23080_Almont Shipping 2_OAR_20050630

*731HSSF4018*
DocumentlD NONCD0001250
Site Name ALMONT SHIPPING
DocumentType Site Assessment Rpt (SAR)
Rpt5egment 1
DocDate 6/30/2005
DocRcvd 2/20/2007
Box SF4018
AccessLevel PUBLIC
Division WASTE MANAGEMENT
Section SUPERFUND
Program IHS (IHS)
DocCat FACILITY

�` y
lC'k ,0.r Y
s
40 COMPREHENSIVE SITE ASSESSMENT LJUL tl 1 20U6
ALMONT SHIPPING TERMINALS
ONE HANOVER STREET-
WILMINGTON, NEW HANOVER COUNTY, NORTH CAROLINA
June 30, 2005
Responsible Party:
Almont Shipping Terminals
One Hanover Street
P.O. Box 1726
Wilmington, North Carolina 28402-1726
[phone]
Attention: Sidney Camden
Current Property Owner:
Almont Shipping Terminals
One Hanover Street
P.O. Box 1726
Wilmington, North Carolina 28402-1726
[phone]
Attention: Sidney Camden
Consultant:
Babb & Associates, P.A.
P.O. Box 37697
Raleigh, North Carolina 27627
[phone]
Release Discovery Date: 1997-2004
Cause and Source of Release: Leaking USTs, Materials Bulk Storage
Latitude: 340 14' 40", Longitude: 770 57' 00"
1'$geaeae��cc,�
F •°e y e
Gary . Ba , P.G. f SE AL
Preside = 488 _
`•cF
aEOG\��" �9
''BBC'as OOG G00 A9%y0

ALMONT SHIPPING TERMINALS
J�'K T FR
OEST. I, 1870
July 1, 2005 JUL, 0 7 Z005
Dr. Charles Stehman
Aquifer Protection Supervisor
NC Department of Environment
And Natural Resources
127 Cardinal Drive Extension
Wilmington, NC 28405
Dear Dr. Stehman:
Please find enclosed one copy of the completed COMPREHENSIVE SITE
. ASSESSMENT for the Almont Shipping property.
We look forward to our meeting with you on July 7, 2005 to discuss this with you.
Sincerely,
r
Donalde�verman
Chief Executive Officer
Enclosure
One Hanover Street • P.O. Box 1726 9 Wilmington, NC 28402-1726 9 Phone: [phone] • Fax: [phone]

Almont / PPD Strategy:
1. PPD has agreement with the city to pretreat dewater water and send to north /
south side treatment plant
2. This dewatering program will end at some near time in the future.
3. Marina configuration will extent nearly to Nutt Street
4. Discharge to the river should be intercepted and sent to the former PPD
pretreatment system
5. Monitoring on PPD site and down gradient of interceptor system should continue
until compliance is achieved
6. Is PCP area north of Front Street property of Almont of PPD?
w

N
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street, Wilmington New Hanover County, North Carolina
0 1.0 EXECUTIVE SUMMARY
1.1 Source Information
The Almont Shipping facility is located west of North Front/Second Street in
Wilmington, North Carolina and consists of an approximately 28-acre parcel of land that
once contained numerous buildings associated with Almont Shipping's bulk shipping and
storage operations (hereinafter referred to as the "Site"). The subject Site is bordered to
the north by industrial property, to the east by industrial and institutional properties, to the
south by commercial and vacant properties, and to the west by the Cape Fear River. The
subject and nearby properties are shown in Figures 1 and 2.
Almont Shipping has occupied various portions of the Site since as early as 1965 and has
used it since that time as a bulk commodity shipping terminal. However, portions of the
Site itself have reportedly been used since 1870 up until 1965 by others also as a
shipping/terminal facility.
• Most recently, Almont Shipping has used the Site for receiving, storing and shipping bulk
pelletized urea, chromium ore, salt and salt cake. Historical uses of the Site also include
the storage and distribution of potash, zircon sand, granite, limestone, canola meal,
calcium nitrate, ammonium nitrate and iron ore pellets. The southeastern portions of the
Site were also once owned and utilized by Standard Oil Company for the bulk storage of
petroleum products from 1893 up until about 1951.
Past soil and groundwater studies completed at the Site by others determined that the
major subsurface soil and groundwater contaminants identified at the Site are
tetrachloroethene (PCE), trichloroethene (TCE), arsenic, nitrates, total nitrogen,
ammonia, sulfate and chloride. The presence of total nitrates, nitrogen, ammonia sulfate
and chloride at the Site can be attributed to its past association with handling and storage
of nutrients including: urea, calcium nitrate, ammonium nitrate, salt and salt cake.
However, there is no known source(s) for the arsenic, PCE and TCE detected during the
previous investigations.
In addition to the contaminants described above, the Site also has a long association with
petroleum products including its partial use by Standard Oil Company as a petroleum

Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street, Wilmington, New Hanover County. North Carolina
• bulk storage facility from 1893 up until about 1951. The most notable petroleum incident
was a release (due to structural failure) from a 2.5 million -gallon diesel above ground
storage tank that occurred in 1982 at the former CSX facility located immediately north
of the Site. It was reported that approximately 2,486,000 gallons of diesel was released
and approximately 2,437,000 gallons were recovered. While the majority of the diesel
fuel was recovered it is likely that a petroleum groundwater contaminant plume has
impacted the northernmost portions of the Site.
A second potential off -Site petroleum source is an empty lot located immediately south of
the Site and adjacent to the Cape Fear River. This property was reportedly once used for
the bulk storage of petroleum products as evidenced by the presence of weathered free
product tentatively identified as diesel fuel that was found to accumulate in monitoring
well MW-11 installed for completion of this CSA.
Finally, it should be noted that the Site itself once contained three known petroleum
Underground Storage Tanks (USTs), all of which have subsequently been removed. One
of these tanks may explain the presence of free product tentatively identified as diesel fuel
is in monitoring well MW-16 located immediately adjacent to the former UST area.
See Figure 1 for Site location map and Figure 2 for Site map with monitoring well and
former contaminant source locations.
1.2 Initial Abatement/Emergency Response Information
The releases discussed above were confirmed by two investigations completed by others'
that identified the presence of tetrachloroethylene (PCE), trichloroethylene (TCE),
arsenic, total nitrogen, ammonia, sulfate and chloride at various locations throughout the
Site. Due to the commencement of redevelopment activities there will soon be no
pelletized urea or salt stored at the Site. With removal of these contaminant sources the
total nitrogen, nitrates, ammonia, sulfate and chloride concentrations in soil and
1 "Phase H Environmental Site Assessment of Almont Shipping +/- 6.8 Acres SW Corner of Harnett Street
and North Street, Wilmington, North Carolina" prepared by Land Management Group, Inc., October 11,
2004. and;
• "Phase II Environmental Site Assessment of Almont Shipping Office 1.25 Acres One Hanover Street,
Wilmington, North Carolina" prepared by Land Management Group, Inc., January 11, 2005.

4
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street. Wilmington New Hanover Coun!L North Carolina
groundwater are expected to decline as the processes of natural attenuation and
biodegradation begin to absorb and break down these contaminants. Further, the
northeastern portion of the Site has been excavated and is currently being dewatered for
the construction of an office building to be completed in this area. While this dewatering
process is being completed for construction purposes it is also resulting in the disposal of
a large volume of groundwater contaminated by arsenic, total nitrogen, nitrates, ammonia,
sulfate and chloride.
Finally, while the petroleum and PCE contamination is not being cleaned up by the
construction operations, the sources of these contaminants are believed to have been
removed and these contaminant concentrations are also expected to decline as the
processes of natural attenuation and biodegradation absorb and break down these
contaminants.
1.3 Receptor Information
IDNo water supply wells are known to be located within 1,500-feet of the Site.
The Site and locations within 1,500-feet of the release area are supplied water by the City
of Wilmington municipal water supply. The City of Wilmington maintains buried water
lines that supply potable water to the Site and surrounding properties, as well as buried
sanitary and storm sewer lines. The nearest surface water body is the Cape Fear River,
which is immediately adjacent and west of the Site. No wellhead protection zones were
identified within 1,000-feet of the site. The Site does lie within the Coast Plain
Physiographic Region.
The only known receptor is the Cape Fear River located immediately adjacent to the
western portion of the Site.
0

W
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street. Wilmington New Hanover County, North Carolina
• 1.4 Sampling/Investigative Results
1.4.1 May 10 - May 17, 2005 Soil Sampling Event
Analytical data for soil samples collected at an average depth of 1 to 2 feet below land
surface were obtained while installing fifteen groundwater monitoring wells during the
time period of May 10 - May 17, 2005. If possible, the soil samples were collected from
above the water table and also screened using an Organic Vapor Analyzer (OVA). Split
samples were also immediately placed into laboratory supplied bottles for submittal to the
analytical laboratory.
All of the borings were later converted to monitoring wells for the collection of
groundwater samples and also to establish the depth to groundwater and the hydraulic
gradient in the shallow aquifer.
The soil samples were submitted to Paradigm Analytical Laboratories of Wilmington, NC
(NCDENR laboratory certification # 481) for laboratory analysis by EPA 8260 for
• volatile organic compounds and also for total RCRA metals, chloride, sulfate, nitrate,
T.K.N, ammonia, phosphorus and total nitrogen.
Soil analytical results indicated the presence of minor levels of volatile organic
compounds in only three of the fifteen soil samples submitted for laboratory analysis.
However, ammonia, chloride, nitrates, phosphorus, sulfate, arsenic, barium, cadmium,
chromium, lead and mercury were detected in many of the soil samples submitted for
laboratory analysis.
There are currently no Soil to Groundwater Maximum Soil Contaminant Concentrations
set forth by the North Carolina Department of Environment and Natural Resources
(NCDENR) Groundwater Section or Soil Screening Levels established by the North
Carolina Hazardous Waste Section for the ammonia, chloride, nitrates, phosphorus and
sulfate detected in the soils during this investigation.
The (NCDENR) Hazardous Waste Section has established Soil Screening Levels for total
RCRA metals including the arsenic, barium, cadmium, chromium, lead and mercury
0

Z
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmineton New Hanover County, North Carolina
• detected in the soils. Finally, arsenic, chromium and mercury levels exceeded their Soil
Screening Levels in several of the soil samples submitted for laboratory analysis.
A soil isoconcentration map for selected contaminants has been prepared and can be
found in Figure 3. Table 1 is a summary of analytical results for the May 2005 sampling
events. Laboratory reports for this sampling event are presented in Appendix C.
1.5 Groundwater Samples
1.5.1 May 25, 2005 Groundwater Sampling Event
Groundwater sampling for completion of this CSA was conducted on May 25, 2005 and
included the installation and sampling of newly installed groundwater monitoring wells
MW-1 through MW-15, DW-1, DW-2 and existing wells MW-16 and LMW-13.
Monitoring wells MW-1 through MW-15 were all installed to roughly 12 feet beneath
surface grade with the well screen placed from 2 to 12 feet below land surface. DW-1
• and DW-2 were both installed to a total depth of 40 feet below land surface and screened
from a depth of 35 to 40 feet below land surface. All permanent monitoring wells
installed by Babb & Associates were constructed using 2" diameter PVC slotted screens
and solid PVC riser pipe with the exception of DW-1 which was completed as a double
cased Type III monitoring well.
All of the monitoring wells discussed previously were sampled on May 25, 2005 and the
samples submitted to Paradigm Analytical Laboratories of Wilmington, NC (NCDENR
laboratory certification # 481) for chemical analysis by EPA Method 8260 (volatile
organic compounds) and also for total RCRA metals, chloride, sulfate, nitrate, T.K.N,
ammonia, phosphorus and total nitrogen.
All of the sampling activities described above were completed using new disposable
bailers and nitrile sampling gloves. All of the monitoring wells were developed using
disposable PVC bailers prior to collecting groundwater samples.
Groundwater samples obtained from the groundwater monitoring wells described above
• and analyzed by EPA Method 8260 revealed the presence of several compounds in the

7
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street, Wilmington New Hanover County, North Carolina
• samples collected from monitoring wells MW-1, MW-2, MW-8, MW-16, and LMW-13
at concentrations in excess of their method detection limits. However, only
tetrachloroethene (PCE) (detected in MW-1, and LMW-13 at concentrations of 0.00217
and 1.600 mg/l, respectively), trichloroethene (TCE) (detected in MW-1 and LMW-13 at
concentrations of 0.00562 and 0.024 mg/l, respectively), naphthalene (0.0452 mg/1 in
MW-2), and 4-isopropyltoluene (MW-1 at 0.140 mg/1) were detected at concentrations in
excess of their maximum allowable levels as set forth in the 15A NCAC 2L .0202 upon
testing by this analytical method.
Groundwater samples obtained from the groundwater monitoring wells described above
and analyzed for nutrients revealed the presence of one or more compounds including
chloride, nitrates and sulfates in the samples collected from monitoring wells MW-3
through TMW-15 at concentrations in excess of their maximum allowable levels set forth
in the 15A NCAC 2L .0202 upon analytical testing.
Finally the groundwater samples analyzed for total RCRA metals revealed the presence of
arsenic, lead, mercury and selenium in several of the groundwater samples submitted for
• analysis at concentrations in excess of their maximum allowable levels set forth in 15A
NCAC 2L .0202 upon analytical testing.
Isoconcentration maps for selected groundwater contaminants have been prepared and
can be found in Figures 4 through 11. Table 2 is a summary of analytical results for the
May 25, 2005 sampling event. Laboratory reports for this sampling event are presented
in Appendix C.
1.6 Site Specific Conditions Related to Risk Classification
Site -specific conditions related to risk classification at the location include:
1) The availability of potable water at the Site.
2) The proximity to nearby receptors including the Cape Fear River.
0

1
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover County, North Carolina
• 1.7 Conclusions and Recommendations
Babb & Associates has completed this Comprehensive Site Assessment in order to
comply with NCGS 143-215.84, NCAC 15A, 2L .0106(g) and the NCDENR
Groundwater Section's, "Guidelines for Investigation and Remediation of Soil and
Groundwater", Effective July 2000.
Babb & Associates concludes from the investigative activities conducted for completion
of this CSA that several separate releases on the Site have impacted the Site's soils and
surficial groundwater aquifer at more than one location.
Free phase petroleum product identified as weathered diesel fuel has been identified in
on -Site groundwater monitoring well MW-17 and off -Site monitoring well MW-11.
Analytical results for soil samples collected for completion of CSA activities identified
the presence of targeted contaminants at levels in excess of their Soil Screening Levels for
arsenic, chromium and mercury in several of the soil samples submitted for laboratory
analysis.
Analytical results for the groundwater samples collected for completion of this CSA
detected tetrachloroethene, trichloroethene, naphthalene 4-isopropyltoluene, chloride,
nitrates, sulfates, arsenic, lead, mercury and selenium at concentrations in excess of their
maximum allowable levels as set forth in the 15A NCAC 2L .0202 upon laboratory
testing.
The risk criteria pertaining to the releases at the Site include the following: 1) MW-17
contains free phase product identified as weathered diesel fuel; 2) there are no potable
water supply wells located within 1,000 feet of the source area; 3) the Cape Fear River is
located immediately west of the Site; 4) the Site is used for commercial purposes; 5) the
Site is surrounded by a mix of commercial properties; and 6) the Site is located in the
Coastal Plain Physiographic Province.
Babb & Associates recommends that the Almont Shipping submit a copy of this CSA to
the NCDENR-DWQ, Wilmington Regional Office, to the attention of Mr. Charles
• Stehman.

GJ
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilminl*ton New Hanover County, North Carolina
• TABLE OF CONTENTS
1.0 EXECUTIVE SUMMARY...................................................................................2
1.1
SOURCE INFORMATION..............................................................................................2
1.2
INITIAL ABATEMENT/EMERGENCY RESPONSE INFORMATION....................................3
1.3
RECEPTOR INFORMATION..........................................................................................4
1.4
SAMPLING/INVESTIGATIVE RESULTS.........................................................................5
1.4.1
May 10 - May 17, 2005 Soil Sampling Event.......................................................5
1.5
GROUNDWATER SAMPLES........................................................................................6
1.5.1 May 25, 2005 Groundwater Sampling Event.......................................................6
1.6 .
SITE SPECIFIC CONDITIONS RELATED TO RISK CLASSIFICATION................................7
1.7
CONCLUSIONS AND RECOMMENDATIONS..................................................................8
TABLEOF CONTENTS..................................................................................................9
2.0
SITE HISTORY AND SOURCE CHARACTERIZATION ...........................12
3.0
RECEPTOR INFORMATION...........................................................................14
3.1
WATER SUPPLY WELLS..........................................................................................14
3.2
PUBLIC WATER SUPPLIES........................................................................................14
3.3
SURFACE WATER....................................................................................................14
•
3.4
WELLHEAD PROTECTION AREAS.............................................................................14
3.5
DEEP AQUIFERS IN THE COASTAL PLAIN PHYSIOGRAPHIC REGION .........................14
3.6
SUBSURFACE STRUCTURES.....................................................................................16
3.7
LAND USE...............................................................................................................16
3.8
PROPERTY OWNERS AND OCCUPANTS....................................................................16
3.9
POSSIBLE HUMAN EXPOSURE..................................................................................17
4.0
REGIONAL GEOLOGY AND HYDROGEOLOGY......................................18
4.1
SITE GEOLOGY AND HYDROGEOLOGY....................................................................18
4.2
REGIONAL HYDROGEOLOGY...................................................................................19
5.0
SOIL SAMPING RESULTS...............................................................................21
5.1
SOIL BORING INSTALLATIONS (MAY 10 -17, 2005)...............................................21
6.0
GROUNDWATER INVESTIGATION.............................................................23
6.1
LOCATION AND INSTALLATION OF MONITORING WELLS.........................................23
6.2
MAY 25, 2005 SAMPLING EVENT............................................................................24
7.0
FREE PRODUCT INVESTIGATION AND RECOVERY .............................26
7.1
FREE PRODUCT INVESTIGATION..............................................................................26
8.0
HYDROGEOLOGIC INVESTIGATION.........................................................26
8.1
HORIZONTAL GROUNDWATER HYDRAULIC GRADIENT...........................................26

•
Ll
0
10
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street, Wilmington New Hanover County, North Carolina
8.2 VERTICAL GROUNDWATER GRADIENT....................................................................27
8.3 AQUIFER TESTING...................................................................................................27
8.3 GROUNDWATER MODELING RESULTS.....................................................................28
9.0 DISCUSSION.......................................................................................................29
9.1 NATURE AND EXTENT OF CONTAMINATION............................................................29
9.2 CONTAMINANT MIGRATION AND POTENTIALLY AFFECTED RECEPTORS .................29
9.3 LOWERING RISK CLASSIFICATION...........................................................................30
9.4 APPLICABLE CLEANUP LEVELS...............................................................................30
10.0 CONCLUSIONS AND RECOMMENDATIONS.............................................32
REFERENCES.................................................................................................................33

•
11
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover County, North Carolina
APPENDICES
Figures
Figure 1
Area Location Map
Figure 2
Site Map with Release and Monitoring Well Locations
Figure 3
Soil Contaminant Isoconcentration Map (chloride, nitrates, arsenic,
mercury)
Figure 4
Groundwater Contaminant Isoconcentration Map (Chloride)
Figure 5
Groundwater Contaminant Isoconcentration Map (Nitrates)
Figure 6
Groundwater Contaminant Isoconcentration Map (Sulfates)
Figure 7
Groundwater Contaminant Isoconcentration Map (Arsenic)
Figure 8
Groundwater Contaminant Isoconcentration Map (PCE)
Figure 9
Contaminant Cross -Section Location Map.
Figure 10
Soil Contaminant Cross -Section A -A'.
Figure 11
Soil Contaminant Cross -Section B-B'.
Figure 12
Groundwater Hydraulic Gradient Map (May 24, 2005)
Figure 13
Groundwater Hydraulic Gradient Map (June 16, 2005)
Tables
Table 1
Results of Soil Samples
Table 2
Results of Groundwater Samples
Table 3
Monitoring Well Construction Data
Table 4
Results of Monitoring Well Gauging
Appendix A Boring Logs/Well Construction Records
Appendix B Aquifer Testing Results
Appendix C Laboratory Reports
11

12
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street. Wilmington New Hanover County. North Carolina
• 2.0 SITE HISTORY AND SOURCE CHARACTERIZATION
The Almont Shipping facility is located west of North Front/Second Street in
Wilmington, North Carolina and consists of an approximately 28-acre parcel of land that
once contained numerous buildings associated with Almont Shipping's bulk shipping and
storage operations (hereinafter referred to as the "Site"). The subject Site is bordered to
the north by industrial property, to the east by industrial and institutional properties, to the
south by commercial and vacant properties, and to the west by the Cape Fear River. The
subject and nearby properties are shown in Figures 1 and 2.
Almont Shipping has occupied various portions of the Site since as early as 1965 and has
used it since that time as a bulk commodity shipping terminal. However, portions of the
Site itself have also reportedly been used from 1870 up until 1965 by others also as a
shipping/terminal facility.
Most recently, Almont Shipping has used the Site for receiving, storing and shipping bulk
pelletized urea, chromium ore, salt and salt cake. Historical uses of the Site also include
the storage and distribution of potash, zircon sand, granite, limestone, canola meal,
calcium nitrate, ammonium nitrate and iron ore pellets. The southeastern portions of the
Site were also once owned and utilized by Standard Oil Company for the bulk storage of
petroleum products from 1893 up until about 1951.
Past soil and groundwater studies completed at the Site by others determined that the
major subsurface contaminants identified at the Site are tetrachloroethene (PCE),
trichloroethene (TCE), arsenic, nitrates, total nitrogen, ammonia, sulfate and chloride.
The presence of total nitrates, nitrogen, ammonia sulfate and chloride at the Site can be
attributed to its past association with handling and storage of nutrients including: urea,
calcium nitrate, ammonium nitrate, salt and salt cake. However, there is no known source
for arsenic, PCE and TCE detected during the previous investigations.
In addition to the contaminants described above the Site also has a long association with
petroleum products including its partial use by Standard Oil Company as a petroleum
bulk storage facility from 1893 up until about 1951. The most notable petroleum incident
was a release (due to structural failure) from a 2.5 million -gallon diesel above ground
0 storage tank that occurred in 1982 at the CSX facility located immediately north of the

13
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street, Wilmington New Hanover County, North Carolina
', Site. It was reported that approximately 2,486,000 gallons of diesel was released and
approximately 2,437,000 gallons were recovered. While the majority of the diesel fuel
was recovered it is likely that a groundwater contaminant plume has impacted the
northernmost portion of the Site.
A second potential off -Site petroleum source is an empty lot located immediately south of
the Site and adjacent to the Cape Fear River. This property was reportedly once used for
the bulk storage of petroleum products as evidenced by the presence of weathered free
product tentatively identified as diesel fuel that was found to accumulate in monitoring
well MW-11 installed for completion of this CSA.
Finally, it should be noted that the Site itself once contained three known petroleum
Underground Storage Tanks (USTs), all of which have subsequently been removed. One
of these tanks may explain the presence of free product tentatively identified as diesel fuel
in monitoring well MW-16 located on -Site and immediately adjacent to the former UST
area.
See Figure 1 for Site location map and Figure 2 for Site map with monitoring well and
former contaminant source locations.)
0

•
14
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street, Wilmington New Hanover County North Carolina
3.0 RECEPTOR INFORMATION
3.1 Water Supply Wells
No known water supply wells are located within 1,500-feet of the release. The Site and
locations within 1,500-feet of the release area are supplied water by City of Wilmington
municipal water supply.
3.2 Public Water Supplies
The City of Wilmington has installed buried water lines that supply potable water to the
subject Site.
3.3 Surface Water
rThe nearest surface water body is the Cape Fear River, located immediately adjacent and
west of the Site.
3.4 Wellhead Protection Areas
No wellhead protection zones were identified within 1,500-feet of the Site.
3.5 Deep Aquifers in the Coastal Plain Physiographic Region
The Site and New Hanover County are underlain by sediments ranging in age from
Cretaceous to Holocene. These sediments occur in layers most of which tend to slope at
low angles towards the Atlantic coast. They are composed of sands, clays, and limestone
and lie on a floor of hard consolidated granitic bedrock at a depth of about 1,100 feet
below land surface. A large volume of water is stored in sediments of the Coastal Plain,
0

15
Comprehensive Site Assessment
Ahnont Shipping Terminals
One Hanover Street, Wilmington New Hanover County, North Carolina
. but sediments below depths of approximately 300-feet contain water that is too salty for
normal use2.
The usable groundwater at the Site occurs in three major aquifers. The uppermost aquifer
is that of surficial sands, of Miocene and Pleistocene age. This aquifer is replenished by
precipitation directly. This is the aquifer that has been impacted by contaminants at the
Site. Babb & Associates installed "deep profile" well DW-I to a depth of 40-feet below
land surface at the Site as part of this CSA. This surficial sand aquifer was found down
to a depth of 18 feet below land surface followed by a brown -tan clay layer from 18 to 28
feet below land surface. From 28 to 40 feet below land surface alternating layers of sand,
clay and limestone were encountered. Deep well DW-2 was installed to a depth of 40
feet below land surface and only the surficial Pleistocene sands were found throughout
the length of this boring.
Below the surficial Pleistocene aquifer is the Castle Hayne Limestone of Eocene age.
This limestone unit is reportedly thin in the vicinity of the Site as it was deposited in
channels on top of the underlying Peedee Formation. The irregular thickness of this
• formation can also be attributed to its deposition on an eroded surface of the upper
Peedee Formation and from subsequent erosion and solution of the upper surface of the
Castle Hayne. The bottom of the Castle Hayne consists of a basal shell conglomerate
containing much overworked material from the Peedee Formation. Above this is
glauconitic shell limestone. It is light gray toward the top and yellow dolomitic toward
the bottom. This shell facies is overlain by a dense, chalk white siliceous limestone that
contains phosphate at its base. This limestone which is referred to as "cap rock" averages
about three feet in thickness throughout the county. Overlying the "cap rock" is a cream
to light green glauconitic, bryazoan-bearing "shell hash". The Castle Hayne Formation
can yield as much as 650 gallons per minute (gpm) but generally yields closer to 150
gpm.
Underlying the Castle Hayne Limestone and normally separated from it by some
relatively impermeable clays is the sandstone Peedee Formation of Late Cretaceous age.
The Peedee Formation typically consists of unconsolidated greenish -gray to dark gray silt,
. 2Reference: Bain, George L., "Geology and Groundwater Resources of New Hanover County, North Carolina", North Carolina
Department of Water Resources, Division of Groundwater. Bulletin 17

16
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street. Wilmington New Hanover County, North Carolina
olive-green to gray sand, and massive black clay interbedded with consolidated
calcareous sandstone and impure limestone. It yields 200 gpm to many wells and in
excess of 400 gpm in some cases. This aquifer is generally separated from underlying
beds containing salty water by 100 to 150-feet of relatively impermeable clay. The top of
the Peedee Formation is generally expected to be approximately 20 to 30-feet below land er�l
surface in the vicinity of the Site. A nearby supply well found that the Peedee formation
is approximately 700 feet thick in the vicinity of the Site. Although each of the aquifers
is to a great degree a separate unit, the less permeable material between the aquifers
allows some interchange of water
3.6 Subsurface Structures
Subsurface structures located throughout the Site include buried water supply, storm
water and storm sewer lines.
3.7 Land Use
The Site is an approximately 28-acre parcel of land owned by Almont Shipping that was
most recently used for receiving, storing and distributing bulk pelletized urea, chromium
ore, salt and salt cake. Historical uses of the Site also include the storage and distribution
of potash, zircon sand, granite, limestone, canola meal, calcium nitrate, ammonium
nitrate and iron ore pellets.
3.8 Property Owners and Occupants
Properties immediately adjacent to the subject property are commercial and industrial.
Adjacent properties to the north included a vacant CSX Transportation tract and
additional Almont property not part of this ESA. Adjacent properties to the east are
commercial (Salvation Army and a Greyhound Bus Lines bus station), institutional (Cape
Fear Community College facilities), and parking areas. Adjacent properties to the south
are commercial (WWAY TV Channel 3 studio) and institutional (Cape Fear Community
College facilities). Additional Almont property not part of this ESA and the Northeast
Cape Fear River are west of the subject property. The subject property is located in an
0

17
Comprehensive Site Assessment
Ahnont Shipping Terminals
One Hanover Street. Wilmington New Hanover County. North Carolina
iarea of Wilmington that has been developed for industrial/commercial purposes for many
years.
3.9 Possible Human Exposure
If the soils identified as containing the elevated nutrient and metals concentrations are left
buried and undisturbed, human contact is unlikely. If they are disturbed it is probable that
the ammonia, nitrates, phosphorus and sulfate will breakdown and dissipate rather rapidly
upon exposure to the atmosphere. Finally, the most likely route of human exposure
would initially be through inhalation. However, the nutrient levels in air would be
expected do decline with time after the soils have been exposed to the atmosphere. Also,
after the planned development of the Site is complete, most of the soil will be covered
with buildings or parking areas, thereby restricting access to the contaminants.
0,

IV
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover County, North Carolina
4.0 REGIONAL GEOLOGY AND HYDROGEOLOGY
4.1 Site Geology and Hydrogeology
The U.S. Geological Survey Map (Wilmington, N.C. Quadrangle) identifies the Site as
having an elevation ranging from approximately 39 to 19 feet above sea level. The
subject property generally slopes from the east, along North Front Street, to the west,
toward the Northeast Cape Fear River. The Site has been graded to accommodate facility
components including warehouses, office buildings, storage pads, and railroad tracks.
The Soil Survey of New Hanover County, North Carolina3 prepared by the USDA Soil
Conservation Service (1977), the subject property is comprised of one soil type. The
entire property consists of Urban Land (Ur). Urban land consists of areas where the
original soil has been cut, filled, graded, paved, or otherwise reworked so that most soil
properties have been altered to such an extent that a soil series is not recognizable.
The Geologic Map of North Carolina4 describes the subject Site as being located in the
Coastal Plain Physiographic Province of North Carolina, in an area defined as the Peedee
Formation of Cretaceous Age. This formation is described as sand, clayey sand, and
sand, greenish gray to olive black, massive, glauconitic, locally fossiliferous and
calcareous with patches of sandy molluscan -mold limestone in the upper part.
Unsaturated soils encountered while completing the shallow soil borings and monitoring
wells installed for this CSA consisted of tan -brown -black well sorted medium grained
sand.
Groundwater in the monitoring wells installed throughout the release areas was found to
range in depth from approximately 0.4 to 6-feet beneath surface grade.
3,Reference: Soil Survey, New Hanover County, North Carolina. United States Department of Agriculture, Soil Conservation
Service, In cooperation with North Carolina Agriculture Experiment Station and the New Hanover County Board of Commissioners.
4Reference: Geologic Map of North Carolina, Department of Natural Resources and Community Development, Division of Land
Resources, 1985 edition.

19
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street. Wilmington New Hanover County, North Carolina
• 4.2 Regional Hydrogeology
The deposits underlying New Hanover County may be grouped according to their ability
to transmit water. The chief water bearing zones or aquifers in New Hanover County are:
1) undifferentiated surface deposits consisting of beds of sand and coquina at the land
surface; 2) sandy limestone in the underlying Castle Hayne Formation; and 3) the
indurated calcareous sand in the upper part of the Peedee Formations.
The undifferentiated surface deposits include terraced materials and related beach sands,
the present day beaches, sandy coquina beds marking Pleistocene beaches and inlets, high
fossil sand dunes, Pleistocene channels filled with coarse sand and silty interstream
deposits. This surface material contains the uppermost water bearing body and the
configuration of the water table approximates that of land surface.
The Castle Hayne Formation underlies the undifferentiated surface deposits. This
formation is absent in an area west and northwest of Wilmington but it obtains a
thickness of more than 100 feet in the southeastern portion of New Hanover County. It is
predominately a sandy shell limestone but in some places it is a hard limestone.
Although it contains some relatively impermeable beds of marl or dense limestone, much
of it is highly permeable; the permeability resulting from solution of the rock by
circulating groundwater. The depth to the Castle Hayne varies throughout New Hanover
County, being at or near land surface at the northern part to a depth of more than 100 feet
in the southern part of the county. The water bearing capacities of the Castle Hayne are
variable from place to place and well yields can be as high as 600 gallons per minute,
however well yields of 150 gallons per minute are more typical.
Underlying the Castle Hayne Formation and separated from it by some relatively
impermeable clays is the Peedee Formation. The most productive zone of this aquifer is
an approximately 35 foot thick bed of quartz sand in the upper part of this aquifer. This
zone is generally 10 to 25 feet below land surface in the northwestern part of the county
but is more than 150 feet below land surface along the Atlantic coast. It is overlain by a
clay bed that ranges in thickness from only a few feet to more than 50 feet. This clay
retards the movement of water into and out of the sand. The Peedee Formation yields 200
5 "Geology and Groundwater Resources of New Hanover County, North Carolina", prepared by George
Bain, Geologist, U.S. Geological Survey.

OW
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington, New Hanover County, North Carolina
gallons per minute to many wells and in excess of 400 gallons pre minute to some; in
most places it is used in conjunction with the Castle Hayne aquifer.
•
0

21
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover County, North Carolina
• 5.0 SOIL SAMPING RESULTS
5.1 Soil Boring Installations (May 10 —17, 2005)
Analytical data for soil samples obtained while completing fifteen of seventeen
groundwater monitoring wells installed by Babb & Associates during the time period of
May 10 - May 17, 2005 indicated the presence of targeted analytes in many of the soil
samples submitted for laboratory analysis. The Geoprobe drill rig provided continuous
soil sampling from land surface to the groundwater table, which ranged from 0.4 and 6-
feet below land surface in the borings. Representative soil samples were collected from
an average depth of 1 to 2 feet below land surface and above the groundwater table
(where possible) for screening using an Organic Vapor Analyzer (OVA). The OVA
results are displayed on the boring logs included in Appendix A. Split samples were also
immediately placed into laboratory supplied bottles for submittal to the analytical
laboratory (It should be noted that the soil samples collected from MW-2, MW-3, MW-4
and MW-10 and submitted for laboratory analysis may actually have come from below
the groundwater table because groundwater was found to stabilize at depths of less that
two feet below land surface in these wells. Also, the samples collected from MW-13,
MW-14 and MW-15 were disturbed soils that had recently been placed in these areas as
part of the excavation and dewatering activities being competed for construction of an
adjacent office building).
All of the borings were converted to monitoring wells for the collection of groundwater
samples and also to establish the depth to groundwater and the hydraulic gradient in the
shallow aquifer.
The soil samples were submitted to Paradigm Analytical Laboratories of Wilmington, NC
(NCDENR laboratory certification # 481) for laboratory analysis by EPA 8260 for
volatile organic compounds and also for total RCRA metals, chloride, sulfate, nitrate,
T.K.N, ammonia, phosphorus and total nitrogen.
Soil analytical results indicated the presence of minor levels of volatile organic
compounds in only three of the fifteen soil samples submitted for laboratory analysis.
Ammonia, chloride, nitrates, phosphorus, sulfate, arsenic, barium, cadmium, chromium,
0

22
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover County. North Carolina
I* lead and mercury were also detected in many of the soil samples submitted for laboratory
analysis.
There are currently no Soil to Groundwater Maximum Soil Contaminant Concentrations
set forth by the North Carolina Department of Environment and Natural Resources
(NCDENR) Groundwater Section or Soil Screening Levels established by the North
Carolina Hazardous Waste Section for the ammonia, chloride, nitrates, phosphorus and
sulfate detected in the soils during this investigation.
The NCDENR Hazardous Waste Section has established Soil Screening Levels for RCRA
metals including arsenic, barium, cadmium, chromium, lead and mercury which were
detected in the soil samples. Further, only arsenic, chromium and mercury were detected
at levels in excess of their Soil Screening Levels in several of the soil samples submitted
for laboratory analysis. However, as stated previously the soil samples collected from
MW-2, MW-3, MW-4 and MW-10 and submitted for laboratory analysis may actually
have originated from below the surficial groundwater table and the presence of
contaminants in these samples may reflect groundwater contamination in these areas.
is The analytical results for the soil samples collected from MW-13, MW-14 and MW-15
also may not be representative of these areas as they were disturbed before and since the
samples were collected as a result of construction activities.
A soil isoconcentration map for selected contaminants has been prepared and can be
found in Figure I Table 1 is a summary of analytical results for the May 2005 sampling
events. Laboratory reports for these sampling events are presented in Appendix C.
11

23
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street. Wilmington New Hanover CountyNorth Carolina
• 6.0 GROUNDWATER INVESTIGATION
6.1 Location and Installation of Monitoring Wells
Investigative activities related to the groundwaters of the Site for completion of this CSA
were conducted during the week of May 10 — 13 and May 17, 2005 and included the
installation and sampling of newly installed groundwater monitoring wells MW-1
through MW-15, DW-1, DW-2 and existing wells MW-16 and LMW-13.
Monitoring wells MW-1 through MW-15 were all installed to roughly 12-feet beneath
surface grade using a 3.5 inch diameter Geoprobe push probe and constructed using 2"
diameter PVC slotted screens and solid PVC riser pipe. The wells screen was placed
from 2 to 12-feet below land surface. One foot bentonite plugs were placed in these wells
from approximately 0.5 to 1.5 feet below land surface, and the remaining boring grouted
to land surface. Finally, the subject shallow wells (excluding MW-13, MW-14 and MW-
5 which have subsequently been destroyed) were completed at land surface and finished
with 6-inch diameter manhole covers and concrete pads.
DW-2 were installed to a total depth of 40-feet below land surface using 6 1/a inch O.D.
hollow stem augur and screened from a depth of 35 to 40-feet below land surface using
2" diameter PVC slotted screen and solid 2" PVC riser pipe from 35 feet to land surface.
A two foot thick bentonite plug was placed in DW-2 from approximately 32 to 34 feet
below land surface, and the remainder of this well was grouted to land surface. Finally,
DW-2 was grouted to land surface and finished with a 6 inch diameter manhole cover and
concrete pad.
Monitoring well DW-1 was advanced to a total depth of 40 feet below land surface and
completed as a double cased well. First, DW-1 was advanced to 28-feet below land
surface using 6 1/a inch O.D. hollow stem augur. A 4 inch O.D. PVC outer casing was
installed into the borehole to a depth of 28 feet below land surface and the remaining
borehole annulus was grouted throughout its entire length and allowed to set up
overnight. Next, the boring was advanced into the underlying limestone formation to a
depth of 40-feet below land surface using an air hammer. The inner casing (consisting of
2-inch O.D. PVC pipe) was placed into the boring to a total depth of 35 feet below land
surface and completed at the bottom with 5 feet of 2-inch O.D. well screen from 35 to 40

24
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover County North Carolina
feet below land surface. Filter sand was placed around the well screen from 34 to 40 feet
below land surface. Finally, a 2 foot bentonite plug was installed from 34 to 32 feet
below land surface and the remaining boring annulus was grouted from 28 feet to land
surface.
Boring logs and well construction diagrams for the monitoring wells installed for
completion of this CSA are included in Appendix A, while a summary of the well
construction details can be found in Table 3. The monitoring well locations can be found
in Figure 2.
6.2 May 25, 2005 Sampling Event
All of the monitoring wells discussed previously were sampled on May 25, 2005 and the
samples submitted to Paradigm Analytical Laboratories of Wilmington, NC (NCDENR
laboratory certification # 481) for chemical analysis by EPA Method 8260 (volatile
organic compounds) and also for total RCRA metals, chloride, sulfate, nitrate, T.K.N,
ammonia, phosphorus and total nitrogen.
Samples from each of the wells were obtained after a minimum of three (3) volumes of
water had been purged or the wells went dry. Prior to purging, the relative groundwater
elevation at each location was measured utilizing a conductive water level indicator. All
of the sampling activities described above were completed using new disposable bailers
and nitrile sampling gloves.
Groundwater samples obtained from the groundwater monitoring wells described above
and analyzed by EPA Method 8260 revealed the presence of several compounds in the
samples collected from monitoring wells MW-I, MW-2, MW-8, MW-16, and LMW-13
at concentrations in excess of their method detection limits. However, only
tetrachloroethene (PCE) (detected in MW-1, and LMW-13 at concentrations of 0.00217
and 1.6000 mg/l, respectively), trichloroethene (TCE) (detected in MW-1 and LMW-13 at
concentrations of 0.00562 and 0.024 mg/l, respectively), naphthalene (0.0452 mg/1 in
MW-2), and 4-isopropyltoluene (MW-1 at 0.140 mg/1) were detected at concentrations in
excess of their maximum allowable levels as set forth in the 15A NCAC 2L .0202 upon
0 testing by this analytical method.

25
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street. Wilmington New Hanover County. North Carolina
• Groundwater samples obtained from the groundwater monitoring wells described above
and analyzed for nutrients revealed the presence of one or more compounds including
chloride, nitrates and sulfates in the samples collected from monitoring wells MW-3
through MW-15 at concentrations in excess of their maximum allowable levels as set
forth in the 15A NCAC 2L .0202 upon testing by this analytical method.
Finally the groundwater samples analyzed for total RCRA metals revealed the presence of
arsenic, lead, mercury and selenium in several of the groundwater samples submitted for
analysis at concentrations in excess of their maximum allowable levels as set forth in the
15A NCAC 2L .0202 upon testing by this analytical method.
Isoconcentration maps for selected groundwater contaminants have been prepared and
can be found in Figures 4 through 8. Figures 9 through 11 are soil and groundwater
contaminant cross section maps indicating the vertical extent of soil and groundwater
contamination identified by this CSA. Table 2 is a summary of analytical results for the
May 25, 2005 sampling event. Laboratory reports for this sampling event are presented
in Appendix C.

0
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover County. North Carolina
0 7.0 FREE PRODUCT INVESTIGATION AND RECOVERY
7.1 Free Product Investigation
The investigation of free product in the subsurface of the Site has been conducted through
the installation of monitoring wells MW-1 through MW-15, in addition to monitoring
wells MW-16, MW-17, LMW-12, LMW-13 and RC-4 installed by others as part of
previous groundwater investigations. Weathered free product tentatively identified as
diesel fuel was identified in monitoring wells MW-17 and MW-11. However, this fuel
was so weathered that it was not possible to accurately determine the product thicknesses
in these wells. The product measured in off -Site well MW-11 is likely the result of past
use of this neighboring property while the diesel fuel measured in MW-17 may be the
result of a release of diesel fuel from UST systems removed from the Almont Shipping
property during January 1998. Figure 2 indicates free product locations in relation to the
Site.
0 8.0 HYDROGEOLOGIC INVESTIGATION
8.1 Horizontal Groundwater Hydraulic Gradient
The hydraulic gradient was obtained from gauging of wells on the Site and triangulation
of the data. Data for the May 24, 2005 and June 16, 2005 gauging events was
triangulated to determine average hydraulic gradients throughout the Site for the subject
gauging dates. The results for these measuring events were used to product the hydraulic
gradient maps found in Figures 12 and 13.
As stated above, Babb & Associates personnel measured water levels in monitoring wells
on May 24, 2005 and June 16, 2005. The groundwater flow direction was determined to
be toward the west as displayed in Figures 12 and 13, while the gradients were calculated
to be 0.022 ft/ft and 0.023 ft/ft for the May 24, 2005 and June 16, 2005 guaging events
respectively. Table 4 includes a summary of the measuring results for the May 24 and
June 16, 2005 gauging events.
is

•
P*A
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street. Wilmington New Hanover County, North Carolina
8.2 Vertical Groundwater Gradient
The vertical gradient of groundwater flow was also assessed by measuring the
groundwater elevations in MW-1 and DW-1, as well as MW-10 and DW-2 located
approximately 5 feet from each other, on May 24 and June 16, 2005. Using these
measurements, the vertical hydraulic gradient was determined to be 0.05 and 0.03 ft/ft
downward on May 24 and June 16, 2005 at the MW-1/DW-1 location, respectively.
Finally, the vertical hydraulic gradient was determined to be 0.0066 and 0.0077 ft/ft
downward on May 24 and June 16, 2005 at the MW-10/DW-2 location, respectively.
8.3 Aquifer Testing
Babb & Associates completed rising and falling head tests (slug tests) on monitoring wells
MW-I, MW-3, MW-6, MW-10, DW-1 and DW-2 on June 16, 2005. All of these
monitoring wells were installed by Babb & Associates as part of this CSA investigation.
The tests were performed using a 1-inch diameter, 5.5-foot long PVC slug to create an
instantaneous change in the water level (head) at each selected well. A MiniTroll Model
SSP-100 pressure transducer was used to measure water level fluctuations during each test.
The pressure transducer was attached to a laptop computer in order to record the water
fluctuations at three second intervals. The depth to water from the top of the PVC well
casing was measured prior to insertion of the pressure transducer and slug. Water levels
were also measured by hand at various times during each test, and at the completion of each
test, to verify the electronic data.
Rising and falling head tests were conducted during the field investigation. Falling head
tests consisted of rapidly lowering the PVC slug into the well and simultaneously initiating
a logarithmic recording interval on the data logger. Rising head tests were conducted by
removing the slug and initiating a new logarithmic recording step on the data logger.
The slug test data was analyzed using the Bouwer and Rice method, which accounts for the
effects of partial well penetration and changing aquifer thickness' (water table conditions).

Comprehensive Site Assessment
Ahnont Shipping Terminals
One Hanover Street Wilmington, New Hanover County, North Carolina
• The aquifer thickness was estimated from boring logs to be between eighteen and forty feet.
A packing porosity of 25 percent for the well filter pack was assumed.
The results of the slug test data analyses using the Bouwer and Rice method is summarized
on the table below:
WELL
BOUWER AND RICE METHOD
CONDUCTIVITY(feet/day)
TYPE OF TEST
MW-1
2.306
Falling Head
MW-3
2.52
Falling Head
MW-3
0.90
Rising Head
MW-6
1.96
Rising Head
MW-10
1.65
Falling Head
MW-10
1.06
Rising Head
DW-I
0.12
Falling Head
DW-2
0.397
Falling Head
DW-2
0.14
Rising Head
The hydraulic conductivity values for the water table aquifer obtained as a result of this
investigation were on the order of 10 1feet per day (ft/day). The geometric average of the
hydraulic conductivity estimate using the Bouwer and Rice method is 1.22 ft/day. These
values are consistent with a silty sand to sandy water table aquifer.
The results for the rising and falling head slug tests can be reviewed in Appendix B.
8.3 Groundwater Modeling Results
Groundwater modeling was not completed as part of this CSA. Groundwater modeling
may be necessary for the forthcoming Corrective Action Plan.
0

29
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover County. North Carolina
9.0 DISCUSSION
9.1 Nature and Extent of Contamination
The nature of the major contaminants assessed by Babb & Associates at the Site comprise
a variety of soil and groundwater contaminants including: diesel fuel, PCE, TCE,
ammonia, chloride, nitrates, total nitrogen, phosphorus, sulfate, and arsenic. The
presence of total nitrates, nitrogen, ammonia and chloride at the Site can be attributed to
its association with the handling and storage of nutrients including: urea, calcium nitrate,
ammonium nitrate, salt and salt cake. However, there is no known source(s) for the
arsenic, PCE and TCE detected during this investigation. Finally, the presence of diesel
fuel in MW-17 and MW-11 can be attributed to former on -Site UST systems and the past
usage of off -Site neighboring properties.
The presence of PCE, TCE and diesel fuel is localized and appears to be limited to the
southern portion of the Site. The total nitrates, nitrogen, ammonia, chloride and arsenic
contamination is more wide spread and includes much of the central portion of the Site as
• indicated in Figures 4 through 11.
9.2 Contaminant Migration and Potentially Affected Receptors
The receptor which is most likely to be impacted by the detected soil and groundwater
contaminants is the Cape Fear River, located immediately west of the Site. Further,
surflcial groundwater hydraulic gradient maps prepared for completion of this CSA
indicate that groundwater movement is mimicking topography and flowing across the Site
and west toward the Cape Fear River. While the detected soil and groundwater
contaminants should be degrading on -Site due to the processes of natural attenuation and
biodegradation it is likely that some of these contaminants are migrating with
groundwater and ultimately may discharge into the Cape Fear River. Finally, there are no
potable or non -potable groundwater supply wells located within or downgradient of the
contaminant plume.
While the presence of inorganic contaminants detected at the Site including the ammonia,
chloride, nitrates, total nitrogen, phosphorus and sulfate detected in both soils and
0

30
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover County. North Carolina
groundwater can be explained by the Site's history of bulk storage activities, there is no
obvious source for the arsenic detected in the soil and groundwater samples.
Inorganic arsenic is a naturally occurring element that is released by the weathering of
arsenic containing minerals and ores and is also associated with industrial processes
including wood treating and metal smelters. The most common type of human exposure
to inorganic arsenic is through ingestion of contaminated foods such as fish and shellfish.
The EPA has classified arsenic as a Group A, human carcinogen.
The other detected contaminant the source of which cannot be explained is PCE. TCE is
a breakdown product of PCE which is the likely explanation for the presence of this
compound. However, PCE is man made and does not occur naturally. It is widely
associated with the dry cleaning industry but it has also been used for parts cleaning,
vapor degreasing and by makers of rubber coatings. While PCE evaporates quickly in air
it dissolves only slightly when mixed with water.
• 9.3 Lowering Risk Classification
Currently, the Site can be classified as intermediate risk because the Cape Fear River is
located immediately downgradient of the groundwater contaminant plume(s) and is
considered to be a contaminant receptor.
9.4 Applicable Cleanup Levels
There are currently no Soil to Groundwater Maximum Soil Contaminant Concentrations
set forth by the NCDENR Groundwater Section or Soil Screening Levels established by
the North Carolina Hazardous Waste Section for the ammonia, chloride, nitrates,
phosphorus and sulfate detected in the soils during this investigation.
The NCDENR Hazardous Waste Section has established Soil Screening Levels for RCRA
metals including: arsenic, barium, cadmium, chromium, lead and mercury which were
detected in the soil samples. Further, only arsenic, chromium and mercury were detected
at levels in excess of their Soil Screening Levels in several of the soil samples submitted
for laboratory analysis. However, as stated previously the soil samples collected from

31
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover County North Carolina
MW-2, MW-3, MW-4 and MW-10 and submitted for laboratory analysis may actually
have originated from below the surficial groundwater table and the presence of
contaminants in these samples may reflect groundwater contamination in these areas.
The analytical results for the soil samples collected from MW-13, MW-14 and MW-15
also may not be representative of these areas as the soils at these locations have been
disturbed before and since the samples were collected as a result of construction
activities.
Groundwater samples analyzed by EPA Method 8260 revealed the presence of several
compounds in the samples including tetrachloroethene (PCE), trichloroethene (TCE),
naphthalene, and 4-isopropyltoluene at concentrations in excess of their maximum
allowable levels as set forth in 15A NCAC 2L .0202 (2L Standards) upon testing by this
analytical method. The established 2L Standards for PCE, TCE and naphthalene are
0.0007 mg/1, 0.0028 mg/1, and 0.021 mg/1, respectively. The compound 4-
isoporopyltoluene currently has no established 2L Standard, therefore any detectable
amount is considered to be a violation.
is Groundwater samples obtained from the groundwater monitoring wells and analyzed for
nutrients revealed the presence of one or more compounds including chloride, nitrates and
sulfates in samples at concentrations in excess of their maximum allowable levels of 250,
10, and 250 mg/1 respectively, as set forth in the 15A NCAC 2L .0202 upon testing by
this analytical method.
Finally the groundwater samples analyzed for total RCRA metals revealed the presence of
arsenic, lead, mercury and selenium in several of the groundwater samples submitted for
analysis at concentrations in excess of their maximum allowable levels of 0.05, 0.015,
0.0011 and 0.050 mg/1 respectively, as set forth in the 15A NCAC 2L .0202 upon testing
by this analytical method.
U

32
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street. Wilmington New Hanover County North Carolina
10.0 CONCLUSIONS AND RECOMAMNDATIONS
Babb & Associates has completed this Comprehensive Site Assessment in order to
comply with NCGS 143-215.84, NCAC 15A, 2L .0106(g) and the NCDENR
Groundwater Section's, "Guidelines for Investigation and Remediation of Soil and
Groundwater". Effective July 2000.
Babb & Associates concludes from the investigative activities conducted for completion
of this CSA that several separate releases on the Site have impacted the Site's soils and
surficial groundwater aquifer at more than one location.
Free phase petroleum product identified as weathered diesel fuel has been identified in
on -Site groundwater monitoring well MW-17 and off -Site monitoring well MW-11.
Analytical results for soil samples collected for completion of CSA activities identified
the presence of targeted contaminants at levels in excess of their Soil Screening Levels for
arsenic, chromium and mercury in several of the soil samples submitted for laboratory
. analysis.
Analytical results for the groundwater samples collected for completion of this CSA
detected TCE, PCE, naphthalene 4-isopropyltoluene, chloride, nitrates, sulfates, arsenic,
lead, mercury and selenium at concentrations in excess of their maximum allowable
levels as set forth in the 15A NCAC 2L .0202 upon laboratory testing.
The risk criteria pertaining to the releases at the Site include the following: 1) MW-17
contains product identified as diesel; 2) there are no potable water supply wells located
within 1,000-feet of the source area; 3) the Cape Fear River is located immediately west
of the Site; 4) the Site is used for commercial purposes; 5) the Site is surrounded by a mix
of commercial properties; and 6) the Site is located in the Coastal Plain Physiographic
Province.
Babb & Associates recommends that the Almont Shipping submit a copy of this CSA to
the NCDENR-DWQ, Wilmington Regional Office, to the attention of Mr. Charles
Stehman.

33
Comprehensive Site Assessment
Almont Shipping Terminals
One Hanover Street Wilmington New Hanover Countt+ North Carolina
•
REFERENCES
City of Raleigh, North Carolina, Public Works Department
Wake County, North Carolina, Tax Office
Geologic Map of North Carolina, Department of Natural Resources and Community
Development, Division of Land Resources
Groundwater Section Guidelines for the Investigation and Remediation of Soils and
Groundwater, Volume II Petroleum Underground Storage Tanks North Carolina
Department of Environment and Natural Resources, Division of Water Quality,
Groundwater Section, January 2, 1998.
United States Geological Survey, Raleigh, North Carolina.
Geology and Groundwater Resources in the Raleigh Area, North Carolina: North
Carolina Department of Water and Air Resources, Division of Groundwater, Bulletin 15,
V.J May and J.D. Thomas, 1968.
North Carolina Administrative Code, Title 15, Subchapter 2L, Section .0100, 0115 and
.0200.
North Carolina Department of Environment, Health and Natural Resources, Division of
Environmental Management, Groundwater Section, Pollution Control Branch.
Soil Survey of Wake County, North Carolina. United States Department of Agriculture,
Soil Conservation Service.
0

w

Babb & Associates, P.A.
TITLE.•
AREA LOCATION MAP
Almont Shipping
Wilmington, North Carolina
FAWW MD: SCALE. PAOxCr No
Figure 1 1 1 12,800
amiv or.. I a u#w er.• I mm .
GD8 I TRW 1 7/1/05

\ ,� '�• mac, J pI,81,IC R/w) — —.� NORTH SECOND Slrccc�
NOR
O,Q • � _ _ _ I ` _ _ —. _
\ 7�F •\ �___--- -_—__TH FROM RSTREET NORTH FRONT STREET
/.6 j
s
- ;
W r
/ 1 vENTuRES. LLC^
RIVER 1 I \ \
81.
\ Former CSX Aboveground !� I \ •\ \ \ I I I I I _
j/ / Tank Fuel Area
Storage Ta. �� I Standard Oil Company
IN Former Sta J I
�� 2.5 Mil. Gallon Diesel Fuel Spill r m Bulk Storage Tank Area \ �'�,` I L - � FRONT (P1su`----
\ / I� j Petroleum Ik S \ _ _ -- — STREET
From This Location in 1982.
•: ' _ — —
UST Locotion
\ \ > \�• Mw�-13\� \�\(\�Im\o ted \�Loco\sEAsp� COAST LgR�(Estim\oted Location)
;I I
I'I
,,/:.,� /� ��,"�-_---�----_--O=—�LD -IR--O_—NY'S°rn•�_ETR.�._�—r--•-- ---_ —
�-.�--/-«— t----" \\\\ \\\\\\\\\ \\\\\
—�ao3------ pping Urea
\\ \\\\\\\ I I®LMW 13 LMW 12
�,IRr -\ \Former AImontSouse Area\ kc-4
�\\\Bulk Storage \ - - -- ----
---- ` ed Location
� \„ � II
------------
—
-__=----
-R
__�„__�----..— 30• UTILITY R./`� — _ _ w DW—
t I Mw-il
I- 10
Mw-t cR
/y/ /'''uY '�• - i� —_ — tole i pi Urea j Former Almont Shipping 'I
a — MW �� r Almont Sh pP ea I Petroleum UST Areo
e A
j MW-9 0 Chromium Ore j j �\ \B rm Storage �\ �����\\\\ j I (Former y Petroleum
Oil
\ ulk ,Company Petroleum Bul
-
Storage Area
%'
m
r
I 'i♦N j
\\\\\\\\
\ \\ NIW-17 16
� \\\\ _ ®MW-
IStoro a Tank Property
' (Exact Source Location
�:
\�\�\�].\�.
lunknown)
MW-3
F '
I
Mw-g
1
-,,OR TH EA _ x�
— \ ®MW-7
ST CAPE F
fAR RiVERti
~NORTH
I� ^'NORTH E
AST CAPE F
_ C\_ eqR R/VER_
IOMW-13, MW-14 and MW-15 have been destroyed
as a result of construction activities on behalf of
new property owner
EAST CAPE f
FARR/-�
ree VER. ' __ _
I
I
I I
I
j
I
I
II
DATE:
7/ 1 /05

SECOND ST
- FRONT ORTH FRO
STREET I `" - STREET
(PUBLIC R/W) - J NORTH �L1G�� I I I
NORTH(P(PUBLIC R/W) _ NNT S
-
- I - Ammonia
474 IW�N ;1I 'WWChlonde
-RIVER VENTURES. PLC^ Nitrates ND �NI'I^��
�0
/ / I Phos. 132
�m Sulfote 51.6 \ �� yTs., I� of 0i� I
/ a ' Arsenic ND \ R TRF\ lion s!"
P2Jv� /�� Ammonia 359
A, �� IN I Chloride 327 \ ,\ �•\ \ -J L �__- -" (PUBLIC /W -
Nitrates 348 \ \-` I NORTH FRONT STREET ���- - -
Phos. 8.19
li Sulfate 194
Arsenic NO • MW--14 ® ) a
Ammonia 213 � � �" ;•� � 1I
\--__ ted Location
I M (EstimO Chloride 84.7
\ 7. -SEABOARD COAST _ (Estimated Location) Nitrates 13.5
l ^'SEAB LINE R
/w - - -- _ Ammonia 108
_ _ Chloride 669 Phos. 149 ` I
/ aD raor+r STREET R w------. as faa+T sttET R� t°D1 Nitrates 1.14 Sulfate 186
.' faosca
Phos, 204
%./�^ 1/ / % �Sa_ _s"vwr ta•r 7` -rti[-�,. \ ogslr'ke I Arsenic7®.70 _ LMW-(soL�MW-1_2
`� --
-__
L
_;.__ Sulfate 165
'"e"e, -------------------
I Arsnc R-- -
(Estimoted
Ammonia 6
- -
' \
Chloride 2346 -\,\ `---"•�.. � R 1�----�--- ----�--- �,_�_-'�-� ---- ----L: ------- `,
/ QJ� Nitrates 2.47
,Rr ' \ 1 - _ NUTi STREET CLOSEDZ - - --I
Phos. 260 A(tr'ia \ Y - - -- - I 1 1
_=_-y-- -30 uTlt_li R W I M 1�DW I (BMW- 1
�4.// Sulfate 64.7 tl W- Ammonia 42.9
j P �A j / Arsenic 4.18 C CqupgNY A W I O w DW J i I Ammonia 49 I Chloride 110
Chloride 13.2 Nitrates NO
Ammonia 38 Nitrates 0.94 Phos. 158
MW-9 ® $ I �{u Chloride 47.2
\r'V Ammonia 57 �'W I Nitrates 5.87 h -1 - 76.4 ' Sulfate 24.7
/ v a I �_ It 6 Arsenic 2.55
Chloride 12.2 _IN Phos 217
Nitrates 0.88 Sulfate 68.4 Ammonia 815 Ars c ND I
Ammonia 48 �Iz I Arsenic 25.8 Chloride 40.5
(' Phos.
260 Chloride 36.4 i= Nitrates 44.9 ®MW-3
Sulfate 84 '• Q Nitrates NO ,I I Phos. 1
Arsenic ND �/ / 26
Phos. 150 I I Sulfate \ 4 00 I
Sulfate 56.4 I ®MW 6 Arsenic 3.41
I
\ .`, Arsenic NO
Ammonia 29
®MW- 7 I I Chloride 842
CAP
f FEq Nitrates 1.47 4 i MW- 2
ItOO_ R RIVERti I Phos. 76 ® W
tmoted\L-C"C Ammonia 100
Sulfote 27 in) �I
Ammonia 93 / Chloride 14.4
Arsenic NO 7
.
Nitrates 3
Chloride 3.5 I
Nitrotes 3 .4 1 % Phos. 7.29 I
Sulfate 55.3
1 Ammonia 61 Phos. 26 I
Sulfate 95.d Arsenic 11.9
Chloride '27
Nitrates 1.76 Arsenic 30.2
~NORTH E qST ` Phos. 233
CnP6 FEAR �--Sulfote 56.8
R/ As nic 7.17
r E ,,,
1� � R _
~NOR
TN EAST CAPE
E,4
iep now R RlVER-
MW-13, MW-14 and MW-15 have been destroyed
as a result of construction activities on behalf of
new property owner
DATE:
7/1/05

J
-- —TREE
FR(PUBLONT ST T
STREE T
c /W) ----J
(auBu R --_—
\
NORTH
_
NORTH FRONT
--
S--r--
_—�— —"—
I /
-F4VER VENDS' LLC-
I
MW-12\ \
\428
�A.
�/
IW
6,888
—sE"e°"Ro COAST
f-------__—_ —
0
W—t3 (Estim
(Estimated Location)
-�--- adraawi
—Y
..,NORTH EAST C
APE
-W- _FEAR R�VERti
-NORTH EAST A \
CAPE Fw AP FEAR RIVER -
~NORTH EAST CAPE F
,,. c� EAR RiVER-
MW-13, MW-14 and MW-15 have been destroyed
as a result of construction activities on behalf of
new property owner
NORTH SE coN_'
u'
rIs
z 1
J
..----- T STREET (PUBUC R/'�_
FRON
�-
—
NORTH838
--_ �—
ed Location)
I I
`II I
14,726
I
I
I 18.5 W
I:
LMW-12 _-_--__ . l-- —
�L2C-4 -- -- -
.
5®
MW-1oton
Loc
_LMW-13
� -- _--- --
(Estimoted
oW-1 j ®Mw-11
�89
I
I
17 I
w-16
,6 I
/ I
® W MW-2 -4 1 ® I
o io^)
stimoted Loc10
I
I �I
� I
\ I I " 7
I

_
FRONT STREET TM FRONT STREET
( R
—`
�oG�'p
NOR (PUBLIC R/►)
I /
1II «RIVER VENTURES. LLC- I
\ \
`44
ICA
IT
28.7
�
�
\ \ i
•
__
-SE"901gp CO"St LINE RAW,,
I I
W-13
) (Estimc
moted LOCOtIOn �
• \ /
/� — —
(Est'I
FiFk S TaceT R w,-—�aosm}-------
ie/'w (a oSED)
\
ANY
x'
`"e'
Np.;\
i
NORTij SECOND STKt-'_
I I�Fu
r�
I
ZIP I
\ \ \ \ .J I L NORTH FRONT STREET (PUBLIC
\ `•\ -�
14
140
ed® cotion) o
317 I 3.15 I °' I
:
\ I IRC-4 LMW-13 LMW-12
_1�
_ --T
MW
ND
MW-10
.27 188 I
MW-9
ND
Y
tiNORrij `-_✓ x� —
CASr CAPE
AP �'-
-��-FEAR RIVER
1 �I�
W � r
I I
t I 59.1
00
MW-6
I I
I
0.05 w-
4 \
'I I 59.1
stimoted Loco ion) �
0.64 \\ \
tiNORrN EAST APE
C FEAR
ryNORrH Eq
S r CAPE
FEA
R
MW-13, MW-14 and MW-15 have been destroyed
as a result of construction activities on behalf of
new property owner
TITLE: FIGURE NO:
a
NITRATE G.W. CONTAMINANT 5
PISOCONCENTRATION MAP (MG/L)
REV. BY:
Almont Shipping
Wilmington, GDB
ton, North Carolina
Babb &Associates, P.A. 9
IN
SCALE:
1 " =150'
PREP. BY:
TRW
PROJECT NO.
DATE:
7/1/05

7 576
NORi�(PUfBUC R-Tli FRONT STREET
94
OD
IN
STREE
NORTH FRONT
-SE
ABOARO CCAST LINEp/w` ---------' ---
~. '------------_---_----����`~-_---_-
ww-* 0
128
~�
~*oR0
/
EA'APE PEAR
---- `-~_`
r�
u�
_-__� � ~^
//
�
-------------------
---------------------
��58 u�ww-�o �
\
\ � .
. \ .
�
. � \~_
/.
\---
\ \ 29
� u�wW, . \
/ / \
ND
' 7
'`~ ww- \ \ \
2
~~ | \
\ 1OO | '
-_' ^ .
620
-- \ \
302\ \
EAST
[ASrcAw'
^qEAR
x»VCR-
EAST
_--_---------_- \'-~' \ ` �--_
--~ ----__--- �
~-��-� �w,
-- `~. --_--- \
K�VV-1��. K�VV-14 and NiVV-15 hove been destroyed
- OS a result of construction activities on behalf Of
new property owner

t.
ti \, I J I `-- PUBLIC R/ NORTH SEPCN�c.�Jy4—
-FRONT STREET TH FRONT STREES (— —Ti6
NORTH (PUSUC R/ -�-°R I I I I I I
0 'y - \
R S
r" I I
• I"-- RIVER VENTURES, LLCM
ND :MS
J NORTH FRONT STREET (PUBUc R/W)
0.0622.
0.0137 ---
\ / ®O ion)
-SEABOARD MW-13 (Etimoted Locat
s
COASTUNER/W` CotiL(Estimote
I
I Ig I
j-7L-0L r'MRf rsRer�r—(aoco}— - i m
N
1 D
- // --- —`-- rr
,. , (_-_ 12
b_ - -----' ---- ---- -
E - - -
-otlon®0.05MW 3 LM�C- 4 -om-
Esmted o --
- _ --
- - -
_ -----
'��`/ /. ~�QyT'`•,,•- \' L_.—__'="::�_ _ -Y _ - :., j M 1�Dw-1 1 ®MW-11
G
10 0.0248 ND µYI F �W� 0 0.0937
W I ;1
0.713 I
Mw-9 I
0.0133 > " S\ OJ ®MWMW-16 I
I FI> I o �_
0.0129 j
9/1 I I j
MW-�
...NORTH EAST CAPE ✓' x �'-.\I I I j ND \
� I n FEAR " 0.0881 -4
-
'�.timoted Loco ion)
0.9111 �
ND ®Mw- 5
1
V1 SNORT H CAST
CAPE FEAR `• '`''_-.,�-
~NORTH EAST CAPE F `- `• __ _
E _
_ C` AR RIVER_
l0 MW-13, MW-14 and MW-15 have been destroyed
as a result of construction activities on behalf of
new property owner
� 1
I I
I
1
I
I
I I
I I
� I
I
I
I
I

\` __ NORTH FRONT STRE I NOR7 FRONT STREET (_ � R/W) J NORTH
Q CON
�oo� (PUBLIC R/R) _ t— _ _ _ I I I j I I
T
I / / �RryER VENTURES. LLC^
� I Y
�RTs I Z. j °'� I
7REET (PUBLIC
NORM FRONT
s
\ / / -SEABOARD MW-13 ® (Estimated cation)
COAST�qyE Raw„' �- oted Location)
(Estimj
FRONTS _ - 1 STREET R/'M (CLOSEDi _ _ I
iREE7 Rh iCLO5E0}�_ pp IRON —„_ I I 1 . G 00\
\LMW-13 LMW—
_12
swr '-..___ -- -rt; 'g I KC-4 -
r --- j M ---
' � -�t�� ••-.,, \ \ (Estimated Location
—
/1� DW 1 MW-11
0.00217 0
M)N-9 ® Ij
�I ���-
W ND
Mw- 3
�•�- f� � I I 11 ®MW-6 /
~NORTH EAST \ ®MW-7 I I I
CgpE -i I
FEAR RIVER
I ®W ted Loco ion)
ISlim-
-5
� J
I I
®MW
W I
EA
ST CAPCFEAR
E•p VER- I
~NORTH EAST CAPE FEL---
AR
MW-13, MW-14 and MW-15 have been destroyed
as a result of construction activities on behalf of
new property owner

ti .\ - -i I ` — (PUBUC R/ 1 —_ _J NORTHfi SECOND )— — I 1
pR FRONT STREET RTH FRONT STREET _
(PUWc R/*)t►�� F i I j I I
FT -----
\ •. I Ir I j � j
RIVER VFN'NRES. LLC^' I \, • \ `' \ ti\ �A I I �' I
IR
RONT TREE
\ '86'.
F`'
/ I NORTH ,� •\,, ,\ / IZ \ �,_ NOR
y / • M 14 a
MW-13~sEAao�oco,sru
(Estimated Location
(Estimated LoC tio )
I
T S1REE7 Ri'M (CLOSED) �_--- OLD fRONi STaEET R -pp iaOM JI
W'—T$---�--. __— ' I • 12
C-4
MW-15® ® - :_"- _'---I2LMW-13 LMW
-_
—
~f��"-� ted Locations
-. tmo _ -
, BEET ---
4� 30!4i�R%►= -- �W-1 MW-11
j Mw- j I
1 r r
I
w
MW
o-
r
' � W
®MW-3
-"-NORTH CAST CAS \ ®MW-7
CAPE F �i.
` EAR R,VCRti �'.� I I W-4 MW-2 ® j
stimoted Loco ion)
MW-5 1 I
�i
('I -NORTH EAST CAPE
Eep `wm FEAR RIVER,.,
NORTH EAST CAPE R L_---
PE I
RIVERry -- 1
MW-13, MW-14 and MW-15 have been destroyed
as a result of construction activities on behalf of
new property owner

•
A
10.00
0.00
•
- 10.0 -
- 20.0
- 30.0
L
cloy=
Wet Ton -brown medium grained San dl
-Limestone w. sond layers_
20.00
10.00
0.0
wn medium grained Sand
-1O0
Hotizon tol
"
Scale. l
'
= l5o
% o '
ORA
M
TITLE:
G.W. CONTAMINANT CROSS—SECTION
A — A'
Almon+ Shi in
FIGURE NO:
10
SCALE:
1" = 150'
PROJECT NO.
Vertical
Scol e " 1 „ _
FF g REV. BY: PREP. BY: DATE:
Wilmington, North Carolina GDB TRW 7/1 /05
Babb &Associates, P.A.

B'
1�
-
- _
- -
i
-
-
--
30.0
'0 �5
ae
--
20.00
20.00
�0
- -
10 !_)
-- -- - - --
10.00
Dry brown sandy Backfill yj
ffi debris
Wet Tan -brown medium
grained Sand
Groundwater Elevation
June 16,
0.0
lExtent of Nutrient and
r enic Groundwater Contamination
- 10.0
/
---
-10.0
Wet To -brown medium
grained n
g dSad
7 -7-
-
- 20.0
Wet Tan -brown
medium rained Sand
/
- 30.0
f
/-Z' L /
-
- 40.0
--- - 40 C'
•
Hotizon tol Scale.
„
l = 150
TITLE: FIGURE NO:
G.W. CONTAMINANT CROSS-SECTION 11
PAM
SCALE: PROJECT NO.
1" = 150'
Vertical Scale 1
= 10
B -B'
Almont Shipping
REV. BY:
PREP. BY: DATE:
Babb &Associates, P.A. Wilmington,
North Carolina GDB
TRW 7/1 /05

\ •\•\j,oG:'\tiQ• ,\ '\, �' -—INTH 6SEPlClOgtN�I) 8S/
�` �N
qpHRRSTREET STREET
NRTFORTFFRONT
(PUeUC/W) y4 _
j I I Ii I
_.—_-- '`•• I I I I
S
�R1VER VENTURES, LLC— 'I COO NY
—__—_ , 12
J' Vila
00
Z oi.
0 \ \ \ ` ' J L- FR T SHEET (pUSUC RM
15.0 —
U7.
I Fee f �, �, I NORTH °N --- — r-- — --
�; •. — Location) ;I I
\ " � "' • - (st of d
/ sE�eo t o
,vr° MW
AST �vE Loco i n)
cow E im ,
---- `"------------' (Estimated I � I
--------.--- ------ :----
7L--------- r Rn� taosEoi I I 1 0. 34 07
ao raoMr smeer n n—�aasco}'— ao ma+r smcE ---
///
— - - _
_ I �C 4 LMW 13 LMW 1- � L
E..._$ MW-15 ® _
�......t,� :•. \ I .I 1 .0 Feet j =` - ---___ —._— --
`/-:`� —_ -
L _
. k—
�<"�` /,r'`•. L'_—__� - -- UTi4TY RJ� — _ MW- I MW-11
2.74
---------- -1009 j I I
Go / w Iy�t 5.0 Feet 5.I I
/ Mw-93.74
® I► 'I I
I 'I (jDMw 1
4.0 Feet 4.00
Mw
— -7 _ 3.89
EA ` I I
NpRrN ST CAPE F ` ' _, \ ®j j
C� EAR R1VFRti �._ 3.70 j l 'I W-4 , MW-2
io
stimoted Loco n) 3.24 I
MW-5 1 I
®3.15 3.0 Feet
I
V! k EAST CAPE
AP FEA R/
Rti � I
tiNpRTN EAST '\ ` ``-•_._ � I
CAPE
R R�VERti I
MW-13, MW-14 and MW-15 have been destroyed
as a result of construction activities on behalf of
new property owner

SECOND SAKM
ov
— -- — -- FRONT STREET OR7H FRONT STREET
(PUBLIC R/W)
11
3.85
\ _-50 Feet--
3.
3.91
�YS
(N~~
`~3�S2
\ \
`Anc LAl?_�____
— 'nV��
~_
\
'
\
Lu"".
\
0 Feet
.`
�
\
\
2.75 /
0�
----^ —~
c*sr
|
^ 'cA��»
�~
~*opry
[Anr
'EA1
RIVER-
MW-13,
as a result of construction activities on behalf of POE GROUNDWATER HYDRAULIC GRAD!EN
new property owner 6-16-05 (Feet)
Almont Shipping
Babb & Associates, P.A. Wilmington, North Corolina
FIGURE NO
13
REV. BY:
GDB
SCALE:
1" =150'
PREP. BY:
---
PROJECT NO.
D/QI:

rN
Ji
�i-

ile 1
Summary of Analytical Data — Soil
Almont Sipping
T7�Ttlminhnn VO
8260
8260
8260
tonal . 'cal.Nietliod � .`. "-r
O r.
M1. o tam iant if CQi%eerri > = . Y`-
m
8260
QUA
2,l
a
4
o,oS
H �,
i�.'7`6
�,
Sair ple
ID
Sampke-=
T:7epf
,=
...Date,- ' `
Co leclecl
a
MW-1
1' - 2'
5/10/05
0.0524
0.0596
ND
ND
MW-2
1' - 2'
5110105
ND
ND
ND
ND
MW-3
1' - 2'
5/10/05
ND
ND
ND
ND
MW-4
1' - 2'
5110105
ND
ND
ND
ND
MW-5
1' - 2'
5/11/05
ND
ND
ND
ND
MW-6
1' - 2'
5/11/05
ND
ND
ND
ND
ND
0.0081
ND
MW-7
1' - 2'
5/11/05
ND
MW-8
l' - 2'
5/11/05
ND
ND
ND
MW-9
1' - 2'
5/11/05
ND
ND
ND
ND
MW-10
1' - 2'
5/11/05
ND
ND
ND
.00804
MW-11
1' - 2'
5/17/05
ND
ND
ND
ND
MW-12
l' - 2'
5/17/05
ND
ND
ND
ND
MW-13
1' - 2'
5/17/05
ND
ND
ND
ND
MW-14
1' - 2'
5/17/05
ND
ND
ND
ND
MW-15
1' - 2'
5/17/05
ND
ND
ND
ND
iYC4 T VVS::S;_Concenratiijz% `
2.81
NRS
0.0183
NRs
Results are in mg/kg
Bold results indicate exceedence of North Carolina Hazardous Waste Section Soil Screening Level

Ale 1
Summary oytical Data - Soil
Almont Shipping
Wilminiton, NC
Analytical Method >
Contaminant
of Concern
>
Sample
Sample
Date
ID
Depth
Collected
O
z
(m/dd/yy)
o
Z
U
Wa
�
z
CZ
zz
�
b
a o
o
0
C�7
Z O
rCi O
O
Q
v'
�
,�
CZ
sO�
sa
N
O
.0
Cn Cn
H E-+
H
U
U
MW-1
1' - 2'
5/10/05
49
14.4
0.94
76.4
676
486
486
ND
11.3
ND
2.69
32.1
0.0693
MW-2
1' - 2'
5/10/05
100
13.2
3.7
7.29
55.3
2078
2080
11.9
21.7
ND
19.0
166
0.725
MW-3
P - 2'
5/10/05
815
40.5
44.9
126
400
3806
3810
3.41
18.0
ND
8.72
25.0
0.0641
MW-4
1' - 2'
5/10/05
93
13.5
35.4
266
95.4
1108
1112
30.2
36.2
ND
42.6
93.4
0.176
MW-5
1' - 2'
5/10/05
61
27
1.76
233
56.8
526
529
7.17
43.2
ND
15.6
76.3
0.142
MW-6
1' - 2'
5/11/05
29
842
1.47
76
127
120
122
ND
ND
ND
6.07
1.49
ND
MW-7
1' - 2'
5/11/05
48
36.4
ND
150
56.4
448
448
ND
ND
ND
2.14
3.79
ND
MW-8
1' - 2'
5/11/05
67
2346
2.47
260
64.7
856
858
4.18
42.4
ND
29.5
1260
0.0811
MW-9
1' - 2'
5/11/05
57
12.2
0.88
84
54.1
65
66
ND
ND
ND
0.957
1.20
ND
MW-10
1' - 2'
5/11/05
38
47.2
5.87
217
68.4
285
361
25.8
21.5
ND
11.8
52.4
0.138
MW-11
1' - 2'
5/12/05
42.9
110
ND
158
24.7
1675
1676
2.55
ND
ND
2.33
28.3
0.216
MW-12
1' - 2'
5/17/05
15
474
ND
132
51.6
489
490
ND
ND
ND
1.01
5.83
0.0360
MW-13
1' - 2'
5/17/05
359
327
348
8.19
194
3415
3422
ND
ND
ND
1.96
2.92
ND
MW-14
1' - 2'
5/17/05
108
669
1.14
204
165
354
365
ND
ND
ND
2.10
10.6
0.0315
MW-15
1' - 2'
5/17/05
213
84.7
13.5
149
186
508
531
7.70
ND
ND
19.0
5.91
ND
x
NRS
I NRS
NRS
NRS
NRS
NRS
NRS
15.24
848
2.72
1 27.2
270
0.0154
Results are in mg/kg
Bold results indicate exceedence of North Carolina Hazardous Waste Section Soil Screening Level

TahlQ 2 •
` Summary of Analytioata - Groundwater
Almont Shipping
8260
8260
vv 11111111
8260
lval,
8260
♦.—
8260
8260
8260
8260
8260
8260
Analytical
Method >
Contaminant
of Concern
>
r0
v�
o
O
p
O
cz W
H
O
v
N
Well
ID
Sample ID
Date
Collected
0.00488
0.140
0.00217
0.00562
ND
ND
ND
ND
ND
ND
MW-1
MW-1
5/25/05
ND
ND
ND
ND
o.oas2
ND
ND
ND
ND
ND
MW-2
MW-2
5/25/05
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-3
MW-3
5/25/05
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-4
MW-4
5/25/05
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-5
MW-5
5/25/05
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-6
MW-6
5/25/05
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-7
MW-7
5/25/05
ND
0.00331
0.00121
ND
ND
ND
0.00112
0.00407
0.00302
ND
ND
MW-8
MW-8
5/25/05
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-9
MW-9
5/25/05
MW-10
MW-10
5/25/05
ND
ND
ND
ND
ND
ND
ND
ND
0.070
ND
ND
ND
ND
ND
ND
ND
ND
NRS
ND
ND
ND
ND
ND
1.600
ND
ND
0.0007
ND
ND
ND
ND
ND
0.024
ND
ND
0.0028
ND
ND
ND
ND
ND
ND
ND
ND
0.021
ND
ND
ND
ND
ND
ND
ND
ND
0.070
ND
ND
ND
ND
ND
ND
ND
ND
0.070
ND
ND
ND
ND
ND
ND
ND
ND
0.070
ND
ND
ND
ND
0.00143
ND
ND
ND
0.200
ND
ND
ND
ND
ND
0.0127
ND
ND
0.070
MW-12
MW-12
5/25/05
MW-13
MW-13
5/25/05
MW-14
MW-14
5/25/05
5/25/05
MW-15
MW45
MW-16
MW-16
5/25/05
LM-13
LM-13
5/25/05
DW-1
DW-1
5/25/05
DW-2
DW-2
5/25/05
2L Standard
m 1
Results are in mg/l
Bold results indicate exceedence of 2L Standards

T* •
Summary of Analytical Data - Groundwater
Almont Shipping
«Iilminotnn Mr'
Analytical Method >
Contaminant
of Concern
>
o
oz
M
xx
¢z
b
O
Zo
Uz
I I
zz
a
o
C)
a
°
z
6
�H
z'
ate+
�
¢`'
as
O
U
a
Well
ID
Sample
ID
Date
Collected
(m/dd/yy)
MW-1
MW-1
5/25/05
8.4
9.5
ND
0.94
58
91
91
0.0248
ND
ND
ND
ND
ND
ND
MW-2
MW-2
5/25/05
0.6
10
1.54
2.57
106
4.5
6
0.0304
ND
ND
ND
ND
ND
ND
MW-3
MW-3
5/25/05
86.2
135
59.1
0.49
538
115
184
ND
ND
ND
ND
ND
ND
ND
MW-4
MW-4
5/25/05
1,123
245
59.1
4.51
620
1,154
1,213
0.911
ND
ND
0.0253
0.0334
0.0042
ND
MW-5
MW-5
5/25/05
0.7
2,185
0.64
0.48
302
3.9
4.5
ND
ND
ND
ND
0.0137
ND
ND
MW-6
MW-6
5/25/05
24.1
1,354
ND
0.72
29
44.8
44.8
ND
0.0129
ND
ND
ND
ND
ND
MW-7
MW-7
5/25/05
7.6
3,491
0.05
1.73
ND
8.4
8.4
0.0881
ND
ND
0.0253
ND
ND
ND
MW-8
MW-8
5/25/05
4.6
20,901
ND
0.35
260
10.6
10.6
0.0266
0.315
ND
ND
ND
ND
ND
MW-9
MW-9
5/25/05
2.2
290
ND
1.65
128
6.7
6.7
0.0133
ND
ND
ND
ND
ND
ND
MW-10
MW-10
5/25/05
1,820
712
27
5.07
585
2,100
2,244
0.713
ND
ND
ND
ND
0.00026
0.0240
MW-12
MW-12
5/25/05
35.6
428
44
0.13
94
37.8
88.1
ND
ND
ND
ND
ND
ND
ND
MW-13
MW-13
5/25/05
284
6,888
28.7
0.16
730
297
344
0.0137
0.413
ND
ND
ND
ND
ND
MW-14
MW-14
5/25/05
2,919
7,838
614
0.91
1,710
3,332
4,285
0.0622
ND
ND
ND
ND
ND
0.0443
MW-15
MW-15
5/25/05
3,180
14,726
317
5.21
2,790
3,920
4,250
0.0596
ND
ND
0.0144
0.0308
0.00165
0.0645
MW-16
MW-16
5/25/05
23.9
176
ND
2.5
158
29.1
29.1
0.0129
0.115
ND
ND
ND
ND
ND
LM-13
LM-13
5/25/05
0.4
18.5
3.15
0.94
33
2
5.2
ND
ND
ND
ND
ND
ND
ND
DW-I
DW-1
5/25/05
1.7
89
ND
0.15
16
6.2
6.2
ND
ND
ND
ND
ND
ND
ND
DW-2
DW-2
5/25/05
2,394
2,209
188
3.49
392
3,780
4,075
0.0937
ND
ND
0.0278
ND
ND
0.0583
2L Standard m 1
NRS
250
10
NRS
250
NRS
NRS
0.050
2.0
0.005
1 0.050
0.015
0.0011
0.050
Results are in mg/l
Bold results indicate exceedence of 2L Standards

•
Table 3
Well Construction Information
Almont Shipping
\I7: 7.�.:... ..+.... AT-4, 1-nrn1ina
Well
Casing
YY 11111111
Screened
Interval
lVll1
Bottom of
Well
Top of
Casing
Elevation
Depth to
Water
TOC
Free
Product
Thickness
Groundwater
Elevation
6-16-05
Comments
Well ID
Date
Installed
Date Water
Level
Measured
MW-1
5/10/05
6/16/05
-Depth
0-2
2-12
12
8.00
N/a
3.82
MW-2
5/10/05
6/16/05
0-2
2-12
12
4.96
2.15
2.15
N/a
2.81
MW-3
5/10/05
6/16/05
0-2
2-12
12
4.90
1.10
N/a
3.80
MW-4
5/10/05
6/16/05
0-2
2-12
12
-
N/a
-
MW-5
5/10/05
6/16/05
0-2
2-12
12
8.30
5.55
N/a
2.75
MW-6
5/11/05
6/16/05
0-2
2-12
12
7.96
4.05
N/a
3.91
MW-7
5/11/05
6/16/05
0-2
2-12
12
9.10
5.18
N/a
3.92
MW-8
5/11/05
6/16/05
0-2
2-12
12
9.23
5.24
N/a
3.99
MW-9
5/11/05
6/16/05
0-2
2-12
12
7.77
3.91
N/a
3.86
MW-10
5/11/05
6/16/O5
0-2
2-12
12
7.41
1.94
N/a
5.47
MW-11
5/12/05
6/16/05
0-2
2-12
12
6.49
3.37
N/a
3.12
MW-12
5/17/05
6/16/O5
0-2
2-12
12
28.23
6.08
N/a
22.15
MW-13
5/17/05
6/16/05
0-2
2-12
12
-
-
N/a
-
MW-14
5/17/05
6/16/05
0-2
2-12
.12
-
-
N/a
-
MW-15
5/17/05
6/16/05
0-2
2-12
12
-
-
N/a
-
MW-16
Unknown
6/16/05
6/16/05
Unknown
0-2
Unknown
2-12
Unknown
12
5.11
5.51
1.63
Product
N/a
N/a
3.48
-
Diesel
MW-17
Unknown
LMW-12
12/04
6/16/05
0-2
2-12
12
11.10
2.62
N/a
8.48
LMW-13
12/04
6/16/05
0-2
2-12
12
12.54
2.93
N/a
9.61
RC-4
Unknown
6/16/05
Unknown
Unknown
15
12.39
3.00
N/a
9.39
DW-1
5/12/05
6/16/05
0-35
35-40
40
7.44
5.41
N/a
2.03
DW-2
5/12/05
6/16/05
0-35
35-40
40
7.66
2.47
N/a
5.19

Table 4
Summary of
Groundwater Elevation Data
Almont Shipping
Wilmington, North Carolina
:OSr 2 5
1
levTO
creen:
S
e db av
.F et
e
Int xv
o
. -.: o,.
Relative:
'
:Be o
�.
.Datum
4.03
4.18
3.82
MW-1
8.00
2 -12
3.97
MW-2
4.96
2 -12
1.72
3.24
2.15
2.81
MW-3
4.90
2 -12
0.90
4.00
1.10
3.80
MW-4
-
2 -12
0.40
-
-
-
MW-5
8.30
2 -12
5.15
3.15
5.55
2.75
MW-6
7.96
2 -12
4.07
3.89
4.05
3.91
MW-7
9.10
2 -12
5.40
3.70
5.18
3.92
MW-8
9.23
2 -12
5.02
4.21
5.24
3.99
MW-9
7.77
2 -12
4.03
3.74
3.91
3.86
MW-10
7.41
2-12
1.61
5.80
1.94
5.47
MW-11
6.49
2 -12
-
-
3.37
3.12
MW-12
28.23
2 -12
6.98
21.25
6.08
22.15
MW-13
-
2 -12
-
-
-
-
Page 1 of 2

0 0 0
Table 4
Summary of Groundwater Elevation Data
Almont Shipping
Wilmington, North Carolina
T. lv
Fe a -ov
Relative-
datum
S'careen,'
.- Tnterv. _
eet Beloty
T ' C
4-0
6�X. 6-05:
_
ar;
C7: a�
,.,.
.,
MW-14
-
2-12
-
-
-
-
MW-15
-
2-12
-
-
-
-
MW-16
5.11
Unknown
-
-
1.63
3.48
MW-17
5.51
Unknown
Product
-
Product
-
LMW-12
11.10
2 —12
-
-
2.62
8.48
LMW-13
12.54
2 —12
2.20
10.34
2.93
9.61
RC-4
12.39
Unknown
-
-
3.0
9.39
DW-1
7.44
35 — 40
4.70
2.74
5.41
2.03
DW-2
7.66
35 — 40
2.10
5.56
2.47
5.19
Notes:
TOC = Top of well casing.
D.T.W = Depth to Groundwater
Page 2 of 2

MAY.16_2005 12:4q-AM t r-DENR WIR0
N4.159 ?_F-
•
•
11
NORTH CAR.OLA
VWMMIEl+iT4L1 AN-4mu"fLOlwSSION
DEPARTMMNT OF ENVIRONMMW AND NATURAL USOURCES
RAI,EIGH, NORTH CAROLINA
PST FOR THE CONSTRUCTION OF A WELL OR WELL SYSTM
In woordsnco With the provisions of Article 7, Ch�-a� t 87, North Carolsna ne State
and other applicable Laws, R !es and 1-110 lations,
PERMISSION IS HEMP GRAI iTEH TO
.Almont 5hippft
FOR TFM CONMUMON OF six ( monitoring we% which will be aqm=4 to the
stwficia: aquift, and which will to located in Wftir ton, New 11anover County, in aecvrdans
vith the m5plickdon dated April 29, 2004, and m ►,onformtty with �cetiom and supporf ling
data, all cf yhich av filed with the Oegarane= of Environment:2'N rat i cso=es and we
considered a pert of this Permit,
This Permit is for well constmcdon only, and does not wswe an provisions or regents of
the W Use Act of 1967, or any other applicable Imys or reatious. Well co truction shall
be in. complince with she North Carolina -Well +Cone t'tiotion gulations wd Standards.
This Permit will be emotive ftom the d4te of its isomw =W November 17, 2005, and shall be
subj,W to Ohm sNrificd conditions, limi ous, or exceptions as follows:
The Well ) shall be located and consbucW as shovm on the atiachments
submitted as part of the permit application,
2. Well cons Lion mords must be sullied to the Division within 30 d4ys
of weLf completion.
If an rwui eats or limita�iions of this Permit are unaeoe table, you have the right to an
� . hewing, upon written request Nvithin 30 clays, a quest must he in the form of a
F
iRh-
pe�te C7447. Unless st3ch demo is �, the tom$ is na�3 a i biz is:g.
Permit issued this the 16th day of May 2005.
NOSH CAROLINA ENVMON3EMAL MANAGEENT CONMSSION
Coles, St,--tunan, ^�-irc eQ 'onSupervisor I
Division of S"ater �ty ai
By Aulhority of the Environ=memW It4aa40ement commission
PU,IT NO. ir'-MOS00699
C F8 $PW
v: TOM Will, 8W Coast EnvironmcnW

NORTH CAROLINA DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER QUALITY - GROUNDWATER SECTION
APPLICATION FOR PERMIT TO CONSTRUCT A MONITORING WELL SYSTEM
(Please Type or Print Clearly)
*ate: 4-29 2005 County New Hannvar
In accordance with the provisions of Article 7, Chapter 87, General Statutes of North Carolina and regulations pursuant
thereto, application is hereby made for a permit to construct monitoring wells.
1. Name of Applicant: Alinoiat Shi ppincl (Telephone: [phone]
Applicant's Mailing Address: One Hanover Street, P.O. Box 1726, Wilmington., NC 28402
2. Name of Property Owner (if different from Well Owner): Pharmaceutical Product T)eVP1 nr MPnt
Owner's Mailing Address: 31 51 1 7 h Street- Fxtensi_ nn , Wilmington, me 28412
3. Contact Person: J11dd Hartman (Telephone: )
4. Location of Property:
5. Reason for Monitoring Well(s): Environmental Assessment -
(ex: nondischarge permit requirements, suspected contamination, environmental assessment, etc.)
6. Type of facility or site for which the monitoring well(s) is needed: Storage
(ex: nondischarge facility, waste disposal site, landfill, underground storage tank, etc.)
7. Type of contamination being monitored (if applicable): nutrient, VOC -s, Metals,
(ex: nutrients, organics, heavy metals, etc.)
�8. Are any existing recovery wells associated with the monitoring well(s)? No If yes, how many?
Recovery Well Construction Permit No.
9. Distance to a known waste or pollution source: __ILLA— feet
10. Are any water supply wells located less than 500 feet from the proposed monitoring wells? No
If yes, give distance: feet
11. Well Contractor. ouantex, Inc
12. Well Contractor Certification #: 31 0 6
13. Well Contractor's Address: P.O. Box 41673, Raleigh, Nr 27629 1 673
.._--- - -- -
Total Number of Wells to be constructed: ?, 6 (0 ; (A) Number to be completed in bedrock? O f
(B) Number to be completed in unconsolidated material? 5
2. Estimated depth of well(s): 12 feet
3. Grave or san pac n erval t a op
From 2 feet To 1 2 feet
4. Type c casing use : PVC
(ex: PVC, stainless steel, galvanized steel, etc.)
5. Diameter of casing: 2 inches
GW-22M (REV 3/2000) (Onntintmd nn RAVRrcal
FOR OFFICE USE ONLY
— PERMITTED ACTIVITY
_ U.S.T. LEAK DETECTION
_ GROUNDWATER QUALITY STANDARDS
VIOLATIONS SUSPECTED FROM UNPERMITTED
ACTIVITIES
NOTICE OF NON-COMPLIANCE AT
UNPERMITTED FACILITIES
PERMIT NO. ISSUED 19
INCIDENT #

East Coast Environmental, P.A.
SOIL BORING LOG
BORING #: MW-1
PROJECT: Almont Shippinglob
No:
TENT: Almont Shi in
Page No: 1 of 1
LING CONTRACTOR: Quantex, Inc.
DRILLING EQUIPMENT: Geo robe
Outer Casing
Inner Casing
Location: Wilmington
Driller Registration: 3106
Date Started: 5110105
Depth
Interval
Casing Mail.
Well Type
Hole Depth
Casing
Screen
Sampler
Well Mat.
Date Completed: 5110105
n/a
n/a
n/a
II
12'
0-2'
2-10'
Tube
PVC
Driller: Barker
Prepared By: Will
Depth
(FT)
Sample
Depth
Range
Sample
Number
VOC
(PPM)
FIELD CLASSIFICATION AND REMARKS
2.5
Dry gray -black sandy backfill
with wood/brick/organic layers
5
*1
320
AIM 7.5
Wet P-ray-yellow well sorted Sand
10
12.5
15
17.5
20
Boring Terminated at 12-feet B.L.S
NOTES: * Split portion of this sample submitted for laboratory analysis

East Coast Environmental, P.A.
SOIL BORING LOG
PROJECT: Almont Shipping
LIENT: Almont Shipping
LLING CONTRACTOR: Quantex, Inc.
DRILLING EQUIPMENT: Geo robe
Outer Casing
Depth Interval Casing Matl. well Type Hole Depth Casing
n/a n/a n/a 1 II 12' 0-2'
Depth I Sample
(FT) Depth
2.5
5
7.5
10
15
17.5
20
BORING #: MW-2
Job No:
Page No: 1 of 1
Location: Wilmington
Driller Registration: 3106
Inner Casing Date Started: 5110105
Screen Sampler well Mat. Date Completed: 5110105
2-12' tube Pvc Driller: Barker
Prepared By: Will
Sample I VOC
Number I (PPM) IFIELD CLASSIFICATION AND REMARKS
Moist black sandy backfill with wood
cinders and shell traaments
Wet brown -tan medium Grained
well sorted Sand
Boring Terminated at 12-teet B.L.S
OTES: * Split portion of this sample submitted for laboratory analysis

East Coast Environmental, P.A.
BORING #: MW-3
SOIL BORING LOG
PROJECT:
Almont Shipping
Job No:
IENT: Almont Shipping
Page No: 1 of 1
LLING CONTRACTOR: Quantex, Inc.
Location: Wilmington
DRILLING
EQUIPMENT: Geo robe
Driller Registration. 3106
Outer Casing
Inner Casing
Date Started: 5/10/05
Depth
Interval
Casing Matl.
Well Type
Hole Depth
Casing
Screen
Sampler
Well Mat.
Date Completed: 5/10/05
n/a
n/a
n/a
II
IT
0-2'
2-12'
tube
PVC
Driller: Barker
Prepared By: Will
Depth
Sample
Sample
VOC
(FT)
Depth
Number
(PPM)
FIELD CLASSIFICATION AND REMARKS
Range
*1
120
Moist gray -black sandy -gravelly backtill
2.5
5
7.5
Wet brown -tan medium Grained
well sorted Sand
10
12.s
Boring 'Terminated at 12-feet B.L.S
15
17.5
20
NU'1'BS: *Split portion of this sample submitted for laboratory analysis

East Coast Environmental, P.A.
SOIL BORING LOG
BORING #: MW-4
PROJECT: Almont Shipping
Job No:
CLIENT: Almont Shipping
Page No: 1 of 1
RILLING CONTRACTOR: Quantex, Inc.
Location: Wilmington
DRILLING EQUIPMENT: Geo robe
Driller Registration: 3106
Outer Casing
Inner Casing
Date Started: 5/10/05
Depth
Interval
Casing Matl.
Well Type
Hole Depth
Casing
Screen
Sampler
Well Mat.
Date Completed: 5110105
n/a
n/a
n/a
II
12'
0-2'
2-12'
tube
PVC
Driller: Barker
Prepared By: Will
Depth
(FT)
Sample
Depth
Range
Sample
Number
VOC
(PPM)
FIELD CLASSIFICATION AND REMARKS
2.5
*1
40
Moist orange -brown -black sandy rill
with brick fragments
5
Wet tan -brown medium ,;rained
well sorted Sand with strong ammonia odors
7.5
10
............
12.5
Boring 'Terminated at 12-feet B.L.S
15
17.5
20
NOTES: * Split portion of this Sample submitted for laboratory analysis

East Coast Environmental, P.A.
SOIL BORING LOG
PROJECT: Almont Shipping
�IENT: Almont Shipping
LLING CONTRACTOR: Quantex, Inc.
DRILLING EQUIPMENT: Geoprobe
Outer Casing
Depth Interval Casing Mad. Well Type Hole Depth Casing
/a n/a n/a II IT 0-T
Depth Sample Sample Voc
(FT) Depth Number (PPM)
Range
........... ............
...........
..........
..........
...........
............
............
.... 40
............
2.5
5
7.5
10
15
17.5
20
BORING #: MW-5
Job No:
Pa e No: I of 1
Location: Wilmington
Driller Registration: 3106
Inner Casing Date Started: 5110105
Screen Sampler Well Mat. Date Completed: 5110105
2-IT tube Pvc Driller: Barker
Prenared Bv: Will
CLASSIFICATION AND REMARKS
Moist to wet fill including bricks -wood -rock, etc.
Wet black muddy Silt
Boring Terminated at 12-feet B.L.S
.rES: * Split portion of this sample submitted for laboratory analysis

East Coast Environmental, P.A. 14>
SOIL BORING LOG
BOILING #: MW-6
PROJECT: Almont Shipping
Job No:
LIENT: Almont Shipping
Page No: 1 of 1
LLING CONTRACTOR: Quantex, Inc.
Location: Wilmington
DRILLING EQUIPMENT: Geo robe
Driller Registration: 3106
Outer Casing
Inner Casing
Date Started: 5/11/05
Depth
Interval
Casing Mati.
Well Type
Hole Depth
Casing
Screen
Sampler _
Well Mat.
Date Completed: 5111105
n/a
n/a
n/a
II
12'
0-2'
2-12'
tube
PVC
Driller: Barker
Prepared By: Will
Depth
(FT)
Sample
Depth
Range
Sample
Number
VOC
(PPM)
FIELD CLASSIFICATION AND REMARKS
2.5
5
*1
20
Dry gray -white Gravel backfill
Dry tan -brown moist medium grained
well sorted Sand
Wet gray -black Sand with rounded quartz pebbles
7.5
to
Wet t,rav-white well sorted Sand
12.5
Boring Terminated at 12-feet B.L.S
15
17.5
20
NOTES: * Sample submitted for laboratory analysis

East Coast Environmental, P.A.
SOIL BORING LOG
BOILING #: MW-7
JECT: Almont Shi in
Job No:
ENT: Almont ShippingPage
No: 1 of 1
J1PRC2
LLING CONTRACTOR: Quantex, Inc.
DRILLING EQUIPMENT: Geo robe
Outer Casing Inner Casing
Location: Wilmington
Driller Registration: 3106
Date Started: 5/11/05
Depth
n/a
Interval Casing
n/a
Mad.
n/a
Well Type
II
Hole Depth
12'
Casing
0-2'
Screen
2-12'
Sampler
tube
well Mat.
PVC
Date Completed: 5/11/05
Driller: Barker
Prepared By: Will
Depth
(FT)
Sample
Depth
Range
Sample
Number
VOC
(PPM)
FIELD CLASSIFICATION AND REMARKS
2.5
5
*1
20
Dry gray -black sandy Silt backtill
Maroon -black sand with iron ore pellets
Dry tan -medium grained Sand
7.5
Wet tan medium grained Sand
10
12.5
Boring 11,emunated at 12-feet B.L.S
15
17.5
20
NOTES:

Y
East Coast Environmental, P.A.
SOIL BORING LOG
PROJECT: Almont Shipping
LIENT: Almont Shipping
LING CONTRACTOR: Quantex, Inc.
DRILLING EQUIPMENT: Geo robe
Outer Casing
Depth Interval Casing Matl. Well Type Hole Depth Casing
n/a n/a n/a II 12' 0-2'
Depth I Sample
(FT) Depth
2.5
E
7.5
10
12.5
15
17.5
20
Sample VOC
Number (PPM)
*1 I 440
'ES: * Sample submitted for laboratory analysis
BORING #: MW-8
Job No:
Page No: 1 of 1
Location: Wilmington
Driller Registration: 3106
Inner Casing Date Started: 5/11/05
Screen sampler Well Mat. Date Completed: 5111105
2-9' tube Pvc Driller: Barker
Prepared By: Will
CLASSIFICATION AND REMARKS
Intermitnat layers of medium grained brown sand
and brick
Wet black muddy sand with wood frapments
Oil sheen in samples from 5 to 12 feet B.L.S.
Boring 'Terminated at 9-feet B.L.S

East Coast Environmental, P.A.
SOIL BORING LOG
PROJECT: Almont Shipping
LIENT: Almont Shipping
LLING CONTRACTOR: Quantex, Inc.
rD��/a
LLING EQUIPMENT: Geo robe Driller Registration: 3106
Outer Casing Inner CasingDate Started: 5111105
pth Interval Casing Mad. Well Type Hole Depth Casing Screen Sampler Well Mat. Date Completed: 5/11/05
n/a n/a II Iz� 0-2� 2-12' tube Pvc Driller: Barker
Prepared By: Will
Depth I Sample
(FT) Depth
2.5
5
7.5
10
15
17.5
20
Sample VOC
Number (PPM)
*1 1 20
OTES: *Sample submitted for laboratory analysis
G #: MW-9
Job No:
Page No: 1 of 1
r ,,,..,.:,,,,. 11T,1 „
CLASSIFICATION AND REMARKS
Fill with asphalt, clayey sand and iron ore pellets
Wet tan -brown medium grained Sand
w minor clay layers
Wet tan -brown medium grained Sand
Boring Terminated at 12-feet B.L.S

East Coast Environmental, P.A.
SOIL BORING LOG
BOILING #: MW-10
PROJECT: Almont Shipping
Job No:
LIENT: Almont Shipping
Page No: 1 of 1
LLING CONTRACTOR: Quantex, Inc.
Location: Wilmington
DRILLING EQUIPMENT: Geo robe
Driller Registration: 3106
Outer Casing
Inner Casing
Date Started: 5/11/05
Depth
Interval
Casing Mad.
Well Type
Hole Depth
Casing
Screen
Sampler
Well Mat.
Date Completed: 5111105
n/a
n/a
n/a
II
12'
0-2'
2-12'
tube
PVC
Driller: Barker
Prepared By: Will
Depth
(FT)
Sample
Depth
Range
Sample
Number
VOC
(PPM)
FIELD CLASSIFICATION AND REZVZF�RKS
2.5
*1
180
Dry brown -tan sandy Gravel Backfill
5
Wet brown -tan medium grained Sand
7.5
Wet tan -brown medium grained Sand
with strong ammonia odors
10
12.5
Boring Terminated at 12-feet B.L.S
15
17.5
20
NOTES: * Sample submitted for laboratory analysis

East Coast Environmental, P.A.
SOIL BORING LOG
PROJECT: Almont Shipping Job No:
kU
ENT: Almont Shi in Page No: 1 of 1
LLING CONTRACTOR: uantex, Inc. Location: Wilmin on
ING EQUIPMENT: Geo robe Driller Registration: 3106
Outer Casing Inner Casing Date Started: 5/17/05
Depth Interval Casing Matl. Well Type Hole Depth Casing Screen Sampler Well Mat. Date Completed: 5/17/05
n/a n/a n/a II 12' 0-2' 2-12' tube PVC Driller: Barker —
Prepared By: Will
Depth I Sample
(FT) Depth
2.5
5
7.5
10
15
17.5
20
Sample VOC
Number (PPM)
* 1 10,000
NOTES: * Sample submitted for laboratory analvsis
BORING #: MW-11
CLASSIFICATION AND REMARKS
Sand with Brick
Wet wood -dirt -sand Backfill
with strong petroleum odor
Wet gray stained medium grained Sand
with strong petroleum odor
Wet tan -brown medium grained Sand
with strong petroleum odors
Boring Terminated at 12-feet B.L.S

East Coast Environmental; P.A. 10>
SOIL BORING LOG
BORING #: MW-12
PROJECT: Almont Shipping
Job No:
NT: Almont Shi in
Pa e No: 1 of 1
LING CONTRACTOR: Quantex, Inc.
kIERLING
Location: Wilmington
DILEQUIPMENT: Geo robe
Driller Registration: 3106
Outer Casing
Inner Casing
Date Started: 5/17/05
Depth
Interval
Casing Mad.
well Type
Hole Depth
Casing
Screen
Sampler
well Mat.
Date Completed: 5/17/05
n/a
n/a
n/a
H
12'
0-2'
2-I2'
tube
Pvc
Driller: Barker
Prepared By: Will
Depth
(FT)
Sample
Depth
Range
Sample
Number
VOC
(PPM)
FIELD CLASSIFICATION AND REMARKS
2.5
* 1
2U
Dry gray -brown sand Backfill
5
ry gray -brown Samd with grave
7.5
Wet gray -brown medium grained Sand
10
12.5
Boring Terminated at 12-feet B.L.S
i
15
17.5
20
NU'1'ES: * Sample submitted for laboratory analysis

East Coast Environmental, P.A.
SOIL BORING LOG
BORING #: MW-13
PROJECT: Almont Shipping
Job No:
IENT: Almont Shipping
Page No: 1 of 1
LING CONTRACTOR: Quantex, Inc.
Location: Wilmington
DRILLING EQUIPMENT: Geo robe
Outer Casing Inner Casing
Driller Registration: 3106
Date Started: 5111105
Depth
Interval
Casing Matt.
Well Type
Hole Depth
Casing
Screen
Sampler
Well Mat.
Date Completed: 5/11/05
n/a
n/a
n/a
II
12'
0-3'
3-13'
tube
PVC
Driller: Barker
Prepared By: Will
Depth
(FT)
Sample
Depth
Range
Sample
Number
VOC
(PPM)
FIELD CLASSIFICATION AND REMARKS
2.5
* 1
40
Dry black -gray sand Backfill
5
Wet yellow -gray mottled wet Sand
with strong ammonia odor
7.5
10
Wet black -brown medium grained well
sorted Sand with strong ammonia odor
12.5
Brown -white sandy Clay
Limestone
15
Boring terminated at 14-feet B.L.S
17.5
20
NOTES: * Sample submitted for laboratory analysis

East Coast Environmental, P.A.
SOIL BORING LOG 4>
BORING ##: MW-15
PROJECT: Almont Shipping
Job No:
LIENT: Almont Shipping
Page No: 1 of 1
RILLING CONTRACTOR: Quantex, Inc.
Location: Wilmington
DRILLING EQUIPMENT: Geo robe
Driller Registration: 3106
Outer Casing
I
Inner Cas' ing
jDate Started: 5/17/05
Depth
Interval
Casing Matl.
Well Type
Hole Depth
Casing
Screen
Sampler
Well Mat.
Date Completed: 5/ 17/05
n/a
n/a
n/a
II
12'
0-2'
2-12'
tube
PVC
Driller: Barker
Prepared By: Will
Depth
(FT)
Sample
Depth
Range
Sample
Number
VOC
(PP1v1)
FIELD CLASSIFICATION AND REMARKS
2.5
*1
60
Wet black -brown sandy Backtill
w brick fragments and strong ammonia odor
5
Yellow -gray sandy Clay with
stroniz ammonia odor
7.5
Wet black -brown medium gained well
sorted Sand with strong ammonia odor
10
12.5
Boring terminated at 12-feet B.L.S
15
17.5
20
'PS: * Sample submitted for laboratory analysis
t

East Coast Environmental, P.A. 10>
SOIL BORING LOG
BORING #: DW-1
PROJECT: Almont Shipping
Job No:
IENT: Almont Shipping
Page No: 1 of 1
LLING CONTRACTOR: Quantex, Inc.
Location: Raleigh
DRILLING EQUIPMENT: CME 55
Driller Registration: 3106
Outer Casing
InnerCasmg
Date Started: 5/12/05
Depth I
Interval
Casing Matl.
Well Type
Hole Depth
Casing
Screen
Sampler
Well Mat.
Date Completed: 5/13/05
1/28/1900
n/a
PVC
III
40'
0-35'
35'40'
Spoon
PVC
Driller: Barker
Prenared Bv: Will
Depth
Sample
Sample
VOC
(FT)
Depth
Number
(PPW
FIELD
10
15
20
25
30
40
FE5:
CLASSIFICATION AND REMARKS
Wet gray -yellow well sorted Sand
Moist gray -brown Clay
Alternating Limestone and Sand lavers
Boring terminated at 40-feet bls

East Coast Environmental, P.A.
SOIL BORING LOG
PROJECT: Almont Shipping
IENT: Almont Shipping
LLING CONTRACTOR: Quantex, Inc.
DRILLING EQUIPMENT: CME 55
Outer Casing
Depth
Interval
Casing Mad.
Well Type
Hole Depth
Casing
1/28/1900
n/a
PVC
III
40'
0-35'
Depth
(FT)
Sample
Depth
I
Sample
Number
VOC
(PPM)
FIELD
10
15
20
25
30
35 I I:::::::::::
NOTES:
RING #: DW-2
Job No:
Page No: 1 of 1
Location: Raleigh
Driller Registration: 3106
Inner Casing Date Started: 5/12/05
Screen Sampler Well Mat. Date Completed: 5/12/05
75'-40, Spoon Pvc Driller: Barker
Prenared Bv: Will
CLASSIFICATION AND REMARKS
Wet Gray -yellow well sorted Sand
with strong ammonia odors
Wet brown -black flowiniz Sand
with strong ammonia odors
Boring terminated at 40-feet bls

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
ELL CONSTRUCTION RECORD
rvio - I
WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
Agricultural ❑ Monitoring
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 00"/34 deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.)
3. OWNER Almont Shipping
Address One Hanover Street
(Street or Route No.)
- --- —Wilmington- NC 28401
City or Town- State Zip Code
4. DATE DRILLED 5-101-05
5. TOTAL DEPTH 12" Ft.
6. CUTTINGS COLLECTED YES ® NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO ®'
8. STATIC WATER LEVEL Below top of Casing: -7- FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASIING IS (-0.20') FT. Above Land Surface
*Top if casing terminated attor below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
0 WATER ZONES (depth): 7'
12. CHLORINATION: Type NIA Amount WA
13. CASING
Wall Thickness
Depth Diameter Or Weight/Ft Material
From 0' To 2' Ft. 2" sch 40 PVC
From To Ft.
From To Ft.
14. GROUT:
Depth
From o' To 1' Ft.
From V To 1.5' Ft.
15. SCREEN:
Material Method
Portland Cement Inject
Bentonite Place/Hydrate
Depth Diameter Slot Size Material
From 2' To 12' Ft. 2" dia. in. 0.010" in. PVC
From To Ft. in. in.
From To Ft. in. in.
16. SAND/GRAVEL PACK:
Depth Size Material
From 1.5 To I Ft. #2 Silica Sand
From To Ft.
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL W CONS RUCT IN.A
STANDARDS, AND THAT A COPY OF THIS ORD IS BE d PR9
Alik
IR�FICIE USE ONLYQuaSubmit
Seri
DRILLING LOG
From To
0' 2'
2' 12'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
I f o mi 0.5 1
ANCE WITH 15A NCAC 2C, WELL CONSTRUCTIONS
TO THE WELL OWNER.
(�-9'05
to Division of Water Quality, Groundwater Section within 30 days
GWA REV. 12/99

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
ELL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
- 2 STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 00"/34 deg 16 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.)
3. OWNER Almont Shipping
Address One Hanover Street
(Street or Route No.)
_Wilmington_.__ _ _ NC 28401
City or Town- State Zip Code
4:_ DATE DRILLED'' 5.- i01- 05.,
5: TOTAL DEPTH' 12' Ft:
6. CUTTINGS COLLECTED YES 0 NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: -7- FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASTING IS (-0.20') FT. Above Land Surface'
Top if casing terminated at/or below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
46, WATER ZONES (depth): 7'
12. CHLORINATION: Type N/A Amount N/A
13. CASING
Wall Thickness
Depth
Diameter Or Weight/Ft. Material
From 0'
To Z
Ft.
2" sch 40 PVC
From
To
Ft.
From
To
Ft.
14. GROUT:
Depth
Material Method
From 0'
To 1'
Ft.'
Portland Cement Inject
From 1'
To 1.5'
Ft.
Bentonite Place/Hydrate
15. SCREEN:
Depth
Diameter Slot Size Material
From 2'
To 12' Ft.
2"
dia. in. 0.010" in. PVC
From
To Ft.
in. in.
From
To Ft.
in. _ in.
16. SAND/GRAVEL PACK:
Depth Size
From 1.5' To 12' Ft. #2
From To Ft.
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL 1
STANDARDS, AND THAT A COPY OF THIS
SROSubmit
Material
Silica Sand
DRILLING LOG
From To
0' 2'
2' 1 Z
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points) .
10 mi 0.5 1
:TED AC ORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTIONS
!EE RO ED'TO THE WELL OWNER.
&"15 -o5
to Division of Water Quality, Groundwater Section within 30 days
GW-1 REV. 12199

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
LL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
AU) STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 0034 deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.)
3. OWNER Almont Shipping
Address One Hanover Street
(Street or Route No.)
-Wilmington NC 28401
City orToVM State Zip Code
4: DATEDRILLED- 54to-0,rj,
5. TOTAL DEPTH." 1Z. Ft.
6. CUTTINGS COLLECTED YES Z NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: —7- FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASTING IS (-0.20') FT. Above Land Surface
*Top if casing terminated at/or below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
WATER ZONES (depth): 7'
12. CHLORINATION:
13. CASING
Type N/A
Depth Diameter
From o' To 2' Ft. 2"
From To Ft.
From To Ft.
14, GROUT:
Depth
From 0' To T
From 1' To 1.5'
15'. SCREEN:
Depth
From 2' To 12' Ft.
From To Ft.
From To Ft.
16. SAND/GRAVEL PACK:
17.
Depth
From 1.6 To
From To
REMARKS:
12'
Amount N/A
Wall Thickness
Or Weight/Ft. Material
sch 40 PVC
Material Method
Ft. Portland Cement Inject
Ft, Bentonite Place/Hydrate
Diameter Slot Size Material
2" dia. in. 0.010" in. PVC
in. in.
in. in.
Size Material
Ft. #2 Silica Sand
Ft.
I DO HEREBY CERTIFY THAT THIS WELL Vt
SAND THAT A COPY OF THI
,R OFFICE USE ONLY
TANDARDS,
d No:Submit
al No.
DRILLING LOG
From To
0' 2'
2' 12'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
IN A CORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTIONS
PR IDED TO THE WELL OWNER.
to Division of Water Quality, Groundwater Section within 30 days
GW-1 REV. 12/99

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
ELL CONSTRUCTION RECORD
WELL CONTRACTOR: James D. Barker
4 WELL CONTRACTOR CERTIFICATION #: 3106
4- STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential El Municipal [I Industrial ❑ Agricultural El Monitoring
Recovery El Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77
One Hanover Street, Wilmington, NC 28401
57' 0034 deg 15' 00"
(Road name and Numbers, Community, or Subdivision and Lot No.) DRILLING LOG
3. OWNER AlmontShipping
Address One Hanover Street
(Street'or Route No.)
Wilmington. - NC 28401
-City or Town State Zip Code.
4: DATE:DRILLED.5-P-U.S
5. TOTAL DEPTH 12" Ft. .
6. CUTTINGS COLLECTED YES' ® NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: -7- FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASIING IS (-0.20') FT. Above Land Surface
Top if casing terminated at/or below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
40 WATER ZONES (depth): 7'
12. CHLORINATION: Type N/A Amount N/A
13. CASING
Wall Thickness
Depth Diameter Or Weight/Ft. Material
From 0' To 2' Ft. 2" sch 40 PVC
From To Ft.
From To Ft.
14. GROUT:
From 0'
From 1'
15. SCREEN:
Depth Material
To T Ft. Portland Cement
To 1.6 Ft. Bentonite
Depth
From 2' To 12' Ft.
From To Ft.
From To Ft.
16. SAND/GRAVEL PACK:
Method
Inject
Place/Hydrate
Diameter Slot Size Material
2" dia. in. 0.010" in. PVC
in. in.
in. in.
Depth Size
From 1.6 To 12' Ft. #2
From To Ft.
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS CO
STANDARDS, AND THAT A COPY OF THIS RECO
R OFFICE USE ONLY
0.2d No:
Submit original to
Serial No.
Material
Silica Sand
From To
0' 2'
2' 12'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
10 mi 0.5 1
:;E WITH 15A NCAC 2C, WELL CONSTRUCTIONS
THE WELL OWNER.
6.00-05
of Water Quality, Groundwater Section within 30 days
GWA REV. 12/99

IN

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
DELL CONSTRUCTION RECORD
mw -S
WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 0034 deg 15' 00"
One Hanover Street, Wilmington, NC 28401 ,
(Road name and Numbers, Community, or Subdivision and Lot No.) DRILLING LOG
3. OWNER AlmontShipping
Address One Hanover Street
(Street or Route No.)
- -Wilmington- - NC 28401
City or Town State Zip Code
4.. DATE DRILLED- 5=-10-6q, .
5. TOTAL.DEPTH 12' - FL -
6. CUTTINGS COLLECTED YES ® NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: — 7' FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASTING IS (-0.20') FT. Above Land Surface
Top if casing terminated at/or below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
40 WATER ZONES (depth): 7'
12. CHLORINATION: Type N/A Amount N/A
13. CASING
Wall Thickness
Depth Diameter Or Weight/Ft. Material
From o' To 2' Ft. 2" sch 40 PVC
From To Ft.
From To Ft.
14. GROUT:
Depth
From 0' To T Ft.
From V To 1.5' Ft.
15. SCREEN:
Material Method,
Portland' Cement Inject
Bentonite Place/Hydrate
Depth
Diameter
Slot Size Material
From
2' To 12'
Ft.
2" dia. in.
0.010" in. PVC
From
To
Ft.
—in.
From
To
Ft.
—in.
—in.
16. SAND/GRAVEL PACK:
—in.
Depth
Size
Material
From
1.5' To
12'
Ft. #2
Silica Sand
From
To
Ft.
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS CO RUCTED IN A
STANDARDS, AND THAT A COPY OF THIS RECOKD F)AS BEA Pt*
R OFFICE USE ONLY
uad No:
Submit original
Serial No.
From To
0' 2'
2' 12'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or -other map reference points)
CE WITH 15A NCAC 2C, WELL CONSTRUCTIONS
THE WELL OWNER.
(0-2).v5
MNSTRUCTING THE WELL DATE
of Water Quality, Groundwater Section within 30 days
GW-1 REV. 12/99

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
ELL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
4 WELL CONTRACTOR CERTIFICATION #: 3106
STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 00"/34 deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.) DRILLING LOG DEPTH
3. OWNER Almont Shipping From To Formation Description
Address One Hanover Street 0' 2' overburden, misc. ground cover, gravel
(Street or Route No.) 2' 12' fine to medium grain sands
Wilmington. NC 28401
City or Town State Zip Code
4: - DATE. DRILLED
5. TOTAL DEPTH 1Z . Ft
6. CUTTINGS COLLECTED YES ® NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: -- 7' FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASIING IS (-0.20') FT. Above Land Surface
Top if casing terminated attor below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A -
11 WATER ZONES (depth): 7'
02. CHLORINATION: Type N/A Amount N/A If additional space is needed use back of form
13. CASING
Wall Thickness
Depth Diameter Or Weight/Ft. Material
From 0' To 2' Ft. 2" sch 40 PVC
From To Ft.
From To Ft.
14. GROUT:
Depth Material Method
From 0' TO 1Ft. Portland Cement Inject
From V TO 1.5' Ft. Bentonite Place/Hydrate
15. SCREEN:
Depth Diameter Slot Size Material
From 2' To 12' Ft. 2" dia. in. 0.010" in. PVC
From To Ft. -in. -in.
From To Ft. -in. -in.
16. SAND/GRAVEL PACK:
Depth Size
From 1.5' To 12' Ft. #2
From To Ft.
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS
STANDARDS, AND THAT A COPY OF THIS RE(
R OFFICE USE ONLY
ad No:
Serial No.
Submit original to
Material
Silica Sand
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
1r0 mi 0.5 1
IN A f )PNCE WITH 15A NCAC 2C, WELL CONSTRUCTIONS
PR IDED O THE WELL OWNER.
NATURE OPPERSON CONSTRUCTING THE WELL DA'
of Water Quality, Groundwater Section within 30 days
GWA REV. 12199

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
10 LL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
gj STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 00"/34 deg 16 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.) DRILLING LOG
3. OWNER AlmontShipping
Address One Hanover Street
. (Street or Route No.)
" Wilmington __ - - NC 28401
City or Town, State Zip Code
4. 'DATE DRILLED- 5-11-05
5. TOTAL DEPTH 9` Ft.
6. CUTTINGS COLLECTED YES ® NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: - 5' FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASIING IS (-0.20") FT. Above Land Surface
*Top if casing terminated atior below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
• WATER ZONES (depth): 5'
12. CHLORINATION: Type N/A
13. CASING
Depth Diameter
From 0' To Z Ft. 2"
From To Ft.
From To Ft.
14. GROUT:
Depth
From o' To 1' Ft.
From 1' To 1.5' Ft.
15. SCREEN:
From
0'
To
2'
Z
9'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
Amount N/A If additional space is needed use back of form
Wall Thickness
Or Weight/FL Material
sch 40 PVC
Material Method
Portland Cement Inject
Bentonite Place/Hydrate
Depth Diameter
From 2' To 9' Ft. 2" dia. in.
From To Ft. in.
From To Ft. in.
16. SAND/GRAVEL PACK:
Depth Size
From 1.5' To 9' Ft. #2
From To Ft.
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL Vt
STANDARDS, AND THAT A COPY OF THIS I
R OFFICE USE ONLY
Quad No:
Submit
Serial No.
Slot Size Material
0.010" in. PVC
in.
in.
Material
Silica Sand
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
I
j 1,0 mi 0.5 1
IANCE WITH 15A NCAC 2C, WELL CONSTRUCTIONS
TO THE WELL OWNER.
C, off
SIGNATURE OF PERSON CONSTRUCTING THE WELL
to Division of Water Quality, Groundwater Section within 30 days
GWA REV. 12199

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
#LL CONSTRUCTION RECORD
vv1vJ . 11
WELL CONTRACTOR: ,lames D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
Agricultural ❑ Monitoring
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington - County: New Hanover 77 deg 57' 00"/34 deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.) DRILLING LOG
3. OWNER Almont Shipping
Address One Hanover Street
(Street or Route No.)
-Wilmington- NC 28401
City or Town state Zip Code
4- DATE- DRI,L= LED -- - If -0-S
5. TOTAL DEPTH 12' ' Ft.
6. CUTTINGS COLLECTED YES ® NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: -7- FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASIING IS (-0.20') FT. Above Land Surface
*Top if casing terminated attor below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
0 WATER ZONES (depth): 7'
12. CHLORINATION: Type N/A Amount N/A
13. CASING
Wall Thickness
Depth Diameter Or Weight/Ft. Material
From 0' To 2' Ft. 2" sch 40 PVC
From To Ft.
From To Ft.
14. GROUT:
Depth
Material
Method
From 0'
To V
Ft.
Portland:Cement
Inject
From 1'
To 1.5'
Ft.
Bentonite
Place/Hydrate
15. SCREEN:
Depth
Diameter Slot Size
Material
From 2'
To 12, Ft.
2" dia. in. 0.010"
in. PVC
From
To Ft.
-in.
From
To -Ft.
-in.
-in.
-in.
16. SAND/GRAVEL PACK:
Depth
Size
Material
From 1.6
To 12,
Ft.
#t2 Silica Sand
From
To
Ft.
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS CO,piStRUCTED0 ACs
STANDARDS, AND THAT A COPY OF THIS RECO D JAS BEEq 'ROVj
Iual
R OFFICE USE ONLY
d No:
Submit original to
No.
From To
0' 2'
2' 12'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
�0 mi 0.5 1
WITH 15A NCAC 2C, WELL CONSTRUCTIONS
E WELL OWNER.
c' 0j=)
of Water Quality, Groundwater Section within 30 days
GWA REV. 12199

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
LL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
ftiW , 10
STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
Agricultural ❑ Monitoring ED
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 00"/34 deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.) DRILLING LOG
3. OWNER Almont Shipping
Address One Hanover Street
(Street or Route No.)
--: --- ---Wilmington- - - - . - NC 28401
City or'Town- State Zip Code
4. DATE' DRILLED $ -12 -0,5
5. TOTAL DEPTH I Ft
6. CUTTINGS COLLECTED YES ® NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: - 7' FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASIING IS (-0.20') FT. Above Land Surface
Top if casing terminated at/or below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
0 WATER ZONES (depth): 7'
12. CHLORINATION: Type NIA Amount N/A
13. CASING
Depth Diameter
From 0' To 2' Ft. 2"
From To Ft.
From To Ft.
14. GROUT:
Depth
From o' To 1' Ft.
From 1' To 1.5' Ft.
15. SCREEN:
Depth
From
2' To 12'
Ft.
From
To
Ft.
From
To
Ft.
16. SAND/GRAVEL PACK:
Depth
From
1.5' To
12'
From
To
17. REMARKS:
Wall Thickness
Or Weight/Ft. Material
sch 40 PVC
Material Method
Portland. Cement Inject
Bentonite Place/Hydrate
Diameter Slot Size Material
2" dia. in. 0.01o" in. PVC
in. in.
in. in.
Size Material
Ft. #2 Silica Sand
Ft.
I DO HEREBY CERTIFY THAT THIS WELL WAS C(
STANDARDS, AND THAT A COPY OF THIS RECOI
oR OFFICE USE ONLY
uad No:
Submit original
Serial No.
From To
0' 2'
Z 1Z
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map referbnce points)
10 mi 0.5 1
CTED I CCO ANCE WITH 15A NCAC 2C, WELL CONSTRUCTIONS
BEEN OVI TO HE WELL OWNER.
GNATURE O PERSON CONSTRUCTING THE WELL DATE
i of Water Quality, Groundwater Section within 30 days
GW-1 REV. 12/99

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
ELL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
t�Y1Ll} j STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring N
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 00"/34'deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.) DRILLING LOG
3. OWNER AlmontShipping
Address One Hanover Street
(Street or Route No.)
�- .- - • --Wilmington NC 28401
City or Town State Zip Code
_ 4:. - DATE DRILLED 5 -13 -US•
5. TOTAL DEPTH. 1Z FL
6. CUTTINGS COLLECTED YES N NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO N
8. STATIC WATER LEVEL Below top of Casing: - 7' FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASTING IS (-0.20') FT. Above Land Surface
Top if casing terminated attor below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
40 WATER ZONES (depth): 7'
12. CHLORINATION: Type NIA Amount N/A
13. CASING
Wall Thickness
Depth Diameter Or Weight/Ft. Material
From 0' To 2' Ft. 2" sch 40 PVC
From To Ft.
From To Ft.
14. GROUT:
Depth Material Method
From 0' To 1' Ft. Portland Cement Inject
From 1' To 1.5' Ft. Bentonite Place/Hydrate
15. SCREEN:
Depth Diameter Slot Size Material
From 2' To 12' Ft. 2" dia. in. 0.010" in. PVC
From To Ft. -in. -in.
From To Ft. in. in.
16. SAND/GRAVEL PACK:
Depth Size Material
From 1.5' To 12' Ft. #2 Silica Sand
From To Ft.
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS COj>RUCTED A
STANDARDS, AND THAT A COPY OF THIS RECOJqD FIAS BEENMC
R OFFICE USE ONLY
ad No:
Submit original to
Serial No.
From To
0' 2'
2' 12'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION' SKETCH
(Show, direction, arid' -distance from at least two State
Roads., or other_ man. reference points)
SJ+l1•�J
Y f r ` Wiz,+ +rz� • x �� �� -.� �'
'{.�- V.r'� J ' � ,•'�`ra ciG[l�S���� rs..' 7 «. '4""... �:._ ..ems
to mi 0.5 1
iANC E WITH-15A NCAC2C, wEiLL CONSTRUCTIONS
TO 7HE WELL OWNER.
of Water Quality, Groundwater Section within 30 days
GW-1 REV. 12/99

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
46 ELL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
VAW ,) 3 STATE WELL CONSTRUCTION PERMIT #: WA
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
Agricultural ❑ Monitoring
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 0034 deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.)
3. OWNER AlmontShipping
Address One Hanover Street
(Street or Route No.)
�•— Wilmington.. NC 28401
Cityor•Town State Zip Code
4. DATE DRILLED 5_t3---CG -
5. TOTAL DEPTH 12'' FL
6. CUTTINGS COLLECTED YES ® NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: -7- FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASTING IS (-0.20') FT. Above Land Surface
Top if casing terminated attor below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
0WATER ZONES (depth): 7'
. CHLORINATION: Type N/A Amount N/A
13. CASING
Wall Thickness
Depth
Diameter Or Weight/Ft. Material
From 0'
To 2'
Ft.
2" sch 40 PVC
From
To
Ft.
From
To
Ft.
14. GROUT:
Depth
Material Method
From 0'
To 1'
Ft.
Portland'Cement Inject
From 1'
To 1.5'
Ft.
Bentonite Place/Hydrate
15. SCREEN:
Depth
Diameter Slot Size Material
From 2'
To 12 Ft.
2"
dia. in. 0.010" in. PVC
From
To Ft.
—in. —in.
From
To Ft.
in. in.
16. SAND/GRAVEL PACK:
Depth Size
From 1.5' To 12' Ft. #2 _
From To Ft. _
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS C
STANDARDS, AND THAT A COPY OF THIS REC C
ra
R OFFICE USE ONLY
d No:
Submit original to
Serial No.
Material
Silica Sand
DRILLING LOG
From To
0' 2'
2' 12'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction- and. distance from at least two State
Roads, or, other map reference points)
i ,O mi 0.5 r
CTED I C AN E WITH 15A NCAC 2C, WELL CONSTRUCTIONS
BEEN P VI O HE WELL OWNER.
V- G - a -05
GNATURE OF PERS N CONSTRUCTING THE WELL DATE
i of Water Quality, Groundwater Section within 30 days
GWA REV. 12199

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
4 ELL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #. 3106
V' w - STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 00"/34 deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.)
3. OWNER Almont Shipping
Address One Hanover Street
(Street or Route No.)
77­-- --Wilmington- NC 28401
CityorTown -- State Zip Code
4,- DATE -:DRILLED` 5._
5- TOTAL DEPTH' 12' Ft
6. CUTTINGS COLLECTED YES ®K NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: - 7' FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASTING IS (-0.20') FT. Above Land Surface+
Top if casing terminated atfor below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
11 WATER ZONES (depth): 7'
02. CHLORINATION: Type NIA Amount NIA
13. CASING
Wall Thickness
Depth Diameter Or Weight/Ft. Material
From 0' To 2' Ft. 2" sch 40 PVC
From To Ft.
From To Ft.
14; GROUT:
Depth
From 0' To V Ft.
From. V To 1.5' Ft.
1-5. SCREEN:
Material Method
Portland Cement Inject
Bentonite Place/Hydrate
Depth
Diameter
Slot Size Material
From 2' To 12'
Ft.
2" dia. in.
0.010" in. PVC
From To
Ft.
in.
in.
From To
Ft.
in.
in.
16. SAND/GRAVEL PACK:
Depth
Size
Material
From 1.5' To
12'
Ft. #2
Silica Sand
From To
Ft.
17. REMARKS:
'
CERTIFYI DO HEREBY THIS WELL WAS
INA
STANDARDS, AND THAT A COPY OF THIS RECJ6R HAS BE�NN PRJ
R OFFICE USE ONLY
ad No:
Submit
Serial No.
DRILLING LOG
From To
0' 2'
2' 12'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium gran sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
CE WITH 15A NCAC 2C, WELL CONSTRUCTIONS
THE WELL OWNER.
6 - 0)- d5
to Division of Water Quality, Groundwater Section within 30 days
GW-1 REV. 12J99

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
4 ELL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
I A A W , 15 STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
Agricultural ❑ Monitoring
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 00"/34 deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.)
3. OWNER AlmontShipping
Address One Hanover Street
(Street or Route No.)
Wilmingtort.. _._ NC 28401
CityorTown State Zip Code
4.. D'ATEI-DRILLED
5. TOTAL. DEPTH -12' Ft:
6. CUTTINGS COLLECTED YES ® NO ❑
7. DOES -WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: ~ 7' FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASIING IS (-0.20') FT. Above Land Surface
.Top if casing terminated at/or below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
1 WATER ZONES (depth): 7'
'R2. CHLORINATION: Type N/A Amount N/A
13. CASING
Wall Thickness
Depth
Diameter Or Weight/Ft. Material
From 0'
To 2'
Ft. 2" sch 40 PVC
From
To
Ft.
From
To
Ft.
14. GROUT:
Depth
Material Method
From 0'
To 1'
Ft. Portland Cement Inject
From 1'
TO 1.5'
Ft. Bentonite Place/Hydrate
15. SCREEN:
Depth
Diameter Slot Size Material
From 2'
To 12' Ft.
2" dia. in. 0.010" in. PVC
From
To Ft.
in. in.
From
To Ft.
-in. -in.
16. SAND/GRAVEL PACK:
Depth-
Size Material
From 1.5'
To 12'
Ft. #2 Silica Sand
From
To
Ft.
17. REMARKS:
DRILLING LOG
From To
0' 2'
2' 12'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
!0 mi 0.5 1
I DO HEREBY CERTIFY THAT THIS WELL WAS N RUCTED AC RD CE WITH 15A NCAC 2C, WELL CONSTRUCTIONS
STANDARDS, AND THAT A COPY OF THIS REC RD AS BEE P O EDT THE WELL OWNER.
R OFFICE USE ONLY
uad No: SIGNATURE PERSON CONSTRUCTING THE WELL DATE
Submit original t 'Division of Water Quality, Groundwater Section within 30 days
Serial No. GWA REV. 12199

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
46 ELL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
STATE WELL CONSTRUCTION PERMIT #: N/A
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑ Agricultural ❑
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 00"134 deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.) DRILLING LOG
3. OWNER AlmontShipping
Address One Hanover Street
(Street or Route No.)
Wilmington- - ____ _ _ .. - NC 28401
CityorTown- State Zip Code
4. DATE DRILLED,,
5. TOTAL'DEPTH 40" FL
6. CUTTINGS COLLECTED YES ® NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: —7- FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASTING IS (-0.20') FT. Above Land Surface
'Top if casing terminated atfor below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): N/A METHOD OF TEST N/A
40 WATER ZONES (depth): 7', 24', 38'
12. CHLORINATION: Type N/A Amount N/A
13. CASING
Wall Thickness
Depth
Diameter
Or Weight/Ft. Material
From
0' To 35'
Ft. 2"
sch 40 PVC
From
0' To 28'
Ft. 4"
sch 40 PVC
From
To
Ft.
14. GROUT:
Depth
From 0' To 32' Ft.
From 32' To 34' Ft.
15. SCREEN:
Material Method
Portland Cement Inject
Bentonite. Place/Hydrate
Depth
Diameter
Slot Size Material
From 35' TO 40'
Ft.
2" dia. in.
0.010" in. PVC
From To
Ft.
-in.
From To
Ft.
-in.
-in.
-in.
16. SAND/GRAVEL PACK:
Depth
Size
Material
From 34' To
40'
Ft. #2
Silica Sand
From To
Ft.
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS CONST U TED IN A
STANDARDS, AND THAT A COPY OF THIS RECORD AS KEN PR4
R OFFICE USE ONLY
ad No:
Submit original to
Serial No.
From To
0' 1'
1' 12'
12' 40'
Monitoring
DEPTH
Formation Description
overburden, misc. ground cover
fine sands
fine sands, sandy clay, shell deposits
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
10 mi 0.5 1
FITH 15A NCAC 2C, WELL CONSTRUCTIONS
WELL OWNER.
(0--5-05
NATURE OF PERSON CONSTRUCTING THE WELL
of Water Quality, Groundwater Section within 30 days
GWA REV. 12/99

North Carolina -Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636 - Phone [phone]
OfLL CONSTRUCTION RECORD WELL CONTRACTOR: James D. Barker
WELL CONTRACTOR CERTIFICATION #: 3106
STATE WELL CONSTRUCTION PERMIT #: NIA
1. WELL USE (Check Applicable Box): Residential ❑ Municipal ❑ Industrial ❑
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
Agricultural ❑ Monitoring
WELL LOCATION: (Show sketch of the location below)
Nearest Town: Wilmington County: New Hanover 77 deg 57' 00"/34 deg 15' 00"
One Hanover Street, Wilmington, NC 28401
(Road name and Numbers, Community, or Subdivision and Lot No.)
3. OWNER Almont Shipping
Address One Hanover Street
(Street or Route No.)
__. _ • • VNifmington - - NC 28401
City, or Town` , State Zip Code
4.. DA_TE'DRILLED ' 5-13-05
5. TOTAL DEPTH 40' Ft
6. CUTTINGS COLLECTED YES ® NO ❑
7. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
8. STATIC WATER LEVEL Below top of Casing: — 7' FT.
(Use "+" if Above Top of Casing)
9. TOP OF CASTING IS (-0.20') FT. Above Land Surface
Top if casing terminated at/or below land surface required a variance in accor-
dance with 15A NCAC 2C .0118
10. YIELD (gmp): NIA METHOD OF TEST N/A
0 WATER ZONES (depth): 7'
12. CHLORINATION: Type N/A Amount NIA
13. CASING
Wall Thickness
Depth Diameter Or Weight/Ft. Material
From 0' To 35, Ft. ' 2" sch 40 PVC
From To Ft.
From To Ft.
14. GROUT:
Depth
Material
Method,
From 0'
To 32'
Ft. Portland Cement
Inject
From 32'
TO
Ft. Bentonite
Place/Hydrate
15. SCREEN:
Depth
Diameter Slot Size
Material
From 35'
To 40' Ft.
2" dia. in. o.olo"
' in. PVC
From
To Ft.
in.
in.
From
To Ft.
in.
in.
16. SAND/GRAVEL PACK:
Depth Size
From 34' To 40, Ft. #2
From To Ft.
17. REMARKS:
I DO HEREBY CERTIFY THAT THIS WELL WAS
STANDARDS, AND THAT A COPY OF THIS
OR OFFICE USE ONLY
Quad No:
Submit o
Serial No.
Material
Silica Sand
DRILLING LOG
From To
0' 2'
2' 40'
DEPTH
Formation Description
overburden, misc. ground cover, gravel
fine to medium grain sands
If additional space is needed use back of form
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
NSTRUCT D IN CO ANCE WITH 15A NCAC 2C, WELL CONSTRUCTIONS
O D HAS N ID TO THE WELL OWNER.
SIGNAT E OF PERSON CONSTRUCTING THE WELL DATE
ial to Division of Water Quality, Groundwater Section within 30 days
GWA REV. 12t99

•
•
Almont Shipping
Almont Shipping June 16, 2005
Almont Shipping Wilmington, North Carlolina
1. a
* 0
to
•••
ot
41000*
Hydraulic Conductivity = 2.306 feet/day
Transmissivity = 41.51 ft2/day
Client: Almont Shipping
Analysis by Page 1
6f23/2005
Bouwer and Rice Graph
MW-1 Falling Head
Bouwer and Rice parameter A = 3.179
Bouwer and Rice parameter B = 0.6662
ln(Re/Rw) = 2.770971e*000
Analysis starts at time 6. seconds
Analysis ends at time 3.2 minutes
63 Measurements analyzed from 4 to 66
9060*600
Adjusted Time (minutes)
Ho is 1.82 feet at 6. seconds

•
0
•
Almont Shipping
Ahnont Shipping June 16, 2005
Almont Shipping Wilmington, North Carlolina
1. -a
_ 0.1
b
x •• •
Hydraulic Conductivity = 0.9011 feet/day
Transmissivity = 36.04 ft2/day
Client: Ahnont Shipping
Analysis by Page 1
6/23/2005
3
Bouwer and Rice Graph
MW-3 Rising Head
Bouwer and Rice parameter A = 3.163
Bouwer and Rice parameter B = 0.6638
ln(Re/Rw) = 2.682132e+000
Analysis starts at time 6. seconds
Analysis ends at time 5.6 minutes
111 Measurements analyzed from 3 to 113
20 Points not plotted because head ratio — 0.0
These points are not included in the analysis
•
•
•
Adjusted Time (minutes)
Ho is 1.389 feet at 6. seconds

•
•
Almont Shipping
Almont Shipping June 16, 2005
Almont Shipping Wilmington, North Carlohna
1.
Hydraulic Conductivity = 2.525 feetfday
Transmissivity = 101. ft2/day
Client: Almont Slipping
Analysis by Page 1
623/2005
Bouwer and Rice Graph
MW-3 Falling Head
Bouwer and Rice parameter A = 3.153
Bouwer and Rice parameter B = 0.6638
In(Re/Rw) = 2.682132e+000
Analysis starts at time 9. seconds
Analysis ends at time 3.95 minutes
77 Measurements analyzed from 4 to 80
21 Points not plotted because head ratio <= 0.0
These points are not included In the analysis
•
M
Adjusted Time (minutes)
Ho is 1.188 feet at 9. seconds

•
0
Almont Shipping
Ahnont Shipping June 16, 2005
Aimont Shipping Wilmington, North Carlohna
1.
ti
•
Hydraulic Conductivity =1.946 feet/day
Transmissivity = 77.84 ft2/day
0 1
Client: Almont Shipping
Analysis by Page 1
6/232005
Bouwer and Rice Graph
MW-6 Rising Head
Bouwer and Rice parameter A = 3.179
Bouwer and Rice parameter B = 0.6662
In(Re/Rw) = 2.686204e+000
Analysis starts at time 3. seconds
Analysis ends at time 3.55 minutes
71 Measurements analyzed from 2 to 72
14 Points not plotted because head ratio — 0.0
These points are not included in the analysis
Adjusted Time (minutes)
Ho is 2.13 feet at 3. seconds

Almont Shipping
Almont Shipping June 16, 2005
Almont Slipping Wilmington, North Carlolina
1.
0.1
Hydraulic Conductivity=1.992e-003 feet/day
Transmissivity = 7.97e-002 Wday
Client: Almont Shipping
Analysis by Page 1
•
•
U23/2005
Bouwer and Rice Graph
MW-6 Falling Head
Bouwer and Rice parameter A = 3.179
Bouwer and Rice parameter B = 0.6662
ln(Re/Rw) = 2.686204e+000
Analysis starts at time 9. seconds
Analysis ends at time 2.7 minutes
52 Measurements analyzed from 4 to 55
Adjusted Time (minutes)
Ho is 66.76 feet at 9. seconds

•
C
•
Almont shipping
Almont Shipping June 16, 2005
Almont Shipping Wilmington, North Carlolina
I.
•
•
Hydraulic Conductivity =1.656 feet/day
Transmissivity = 66.25 ft2/day
Client: Almont Shipping
Analysis by Page 1
6/23/2005
n
Bouwer and Rice Graph
MW-10 Falling Head
Bouwer and Rice parameter A = 3.179
Bouwer and Rice parameter B = 0.6662
In(Re/RW) = 2.686204e+000
Analysis starts at time 3. seconds
Analysis ends at time 3.85 minutes
77 Measurements analyzed from 2 to 78
Adjusted Time (minutes)
He is 1.325 feet at 3. seconds

Almont Shipping
Almost Shipping June 16, 2005
Ahnont Shipping Wilmington, North Carlolina
1. r.
Hydraulic Conductivity = 1.065 feet/day
Transmissivity = 42.69 ft2/day
Client: Almont Slipping
Analysis by Page 1
•
6/2=005
Bonwer and Rice Graph
MW-10 Rising Head
Bouwer and Rice parameter A = 3.179
Bouwer and Rice parameter B = 0.6662
in(Re/RW) = 2.686204e+000
Analysis starts at time 3, seconds
Analysis ends at time 6.25 minutes
125 Measurements analyzed from 2 to 126
6 Points not plotted because head ratio <= 0.0
These points are not included in the analysis
Jip
Adjusted Timo (minutes)
Ho is 1.074 feet at 3. seconds

(a
•
•
Almont Shipping
Ahnont Shipping June 16, 2005
Almont Shipping Wilmington, North Carlolina
1.
Hydraulic Conductivity = 0.1274 feet/day
Transmissivity = 3.823 ft2/day
Client: Ahnont Shipping
Analysis by Page 1
t3I23/2005
Bouwer and Rice Graph
DW-1 Falling Head
Bouwer and Rice parameter A = 2.7
Bouwer and Rice parameter B = 0.5
In(Re/Rw) = 3.274151ef000
Analysis starts at time 3. seconds
Analysis ends at time 3.75 minutes
75 Measurements analyzed from 2 to 76
1 points not plotted because head ratio — 0.0
These points are not included in the analysis
Adjusted Time (minutes)
Ho is 0.586 feet at 3. seconds

•
•
•
Almont Shipping
Almont Shipping June 16, 2005
Almont Shipping Wilmington, North Carlolina
1.
o.l
M4
Hydraulic Conductivity = 0.1417 feet/day
Transmissivity = 5.67 f0day
Client: Almont Shipping
Analysis by Page 1
Bouwer and Rice Graph
DW-2 Rising Head
Bouwer and Rice parameter A = 2.512
Bouwer and Rice parameter B = 0.4732
In(Re/Rw) = 2,912275e+000
Analysis starts at time 6. seconds
Analysis ends at time 19.4 minutes
387 Measurements analyzed from 3 to 389
to is
6/23/2005
Adjusted Time (minutcs)
Ho is 2.342 feet at 6. seconds

•
•
•
Almont Shipping
Almont Shipping June 16, 2005
Almont Shipping Wilmington, North Culohna
1.
Hydraulic Conductivity = 0.3947 feetiday
Transmissivity = 15.79 ft2/day
Client: Almont Shipping
Analysis by Page 1
6/23/2005
Bouwer and Rice Graph
DW-2 Failing Head
Bouwer and Rice parameter A = 2.512
Bouwer and Rice parameter B = 0.4732
ln(Re/RW) = 2.912275e+000
Analysis starts at time 6. seconds
Analysis ends at time 15.3 minutes
305 Measurements analyzed from 3 to 307
3 Points not plotted because head ratio <= 0.0
These points are not included in the analysis
a
I
10 13
Adjusted Time (minutes)
He is 2981 feet at 6. seconds

PARADIGM ANALYTICAL LABORATORIES, INC.
•
Mr. Gary Babb
Babb & Associate
P.O. Box 37697
Raleigh NC 27627
ReportNumber: G121-328
Client Project: Almont Shipping
Dear Mr. Babb:
Enclosed are the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call Paradigm at [phone]. We will be happy to answer any questions or
concerns which you may have.
Thank you for using Paradigm Analytical Labs for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely,
Paradigm Analytical Laboratories, Inc.
dl
a oratoryf-5—i7rL=4-- Iatee
J. Patrick Weaver
N.C. CERTIFICATION #481
1 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260.5035
Olient Sample ID: MW-1 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-10-200513:00
Lab Sample ID G121-328-1A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 91.3
Report Name
Result
Quantitation
Dilution
Date
Compound
UG1KG
Limit UG/KG
Factor
Analyzed
Acetone
52.4
49.3
1
5/17105
Benzene
BQL
4.93
1
5/17/05
Bromobenzene
BQL
4.93
1
5/17/05
Bromochioromethane
BQL
4.93
1
5/17/05
Bromodichloromethane
BQL
4.93
1
5/17/05
Bromoform
BQL
4.93
1
5/17/05
Bromomethane
BQL
4.93
1
5/17/05
2-Butanone
BQL
24.6
1
5/17/05
n-Butyibenzene
BQL
4.93
1
5/17/05
sec-Butylbenzene
BQL
4.93
1
5/17/05
tert-Butylbenzene
BQL
4.93
1
5/17/05
Carbon disulfide
BQL
4.93
1
5/17105
Carbon tetrachloride
BQL
4.93
1
5/17/05
Chiorobenzene
BQL
4.93
1
5/17/05
Chloroethane
BQL
4.93
1
5/17/05
Chloroform
BQL
4.93
1
5/17/05
Chloromethane
BQL
4.93
1
5/17/05
2-Chlorotoluene
BQL
4.93
1
5/17/05
4-Chlorotoluene
BQL
4.93
1
5/17/05
Dibromochioromethane
BQL
4.93
1
5/17/05
1,2-Dibromo-3-chloropropane
BQL
4.93
1
5/17/05
Dibromomethane
BQL
4.93
1
6/17/05
1,2-Dibromoethane (EDB)
BQL
4.93
1
5/17/05
1,2-Dichlorobenzene
BQL
4.93
1
5/17/05
1,3-Dichlorobenzene
BQL
4.93
1
5/17/05
1,4-Dichlorobenzene
BQL
4.93
1
5/17/05
trans-1,4-Dichloro-2-butene
BQL
4.93
1
5/17/05
1,1-Dichloroethane
BQL
4.93
1
5117/05
1,1-Dichloroethene
BQL
4.93
1
5/17/05
1,2-Dichloroethane
BQL
4.93
1
5/17/05
cis-1,2-Dichloroethene
BQL
4.93
1
5/17/05
trans-1,2-dichloroethene
BQL
4.93
1
5/17/05
1,2-Dichloropropane
BQL
4.93
1
5/17/05
1,3-Dichloropropane
BQL
4.93
1
5/17/05
2,2-Dichloropropane
BQL
4.93
1
5/17/05
1,1-Dichloropropene
BQL
4.93
1
5/17/05
cis-1,3-Dichloropropene
BQL
4.93
1
5/17105
trans-1,3-Dichloropropene
BQL
4.93
1
5/17/05
Dichlorodifluoromethane
BQL
4.93
1
5/17/05
Diisopropyl ether (DIPE)
BQL
4.93
1
5/17/05
. Ethylbenzene
BQL
4.93
1
5/17/05
Hexachiorobutadiene
BQL
4.93
1
5/17/05
Pa e 1 of 2 GCMS UMS S0L0 V1 3 )s2 of 43
N.C. CERTIFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260.5035
*Client Sample ID: MW-1 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-10-200513:00
Lab Sample ID G121-328-1A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 91.3
Report Name
Result
Quantitation
Dilution
Date
Compound
UGIKG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
4.93
1
5/17/05
lodomethane
BQL
4.93
1
5/17105
isopropyibenzene
BQL
4.93
1
5/17/05
4-isopropyitoluene
59.6
4.93
1
5/17/05
Methylene chloride
BQL
19.7
1
5/17/05
4-Methyl-2-pentanone
BQL
4.93
1
5/17/05
Methyl-tert-butyl ether (MTBE)
BQL
4.93
1
5/17/05
Naphthalene
BQL
4.93
1
5/17/05
n-Propyl benzene
BQL
4.93
1
5/17/05
Styrene
BQL
4.93
1
5/17/05
1,1,1,2-Tetrachloroethane
BQL
4.93
1
5/17/05
1,1,2,2-Tetrachloroethane
BQL
4.93
1
5/17/05
Tetrachloroethene
BQL
4.93
1
5/17/05
Toluene
BQL
4.93
1
5/17/05
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
BQL
BQL
4.93
4.93
1
1
5/17105
5/17/05
Trichloroethene
BQL
4.93
1
5/17/05
1,1,1-Trichloroethane
BQL
4.93
1
5/17/05
1,1,2-Trichloroethane
BQL
4.93
1
5/17105
Trichlorofluoromethane
BQL
4.93
1
5/17/05
1,2,3-Trichloropropane
BQL
4.93
1
5/17/05
1,2,4-Trimethylbenzene
BQL
4.93
1
5/17/05
1,3,5-Trimethylbenzene
BQL
4.93
1
5/17/05
Vinyl chloride
BQL
4.93
1
5/17/05
m-,p-Xylene
BQL
9.86
1
5/17/05
o-Xylene
BQL
4.93
1
5/17/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
50
60.9
122
1,2-Dichloroethane-d4
50
62.4
125
Toluene-d8
50
54.8
110
Comments:
Flags:
BQL = Below Quantitation Limits.
r�
Reviewed By: V-�-+P
Page 2 of 2 ccMs_uMs solo v, 3.x'3 of 43
N.C. CERTIFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
SClient
by GCMS 8260-5035
Sample ID: MW-2
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 05-10-2005
14:10
Lab Sample ID G121-328-2A
Date Received: 5/12/05
Lab Project ID: G121-328
Matrix: Soil
Report Basis: Dry Weight
%Solids: 83.2
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
47.0
1
5/17/05
Benzene
BQL
4.70
1
5/17105
Bromobenzene
BQL
4.70
1
5/17/05
Bromochloromethane
BQL
4.70
1
5/17/05
Bromodichloromethane
BQL
4.70
1
5/17/05
Bromoform
BQL
4.70
1
5/17/05
Bromomethane
BQL
4.70
1
5/17/05
2-Butanone
BQL
23.5
1
5/17/05
n-Butylbenzene
BQL
4.70
1
5/17/06
sec-Butylbenzene
BQL
4.70
1
5/17/05
tert-Butylbenzene
BQL
4.70
1
5/17/05
Carbon disulfide
BQL
4.70
1
5/17/05
Carbon tetrachloride
BQL
4.70
1
5/17/05
Chlorobenzene
BQL
4.70
1
5/17/05
Chloroethane
BQL
4.70
1
5/17/05
Chloroform
BQL
4.70
1
5/17/05
Chloromethane
BQL
4.70
1
5/17/05
2-Chlorotoluene
BQL
4.70
1
5/17/05
4-Chlorotoluene
BQL
4.70
1
5117/05
Dibromochloromethane
BQL
4.70
1
5/17/05
1,2-Dibromo-3-chloropropane
BQL
4.70
1
5/17/05
Dibromomethane
BQL
4.70
1
5/17/05
1,2-Dibromoethane (EDB)
BQL
4.70
1
5/17/05
1,2-Dichlorobenzene
BQL
4.70
1
5/17/05
1,3-Dichlorobenzene
BQL
4.70
1
5/17105
1,4-Dichlorobenzene
BQL
4.70
1
5/17/05
trans-1,4-Dichloro-2-butene
BQL
4.70
1
5/17/05
1,1-Dichloroethane
BQL
4.70
1
5/17/05
1,1-Dichloroethene
BQL
4.70
1
5/17105
1,2-Dichloroethane
BQL
4.70
1
5/17/05
cis-1,2-Dichloroethene
BQL
4.70
1
5/17/05
trans-1,2-dichloroethene
BQL
4.70
1
5/17/05
1,2-Dichloropropane
BQL
4.70
1
5/17/05
1,3-Dichloropropane
BQL
4.70
1
5/17105
2,2-Dichloropropane
BQL
4.70
1
5/17/05
1,1-Dichloropropene
BQL
4.70
1
5/17/05
cis-1,3-Dichloropropene
BQL
4.70
1
5/17/05
trans-1,3-Dichloropropene
BQL
4.70
1
5/17/05
Dichlorodifluoromethane
BQL
4.70
1
5/17/05
Diisopropyl ether (DIPE)
BQL
4.70
1
5/17/05
Ethylbenzene
BQL
4.70
1
5/17/05
Hexachlorobutadiene
BQL
4.70
1
5/17/05
Page 1 of 2 GCMS LIMS_S0L0 V1.3A4' of 43
N.C. CERTIFICATION W1

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260-5035
eclient Sample ID: MW-2
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 05-10-2005 14: 10
Lab Sample ID G121-328-2A
Date Received:, 5/12/05
Lab Project ID: G121-328
Matrix: Soil
Report Basis: Dry Weight
%Solids: 83.2
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
4.70
1
5/17/05
lodomethane
BQL
4.70
1
5/17/05
Isopropyibenzene
BQL
4.70
1
5/17/05
4-Isopropyltoluene
BQL
4.70
1
5/17/05
Methylene chloride
BQL
18.8
1
5/17/05
4-Methyl-2-pentanone
BQL
4.70
1
5/17105
Methyl-tert-butyl ether (MTBE)
BQL
4.70
1
5/17/05
Naphthalene
BQL
4.70
1
5/17/05
n-Propyl benzene
BQL
4.70
1
5/17/05
Styrene
BQL
4.70
1
5/17/05
1,1,1,2-Tetrachloroethane
BQL
4.70
1
5/17/05
1,1,2,2-Tetrachloroethane
BQL
4.70
1
5/17/05
Tetrachloroethene
BQL
4.70
1
5/17105
Toluene
BQL
4.70
1
5/17/05
1,2,3-Trichlorobenzene
BQL
4.70
1
5117/05
• 1,2,4-Trichlorobenzene
BQL
4.70
1
5/17/05
Trichloroethene
BQL
4.70
1
5/17/05
1,1,1-Trichloroethane
BQL
4.70
1
5/17/05
1,1,2-Trichloroethane
BQL
4.70
1
5/17/05
Trichlorofluoromethane
BQL
4.70
1
5/17/05
1,2,3-Trichloropropane
BQL
4.70
1
5/17/05
1,2,4-Trimethylbenzene
BQL
4.70
1
5/17105
1,3,5-Trimethylbenzene
BQL
4.70
1
5/17/05
Vinyl chloride
BQL
4.70
1
5/17/05
m-,p-Xylene
BQL
9.40
1
5/17/05
o-Xylene
BQL
4.70
1
5/17/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
50
58.6
117
1,2-Dichloroethane-d4
50
62.7
125
Toluene-d8
50
54.4
109
Comments:
Flags:
BQL = Below Quantitation Limits.
E
Reviewed By: f-,AP
Page 2 of 2 GCMS_LIMS_SOLO V1.3 A of 43
N.C. CERTIFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260-5035
ID: MW-3
Analyzed By: JTF
Client Sample
Date Collected: 05-10-200515:00
Client Project ID: Almont Shipping
Date Received:
5
Lab Sample ID G121-328-3A
oil S
Matrix: Soil
Lab Project ID: G121-328
Report Basis: Dry Weight
%Solids: 82.6
Report Name
Result
Quantitation
Dilution
Factor
Date
Analyzed
Compound
UG/KG
Limit UGIKG
5/17105
Acetone
BQL
50.7
1
1
5/17/05
Benzene
BQL
5.07
1
5/17/05
Bromobenzene
BQL
5.07
1
5/17/05
Bromochloromethane
BQL
5.07
1
5/17/05
Bromodichloromethane
BQL
5.07
1
5/17/05
Bromoform
BQL
5.07
1
5/17/05
Bromomethane
BQL
5.07
1
5/17/05
2-Butanone
BQL
25.4
1
5/17/05
n-Butylbenzene
BQL
5.07
1
5/17/05
sec-Butylbenzene
BQL
5.07
1
5/17/05
tert-Butylbenzene
BQL
5.07
1
5/17/05
Carbon disulfide
BQL
5.07
1
5/17/05
Carbon tetrachloride
BQL
5.07
1
5/17/05
Chlorobenzene
BQL
5.07
1
5/17/05
Chloroethane
BQL
5.07
1
5/17/05
Chloroform
BQL
5.07
1
5/17/05
Chloromethane
BQL
5.07
1
5/17/05
2-Chlorotoluene
BQL
5.07
1
5/17/05
4-Chlorotoluene
BQL
5.07
1
5117/05
Dibromochloromethane
BQL
5.07
1
5/17/05
1,2-Dibromo-3-chloropropane
BQL
5.07
1
5/17/05
Dibromomethane
BQL
5.07
1
5/17/05
1,2-Dibromoethane (EDB)
BQL
5.07
1
5/17/05
1,2-Dichlorobenzene
BQL
5.07
1
5/17/05
1,3-Dichlorobenzene
BQL
5.07
1
5/17/05
1,4-Dichlorobenzene
BQL
5.07
1
5/17/05
trans-1,4-Dichloro-2-butene
BQL
5.07
1
5/17/05
1,1-Dichloroethane
BQL
5.07
1
5/17/05
1,1-Dichloroethene
BQL
5.07
1
5/17/05
1,2-Dichloroethane
BQL
5.07
1
5/17/05
cis-1,2-Dichloroethene
BQL
5.07
1
5/17/05
trans-1,2-dichloroethene
BQL
5.07
1
5/17/05
1,2-Dichloropropane
BQL
5.07
1
5/17/05
1,3-Dichloropropane
BQL
5.07
1
5/17/05
2,2-Dichloropropane
BQL
5.07
1
5/17/05
1,1-Dichloropropene
BQL
5.07
1
5/17/05
cis-1,3-Dichloropropene
BQL
5.07
1
5/17/05
trans-1,3-Dichloropropene
BQL
5.07
1
5/17105
Dichlorodifluoromethane
BQL
5.07
1
5/17/05
IsDiisopropyi ether (DIPE)
BQL
5.07
1
5/17/05
Ethylbenzene
BQL
5.07
1
5/17/05
Hexachlorobutadiene
BQL
5.07
Pa e 1 of 2 GCMS LIMS_SOLO V1.31 of 43
N.C. CER�FICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260-5035
Wient ID: MW-3
Analyzed By: JTF
Sample
Client Project ID: Almont Shipping
Date Collected: 05-10-2005
15:00
Lab Sample ID G121-328-3A
Date Received: 5/12/05
Lab Project ID: G121-328
Matrix: Soil
Report Basis: Dry Weight
%Solids: 82.6
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
5.07
1
5/17/05
lodomethane
BQL
5.07
1
5/17/05
Isopropylbenzene
BQL
5.07
1
5/17/05
4-Isopropyitoluene
BQL
5.07
1
5/17105
Methylene chloride
BQL
20.3
1
5/17105
4-Methyl-2-pentanone
BQL
5.07
1
5/17/05
Methyl-tert-butyl ether (MTBE)
BQL
5.07
1
5117/05
Naphthalene
BQL
5.07
1
5/17/05
n-Propyi benzene
BQL
5.07
1
5/17/05
Styrene
BQL
5.07
1
5/17/05
1,1,1,2-Tetrachloroethane
BQL
5.07
1
5/17/05
1,1,2,2-Tetrachloroethane
BQL
5.07
1
5/17/05
Tetrachloroethene
BQL
5.07
1
5/17/05
Toluene
BQL
5.07
1
5/17/06
BQL
5.07
1
1
5/17105
5/17/05
.1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
BQL
5.07
1
5/17/05
Trichloroethene
BQL
5.07
1
5/17/05
1,1,1-Trichloroethane
BQL
5.07
1
5/17/05
1,1,2-Trichloroethane
BQL
5.07
Trichlorofluoromethane
BQL
5.07
1
5/17/05
1,2,3-Trichloropropane
BQL
5.07
1
1
5/17/05
5/17/05
1,2,4-Trimethylbenzene
BQL
5.07
1
5/17/05
1,3,5-Trimethylbenzene
BQL
5.07
1
5/17/06
Vinyl chloride
BQL
5.07
1
5/17/05
m-,p-Xylene
BQL
10.1
1
5/17/05
o-Xylene
BQL
5.07
Spike Spike
Percent
Added Result Recovered
4-Bromofluorobenzene
50 56.5
113
1,2-Dichloroethane-d4
50 62.3
125
Toluene-d8
50 53
106
Comments:
Flags:
BQL = Below Quantitation Limits.
•
Reviewed By: _1z�_
Fa 8 2 Of 2 GCMS uMS S0L0 V1.3."L of 43
N.C. CER I IFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260-5035
Wient Sample ID: MW-4 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-10-2005 15:50
Lab Sample ID G121-328-4A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 89.2
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
50.0
1
5/17/05
Benzene
BQL
5.00
1
5/17/05
Bromobenzene
BQL
5.00
1
5/17/05
Bromochloromethane
BQL
5.00
1
5/17/05
Bromodichloromethane
BQL
5.00
1
5117/05
Bromoform
BQL
5.00
1
5/17/05
Bromomethane
BQL
5.00
1
5/17/05
2-Butanone
BQL
25.0
1
5/17/05
n-Butylbenzene
BQL
5.00
1
5/17/05
sec-Butylbenzene
BQL
5.00
1
5117/05
tert-Butylbenzene
BQL
5.00
1
5117/05
Carbon disulfide
BQL
5.00
1
5/17/05
Carbon tetrachloride
BQL
5.00
1
5/17/05
Chlorobenzene
BQL
5.00
1
5117/05
Chioroethane
BQL
5.00
1
5/17/05
Chloroform
BQL
5.00
1
5/17/05
Chloromethane
BQL
5.00
1
5/17/05
2-Chlorotoluene
BQL
5.00
1
5/17/05
4-Chlorotoluene
BQL
5.00
1
5/17/05
Dibromochloromethane
BQL
5.00
1
5117/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/17/05
Dibromomethane
BQL
5.00
1
5/17/05
1,2-Dibromoethane (EDB)
BQL
5.00
1
5/17/05
1,2-Dichlorobenzene
BQL
5.00
1
5/17/05
1,3-Dichlorobenzene
BQL
5.00
1
5/17/05
1,4-Dichlorobenzene
BQL
5.00
1
5/17/05
trans-1,4-Dichioro-2-butene
BQL
5.00
1
5/17/05
1,1-Dichloroethane
BQL
5.00
1
5117/05
1,1-Dichloroethene
BQL
5.00
1
5/17/05
1,2-Dichloroethane
BQL
5.00
1
5/17/05
cis-1,2-Dichloroethene
BQL
5.00
1
5/17/05
trans-1,2-dichloroethene
BQL
5.00
1
5/17/05
1,2-Dichloropropane
BQL
5.00
1
5/17/05
1,3-Dichloropropane
BQL
5.00
1
5/17/05
2,2-Dichloropropane
BQL
5.00
1
5/17/05
1,1-Dichloropropene
BQL
5.00
1
5/17/05
cis-1,3-Dichloropropene
BQL
5.00
1
5/17/05
trans-1,3-Dichloropropene
BQL
5.00
1
5/17/05
Dichlorodifluoromethane
BQL
5.00
1
5/17/05
Diisopropyl ether (DIPS)
BQL
5.00
1
5/17/05
Ethylbenzene
BQL
5.00
1
5/17/05
Hexachlorobutadiene
BQL
5.00
1
5/17/06
Page 1 of 2 OCMS_LIMS SOLO V1.3 A of 43
N.C. CERTIFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260-5035
.Client Sample ID: MW-4 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-10-200515:50
Lab Sample ID G121-328-4A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 89.2
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/17/05
lodomethane
BQL
5.00
1
5/17/05
Isopropylbenzene
BQL
5.00
1
5/17/05
4-Isopropyltoluene
BQL
5.00
1
5/17105
Methylene chloride
BQL
20.0
1
5/17/05
4-Methyl-2-pentanone
BQL
5.00
1
5/17/05
Methyl-tert-butyl ether (MTBE)
BQL
5.00
1
5/17/05
Naphthalene
BQL
5.00
1
5/17/05
n-Propyl benzene
BQL
5.00
1
5/17/05
Styrene
BQL
5.00
1
5/17/05
1,1,1,2-Tetrachloroethane
BQL
5.00
1
5/17/05
1,1,2,2-Tetrachloroethane
BQL
5.00
1
5/17/05
Tetrachloroethene
BQL
5.00
1
5/17/05
Toluene
BQL
5.00
1
5/17/05
1,2,3-Trichlorobenzene
BQL
5.00
1
5/17/05
•1,2,4-Trichlorobenzene
BQL
5.00
1
5/17/05
Trichloroethene
BQL
5.00
1
5/17/05
1, 1, 1 -Trichloroethane
BQL
5.00
1
5/17/05
1,1,2-Trichloroethane
BQL
5.00
1
5/17/05
Trichlorofluoromethene
BQL
5.00
1
5/17/05
1,2,3-Trichloropropane
BQL
5.00
1
5/17/05
1,2,4-Trimethylbenzene
BQL
5.00
1
5/17/05
1,3,5-Trimethylbenzene
BQL
5.00
1
5/17/05
Vinyl chloride
BQL
5.00
1
5/17/05
m-,p-Xylene
BQL
10.0
1
5/17/05
o-Xylene
BQL
5.00
1
5/17/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
50
59.1
118
1,2-Dichloroethane-d4
50
63.2
126
Toluene-d8
50
55.9
112
Comments:
Flags:
BQL = Below Quantitation Limits.
•
Reviewed By: _9+s?
Page 2 Of 2 GCMS_LIMS_S0L0_ i.3.x1}, of 43
N.C. CERTIFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260-5035
Went Sample ID: MW-5 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-10-200517:30
Lab Sample ID G121-328-5A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 87.8
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
47.4
1
5/17/05
Benzene
BQL
4.74
1
5/17/05
Bromobenzene
BQL
4.74
1
5/17/05
Bromochioromethane
BQL
4.74
1
5/17/05
Bromodichloromethane
BQL
4.74
1
5/17/05
Bromoform
BQL
4.74
1
5/17/05
Bromomethane
BQL
4.74
1
5/17/05
2-Butanone
BQL
23.7
1
5/17/05
n-Butylbenzene
BQL
4.74
1
5/17/05
sec-Butylbenzene
BQL
4.74
1
5/17/05
tert-Butylbenzene
BQL
4.74
1
5/17105
Carbon disulfide
BQL
'4.74
1
5/17/05
Carbon tetrachloride
BQL
4.74
1
5/17/05
Chlorobenzene
BQL
4.74
1
5/17/05
Chloroethane
BQL
4.74
1
1
5117/05
5/17/05
• Chloroform
BQL
4.74
1
5117/05
Chioromethane
BQL
4.74
1
5/17/05
2-Chlorotoluene
BQL
4.74
4-Chlorotoluene
BQL
4.74
1
5/17/05
Dibromochloromethane
BQL
4.74
1
5/17/05
1,2-Dibromo-3-chloropropane
BQL
4.74
1
5/17/05
Dibromomethane
BQL
4.74
1
5/17/05
1,2-Dibromoethane (EDB)
BQL
4.74
1
5117/05
1,2-Dichlorobenzene
BQL
4.74
1
5/17/05
1,3-Dichlorobenzene
BQL
4.74
1
5/17/05
1,4-Dichlorobenzene
BQL
4.74
1
5/17/05
trans-1,4-Dichloro-2-butene
BQL
4.74
1
5/17/05
1, 1 -Dichloroethane
BQL
4.74
1
5/17/05
1,1-Dichloroethene
BQL
4.74
1
5/17/05
1,2-Dichloroethane
BQL
4.74
1
5/17/05
cis-1,2-Dichloroethene
BQL
4.74
1
5/17/05
trans-1,2-dichloroethene
BQL
4.74
1
5/17/05
1,2-Dichloropropane
BQL
4.74
1
5/17/05
1,3-Dichloropropane
BQL
4.74
1
5117/05
2,2-Dichloropropane
BQL
4.74
1
5/17/05
1,1-Dichloropropene
BQL
4.74
1
5/17/05
cis-1,3-Dichloropropene
BQL
4.74
1
5/17/05
trans-1,3-Dichloropropene
BQL
4.74
1
6/17105
Dichlorodifluoromethane
BQL
4.74
1
5/17105
ether (DIPE)
BQL
4.74
1
5/17/05
•Diisopropyl
Ethylbenzene
BQL
4.74
1
5/17/05
Hexachlorobutadiene
BQL
4.74
1
5/17/05
Pag e 1 of 2 ocM$_uMs_soLo VU.X'10 of 43
N.C. CER I IFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260-5035
*Client Sample ID: MW-5
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 05-10-200517:30
Lab Sample ID G121-328-5A
Date Received: 5/12/05
Lab Project ID: G121-328
Matrix: Soil
Report Basis: Dry Weight
%Solids: 87.8
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
4.74
1
5/17/05
lodomethane
BQL
4.74
1
5/17/05
Isopropylbenzene
BQL
4.74
1
5/17/05
4-Isopropyltoluene
BQL
4.74
1
5/17/05
Methylene chloride
BQL
19.0
1
5/17/05
4-Methyl-2-pentanone
BQL
4.74
1
5/17/05
Methyl-tert-butyl ether (MTBE)
BQL
4.74
1
5/17/05
Naphthalene
BQL
4.74
1
5/17/05
n-Propyl benzene
BQL
4.74
1
5/17/06
Styrene
BQL
4.74
1
5/17/05
1,1,1,2-Tetrachloroethane
BQL
4.74
1
5/17/05
1,1,2,2-Tetrachloroethane
BQL
4.74
1
5/17/05
Tetrachloroethene
BQL
4.74
1
5/17/05
Toluene
BQL
4.74
1
5/17/05
1,2,3-Trichlorobenzene
BQL
4.74
1
5/17/05
1,2,4-Trichlorobenzene
BQL
4.74
1
5/17/05
Trichloroethane
BQL
4.74
1
5/17/05
1,1,1-Trichloroethane
BQL
4.74
1
5/17/05
1,1,2-Trichloroethane
BQL
4.74
1
5/17/05
Trichlorofluoromethane
BQL
4.74
1
5/17/05
1,2,3-Trichloropropane
BQL
4.74
1
5/17/05
1,2,4-Trimethylbenzene
BQL
4.74
1
5/17/05
1,3,5-Trimethylbenzene
BQL
4.74
1
5/17/06
Vinyl chloride
BQL
4.74
1
5/17/05
m-,p-Xylene
BQL
9.48
1
5/17/05
o-Xylene
BQL
4.74
1
5/17/05
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
Comments:
Flags:
BQL = Below Quantitation Limits.
•
Spike
Spike
Percent
Added
Result
Recovered
50
60.4
121
50
65.3
131
50
55.3
111
Pa e2 f2
N.C. CER�IFOATION #481
Reviewed By:
GCMS UMS_SOLO V1.3A1 1 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260.5035
0Client Sample ID: MW-6
Analyzed By: JTF
Client Project ID: Himont Shipping
Date Collected: 05-11-2005
09:30
Lab Sample ID G121-328-6A
Date Received: 5/12/05
Lab Project ID: G121-328
Matrix: Soil
Report Basis: Dry Weight
%Solids: 96.4
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
47.7
1
5/17/05
Benzene
BQL
4.77
1
5/17/05
Bromobenzene
BQL
4.77
1
5/17/05
Bromochloromethane
BQL
4.77
1
5/17/05
Bromodichloromethane
BQL
4.77
1
5/17/05
Bromoform
BQL
4.77
1
5/17/05
Bromomethane
BQL
4.77
1
5/17105
2-Butanone
BQL
23.8
1
5/17/05
n-Butylbenzene
BQL
4.77
1
5/17/05
sac-Butylbenzene
BQL
4.77
1
5/17/05
tert-Butylbenzene
BQL
4.77
1
5/17/05
Carbon disulfide
BQL
4.77
1
5117/05
Carbon tetrachloride
BQL
4.77
1
5/17/05
Chlorobenzene
BQL
4.77
1
5/17/05
Chloroethane
BQL
4.77
1
5/17/05
Chloroform
BQL
4.77
1
5117/05
Chioromethane
BQL
4.77
1
5117/05
2-Chlorotoluene
BQL
4.77
1
5/17/05
4-Chlorotoluene
BQL
4.77
1
5/17/05
Dibromochloromethane
BQL
4.77
1
5/17/05
1,2-Dibromo-3-chloropropane
BQL
4.77
1
5/17/05
Dibromomethane
BQL
4.77
1
5117105
1,2-Dibromoethane (EDB)
BQL
4.77
1
5117/05
1,2-Dichlorobenzene
BQL
4.77
1
5/17/05
1,3-Dichlorobenzene
BQL
4.77
1
5/17/05
1,4-Dichlorobenzene
BQL
4.77
1
5/17105
trans-1,4-Dichloro-2-butene
BQL
4.77
1
5/17/05
1,1-Dichloroethane
BQL
4.77
1
5/17105
1,1-Dichloroethene
BQL
4.77
1
5117/05
1,2-Dichloroethane
BQL
4.77
1
5/17/05
cis-1,2-Dichloroethene
BQL
4.77
1
5/17/05
trans-1,2-dichloroethene
BQL
4.77
1
5/17/05
1,2-Dichloropropane
BQL
4.77
1
5/17/05
1,3-Dichloropropane
BQL
4.77
1
5/17/05
2,2-Dichloropropane
SQL
4.77
1
5/17/05
1,1-Dichloropropene
BQL
4.77
1
5/17/05
cis-1,3-Dichloropropene
BQL
4.77
1
5/17/05
trans-1,3-Dichloropropene
BQL
4.77
1
5/17/05
Dichlorodifluoromethane
BQL
4.77
1
5/17/05
Diisopropyl ether (DIPE)
BQL
4.77
1
5/17/05
Ethyibenzene
BQL
4.77
1
5/17/05
Hexachlorobutadiene
BQL
4.77
1
5/17105
Pa e 1 f 2 GGMS LIMS_S0L0 V1.3.x) 2 of 43
N.C. CER-FIF118ATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260-5035
client Sample ID: MW-6
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 05-11-2005
09:30
Lab Sample ID G121-328-6A
Date Received: 5112/05
Lab Project ID: G121-328
Matrix: Soil
Report Basis: Dry Weight
%Solids: 96.4
Report Name
Result
Quantitation
Dilution
Date
Compound
UGJKG
Limit UG1KG
Factor
Analyzed
2-Hexanone
BQL
4.77
1
5/17/05
lodomethane
BQL
4.77
1
5/17105
Isopropylbenzene
BQL
4.77
1
5/17105
4-Isopropyltoluene
BQL
4.77
1
5117105
Methylene chloride
BQL
19.1
1
5/17/05
4-Methyl-2-pentanone
BQL
4.77
1
5/17/05
Methyl -tent -butyl ether (MTBE)
BQL
4.77
1
5/17/05
Naphthalene
BQL
4.77
1
5/17/05
n-Propyl benzene
BQL
4.77
1
5/17/05
Styrene
BQL
4.77
1
5/17/05
1,1,1,2-Tetrachloroethane
BQL
4.77
1
5/17/05
1,1,2,2-Tetrachloroethane
BQL
4.77
1
5/17/05
Tetrachloroethene
BQL
4.77
1
5/17/05
Toluene
BQL
4.77
1
6/17/05
1,2,3-Trichlorobenzene
BQL
4.77
1
5/17105
1,2,4-Trichlorobenzene
BQL
4.77
1
5/17105
Trichloroethene
BQL
4.77
1
5/17/05
1,1,1-Trichloroethane
BQL
4.77
1
5/17/05
1,1,2-Trichloroethane
BQL
4.77
1
5/17/05
Trichlorofluoromethane
BQL
4.77
1
5117/05
1,2,3-Trichloropropane
BQL
4.77
1
5/17/05
1,2,4-Trimethylbenzene
BQL
4.77
1
5/17/05
1,3,5-Trimethylbenzene
BQL
4.77
1
5/17/05
Vinyl chloride
BQL
4.77
1
5/17/05
m-,p-Xylene
BQL
9.53
1
5/17/05
o-Xylene
BQL
4.77
1
5/17/05
Spike Spike
Percent
Added Result
Recovered
4-Bromofluorobenzene
50 61.4
123
1,2-Dichioroethane-d4
50 65.9
132
Toluene-d8
50 54.4
109
Comments:
Flags:
BQL = Below Quantitation Limits.
Reviewed By: 'l-W
Page 2 of 2 GCM4_UMS_S0L0 V1 3.X) 3 of 43
N.C. CERTIFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS $260-5035
Client Sample ID: MW-7 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-11-200510:30
Lab Sample ID G121-328-7A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 85.7
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
47.6
1
5/17/05
Benzene
BQL
4.76
1
5/17/05
Bromobenzene
BQL
4.76
1
5/17/05
Bromochloromethane
BQL
4.76
1
5/17/05
Bromodichloromethane
BQL
4.76
1
5/17/05
Bromoform
BQL
4.76
1
5/17/05
Bromomethane
BQL
4.76
1
5/17/05
2-Butanone
BQL
23.8
1
5/17/05
n-Butylbenzene
BQL
4.76
1
5/17/05
sec-Butylbenzene
BQL
4.76
1
5/17/05
tert-Butylbenzene
BQL
4.76
1
5/17/05
Carbon disulfide
BQL
4.76
1
5/17/05
Carbon tetrachloride
BQL
4.76
1
5/17/05
Chlorobenzene
BQL
4.76
1
5/17/05
Chioroethane
BQL
4.76
1
5/17/05
�• Chloroform
BQL
4.76
1
5/17/05
Chioromethane
BQL
4.76
1
5/17/05
2-Chiorotoluene
BQL
4.76
1
5/17/05
4-Chlorotoluene
BQL
4.76
1
5/17/05
Dibromochloromethane
BQL
4.76
1
5/17/05
1,2-Dibromo-3-chloropropane
BQL
4.76
1
5/17/05
Dibromomethane
BQL
4.76
1
5/17/05
1,2-Dibromoethane (EDB)
BQL
4.76
1
5/17/05
1,2-Dichlorobenzene
BQL
4.76
1
5/17/05
1,3-Dichlorobenzene
BQL
4.76
1
5/17/05
1,4-Dichlorobenzene
BQL
4.76
1
5/17/05
trans-1,4-Dichloro-2-butene
BQL
4.76
1
5/17/05
1,1-Dichloroethane
BQL
4.76
1
5/17/05
1,1-Dichloroethene
BQL
4.76
1
5/17/05
1,2-Dichloroethane
BQL
4.76
1
5/17/05
cis-1,2-Dichloroethene
BQL
4.76
1
5/17/05
trans-1,2-dichioroethene
BQL
4.76
1
5/17105
1,2-Dichloropropane
BQL
4.76
1
5/17/05
1,3-Dichloropropane
BQL
4.76
1
5/17105
2,2-Dichloropropane
BQL
4.76
1
5/17/05
1,1-Dichloropropene
BQL
4.76
1
5/17/05
cis-1,3-Dichloropropene
BQL
4.76
1
5/17/05
trans-1,3-Dichloropropene
BQL
4.76
1
5/17/05
Dichlorodifluoromethane
Ditsopropyl ether (DIPS)
BQL
BQL
4.76
4.76
1
1
5/17/05
5/17/05
Ethylbenzene
BQL
4.76
1
5/17/05
Hexachlorobutadtene
BQL
4.76
1
5/17/05
Page 1 of 2 GCMS LIMS SOLO V1 3 xis
N.C. CERTIFICATION #481 14 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
�• by GCM5 8260.5035
Client Sample ID: MW-7 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-11-200510:30
Lab Sample ID G121-328-7A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 85.7
Report Name
Result
Quantitation
Dilution
Date
Compound
UGlKG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
4.76
1
5/17/05
lodomethane
BQL
4.76
1
5/17/05
Isopropyibenzene
BQL
4.76
1
5/17/05
4-Isopropyltoluene
BQL
4.76
1
5/17/05
Methylene chloride
BQL
19.0
1
5/17/05
4-Methyl-2-pentanone
BQL
4.76
1
5/17/05
Methyl-tert-butyl ether (MTBE)
BQL
4.76
1
5/17/05
Naphthalene
BQL
4.76
1
5/17/05
n-Propyl benzene
BQL
4.76
1
5/17/05
Styrene
BQL
4.76
1
5117/05
1,1,1,2-Tetrachloroethane
BQL
4.76
1
5/17/05
1,1,2,2-Tetrachloroethane
BQL
4.76
1
5/17/05
Tetrachloroethene
BQL
4.76
1
5/17/05
Toluene
BQL
4.76
1
5/17/05
BQL
4.76
1
5117/05
�.1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
BQL
4.76
1
5/17/05
Trichloroethane
8.01
4.76
1
5/17/05
1,1,1-Trichloroethane
BQL
4.76
1
5/17/05
1,1,2-Trichloroethane
BQL
4.76
1
5/17/05
Trichlorofluoromethane
BQL
4.76
1
5/17/05
1,2,3-Trichloropropane
BQL
4.76
1
5/17/05
1,2,4-Trimethyibenzene
BQL
4.76
1
5/17/05
1,3,5-Trimethylbenzene
BQL
4.76
1
5/17/05
Vinyl chloride
BQL
4.76
1
5/17/05
m-,p-Xylene
BQL
9.52
1
5/17/05
o-Xylene
BQL
4.76
1
5/17/05
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
Comments:
Flags:
BQL = Below Quantitation Limits.
�e
Spike
Spike
Percent
Added
Result
Recovered
50
59.7
119
50
64.2
128
50
54.2
108
N.C. CERPIFI&ION #481
Reviewed By:
GCMS UMS S0L0 V1.3.x15 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8250-5035
�-- Client Sample ID: MW-8 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-11-200511:00
Lab Sample ID G121-328-8A Date Received: 5112/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 85.1
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
44.3
1
5/17/05
Benzene
BQL
4.43
1
5/17/05
Bromobenzene
BQL
4.43
1
5/17/05
Bromochioromethane
BQL
4.43
1
5/17/05
Bromodichloromethane
BQL
4.43
1
5/17/05
Bromoform
BQL
4.43
1
5/17/05
Bromomethane
BQL
4.43
1
5/17105
2-Butanone
BQL
22.1
1
5/17/05
n-Butylbenzene
BQL
4.43
1
5/17/05
sec-Butylbenzene
BQL
4.43
1
5/17/05
tert-Butylbenzene
BQL
4.43
1
5/17/05
Carbon disulfide
BQL
4.43
1
5/17/05
Carbon tetrachloride
BQL
4.43
1
5/17/05
Chlorobenzene
BQL
4.43
1
5/17/05
Chloroethane
BQL
4.43
1
5/17/05
Chloroform
BQL
4.43
1
5/17/05
Chioromethane
BQL
4.43
1
5/17/05
2-Chlorotoluene
BQL
4.43
1
5/17/05
4-Chlorotoluene
BQL
4.43
1
5/17/05
Dibromochloromethane
BQL
4.43
1
5/17/05
1,2-Dibromo-3-chloropropane
BQL
4.43
1
5/17/05
Dibromomethane
BQL
4.43
1
5/17/05
1,2-Dibromoethane (EDB)
BQL
4.43
1
5/17/05
1,2-Dichlorobenzene
BQL
4.43
1
5/17/05
1,3-Dichlorobenzene
BQL
4.43
1
5/17/05
1,4-Dichlorobenzene
BQL
4.43
1
5/17/05
trans-1,4-Dichloro-2-butene
BQL
4.43
1
5/17/05
1,1-Dichloroethane
BQL
4.43
1
5/17/05
1,1-Dichloroethene
BQL
4.43
1
5/17/05
1,2-Dichloroethane
BQL
4.43
1
5/17/05
cis-1,2-Dichioroethene
BQL
4.43
1
5/17/05
trans-1,2-dichloroethene
BQL
4.43
1
5/17/05
1,2-Dichloropropane
BQL
4.43
1
5/17/05
1,3-Dichloropropane
BQL
4.43
1
5/17/05
2,2-Dichloropropane
BQL
4.43
1
5/17/05
1,1-Dichloropropene
BQL
4.43
1
5/17/05
cis-1,3-Dichloropropene
BQL
4.43
1
5/17/05
trans-1,3-Dichloropropene
BQL
4.43
1
5/17/05
Dichiorodittuoromethane
BQL
4.43
1
5/17/05
Diisopropyl ether (DIPE)
BQL
4.43
1
5/17/05
�• Ethylbenzene
BQL
4.43
1
5/17/05
Hexachlorobutadiene
BQL
4.43
1
5/17/05
Pale 1 of 2 GCMS LIMS_SOLO Vt.3A"
N.C. CERTIFICATION #481 16 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiies
• by GCMS 8260-5035
Client Sample ID: MW-8 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-11-200511:00
Lab Sample ID G121-328-8A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 85.1
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UGIKG
Factor
Analyzed
2-Hexanone
BQL
4.43
1
5/17/05
lodomethane
BQL
4.43
1
5/17/05
Isopropylbenzene
BQL
4.43
1
5/17/05
4-Isopropyltoluene
BQL
4.43
1
5/17/05
Methylene chloride
BQL
17.7
1
5/17/05
4-Methyl-2-pentanone
BQL
4.43
1
5/17/05
Methyl-tert-butyl ether (MTBE)
BQL
4.43
1
5/17/05
Naphthalene
BQL
4.43
1
5/17/05
n-Propyi benzene
BQL
4.43
1
5/17/05
Styrene
BQL
4.43
1
5/17/05
1,1,1,2-Tetrachloroethane
BQL
4.43
1
5/17/05
1,1,2,2-Tetrachloroethane
BQL
4.43
1
5/17/05
Tetrachloroethene
BQL
4.43
1
5/17/05
Toluene
BQL
4.43
1
5/17/05
1,2,3-Trichiorobenzene
BQL
4.43
1
5/17/05
1,2,4-Trichlorobenzene
BQL
4.43
1
5/17/05
Trichloroethene
BQL
4.43
1
5/17/05
1, 1, 1 -Trichloroethane
BQL
4.43
1
5/17/05
1,1,2-Trichloroethane
BQL
4.43
1
5/17/05
Trichlorofluoromethene
BQL
4.43
1
5/17/05
1,2,3-Trichloropropane
BQL
4.43
1
5/17/05
1,2,4-Trimethylbenzene
BQL
4.43
1
5/17/05
1,3,5-Trimethylbenzene
BQL
4.43
1
5/17/05
Vinyl chloride
BQL
4.43 .
1
5/17/05
m-,p-Xylene
BQL
8.85
1
5/17/05
o-Xylene
BQL
4.43
1
5/17/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
50
64.4
129
1,2-Dichloroethane-d4
50
64.9
130
Toluene-d8
50
55.6
111
Comments:
Flags:
BQL = Below Quantitation Limits.
I.
Reviewed By: _ice. P
N.C. CERTIFICATION #481 S S GCMS_LIMOLO V1.3.tts17 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
C by GCMS 8260-5035
Client Sample ID: MW-9 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-11-2005 12:30
Lab Sample ID G121-328-9A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 98.1
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
51.6
1
5/17/05
Benzene
BQL
5.16
1
5/17/05
Bromobenzene
BQL
5.16
1
5/17105
Bromochloromethane
BQL
5.16
1
5/17/05
Bromodichloromethane
BQL
5.16
1
5/17/05
Bromoform
BQL
5.16
1
5/17/05
Bromomethane
BQL
5.16
1
5/17/05
2-Butanone
BQL
25.8
1
5/17/05
n-Butylbenzene
BQL
5.16
1
5/17/05
sec-Butylbenzene
BQL
5.16
1
5/17/05
tert-Butylbenzene
BQL
5.16
1
5/17/05
Carbon disulfide
BQL
5.16
1
5/17/05
Carbon tetrachloride
BQL
5.16
1
5/17/05
Chlorobenzene
BQL
5.16
1
5/17/05
�Chloroethane
BQL
5.16
1
5/17/05
-
Chloroform
BQL
5.16
1
5/17/05
Chloromethane
BQL
5.16
1
5/17/05
2-Chiorotoluene
BQL
5.16
1
5/17/05
4-Chiorotoluene
BQL
5.16
1
5/17/05
Dibromochloromethane
BQL
5.16
1
5/17/05
1,2-Dibromo-3-chloropropane
BQL
5.16
1
5/17/05
Dibromomethane
BQL
5.16
1
5/17/05
1,2-Dibromoethane (EDB)
BQL
5.16
1
5/17/05
1,2-Dichlorobenzene
BQL
5.16
1
5/17/05
1,3-Dichlorobenzene
BQL
5.16
1
5/17/05
1,4-Dichlorobenzene
BQL
5.16
1
5/17/05
trans-1,4-Dichloro-2-butene
BQL
5.16
1
5/17/05
1,1-Dichloroethane
BQL
5.16
1
5/17/05
1,1-Dichloroethene
BQL
5.16
1
5/17/05
1,2-Dichloroethane
BQL
5.16
1
5/17/05
cis-1,2-Dichloroethene
BQL
5.16
1
5/17/05
trans-1,2-dichloroethene
BQL
5.16
1
5/17/05
1,2-Dichloropropane
BQL
5.16
1
5/17105
1,3-Dichloropropane
BQL
5.16
1
5/17/05
2,2-Dichloropropane
BQL
5.16
1
5/17/05
1,1-Dichloropropene
BQL
5.16
1
5/17/05
cis-1,3-Dichloropropene
BQL
5.16
1
5/17/05
trans-1,3-Dichloropropene
BQL
5.16
1
5/17/05
Dichlorodifluoromethane
Diisopropyl ether (DIPE)
BQL
BQL
5.16
5.16
1
1
5/17/05
5/17/05
Ethyibenzene
BQL
5.16
1
5/17/05
Hexachlorobutadiene
BQL
5.16
1
5/17/05
Page 1 of 2 GCMS_LIMS_SOLO V1.3.x1s
N.C.CERTIFICATION #481 18 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
!� by GCMS 8260-5035
Client Sample ID: MW-9 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-11-200512:30
Lab Sample ID G121-328-9A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 98.1
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
5.16
1
5/17/05
lodomethane
BQL
5.16
1
5/17/05
Isopropylbenzene
BQL
5.16
1
5/17/05
4-isopropyltoluene
BQL
5.16
1
5/17/05
Methylene chloride
BQL
20.6
1
5/17/05
4-Methyl-2-pentanone
BQL
5.16
1
5/17/05
Methyl-tert-butyl ether (MTBE)
BQL
5.16
1
5/17/05
Naphthalene
BQL
5.16
1
5/17/05
n-Propyl benzene
BQL
5.16
1
5/17/05
Styrene
BQL
5.16
1
5/17/05
1,1,1,2-Tetrachloroethane
BQL
5.16
1
5/17/05
1,1,2,2-Tetrachloroethane
BQL
5.16
1
5/17/05
Tetrachloroethene
BQL
5.16
1
5/17/05
Toluene
BQL
5.16
1
5/17/05
1,2,3-Trichlorobenzene
BQL
5.16
1
5/17/05
1,2,4-Trichlorobenzene
BQL
5.16
1
5/17/05
Trichloroethane
BQL
5.16
1
5/17/05
1,1,1-Trichloroethane
BQL
5.16
1
5/17/05
1,1,2-Trichloroethane
BQL
5.16
1
5/17/05
Trichlorofluoromethane
BQL
5.16
1
5/17/05
1,2,3-Trichloropropane
BQL
5.16
1
5/17/05
1,2,4-Trimethylbenzene
BQL
5.16
1
5/17/05
1,3,5-Trimethylbenzene
BQL
5.16
1
5/17/05
Vinyl chloride
BQL
5.16
1
5/17/05
m-,p-Xylene
BQL
10.3
1
5/17/05
o-Xylene
BQL
5.16
1
5/17/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
50
57.5
115
1,2-Dichloroethane-d4
50
66.2
132
Toluene-d8
50
54.3
109
Comments:
Flags:
BQL = Below Quantitation Limits.
Reviewed By:
N.C. C9V1A6A"TION #481 WMs_uM4_S0LC V1.3.x1319 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
. by GCMS 8260-5035
Client Sample ID: MW-10 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-11-200515:30
Lab Sample ID G121-328-10A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 90.5
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
44.8
1
5/17/05
Benzene
BQL
4.48
1
5/17/05
Bromobenzene
BQL
4.48
1
5/17/05
Bromochloromethane
BQL
4.48
1
5/17/05
Bromodichloromethane
BQL
4.48
1
5/17/05
Bromoform
BQL
4.48
1
5/17/05
Bromomethane
8.04
4.48
1
5/17/05
2-Butanone
BQL
22.4
1
5/17/05
n-Butylbenzene
BQL
4.48
1
5/17105
sec-Butylbenzene
BQL
4.48
1
5/17/05
tert-Butylbenzene
BQL
4.48
1
5117/05
Carbon disulfide
BQL
4.48
1
5/17/05
Carbon tetrachloride
BQL
4.48
1
5/17/05
Chlorobenzene
BQL
4.48
1
5/17/05
�• Chioroethane
BQL
4.48
1
5/17/05
Chloroform
BQL
4.48
1
5/17/05
Chloromethane
BQL
4.48
1
5/17/05
2-Chiorotoluene
BQL
4.48
1
5/17/05
4-Chlorotoluene
BQL
4.48
1
5/17/05
Dibromochioromethane
BQL
4.48
1
5/17/05
1,2-Dibromo-3-chloropropane
BQL
4.48
1
5/17/05
Dibromomethane
BQL
4.48
1
5/17/05
1,2-Dibromoethane (EDB)
BQL
4.48
1
5/17/05
1,2-Dichlorobenzene
BQL
4.48
1
5/17/05
1,3-Dichlorobenzene
BQL
4.48
1
5/17/05
1,4-Dichlorobenzene
BQL
4.48
1
5/17/05
trans-1,4-Dichloro-2-butene
BQL
4.48
1
5/17/05
1,1-Dichloroethane
BQL
4.48
1
5/17/05
1,1-Dichloroethene
BQL
4.48
1
5/17/05
1,2-Dichloroethane
BQL
4.48
1
5117/05
cis-1,2-Dichloroethene
BQL
4.48
1
5/17/05
trans-1,2-dichloroethene
BQL
4.48
1
5117105
1,2-Dichloropropane
BQL
4.48
1
5/17/05
1,3-Dichloropropane
BQL
4.48
1
5/17/05
2,2-Dichloropropane
BQL
4.48
1
5/17/05
1,1-Dichloropropene
BQL
4.48
1
5/17/05
cis-1,3-Dichloropropene
BQL
4.48
1
5/17/05
trans-1,3-Dichloropropene
BQL
4.48
1
5/17/05
Dichlorodifluoromethane
BQL
4.48
1
5117/05
Diisopropyl ether (DIPE)
BQL
4.48
1
5/17/05
Ethylbenzene
BQL
4.48
1
5/17/05
Hexachlorobutadiene
BQL
4.48
1
5/17/05
N.C. CERTIFICATION #481 GMLIMB SOLO V1 3 LO of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
C.- Client Sample ID: MW-10 by GCMS 8260.5035Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-11-200515:30
Lab Sample ID G121-328-10A Date Received: 5/12/05
Lab Project ID: G121-328 Matrix: Soil
Report Basis: Dry Weight %Solids: 90.5
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
4.48
1
5/17/05
lodomethane
BQL
4.48
1
5/17/05
Isopropylbenzene
BQL
4.48
1
5117/05
4-Isopropyltoluene
BQL
4.48
1
5/17/05
Methylene chloride
BQL
17.9
1
5/17/05
4-Methyl-2-pentanone
BQL
4.48
1
5/17/05
Methyl-tert-butyl ether (MTBE)
BQL
4.48
1
5/17/05
Naphthalene
BQL
4.48
1
5/17/05
n-Propyl benzene
BQL
4.48
1
5/17/05
Styrene
BQL
4.48
1
5/17/05
1,1,1,2-Tetrachloroethane
BQL
4.48
1
5/17/05
1,1,2,2-Tetrachloroethane
BQL
4.48
1
5/17/05
Tetrachloroethene
BQL
4.48
1
5/17/05
Toluene
BQL
4.48
1
5/17/05
• 1,2,3-Trichlorobenzene
BQL
4.48
1
5/17/05
1,2,4-Trichlorobenzene
BQL
4.48
1
5/17/05
Trichloroethene
BQL
4.48
1
5/17/05
1,1,1-Trichloroethane
BQL
4.48
1
5/17/05
1,1,2-Trichloroethane
BQL
4.48
1
5/17/05
Trichlorofluoromethane
BQL
4.48
1
5/17/05
1,2,3-Trichloropropane
BQL
4.48
1
5/17/05
1,2,4-Trimethylbenzene
BQL
4.48
1
5/17/05
1,3,5-Trimethylbenzene
BQL
4.48
1
5/17/05
Vinyl chloride
BQL
4.48
1
5/17/05
m-,p-Xylene
BQL
8.97
1
5/17/05
o-Xylene
BQL
4.48
1
5/17/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
50
72.1
144
1,2-Dichloroethane-d4
50
63.4
127
Toluene-d8
50
60.5
121
Comments:
Flags:
BQL = Below Quantitation Limits.
11
Reviewed By: !gam
12 N.C. CA IMATION #481 ccMs uMs soLo v,.s��1 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
(•
Client Sample ID:
MW-1
Analyzed By:
PSW
Client Project ID:
Aimont Shipping
Date Collected:
5/10/200513:00
Lab Sample ID:
G121-328-1
Date Received:
5/12/2005
Lab Project ID:
G121-328
Matrix:
SOIL
Batch ID:
2845 2884
Solids
91.25
Report Basis:
Dry
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
BQL
1.10
1
MG/KG
6010B
5/23/2005
Barium
11.3
11.0
1
MG/KG
6010B
5/23/2005
Cadmium
BQL
1.10
1
MG/KG
6010E
5/23/2005
Chromium
2.69
1.10
1
MG/KG
6010B
5/23/2005
Lead
32.1
1.10
1
MG/KG
6010E
5/23/2005
Mercury
0.0693
0.0196
1
MG/KG
7471
5/25/2005
Selenium
BQL
2.19
1
MG/KG
6010E
5/23/2005
Silver
BQL
1.10
1
MG/KG
6010B
5/23/2005
Comments
BQL = Below Quantitation
Limits
10
DF = Dilution Factor
J = Between MDL
and RL
Reviewed By: V--✓
MEr uMs_s.
N.C. CERTIFICATION #481
2 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
(A
Client Sample ID: MW-2
Analyzed By:
PSW
Client Project ID: Almont Shipping
Date Collected:
5110/200514:10
Lab Sample ID: G121-328-2
Date Received:
5/12/2005
'Lab Project ID: G121-328
Matrix:
SOIL
Batch ID: 2845 2884
Solids
83.21
Report Basis: Dry
Metals Result
RL
DF
Units
Method
Date
Analyzed
Arsenic 11.9
1.02
1
MG/KG
6010E
5/24/2005
Barium 21.7
10.2
1
MG/KG
6010B
5/24/2005
Cadmium BQL
1.02
1
MG/KG
6010B
5/24/2005
Chromium 19.0
1.02
1
MG/KG
6010E
5/24/2005
Lead 166
1.02
1
MG/KG
6010E
5/24/2005
Mercury 0.725
0.0211
1
MG/KG
7471
5/25/2005
Selenium BQL
2.04
1
MG/KG
6010B
6/24/2005
Silver BQL
1.02
1
MG/KG
6010B
5/24/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
Reviewed By: &�g_
MET_LIMS_3.
3 43
N.C. CERTIFICATION #481
of

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
C•
Client Sample ID:
MW-3
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/10/200515:00
Lab Sample ID:
G121-328-3
Date Received:
5/12/2005
Lab Project ID:
G121-328
Matrix:
SOIL
Batch ID:
2845 2884
Solids
82.57
Report Basis:
Dry
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
3.41
1.14
1
MG/KG
6010E
5/24/2005
Barium
18.0
11.4
1
MG/KG
6010B
5/24/2005
Cadmium
BQL
1.14
1
MG/KG
6010B
5/24/2005
Chromium
8.72
1.14
1
MG/KG
6010E
5/24/2005
Lead
25.0
1.14
1
MG/KG
6010B
5/24/2005
Mercury
0.0641
0.0237
1
MG/KG
7471
5/25/2005
Selenium
BQL
2.29
1
MG/KG
6010B
5/24/2005
Silver
BQL
1.14
1
MG/KG
6010E
5/24/2005
Comments
BQL = Below Quantitation
Limits
DF = Dilution Factor
J = Between MDL
and RL
Reviewed By: (z-W_
N.C. CERTIFICATION #481
MET_LIMS-3.
4 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Client Sample ID:
MW-4
Client Project ID:
Almont Shipping
Lab Sample ID:
G121-328-4
Lab Project ID:
G121-328
Batch ID:
2845 2884
Report Basis:
Dry
Metals
Result RL
\•
Results for Metals
Analyzed By:
PSW
Date Collected:
5/10/200515:50
Date Received:
5/12/2005
Matrix:
SOIL
Solids
89.15
DF Units Method
Arsenic
30.2
1.00
1
MG/KG
6010E
Barium
36.2
10.0
1
MG/KG
6010E
Cadmium
BQL
1.00
1
MG/KG
6010E
Chromium
42.6
1.00
1
MG/KG
6010E
Lead
93.4
1.00
1
MG/KG
6010B
Mercury
0.176
0.0204
1
MG/KG
7471
Selenium
BOIL
2.00
1
MG/KG
6010E
Silver
BQL
1.00
1
MG/KG
6010B
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
N.C. CERTIFICATION #481
Date
Analyzed
6/24/2005
5124/2005
5/24/2005
5/24/2005
5/24/2005
5/25/2005
5/24/2005
5/24/2005
Reviewed By: ig-W-
MEr uMs_s.�
25 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
C
Client Sample ID:
MW-5
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/101200517:30
Lab Sample ID:
G121-328-5
Date Received:
5/12/2005
Lab Project ID:
G121-328
Matrix:
SOIL
Batch ID:
2845 2884
Solids
87.79
Report Basis:
Dry
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
7.17
1.10
1
MG/KG
6010E
5/24/2005
Barium
43.2
11.0
1
MG/KG
6010B
5/24/2005
Cadmium
BQL
1.10
1
MG/KG
6010E
5/24/2005
Chromium
15.6
1.10
1
MG/KG
6010B
5/24/2006
Lead
76.3
1.10
1
MG/KG
6010B
5/24/2005
Mercury
0.142
0.0228
1
MG/KG
7471
5/25/2005
Selenium
BQL
2.19
1
MG/KG
6010B
5/24/2005
Silver
BQL
1.10
1
MG/KG
6010B
5/24/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL
and RL
Reviewed By:
Mer uMs P.� 6 43
N.C. CERTIFICATION
MI
of

(4
PARADIGM ANALYTICAL LABORATORIES, INC.
Client Sample ID:
MW-6
Client Project ID:
Almont Shipping
Lab Sample ID:
G121-328-6
Lab Project ID:
G121-328
Batch ID:
2845 2884
Report Basis:
Dry
Metals
Result
RL
Arsenic
BQL
0.879
Barium
BQL
8.79
Cadmium
BQL
0.879
Chromium
6.07
0.879
Lead
1.49
0.879
Mercury
BQL
0.0185
Selenium
BQL
1.76
Silver
BQL
0.879
Comments
C
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
(is
Results for Metals
Analyzed By:
PSW
Date Collected:
5/11/2005 09:30
Date Received:
5/12/2005
Matrix:
SOIL
Solids
96.42
DF Units Method
1 MG/KG
6010E
1 MG/KG
6010E
1 MG/KG
6010B
1 MG/KG
6010B
1 MG/KG
6010B
1 MG/KG
7471
1 MG/KG
6010B
1 MG/KG
6010B
N.C. CERTIFICATION #481
Date
Analyzed
5/24/2005
5/24/2005
5/24/2005
5/24/2005
5/24/2005
5/25/2005
5/24/2005
5/24/2005
Reviewed By: 94--V
MET-"MS-117 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
•
Client Sample ID:
MW-7
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
6/11/200510:30
Lab Sample ID:
G121-328-7
Date Received:
5/12/2005
Lab Project ID:
G121-328
Matrix:
SOIL
Batch ID:
2845 2884
Solids
85.68
Report Basis:
Dry
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
BQL
1.08
1
MG/KG
6010B
5/24/2005
Barium
BQL
10.8
1
MG/KG
6010B
5/24/2005
Cadmium
BQL
1.08
1
MG/KG
6010B
5/24/2005
Chromium
2.14
1.08
1
MG/KG
601013
5/24/2005
Lead
3.79
1.08
1
MG/KG
6010E
5/24/2005
Mercury
BQL
0.0208
1
MG/KG
7471
5/25/2005
Selenium
BQL
2.16
1
MG/KG
6010B
5/24/2005
Silver
BQL
1.08
1
MG/KG
6010B
5/24/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL
and RL
Reviewed By: _V44_
N.C. CERTIFICATION #481
ME7!- uM 3-�8 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Client Sample ID:
MW-8
Client Project ID:
Almont Shipping
Lab Sample ID:
G121-328-8
Lab Project ID:
G121-328
Batch ID:
2845 2884
Report Basis:
Dry
Metals
Result
RL
Arsenic
4.18
0.996
Barium
42.4
9.96
Cadmium
BQL
0.996
Chromium
29.5
0.996
Lead
1260
0.996
Mercury
0.0811
0.0222
Selenium
BQL
1.99
Silver
BQL
0.996
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
(9
Results for Metals
Analyzed By:
PSW
Date Collected:
5/11/200511:00
Date Received:
5/12105
Matrix:
SOIL
Solids
85.06
DF
Units
Method
Date
Analyzed
1
MG/KG
6010E
5/24105
1
MG/KG
6010B
5/24/05
1
MG/KG
6010B
5/24/05
1
MG/KG
6010B
5/24105
1
MG/KG
6010B
5/24/05
1
MG/KG
7471
5/25105
1
MG/KG
6010B
5/24/05
1
MG/KG
6010B
5/24/05
Reviewed By:
MET LIMB 32
N.C. CERTIFICATION #481 29 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
Client Sample ID:
MW-9
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/11/200512:30
Lab Sample 1D:
G121-328-9
Date Received:
5/12/2005
Lab Project ID:
G121-328
Matrix:
SOIL
Batch ID:
2845 2884
Solids
98.11
Report Basis:
Dry
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
BQL
0.894
1
MG/KG
6010B
5/24/2005
Barium
BQL
8.94
1
MG/KG
6010B
5/24/2005
Cadmium
BQL
0.894
1
MG/KG
6010B
5/24/2005
Chromium
0.957
0.894
1
MG/KG
6010B
5/24/2005
Lead
1.20
0.894
1
MG/KG
6010B
5/24/2005
Mercury
BQL
0.0170
1
MG/KG
7471
5/25/2005
Selenium
BQL
1.79
1
MG/KG
6010B
5/24/2005
Silver
BQL
0.894
1
MG/KG
6010B
5/24/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL
and RL
Reviewed By: ?-,0
N.C. CERTIFICATION #481
MET LIMB 31
$0 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
•
Client Sample ID:
MW 10
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/11/200515:30
Lab Sample ID:
G121-328-10
Date Received:
5/12/2005
Lab Project ID:
G121-328
Matrix:
SOIL
Batch ID:
2845 2884
Solids
90.49
Report Basis:
Dry
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
25.8
1.04
1
MG/KG
6010E
5/24/2005
Barium
21.5
10.4
1
MG/KG
6010B
5/24/2005
Cadmium
BQL
1.04
1
MG/KG
6010B
5/24/2005
Chromium
11.8
1.04
1
MG/KG
6010B
5/24/2005
Lead
52.4
1.04
1
MG/KG
6010B
5/24/2005
Mercury
0.138
0.0194
1
MG/KG
7471
5/25/2005
Selenium
BQL
2.09
1
MG/KG
6010E
5/24/2005
Silver
BQL
1.04
1
MG/KG
6010B
5/24/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL
and RL
Reviewed By:
bIET_LIMS 3
N.C. CERTIFICATION #481
1 of 43

10
L�
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 1 Date Collected: 5/10/2005
Client Project ID: Almont Shipping Date Received: 5/12/2005
Lab Sample ID: G121-328-1 Matrix: Soil
Lab Project ID: G121-328
Analyte
Result
RL
Ammonia
49
0.1
Chloride
14.4
0.1
Nitrate
0.94
0.21
Phosphorus
76.4
0.5
Sulfate
676
50
TKN
486
0.1
Total Nitrogen
486
0.22
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
Units
Method
Date
Analyst
Analyzed
mg/kg
350.2
5/17/2005
Envirochem
mg/kg
SM 4500 CI-B
5/31/2005
Envirochem
mg/kg
353.3
5/26/2005
Envirochem
mg/kg
365.2
5/20/2005
Envirochem
mg/kg
375.4
6/1/2005
Envirochem
mg/kg
351.3
5/19/2005
Envirochem
mg/kg
353.1/351.3
5/19/2005
Envirochem
N.C. CERTIFICATION #481
Reviewed By: yz-AL
32 of 43

(0
L�
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID:
MW 2
Date Collected:
5/10/2005
Client Project ID:
Almont Shipping
Date Received:
5/12/2005
Lab Sample ID:
G121-328-2
Matrix:
Soil
Lab Project ID:
G121-328
Anaiyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
100
0.1
mg/kg
350.2
5/17/2005
Envirochem
Chloride
13.2
0.1
mg/kg
SM 4600 CI-B
5/31/2005
Envirochem
Nitrate
3.7
0.21
mg/kg
353.3
5/26/2005
Envirochem
Phosphorus
7.29
0.5
mg/kg
365.2
5/20/2005
Envirochem
Sulfate
55.3
50
mg/kg
375.4
6/1/2005
Envirochem
TKN
2078
0.1
mg/kg
351.3
5/19/2005
Envirochem
Total Nitrogen
2080
0.22
mg/kg
353.1/351.3
5/19/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
N.C. CERTIFICATION #481
Reviewed By:.g�
33 of 43

CID
(0
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 3 Date Collected: 5/10/2005
Client Project ID: Almont Shipping Date Received: 5/12/2005
Lab Sample ID: G121-328-3 Matrix: Soil
Lab Project ID: G121-328
Analyte
Result
RL.
Units
Method
Date
Analyst
Analyzed
Ammonia
816
0.1
mg/kg
350.2
5/17/2005
Envirochem
Chloride
40.5
0.1
mg/kg
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
44.9
0.21
mg/kg
353.3
5/26/2005
Envirochem
Phosphorus
126
0.5
mg/kg
365.2
5/20/2005
Envirochem
Sulfate
400
50
mg/kg
375.4
6/1/2005
Envirochem
TKN
3806
0.1
mg/kg
351.3
5/19/2005
Envirochem
Total Nitrogen
3810
0.22
mg/kg
353.1/351.3
5/19/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
N.C. CERTIFICATION #481
Reviewed By: ga
34 of 43

C9
(0
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW-4 Date Collected: 5/10/2005
Client Project ID: Almont Shipping Date Received: 5/12/2005
Lab Sample ID: G121-328-4 Matrix: Soil
Lab Project ID: G121-328
Analyte
Result
RL
Ammonia
93
0.1
Chloride
13.5
0.1
Nitrate
35.4
0.21
Phosphorus
266
0.5
Sulfate
95.4
50
TKN
1108
0.1
Total Nitrogen
1112
0.22
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
Units
Method
Date
Analyst
Analyzed
mg/kg
350.2
5/17/2005
Envirochem
mg/kg
SM 4500 CI-B
5/31/2005
Envirochem
mg/kg
353.3
5/26/2005
Envirochem
mg/kg
365.2
5/20/2005
Envirochem
mg/kg
375.4
6/1/2005
Envirochem
mg/kg
351.3
5/19/2005
Envirochem
mg/kg
353.1/351.3
5/19/2005
Envirochem
N.C. CERTIFICATION W1
Reviewed By: gr-
35 of 43

L0-
(to
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID:
MW 5
Date Collected:
5/10/2005
Client Project ID:
Almont Shipping
Date Received:
5/12/2005
Lab Sample ID:
G121-328-5
Matrix:
Soil
Lab Project ID:
G121-328
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
61
0.1
mg/kg
350.2
5/17/2005
Envirochem
Chloride
27
0.1
mg/kg
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
1.76
0.21
mg/kg
353.3
5/26/2005
Envirochem
Phosphorus
223
0.5
mg/kg
365.2
5/20/2005
Envirochem
Sulfate
56.8
50
mg/kg
375.4
6/1/2005
Envirochem
TKN
626
0.1
mg/kg
351.3
5/19/2005
Envirochem
Total Nitrogen
529
0.22
mg/kg
353.1/351.3
5/19/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
N.C. CERTIFICATION #481
Reviewed By: _ g�
36 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW-6 Date Collected: 5/11/2005
Client Project ID: Almont Shipping Date Received: 5/12/2005
Lab Sample ID: G121-328-6 Matrix: Soil
Lab Project ID: G121-328
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
29
0.1
mg/kg
350.2
5/17/2005
Envirochem
Chloride
842
0.1
mg/kg
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
1.47
0.21
mg/kg
353.3
5/26/2005
Envirochem
Phosphorus
76
0.5
mg/kg
365.2
5/20/2005
Envirochem
Sulfate
127
50
mg/kg
375.4
6/1/2005
Envirochem
TKN
120
0.1
mglkg
351.3
5/19/2005
Envirochem
Total Nitrogen
122
0.22
mg/kg
353.1/351.3
5/19/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
N.C. CERTIFICATION #481
Reviewed By:
37 of 43

1•
A
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 7 Date Collected: 5/11/2005
Client Project ID: Almont Shipping Date Received: 5/12/2005
Lab Sample ID: G121-328-7 Matrix: Soil
Lab Project ID: G121-328
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
48
0.1
mg/kg
350.2
5/17/2005
Envirochem
Chloride
36.4
0.1
mg/kg
SM 4500 CI-B
5/31/2006
Envirochem
Nitrate
BQL
0.21
mg/kg
353.3
5/26/2005
Envirochem
Phosphorus
150
0.5
mg/kg
365.2
5/20/2005
Envirochem
Sulfate
66.8
50
mg/kg
375.4
6/1/2005
Envirochem
TKN
448
0.1
mg/kg
351.3
5/19/2005
Envirochem
Total Nitrogen
448
0.22
mg/kg
353.1/351.3
5/19/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
N.C. CERTIFICATION #481
Reviewed By: _
38 of 43

(0
CIO
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW-8
Client Project ID: Almont Shipping
Lab Sample ID: G121-328-8
Lab Project ID: G121-328
Date Collected: 5/11/2005
Date Received: 5/12/2005
Matrix: Soil
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
67
0.1
mg/kg
350.2
5/17/2005
Envirochem
Chloride
2346
0.1
mg/kg
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
2.47
0.21
mg/kg
353.3
5/26/2005
Envirochem
Phosphorus
260
0.5
mg/kg
365.2
5/20/2005
Envirochem
Sulfate
64.7
50
mg/kg
375.4
6/1/2005
Envirochem
TKN
856
0.1
mg/kg
351.3
5/19/2005
Envirochem
Total Nitrogen
858
0.22
mg/kg
353.1/351.3
5/19/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
N.C. CERTIFICATION #481
Review By: �2�
39 of 43

CIO
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW-9
Client Project ID: Almont Shipping
Lab Sample ID: G121-328-9
Lab Project ID: G121-328
Date Collected: 5/11/2005
Date Received: 5/12/2005
Matrix: Soil
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
57
0.1
mg/kg
350.2
5/17/2005
Envirochem
Chloride
12.2
0.1
mg/kg
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
0.88
0.21
mg/kg
353.3
5/26/2005
Envirochem
Phosphorus
84
0.5
mg/kg
365.2
5/20/2005
Envirochem
Sulfate
54.1
50
mg/kg
375.4
6/1/2005
Envirochem
TKN
65
0.1
mg/kg
351.3
5/19/2005
Envirochem
Total Nitrogen
66
0.22
mg/kg
353.1/351.3
5/19/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
N.C. CERTIFICATION #481
Reviewed By: , w
40 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
�• Client Sample ID: MW 10 Date Collected: 5/11/2005
Client Project ID: Almont Shipping Date Received: 5/12/2005
Lab Sample ID: G121-328-10 Matrix: Soil
Lab Project ID: G121-328
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
38
0.1
mg/kg
350.2
5/17/2005
Envirochem
Chloride
47.2
0.1
mg/kg
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
5.87
0.21
mg/kg
353.3
5/26/2005
Envirochem
Phosphorus
217
0.5
mg/kg
365.2
5/20/2005
Envirochem
Sulfate
68.4
50
mg/kg
375.4
6/1/2005
Envirochem
TKN
285
0.1
mg/kg
351.3
5/19/2005
Envirochem
Total Nitrogen
361
0.22
mg/kg
353.1/351.3
5/19/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
1�
Reviewed By:
N.C. CERTIFICATION #481 41 of 43

PARADIGM ANALYTICAL LABORATORIES, INC.
�O
List of Reporting Abbreviations
and Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantitation Limit
DF = Dilution Factor
Dup = Duplicate
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL = Reporting Limit
RPD = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% solids = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
M134.011404.1
N.C. CERTIFICATION #481 42 of 43

PARADIO-IFFANALYTICAL LABORATORIES, INC. — cOC# 4 6 9
5500 Business Drive, Wilmington, NC 28405 Chain -of Custody Record & Analytical Request 9
Phone: [phone] FAX: [phone] Page / of
Client: [�ol�b� �15lbL1 Project ID: �,�""°`' Sh'�p,^g Elate: �Z v� Report To• a
Address: Contact: Thrnaround: S' ►.d o�i
Address: Phone: Job Number:
Quote P. Fax: P.O. Number: - Invoice To:
4 Sp
d
7 .I
_
UAIMM■■■■RA
WERRA
MBROA■
M��M
�
����
■■■■
■nmmmmmmo■
�
a■���
■■■■
►,�mmmm►gym©m■
'IiVvliMl'' I
�•
�
MIRYdII
T.1+{:.%SrYaiE.,C
3M`G.. - ,` 7 t.L-aatitt'a1r -ecif:fleY.. lSEE
REVERSE FOR
W

PARADIGM ANALYTICAL LABORATORIES, INC.
Mr. Gary Babb
Babb & Associate
P.O. Box 37697
Raleigh NC 27627
ReportNumber: G121-330
Client Project: Almont Shipping
Dear Mr. Babb:
Enclosed are the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
10 they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call Paradigm at [phone]. We will be happy to answer any questions or
concerns which you may have.
Thank you for using Paradigm Analytical Labs for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely,
Paradigm Analytical Laboratories, Inc.
' D` ` �, ' (a j 9J'RmV-17 --- - -
La orat ry &rector ate
J. Patrick Weaver
N.C. CERTIFICATION #481 1 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260-5035
l Client Sample ID: MW-11
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 05-17-2005
10:00
Lab Sample ID G121-330-1A
Date Received: 5/17/05
Lab Project ID: G121-330
Matrix: Soil
Report Basis: Dry Weight
%Solids: 91.1
Report Name
Result
Quantitation
Dilution
Date
Compound
UG1KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
44.6
1
5/22/05
Benzene
BQL
4.46
1
5/22/05
Bromobenzene
BQL
4.46
1
5/22/05
Bromochloromethane
BQL
4.46
1
5/22105
Bromodichloromethane
BQL
4.46
1
5/22/05
Bromoform
BQL
4.46
1
5/22/05
Bromomethane
BQL
4.46
1
5/22/05
2-Butanone
BQL
22.3
1
5/22/05
n-Butylbenzene
BQL
4.46
1
5/22/05
sec-Butylbenzene
BQL
4.46
1
5/22/05
tert-Butylbenzene
BQL
'4.46
1
5/22/05
Carbon disulfide
BQL
4.46
1
5/22/05
Carbon tetrachloride
BQL
4.46
1
5/22/05
Chlorobenzene
BQL
4.46
1
5/22/05
CChloroethane
BQL
4.46
1
5/22/05
Chloroform
BQL
4.46
1
5/22/05
Chloromethane
BQL
4.46
1
5/22/05
2-Chlorotoluene
BQL
4.46
1
5122/05
4-Chlorotoluene
BQL
4.46
1
5/22/05
Dibromochloromethane
BQL
4.46
1
5/22/05
1,2-Dibromo-3-chloropropane
BQL
4.46
1
5/22/05
Dibromomethane
BQL
4.46
1
5/22/05
1,2-Dibromoethane (EDB)
BQL
4.46
1
5/22/05
1,2-Dichlorobenzene
BQL
4.46
1
5/22/05
1,3-Dichlorobenzene
BQL
4.46
1
5/22/05
1,4-Dichlorobenzene
BQL
4.46
1
5/22/05
trans-1,4-Dichloro-2-butene
BQL
4.46
1
5/22105
1,1-Dichloroethane
BQL
4.46
1
5/22/05
1,1-Dichloroethene
BQL
4.46
1
5/22/05
1,2-Dichloroethane
BQL
4.46
1
5/22/05
cis-1,2-Dichloroethene
BQL
4.46
1
5/22/05
trans-1,2-dichloroethene
BQL
4.46
1
5/22/05
1,2-Dichloropropane
BQL
4.46
1
5/22/05
1,3-Dichloropropane
BQL
4.46
1
5/22/05
2,2-Dichloropropane
BQL
4.46
1
5/22105
1,1-Dichloropropene
BQL
4.46
1
5/22/06
cis-1,3-Dichloropropene
BQL
4.46
1
5/22/05
trans-1,3-Dichloropropene
BQL
4.46
1
5/22/05
Dichlorodifluorometharie
BQL
4.46
1
5/22/05
Diisopropyl ether (DIPE)
BQL
4.46
1
5/22/05
Ethylbenzene
BQL
4.46
1
5/22/05
Hexachlorobutadiene
BQL
4.46
1
5/22/05
Page 1 of 2 GCMS_LIMS SOLO V1 31
N.C. CERTIFICATION #481 2 Of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
C•
by GCMS 8260-5035
Client Sample ID: MWA 1
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 05-17-200510:00
Lab Sample ID G121-330-1A
Date Received: 5/17/05
Lab Project ID: G121-330
Matrix: Soil
Report Basis: Dry Weight
%Solids: 91.1
Report Name
Result
Quantitation
Dilution
Date
Compound
UGIKG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
4.46
1
5/22/05
lodomethane
BQL
4.46
1
5/22/05
Isopropylbenzene
BQL
4.46
1
5/22/05
4-Isopropyltoluene
BQL
4.46
1
5/22/05
Methylene chloride
BQL
17.8
1
5/22/05
4-Methyl-2-pentanone
BQL
4.46
1
5/22/05
Methyl-tert-butyl ether (MTBE)
BQL
4.46
1
5/22/05
Naphthalene
BQL
4.46
1
5/22/05
n-Propyi benzene
BQL
4.46
1
5/22/05
Styrene
BQL
4.46
1
5/22/05
1,1,1,2-Tetrachloroethane
BQL
4.46
1
5/22/05
1,1,2,2-Tetrachloroethane
BQL
4.46
1
5122/05
Tetrachloroethene
BQL
4.46
1
5/22/05
Toluene
BQL
4.46
1
5/22/05
f1,2,3-Trichlorobenzene
C0
BQL
4.46
1
5/22/05
1,2,4-Trichlorobenzene
BQL
4.46
1
5/22/05
Trichloroethene
BQL
4.46
1
5/22/05
1,1,1-Trichloroethane
BQL
4.46
1
5/22/05
1,1,2-Trichloroethane
BQL
4.46
1
5/22/05
Trichlorofluoromethane
BQL
4.46
11
5/22/05
1,2,3-Trichloropropane
BQL
4.46
1
5/22/05
1,2,4-Trimethylbenzene
BQL
4.46
1
5/22/05
1,3,5-Trimethylbenzene
BQL
4.46
1
5122/05
Vinyl chloride
BQL
4.46
1
5/22/05
m-,p-Xylene
BQL
8.92
1
5/22/05
o-Xylene
BQL
4.46
1
5/22/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
50
56
112
1,2-Dichloroethane-d4
50
49.5
99
Toluene-d8
50
50.4
101
Comments:
Flags:
BQL = Below Quantitation Limits.
Reviewed By: fL►y°
N.C. CERI IFI�ATION #481 ccMs `1"'S �`° �' 3"'3 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
Client Sample ID: MW-12 by GCMS 8260.5035 Analyzed By: J7F
Client Project ID: Himont Shipping Date Collected: 05-17-200511:00
Lab Sample ID G121-330-2A Date Received: 5/17/05
Lab Project ID: G121-330 Matrix: Soil
Report Basis: Dry Weight %Solids: 97.6
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UGIKG
Factor
Analyzed
Acetone
BQL
47.5
1
5/22/05
Benzene
BQL
4.75
1
5/22/05
Bromobenzene
BQL
4.75
1
5/22/05
Bromochloromethane
BQL
4.75
1
5/22/06
Bromodichloromethane
BQL
4.75
1
5/22/05
Bromoform
BQL
4.75
1
5/22/05
Bromomethane
BQL
4.75
1
5/22105
2-Butanone
BQL
23.8
1
5/22/05
n-Butylbenzene
BQL
4.75
1
5/22/05
sec-Butylbenzene
BQL
4.75
1
5/22/05
tert-Butylbenzene
BQL
4.75
1
5/22/05
Carbon disulfide
BQL
4.75
1
5/22/05
Carbon tetrachloride
BQL
4.75
1
5/22/05
Chlorobenzene
BQL
4.75
1
5/22105
VChloroethane
BQL
4.75
1
5/22/05
Chloroform
BQL
4.75
1
5/22/05
Chloromethane
BQL
4.75
1
5/22/05
2-Chlorotoluene
BQL
4.75
1
5/22/05
4-Chlorotoluene
BQL
4.75
1
5/22/05
Dibromochloromethane
BQL
4.75
1
5/22/05
1,2-Dibromo-3-chloropropane
BQL
4.75
1
5/22/05
Dibromomethane
BQL
4.75
1
5122/05
1,2-Dibromoethane (EDB)
BQL
4.75
1
5/22/06
1,2-Dichlorobenzene
BQL
4.75
1
5/22/05
1,3-Dichlorobenzene
BQL
4.75
1
5/22/05
1,4-Dichlorobenzene
BQL
4.75
1
5/22105
trans-1,4-Dichloro-2-butene
BQL
4.75
1
5/22/05
1,1-Dichloroethane
BQL
4.75
1
5/22/05
1,1-Dichloroethene
BQL
4.75
1
5/22/05
1,2-Dichloroethane
BQL
4.75
1
5/22/05
cis-1,2-Dichloroethene
BQL
4.75
1
5/22/05
trans-1,2-dichloroethene
BQL
4.75
1
5/22/05
1,2-Dichloropropane
BQL
4.75
1
5/22105
1,3-Dichloropropane
BQL
4.75
1
5/22/05
2,2-Dichloropropane
BQL
4.75
1
5/22/05
1,1-Dichloropropene
BQL
4.75
1
5/22/05
cis-1,3-Dichloropropene
BQL
4.75
1
5/22/05
trans-1,3-Dichloropropene
BQL
4.75
1
5/22/05
Dichlorodifluoromethane
Diisopropyl ether (DIPE)
BQL
BQL
4.75
4.75
1
1
5/22/05
5/22/05
Ethylbenzene
BQL
4.75
1
5/22/05
Hexachiorobutadiene
BQL
4.75
1
5/22/05
Page 1 of 2 GCM8 1MS SOLO V1.3ads
N.C. CER I IFICATION #481 4 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
lk
by GCMS 8260-5035
ient Sample ID: MW-12
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 05-17-200511:00
Lab Sample ID G121-330-2A
Date Received: 5/17/05
Lab Project ID: G121-330
Matrix: Soil
Report Basis: Dry Weight
%Solids: 97.6
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
4.75
1
5/22/05
lodomethane
BQL
4.75
1
5/22/05
Isopropylbenzene
BQL
4.75
1
5/22/05
4-Isopropyltoluene
BQL
4.75
1
5/22/05
Methylene chloride
BQL
19.0
1
5/22/05
4-Methyl-2-pentanone
BQL
4.75
1
5/22/05
Methyl-tert-butyl ether (MTBE)
BQL
4.75
1
5/22/05
Naphthalene
BQL
4.75
1
5/22/05
n-Propyl benzene
BQL
4.75
1
5/22/05
Styrene
BQL
4.75
1
5/22105
1,1,1,2-Tetrachloroethane
BQL
4.75
1
5/22/05
1,1,2,2-Tetrachloroethane
BQL
4.75
1
5/22/05
Tetrachloroethene
BQL
4.75
1
5/22/05
Toluene
BQL
4.75
1
5/22/05
1,2,3-Trichlorobenzene
BQL
4.75
1
5/22/05
1,2,4-Trichlorobenzene
BQL
4.75
1
5122/05
Trichloroethene
BQL
4.75
1
5/22/05
1,1,1-Trichloroethane
BQL
4.75
1
5/22/05
1,1,2-Trichloroethane
BQL
4.75
1
5/22/05
Trichlorofluoromethane
BQL
4.75
1
5/22/05
1,2,3-Trichloropropane
BQL
4.75
1
5/22/05
1,2,4-Trimethylbenzene
BQL
4.75
1
5/22/05
1,3,5-Trimethylbenzene
BQL
4.75
1
5/22/05
Vinyl chloride
BQL
4.75
1
5/22/05
m-,p-Xylene
BQL
9.51
1
5/22/05
o-Xylene
BQL
4.75
1
5/22/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
50
54.8
110
1,2-Dichloroethane-d4
50
50.5
101
Toluene-d8
50
50.7
101
Comments:
Flags:
BQL = Below Quantitation Limits.
0-
Reviewed By: _fz-aP
Page 2 of 2 GCMS_UMS_SOLO V1.3 xis
N.C. CERTIFICATION #481 5 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
lkient
by GCMS 8260.5035
Sample ID: MWA 3
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 05-17-200512:30
Lab Sample ID G121-330-3A
Date Received: 5/17/05
Lab Project ID: G121-330
Matrix: Soil
Report Basis: Dry Weight
%Solids: 88.8
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
44.7
1
5/22/05
Benzene
BQL
4.47
1
5/22/05
Bromobenzene
BQL
4.47
1
5/22/05
Bromochloromethane
BQL
4.47
1
5/22/05
Bromodichloromethane
BQL
4.47
1
5/22/05
Bromoform
BQL
4.47
1
5/22/05
Bromomethane
BQL
4.47
1
5/22/05
2-Butanone
BQL
22.4
1
5/22/05
n-Butylbenzene
BQL
4.47
1
5/22105
sec-Butylbenzene
BQL
4.47
1
5/22/05
tert-Butylbenzene
BQL
4.47
1
5/22/05
Carbon disulfide
BQL
4.47
1
5/22/05
Carbon tetrachloride
BQL
4.47
1
5/22/05
Chlorobenzene
BQL
4.47
1
5/22/05
hloroethane
1W,
BQL4.47
1
5/22/05
hloroform
BQL
4.47
1
5/22/05
Chloromethane
BQL
4.47
1
5/22/05
2-Chlorotoluene
BQL
4.47
1
5122/05
4-Chlorotoluene
BQL
4.47
1
5/22/05
Dibromochloromethane
BQL
4.47
1
5/22/05
1,2-Dibromo-3-chloropropane
BQL
4.47
1
5122105
Dibromomethene
BQL
4.47
1
5/22/05
1,2-Dibromoethane (EDB)
BQL
4.47
1
5/22/05
1,2-Dichlorobenzene
BQL
4.47
1
5/22/05
1,3-Dichlorobenzene
BQL
4.47
1
5/22/05
1,4-Dichlorobenzene
BQL
4.47
1
5/22/05
trans-1,4-Dichloro-2-butene
BQL
4.47
1
5/22/05
1,1-Dichloroethane
BQL
4.47
1
5/22/05
1,1-Dichloroethene
BQL
4.47
1
5/22/05
1,2-Dichloroethane
BQL
4.47
1
5/22/05
cis-1,2-Dichloroethene
BQL
4.47
1
5/22/05
trans-1,2-dichioroethene
BQL
4.47
1
5/22/05
1,2-Dichloropropane
BQL
4.47
1
5/22/05
1,3-Dichloropropane
BQL
4.47
1
5/22105
2,2-Dichloropropane
BQL
4.47
1
5/22/05
1,1-Dichloropropene
BQL
4.47
1
5/22/05
cis-1,3-Dichloropropene
BQL
4.47
1
5/22/05
trans-1,3-Dichloropropene
BQL
4.47
1
5122/05
Dichlorodifluoromethane
Diisopropyl ether (DIPS)
BQL
BQL
4.47
4.47
1
1
5/22/05
5/22/05
Ethylbenzene
BQL
4.47
1
5/22/05
Hexachlorobutadiene
BQL
4.47
1
5/22/05
Pa e 1 of 2 GCMS_LIMS SOLO V1.3.x1s
N.C. CEIFICATION #481 6 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260.5035
Client Sample ID: MW-13
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 05-17-2005
12:30
Lab Sample ID G121-330-3A
Date Received: 5/17/05
Lab Project ID: G121-330
Matrix: Soil
Report Basis: Dry Weight
%Solids: 88.8
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
4.47
1
5/22/05
lodomethane
BQL
4.47
1
5/22/05
Isopropylbenzene
BQL
4.47
1
5/22/05
4-Isopropyltoluene
BQL
4.47
1
5/22/05
Methylene chloride
BQL
17.9
1
5/22/05
4-Methyl-2-pentanone
BQL
4.47
1
5/22/05
Methyl-tert-butyl ether (MTBE)
BQL
4.47
1
5/22/05
Naphthalene
BQL
4.47
1
5122/05
n-Propyl benzene
BQL
4.47
1
5/22/05
Styrene
BQL
4.47
1
5/22/05
1,1,1,2-Tetrachloroethane
BQL
4.47
1
5/22/05
1,1,2,2-Tetrachloroethane
BQL
4.47
1
5/22/05
Tetrachloroethene
BQL
4.47
1
5/22/05
Toluene
BQL
4.47
1
5/22/05
1,2,3-Trichlorobenzene
BQL
4.47
1
5/22/05
1,2,4-Trichlorobenzene
BQL
4.47
1
5/22/05
Trichloroethene
BQL
4.47
1
5/22/05
1,1,1-Trichloroethane
BQL
4.47
1
5/22/05
1,1,2-Trichloroethane
BQL
4.47
1
5/22/05
Trichlorofluoromethane
BQL
4.47
1
5/22/05
1,2,3-Trichloropropane
BQL
4.47
1
5/22/05
1,2,4-Trimethylbenzene
BQL
4.47
1
5/22/05
1,3,5-Trimethylbenzene
BQL
4.47
1
5/22/05
Vinyl chloride
BQL
4.47
1
5/22/05
m-,p-Xylene
BQL
8.95
1
5/22105
o-Xylene
BQL
4.47
1
5/22/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
50
54.5
109
1,2-Dichloroethane-d4
50
47.9
96
Toluene-d8
50
49.8
100
Comments:
Flags:
BQL = Below Quantitation Limits.
0
Reviewed By: 9-YAP
Page 2 of 2 GCMS UMS SOLO V1 Ul
N.C. CERTIFICATION #481 � of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
(0-client
by GCMS 8260-5035
Sample ID: MW-14
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 05-17-2005
13:30
Lab Sample ID G121-330-4A
Date Received: 5/17/05
Lab Project ID: G121-330
Matrix: Soil
Report Basis: Dry Weight
%Solids: 93.6
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
42.3
1
5/22/05
Benzene
BQL
4.23
1
5/22/05
Bromobenzene
BQL
4.23
1
5/22/05
Bromochloromethane
BQL
4.23
1
5/22/05
Bromodichloromethane
BQL
4.23
1
5/22/05
Bromoform
BQL
4.23
1
5/22/05
Bromomethane
BQL
4.23
1
5/22/05
2-Butanone
BQL
21.1
1
5/22105
n-Butylbenzene
BQL
4.23
1
5/22/05
sec-Butylbenzene
BQL
4.23
1
5/22/05
tert-Butyl benzene
BQL
4.23
1
5/22105
Carbon disulfide
BQL
4.23
1
5/22/05
Carbon tetrachloride
BQL
4.23
1
5/22/05
Chlorobenzene
BQL
4.23
1
5/22/05
Chloroethane
A-Chloroform
BQL
4.23
1
5/22/05
BQL
4.23
1
5/22/05
Chloromethane
BQL
4.23
1
5/22/05
2-Chlorotoluene
BQL
4.23
1
5/22/05
4-Chlorotoluene
BQL
4.23
1
5/22/05
Dibromochloromethane
BQL
4.23
1
5/22/05
1,2-Dibromo-3-chioropropane
BQL
4.23
1
5/22/05
Dibromomethane
BQL
4.23
1
5/22/05
1,2-Dibromoethane (EDB)
BQL
4.23
1
5/22105
1,2-Dichlorobenzene
BQL
4.23
1
5/22/05
1,3-Dichlorobenzene
BQL
4.23
1
5/22/05
1,4-Dichlorobenzene
BQL
4.23
1
5/22/05
trans-1,4-Dichloro-2-butene
BQL
4.23
1
5/22/05
1,1-Dichloroethane
BQL
4.23
1
5/22/05
1,1-Dichioroethene
BQL
4.23
1
5/22/05
1,2-Dichloroethane
BQL
4.23
1
5/22/05
cis-1,2-Dichloroethane
BQL
4.23
1
5/22/05
trans-1,2-dichloroethene
BQL
4.23
1
5/22/05
1,2-Dichloropropane
BQL
4.23
1
5/22/05
1,3-Dichloropropane
BQL
4.23
1
5/22/05
2,2-Dichloropropane
BQL
4.23
1
5/22/05
1,1-Dichloropropene
BQL
4.23
1
5/22/05
cis-1,3-Dichloropropene
BQL
4.23
1
5/22/05
trans-1,3-Dichloropropene
BQL
4.23
1
5/22/05
Dichlorodifluoromethane
BQL
4.23
1
5/22/05
Diisopropyl ether (DIPE)
BQL
4.23
1
5/22/05
Ethylbenzene
BQL
4.23
1
5/22/05
Hexachiorobutadiene
BQL
4.23
1
5/22/05
Page 1 of 2 GCMS LIMS_SOLO V7.3 xla
N.C. CERTIFICATION #481 8 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
(0
by GCMS 8280-5035
Client Sample ID: MW-14
Analyzed B
Y Y: JTF
Client Project ID: Almont Shipping
Date Collected: 05-17-200513:30
Lab Sample ID G121-330-4A
Date Received: 5/17105
Lab Project ID: G121-330
Matrix: Soil
Report Basis: Dry Weight
%Solids: 93.6
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
4.23
1
5/22/05
lodomethane
BQL
4.23
1
5/22/05
Isopropylbenzene
BQL
4.23
1
5/22/05
4-Isopropyltoluene
BQL
4.23
1
5/22/05
Methylene chloride
BQL
16.9
1
5/22/05
4-Methyl-2-pentanone
BQL
4.23
1
5/22/05
Methyl-tert-butyl ether (MTBE)
BQL
4.23
1
5/22/05
Naphthalene
BQL
4.23
1
5/22/05
n-Propyl benzene
BQL
4.23
1
5/22/05
Styrene
BQL
4.23
1
5/22/05
1,1,1,2-Tetrachloroethane
BQL
4.23
1
5/22/05
1,1,2,2-Tetrachloroethane
BQL
4.23
1
5/22/05
Tetrachloroethene
BQL
4.23
1
5/22/05
Toluene
BQL
4.23
1
5/22/05
1,2,3-Trichlorobenzene
BQL
4.23
1
5/22/05
1,2,4-Trichlorobenzene
BQL
4.23
1
5/22/05
Trichloroethene
BQL
4.23
1
5/22/05
1,1,1-Trichloroethane
BQL
4.23
1
5/22/05
1,1,2-Trichloroethane
BQL
4.23
1
5/22/05
Trichlorofluoromethane
BQL
4.23
1
5/22/05
1,2,3-Trichloropropane
BQL
4.23
1
5/22105
1,2,4-Trimethylbenzene
BQL
4.23
1
5/22/05
1,3,5-Trimethylbenzene
BQL
4.23
1
5/22/05
Vinyl chloride
BQL
4.23
1
5/22/05
m-,p-Xylene
BQL
8.45
1
5/22/05
o-Xylene
BQL
4.23
1
5/22/05
4-Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
Comments:
Flags:
BQL = Below Quantitation Limits.
Spike
Spike
Percent
Added
Result
Recovered
50
55.3
111
50
49.3
99
50
50.5
101
N.G. CER� IFI8ATION #481
Reviewed By: _tom_
GCMS LIMS SOLO V1.3A'b of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260-5035
Client Sample ID: MW-15
Analyzed By: J7F
Client Project ID: Almont Shipping
Date Collected: 05-17-2005
15:00
Lab Sample ID G121-330-5A
Date Received: 5/17/05
Lab Project ID: G121-330
Matrix: Soil
Report Basis: Dry Weight
%Solids: 88.1
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
Acetone
BQL
44.7
1
5/22/05
Benzene
BQL
4.47
1
5/22/05
Bromobenzene
BQL
4.47
1
5122/05
Bromochioromethane
BQL
4.47
1
5/22/05
Bromodichloromethane
BQL
4.47
1
5/22/05
Bromoform
BQL
4.47
1
5/22/05
Bromomethane
BQL
4.47
1
5/22/05
2-Butanone
BQL
22.4
1
5/22/05
n-Butylbenzene
BQL
4.47
1
5/22/05
sec-Butylbenzene
BQL
4.47
1
5/22/05
tert-Butylbenzene
BQL
4.47
1
5/22/05
Carbon disulfide
BQL
4.47
1
5/22/05
Carbon tetrachloride
BQL
4.47
1
5/22/05
Chlorobenzene
BQL
4.47
1
5/22/05
BQL
4.47
1
5/22/05
(�Chloroethane
Chloroform
BQL
4.47
1
5/22/05
Chloromethane
BQL
4.47
1
5/22/05
2-Chlorotoluene
BQL
4.47
1
5/22/05
4-Chlorotoluene
BQL
4.47
1
5/22105
Dibromochloromethane
BQL
4.47
1
5/22/05
1,2-Dibromo-3-chloropropane
BQL
4.47
1
5/22/05
Dibromomethane
BQL
4.47
1
5/22/05
1,2-Dibromoethane (EDB)
BQL
4.47
1
5/22105
1,2-Dichlorobenzene
BQL
4.47
1
5/22/05
1,3-Dichlorobenzene
BQL
4.47
1
5/22105
1,4-Dichlorobenzene
BQL
4.47
1
5/22/05
trans-1,4-Dichioro-2-butene
BQL
4.47
1
5/22/05
1,1-Dichloroethane
BQL
4.47
1
5/22/05
1,1-Dichloroethene
BQL
4.47
1
5/22/05
1,2-Dichloroethane
BQL
4.47
1
5/22/05
cis-1,2-Dichloroethene
BQL
4.47
1
5/22/05
trans-1,2-dichloroethene
BQL
4.47
1
5/22/05
1,2-Dichloropropane
BQL
4.47
1
5/22/05
1,3-Dichloropropane
BQL
4.47
1
5/22/05
2,2-Dichloropropane
BQL
4.47
1
5/22/05
1,1-Dichloropropene
BQL
4.47
1
5/22/05
cis-1,3-Dichloropropene
BQL
4.47
1
5/22/05
trans-1,3-Dichloropropene
BQL
4.47
1
5/22/05
Dichlorodiluoromethane
BQL
4.47
1
5/22/05
.Diisopropyl ether (DIPE)
BQL
4.47
1
5/22/05
Ethylbenzene
BQL
4.47
1
5/22/05
Hexachlorobutadiene
BQL
4.47
1
5/22/05
N.C. CEFZ I IF CATION #481 �Ms ��Ms_so�o ��.3 �• 14 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
�. by GCMS 8260-5035
Client Sample ID: MW-15 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 05-17-200515:00
Lab Sample ID G121-330-5A Date Received: 5117/05
Lab Project ID: G121-330 Matrix: Soil
Report Basis: Dry Weight %Solids: 88.1
Report Name
Result
Quantitation
Dilution
Date
Compound
UG/KG
Limit UG/KG
Factor
Analyzed
2-Hexanone
BQL
4.47
1
5/22/05
lodomethane
BQL
4.47
1
5/22/05
Isopropylbenzene
BQL
4.47
1
5/22/05
4-Isopropyltoluene
BQL
4.47
1
5/22/06
Methylene chloride
BQL
17.9
1
5/22/05
4-Methyl-2-pentanone
BQL
4.47
1
5/22/05
Methyl-tert-butyl ether (MTBE)
BQL
4.47
1
5/22/05
Naphthalene
BQL
4.47
1
5/22/05
n-Propyl benzene
BQL
4.47
1
5/22/05
Styrene
BQL
4.47
1
5/22/05
1,1,1,2-Tetrachloroethane
BQL
4.47
1
5/22/05
1,1,2,2-Tetrachloroethane
BQL
4.47
1
5/22/05
Tetrachloroethene
BQL
4.47
1
5/22/05
Toluene
BQL
4.47
1
5/22/05
1,2,3-Trichlorobenzene
BQL
4.47
1
5/22/05
1,2,4-Trichlorobenzene
BQL
4.47
1
5/22/05
Trichloroethene
BQL
4.47
1
5/22/05
1, 1, 1 -Trichloroethane
BQL
4.47
1
5/22/05
1,1,2-Trichloroethane
BQL
4.47
1
5/22/05
Trichlorofluoromethane
BQL
4.47
1
5/22/05
1,2,3-Trichloropropane
BQL
4.47
1
5/22/05
1,2,4-Trimethylbenzene
BQL
4.47
1
5/22105
1,3,5-Trimethylbenzene
BQL
4.47
1
5/22105
Vinyl chloride
BQL
4.47
1
5/22/05
m-,p-Xylene
BQL
8.95
1
5/22/05
o-Xylene
BQL
4.47
1
5/22/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
50
55.1
110
1,2-Dichloroethane-d4
50
50
100
Toluene-d8
50
50.6
101
Comments:
Flags:
BQL = Below Quantitation Limits.
A
Reviewed By: ?-IAP _
Pac �a 212 GCMSLIMSS0L0 Vt 3.xls
N.C. CER f IFICATION #481 __11 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
C�
Client Sample ID:
MW-11
Analyzed By:
PSW
Client Project ID:
Aimont Shipping
Date Collected:
5/17/200510:00
Lab Sample ID:
G121-330-1
Date Received:
5/17/2005
Lab Project ID:
G121-330
Matrix:
SOIL
Batch ID:
2846 2884
Solids
91.10
Report Basis:
Dry
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
2.55
0.998
1
MG1KG
6010E
6/5/2005
Barium
BQL
9.98
1
MG/KG
6010E
6/5/2005
Cadmium
BQL
0.998
1
MG/KG
6010B
6/5/2005
Chromium
2.33
0.998
1
MG/KG
6010E
6/5/2005
Lead
28.8
0.998
1
MG/KG
6010E
6/5/2005
Mercury
0.216
0.0196
1
MG/KG
7471
5/25/2005
Selenium
BQL
2.00
1
MG/KG
6010B
6/5/2005
Silver
BQL
0.998
1
MG/KG
6010E
6/5/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL
and RL
Reviewed By: a-,✓
N.C. CERTIFICATION
#481
MET LIMS 9.1
12 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
�•
Client Sample ID: MW-12
Analyzed By:
PSW
Client Project ID: Almont Shipping
Date Collected:
5/17/2005 11:00
Lab Sample ID: G121-330-2
Date Received:
5/17/2005
Lab Project ID: G121-330
Matrix:
SOIL
Batch ID: 2846 2884
Solids
97.58
Report Basis: Dry
Metals Result
RL
DF
Units
Method
Date
Analyzed
Arsenic BQL
0.986
1
MG/KG
6010B
6/5/2005
Barium BQL
9.86
1
MG/KG
6010B
6/5/2005
Cadmium BQL
0.986
1
MG/KG
6010B
6/5/2005
Chromium 1.01
0.986
1
MG/KG
6010B
6/5/2005
Lead 5.83
0.986
1
MG/KG
6010B
6/5/2005
Mercury 0.0360
0.0197
1
MG/KG
7471
5/25/2005
Selenium BQL
1.97
1
MG/KG
6010E
6/5/2005
Silver BQL
0.986
1
MG/KG
6010E
6/5/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
Reviewed By: irO
MET LIMS_3.1
N.C. CERTIFICATION #481
13 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
Client Sample ID: MW-13
Analyzed By:
PSW
Client Project ID: Almont Shipping
Date Collected:
5117/200512:30
Lab Sample ID: G121-330-3
Date Received:
5/17/2005
Lab Project ID: G121-330
Matrix:
SOIL
Batch ID: 2846 2884
Solids
88.83
Report Basis: Dry
Metals Result
RL
DF
Units
Method
Date
Analyzed
Arsenic BQL
1.08
1
MG/KG
6010B
6/5/2005
Barium BQL
10.8
1
MG/KG
6010E
6/5/2005
Cadmium BQL
1.08
1
MG/KG
6010B
6/5/2005
Chromium 1.96
1.08
1
MG/KG
6010B
6/5/2005
Lead 2.92
1.08
1
MG/KG
6010E
6/5/2005
Mercury BQL
0.0212
1
MG/KG
7471
5/25/2005
Selenium BQL
2.16
1
MG/KG
6010B
6/5/2005
Silver BQL
1.08
1
MG/KG
6010B
6/5/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
Reviewed By: 9,,,o
MET uMs_3.1
N.C. CERTIFICATION #481
14 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
C •
Client Sample ID: MW-14
Analyzed B
Yz Y�
PSW
Client Project ID: Almont Shipping
Date Collected:
5/17/200513:30
Lab Sample ID: G121-330-4
Date Received:
5/17/2005
Lab Project ID: G121-330
Matrix:
SOIL
Batch ID: 2846 2884
Solids
93.59
Report Basis: Dry
Metals Result
RL
DF
Units
Method
Date
Analyzed
Arsenic BQL
0,989
1
MG/KG
6010E
6/5/2005
Barium BQL
9.89
1
MG/KG
60101B
6/5/2005
Cadmium BQL
0.989
1
MG/KG
6010E
6/5/2005
Chromium 2.10
0.989
1
MG/KG
6010E
6/5/2005
Lead 10.6
0.989
1
MG/KG
601013
6/5/2005
Mercury 0.0315
0.0198
1
MG/KG
7471
5/25/2005
Selenium BQL
1.98
1
MG/KG
6010E
6/5/2005
Silver BQL
0.989
1
MG/KG
6010B
6/5/2005
Comments
�•
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
Reviewed By: 2w,A
N.C. CERTIFICATION #481
Mer_uras 3.1
15 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
C0
Client Sample ID:
MW-15
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5117/200515:00
Lab Sample ID:
G121-330-5
Date Received:
5/17/2005
Lab Project ID:
G121-330
Matrix:
SOIL
Batch ID:
2846 2884
Solids
88.14
Report Basis:
Dry
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
7.70
0.945
1
MG/KG
6010B
6/5/2005
Barium
BQL
9.45
1
MG/KG
6010B
6/5/2005
Cadmium
BQL
0.945
1
MG/KG
6010E
6/5/2005
Chromium
19.0
0.945
1
MG/KG
6010B
6/5/2005
Lead
5.91
0.945
1
MG/KG
6010B
6/5/2005
Mercury
BQL
0.0206
1
MG/KG
7471
5/25/2005
Selenium
BQL
1.89
1
MG/KG
6010E
6/5/2005
Silver
BQL
0.945
1
MG/KG
6010E
6/5/2005
Comments
Ice
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL
and RL
Reviewed By: _
MET uMUA
N.C. CERTIFICATION
#481
16 of 23

C9
(•
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 11 Date Collected: 5/17/2005
Client Project ID: Almont Shipping Date Received: 5/17/2005
Lab Sample ID: G121-330-1 Matrix: Soil
Lab Project ID: G121-330
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
42.9
0.1
mg/kg
350.2
5/24/2005
Envirochem
Chloride
110
0.1
mg/kg
SM 4500CI-B
6/17/2005
Envirochem
Nitrate
BQL
0.29
mg/kg
353.3
6/9/2005
Envirochem
Phosphorus
158
0.5
mg/kg
365.2
5/20/2005
Envirochem
Sulfate
24.7
5
mg/kg
375.4
6/13/2005
Envirochem
TKN
1675
0.1
mg/kg
351.3
5/23/2005
Envirochem
Total Nitrogen
1676
0.2
mg/kg
353.3*/351.3
5/19/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
N.C. CERTIFICATION #481
Reviewed By:
17 of 23

1, •
co
0-
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 12
Client Project ID: Almont Shipping
Lab Sample ID: G121-330-2
Lab Project ID: G121-330
Analyte Result
Ammonia
15
Chloride
474
Nitrate
BQL
Phosphorus
132
Sulfate
51.6
TKN
489
Total Nitrogen
490
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Date Collected: 5/17/2005
Date Received: 5/17/2005
Matrix: Soil
RL
Units
Method
Date
Analyst
Analyzed
0.1
mg/kg
350.2
5/24/2005
Envirochem
0.1
mg/kg
SM 4500CI-B
6/17/2005
Envirochem
0.27
mg/kg
353.3
6/9/2005
Envirochem
0.5
mg/kg
365.2
5/20/2005
Envirochem
5
mg/kg
375.4
6/13/2005
Envirochem
0.1
mg/kg
351.3
5/23/2005
Envirochem
0.2
mg/kg
353.3*/351.3
5/19/2005
Envirochem
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
N.C. CERTIFICATION #481
Reviewed By:
18 of 23

L�
\q
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 13 Date Collected: 5/17/2006
Client Project ID: Almont Shipping Date Received: 5/17/2005
Lab Sample ID: G121-330-3 Matrix: Soil
J
Lab Project ID: G121-330
Analyse
Result
RL
Ammonia
359
0.1
Chloride
327
0.1
Nitrate
348
0.27
Phosphorus
8.19
0.5
Sulfate
194
5
TKN
3415
0.1
Total Nitrogen
3422
0.2
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
Units
Method
Date
Analyst
Analyzed
mg/kg
350.2
5/24/2005
Envirochem
mg/kg
SM 4500C1-B
6/17/2005
Envirochem
mg/kg
353.3
6/9/2005
Envirochem
mg/kg
365.2
5/20/2005
Envirochem
mg/kg
375.4
6/13/2005
Envirochem
mg/kg
351.3
5/23/2005
Envirochem
mg/kg
353.3*/351.3
5/19/2005
Envirochem
N.C. CERTIFICATION #481
Reviewed By:
19 of 23

A
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 14 Date Collected: 5/17/2005
Client Project ID: Almont Shipping Date Received: 5/17/2005
Lab Sample ID: G121-330-4 Matrix: Soil
Lab Project ID: G121-330
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
108
0.1
mg/kg
350.2
5/24/2005
Envirochem
Chloride
669
0.1
mg/kg
SM 4500CI-B
6/17/2005
Envirochem
Nitrate
1.14
0.27
mg/kg
353.3
6/9/2005
Envirochem
Phosphorus
204
0.5
mg/kg
365.2
5/20/2005
Envirochem
Sulfate
165
5
mg/kg
375.4
6/13/2005
Envirochem
TKN
364
0.1
mg/kg
351.3
5/23/2005
Envirochem
Total Nitrogen
365
0.2
mg/kg
353.3*/351.3
5/19/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
N.C. CERTIFICATION #481
Reviewed By:
20 of 23

c•
10
(0
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 15 Date Collected: 5/17/2005
Client Project ID: Almont Shipping Date Received: 5/17/2006
Lab Sample ID: G121-330-5 Matrix: Soil
Lab Project ID: G121-330
Analyte
Result
RL
Ammonia
213
0A
Chloride
84.7
0.1
Nitrate
13.5
0.27
Phosphorus
149
0.5
Sulfate
186
5
TKN
508
0.1
Total Nitrogen
531
0.2
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
Samples reported on dry weight basis.
MDL and PQL adjusted for dry weights.
Units
Method
Date
Analyst
Analyzed
mg/kg
350.2
5/24/2005
Envirochem
mg/kg
SM 4500CI-B
6/17/2005
Envirochem
mg/kg
353.3
6/9/2005
Envirochem
mg/kg
365.2
5/20/2005
Envirochem
mg/kg
375.4
6/13/2005
Envirochem
mg/kg
351.3
5/23/2005
Envirochem
mg/kg
353.3"/351.3
5/19/2005
Envirochem
N.C. CERTIFICATION #481
Reviewed By:
21 of 23

PARADIGM ANALYTICAL LABORATORIES, INC.
co List of Reporting Abbreviations
and Data Qualifiers
16
B = Compound also detected in batch blank
BQL = Below Quantitation Limit
DF = Dilution Factor
Dup = Duplicate
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL = Reporting Limit
RPD = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% solids = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
M134.011404.1
N.C. CERTIFICATION #481 22 of 23

*Ad
V
PARADIGM ANALYTICAL LABORATORIES, INC.
5500 Business Drive, Wilmington, NC 28405
Phone: [phone] FAX: [phone]
Chain -of Custody Record & Analytical Request
M
N
cOC# 46906 14
Page Of
Client: P3gRhA 1 A5JUU Project ID: AIV-�
ShIPRO Date:
Address: Contact: lbrnaround:
Address: Phone: Job Number:
I_U._+o W. Tiow• P_tl_ Nnmher! Invoice To:
oil
•_ 1
1
000
0
NFA411
INMAN
AF41
AMEN
�..■.PAJrl
NA
ISMORONIn
-�
MOEN
E
ff-IMUMIN
0000
IN,
Mid
k
I
I d
6 W-, A,
FAV
64P
m
rid,
104
1
FWAINE
:rYF..1�r1!
nT��rl�i
WAa
C
NC SC Other
SEE REVERSE FOR
—TERMS AND CONDMONS
alit

PARADIGM ANALYTICAL LABORATORIES, INC.
Mr. Gary Babb
Babb & Associate
P.O. Box 37697
Raleigh NC 27627
ReportNumber: G121-333
Client Project: Almont Shipping
Dear Mr. Babb:
Enclosed are the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call Paradigm at [phone]. We will be happy to answer any questions or
concerns which you may have.
Thank you for using Paradigm Analytical Labs for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely,
Paradigm Analytical Laboratories, Inc.
Lao tor; erector
J. Patrick Weaver
0
ate
N.C. CERTIFICATION #481
1 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 82606
�. Client Sample ID: MW-1 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 7:00
Lab Sample ID: G121-333-1A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UG/L
Factor
Analyzed
Acetone
BQL
25.0
1
5/26/05
Benzene
BQL
1.00
1
5126/05
Bromobenzene
BQL
1.00
1
5/26/05
Bromochloromethane
BQL
1.00
1
5/26/05
Bromodichloromethane
BQL
1.00
1
5/26/05
Bromoform
BQL
1.00
1
5/26/05
Bromomethane
BQL
1.00
1
5/26/05
2-Butanone
BQL
25.0
1
5126/05
n-Butylbenzene
BQL
1.00
1
5/26/05
sec-Butylbenzene
4.88
1.00
1
5/26/05
tert-Butylbenzene
BQL
1.00
1
5/26/05
Carbon disulfide
BQL
1.00
1
5/26/05
Carbon tetrachloride
BQL
1.00
1
5/26/05
Chlorobenzene
BQL
1.00
1
5/26/05
Chloroethane
BQL
1.00
1
5/26/05
Chloroform
BQL
1.00
1
5/26/05
Chloromethane
BQL
1.00
1
5/26/05
2-Chlorotoluene
BQL
1.00
1
5/26/05
4-Chlorotoluene
BQL
1.00
1
5/26105
Dibromochloromethane
BQL
1.00
1
5/26/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/26/05
Dibromomethane
BQL
1.00
1
5/26/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/26/05
1,2-Dichlorobenzene
BQL
1.00
1
5/26/05
1,3-Dichlorobenzene
BQL
1.00
1
5/26/05
1,4-Dichlorobenzene
BQL
1.00
1
5/26/05
trans-1,4-Dichioro-2-butene
BQL
5.00
1
5/26/05
1,1-Dichloroethane
BQL
1.00
1
5126/05
1,1-Dichloroethene
BQL
1.00
1
5/26/05
1,2-Dichloroethane
BQL
1.00
1
5/26/05
cis-1,2-Dichloroethene
BQL
1.00
1
5/26/05
trans- 1,2-dichloroethene
BQL
1.00
1
5/26/05
1,2-Dichloropropane
BQL
1.00
1
5/26/05
1,3-Dichloropropane
BQL
1.00
1
5/26/05
2,2-Dichloropropane
BQL
1.00
1
5/26/05
1,1-Dichloropropene
BQL
1.00
1
5/26/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/26/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/26/05
Dichiorodifluoromethane
BQL
5.00
1
5126/05
ether (DIPE)
BQL
1.00
1
5/26/05
iDiisopropyl
Etylbenzene
BQL
1.00
1
5/26/05
Hexachlorobutadiene
BQL
1.00
1
5126/05
Page 1 of 2 GCMS LIMS Q.82 xx s, of 77
N.C. CERTIFICATION IFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
COClient Sample ID: MW-1 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 7:00
Lab Sample ID: G121-333-1A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UGIL
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/26/05
lodomethane
BQL
1.00
1
5126/05
Isopropyibenzene
BQL
1.00
1
5/26/05
4-Isopropyltoluene
140
10.0
10
5/27/05
Methylene chloride
BQL
5.00
1
5/26105
4-Methyl-2-pentanone
BQL
5.00
1
5/26105
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/26/05
Naphthalene
BQL
1.00
1
5/26/05
n-Propyl benzene
BQL
1.00
1
5/26/05
Styrene
BQL
1.00
1
5/26/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/26/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/26/05
Tetrachloroethene
2.17
1.00
1
5/26/05
Toluene
BQL
1.00
1
5/26/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5/26/05
1,2,4-Trichlorobenzene
BQL
1.00
1
6/26/05
Trichloroethene
5.62
1.00
1
5/26/05
1,1,1-Trichloroethane
BQL
1.00
1
5/26/05
1,1,2-Trichloroethane
BQL
1.00
1
5/26/05
Trichlorofluoromethane
BQL
1.00
1
5/26/05
1,2,3-Trichloropropane
BQL
1.00
1
5/26/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/26/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/26/05
Vinyl chloride
BQL
1.00
1
5/26/05
m-,p-Xylene
BQL
2.00
1
5/26/05
o-Xylene
BQL
1.00
1
5/26/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
9.96
100
1,2-Dichloroethane-d4
10
9.48
95
Toluene-d8
10
10.1
101
Comments:
Flags:
BQL = Below Quantitation Limits.
(•
Reviewed By:
Pale 2 of 2 GCMS LIMS vz.62 xl
N.C. CER I IFICATION #481 Of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
((�� by GCMS 8260E
` * Client Sample ID: MW-2 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 7:20
Lab Sample ID: G121-333-213 Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UGIL
Factor
Analyzed
Acetone
BQL
25.0
1
5/27/05
Benzene
BQL
1.00
1
5/27/05
Bromobenzene
BQL
1.00
1
5/27/05
Bromochloromethane
BQL
1.00
1
5127/05
Bromodichloromethane
BQL
1.00
1
5/27/05
Bromoform
BQL
1.00
1
5/27/05
Bromomethane
BQL
1.00
1
5/27/05
2-Butanone
BQL
25.0
1
5/27/05
n-Butylbenzene
BQL
1.00
1
5/27/05
sec-Butylbenzene
BQL
1.00
1
5/27105
tert-Butylbenzene
BQL
1.00
1
5/27/05
Carbon disulfide
BQL
1.00
1
5/27/05
Carbon tetrachloride
BQL
1.00
1
5/27105
Chlorobenzene
BQL
1.00
1
5/27/05
Chloroethane
�. Chloroform
BQL
BQL
1.00
1.00
1
1
5/27/05
5/27/05
Chloromethane
BQL
1.00
1
5/27/05
2-Chlorotoluene
BQL
1.00
1
5/27/05
4-Chlorotoluene
BQL
1.00
1
5/27/05
Dibromochloromethane
BQL
1.00
1
5/27/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/27/05
Dibromomethane
BQL
1.00
1
5/27/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/27/05
1,2-Dichlorobenzene
BQL
1.00
1
5/27/05
1,3-Dichlorobenzene
BQL
1.00
1
5/27/05
1,4-Dichlorobenzene
BQL
1.00
1
5/27/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/27/05
1,1-Dichloroethane
BQL
1.00
1
5/27/05
1,1-Dichloroethene
BQL
1.00
1
5/27/05
1,2-Dichloroethane
BQL
1.00
1
5/27/05
cis-1,2-Dichloroethene
BQL
1.00
1
5/27105
trans-1,2-dichloroethene
BQL
1.00
1
5/27/05
1,2-Dichloropropane
BQL
1.00
1
5/27/05
1,3-Dichloropropane
BQL
1.00
1
5/27/05
2,2-Dichloropropane
BQL
1.00
1
5/27/05
1,1-Dichloropropene
BQL
1.00
1
5/27105
cis-1,3-Dichloropropene
BQL
1.00
1
5127/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/27/05
Dichlorodifluoromethane
BQL
5.00
1
5/27/05
Diisopropyl ether (DIPE)
BQL
1.00
1
5/27/05
Ethylbenzene
BQL
1.00
1
5/27/05
Hexachlorobutadiene
BQL
1.00
1
5/27/05
N.C. CER-FICATION #481 GCMS_LIM4-y282.1
of
77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
CO Client Sample ID: MW-2 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 7:20
Lab Sample ID: G121-333-213 Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/27/05
lodomethane
BQL
1.00
1
5/27/05
Isopropylbenzene
BQL
1.00
1
5/27/05
4-Isopropyitoluene
BQL
1.00
1
5/27/05
Methylene chloride
BQL
5.00
1
5/27/05
4-Methyl-2-pentanone
BQL
5.00
1
5/27/05
Methyl -tent -butyl ether (MTBE)
BQL
1.00
1
5/27/05
Naphthalene
45.2
5.00
5
5/31/05
n-Propyl benzene
BQL
1.00
1
5/27/05
Styrene
BQL
1.00
1
5/27/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/27/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/27/05
Tetrachloroethene
BQL
1.00
11
5/27/05
Toluene
BQL
1.00
1
5/27/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5/27/05
C• 1,2,4-Trichlorobenzene
BQL
1.00
1
5/27/05
Trichloroethene
BQL
1.00
1
5/27/05
1,1,1-Trichloroethane
BQL
1.00
1
5/27/05
1,1,2-Trichloroethane
BQL
1.00
1
5/27/05
Trichlorofluoromethane
BQL
1.00
1
5/27/05
1,2,3-Trichloropropane
BQL
1.00
1
5127/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/27/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5127/05
Vinyl chloride
BQL
1.00
1
5/27/05
m-,p-Xylene
BQL
2.00
1
5/27/05
o-Xylene
BQL
1.00
1
5127/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
9.86
99
1,2-Dichloroethane-d4
10
10.4
104
Toluene-d8
10
10
100
Comments:
Flags:
BQL = Below Quantitation Limits.
,.
Reviewed By: 7-ti/'
Pa 2 Of 2 GCMS_LIMS v2,62.x1
N.C. CER 1 IFICATION #481 Of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
CoClient Sample ID: MW-3 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 7:40
Lab Sample ID: G121-333-313 Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UGIL
Factor
Analyzed
Acetone
BQL
25.0
1
5/27/05
Benzene
BQL
1.00
1
5/27/05
Bromobenzene
BQL
1.00
1
5/27/05
Bromochloromethane
BQL
1.00
1
5/27/05
Bromodichioromethane
BQL
1.00
1
5/27/05
Bromoform
BQL
1.00
1
5/27/05
Bromomethane
BQL
1.00
1
5/27105
2-Butanone
BQL
25.0
1
5/27105
n-Butylbenzene
BQL
1.00
1
5/27/05
sec-Butylbenzene
BQL
1.00
1
5/27/05
tert-Butylbenzene
BQL
1.00
1
5/27/05
Carbon disulfide
BQL
1.00
1
5/27/05
Carbon tetrachloride
BQL
1.00
1
5/27/05
Chlorobenzene
BQL
1.00
1
5/27/05
Chloroethane
BQL
1.00
1
5/27/05
�• Chloroform
BQL
1.00
1
5/27/05
Chloromethane
BQL
1.00
1
5/27/05
2-Chlorotoluene
BQL
1.00
1
5/27/05
4-Chlorotoluene
BQL
1.00
1
5/27/05
Dibromochloromethane
BQL
1.00
1
5/27105
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/27/05
Dibromomethane
BQL
1.00
1
5/27/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/27/05
1,2-Dichlorobenzene
BQL
1.00
1
5/27/05
1,3-Dichlorobenzene
BQL
1.00
1
5/27/05
1,4-Dichlorobenzene
BQL
1.00
1
6/27/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5127105
1,1-Dichloroethane
BQL
1.00
1
5/27/05
1,1-Dichloroethene
BQL
1.00
1
5/27/05
1,2-Dichloroethane
BQL
1.00
1
5/27/05
cis-1,2-Dichloroethene
BQL
1.00
1
5/27/05
trans-1,2-dichloroethene
BQL
1.00
1
5/27/05
1,2-Dichloropropane
BQL
1.00
1
5/27/05
1,3-Dichloropropane
BQL
1.00
1
5/27/05
2,2-Dichloropropane
BQL
1.00
1
5/27105
1,1-Dichioropropene
BQL
1.00
1
5/27/05
cis-1,3-Dichioropropene
BQL
1.00
1
5/27/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/27/05
Dichlorodifluoromethane
BQL
5.00
1
5/27/05
Diisopropyl ether (DIPE)
BQL
1.00
1
5/27/05
Ethylbenzene
BQL
1.00
1
5/27/05
Hexachlorobutadiene
BQL
1.00
1
5/27105
N.C. CEM ICATION #481 ccMS_LIMSy2.62.x1F, of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
(*Client Sample ID: MW-3 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 7:40
Lab Sample ID: G121-333-313 Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG1L
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/27/05
lodomethane
BQL
1.00
1
5/27/05
Isopropylbenzene
BQL
1.00
1
5/27/05
4-isopropyitoluene
BQL
1.00
1
5/27/05
Methylene chloride
BQL
5.00
1
5/27/05
4-Methyl-2-pentanone
BQL
5.00
1
5/27/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/27/05
Naphthalene
BQL
1.00
1
5/27/05
n-Propyl benzene
BQL
1.00
1
5/27/05
Styrene
BQL
1.00
1
5/27/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/27/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/27/05
Tetrachloroethene
BQL
1.00
1
5/27/05
Toluene
BQL
1.00
1
5/27/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5/27/05
�.1,2,4-Trichlorobenzene
BQL
1.00
1
5/27/05
Trichloroethene
BQL
1.00
1
5/27105
1,1,1-Trichloroethane
BQL
1.00
1
5/27/05
1,1,2-Trichloroethane
BQL
1.00
1
5/27/05
Trichlorofluoromethane
BQL
1.00
1
5/27/05
1,2,3-Trichloropropane
BQL
1.00
1
5/27/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/27/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/27/05
Vinyl chloride
BQL
1.00
1
5127/05
m-,p-Xylene
BQL
2.00
1
5/27/05
o-Xylene
BQL
1.00
1
5/27/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
10
100
1,2-Dichloroethane-d4
10
10.6
106
Toluene-d8
10
10
100
Comments:
Flags:
BQL = Below Quantitation Limits.
Reviewed By:
18
N.C. CER a 2 O' TION #481 GCMS LIMS N2.62.x� of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
•Client Sample ID: MW-4 Analyzed By: JTF
Client Project ID: Aimont Shipping Date Collected: 5/25/05 8:00
Lab Sample ID: G121-333-4A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UGIL
Factor
Analyzed
Acetone
BQL
200
8
5/31/05
Benzene
BQL
8.00
8
5/31/05
Bromobenzene
BQL
8.00
8
5/31/05
Bromochioromethane
BQL
8.00
8
5131/05
Bromodichloromethane
BQL
8.00
8
5/31/05
Bromoform
BQL
8.00
8
5/31/05
Bromomethane
BQL
8.00
8
5/31/05
2-Butanone
BQL
200
8
5/31/05
n-Butylbenzene
BQL
8.00
8
5131105
sec-Butylbenzene
BQL
8.00
8
5/31/05
tert-Butylbenzene
BQL
8.00
8
5131/05
Carbon disulfide
BQL
8.00
8
5/31/05
Carbon tetrachloride
BQL
8.00
8
5/31/05
Chlorobenzene
BQL
8.00
8
5/31/05
Chloroethane
BQL
8.00
8
5/31/05
Ice Chloroform
BQL
8.00
8
5/31/05
Chloromethane
BQL
8.00
8
5/31/05
2-Chlorotoluene
BQL
8.00
8
5/31/05
4-Chlorotoluene
BQL
8.00
8
5/31/05
Dibromochloromethane
BQL
8.00
8
6/31/05
1,2-Dibromo-3-chloropropane
BQL
40.0
8
5/31/05
Dibromomethane
BQL
8.00
8
5/31/05
1,2-Dibromoethane (EDB)
BQL
8.00
8
5/31/05
1,2-Dichlorobenzene
BQL
8.00
8
5/31/05
1,3-Dichlorobenzene
BQL
8.00
8
5/31/05
1,4-Dichlorobenzene
BQL
8.00
8
5/31/05
trans-1,4-Dichloro-2-butene
BQL
40.0
8
5/31/05
1,1-Dichloroethane
BQL
8.00
8
5/31/05
1,1-Dichioroethene
BQL
8.00
8
5131/05
1,2-Dichloroethane
BQL
8.00
8
5/31/05
cis-1,2-Dichloroethene
BQL
8.00
8
5/31/05
trans-1,2-dichloroethene
BQL
8.00
8
5/31/05
1,2-Dichloropropane
BQL
8.00
8
5/31/05
1,3-Dichloropropane
BQL
8.00
8
5/31/05
2,2-Dichloropropane
BQL
8.00
8
5/31/05
1,1-Dichloropropene
BQL
8.00
8
5/31/05
cis-1,3-Dichloropropene
BQL
8.00
8
5/31/05
trans-1,3-Dichloropropene
BQL
8.00
8
5/31/05
Dichlorodifluoromethane
BQL
40.0
8
5/31/05
Diisopropyl ether (DIPE)
BQL
8.00
8
5/31/05
Ethylbenzene
BQL
8.00
8
5/31/05
Hexachlorobutadiene
BQL
8.00
8
5/31/05
N.C. CER�FICATION #481 ccMS_LIMS_�I262x1t, of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
C. Client Sample ID: MW-4 by GCMS 8260E Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 8:00
Lab Sample ID: G121-3334A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
40.0
8
5/31/05
lodomethane
BQL
8.00
8
5/31/05
Isopropylbenzene
BQL
8.00
8
5/31/05
4-Isopropyitoluene
BQL
8.00
8
5/31/05
Methylene chloride
BQL
40.0
8
5/31/05
4-Methyl-2-pentanone
BQL
40.0
8
5/31/05
Methyl-tert-butyl ether (MTBE)
BQL
8.00
8
5/31/05
Naphthalene
BQL
8.00
8
5/31/05
n-Propyl benzene
BQL
8.00
8
5/31/05
Styrene
BQL
8.00
8
5/31/05
1,1,1,2-Tetrachloroethane
BQL
8.00
8
5/31/05
1,1,2,2-Tetrachloroethane
BQL
8.00
8
5/31/05
Tetrachloroethene
BQL
8.00
8
5/31/05
Toluene
BQL
8.00
8
5/31/05
1,2,3-Trichlorobenzene
BQL
8.00
8
5/31/05
.1,2,4-Trichlorobenzene
BQL
8.00
8
5/31/05
Trichloroethene
BQL
8.00
8
5/31/05
1,1,1-Trichloroethane
BQL
8.00
8
5131/05
1,1,2-Trichloroethane
BQL
8.00
8
5/31/05
Trichlorofluoromethane
BQL
8.00
8
5131/05
1,2,3-Trichloropropane
BQL
8.00
8
5131/05
1,2,4-Trimethylbenzene
BQL
8.00
8
5/31/05
1,3,5-Trimethylbenzene
BQL
8.00
8
5/31/05
Vinyl chloride
BQL
8.00
8
5/31/05
m-,p-Xylene
BQL
16.0
8
5/31/05
o-Xylene
BQL
8.00
8
5131/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
9.94
99
1,2-Dichloroethane-d4
10
10.4
104
Toluene-d8
10
10.1
101
Comments:
Sample diluted for foaming.
Flags:
BQL = Below Quantitation Limits.
0-
Reviewed By: F-r�V_
N.C. CERTIFI&ION #481 GCMS LIMS v2.62Ai of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8280E
CeClient Sample ID: MW-5 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25105 8:20
Lab Sample ID: G121-333-5A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
Acetone
BQL
25.0
1
5/26/05
Benzene
BQL
1.00
1
5/26/05
Bromobenzene
BQL
1.00
1
5/26/05
Bromochioromethane
BQL
1.00
1
5/26/05
Bromodichloromethane
BQL
1.00
1
5/26/05
Bromoform
BQL
1.00
1
5/26/05
Bromomethane
BQL
1.00
1
5/26/05
2-Butanone
BQL
25.0
1
5/26/05
n-Butylbenzene
BQL
1.00
1
5126/05
sec-Butyibenzene
BQL
1.00
1
5/26/05
tert-Butylbenzene
BQL
1.00
1
5/26/05
Carbon disulfide
BQL
1.00
1
5/26/05
Carbon tetrachloride
BQL
1.00
1
5/26/05
Chlorobenzene
BQL
1.00
1
5/26/05
�•
Chloroethane
Chloroform
BQL
BQL
1.00
1.00
1
1
5/26/05
5/26/05
Chloromethane
BQL
1.00
1
5126/05
2-Chlorotoluene
BQL
1.00
1
5/26/05
4-Chlorotoluene
BQL
1.00
1
5/26/05
Dibromochloromethane
BQL
1.00
1
5/26/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/26/05
Dibromomethane
BQL
1.00
1
5/26/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/26/05
1,2-Dichlorobenzene
BQL
1.00
1
5/26/05
1,3-Dichlorobenzene
BQL
1.00
1
5126/05
1,4-Dichlorobenzene
BQL
1.00
1
5/26/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/26/05
1,1-Dichloroethene
BQL
1.00
1
5/26/05
1,1-Dichloroethene
BQL
1.00
1
5/26105
1,2-Dichloroethane
BQL
1.00
1
5/26/05
cis-1,2-Dichloroethene
BQL
1.00
1
5/26/05
trans-1,2-dichloroethene
BQL
1.00
1
5126/05
1,2-Dichloropropane
BQL
1.00
1
5/26/05
1,3-Dichloropropane
BQL
1.00
1
5/26/05
2,2-Dichloropropane
BQL
1.00
1
5/26/05
1,1-Dichloropropene
BQL
1.00
1
5/26/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/26/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/26/05
Dichlorodifluoromethane
BQL
5.00
1
5/26/05
ether (DIPE)
BQL
1.00
1
5/26/05
\.Dilsopropyl
Etylbenzene
BQL
1.00
1
5/26/05
Hexachlorobutadiene
BQL
1.00
1
5/26/05
N.C. CER%IdalON #481 CMS uMs_va,62.X110 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
Client Sample ID: MW-5 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 8:20
Lab Sample ID: G121-333-5A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/26105
lodomethane
BQL
1.00
1
5/26/05
Isopropylbenzene
BQL
1.00
1
5/26/05
4-Isopropyltoluene
BQL
1.00
1
5/26/05
Methylene chloride
BQL
5.00
1
5/26/05
4-Methyl-2-pentanone
BQL
5.00
1
5/26/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/26/05
Naphthalene
BQL
1.00
1
5/26/05
n-Propyl benzene
BQL
1.00
1
5/26/05
Styrene
BQL
1.00
1
5/26/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/26/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/26/05
Tetrachloroethene
BQL
1.00
1
5/26/05
Toluene
BQL
1.00
1
5/26/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5/26/05
�• 1,2,4-Trichlorobenzene
BQL
1.00
1
5/26/05
Trichloroethene
BQL
1.00
1
5/26105
1,1,1-Trichloroethane
BQL
1.00
1
5/26/05
1,1,2-Trichloroethane
BQL
1.00
1
5/26/05
Trichlorofluoromethane
BQL
1.00
1
5/26/05
1,2,3-Trichloropropane
BQL
1.00
1
5126/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/26/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/26/05
Vinyl chloride
BQL
1.00
1
5/26/05
m-,p-Xylene
BQL
2.00
1
5/26/05
o-Xylene
BQL
1.00
1
5/26/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
10.2
102
1,2-Dichloroethane-d4
10
9.45
95
Toluene-d8
10
10.1
101
Comments:
Flags:
BQL = Below Quantitation Limits.
•
Reviewed By: -_
N.C. CER%fdalON #481 GCMS LIMS_t2.62.1 1 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
Client Sample ID: MW-6 by GCMS 82606 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25105 8:40
Lab Sample ID: G121-333-6A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
Acetone
BQL
25.0
1
5/26/05
Benzene
BQL
1.00
1
5/26/05
Bromobenzene
BQL
1.00
1
5/26/05
Bromochloromethane
BQL
1.00
1
5/26/05
Bromodichioromethane
BQL
1.00
1
5/26/05
Bromoform
BQL
1.00
1
5126/05
Bromomethane
BQL
1.00
1
5/26/05
2-Butanone
BQL
25.0
1
5/26/05
n-Butylbenzene
BQL
1.00
1
5/26/05
sec-Butylbenzene
BQL
1.00
1
5/26/05
tert-Butylbenzene
BQL
1.00
1
5/26/05
Carbon disulfide
BQL
1.00
1
5/26/05
Carbon tetrachloride
BQL
1.00
1
5/26/05
Chlorobenzene
BQL
1.00
1
5/26/05
Chloroethane
BQL
1.00
1
5/26/05
Chloroform
BQL
1.00
1
5/26/05
Chloromethane
BQL
1.00
1
5126/05
2-Chlorotoluene
BQL
1.00
1
5/26/05
4-Chlorotoluene
BQL
1.00
1
5/26/05
Dibromochioromethane
BQL
1.00
1
5/26/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/26/05
Dibromomethane
BQL
1.00
1
5/26/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/26/05
1,2-Dichlorobenzene
BQL
1.00
1
5/26/05
1,3-Dichlorobenzene
BQL
1.00
1
5/26/05
1,4-Dichlorobenzene
BQL
1.00
1
5/26/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/26/05
1,1-Dichloroethane
BQL
1.00
1
5/26/05
1,1-Dichloroethene
BQL
1.00
1
5/26/05
1,2-Dichloroethane
BQL
1.00
1
5/26/05
cis-1,2-Dichloroethene
BQL
1.00
1
5/26/05
trans-1,2-dichloroethene
BQL
1.00
1
5/26105
1,2-Dichloropropane
BQL
1.00
1
5/26/05
1,3-Dichloropropane
BQL
1.00
1
5/26/05
2,2-Dichloropropane
BQL
1.00
1
5126/05
1,1-Dichloropropene
BQL
1.00
1
5126/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/26/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/26105
Dichlorodifluoromethane
BQL
5.00
1
5/26/05
Diisopropyl ether (DIPE)
BQL
1.00
1
5/26/05
Ethylbenzene
BQL
1.00
1
5/26/05
Hexachlorobutadiene
BQL
1.00
1
5/26/05
Pa e 1 of 2 GCM9 UMS v2.62.x1
N.C. CERTIFICATION #481 12 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
Client Sample ID: MW-6 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 8:40
Lab Sample ID: G121-333-6A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/26/05
lodomethane
BQL
1.00
1
5/26/05
isopropylbenzene
BQL
1.00
1
5/26/05
4-Isopropyltoluene
BQL
1.00
1
5/26/05
Methylene chloride
BQL
5.00
1
5/26/05
4-Methyl-2-pentanone
BQL
5.00
1
5/26/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/26/05
Naphthalene
BQL
1.00
1
5/26/05
n-Propyl benzene
BQL
1.00
1
5/26/05
Styrene
BQL
1.00
1
5/26/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/26/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/26/05
Tetrachloroethene
BQL
1.00
1
5/26/05
Toluene
BQL
1.00
1
5/26/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5/26/05
.1,2,4-Trichlorobenzene
BQL
1.00
1
5/26/05
Trichloroethene
BQL
1.00
1
5/26/05
1, 1, 1 -Trichloroethane
BQL
1.00
1
5/26/05
1,1,2-Trichloroethane
BQL
1.00
1
5/26/05
Trichlorofluoromethane
BQL
1.00
1
5/26/05
1,2,3-Trichloropropane
BQL
1.00
1
5/26/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/26/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/26/05
Vinyl chloride
BQL
1.00
1
5/26/05
m-,p-Xylene
BQL
2.00
1
5/26/05
o-Xylene
BQL
1.00
1
5/26/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
10
100
1,2-Dichloroethane-d4
10
9.4
94
Toluene-d8
10
10.1
101
Comments:
Flags:
BQL = Below Quantitation Limits.
0
Reviewed By: End
Pa e 2 of 2 GCM8 LIMB v2.62A 3 of 77
N.C. CERTIFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
Ce Client Sample ID: MW-7 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 9:00
Lab Sample ID: G121-333-7A Date Received: 5125/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
Acetone
BQL
25.0
1
5/26/05
Benzene
BQL
1.00
1
5/26105
Bromobenzene
BQL
1.00
1
5/26/05
Bromochloromethane
BQL
1.00
1
5/26/05
Bromodichloromethane
BQL
1.00
1
5/26/05
Bromoform
BQL
1.00
1
5/26/05
Bromomethane
BQL
1.00
1
5/26/05
2-Butanone
BQL
25.0
1
5/26/05
n-Butylbenzene
BQL
1.00
1
5/26/05
sec-Butylbenzene
BQL
1.00
1
5/26/05
tert-Butyibenzene
BQL
1.00
1
5/26/05
Carbon disulfide
BQL
1.00
1
5/26/05
Carbon tetrachloride
BQL
1.00
1
5/26/05
Chlorobenzene
BQL
1.00
1
5/26/05
Chloroethane
�• Chloroform
BQL
BQL
1.00
1.00
1
1
5/26/05
5/26/05
` Chloromethane
BQL
1.00
1
5/26/05
2-Chlorotoluene
BQL
1.00
1
5/26/05
4-Chlorotoluene
BQL
1.00
1
5/26/05
Dibromochloromethane
BQL
1.00
1
5/26/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/26/06
Dibromomethane
BQL
1.00
1
5/26/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/26/05
1,2-Dichlorobenzene
BQL
1.00
1
5/26/05
1,3-Dichlorobenzene
BQL
1.00
1
5/26/05
1,4-Dichlorobenzene
BQL
1.00
1
5/26/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/26/05
1,1-Dichloroethane
BQL
1.00
1
5/26/05
1,1-Dichloroethene
BQL
1.00
1
5/26/05
1,2-Dichloroethane
BQL
1.00
1
5126/05
cis-1,2-Dichloroethene
BQL
1.00
1
5/26/05
trans-1,2-dichloroethene
BQL
1.00
1
5/26/05
1,2-Dichloropropane
BQL
1.00
1
5/26/06
1,3-Dichloropropane
BQL
1.00
1
5126/05
2,2-Dichloropropane
BQL
1.00
1
5/26/05
1,1-Dichloropropene
BQL
1.00
1
5/26/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/26/05
trans-1,3-Dichloropropene
BQL
1.00
1
5126/05
Dichlorodifluoromethane
BQL
5.00
1
5/26/05
ether (DIPE)
BQL
1.00
1
5126/05
.Diisopropyl
Ethylbenzene
BQL
1.00
1
5/26/05
Hexachlorobutadiene
BQL
1.00
1
5/26/05
N.C. CERTIFICATION #481 �Ms_LIM9 V1.824 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260B
Client Sample ID: MW-7 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 9:00
Lab Sample ID: G121-333-7A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UGIL
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/26/05
lodomethane
BQL
1.00
1
5/26/05
Isopropylbenzene
BQL
1.00
1
5/26/05
4-Isopropyltoluene
BQL
1.00
1
5/26/05
Methylene chloride
BQL
5.00
1
5/26/05
4-Methyl-2-pentanone
BQL
5.00
1
5/26/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/26/05
Naphthalene
BQL
1.00
1
5/26/05
n-Propyl benzene
BQL
1.00
1
5/26/05
Styrene
BQL
1.00
1
5/26/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/26/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/26/05
Tetrachloroethene
BQL
1.00
1
5/26/05
Toluene
BQL
1.00
1
5/26/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5/26/05
.1,2,4-Trichlorobenzene
BQL
1.00
1
5/26/05
Trichloroethene
BQL
1.00
1
5/26/05
1,1,1-Trichloroethane
BQL
1.00
1
5/26/05
1,1,2-Trichloroethane
BQL
1.00
1
5/26/05
Trichlorofluoromethane
BQL
1.00
1
5/26/05
1,2,3-Trichloropropane
BQL
1,00
1
5/26/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/26/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/26105
Vinyl chloride
BQL
1.00
1
5126/05
m-,p-Xylene
BQL
2.00
1
5/26/05
o-Xylene
BQL
1.00
1
5/26/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
10.2
102
1,2-Dichloroethane-d4
10
9.41
94
Toluene-d8
10
10.2
102
Comments:
Flags:
BQL = Below Quantitation Limits.
10
Reviewed By: ,moo
N.C. CEWWaION #481 GCMS uMs Q.e2A15 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Yolatiles
by GCMS 8260B
�• Client Sample ID: MW-8 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 9:20
Lab Sample ID: G121-333-8A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UG/L
Factor
Analyzed
Acetone
BQL
25.0
1
5/27/05
Benzene
BQL
1.00
1
5/27/05
Bromobenzene
BQL
1.00
1
5/27/05
Bromochloromethane
BQL
1.00
1
5/27/05
Bromodichloromethane
BQL
1.00
1
5/27/05
Bromoform
BQL
1.00
1
5/27/05
Bromomethane
BQL
1.00
1
5/27/05
2-Butanone
BQL
25.0
1
5/27/05
n-Butylbenzene
1.12
1.00
1
5/27/05
sec-Butylbenzene
3.31
1.00
1
5/27/05
tert-Butylbenzene
BQL
1.00
1
5/27/05
Carbon disulfide
BQL
1.00
1
5/27/05
Carbon tetrachloride
BQL
1.00
1
5/27/05
Chlorobenzene
BQL
1.00
1
5/27/05
Chioroethane
Chloroform
BQL
BQL
1.00
1.00
1
1
5/27/05
5/27/05
Chloromethane
BQL
1.00
1
5/27/05
2-Chlorotoluene
BQL
1.00
1
5/27/05
4-Chlorotoluene
BQL
1.00
1
5/27/05
Dibromochloromethane
BQL
1.00
1
5/27/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/27/05
Dibromomethane
BQL
1.00
1
5/27/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/27/05
1,2-Dichlorobenzene
BQL
1.00
1
5127/05
1,3-Dichlorobenzene
BQL
1.00
1
5/27/05
1,4-Dichlorobenzene
BQL
1.00
1
5/27/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/27/05
1,1-Dichloroethane
BQL
1.00
1
5127/05
1,1-Dichloroethene
BQL
1.00
1
5/27/05
1,2-Dichloroethane
BQL
1.00
1
5/27/05
cis-1,2-Dichloroethene
BQL
1.00
1
5127/05
trans-1,2-dichloroethene
BQL
1.00
1
5/27/05
1,2-Dichloropropane
BQL
1.00
1
5/27/05
1,3-Dichloropropane
BQL
1.00
1
5/27/05
2,2-Dichloropropane
BQL
1.00
1
5/27/05
1,1-Dichloropropene
BQL
1.00
1
5/27/05
cis-1,3-Dichloropropene
BQL
1.00
1
5127/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/27/05
Dichlorodifluoromethane
BQL
5.00
1
5/27/05
ether (DIPE)
BQL
1.00
1
5/27/05
•Diisopropyl
Etylbenzene
BQL
1.00
1
5/27/05
Hexachlorobutadiene
BQL
1.00
1
5/27/05
N.C. CERW (CATION #481 GCMS LIMS_J2.82x16 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260B
aClient Sample ID: MW-8 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 9:20
Lab Sample ID: G121-333-8A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UGIL
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/27/05
lodomethane
BQL
1.00
1
5/27/05
Isopropylbenzene
4.07
1.00
1
5/27/05
4-Isopropyltoluene
1.21
1.00
1
5/27/05
Methylene chloride
BQL
5.00
1
5/27/05
4-Methyl-2-pentanone
BQL
5.00
1
5/27/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/27/05
Naphthalene
BQL
1.00
1
5/27/05
n-Propyl benzene
3.02
1.00
1
5/27/05
Styrene
BQL
1.00
1
5/27/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/27/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/27/05
Tetrachloroethene
BQL
1.00
1
5/27/05
Toluene
BQL
1.00
1
5/27/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5/27/05
1,2,4-Trichlorobenzene
BQL
1.00
1
5/27/05
Trichloroethane
BQL
1.00
1
5/27/05
1,1,1-Trichloroethane
BQL
1.00
1
5127/05
1,1,2-Trichloroethane
BQL
1.00
1
6/27/05
Trichlorofluoromethane
BQL
1.00
1
5/27/05
1,2,3-Trichloropropane
BQL
1.00
1
5/27/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5127/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5127105
Vinyl chloride
BQL
1.00
1
5/27/05
m-,p-Xylene
BQL
2.00
1
5/27/05
o-Xylene
BQL
1.00
1
5/27/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
10.2
102
1,2-Dichloroethane-d4
10
9.81
98
Toluene-d8
10
10.1
101
Comments:
Flags:
BQL = Below Quantitation Limits.
Reviewed By: V-.,o
N.C. CERWFICATION #481 GCMS LIMS vz62.x1�7 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 82606
�• Client Sample ID: MW-9
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 5/25/06 9:40
Lab Sample ID: G121-333-9A
Date Received: 5/25/05
Lab Project ID: G121-333
Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
Acetone
BQL
25.0
1
5/26/05
Benzene
BQL
1.00
1
5/26/05
Bromobenzene
BQL
1.00
1
5/26/05
Bromochloromethane
BQL
1.00
1
5/26/05
Bromodichloromethane
BQL
1.00
1
5/26/05
Bromoform
BQL
1.00
1
5/26/05
Bromomethane
BQL
1.00
1
5/26/05
2-Butanone
BQL
25.0
1
5/26/05
n-Butylbenzene
BQL
1.00
1
5/26/05
sec-Butylbenzene
BQL
1.00
1
5/26/05
tert-Butylbenzene
BQL
1.00
1
5/26/05
Carbon disulfide
BQL
1.00
1
5126/05
Carbon tetrachloride
BQL
1.00
1
5/26/05
Chiorobenzene
BQL
1.00
1
5/26/05
Chloroethane
BQL
1.00
1
5/26/05
Chloroform
BQL
1.00
1
5/26/05
Chloromethane
BQL
1.00
1
5/26/05
2-Chlorotoluene
BQL
1.00
1
5/26/05
4-Chlorotoluene
BQL
1.00
1
5/26/06
Dibromochloromethane
BQL
1.00
1
5/26/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/26/05
Dibromomethane
BQL
1.00
1
5/26/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/26/05
1,2-Dichlorobenzene
BQL
1.00
1
5/26/05
1,3-Dichlorobenzene
BQL
1.00
1
5/26/05
1,4-Dichlorobenzene
BQL
1.00
1
5/26/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/26/05
1,1-Dichloroethane
BQL
1.00
1
5126/05
1,1-Dichloroethene
BQL
1.00
1
5/26/05
1,2-Dichloroethane
BQL
1.00
1
5/26/05
cis-1,2-Dichloroethene
BQL
1.00
1
5/26/05
trans- 1,2-dichloroethene
BQL
1.00
1
5/26/05
1,2-Dichloropropane
BQL
1.00
1
5126/05
1,3-Dichloropropane
BQL
1.00
1
5/26/05
2,2-Dichloropropane
BQL
1.00
1
5/26/05
1,1-Dichloropropene
BQL
1.00
1
5/26/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/26/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/26/05
Dichlorodifluoromethane
BQL
5.00
1
5/26/05
Diisopropyl ether (DIPE)
BQL
1.00
1
5/26/05
Ethylbenzene
BQL
1.00
1
5/26/05
Hexachlorobutadiene
BQL
1.00
1
5/26/05
N.C. CER%Ida[ON #481 GCMS LIMB v2.62.x118 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260B
ceClient Sample ID: MW-9 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 9:40
Lab Sample ID: G121-333-9A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UGIL
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/26/05
lodomethane
BQL
1.00
1
5126/05
Isopropylbenzene
BQL
1.00
1
5/26/05
4-Isopropyltoluene
BQL
1.00
1
5/26/05
Methylene chloride
BQL
5.00
1
5/26/05
4-Methyl-2-pentanone
BQL
5.00
1
5/26/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/26/05
Naphthalene
BQL
1.00
1
5/26/05
n-Propyl benzene
BQL
1.00
1
5/26/05
Styrene
BQL
1.00
1
5/26/05
1, 1, 1,2-Tetrachloroethane
BQL
1.00
1
5/26/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/26/05
Tetrachloroethene
BQL
1.00
1
5/26/05
Toluene
BQL
1.00
1
5/26/05
1,2,3-Trichiorobenzene
BQL
1.00
1
5/26/05
• 1,2,4-Trichlorobenzene
BQL
1.00
1
5/26/05
Trichloroethene
BQL
1.00
1
5/26/05
1, 1, 1 -Trichloroethane
BQL
1.00
1
5/26/05
1,1,2-Trichloroethane
BQL
1.00
1
5/26/05
Trichiorofluoromethane
BQL
1.00
1
5/26/05
1,2,3-Trichloropropane
BQL
1.00
1
5/26/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/26/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/26/05
Vinyl chloride
BQL
1.00
1
5126/05
m-,p-Xylene
BQL
2.00
1
5/26/05
o-Xylene
BQL
1.00
1
5/26/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
9.97
100
1,2-Dichloroethane-d4
10
9.32
93
Toluene-d8
10
10.1
101
Comments:
Flags:
BQL = Below Quantitation Limits.
Reviewed By:
N.C. CEKWdalON #481 GCMS_LIMS_V2.62.x119 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
coClient Sample ID: MW-10
Client Project ID: Almont Shipping
Lab Sample ID: G121-333-10C
Lab Project ID: G121-333
Results for Volatiles
by GCMS 8260E
Analyzed By: JTF
Date Collected: 5/25/0510:00
Date Received: 5125/05
Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UG/L
Factor
Analyzed
Acetone
BQL
200
8
5/31/05
Benzene
BQL
8.00
8
5131/05
Bromobenzene
BQL
8.00
8
5/31/05
Bromochloromethane
BQL
8.00
8
5/31/05
Bromodichloromethane
BQL
8.00
8
5/31/05
Bromoform
BQL
8.00
8
5/31/05
Bromomethane
BQL
8.00
8
5/31/05
2-Butanone
BQL
200
8
5/31/05
n-Butylbenzene
BQL
8.00
8
5/31/05
sec-Butylbenzene
BQL
8.00
8
5/31/05
tert-Butylbenzene
BQL
8.00
8
5/31/05
Carbon disulfide
BQL
8.00
8
5/31/05
Carbon tetrachloride
BQL
8.00
8
5/31/05
Chlorobenzene
BQL
8.00
8
5/31/05
Chloroethane
BQL
8.00
8
5/31/05
Chloroform
BQL
8.00
8
5/31/05
Chloromethane
BQL
8.00
8
5/31/05
2-Chlorotoluene
BQL
8.00
8
5/31/05
4-Chlorotoluene
BQL
8.00
8
5/31/05
Dibromochloromethane
BQL
8.00
8
5/31/05
1,2-Dibromo-3-chloropropane
BQL
40.0
8
5/31/05
Dibromomethane
BQL
8.00
8
5131/05
1,2-Dibromoethane (EDB)
BQL
8.00
8
5/31105
1,2-Dichlorobenzene
BQL
8.00
8
5/31/05
1,3-Dichlorobenzene
BQL
8.00
8
5/31/05
1,4-Dichlorobenzene
BQL
8.00
8
5/31/05
trans-1,4-Dichloro-2-butene
BQL
40.0
8
5131/05
1,1-Dichloroethane
BQL
8.00
8
5/31/05
1,1-Dichloroethene
BQL
8.00
8
5/31/05
1,2-Dichloroethane
BQL
8.00
8
5/31/05
cis-1,2-Dichloroethene
BQL
8.00
8
5/31/05
trans-1,2-dichloroethene
BQL
8.00
8
5/31/05
1,2-Dichloropropane
BQL
8.00
8
5/31/05
1,3-Dichloropropane
BQL
8.00
8
5/31/05
2,2-Dichloropropane
BQL
8.00
8
5/31/05
1,1-Dichloropropene
BQL
8.00
8
5/31/05
cis-1,3-Dichloropropene
BQL
8.00
8
5/31/05
trans-1,3-Dichloropropene
BQL
8.00
8
5/31/05
Dichlorodifluoromethane
BQL
40.0
8
5/31/05
ether (DIPE)
BQL
8.00
8
5/31/05
•Diisopropyl
Ethylbenzene
BQL
8.00
8
5/31/05
Hexachlorobutadiene
BQL
8.00
8
5/31/05
Pa 1 of 2 GCMS-ups '2.62.10 Of 7%
N.C. CER-ffFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260B
coClient Sample ID: MW-10 Analyzed By: JTF
Client Project ID: Aimont Shipping Date Collected: 5/25/0510:00
Lab Sample ID: G121-333-10C Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
40.0
8
5/31/05
lodomethane
BQL
8.00
8
5/31/05
Isopropylbenzene
BQL
8.00
8
5/31/05
4-Isopropyltoluene
BQL
8.00
8
5/31/05
Methylene chloride
BQL
40.0
8
5/31/05
4-Methyl-2-pentanone
BQL
40.0
8
5/31/06
Methyl-tert-butyl ether (MTBE)
BQL
8.00
8
5/31/05
Naphthalene
BQL
8.00
8
5/31/05
n-Propyl benzene
BQL
8.00
8
5/31/05
Styrene
BQL
8.00
8
5/31/05
1,1,1,2-Tetrachloroethane
BQL
8.00
8
5/31/05
1,1,2,2-Tetrachloroethane
BQL
8.00
8
5/31/05
Tetrachloroethene
BQL
8.00
8
5131/05
Toluene
BQL
8.00
8
5/31/05
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
BQL
BQL
8.00
8.00
8
8
5/31/05
5/31/05
Trichloroethene
BQL
8.00
8
5/31/05
1,1,1-Trichloroethane
BQL
8.00
8
5/31/05
1,1,2-Trichloroethane
BQL
8.00
8
5/31/05
Trichlorofluoromethane
BQL
8.00
8
5/31/05
1,2,3-Trichloropropane
BQL
8.00
8
5131/05
1,2,4-Trimethylbenzene
BQL
8.00
8
5/31/05
1,3,5-Trimethylbenzene
BQL
8.00
8
5/31/05
Vinyl chloride
BQL
8.00
8
5131/05
m-,p-Xylene
BQL
16.0
8
5/31/05
o-Xylene
BQL
8.00
8
5/31/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
10
100
1,2-Dichloroethane-d4
10
10.2
102
Toluene-d8
10
9.9
99
Comments:
Sample diluted for foaming.
Flags:
BQL = Below Quantitation Limits.
Reviewed By: «
N.C. CEWVI&TION #481 GCMS_LIM3y2.82xtl of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
CID Client Sample ID: MW-12 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 6/25/0510:40
Lab Sample ID: G121-333-11A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG1L
Factor
Analyzed
Acetone
BQL
25.0
1
5/28/05
Benzene
BQL
1.00
1
5/28/05
Bromobenzene
BQL
1.00
1
5/28/05
Bromochloromethane
BQL
1.00
1
5/28/05
Bromodichioromethane
BQL
1.00
1
5/28/05
Bromoform
BQL
1.00
1
5/28/05
Bromomethane
BQL
1.00
1
5/28/05
2-Butanone
BQL
25.0
1
5/28/05
n-Butylbenzene
BQL
1.00
1
5/28/05
sec-Butylbenzene
BQL
1.00
1
5/28/05
tert-Butylbenzene
BQL
1.00
1
5/28/05
Carbon disulfide
BQL
1.00
1
5/28/05
Carbon tetrachloride
BQL
1.00
1
5/28/05
Chlorobenzene
BQL
1.00
1
5/28/05
Chloroethane
BQL
1.00
1
5/28/05
Chloroform
BQL
1.00
1
5/28/05
Chloromethane
BQL
1.00
1
5/28/05
2-Chlorotoluene
BQL
1.00
1
5128/05
4-Chlorotoluene
BQL
1.00
1
5/28/05
Dibromochloromethane
BQL
1.00
1
5/28/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/28/05
Dibromomethane
BQL
1.00
1
5/28/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/28/05
1,2-Dichlorobenzene
BQL
1.00
1
5/28/05
1,3-Dichlorobenzene
BQL
1.00
1
5/28/05
1,4-Dichlorobenzene
BQL
1.00
1
5128/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/28/05
1,1-Dichloroethane
BQL
1.00
1
5/28/05
1,1-Dichloroethene
BQL
1.00
1
5/28/05
1,2-Dichloroethane
BQL
1.00
1
5/28/05
cis-1,2-Dichloroethene
BQL
1.00
1
5/28/05
trans-1,2-dichloroethene
BQL
1.00
1
5/28/05
1,2-Dichloropropane
BQL
1.00
1
5128/05
1,3-Dichloropropane
BQL
1.00
1
5128/05
2,2-Dichloropropane
BQL
1.00
1
5/28/05
1,1-Dichloropropene
BQL
1.00
1
5/28/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/28/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/28/05
Dichlorodifluoromethane
BQL
5.00
1
5/28105
ether (DIPE)
BQL
1.00
1
5/28/05
.Diisopropyl
Ethylbenzene
BQL
1.00
1
5/28/05
Hexachlorobutadiene
BQL
1.00
1
5/28/05
Pa e 1 of 2 MMS_uMs_Y2.62 L2 of 77
N.C. CERTIFICATION #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260B
Cement Sample ID: MW-12 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/0510:40
Lab Sample ID: G121-333-11A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UGIL
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5128/05
lodomethane
BQL
1.00
1
5/28/05
Isopropylbenzene
BQL
1.00
1
5128/05
4-Isopropyitoluene
BQL
1.00
1
5/28/05
Methylene chloride
BQL
5.00
1
5/28/05
4-Methyl-2-pentanone
BQL
5.00
1
5/28/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/28/05
Naphthalene
BQL
1.00
1
5/28/05
n-Propyl benzene
BQL
1.00
1
5/28/05
Styrene
BQL
1.00
1
5/28105
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/28/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/28/05
Tetrachloroethene
BQL
1.00
1
5/28/05
Toluene
BQL
1.00
1
5/28/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5/28/05
.1,2,4-Trichlorobenzene
BQL
1.00
1
5/28/05
Trichloroethene
BQL
1.00
1
5/28/05
1,1,1-Trichloroethane
BQL
1.00
1
5/28/05
1,1,2-Trichloroethane
BQL
1.00
1
5/28/05
Trichlorofluoromethane
BQL
1.00
1
5/28/05
1,2,3-Trichloropropane
BQL
1.00
1
5/28/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/28/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/28/05
Vinyl chloride
BQL
1.00
1
5/28/05
m-,p-Xylene
BQL
2.00
1
5/28/05
o-Xylene
BQL
1.00
1
5128/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
10.1
101
1,2-Dichloroethane-d4
10
10.6
106
Toluene-d8
10
10.2
102
Comments:
Flags:
BQL = Below Quantitation Limits.
Reviewed By:
N.C. CER I I ?&C ION #481 GCMS LIMS vz.sz•%�L3 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
CrClient Sample ID: MW-13 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5125/0511:20
Lab Sample ID: G121-333-12A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
Acetone
BQL
25.0
1
5/28/05
Benzene
BQL
1.00
1
5/28105
Bromobenzene
BQL
1.00
1
5/28/05
Bromochloromethane
BQL
1.00
1
5/28/05
Bromodichloromethane
BQL
1.00
1
5/28/05
Bromoform
BQL
1.00
1
5/28/05
Bromomethane
BQL
1.00
1
5/28/05
2-Butanone
BQL
25.0
1
5/28/05
n-Butylbenzene
BQL
1.00
1
5/28/05
sec-Butylbenzene
BQL
1.00
1
5/28/05
tert-Butylbenzene
BQL
1.00
1
5128/05
Carbon disulfide
BQL
1.00
1
5/28/05
Carbon tetrachloride
BQL
1.00
1
5128/05
Chlorobenzene
BQL
1.00
1
5/28105
Chloroethane
BQL
1.00
1
5/28/05
C�Chloroform
BQL
1.00
1
5/28/05
Chloromethane
BQL
1.00
1
5/28/05
2-Chlorotoluene
BQL
1.00
1
5/28/05
4-Chlorotoluene
BQL
1.00
1
5/28/05
Dibromochloromethane
BQL
1.00
1
5/28/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/28/05
Dibromomethane
BQL
1.00
1
5/28/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/28/05
1,2-Dichlorobenzene
BQL
1.00
1
5/28/05
1,3-Dichlorobenzene
BQL
1.00
1
5/28/05
1,4-Dichlorobenzene
BQL
1.00
1
5/28/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/28/05
1,1-Dichloroethane
BQL
1.00
1
5/28/05
1,1-Dichloroethene
BQL
1.00
1
5/28/05
1,2-Dichloroethane
BQL
1.00
1
5/28/05
cis-1,2-Dichloroethene
BQL
1.00
1
5/28/05
trans-1,2-dichloroethene
BQL
1.00
1
5/28/05
1,2-Dichloropropane
BQL
1.00
1
5/28/06
1,3-Dichloropropane
BQL
1.00
1
5/28/05
2,2-Dichloropropane
BQL
1.00
1
5/28/06
1,1-Dichloropropene
BQL
1.00
1
5/28/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/28/05
trans-1,3-Dichloropropene
BQL
1.00
1
5128/05
Dichlorodifluoromethane
BQL
5.00
1
5/28/05
Diisopropyl ether (DIPE)
BQL
1.00
1
5/28/05
Ethylbenzene
BQL
1.00
1
5/28/05
Hexachlorobutadiene
BQL
1.00
1
5/28/05
N.C. CEK I"It-I&ION #481 GCMS LIMS A.62.xN of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260B
. Client Sample ID: MW-13 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/0511:20
Lab Sample ID: G121-333-12A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/28/05
lodomethane
BQL
1.00
1
5/28/05
Isopropylbenzene
BQL
1.00
1
5/28/05
4-Isopropyltoluene
BQL
1.00
1
5/28/05
Methylene chloride
BQL
5.00
1
5/28/05
4-Methyl-2-pentanone
BQL
5.00
1
5/28/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/28/05
Naphthalene
BQL
1.00
1
5/28/05
n-Propyl benzene
BQL
1.00
1
5/28/05
Styrene
BQL
1.00
1
5/28/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/28/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/28/05
Tetrachloroethene
BQL
1.00
1
5/28/05
Toluene
BQL
1.00
1
5/28/05
1,2,3-Trichlorobenzene
(!� 1,2,4-Trichlorobenzene
BQL
BQL
1.00
1.00
1
1
5/28105
5/28/05
`— Trichloroethene
BQL
1.00
1
5/28/05
1, 1, 1 -Trichloroethane
BQL
1.00
1
5/28/05
1,1,2-Trichloroethane
BQL
1.00
1
5/28/05
Trichlorofluoromethane
BQL
1.00
1
5/28/05
1,2,3-Trichloropropane
BQL
1.00
1
5/28/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/28/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/28/05
Vinyl chloride
BQL
1.00
1
5/28/05
m-,p-Xylene
BQL
2.00
1
5/28105
o-Xylene
BQL
1.00
1
5/28/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
10.1
101
1,2-Dichloroethane-d4
10
11
110
Toluene-d8
10
9.99
100
Comments:
Flags:
BQL = Below Quantitation Limits.
r�
Reviewed By:v
N.C. CERYIWA�ION #481 cMS LIMS V2.62 15 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
Ce Client Sample ID: MW-14 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5125/05 11:40
Lab Sample ID: G121-333-13C Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UG1L
Factor
Analyzed
Acetone
BQL
50.0
2
5/31/05
Benzene
BQL
2.00
2
5/31/05
Bromobenzene
BQL
2.00
2
5/31/05
Bromochloromethane
BQL
2.00
2
5/31/05
Bromodichloromethane
BQL
2.00
2
5/31/05
Bromoform
BQL
2.00
2
5/31/05
Bromomethane
BQL
2.00
2
5/31/05
2-Butanone
BQL
50.0
2
5/31/05
n-Butylbenzene
BQL
2.00
2
5/31105
sec-Butylbenzene
BQL
2.00
2
5/31/05
tert-Butylbenzene
BQL
2.00
2
5/31/05
Carbon disulfide
BQL
2.00
2
5/31/05
Carbon tetrachloride
BQL
2.00
2
5/31/05
Chlorobenzene
BQL
2.00
2
5/31/05
Chloroethane
BQL
2.00
2
5/31/05
• Chloroform
BQL
2.00
2
5/31/05
Chloromethane
BQL
2.00
2
5/31/05
2-Chlorotoluene
BQL
2.00
2
5/31/05
4-Chlorotoluene
BQL
2.00
2
5/31/05
Dibromochloromethane
BQL
2.00
2
5/31/05
1,2-Dibromo-3-chloropropane
BQL
10.0
2
5/31/05
Dibromomethane
BQL
2.00
2
5/31/05
1,2-Dibromoethane (EDB)
BQL
2.00
2
5/31/05
1,2-Dichlorobenzene
BQL
2.00
2
5/31/05
1,3-Dichlorobenzene
BQL
2.00
2
5/31/05
1,4-Dichlorobenzene
BQL
2.00
2
5/31/05
trans-1,4-Dichloro-2-butene
BQL
10.0
2
5131/05
1,1-Dichloroethane
BQL
2.00
2
5131/05
1,1-Dichloroethene
BQL
2.00
2
5/31/05
1,2-Dichloroethane
BQL
2.00
2
5/31/05
cis-1,2-Dichloroethene
BQL
2.00
2
5/31/05
trans-1,2-dichloroethene
BQL
2.00
2
5/31/05
1,2-Dichloropropane
BQL
2.00
2
5131/05
1,3-Dichloropropane
BQL
2.00
2
5/31/05
2,2-Dichloropropane
BQL
2.00
2
5/31/05
1,1-Dichloropropene
BQL
2.00
2
5/31/05
cis-1,3-Dichloropropene
BQL
2.00
2
5/31/05
trans-1,3-Dichloropropene
BQL
2.00
2
5/31105
Dichlorodifluoromethane
BQL
10.0
2
5/31/05
Diisopropyl ether (DIPE)
BQL
2.00
2
5/31/05
�• Eth Y(benzene
�
BQL
2.00
2
5/31/05
Hexachlorobutadiene
BQL
2.00
2
5/31/05
N.C. CEM ICATION #481 GCMS LIMS_t2.82.x{h6 Of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
` by GCMS 8260E
(``• Client Sample ID: MW-14 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/0511:40
Lab Sample ID: G121-333-13C Date Received: 5/26/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
10.0
2
5/31/05
lodomethane
BQL
2.00
2
5/31/05
Isopropyibenzene
BQL
2.00
2
5/31/05
4-Isopropyitoluene
BQL
2.00
2
5/31/05
Methylene chloride
BQL
10.0
2
5/31/05
4-Methyl-2-pentanone
BQL
10.0
2
5/31/05
Methyl-tert-butyl ether (MTBE)
BQL
2.00
2
5/31/05
Naphthalene
BQL
2.00
2
5/31/05
n-Propyl benzene
BQL
2.00
2
5/31/05
Styrene
BQL
2.00
2
5/31/05
1,1,1,2-Tetrachloroethane
BQL
2.00
2
5/31/05
1,1,2,2-Tetrachloroethane
BQL
2.00
2
5/31/05
Tetrachloroethene
BQL
2.00
2
5/31/05
Toluene
BQL
2.00
2
5/31/05
1,2,3-Trichlorobenzene
BQL
2.00
2
5/31/05
�i 1,2,4-Trichlorobenzene
BQL
2.00
2
5/31/05
Trichloroethene
BQL
2.00
2
5131/05
1, 1, 1 -Trichloroethane
BQL
2.00
2
5/31/05
1,1,2-Trichloroethane
BQL
2.00
2
5/31/05
Trichlorofluoromethane
BQL
2.00
2
5/31/05
1,2,3-Trichloropropane
BQL
2.00
2
5131/05
1,2,4-Trimethylbenzene
BQL
2.00
2
5/31/05
1,3,5-Trimethylbenzene
BQL
2.00
2
5/31/05
Vinyl chloride
BQL
2.00
2
5/31/05
m-,p-Xylene
BQL
4.00
2
5/31/05
o-Xylene
BQL
2.00
2
5/31/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
10
100
1,2-Dichloroethane-d4
10
11.1
111
Toluene-d8
10
10.2
102
Comments:
Sample diluted for foaming.
Flags:
BQL = Below Quantitation Limits.
0
Reviewed By:
N.C. CER%fdAf TION #481 GCMS LIMS-V2.62 27 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 82608
�. Client Sample ID: MWA 5 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/0512:00
Lab Sample ID: G121-333-14C Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
Acetone
BQL
50.0
2
5/31/05
Benzene
BQL
2.00
2
5/31/05
Bromobenzene
BQL
2.00
2
5/31/05
Bromochloromethane
BQL
2.00
2
5/31/05
Bromodichloromethane
BQL
2.00
2
5/31/05
Bromoform
BQL
2.00
2
5/31/05
Bromomethane
BQL
2.00
2
5/31/05
2-Butanone
BQL
50.0
2
5/31/05
n-Butylbenzene
BQL
2.00
2
5/31/05
sec-Butylbenzene
BQL
2.00
2
5/31/05
tent-Butylbenzene
BQL
2.00
2
5/31/05
Carbon disulfide
BQL
2.00
2
5/31/05
Carbon tetrachloride
BQL
2.00
2
5/31/05
Chlorobenzene
BQL
2.00
2
5/31/05
Chloroethane
Chloroform
BQL
BQL
2.00
2.00
2
2
5/31/05
5/31/05
Chloromethane
BQL
2.00
2
5/31105
2-Chlorotoluene
BQL
2.00
2
5/31/05
4-Chlorotoluene
BQL
2.00
2
5/31/05
Dibromochloromethane
BQL
2.00
2
5/31/05
1,2-Dibromo-3-chloropropane
BQL
10.0
2
5/31/06
Dibromomethane
BQL
2.00
2
5/31/05
1,2-Dibromoethene (EDB)
BQL
2.00
2
5/31/05
1,2-Dichlorobenzene
BQL
2.00
2
5/31/05
1,3-Dichlorobenzene
BQL
2.00
2
5/31/05
1,4-Dichlorobenzene
BQL
2.00
2
5/31/05
trans-1,4-Dichloro-2-butene
BQL
10.0
2
5/31/05
1,1-Dichloroethane
BQL
2.00
2
5/31/05
1,1-Dichloroethene
BQL
2.00
2
5/31/05
1,2-Dichloroethane
BQL
2.00
2
5/31/05
cis-1,2=Dichloroethene
BQL
2.00
2
5/31/05
trans- 1,2-dichloroethene
BQL
2.00
2
5/31/05
1,2-Dichloropropane
BQL
2.00
2
5/31/05
1,3-Dichloropropane
BQL
2.00
2
5/31/05
2,2-Dichloropropane
BQL
2.00
2
5/31105
1,1-Dichloropropene
BQL
2.00
2
5/31/05
cis-1,3-Dichloropropene
BQL
2.00
2
5/31/05
trans-1,3-Dichloropropene
BQL
2.00
2
5/31/05
Dichlorodifluoromethane
BQL
10.0
2
5/31/05
Diisopropyl ether (DIPE)
BQL
2.00
2
5/31/05
�•
Ethylbenzene
BQL
2.00
2
5/31/05
-
Hexachlorobutadiene
BQL
2.00
2
5/31/05
N.C. CERW ICATION #481 GCMS LIMB vi.s2.xly,Q Of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 82608
• Client Sample ID: MW-15 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/0512:00
Lab Sample ID: G121-333-14C Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
10.0
2
5/31/05
lodomethane
BQL
2.00
2
5/31/05
Isopropyibenzene
BQL
2.00
2
5/31/05
4-Isopropyltoluene
BQL
2.00
2
5/31/05
Methylene chloride
BQL
10.0
2
5/31/05
4-Methyl-2-pentanone
BQL
10.0
2
5/31/05
Methyl-tert-butyl ether (MTBE)
BQL
2.00
2
5/31/05
Naphthalene
BQL
2.00
2
5/31/05
n-Propyl benzene
BQL
2.00
2
5/31/05
Styrene
BQL
2.00
2
5/31/05
1,1,1,2-Tetrachloroethane
BQL
2.00
2
5/31/05
1,1,2,2-Tetrachloroethane
BQL
2.00
2
5/31/05
Tetrachloroethene
BQL
2.00
2
5131/05
Toluene
BQL
2.00
2
5131/05
1,2,3-Trichlorobenzene
• 1,2,4-Trichlorobenzene
BQL
BQL
2.00
2.00
2
2
5/31/05
5/31/05
Trichloroethene
BQL
2.00
2
5/31/05
1,1,1-Trichloroethane
BQL
2.00
2
5/31/05
1,1,2-Trichloroethane
BQL
2.00
2
5131/05
Trichlorofluoromethane
BQL
2.00
2
5/31/05
1,2,3-Trichloropropane
BQL
2.00
2
5/31/05
1,2,4-Trimethylbenzene
BQL
2.00
2
5/31/05
1,3,5-Trimethylbenzene
BQL
2.00
2
5/31/05
Vinyl chloride
BQL
2.00
2
5/31/05
m-,p-Xylene
BQL
4.00
2
5/31/05
o-Xylene
BQL
2.00
2
5/31/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
9.88
99
1,2-Dichloroethane-d4
10
10.7
107
Toluene-d8
10
9.99
100
Comments:
Sample diluted for foaming.
Flags:
BQL = Below Quantitation Limits.
0
Reviewed By: tz-w _
N.C. CER'FlVdalON #481 GCMS,_UMSLA62.xt9 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 82606
A Client Sample ID: DW-1 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 12:20
Lab Sample ID: G121-333-15A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UG/L
Factor
Analyzed
Acetone
BQL
25.0
1
5/28/05
Benzene
BQL
1.00
1
5128/05
Bromobenzene
BQL
1.00
1
5/28/05
Bromochloromethane
BQL
1.00
1
5/28105
Bromodichloromethane
BQL
1.00
1
5/28/05
Bromoform
BQL
1.00
1
5/28/05
Bromomethane
BQL
1.00
1
5/28/05
2-Butanone
BQL
25.0
1
5/28/05
n-Butyibenzene
BQL
1.00
1
5/28/05
sec-Butyibenzene
BQL
1.00
1
5/28/05
tert-Butyibenzene
BQL
1.00
1
5/28/05
Carbon disulfide
BQL
1.00
1
5/28/05
Carbon tetrachloride
BQL
1.00
1
5/28/05
Chlorobenzene
BQL
1.00
1
5/28/05
Chloroethane
BQL
1.00
1
5/28/05
0Chloroform
BQL
1.00
1
5/28/05
Chloromethane
BQL
1.00
1
5128/05
2-Chlorotoluene
BQL
1.00
1
5/28/05
4-Chlorotoluene
BQL
1.00
1
5128/05
Dibromochloromethane
BQL
1.00
1
5128/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5128105
Dibromomethane
BQL
1.00
1
5/28/05
1,2-Dibromoethane (EDB)
BQL
1.00
Ir
5/28/05
1,2-Dichlorobenzene
BQL
1.00
1
5/28/05
1,3-Dichlorobenzene
BQL
1.00
1
5/28/05
1,4-Dichlorobenzene
BQL
1.00
1
5128/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/28/05
1,1-Dichioroethane
BQL
1.00
1
5/28/05
1,1-Dichloroethene
BQL
1.00
1
5/28/05
1,2-Dichioroethane
BQL
1.00
1
5/28105
cis-1,2-Dichloroethene
SQL
1.00
1
5/28/05
trans-1,2-dichloroethene
SQL
1.00
1
5/28/05
1,2-Dichloropropane
BQL
1.00
1
5/28/05
1,3-Dichloropropane
BQL
1.00
1
5/28/05
2,2-Dichloropropane
BQL
1.00
1
5/28/05
1,1-Dichloropropene
BQL
1.00
1
5/28/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/28/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/28/05
Dichlorodifluoromethane
BQL
5.00
1
5128/05
Diisopropyl ether (DIPE)
BQL
1.00
1
5/28/05
Ethylbenzene
BQL
1.00
1
5128/05
Hexachlorobutadiene
BQL
1.00
1
5/28/05
N.C. CER�( IFICAT10N #481 ccM8 LIMS_d2.82.xI D Of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 82606
�• Client Sample ID: DW-1 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/0512:20
Lab Sample ID: G121-333-15A Date Received: 5/25105
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/28/05
lodomethane
BQL
1.00
1
5/28/05
isopropylbenzene
BQL
1.00
1
5/28/05
4-Isopropyltoluene
BQL
1.00
1
5/28/05
Methylehe chloride
BQL
5.00
1
5/28/05
4-Methyl-2-pentanone
BQL
5.00
1
5/28/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/28105
Naphthalene
BQL
1.00
1
5/28/05
n-Propyl benzene
BQL
1.00
1
5/28/05
Styrene
BQL
1.00
1
5/28/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/28/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/28/05
Tetrachloroethane
SQL
1.00
1
5/28/05
Toluene
BQL
1.00
1
5/28/05
1,2,3-Trichiorobenzene
BQL
1.00
1
5/28/05
1,2,4-Trichlorobenzene
BQL
1.00
1
5/28/05
Trichloroethene
BQL
1.00
1
5/28/05
1,1,1-Trichioroethane
BQL
1.00
1
5/28/05
1,1,2-Trichioroethane
BQL
1.00
1
5/28/05
Trichlorofluoromethane
BQL
1.00
1
5/28/05
1,2,3-Trichloropropane
BQL
1.00
1
5/28/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/28/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/28/05
Vinyl chloride
BQL
1.00
1
5/28/05
m-,p-Xylene
BQL
2.00
1
5/28/05
o-Xylene
BQL
1.00
1
5/28/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
9.67
97
1,2-Dichloroethane-d4
10
10.6
106
Toluene-d8
10
10
100
Comments:
Flags:
BQL = Below Quantitation Limits.
c0
Reviewed By: Vv V
N.C. CERMRMG ION #481 ccMs "'"S ,�'6Z 31 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
�• Client Sample ID: DW-2 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/05 12:40
Lab Sample ID: G121-333-16A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
Acetone
BQL
25.0
1
5/28/05
Benzene
BQL
1.00
1
5/28/05
Bromobenzene
BQL
1.00
1
5/28/05
Bromochloromethane
BQL
1.00
1
5/28/05
Bromodichloromethane
BQL
1.00
1
5/28/05
Bromoform
BQL
1.00
1
5/28/05
Bromomethane
BQL
1.00
1
5/28/05
2-Butanone
BQL
25.0
1
5/28/05
n-Butylbenzene
BQL
1.00
1
5/28/05
sec-Butyibenzene
BQL
1.00
1
5/28/05
tert-Butylbenzene
BQL
1.00
1
5/28/05
Carbon disulfide
BQL
1.00
1
5/28/05
Carbon tetrachloride
BQL
1.00
1
5/28/05
Chlorobenzene
BQL
1.00
1
5/28/05
Chloroethane
BQL
1.00
1
5/28/05
Chloroform
BQL
1.00
1
5/28/05
Chloromethane
BQL
1.00
1
5/28/05
2-Chlorotoluene
BQL
1.00
1
5/28/05
4-Chlorotoluene
BQL
1.00
1
5/28/05
Dibromochloromethane
BQL
1.00
1
5/28/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/28/05
Dibromomethane
BQL
1.00
1
5/28/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/28/05
1,2-Dichlorobenzene
BQL
1.00
1
5128/05
1,3-Dichlorobenzene
BQL
1.00
1
5/28/05
1,4-Dichlorobenzene
BQL
1.00
1
5/28/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/28/05
1,1-Dichloroethane
BQL
1.00
1
5/28/05
1,1-Dichloroethene
BQL
1.00
1
5/28/05
1,2-Dichloroethane
BQL
1.00
1
5/28/05
cis-1,2-Dichloroethene
BQL
1.00
1
5128/05
trans-1,2-dichloroethene
BQL
1.00
1
5/28/05
1,2-Dichloropropane
BQL
1.00
1
5/28/05
1,3-Dichloropropane
BQL
1.00
1
5/28/05
2,2-Dichloropropane
BQL
1.00
1
5128/05
1,1-Dichloropropene
BQL
1.00
1
5/28/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/28/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/28/05
Dichlorodifluoromethane
BQL
5.00
1
5/28/05
Diisopropyl ether (DIPE)
BQL
1.00
1
5/28/05
(� Ethyibenzene
BQL
1.00
1
5/28/05
Hexachlorobutadiene
BQL
1.00
1
5/28/05
N.C. CE 1G4tA 10N #481 GCMS LIMS_y2Uxt2 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260E
�. Client Sample ID: DW-2 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/0512:40
Lab Sample ID: G121-333-16A Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/28/05
lodomethane
BQL
1.00
1
5/28/05
Isopropylbenzene
BQL
1.00
1
5/28/05
4-Isopropyltoluene
BQL
1.00
1
5/28/05
Methylene chloride
BQL
5.00
1
5/28/05
4-Methyl-2-pentanone
BQL
5.00
1
5/28/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/28/05
Naphthalene
BQL
1.00
1
5/28/05
n-Propyl benzene
BQL
1.00
1
5/28/05
Styrene
BQL
1.00
1
5/28/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/28/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/28/05
Tetrachloroethene
BQL
1.00
1
5/28/05
Toluene
BQL
1.00
1
5/28/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5/28105
1,2,4-Trichlorobenzene
BQL
1.00
1
5/28/05
Trichloroethene
BQL
1.00
1
5/28/05
1,1, 1 -Trichloroethane
BQL
1.00
1
5/28/05
1,1,2-Trichloroethane
BQL
1.00
1
5/28/05
Trichlorofluoromethane
BQL
1.00
1
5/28105
1,2,3-Trichloropropane
BQL
1.00
1
6/28105
1,2,4-Trimethylbenzene
BQL
1.00
1
5/28/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/28/05
Vinyl chloride
BQL
1.00
1
5/28/05
m-,p-Xylene
BQL
2.00
1
5/28/05
o-Xylene
BQL
1.00
1
5/28/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
9.83
98
1,2-Dichloroethane-d4
10
10.9
109
Toluene-d8
10
9.95
99
Comments:
Flags:
BQL = Below Quantitation Limits.
P
Reviewed By: r
N.C. CEK r1r dalON #481 ccMS_-UM4_v262x�33 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 8260B
l\ oClient Sample ID: MWA6
Analyzed By: JTF
Client Project ID: Almont Shipping
Date Collected: 5/25/05 11:00
Lab Sample ID: G121-333-17B
Date Received: 5125/05
Lab Project ID: G121-333
Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UGIL
Factor
Analyzed
Acetone
BQL
25.0
1
5127105
Benzene
BQL
1.00
1
5/27/05
Bromobenzene
BQL
1.00
1
5/27/05
Bromochloromethane
BQL
1.00
1
5/27/05
Bromodichloromethane
BQL
1.00
1
5/27/05
Bromoform
BQL
1.00
1
5/27/05
Bromomethane
BQL
1.00
1
6/27/05
2-Butanone
BQL
25.0
1
5/27/05
n-Butylbenzene
BQL
1.00
1
5/27/05
sec-Butyibenzene
BQL
1.00
1
5/27/05
tert-Butylbenzene
BQL
1.00
1
5/27/05
Carbon disulfide
BQL
1.00
1
5/27/05
Carbon tetrachloride
BQL
1.00
1
5/27/05
Chiorobenzene
BQL
1.00
1
5/27/05
Chioroethane
BQL
1.00
1
5/27/05
Chloroform
BQL
1.00
1
5/27/05
Chloromethane
BQL
1.00
1
5127/05
2-Chlorotoluene
BQL
1.00
1
5/27/05
4-Chlorotoluene
BQL
1.00
1
5/27/05
Dibromochloromethane
BQL
1.00
1
5/27/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/27/05
Dibromomethane
BQL
1.00
1
5/27/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5/27105
1,2-Dichlorobenzene
BQL
1.00
1
5/27/05
1,3-Dichlorobenzene
BQL
1.00.
1
5/27105
1,4-Dichlorobenzene
BQL
1.00
1
5/27/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/27/05
1,1-Dichloroethane
BQL
1.00
1
5/27/05
1,1-Dichloroethene
BQL
1.00
1
5/27/05
1,2-Dichloroethane
BQL
1.00
1
5/27/05
cis-1,2-Dichloroethene
BQL
1.00
1
5/27/05
trans-1,2-dichloroethene
BQL
1.00
1
5/27/05
1,2-Dichloropropane
BQL
1.00
1
5/27105
1,3-Dichloropropane
BQL
1.00
1
5/27/05
2,2-Dichloropropane
BQL
1.00
1
5/27/06
1,1-Dichloropropene
BQL
1.00
1
5/27/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/27/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/27/05
Dichlorodifluoromethane
BQL
5.00
1
5/27/05
ether (DIPE)
BQL
1.00
1
5/27/05
•Diisopropyl
Etylbenzene
BQL
1.00
1
5/27/05
Hexachlorobutadiene
BQL
1.00
1
5/27/05
N.C. CERTIFICATION #481 ccMs_LIMS_�l.ex�'34 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 82606
AClient Sample ID: MW-16 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/0511:00
Lab Sample ID: G121-333-17B Date Received: 5/25/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UG/L
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/27105
lodomethane
BQL
1.00
1
5/27/05
Isopropylbenzene
BQL
1.00
1
5/27/05
4-Isopropyltoluene
BQL
1.00
1
5/27/05
Methylene chloride
BQL
5.00
1
5/27/05
4-Methyl-2-pentenone
BQL
5.00
1
5/27/05
Methyl-tert-butyl ether (MTBE)
1.43
1.00
1
5/27/05
Naphthalene
BQL
1.00
1
5/27/05
n-Propyl benzene
BQL
1.00
1
5/27/05
Styrene
BQL
1.00
1
5/27/05
1,1,1,2-Tetrachloroethane
BQL
1.00
1
5/27105
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/27/05
Tetrachloroethene
BQL
1.00
1
5/27/05
Toluene
BQL
1.00
1
5/27/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5/27/05
1,2,4-Trichlorobenzene
BQL
1.00
1
5/27/05
Trichloroethene
BQL
1.00
1
5/27/05
1, 1, 1 -Trichloroethane
BQL
1.00
1
5/27/05
1,1,2-Trichloroethane
BQL
1.00
1
5/27/05
Trichlorofluoromethane
BQL
1.00
1
5127/05
1,2,3-Trichloropropane
BQL
1.00
1
5/27/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/27/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/27/05
Vinyl chloride
BQL
1.00
1
5/27/05
m-,p-Xylene
BQL
2.00
1
5/27/05
o-Xylene
BQL
1.00
1
5/27/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
10.2
102
1,2-Dichloroethane-d4
10
10.6
106
Toluene-d8
1'0
9.94
99
Comments:
Flags:
BQL = Below Quantitation Limits.
19,
Reviewed By: _qn-V
N.C. CERTIFICATION #481 GCMS LIMS �182t5 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
// by GCMS 82608
4� Client Sample ID: LM-13 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/0513:00
Lab Sample ID: G121-333-18A Date Received: 5/25105
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UGIL
Factor
Analyzed
Acetone
BQL
25.0
1
5/28/05
Benzene
BQL
1.00
1
5/28/05
Bromobenzene
BQL
1.00
1
5/28/05
Bromochloromethane
BQL
1.00
1
5/28/05
Bromodichloromethane
BQL
1.00
1
5/28/05
Bromoform
BQL
1.00
1
5/28/05
Bromomethane
BQL
1.00
1
5/28/05
2-Butanone
BQL
25.0
1
5/28/05
n-Butylbenzene
BQL
1.00
1
5/28/05
sec-Butylbenzene
BQL
1.00
1
5/28/05
tent-Butylbenzene
BQL
1.00
1
5/28/05
Carbon disulfide
BQL
1.00
1
5/28/05
Carbon tetrachloride
BQL
1.00
1
5/28/05
Chlorobenzene
BQL
1.00
1
5/28/05
Chloroethane
BQL
1.00
1
5/28/05
(. Chloroform
BQL
1.00
1
5/28/05
Chloromethane
BQL
1.00
1
5128/05
2-Chiorotoluene
BQL
1.00
1
5128/05
4-Chlorotoluene
BQL
1.00
1
5128/05
Dibromochloromethane
BQL
1.00
1
5/28/05
1,2-Dibromo-3-chloropropane
BQL
5.00
1
5/28/05
Dibromomethane
BQL
1.00
1
5/28/05
1,2-Dibromoethane (EDB)
BQL
1.00
1
5128/05
1,2-Dichlorobenzene
BQL
1.00
1
5/28/05
1,3-Dichlorobenzene
BQL
1.00
1
5/28/05
1,4-Dichlorobenzene
BQL
1.00
1
5/28/05
trans-1,4-Dichloro-2-butene
BQL
5.00
1
5/28/05
1,1-Dichloroethane
BQL
1.00
1'
5/28/05
1,1-Dichloroethene
BQL
1.00
1
5/28/05
1,2-Dichloroethane
BQL
1.00
1
5/28/05
cis-1,2-Dichloroethene
12.7
1.00
1
5/28/05
trans-1,2-dichloroethene
BQL
1.00
1
5/28/05
1,2-Dichloropropane
BQL
1.00
1
5128/05
1,3-Dichloropropane
BQL
1.00
1
5/28/05
2,2-Dichloropropane
BQL
1.00
1
5/28/05
1,1-Dichloropropene
BQL
1.00
1
5/28/05
cis-1,3-Dichloropropene
BQL
1.00
1
5/28/05
trans-1,3-Dichloropropene
BQL
1.00
1
5/28/05
Dichlorodifluoromethane
BQL
5.00
1
5/28/05
Diisopropyl ether (DIPE)
BQL
1.00
1
5/28/05
�. Etylbenzene
BQL
1.00
1
5/28/05
Hexachlorobutadiene
BQL
1.00
1
5/28/05
N.C. CE�PV&ION #481 GCMS_LIMS A.62."36 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 82606
C. Client Sample ID: LM-13 Analyzed By: JTF
Client Project ID: Almont Shipping Date Collected: 5/25/0513:00
Lab Sample ID: G121-333-18A Date Received: 5125/05
Lab Project ID: G121-333 Matrix: Water
Result
Quantitation
Dilution
Date
Compound
UGIL
Limit UG/L
Factor
Analyzed
2-Hexanone
BQL
5.00
1
5/28/05
lodomethane
BQL
1.00
1
5/28/05
Isopropylbenzene
BQL
1.00
1
5/28/05
4-Isopropyltoluene
BQL
1.00
1
5/28/05
Methylene chloride
BQL
5.00
1
5/28/05
4-Methyl-2-pentanone
BQL
5.00
1
5128/05
Methyl-tert-butyl ether (MTBE)
BQL
1.00
1
5/28/05
Naphthalene
BQL
1.00
1
5/28/05
n-Propyl benzene
BQL
1.00
1
5/28/05
Styrene
BQL
1.00
1
5/28/05
1',1,1,2-Tetrachloroethane
BQL
1.00
1
5/28/05
1,1,2,2-Tetrachloroethane
BQL
1.00
1
5/28/05
Tetrachloroethene
1600
50.0
50
5/31/05
Toluene
BQL
1.00
1
5/28/05
1,2,3-Trichlorobenzene
BQL
1.00
1
5128/05
1,2,4-Trichlorobenzene
BQL
1.00
1
5/28/05
Trichloroethene
24.0
1.00
1
5/28/05
1,1,1-Trichloroethane
BQL
1.00
1
5/28/05
1,1,2-Trichloroethane
BQL
1.00
1
5/28/05
Trichlorofluoromethane
BQL
1.00
1
5/28/05
1,2,3-Trichloropropane
BQL
1.00
1
5/28/05
1,2,4-Trimethylbenzene
BQL
1.00
1
5/28/05
1,3,5-Trimethylbenzene
BQL
1.00
1
5/28/05
Vinyl chloride
BQL
1.00
1
5/28/05
m-,p-Xylene
BQL
2.00
1
5/28/05
o-Xylene
BQL
1.00
1
5/28/05
Spike
Spike
Percent
Added
Result
Recovered
4-Bromofluorobenzene
10
9.98
100
1,2-Dichloroethane-d4
10
10.5
105
Toluene-d8
10
9.96
100
Comments:
Flags:
BQL = Below Quantitation Limits.
10
Reviewed By: _v..,Ao_
N.C. CERTIFI&ION #481 GCMS LIMS Q62A57 of 77

(9
0-
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 1 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2005
Lab Sample ID: G121-333-1 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
8.4
0.1
mg/l
350.2
6/2/2005
Envirochem
Chloride
9.5
0.1
mg/l
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
BQL
0.025
mg/I
353.3
5/31/2005
Envirochem
Phosphors
0.94
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
58
5
mg/,I
375.4
6/1/2005
Envirochem
TKN
91
0.1
mg/I
351.3
6/1/2005
Envirochem
Total Nitrogen
91
0.1
mg/I
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By:
38 of 77

C�
L�
0
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW-2 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2005
Lab Sample ID: G121-333-2 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
0.6
0.1
mg/l
350.2
6/2/2005
Envirochem
Chloride
10
0.1
mg/l
SM 4600 CI-B
5/31/2005
Envirochem
Nitrate
1.54
0.025
mg/l
353.3
5/31/2005
Envirochem
Phosphorus
2.67
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
106
5
mg/I
376.4
6/1/2005
Envirochem
TKN
4.5
0.1
mg/l
351.3
6/1/2005
Envirochem
Total Nitrogen
6
0.1
mg/I
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: r=tj&
39 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
l Client Sample ID:
MW 3
Date Collected:
6/25/2005
Client Project ID:
Almont Shipping
Date Received:
5/25/2005
Lab Sample ID:
G121-333-3
Matrix:
Water
Lab Project ID:
G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
86.2
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
135
0.1
mg/l
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
59.1
0.025
mg/1
353.3
5/31/2005
Envirachem
Phosphorus
0.49
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
538
5
mg/1
375.4
6/1/2005
Envirochem
TKN
115
0.1
mg/l
351.3
6/1/2005
Envirochem
Total Nitrogen
184
0.1
mg/I
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
0
N.C. CERTIFICATION #481
Reviewed By:
40 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
�• Client Sample ID:
MW-4
Date Collected:
5/25/2005
Client Project ID:
Almont Shipping
Date Received:
5/25/2005
Lab Sample ID:
G121-333-4
Matrix:
Water
Lab Project ID:
G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
1123
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
245
0.1
mg/I
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
59.1
0.025
mg/I
353.3
5/31/2005
Envirochem
Phosphorus
4.51
0.02
mg/l
365.2
5/27/2005
Envirochem
Sulfate
620
5
mg/I
375.4
6/1/2005
Envirochem
TKN
1154
0.1
mgll
351.3
6/1/2005
Envirochem
Total Nitrogen
1213
0.1
mg/I
353.3/351.3
6/1/2005
Envirochem
L�
0-
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By:
41 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
coClient Sample ID: MW 5 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2006
Lab Sample ID: G121-333-5 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
0.7
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
2185
0.1
mg/I
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
0.64
0.025
mg/I
353.3
5/31/2005
Envirochem
Phosphorus
0.48
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
302
5
mg/I
375.4
6/1/2005
Envirochem
TKN
3.9
0.1
mg/l
351.3
6/1/2005
Envirochem
Total Nitrogen
4.5
0.1
mg/1
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
0-
Reviewed By:
N.C. CERTIFICATION #481 42 of 77

(0
161
0-
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW-6 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2005
Lab Sample ID: G121-333-6 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
24.1
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
1364
0.1
mg/I
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
BQL
0.025
mg[I
353.3
5/31/2005
Envirochem
Phosphorus
0.72
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
29
5
mg/l
375.4
6/1/2005
Envirochem
TKN
44.8
0.1
mg/I
351.3
6/1/2005
Envirochem
Total Nitrogen
44.8
0.1
mg/l
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: c4,-0
43 of 77

(9-
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 7 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2005
Lab Sample ID: G121-333-7 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
7.6
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
3491
0.1
mg/I
SM 4500 CI-B
5/3M005
Envirochem
Nitrate
0.05
0.025
mg/I
353.3
5/31/2005
Envirochem
Phosphorus
1.73
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
BQL
5
mg/I
375.4
6/1/2005
Envirochem
TKN
8.4
0.1
mg/l
351.3
6/1/2005
Envirochem
Total Nitrogen
8.4
0.1
mg/1
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: _ ftiiP-
44 of 77

(6
0
i
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW-8 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/26/2005
Lab Sample ID: G121-333-8 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
4.6
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
20901
0.1
mg/I
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
BQL
0.025
mg/l
353.3
5/31/2005
Envirochem
Phosphorus
0.35
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
260
5
mg/l
375.4
6/1/2005
Envirochem
TKN
10.6
0.1
mg/I
351.3
6/1/2005
Envirochem
Total Nitrogen
10.6
0.1
mg/I
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: fZr1P
45 of 77

(9
0
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW-9 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2005
Lab Sample ID: G121-333-9 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
2.2
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
290
0.1
mg/I
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
BQL
0.025
mg/I
353.3
5/31/2005
Envirochem
Phosphorus
1.65
0.02
mg/I
365.2
5/27/2006
Envirochem
Sulfate
128
5
mg/I
375.4
6/1/2005
Envirochem
TKN
6.7
0.1
mg/I
351.3
6/1/2005
Envirochem
Total Nitrogen
6.7
0.1
mg/I
353.31351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: V-NQ
46 of 77

c.
(0
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 10 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2005
Lab Sample ID: G121-333-10 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
1820
0.1
mg/1
350.2
6/2/2005
Envirochem
Chloride
712
0.1
mg/l
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
27
0.025
mg/1
353.3
5/31/2005
Envirochem
Phosphorus
6.07
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
585
5
mg/I
375.4
6/1/2005
Envirochem
TKN
2100
0.1
mg/I
351.3
6/1/2005
Envirochem
Total Nitrogen
22"
0.1
mg/1
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: F-W
47 of 77

(•
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID:
MW 12 Date Collected: 5/25/2006
Client Project ID:
Almont Shipping Date Received: 5/25/2005
Lab Sample ID:
G121-333-11 Matrix: Water
Lab Project ID:
G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
35.6
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
428
0.1
mg/I
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
44
0.025
mg/l
353.3
5/31/2005
Envirochem
Phosphorus
0.13
0.02
mg/1
365.2
5/27/2005
Envirochem
Sulfate
94
5
mg/l
375.4
6/1/2005
Envirochem
TKN
37.8
0.1
mgll
351.3
6/1/2005
Envirochem
Total Nitrogen
88.1
0.1
mg/l
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: IzW
48 of 77

\•
L�
10
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID:
MW 13 Date Collected: 5/25/2005
Client Project ID:
Almont Shipping Date Received: 5/25/2005
Lab Sample ID:
G121-333-12 Matrix: Water
Lab Project ID:
G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
284
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
6888
0.1
mg/l
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
28.7
0.025
mg/I
353.3
5/31/2005
Envirochem
Phosphorus
0.16
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
730
5
mg/I
375.4
6/1/2005
Envirochem
TKN
297
0.1
mg/I
351.3
6/1/2005
Envirochem
Total Nitrogen
344
0.1
mg/I
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: PAID
49 of 77

AD
0-
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 14 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2005
Lab Sample ID: G121-333-13 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
2919
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
7838
0.1
mg/I
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
614
0.025
mg/l
353.3
5/31/2005
Envirochem
Phosphorus
0.91
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
1710
5
mg/I
375.4
6/1/2005
Envirochem
TKN
3332
0.1
mg/I
351.3
6/1/2005
Envirochem
Total Nitrogen
4286
0.1
mg/I
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: (tt-('
50 of 77

c0
0-
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: MW 15 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2005
Lab Sample ID: G121-333-14 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
3180
0.1
mg/i
350.2
6/2/2005
Envirochem
Chloride
14726
0.1
mg/1
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
317
0.025
mg/I
353.3
5/31/2005
Envirochem
Phosphorus
5.21
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
2790
5
mg/I
375.4
6/1/2005
Envirochem
TKN
3920
0.1
mg/1
351.3
6/1/2005
Envirochem
Total Nitrogen
4250
0.1
mg/I
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: *s P
51 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
co, Client Sample ID: MW-16 Date Collected: 5/25/2005
Client Project ID:
Almont Shipping
Date Received:
5/25/2005
Lab Sample ID:
G121-333-17
Matrix:
Water
Lab Project ID:
G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
23.9
0.1
mg/l
350.2
6/2/2005
Envirochem
Chloride
176
0.1
mg/I
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
BQL
0.025
mg/I
353.3
5/31/2005
Envirochem
Phosphorus
2.5
0.02
mg/1
365.2
5/27/2005
Envirochem
Sulfate
158
5
mg/I
375.4
6/1/2005
Envirochem
TKN
29.1
0.1
mg/l
351.3
6/1/2005
Envirochem
Total Nitrogen
29.1
0.1
mg/l
353.31351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
(0
N.C. CERTIFICATION #481
Reviewed By: "
54 of 77

(0
0-
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: LM-13 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2005
Lab Sample ID: G121-333-18 Matrix: Water
Lab Project ID: G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
0.4
0.1
mg/l
350.2
6/2/2005
Envirochem
Chloride
18.6
0.1
mg/l
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
3.16
0.025
mg/I
353.3
5/31/2005
Envirochem
Phosphorus
0.94
0.02
mg/l
365.2
5/27/2005
Envirochem
Sulfate
33
5
mg/I
375.4
6/1/2005
Envirochem
TKN
2
0.1
mg/l
351.3
6/1/2005
Envirochem
Total Nitrogen
5.2
0.1
mg/l
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By: 0t-d -_
55 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID:
DW 1
Date Collected:
5/25/2005
Client Project ID:
Almont Shipping
Date Received:
5/25/2005
Lab Sample ID:
G121-333-15
Matrix:
Water
Lab Project ID:
G121-333
Analyte
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
1.7
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
89
0.1
mg/I
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
BQL
0.025
mg/l
353.3
5/31/2005
Envirochem
Phosphorus
0.15
0.02
mg/I
365.2
5/27/2005
Envirochem
Sulfate
16
5
mg/l
375.4
6/1/2005
Envirochem
TKN
6.2
0.1
mg/I
351.3
6/1/2005
Envirochem
Total Nitrogen
6.2
0.1
mg/I
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
0-
N.C. CERTIFICATION #481
Reviewed By: 0-tO
52 of 77

(0
0-
10
PARADIGM ANALYTICAL LABORATORIES, INC.
Analytical Results
Client Sample ID: DW 2 Date Collected: 5/25/2005
Client Project ID: Almont Shipping Date Received: 5/25/2005
Lab Sample ID: G121-333-16 Matrix: Water
Lab Project ID: G121-333
Analyse
Result
RL
Units
Method
Date
Analyst
Analyzed
Ammonia
2394
0.1
mg/I
350.2
6/2/2005
Envirochem
Chloride
2209
0.1
mg/I
SM 4500 CI-B
5/31/2005
Envirochem
Nitrate
188
0.025
mg/I
353.3
5/31/2005
Envirochem
Phosphorus
3.49
0.02
mg/1
365.2
5/27/2005
Envirochem
Sulfate
392
5
mg/I
375.4
6/1/2005
Envirochem
TKN
3780
0.1
mg/l
351.3
6/1/2005
Envirochem
Total Nitrogen
4075
0.1
mg/l
353.3/351.3
6/1/2005
Envirochem
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
RL = Report Limit
N.C. CERTIFICATION #481
Reviewed By:
53 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
Client Sample ID:
MW-1
Client Project ID:
Almont Shipping
Lab Sample ID:
G121-333-1
Lab Project ID:
G121-333
Batch ID:
2909 2985
Analyzed By:
PSW
Date Collected:
5/25/2005 07:00
Date Received:
5/25/2005
Matrix:
WATER
Metals
Result
RL
DF
Units
Method
Arsenic
0.0248
0.0100
1
MG/L
6010B
Barium
BQL
0.100
1
MG/L
6010B
Cadmium
BQL
0.0100
1
MG/L
6010B
Chromium
BQL
0.0100
1
MG/L
6010B
Lead
BQL
0.0100.
1
MG/L
6010E
Mercury
BQL
0.000250
1
MG/L
7470
Selenium
BQL
0.0200
1
MG/L
6010B
Silver
BQL
0.0100
1
MG/L
6010B
Comments
BQL = Below Quantitation Limits
�- DF = Dilution Factor
J = Between MDL and RL
0-
N.C. CERTIFICATION #481
Date
Analyzed
6/7/2005
6/7/2005
6/9/2005
6/7/2005
6/7/2005
6/9/2005
6/7/2005
6/7/2005
Reviewed By: V-tV _
MET_UMS_3.1
56 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
•
Client Sample ID:
MW-2
Analyzed B
Y Y�
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/25/2005 07:20
Lab Sample ID:
G121-333-2
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
0.0304
0.0100
1
MG/L
6010B
6/7/2005
Barium
BQL
0.100
1
MG/L
6010E
6/7/2005
Cadmium
BQL
0.0100
1
MG/L
6010E
6/9/2005
Chromium
BQL
0.0100
1
MG/L
6010B
•617/2005
Lead
BQL
0.0100
1
MG/L
6010B
6/7/2005
Mercury
BQL
0.000250
1
MG/L
7470
6/9/2005
Selenium
BQL
0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL
0.0100
1
MG/L
6010B
6/7/2005
Comments
L BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
10
N.C. CERTIFICATION #481
Reviewed By: g -
"'--1.1
57 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
Client Sample ID:
MW-3
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/25/2005 07:40
Lab Sample ID:
G121-333-3
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
BQL
0.0100
1
MG/L
6010B
6/7/2005
Barium
BQL
0.100
1
MG/L
6010B
6/7/2005
Cadmium
BQL
0.0100
1
MG/L
6010B
6/9/2005
Chromium
BQL
0.0100
1
MG/L
6010E
6/7/2005
Lead
BQL
0.0100
1
MG/L
6010B
6/7/2005
Mercury
BQL
0.000250
1
MG/L
7470
6/9/2005
Selenium
BQL
0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL
0.0100
1
MG/L
6010B
6/7/2005
Commonts
( BQL = Below Quantitation Limits
\- DF = Dilution Factor
J = Between MDL and RL
(0
N.C. CERTIFICATION #481
Reviewed By: 94
MET LIMS Sad of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
��•
PSW
Client Sample ID:
MW-4
Analyzed By:
Client Project ID:
Almont Shipping
Date Collected:
5/25/2005 08:00
Lab Sample ID:
G121-333-4
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
0.911
0.0100
1
MG/L
6010E
6/7/2005
Barium
BQL
0.100
1
MG/L
6010B
6/7/2005
Cadmium
BQL
0.0100
1
MG/L
6010B
6/9/2005
Chromium
0.0253
0.0100
1
MG/L
6010B
6/7/2005
Lead
0.0334
0.0100
1
MG/L
6010B
6/7/2005
Mercury
0.00427
0.000250
1
MG/L
7470
6/9/2005
Selenium
BQL
0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL
0.0100
1
MG/L
6010E
6/7/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
l�
N.C. CERTIFICATION #481
Reviewed By:
MET-UMs 189 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
C
PSW
Client Sample ID:
MW-S
Analyzed By:
Client Project ID:
Almont Shipping
Date Collected:
5/25/2005 08:20
Lab Sample ID:
G121-333-5
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
BQL
0.0100
1
MG/L
6010B
6/7/2005
Barium
BQL
0.100
1
MG/L
6010B
6/7/2005
Cadmium
BQL
0.0100
1
MG/L
6010B
6/9/2005
Chromium
BQL
0.0100
1
MG/L
6010B
6/7/2005
Lead
0.0137
0.0100
1
MG/L
6010B
6/7/2006
Mercury
BQL
0.000250
1
MG/L
7470
6/9/2005
Selenium
BQL
0.0200
1
MG/L
6010E
6/7/2005
Silver
BQL
0.0100
1
MG/L
6010B
6/7/2005
• Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
N.C. CERTIFICATION #481
Reviewed By:
ME` `W- 360 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
Client Sample ID:
MW-6
Analyzed By:
PSW
Client Project ID:
Aimont Shipping
Date Collected:
5/25/2005 08:40
Lab Sample ID:
G121-333-6
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
BQL
0.0100
1
MG/L
6010E
6/7/2005
Barium
0.129
0.100
1
MG/L
6010E
6/7/2005
Cadmium
BQL
0.0100
1
MG/L
6010B
6/9/2005
Chromium
BQL
0.0100
1
MG/L
6010B
6/7/2005
Lead
BQL
0.0100
1
MG/L
6010E
6/7/2005
Mercury
BQL
0.000250
1
MG/L
7470
6/9/2005
Selenium
BQL
0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL
0.0100
1
MG/L
6010B
6/7/2005
• Comments
BQL = Below Quantitation Limits
_ DF = Dilution Factor
J = Between MDL and RL
•
N.C. CERTIFICATION #481
Reviewed By: # -� 4
MET_.IM8_3.1
61 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
coClient Sample ID: MW-7
Client Project ID: Almont Shipping
Lab Sample ID: G121-333-7
Lab Project ID: G121-333
Batch ID: 2909 2985
•
Analyzed By:
PSW
Date Collected:
5/25/2005 09:00
Date Received:
5/25/2005
Matrix:
WATER
Metals
Result
RL
DF
Units
Method
Arsenic
0.0881
0.0100
1
MG/L
6010B
Barium
BQL
0.100
1
MG/L
6010B
Cadmium
BQL
0.0100
1
MG/L
6010B
Chromium
0.0253
0.0100
1
MG/L
6010E
Lead
BQL
0.0100
1
MG/L
6010B
Mercury
BQL
0.000250
1
MG/L
7470
Selenium
BQL
0.0200
1
MG/L
6010B
Silver
BQL
0.0100
1
MG/L
6010B
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
N.C. CERTIFICATION #481
Date
Analyzed
6/7/2005
6/7/2005
6/9/2005
6/7/2005
6/7/2005
6/9/2005
6/7/2005
6/7/2005
Reviewed By: V-a_
MET'- L"' 62 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
`'• Client Sample ID:
MW-8
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/25/2005 09:20
Lab Sample ID:
G121-333-8
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result
RL
DF
Units
Method
Date
Analyzed
Arsenic
0.0266
0.0100
1
MG/L
6010E
6/7/2005
Barium
0.315
0.100
1
MG/L
6010E
6/7/2005
Cadmium
BQL
0.0100
1
MG/L
6010B
6/9/2005
Chromium
BQL
0.0100
1
MG/L
6010B
6/7/2005
Lead
BQL
0.0100
1
MG/L
6010B
6/7/2005
Mercury
BQL
0.000250
1
MG/L
7470
6/9/2005
Selenium
BQL
0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL
0.0100
1
MG/L
6010B
6/7/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
0
N.C. CERTIFICATION #481
Reviewed By: g+,ie
uMs_63 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
By:
PSW
`. Client Sample ID:
MW-9
Analyzed
Client Project ID:
Aimont Shipping
Date Collected:
5/25/2005 09:40
Lab Sample ID:
G121-333-9
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result
RL
OF
Units
Method
Date
Analyzed
Arsenic
0.0133
0.0100
1
MG/L
6010B
6/7/2005
Barium
BQL
0.100
1
MG/L
6010B
617/2005
Cadmium
BQL
0.0100
1
MG/L
6010B
6/9/2005
Chromium
BQL
0.0100
1
MG/L
6010B
6/7/2005
Lead
BQL
0.0100
1
MG/L
6010B
6/7/2005
Mercury
BQL
0.000260
1
MG/L
7470
6/9/2005
Selenium
BQL
0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL
0.0100
1
MG/L
6010B
6/7/2005
Comments
BQL = Below Quantitation Limits
CP DF = Dilution Factor
J = Between MDL and RL
0 1,
Reviewed By: f-4_
MET_LMIS_3.1
N.C. CERTIFICATION #481 64 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
By:
PSW
Client Sample ID:
MW-10
Analyzed
Client Project ID:
Aimont Shipping
Date Collected:
5/25/200510:00
Lab Sample ID:
G121-333-10
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result RL
OF
Units
Method
Date
Analyzed
Arsenic
0.713 0.0100
1
MG/L
6010B
6/7/2005
Barium
BQL 0.100
1
MG/L
6010B
6/7/2005
Cadmium
BQL 0.0100
1
MG/L
6010E
6/9/2005
Chromium
BQL 0.0100
1
MG/L
6010B
6/7/2005
Lead
BQL 0.0100
1
MG/L
60108
6/7/2005
Mercury
0.000269 0.000250
1
MG/L
7470
6/9/2005
Selenium
0.0240 0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL 0.0100
1
MG/L
6010B
6/7/2005
Comments
BQL = Below Quantitation Limits
le DF = Dilution Factor
J = Between MDL and RL
`w
N.C. CERTIFICATION #481
Reviewed By: ?d
MET_`" 65 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
Client Sample ID:
MW-12
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/25/200510:40
Lab Sample ID:
G121-333-11
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result RL
DF
Units
Method
Date
Analyzed
Arsenic
BQL 0.0100
1
MG/L
6010E
6/7/2005
Barium
BQL 0.100
1
MG/L
6010B
6/7/2005
Cadmium
BQL 0.0100
1
MG/L
6010B
6/9/2005
Chromium
BQL 0.0100
1
MG/L
6010B
6/7/2005
Lead
BQL 0.0100
1
MG/L
6010B
6/7/2005
Mercury
BQL 0.000250
1
MG/L
7470
6/9/2005
Selenium
BQL 0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL 0.0100
1
MG/L
6010B
6/7/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
t.•
N.C. CERTIFICATION #481
Reviewed By: CAP
"366 0f 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
=� Client Sample ID:
MW-13
Client Project ID:
Almont Shipping
Lab Sample ID:
G121-333-12
Lab Project ID:
G121-333
Batch ID:
2909 2985
Analyzed By:
PSW
Date Collected:
5/25/200511:20
Date Received:
5/25/2005
Matrix:
WATER
Metals
Result
RL
DF
Units
Method
Arsenic
0.0137
0.0100
1
MG/L
6010B
Barium
0.413
0.100
1
MG/L
6010B
Cadmium
BQL
0.0100
1
MG/L
6010B
Chromium
BQL
0.0100
1
MG/L
6010B
Lead
BQL
0.0100
1
MG/L
6010B
Mercury
BQL
0.000250
1
MG/L
7470
Selenium
BQL
0.0200
1
MG/L
6010B
Silver
BQL
0.0100
1
MG/L
6010B
• Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
A
Date
Analyzed
6/7/2005
6/7/2005
6/9/2005
6/7/2005
6/7/2005
6/9/2005
6/7/2005
6/7/2005
Reviewed By: V-v-+P
MET LIMS_3.i
N.C. CERTIFICATION #481 67 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
�•
Client Sample ID:
MW-14
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/25/200511:40
Lab Sample ID:
G121-333-13
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result RL
DF
Units
Method
Date
Analyzed
Arsenic
0.0622 0.0100
1
MG/L
6010E
6/7/2005
Barium
BQL 0.100
1
MG/L
6010E
6/7/2005
Cadmium
BQL 0.0100
1
MG/L
6010B
6/9/2005
Chromium
BQL 0.0100
1
MG/L
6010B
6/7/2005
Lead
BQL 0.0100
1
MG/L
6010B
6/7/2005
Mercury
BQL 0.000250
1
MG/L
7470
6/9/2005
Selenium
0.0443 0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL 0.0100
1
MG/L
6010B
6/7/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
N.C. CERTIFICATION #481
Reviewed By: q-4_
MET 41 3.1
68 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
Analyzed By:
PSW
Client Sample ID:
MW-15
Client Project ID:
Almont Shipping
Date Collected:
5/25/200512:00
Lab Sample ID:
G121-333-14
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result RL
DF
Units
Method
Date
Analyzed
Arsenic
0.0596 0.0100
1
MG/L
6010B
6/7/2005
Barium
BQL 0.100
1
MG/L
6010B
6/7/2005
Cadmium
BQL 0.0100
1
MG/L
6010B
6/9/2005
Chromium
0.0144 0.0100
1
MG/L
6010B
6/7/2005
Lead
0.0308 0.0100
1
MG/L
6010B
6/7/2005
Mercury
0.00165 0.000250
1
MG/L
7470
6/9/2005
Selenium
0.0645 0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL 0.0100
1
MG/L
6010E
6/7/2005
• Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
11
N.C. CERTIFICATION #481
Reviewed By: _ F:a1!<
MET_LN 369 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
Client Sample ID:
MWA6
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/25/200511:00
Lab Sample ID:
G121-333-17
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2965
Metals
Result RL
DF
Units
Method
Date
Analyzed
Arsenic
0.0129 0.0100
1
MG/L
6010B
6/7/2005
Barium
0.115 0.100
1
MG/L
6010B
6/7/2005
Cadmium
BQL 0.0100
1
MG/L
6010B
6/9/2005
Chromium
BQL 0.0100
1
MG/L
6010B
6/7/2005
Lead
BQL 0.0100
1
MG/L
6010B
6/7/2005
Mercury
BQL 0.000260
1
MG/L
7470
6/9/2005
Selenium
BQL 0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL 0.0100
1
MG/L
6010B
6/7/2005
Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
N.C. CERTIFICATION #481
Reviewed By: V-4_
MEf UMS_3.1
72 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
�•
Client Sample ID:
LM-13
Analyzed By:
PSW
Client Project ID:
Almont Shipping
Date Collected:
5/25/200513:00
Lab Sample ID:
G121-333-18
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result RL
DF
Units
Method
Date
Analyzed
Arsenic
BQL 0.0100
1
MG/L
6010B
6/7/2005
Barium
BQL 0.100
1
MG/L
6010B
6/7/2005
Cadmium
BQL 0.0100
1
MG/L
6010E
6/9/2005
Chromium
BQL 0.0100
1
MG/L
6010B
6/7/2005
Lead
BQL 0.0100
1
MG/L
6010B
6/7/2005
Mercury
BQL 0.000250
1
MG/L
7470
6/9/2005
Selenium
BQL 0.0200
1
MG/L
6010B
6/9/2005
Silver
BQL 0.0100
1
MG/L
6010B
6/7/2005
• Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
N.C. CERTIFICATION #481
Reviewed By: V-d
eer_um 3 3 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
Client Sample ID:
DW-1
Analyzed By:
PSW
Client Project ID:
Aimont Shipping
Date Collected:
5/25/200512:20
Lab Sample ID:
G121-333-15
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result RL
DF
Units
Method
Date
Analyzed
Arsenic
BQL 0.0100
1
MG/L
6010B
6/7/2005
Barium
BQL 0.100
1
MG/L
6010B
6/7/2005
Cadmium
BQL 0.0100
1
MG/L
6010B
6/9/2005
Chromium
BQL 0.0100
1
MG/L
6010B
6/7/2005
Lead
BQL 0.0100
1
MG/L
6010E
6/7/2005
Mercury
BQL 0.000250
1
MG/L
7470
6/9/2005
Selenium
BQL 0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL 0.0100
1
MG/L
6010B
6/7/2005
• Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
A
Reviewed By: _g a
MET IIMS_3
N.C. CERTIFICATION #481 0 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Metals
`• Client Sample ID:
DW-2
Analyzed By:
PSW
Client Project ID:
Aimont Shipping
Date Collected:
5/25/200512:40
Lab Sample ID:
G121-333-16
Date Received:
5/25/2005
Lab Project ID:
G121-333
Matrix:
WATER
Batch ID:
2909 2985
Metals
Result RL
DF
Units
Method
Date
Analyzed
Arsenic
0.0937 0.0100
1
MG/L
6010B
6/7/2006
Barium
BQL 0.100
1
MG/L
6010B
6/7/2005
Cadmium
BQL 0.0100
1
MG/L
6010B
6/9/2005
Chromium
0.0278 0.0100
1
MG/L
6010E
6/7/2005
Lead
BQL 0.0100
1
MG/L
6010B
6/7/2005
Mercury
BQL 0.000250
1
MG/L
7470
6/9/2005
Selenium
0.0583 0.0200
1
MG/L
6010B
6/7/2005
Silver
BQL 0.0100
1
MG/L
6010B
6/7/2005
Ce Comments
BQL = Below Quantitation Limits
DF = Dilution Factor
J = Between MDL and RL
A
Reviewed By: V--tJ
'Ms s
N.C. CERTIFICATION #481 1 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
A
(0
(•
Results for Total Petroleum Hydrocarbons Product Identification
by GC/FID 8015
Client Sample ID: MW-11
Client Project ID: Almont Shipping
Lab Sample ID: G121-333-19
Lab Project ID: G121-333
Analyzed By: DCS
Date Collected: 5/25/0512:10
Date Received: 5/25/05
Matrix: Product
Analyte Prep Date
Method Analyzed
Diesel Range Organics 3520 06/09/05
The chromatogram elutes in the diesel #2 time range. However, the pattern is not
similar to the diesel #2 standard.
The chromatogram profile suggests the sample may contain severely degraded
diesel or heating all.
Additionally, several large peaks eluted near the ending time for diesel #2.
A GC/MS analysis is required for identification of these peaks.
Reviewed By:
N.C. CERTIFICATION #481 TaH LIB %1.71 l4 of 77

PARADIGM ANALYTICAL LABORATORIES, INC.
List of Reporting Abbreviations
and Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantitation Limit
DF = Dilution Factor
Dup = Duplicate
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL = Reporting Limit
RPD = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
M134.011404.1
N.C. CERTIFICATION #481 75 of 77

PARADIGM ANALYTICAL LABORATORIES, INC. 47130 CO
5500 Business Drive, Wilmington, NC 28405 Chain -of Custody Record & Analytical Request r`
Phone: [phone] 'FAX: [phone] Page // ofV
Client: Project ID: Date: 5 b \� Report To: �' b 13�3'Ag
oZ
Address: Contact: Turnaround:
Address., Phone: Job Number:
nnntp. #- Fax: P.O. Number: Invoice To:
NO
Erg
NIMBI
NOME
SO.S.
NPA
WONVAOL
PAS
ml
S
FAI
WON
Film-
�-
■■
: 0inNONE►��,�►�Nip
���/:�011
■■
��
0000
&41
Q4SON
�+�mommumr�►�a�
N

PARADIGM ANALYTICAL LABORATORIES, INC.
5500 Business Drive, Wilmington, NC 28405
Phone• 910)-350-1903 FAX: [phone]
l..IN A P-11m),
Client: V
Address:
Address:
[note A
Project ID;
Contact:
Phone:
Fax:
Chain -of Custody Record & Analytical Request
Date: s ��
Turnaround:
Job Number: a �
P.O. Number:
cOc# 47128 f-
Page —:I-- of7z—
Report To: V;M� J f��\tb
Invoice To:
Ak
M
PU
IS
00
0000
AN
FAWN
4
RAL
1
IN
IN
AN,
AM
14
5
W
AN
6% "
MWARM
I ri
W 9
k
NEW
MES9
1MM=EFJLAQ4R%
Or
WON
.14
01AG
0
o
n
IMMEM111130
A.
6
11M
A M4k
F4&Jk
a
0
A
SEMI
0
0000
11010430100631A
FNAM
1111101111
MEMO
HE
®R,
IS
VIA
%L
moommommommommom
o�m
ZjF al