 JLB P010844 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 9/18/20 23:19 JLB P010844 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260D 9/18/20 23:19 JLB P010844 Toluene BRL ug/L 0.50 0.044 1 8260D 9/18/20 23:19 JLB P010844 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 9/18/20 23:19 JLB P010844 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 9/18/20 23:19 JLB P010844 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 9/18/20 23:19 JLB P010844 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 23:19 JLB P010844 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 9/18/20 23:19 JLB P010844 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 9/18/20 23:19 JLB P010844 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 9/18/20 23:19 JLB P010844 Surrogate Recovery Control Limits 4-Bromofluorobenzene 100 % 80-124 Dibromofluoromethane 104 % 75-129 Toluene-d8 97 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-6W Attn: Tom Proctor Sample ID: 0090162-06 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 16:10 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 3.0 1 8270E 9/17/20 20:14 JMV P010794 1,2-Dichlorobenzene BRL ug/L 10 2.5 1 8270E 9/17/20 20:14 JMV P010794 1,3-Dichlorobenzene BRL ug/L 10 3.9 1 8270E 9/17/20 20:14 JMV P010794 1,4-Dichlorobenzene BRL ug/L 10 4.2 1 8270E 9/17/20 20:14 JMV P010794 1-Methyl naphthalene BRL ug/L 10 1.1 1 8270E 9/17/20 20:14 JMV P010794 2,4,5-Trichlorophenol BRL ug/L 20 3.7 1 8270E 9/17/20 20:14 JMV P010794 2,4,6-Trichlorophenol BRL ug/L 20 4.6 1 8270E 9/17/20 20:14 JMV P010794 2,4-Dichlorophenol BRL ug/L 10 2.7 1 8270E 9/17/20 20:14 JMV P010794 2,4-Dimethylphenol BRL ug/L 10 4.9 1 8270E 9/17/20 20:14 JMV P010794 2,4-Dinitrophenol BRL ug/L 51 12 1 8270E 9/17/20 20:14 JMV P010794 2,4-Dinitrotoluene BRL ug/L 10 4.2 1 8270E 9/17/20 20:14 JMV P010794 2,6-Dinitrotoluene BRL ug/L 20 4.0 1 8270E 9/17/20 20:14 JMV P010794 2-Chloronaphthalene BRL ug/L 20 4.7 1 8270E 9/17/20 20:14 JMV P010794 2-Chlorophenol BRL ug/L 10 2.7 1 8270E 9/17/20 20:14 JMV P010794 2-Methyl naphthalene BRL ug/L 10 1.2 1 8270E 9/17/20 20:14 JMV P010794 2-Methylphenol BRL ug/L 10 2.5 1 8270E 9/17/20 20:14 JMV P010794 2-Nitroaniline BRL ug/L 10 4.1 1 8270E 9/17/20 20:14 JMV P010794 2-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 20:14 JMV P010794 3,3'-Dichlorobenzidine BRL ug/L 10 4.0 1 8270E 9/17/20 20:14 JMV P010794 3/4-Methyl phenol BRL ug/L 10 2.5 1 8270E 9/17/20 20:14 JMV P010794 3-Nitroaniline BRL ug/L 10 3.8 1 8270E 9/17/20 20:14 JMV P010794 4,6-Dinitro-2-methylphenol BRL ug/L 51 11 1 8270E 9/17/20 20:14 JMV P010794 4-Bromophenyl phenyl ether BRL ug/L 20 4.4 1 8270E 9/17/20 20:14 JMV P010794 4-Chloro-3-methylphenol BRL ug/L 10 3.0 1 8270E 9/17/20 20:14 JMV P010794 4-Chloroaniline BRL ug/L 10 3.5 1 8270E 9/17/20 20:14 JMV P010794 4-Chlorophenyl phenyl ether BRL ug/L 20 4.7 1 8270E 9/17/20 20:14 JMV P010794 4-Nitroaniline BRL ug/L 10 4.2 1 8270E 9/17/20 20:14 JMV P010794 4-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 20:14 JMV P010794 Acenaphthene BRL ug/L 10 0.77 1 8270E 9/17/20 20:14 JMV P010794 Acenaphthylene BRL ug/L 20 0.60 1 8270E 9/17/20 20:14 JMV P010794 Aniline BRL ug/L 51 12 1 8270E 9/17/20 20:14 JMV P010794 Anthracene BRL ug/L 10 0.48 1 8270E 9/17/20 20:14 JMV P010794 Azobenzene BRL ug/L 10 3.2 1 8270E 9/17/20 20:14 JMV P010794 Benzo(a)anthracene BRL ug/L 10 0.75 1 8270E 9/17/20 20:14 JMV P010794 Benzo(a)pyrene BRL ug/L 10 0.45 1 8270E 9/17/20 20:14 JMV P010794 Benzo(b)fluoranthene BRL ug/L 10 0.88 1 8270E 9/17/20 20:14 JMV P010794 Benzo(g,hJ)perylene BRL ug/L 10 0.99 1 8270E 9/17/20 20:14 JMV P010794 Benzo(k)fluoranthene BRL ug/L 10 0.82 1 8270E 9/17/20 20:14 JMV P010794 Benzoic Acid BRL ug/L 100 19 1 8270E 9/17/20 20:14 JMV P010794 Benzyl alcohol BRL ug/L 10 2.5 1 8270E 9/17/20 20:14 JMV P010794 bis(2-Chloroethoxy)methane BRL ug/L 10 3.8 1 8270E 9/17/20 20:14 JMV P010794 Bis(2-Chloroethyl)ether BRL ug/L 10 2.6 1 8270E 9/17/20 20:14 JMV P010794 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-6W Attn: Tom Proctor Sample ID: 0090162-06 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 16:10 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Bis(2-chloroisopropyl)ether BRL ug/L 10 2.8 1 8270E 9/17/20 20:14 JMV P010794 Bis(2-Ethylhexyl)phthaIate BRL ug/L 10 3.8 1 8270E 9/17/20 20:14 JMV P010794 Butyl benzyl phthalate BRL ug/L 10 3.0 1 8270E 9/17/20 20:14 JMV P010794 Chrysene BRL ug/L 10 0.99 1 8270E 9/17/20 20:14 JMV P010794 Dibenzo(a,h)anthracene BRL ug/L 20 1.6 1 8270E 9/17/20 20:14 JMV P010794 Dibenzofuran BRL ug/L 20 4.2 1 8270E 9/17/20 20:14 JMV P010794 Diethyl phthalate BRL ug/L 20 4.2 1 8270E 9/17/20 20:14 JMV P010794 Dimethyl phthalate BRL ug/L 10 4.1 1 8270E 9/17/20 20:14 JMV P010794 Di-n-butyl phthalate BRL ug/L 10 4.4 1 8270E 9/17/20 20:14 JMV P010794 Di-n-octyl phthalate BRL ug/L 10 4.6 1 8270E 9/17/20 20:14 JMV P010794 Fluoranthene BRL ug/L 10 0.57 1 8270E 9/17/20 20:14 JMV P010794 Fluorene BRL ug/L 10 0.46 1 8270E 9/17/20 20:14 JMV P010794 Hexachlorobenzene BRL ug/L 20 3.9 1 8270E 9/17/20 20:14 JMV P010794 Hexachlorobutadiene BRL ug/L 20 4.5 1 8270E 9/17/20 20:14 JMV P010794 Hexachlorocyclopentadiene BRL ug/L 20 7.3 1 8270E 9/17/20 20:14 JMV P010794 Hexachloroethane BRL ug/L 10 3.8 1 8270E 9/17/20 20:14 JMV P010794 Indeno(1,2,3-cd)pyrene BRL ug/L 10 0.76 1 8270E 9/17/20 20:14 JMV P010794 Isophorone BRL ug/L 10 4.1 1 8270E 9/17/20 20:14 JMV P010794 Naphthalene BRL ug/L 10 1.3 1 8270E 9/17/20 20:14 JMV P010794 Nitrobenzene BRL ug/L 10 3.9 1 8270E 9/17/20 20:14 JMV P010794 N-Nitroso-di-n-propylamine BRL ug/L 20 3.3 1 8270E 9/17/20 20:14 JMV P010794 N-Nitrosodiphenylamine BRL ug/L 20 4.5 1 8270E 9/17/20 20:14 JMV P010794 Pentachlorophenol BRL ug/L 51 11 1 8270E 9/17/20 20:14 JMV P010794 Phenanthrene BRL ug/L 10 0.41 1 8270E 9/17/20 20:14 JMV P010794 Phenol BRL ug/L 10 1.4 1 8270E 9/17/20 20:14 JMV P010794 Pyrene BRL ug/L 10 0.68 1 8270E 9/17/20 20:14 JMV P010794 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 115 % 43-140 2-Fluorobiphenyl 77 % 44-119 2-Fluorophenol 38 % 19-119 Nitrobenzene-d5 64 % 44-120 Phenol-d5 27 % 11-52 Terphenyl-d14 94 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 9/18/20 23:47 JLB P010844 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 9/18/20 23:47 JLB P010844 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 9/18/20 23:47 JLB P010844 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 23:47 JLB P010844 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 9/18/20 23:47 JLB P010844 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 9/18/20 23:47 JLB P010844 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 9/18/20 23:47 JLB P010844 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 9/18/20 23:47 JLB P010844 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 9/18/20 23:47 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-6W Attn: Tom Proctor Sample ID: 0090162-06 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 16:10 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 9/18/20 23:47 JLB P010844 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 23:47 JLB P010844 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 9/18/20 23:47 JLB P010844 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 9/18/20 23:47 JLB P010844 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 23:47 JLB P010844 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 23:47 JLB P010844 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 9/18/20 23:47 JLB P010844 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 23:47 JLB P010844 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 23:47 JLB P010844 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 9/18/20 23:47 JLB P010844 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 9/18/20 23:47 JLB P010844 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 9/18/20 23:47 JLB P010844 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 9/18/20 23:47 JLB P010844 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 9/18/20 23:47 JLB P010844 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 9/18/20 23:47 JLB P010844 Acetone BRL ug/L 5.0 0.31 1 8260D 9/18/20 23:47 JLB P010844 Acrolein BRL ug/L 20 0.20 1 8260D 9/18/20 23:47 JLB P010844 Acrylonitrile BRL ug/L 20 0.20 1 8260D 9/18/20 23:47 JLB P010844 Benzene BRL ug/L 0.50 0.048 1 8260D 9/18/20 23:47 JLB P010844 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 9/18/20 23:47 JLB P010844 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 9/18/20 23:47 JLB P010844 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 23:47 JLB P010844 Bromoform BRL ug/L 1.0 0.040 1 8260D 9/18/20 23:47 JLB P010844 Bromomethane BRL ug/L 1.0 0.18 1 8260D 9/18/20 23:47 JLB P010844 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 9/18/20 23:47 JLB P010844 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 9/18/20 23:47 JLB P010844 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 9/18/20 23:47 JLB P010844 Chloroethane BRL ug/L 0.50 0.22 1 8260D 9/18/20 23:47 JLB P010844 Chloroform BRL ug/L 0.50 0.076 1 8260D 9/18/20 23:47 JLB P010844 Chloromethane BRL ug/L 0.50 0.079 1 8260D 9/18/20 23:47 JLB P010844 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 9/18/20 23:47 JLB P010844 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 9/18/20 23:47 JLB P010844 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 9/18/20 23:47 JLB P010844 Dibromomethane BRL ug/L 0.50 0.065 1 8260D 9/18/20 23:47 JLB P010844 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 9/18/20 23:47 JLB P010844 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 9/18/20 23:47 JLB P010844 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 9/18/20 23:47 JLB P010844 Isopropyl Ether BRL ug/L 5.0 0.96 1 8260D 9/18/20 23:47 JLB P010844 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 9/18/20 23:47 JLB P010844 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 9/18/20 23:47 JLB P010844 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 9/18/20 23:47 JLB P010844 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260D 9/18/20 23:47 JLB P010844 Methyl Isobutyl Ketone BRL ug/L 5.0 1.0 1 8260D 9/18/20 23:47 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 0f 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-6W Attn: Tom Proctor Sample ID: 0090162-06 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 16:10 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methylene Chloride BRL ug/L 1.0 0.083 1 8260D 9/18/20 23:47 JLB P010844 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 9/18/20 23:47 JLB P010844 Naphthalene BRL ug/L 1.0 0.30 1 8260D 9/18/20 23:47 JLB P010844 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 9/18/20 23:47 JLB P010844 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 9/18/20 23:47 JLB P010844 o-Xylene BRL ug/L 0.50 0.044 1 8260D 9/18/20 23:47 JLB P010844 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 23:47 JLB P010844 Styrene BRL ug/L 0.50 0.047 1 8260D 9/18/20 23:47 JLB P010844 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 9/18/20 23:47 JLB P010844 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260D 9/18/20 23:47 JLB P010844 Toluene BRL ug/L 0.50 0.044 1 8260D 9/18/20 23:47 JLB P010844 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 9/18/20 23:47 JLB P010844 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 9/18/20 23:47 JLB P010844 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 9/18/20 23:47 JLB P010844 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 23:47 JLB P010844 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 9/18/20 23:47 JLB P010844 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 9/18/20 23:47 JLB P010844 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 9/18/20 23:47 JLB P010844 Surrogate Recovery Control Limits 4-Bromofluorobenzene 103 % 80-124 Dibromofluoromethane 102 % 75-129 Toluene-d8 97 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-7W Attn: Tom Proctor Sample ID: 0090162-07 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 17:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 3.0 1 8270E 9/17/20 20:36 JMV P010794 1,2-Dichlorobenzene BRL ug/L 10 2.5 1 8270E 9/17/20 20:36 JMV P010794 1,3-Dichlorobenzene BRL ug/L 10 3.9 1 8270E 9/17/20 20:36 JMV P010794 1,4-Dichlorobenzene BRL ug/L 10 4.2 1 8270E 9/17/20 20:36 JMV P010794 1-Methyl naphthalene BRL ug/L 10 1.1 1 8270E 9/17/20 20:36 JMV P010794 2,4,5-Trichlorophenol BRL ug/L 20 3.7 1 8270E 9/17/20 20:36 JMV P010794 2,4,6-Trichlorophenol BRL ug/L 20 4.6 1 8270E 9/17/20 20:36 JMV P010794 2,4-Dichlorophenol BRL ug/L 10 2.7 1 8270E 9/17/20 20:36 JMV P010794 2,4-Dimethylphenol BRL ug/L 10 4.9 1 8270E 9/17/20 20:36 JMV P010794 2,4-Dinitrophenol BRL ug/L 51 12 1 8270E 9/17/20 20:36 JMV P010794 2,4-Dinitrotoluene BRL ug/L 10 4.2 1 8270E 9/17/20 20:36 JMV P010794 2,6-Dinitrotoluene BRL ug/L 20 4.0 1 8270E 9/17/20 20:36 JMV P010794 2-Chloronaphthalene BRL ug/L 20 4.7 1 8270E 9/17/20 20:36 JMV P010794 2-Chlorophenol BRL ug/L 10 2.7 1 8270E 9/17/20 20:36 JMV P010794 2-Methyl naphthalene BRL ug/L 10 1.2 1 8270E 9/17/20 20:36 JMV P010794 2-Methylphenol BRL ug/L 10 2.5 1 8270E 9/17/20 20:36 JMV P010794 2-Nitroaniline BRL ug/L 10 4.1 1 8270E 9/17/20 20:36 JMV P010794 2-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 20:36 JMV P010794 3,3'-Dichlorobenzidine BRL ug/L 10 4.0 1 8270E 9/17/20 20:36 JMV P010794 3/4-Methyl phenol BRL ug/L 10 2.5 1 8270E 9/17/20 20:36 JMV P010794 3-Nitroaniline BRL ug/L 10 3.8 1 8270E 9/17/20 20:36 JMV P010794 4,6-Dinitro-2-methylphenol BRL ug/L 51 11 1 8270E 9/17/20 20:36 JMV P010794 4-Bromophenyl phenyl ether BRL ug/L 20 4.4 1 8270E 9/17/20 20:36 JMV P010794 4-Chloro-3-methylphenol BRL ug/L 10 3.0 1 8270E 9/17/20 20:36 JMV P010794 4-Chloroaniline BRL ug/L 10 3.5 1 8270E 9/17/20 20:36 JMV P010794 4-Chlorophenyl phenyl ether BRL ug/L 20 4.7 1 8270E 9/17/20 20:36 JMV P010794 4-Nitroaniline BRL ug/L 10 4.2 1 8270E 9/17/20 20:36 JMV P010794 4-Nitrophenol BRL ug/L 10 2.6 1 8270E 9/17/20 20:36 JMV P010794 Acenaphthene BRL ug/L 10 0.77 1 8270E 9/17/20 20:36 JMV P010794 Acenaphthylene BRL ug/L 20 0.60 1 8270E 9/17/20 20:36 JMV P010794 Aniline BRL ug/L 51 12 1 8270E 9/17/20 20:36 JMV P010794 Anthracene BRL ug/L 10 0.48 1 8270E 9/17/20 20:36 JMV P010794 Azobenzene BRL ug/L 10 3.2 1 8270E 9/17/20 20:36 JMV P010794 Benzo(a)anthracene BRL ug/L 10 0.75 1 8270E 9/17/20 20:36 JMV P010794 Benzo(a)pyrene BRL ug/L 10 0.45 1 8270E 9/17/20 20:36 JMV P010794 Benzo(b)fluoranthene BRL ug/L 10 0.88 1 8270E 9/17/20 20:36 JMV P010794 Benzo(g,hJ)perylene BRL ug/L 10 0.99 1 8270E 9/17/20 20:36 JMV P010794 Benzo(k)fluoranthene BRL ug/L 10 0.82 1 8270E 9/17/20 20:36 JMV P010794 Benzoic Acid BRL ug/L 100 19 1 8270E 9/17/20 20:36 JMV P010794 Benzyl alcohol BRL ug/L 10 2.5 1 8270E 9/17/20 20:36 JMV P010794 bis(2-Chloroethoxy)methane BRL ug/L 10 3.8 1 8270E 9/17/20 20:36 JMV P010794 Bis(2-Chloroethyl)ether BRL ug/L 10 2.6 1 8270E 9/17/20 20:36 JMV P010794 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-7W Attn: Tom Proctor Sample ID: 0090162-07 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 17:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Bis(2-chloroisopropyl)ether BRL ug/L 10 2.8 1 8270E 9/17/20 20:36 JMV P010794 Bis(2-Ethylhexyl)phthaIate BRL ug/L 10 3.8 1 8270E 9/17/20 20:36 JMV P010794 Butyl benzyl phthalate BRL ug/L 10 3.0 1 8270E 9/17/20 20:36 JMV P010794 Chrysene BRL ug/L 10 0.99 1 8270E 9/17/20 20:36 JMV P010794 Dibenzo(a,h)anthracene BRL ug/L 20 1.6 1 8270E 9/17/20 20:36 JMV P010794 Dibenzofuran BRL ug/L 20 4.2 1 8270E 9/17/20 20:36 JMV P010794 Diethyl phthalate BRL ug/L 20 4.2 1 8270E 9/17/20 20:36 JMV P010794 Dimethyl phthalate BRL ug/L 10 4.1 1 8270E 9/17/20 20:36 JMV P010794 Di-n-butyl phthalate BRL ug/L 10 4.4 1 8270E 9/17/20 20:36 JMV P010794 Di-n-octyl phthalate BRL ug/L 10 4.6 1 8270E 9/17/20 20:36 JMV P010794 Fluoranthene BRL ug/L 10 0.57 1 8270E 9/17/20 20:36 JMV P010794 Fluorene BRL ug/L 10 0.46 1 8270E 9/17/20 20:36 JMV P010794 Hexachlorobenzene BRL ug/L 20 3.9 1 8270E 9/17/20 20:36 JMV P010794 Hexachlorobutadiene BRL ug/L 20 4.5 1 8270E 9/17/20 20:36 JMV P010794 Hexachlorocyclopentadiene BRL ug/L 20 7.3 1 8270E 9/17/20 20:36 JMV P010794 Hexachloroethane BRL ug/L 10 3.8 1 8270E 9/17/20 20:36 JMV P010794 Indeno(1,2,3-cd)pyrene BRL ug/L 10 0.76 1 8270E 9/17/20 20:36 JMV P010794 Isophorone BRL ug/L 10 4.1 1 8270E 9/17/20 20:36 JMV P010794 Naphthalene BRL ug/L 10 1.3 1 8270E 9/17/20 20:36 JMV P010794 Nitrobenzene BRL ug/L 10 3.9 1 8270E 9/17/20 20:36 JMV P010794 N-Nitroso-di-n-propylamine BRL ug/L 20 3.3 1 8270E 9/17/20 20:36 JMV P010794 N-Nitrosodiphenylamine BRL ug/L 20 4.5 1 8270E 9/17/20 20:36 JMV P010794 Pentachlorophenol BRL ug/L 51 11 1 8270E 9/17/20 20:36 JMV P010794 Phenanthrene BRL ug/L 10 0.41 1 8270E 9/17/20 20:36 JMV P010794 Phenol BRL ug/L 10 1.4 1 8270E 9/17/20 20:36 JMV P010794 Pyrene BRL ug/L 10 0.68 1 8270E 9/17/20 20:36 JMV P010794 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 109 % 43-140 2-Fluorobiphenyl 70 % 44-119 2-Fluorophenol 38 % 19-119 Nitrobenzene-d5 57 % 44-120 Phenol-d5 29 % 11-52 Terphenyl-d14 88 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 9/19/20 0:15 JLB P010844 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 9/19/20 0:15 JLB P010844 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 9/19/20 0:15 JLB P010844 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 9/19/20 0:15 JLB P010844 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 9/19/20 0:15 JLB P010844 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 9/19/20 0:15 JLB P010844 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 9/19/20 0:15 JLB P010844 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 9/19/20 0:15 JLB P010844 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 9/19/20 0:15 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-7W Attn: Tom Proctor Sample ID: 0090162-07 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 17:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 9/19/20 0:15 JLB P010844 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 9/19/20 0:15 JLB P010844 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 9/19/20 0:15 JLB P010844 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 9/19/20 0:15 JLB P010844 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 9/19/20 0:15 JLB P010844 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 9/19/20 0:15 JLB P010844 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 9/19/20 0:15 JLB P010844 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 9/19/20 0:15 JLB P010844 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 9/19/20 0:15 JLB P010844 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 9/19/20 0:15 JLB P010844 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 9/19/20 0:15 JLB P010844 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 9/19/20 0:15 JLB P010844 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 9/19/20 0:15 JLB P010844 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 9/19/20 0:15 JLB P010844 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 9/19/20 0:15 JLB P010844 Acetone BRL ug/L 5.0 0.31 1 8260D 9/19/20 0:15 JLB P010844 Acrolein BRL ug/L 20 0.20 1 8260D 9/19/20 0:15 JLB P010844 Acrylonitrile BRL ug/L 20 0.20 1 8260D 9/19/20 0:15 JLB P010844 Benzene BRL ug/L 0.50 0.048 1 8260D 9/19/20 0:15 JLB P010844 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 9/19/20 0:15 JLB P010844 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 9/19/20 0:15 JLB P010844 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 9/19/20 0:15 JLB P010844 Bromoform BRL ug/L 1.0 0.040 1 8260D 9/19/20 0:15 JLB P010844 Bromomethane BRL ug/L 1.0 0.18 1 8260D 9/19/20 0:15 JLB P010844 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 9/19/20 0:15 JLB P010844 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 9/19/20 0:15 JLB P010844 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 9/19/20 0:15 JLB P010844 Chloroethane BRL ug/L 0.50 0.22 1 8260D 9/19/20 0:15 JLB P010844 Chloroform 0.23 J ug/L 0.50 0.076 1 8260D 9119/20 0:15 JLB P010844 Chloromethane BRL ug/L 0.50 0.079 1 8260D 9/19/20 0:15 JLB P010844 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 9/19/20 0:15 JLB P010844 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 9/19/20 0:15 JLB P010844 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 9/19/20 0:15 JLB P010844 Dibromomethane BRL ug/L 0.50 0.065 1 8260D 9/19/20 0:15 JLB P010844 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 9/19/20 0:15 JLB P010844 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 9/19/20 0:15 JLB P010844 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 9/19/20 0:15 JLB P010844 Isopropyl Ether BRL ug/L 5.0 0.96 1 8260D 9/19/20 0:15 JLB P010844 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 9/19/20 0:15 JLB P010844 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 9/19/20 0:15 JLB P010844 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 9/19/20 0:15 JLB P010844 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260D 9/19/20 0:15 JLB P010844 Methyl Isobutyl Ketone BRL ug/L 5.0 1.0 1 8260D 9/19/20 0:15 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 0f 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-7W Attn: Tom Proctor Sample ID: 0090162-07 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 17:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methylene Chloride BRL ug/L 1.0 0.083 1 8260D 9/19/20 0:15 JLB P010844 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 9/19/20 0:15 JLB P010844 Naphthalene BRL ug/L 1.0 0.30 1 8260D 9/19/20 0:15 JLB P010844 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 9/19/20 0:15 JLB P010844 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 9/19/20 0:15 JLB P010844 o-Xylene BRL ug/L 0.50 0.044 1 8260D 9/19/20 0:15 JLB P010844 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 9/19/20 0:15 JLB P010844 Styrene BRL ug/L 0.50 0.047 1 8260D 9/19/20 0:15 JLB P010844 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 9/19/20 0:15 JLB P010844 Tetrachloroethylene 0.27 J ug/L 0.50 0.098 1 8260D 9/19/20 0:15 JLB P010844 Toluene BRL ug/L 0.50 0.044 1 8260D 9/19/20 0:15 JLB P010844 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 9/19/20 0:15 JLB P010844 trans- 1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 9/19/20 0:15 JLB P010844 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 9/19/20 0:15 JLB P010844 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 9/19/20 0:15 JLB P010844 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 9/19/20 0:15 JLB P010844 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 9/19/20 0:15 JLB P010844 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 9/19/20 0:15 JLB P010844 Surrogate Recovery Control Limits 4-Bromofluorobenzene 104 % 80-124 Dibromofluoromethane 104 % 75-129 Toluene-d8 98 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 of 93 Laboratory Report • � 10/13/2020 PA Waynt. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-2S Attn: Tom Proctor Sample ID: 0090162-08 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 14:30 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 88.2 % by 0.100 0.100 1 *SM2540 G 9/17/20 13:00 EDV P010783 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.75 0.13 1 8270E 9/16/20 18:47 JMV P010771 1,2-Dichlorobenzene BRL mg/kg dry 0.75 0.12 1 8270E 9/16/20 18:47 JMV P010771 1,3-Dichlorobenzene BRL mg/kg dry 0.75 0.11 1 8270E 9/16/20 18:47 JMV P010771 1,4-Dichlorobenzene BRL mg/kg dry 0.37 0.12 1 8270E 9/16/20 18:47 JMV P010771 1-Methyl naphthalene BRL mg/kg dry 0.75 0.011 1 8270E 9/16/20 18:47 JMV P010771 2,4,5-Trichlorophenol BRL mg/kg dry 0.75 0.16 1 8270E 9/16/20 18:47 JMV P010771 2,4,6-Trichlorophenol BRL mg/kg dry 0.75 0.18 1 8270E 9/16/20 18:47 JMV P010771 2,4-Dichlorophenol BRL mg/kg dry 0.75 0.15 1 8270E 9/16/20 18:47 JMV P010771 2,4-Dimethylphenol BRL mg/kg dry 0.37 0.16 1 8270E 9/16/20 18:47 JMV P010771 2,4-Dinitrophenol BRL mg/kg dry 1.7 0.44 1 8270E 9/16/20 18:47 JMV P010771 2,4-Dinitrotoluene BRL mg/kg dry 0.75 0.20 1 8270E 9/16/20 18:47 JMV P010771 2,6-Dinitrotoluene BRL mg/kg dry 0.75 0.19 1 8270E 9/16/20 18:47 JMV P010771 2-Chloronaphthalene BRL mg/kg dry 0.75 0.18 1 8270E 9/16/20 18:47 JMV P010771 2-Chlorophenol BRL mg/kg dry 0.75 0.14 1 8270E 9/16/20 18:47 JMV P010771 2-Methyl naphthalene BRL mg/kg dry 0.75 0.015 1 8270E 9/16/20 18:47 JMV P010771 2-Methylphenol BRL mg/kg dry 0.75 0.14 1 8270E 9/16/20 18:47 JMV P010771 2-Nitrophenol BRL mg/kg dry 0.75 0.12 1 8270E 9/16/20 18:47 JMV P010771 3,3'-Dichlorobenzidine BRL mg/kg dry 0.75 0.15 1 8270E 9/16/20 18:47 JMV P010771 3/4-Methyl phenol BRL mg/kg dry 0.75 0.16 1 8270E 9/16/20 18:47 JMV P010771 4,6-Dinitro-2-methylphenol BRL mg/kg dry 1.7 0.41 1 8270E 9/16/20 18:47 JMV P010771 4-Bromophenyl phenyl ether BRL mg/kg dry 0.75 0.18 1 8270E 9/16/20 18:47 JMV P010771 4-Chloro-3-methylphenol BRL mg/kg dry 0.75 0.14 1 8270E 9/16/20 18:47 JMV P010771 4-Chloroaniline BRL mg/kg dry 0.37 0.091 1 8270E 9/16/20 18:47 JMV P010771 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.1 0.23 1 8270E 9/16/20 18:47 JMV P010771 4-Nitrophenol BRL mg/kg dry 0.75 0.18 1 8270E 9/16/20 18:47 JMV P010771 Acenaphthene BRL mg/kg dry 0.75 0.017 1 8270E 9/16/20 18:47 JMV P010771 Acenaphthylene BRL mg/kg dry 0.75 0.015 1 8270E 9/16/20 18:47 JMV P010771 Anthracene BRL mg/kg dry 0.75 0.0083 1 8270E 9/16/20 18:47 JMV P010771 Azobenzene BRL mg/kg dry 0.75 0.16 1 8270E 9/16/20 18:47 JMV P010771 Benzo(a)anthracene BRL mg/kg dry 0.75 0.0089 1 8270E 9/16/20 18:47 JMV P010771 Benzo(a)pyrene BRL mg/kg dry 0.75 0.0067 1 8270E 9/16/20 18:47 JMV P010771 Benzo(b)fluoranthene BRL mg/kg dry 0.75 0.0069 1 8270E 9/16/20 18:47 JMV P010771 Benzo(g,h,i)perylene BRL mg/kg dry 0.75 0.0074 1 8270E 9/16/20 18:47 JMV P010771 Benzo(k)fluoranthene BRL mg/kg dry 0.75 0.0079 1 8270E 9/16/20 18:47 JMV P010771 Benzoic Acid BRL mg/kg dry 2.3 0.62 1 8270E 9/16/20 18:47 JMV P010771 Benzyl alcohol BRL mg/kg dry 0.75 0.14 1 8270E 9/16/20 18:47 JMV P010771 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.75 0.14 1 8270E 9/16/20 18:47 JMV P010771 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.75 0.12 1 8270E 9/16/20 18:47 JMV P010771 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.37 0.13 1 8270E 9/16/20 18:47 JMV P010771 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 32 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-2S Attn: Tom Proctor Sample ID: 0090162-08 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 14:30 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Bis(2-Ethylhexyl)phthaIate BRL mg/kg dry 0.75 0.17 1 8270E 9/16/20 18:47 JMV P010771 Butyl benzyl phthalate BRL mg/kg dry 0.37 0.13 1 8270E 9/16/20 18:47 JMV P010771 Chrysene BRL mg/kg dry 0.75 0.0088 1 8270E 9/16/20 18:47 JMV P010771 Dibenzo(a,h)anthracene BRL mg/kg dry 0.75 0.022 1 8270E 9/16/20 18:47 JMV P010771 Dibenzofuran BRL mg/kg dry 0.75 0.20 1 8270E 9/16/20 18:47 JMV P010771 Diethyl phthalate BRL mg/kg dry 0.75 0.19 1 8270E 9/16/20 18:47 JMV P010771 Dimethyl phthalate BRL mg/kg dry 0.75 0.18 1 8270E 9/16/20 18:47 JMV P010771 Di-n-butyl phthalate BRL mg/kg dry 0.75 0.19 1 8270E 9/16/20 18:47 JMV P010771 Di-n-octyl phthalate BRL mg/kg dry 0.37 0.19 1 8270E 9/16/20 18:47 JMV P010771 Fluoranthene BRL mg/kg dry 0.75 0.0085 1 8270E 9/16/20 18:47 JMV P010771 Fluorene BRL mg/kg dry 0.75 0.013 1 8270E 9/16/20 18:47 JMV P010771 Hexachlorobenzene BRL mg/kg dry 0.75 0.16 1 8270E 9/16/20 18:47 JMV P010771 Hexachlorobutadiene BRL mg/kg dry 0.75 0.17 1 8270E 9/16/20 18:47 JMV P010771 Hexachlorocyclopentadiene BRL mg/kg dry 0.75 0.26 1 8270E 9/16/20 18:47 JMV P010771 Hexachloroethane BRL mg/kg dry 0.75 0.12 1 8270E 9/16/20 18:47 JMV P010771 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.75 0.021 1 8270E 9/16/20 18:47 JMV P010771 Isophorone BRL mg/kg dry 0.75 0.16 1 8270E 9/16/20 18:47 JMV P010771 Naphthalene BRL mg/kg dry 0.75 0.016 1 8270E 9/16/20 18:47 JMV P010771 Nitrobenzene BRL mg/kg dry 0.37 0.16 1 8270E 9/16/20 18:47 JMV P010771 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.75 0.17 1 8270E 9/16/20 18:47 JMV P010771 N-Nitrosodiphenylamine BRL mg/kg dry 0.75 0.21 1 8270E 9/16/20 18:47 JMV P010771 Pentachlorophenol BRL mg/kg dry 1.1 0.48 1 8270E 9/16/20 18:47 JMV P010771 Phenanthrene BRL mg/kg dry 0.75 0.0082 1 8270E 9/16/20 18:47 JMV P010771 Phenol BRL mg/kg dry 0.75 0.12 1 8270E 9/16/20 18:47 JMV P010771 Pyrene BRL mg/kg dry 0.75 0.011 1 8270E 9/16/20 18:47 JMV P010771 Pyridine BRL mg/kg dry 0.37 0.071 1 8270E 9/16/20 18:47 JMV P010771 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 96 % 39-132 2-Fluorobiphenyl 76 % 44-115 2-Fluorophenol 72 % 35-115 Nitrobenzene-d5 63 % 37-122 Phenol-d5 71 % 34-121 Terphenyl-d14 76 % 54-127 Total Metals Hexavalent Chromium BRL mg/kg dry 0.45 0.17 1 7196A 10/13/20 13:15 BMS PQJ0158 Mercury BRL mg/kg dry 0.057 0.017 1 *7471B 9/21/20 13:33 EDV P010869 Arsenic BRL mg/kg dry 1.1 0.14 1 *601OD 9/17/20 22:34 JAB P010770 Barium BRL mg/kg dry 11 1.0 1 *601OD 9/17/20 22:34 JAB P010770 Cadmium BRL mg/kg dry 0.57 0.053 1 *601OD 9/17/20 22:34 JAB P010770 Chromium 1.7 mg/kg dry 1.1 0.16 1 *6010D 9/17/20 22:34 JAB P010770 Lead 3.8 mg/kg dry 1.1 0.14 1 *60101) 9/17/20 22:34 JAB P010770 Selenium BRL mg/kg dry 1.1 0.20 1 *601OD 9/18/20 21:20 JAB P010770 Silver BRL mg/kg dry 0.57 0.054 1 *601OD 9/17/20 22:34 JAB P010770 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-2S Attn: Tom Proctor Sample ID: 0090162-08 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 14:30 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0051 0.00062 1 8260D 9/16/20 15:52 TBL P010790 1,1,1-Trichloroethane BRL mg/kg dry 0.0051 0.00075 1 8260D 9/16/20 15:52 TBL P010790 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0051 0.00037 1 8260D 9/16/20 15:52 TBL P010790 1,1,2-Trichloroethane BRL mg/kg dry 0.0051 0.00055 1 8260D 9/16/20 15:52 TBL P010790 1,1-Dichloroethane BRL mg/kg dry 0.0051 0.00092 1 8260D 9/16/20 15:52 TBL P010790 1,1-Dichloroethylene BRL mg/kg dry 0.0051 0.00094 1 8260D 9/16/20 15:52 TBL P010790 1,1-Dichloropropylene BRL mg/kg dry 0.0051 0.00079 1 8260D 9/16/20 15:52 TBL P010790 1,2,3-Trichlorobenzene BRL mg/kg dry 0.010 0.00073 1 8260D 9/16/20 15:52 TBL P010790 1,2,3-Trichloropropane BRL mg/kg dry 0.0051 0.00058 1 8260D 9/16/20 15:52 TBL P010790 1,2,4-Trichlorobenzene BRL mg/kg dry 0.010 0.00049 1 8260D 9/16/20 15:52 TBL P010790 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0051 0.00054 1 8260D 9/16/20 15:52 TBL P010790 1,2-Dibromoethane BRL mg/kg dry 0.0051 0.00046 1 8260D 9/16/20 15:52 TBL P010790 1,2-Dichlorobenzene BRL mg/kg dry 0.0051 0.00057 1 8260D 9/16/20 15:52 TBL P010790 1,2-Dichloroethane BRL mg/kg dry 0.0051 0.00061 1 8260D 9/16/20 15:52 TBL P010790 1,2-Dichloropropane BRL mg/kg dry 0.0051 0.00077 1 8260D 9/16/20 15:52 TBL P010790 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0051 0.00064 1 8260D 9/16/20 15:52 TBL P010790 1,3-Dichlorobenzene BRL mg/kg dry 0.0051 0.00064 1 8260D 9/16/20 15:52 TBL P010790 1,3-Dichloropropane BRL mg/kg dry 0.0051 0.00043 1 8260D 9/16/20 15:52 TBL P010790 1,4-Dichlorobenzene BRL mg/kg dry 0.0051 0.00065 1 8260D 9/16/20 15:52 TBL P010790 2,2-Dichloropropane BRL mg/kg dry 0.0051 0.00064 1 8260D 9/16/20 15:52 TBL P010790 2-Chlorotoluene BRL mg/kg dry 0.0051 0.00068 1 8260D 9/16/20 15:52 TBL P010790 4-Chlorotoluene BRL mg/kg dry 0.0051 0.00058 1 8260D 9/16/20 15:52 TBL P010790 4-Isopropyltoluene BRL mg/kg dry 0.0051 0.0013 1 8260D 9/16/20 15:52 TBL P010790 Acetone BRL CCVH mg/kg dry 0.020 0.0013 1 8260D 9/16/20 15:52 TBL P010790 Benzene BRL mg/kg dry 0.0051 0.00080 1 8260D 9/16/20 15:52 TBL P010790 Bromobenzene BRL mg/kg dry 0.0051 0.00071 1 8260D 9/16/20 15:52 TBL P010790 Bromochloromethane BRL mg/kg dry 0.0051 0.00084 1 8260D 9/16/20 15:52 TBL P010790 Bromodichloromethane BRL mg/kg dry 0.0051 0.00049 1 8260D 9/16/20 15:52 TBL P010790 Bromoform BRL mg/kg dry 0.0051 0.00040 1 8260D 9/16/20 15:52 TBL P010790 Bromomethane BRL mg/kg dry 0.010 0.0025 1 8260D 9/16/20 15:52 TBL P010790 Carbon Tetrachloride BRL mg/kg dry 0.0051 0.0010 1 8260D 9/16/20 15:52 TBL P010790 Chlorobenzene BRL mg/kg dry 0.0051 0.00080 1 8260D 9/16/20 15:52 TBL P010790 Chloroethane BRL mg/kg dry 0.010 0.00097 1 8260D 9/16/20 15:52 TBL P010790 Chloroform BRL mg/kg dry 0.0051 0.00063 1 8260D 9/16/20 15:52 TBL P010790 Chloromethane BRL mg/kg dry 0.010 0.0016 1 8260D 9/16/20 15:52 TBL P010790 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0051 0.00080 1 8260D 9/16/20 15:52 TBL P010790 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0051 0.00050 1 8260D 9/16/20 15:52 TBL P010790 Dibromochloromethane BRL mg/kg dry 0.0051 0.00034 1 8260D 9/16/20 15:52 TBL P010790 Dichlorodifluoromethane BRL mg/kg dry 0.010 0.0014 1 8260D 9/16/20 15:52 TBL P010790 Ethylbenzene BRL mg/kg dry 0.0051 0.00077 1 8260D 9/16/20 15:52 TBL P010790 Isopropyl Ether BRL mg/kg dry 0.0051 0.00075 1 8260D 9/16/20 15:52 TBL P010790 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0051 0.00059 1 8260D 9/16/20 15:52 TBL P010790 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-2S Attn: Tom Proctor Sample ID: 0090162-08 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 14:30 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID m,p-Xylenes BRL mg/kg dry 0.010 0.0013 1 8260D 9/16/20 15:52 TBL P010790 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.020 0.00035 1 8260D 9/16/20 15:52 TBL P010790 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.020 0.0012 1 8260D 9/16/20 15:52 TBL P010790 Methyl Isobutyl Ketone BRL mg/kg dry 0.020 0.00042 1 8260D 9/16/20 15:52 TBL P010790 Methylene Chloride 0.0052 mg/kg dry 0.0051 0.00083 1 8260D 9116/20 15:52 TBL P010790 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0051 0.00072 1 8260D 9/16/20 15:52 TBL P010790 Naphthalene BRL mg/kg dry 0.010 0.00052 1 8260D 9/16/20 15:52 TBL P010790 n-Butylbenzene BRL mg/kg dry 0.0051 0.00048 1 8260D 9/16/20 15:52 TBL P010790 n-Propylbenzene BRL mg/kg dry 0.0051 0.00074 1 8260D 9/16/20 15:52 TBL P010790 o-Xylene BRL mg/kg dry 0.0051 0.00054 1 8260D 9/16/20 15:52 TBL P010790 sec-Butylbenzene BRL mg/kg dry 0.0051 0.00055 1 8260D 9/16/20 15:52 TBL P010790 Styrene BRL mg/kg dry 0.0051 0.00050 1 8260D 9/16/20 15:52 TBL P010790 tert-Butylbenzene BRL mg/kg dry 0.0051 0.00061 1 8260D 9/16/20 15:52 TBL P010790 Tetrachloroethylene BRL mg/kg dry 0.0051 0.00092 1 8260D 9/16/20 15:52 TBL P010790 Toluene BRL mg/kg dry 0.0051 0.00081 1 8260D 9/16/20 15:52 TBL P010790 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0051 0.00098 1 8260D 9/16/20 15:52 TBL P010790 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0051 0.00044 1 8260D 9/16/20 15:52 TBL P010790 Trichloroethylene BRL mg/kg dry 0.0051 0.00099 1 8260D 9/16/20 15:52 TBL P010790 Trichlorofluoromethane BRL mg/kg dry 0.010 0.0014 1 8260D 9/16/20 15:52 TBL P010790 Vinyl acetate BRL mg/kg dry 0.010 0.00055 1 8260D 9/16/20 15:52 TBL P010790 Vinyl chloride BRL mg/kg dry 0.010 0.0010 1 8260D 9/16/20 15:52 TBL P010790 Xylenes, total BRL mg/kg dry 0.015 0.0018 1 8260D 9/16/20 15:52 TBL P010790 Surrogate Recovery Control Limits 4-Bromofluorobenzene 103 % 70-130 Dibromofluoromethane 98 % 84-123 Toluene-d8 92 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 35 of 93 Laboratory Report • � 10/13/2020 PA Waynt. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-3S Attn: Tom Proctor Sample ID: 0090162-09 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 13:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 90.1 % by 0.100 0.100 1 *SM2540 G 9/17/20 13:00 EDV P010783 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.73 0.13 1 8270E 9/16/20 19:09 JMV P010771 1,2-Dichlorobenzene BRL mg/kg dry 0.73 0.12 1 8270E 9/16/20 19:09 JMV P010771 1,3-Dichlorobenzene BRL mg/kg dry 0.73 0.11 1 8270E 9/16/20 19:09 JMV P010771 1,4-Dichlorobenzene BRL mg/kg dry 0.37 0.12 1 8270E 9/16/20 19:09 JMV P010771 1-Methyl naphthalene BRL mg/kg dry 0.73 0.011 1 8270E 9/16/20 19:09 JMV P010771 2,4,5-Trichlorophenol BRL mg/kg dry 0.73 0.16 1 8270E 9/16/20 19:09 JMV P010771 2,4,6-Trichlorophenol BRL mg/kg dry 0.73 0.18 1 8270E 9/16/20 19:09 JMV P010771 2,4-Dichlorophenol BRL mg/kg dry 0.73 0.14 1 8270E 9/16/20 19:09 JMV P010771 2,4-Dimethylphenol BRL mg/kg dry 0.37 0.15 1 8270E 9/16/20 19:09 JMV P010771 2,4-Dinitrophenol BRL mg/kg dry 1.7 0.43 1 8270E 9/16/20 19:09 JMV P010771 2,4-Dinitrotoluene BRL mg/kg dry 0.73 0.19 1 8270E 9/16/20 19:09 JMV P010771 2,6-Dinitrotoluene BRL mg/kg dry 0.73 0.19 1 8270E 9/16/20 19:09 JMV P010771 2-Chloronaphthalene BRL mg/kg dry 0.73 0.18 1 8270E 9/16/20 19:09 JMV P010771 2-Chlorophenol BRL mg/kg dry 0.73 0.14 1 8270E 9/16/20 19:09 JMV P010771 2-Methyl naphthalene BRL mg/kg dry 0.73 0.014 1 8270E 9/16/20 19:09 JMV P010771 2-Methylphenol BRL mg/kg dry 0.73 0.14 1 8270E 9/16/20 19:09 JMV P010771 2-Nitrophenol BRL mg/kg dry 0.73 0.12 1 8270E 9/16/20 19:09 JMV P010771 3,3'-Dichlorobenzidine BRL mg/kg dry 0.73 0.15 1 8270E 9/16/20 19:09 JMV P010771 3/4-Methyl phenol BRL mg/kg dry 0.73 0.16 1 8270E 9/16/20 19:09 JMV P010771 4,6-Dinitro-2-methylphenol BRL mg/kg dry 1.7 0.40 1 8270E 9/16/20 19:09 JMV P010771 4-Bromophenyl phenyl ether BRL mg/kg dry 0.73 0.17 1 8270E 9/16/20 19:09 JMV P010771 4-Chloro-3-methylphenol BRL mg/kg dry 0.73 0.14 1 8270E 9/16/20 19:09 JMV P010771 4-Chloroaniline BRL mg/kg dry 0.37 0.089 1 8270E 9/16/20 19:09 JMV P010771 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.1 0.22 1 8270E 9/16/20 19:09 JMV P010771 4-Nitrophenol BRL mg/kg dry 0.73 0.18 1 8270E 9/16/20 19:09 JMV P010771 Acenaphthene BRL mg/kg dry 0.73 0.017 1 8270E 9/16/20 19:09 JMV P010771 Acenaphthylene BRL mg/kg dry 0.73 0.014 1 8270E 9/16/20 19:09 JMV P010771 Anthracene BRL mg/kg dry 0.73 0.0081 1 8270E 9/16/20 19:09 JMV P010771 Azobenzene BRL mg/kg dry 0.73 0.16 1 8270E 9/16/20 19:09 JMV P010771 Benzo(a)anthracene BRL mg/kg dry 0.73 0.0088 1 8270E 9/16/20 19:09 JMV P010771 Benzo(a)pyrene BRL mg/kg dry 0.73 0.0065 1 8270E 9/16/20 19:09 JMV P010771 Benzo(b)fluoranthene BRL mg/kg dry 0.73 0.0068 1 8270E 9/16/20 19:09 JMV P010771 Benzo(g,h,i)perylene BRL mg/kg dry 0.73 0.0072 1 8270E 9/16/20 19:09 JMV P010771 Benzo(k)fluoranthene BRL mg/kg dry 0.73 0.0078 1 8270E 9/16/20 19:09 JMV P010771 Benzoic Acid BRL mg/kg dry 2.2 0.61 1 8270E 9/16/20 19:09 JMV P010771 Benzyl alcohol BRL mg/kg dry 0.73 0.14 1 8270E 9/16/20 19:09 JMV P010771 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.73 0.14 1 8270E 9/16/20 19:09 JMV P010771 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.73 0.12 1 8270E 9/16/20 19:09 JMV P010771 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.37 0.13 1 8270E 9/16/20 19:09 JMV P010771 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 36 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-3S Attn: Tom Proctor Sample ID: 0090162-09 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 13:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Bis(2-Ethylhexyl)phthaIate BRL mg/kg dry 0.73 0.17 1 8270E 9/16/20 19:09 JMV P010771 Butyl benzyl phthalate BRL mg/kg dry 0.37 0.13 1 8270E 9/16/20 19:09 JMV P010771 Chrysene BRL mg/kg dry 0.73 0.0087 1 8270E 9/16/20 19:09 JMV P010771 Dibenzo(a,h)anthracene BRL mg/kg dry 0.73 0.021 1 8270E 9/16/20 19:09 JMV P010771 Dibenzofuran BRL mg/kg dry 0.73 0.20 1 8270E 9/16/20 19:09 JMV P010771 Diethyl phthalate BRL mg/kg dry 0.73 0.19 1 8270E 9/16/20 19:09 JMV P010771 Dimethyl phthalate BRL mg/kg dry 0.73 0.18 1 8270E 9/16/20 19:09 JMV P010771 Di-n-butyl phthalate BRL mg/kg dry 0.73 0.18 1 8270E 9/16/20 19:09 JMV P010771 Di-n-octyl phthalate BRL mg/kg dry 0.37 0.19 1 8270E 9/16/20 19:09 JMV P010771 Fluoranthene BRL mg/kg dry 0.73 0.0083 1 8270E 9/16/20 19:09 JMV P010771 Fluorene BRL mg/kg dry 0.73 0.013 1 8270E 9/16/20 19:09 JMV P010771 Hexachlorobenzene BRL mg/kg dry 0.73 0.16 1 8270E 9/16/20 19:09 JMV P010771 Hexachlorobutadiene BRL mg/kg dry 0.73 0.17 1 8270E 9/16/20 19:09 JMV P010771 Hexachlorocyclopentadiene BRL mg/kg dry 0.73 0.25 1 8270E 9/16/20 19:09 JMV P010771 Hexachloroethane BRL mg/kg dry 0.73 0.12 1 8270E 9/16/20 19:09 JMV P010771 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.73 0.021 1 8270E 9/16/20 19:09 JMV P010771 Isophorone BRL mg/kg dry 0.73 0.16 1 8270E 9/16/20 19:09 JMV P010771 Naphthalene BRL mg/kg dry 0.73 0.016 1 8270E 9/16/20 19:09 JMV P010771 Nitrobenzene BRL mg/kg dry 0.37 0.16 1 8270E 9/16/20 19:09 JMV P010771 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.73 0.17 1 8270E 9/16/20 19:09 JMV P010771 N-Nitrosodiphenylamine BRL mg/kg dry 0.73 0.20 1 8270E 9/16/20 19:09 JMV P010771 Pentachlorophenol BRL mg/kg dry 1.1 0.47 1 8270E 9/16/20 19:09 JMV P010771 Phenanthrene BRL mg/kg dry 0.73 0.0080 1 8270E 9/16/20 19:09 JMV P010771 Phenol BRL mg/kg dry 0.73 0.12 1 8270E 9/16/20 19:09 JMV P010771 Pyrene BRL mg/kg dry 0.73 0.011 1 8270E 9/16/20 19:09 JMV P010771 Pyridine BRL mg/kg dry 0.37 0.070 1 8270E 9/16/20 19:09 JMV P010771 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 90 % 39-132 2-Fluorobiphenyl 73 % 44-115 2-Fluorophenol 70 % 35-115 Nitrobenzene-d5 61 % 37-122 Phenol-d5 69 % 34-121 Terphenyl-d14 74 % 54-127 Total Metals Mercury BRL mg/kg dry 0.055 0.017 1 *7471B 9/21/20 13:55 EDV P010869 Arsenic BRL mg/kg dry 1.1 0.14 1 *601OD 9/17/20 22:41 JAB P010770 Barium BRL mg/kg dry 11 1.0 1 *601OD 9/17/20 22:41 JAB P010770 Cadmium BRL mg/kg dry 0.55 0.052 1 *601OD 9/17/20 22:41 JAB P010770 Chromium 1.5 mg/kg dry 1.1 0.15 1 *6010D 9/17120 22:41 JAB P010770 Lead 1.4 mg/kg dry 1.1 0.13 1 *60101) 9/17/20 22:41 JAB P010770 Selenium BRL mg/kg dry 1.1 0.20 1 *6010D 9/18/20 21:27 JAB P010770 Silver BRL mg/kg dry 0.55 0.053 1 *6010D 9/17/20 22:41 JAB P010770 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 37 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-3S Attn: Tom Proctor Sample ID: 0090162-09 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 13:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0045 0.00055 1 8260D 9/16/20 16:22 TBL P010790 1,1,1-Trichloroethane BRL mg/kg dry 0.0045 0.00066 1 8260D 9/16/20 16:22 TBL P010790 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0045 0.00033 1 8260D 9/16/20 16:22 TBL P010790 1,1,2-Trichloroethane BRL mg/kg dry 0.0045 0.00048 1 8260D 9/16/20 16:22 TBL P010790 1,1-Dichloroethane BRL mg/kg dry 0.0045 0.00081 1 8260D 9/16/20 16:22 TBL P010790 1,1-Dichloroethylene BRL mg/kg dry 0.0045 0.00082 1 8260D 9/16/20 16:22 TBL P010790 1,1-Dichloropropylene BRL mg/kg dry 0.0045 0.00069 1 8260D 9/16/20 16:22 TBL P010790 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0089 0.00064 1 8260D 9/16/20 16:22 TBL P010790 1,2,3-Trichloropropane BRL mg/kg dry 0.0045 0.00051 1 8260D 9/16/20 16:22 TBL P010790 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0089 0.00043 1 8260D 9/16/20 16:22 TBL P010790 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0045 0.00047 1 8260D 9/16/20 16:22 TBL P010790 1,2-Dibromoethane BRL mg/kg dry 0.0045 0.00040 1 8260D 9/16/20 16:22 TBL P010790 1,2-Dichlorobenzene BRL mg/kg dry 0.0045 0.00050 1 8260D 9/16/20 16:22 TBL P010790 1,2-Dichloroethane BRL mg/kg dry 0.0045 0.00053 1 8260D 9/16/20 16:22 TBL P010790 1,2-Dichloropropane BRL mg/kg dry 0.0045 0.00067 1 8260D 9/16/20 16:22 TBL P010790 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0045 0.00056 1 8260D 9/16/20 16:22 TBL P010790 1,3-Dichlorobenzene BRL mg/kg dry 0.0045 0.00056 1 8260D 9/16/20 16:22 TBL P010790 1,3-Dichloropropane BRL mg/kg dry 0.0045 0.00037 1 8260D 9/16/20 16:22 TBL P010790 1,4-Dichlorobenzene BRL mg/kg dry 0.0045 0.00057 1 8260D 9/16/20 16:22 TBL P010790 2,2-Dichloropropane BRL mg/kg dry 0.0045 0.00056 1 8260D 9/16/20 16:22 TBL P010790 2-Chlorotoluene BRL mg/kg dry 0.0045 0.00060 1 8260D 9/16/20 16:22 TBL P010790 4-Chlorotoluene BRL mg/kg dry 0.0045 0.00051 1 8260D 9/16/20 16:22 TBL P010790 4-Isopropyltoluene BRL mg/kg dry 0.0045 0.0011 1 8260D 9/16/20 16:22 TBL P010790 Acetone BRL CCVH mg/kg dry 0.018 0.0011 1 8260D 9/16/20 16:22 TBL P010790 Benzene BRL mg/kg dry 0.0045 0.00070 1 8260D 9/16/20 16:22 TBL P010790 Bromobenzene BRL mg/kg dry 0.0045 0.00062 1 8260D 9/16/20 16:22 TBL P010790 Bromochloromethane BRL mg/kg dry 0.0045 0.00074 1 8260D 9/16/20 16:22 TBL P010790 Bromodichloromethane BRL mg/kg dry 0.0045 0.00043 1 8260D 9/16/20 16:22 TBL P010790 Bromoform BRL mg/kg dry 0.0045 0.00035 1 8260D 9/16/20 16:22 TBL P010790 Bromomethane BRL mg/kg dry 0.0089 0.0022 1 8260D 9/16/20 16:22 TBL P010790 Carbon Tetrachloride BRL mg/kg dry 0.0045 0.00088 1 8260D 9/16/20 16:22 TBL P010790 Chlorobenzene BRL mg/kg dry 0.0045 0.00070 1 8260D 9/16/20 16:22 TBL P010790 Chloroethane BRL mg/kg dry 0.0089 0.00085 1 8260D 9/16/20 16:22 TBL P010790 Chloroform BRL mg/kg dry 0.0045 0.00055 1 8260D 9/16/20 16:22 TBL P010790 Chloromethane BRL mg/kg dry 0.0089 0.0014 1 8260D 9/16/20 16:22 TBL P010790 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0045 0.00070 1 8260D 9/16/20 16:22 TBL P010790 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0045 0.00044 1 8260D 9/16/20 16:22 TBL P010790 Dibromochloromethane BRL mg/kg dry 0.0045 0.00030 1 8260D 9/16/20 16:22 TBL P010790 Dichlorodifluoromethane BRL mg/kg dry 0.0089 0.0013 1 8260D 9/16/20 16:22 TBL P010790 Ethylbenzene BRL mg/kg dry 0.0045 0.00067 1 8260D 9/16/20 16:22 TBL P010790 Isopropyl Ether BRL mg/kg dry 0.0045 0.00066 1 8260D 9/16/20 16:22 TBL P010790 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0045 0.00052 1 8260D 9/16/20 16:22 TBL P010790 m,p-Xylenes BRL mg/kg dry 0.0089 0.0011 1 8260D 9/16/20 16:22 TBL P010790 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 38 0f 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-3S Attn: Tom Proctor Sample ID: 0090162-09 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 13:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.018 0.00031 1 8260D 9/16/20 16:22 TBL P010790 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.018 0.0010 1 8260D 9/16/20 16:22 TBL P010790 Methyl Isobutyl Ketone BRL mg/kg dry 0.018 0.00037 1 8260D 9/16/20 16:22 TBL P010790 Methylene Chloride 0.0032 J mg/kg dry 0.0045 0.00072 1 8260D 9/16/20 16:22 TBL P010790 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0045 0.00063 1 8260D 9/16/20 16:22 TBL P010790 Naphthalene BRL mg/kg dry 0.0089 0.00045 1 8260D 9/16/20 16:22 TBL P010790 n-Butylbenzene BRL mg/kg dry 0.0045 0.00042 1 8260D 9/16/20 16:22 TBL P010790 n-Propylbenzene BRL mg/kg dry 0.0045 0.00065 1 8260D 9/16/20 16:22 TBL P010790 o-Xylene BRL mg/kg dry 0.0045 0.00048 1 8260D 9/16/20 16:22 TBL P010790 sec-Butylbenzene BRL mg/kg dry 0.0045 0.00048 1 8260D 9/16/20 16:22 TBL P010790 Styrene BRL mg/kg dry 0.0045 0.00043 1 8260D 9/16/20 16:22 TBL P010790 tert-Butylbenzene BRL mg/kg dry 0.0045 0.00053 1 8260D 9/16/20 16:22 TBL P010790 Tetrachloroethylene BRL mg/kg dry 0.0045 0.00081 1 8260D 9/16/20 16:22 TBL P010790 Toluene BRL mg/kg dry 0.0045 0.00071 1 8260D 9/16/20 16:22 TBL P010790 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0045 0.00086 1 8260D 9/16/20 16:22 TBL P010790 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0045 0.00038 1 8260D 9/16/20 16:22 TBL P010790 Trichloroethylene BRL mg/kg dry 0.0045 0.00087 1 8260D 9/16/20 16:22 TBL P010790 Trichlorofluoromethane BRL mg/kg dry 0.0089 0.0012 1 8260D 9/16/20 16:22 TBL P010790 Vinyl acetate BRL mg/kg dry 0.0089 0.00049 1 8260D 9/16/20 16:22 TBL P010790 Vinyl chloride BRL mg/kg dry 0.0089 0.00089 1 8260D 9/16/20 16:22 TBL P010790 Xylenes, total BRL mg/kg dry 0.013 0.0016 1 8260D 9/16/20 16:22 TBL P010790 Surrogate Recovery Control Limits 4-Bromofluorobenzene 100 % 70-130 Dibromofluoromethane 101 % 84-123 Toluene-d8 92 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 39 of 93 Laboratory Report • � 10/13/2020 PA Waynt. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-4S Attn: Tom Proctor Sample ID: 0090162-10 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 13:50 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 80.1 % by 0.100 0.100 1 *SM2540 G 9/17/20 13:00 EDV P010783 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.81 0.14 1 8270E 9/16/20 19:32 JMV P010771 1,2-Dichlorobenzene BRL mg/kg dry 0.81 0.13 1 8270E 9/16/20 19:32 JMV P010771 1,3-Dichlorobenzene BRL mg/kg dry 0.81 0.12 1 8270E 9/16/20 19:32 JMV P010771 1,4-Dichlorobenzene BRL mg/kg dry 0.41 0.13 1 8270E 9/16/20 19:32 JMV P010771 1-Methyl naphthalene BRL mg/kg dry 0.81 0.012 1 8270E 9/16/20 19:32 JMV P010771 2,4,5-Trichlorophenol BRL mg/kg dry 0.81 0.17 1 8270E 9/16/20 19:32 JMV P010771 2,4,6-Trichlorophenol BRL mg/kg dry 0.81 0.20 1 8270E 9/16/20 19:32 JMV P010771 2,4-Dichlorophenol BRL mg/kg dry 0.81 0.16 1 8270E 9/16/20 19:32 JMV P010771 2,4-Dimethylphenol BRL mg/kg dry 0.41 0.17 1 8270E 9/16/20 19:32 JMV P010771 2,4-Dinitrophenol BRL mg/kg dry 1.9 0.48 1 8270E 9/16/20 19:32 JMV P010771 2,4-Dinitrotoluene BRL mg/kg dry 0.81 0.22 1 8270E 9/16/20 19:32 JMV P010771 2,6-Dinitrotoluene BRL mg/kg dry 0.81 0.21 1 8270E 9/16/20 19:32 JMV P010771 2-Chloronaphthalene BRL mg/kg dry 0.81 0.20 1 8270E 9/16/20 19:32 JMV P010771 2-Chlorophenol BRL mg/kg dry 0.81 0.16 1 8270E 9/16/20 19:32 JMV P010771 2-Methyl naphthalene BRL mg/kg dry 0.81 0.016 1 8270E 9/16/20 19:32 JMV P010771 2-Methylphenol BRL mg/kg dry 0.81 0.16 1 8270E 9/16/20 19:32 JMV P010771 2-Nitrophenol BRL mg/kg dry 0.81 0.14 1 8270E 9/16/20 19:32 JMV P010771 3,3'-Dichlorobenzidine BRL mg/kg dry 0.81 0.16 1 8270E 9/16/20 19:32 JMV P010771 3/4-Methyl phenol BRL mg/kg dry 0.81 0.18 1 8270E 9/16/20 19:32 JMV P010771 4,6-Dinitro-2-methylphenol BRL mg/kg dry 1.9 0.45 1 8270E 9/16/20 19:32 JMV P010771 4-Bromophenyl phenyl ether BRL mg/kg dry 0.81 0.19 1 8270E 9/16/20 19:32 JMV P010771 4-Chloro-3-methylphenol BRL mg/kg dry 0.81 0.16 1 8270E 9/16/20 19:32 JMV P010771 4-Chloroaniline BRL mg/kg dry 0.41 0.099 1 8270E 9/16/20 19:32 JMV P010771 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.2 0.25 1 8270E 9/16/20 19:32 JMV P010771 4-Nitrophenol BRL mg/kg dry 0.81 0.20 1 8270E 9/16/20 19:32 JMV P010771 Acenaphthene BRL mg/kg dry 0.81 0.019 1 8270E 9/16/20 19:32 JMV P010771 Acenaphthylene BRL mg/kg dry 0.81 0.016 1 8270E 9/16/20 19:32 JMV P010771 Anthracene BRL mg/kg dry 0.81 0.0090 1 8270E 9/16/20 19:32 JMV P010771 Azobenzene BRL mg/kg dry 0.81 0.17 1 8270E 9/16/20 19:32 JMV P010771 Benzo(a)anthracene BRL mg/kg dry 0.81 0.0097 1 8270E 9/16/20 19:32 JMV P010771 Benzo(a)pyrene BRL mg/kg dry 0.81 0.0073 1 8270E 9/16/20 19:32 JMV P010771 Benzo(b)fluoranthene BRL mg/kg dry 0.81 0.0075 1 8270E 9/16/20 19:32 JMV P010771 Benzo(g,h,i)perylene BRL mg/kg dry 0.81 0.0080 1 8270E 9/16/20 19:32 JMV P010771 Benzo(k)fluoranthene BRL mg/kg dry 0.81 0.0086 1 8270E 9/16/20 19:32 JMV P010771 Benzoic Acid BRL mg/kg dry 2.5 0.68 1 8270E 9/16/20 19:32 JMV P010771 Benzyl alcohol BRL mg/kg dry 0.81 0.15 1 8270E 9/16/20 19:32 JMV P010771 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.81 0.16 1 8270E 9/16/20 19:32 JMV P010771 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.81 0.13 1 8270E 9/16/20 19:32 JMV P010771 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.41 0.15 1 8270E 9/16/20 19:32 JMV P010771 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 40 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-4S Attn: Tom Proctor Sample ID: 0090162-10 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 13:50 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Bis(2-Ethylhexyl)phthaIate BRL mg/kg dry 0.81 0.18 1 8270E 9/16/20 19:32 JMV P010771 Butyl benzyl phthalate BRL mg/kg dry 0.41 0.14 1 8270E 9/16/20 19:32 JMV P010771 Chrysene BRL mg/kg dry 0.81 0.0096 1 8270E 9/16/20 19:32 JMV P010771 Dibenzo(a,h)anthracene BRL mg/kg dry 0.81 0.023 1 8270E 9/16/20 19:32 JMV P010771 Dibenzofuran BRL mg/kg dry 0.81 0.22 1 8270E 9/16/20 19:32 JMV P010771 Diethyl phthalate BRL mg/kg dry 0.81 0.21 1 8270E 9/16/20 19:32 JMV P010771 Dimethyl phthalate BRL mg/kg dry 0.81 0.19 1 8270E 9/16/20 19:32 JMV P010771 Di-n-butyl phthalate BRL mg/kg dry 0.81 0.20 1 8270E 9/16/20 19:32 JMV P010771 Di-n-octyl phthalate BRL mg/kg dry 0.41 0.21 1 8270E 9/16/20 19:32 JMV P010771 Fluoranthene BRL mg/kg dry 0.81 0.0093 1 8270E 9/16/20 19:32 JMV P010771 Fluorene BRL mg/kg dry 0.81 0.014 1 8270E 9/16/20 19:32 JMV P010771 Hexachlorobenzene BRL mg/kg dry 0.81 0.18 1 8270E 9/16/20 19:32 JMV P010771 Hexachlorobutadiene BRL mg/kg dry 0.81 0.18 1 8270E 9/16/20 19:32 JMV P010771 Hexachlorocyclopentadiene BRL mg/kg dry 0.81 0.28 1 8270E 9/16/20 19:32 JMV P010771 Hexachloroethane BRL mg/kg dry 0.81 0.13 1 8270E 9/16/20 19:32 JMV P010771 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.81 0.023 1 8270E 9/16/20 19:32 JMV P010771 Isophorone BRL mg/kg dry 0.81 0.18 1 8270E 9/16/20 19:32 JMV P010771 Naphthalene BRL mg/kg dry 0.81 0.017 1 8270E 9/16/20 19:32 JMV P010771 Nitrobenzene BRL mg/kg dry 0.41 0.17 1 8270E 9/16/20 19:32 JMV P010771 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.81 0.19 1 8270E 9/16/20 19:32 JMV P010771 N-Nitrosodiphenylamine BRL mg/kg dry 0.81 0.22 1 8270E 9/16/20 19:32 JMV P010771 Pentachlorophenol BRL mg/kg dry 1.2 0.52 1 8270E 9/16/20 19:32 JMV P010771 Phenanthrene BRL mg/kg dry 0.81 0.0089 1 8270E 9/16/20 19:32 JMV P010771 Phenol BRL mg/kg dry 0.81 0.13 1 8270E 9/16/20 19:32 JMV P010771 Pyrene BRL mg/kg dry 0.81 0.012 1 8270E 9/16/20 19:32 JMV P010771 Pyridine BRL mg/kg dry 0.41 0.078 1 8270E 9/16/20 19:32 JMV P010771 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 97 % 39-132 2-Fluorobiphenyl 77 % 44-115 2-Fluorophenol 76 % 35-115 Nitrobenzene-d5 65 % 37-122 Phenol-d5 74 % 34-121 Terphenyl-d14 79 % 54-127 Total Metals Mercury BRL mg/kg dry 0.062 0.019 1 *7471B 9/21/20 13:59 EDV P010869 Arsenic BRL mg/kg dry 1.2 0.15 1 *601OD 9/17/20 22:47 JAB P010770 Barium BRL mg/kg dry 12 1.1 1 *601OD 9/17/20 22:47 JAB P010770 Cadmium BRL mg/kg dry 0.62 0.059 1 *601OD 9/17/20 22:47 JAB P010770 Chromium 1.3 mg/kg dry 1.2 0.17 1 *6010D 9/17/20 22:47 JAB P010770 Lead BRL mg/kg dry 1.2 0.15 1 *601OD 9/17/20 22:47 JAB P010770 Selenium BRL mg/kg dry 1.2 0.22 1 *601OD 9/18/20 21:34 JAB P010770 Silver BRL mg/kg dry 0.62 0.060 1 *601OD 9/17/20 22:47 JAB P010770 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 41 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-4S Attn: Tom Proctor Sample ID: 0090162-10 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 13:50 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0054 0.00066 1 8260D 9/16/20 16:51 TBL P010790 1,1,1-Trichloroethane BRL mg/kg dry 0.0054 0.00079 1 8260D 9/16/20 16:51 TBL P010790 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0054 0.00039 1 8260D 9/16/20 16:51 TBL P010790 1,1,2-Trichloroethane BRL mg/kg dry 0.0054 0.00058 1 8260D 9/16/20 16:51 TBL P010790 1,1-Dichloroethane BRL mg/kg dry 0.0054 0.00097 1 8260D 9/16/20 16:51 TBL P010790 1,1-Dichloroethylene BRL mg/kg dry 0.0054 0.00099 1 8260D 9/16/20 16:51 TBL P010790 1,1-Dichloropropylene BRL mg/kg dry 0.0054 0.00083 1 8260D 9/16/20 16:51 TBL P010790 1,2,3-Trichlorobenzene BRL mg/kg dry 0.011 0.00077 1 8260D 9/16/20 16:51 TBL P010790 1,2,3-Trichloropropane BRL mg/kg dry 0.0054 0.00061 1 8260D 9/16/20 16:51 TBL P010790 1,2,4-Trichlorobenzene BRL mg/kg dry 0.011 0.00052 1 8260D 9/16/20 16:51 TBL P010790 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0054 0.00057 1 8260D 9/16/20 16:51 TBL P010790 1,2-Dibromoethane BRL mg/kg dry 0.0054 0.00048 1 8260D 9/16/20 16:51 TBL P010790 1,2-Dichlorobenzene BRL mg/kg dry 0.0054 0.00060 1 8260D 9/16/20 16:51 TBL P010790 1,2-Dichloroethane BRL mg/kg dry 0.0054 0.00064 1 8260D 9/16/20 16:51 TBL P010790 1,2-Dichloropropane BRL mg/kg dry 0.0054 0.00081 1 8260D 9/16/20 16:51 TBL P010790 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0054 0.00068 1 8260D 9/16/20 16:51 TBL P010790 1,3-Dichlorobenzene BRL mg/kg dry 0.0054 0.00067 1 8260D 9/16/20 16:51 TBL P010790 1,3-Dichloropropane BRL mg/kg dry 0.0054 0.00045 1 8260D 9/16/20 16:51 TBL P010790 1,4-Dichlorobenzene BRL mg/kg dry 0.0054 0.00068 1 8260D 9/16/20 16:51 TBL P010790 2,2-Dichloropropane BRL mg/kg dry 0.0054 0.00067 1 8260D 9/16/20 16:51 TBL P010790 2-Chlorotoluene BRL mg/kg dry 0.0054 0.00072 1 8260D 9/16/20 16:51 TBL P010790 4-Chlorotoluene BRL mg/kg dry 0.0054 0.00062 1 8260D 9/16/20 16:51 TBL P010790 4-Isopropyltoluene BRL mg/kg dry 0.0054 0.0014 1 8260D 9/16/20 16:51 TBL P010790 Acetone BRL CCVH mg/kg dry 0.022 0.0014 1 8260D 9/16/20 16:51 TBL P010790 Benzene BRL mg/kg dry 0.0054 0.00084 1 8260D 9/16/20 16:51 TBL P010790 Bromobenzene BRL mg/kg dry 0.0054 0.00075 1 8260D 9/16/20 16:51 TBL P010790 Bromochloromethane BRL mg/kg dry 0.0054 0.00089 1 8260D 9/16/20 16:51 TBL P010790 Bromodichloromethane BRL mg/kg dry 0.0054 0.00051 1 8260D 9/16/20 16:51 TBL P010790 Bromoform BRL mg/kg dry 0.0054 0.00042 1 8260D 9/16/20 16:51 TBL P010790 Bromomethane BRL mg/kg dry 0.011 0.0026 1 8260D 9/16/20 16:51 TBL P010790 Carbon Tetrachloride BRL mg/kg dry 0.0054 0.0011 1 8260D 9/16/20 16:51 TBL P010790 Chlorobenzene BRL mg/kg dry 0.0054 0.00084 1 8260D 9/16/20 16:51 TBL P010790 Chloroethane BRL mg/kg dry 0.011 0.0010 1 8260D 9/16/20 16:51 TBL P010790 Chloroform BRL mg/kg dry 0.0054 0.00066 1 8260D 9/16/20 16:51 TBL P010790 Chloromethane BRL mg/kg dry 0.011 0.0016 1 8260D 9/16/20 16:51 TBL P010790 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0054 0.00085 1 8260D 9/16/20 16:51 TBL P010790 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0054 0.00053 1 8260D 9/16/20 16:51 TBL P010790 Dibromochloromethane BRL mg/kg dry 0.0054 0.00036 1 8260D 9/16/20 16:51 TBL P010790 Dichlorodifluoromethane BRL mg/kg dry 0.011 0.0015 1 8260D 9/16/20 16:51 TBL P010790 Ethylbenzene BRL mg/kg dry 0.0054 0.00081 1 8260D 9/16/20 16:51 TBL P010790 Isopropyl Ether BRL mg/kg dry 0.0054 0.00079 1 8260D 9/16/20 16:51 TBL P010790 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0054 0.00063 1 8260D 9/16/20 16:51 TBL P010790 m,p-Xylenes BRL mg/kg dry 0.011 0.0014 1 8260D 9/16/20 16:51 TBL P010790 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 42 0f 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-4S Attn: Tom Proctor Sample ID: 0090162-10 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 13:50 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.022 0.00037 1 8260D 9/16/20 16:51 TBL P010790 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.022 0.0013 1 8260D 9/16/20 16:51 TBL P010790 Methyl Isobutyl Ketone BRL mg/kg dry 0.022 0.00044 1 8260D 9/16/20 16:51 TBL P010790 Methylene Chloride 0.0035 J mg/kg dry 0.0054 0.00087 1 8260D 9/16/20 16:51 TBL P010790 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0054 0.00076 1 8260D 9/16/20 16:51 TBL P010790 Naphthalene BRL mg/kg dry 0.011 0.00055 1 8260D 9/16/20 16:51 TBL P010790 n-Butylbenzene BRL mg/kg dry 0.0054 0.00051 1 8260D 9/16/20 16:51 TBL P010790 n-Propylbenzene BRL mg/kg dry 0.0054 0.00078 1 8260D 9/16/20 16:51 TBL P010790 o-Xylene BRL mg/kg dry 0.0054 0.00057 1 8260D 9/16/20 16:51 TBL P010790 sec-Butylbenzene BRL mg/kg dry 0.0054 0.00058 1 8260D 9/16/20 16:51 TBL P010790 Styrene BRL mg/kg dry 0.0054 0.00052 1 8260D 9/16/20 16:51 TBL P010790 tert-Butylbenzene BRL mg/kg dry 0.0054 0.00064 1 8260D 9/16/20 16:51 TBL P010790 Tetrachloroethylene BRL mg/kg dry 0.0054 0.00098 1 8260D 9/16/20 16:51 TBL P010790 Toluene BRL mg/kg dry 0.0054 0.00086 1 8260D 9/16/20 16:51 TBL P010790 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0054 0.0010 1 8260D 9/16/20 16:51 TBL P010790 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0054 0.00046 1 8260D 9/16/20 16:51 TBL P010790 Trichloroethylene BRL mg/kg dry 0.0054 0.0010 1 8260D 9/16/20 16:51 TBL P010790 Trichlorofluoromethane BRL mg/kg dry 0.011 0.0015 1 8260D 9/16/20 16:51 TBL P010790 Vinyl acetate BRL mg/kg dry 0.011 0.00059 1 8260D 9/16/20 16:51 TBL P010790 Vinyl chloride BRL mg/kg dry 0.011 0.0011 1 8260D 9/16/20 16:51 TBL P010790 Xylenes, total BRL mg/kg dry 0.016 0.0019 1 8260D 9/16/20 16:51 TBL P010790 Surrogate Recovery Control Limits 4-Bromofluorobenzene 100 % 70-130 Dibromofluoromethane 102 % 84-123 Toluene-d8 93 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 43 of 93 Laboratory Report • � 10/13/2020 PA Waynt. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-5S Attn: Tom Proctor Sample ID: 0090162-11 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 14:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 78.9 % by 0.100 0.100 1 *SM2540 G 9/17/20 13:00 EDV P010783 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.83 0.15 1 8270E 9/16/20 19:54 JMV P010771 1,2-Dichlorobenzene BRL mg/kg dry 0.83 0.13 1 8270E 9/16/20 19:54 JMV P010771 1,3-Dichlorobenzene BRL mg/kg dry 0.83 0.12 1 8270E 9/16/20 19:54 JMV P010771 1,4-Dichlorobenzene BRL mg/kg dry 0.42 0.13 1 8270E 9/16/20 19:54 JMV P010771 1-Methyl naphthalene BRL mg/kg dry 0.83 0.013 1 8270E 9/16/20 19:54 JMV P010771 2,4,5-Trichlorophenol BRL mg/kg dry 0.83 0.18 1 8270E 9/16/20 19:54 JMV P010771 2,4,6-Trichlorophenol BRL mg/kg dry 0.83 0.20 1 8270E 9/16/20 19:54 JMV P010771 2,4-Dichlorophenol BRL mg/kg dry 0.83 0.16 1 8270E 9/16/20 19:54 JMV P010771 2,4-Dimethylphenol BRL mg/kg dry 0.42 0.17 1 8270E 9/16/20 19:54 JMV P010771 2,4-Dinitrophenol BRL mg/kg dry 1.9 0.49 1 8270E 9/16/20 19:54 JMV P010771 2,4-Dinitrotoluene BRL mg/kg dry 0.83 0.22 1 8270E 9/16/20 19:54 JMV P010771 2,6-Dinitrotoluene BRL mg/kg dry 0.83 0.22 1 8270E 9/16/20 19:54 JMV P010771 2-Chloronaphthalene BRL mg/kg dry 0.83 0.20 1 8270E 9/16/20 19:54 JMV P010771 2-Chlorophenol BRL mg/kg dry 0.83 0.16 1 8270E 9/16/20 19:54 JMV P010771 2-Methyl naphthalene BRL mg/kg dry 0.83 0.016 1 8270E 9/16/20 19:54 JMV P010771 2-Methylphenol BRL mg/kg dry 0.83 0.16 1 8270E 9/16/20 19:54 JMV P010771 2-Nitrophenol BRL mg/kg dry 0.83 0.14 1 8270E 9/16/20 19:54 JMV P010771 3,3'-Dichlorobenzidine BRL mg/kg dry 0.83 0.17 1 8270E 9/16/20 19:54 JMV P010771 3/4-Methyl phenol BRL mg/kg dry 0.83 0.18 1 8270E 9/16/20 19:54 JMV P010771 4,6-Dinitro-2-methylphenol BRL mg/kg dry 1.9 0.46 1 8270E 9/16/20 19:54 JMV P010771 4-Bromophenyl phenyl ether BRL mg/kg dry 0.83 0.20 1 8270E 9/16/20 19:54 JMV P010771 4-Chloro-3-methylphenol BRL mg/kg dry 0.83 0.16 1 8270E 9/16/20 19:54 JMV P010771 4-Chloroaniline BRL mg/kg dry 0.42 0.10 1 8270E 9/16/20 19:54 JMV P010771 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.3 0.25 1 8270E 9/16/20 19:54 JMV P010771 4-Nitrophenol BRL mg/kg dry 0.83 0.21 1 8270E 9/16/20 19:54 JMV P010771 Acenaphthene BRL mg/kg dry 0.83 0.019 1 8270E 9/16/20 19:54 JMV P010771 Acenaphthylene BRL mg/kg dry 0.83 0.016 1 8270E 9/16/20 19:54 JMV P010771 Anthracene BRL mg/kg dry 0.83 0.0092 1 8270E 9/16/20 19:54 JMV P010771 Azobenzene BRL mg/kg dry 0.83 0.18 1 8270E 9/16/20 19:54 JMV P010771 Benzo(a)anthracene BRL mg/kg dry 0.83 0.010 1 8270E 9/16/20 19:54 JMV P010771 Benzo(a)pyrene BRL mg/kg dry 0.83 0.0074 1 8270E 9/16/20 19:54 JMV P010771 Benzo(b)fluoranthene BRL mg/kg dry 0.83 0.0077 1 8270E 9/16/20 19:54 JMV P010771 Benzo(g,h,i)perylene BRL mg/kg dry 0.83 0.0082 1 8270E 9/16/20 19:54 JMV P010771 Benzo(k)fluoranthene BRL mg/kg dry 0.83 0.0088 1 8270E 9/16/20 19:54 JMV P010771 Benzoic Acid BRL mg/kg dry 2.5 0.69 1 8270E 9/16/20 19:54 JMV P010771 Benzyl alcohol BRL mg/kg dry 0.83 0.16 1 8270E 9/16/20 19:54 JMV P010771 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.83 0.16 1 8270E 9/16/20 19:54 JMV P010771 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.83 0.13 1 8270E 9/16/20 19:54 JMV P010771 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.42 0.15 1 8270E 9/16/20 19:54 JMV P010771 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 44 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-5S Attn: Tom Proctor Sample ID: 0090162-11 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 14:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Bis(2-Ethylhexyl)phthaIate BRL mg/kg dry 0.83 0.19 1 8270E 9/16/20 19:54 JMV P010771 Butyl benzyl phthalate BRL mg/kg dry 0.42 0.14 1 8270E 9/16/20 19:54 JMV P010771 Chrysene BRL mg/kg dry 0.83 0.0098 1 8270E 9/16/20 19:54 JMV P010771 Dibenzo(a,h)anthracene BRL mg/kg dry 0.83 0.024 1 8270E 9/16/20 19:54 JMV P010771 Dibenzofuran BRL mg/kg dry 0.83 0.22 1 8270E 9/16/20 19:54 JMV P010771 Diethyl phthalate BRL mg/kg dry 0.83 0.21 1 8270E 9/16/20 19:54 JMV P010771 Dimethyl phthalate BRL mg/kg dry 0.83 0.20 1 8270E 9/16/20 19:54 JMV P010771 Di-n-butyl phthalate BRL mg/kg dry 0.83 0.21 1 8270E 9/16/20 19:54 JMV P010771 Di-n-octyl phthalate BRL mg/kg dry 0.42 0.22 1 8270E 9/16/20 19:54 JMV P010771 Fluoranthene BRL mg/kg dry 0.83 0.0095 1 8270E 9/16/20 19:54 JMV P010771 Fluorene BRL mg/kg dry 0.83 0.014 1 8270E 9/16/20 19:54 JMV P010771 Hexachlorobenzene BRL mg/kg dry 0.83 0.18 1 8270E 9/16/20 19:54 JMV P010771 Hexachlorobutadiene BRL mg/kg dry 0.83 0.19 1 8270E 9/16/20 19:54 JMV P010771 Hexachlorocyclopentadiene BRL mg/kg dry 0.83 0.29 1 8270E 9/16/20 19:54 JMV P010771 Hexachloroethane BRL mg/kg dry 0.83 0.13 1 8270E 9/16/20 19:54 JMV P010771 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.83 0.023 1 8270E 9/16/20 19:54 JMV P010771 Isophorone BRL mg/kg dry 0.83 0.18 1 8270E 9/16/20 19:54 JMV P010771 Naphthalene BRL mg/kg dry 0.83 0.018 1 8270E 9/16/20 19:54 JMV P010771 Nitrobenzene BRL mg/kg dry 0.42 0.18 1 8270E 9/16/20 19:54 JMV P010771 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.83 0.19 1 8270E 9/16/20 19:54 JMV P010771 N-Nitrosodiphenylamine BRL mg/kg dry 0.83 0.23 1 8270E 9/16/20 19:54 JMV P010771 Pentachlorophenol BRL mg/kg dry 1.3 0.53 1 8270E 9/16/20 19:54 JMV P010771 Phenanthrene BRL mg/kg dry 0.83 0.0091 1 8270E 9/16/20 19:54 JMV P010771 Phenol BRL mg/kg dry 0.83 0.14 1 8270E 9/16/20 19:54 JMV P010771 Pyrene BRL mg/kg dry 0.83 0.012 1 8270E 9/16/20 19:54 JMV P010771 Pyridine BRL mg/kg dry 0.42 0.079 1 8270E 9/16/20 19:54 JMV P010771 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 90 % 39-132 2-Fluorobiphenyl 74 % 44-115 2-Fluorophenol 72 % 35-115 Nitrobenzene-d5 60 % 37-122 Phenol-d5 71 % 34-121 Terphenyl-d14 74 % 54-127 Total Metals Mercury BRL mg/kg dry 0.063 0.019 1 *7471B 9/21/20 14:13 EDV P010869 Arsenic BRL mg/kg dry 1.3 0.16 1 *601OD 9/17/20 22:54 JAB P010770 Barium BRL mg/kg dry 13 1.1 1 *601OD 9/17/20 22:54 JAB P010770 Cadmium BRL mg/kg dry 0.63 0.060 1 *601OD 9/17/20 22:54 JAB P010770 Chromium BRL mg/kg dry 1.3 0.17 1 *601OD 9/17/20 22:54 JAB P010770 Lead BRL mg/kg dry 1.3 0.15 1 *601OD 9/17/20 22:54 JAB P010770 Selenium BRL mg/kg dry 1.3 0.23 1 *601OD 9/18/20 21:41 JAB P010770 Silver BRL mg/kg dry 0.63 0.061 1 *601OD 9/17/20 22:54 JAB P010770 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 45 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-5S Attn: Tom Proctor Sample ID: 0090162-11 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 14:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0054 0.00066 1 8260D 9/16/20 17:21 TBL P010790 1,1,1-Trichloroethane BRL mg/kg dry 0.0054 0.00080 1 8260D 9/16/20 17:21 TBL P010790 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0054 0.00039 1 8260D 9/16/20 17:21 TBL P010790 1,1,2-Trichloroethane BRL mg/kg dry 0.0054 0.00059 1 8260D 9/16/20 17:21 TBL P010790 1,1-Dichloroethane BRL mg/kg dry 0.0054 0.00098 1 8260D 9/16/20 17:21 TBL P010790 1,1-Dichloroethylene BRL mg/kg dry 0.0054 0.00099 1 8260D 9/16/20 17:21 TBL P010790 1,1-Dichloropropylene BRL mg/kg dry 0.0054 0.00084 1 8260D 9/16/20 17:21 TBL P010790 1,2,3-Trichlorobenzene BRL mg/kg dry 0.011 0.00078 1 8260D 9/16/20 17:21 TBL P010790 1,2,3-Trichloropropane BRL mg/kg dry 0.0054 0.00062 1 8260D 9/16/20 17:21 TBL P010790 1,2,4-Trichlorobenzene BRL mg/kg dry 0.011 0.00052 1 8260D 9/16/20 17:21 TBL P010790 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0054 0.00057 1 8260D 9/16/20 17:21 TBL P010790 1,2-Dibromoethane BRL mg/kg dry 0.0054 0.00049 1 8260D 9/16/20 17:21 TBL P010790 1,2-Dichlorobenzene BRL mg/kg dry 0.0054 0.00060 1 8260D 9/16/20 17:21 TBL P010790 1,2-Dichloroethane BRL mg/kg dry 0.0054 0.00064 1 8260D 9/16/20 17:21 TBL P010790 1,2-Dichloropropane BRL mg/kg dry 0.0054 0.00082 1 8260D 9/16/20 17:21 TBL P010790 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0054 0.00068 1 8260D 9/16/20 17:21 TBL P010790 1,3-Dichlorobenzene BRL mg/kg dry 0.0054 0.00067 1 8260D 9/16/20 17:21 TBL P010790 1,3-Dichloropropane BRL mg/kg dry 0.0054 0.00045 1 8260D 9/16/20 17:21 TBL P010790 1,4-Dichlorobenzene BRL mg/kg dry 0.0054 0.00069 1 8260D 9/16/20 17:21 TBL P010790 2,2-Dichloropropane BRL mg/kg dry 0.0054 0.00068 1 8260D 9/16/20 17:21 TBL P010790 2-Chlorotoluene BRL mg/kg dry 0.0054 0.00073 1 8260D 9/16/20 17:21 TBL P010790 4-Chlorotoluene BRL mg/kg dry 0.0054 0.00062 1 8260D 9/16/20 17:21 TBL P010790 4-Isopropyltoluene BRL mg/kg dry 0.0054 0.0014 1 8260D 9/16/20 17:21 TBL P010790 Acetone BRL CCVH mg/kg dry 0.022 0.0014 1 8260D 9/16/20 17:21 TBL P010790 Benzene BRL mg/kg dry 0.0054 0.00085 1 8260D 9/16/20 17:21 TBL P010790 Bromobenzene BRL mg/kg dry 0.0054 0.00075 1 8260D 9/16/20 17:21 TBL P010790 Bromochloromethane BRL mg/kg dry 0.0054 0.00089 1 8260D 9/16/20 17:21 TBL P010790 Bromodichloromethane BRL mg/kg dry 0.0054 0.00051 1 8260D 9/16/20 17:21 TBL P010790 Bromoform BRL mg/kg dry 0.0054 0.00042 1 8260D 9/16/20 17:21 TBL P010790 Bromomethane BRL mg/kg dry 0.011 0.0027 1 8260D 9/16/20 17:21 TBL P010790 Carbon Tetrachloride BRL mg/kg dry 0.0054 0.0011 1 8260D 9/16/20 17:21 TBL P010790 Chlorobenzene BRL mg/kg dry 0.0054 0.00085 1 8260D 9/16/20 17:21 TBL P010790 Chloroethane BRL mg/kg dry 0.011 0.0010 1 8260D 9/16/20 17:21 TBL P010790 Chloroform BRL mg/kg dry 0.0054 0.00066 1 8260D 9/16/20 17:21 TBL P010790 Chloromethane BRL mg/kg dry 0.011 0.0016 1 8260D 9/16/20 17:21 TBL P010790 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0054 0.00085 1 8260D 9/16/20 17:21 TBL P010790 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0054 0.00053 1 8260D 9/16/20 17:21 TBL P010790 Dibromochloromethane BRL mg/kg dry 0.0054 0.00036 1 8260D 9/16/20 17:21 TBL P010790 Dichlorodifluoromethane BRL mg/kg dry 0.011 0.0015 1 8260D 9/16/20 17:21 TBL P010790 Ethylbenzene BRL mg/kg dry 0.0054 0.00082 1 8260D 9/16/20 17:21 TBL P010790 Isopropyl Ether BRL mg/kg dry 0.0054 0.00080 1 8260D 9/16/20 17:21 TBL P010790 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0054 0.00063 1 8260D 9/16/20 17:21 TBL P010790 m,p-Xylenes BRL mg/kg dry 0.011 0.0014 1 8260D 9/16/20 17:21 TBL P010790 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 46 0f 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-5S Attn: Tom Proctor Sample ID: 0090162-11 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 14:40 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.022 0.00038 1 8260D 9/16/20 17:21 TBL P010790 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.022 0.0013 1 8260D 9/16/20 17:21 TBL P010790 Methyl Isobutyl Ketone BRL mg/kg dry 0.022 0.00044 1 8260D 9/16/20 17:21 TBL P010790 Methylene Chloride 0.0030 J mg/kg dry 0.0054 0.00088 1 8260D 9/16/20 17:21 TBL P010790 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0054 0.00076 1 8260D 9/16/20 17:21 TBL P010790 Naphthalene BRL mg/kg dry 0.011 0.00055 1 8260D 9/16/20 17:21 TBL P010790 n-Butylbenzene BRL mg/kg dry 0.0054 0.00051 1 8260D 9/16/20 17:21 TBL P010790 n-Propylbenzene BRL mg/kg dry 0.0054 0.00079 1 8260D 9/16/20 17:21 TBL P010790 o-Xylene BRL mg/kg dry 0.0054 0.00058 1 8260D 9/16/20 17:21 TBL P010790 sec-Butylbenzene BRL mg/kg dry 0.0054 0.00059 1 8260D 9/16/20 17:21 TBL P010790 Styrene BRL mg/kg dry 0.0054 0.00053 1 8260D 9/16/20 17:21 TBL P010790 tert-Butylbenzene BRL mg/kg dry 0.0054 0.00064 1 8260D 9/16/20 17:21 TBL P010790 Tetrachloroethylene BRL mg/kg dry 0.0054 0.00098 1 8260D 9/16/20 17:21 TBL P010790 Toluene BRL mg/kg dry 0.0054 0.00086 1 8260D 9/16/20 17:21 TBL P010790 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0054 0.0010 1 8260D 9/16/20 17:21 TBL P010790 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0054 0.00046 1 8260D 9/16/20 17:21 TBL P010790 Trichloroethylene BRL mg/kg dry 0.0054 0.0011 1 8260D 9/16/20 17:21 TBL P010790 Trichlorofluoromethane BRL mg/kg dry 0.011 0.0015 1 8260D 9/16/20 17:21 TBL P010790 Vinyl acetate BRL mg/kg dry 0.011 0.00059 1 8260D 9/16/20 17:21 TBL P010790 Vinyl chloride BRL mg/kg dry 0.011 0.0011 1 8260D 9/16/20 17:21 TBL P010790 Xylenes, total BRL mg/kg dry 0.016 0.0020 1 8260D 9/16/20 17:21 TBL P010790 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 70-130 Dibromofluoromethane 101 % 84-123 Toluene-d8 93 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 47 of 93 Laboratory Report • � 10/13/2020 PA Waynt. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-6S Attn: Tom Proctor Sample ID: 0090162-12 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 16:10 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 93.5 % by 0.100 0.100 1 *SM2540 G 9/17/20 13:00 EDV P010783 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.71 0.13 1 8270E 9/16/20 20:17 JMV P010771 1,2-Dichlorobenzene BRL mg/kg dry 0.71 0.11 1 8270E 9/16/20 20:17 JMV P010771 1,3-Dichlorobenzene BRL mg/kg dry 0.71 0.10 1 8270E 9/16/20 20:17 JMV P010771 1,4-Dichlorobenzene BRL mg/kg dry 0.35 0.11 1 8270E 9/16/20 20:17 JMV P010771 1-Methyl naphthalene BRL mg/kg dry 0.71 0.011 1 8270E 9/16/20 20:17 JMV P010771 2,4,5-Trichlorophenol BRL mg/kg dry 0.71 0.15 1 8270E 9/16/20 20:17 JMV P010771 2,4,6-Trichlorophenol BRL mg/kg dry 0.71 0.17 1 8270E 9/16/20 20:17 JMV P010771 2,4-Dichlorophenol BRL mg/kg dry 0.71 0.14 1 8270E 9/16/20 20:17 JMV P010771 2,4-Dimethylphenol BRL mg/kg dry 0.35 0.15 1 8270E 9/16/20 20:17 JMV P010771 2,4-Dinitrophenol BRL mg/kg dry 1.6 0.41 1 8270E 9/16/20 20:17 JMV P010771 2,4-Dinitrotoluene BRL mg/kg dry 0.71 0.19 1 8270E 9/16/20 20:17 JMV P010771 2,6-Dinitrotoluene BRL mg/kg dry 0.71 0.18 1 8270E 9/16/20 20:17 JMV P010771 2-Chloronaphthalene BRL mg/kg dry 0.71 0.17 1 8270E 9/16/20 20:17 JMV P010771 2-Chlorophenol BRL mg/kg dry 0.71 0.13 1 8270E 9/16/20 20:17 JMV P010771 2-Methyl naphthalene BRL mg/kg dry 0.71 0.014 1 8270E 9/16/20 20:17 JMV P010771 2-Methylphenol BRL mg/kg dry 0.71 0.13 1 8270E 9/16/20 20:17 JMV P010771 2-Nitrophenol BRL mg/kg dry 0.71 0.12 1 8270E 9/16/20 20:17 JMV P010771 3,3'-Dichlorobenzidine BRL mg/kg dry 0.71 0.14 1 8270E 9/16/20 20:17 JMV P010771 3/4-Methyl phenol BRL mg/kg dry 0.71 0.15 1 8270E 9/16/20 20:17 JMV P010771 4,6-Dinitro-2-methylphenol BRL mg/kg dry 1.6 0.39 1 8270E 9/16/20 20:17 JMV P010771 4-Bromophenyl phenyl ether BRL mg/kg dry 0.71 0.17 1 8270E 9/16/20 20:17 JMV P010771 4-Chloro-3-methylphenol BRL mg/kg dry 0.71 0.13 1 8270E 9/16/20 20:17 JMV P010771 4-Chloroaniline BRL mg/kg dry 0.35 0.086 1 8270E 9/16/20 20:17 JMV P010771 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.1 0.22 1 8270E 9/16/20 20:17 JMV P010771 4-Nitrophenol BRL mg/kg dry 0.71 0.17 1 8270E 9/16/20 20:17 JMV P010771 Acenaphthene BRL mg/kg dry 0.71 0.016 1 8270E 9/16/20 20:17 JMV P010771 Acenaphthylene BRL mg/kg dry 0.71 0.014 1 8270E 9/16/20 20:17 JMV P010771 Anthracene BRL mg/kg dry 0.71 0.0078 1 8270E 9/16/20 20:17 JMV P010771 Azobenzene BRL mg/kg dry 0.71 0.15 1 8270E 9/16/20 20:17 JMV P010771 Benzo(a)anthracene BRL mg/kg dry 0.71 0.0085 1 8270E 9/16/20 20:17 JMV P010771 Benzo(a)pyrene BRL mg/kg dry 0.71 0.0063 1 8270E 9/16/20 20:17 JMV P010771 Benzo(b)fluoranthene BRL mg/kg dry 0.71 0.0065 1 8270E 9/16/20 20:17 JMV P010771 Benzo(g,h,i)perylene BRL mg/kg dry 0.71 0.0070 1 8270E 9/16/20 20:17 JMV P010771 Benzo(k)fluoranthene BRL mg/kg dry 0.71 0.0075 1 8270E 9/16/20 20:17 JMV P010771 Benzoic Acid BRL mg/kg dry 2.1 0.59 1 8270E 9/16/20 20:17 JMV P010771 Benzyl alcohol BRL mg/kg dry 0.71 0.13 1 8270E 9/16/20 20:17 JMV P010771 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.71 0.13 1 8270E 9/16/20 20:17 JMV P010771 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.71 0.11 1 8270E 9/16/20 20:17 JMV P010771 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.35 0.13 1 8270E 9/16/20 20:17 JMV P010771 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 48 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-6S Attn: Tom Proctor Sample ID: 0090162-12 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 16:10 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Bis(2-Ethylhexyl)phthaIate BRL mg/kg dry 0.71 0.16 1 8270E 9/16/20 20:17 JMV P010771 Butyl benzyl phthalate BRL mg/kg dry 0.35 0.12 1 8270E 9/16/20 20:17 JMV P010771 Chrysene BRL mg/kg dry 0.71 0.0083 1 8270E 9/16/20 20:17 JMV P010771 Dibenzo(a,h)anthracene BRL mg/kg dry 0.71 0.020 1 8270E 9/16/20 20:17 JMV P010771 Dibenzofuran BRL mg/kg dry 0.71 0.19 1 8270E 9/16/20 20:17 JMV P010771 Diethyl phthalate BRL mg/kg dry 0.71 0.18 1 8270E 9/16/20 20:17 JMV P010771 Dimethyl phthalate BRL mg/kg dry 0.71 0.17 1 8270E 9/16/20 20:17 JMV P010771 Di-n-butyl phthalate BRL mg/kg dry 0.71 0.18 1 8270E 9/16/20 20:17 JMV P010771 Di-n-octyl phthalate BRL mg/kg dry 0.35 0.18 1 8270E 9/16/20 20:17 JMV P010771 Fluoranthene BRL mg/kg dry 0.71 0.0080 1 8270E 9/16/20 20:17 JMV P010771 Fluorene BRL mg/kg dry 0.71 0.012 1 8270E 9/16/20 20:17 JMV P010771 Hexachlorobenzene BRL mg/kg dry 0.71 0.16 1 8270E 9/16/20 20:17 JMV P010771 Hexachlorobutadiene BRL mg/kg dry 0.71 0.16 1 8270E 9/16/20 20:17 JMV P010771 Hexachlorocyclopentadiene BRL mg/kg dry 0.71 0.24 1 8270E 9/16/20 20:17 JMV P010771 Hexachloroethane BRL mg/kg dry 0.71 0.11 1 8270E 9/16/20 20:17 JMV P010771 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.71 0.020 1 8270E 9/16/20 20:17 JMV P010771 Isophorone BRL mg/kg dry 0.71 0.15 1 8270E 9/16/20 20:17 JMV P010771 Naphthalene BRL mg/kg dry 0.71 0.015 1 8270E 9/16/20 20:17 JMV P010771 Nitrobenzene BRL mg/kg dry 0.35 0.15 1 8270E 9/16/20 20:17 JMV P010771 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.71 0.16 1 8270E 9/16/20 20:17 JMV P010771 N-Nitrosodiphenylamine BRL mg/kg dry 0.71 0.19 1 8270E 9/16/20 20:17 JMV P010771 Pentachlorophenol BRL mg/kg dry 1.1 0.45 1 8270E 9/16/20 20:17 JMV P010771 Phenanthrene BRL mg/kg dry 0.71 0.0077 1 8270E 9/16/20 20:17 JMV P010771 Phenol BRL mg/kg dry 0.71 0.12 1 8270E 9/16/20 20:17 JMV P010771 Pyrene BRL mg/kg dry 0.71 0.010 1 8270E 9/16/20 20:17 JMV P010771 Pyridine BRL mg/kg dry 0.35 0.067 1 8270E 9/16/20 20:17 JMV P010771 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 98 % 39-132 2-Fluorobiphenyl 77 % 44-115 2-Fluorophenol 76 % 35-115 Nitrobenzene-d5 64 % 37-122 Phenol-d5 74 % 34-121 Terphenyl-d14 81 % 54-127 Total Metals Mercury BRL mg/kg dry 0.053 0.016 1 *7471B 9/21/20 14:39 EDV P010869 Arsenic BRL mg/kg dry 1.1 0.13 1 *601OD 9/17/20 23:01 JAB P010770 Barium BRL mg/kg dry 11 0.96 1 *601OD 9/17/20 23:01 JAB P010770 Cadmium BRL mg/kg dry 0.53 0.050 1 *601OD 9/17/20 23:01 JAB P010770 Chromium 1.4 mg/kg dry 1.1 0.15 1 *6010D 9/17120 23:01 JAB P010770 Lead 1.6 mg/kg dry 1.1 0.13 1 *60101) 9/17/20 23:01 JAB P010770 Selenium BRL mg/kg dry 1.1 0.19 1 *6010D 9/18/20 21:47 JAB P010770 Silver BRL mg/kg dry 0.53 0.051 1 *6010D 9/17/20 23:01 JAB P010770 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 49 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-6S Attn: Tom Proctor Sample ID: 0090162-12 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 16:10 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0046 0.00057 1 8260D 9/16/20 17:51 TBL P010790 1,1,1-Trichloroethane BRL mg/kg dry 0.0046 0.00068 1 8260D 9/16/20 17:51 TBL P010790 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0046 0.00034 1 8260D 9/16/20 17:51 TBL P010790 1,1,2-Trichloroethane BRL mg/kg dry 0.0046 0.00050 1 8260D 9/16/20 17:51 TBL P010790 1,1-Dichloroethane BRL mg/kg dry 0.0046 0.00084 1 8260D 9/16/20 17:51 TBL P010790 1,1-Dichloroethylene BRL mg/kg dry 0.0046 0.00085 1 8260D 9/16/20 17:51 TBL P010790 1,1-Dichloropropylene BRL mg/kg dry 0.0046 0.00071 1 8260D 9/16/20 17:51 TBL P010790 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0093 0.00066 1 8260D 9/16/20 17:51 TBL P010790 1,2,3-Trichloropropane BRL mg/kg dry 0.0046 0.00053 1 8260D 9/16/20 17:51 TBL P010790 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0093 0.00044 1 8260D 9/16/20 17:51 TBL P010790 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0046 0.00049 1 8260D 9/16/20 17:51 TBL P010790 1,2-Dibromoethane BRL mg/kg dry 0.0046 0.00042 1 8260D 9/16/20 17:51 TBL P010790 1,2-Dichlorobenzene BRL mg/kg dry 0.0046 0.00052 1 8260D 9/16/20 17:51 TBL P010790 1,2-Dichloroethane BRL mg/kg dry 0.0046 0.00055 1 8260D 9/16/20 17:51 TBL P010790 1,2-Dichloropropane BRL mg/kg dry 0.0046 0.00070 1 8260D 9/16/20 17:51 TBL P010790 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0046 0.00058 1 8260D 9/16/20 17:51 TBL P010790 1,3-Dichlorobenzene BRL mg/kg dry 0.0046 0.00058 1 8260D 9/16/20 17:51 TBL P010790 1,3-Dichloropropane BRL mg/kg dry 0.0046 0.00039 1 8260D 9/16/20 17:51 TBL P010790 1,4-Dichlorobenzene BRL mg/kg dry 0.0046 0.00059 1 8260D 9/16/20 17:51 TBL P010790 2,2-Dichloropropane BRL mg/kg dry 0.0046 0.00058 1 8260D 9/16/20 17:51 TBL P010790 2-Chlorotoluene BRL mg/kg dry 0.0046 0.00062 1 8260D 9/16/20 17:51 TBL P010790 4-Chlorotoluene BRL mg/kg dry 0.0046 0.00053 1 8260D 9/16/20 17:51 TBL P010790 4-Isopropyltoluene BRL mg/kg dry 0.0046 0.0012 1 8260D 9/16/20 17:51 TBL P010790 Acetone BRL CCVH mg/kg dry 0.019 0.0012 1 8260D 9/16/20 17:51 TBL P010790 Benzene BRL mg/kg dry 0.0046 0.00072 1 8260D 9/16/20 17:51 TBL P010790 Bromobenzene BRL mg/kg dry 0.0046 0.00064 1 8260D 9/16/20 17:51 TBL P010790 Bromochloromethane BRL mg/kg dry 0.0046 0.00076 1 8260D 9/16/20 17:51 TBL P010790 Bromodichloromethane BRL mg/kg dry 0.0046 0.00044 1 8260D 9/16/20 17:51 TBL P010790 Bromoform BRL mg/kg dry 0.0046 0.00036 1 8260D 9/16/20 17:51 TBL P010790 Bromomethane BRL mg/kg dry 0.0093 0.0023 1 8260D 9/16/20 17:51 TBL P010790 Carbon Tetrachloride BRL mg/kg dry 0.0046 0.00091 1 8260D 9/16/20 17:51 TBL P010790 Chlorobenzene BRL mg/kg dry 0.0046 0.00072 1 8260D 9/16/20 17:51 TBL P010790 Chloroethane BRL mg/kg dry 0.0093 0.00088 1 8260D 9/16/20 17:51 TBL P010790 Chloroform BRL mg/kg dry 0.0046 0.00057 1 8260D 9/16/20 17:51 TBL P010790 Chloromethane BRL mg/kg dry 0.0093 0.0014 1 8260D 9/16/20 17:51 TBL P010790 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0046 0.00073 1 8260D 9/16/20 17:51 TBL P010790 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0046 0.00046 1 8260D 9/16/20 17:51 TBL P010790 Dibromochloromethane BRL mg/kg dry 0.0046 0.00031 1 8260D 9/16/20 17:51 TBL P010790 Dichlorodifluoromethane BRL mg/kg dry 0.0093 0.0013 1 8260D 9/16/20 17:51 TBL P010790 Ethylbenzene BRL mg/kg dry 0.0046 0.00070 1 8260D 9/16/20 17:51 TBL P010790 Isopropyl Ether BRL mg/kg dry 0.0046 0.00068 1 8260D 9/16/20 17:51 TBL P010790 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0046 0.00054 1 8260D 9/16/20 17:51 TBL P010790 m,p-Xylenes BRL mg/kg dry 0.0093 0.0012 1 8260D 9/16/20 17:51 TBL P010790 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 50 0f 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-6S Attn: Tom Proctor Sample ID: 0090162-12 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 16:10 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.019 0.00032 1 8260D 9/16/20 17:51 TBL P010790 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.019 0.0011 1 8260D 9/16/20 17:51 TBL P010790 Methyl Isobutyl Ketone BRL mg/kg dry 0.019 0.00038 1 8260D 9/16/20 17:51 TBL P010790 Methylene Chloride 0.0031 J mg/kg dry 0.0046 0.00075 1 8260D 9/16/20 17:51 TBL P010790 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0046 0.00065 1 8260D 9/16/20 17:51 TBL P010790 Naphthalene BRL mg/kg dry 0.0093 0.00047 1 8260D 9/16/20 17:51 TBL P010790 n-Butylbenzene BRL mg/kg dry 0.0046 0.00043 1 8260D 9/16/20 17:51 TBL P010790 n-Propylbenzene BRL mg/kg dry 0.0046 0.00067 1 8260D 9/16/20 17:51 TBL P010790 o-Xylene BRL mg/kg dry 0.0046 0.00049 1 8260D 9/16/20 17:51 TBL P010790 sec-Butylbenzene BRL mg/kg dry 0.0046 0.00050 1 8260D 9/16/20 17:51 TBL P010790 Styrene BRL mg/kg dry 0.0046 0.00045 1 8260D 9/16/20 17:51 TBL P010790 tert-Butylbenzene BRL mg/kg dry 0.0046 0.00055 1 8260D 9/16/20 17:51 TBL P010790 Tetrachloroethylene BRL mg/kg dry 0.0046 0.00084 1 8260D 9/16/20 17:51 TBL P010790 Toluene BRL mg/kg dry 0.0046 0.00074 1 8260D 9/16/20 17:51 TBL P010790 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0046 0.00089 1 8260D 9/16/20 17:51 TBL P010790 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0046 0.00040 1 8260D 9/16/20 17:51 TBL P010790 Trichloroethylene BRL mg/kg dry 0.0046 0.00090 1 8260D 9/16/20 17:51 TBL P010790 Trichlorofluoromethane BRL mg/kg dry 0.0093 0.0013 1 8260D 9/16/20 17:51 TBL P010790 Vinyl acetate BRL mg/kg dry 0.0093 0.00050 1 8260D 9/16/20 17:51 TBL P010790 Vinyl chloride BRL mg/kg dry 0.0093 0.00092 1 8260D 9/16/20 17:51 TBL P010790 Xylenes, total BRL mg/kg dry 0.014 0.0017 1 8260D 9/16/20 17:51 TBL P010790 Surrogate Recovery Control Limits 4-Bromofluorobenzene 103 % 70-130 Dibromofluoromethane 99 % 84-123 Toluene-d8 91 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 51 of 93 Laboratory Report • � 10/13/2020 PA Waynt. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-7S Attn: Tom Proctor Sample ID: 0090162-13 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 17:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters % Solids 76.1 % by 0.100 0.100 1 *SM2540 G 9/17/20 13:00 EDV P010783 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.87 0.15 1 8270E 9/16/20 20:39 JMV P010771 1,2-Dichlorobenzene BRL mg/kg dry 0.87 0.14 1 8270E 9/16/20 20:39 JMV P010771 1,3-Dichlorobenzene BRL mg/kg dry 0.87 0.13 1 8270E 9/16/20 20:39 JMV P010771 1,4-Dichlorobenzene BRL mg/kg dry 0.43 0.14 1 8270E 9/16/20 20:39 JMV P010771 1-Methyl naphthalene BRL mg/kg dry 0.87 0.013 1 8270E 9/16/20 20:39 JMV P010771 2,4,5-Trichlorophenol BRL mg/kg dry 0.87 0.18 1 8270E 9/16/20 20:39 JMV P010771 2,4,6-Trichlorophenol BRL mg/kg dry 0.87 0.21 1 8270E 9/16/20 20:39 JMV P010771 2,4-Dichlorophenol BRL mg/kg dry 0.87 0.17 1 8270E 9/16/20 20:39 JMV P010771 2,4-Dimethylphenol BRL mg/kg dry 0.43 0.18 1 8270E 9/16/20 20:39 JMV P010771 2,4-Dinitrophenol BRL mg/kg dry 2.0 0.51 1 8270E 9/16/20 20:39 JMV P010771 2,4-Dinitrotoluene BRL mg/kg dry 0.87 0.23 1 8270E 9/16/20 20:39 JMV P010771 2,6-Dinitrotoluene BRL mg/kg dry 0.87 0.22 1 8270E 9/16/20 20:39 JMV P010771 2-Chloronaphthalene BRL mg/kg dry 0.87 0.21 1 8270E 9/16/20 20:39 JMV P010771 2-Chlorophenol BRL mg/kg dry 0.87 0.17 1 8270E 9/16/20 20:39 JMV P010771 2-Methyl naphthalene BRL mg/kg dry 0.87 0.017 1 8270E 9/16/20 20:39 JMV P010771 2-Methylphenol BRL mg/kg dry 0.87 0.17 1 8270E 9/16/20 20:39 JMV P010771 2-Nitrophenol BRL mg/kg dry 0.87 0.14 1 8270E 9/16/20 20:39 JMV P010771 3,3'-Dichlorobenzidine BRL mg/kg dry 0.87 0.17 1 8270E 9/16/20 20:39 JMV P010771 3/4-Methyl phenol BRL mg/kg dry 0.87 0.19 1 8270E 9/16/20 20:39 JMV P010771 4,6-Dinitro-2-methylphenol BRL mg/kg dry 2.0 0.48 1 8270E 9/16/20 20:39 JMV P010771 4-Bromophenyl phenyl ether BRL mg/kg dry 0.87 0.20 1 8270E 9/16/20 20:39 JMV P010771 4-Chloro-3-methylphenol BRL mg/kg dry 0.87 0.17 1 8270E 9/16/20 20:39 JMV P010771 4-Chloroaniline BRL mg/kg dry 0.43 0.11 1 8270E 9/16/20 20:39 JMV P010771 4-Chlorophenyl phenyl ether BRL mg/kg dry 1.3 0.27 1 8270E 9/16/20 20:39 JMV P010771 4-Nitrophenol BRL mg/kg dry 0.87 0.21 1 8270E 9/16/20 20:39 JMV P010771 Acenaphthene BRL mg/kg dry 0.87 0.020 1 8270E 9/16/20 20:39 JMV P010771 Acenaphthylene BRL mg/kg dry 0.87 0.017 1 8270E 9/16/20 20:39 JMV P010771 Anthracene BRL mg/kg dry 0.87 0.0096 1 8270E 9/16/20 20:39 JMV P010771 Azobenzene BRL mg/kg dry 0.87 0.19 1 8270E 9/16/20 20:39 JMV P010771 Benzo(a)anthracene BRL mg/kg dry 0.87 0.010 1 8270E 9/16/20 20:39 JMV P010771 Benzo(a)pyrene 0.038 J mg/kg dry 0.87 0.0077 1 8270E 9/16/20 20:39 JMV P010771 Benzo(b)fluoranthene 0.046 J mg/kg dry 0.87 0.0080 1 8270E 9/16/20 20:39 JMV P010771 Benzo(g,hJ)perylene BRL mg/kg dry 0.87 0.0085 1 8270E 9/16/20 20:39 JMV P010771 Benzo(k)fluoranthene BRL mg/kg dry 0.87 0.0092 1 8270E 9/16/20 20:39 JMV P010771 Benzoic Acid BRL mg/kg dry 2.6 0.72 1 8270E 9/16/20 20:39 JMV P010771 Benzyl alcohol BRL mg/kg dry 0.87 0.16 1 8270E 9/16/20 20:39 JMV P010771 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.87 0.17 1 8270E 9/16/20 20:39 JMV P010771 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.87 0.14 1 8270E 9/16/20 20:39 JMV P010771 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.43 0.15 1 8270E 9/16/20 20:39 JMV P010771 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 52 0f 93 Laboratory Report • �. Waynt. 10/13/2020 PA ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-7S Attn: Tom Proctor Sample ID: 0090162-13 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 17:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Bis(2-Ethylhexyl)phthaIate BRL mg/kg dry 0.87 0.20 1 8270E 9/16/20 20:39 JMV P010771 Butyl benzyl phthalate BRL mg/kg dry 0.43 0.15 1 8270E 9/16/20 20:39 JMV P010771 Chrysene BRL mg/kg dry 0.87 0.010 1 8270E 9/16/20 20:39 JMV P010771 Dibenzo(a,h)anthracene BRL mg/kg dry 0.87 0.025 1 8270E 9/16/20 20:39 JMV P010771 Dibenzofuran BRL mg/kg dry 0.87 0.23 1 8270E 9/16/20 20:39 JMV P010771 Diethyl phthalate BRL mg/kg dry 0.87 0.22 1 8270E 9/16/20 20:39 JMV P010771 Dimethyl phthalate BRL mg/kg dry 0.87 0.21 1 8270E 9/16/20 20:39 JMV P010771 Di-n-butyl phthalate BRL mg/kg dry 0.87 0.22 1 8270E 9/16/20 20:39 JMV P010771 Di-n-octyl phthalate BRL mg/kg dry 0.43 0.22 1 8270E 9/16/20 20:39 JMV P010771 Fluoranthene 0.053 J mg/kg dry 0.87 0.0098 1 8270E 9/16/20 20:39 JMV P010771 Fluorene BRL mg/kg dry 0.87 0.015 1 8270E 9/16/20 20:39 JMV P010771 Hexachlorobenzene BRL mg/kg dry 0.87 0.19 1 8270E 9/16/20 20:39 JMV P010771 Hexachlorobutadiene BRL mg/kg dry 0.87 0.20 1 8270E 9/16/20 20:39 JMV P010771 Hexachlorocyclopentadiene BRL mg/kg dry 0.87 0.30 1 8270E 9/16/20 20:39 JMV P010771 Hexachloroethane BRL mg/kg dry 0.87 0.14 1 8270E 9/16/20 20:39 JMV P010771 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.87 0.024 1 8270E 9/16/20 20:39 JMV P010771 Isophorone BRL mg/kg dry 0.87 0.19 1 8270E 9/16/20 20:39 JMV P010771 Naphthalene BRL mg/kg dry 0.87 0.018 1 8270E 9/16/20 20:39 JMV P010771 Nitrobenzene BRL mg/kg dry 0.43 0.18 1 8270E 9/16/20 20:39 JMV P010771 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.87 0.20 1 8270E 9/16/20 20:39 JMV P010771 N-Nitrosodiphenylamine BRL mg/kg dry 0.87 0.24 1 8270E 9/16/20 20:39 JMV P010771 Pentachlorophenol BRL mg/kg dry 1.3 0.55 1 8270E 9/16/20 20:39 JMV P010771 Phenanthrene BRL mg/kg dry 0.87 0.0095 1 8270E 9/16/20 20:39 JMV P010771 Phenol BRL mg/kg dry 0.87 0.14 1 8270E 9/16/20 20:39 JMV P010771 Pyrene 0.047 J mg/kg dry 0.87 0.013 1 8270E 9/16/20 20:39 JMV P010771 Pyridine BRL mg/kg dry 0.43 0.083 1 8270E 9/16/20 20:39 JMV P010771 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 75 % 39-132 2-Fluorobiphenyl 61 % 44-115 2-Fluorophenol 59 % 35-115 Nitrobenzene-d5 50 % 37-122 Phenol-d5 58 % 34-121 Terphenyl-d14 62 % 54-127 Total Metals Hexavalent Chromium BRL mg/kg dry 0.53 0.20 1 7196A 10/13/20 13:15 BMS POJ0158 Mercury BRL mg/kg dry 0.066 0.020 1 *7471B 9/21/20 14:22 EDV P010869 Arsenic BRL mg/kg dry 1.3 0.16 1 *6010D 9/17/20 23:09 JAB P010770 Barium BRL mg/kg dry 13 1.2 1 *6010D 9/17/20 23:09 JAB P010770 Cadmium BRL mg/kg dry 0.66 0.062 1 *601OD 9/17/20 23:09 JAB P010770 Chromium 2.1 mg/kg dry 1.3 0.18 1 *60101) 9/17/20 23:09 JAB P010770 Lead 8.7 mg/kg dry 1.3 0.16 1 *60101) 9/17/20 23:09 JAB P010770 Selenium BRL mg/kg dry 1.3 0.24 1 *6010D 9/18/20 21:55 JAB P010770 Silver BRL mg/kg dry 0.66 0.063 1 *6010D 9/17/20 23:09 JAB P010770 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 53 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-7S Attn: Tom Proctor Sample ID: 0090162-13 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 17:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0055 0.00067 1 8260D 9/16/20 18:21 TBL P010790 1,1,1-Trichloroethane BRL mg/kg dry 0.0055 0.00081 1 8260D 9/16/20 18:21 TBL P010790 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0055 0.00040 1 8260D 9/16/20 18:21 TBL P010790 1,1,2-Trichloroethane BRL mg/kg dry 0.0055 0.00059 1 8260D 9/16/20 18:21 TBL P010790 1,1-Dichloroethane BRL mg/kg dry 0.0055 0.00099 1 8260D 9/16/20 18:21 TBL P010790 1,1-Dichloroethylene BRL mg/kg dry 0.0055 0.0010 1 8260D 9/16/20 18:21 TBL P010790 1,1-Dichloropropylene BRL mg/kg dry 0.0055 0.00085 1 8260D 9/16/20 18:21 TBL P010790 1,2,3-Trichlorobenzene BRL mg/kg dry 0.011 0.00079 1 8260D 9/16/20 18:21 TBL P010790 1,2,3-Trichloropropane BRL mg/kg dry 0.0055 0.00062 1 8260D 9/16/20 18:21 TBL P010790 1,2,4-Trichlorobenzene BRL mg/kg dry 0.011 0.00052 1 8260D 9/16/20 18:21 TBL P010790 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0055 0.00058 1 8260D 9/16/20 18:21 TBL P010790 1,2-Dibromoethane BRL mg/kg dry 0.0055 0.00049 1 8260D 9/16/20 18:21 TBL P010790 1,2-Dichlorobenzene BRL mg/kg dry 0.0055 0.00061 1 8260D 9/16/20 18:21 TBL P010790 1,2-Dichloroethane BRL mg/kg dry 0.0055 0.00065 1 8260D 9/16/20 18:21 TBL P010790 1,2-Dichloropropane BRL mg/kg dry 0.0055 0.00083 1 8260D 9/16/20 18:21 TBL P010790 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0055 0.00069 1 8260D 9/16/20 18:21 TBL P010790 1,3-Dichlorobenzene BRL mg/kg dry 0.0055 0.00068 1 8260D 9/16/20 18:21 TBL P010790 1,3-Dichloropropane BRL mg/kg dry 0.0055 0.00046 1 8260D 9/16/20 18:21 TBL P010790 1,4-Dichlorobenzene BRL mg/kg dry 0.0055 0.00070 1 8260D 9/16/20 18:21 TBL P010790 2,2-Dichloropropane BRL mg/kg dry 0.0055 0.00069 1 8260D 9/16/20 18:21 TBL P010790 2-Chlorotoluene BRL mg/kg dry 0.0055 0.00074 1 8260D 9/16/20 18:21 TBL P010790 4-Chlorotoluene BRL mg/kg dry 0.0055 0.00063 1 8260D 9/16/20 18:21 TBL P010790 4-Isopropyltoluene BRL mg/kg dry 0.0055 0.0014 1 8260D 9/16/20 18:21 TBL P010790 Acetone BRL CCVH mg/kg dry 0.022 0.0014 1 8260D 9/16/20 18:21 TBL P010790 Benzene BRL mg/kg dry 0.0055 0.00086 1 8260D 9/16/20 18:21 TBL P010790 Bromobenzene BRL mg/kg dry 0.0055 0.00076 1 8260D 9/16/20 18:21 TBL P010790 Bromochloromethane BRL mg/kg dry 0.0055 0.00090 1 8260D 9/16/20 18:21 TBL P010790 Bromodichloromethane BRL mg/kg dry 0.0055 0.00052 1 8260D 9/16/20 18:21 TBL P010790 Bromoform BRL mg/kg dry 0.0055 0.00043 1 8260D 9/16/20 18:21 TBL P010790 Bromomethane BRL mg/kg dry 0.011 0.0027 1 8260D 9/16/20 18:21 TBL P010790 Carbon Tetrachloride BRL mg/kg dry 0.0055 0.0011 1 8260D 9/16/20 18:21 TBL P010790 Chlorobenzene BRL mg/kg dry 0.0055 0.00086 1 8260D 9/16/20 18:21 TBL P010790 Chloroethane BRL mg/kg dry 0.011 0.0010 1 8260D 9/16/20 18:21 TBL P010790 Chloroform BRL mg/kg dry 0.0055 0.00067 1 8260D 9/16/20 18:21 TBL P010790 Chloromethane BRL mg/kg dry 0.011 0.0017 1 8260D 9/16/20 18:21 TBL P010790 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0055 0.00086 1 8260D 9/16/20 18:21 TBL P010790 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0055 0.00054 1 8260D 9/16/20 18:21 TBL P010790 Dibromochloromethane BRL mg/kg dry 0.0055 0.00037 1 8260D 9/16/20 18:21 TBL P010790 Dichlorodifluoromethane BRL mg/kg dry 0.011 0.0016 1 8260D 9/16/20 18:21 TBL P010790 Ethylbenzene BRL mg/kg dry 0.0055 0.00083 1 8260D 9/16/20 18:21 TBL P010790 Isopropyl Ether BRL mg/kg dry 0.0055 0.00081 1 8260D 9/16/20 18:21 TBL P010790 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0055 0.00064 1 8260D 9/16/20 18:21 TBL P010790 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 54 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: TW-7S Attn: Tom Proctor Sample ID: 0090162-13 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Solid Time Collected: 09/11/20 17:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID m,p-Xylenes BRL mg/kg dry 0.011 0.0014 1 8260D 9/16/20 18:21 TBL P010790 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.022 0.00038 1 8260D 9/16/20 18:21 TBL P010790 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.022 0.0013 1 8260D 9/16/20 18:21 TBL P010790 Methyl Isobutyl Ketone BRL mg/kg dry 0.022 0.00045 1 8260D 9/16/20 18:21 TBL P010790 Methylene Chloride 0.0035 J mg/kg dry 0.0055 0.00089 1 8260D 9116/20 18:21 TBL P010790 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0055 0.00077 1 8260D 9/16/20 18:21 TBL P010790 Naphthalene BRL mg/kg dry 0.011 0.00056 1 8260D 9/16/20 18:21 TBL P010790 n-Butylbenzene BRL mg/kg dry 0.0055 0.00051 1 8260D 9/16/20 18:21 TBL P010790 n-Propylbenzene BRL mg/kg dry 0.0055 0.00080 1 8260D 9/16/20 18:21 TBL P010790 o-Xylene BRL mg/kg dry 0.0055 0.00059 1 8260D 9/16/20 18:21 TBL P010790 sec-Butylbenzene BRL mg/kg dry 0.0055 0.00059 1 8260D 9/16/20 18:21 TBL P010790 Styrene BRL mg/kg dry 0.0055 0.00053 1 8260D 9/16/20 18:21 TBL P010790 tert-Butylbenzene BRL mg/kg dry 0.0055 0.00065 1 8260D 9/16/20 18:21 TBL P010790 Tetrachloroethylene BRL mg/kg dry 0.0055 0.0010 1 8260D 9/16/20 18:21 TBL P010790 Toluene BRL mg/kg dry 0.0055 0.00088 1 8260D 9/16/20 18:21 TBL P010790 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0055 0.0011 1 8260D 9/16/20 18:21 TBL P010790 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0055 0.00047 1 8260D 9/16/20 18:21 TBL P010790 Trichloroethylene BRL mg/kg dry 0.0055 0.0011 1 8260D 9/16/20 18:21 TBL P010790 Trichlorofluoromethane BRL mg/kg dry 0.011 0.0015 1 8260D 9/16/20 18:21 TBL P010790 Vinyl acetate BRL mg/kg dry 0.011 0.00060 1 8260D 9/16/20 18:21 TBL P010790 Vinyl chloride BRL mg/kg dry 0.011 0.0011 1 8260D 9/16/20 18:21 TBL P010790 Xylenes, total BRL mg/kg dry 0.017 0.0020 1 8260D 9/16/20 18:21 TBL P010790 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 70-130 Dibromofluoromethane 100 % 84-123 Toluene-d8 91 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 55 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: Dupe Attn: Tom Proctor Sample ID: 0090162-14 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 00:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 9/19/20 0:43 JLB P010844 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 9/19/20 0:43 JLB P010844 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 9/19/20 0:43 JLB P010844 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 9/19/20 0:43 JLB P010844 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 9/19/20 0:43 JLB P010844 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 9/19/20 0:43 JLB P010844 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 9/19/20 0:43 JLB P010844 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 9/19/20 0:43 JLB P010844 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 9/19/20 0:43 JLB P010844 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 9/19/20 0:43 JLB P010844 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 9/19/20 0:43 JLB P010844 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 9/19/20 0:43 JLB P010844 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 9/19/20 0:43 JLB P010844 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 9/19/20 0:43 JLB P010844 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 9/19/20 0:43 JLB P010844 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 9/19/20 0:43 JLB P010844 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 9/19/20 0:43 JLB P010844 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 9/19/20 0:43 JLB P010844 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 9/19/20 0:43 JLB P010844 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 9/19/20 0:43 JLB P010844 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 9/19/20 0:43 JLB P010844 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 9/19/20 0:43 JLB P010844 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 9/19/20 0:43 JLB P010844 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 9/19/20 0:43 JLB P010844 Acetone BRL ug/L 5.0 0.31 1 8260D 9/19/20 0:43 JLB P010844 Acrolein BRL ug/L 20 0.20 1 8260D 9/19/20 0:43 JLB P010844 Acrylonitrile BRL ug/L 20 0.20 1 8260D 9/19/20 0:43 JLB P010844 Benzene BRL ug/L 0.50 0.048 1 8260D 9/19/20 0:43 JLB P010844 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 9/19/20 0:43 JLB P010844 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 9/19/20 0:43 JLB P010844 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 9/19/20 0:43 JLB P010844 Bromoform BRL ug/L 1.0 0.040 1 8260D 9/19/20 0:43 JLB P010844 Bromomethane BRL ug/L 1.0 0.18 1 8260D 9/19/20 0:43 JLB P010844 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 9/19/20 0:43 JLB P010844 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 9/19/20 0:43 JLB P010844 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 9/19/20 0:43 JLB P010844 Chloroethane BRL ug/L 0.50 0.22 1 8260D 9/19/20 0:43 JLB P010844 Chloroform BRL ug/L 0.50 0.076 1 8260D 9/19/20 0:43 JLB P010844 Chloromethane BRL ug/L 0.50 0.079 1 8260D 9/19/20 0:43 JLB P010844 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 9/19/20 0:43 JLB P010844 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 9/19/20 0:43 JLB P010844 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 9/19/20 0:43 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 56 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: Dupe Attn: Tom Proctor Sample ID: 0090162-14 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 00:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Dibromomethane BRL ug/L 0.50 0.065 1 8260D 9/19/20 0:43 JLB P010844 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 9/19/20 0:43 JLB P010844 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 9/19/20 0:43 JLB P010844 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 9/19/20 0:43 JLB P010844 Isopropyl Ether BRL ug/L 5.0 0.96 1 8260D 9/19/20 0:43 JLB P010844 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 9/19/20 0:43 JLB P010844 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 9/19/20 0:43 JLB P010844 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 9/19/20 0:43 JLB P010844 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260D 9/19/20 0:43 JLB P010844 Methyl Isobutyl Ketone BRL ug/L 5.0 1.0 1 8260D 9/19/20 0:43 JLB P010844 Methylene Chloride BRL ug/L 1.0 0.083 1 8260D 9/19/20 0:43 JLB P010844 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 9/19/20 0:43 JLB P010844 Naphthalene BRL ug/L 1.0 0.30 1 8260D 9/19/20 0:43 JLB P010844 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 9/19/20 0:43 JLB P010844 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 9/19/20 0:43 JLB P010844 o-Xylene BRL ug/L 0.50 0.044 1 8260D 9/19/20 0:43 JLB P010844 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 9/19/20 0:43 JLB P010844 Styrene BRL ug/L 0.50 0.047 1 8260D 9/19/20 0:43 JLB P010844 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 9/19/20 0:43 JLB P010844 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260D 9/19/20 0:43 JLB P010844 Toluene BRL ug/L 0.50 0.044 1 8260D 9/19/20 0:43 JLB P010844 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 9/19/20 0:43 JLB P010844 trans- 1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 9/19/20 0:43 JLB P010844 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 9/19/20 0:43 JLB P010844 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 9/19/20 0:43 JLB P010844 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 9/19/20 0:43 JLB P010844 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 9/19/20 0:43 JLB P010844 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 9/19/20 0:43 JLB P010844 Surrogate Recovery Control Limits 4-Bromofluorobenzene 104 % 80-124 Dibromofluoromethane 105 % 75-129 Toluene-d8 96 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 57 of 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: Trip Blank Attn: Tom Proctor Sample ID: 0090162-15 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 00:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 9/18/20 19:10 JLB P010844 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 9/18/20 19:10 JLB P010844 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 9/18/20 19:10 JLB P010844 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 19:10 JLB P010844 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 9/18/20 19:10 JLB P010844 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 9/18/20 19:10 JLB P010844 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 9/18/20 19:10 JLB P010844 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 9/18/20 19:10 JLB P010844 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 9/18/20 19:10 JLB P010844 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 9/18/20 19:10 JLB P010844 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 19:10 JLB P010844 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 9/18/20 19:10 JLB P010844 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 9/18/20 19:10 JLB P010844 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 19:10 JLB P010844 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 9/18/20 19:10 JLB P010844 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 9/18/20 19:10 JLB P010844 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 19:10 JLB P010844 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 9/18/20 19:10 JLB P010844 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 9/18/20 19:10 JLB P010844 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 9/18/20 19:10 JLB P010844 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 9/18/20 19:10 JLB P010844 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 9/18/20 19:10 JLB P010844 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 9/18/20 19:10 JLB P010844 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 9/18/20 19:10 JLB P010844 Acetone BRL ug/L 5.0 0.31 1 8260D 9/18/20 19:10 JLB P010844 Acrolein BRL ug/L 20 0.20 1 8260D 9/18/20 19:10 JLB P010844 Acrylonitrile BRL ug/L 20 0.20 1 8260D 9/18/20 19:10 JLB P010844 Benzene BRL ug/L 0.50 0.048 1 8260D 9/18/20 19:10 JLB P010844 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 9/18/20 19:10 JLB P010844 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 9/18/20 19:10 JLB P010844 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 19:10 JLB P010844 Bromoform BRL ug/L 1.0 0.040 1 8260D 9/18/20 19:10 JLB P010844 Bromomethane BRL ug/L 1.0 0.18 1 8260D 9/18/20 19:10 JLB P010844 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 9/18/20 19:10 JLB P010844 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 9/18/20 19:10 JLB P010844 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 9/18/20 19:10 JLB P010844 Chloroethane BRL ug/L 0.50 0.22 1 8260D 9/18/20 19:10 JLB P010844 Chloroform BRL ug/L 0.50 0.076 1 8260D 9/18/20 19:10 JLB P010844 Chloromethane BRL ug/L 0.50 0.079 1 8260D 9/18/20 19:10 JLB P010844 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 9/18/20 19:10 JLB P010844 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 9/18/20 19:10 JLB P010844 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 9/18/20 19:10 JLB P010844 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 58 0f 93 Laboratory Report S A i • .0 10/13/2020 - -ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Client Sample ID: Trip Blank Attn: Tom Proctor Sample ID: 0090162-15 5113 Yachtsman Ct. Work Order: 0090162 Raleigh, NC 27615 Sample Matrix: Water Time Collected: 09/11/20 00:00 Time Submitted: 09/15/20 12:00 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Dibromomethane BRL ug/L 0.50 0.065 1 8260D 9/18/20 19:10 JLB P010844 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 9/18/20 19:10 JLB P010844 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 9/18/20 19:10 JLB P010844 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 9/18/20 19:10 JLB P010844 Isopropyl Ether BRL ug/L 5.0 0.96 1 8260D 9/18/20 19:10 JLB P010844 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 9/18/20 19:10 JLB P010844 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 9/18/20 19:10 JLB P010844 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 9/18/20 19:10 JLB P010844 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260D 9/18/20 19:10 JLB P010844 Methyl Isobutyl Ketone BRL ug/L 5.0 1.0 1 8260D 9/18/20 19:10 JLB P010844 Methylene Chloride BRL ug/L 1.0 0.083 1 8260D 9/18/20 19:10 JLB P010844 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 9/18/20 19:10 JLB P010844 Naphthalene BRL ug/L 1.0 0.30 1 8260D 9/18/20 19:10 JLB P010844 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 9/18/20 19:10 JLB P010844 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 9/18/20 19:10 JLB P010844 o-Xylene BRL ug/L 0.50 0.044 1 8260D 9/18/20 19:10 JLB P010844 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 9/18/20 19:10 JLB P010844 Styrene BRL ug/L 0.50 0.047 1 8260D 9/18/20 19:10 JLB P010844 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 9/18/20 19:10 JLB P010844 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260D 9/18/20 19:10 JLB P010844 Toluene BRL ug/L 0.50 0.044 1 8260D 9/18/20 19:10 JLB P010844 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 9/18/20 19:10 JLB P010844 trans- 1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 9/18/20 19:10 JLB P010844 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 9/18/20 19:10 JLB P010844 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 9/18/20 19:10 JLB P010844 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 9/18/20 19:10 JLB P010844 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 9/18/20 19:10 JLB P010844 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 9/18/20 19:10 JLB P010844 Surrogate Recovery Control Limits 4-Bromofluorobenzene 103 % 80-124 Dibromofluoromethane 93 % 75-129 Toluene-d8 101 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 59 of 93 Waypo�nt ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P010790 - 5035 Reporting Result Limit Units Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (12010790-131-K1) Prepared & Analyzed: 09/16/20 1,1,1,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.010 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.010 mg/kg wet 1,2,4-Trimethyl benzene BRL 0.0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethyl benzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone 0.00205 0.020 mg/kg wet J Benzene BRL 0.0050 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.010 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.010 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.020 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.020 mg/kg wet Methyl Isobutyl Ketone BRL 0.020 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 60 of 93 Waypoint ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010790 - 5035 Blank (P010790-BLK1) Prepared & Analyzed: 09/16/20 Methylene Chloride 0.00218 0.0050 mg/kg wet Methyl-tert-Butyl Ether BRL 0.0050 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butyl benzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans- 1,2-Dichloroethylene BRL 0.0050 mg/kg wet trans- 1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichloroethylene BRL 0.0050 mg/kg wet Trichlorofluoromethane BRL 0.010 mg/kg wet Vinyl acetate BRL 0.010 mg/kg wet Vinyl chloride BRL 0.010 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate:4-Bromofluorobenzene 50.9 ug/L 50.00 102 70-130 Surrogate: Dibromofluoromethane 49.4 ug/L 50.00 99 84-123 Surrogate: Toluene-d8 46.2 ug/L 50.00 92 76-129 LCS (P010790-BSI) Prepared &Analyzed: 09/16/20 1,1,1,2-Tetrachloroethane 0.0481 0.0050 mg/kg wet 0.05000 96 72-115 1,1,1-Trichloroethane 0.0495 0.0050 mg/kg wet 0.05000 99 67-131 1,1,2,2-Tetrachloroethane 0.0504 0.0050 mg/kg wet 0.05000 101 56-126 1,1,2-Trichloroethane 0.0474 0.0050 mg/kg wet 0.05000 95 70-133 1,1-Dichloroethane 0.0498 0.0050 mg/kg wet 0.05000 100 74-127 1,1-Dichloroethylene 0.0493 0.0050 mg/kg wet 0.05000 99 67-149 1, 1 -Dichloropropylene 0.0487 0.0050 mg/kg wet 0.05000 97 71-130 1,2,3-Trichlorobenzene 0.0464 0.010 mg/kg wet 0.05000 93 68-130 1,2,3-Trichloropropane 0.0492 0.0050 mg/kg wet 0.05000 98 60-137 1,2,4-Trichlorobenzene 0.0462 0.010 mg/kg wet 0.05000 92 66-125 1,2,4-Trimethylbenzene 0.0453 0.0050 mg/kg wet 0.05000 91 69-129 1,2-Dibromoethane 0.0495 0.0050 mg/kg wet 0.05000 99 70-132 1,2-Dichlorobenzene 0.0447 0.0050 mg/kg wet 0.05000 89 72-123 1,2-Dichloroethane 0.0500 0.0050 mg/kg wet 0.05000 100 68-128 1,2-Dichloropropane 0.0501 0.0050 mg/kg wet 0.05000 100 73-130 1,3,5-Trimethylbenzene 0.0441 0.0050 mg/kg wet 0.05000 88 69-128 1,3-Dichlorobenzene 0.0445 0.0050 mg/kg wet 0.05000 89 71-120 1,3-Dichloropropane 0.0470 0.0050 mg/kg wet 0.05000 94 75-124 1,4-Dichlorobenzene 0.0449 0.0050 mg/kg wet 0.05000 90 71-123 2,2-Dichloropropane 0.0530 0.0050 mg/kg wet 0.05000 106 50-142 2-Chlorotoluene 0.0443 0.0050 mg/kg wet 0.05000 89 67-124 4-Chlorotoluene 0.0443 0.0050 mg/kg wet 0.05000 89 71-126 4-Isopropyltoluene 0.0454 0.0050 mg/kg wet 0.05000 91 68-129 Acetone 0.146 0.020 mg/kg wet 0.1000 146 29-198 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 61 0 93 Waypoint ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P010790 - 5035 Reporting Result Limit Units Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P010790-BS1) Prepared &Analyzed: 09/16/20 Benzene 0.0496 0.0050 mg/kg wet 0.05000 99 74-127 Bromobenzene 0.0438 0.0050 mg/kg wet 0.05000 88 73-125 Bromochloromethane 0.0524 0.0050 mg/kg wet 0.05000 105 72-134 Bromodichloromethane 0.0504 0.0050 mg/kg wet 0.05000 101 75-122 Bromoform 0.0465 0.0050 mg/kg wet 0.05000 93 66-135 Bromomethane 0.0393 0.010 mg/kg wet 0.05000 79 20-180 Carbon Tetrachloride 0.0525 0.0050 mg/kg wet 0.05000 105 64-143 Chlorobenzene 0.0455 0.0050 mg/kg wet 0.05000 91 74-118 Chloroethane 0.0242 0.010 mg/kg wet 0.05000 48 33-149 Chloroform 0.0487 0.0050 mg/kg wet 0.05000 97 73-127 Chloromethane 0.0401 0.010 mg/kg wet 0.05000 80 45-143 cis-1,2-Dichloroethylene 0.0497 0.0050 mg/kg wet 0.05000 99 76-134 cis-1,3-Dichloropropylene 0.0522 0.0050 mg/kg wet 0.05000 104 71-125 Dibromochloromethane 0.0492 0.0050 mg/kg wet 0.05000 98 73-122 Dichlorodifluoromethane 0.0306 0.010 mg/kg wet 0.05000 61 26-146 Ethylbenzene 0.0454 0.0050 mg/kg wet 0.05000 91 74-128 Isopropyl Ether 0.0499 0.0050 mg/kg wet 0.05000 100 59-159 Isopropylbenzene (Cumene) 0.0441 0.0050 mg/kg wet 0.05000 88 68-126 m,p-Xylenes 0.0931 0.010 mg/kg wet 0.1000 93 75-124 Methyl Butyl Ketone (2-Hexanone) 0.0671 0.020 mg/kg wet 0.05000 134 61-157 Methyl Ethyl Ketone (2-Butanone) 0.0727 0.020 mg/kg wet 0.05000 145 63-149 Methyl Isobutyl Ketone 0.0647 0.020 mg/kg wet 0.05000 129 57-162 Methylene Chloride 0.0556 0.0050 mg/kg wet 0.05000 ill 74-129 Methyl-tert-Butyl Ether 0.0520 0.0050 mg/kg wet 0.05000 104 70-130 Naphthalene 0.0482 0.010 mg/kg wet 0.05000 96 57-157 n-Butylbenzene 0.0459 0.0050 mg/kg wet 0.05000 92 65-135 n-Propylbenzene 0.0442 0.0050 mg/kg wet 0.05000 88 67-130 o-Xylene 0.0463 0.0050 mg/kg wet 0.05000 93 74-126 sec-Butylbenzene 0.0441 0.0050 mg/kg wet 0.05000 88 66-131 Styrene 0.0487 0.0050 mg/kg wet 0.05000 97 77-121 tert-Butyl benzene 0.0446 0.0050 mg/kg wet 0.05000 89 67-132 Tetrachloroethylene 0.0495 0.0050 mg/kg wet 0.05000 99 68-130 Toluene 0.0496 0.0050 mg/kg wet 0.05000 99 71-129 trans- 1,2-Dichloroethylene 0.0498 0.0050 mg/kg wet 0.05000 100 73-132 trans- 1,3-Dichloropropylene 0.0554 0.0050 mg/kg wet 0.05000 ill 68-123 Trichloroethylene 0.0496 0.0050 mg/kg wet 0.05000 99 75-133 Trichlorofluoromethane 0.0420 0.010 mg/kg wet 0.05000 84 44-146 Vinyl acetate 0.0568 0.010 mg/kg wet 0.05000 114 85-161 Vinyl chloride 0.0424 0.010 mg/kg wet 0.05000 85 48-147 Xylenes, total 0.139 0.015 mg/kg wet 0.1500 93 74-126 Surrogate:4-Bromofluorobenzene 49.6 ug/L 50.00 99 70-130 Surrogate: Dibromofluoromethane 48.1 ug/L 50.00 96 84-123 Surrogate: Toluene-d8 45.5 ug/L 50.00 91 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 62 0 93 Waypoint ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010790 - 5035 Matrix Spike (P010790-MS1) Source: 0090162-08 Prepared &Analyzed: 09/16/20 1,1,1,2-Tetrachloroethane 0.0526 0.0057 mg/kg dry 0.05670 BRL 93 60-120 1,1,1-Trichloroethane 0.0582 0.0057 mg/kg dry 0.05670 BRL 103 52-139 1,1,2,2-Tetrachloroethane 0.0440 0.0057 mg/kg dry 0.05670 BRL 78 39-135 1,1,2-Trichloroethane 0.0474 0.0057 mg/kg dry 0.05670 BRL 84 44-140 1,1-Dichloroethane 0.0553 0.0057 mg/kg dry 0.05670 BRL 98 59-137 1,1-Dichloroethylene 0.0566 0.0057 mg/kg dry 0.05670 BRL 100 54-162 1, 1 -Dichloropropylene 0.0538 0.0057 mg/kg dry 0.05670 BRL 95 55-137 1,2,3-Trichlorobenzene 0.0345 0.011 mg/kg dry 0.05670 BRL 61 34-120 1,2,3-Trichloropropane 0.0419 0.0057 mg/kg dry 0.05670 BRL 74 45-139 1,2,4-Trichlorobenzene 0.0349 0.011 mg/kg dry 0.05670 BRL 62 35-116 1,2,4-Trimethylbenzene 0.0453 0.0057 mg/kg dry 0.05670 BRL 80 38-142 1,2-Dibromoethane 0.0475 0.0057 mg/kg dry 0.05670 BRL 84 49-132 1,2-Dichlorobenzene 0.0427 0.0057 mg/kg dry 0.05670 BRL 75 42-130 1,2-Dichloroethane 0.0527 0.0057 mg/kg dry 0.05670 BRL 93 51-131 1,2-Dichloropropane 0.0551 0.0057 mg/kg dry 0.05670 BRL 97 55-138 1,3,5-Trimethylbenzene 0.0467 0.0057 mg/kg dry 0.05670 BRL 82 44-140 1,3-Dichlorobenzene 0.0421 0.0057 mg/kg dry 0.05670 BRL 74 41-129 1,3-Dichloropropane 0.0481 0.0057 mg/kg dry 0.05670 BRL 85 53-129 1,4-Dichlorobenzene 0.0416 0.0057 mg/kg dry 0.05670 BRL 73 44-134 2,2-Dichloropropane 0.0566 0.0057 mg/kg dry 0.05670 BRL 100 30-147 2-Chlorotoluene 0.0439 0.0057 mg/kg dry 0.05670 BRL 77 46-132 4-Chlorotoluene 0.0438 0.0057 mg/kg dry 0.05670 BRL 77 44-135 4-Isopropyltoluene 0.0451 0.0057 mg/kg dry 0.05670 BRL 80 32-144 Acetone 0.0733 0.023 mg/kg dry 0.1134 BRL 65 34-143 Benzene 0.0546 0.0057 mg/kg dry 0.05670 BRL 96 60-135 Bromobenzene 0.0446 0.0057 mg/kg dry 0.05670 BRL 79 45-135 Bromochloromethane 0.0545 0.0057 mg/kg dry 0.05670 BRL 96 55-136 Bromodichloromethane 0.0553 0.0057 mg/kg dry 0.05670 BRL 98 55-127 Bromoform 0.0445 0.0057 mg/kg dry 0.05670 BRL 78 40-136 Bromomethane 0.0273 0.011 mg/kg dry 0.05670 BRL 48 30-137 Carbon Tetrachloride 0.0622 0.0057 mg/kg dry 0.05670 BRL 110 48-153 Chlorobenzene 0.0479 0.0057 mg/kg dry 0.05670 BRL 84 57-125 Chloroethane 0.0237 0.011 mg/kg dry 0.05670 BRL 42 16-177 Chloroform 0.0545 0.0057 mg/kg dry 0.05670 BRL 96 56-137 Chloromethane 0.00485 0.011 mg/kg dry 0.05670 BRL 9 40-145 M, J cis-1,2-Dichloroethylene 0.0543 0.0057 mg/kg dry 0.05670 BRL 96 58-140 cis-1,3-Dichloropropylene 0.0521 0.0057 mg/kg dry 0.05670 BRL 92 42-135 Dibromochloromethane 0.0513 0.0057 mg/kg dry 0.05670 BRL 90 49-127 Dichlorodifluoromethane BRL 0.011 mg/kg dry 0.05670 BRL 25-151 M Ethylbenzene 0.0493 0.0057 mg/kg dry 0.05670 BRL 87 44-144 Isopropyl Ether 0.0524 0.0057 mg/kg dry 0.05670 BRL 92 51-155 Isopropylbenzene (Cumene) 0.0467 0.0057 mg/kg dry 0.05670 BRL 82 41-140 m,p-Xylenes 0.100 0.011 mg/kg dry 0.1134 BRL 88 36-148 Methyl Butyl Ketone (2-Hexanone) 0.0405 0.023 mg/kg dry 0.05670 BRL 71 30-147 Methyl Ethyl Ketone (2-Butanone) 0.0423 0.023 mg/kg dry 0.05670 BRL 75 24-160 Methyl Isobutyl Ketone 0.0487 0.023 mg/kg dry 0.05670 BRL 86 25-163 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 63 0 93 Waypoint ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010790 - 5035 Matrix Spike (P010790-MS1) Source: 0090162-08 Prepared &Analyzed: 09/16/20 Methylene Chloride 0.0583 0.0057 mg/kg dry 0.05670 0.00522 94 53-144 Methyl-tert-Butyl Ether 0.0494 0.0057 mg/kg dry 0.05670 BRL 87 49-135 Naphthalene 0.0349 0.011 mg/kg dry 0.05670 BRL 62 32-127 n-Butylbenzene 0.0417 0.0057 mg/kg dry 0.05670 BRL 73 23-148 n-Propylbenzene 0.0455 0.0057 mg/kg dry 0.05670 BRL 80 35-144 o-Xylene 0.0498 0.0057 mg/kg dry 0.05670 BRL 88 43-143 sec-Butylbenzene 0.0443 0.0057 mg/kg dry 0.05670 BRL 78 34-144 Styrene 0.0502 0.0057 mg/kg dry 0.05670 BRL 88 42-132 tert-Butyl benzene 0.0462 0.0057 mg/kg dry 0.05670 BRL 81 36-150 Tetrachloroethylene 0.0534 0.0057 mg/kg dry 0.05670 BRL 94 47-142 Toluene 0.0549 0.0057 mg/kg dry 0.05670 BRL 97 57-135 trans- 1,2-Dichloroethylene 0.0534 0.0057 mg/kg dry 0.05670 BRL 94 58-141 trans- 1,3-Dichloropropylene 0.0512 0.0057 mg/kg dry 0.05670 BRL 90 41-124 Trichloroethylene 0.0525 0.0057 mg/kg dry 0.05670 BRL 93 38-164 Trichlorofluoromethane 0.0275 0.011 mg/kg dry 0.05670 BRL 49 30-157 Vinyl acetate 0.00679 0.011 mg/kg dry 0.05670 BRL 12 61-154 M, J Vinyl chloride 0.00796 0.011 mg/kg dry 0.05670 BRL 14 40-156 M, J Xylenes, total 0.150 0.017 mg/kg dry 0.1701 BRL 88 36-148 Surrogate:4-Bromofluorobenzene 49.0 ug/L 50.00 98 70-130 Surrogate: Dibromofluoromethane 49.0 ug/L 50.00 98 84-123 Surrogate: Toluene-d8 46.2 ug/L 50.00 92 76-129 Matrix Spike Dup (P010790-MSD1) Source: 0090162-08 Prepared & Analyzed: 09/16/20 1,1,1,2-Tetrachloroethane 0.0512 0.0057 mg/kg dry 0.05670 BRL 90 60-120 3 15 1,1,1-Trichloroethane 0.0557 0.0057 mg/kg dry 0.05670 BRL 98 52-139 4 21 1,1,2,2-Tetrachloroethane 0.0440 0.0057 mg/kg dry 0.05670 BRL 78 39-135 0.08 22 1,1,2-Trichloroethane 0.0480 0.0057 mg/kg dry 0.05670 BRL 85 44-140 1 21 1,1-Dichloroethane 0.0537 0.0057 mg/kg dry 0.05670 BRL 95 59-137 3 21 1,1-Dichloroethylene 0.0527 0.0057 mg/kg dry 0.05670 BRL 93 54-162 7 22 1, 1 -Dichloropropylene 0.0508 0.0057 mg/kg dry 0.05670 BRL 90 55-137 6 19 1,2,3-Trichlorobenzene 0.0335 0.011 mg/kg dry 0.05670 BRL 59 34-120 3 41 1,2,3-Trichloropropane 0.0423 0.0057 mg/kg dry 0.05670 BRL 75 45-139 0.8 25 1,2,4-Trichlorobenzene 0.0332 0.011 mg/kg dry 0.05670 BRL 59 35-116 5 62 1,2,4-Trimethylbenzene 0.0435 0.0057 mg/kg dry 0.05670 BRL 77 38-142 4 24 1,2-Dibromoethane 0.0465 0.0057 mg/kg dry 0.05670 BRL 82 49-132 2 15 1,2-Dichlorobenzene 0.0416 0.0057 mg/kg dry 0.05670 BRL 73 42-130 3 21 1,2-Dichloroethane 0.0514 0.0057 mg/kg dry 0.05670 BRL 91 51-131 2 13 1,2-Dichloropropane 0.0528 0.0057 mg/kg dry 0.05670 BRL 93 55-138 4 16 1,3,5-Trimethylbenzene 0.0448 0.0057 mg/kg dry 0.05670 BRL 79 44-140 4 29 1,3-Dichlorobenzene 0.0405 0.0057 mg/kg dry 0.05670 BRL 71 41-129 4 24 1,3-Dichloropropane 0.0472 0.0057 mg/kg dry 0.05670 BRL 83 53-129 2 15 1,4-Dichlorobenzene 0.0400 0.0057 mg/kg dry 0.05670 BRL 71 44-134 4 21 2,2-Dichloropropane 0.0547 0.0057 mg/kg dry 0.05670 BRL 96 30-147 4 20 2-Chlorotoluene 0.0420 0.0057 mg/kg dry 0.05670 BRL 74 46-132 4 29 4-Chlorotoluene 0.0420 0.0057 mg/kg dry 0.05670 BRL 74 44-135 4 23 4-Isopropyltoluene 0.0426 0.0057 mg/kg dry 0.05670 BRL 75 32-144 6 22 Acetone 0.0751 0.023 mg/kg dry 0.1134 BRL 66 34-143 2 49 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 64 0 93 Waypoint ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010790 - 5035 Matrix Spike Dup (P010790-MSD1) Source: 0090162-08 Prepared &Analyzed: 09/16/20 Benzene 0.0529 0.0057 mg/kg dry 0.05670 BRL 93 60-135 3 20 Bromobenzene 0.0427 0.0057 mg/kg dry 0.05670 BRL 75 45-135 4 25 Bromochloromethane 0.0533 0.0057 mg/kg dry 0.05670 BRL 94 55-136 2 18 Bromodichloromethane 0.0543 0.0057 mg/kg dry 0.05670 BRL 96 55-127 2 17 Bromoform 0.0448 0.0057 mg/kg dry 0.05670 BRL 79 40-136 0.6 35 Bromomethane 0.0218 0.011 mg/kg dry 0.05670 BRL 38 30-137 22 30 Carbon Tetrachloride 0.0570 0.0057 mg/kg dry 0.05670 BRL 100 48-153 9 23 Chlorobenzene 0.0463 0.0057 mg/kg dry 0.05670 BRL 82 57-125 3 14 Chloroethane 0.0218 0.011 mg/kg dry 0.05670 BRL 38 16-177 9 47 Chloroform 0.0531 0.0057 mg/kg dry 0.05670 BRL 94 56-137 2 18 Chloromethane 0.00493 0.011 mg/kg dry 0.05670 BRL 9 40-145 2 26 M, J cis-1,2-Dichloroethylene 0.0523 0.0057 mg/kg dry 0.05670 BRL 92 58-140 4 28 cis-1,3-Dichloropropylene 0.0515 0.0057 mg/kg dry 0.05670 BRL 91 42-135 1 32 Dibromochloromethane 0.0511 0.0057 mg/kg dry 0.05670 BRL 90 49-127 0.3 24 Dichlorodifluoromethane BRL 0.011 mg/kg dry 0.05670 BRL 25-151 37 M Ethylbenzene 0.0469 0.0057 mg/kg dry 0.05670 BRL 83 44-144 5 19 Isopropyl Ether 0.0513 0.0057 mg/kg dry 0.05670 BRL 90 51-155 2 13 Isopropylbenzene (Cumene) 0.0448 0.0057 mg/kg dry 0.05670 BRL 79 41-140 4 27 m,p-Xylenes 0.0953 0.011 mg/kg dry 0.1134 BRL 84 36-148 5 20 Methyl Butyl Ketone (2-Hexanone) 0.0409 0.023 mg/kg dry 0.05670 BRL 72 30-147 1 42 Methyl Ethyl Ketone (2-Butanone) 0.0428 0.023 mg/kg dry 0.05670 BRL 76 24-160 1 42 Methyl Isobutyl Ketone 0.0483 0.023 mg/kg dry 0.05670 BRL 85 25-163 1 44 Methylene Chloride 0.0568 0.0057 mg/kg dry 0.05670 0.00522 91 53-144 3 14 Methyl-tert-Butyl Ether 0.0489 0.0057 mg/kg dry 0.05670 BRL 86 49-135 0.9 22 Naphthalene 0.0343 0.011 mg/kg dry 0.05670 BRL 60 32-127 2 44 n-Butylbenzene 0.0390 0.0057 mg/kg dry 0.05670 BRL 69 23-148 7 39 n-Propylbenzene 0.0431 0.0057 mg/kg dry 0.05670 BRL 76 35-144 5 27 o-Xylene 0.0477 0.0057 mg/kg dry 0.05670 BRL 84 43-143 4 17 sec-Butylbenzene 0.0425 0.0057 mg/kg dry 0.05670 BRL 75 34-144 4 28 Styrene 0.0479 0.0057 mg/kg dry 0.05670 BRL 84 42-132 5 28 tert-Butyl benzene 0.0444 0.0057 mg/kg dry 0.05670 BRL 78 36-150 4 29 Tetrachloroethylene 0.0508 0.0057 mg/kg dry 0.05670 BRL 90 47-142 5 26 Toluene 0.0523 0.0057 mg/kg dry 0.05670 BRL 92 57-135 5 22 trans- 1,2-Dichloroethylene 0.0509 0.0057 mg/kg dry 0.05670 BRL 90 58-141 5 18 trans- 1,3-Dichloropropylene 0.0514 0.0057 mg/kg dry 0.05670 BRL 91 41-124 0.5 20 Trichloroethylene 0.0503 0.0057 mg/kg dry 0.05670 BRL 89 38-164 4 18 Trichlorofluoromethane 0.0257 0.011 mg/kg dry 0.05670 BRL 45 30-157 7 27 Vinyl acetate 0.00565 0.011 mg/kg dry 0.05670 BRL 10 61-154 18 35 M, J Vinyl chloride 0.00759 0.011 mg/kg dry 0.05670 BRL 13 40-156 5 35 M, J Xylenes, total 0.143 0.017 mg/kg dry 0.1701 BRL 84 36-148 5 20 Surrogate:4-Bromofluorobenzene 48.6 ug/L 50.00 97 70-130 Surrogate: Dibromofluoromethane 48.1 ug/L 50.00 96 84-123 Surrogate: Toluene-d8 45.6 ug/L 50.00 91 76-129 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 65 0 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010844 - 5030B Blank (P010844-BLK1) 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethylene 1,1-Dichloropropylene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethyl benzene 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethyl benzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Chlorotoluene 4-Chlorotoluene 4-Isopropyltoluene Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethylene cis-1,3-Dichloropropylene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Ethylbenzene Hexachlorobutadiene Prepared & Analyzed: 09/18/20 BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 2.0 ug/L BRL 1.0 ug/L BRL 1.0 ug/L BRL 0.50 ug/L BRL 2.0 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 2.0 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L 1.16 5.0 ug/L BRL 20 ug/L BRL 20 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 1.0 ug/L BRL 1.0 ug/L BRL 5.0 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 5.0 ug/L BRL 0.50 ug/L BRL 2.0 ug/L J This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 66 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010844 - 5030B Blank (P010844-BLK1) Prepared & Analyzed: 09/18/20 Isopropyl Ether BRL 5.0 ug/L Isopropylbenzene (Cumene) BRL 0.50 ug/L m,p-Xylenes BRL 1.0 ug/L Methyl Butyl Ketone (2-Hexanone) BRL 5.0 ug/L Methyl Ethyl Ketone (2-Butanone) BRL 5.0 ug/L Methyl Isobutyl Ketone BRL 5.0 ug/L Methylene Chloride BRL 1.0 ug/L Methyl-tert-Butyl Ether BRL 0.50 ug/L Naphthalene 0.370 1.0 ug/L n-Butylbenzene BRL 1.0 ug/L n-Propylbenzene BRL 0.50 ug/L o-Xylene BRL 0.50 ug/L sec-Butylbenzene BRL 0.50 ug/L Styrene BRL 0.50 ug/L tert-Butylbenzene BRL 0.50 ug/L Tetrachloroethylene BRL 0.50 ug/L Toluene BRL 0.50 ug/L trans-1,2-Dichloroethylene BRL 0.50 ug/L trans-1,3-Dichloropropylene BRL 0.50 ug/L Trichloroethylene BRL 0.50 ug/L Trichlorofluoromethane BRL 0.50 ug/L Vinyl acetate BRL 2.0 ug/L Vinyl chloride BRL 0.50 ug/L Xylenes, total BRL 1.5 ug/L Heptane 0.00 ug/L Surrogate:4-Bromofluorobenzene 50.5 ug/L 50.00 101 80-124 Surrogate: Dibromofluoromethane 51.1 ug/L 50.00 102 75-129 Surrogate: Toluene-d8 54.0 ug/L 50.00 108 77-123 J This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 67 of 93 Waypoint ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P010844 - 5030B Reporting Result Limit Units Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P010844-BS1) Prepared & Analyzed: 09/18/20 1,1,1,2-Tetrachloroethane 20.0 0.50 ug/L 20.00 100 79-134 1,1,1-Trichloroethane 21.6 0.50 ug/L 20.00 108 75-136 1,1,2,2-Tetrachloroethane 20.6 0.50 ug/L 20.00 103 62-127 1,1,2-Trichloroethane 23.4 0.50 ug/L 20.00 117 70-140 1,1-Dichloroethane 23.4 0.50 ug/L 20.00 117 78-130 1,1-Dichloroethylene 21.4 0.50 ug/L 20.00 107 70-154 1, 1 -Dichloropropylene 21.3 0.50 ug/L 20.00 107 71-136 1,2,3-Trichlorobenzene 18.9 2.0 ug/L 20.00 94 58-144 1,2,3-Trichloropropane 19.5 1.0 ug/L 20.00 98 71-127 1,2,4-Trichlorobenzene 19.6 1.0 ug/L 20.00 98 66-139 1,2,4-Trimethylbenzene 20.8 0.50 ug/L 20.00 104 75-133 1,2-Dibromo-3-chloropropane 19.8 2.0 ug/L 20.00 99 63-134 1,2-Dibromoethane 21.8 0.50 ug/L 20.00 109 77-135 1,2-Dichlorobenzene 19.4 0.50 ug/L 20.00 97 78-128 1,2-Dichloroethane 20.0 0.50 ug/L 20.00 100 68-131 1,2-Dichloropropane 19.9 0.50 ug/L 20.00 99 77-130 1,3,5-Trimethylbenzene 20.6 0.50 ug/L 20.00 103 75-131 1,3-Dichlorobenzene 19.7 0.50 ug/L 20.00 98 77-125 1,3-Dichloropropane 21.7 0.50 ug/L 20.00 109 76-132 1,4-Dichlorobenzene 19.8 0.50 ug/L 20.00 99 75-126 2,2-Dichloropropane 21.8 2.0 ug/L 20.00 109 29-149 2-Chlorotoluene 19.7 0.50 ug/L 20.00 99 74-126 4-Chlorotoluene 20.3 0.50 ug/L 20.00 101 78-129 4-Isopropyltoluene 20.7 0.50 ug/L 20.00 104 69-132 Acetone 34.6 5.0 ug/L 40.00 87 40-166 Acrolein 47.4 20 ug/L 40.00 119 70-130 Acrylonitrile 46.0 20 ug/L 40.00 115 81-127 Benzene 22.0 0.50 ug/L 20.00 110 77-128 Bromobenzene 19.4 0.50 ug/L 20.00 97 78-129 Bromochloromethane 22.8 0.50 ug/L 20.00 114 78-135 Bromodichloromethane 20.7 0.50 ug/L 20.00 104 76-138 Bromoform 17.5 1.0 ug/L 20.00 88 71-135 Bromomethane 25.0 1.0 ug/L 20.00 125 41-168 Carbon disulfide 20.0 5.0 ug/L 20.00 100 59-135 Carbon Tetrachloride 21.2 0.50 ug/L 20.00 106 72-142 Chlorobenzene 20.0 0.50 ug/L 20.00 100 78-119 Chloroethane 22.2 0.50 ug/L 20.00 111 57-142 Chloroform 21.6 0.50 ug/L 20.00 108 77-130 Chloromethane 22.1 0.50 ug/L 20.00 111 47-145 cis-1,2-Dichloroethylene 22.3 0.50 ug/L 20.00 112 76-141 cis-1,3-Dichloropropylene 21.0 0.50 ug/L 20.00 105 65-140 Dibromochloromethane 21.2 0.50 ug/L 20.00 106 75-134 Dibromomethane 20.2 0.50 ug/L 20.00 101 76-138 Dichlorodifluoromethane 19.6 5.0 ug/L 20.00 98 28-163 Ethylbenzene 20.0 0.50 ug/L 20.00 100 80-127 Hexachlorobutadiene 20.2 2.0 ug/L 20.00 101 61-134 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 68 0 93 Waypoint ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010844 - 5030B LCS (P010844-BS1) Isopropyl Ether Isopropylbenzene (Cumene) m,p-Xylenes Methyl Butyl Ketone (2-Hexanone) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methylene Chloride Methyl-tert-Butyl Ether Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butylbenzene Styrene tert-Butyl benzene Tetrachloroethylene Toluene trans- 1,2-Dichloroethylene trans- 1,3-Dichloropropylene Trichloroethylene Trich lorofluoromethane Vinyl acetate Vinyl chloride Xylenes, total Surrogate: 4-Bromofluorobenzene Surrogate: Dibromofluoromethane Surrogate: Toluene-d8 Prepared & Analyzed: 09/18/20 23.4 5.0 ug/L 20.00 117 60-154 20.2 0.50 ug/L 20.00 101 70-130 43.1 1.0 ug/L 40.00 108 77-133 20.0 5.0 ug/L 20.00 100 64-137 18.0 5.0 ug/L 20.00 90 71-134 24.3 5.0 ug/L 20.00 121 69-134 20.7 1.0 ug/L 20.00 104 73-131 22.9 0.50 ug/L 20.00 115 68-135 19.2 1.0 ug/L 20.00 96 64-136 19.8 1.0 ug/L 20.00 99 68-134 20.7 0.50 ug/L 20.00 104 72-132 20.1 0.50 ug/L 20.00 101 78-128 20.3 0.50 ug/L 20.00 102 71-131 20.4 0.50 ug/L 20.00 102 78-129 20.0 0.50 ug/L 20.00 100 70-132 19.8 0.50 ug/L 20.00 99 80-129 22.4 0.50 ug/L 20.00 112 76-131 22.5 0.50 ug/L 20.00 113 76-135 23.8 0.50 ug/L 20.00 119 67-140 20.3 0.50 ug/L 20.00 102 77-133 22.1 0.50 ug/L 20.00 110 62-148 24.4 2.0 ug/L 20.00 122 34-167 21.6 0.50 ug/L 20.00 108 57-141 63.2 1.5 ug/L 60.00 105 77-133 49.3 ug/L 50.00 99 80-124 55.9 ug/L 50.00 112 75-129 50.3 ug/L 50.00 101 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 69 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P010844 - 5030B Reporting Result Limit Units Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike (P010844-MS1) Source: 0090162-01 Prepared: 09/18/20 Analyzed: 09/19/20 1,1,1,2-Tetrachloroethane 189 5.0 ug/L 200.0 BRL 94 78-134 1,1,1-Trichloroethane 210 5.0 ug/L 200.0 BRL 105 67-145 1,1,2,2-Tetrachloroethane 217 5.0 ug/L 200.0 BRL 109 68-123 1,1,2-Trichloroethane 208 5.0 ug/L 200.0 BRL 104 75-134 1,1-Dichloroethane 212 5.0 ug/L 200.0 BRL 106 75-134 1,1-Dichloroethylene 201 5.0 ug/L 200.0 BRL 101 65-162 1,1-Dichloropropylene 204 5.0 ug/L 200.0 BRL 102 68-140 1,2,3-Trichlorobenzene 200 20 ug/L 200.0 BRL 100 56-146 1,2,3-Trichloropropane 201 10 ug/L 200.0 BRL 101 73-122 1,2,4-Trichlorobenzene 199 10 ug/L 200.0 BRL 99 67-135 1,2,4-Trimethyl benzene 212 5.0 ug/L 200.0 BRL 106 75-131 1,2-Dibromo-3-chloropropane 196 20 ug/L 200.0 BRL 98 64-133 1,2-Dibromoethane 195 5.0 ug/L 200.0 BRL 98 80-129 1,2-Dichlorobenzene 200 5.0 ug/L 200.0 BRL 100 80-125 1,2-Dichloroethane 197 5.0 ug/L 200.0 BRL 99 69-129 1,2-Dichloropropane 218 5.0 ug/L 200.0 BRL 109 75-131 1,3,5-Trimethyl benzene 210 5.0 ug/L 200.0 BRL 105 75-131 1,3-Dichlorobenzene 196 5.0 ug/L 200.0 BRL 98 79-122 1,3-Dichloropropane 201 5.0 ug/L 200.0 BRL 100 80-125 1,4-Dichlorobenzene 198 5.0 ug/L 200.0 BRL 99 76-124 2,2-Dichloropropane 185 20 ug/L 200.0 BRL 92 21-140 2-Chlorotoluene 207 5.0 ug/L 200.0 BRL 104 75-125 4-Chlorotoluene 206 5.0 ug/L 200.0 BRL 103 76-130 4-Isopropyltoluene 205 5.0 ug/L 200.0 BRL 102 72-129 Acetone 241 50 ug/L 400.0 BRL 60 40-162 Acrolein 370 200 ug/L 400.0 BRL 92 70-130 Acrylonitrile 376 200 ug/L 400.0 BRL 94 78-129 Benzene 210 5.0 ug/L 200.0 BRL 105 73-131 Bromobenzene 207 5.0 ug/L 200.0 BRL 103 80-125 Bromochloromethane 210 5.0 ug/L 200.0 BRL 105 78-135 Bromodichloromethane 210 5.0 ug/L 200.0 BRL 105 74-138 Bromoform 156 10 ug/L 200.0 BRL 78 72-130 Bromomethane 167 10 ug/L 200.0 BRL 84 41-173 Carbon disulfide 186 50 ug/L 200.0 BRL 93 59-138 Carbon Tetrachloride 200 5.0 ug/L 200.0 BRL 100 66-149 Chlorobenzene 200 5.0 ug/L 200.0 BRL 100 76-119 Chloroethane 214 5.0 ug/L 200.0 BRL 107 52-153 Chloroform 206 5.0 ug/L 200.0 BRL 103 74-136 Chloromethane 193 5.0 ug/L 200.0 BRL 97 39-155 cis-1,2-Dichloroethylene 202 5.0 ug/L 200.0 BRL 101 74-144 cis-1,3-Dichloropropylene 215 5.0 ug/L 200.0 BRL 107 64-132 Dibromochloromethane 180 5.0 ug/L 200.0 BRL 90 77-131 Dibromomethane 211 5.0 ug/L 200.0 BRL 105 76-136 Dichlorodifluoromethane 187 50 ug/L 200.0 BRL 94 22-170 Ethylbenzene 202 5.0 ug/L 200.0 BRL 101 78-130 Hexachlorobutadiene 194 20 ug/L 200.0 BRL 97 63-132 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 70 0f 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010844 - 5030B Matrix Spike (P010844-MS1) Source: 0090162-01 Prepared: 09/18/20 Analyzed: 09/19/20 Isopropyl Ether 212 50 ug/L 200.0 BRL 106 62-154 Isopropylbenzene (Cumene) 203 5.0 ug/L 200.0 BRL 101 72-127 m,p-Xylenes 429 10 ug/L 400.0 BRL 107 66-144 Methyl Butyl Ketone (2-Hexanone) 186 50 ug/L 200.0 BRL 93 65-130 Methyl Ethyl Ketone (2-Butanone) 152 50 ug/L 200.0 BRL 76 65-137 Methyl Isobutyl Ketone 198 50 ug/L 200.0 BRL 99 64-137 Methylene Chloride 187 10 ug/L 200.0 BRL 93 71-134 Methyl-tert-Butyl Ether 207 5.0 ug/L 200.0 BRL 104 71-133 Naphthalene 191 10 ug/L 200.0 BRL 96 63-134 n-Butylbenzene 205 10 ug/L 200.0 BRL 102 69-132 n-Propylbenzene 216 5.0 ug/L 200.0 BRL 108 75-130 o-Xylene 203 5.0 ug/L 200.0 BRL 102 75-131 sec-Butylbenzene 208 5.0 ug/L 200.0 BRL 104 72-130 Styrene 202 5.0 ug/L 200.0 BRL 101 77-128 tert-Butylbenzene 206 5.0 ug/L 200.0 BRL 103 72-130 Tetrachloroethylene 187 5.0 ug/L 200.0 BRL 94 76-130 Toluene 211 5.0 ug/L 200.0 BRL 105 72-135 trans-1,2-Dichloroethylene 210 5.0 ug/L 200.0 BRL 105 73-141 trans-1,3-Dichloropropylene 209 5.0 ug/L 200.0 BRL 105 64-137 Trichloroethylene 206 5.0 ug/L 200.0 BRL 103 72-133 Trichlorofluoromethane 223 5.0 ug/L 200.0 BRL ill 61-152 Vinyl acetate 216 20 ug/L 200.0 BRL 108 80-154 Vinyl chloride 200 5.0 ug/L 200.0 BRL 100 54-146 Xylenes, total 632 15 ug/L 600.0 BRL 105 66-144 Surrogate:4-Bromofluorobenzene 47.8 ug/L 50.00 96 80-124 Surrogate: Dibromofluoromethane 52.4 ug/L 50.00 105 75-129 Surrogate: Toluene-d8 47.5 ug/L 50.00 95 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 71 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010844 - 5030B Matrix Spike Dup (P010844-MSD1) Source: 0090162-01 Prepared: 09/18/20 Analyzed: 09/19/20 1,1,1,2-Tetrachloroethane 187 5.0 ug/L 200.0 BRL 94 78-134 1 19 1,1,1-Trichloroethane 204 5.0 ug/L 200.0 BRL 102 67-145 3 18 1,1,2,2-Tetrachloroethane 218 5.0 ug/L 200.0 BRL 109 68-123 0.5 19 1,1,2-Trichloroethane 213 5.0 ug/L 200.0 BRL 106 75-134 2 18 1,1-Dichloroethane 214 5.0 ug/L 200.0 BRL 107 75-134 0.8 18 1,1-Dichloroethylene 197 5.0 ug/L 200.0 BRL 99 65-162 2 20 1,1-Dichloropropylene 205 5.0 ug/L 200.0 BRL 103 68-140 0.6 19 1,2,3-Trichlorobenzene 217 20 ug/L 200.0 BRL 109 56-146 8 31 1,2,3-Trichloropropane 209 10 ug/L 200.0 BRL 104 73-122 4 18 1,2,4-Trichlorobenzene 208 10 ug/L 200.0 BRL 104 67-135 5 20 1,2,4-Trimethyl benzene 208 5.0 ug/L 200.0 BRL 104 75-131 2 18 1,2-Dibromo-3-chloropropane 205 20 ug/L 200.0 BRL 102 64-133 4 25 1,2-Dibromoethane 196 5.0 ug/L 200.0 BRL 98 80-129 0.5 19 1,2-Dichlorobenzene 195 5.0 ug/L 200.0 BRL 98 80-125 2 16 1,2-Dichloroethane 199 5.0 ug/L 200.0 BRL 100 69-129 1 17 1,2-Dichloropropane 217 5.0 ug/L 200.0 BRL 108 75-131 0.7 17 1,3,5-Trimethyl benzene 209 5.0 ug/L 200.0 BRL 105 75-131 0.5 19 1,3-Dichlorobenzene 198 5.0 ug/L 200.0 BRL 99 79-122 0.7 17 1,3-Dichloropropane 204 5.0 ug/L 200.0 BRL 102 80-125 2 18 1,4-Dichlorobenzene 196 5.0 ug/L 200.0 BRL 98 76-124 0.9 17 2,2-Dichloropropane 175 20 ug/L 200.0 BRL 88 21-140 6 19 2-Chlorotoluene 204 5.0 ug/L 200.0 BRL 102 75-125 2 24 4-Chlorotoluene 205 5.0 ug/L 200.0 BRL 103 76-130 0.2 16 4-Isopropyltoluene 199 5.0 ug/L 200.0 BRL 100 72-129 3 19 Acetone 261 50 ug/L 400.0 BRL 65 40-162 8 23 Acrolein 429 200 ug/L 400.0 BRL 107 70-130 15 20 Acrylonitrile 406 200 ug/L 400.0 BRL 101 78-129 8 20 Benzene 211 5.0 ug/L 200.0 BRL 105 73-131 0.4 17 Bromobenzene 203 5.0 ug/L 200.0 BRL 101 80-125 2 18 Bromochloromethane 205 5.0 ug/L 200.0 BRL 102 78-135 2 17 Bromodichloromethane 206 5.0 ug/L 200.0 BRL 103 74-138 2 19 Bromoform 160 10 ug/L 200.0 BRL 80 72-130 3 22 Bromomethane 177 10 ug/L 200.0 BRL 88 41-173 5 33 Carbon disulfide 182 50 ug/L 200.0 BRL 91 59-138 2 27 Carbon Tetrachloride 195 5.0 ug/L 200.0 BRL 97 66-149 2 23 Chlorobenzene 198 5.0 ug/L 200.0 BRL 99 76-119 0.6 20 Chloroethane 190 5.0 ug/L 200.0 BRL 95 52-153 12 24 Chloroform 204 5.0 ug/L 200.0 BRL 102 74-136 0.8 19 Chloromethane 174 5.0 ug/L 200.0 BRL 87 39-155 11 20 cis-1,2-Dichloroethylene 203 5.0 ug/L 200.0 BRL 101 74-144 0.1 17 cis-1,3-Dichloropropylene 210 5.0 ug/L 200.0 BRL 105 64-132 2 18 Dibromochloromethane 186 5.0 ug/L 200.0 BRL 93 77-131 3 21 Dibromomethane 212 5.0 ug/L 200.0 BRL 106 76-136 0.5 18 Dichlorodifluoromethane 178 50 ug/L 200.0 BRL 89 22-170 5 22 Ethylbenzene 201 5.0 ug/L 200.0 BRL 101 78-130 0.4 18 Hexachlorobutadiene 192 20 ug/L 200.0 BRL 96 63-132 1 26 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 72 0f 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010844 - 5030B Matrix Spike Dup (P010844-MSD1) Source: 0090162-01 Prepared: 09/18/20 Analyzed: 09/19/20 Isopropyl Ether 223 50 ug/L 200.0 BRL ill 62-154 5 18 Isopropylbenzene (Cumene) 216 5.0 ug/L 200.0 BRL 108 72-127 7 19 m,p-Xylenes 426 10 ug/L 400.0 BRL 106 66-144 0.8 19 Methyl Butyl Ketone (2-Hexanone) 200 50 ug/L 200.0 BRL 100 65-130 7 23 Methyl Ethyl Ketone (2-Butanone) 166 50 ug/L 200.0 BRL 83 65-137 9 23 Methyl Isobutyl Ketone 208 50 ug/L 200.0 BRL 104 64-137 5 24 Methylene Chloride 188 10 ug/L 200.0 BRL 94 71-134 0.4 17 Methyl-tert-Butyl Ether 209 5.0 ug/L 200.0 BRL 105 71-133 0.9 19 Naphthalene 212 10 ug/L 200.0 BRL 106 63-134 11 32 n-Butylbenzene 201 10 ug/L 200.0 BRL 100 69-132 2 21 n-Propylbenzene 212 5.0 ug/L 200.0 BRL 106 75-130 2 18 o-Xylene 202 5.0 ug/L 200.0 BRL 101 75-131 0.6 20 sec-Butylbenzene 205 5.0 ug/L 200.0 BRL 102 72-130 2 20 Styrene 203 5.0 ug/L 200.0 BRL 101 77-128 0.3 17 tert-Butylbenzene 200 5.0 ug/L 200.0 BRL 100 72-130 3 20 Tetrachloroethylene 178 5.0 ug/L 200.0 BRL 89 76-130 5 20 Toluene 208 5.0 ug/L 200.0 BRL 104 72-135 1 18 trans-1,2-Dichloroethylene 206 5.0 ug/L 200.0 BRL 103 73-141 2 18 trans-1,3-Dichloropropylene 204 5.0 ug/L 200.0 BRL 102 64-137 3 21 Trichloroethylene 205 5.0 ug/L 200.0 BRL 103 72-133 0.5 17 Trichlorofluoromethane 202 5.0 ug/L 200.0 BRL 101 61-152 10 27 Vinyl acetate 224 20 ug/L 200.0 BRL 112 80-154 4 18 Vinyl chloride 190 5.0 ug/L 200.0 BRL 95 54-146 5 25 Xylenes, total 628 15 ug/L 600.0 BRL 105 66-144 0.8 20 Surrogate:4-Bromofluorobenzene 51.8 ug/L 50.00 104 80-124 Surrogate: Dibromofluoromethane 51.9 ug/L 50.00 104 75-129 Surrogate: Toluene-d8 47.5 ug/L 50.00 95 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 73 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Semivolatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010771 - 3546 Blank (P010771-BLK1) 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1-Methyl naphthalene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methyl naphthalene 2-Methylphenol 2-Nitrophenol 3,3'-Dichlorobenzidine 3/4-Methyl phenol 4,6-Dinitro-2-methylphenol 4-Bromophenyl phenyl ether 4-C h loro-3-methyl phenol 4-Chloroaniline 4-Chlorophenyl phenyl ether 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Azobenzene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl alcohol bis(2-Chloroethoxy)methane B is(2-Ch loroethyl )ether Bis(2-chloroisopropyl)ether Bis(2-Ethylhexyl)phthalate Butyl benzyl phthalate Chrysene Dibenzo(a,h)anthracene Dibenzofuran Diethyl phthalate Dimethyl phthalate BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.33 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.33 mg/kg wet 1.5 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 1.5 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.33 mg/kg wet 1.0 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 2.0 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.33 mg/kg wet 0.66 mg/kg wet 0.33 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet 0.66 mg/kg wet Prepared & Analyzed: 09/16/20 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 74 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P010771 - 3546 Blank (P010771-BLK1) Prepared & Analyzed: 09/16/20 Di-n-butyl phthalate BRL 0.66 mg/kg wet Di-n-octyl phthalate BRL 0.33 mg/kg wet Fluoranthene BRL 0.66 mg/kg wet Fluorene BRL 0.66 mg/kg wet Hexachlorobenzene BRL 0.66 mg/kg wet Hexachlorobutadiene BRL 0.66 mg/kg wet Hexachlorocyclopentadiene BRL 0.66 mg/kg wet Hexachloroethane BRL 0.66 mg/kg wet Indeno(1,2,3-cd)pyrene BRL 0.66 mg/kg wet Isophorone BRL 0.66 mg/kg wet Naphthalene BRL 0.66 mg/kg wet Nitrobenzene BRL 0.33 mg/kg wet N-Nitroso-di-n-propylamine BRL 0.66 mg/kg wet N-Nitrosodiphenylamine BRL 0.66 mg/kg wet Pentachlorophenol BRL 1.0 mg/kg wet Phenanthrene BRL 0.66 mg/kg wet Phenol BRL 0.66 mg/kg wet Pyrene BRL 0.66 mg/kg wet Pyridine BRL 0.33 mg/kg wet Surrogate: 2,4,6-Tribromophenol 3.97 mg/kg wet 3.329 119 39-132 Surrogate: 2-Fluorobiphenyl 1.74 mg/kg wet 1.664 105 44-115 Surrogate: 2-Fluorophenol 3.45 mg/kg wet 3.329 104 35-115 Surrogate: Nitrobenzene-d5 1.50 mg/kg wet 1.664 90 37-122 Surrogate: Phenol-d5 3.40 mg/kg wet 3.329 102 34-121 Surrogate: Terphenyl-04 1.87 mg/kg wet 1.664 112 54-127 LCS (P010771-BS1) Prepared &Analyzed: 09/16/20 1,2,4-Trichlorobenzene 1.25 0.66 mg/kg wet 1.663 75 34-118 1,2-Dichlorobenzene 1.35 0.66 mg/kg wet 1.663 81 33-117 1,3-Dichlorobenzene 1.32 0.66 mg/kg wet 1.663 79 30-115 1,4-Dichlorobenzene 1.32 0.33 mg/kg wet 1.663 79 31-115 1-Methyl naphthalene 1.39 0.66 mg/kg wet 1.663 83 40-119 2,4,5-Trichlorophenol 1.65 0.66 mg/kg wet 1.663 99 62-124 2,4,6-Trichlorophenol 1.55 0.66 mg/kg wet 1.663 93 39-126 2,4-Dichlorophenol 1.44 0.66 mg/kg wet 1.663 87 40-122 2,4-Dimethylphenol 1.51 0.33 mg/kg wet 1.663 91 30-127 2,4-Dinitrophenol 1.25 1.5 mg/kg wet 1.663 75 27-129 J 2,4-Dinitrotoluene 1.71 0.66 mg/kg wet 1.663 103 48-126 2,6-Dinitrotoluene 1.70 0.66 mg/kg wet 1.663 102 46-124 2-Chloronaphthalene 1.50 0.66 mg/kg wet 1.663 90 41-114 2-Chlorophenol 1.49 0.66 mg/kg wet 1.663 90 34-121 2-Methyl naphthalene 1.32 0.66 mg/kg wet 1.663 79 38-122 2-Methylphenol 1.49 0.66 mg/kg wet 1.663 90 32-122 2-Nitrophenol 1.35 0.66 mg/kg wet 1.663 81 36-123 3,3'-Dichlorobenzidine 1.62 0.66 mg/kg wet 1.663 98 22-121 3/4-Methyl phenol 1.39 0.66 mg/kg wet 1.663 84 34-119 4,6-Dinitro-2-methylphenol 1.46 1.5 mg/kg wet 1.663 88 29-132 J This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 75 0f 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P010771 - 3546 LCS (P010771-BSI) 4-Bromophenyl phenyl ether 4-C h loro-3-methyl phenol 4-Chloroaniline 4-Chlorophenyl phenyl ether 4-Nitrophenol Acenaphthene Acenaphthylene Anthracene Azobenzene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,hJ)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl alcohol bis(2-Chloroethoxy)methane B i s(2-Ch loroethyl )ether Bis(2-chloroisopropyl)ether Bis(2-Ethylhexyl)phthalate Butyl benzyl phthalate Chrysene Dibenzo(a, h )anthracene Dibenzofuran Diethyl phthalate Dimethyl phthalate Di-n-butyl phthalate Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene N-N itroso-di-n-propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Surrogate: 2, 4, 6-Tribromophenol Reporting Result Limit Units Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Prepared & Analyzed: 09/16/20 1.67 0.66 mg/kg wet 1.663 100 46-124 1.44 0.66 mg/kg wet 1.663 86 45-122 1.28 0.33 mg/kg wet 1.663 77 17-106 1.60 1.0 mg/kg wet 1.663 96 45-121 1.88 0.66 mg/kg wet 1.663 113 30-132 1.55 0.66 mg/kg wet 1.663 93 40-123 1.66 0.66 mg/kg wet 1.663 100 32-132 1.69 0.66 mg/kg wet 1.663 101 47-123 1.49 0.66 mg/kg wet 1.663 90 39-125 1.59 0.66 mg/kg wet 1.663 96 49-126 1.89 0.66 mg/kg wet 1.663 113 45-129 1.80 0.66 mg/kg wet 1.663 108 45-132 1.90 0.66 mg/kg wet 1.663 114 43-134 1.73 0.66 mg/kg wet 1.663 104 47-132 1.31 2.0 mg/kg wet 1.663 78 10-83 1.52 0.66 mg/kg wet 1.663 91 29-122 1.38 0.66 mg/kg wet 1.663 83 36-121 1.42 0.66 mg/kg wet 1.663 85 31-120 1.25 0.33 mg/kg wet 1.663 75 33-131 1.76 0.66 mg/kg wet 1.663 106 51-133 1.69 0.33 mg/kg wet 1.663 101 48-132 1.61 0.66 mg/kg wet 1.663 97 50-124 1.61 0.66 mg/kg wet 1.663 97 45-134 1.49 0.66 mg/kg wet 1.663 89 44-120 1.65 0.66 mg/kg wet 1.663 99 50-124 1.67 0.66 mg/kg wet 1.663 100 48-124 1.85 0.66 mg/kg wet 1.663 ill 51-128 1.86 0.33 mg/kg wet 1.663 112 45-140 1.74 0.66 mg/kg wet 1.663 105 50-127 1.64 0.66 mg/kg wet 1.663 98 43-125 1.62 0.66 mg/kg wet 1.663 98 45-122 1.42 0.66 mg/kg wet 1.663 85 32-123 1.38 0.66 mg/kg wet 1.663 83 32-117 1.26 0.66 mg/kg wet 1.663 76 28-117 1.94 0.66 mg/kg wet 1.663 116 45-133 1.02 0.66 mg/kg wet 1.663 61 30-122 1.31 0.66 mg/kg wet 1.663 79 35-123 1.17 0.33 mg/kg wet 1.663 70 34-122 1.38 0.66 mg/kg wet 1.663 83 36-120 1.88 0.66 mg/kg wet 1.663 113 38-127 1.74 1.0 mg/kg wet 1.663 105 25-133 1.63 0.66 mg/kg wet 1.663 98 50-121 1.61 0.66 mg/kg wet 1.663 97 34-121 1.68 0.66 mg/kg wet 1.663 101 47-127 0.865 0.33 mg/kg wet 1.663 52 10-60 3.60 mg/kg wet 3.327 108 39-132 J This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 76 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Semivolatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010771 - 3546 LCS (P010771-BSI) Prepared &Analyzed: 09/16/20 Surrogate: 2-Fluorobiphenyl 1.39 mg/kg wet 1.663 84 44-115 Surrogate: 2-Fluorophenol 2.74 mg/kg wet 3.327 82 35-115 Surrogate: Nitrobenzene-d5 1.05 mg/kg wet 1.663 63 37-122 Surrogate: Phenol-d5 2.68 mg/kg wet 3.327 81 34-121 Surrogate: Terphenyl-d14 1.40 mg/kg wet 1.663 84 54-127 Batch P010794 - 351 OC MS Blank (P010794-BLK1) Prepared & Analyzed: 09/17/20 1,2,4-Trichlorobenzene BRL 10 ug/L 1,2-Dichlorobenzene BRL 10 ug/L 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 ug/L 1-Methyl naphthalene BRL 10 ug/L 2,4,5-Trichlorophenol BRL 20 ug/L 2,4,6-Trichlorophenol BRL 20 ug/L 2,4-Dichlorophenol BRL 10 ug/L 2,4-Dimethylphenol BRL 10 ug/L 2,4-Dinitrophenol BRL 50 ug/L 2,4-Dinitrotoluene BRL 10 ug/L 2,6-Dinitrotoluene BRL 20 ug/L 2-Chloronaphthalene BRL 20 ug/L 2-Chlorophenol BRL 10 ug/L 2-Methyl naphthalene BRL 10 ug/L 2-Methylphenol BRL 10 ug/L 2-Nitroaniline BRL 10 ug/L 2-Nitrophenol BRL 10 ug/L 3,3'-Dichlorobenzidine BRL 10 ug/L 3/4-Methyl phenol BRL 10 ug/L 3-Nitroaniline BRL 10 ug/L 4,6-Dinitro-2-methylphenol BRL 50 ug/L 4-Bromophenyl phenyl ether BRL 20 ug/L 4-Chloro-3-methylphenol BRL 10 ug/L 4-Chloroaniline BRL 10 ug/L 4-Chlorophenyl phenyl ether BRL 20 ug/L 4-Nitroaniline BRL 10 ug/L 4-Nitrophenol BRL 10 ug/L Acenaphthene BRL 10 ug/L Acenaphthylene BRL 20 ug/L Aniline BRL 50 ug/L Anthracene BRL 10 ug/L Azobenzene BRL 10 ug/L Benzo(a)anthracene BRL 10 ug/L Benzo(a)pyrene BRL 10 ug/L Benzo(b)fluoranthene BRL 10 ug/L Benzo(g,h,i)perylene BRL 10 ug/L Benzo(k)fluoranthene BRL 10 ug/L This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 77 0f 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Analyte Result Limit Units Batch P010794 - 351 OC MS Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P010794-BLK1) Prepared & Analyzed: 09/17/20 Benzoic Acid BRL 100 ug/L Benzyl alcohol BRL 10 ug/L bis(2-Chloroethoxy)methane BRL 10 ug/L Bis(2-Chloroethyl)ether BRL 10 ug/L Bis(2-chloroisopropyl)ether BRL 10 ug/L Bis(2-Ethylhexyl)phthalate BRL 10 ug/L Butyl benzyl phthalate BRL 10 ug/L Chrysene BRL 10 ug/L Dibenzo(a,h)anthracene BRL 20 ug/L Dibenzofuran BRL 20 ug/L Diethyl phthalate BRL 20 ug/L Dimethyl phthalate BRL 10 ug/L Di-n-butyl phthalate BRL 10 ug/L Di-n-octyl phthalate BRL 10 ug/L Fluoranthene BRL 10 ug/L Fluorene BRL 10 ug/L Hexachlorobenzene BRL 20 ug/L Hexachlorobutadiene BRL 20 ug/L Hexachlorocyclopentadiene BRL 20 ug/L Hexachloroethane BRL 10 ug/L Indeno(1,2,3-cd)pyrene BRL 10 ug/L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitrobenzene BRL 10 ug/L N-Nitroso-di-n-propylamine BRL 20 ug/L N-Nitrosodiphenylamine BRL 20 ug/L Pentachlorophenol BRL 50 ug/L Phenanthrene BRL 10 ug/L Phenol BRL 10 ug/L Pyrene BRL 10 ug/L Surrogate: 2,4,6-Tribromophenol 102 ug/L 100.0 102 43-140 Surrogate:2-Fluorobiphenyl 36.4 ug/L 50.00 73 44-119 Surrogate:2-Fluorophenol 38.6 ug/L 100.0 39 19-119 Surrogate: Nitrobenzene-d5 31.3 ug/L 50.00 63 44-120 Surrogate: Phenol-d5 25.7 ug/L 100.0 26 11-52 Surrogate: Terphenyl-d14 45.1 ug/L 50.00 90 50-134 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 78 of 93 Waypoint ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P010794 - 3510C MS Reporting Result Limit Units Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P010794-BS1) Prepared &Analyzed: 09/17/20 1,2,4-Trichlorobenzene 33.7 10 ug/L 50.00 67 29-126 1,2-Dichlorobenzene 35.0 10 ug/L 50.00 70 32-111 1,3-Dichlorobenzene 33.4 10 ug/L 50.00 67 28-110 1,4-Dichlorobenzene 33.7 10 ug/L 50.00 67 29-112 1-Methyl naphthalene 39.1 10 ug/L 50.00 78 41-119 2,4,5-Trichlorophenol 46.3 20 ug/L 50.00 93 53-123 2,4,6-Trichlorophenol 45.2 20 ug/L 50.00 90 50-125 2,4-Dichlorophenol 40.4 10 ug/L 50.00 81 47-121 2,4-Dimethylphenol 43.0 10 ug/L 50.00 86 31-124 2,4-Dinitrophenol 40.6 50 ug/L 50.00 81 23-143 2,4-Dinitrotoluene 50.7 10 ug/L 50.00 101 57-128 2,6-Dinitrotoluene 49.5 20 ug/L 50.00 99 57-124 2-Chloronaphthalene 41.0 20 ug/L 50.00 82 40-116 2-Chlorophenol 37.8 10 ug/L 50.00 76 38-117 2-Methyl naphthalene 36.8 10 ug/L 50.00 74 40-121 2-Methylphenol 34.9 10 ug/L 50.00 70 30-117 2-Nitroaniline 47.5 10 ug/L 50.00 95 55-127 2-Nitrophenol 39.8 10 ug/L 50.00 80 47-123 3,3'-Dichlorobenzidine 58.4 10 ug/L 50.00 117 27-129 3/4-Methyl phenol 29.5 10 ug/L 50.00 59 29-110 3-Nitroaniline 45.3 10 ug/L 50.00 91 41-128 4,6-Dinitro-2-methylphenol 50.3 50 ug/L 50.00 101 44-137 4-Bromophenyl phenyl ether 49.1 20 ug/L 50.00 98 55-124 4-Chloro-3-methylphenol 42.5 10 ug/L 50.00 85 52-119 4-Chloroaniline 36.4 10 ug/L 50.00 73 33-117 4-Chlorophenyl phenyl ether 45.4 20 ug/L 50.00 91 53-121 4-Nitroaniline 52.8 10 ug/L 50.00 106 45-135 4-Nitrophenol 19.3 10 ug/L 50.00 39 10-77 Acenaphthene 44.6 10 ug/L 50.00 89 47-122 Acenaphthylene 46.9 20 ug/L 50.00 94 41-130 Aniline 27.0 50 ug/L 50.00 54 12-197 Anthracene 49.8 10 ug/L 50.00 100 57-123 Azobenzene 42.1 10 ug/L 50.00 84 61-116 Benzo(a)anthracene 48.1 10 ug/L 50.00 96 58-125 Benzo(a)pyrene 57.7 10 ug/L 50.00 115 54-128 Benzo(b)fluoranthene 54.3 10 ug/L 50.00 109 53-131 Benzo(g,h,i)perylene 57.6 10 ug/L 50.00 115 50-134 Benzo(k)fluoranthene 52.7 10 ug/L 50.00 105 57-129 Benzoic Acid BRL 100 ug/L 50.00 10-125 Benzyl alcohol 34.0 10 ug/L 50.00 68 31-112 bis(2-Chloroethoxy)methane 39.9 10 ug/L 50.00 80 48-120 Bis(2-Chloroethyl)ether 36.6 10 ug/L 50.00 73 43-118 Bis(2-chloroisopropyl)ether 33.9 10 ug/L 50.00 68 37-130 Bis(2-Ethylhexyl)phthalate 54.6 10 ug/L 50.00 109 55-135 Butyl benzyl phthalate 52.4 10 ug/L 50.00 105 53-134 Chrysene 50.3 10 ug/L 50.00 101 59-123 J J L This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 79 0 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Analyte Result Limit Units Batch P010794 - 351 OC MS LCS (P010794-BSI) Dibenzo(a,h)anth racene Dibenzofuran Diethyl phthalate Dimethyl phthalate Di-n-butyl phthalate Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone Naphthalene Nitrobenzene N-N itroso-d i-n-propyla mi ne N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Surrogate: 2, 4, 6-Tribromophenol Surrogate: 2-Fluorobiphenyl Surrogate: 2-Fluoro ph enol Surrogate: Nitrobenzene-d5 Surrogate: Phenol-d5 Surrogate: Terphenyl-04 Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Prepared & Analyzed: 09/17/20 52.3 20 ug/L 50.00 105 51-134 42.0 20 ug/L 50.00 84 53-118 49.1 20 ug/L 50.00 98 56-125 49.1 10 ug/L 50.00 98 45-127 56.6 10 ug/L 50.00 113 59-127 56.8 10 ug/L 50.00 114 51-140 52.8 10 ug/L 50.00 106 57-128 46.7 10 ug/L 50.00 93 52-124 49.0 20 ug/L 50.00 98 53-125 36.9 20 ug/L 50.00 74 22-124 38.7 20 ug/L 50.00 77 32-117 32.0 10 ug/L 50.00 64 21-115 58.7 10 ug/L 50.00 117 52-134 30.0 10 ug/L 50.00 60 42-124 35.6 10 ug/L 50.00 71 40-121 32.7 10 ug/L 50.00 65 45-121 39.3 20 ug/L 50.00 79 49-119 54.8 20 ug/L 50.00 110 51-123 63.7 50 ug/L 50.00 127 35-138 48.6 10 ug/L 50.00 97 59-120 15.4 10 ug/L 50.00 31 12-58 51.3 10 ug/L 50.00 103 57-126 115 ug/L 100.0 115 43-140 39.4 ug/L 50.00 79 44-119 41.3 ug/L 100.0 41 19-119 30.8 ug/L 50.00 62 44-120 27.3 ug/L 100.0 27 11-52 45.2 ug/L 50.00 90 50-134 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 80 of 93 ® Level II QC Report Waynt. � 10/13/20 poi ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Work Order: 0090162 Attn: Tom Proctor Time Submitted: 9/15/2020 12:00:OOPM 5113 Yachtsman Ct. Raleigh, NC 27615 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Notes Batch P010794 - 351 OC MS Matrix Spike (P010794-MS1) Source: 0090162-01 Prepared & Analyzed: 09/17/20 1,2,4-Trichlorobenzene 22.6 20 ug/L 100.0 BRL 23 29-116 MI 1,2-Dichlorobenzene 19.7 20 ug/L 100.0 BRL 20 32-111 Ml, J 1,3-Dichlorobenzene 19.2 20 ug/L 100.0 BRL 19 28-110 MI, J 1,4-Dichlorobenzene 19.2 20 ug/L 100.0 BRL 19 29-112 Ml, J 1-Methyl naphthalene 27.1 20 ug/L 100.0 BRL 27 41-119 MI 2,4,5-Trichlorophenol 16.8 40 ug/L 100.0 BRL 17 53-123 Ml, J 2,4,6-Trichlorophenol 15.5 40 ug/L 100.0 BRL 15 50-125 Ml, J 2,4-Dichlorophenol 15.8 20 ug/L 100.0 BRL 16 47-121 MI, J 2,4-Dimethylphenol 18.6 20 ug/L 100.0 BRL 19 31-124 Ml, J 2,4-Dinitrophenol 25.2 100 ug/L 100.0 BRL 25 23-143 J 2,4-Dinitrotoluene 30.9 20 ug/L 100.0 BRL 31 57-128 MI 2,6-Dinitrotoluene 31.7 40 ug/L 100.0 BRL 32 57-124 Ml, J 2-Chloronaphthalene 27.7 40 ug/L 100.0 BRL 28 40-116 Ml, J 2-Chlorophenol 13.7 20 ug/L 100.0 BRL 14 38-117 MI, J 2-Methyl naphthalene 25.7 20 ug/L 100.0 BRL 26 40-121 MI 2-Methylphenol 15.6 20 ug/L 100.0 BRL 16 30-117 Ml, J 2-Nitroaniline 31.5 20 ug/L 100.0 BRL 31 55-127 MI 2-Nitrophenol 13.3 20 ug/L 100.0 BRL 13 47-123 Ml, J 3,3'-Dichlorobenzidine 32.5 20 ug/L 100.0 BRL 33 27-129 3/4-Methyl phenol 13.2 20 ug/L 100.0 BRL 13 29-110 MI, J 3-Nitroaniline 51.9 20 ug/L 100.0 BRL 52 41-128 4,6-Dinitro-2-methylphenol BRL 100 ug/L 100.0 BRL 44-137 MI 4-Bromophenyl phenyl ether 32.6 40 ug/L 100.0 BRL 33 55-124 MI, J 4-Chloro-3-methylphenol 17.1 20 ug/L 100.0 BRL 17 52-119 Ml, J 4-Chloroaniline 61.9 20 ug/L 100.0 BRL 62 33-117 4-Chlorophenyl phenyl ether 31.0 40 ug/L 100.0 BRL 31 53-121 MI, J 4-Nitroaniline 38.8 20 ug/L 100.0 BRL 39 45-135 MI 4-Nitrophenol 10.8 20 ug/L 100.0 BRL 11 10-105 J Acenaphthene 28.5 20 ug/L 100.0 BRL 29 47-122 MI Acenaphthylene 31.5 40 ug/L 100.0 BRL 32 41-130 Ml, J Aniline 55.6 100 ug/L 100.0 BRL 56 11-124 J Anthracene 35.5 20 ug/L 100.0 BRL 36 57-123 MI Azobenzene 29.6 20 ug/L 100.0 BRL 30 61-116 MI Benzo(a)anthracene 35.3 20 ug/L 100.0 BRL 35 58-125 MI Benzo(a)pyrene 40.3 20 ug/L 100.0 BRL 40 54-128 MI Benzo(b)fluoranthene 39.1 20 ug/L 100.0 BRL 39 53-131 MI Benzo(g,h,i)perylene 39.8 20 ug/L 100.0 BRL 40 50-134 MI Benzo(k)fluoranthene 36.4 20 ug/L 100.0 BRL 36 57-129 MI Benzoic Acid BRL 200 ug/L 100.0 BRL 10-125 MI Benzyl alcohol 44.7 20 ug/L 100.0 BRL 45 31-112 bis(2-Chloroethoxy)methane 25.8 20 ug/L 100.0 BRL 26 48-120 MI Bis(2-Chloroethyl)ether 14.5 20 ug/L 100.0 BRL 15 43-118 MI, J Bis(2-chloroisopropyl)ether 19.4 20 ug/L 100.0 BRL 19 37-130 Ml, J Bis(2-Ethylhexyl)phthalate 40.3 20 ug/L 100.0 BRL 40 55-135 MI Butyl benzyl phthalate 36.4 20 ug/L 100.0 BRL 36 53-134 MI Chrysene 37.3 20 ug/L 100.0 BRL 37 59-123 MI This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 81 0f 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Analyte Result Limit Units Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P010794 - 351 OC MS Matrix Spike (P010794-MS1) Source: 0090162-01 Prepared & Analyzed: 09/17/20 Dibenzo(a,h)anthracene 34.1 40 ug/L 100.0 BRL 34 51-134 MI, J Dibenzofuran 29.0 40 ug/L 100.0 BRL 29 53-118 MI, J Diethyl phthalate 32.7 40 ug/L 100.0 BRL 33 56-125 MI, J Dimethyl phthalate 31.2 20 ug/L 100.0 BRL 31 45-127 MI Di-n-butyl phthalate 42.8 20 ug/L 100.0 BRL 43 59-127 MI Di-n-octyl phthalate 40.2 20 ug/L 100.0 BRL 40 51-140 MI Fluoranthene 37.9 20 ug/L 100.0 BRL 38 57-128 MI Fluorene 32.0 20 ug/L 100.0 BRL 32 52-124 MI Hexachlorobenzene 32.2 40 ug/L 100.0 BRL 32 53-125 MI, J Hexachlorobutadiene 24.6 40 ug/L 100.0 BRL 25 22-124 J Hexachlorocyclopentadiene 24.6 40 ug/L 100.0 BRL 25 26-122 MI, J Hexachloroethane 18.1 20 ug/L 100.0 BRL 18 21-115 MI, J Indeno(1,2,3-cd)pyrene 47.9 20 ug/L 100.0 BRL 48 52-134 MI Isophorone 18.9 20 ug/L 100.0 BRL 19 42-124 MI, J Naphthalene 24.4 20 ug/L 100.0 BRL 24 40-121 MI Nitrobenzene 20.1 20 ug/L 100.0 BRL 20 45-121 MI N-Nitroso-di-n-propylamine 22.1 40 ug/L 100.0 BRL 22 49-119 MI, J N-Nitrosodiphenylamine 38.0 40 ug/L 100.0 BRL 38 51-123 MI, J Pentachlorophenol BRL 100 ug/L 100.0 BRL 35-138 MI Phenanthrene 34.6 20 ug/L 100.0 BRL 35 59-120 MI Phenol 10.6 20 ug/L 100.0 BRL 11 10-68 J Pyrene 38.5 20 ug/L 100.0 BRL 38 57-126 MI Surrogate: 2,4,6-Tribromophenol 32.8 ug/L 200.0 16 43-140 SE Surrogate:2-Fluorobiphenyl 25.3 ug/L 100.0 25 44-119 SE Surrogate:2-Fluorophenol 18.8 ug/L 200.0 9 19-119 SE Surrogate: Nitrobenzene-d5 17.8 ug/L 100.0 18 44-120 SE Surrogate: Phenol-d5 16.8 ug/L 200.0 8 11-52 SE Surrogate: Terphenyl-04 33.0 ug/L 100.0 33 50-134 SE This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 82 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Project: National Linen Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P010794 - 351 OC MS Matrix Spike Dup (P010794-MSD1) Source: 0090162-01 Prepared & Analyzed: 09/17/20 1,2,4-Trichlorobenzene 14.1 20 ug/L 102.0 BRL 14 29-116 46 30 D, MI, J 1,2-Dichlorobenzene 11.5 20 ug/L 102.0 BRL 11 32-111 52 50 D, MI, J 1,3-Dichlorobenzene 11.2 20 ug/L 102.0 BRL 11 28-110 53 50 D, MI, J 1,4-Dichlorobenzene 10.8 20 ug/L 102.0 BRL 11 29-112 56 50 D, MI, J 1-Methyl naphthalene 17.2 20 ug/L 102.0 BRL 17 41-119 45 50 Ml, J 2,4,5-Trichlorophenol 10.8 41 ug/L 102.0 BRL 11 53-123 43 50 MI, J 2,4,6-Trichlorophenol 9.80 41 ug/L 102.0 BRL 10 50-125 45 50 MI, J 2,4-Dichlorophenol 10.6 20 ug/L 102.0 BRL 10 47-121 39 50 MI, J 2,4-Dimethylphenol 11.4 20 ug/L 102.0 BRL 11 31-124 48 50 MI, J 2,4-Dinitrophenol BRL 100 ug/L 102.0 BRL 23-143 50 MI 2,4-Dinitrotoluene 16.9 20 ug/L 102.0 BRL 17 57-128 59 50 D, MI, J 2,6-Dinitrotoluene 17.3 41 ug/L 102.0 BRL 17 57-124 59 50 D, MI, J 2-Chloronaphthalene 17.3 41 ug/L 102.0 BRL 17 40-116 46 50 MI, J 2-Chlorophenol 10.0 20 ug/L 102.0 BRL 10 38-117 31 50 MI, J 2-Methyl naphthalene 16.0 20 ug/L 102.0 BRL 16 40-121 46 50 MI, J 2-Methylphenol 12.1 20 ug/L 102.0 BRL 12 30-117 26 50 MI, J 2-Nitroaniline 17.7 20 ug/L 102.0 BRL 17 55-127 56 50 D, MI, J 2-Nitrophenol 8.29 20 ug/L 102.0 BRL 8 47-123 46 50 MI, J 3,3'-Dichlorobenzidine 19.1 20 ug/L 102.0 BRL 19 27-129 52 50 D, MI, J 3/4-Methyl phenol 11.8 20 ug/L 102.0 BRL 12 29-110 12 50 MI, J 3-Nitroaniline 45.4 20 ug/L 102.0 BRL 44 41-128 13 50 4,6-Dinitro-2-methylphenol BRL 100 ug/L 102.0 BRL 44-137 50 MI 4-Bromophenyl phenyl ether 20.1 41 ug/L 102.0 BRL 20 55-124 47 50 MI, J 4-Chloro-3-methylphenol 12.9 20 ug/L 102.0 BRL 13 52-119 28 50 MI, J 4-Chloroaniline 57.8 20 ug/L 102.0 BRL 57 33-117 7 50 4-Chlorophenyl phenyl ether 19.6 41 ug/L 102.0 BRL 19 53-121 45 50 MI, J 4-Nitroaniline 26.3 20 ug/L 102.0 BRL 26 45-135 38 50 MI 4-Nitrophenol 10.5 20 ug/L 102.0 BRL 10 10-105 3 50 J Acenaphthene 17.9 20 ug/L 102.0 BRL 18 47-122 46 50 MI, J Acenaphthylene 19.8 41 ug/L 102.0 BRL 19 41-130 46 50 MI, J Aniline 48.5 100 ug/L 102.0 BRL 48 11-124 14 50 J Anthracene 23.0 20 ug/L 102.0 BRL 23 57-123 43 50 MI Azobenzene 18.5 20 ug/L 102.0 BRL 18 61-116 46 50 MI, J Benzo(a)anthracene 24.1 20 ug/L 102.0 BRL 24 58-125 38 50 MI Benzo(a)pyrene 27.1 20 ug/L 102.0 BRL 27 54-128 39 50 MI Benzo(b)fluoranthene 26.7 20 ug/L 102.0 BRL 26 53-131 38 50 MI Benzo(g,h,i)perylene 26.5 20 ug/L 102.0 BRL 26 50-134 40 50 MI Benzo(k)fluoranthene 24.4 20 ug/L 102.0 BRL 24 57-129 40 50 MI Benzoic Acid BRL 200 ug/L 102.0 BRL 10-125 50 MI Benzyl alcohol 36.2 20 ug/L 102.0 BRL 35 31-112 21 50 bis(2-Chloroethoxy)methane 14.2 20 ug/L 102.0 BRL 14 48-120 58 50 D, MI, J Bis(2-Chloroethyl)ether 8.55 20 ug/L 102.0 BRL 8 43-118 52 50 D, MI, J Bis(2-chloroisopropyl)ether 10.7 20 ug/L 102.0 BRL 10 37-130 58 50 D, MI, J Bis(2-Ethylhexyl)phthalate 27.8 20 ug/L 102.0 BRL 27 55-135 36 50 MI Butyl benzyl phthalate 23.7 20 ug/L 102.0 BRL 23 53-134 42 50 MI Chrysene 25.3 20 ug/L 102.0 BRL 25 59-123 38 50 MI This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 83 0f 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Project: National Linen Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Semivolatile Organic Compounds by GC/MS - Quality Control Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010794 - 351 OC MS Matrix Spike Dup (P010794-MSD1) Source: 0090162-01 Prepared & Analyzed: 09/17/20 Dibenzo(a,h)anthracene 22.7 41 ug/L 102.0 BRL 22 51-134 Dibenzofuran 18.0 41 ug/L 102.0 BRL 18 53-118 Diethyl phthalate 20.5 41 ug/L 102.0 BRL 20 56-125 Dimethyl phthalate 17.4 20 ug/L 102.0 BRL 17 45-127 Di-n-butyl phthalate 28.8 20 ug/L 102.0 BRL 28 59-127 Di-n-octyl phthalate 27.5 20 ug/L 102.0 BRL 27 51-140 Fluoranthene 26.0 20 ug/L 102.0 BRL 26 57-128 Fluorene 20.5 20 ug/L 102.0 BRL 20 52-124 Hexachlorobenzene 21.3 41 ug/L 102.0 BRL 21 53-125 Hexachlorobutadiene 16.1 41 ug/L 102.0 BRL 16 22-124 Hexachlorocyclopentadiene 15.8 41 ug/L 102.0 BRL 15 26-122 Hexachloroethane 11.4 20 ug/L 102.0 BRL 11 21-115 Indeno(1,2,3-cd)pyrene 32.0 20 ug/L 102.0 BRL 31 52-134 Isophorone 10.4 20 ug/L 102.0 BRL 10 42-124 Naphthalene 15.0 20 ug/L 102.0 BRL 15 40-121 Nitrobenzene 11.0 20 ug/L 102.0 BRL 11 45-121 N-Nitroso-di-n-propylamine 12.5 41 ug/L 102.0 BRL 12 49-119 N-Nitrosodiphenylamine 22.5 41 ug/L 102.0 BRL 22 51-123 Pentachlorophenol BRL 100 ug/L 102.0 BRL 35-138 Phenanthrene 22.6 20 ug/L 102.0 BRL 22 59-120 Phenol 9.82 20 ug/L 102.0 BRL 10 10-68 Pyrene 25.8 20 ug/L 102.0 BRL 25 57-126 Surrogate: 2,4,6-Tribromophenol 18.9 ug/L 204.1 9 43-140 Surrogate:2-Fluorobiphenyl 15.7 ug/L 102.0 15 44-119 Surrogate:2-Fluorophenol 16.5 ug/L 204.1 8 19-119 Surrogate: Nitrobenzene-d5 9.29 ug/L 102.0 9 44-120 Surrogate: Phenol-d5 16.2 ug/L 204.1 8 11-52 Surrogate: Terphenyl-04 23.9 ug/L 102.0 23 50-134 40 50 Ml, J 47 50 MI, J 46 50 MI, J 57 50 D, MI, J 39 50 MI 38 50 MI 37 50 MI 44 50 MI 41 50 MI, J 42 50 Ml, J 44 50 MI, J 45 50 MI, J 40 50 MI 58 50 D, MI, J 48 50 MI, J 59 50 D, MI, J 55 50 D, MI, J 51 50 D, MI, J 50 MI 42 50 MI 8 50 MI, J 39 50 MI SE SE SE SE SE SE This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 84 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Total Metals - Quality Control Analyte Batch P010770 - 3050B Level II QC Report 10/13/20 Project: National Linen Work Order: 0090162 Time Submitted: 9/15/2020 12:00:00PM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (P010770-BLK1) Prepared: 09/16/20 Analyzed: 09/17/20 Arsenic BRL 1.0 mg/kg wet Barium BRL 10 mg/kg wet Cadmium BRL 0.50 mg/kg wet Chromium BRL 1.0 mg/kg wet Lead BRL 1.0 mg/kg wet Selenium BRL 1.0 mg/kg wet Silver BRL 0.50 mg/kg wet LCS (P010770-BS1) Prepared: 09/16/20 Analyzed: 09/17/20 Arsenic 12.6 1.0 mg/kg wet 12.50 101 80-120 Barium 13.4 10 mg/kg wet 12.50 107 80-120 Cadmium 12.9 0.50 mg/kg wet 12.50 103 80-120 Chromium 13.2 1.0 mg/kg wet 12.50 106 80-120 Lead 12.8 1.0 mg/kg wet 12.50 103 80-120 Selenium 12.5 1.0 mg/kg wet 12.50 100 80-120 Silver 5.10 0.50 mg/kg wet 5.000 102 80-120 Batch P010799 - 3010A Blank (P010799-BLK1) Prepared: 09/17/20 Analyzed: 09/18/20 Arsenic BRL 0.020 mg/L Barium BRL 0.010 mg/L Cadmium BRL 0.0020 mg/L Chromium BRL 0.010 mg/L Lead BRL 0.0050 mg/L Selenium BRL 0.030 mg/L Silver BRL 0.0050 mg/L This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 85 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Total Metals - Quality Control Analyte Batch P010799 - 3010A Project: National Linen Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:00PM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (P010799-BLK2) Prepared: 09/17/20 Analyzed: 09/18/20 Arsenic BRL 0.020 mg/L Barium BRL 0.010 mg/L Cadmium BRL 0.0020 mg/L Chromium BRL 0.010 mg/L Lead BRL 0.0050 mg/L Selenium BRL 0.030 mg/L Silver BRL 0.0050 mg/L LCS (P010799-BS1) Prepared: 09/17/20 Analyzed: 09/18/20 Arsenic 0.493 0.020 mg/L 0.5001 99 80-120 Barium 0.502 0.010 mg/L 0.5000 100 80-120 Cadmium 0.497 0.0020 mg/L 0.5000 99 80-120 Chromium 0.498 0.010 mg/L 0.5001 100 80-120 Lead 0.496 0.0050 mg/L 0.5001 99 80-120 Selenium 0.498 0.030 mg/L 0.4999 100 80-120 Silver 0.192 0.0050 mg/L 0.2000 96 80-120 Batch P010809 - 7470A Blank (P010809-BLK1) Prepared & Analyzed: 09/18/20 Mercury BRL 0.00020 mg/L LCS (P010809-BS1) Prepared &Analyzed: 09/18/20 Mercury 0.00962 0.00020 mg/L 0.009375 103 80-120 Batch P010869 - 7471 B Blank (P010869-BLK1) Prepared &Analyzed: 09/21/20 Mercury BRL 0.050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 86 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Total Metals - Quality Control Analyte Batch P010869 - 7471 B Project: National Linen Reporting Result Limit Units Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:0OPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P010869-BSI) Prepared &Analyzed: 09/21/20 Mercury 0.395 0.050 mg/kg wet 0.4167 95 80-120 Matrix Spike (P010869-MS1) Source: 0090162-08 Prepared & Analyzed: 09/21/20 Mercury 0.464 0.057 mg/kg dry 0.4725 BRL 98 80-120 Matrix Spike Dup (P010869-MSD1) Source: 0090162-08 Prepared &Analyzed: 09/21/20 Mercury 0.464 0.057 mg/kg dry 0.4725 BRL 98 80-120 0.1 20 Post Spike (P010869-PSI) Source: 0090162-08 Prepared & Analyzed: 09/21/20 Mercury 4.82 ug/L 5.000 0.103 94 85-115 Batch POJ0158 - 3060A Blank (POJ0158-BLK1) Prepared: 10/09/20 Analyzed: 10/13/20 Hexavalent Chromium BRL 0.40 mg/kg wet LCS (POJ0158-BS1) Prepared: 10/09/20 Analyzed: 10/13/20 Hexavalent Chromium 15.9 0.40 mg/kg wet 16.00 100 80-120 LCS (POJ0158-BS2) Prepared: 10/09/20 Analyzed: 10/13/20 Hexavalent Chromium 16.3 0.40 mg/kg wet 16.00 102 80-120 LCS (POJ0158-BS3) Prepared: 10/09/20 Analyzed: 10/13/20 Hexavalent Chromium 16.2 0.40 mg/kg wet 16.00 101 80-120 LCS (POJ0158-BS4) Prepared: 10/09/20 Analyzed: 10/13/20 Hexavalent Chromium 16.2 0.40 mg/kg wet 16.00 101 80-120 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 87 of 93 (2) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 Total Metals - Quality Control Analyte Batch POJ0158 - 3060A Project: National Linen Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:00PM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Matrix Spike (POJ0158-MS1) Source: 0090162-08 Prepared: 10/09/20 Analyzed: 10/13/20 Hexavalent Chromium 18.1 0.45 mg/kg dry 18.14 BRL 100 60-119 Matrix Spike Dup (POJ0158-MSD1) Source: 0090162-08 Prepared: 10/09/20 Analyzed: 10/13/20 Hexavalent Chromium 18.3 0.45 mg/kg dry 18.14 BRL 101 60-119 0.7 20 Post Spike (POJ0158-PSI) Source: 0090162-08 Prepared: 10/09/20 Analyzed: 10/13/20 Hexavalent Chromium 0.416 mg/L 0.4000 0.00 104 85-115 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 88 of 93 Q) Waypoint. ANALYTICAL Proctor Environmental Services, Inc. Attn: Tom Proctor 5113 Yachtsman Ct. Raleigh, NC 27615 General Chemistry Parameters - Quality Control Analyte Project: National Linen Level II QC Report 10/13/20 Work Order: 0090162 Time Submitted: 9/15/2020 12:00:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P010783 - Solids, Dry Weight Duplicate (P010783-11DUP1) Source: 0090162-10 Prepared: 09/16/20 Analyzed: 09/17/20 % Solids 80.0 0.100 % by Weight 80.1 0.1 20 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 89 of 93 Sample Extraction Data Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 0090162-08 P010783 30 g 30 g 09/16/20 11:52 0090162-09 P010783 30 g 30 g 09/16/20 11:52 0090162-10 P010783 30 g 30 g 09/16/20 11:52 0090162-11 P010783 30 g 30 g 09/16/20 11:52 0090162-12 P010783 30 g 30 g 09/16/20 11:52 0090162-13 P010783 30 g 30 g 09/16/20 11:52 Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 0090162-01 P010794 1000 mL 1 mL 09/17/20 8:00 0090162-02 P010794 1000 mL 1 mL 09/17/20 8:00 0090162-03 P010794 1000 mL 1 mL 09/17/20 8:00 0090162-04 P010794 970 mL 1 mL 09/17/20 8:00 0090162-05 P010794 990 mL 1 mL 09/17/20 14:00 0090162-06 P010794 990 mL 1 mL 09/17/20 14:00 0090162-07 P010794 990 mL 1 mL 09/17/20 14:00 Prep Method: 3546 Lab Number Batch Initial Final Date/Time 0090162-08 P010771 30.03 g 1 mL 09/16/20 9:25 0090162-09 P010771 30.02 g 1 mL 09/16/20 9:25 0090162-10 P010771 30.36 g 1 mL 09/16/20 9:25 0090162-11 P010771 30.18 g 1 mL 09/16/20 9:25 0090162-12 P010771 30 g 1 mL 09/16/20 9:25 0090162-13 P010771 30.02 g 1 mL 09/16/20 9:25 Prep Method: 3010A Lab Number Batch Initial Final Date/Time 0090162-03 P010799 50 mL 50 mL 09/17/20 7:47 Prep Method: 3050E Lab Number Batch Initial Final Date/Time 0090162-08 P010770 2 g 50 mL 09/16/20 9:01 0090162-08 P010770 2 g 50 mL 09/16/20 9:01 0090162-09 P010770 2 g 50 mL 09/16/20 9:01 0090162-09 P010770 2 g 50 mL 09/16/20 9:01 0090162-10 P010770 2 g 50 mL 09/16/20 9:01 0090162-10 P010770 2 g 50 mL 09/16/20 9:01 0090162-11 P010770 2 g 50 mL 09/16/20 9:01 0090162-11 P010770 2 g 50 mL 09/16/20 9:01 0090162-12 P010770 2 g 50 mL 09/16/20 9:01 0090162-12 P010770 2 g 50 mL 09/16/20 9:01 0090162-13 P010770 2 g 50 mL 09/16/20 9:01 0090162-13 P010770 2 g 50 mL 09/16/20 9:01 Prep Method: 3060A Lab Number Batch Initial Final Date/Time 0090162-08 POJ0158 2.5 g 100 mL 10/09/20 11:35 0090162-13 POJ0158 2.5 g 100 mL 10/09/20 11:35 Prep Method: 7470A Lab Number Batch Initial Final Date/Time This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 90 of 93 Sample Extraction Data Prep Method: 7470A Lab Number Batch Initial Final Date/Time 0090162-03 P010809 20 mL 30 mL 09/18/20 9:20 Prep Method: 7471E Lab Number Batch Initial Final Date/Time 0090162-08 P010869 0.6 g 50 mL 09/21/20 11:51 0090162-09 P010869 0.6 g 50 mL 09/21/20 11:51 0090162-10 P010869 0.6 g 50 mL 09/21/20 11:51 0090162-11 P010869 0.6 g 50 mL 09/21/20 11:51 0090162-12 P010869 0.6 g 50 mL 09/21/20 11:51 0090162-13 P010869 0.6 g 50 mL 09/21/20 11:51 Prep Method: 5030E Lab Number Batch Initial Final Date/Time 0090162-01 P010844 10 mL 10 mL 09/18/20 10:00 0090162-02 P010844 10 mL 10 mL 09/18/20 10:00 0090162-03 P010844 10 mL 10 mL 09/18/20 10:00 0090162-04 P010844 10 mL 10 mL 09/18/20 10:00 0090162-05 P010844 10 mL 10 mL 09/18/20 10:00 0090162-06 P010844 10 mL 10 mL 09/18/20 10:00 0090162-07 P010844 10 mL 10 mL 09/18/20 10:00 0090162-14 P010844 10 mL 10 mL 09/18/20 10:00 0090162-15 P010844 10 mL 10 mL 09/18/20 10:00 Prep Method: 5035 Lab Number Batch Initial Final Date/Time 0090162-08 P010790 5.55 g 5 mL 09/16/20 13:13 0090162-09 P010790 6.2 g 5 mL 09/16/20 13:13 0090162-10 P010790 5.78 g 5 mL 09/16/20 13:13 0090162-11 P010790 5.85 g 5 mL 09/16/20 13:13 0090162-12 P010790 5.77 g 5 mL 09/16/20 13:13 0090162-13 P010790 5.97 g 5 mL 09/16/20 13:13 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 91 of 93 Waypoint. ANALYTICAL 449 Springbrook Road • Charlotte, NC 21217 Phone 7041529-6 • Fax: 704/525-0409 Client Company Name: (C � (ir Report To/Contact Name: Reporting Address: C IN OF CUSTODY RECORD PAGE of JQUOTE p TOENSURE P OPER BILLING: Project Name:. i} l� L fV Short Hold Analysis (Yes) No UST Project: (Yes (N "Please ATTACH any project specific reporting (QC LEVEL 1 11 provisions and/or QC Requirements Invoice To: Address: YES NO N/A Samples INTACT upon arrival? Received ON WET ICE? PROPER PRESERVATIVES indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES reed W10UT HEADSPACE? PROPER CONTAINERS used? _ �G • �� TEMP: Therm ID: 14- T-15 Observed 2 • Z °C !Corr. lam' Phone: Fax (Yes)(No): Email Address: Purchase Order No./Billing Reference Requested Due Data J 1 Day ❑ Days J 3 Days J 4 Days J 5 Days TO BE FILLEDIN BY CLIENT/SAMPLING PERSONNEL Certification: NELAC FL NC EDD Type: PDF Excel Other Working Days" ]&-9 Daysstandard 10 days J Pie ApprakveMdust Be �F(i' Site Location Name: Samples received after 14:00 will `processed next business day. SC OTHER htlA r Site Location Physical Address: / L Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES NO .ill (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT) Sample Iced Upon Collection; YES NO_ CLIENT DATE TIME COLLECTED MATRIX {SOIL, SAMPLE CONTAINER PRESERVA-� ANALYSIS REG) STIED 'TYPE NO. SITE SAMPLE DESCRIPTION COLLECTED MILITNARY WATER, OR TrVES l� REMARKS ID NO. HOURS SLUDGE) SEE BELOW �1 Q 4 0 X �4 f w s 5 x CA Cv'V3 r' 3mQ CIP a o 00o L Vy IT#a� r e ",_ T 9 3 X X a Sampler's PRESS DOWN FIRMLY - 2 COPIES P f, f Signature ampled By (Print Name) Affiliation ---. I Upon relinquishing, this Chain of Custody Is your authorization for Waypoint Analytical to proceed with the analyses as requested above. Any changes must be submitted in writing to the Waypoint Analytical Project Manager. There will be charges for any changes after analyses have been initialized. Relinquished By: (Signature) Received By (Sgnalure) pate MiKary/Hours Additional Comments: Site Arrival Time; Rellnqushed By: (Signature) Received Fly: (Signature) I�te � Site Departure Time: — Relinquished By: (Signature) Waypoint Analytical By: p to C Field Tech Fee: — ' • ✓" tZ '� I Tom/ Mettwd or Shipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUODY SEALS FOR TRANSPORT N THE Ld,$O TORY. CDC Group No. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINSFv ECENED AT THE 7=. Mileage: LABORAFri ❑UPS UHtnd-delivered C�WaypointAnelybcslFieldSgNice ❑ DES: UST: GROUNDWATER DRINKING WATER: SOLID WASTE: RCRA: BR NFLD J LANDFILL OTHER: �� v NC ❑ SG v NC ❑ SC ❑ NC ❑ SC U NC 'J SC I a0 NC n SC NC O SC NC ❑ SC NC ©SC � N 15C� ' U J U J{ 'CONTAINER TYPE CODES: A . Amber C = Clear J Q I za G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Mead Space) Page 92 of 93 Waypoint. ANALYTICAL 449 Springbrook Road • Charlotte, NC 21217 Phone 7041529-6 4 Fax: 7041525-0409 Client Company Name:_ %LOGS Report To/Contact Name, Reporting Address:_ CHAIN OF CUSTODY RECORD PAGE �C_ OF QUOTE N TOENSURE PROPER BILLING; l Project Name: --�,JI 0� -. "'' f Short Hold Analysis (Yes) (No) UST Project: (Yes) (NO) "Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) provisions and/or QC Requirements Invoice To: Address: _ NO NIA Samples INTACT upon arrival? Received ON WET ICE? PROPER PRESERVATIVES indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES reed WIOUT HEADSPACE? T PROPER CONTAINERS used; _ TEMP: Therm ID: j 4 -1 V Observed Phone: Fax (Yes)(No): �— Purchase Order NOJBIIIIng Reference TO BE FILLEDIN BY CLIENTISAMPLING-KRSONNEL Email Address: EDD Type: PDF_ Excel_Other Site Location Name: Requested Due Date 3 1 Day J 2 ays U 3 Days U 4 Days U 5 Days "Working Days" U 6-9 Days Standard 10 days J Rush Work Must Be Pre Approved Samples received after 14:00 will ocessed next business day Certification: NELAC� FL SC OTHER NC j� N/A Site Location Physical Address, Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS F CONDITIONS REGARDING SERVICES Water Chlorinated: YES— NO-- RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT) Sample iced Upon Collection: YES k NO_ CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER, OR SLUDGE] SAMPLE CONTAINER PRESERVA- TIMES ANALYSIS REQU TED �?fJ REMARKS //Z ID NO. 'TYPE SEE BELOW NO. SIZE .. S �r yoSo - - X "W — s 1610 ti �7y ,S t o-4+ 12, L see f o Sampler's Signature Sampled By (Print Name) _ Affiiiation PRESS DOWN FIRMLY - 2 COPIES Upon relinquishing, this Chain of Custody is your authorization submitted In writing to the Waypoint Analytical Project for Waypoint Analytical to proceed with the analyses as requested above. Any changes must be Manager. There will be charges for any changes after analyses have been initialized. Relinquished By: (Signature) Received By: (Signature) Date MilltarylHours Additional Comments: Site Arrival Time: Relinquished By: (Signature) Received By: (Signature) Date Site Departure Tlms, Relinquished By: (Signature) Received For Waypoint Analytical By: i ��D11ate " 1 ' ' 1 Q %� J Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FORT T10N TO THE LAB ORY. CDC Group No. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORA RY. r O n Ex D UPS Q Hand -delivered ❑ Waypoint Analybca) Field Service ❑ Other NPDES: UST. TER ATHR: LCIb LANDFILL HE Field Tech Fee: Mileage: U SCTE: CJ NC Q SC Z) NCGRO❑ SC NCDRINKI❑ SC Q SC NCISIRWFLD ❑ SC I NC SC I LNC ❑ SC NC ❑ SC IJ Ll jj LJ O UNC 0 Page 93 of 93 "rnAtTAimr-R Tvpp rnnFC• A a a—har r = rlaar (:= Glass P - Plastic: TL = T.fl, ...Llnsd Can VOA = v.,i.m. n.,.�. i— enslvatc f7arn �A Qnarnl C)RIGINAL