23068_Sir Walter Gun Club_O_20130214

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Reconnaissance Investigation Results
Former Sir Falter Gran Club Site
Knightdale, North Carolina
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Hinton Lance LLC
Po Box 1277
Knightdale, NC 27545
AMEC Environment & Infrastructure, Inc.
285 Davidson Avenue, suite 405
Somerset, NJ 08 873
February 14, 2013

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TABLE OF CONTENTS
1.0 INTRODUCTION............................................................................................................... 1
2.0 BACKGROUND INFORMATION....................................................................................... 2
2.1 PHYSICAL SETTING..................................................................................................... 2
2.2 PREVIOUS ENVIRONMENTAL INVESTIGATIONS AND REMEDIAL WORK ............................. 3
2.2.1 1988 Investigation......................................................................................... 3
2.2.2 1991 Remedial Work..................................................................................... 3
2.2.3 2010 Investigation......................................................................................... 4
2.3 REGULATORY STATUS................................................................................................ 5
3.0 METHODS........................................................................................................................ 6
3.1 HISTORICAL REVIEW................................................................................................... 6
3.2 FIELD AND LABORATORY METHODS............................................................................. 6
3.2.1 Field Sieving Analysis of Soil......................................................................... 7
3.2.2 Soil Sampling for Laboratory Analysis........................................................... 8
4.0 FINDINGS......................................................................................................................... 9
4.1 HISTORICAL REVIEW................................................................................................... 9
4.2 FIELD RECONNAISSANCE AND SOIL SAMPLING RESULTS ............................................. 10
4.2.1 Rifle Ranges................................................................................................ 10
4.2.2 Skeet Field.................................................................................................. 11
4.2.3 Area Downrange of Former Rifle Range ...................................................... 11
5.0 CONCLUSIONS.............................................................................................................. 13
6.0 PRELIMINARY DISCUSSION OF REMEDIAL OPTIONS ............................................... 15
6.1 PROPOSED SITE DEVELOPMENT................................................................................ 15
6.2 BERMS.....................................................................................................................15
6.3 SOILS AT SKEET FIELD AND RANGE FLOORS.............................................................. 16
6.4 SOIL STOCKPILE....................................................................................................... 16
7.0 REFERENCES................................................................................................................ 17
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Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 i

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LIST OF TABLES
Table 1 Results of Field Sieving Analysis of Skeet Field Soil Samples
Table 2 Summary of Laboratory Analytical Results for Soil
LIST OF FIGURES
Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Results of Historical Aerial Photographic Analysis - 1959
Figure 4 Results of Historical Aerial Photographic Analysis - 1971
Figure 5 Results of Historical Aerial Photographic Analysis - 2010
Figure 6 Field Reconnaissance and Soil Sample Location Map
LIST OF APPENDICES
Appendix A January 1989 Atwood Memorandum
Appendix B March 1992 Letter by Paragon Environmental Group, Inc.
Appendix C January 2011 Letter Report by S&ME, Inc.
Appendix D October 2000 Memorandum by NCDENR Site Evaluation and
Removal Branch
Appendix E Site Photographs
Appendix F Laboratory Reports
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Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 ii

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LIST OF ACRONYMS AND ABBREVIATIONS
AMEC AMEC Earth & Environmental, Inc.
BMP Best Management Practice
g gram
GIS Geographic Information System
GPS Global positioning system
ITRC Interstate Technology and Regulatory Council
kg
kilogram
mg/kg
Milligrams per kilogram
NCDENR
North Carolina Department of Environment and Natural Resources
NCDOT
North Carolina Department of Transportation
NELAC
National Environmental Laboratory Accreditation Conference
PSRG
NCDENR Preliminary Soil Remediation Goal
SAFR
Small Arms Firing Range
SPLP
Synthetic Precipitation Leaching Procedure
TCLP
Toxicity Characteristic Leaching Procedure
UNC
University of North Carolina
USDA
U.S. Department of Agriculture
USEPA
U.S. Environmental Protection Agency
USGS
United States Geological Survey
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Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 iii

1.0 INTRODUCTION
This report describes the results of a reconnaissance investigation at the site of a former
outdoor small -arms firing range (SAFR) complex which was operated by the Sir Walter Gun
Club (Gun Club) between 1950 and 1988. The subject property, which is owned by Hinton
Land LLC (Client), is located approximately 1,500 feet northeast of the intersection of the US
Hwy 64 East with US Route 540, in Knightdale, Wake County, North Carolina. A site location
map is provided in Figure 1. The property is comprised of two contiguous parcels with a total
land area of approximately 49 acres, as shown in Figure 2.
AMEC Environment & Infrastructure, Inc. (AMEC) was hired by the Client to perform an initial
reconnaissance investigation of the former Gun Club facilities in order to identify and map the
approximate extent of areas which may have been impacted by former Gun Club operations,
and to begin to consider strategies for the cost effective management of lead contaminated
soil (if any) associated with former Gun Club operations. Additionally, the Client requested
that soil sampling be performed at the area of the property located behind (downrange of) the
200-yard impact berm of the former rifle range (refer to Figure 2), to confirm whether there
were environmental impacts in that area associated with former range operations by the Gun
Club.
The scope of the investigation included a review of readily accessible historical information
pertaining to the site, (e.g., property surveys, historic aerial photographs, results of previous
environmental investigations, etc.), a field reconnaissance investigation to verify the nature
and locations of the former Gun Club facilities, and targeted sampling and analysis of surface
soils within and downrange of the former firing ranges.
The specific objectives of the investigation were to:
Evaluate the nature and potential horizontal extent of lead impacts to soil associated
with the former SAFR operations by the Gun Club;
2. Develop a preliminary understanding of the Client's proposed use of the Site; and
3. Begin to identify strategies for the cost effective management of any lead
contaminated soil.
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Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013

2.0 BACKGROUND INFORMATION
The property containing the former outdoor SAFR was part of the historic Midway Plantation,
much of which has been subdivided into commercial lots for redevelopment. The historic
buildings that were formerly present at the main plantation site were relocated to another
property during 2005'. The former Gun Club site is located on one of the remaining
undeveloped parcels. The Gun Club leased a portion of the property from about 1950 until
1988 for use as a recreational firing range. The Gun Club ceased operations at the property
during 1988, at which time it was relocated to a new facility in Creedmoor, North Carolina.
Range facilities that were historically operated by the Gun Club at the site consisted of two
adjacent rifle ranges with nominal target distances of 100 yards and 200 yards; a 50-yard
pistol range; and a combined skeet and trap field (refer to Figure 2). The rifle ranges
included earthen backstops (impact berms), which were approximately 10 feet high and
appear to have been constructed from soil obtained onsite. The skeet field was located
immediately east of the 100-yard range, from which it was separated by an earthen side
berm approximately 80 feet long and 7 feet high. The pistol range, which has been removed
and covered by commercial development, was formerly located on a parcel immediately
south of the subject property, which was subdivided and sold during 2005.
2.1 PHYSICAL SETTING
The property is located at an elevation of approximately 250 to 300 feet above mean sea
level (Figure 1), and situated within the Neuse River Basin. Two small streams (one of which
is an intermittent stream) traverse the property (Figure 2). The streams flow northwest and
converge offsite before discharging into a nearby pond which, in turn, drains into a stream
flowing westward toward Milburnie Lake and the Neuse River.
The property is entirely covered by forest and is densely vegetated. No storm drains,
culverts, or other engineered stormwater collection systems were observed at the property.
Access to the site is from Hinton Oaks Boulevard (Figure 2).
The soils observed during the field reconnaissance typically consisted of fine sandy loam,
with varying proportions of silt, clay, and humic material. According to the soil survey data
available from the U.S. Department of Agriculture (USDA) National Resources Conservation
Service (MRCS), the soil immediately underlying the Gun Club site consists of the following
mapped units:
DuB - Durham loamy sand, 2 to 6 percent slopes
DuB2 - Durham loamy sand, 2 to 6 percent slopes, moderately eroded
LoC - Louisburg loamy sand, 6 to 10 percent slopes
WaY - Worsham sandy loam, 0 to 3 percent slopes
The bedrock beneath the site consists of granitic igneous rocks associated with the
Rollesville batholith. The depth to groundwater was not determined during this investigation.
'Additional information concerning the history of the Midway Plantation is available at the Midway
Plantation website http://www.midwayplantation.com.
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Former Sir Walter Gun Club Site
Knightdale, North Carolina
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2.2 PREVIOUS ENVIRONMENTAL INVESTIGATIONS AND REMEDIAL WORK
2.2.1 1988 Investigation
On November 9, 1988, Mr. Stanley Atwood, a toxicologist with the North Carolina
Department of Environment and Natural Resources (NCDENR) Division of Waste
Management Superfund Branch, collected soil samples from the pistol range, rifle ranges,
and the skeet field for laboratory analysis of metals (arsenic, barium, cadmium, chromium,
copper, lead, mercury, and selenium) and semi -volatile organic compounds. A sample of
groundwater was also collected for analysis of metals from a former 60-foot deep well that
was reportedly located up -range of the former pistol range (Figure 3). The well was located
offsite of the subject property, on the parcel that was previously sold and redeveloped (refer
to Section 2.0). The results were reported in a January 31, 1989 memorandum from Mr.
Atwood to the NCDENR Director of Budget and Analysis, a copy of which was provide to
AMEC by the Gun Club. A copy of the Atwood memorandum is attached as Appendix A.
The Atwood memorandum reported the following laboratory analytical results:
a) All of the analytical results for the groundwater sample were below the reported
laboratory detection limits.
b) Total lead concentrations reported in composite soil samples collected from the 100-
yard and 200-yard impact berms at the rifle ranges were 11,600 and 7,200 mg/kg
(milligrams per kilogram), respectively.
c) A total lead result of 93,000 mg/kg was reported for a sample collected from the pistol
range impact berm.
d) Traces of polynuclear aromatic hydrocarbons (PAHs) were detected in the soil
samples collected from the 100-yard rifle range impact berm and the pistol range
berm. The specific PAH compounds detected in the samples, which were reported at
concentrations below 10 mg/kg, are commonly associated with coal tar products such
as pitch and asphalt. Clay target manufacturers commonly used coal -tar pitch as a
binder.
e) Soil samples that were reportedly collected at unspecified locations at "the edge of
the skeet range" and the "woods beyond the skeet range" both yielded results for lead
below the reported detection limits of 18 to 19 mg/kg. The samples were collected at
depth intervals of 0 to 8 inches and 0 to 10 inches below grade, respectively. Based
on the memorandum, it is unclear whether the samples collected within the skeet field
were also analyzed for PAHs. However no detections of PAHs in the skeet field soils
were noted in the memorandum.
The Atwood memorandum states, "High levels of lead were found in each of the three berms.
In addition, low levels of several polyaromatic hydrocarbons were found in the berms at the
pistol range and the 100 yard rifle range." The conclusion presented in the memorandum
was: "The lead levels in the berms were high enough to be of environmental concern".
2.2.2 1991 Remedial Work
During August and September of 1991, limited excavation, removal, and screening of soils
from the impact berms was performed by Paragon Environmental Group, Inc. (Paragon), on
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Former Sir Walter Gun Club Site
Knightdale, North Carolina
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behalf of the Gun Club. In a March 10, 1992 letter report to the Gun Club (a copy of which is
provided as Appendix B), Paragon reported removing soil from the front (impact) face of
each of the three impact berms (100-yard and 200-yard rifle ranges and the 50-yard pistol
range), which was processed through a mobile, 2-deck, vibratory screening plant equipped
with '/4-inch and 3%-inch mesh screens. The soil was reportedly excavated from each impact
berm face to a depth of approximately 12 inches, from the toe of the berm slope to a height
of 6 feet above the range floor. Above the 6-foot level, the soil was excavated to a depth of
approximately 8 inches. No field observations or laboratory analytical results were provided
in the report to explain the choice of excavation depths.
Based on the berm dimensions and excavation depths described in the Paragon report,
AMEC has calculated an estimated soil removal volume of approximately 200 cubic yards of
soil. The screened soil (i.e., material passing the '/-inch mesh screen) was reportedly
transported to the current Sir Walter Gun Club facility in Creedmoor, North Carolina for
beneficial reuse as impact -berm material. A total of nineteen 55-gallon drums (about 5 cubic
yards) containing mixed bullets and gravel recovered from the soil were shipped to Master
Metals, Inc.2 in Cleveland Ohio for recycling. A total of 11,992.8 pounds of metal was
reportedly recovered and smelted. Assuming an in -situ soil bulk density in the range of 1.3
to 1.5 tons per cubic yard, this is equivalent to a total recoverable metal content (i.e., for
particles larger than '/4 inch in diameter) of between 3 and 3.5% by weight.
2.2.3 2010Investigation
On October 12, 2010, working on behalf of the Gun Club, S&ME, Inc. (S&ME) collected soil
samples from the 100-yard and 200-yard rifle range impact berms for laboratory analysis of
total lead. Selected samples were also analyzed for total arsenic, PAHs, and (or) leachable
lead using the Toxicity Characteristic Leaching Procedure (TCLP)3. The soil samples, which
were collected from the front and rear faces of each of the impact berms, were collected from
6-inch vertical intervals at depths of up to 30 inches below the existing grade (i.e., depth
intervals of 0 to 6, 6 to 18, 18 to 24 and 24 to 30 inches). The results were presented in a
January 4, 2011 letter report submitted to the Gun Club (S&ME, 2011), a copy of which was
provided to AMEC (Attached as Appendix C).
S&ME results for 100-yard berm: Within the 100-yard impact berm, total lead concentrations
ranging from 35 to 5,100 mg/kg were detected in the soil. Test results exceeding the
NCDENR Preliminary Residential Health -Based Soil Remediation Goal (PSRG) of 400 mg/kg
and the Protection of Ground Water PSRG of 270 mg/kg for total lead were reported at
depths of up to 30 inches below grade. Traces of arsenic and PAHs were detected in the
samples collected from the 0 to 6 inch depth interval at concentrations above their respective
PSRGs. The soil sample in which the highest total lead concentration was detected was also
analyzed for TCLP lead. The TCLP lead result was 91 mg/L (milligrams per liter), which was
above the federal the regulatory threshold level of 5 mg/L for disposal of solid waste (40 CFR
§ 261.24). AMEC understands that, under current federal and state regulations, soil yielding
2 US Environmental Protection Agency (USEPA) facility ID No. OHD097613871.
3 The TCLP is a procedure that is used to assess the mobility or "leachability" of contaminants
following disposal in a landfill. AMEC understands that, in the context of disposal of lead
contaminated soils, the TCLP is the principal basis for determining whether the soil must be managed
as hazardous waste or whether it can be disposed of as non -hazardous waste in a local landfill.
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Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013

test results above the 5 mg/L regulatory threshold level for leachable lead (using the EPA
approved TCLP test method) is considered to be hazardous waste if it is to be disposed.
S&ME results for 200-yard berm: The total lead concentrations reported for the samples
collected from the 200-yard impact berm ranged from 100 to 8,200 mg/kg. Test results
above the Health Based and Protection of Ground Water PSRGs for lead were detected in
samples collected from depths of up to 30 inches. A soil sample from the 200-yard berm in
which total lead was detected at 7,800 mg/kg yielded TCLP lead result of 720 mg/L (above
the federal regulatory threshold for disposal as non -hazardous waste).
In its report, S&ME estimated that approximately 590 cubic yards of soil from the front and
rear faces of the impact berms, would likely require excavation and offsite disposal, of which
330 cubic yards would require treatment prior to disposal to render it non -hazardous, and the
balance (260 cubic yards) could be managed as non -hazardous waste.
2.3 REGULATORY STATUS
According to an Oct. 5, 2000, memorandum from Joe Grant, NCDENR Site Evaluation and
Removal Branch, to Charlotte Jesneck, Head, Inactive Hazardous Sites Branch, NC Division
of Waste Management (copy attached as Appendix D), the NCDENR determined that the
Gun Club site did not warrant further action by the Site Evaluation and Removal Branch.
The Gun Club has been listed on the NCDENR Inactive Hazardous Waste Sites Priority List
since at least 1991 (Site ID #NONCD0000019). The most recent (October 2012) revision of
the priority list shows the Gun Club site as having a rank of 444 out of a total of 539 sites,
where a rank of "1 denotes the highest priority for action.
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Former Sir Walter Gun Club Site
Knightdale, North Carolina
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3.0 METHODS
As noted in Section 1.0, this investigation included the following tasks:
® A review of readily accessible maps, reports, aerial photographs and other historical
information pertaining to the site;
® Field reconnaissance to verify the nature and locations of the former Gun Club
facilities; and
® Targeted sampling and analysis of surface soils within and downrange of the former
firing ranges.
The methods used in this investigation are described below
3.1 HISTORICAL REVIEW
Scanned (non -rectified) images of historic aerial photographs from 1959 and 1971 were
obtained online from the University of North Carolina (UNC) University Libraries Geographic
Information Systems (GIS) Services website. The images were then imported into AutoCAD,
and scaled and registered in North Carolina State Plane Feet using known reference points
such as highways and water bodies, in conjunction with Global Position System (GPS)
measurements made during the field reconnaissance. Geo-referenced digital imagery
acquired during April 2010 (North Carolina Statewide Digital Orthoimagery) was obtained
from the Wake County Geospatial & Technology Management Office, along with GIS data
layers containing parcel boundaries, the locations of major surface water bodies, and soil
survey data. A portable document format (.pdf) copy of a January 2011 property survey by
Newcomb Land Surveyors, L.L.C, was provided by the Client. Scanned geo-referenced
versions of the US Geological Survey (USGS) topographic quadrangle maps covering the
site were obtained online from the North Carolina Department of Transportation (NCDOT)
website. All of the information described above was integrated into a single working Auto
CAD file, from which base maps were prepared to support the historical analysis and the field
reconnaissance effort. The results of that analysis are shown in Figures 3, 4, and 5 and are
discussed in Section 4.1.
Additional sources of historic information reviewed during this investigation include reports of
previous environmental investigations and remedial work performed at the site, along with
related correspondence, which were provided to AMEC by the Client and the Gun Club.
3.2 FIELD AND LABORATORY METHODS
The field work to verify the nature and locations of the former Gun Club facilities and to
conduct the targeted sampling was conducted by AMEC on February 21, 2012. Mr. Charles
H. Silver, Jr. of Hinton Land, LLC and Mr. William DiBenedetto of the Sir Walter Gun Club
were present onsite during the initial part of the field investigation.
The field investigation techniques and soil sampling methodologies utilized in this
investigation were developed in accordance the Interstate Technology and Regulatory
Council (ITRC) guidance documents entitled Characterization and Remediation of Soils at
Closed Small Arms Firing Ranges (ITRC, 2003) and Environmental Management at
Operating Outdoor Small Arms Firing Ranges (ITRC, 2005). The features examined during
the reconnaissance investigation were prioritized based on the results of the historical
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Knightdale, North Carolina
February 14, 2013 6

information review. Scaled preliminary maps of the site were prepared using the historic
aerial photographs, for use as base maps in the field. The key features targeted for
investigation included impact berms, firing lines, target lines, range floors, the sites of the
former and existing structures (e.g., skeet houses, trap houses, skeet stations), lead shot -fall
areas, and areas likely to contain clay target debris. Additionally, the area behind
(downrange of) the former rifle range berms (refer to Figure 2) was specifically targeted for
investigation.
Key features identified during the reconnaissance were mapped using a hand-held GPS in
conjunction with a 300-foot tape measure and compass. Photographs were taken of pertinent
features identified during the site reconnaissance.
3.2.1 Field Sieving Analysis of Soil
AMEC collected surface and subsurface soil samples from key locations identified during the
field reconnaissance in order to develop preliminary information concerning the nature and
distribution of particulate metal (i.e., spent bullets and lead shot) in the soil. A mining based
sampling approach was used, in accordance the approach outlined in the ITRC (2003)
guidance.
Rifle range floor: Within the rifle ranges, AMEC collected surface and subsurface soil
samples for field sieving analysis to assess the distribution of spent bullets and bullet
fragments in the soil. The samples were processed through a set of interlocking, 12-inch
diameter sieves with nominal mesh sizes of 19 mm (millimeters) (Y4 inch) and 4.75 mm4.
Faces of impact berms: To assess the vertical extent of particulate metal within the front
(impact surface) of each berm, AMEC excavated subsurface test pits to a depth of
approximately 30 inches within each impact berm (Figure 6, sample locations RB100-5,
RB100-6, RB200-1, RB200-2, RB200-6 and RB200-7), from which soil samples were
collected from successive depth intervals for field sieving analysis. The test pits were
excavated at locations approximately 1 to 3 feet above the range floor (where eroded soil
and bullets were anticipated to be present), and approximately 5 to 6 feet above the range
floor in areas inferred to have received direct bullet impacts. Additionally, AMEC excavated
a test pit within a soil stockpile located adjacent to the northeast end of the 200 yard impact
berm which contained the remains of previously demolished target frames (refer to Figure 6,
sample location RB200-8).
Behind impact berms: AMEC also collected composite surface -soil samples from regularly
spaced sample transects extending downrange from the rear face of each impact berm to
assess the horizontal extent of spent rounds associated with ricochets and over -shots
(Figure 6, sample locations RB100-1, RB100-2, RB100-3, R13100-4, RB200-3, RB200-4,
and RB200-5). The surface soil samples were collected from a depth interval of
approximately 0 to 2" below grade using a shovel. A five -point composite sampling approach
was used as recommended in the ITRC (2003) guidance. At each sampling location, one
discrete sample was collected at a central location and four additional samples were
collected in an "X" pattern extending outward for a distance of approximately 5 feet. The five
discrete samples were then combined on a polyethylene tarp and then homogenized by
alternately lifting each corner of the tarp and rolling the soil diagonally toward the opposite
side. The resulting composite was then subdivided using the "cone and quarter" method to
4 American Society for Testing and Materials (ASTM) No. 4 mesh sieve.
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Knightdale, North Carolina
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produce a representative aliquot of 1-2 kg (kilograms) for field sieving analysis. The soil
samples were then processed through the 19 mm and 4.75 mm sieves to recover particulate
metal from the soil (if any).
Skeet field floor: Within the skeet field, four composite surface soil samples were collected
for sieving analysis along a linear transect, at distances of 250 ft, 300 ft, 350 ft, and 400 ft,
downrange of the skeet stations, using the five -point composite sampling method described
above (refer to Figure 6, samples SK-250, SK-300, SK-350, SK-400). A 1.70 mm (ASTM
No. 12 mesh) bottom sieve and a 3.35 mm (ASTM No 6 mesh) upper sieve were used to
separate the lead shot. The 1.70 mm sieve is capable of capturing shot sizes of No. 9
(2.03 mm) and larger. Because of the cohesive nature of the forest soils within the skeet
field, wet sieving was required to process the samples. The portion of each sample retained
on the 1.70 mm sieve was brought back to the AMEC office, air dried, and hand-picked
under a microscope to remove the lead shot. The recovered shot was then weighed using
an electronic balance with a precision of ±0.01 g, and the number of pellets recovered from
each sample was counted. The corresponding lead shot concentration was estimated on a
weight basis, based on the approximate original sample volume and the estimated bulk
density of the dried soil. The results of the lead shot determinations are summarized in
Table 1, and photographs of the lead shot and the sample locations are provided in
Appendix E.
3.2.2 Soil Sampling for Laboratory Analysis
AMEC collected surface soil samples from six locations within the portion of the property that
is behind the 200-yard berm (downrange of the former rifle range) for laboratory analysis.
The samples were collected from a depth interval of 0 to 6 inches below grade, at regular
intervals along a linear transect oriented roughly parallel to the western margin of the former
rifle range (refer to Figure 6, samples WP-1, WP-2, WP-3, WP-4, WP-2A, WP-4A). The
samples were submitted to a North Carolina certified environmental laboratory (Prism
Laboratories, Inc. in Charlotte, North Carolina) for analysis of total lead, arsenic, antimony,
and copper by USEPA Method 6010C. The results are summarized in Table 2 and the
laboratory reports are provided in Appendix F.
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Knightdale, North Carolina
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4.0 FINDINGS
The findings of this investigation are presented below:
4.1 HISTORICAL REVIEW
Historic aerial photographs of the Gun Club site from 1959, 1971, and 2010 are shown in
Figures 3, 4, and 5, respectively. The rifle ranges, pistol range, and the skeet field are all
visible in the 1959 aerial photograph (refer to Figure 3), and are connected by a series of
unpaved roads. The impact berms and target lines associated with the rifle and pistol ranges
are visible in the image, along with an area of non -vegetated ground immediately behind the
200-yard impact berm (possibly a borrow pit related to the berm construction). The pistol
range firing line appears to be covered by an overhead canopy. Target frames are visible at
distances of 25 and 50 yards downrange of the pistol range firing line. The firing line for the
rifle ranges is obscured by trees. Linear features that appear to be target frames are visible
100, 150, and 200 yards downrange of the inferred firing line location.
Within the skeet field, a high house, low house, and firing stations are visible in the 1959
aerial photograph, with the configuration matching that of a standard skeet field layout. A
geometric projection of the potential horizontal extent of lead shot deposition associated the
skeet field is superimposed over the 1959 aerial photograph in Figure 3. The projections are
based on empirical results reported at other skeet fields by Mackie (2005)5. An open field is
present extending out to a distance of approximately 180 feet northeast and 675 feet
northwest of the skeet field firing stations, beyond which the site is covered by forest.
In the 1971 aerial photograph (Figure 4), the configurations of the rifle ranges, pistol range,
and the skeet field appear to be essentially unchanged relative to the 1959 imagery. At the
rifle ranges, the area located immediately downrange of the 100-yard impact berm is partially
covered by trees, as is the apparent borrow pit located immediately downrange of the 200-
yard impact berm. The firing line for the 100-yard and 200-yard rifle ranges is partially
visible. The northeastern extent of the open area within the skeet field is essentially
unchanged. However the northwest portion of the field is partly overgrown by trees to within
about 475 feet of the skeet firing stations. Two small 1-story buildings are visible
immediately west of the pistol range with approximate horizontal dimensions of 18 by 20 feet
and 26 by 30 feet.
Few details of the existing range structures and facilities are visible in the 2010 aerial
photograph (Figure 5), due to the presence of heavy vegetative overgrowth. Although not
visible in the 2010 aerial photograph, a trap house identified during the field reconnaissance
was added to Figure 5, along with projections of the likely shot -fall pattern associated with
the use of the area as a trap field. The area of the former pistol range (previously removed),
has been redeveloped and is covered with commercial buildings and pavement.
Based on a review of the 1959, 1971, and 2010 aerial photographs described above, it
appears that the areas of the property located downrange of the former rifle range (behind
5 The projections are based on empirical results obtained at other sites over level ground, with no
trees or other obstructions. The horizontal extent of shot -fall can be attenuated by the presence of
trees or uneven topography.
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Knightdale, North Carolina
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the 200-yard berm) and immediately to the southwest of the range have been undeveloped
and covered by forest from at least 1959 through the present.
4.2 FIELD RECONNAISSANCE AND SOIL SAMPLING RESULTS
The results of the field reconnaissance, soil sampling, and analysis are described below.
Photographs taken during the field reconnaissance are provided in Appendix E. A sample
location map is provided in Figure 6, and results of the field sieving analyses and laboratory
analyses of soil are provided in Tables 1 and 2, respectively.
4.2.1 Riffle Ranges
Existing facilities associated with the rifle ranges that were observed during the field
reconnaissance included the 100-yard and 200-yard impact berms, a concrete pad
approximately 8 wide by 125 feet long at the firing line, and the previously described side
berm separating the rifle ranges from the skeet field (refer to Figure 6). Both ranges were
heavily overgrown with trees (refer to photos 1 through 6 in Appendix E). A soil stockpile
containing the remains of previously demolished target frames (concrete and rotted timbers)
was observed adjacent to the northeast end of the 200-yard impact berm (refer to Figure 6
and Photo 9). The front faces of the impact berms were relatively smooth (due to their
having been partially excavated during 1991), and showed no visible signs of "bullet pockets"
that commonly form in areas of concentrated fire. Orange sample flags were observed within
the impact berms, which evidently marked soil sampling sample locations from the October
2011 S&ME investigation.
Spent bullets were recovered from the subsurface test pits excavated within and behind both
impact berms, as described below:
a) 200-Yard Impact Berm: Spent bullets were recovered from test pits excavated into
the front face of the 200-yard impact berm at depths of up to 18 to 20 inches below
the ground surface (Figure 6, samples R13200-1, R6200-2, R13200-6, RB200-7). The
bullets typically consisted of rifle rounds (refer to photos 7 and 8 in Appendix E). All
of the recovered bullets showed evidence of corrosion. No particulate metal was
recovered from the surface soil samples collected from the rear face of the 200-yard
impact berm or from the area immediately behind the berm (refer to Figure 6,
samples RB200-3, RB200-4, RB200-5).
b) Soil Stockpile: No bullets were recovered from the soil stockpile located adjacent to
the 200-yard impact berm, where the remains of former target frames were observed
(Figure 6, sample RB200-8).
c) 100-Yard Impact Berm: Within the 100-yard impact berm, bullets consisting
predominantly of .30 caliber and 9 mm pistol rounds were recovered from depths of
up to 18 inches below the ground surface (Figure 6, samples RB100-5, RB-100-6).
Additional bullets consisting mainly of mainly of .22 caliber rifle rounds were
recovered at depth from approximately 18 inches to 28 inches in test pits RB100-5
and RB100-6. Examples the bullets recovered from the 100-yard impact berm were
provided to Mr. DiBenedetto from the Gun Club during the field investigation. No
particulate metal was recovered from the surface soil samples collected from the rear
face of the 100-yard impact berm or from the area immediately behind the berm (refer
to Figure 6, samples RB100-4, RB100-3, RB100-2, RB100-1).
Reconnaissance Investigation Results
Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 10

4.2.2 Skeet Field
The observed structures associated with the skeet field included a high house and low house
(both constructed from cinder block), concrete pads at the skeet stations, and a cinder -block
trap house (refer to Figure 6). The previously open areas within the skeet field (as described
in Section 4.1), were observed to be heavily overgrown with pine trees (refer to photos 15, 16
and 17 in Appendix E). The skeet stations, which were obscured by forest litter, were
located relative to the positions of the high and low houses, using a tape measure. A series
of elongated stockpiles composed of a mixture of clay target debris and soil was observed
approximately 150 feet northeast (downrange) of the skeet field firing stations (refer Figure 6
and photo 18 in Appendix E), which suggests that some of the clay target debris associated
with the skeet field has been consolidated. The areas located to the east of the stockpile
were covered by deciduous forest (refer to photos 19 and 20). A small northwest -flowing
stream was observed approximately 575 feet northeast of the skeet field firing stations (refer
to Figure 6 and photo 25 in Appendix E). The soils within the skeet field typically consisted of
fine sandy loam, containing abundant humic material in the upper 2 inches of the soil
column.
Surface soil samples were collected for field sieving analysis at distances of 250 feet, 300
feet, 350 feet and 400 feet downrange of the skeet field stations, at the locations shown in
Figure 6 (samples SK-250, SK-300, SK-350, SK-400). Lead shot was recovered from all four
soil samples, as summarized in Table 1. Given that each soil sample represents
approximately 1 square foot of surface area, the corresponding concentrations ranged from
4.0 to 18.2 grams of lead shot per square foot. Photographs of the lead shot recovered from
samples SK-250 and SK-400 are provided in Appendix E (refer to photos 21 to 24). The lead
shot showed evidence of varying degrees of corrosion and dissolution, with some pellets
being coated entirely with alteration products, and others showing evidence of chemical
etching (i.e., surface pitting, irregular faceted shapes). The pellets appeared to consist
principally of No. 8 and No. 9 shot, with lesser amounts of No. 7'/2 shot.
4.2.3 Area Downrange of Former Rifle Range
The laboratory results for the six surface soil samples (Figure 6, samples WP-1, WP-2,
WP-3, WP-4, WP-2A, WP-4A) collected from the area of the property behind (downrange of)
the 200-yard rifle range berm are summarized in Table 2. The lead results, which ranged
from 6.3 to 22 mg/kg, were an order of magnitude or more below the Residential Health
Based PSRG and the Protection of Ground Water PSRG. The results for copper were three
orders of magnitude below the corresponding PSRGs. Antimony was not detected in any of
the samples.
The results for total arsenic, which ranged from 1.5 to 2.9 mg/kg, were slightly above the
Health Based PSRG of 0.39 mg/kg. However the results were within the 4.5 mg/kg average
(mean) background for 3,286 samples of North Carolina Soils analyzed by the North Carolina
Department of Agriculture (NCDAG, 2008), as well as the average (geometric mean) of 7.2
mg/kg reported for soils of the conterminous United States by US Geological Survey
(Shacklette and Boerngen, 1984). Based on the technical guidance provided in the
NCDENR "Guidelines for Assessment and Cleanup" (NCDENR, 2011), AMEC understands
that remediation of soil to levels below site -specific natural background concentrations is not
required. Based on the soil sampling results and AMEC's investigation and observations,
Reconnaissance Investigation Results
Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 11

AMEC believes it is likely the total arsenic results represent natural background
concentrations in the area of the site, rather than impacts from prior SAM operations on the
site.
Reconnaissance Investigation Results
Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 12

5.0 CONCLUSIONS
Based on the findings presented above, AMEC has reached the following conclusions in
connection with this investigation:
1. Based on the laboratory results summarized in Table 2 and the results of our
preliminary field reconnaissance, no evidence was found of range related
contaminants (or other contaminants) at the property that is behind (downrange of)
the 200-yard impact berm of the former rifle range (refer to Figure 6). While some
results for arsenic, were slightly above the most stringent PSRG, all of the results
were within the range of natural background, and are thus not considered to be
evidence of contamination.
2. The fact that no particulate metal was recovered from the surface soil samples
collected immediately downrange of the two rifle range impact berms suggests that
surface lead impacts related to ricochet are likely to be minimal.
3. Prior TCLP lead results (described in the S&ME report, App. C) for the impact berm
soils showed soil contamination above the federal regulatory threshold of 5 mg/L for
disposal as non -hazardous waste. Thus, if the impact berm soils were to be removed
for disposal, at least some of the soil would either require onsite chemical stabilization
to render it non -hazardous, or disposal at a USEPA approved facility that is licensed
to handle hazardous waste.
4. AMEC did not assess whether there are potential environmental impacts from former
SAFR operations at the areas within the rifle ranges where target frames were
formerly present (as identified from the historic aerial photographs), the range floors,
or and the area located immediately downrange of the former firing line (refer to
Figure 6).
5. The shot concentrations recovered from the soil samples collected from the skeet
field suggest that lead is present in the soil at concentrations above the applicable
PRSGs. Assuming that the shot is restricted to the upper 2 inches of the soil, and
using an estimated soil bulk density6 of 1.27 g/cc (grams per cubic centimeter), the
equivalent shot concentration in the soil samples was estimated to be 770 to
3,500 mg/kg. Note that AMEC did not analyze the soil samples for total metals as
part of this reconnaissance investigation. Moreover, an increasing trend was
observed in the shot concentrations measured from 250 to 400 feet downrange,
which suggests that the areas that received the maximum cumulative shot -fall may
not have been fully captured within the sample transect7.
6. Generally, the shot concentrations recovered from the surface soil samples collected
within the skeet field suggest a relatively low intensity of usage by the Gun Club, as
compared with other skeet fields investigated by AMEC. However, the results of the
field reconnaissance investigation of the former skeet field are preliminary in nature;
AMEC did not attempt to fully delineate the extent of the lead impacted areas in the
skeet field.
6 As measured by AMEC using from an air-dried soil sample.
In our experience the area of maximum shot -fall for trap and skeet ranges over open ground is
typically about 475 feet downrange, but may be less in forested areas due to attenuation of the shot
trajectory by trees.
Reconnaissance Investigation Results
Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 13

7. The soil stockpiles containing clay target debris (refer to Figure 6) are likely to contain
PAHs at concentrations above the corresponding PSRGs.
Reconnaissance Investigation Results
Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 14

6.0 PRELIMINARY DISCUSSION OF REMEDIAL OPTIONS
6.1 PROPOSED SITE DEVELOPMENT
The site is in an area that has undergone, and continues to undergo, significant commercial
development. The area of the former pistol range, immediately south of the site, has been
completely covered by commercial development, i.e., buildings and pavement associated
with the Shoppes at Midway Plantation shopping center. Compare Figures 4 and 5. The
Client has informed AMEC that commercial development is being actively considered for the
entire subject site, including the areas that formerly included the rifle and skeet ranges.
6.2 BERMS
Some potential soil management alternatives that may be appropriate for the site (either
alone or in combination) include:
a) Onsite treatment of impact berm soils that are contaminated above the federal
regulatory threshold, consisting of dry screening to remove spent bullets, followed by
chemical stabilization (using a phosphate or magnesium -oxide based stabilizing
agents) to reduce the TCLP lead leachability below the 5 mg/L federal regulatory
threshold. Treatment of the soil would enable the beneficial reuse of the soil as non-
hazardous material or disposal as non -hazardous waste. In AMEC's experience,
disposal of untreated range soil as hazardous waste is unnecessary given the
effectiveness of the chemical stabilization methods that are currently available, and
would be undesirable due to the substantially greater cost and the increased potential
for future environmental liability.
b) Transportation of some impact -berm soil to the current site of the Gun Club in
Creedmoor, North Carolina for beneficial reuse within existing, active ranges at the
facility (as berm material). It is AMEC's understanding that the Gun Club has
expressed an interest in re -use of the berm soil at their current range facility. In
AMEC's opinion, this could potentially be an appropriate and relatively inexpensive
alternative to disposal, if permitted under existing regulations. This type of beneficial
reuse is consistent with the goals outlined in Appendix D of the USEPA (2005)
guidance entitled "Best Management Practices for Lead at Outdoor Shooting Ranges"
which states that:
"As a range management practice, it is environmentally preferable to use soil that
may already contain lead and is on an active portion of the range, which will therefore
undergo regular lead reclamation in the future, than to leave such soil in place and
construct a new backstop with lead-free soil."
c) If the offsite beneficial reuse of impact berm soil at another range location is not
possible because of regulatory constraints, then AMEC believes the berm soil could
potentially be reused onsite as compact fill or sub -base beneath commercial
development, such as structures or parking lots, subject to NCDENR approval.
Reconnaissance Investigation Results
Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 15

d) The lack of particulate metal in surface soil samples collected downrange of the two
rifle range impact berms suggests that surface lead impacts outside of the impact
berms from former SAFR operations are minimal. Onsite use of this surficial soil (and
possibly soil from the range floors) as compact fill may be possible.
6.3 SOILS AT SKEET FIELD AND RANGE FLOORS
AMEC's investigation results suggest shot concentrations within the skeet field indicate a
relatively low intensity of usage by the Gun Club, as compared with other skeet fields
investigated by AMEC. Nevertheless, it seems likely there are areas in the skeet field and on
the rifle range floors where lead is present in the soil at concentrations above applicable
PRSGs. It is also possible, given the extent of weathering of the shot recovered from the
skeet field, that other metals such as arsenic and antimony may be present in the soil in
some skeet field areas.
The planned commercial development of the property may allow for less stringent site -
specific remedial goals for the soils on the rifle range floor and in the skeet field. Such
development would result in capping of a significant portion of the former rifle and skeet
range areas and limit or prevent spread of any remaining contamination or exposure of
humans or wildlife to metals or PAH contaminants. Chemical stabilization of the soil to
reduce lead leachability followed by consolidation and capping of the material beneath the
planned development could provide an environmentally sound and relative low-cost means
of managing the soil onsite.
In AMEC's experience the PAHs that are typically present in clay targets are relatively
immobile in the environment, and thus do not pose a threat to groundwater quality. Chemical
stabilization of lead, arsenic, and antimony associated with the lead shot is also effective in
controlling the leachability of these compounds in the environment. Thus, it is likely that the
metals and PAHs associated with the former skeet field can be effectively contained through
a combination of chemical stabilization and capping. Given that a significant portion of the
site will be paved or covered with buildings as part of the planned development, it is possible
that the soil consolidation and capping could be integrated into the site plan design in a way
that would be both protective of the environment and cost effective.
6.4 SOIL STOCKPILE
The soil stockpile containing clay target debris probably contains PAHs at concentrations
above the applicable PSRGs. If the soil containing clay target debris is found to be free of
significant heavy metals impacts, it is possible that it could be used onsite as pavement sub-
base material.
Reconnaissance Investigation Results
Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 16

7.0 REFERENCES
ITRC. 2003. Characterization and Remediation of Soils at Closed Small Arms Firing Ranges.
Interstate Technology and Regulatory Council, January, 2003.
ITRC. 2005. Environmental Management at Operating Outdoor Small Arms Firing Ranges.
Interstate Technology and Regulatory Council, February, 2005.
ITRC 2012. Incremental Sampling Methodology. The Interstate Technology & Regulatory
Council Incremental Sampling Methodology Team, February 2012
Mackie, D. 2005. Use of Predictive Models for Characterization of Trap and Skeet Ranges:
Case Studies and Model Results. Proceedings of the 21 st Annual Conference on
Contaminated Soils, University of Massachusetts at Amherst, October 19, 2005.
NCDAG. 2008. Heavy Metals in North Carolina Soils Occurrence & Significance. N.C.
Department of Agriculture and Consumer Services, September 2008.
http://www.ncaqr.gov/agronomi/pdffiles/hmetals.pd .
NCDENR 2011. Guidelines for Assessment and Cleanup. Department of Environment and
Natural Resources Division of Waste Management Superfund Section Inactive
Hazardous Sites Branch August 2011.
S&ME. 2011. Additional Soil Testing — Abandoned Rifle Range Berms, Silver Plantation,
Former Sir Walter Gun Club, Knightdale North Carolina, S&ME Project No. 1054-10-
252, January 4, 2011, 36 p.
Shacklette, H.T and J.G. Boerngen. 1984. Element Concentrations in Soils and Other
Surficial Materials of the Conterminous United States. US Geological Survey
Professional Paper 1270, US Government Printing Office, Washington, DC, 1984.
USEPA. 2005. Best Management Practices for Lead at Outdoor Shooting Ranges. United
States Environmental Protection Agency Region 2, EPA-902-B-01-001, Revised June
2005.
Reconnaissance Investigation Results
Former Sir Walter Gun Club Site
Knightdale, North Carolina
February 14, 2013 17

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Legend: Map $OUfCBS: CLIENT: DWN BY: PROJECT DATE:
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PARCEL BOUNDARY 1. North Carolina Statewide Digital Orthoimagery Project 2010, Edition:1.0, Hinton Land L L C CHK'D BY: PROJECT NO:
Wake County, North Carolina Geospatial & Technology Management CH 348112003
CLIENT OWNED PROPERTY Office, flown April 2010. DATUM:
County, p AMEC Environment & NAVD88 TITLE REV. NO.:
STREAM 2. Tax Parcels for Wake County. Wake Coun North Carolina Geos anal
& Technology Management Office (last updated on January 2012). PROJECTION: A
Infrastructure, Inc. ���� NC ZONE3200 SITE MAPp FIGURE No.
3. Recombination Plat (Preliminary) prepared for Charles H. Silver and 285 DAVIDSON AVENUE, SUITE 405 ^
CMR Partners, L.L.C. by Newcomb Land Surveyors, L.L.C, January 11, SCALE: L
2012 SOMERSET, NJ 08873 1 inch = 250 feet

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't. f , "� r t► . OF SHOT FALL +Kr !C
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Legend: Map Sources:
PARCEL BOUNDARY 1. 1959 USDA Historical Aerial Photos of Wake County, North Carolina,
UNC University Libraries, Geographic Information Systems (GIS) Services
CLIENT OWNED PROPERTY (non -rectified images, manuallygeo-referenced).
STREAM 2• Tax Parcels for Wake County. Wake County, North Carolina Geospatial & Technology Management Office (last updated on January 2012).
3. Recombination Plat (Preliminary) prepared for Charles H. Silver and
CMR Partners, L.L.C. by Newcomb Land Surveyors, L.L.C, January 11,
2012.
Oil,
50 YARD RANGE
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i
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' (REMOVED)
•
CLIENT:
Hinton Land LLC
DWN BY:
DM
PROJECT
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DATUM:
NAVD88
AMEC Environment &
Infrastructure, Inc.
285 DAVIDSON AVENUE, SUITE 405
SOMERSET, NJ 08873
���
ame t
TITLE
ANALYSIS OF HISTORIC (1959) AERIAL
PHOTOGRAPHY
PROJNCZONE3200
SCALE:
1inch = 200 feet
. f_
DATE:
14-Feb-13
PROJECT NO:
348112003
REV. NO.:
A
FIGURE No.
3

'0 A
1 7 PROJECTED OFi
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Legend: Map Sources: CLIENT: DWN BY: DIM PROJECT FORMER SIR WALTER GUN CLUB SITE
PARCEL BOUNDARY 1. 1971 USDA Historical Aerial Photos of Wake County, North Carolina, Hinton Land L L C CHICD BY:
UNC University Libraries, Geographic Information Systems (GIS) Services CH
CLIENT OWNED PROPERTY (non -rectified images, manually geo-referenced). DATUM:
2. Tax Parcels for Wake County. Wake County, North Carolina Geospatial AMEC Environment & NAVD88 TITLE
STREAM & Technology Management Office (last updated on January 2012). PROJECTION: a
Infrastructure, Inc. M NC ZONE 3200 ANALYSIS OF HISTORIC (1971) AERIAL
3.Recombination Plat (Preliminary) prepared for Charles H. Silver and 285 DAVIDSON AVENUE, SUITE 405 PHOTOGRAPHY
CMRPartners, L.L.C. by Newcomb Land Surveyors, L.L.C, January 11, SOMERSET, NJ 08873 ec - SCALE:
2012, 1 1 1 1 inch = 200 feet
DATE:
14-Feb-1 3
PROJECT NO:
348112003
REV. NO.:
A
FIGURE No.
4

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DM FORMER SIR WALTER GUN CLUB SITE 14-Feb-13
PARCEL BOUNDARY 1. North Carolina Statewide Digital Orthoimagery Project 2010, Edition:1.0, Hinton Land L LC CHILD BY: PROJECT NO:
Wake County, North Carolina Geospatial 8 Technology Management CH
CLIENT OWNED PROPERTY Office` flown April 2010. DATUM: 348112003
NAVD88 TITLE REV. NO.:
2.Tax
nologParcels for Managemenake t
(lake County,updated on orth
AMEC Environment & PROJECTION: ANALYSIS OF HISTORIC (2010) AERIAL A
STREAM Technology Management Office (last updated on January 2012).
Infrastructure, IncSUITE
�M MC NC ZONE3200
3. Recombination Plat (Preliminary) prepared for Charles H. Silver and 285 DAVIDSON AVENUE, SUITE 405 PHOTOGRAPHY FIGURE No.
CMR Partners, L.L.C. by Newcomb Land Surveyors, L.L.C, January 11, SCALE:
2012 SOMERSET, NJ 08873 1 inch = 200 feet

W P-4A
W P-2A
W P-4-*
3
WP-
RB200-5
WP-2
,�..�III3
B2R 00-4 IM
WP-1
RB200
REAR
-
BERM FACE
RB200-1
0' 100, 200'
1"=150'
PROJECTED AREA
PROJECTED OF HIGHEST
OUTER LIMIT SHOT FALL
OF SHOT FALL
STREAM -----------------
,
,
,
,
,
,
,
200-YD.
IMPACT
BERM
RB200-8
,
SOIL
3 STOCKPILE
100-YD.
RB200-7
RB200-6 IMPACT
FRONT RB100-1 RB100-2 BERM \
BERM FACE ® RB100-3 \\
RB200-2
HIGH
C
vs REaRaA F RB100-6 HOUSE
BERM 1-
RBI )0- SIDE ti
RB100-4 BERM
RIFLE RANGE
FIRING LINE
LIKELY AREA OF CLAY
TARGET DEPOSITION
\_TRAP
HOUSE
HOUSE
,
,
STOCKPILED
CLAY TARGET
DEBRIS
Legend:
-- • —
PARCEL BOUNDARY
CLIENT OWNED PROPERTY
—
STREAM
OBSERVED BULLET IMPACT AREA
PROJECTED EXTENT OF HIGHEST SHOT FALL
PROJECTED EXTENT OF CLAY TARGET DEBRIS
DISCRETE SOIL SAMPLE (LABORATORY ANALYSIS)
COMPOSITE SOIL SAMPLE (SIEVING ANALYSIS)
O
SUBSURFACE TEST PIT (SIEVING ANALYSIS)
Map Sources:
1. North Carolina Statewide Digital Oatial & ech Project snag Edition: 1.0,
Wake County, North Carolina Geospa[ial &Technology Management
Office, flown April 2010.
2. Tax Parcels for Wake County. Wake County, North Carolina Geospatial
& Technology Management Office (last updated on January 2012).
3. Recombination Plat (Preliminary) prepared for Charles H. Silveandr 11
CMR Partners, L.L.C. by Newcomb Land Surveyors, L.L.C, January 11,
2012.
CLIENT:
Hinton Land LLC
DWN BY:
DM
PROJECT
FORMER SIR WALTER GUN CLUB SITE
DATE:
14-Feb-13
CHK'D BY:
CH
PROJECT NO:
348112003
DATUM:
NAVD88
AM EC Environment &
Infrastructure, Inc.
285 DAVIDSON AVENUE, SUITE 405
SOMERSET, NJ 08873
ame
TITLE
FIELD RECONNAISSANCE AND
SAMPLE LOCATION MAP
REV. NO.:
A
PROJECTION:
NC ZONE 3200
FIGURE No-
6
SCALE:
linch = 150feet

Appendix A
January 1989 Atwood Memorandum

MEMORANDUM
To: Allen Gambill, Director
Budget and Analysis
Through: Lee Crosby, Read
0
Superfund Branch Y-
From Stan Atwood', Toxicologist
Superfund Branch
Subject: Sir Walter Gun Club
Attached are the sampling results for the subject
site. High levels of lead were found in each of the three
berms. In addition, low levels of several polyaromatic
hydrocarbons were found in the berms at the pistol range and
the 100 yard rifle range. These compounds are often
associated with waste oils or soot. None of the other
samples, including the well and skeet range, showed
environmental contamination.
The lead levels in the berms are high enough to be
of environmental concern. The Superfund Branch will be
happy to work with the Sir Walter Gun Club in seeking a
solution to the contamination problem. If you have any
questions, please contact me at 2801.
P-6" \f1P
IQ\
)�T

31 January 1989
To: Allen Gambill, Director
Budget and Analysis
Through: Lee Crosby, Head V� Superfund Branch
From : Stan Atwood, 'Toxicologist
Superfund Branch
Subject: Sir Walter Gun Club
CO
�F}�E 3) 1
(�.989
Ct✓�i
l���'6d gv L2o2 �
-rjlrk .` ? Ic3 - 2 kol
Attached are the sampling results for the subject
site. High levels of lead were found in each of the three
berms. in addition, low levels of several polyaromatic
hydrocarbons were found in the berms at the pistol range and
the 100 yard rifle range. These compounds are often
associated with waste oils or soot. None of the other
samples, including the well and skeet range, showed
environmental contamination.
The lead levels in the berms are high enough to be
of environmental concern. The Superfund Branch will be
happy to work with the Sir Walter Gun Club in seeking a
solution to the contamination problem. If you have any
questions, please contact me at 2801.

U-LV1J1bJ1\ U
SOLID HAZARDOUS WASTE M NAGE-K-NT, e NC`d
Chain of Custodt Record
Eczardous Waste Materials
�ocazicn of Sampling: Generator Transporter
Storage Facility Disposal Facility
Other:
:ompany' s Name �- L-),4 f n i 1,1-1 f L„ � Telep ( % r
Lddress . i%
-;ollector's Name T ke'
sigt:ature)ate Sampled %� 9 TType of Process Generating Waste 's�f MAat"-,
-ield ®information
Co1(
Treatment Faci
Landf ill
J v
Field Sample No
•
�r 2— 3 0 3 .313
30 3 5
3r3`
Maain of Possession:
2.
i
signature
3.
ve ou q-io s ng� -
titae inclusive dates
/ / - /®
title inclusive dates
title in A1,,iv-aedLates
:�esu4 is r r e
signature title date
ins::.uctions: Complete all applicable information inclucir.g signatures, and
submit with •analysis reauest forms.

`%OV 2 01988
S � p F_� PLti� D .
G. Department of human Resources
State Laboratory of Public Hcal
SAMPLE ANALYSES REQUEST P. 0. Box 280,
ision of Health Services
306 N. Wilmington Stre
••Raleigh, 276
_ Number T r. A
Field Sample Number
ame of Site r- l A -, e r ,„
C1�� Site 1-ocation 7 6
`.1
n�,
iD# Date Collected A-1) 19 rr
Time /COD -1. c
!leered By .�S A�- .Le;
ype of Sample:
Environmental Concentrate Comments
Groundwater (1)
e
Solid ,(5)
Surface Water (2)
Liquid (6)
Soil (3)
Sludge (7) :� s k i .A
--- Other (4)
Other (B)
INORGANIC C _.
Extractables
"'•' e A*M.
d • �.a
Parameter Results mg/ 1
4:.a� P r'.� .
Parameter Results rn/'�'�
�'••.
Parameter
Results mg/ 1
Arsenic
Arsenic
barium O
Sulfates
Barium
�D° oy.S'"
Zinc
—CadmiumCadmium
Chloride
Ph
Chromium
°y
ZC
Conductivity
Lead
___hromium
Copper C ©�
TDS
® Mercury
Selenium
Fluoride
.I.00
Silver
Iron
.ead < o ®a 3
_
Manganese
Mercury
Nitrate
_
Selenium ` gz
(-)R(YAN1C CHEMISTRY
Parameter ].Results mg/1
Parameter Results mg/1
Parameter Results mg/
P&T:GC/MS
EDB
Methoxychlor
Acid:B/N Ext.
PCB'§
Toxaphene
ITOX
Petroleum
2,4-D
I
Endrin
2,4,5-'rP (silvex)
_
Lindane
MICROBIOLOGY - RA�I�7c:ii� a51 t1
Parameter Parameter Results PCi/ 1
(MF) Coliform Colonies/IOOmis Gross Alpha
(MPN) Coliform Colonies/ I00mis Gross Beta
Date Received
Date Extracted
R ennrrPrl RV
Date Reported
Date Analyzed 02160 1 NOV 14 88 •
Lab Number

Sf E- R jF' D
State Laboratory of Public Heal
C. Department of Human Resources
SAMPLE ANALYSES REQUEST
a P. O. BOX '280,
,ision of Health Services
306 N. Wilmington Stre
Raleigh, 276''
_
J
Field Sample Number
t Number
"
��'- c, 11� �' `"
Ck �.1� ) ,�
Site J.ocation
i c' ' �
ame of Site
-S+'1 -' A +, ', of�1
ID# — }' s Date Collected /�c��
y `' t -- Time /CoC-l3
4
71lected By
_
pe of Sample:
Comments
Environmental Concentrate
1
Groundwater ( )
Solid ( 5 )
r
Surface Water (2)
Liquid (6)
✓ Soil (3)
Sludge (7)
Other 4)
Other (B)i`i,a
INORGANIC CHEMISTRY �A�"���
Extractables
Results mg/ 1
Parameter Results mg/1
"� f- r Results Mg/1
Parameter
✓Arsenic
Arsenic
�..
� 's , 1 y;'�•
"Barium.
ates;
'Barium
Be 0
✓Cadmium _-
Zinc
,�
_ Cadmium
"Chromiumn G ° O
Chloride
Ph
Conductivity
j
-,"Chromium
---'Lead _�_
Mercury ---- ✓Copper
TDS
TOC
'� 5eleniun�
�`�Silver
Fluoride
Iron
�G®tA•�
-"'Lead /q
Manganese
°Mercury O 1
Nitrate,
'
®,CSelenium
ORGANIC CHEMISTRY
Results mg/1 Parameter Results mg/1
Parameter Results mg/:
Parameter
Methoxychlor
4 P$tT:GC/MS
EDB
PCB's
Toxaphene
Acid:B/N Ext.
Petroleum
2,4-D
'tOX
Endrin
2,4,5-TP (silvex)
Lindane
MICROBIOLOGY
RADIOCHEMISTRY
Parameter
Results PCi/ I
Parameter
(MF) Coliform Colonies/100MIs
Gross Alpha
(MPN) Coliform Colonies/100m1s
Gross Beta
Date Received
Date Extracted
Renorred By
Date Reported
Date Analyzed02 1J5 Nov 10 88
Lab Number

Suk p F-P- FUND
C. Department of Human Resources SAMPLE ANALYSES REQUEST
vision of health Services
to plumber
Field Sample Number 1
C��1� _ Site �.oeation
dame of Site ei c- t-J r e - i
A, ID!# LE S Date Collected
allecred By ,r;;•-
qpe of Sample: _
Environmental
Groundwater (I)
Surface Water (2)
Soil (3)
Other (4)
Extractables
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
INORGANIC CHEMISTRY
Parameter Results mg/1
Parameter
✓Arsenic ^O �v 1
Arsenic
6/Barium
✓Baratltn ` J t
�Cadrnium
-! Cadcraiurrt®s----
P
Chloride
Chromium .�--
Lead
�Chrotnium
Mercury _ {� O
--�Copper
,_
---� elenium ® t�®�
I" ®• a
Fluoride
Iron
Silver y/O�
Manganese
`Mercury
Nitrate.
1
Selenium
-
Parameter Results mg/1
P&T:GC/MS
Acid:B/N Ext.
TOX
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/100mis
(MPN) Coliform Colonies/100mis
Date Received
Date Extracted
Reported By
Total
State Laboratory of Public Heal
P. O. Box 280�
306 N. Wilmington Stre
.Raleigh, 276
Time ZCCG—/-L
Results mg/i Parameter Results mg/1
ORGANIC CHEMISTRY
Parameter Results mg/1
EDB
PCB's
Petroleum
Endrin
Lindane
Parameter
Gross Alpha
Gross Beta
Silver
Sulfates
Zinc
Ph
Conductivity
TDS
TOC
Parameter Results mg/1
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
RADIOCHEMISTRY
Results PCi/ I
Date Reported
Date Analyzed // NOVy ��}}
Lab Number 021 7JO O10 88

Sckpaa�--kA"')D
C. Department of Human Resources SAMPLE ANALYSES REQUEST
'ision of Heath Services
State Laboratory of Public Heal
P. 0. Box 280,
306 N. Wilmington Strc
'Raleigh, 276
3
i a
Field Sample Number
c Number
ame of Sire e� c l J A C.
C. ea Ci lr. U
_— Site 1_-ocation
- ��
, - 4 L}" S — Date Collected ����
IDS
y ,�— Time L0 o —13c
',Ilected By ._.�%�g ., ,, „•
< <_ �.
.
ypc of Sample:
Environmental
Concentrate
b
CO
Groundwater (1)
Solid (5)
4 le
Surface Water (2)
Liquid (6)
,
Soil (3)
7 d
Sluge ()
� i ;= "'�•��LL�,"
Other (4)
Other (S)
Y s
Extra actt b esl
INORGANIC CHEMISTRY 4 SOe ;
To _
Parameter
Results trig/I
Parameter
Arsenic
m ®
�rsenic
6 °Barium
• ®
` �Bacium
Cadmium
Q —
✓Cadmium
_
�Chromium
�--�- • �?
Chloride
Lead
�•
ZChrotnium
_
Mercury
®
Zcopper
eleniunl
I
®•
Fluoride
Iron
._Silver
�
� D �
• � _ead
Manganese
�®
-Mercury
orate.
_
Selenium
Parameter Results mg/ 1
P&T:GC/MS
Acid:B/N Ext.
TOX
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/100mis
(MPN) Coliform Colonies/100mis
Date Received
Date Extracted
R rnnrred By -
Results mg/ 1
bra Results crag/ I
S
Silver
Sulfates
Zinc
Ph
Conductivity
TDS
TOC
3 8
/ D
e (�
ORGANIC CHEMISTRY
Parameter Results mg/1
EDB
PCB`.s
Petroleum
Endrin
Lindane
Parameter
Gross Alpha
Gross Beta
Date Reported
Date Analyzed
Lab Number .
Parameter Results mg/ i
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
RADIOCHEMISTRY
Results PCi/ 1
02 I f 57 NOV 10 88

C. Department of Human Resources
ision of Health Services
Scam.t gip- Fu� rl-)D
SAMPLE ANALYSES REQUEST
State Laboratory of Public Heald
P. ®.Box 2804'
306 N. Wilmington Stree
-Raleigh, 2761
Field Sample Number I �'
Number 1 �'9 -�
�. C\kb __
ame of Site
(.,�) fs � �� e � �2 � Site J—Oeaiion
Date Collected Time /CCO-/ 30
fleeted By S,-A ' , • n`'
y pc of Sample:
Concentrate s
'Environmental Concentrate
I 0 �" �(- / ,
1-1
Groundwater (1)
Solid (5) �
Surface Water (2) Liquid (6) f
Soil (3) Sludge (7) ,
Other (4) Other (8)
INORGANIC CHEMISTRY
ExtractaBIes
Parameter Results mg/I Parameter Results mg/1
® Arsenic Arsenic
Barium Barium
v Cadmium — Cadmium
Chromium — Chloride
Lead v{ Chromium
Mercury 5�-� �- Copper
Selenium Fluoride
Silver Iron
Lead
Manganese
Mercury
Nitrate.
Selenium
I
' Parameter Results mg/1
P&T.GC/MS
Acid-B/N Ext.
y' `tOX
MICR®RIOLOGY
Parameter
(MF) Coliforrn Colonies/100mis
(MPN) Coliform Colonies/100mis
Date Received
ORGANIC CHEMISTRY
Parameter Results mg/1
EDB
PCBs
Petroleum
Endrin
Lindane
Parameter
Gross Alpha
Gross Beta
Date Reported
N op pq
Results mg/ I
Silver
Sulfates
Zinc
Ph
Conductivity
TDS
TOC
Parameter Results mg/1
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
RADIOCHEMISTR
Results PC%/ 1
Date Extracted
Reported By
Date Analyzed
Lab Number
02`1 7 58 NOV 10 88
' Parameter Results mg/1
P&T.GC/MS
Acid-B/N Ext.
y' `tOX
MICR®RIOLOGY
Parameter
(MF) Coliforrn Colonies/100mis
(MPN) Coliform Colonies/100mis
Date Received
ORGANIC CHEMISTRY
Parameter Results mg/1
EDB
PCBs
Petroleum
Endrin
Lindane
Parameter
Gross Alpha
Gross Beta
Date Reported
N op pq
Results mg/ I
Silver
Sulfates
Zinc
Ph
Conductivity
TDS
TOC
Parameter Results mg/1
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
RADIOCHEMISTR
Results PC%/ 1
Date Extracted
Reported By
Date Analyzed
Lab Number
02`1 7 58 NOV 10 88

5 Uk P c �Z l°u ►Ll D
C. Department of Human Resources
ision of Hcalth Services
SAMPLE ANALYSES REQUEST
State Laboratory of Public Heal,
P. 9. Box 2i304
• 306 N. Wilmingron Strc
-Raliigh, 2761
: Number
b A Field Sample Number 3
Site J.oca�-ion
ame of Site �1
llected By
ls+"� T �� Ilia , f IDR � S Date Collected /Ua,� T 12k S� Time 1000-136
,Pc of Sample:
Concentrate.. Comments
Environmental
� - - - � • � aso e'�..di:f� i� r : -i-l.P �•A.ncz 0
Groundwater (1) Solid (5)
Surface Water (2) Liquid (6)
✓ Soil (3) Sludge (7)
Ocher (4) Other (8)
INORGANIC CHEMISTRY
Extractables
Total
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1
ilver �° AA
`Arsenic O 1
Arsenic
4
`Barium
Sulfates
`Barium
®o D cg
Cadmium
__!:::::`Cadmium � 1 is
Zinc
c/
Chromium D ' � O
Chloride
/ 'Ll Q
ph
Conductivity
Lead --�--
_ -
�hromium
Copper l 01 is�
TDS
✓mercury
Fluoride
T'OC
Selenium
ilver D
iron
Y
Lead
�—`
anganese 9
o Q
Mercury •
ltrate
Selenium f?
Parameter Results mg/1
P&i:GC/MS
Acid:B/N Ext.
TOX
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/100m1s
(MPN) Coliform Colonies/100mis
Date Received
ORGANIC CHEMISTRY
Parameter Results mg/i
EDB
PCB°s
Petroleum
Endrin
Lindane
Parameter
Gross Alpha
Gross Beta
Date Reported
Parameter Results mg/1
Methoxychlor
Toxaphene
2,4-D
2,495-TP (silvex)
Results PCi/ I
Date Extracted
Reported By
Date Analyzed 02 159 NOV 10 88
Lab Number

S(•,FER PUNl)
C. Department of Human Resources
vision of Health Services
State Laboratory of Public Hcal
P. 0. Box 280,e
- 306 N. Wilmington Stre
l r -Raleigh, 2761
Field Sample Number 313 T
to Number 1 A
c>; r („ j c .. Site Location _ ? �- '
lame of Site `1
ollected By AA — ID# S Bate Collected 64-)) 9 1 - Time ICO ®- / ,3 G
ype of Sample:
Environmental Concentrate
:...
Groundwater (1) Solid (5) 00 i
Surface Water (2) Liquid (6);.�::- :....
Sludge (7)
�Z Soil (3)
Ocher (4) Ocher (8) ftpmiruND'
INORGANIC CHEMISTRY
Extractables
SAMPLE ANALYSES REQUEST
Parameter Results mg/ 1 Parameter
Total
Results mg/ 1 I Parameter Results mg/1
Arsenic L n w O l
�--
Arsenic < 1 d�
t� ��
arium -
vSilver
Sulfates
Barium,
rj a
Cadmium 1 S
Zinc
---
® •!Cadmium �+
✓Chromium
Chloride
Chromium 3
Ph
Conductivity
Lead e
Mercury
✓Copper L 9
TDS
Selenium � -�®�--
Fluoride
TCC
�✓Siiver � �° '� ®
Iron
•
Manganese
✓ Mercury <
—Nitrate.
✓ Selenium 6
Parameter
P&T:GC/MS
Acid:B/N Ext.
TOX
Results mg/ 1
MICRQEIOLOGY
Parameter
(MF) Coliform Colonies/100mts
(MPN) Coliform Colonies/100mis
Date Received
<_52
ORGANIC CHEMISTRY
Parameter Results crag/1
Parameter Results mg/1
BDB
Methoxychlor
PCB..°s
.Toxaphene
Petroleum
2,4-D
Endrin
2,4,5-TP (silvex)
Lindane
. Parameter
Gross Alpha
Gross Beta
Date Reported
RADIOCHEMISTRY
Results PCi/ 1
Date Extracted
Reported By
Date Analyzed
Lab Number
02 I ib0 NOV 10 88

0 LA c' F—'M:V,(O
r'. Department of Hurnan Resources
Sion of Health Services
SAMPLE ANALYSES REQUEST
State Laboratory of Public Heali
P. 0. Box. 2804
306 N. Wilmington Stre<
'Raleigh, 2761
Number
73 Field Sample Number 3 -�
�• C j,�'� �, e r CSite ).ocation
.me Of Sire G
lecced By S+ /-r na IDS+ S Date Collected /29�,L ! r Time 100 o �- / 3 cc
pe of Sample:
Concentrate Cometat�
~;nvironmental
Groundwater (1)
Surface Water (2)
��Soil (3)
Other (4)
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
INORG2
Extractables
dotal
ParameterResults
mg/1
Parameter
Results mg/1
Pararsieter Results mg/1
Arsenic
o . ®1
✓Arsenic
e
Silver 3
Barium
® $
✓Barium
"Cadmium
l
l
Sulfates
Zinc
!Cadmium
Chromium
Lead
�� � ®
®6
Chloride
✓Chromium
'�
Ph
Conductivity
9
TDS
MercuryCopper
,/
�elenium
_4. ® 0 o 5
Fluoride
TOC
Silver
®°`l
on
`®
7 �---
a D
- Lead
a
--
anganese
o �S
Mercury
Nitrate ,
Selenium
—
• 0
Parameter Results trig/ 1
ORGANIC CHEMISTRY
Parameter Results mg/1
—. P&T:GC/MS EDB
® Acid:B/N Ext. PCBs
TOX Petroleum
Endrin
Lindane
MICRO13IOLOGY
Parameter
(MF) Coliform Colonies/100mis
(MPN) Coliform Colonies/100mIs
Date Received
Date Extracted
n..
Parameter
Gross Alpha
Gross Beta
Date Reported
Parameter Results mg/1
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
RADIOCHEMISTR
Results PCi/ 1
Date Analyzed 10 1 n g
Lab Number 02 18 1 mIt 88

State Laboratory of Public Hca
C. Department of Human Resources SAMPLE ANALYSES REQUEST P. 0. Box 28C
vision of Health Services - 306 N. Wilmington Sr,
Rali•igh, 276
tc Number l � �
Field Sample Number 3 a3'
r. C\�.� Site )_.oca.don 7
Jame of Site '
J%a Av �, \ IDS Date Collected /vm1 Time /CO ®-13
nllected BY ..,.,�-�...,.,
f ype of Sample:
Environmental
Groundwater (1)
Surface Water (2)
11z"Soil (3)
Other (4)
Extractables
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
INORGANIC CHEMISTRY
Parameter Results mg/1 Parameter
(S.44mments
AH;.t�t
Total
Results mg/1 I Parameter
✓Arsenic d ® i
Arsenic —_ �•
a rium 9
�ilver
Sulfates
Barium —�---
_ ® �
.,ZCadmium
`Cadmium � �—
Zinc
Ph
r
- Chromium ®- �- 6
, Chloride
Conductivity
Leady
�� i7 �..
�`�� hromium
Cropper 4
TDS
_sL Mercury
elenium 0 ---
—Fluoride
TOC
ilvcr _/ 0o 02 �_
/eaCdIron —
y ( 9
L
—L
anganese
> '_ 4
— Mercury
Nitrate
eleniurn b
Results mg/1
3�
ORGANIC CHEMISTRY
Parameter Results mg/1
Parameter
Results mg/1
Parameter Results mg/-
EDB
Methoxychlor
P&T:GC/MS
PCB's
Toxaphene
Acid:B/N Ext.
Petroleum
2,4-D
TOX
Endrin
2,4,5-TP (silvex)
Linclane
MICROBIOLOGY
RADIOCHEMISTRY
Parameter
Results PCi/ 1
Parameter
Gross Alpha
(MF) Coliform Colonies/100mis
(MPN) Coliform Colonies/100mis
Gross Beta
Date Received
Date Reported
Date Extracted
Date Analyzed
Lab Number
021 Q NOV 10 88

S(-A t) F_ R F; Lx (vim
7. Department of Human Resources
Sion of Health Services
SAMPLE ANALYSES REQUEST
State Laboratory of Public Heald
P. 0. Box 2604'
306 N. Wilmington Stree
Raleigh, 2761
A Field Sample Number
Number
me of Site
n
C\�.� Site l oca,iol
n �'S Date Collected _���� y ! �-� Time I000—/30
leered By JT / r s' {��, 1D�1 _
a
,pe of Sample:
Concentrate iosaanaents --�
nvironmental
Groundwater (1) Solid (5) CZ
6id
Surface Water (2) Liquid ( ) k: "
oil (3) Sludge (7)
B
Other () r_
Other (4) dy IC
INORGANIC CHEMISTRY
Total
Extractables
Parameter Results mg/1 Parameter Results mg/1 Parameter Results mg/1
`/1 <3?
Arsenic
4 O O �
Arsenic
`
Barium
'1
St ver
Sulfates
Barium
Cadmium
•_ 0 O
°'Cadmium
C .=
1- —
Zinc
®„Chromium
4. 0
1 ®�
Chloride
`Chromium
g
Ph
Conductivity
%Lead
` ,
n _ c) O
°SCopper
TDS
Mercury
W/ elenium
<�CL---
Fluoride
TOC
✓ Silver
4
�_
Iron
✓Lead
/ I
!�
Manganese
--
___11,4ercury
-Nitrate.
_ZSelenium
'
Parameter Results mg/1
P&T:GC/MS
Acid:B/N Ext.
I TOX
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/100MIs
(MPN) Coliform Colonies/100mis
Date Received
ORGANIC CHEMISTRY
Parameter Results mg/1 Parameter
Results mg/1
EDB
i
Methoxychlor
PCB's
Toxaphene
Petroleum
2,4-D
Endrin
2,4,5-TP (silvex)
L' d ne -
Parameter
Gross Alpha
Gross Beta
Date Reported
RADIOCHEMISTRY
Results i'LA/ 1
Date Extracted
Date Analyzed
Lab Number
021763 NOV 10 88

5LtPF--- P_�: L,(N T:1
J. C. Department of Human Resources
yvision of Health Services
State Laboratory of Public 1-Iea
P. O. Box 28C
306 N. Wilmington Str
,Raltigh, 27f
;ice Number A
Field Sample Number 3
1 �
r , C��� Site Location,
s c5
Nnme of Site �r Lj A er S+i�a,1 9 /c�-�
:ollected By ._ ,g � pi, �, ; �,;,�- 1D� Date Collected � - Time 1C0®-1 �'
Type of Sample:
Environmental
Groundwater (1)
Surface Water (2)
L�Soil (3)
Other (4)
SAMPLE ANALYSES REQUEST
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Ohr(Al
ter' O...V CYYYYY�'d1163
0
+Y 6989,
ce
INORGANIC CHEMISTRY, ,
Extractables
Parameter
Results mg/1
Parameter
Arsenic
O 1
�
l5,
`Barium
� Q �
�Arsenic
arium
o
Cadmium
_aZCadmium
-Chromium
�-
Chloride
`' Chromium
Z, ad
2
ZCopper
ercury
_
� ® � � �-----
Fluoride
Selenium
Si� r
� � �
L
Iron
1 r�
Lead
Manganese
✓Mercury
—Nitrate.
_iz'gelenium
Parameter
P&T:GC/MS
Acid:B/N Ext.
TOX
Results mg/ 1
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/100mis
(MPN) Coliform Colonies/100mis
Date Received
Results mg/1
�ilver
Sulfates
1
Zinc
Ph
3
Conductivity
C 1 O
TDS
TOC
<1 a�
Q _ O T6
ORGANIC CHEMISTRY
Parameter Results mg/1
EDB
PCB's --
Petroleum ---
Endrin --
Lindane
Parameter
Gross Alpha
Gross Beta
Date Reported
Results mg/1
Parameter Results mg/1
Methoxychlor
Toxaphene
2,4-D
. 14;5-TP (silvex)
RADIOCHEMISTRY
Results PCi/ 1
Date Extracted
Reported By
Date Analyzed
Lab Number
021764 Nov i® 88

SLAP l2 F FWD
C. Department of Human Resources
ision of Health Services
SAMPLE ANALYSES REQUEST
State Laboratory of Public Hcald
P. O. Box 2804'
306 N. Wilmington Strcc
*'Raleigh 2761
7 a Field Sample Number `3
Number l y
Site j_OCatiOn
_Me Of Site �
I L}" Date Collected A-)) 9 1 t L � Time 100 o -13y
,Ilected By+� ^ �" ���' _ - ID#
pe of Sample:
Environmental
Groundwater (1)
Surface Water (2)
_1z�_Soil (3)
Other (4)
Extractables
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
INORGANIC CHEMISTRY
Parameter
Results mg/ 1
Parameter
'Arsenic
✓$arium
L �
17``'"�
LZArsenic
P%$arium
t�Cadmium
�
-Cadmium
O
d 0
hloride
_JZChromiurn
✓Lead
`
. ®O
9-
Chromium
:`Copper
f •�
_jZMercury
L,Selenium
b
og=!� —
Fluoride
=`// Silver
a
®a-
�Ion
C o 00__ _
eOLeaa
Manganese
Mercury
itrate .
Selenium
Parameter
P&i:GC/MS
Acid:B/N Ext.
TOX
Parameter
Results mg/ 1
Results mg/ 1
Cons rneixts j
`,M,
�...,?;
l otale
Parameter
a 5 Sulfates
�) Zinc
Ph
3 Conductivity
L 9 TDS
TOC
ORGANIC CHEMISTRY
Parameter Results rn9/1
_ EDB
PCB's
Petroleum
Endrin
Lindane
(MF) Coliform Colonies/100m1s
(MPN) Coliform Colonies/100mis
Date Received
Parameter
Gross Alpha
Gross Beta
Date Reported
Results mg/1
Parameter Results mg/1
Methoxychlor
Toxaphene
2,4-D
2,4,5®TP (silvex)
Results PCi/ 1
Date Extracted
Reported By
Date Analyzed
Lab Number
021 ?65 NOV 10 88

'DIVISION OF U.E.PLT-B SERVICES �`
SOLID -) HAZARDOUS 'WASTE KU-AG—M- Ri'�, -NCH
Locatica of Sampling:
Chain of Custod` Record
Hazardous Waste hat
Generator
Storage Facility
Other:
a/ItE
�.r
ansnorter
SnOSaP F acili
FOA
Treatment Fac:
Landf ill
MANCHE
;ompany- e S Name 0 �� )
kddress )4,,y F
Collector` s name Teleahone3.� --2o"o
signature
Date Sampled if 29 Time Sampled /®oo— /3oC)
Tyre of Process Generating Waste
Field Information
O,-, 1 0 ; .s �-A d- r; -- I-e- r,
-Fi ele. Sample No. q115
l4} 32
12.
l
7
/43S_
L41 le JW7 400 L/J ,? J
C-nain. of Possession:
signature title inclusive dates
2. C `ice 4....
signature title ' inclusive dates
3.
:�esu_zs reported
signature
signature
title
title
inclusive dates
Gate
Instructions: Complete all applicable information including signatures, and
submit with' analysis request forms.

SU l l : 1- p` LA A)
N. C. Department of Human Resources SAMPLE ANALYSES REQUEST
)ivision of Health Services
Site Number1 R> A Field Sample Number
Dame of Site �; Q A c C Q `"1' Site J-ocaFion
Collected By 5+� ^ �, �� 1 �_ ID# s Date Collette
Type of Sample:
Environmental Concentrate
Groundwater (1) Solid (5) Q-►2= 5 ' ` . t`
Surface Water (2) Liquid (6)
t O
oil
(7 Sludge Soil (3) g ) :•�,
Other (4) Other (8)
Extractasbles
Parameter Results mg/ 1
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Parameter
-ZP& T:GC/MS
Acid-B/N Ext.
TOX
Results mg/1
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/ 100mis
(MPN) Coliform Colonies/ 100mis
INORGANIC CHEMISTRY
Parameter Results mg/1
Arsenic
Barium
-- Cadmium
Chloride
Chromium
Copper
Fluoride
Iron
Lead
Manganese
Mercury
Nitrate,
Selenium
ORGANIC CHEMISTRY
Parameter Results mg/ 1
EDB
PCB's
Petroleum
Endrin
Lindane
Parameter
MAW
s
Total
Gross Alpha
Gross Beta
at aboratory of Public
P. O. Box
3 . W-'ImlMon
cc`�3 �a4li ll, '2:
LJ
Time /00 0 - 13 c
Parameter Results mg/ 1
Silver
Sulfates
Zinc
Ph
Conductivity
®'TDS
TOC
Parameter Results mg/1
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
Results PCi/ i
Date Received t i) ''� Date Reported
Date Extracted _ Hate Analyzed
t� �-
Reported By
• �� Lab Number

r
N. C. Department of Human Resources
Division of Health Services
.SLAPERFU,ruD
SAMPLE ANALYSES REQUEST
Site Number 1 a A Field Sample Number _
Name of Site S,- Q A ` rf_r Cl,,,, C``"� Site location—i.
Collected By _ 5�'a�b n�� �- ID#i _ 9- S Date Collected
G
Type of Sample: ,1�ti�
Environmental Concentrate �'
Groundwater (1) Solid (5) Co`"`Qas' IP
f
Surface Water (2) Liquid (6)
Soil (3) Sludge (7) -
Other (4) Other (8)
INORGANIC CHEMISTRY
ral
ot#Ezaboraltory of R.ublic H
P. O.\Box 2
306 N. Vi/iltnt Aton
j$ �` I a.kh"i 2
ICCo-1
Extractables
Total
Parameter Results mg/1
Parameter Results mg/ I
Parameter Results mg/
Arsenic
Arsenic
- Silver
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
Chloride
Ph
Lead
Chromium
Conductivity Y r
^_
Mercury
Copper.
TDS
Selenium
Fluoride
TOC
Silver
Iron
Lead
_
Manganese
Mercury
Nitrate
Selenium
Parameter Results mg/1
Parameter Results mg/ 1
Parameter Results mg
P&T:GC/MS
EDB
Methoxychlor
17 Acid:B/N Ext.
PCB's
Toxaphene
TOX
Petroleum
2,4-D
Endrin
2,4,5-TP (silvex)
Lindane
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/ 100MIs
(MPN) Coliform Colonies/100mis
Parameter Results PCi/I'
Gross Alpha
Gross Beta
I � 1
Date Received 4 ri 1- l 0 "? S Date Reported
Date Extracted 1' IS' SISbt"� Date Analyzed b '2°i'J2-/ - TeE ZZA
Renorted By Lab Number
502E i

LAI
rr306
atory'of
N. iC.s Department of Human Resources SAMPLE ANALYSES REQUEST P. 0
St
of Health Services N, Wilmi
ro
Site' Number 1 a A Field Sample Number '"`"
//�+
�) R �2 f- C), `-`�� __ Site J-Oca�lon
Niine of Site �.
Collected By 5�� ! +� ' n�, ID# ._ S Date Collected . Na,� 9� 1 c `Y is'
Type of Sample:JV
•Sy4 -
Environmental Concentrate Commernxs
11 M1. � '
Groundwater (1) Solid (5) �- base 0T; berms 100: tick 6, i Lie_ Orn.
"ol
Y
Surface Water (2) Ligtdd (6) _.
Soil (3) Sludge (7)
Other (4) Other (8)
INORGANIC CHEMISTRY
l
Extractables
Total
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg.
Arsenic
Arsenic
Silver
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
- Chloride
Ph
Lead
Chromium
Conductivity
_._._
Mercury
Copper
TDS
Selenium
Fluoride
TOC
_ Silver
Iron
Lead
_^
Manganese
_
Mercury
Nitrate .
Selenium
WO) ctgf;.Ul(Ky;# &IRJtW4
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg
T:GC/MS
EDB
Methoxychlor
Acid:B/N Ext..
PCB'''s
Toxaphene
TOX
Petroleum
2,4-D
Endrin
2,4,5-TP (silvex)
Lindane
MICROBIOLOGY iKAlJ1VUHCMt,'l K Y
Parameter Parameter Results PCi/ I
(MF) Coliform Colonies/100mis Gross Alpha
(MPN) Coliform Colonies/100mis Gross Beta
Date Received i3rJI - 10 - IT Date Reported
Date Extracted IS "91 A i Date Analyzed
8028
Reported By Lab Number

Si-t'� P-R,F vA►v D
It N. C. Department of Human Resources
Division of Health Services
a
SAMPLE ANALYSES REQUEST
Site Number i B A Field Sample Number
C�u�
Name of Site �� � Q A I }e � �L •" -Site I..ocaltion-
Collected By S+A n /' h :,Una) A ID# S Date Collected
Type of Sam -le: -
Environmental Concentrate
Groundwater (1) Solid (5)
Surface Water (2) Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
INORGI
P Box
306 N. Wiltgoon
- , R-gigh,
a
Extractables
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg
Arsenic
Arsenic
Silver
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
Chloride
Ph -----=- --
_ Lead
Chromium
Conductivity
_. Mercury
.Copper
TDS
Selenium
Fluoride
TOC
Silver
Iron
Lead
Manganese
Mercury
Nitrate
Selenium
re) z'TCY ZICox*a VT5IR!4M
Parameter Results mg/1
Parameter Results n9/1
Parameter Results mi
P&T:GC/MS
EDB
Methoxychlor
Acid:B/N Ext.
PCB's
Toxaphene
TOX
Petroleum
2,4-D
Endrin
2,4,5-TP (silvex)
Lindane
MICROBIOLOGY
1 Parameter
(MF) Coliform Colonies/100m1s
(MPN) Coliform Colonies/100mis
Parameter
Gross Alpha
Gross Beta
a f:-
ts
Date Received 11' 10-Yi AA Date Reported
BN A-
DateExtracted j1-1$-iSBb(i3 Date Analyzed 8` 30-Y�B� ss102-15�8b'"
Lab Number

S LA P l= 2. r U 0 f)
N. C. Department of Human Resources
Division of Health Services
SAMPLE ANALYSES REQUEST
Site Number i a A Field Sample Number
Name of Site C� Q A I �e l- -3,. a Q 1\2 Site Location _!
Collected By n ID# 4- S Date Collected
Type -of Sample:
Environmental Concentrate l r
Groundwater (1) Solid (5) 12 6'tSe t�
Surface Water (2) Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
INORGANIC CHEMISTRY
y133
306 N.
JAB! 6 '
K,Public 1
,Box,
Extractables
Total`'""'""��
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg,
Arsenic
Arsenic
Silver
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
Chloride
Ph
Lead
Chromium
Conductivity
Mercury
"Copper
TDS
Selenium
Fluoride
TOC
Silver
Iran
Lead
_
- Manganese
Mercury
Nitrate .
Selenium
ORGANIC CHEMISTRY
Parameter Results mg/I
Parameter Results mg/1
Parameter Results mg
Pl&T:GC/MS
EDB
Methoxychlor
c/ Acid:B/N Ext.
PCBs
Toxaphene'
TOX
Petroleum
2,4-D
Endrin
2,4,5 TP (silvex)
-Landane
RADIOCHEMISTR
Parameter Parameter Results PCi/ 1
(MF) Coliform Colonies/100mis Gross Alpha
(MPN) Coliform Colonies/100mis Gross Beta
i Date Received E3+J4~ tD'. g Date Reported
pA
Date Extracted 95 "$160. AA Date Analyzed jBI t-30-V 13& �a• 1�"$� 7ULr'
802874
u ..-__.._a In., ia6 Number ___---

SL? E.jZ_ (=- a(j �-
N. C. Department of Human Resources r' St `i o y Public 1
r1 Division of Health Services SAMPLE ANALYSES REQUEST P. 6i_�,Box :
306 N. Wilmitt�' ton
aleigh,
Site Number
1 aA Field Sample Number
A
`t
�.t
Name of Site A � e r ,' ^
5�
C \ Site 1_.ocaition )'
Collected By 5-t•A
/} } �. ID# ,S Date Collected _ �� `; 1T r�QO o
.^ � , � ^�
Type of Sample:
Environmental Concentrate
i
Groundwater (1) Solid (5) G g °* S e e z
Surface Water (2) Liquid (6) ;
✓ Soil (3) Sludge (7)
Other (4) Other (8)
INORGANIC
K
M
Extractables
Total^
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg
Arsenic
- Arsenic
Silver
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
Chloride
Ph
_ Lead
Chromium
Conductivity
Mercury
Copper
TDS
Selenium
Fluoride
TOC
Silver
Iron
Lead
Manganese
Mercury
Nitrate
Selenium
:e):CCE1101 [KI"; M61 "4ilm
Parameter Results mg/1
Parameter Results mg/1
Parameter Results tnj
EDB
Methoxychlor
�T:GC/MS
Acid:B/N Ext.
PCB's
Toxaphene
TOX
Petroleum
2,4-D
Endrin
2,4,5 TP (silvex)
Lindane
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/100MIs
(MPN) Coliform Colonies/100mis
ictsuiva.nr ma.� a n x
Parameter Results PCi/1
Gross Alpha
Gross Beta
Date Received 1'1 g Q ' �� Date Reported
- PA
Date Extracted 1� "a�-��i Z�,.�.�- Date Analyzed I I"3Q-,�t
Retorted By
Lab Number

St i' F_ R FLAB v
N. C. Department of Human Resources
Division of Health Services
SAMPLE ANALYSES REQUEST ev� r-_ ''�
Site Number ! B A Field Sample Number
Name of Site 5� �) A }e "'� ^ Site J.ocgion .
Collected By 5+, n IDS# � � Date Coll
Type of Sample:
Environmental Concentrate
Groundwater (1) Solid (5)
Surface Water (2) Liquid (6) `-
_ZSoil (3) Sludge (7)���p
Other (4) Other (8)
INORGANIC CHEMISTRY
try of Public 1
,�P-O.Box 2
306 N. T4rnington
;,,Raleigh, 2
d.
r
Extractables
Total
Parameter Results mg/1
Parameter Results'mg/1
Parameter Results mg,
Arsenic
Arsenic
Silver
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
Chloride
Ph
Lead
Chromium
Conductivity
Mercury
C©pper
TDS
Selenium
Fluoride
TOC
Silver
Iron
Lead
Manganese
Mercury
Nitrate
Selenium
lei Zf 14?z1V i617 � 11I"Iis1
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg
�P&T:GC/MS
EDB
Methoxychlor '
✓Acid:B/N Ext.
PCB'.s
Toxaphene
TOX
Petroleum
2,4-D
Endrin
2,4,5 TP (silvex)
Lindane
ttxuiv%:ricnmio i tc
Parameter Parameter Results PCi/1
(MF) Coliform Colonies/100m1s Gross Alpha
(MPN)_Coliform Colonies/100mis Gross Beta
Date Received 1 I —11)- yl,' 6 Date Reported
Date Extracted aq "n X A 0 R, Date Analyzed i 1_30" V IS& �r1 9L-1 Ct -S$ -yu l
n .._.,_ -A a.. -_ _ _ Lab Number

I
FLANS
306 N. N
1k% 6 _
Site Number 1 3 _ A Field Sample Number s
Name of Site
l �t C \ k Site Location Pulle
e� � � A �� �
ID# Date Collected Ah) 9 - �` +
Collected By S+A � /� �' -E� nr, 5
Type of Sample: - (� Y
- Environmental Concentrate Zom ents
i Groundwater (1) Solid (5) tD o a S �� r,
Surface Water (2) Liquid (6)
Soil (3) Sludge (7) - f-
Other (4) Other (8)
,
N. C. Department of Human Resources
Division of Health Services
SAMPLE ANALYSES REQUEST �
INORGANIC CHEMISTIi.Yr ,
`dt Pbblic F.
P. 0. %x 2
h1mingtp11 ;
+ri
L
+ilk''.: _.
Extractables
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results: mg/
Arsenic
Arsenic
Silver
Barium
Barium
Sulfates _
— Cadmium
- Cadmium
Zinc
Chromium
Chloride
Ph
_ Lead
Chromium
Conductivity
-- Mercury
Copper
TDS
Selenium
Fluoride
TOC
Silver
Iron
Lead
Manganese
- Mercury
Nitrate
Selenium
ri�Te""ito" *l-:ut &trA!4
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg,
-ZF&T:GC/MS
EDB
Methoxychlor
Acid:B/N Ext.
PCB's
Toxaphene
TOX
Petroleum
2,4-D
Endrin
2,4,5 TP (silvex)
Lindane
Parameter Parameter Results PCi/1
(MF) Coliform Colonies/100m1s Gross Alpha
(MPN) Coliform Colonies/100m1s Gross Beta
Date Received O�o- i� Date Reported
Date Extracted I I - A,99 5X Q•0---' Date Analyzed '" W 1 cl �91 'UC-
- --- n Lab Number

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH :SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 - 306 N. WILMINGTON, ST.. RALEIGH. N.C. 27611
--'WE/REUTRAL AND ACID
EXTRACTABLES
E. G
J
��tr.��+IYA..II�.
i
S
W
maim
• .
119IGhL•�
__
heiachlbrobutAidiene
2... ..
,diethyl phthalate
me MM
Rl D L_
3 - Estimated value. �zO�SoIL
:K - Actual value is known to be less than value given.
L - Actual value is known to be greater than value given.
'U - material was analyzed for but not detected. The number is the Minimum Detection Limit- M2)L
NA - Not analyzed. �~
A/ - Tentative identification. ~^
12/ - On NRDC List of Priority Pollutants.

STATE LABORATORY OF PUBLIC HEALTH
t DIVISION OF HEALTH SERVICES. N.C. DEPARTMENT OF HUMAN RESOURCES-
P.O. BOX 28047 - 306 N. WILMINGTON, ST.. RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
1 ASE/NEUTRAL AND ACID LAB NO ©"-&7 V0J-Y/.j? 21QZffy Z�'
EXTRACTABLES FIELD ItZ0 1,2C7Zle,1413 Q
COMPOUND TYPE f 3.
UNi:TS /1 /k /k . /k /k
pXrene
�'JL� t •
►
A r
•binzYl
ghthalate
WAOEIMM_M_=
-
M�=�W
a1 #
1-LM
'lr=,� r��i�si
•
�__��iq�ilii�Ml�hJ��
.. .. thene
b6nzoic acid
ben�Xl alcohol
• _
sfff.•rr sn.fffff.�,nff..�
��
��
maw
3 - Estimated value. Ns0/SC/L
K - Actual value is known to be less than value given.
L - Actual value is known to be greater than value given.
u - Material was analyzed for but not detected. The number is the Minimum Detection Limit. M':z i
NA Not analyzed. -- �-
1/ - Tentative identification.
2/ - On NRDC List of Priority Pollutants.

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT Of HLK4AN RESGURCES
P.O. BOX 28047 - 306 N. WILMINGTON. ST., RALEIGH. N.C. 27611
TNTrAt AMA[ YCTt
..
EU
OR=
_
aF.
...
'�®�®�®�
Ownanthrene
Estimated value. 92.0%50/1—
K - Actual value is known to be less than value given:
L - Actual value is known to be greater than value given.
't! - Material was ,analyzed for but not detected. The number is the Minimum Detection Limit. r}Zj L
Not analyzed:
Tentative identification.
/ - On'NRDC List of Priority Pollutants.
J.C. Div&5ion o6 Heal th Senv.icu

STATE LAB WATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMM RESOURCES-
P.O. BOX 28047 - 306 N. WILMINGTON. ST., RALEIGH. N.C. 27611
ORGANIC CHEMICAL ANALYSIS
BASE/NEUTRAL AND ACID
EXTRACTABLES
.. • • �
�,��
�':�sslil
�ew�,�y�
may- 7
1r.77
rJ C1t�
� i cA3./1
f
mm�mmw/!�►�==®IN
ne
benzoic acid
• • •
WM--__iM—
WI
' • •
f•►'If--yam--_�®�—���
f • f
MDL-
3 - Estimated value. H&OIS40/1-
K - Actual value is known to be less than value given.
L - Actual value is known to be greater than value given.
U - material was analyzed for but not detected. The number is the Minimum Detection Limit. Mal.
NA - Not analyzed. — — '-
�, 1/ - Tentative identification.
2/ - On NRQC List of Priority Pollutants.

�f
SIATE LABORATORY OF PUBLIC NEALI._
DIVISION OF HEALTH SERVICES. O.C..UEPARViEHT 'OF HUt" RESOURCES
P.O. BOX 28047 - 306 N. WILHINGTON. S7.. RALEICH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
,. • •
.. .
IMA ..
90�
Y
���\Ilq \.�GV Y\SIUe..
K - Actual value is known to be less than value given.
L - Actual value -is known to be greater than value given.
U - material was analyzed for but not detected. The number is the Minimum Detection Limit.
NA - Not analyzed.
1/ - Tentative identification.
2/ - On NRDC List of Priority Pollutants.
N.C. Division of Health Services

I
STATE LABORATORY OF PUBLIC HEAL1-mi
DIVISION OF HEALTH SERVICES. N•.C_ I)EPARTItcNT OF HUMAN RESOURCES
P.O. BOX 26047 - 306 N. WILMINGTON, ST., RALEIGH. N.C_ 27611
ORCANIC CHEMICAL ANALYSIS
�1M�.
•1
. . .
• '
�
1(La1'�
a a • • • ♦ -
rrr_r_r_r_�_
• • •
rrr_r�r_r�t_
• • .
r®r_r_r�r
rrr_r�r�r®r�
�r_
• • • • �.-
rrr_r�r�r�r-
• • •
rrr_r_r®
�®_
• •
carbontetrachlbride
• •• - • • •
rrr__rr�r_r�
tri-chl• •
rrr__rr_r_r_
rrr__rr®r_®_
• •
rrr_�rr�r_r�
OMNI
. • • • ��
r®r�_rr
r�r_
• •
rrr__rr�
�r_
• •
rrr-_rr_r-r_
rrr_-rr�r�®
. •
rrr�r-r�r-r_
• •
rrr�r_r-r�r�
rrr�rr�rrrrrrrrrrrrr�
:�..
irrrrrrrrrrrrrrrr�rrrrr
r�►�rr�rrrr�rr
r�►irrr��
i��r■rr�
rr�r
rr�
�rrrrr
- cs-umaLea vawe.
K - Actual value is known to be less than value given.
' L - Actual value- is known to be greater than value given.
U - Material was analyzed for but not detected. The nurber is the Minimum Detection Limit.
NA - Not analyzed.
I/ - Tentative identification.
7/ - On NROC List of Priority Pollutants.
1 N.C. Division of Health Services

a....
'.N. C. Department of Human Resources
Division of Health Services
5(-"?F.Z�` (0D
SAMPLE ANALYSES REQUEST
i -P..A Field Sample Number
Site Number
Name of Site
' )Ali < C-�'^� Site location
J� ID# -S Date Col jtcFd
Collected By Spa ^ �` `'"
Type of Sample: -
i
Environmental Concentrate '
1/ Solid (5}
Groundwater (1)
Surface Water (2) Liquid (6)
J
Soil (3) Sludge (7)
Other (4) Other (8)
INORGANIC CHEMIS'I�-•:
-
StrJ306
*f%Tbc¢ 6FI5
P. O.
N. Wilmit
' Z �) AN)al
1arl-Ci
F�
H
Total
Extractables
Results mg/ 1
Parameter
Results m / 1
Parameter Results mg/
Parameter
Silver
Arsenic
Arsenic
Sulfates
Barium
Barium
Cadmium
Zinc
Cadmium
Chloride
Ph
Chromium
Chromium
Conductivity ,
Lead
Copper
TDS
Mercury
Fluoride
TOC
Selenium
Silver
Iron
Lead
Manganese
Mercury
i
Nitrate •
J
Selenium
ORGANIC CHEMISTRY'
Parameter Results mg/ 1
Parameter
Results mg/ 1
Parameter Results mg
EDB
Methoxychlor
P&T:GC/M S
PCB.'s
Toxaphene
,�ACId:B/N Ext.
Petroleum
2,4-D
TOX
Endrin
-
2,$,5.TP (silvex)
Lindane
MICROBIOLOGY
RADIOCHEMISTRY
Parameter
Results PCi/1
Parameter
(MF) Coliform Colonies/100m1s
Gross Alpha
(MPN) Coliform Colonies/ 100mis
Gross Beta
(� 1(i R
- Date Reported
Date Received
l3 iS�
I I' Z Z ' 8 N��
Date Extracted �—�
/
Date Analyzed
t-Z`t-Sh�
Lab Number
Rcoorted By

I
S�_& �> t_.;;Z_r,APJ D
N. C. Department of Human Resources
,,nivision of Health Services
SAMPLE ANALYSES REQUEST
Site Number 1 i3 A Field Sample Number
•Name of Site S,
Lj
A Climb Site L.oca;ion
-,,Collected By Lf/ ted
- �� — S Date Collec
iType of Sample:
Environmental Concentrate
Groundwater (1) Solid (5) e_`�
_ Surface Water (2) Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
Extractables
�....p,Stat&Laboratory of Public He
`
Box 2E
t itagpri Si
Raleigh, 27
1 2 '7
�
�A� yi 1RR•i ;d,.
%j
A,
Time _00- 1
:ornments
lAN 1 14PI9
-_21
SUPFRF:UND..t`'�
INORGANIC CHEMISTRY ' `��lN
Total
Parameter Results mg/1
Parameter Results mg/1
Arsenic
Arsenic
Barium
Barium
Cadmium
Cadmium
Chromium
Chloride
.__ Lead
Chromium
Mercury
Copper
Selenium
Fluoride
Silver
Iron
Lead
Manganese
Mercury
Nitrate .
Selenium
ORGANIC CHEMISTRY
Parameter Results mg/ 1
Parameter Results mg/ 1
P&T:GC/MS
EDB
Ext.
PCB's
_2Acid:B/N
TOX
Petroleum
Endrin
_
Lindane
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/100mis
(MPN) Coliform Colonies/ 100mis
Parameter
Gross Alpha
Gross Beta
Parameter Results m.g/:
Silver
Sulfates
Zinc
Ph
Conductivity
TDS
TOC
Parameter Results mg,
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
Results PCi/ I
Date Received 1 Date Reported
ON A PT'
Date Extracted l� ��� Date Analyzed 1 1-7- '-Ygb o la-4—
I Reported By
Lab Number �;'��

SZ t— LAN.D
N. C. Department of Human Resources
SAMPLE ANALYSES REQUEST
State Laboratory of Public H
ox 21
I Division of Health Services
f 306 itiii toh.E
.. Raleigh, 2'
Z�
_
I
Field Sample Number
Sire Number
5� (�� � 1r r- t 7
L\�.� l
� _ -Site 1_.oca�ion
Name of S ice I- A �
S �'' ^°'
ID# S - Date Collected ALJ`}
leto �'. 'me O0
Collected By ` . `�
Type of Sample:
S ���.
T,
Environmental Concentrate r
' n
Groundwater (1)
Solid (5) `Te `
- _
Surface Water (2)
Liquid (6) -?
- Soil (3)
SIudge (7)
C :•guy p -
Other (4)
Other (8) .
v
CHEMISTRY•',+�
INORGANIC.
1
Cal•
Extractables
R_aoS
Parameter Results mg/1
-J�aTameter Results rug/
Parameter Results mg/1
Arsenic
Arsenic
- Silver
- Sulfates
Barium
Barium
Cadmium
Zinc
_ Cadmium
Chloride
- Ph
Chromium
Lead
Chromium
Conductivity
Mercury
.Copper
Fluoride
TDS
TOC
Selenium
Silver
Iron
Lead
Manganese
Mercury
Nitrate,
Selenium
nUMANIC CHEMISTRY
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg
P&T•GC/MS
EDB
Methoxychlor
=Acid:B/N Ext.
PCB's
Toxaphene
TOX
Petroleum
2,4-D
Endrin
2,4,5-TP (silvex)
Lindane
E IST1D s'
MIC:KVl31VLV�i ][
Parameter
(MF) Coliform Colonies/ 100MIs
(MPN) Coliform Colonies/100mis
Parameter
Gross Alpha
Gross Beta
RADIOCH M
Results PCi/ 1
Date Received f 1y Date Reported
eN jft
-za-4s'� (3r4 Pia-a-SS�v'
Date Extracted I I `11"V Y'i3 Date Analyzed
Reported By
Lab Number

N, C. Department of Human Resources
Division of Health Services
Swe 6- p-r-uN-
SAMPLE ANALYSES REQUEST
I
Site Nuttiber l a AField Sample Number
CA �� G.. _ C.\,,.b Site Loca;ion�
Name of Site • » �
Collected By Sta ^ Ai,, ^r' ID# Date Collected
Type of Sample:
Environmental Concentrate
Groundwater (1) Solid (5) 2 S
Zfi
Surface Water (2) Liquid (6) .
.E
✓ Soil (3) Sludge (7)
Other (4) Other (8) --
INORGANIC CHEMISTRY
wry of Public F
P. O. Box 2
st
306 N. Vlilm►ngton
R%leig h, 2
z ro 1gg9
rTurt CC O
Comments
Extractables
Total
Parameter Results mg/1 ;
Parameter Results mg/1
Parameter Results mg,
Arsenic
Arsenic
Silver
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
Chloride
Ph
Lead
Chromium
Conductivity
_
Mercury
Copper
TDS
Selenium
Fluoride
TOC
Silver
Iron
Lead
Manganese
Mercury
Nitrate ,
Selenium
t 1K"ALIN 1%. %.r1DfnLa I rL a
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg
P&T:GC/MS
EDB
Methoxychlor
✓ Acid:B/N Ext.
PCB-'s
Toxaphene
TOX
Petroleum
2,4-D
Endrin
-2,4,5-TP (silvex)
Lindane
MICROBIOLOGY tcn t�iv�,ncnua i n z
Parameter Parameter Results PCi/1
(MF) Coliform Colonies/ 100mis Gross Alpha
(MPN) Coliform Colonies/100mis Gross Beta
Date Received j (— /6 - n X Date Reported
[3NA 1511
Datt Extracted i` 1`a� 8$bCR Date Analyzed Zq,���' S� ���.-•1-8$-'
Reported By Lab Num" er 802! a o

Appendix E
March 1992 Letter by Paragon Environmental Group, Inc.

FIR
RANGE GLEAN -UP piViSi(?N
j 4rch.•10, ' 1902 -.
`�2r.: Rcn xd: bb:' : t.•i:3PMty_i2,:.
Sir Wal'er` Gun Club: 3 . y• '
P:6 'Box i026 . • "' 340:: - '.: ; ,
Ralei.gh,. I1: C;'. 21*603
:. ,.. ••
R8. ' ,RXXON OF &EAD ddWTAXX!fA�Tq FROM.BBIL.
:. F.L 1NT�l ION$, '�IT� CIF .'t E.',7 HAhT3?GN A: BgOfJTIXti A�TGE. t RMES{%.X
i T2LI2 D,1B.X. tR: Ai 'BR; iTN Ct U$;
'� .• ♦ • ty-• • .. ,)tom ,i`' — ' . •+
Ae cliectiss ed''tY�ie Acope; ' � _'tanr3t'; pe o nes .fcic }Six'..Walt�r:`Gun`.Club -
�4onaf sted of . tha :o11Qwyriq
'°Location - The ilivar Plantation i* ih''Wake: 'County ,No a ' '7
r.• _- rth:Caral n
. :eagt-:of the.':oi y 2 :aiit`..of Raleigh 'arid sae t:'of-.the--:61iy .limit
it-1 o" to`'and oP.'.
a• • g �u : accessed .'fr�iia • �ts'•hi.'Qhway 64.. ' • . ...• :,.
; aTo� & RI LE s ty ail' sfoifago, vas - .trimmed .ri'o'r`-.-to• -, —n
pzragori' a mobile :soil' 'sCX�is�nin lain: pars on g
farmed triple '
• screening on -`the .'en i>re lar e:'of the i�ackgtop 'of the p still berm;
which 161g:'by y10' •'high, •the '®oil'=bras• sreeid to =a�
level' 'af .8". deep, st` a 'mIl imurk.. on°-the•,•ent re backstop =fern, and k :: depth.' of 1 'al'oncl the • +snt rep:center ':face of•, tii+ 'backstop: at -the ._
Rahootng tone - ^ieviil ' (or ;C ! Nbrth `erld South.:top to :`attom • =as . 'yau:..:
#ice •tie berm/b�tcki�
is The . scree iirng`••plant- • has � .4 peck .Vibra�ir screen ` that is mouhted :
on a *'60 'cieyx'ae ang3,e: .Matarj,al was excavated .:using `a backiiae.'
:Material is c#roppeci onto.'the -h6pper.. �ah'i:ch' ii equipped With •drizzly
bats: ..t*,o ' pro�ebt' -•from; ,large kock,:•_or' tree.:.liimbs :entering ;`the
`system. The mat ria ' is ti inn Carr* J4ii,�by :gdnveyor up,'the .ii�achine:
where -' -it 'drops': oti�b 0he top deck ;of th®:.vibrating 'screenA'�shoot a=
is a aohed ito..the top .screen that aXla�is. a .patktwa ,fbr cur
y _ '.'
water• a� to move':and accutaUlate. `he :square mesh on':fhe .top n �r scree :i'
is 2 . by 'Z"•,; =:''T#�ex•efcire', :any : taaterial ' :greaten. that " 2"bass'
x t iroUgh the _top' "screen `down ,.¢nto the bb. tom screen' ihat lea"cures
!. 3 f41' •from :opposite corners- of. ths': nOide"lueSb ' .-Hateris1 ':greater
than 1141! Wi2-1,-rol'l. off-'of.'the bottvin acre®n :deck :and;$Gctiiaulate
:a' secgrid �p.# le 'ccsez to ilia
niaahrie. '�:

: . r • �9rs"t %T
' '= r •... •s .• r•~•�• '•�•.r• eS: . Va .. s:� j• •_. •:• . •S :+. ,•s
M IT
Material `that passive h ' :.. . :{
ydx'aiil rough 't?}e `i'/. ti, bottom "deck :d O s =' ` .
a`' second' h Jo nvayrr►. which' 'car er x P down ,onto '•.:
de e• ari g ' • . the: 'mat-ar l _
gre gIe'b o�.zt:-dro s'do n':o t ?,a
': shetilig. This grocecue :.Wag':.re �' n o: U' milliinetor.. pozxethylene''
p at$d .two More dimes .b placing.
the :fin 3y croenecl soils :#pack t}iroucjh :t.... stems "iri y'
capture' Ied '�nater'ial a could, Y a'' egrt' tci.
:3�q ri :sc en . hat':.c u ;la'vra pos�sibYe passed throe' he
re Iivwever; , the 2 ii deck `' t
al : ttnnr hen i Was` .re 3 aced :with'' ;►
screen .'sb dater , p. a ."1 : 'harp..
- :greater• the' ��oud'paaO-through, and::materi n -�,.• �otfid''rol al
course matrial:pi�;e 1 off the:;c�eck:.tiirough the shoot
• - 'the ` •�� .,:• • ':tee•.' •r: ••° •• .• s't.�l, �••�•
• i I4 . bottom cTck 'acreeri
Y cdla.ber' :w •washiose zb.... ma ort ' y
eapan.''fi • d:''-lino' �.` cause 'the. y.'of.,
the backstop has a, a2 •
cal�.bert ''3'riches' _ Tw16nty '
bulgy et by. ' n hire .til' is •theaset- tb,: the ,.�4" me8� .size ' het2 `
•... •. .. I : • '�' T..
xt nt i :�xpan, when 'fared am.. f lane o "so e .
�.ed ' e der n het': nay$ c n:r ut t m
allow =the / �f _:rites g men .caht taY ; of =this p oaeisa woui
t' sc�e. t� tir® al _ d
maehihe P molt .ill o the e. T)ie
1 . zs . nct ,ab] 2 'tc
f :rc k d3fterQn'ti,ate betty an' .a reatet ��. . and lead 6ii'4 i . a :F 5 khan , j,4'
ent� otunatel d
:of:•roc]t. tjh't 'waul Tito y% the moil; �iad a' Ziinite
d tali .. phis `cat y.;
i •Thy. .• %'. ,. ..•`:y-:y. y: ••r. ._.,' ;,y ;
�. lead%rcick' mate }�
trans d. rx l' - t W, a .stored .in llo
t4:ortec3r=t Mastr:ietals`.(85p st Thr n dins,, s�rtd r
4113► phone ' .'(21) f2� .2.361' ire'St•.r.levand, 'Ohio
a' Pareg'on bolt trick •for :fie' coritaot.'is
OHDog7613871.Me£aie�
hie rif],e berm "d men* cins'-%of both
9h, and 40 Yong by 1p`i 'h-..s' are: 90 bong tv 10,;
:prc�cdurea used'Qx' b4thi rill g - f
'used • for. -the: _ • 'ruts°. 'tirrox• .the''•'. x'o�e8rir k ,,
berms .weree' ca ated o Tn a :entir@?aaktop Ace -.Of
shootiri ,. n, :depth, •:. incrasfnq :to a ..j� e' depth •s
the backsstog Zb�2ori 6 eNor�htant�' 'South) top to bottok :aa you fa,*
•
.. � • t� ir�le�ii�ti�s "• - _' •:
' eritire�"prQect; tcoll� ted drums
l c -19 `af6ad :mat .ia ` d'ro k' :.:
:..P�4�nds siz S. Theh totOcte weight :of mate3a3,' "smelted was :1 ° :Q
weathisr, :the' .d tee of ' .wok p r caned in iv* phales due ="tQ ad
9�3%9�, tb-9�8%91t W4 performed were `8/22/91=to�s�9� ..an11
:If you 'have . r
'a:hy- �questjctz�s
"
-�' nC�rB�y;
_' • � • _ i•��h�i Tr�• 4• •aS s7St` •�. .J• '`l.•f'• .t.• _;( :
J '_: ••. •t try ♦'t ••' s-q ••% 't tis ii .� .f•:rl •

January 2011 Letter Report by S&NEE, Inc.

January 4, 2011
Sir Walter Gun Club
P.O. Box 585
Creedmoor, NC 27522-0585
C/O Mr. Richard Cobb
1636 Brook Run Dr
Raleigh, NC 27614
Attention: Mr. Richard Cobb
Reference: Additional Soil Testing - Abandoned Rifle Range Berms
Silver Plantation, Former Sir Walter Gun Club
Knightdale, North Carolina
S&ME Project No. 1054-10-252
Dear Mr. Cobb:
S&ME is submitting the findings of additional soil testing performed for the Sir Walter Gun
Club (SWGC) on the 100-Yard Rifle Range Berm and 200-Yard Rifle Range Berm at the former
SWGC Knightdale rifle range. Our services were performed in general accordance with S&ME
Proposal P128-1 OV dated June 30, 2010. The additional testing was authorized by you in a
telephone conversation with David Wells of S&ME on December 10, 2010.
PROJECT INFORMATION
Sir Walter Gun Club formerly used the Silver Plantation property located in Knightdale, North
Carolina as a shooting range. The location of the former rifle range is shown on Figure 1. In
August and September 1991 environmental assessment and remediation was performed by
Paragon Environmental Group on behalf of Sir Walter Gun Club on earthen berm backstops at
the former pistol and rifle ranges at the Knightdale site. Paragon screened the surface soil from
the faces of the shooting range berm backstops to separate the lead bullets and lead fragments
from the earthen material. The lead was reportedly removed from the property and sent to
Master Metals of Cleveland, Ohio for disposal. The stripped and screened soil from the berm
surfaces was reportedly transported to the Sir Walter Gun Club facility in Creedmoor, North
Carolina where it was used as berm material in the shooting range facility in Creedmoor.
According to information you provided, two rifle range soil backstop berms are located on the
Knightdale site. We understand that the earthen berm backstops have undergone maintenance
since they were constructed to repair weathered surfaces, maintain the berm heights, and to
restore the berm thicknesses in the shooting zone, and that not all lead contaminated soil was
removed during the August and September 1991 remediation performed by Paragon.

Additional Soil Testing - Abandoned Rifle Range Berms S&ME Project 1054-10-252
Silver Plantation, Former Sir Walter Gun Club
Kniahtdale, North Carolina January 4 2011
As requested, S&ME performed confirmation sampling in the two rifle range berm backstops to
assess the earthen berm material for contaminants resulting from the shooting operations.
S&ME prepared a report Findings of the Limited Soil Assessment - Abandoned Rifle Range
Berms, dated November 18, 2010. After reviewing S&ME's report, SWGC authorized S&ME to
analyze samples already in the laboratory for total lead or extractable lead concentrations. The
following summarizes the results of additional testing performed on soil samples collected from
the soil berms.
ASSESSMENT FINDINGS
S&ME performed soil sampling activities on the two former rifle range berms on October 12,
2010. Samples were collected with a stainless steel hand auger that was decontaminated
between boring locations and between sample intervals in accordance with S&ME's Remedial
Investigation Work Plan. Six soil sample locations, three in each rifle range berm, were used to
assess the soil. Each of the six sample locations consisted of four borings (twenty-four total soil
borings) to depths of approximately 30 inches into the berm. The locations of the borings were
positioned on the front and back of the berm and were completed near the base, middle or top
portions of the berm. A portable global positioning survey (GPS) instrument was used to collect
coordinate locations of the boring locations and perimeter points on the former rifle range berms.
The berm and sample locations are shown on Figures 2 and 3, respectively.
Soil borings were advanced into the soil berms to collect grab samples at three depth intervals
from 0 to 6 inches, 12 to 18 inches and 24 to 30 inches. Four grab samples from the same depth
interval were mixed together for each sample location to form composite samples representative
of the three sample depth intervals.
One grab and one composite sample per sample location were placed into laboratory containers
and submitted to the laboratory for analysis. The remaining composite samples were placed into
laboratory containers that were also sent to the laboratory; however, testing was held pending the
results of the initial grab and composite sample analyses. The soil samples were packed in an
insulated cooler with ice and delivered under chain -of -custody protocol to Environmental
Science Corporation (ESC) in Mt. Juliet, Tennessee. Additional testing for total lead
concentrations were requested and performed on samples held in the laboratory. Two samples
previously analyzed for total lead were also requested to be analyzed for extractable lead by the
Toxicity Characteristic Leaching Procedure (TCL,P) by EPA Method 1311. The laboratory did
not have sufficient sample volume remaining to run the TCL,P analyses, therefore, S&ME
delivered additional sample volume from the original sample containers collected and retained
by S&ME.
100-Yard Rohe Range Berm
Berm Surface to 6"
Total lead analyses for soil samples S-1-C-3, S-1 Comp, S-3 C-2 (Grab), and S-3 Comp were
discussed in S&ME's November 18, 2010 Findings of the Limited Soil Assessment - Abandoned
Rifle Range Berms. Total lead results from soil samples analyzed from the former 100-yard rifle
range berm indicated that soil to a depth of six -inches on both the front and back of the berm is
impacted with total lead concentrations at levels exceeding either North Carolina Department of
2

Additional Soil Testing - Abandoned Rifle Range Berms SME Project 1054-10-252
Silver Plantation, Former Sir Walter Gun Club
Kniohtdale North Carolina January 4 2011
Environment and Natural Resources (NCDENR) Inactive Hazardous Sites Branch (IHSB)
Preliminary Health -Based or Protection of Groundwater Soil Remediation Goals (PSRGs). Lead
concentrations in soil from the berm surface to a depth of 6 inches from the berm surface ranged
from 78 milligram per kilogram (mg/Kg) to 5,100 mg/Kg. These samples were also previously
analyzed for semi -volatile organic compounds (SV®Cs) where up to seven poly aromatic
hydrocarbon compound concentrations were detected at levels above IHSB PSRGs.
TCLP analysis performed on soil sample S-1 Comp (0-6") detected 91 milligram per liter (mg/L)
lead in the extracted leachate. This extracted lead concentration is above the Hazardous Waste
Section Level of 5 mg/L which prohibits non -hazardous disposal without pretreatment.
12"-18" from Berm Surface
Total lead was analyzed from soil samples S-I Comp, S-2 Comp, and S-3 Comp from the former
100-yard rifle range berm from the depth interval of 12 to 18 inches. Lead concentrations in soil
sampled between 12 inches and 18 inches from the berm surface ranged from 260 mg/Kg to
3,200 mg/Kg which indicated that soil on both the front and back of the berm is impacted with
total lead concentrations at levels above IHSB PSRGs.
No samples were analyzed for TCLP lead or SV®Cs from the depth interval between 12 inches
and 18 inches in the former 100-yard rifle range berm.
24"-30" from Berm Surface
Total lead was analyzed from soil samples S-1 Comp, S-2 Comp, and S-3 Comp from the former
100-yard rifle range berm from the depth interval of 24 to 30 inches. Lead concentrations in soil
sampled between 24 inches and 30 inches from the berm surface ranged from 35 mg/Kg to 470
mg/Kg which indicated that soil on both the front and back of the berm is impacted with total
lead concentrations at levels above IHSB PSRGs in some of the berm.
No samples were analyzed for TCLP lead or SV®Cs from the depth interval between 24 inches
and 30 inches in the former 100-yard rifle range berm.
Berm Surface to 6"
Total lead analyses for soil samples S-4 C-1 (grab), S-4 Comp, S-6 C-1 (grab) and S-6 Comp
were discussed in S&ME's November 18, 2010 Findings of the Limited Soil Assessment -
Abandoned Rifle Range Berms. Total lead concentrations in three of four samples analyzed
exceed one or both of the IHSB PSRGs. Total lead concentrations ranged from 160 to 7,800
mg/Kg. The test results for soil in the 200-yard berm indicate that soil to a depth of six -inches
on both the front and back of the berm is impacted with total lead at levels above IHSB PSRGs.
No samples were analyzed for SV®Cs from the former 200-yard rifle range berm.
TCLP analysis performed on soil sample S-4 C-1 (Grab) from 0-6" detected 720 mg/L lead in
the extracted leachate. This extracted lead concentration is above the Hazardous Waste Section
Level of 5 mg/L which prohibits non -hazardous disposal considerations without pre-treatment.
3

Additional Soil Vesting - Abandoned Rifle Range Berms S&ME Project 1054-10-252
Silver Plantation, Former Sir Walter Gun Club
Kni4htdale, North Carolina January 4 2011
12"-18" from Berm Surface
Total lead was analyzed from soil samples S-4 Comp, S-5 Comp, and S-6 Comp from the former
200-yard rifle range berm from the depth interval of 12 to 18 inches. Lead concentrations in soil
sampled between 12 inches and 18 inches from the berm surface ranged from 100 mg/Kg to
8,200 mg/Kg which indicated that soil on both the front and back of the berm is impacted with
total lead concentrations at levels above IHSB PSRGs in some of the berm.
No samples were analyzed for TCLP lead or SVOCs from the depth interval between 12 inches
and 18 inches in the former 200-yard rifle range berm.
24"-30" from Berm Surface
Total lead was analyzed from soil samples S-4 Comp, S-5 Comp, and S-6 Comp from the former
200-yard rifle range berm from the depth interval of 24 to 30 inches. Lead concentrations in soil
sampled between 24 inches and 30 inches from the berm surface ranged from 280 mg/Kg to 560
mg/Kg which indicated that soil on both the front and back of the berm is impacted with total
lead concentrations at levels above 1HSB PSRGs in the berm.
No samples were analyzed for TCLP lead or SVOCs from the depth interval between 24 inches
and 30 inches in the former 200-yard rifle range berm.
The results of the additional analytical tests from samples collected October 12, 2010 are
summarized in 'fable I. (Soil test data from 1988 is also included in Table 1). A copy of the
analytical reports for the additional total lead and TCLP lead testing is attached in Appendix II.
DISCUSSION
The analytical results from the limited soil assessment and the additional testing reported herein
were reviewed.
Soil — 24"-30" from Berm Surface — Both Berms
Three composite soil samples were analyzed from the 24 and 30 inch depth from both the former
100-yard and 200-yard rifle range berms (six total samples). The analytical data indicated that
total lead concentrations ranged from 35 to 560 mg/Kg. Four of the soil samples contained total
lead marginally above the NCDENR IHSB PSRGs. Two of the soil samples did not contain lead
levels in soil above the NCDENR IHSB PSRGs. It is likely that soil from the 24 inch depth and
deeper would not exceed lead leachable levels of 5 mg/L, which is the Hazardous Waste Section
Level for non -hazardous disposal considerations without preliminary treatment.
Soil — from Berm Surface to 18" Deep — Both Berms
Two soil samples with known total lead concentrations (5,100 mg/Kg and 7,800 mg/Kg) were
analyzed to assess the soil for extractable lead concentrations. The TCLP analyses detected
extractable lead concentrations of 91 mg/Kg and 720 mg/Kg, respectively. Both sample
concentrations exceeded 5 mg/L which is the Hazardous Waste Section Level for non -hazardous
disposal considerations without preliminary treatment. Elevated total lead concentrations (1,200
mg/Kg to 8,200 mg/Kg) were detected in four of six composite samples collected from
penetration depths of approximately 18 inches. Based on the elevated lead concentrations, it is
L

Additional Soil Testing - Abandoned Rifle Range Berms SME Project 1054-10-252
Silver Plantation, Former Sir Walter Gun Club
Kniuhtdale, North Carolina January 4 2011
likely that extractable lead levels above 5 mg/L are present in soils from the penetration depth of
approximately 18 inches or deeper in some berm segments.
Using the dimensions of the berms approximated from S& N1E's site visit and the total lead
concentrations from soil samples collected on October 12, 2010, the volume of soil that is likely
contaminated with lead in the former rifle range berms was estimated.
Volume estimates for lead -contaminated soil that will likely require treatment and/or disposal are
based on the following assumptions:
• The former rifle range berms were divided into segments based on grab sample locations
and analytical test results.
• Each sample area (S-1 through S-6) is representative of approximately 25 to 35 feet of
berm segment.
• Dimensions of the berm segments were estimated from site measurements and
observations made on October 12, 2010 by S&ME personnel.
• Extractable lead concentrations above 5 mg/L are assumed present in soil up to a depth of
approximately 18 inches on the face and back of both former rifle range berms in five of
six berm segments.
• Total lead concentrations above IHSB PSRGs for lead impact a zone of five of six former
rifle range berm segments. The lead contamination ranges in penetration depth from less
than two to over 3.5 feet from the face and back of the former 100-yard rifle range berm a
penetration depth of approximately 1.5 to 3.5 feet from the face and back of the former
200-yard rifle range berm.
• Soil at the core of the former rifle range berms is assumed to have lead concentrations
that may remain on -site.
• A 20 percent factor is assumed for the volume estimates due to the level of accuracy of
berm measurements.
The following table summarizes the estimated volumes of lead contaminated soil in the former
rifle range berms.
Soil Sample Area
Berm Segment
Berm
Segment
Location
a Soil Volume in
cubic yards with
Lead >5 mg/L
— Soil Volume in cubic
yards with Lead <5
L and >PSRGs
S-1
100-yard
38
32
S-2
100-yard
40
0
S-3
100- and
50
22
S-4
200- and
95
76
S-5
200-yard
107
60
S-6
200-yard
0
70
Estimated Total
—330
—260
Calculations used to estimate the lead -contaminated soil volumes are summarized in Appendix
I.

Additional Soil Vesting - Abandoned Rifle Range Berms S&ME Project 1054-10-252
Silver Plantation, Former Sir Walter Gun Club
Knightdale, North Carolina January 4 2011
CONCLUSIONS
S&ME visited the site on October 12, 2010 to collect soil samples. Initial soil assessment data
from this sampling event was reported by S&ME in their Findings of the Limited Soil
Assessment - Abandoned Rifle Range Berms, dated November 18, 2010. Additional soil samples
were analyzed to assess the depth of penetration of lead contamination in the former rifle range
berms. The analytical data indicated that total lead concentrations above the NCDENR IHSB
PSRGs were present in soil samples collected at penetration depths between 24 and 30 inches
from both the former 100-yard and 200-yard rifle range berms.
TCLP analysis from two soil samples with known total concentrations detected extractable lead
concentrations that exceeded 5 mg/L. The Hazardous Waste Section bevel for non -hazardous
disposal considerations without preliminary treatment is 5 mg/L of extractable lead by TCLP
analyses.
Based on analytical results of total and extractable lead concentrations, field measurements and
site observations used to estimate berm volume, S&ME estimates that approximately 330 cubic
yards of berm soil may contain extractable lead concentrations above 5 mg/L, and approximately
260 cubic yards of soil berm material may be contaminated with non -hazardous concentrations
of lead that may exceed IHSB PSRGs.
RECOMMENDATIONS
Based on the results of this limited assessment, S&ME recommends obtaining bids from
qualified environmental contractors for services to treat transport and dispose of the lead
impacted soil. The request to bidders should include but not be limited to: summaries of
previous projects, references, description of their treatment method to reduce the leaching
potential, confirmation testing to document extractable lead concentrations post treatment,
location and type of permitted disposal facility, as well as unit rates with estimated total costs.
After the bids are procured, a remedial action plan to remediate the impacted material at the site
can be prepared and implemented in general accordance with IHSB requirements. Once the
remedial action is performed and confirmation sample results are below the NCDENR IHSB
PSRGs, then a soil remediation report with an incident closure request may be made to the
NCDENR IHSB.
LIMITATIONS
This report and resulting documents, including the final report, are limited to the referenced
project and client. No other use is authorized by S&ME.
6

Additional Soil Testing - Abandoned Rifle Range Berms S&ME Project 1054-10-252
Silver Plantation, Former Sir Walter Gun Club
Kniohtdale. North Carolina January 4 2011
CLOSURE
We appreciate the opportunity to submit this proposal and look forward to continuing to work
with you on this project. If you have any questions regarding this proposal, please contact us.
Sincerely,
S&ME, Inc.
David B. Wells, P.G.
Senior Geologist
om Raymond, P.E.
Senior Consultant
Attachments: Table 1 Summary of Soil Analytical Data — October 12, 2010
Figure 1 Vicinity Map
Figure 2 Site Map
Figure 3 Sample Locations
Appendix I Calculations
Appendix II Laboratory Report
S:\iTROJECTS\2010\10-252 Sir Walter Club Soil Assessment Abandoned Rifle Range Berms\Report\Lead in Soil Report\Lead In
Soil - Rifle Range Berms.doc
7

TABLE I
SOIL ANALYTICAL DATA (October 12, 2010)
FORMER RIFLE RANGE BERMS - SIR WALTER GUN CLUB
KNIGHTDALE BOULEVARD
KNIGHTDALE, NORTH CAROLINA
NCDENR IHSB ID NONCDO000019
S&ME Project No.1054-10-252

-777
it
l.�r �u,e,d�.i:•.= d..+'iE1 �,1:..._..���td•,i�r,--_���,.dc.r..ar..�a�..il„_.a,r�c:uu.v>-_�.\\�,.a:�4:,:�r-s,s�il:.: _ „: �a�=--s1i:.�i;.�ti. w .,,.,
�:• c;.� ( / r.l; -�� �.{c�/•,\":� - � It I.! >}�•� , C��lar c=::.+T'r`l�lr.+•t'�r'j� 'r .r-i-,: 'C.
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�7�

GRAPHIC SCALE
F50 0 75 150 300
IMAGE SOURCE: NC
ONEMAP, RALEIGH, DATED 2007
( IN FEET
A,-199'i
sCu..� 1 N = 300'
DATE: Nov. 2010
*S&M E
SITE MAP
�`
DRAWN M BTR
WWW.SMEINC
2
PROJECT NO:
COM
NC ENGINEER LICENSE NF-0176
SIR WALTER GUN CLUB, INC. - ABANDONED RANGE
„
1054-10-252
3201 SPRING FOREST RD, RALEIGH, NC 27616
KNIGHTDALE, NORTH CAROLINA

GRAB GRAB
S-4 C-2 S-4 C-3
S-5 C-1 S-5 C-2 S-6 C-1 S-6 C-2
- - --� �---
1
S-4 C-1 S-4 C-4
WEST END
S-5 C-3
S-5 C-4 S-6 C-4
200 YARD SOIL BERM
APPROXIMATE DIMENSIONS:
90 TO 95 FEET LONG
20 TO 49 FEET WIDE
10 TO 18 FEET HIGH
GRAB
DUP-1
S-1 C-
GRAB
S-3 C-2 S-3 C-3
S-1C1 -- -- _....v---- L/--s'
S-1 C-4
WEST END S-• -1 GRAB S-3 C-1 •
S-1 C-2 S-2 C-4 S-3 C4
APPROXIMATE DIMENSIONS:
90 TO 95 FEET LONG
18 TO 22 FEET WIDE
6 TO 8 FEET HIGH
S-6 C-3
EAST END
EAST END
LEGEND
SAMPLE BORING ON FRONT FACE OF BERM
0 SAMPLE BORING ON BACK OF BERM
SOIL SAMPLES COLLECTED ON OCT. 12, 2010
NOTE: SAMPLE INTERVALS FOR GRAB AND/OR COMPOSITE SAMPLES:
INTERVAL 1, 0 - 6 INCHES
INTERVAL 2,12 -18 INCHES
INTERVAL 3,24 - 30 INCHES
SCALE: _ 1" = 20' •-1 92
*S&ME FIGURE No.
DA1� Nov.2olo SOIL BORING LOCATIONS
DRAM BY. BTR °
WWW.SMEINC.COM SIR WALTER GUN CLUB, INC. - ABANDONED RANGE
PRc3aF "® NC 1 SPRING FOREST RD, RALE KNIGHTDALE, NORTH CAROLINA
1054-10-252 s201 SPRING FOREST RD, RALEIGH, NC 27616

Sir Waiter (gun Club
Knightdale, North Carolina
SME Project No. 1054-10-252
Summary Lead Analyses
Berm
Se meat
Extractable: e ,
m /L
Total Lead m /K
Approximate Berm Segment
Dimensions Feet
0-6"
12418"
24-30"
Length
Width
Height
S-1
91
5,100
1,200
470
25
18
8
S-2
NA
260
35
35
20
9
S-3
3,000
3,200
220
30
22
6
S-4 Grab
720
7,800
NA
NA
NA
NA
NA
S-4 Comp
3,400
8,200
440
27
49
12
S-5
NA
3,500_
560
30
32
12
S-6
410
100
280 1
33
25
10
Action Level <5 mg/L 400/270 mg/Kg
Volume estimates for lead -contaminated soil that must be treated and/or disposed are based on the following
assumptions:
• The former ride range berms were divided into segments based on grab sample locations and analytical test
results.
Each sample area (S-1 through S-6) is representative of approximately 25 to 35 feet of berm segment.
• Dimensions of the berm segments were estimated from site measurements and observations made on October
12, 2010 by S&NIE personnel.
® Extractable lead concentrations above 5 mg/i., are assumed present in soil up to a depth of approximately 18
inches on the face and back of both former rifle range berms in five of six berm segments.
• Total lead concentrations above I):iSB PSRGs for lead impact a zone of five of six former rifle range berm
segments. The lead contamination ranges in penetration depth from less than two to over 3.5 feet from the face and
back of the former 100-yard rifle range berm a penetration depth of approximately 1.5 to 3.5 feet from the face and
back of the former 200-yard rifle range berm.
site.
Soil at the core of the former rifle range berms is assumed to have lead concentrations that may remain on -
A 20 percent factor is assumed for the volume estimates due to the level of accuracy of berm measurements.

Calculations (Continued)
Segment S-1
Leachable Lead >5mg/L
Lead >IHSB PSRGs and <5 mg/L
Segment S-2
100-Yard Berm
Leachable Lead >5mg/L
Lead >IHSB PSRGs and <5 mg/L
Segment S-3
Leachable Lead >5mg/L
Lead >IHSB PSRGs and <5 mg/L
Length Width
Thicness
-cubic feet
cubic yards
25
21
1.6
840
31
25
14
2
700
26
Length Width
Thicness
-cubic feet
-cubic yards
35
25
1
875
32
0
0
Length Width
Thicness
cubic feet
cubic yards
30
21
1.8
1134
42
30
16
1
480
18
Segment S4
Length Width
Thicness
-cubic feet
-cubic yards
Leachable Lead >5mgfL
27
49
1.6
2116.8
78
Lead >IHSB PSRGs and <5. mg/L,
27
42
1.5
1701
63
Segment S-5
Length Width
Thicness
-cubic feet
-cubic yards
200-Yard Berm
Leachable Lead >5mg/L,
30
40
2
2400
89
Lead >IHSB PSRGs and <5 mg/L,
30
30
1.5
1350
50
Segment S-6
Length Width
Thicness
-cubic feet
-cubic yards
Leachable Lead >5mg/L,
0
0
Lead >IHSB PSRGs and <5 mg/L
33
32
1.5
1584
59
Estimated Soil Volume 100-Yard Beret
-Cubic Yards
Leachable Lead >5mg/L
106
Lead >IHSB PSRGs and <5 mg/L
44
Estimated Soil Volume 200-Yard Berm
Leachable Lead >5mg/L
167
Lead >IHSB PSRGs and <5 mg/L
172
Volume Soil Plus 20% Contingency
Leachable Lead >5mg/L
327
Lead >IHSB PSRGs and <5 mg/L,
258

1
10
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
David Wells
S&KE Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
Report Summary
Monday.December 20, 2010
Report Number: L493179
Samples Received: 10/14/10
Client Project: 1054-10-252
Description: Sir Walter Gun C
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have an
questions regarding this data package, please do not hesitate to caly
l.
Entire Report Reviewed By:��
Tom Mellette , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT - PH-0197, FL - E87487
GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704, ND - R-140
NJ - TN002,NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 00109, WV - 233
AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032008A,
TX - T104704245, OK-9915
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA ELAP-
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 15

JOESC
L•A•S S•C•1•£•I -C E•5
lsmmalmmnanffm•
David Wells
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800--767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 20,2010
Date Received
October 14, 2010
ESC Sample #
L493179-01
Description
Sir Walter Gun Club
Site ID
Sample ID
S-1 COMP 12-18 IN
Collected By
Project #
1054-10-252
Collection Date
10/12/10 13:00
Parameter
Dry Result
Det. Limit Units Method
Date Dil.
Total Solids
88.4
% 254OG
12/15/10 1
Lead
1200
0.28 mg/kg 6010B
12/19/10 1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 2 of 15

I
L•A•B S•c•f•E-N•c•E•6
• -
REPORT OF ANALYSIS
David Wells
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 20,2010
ESC Sample #
: L493179-02•
Date Received
October 14, 2010
Description
Sir Walter Gun Club
Site ID
Sample ID
S-1 COMP 24-30 IN
Project #
1054-10-252
Collected By
Collection Date
10/12/10 13:00
Parameter
Dry Result
Det. Limit Units Method
Date Dil.
Total Solids
92.2
% 2540G
12/15/10 1
Lead
470
0.27 mg/kg 6010B
12/19/10 1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 3 of 15

3
JOESC
L-A,® S•C-f•E•M•C•E•S
-1
REPORT OF ANALYSIS
David Wells
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 20,2010
ESC Sample #
L493179-03
Date Received
October 14, 2010
Description
Sir Walter Gun Club
Site ID
Sample ID
S-2 COMP 12-18 IN
Project #
1054-10-252
Collected By
Collection Date
10/12/10 13:45
Parameter
Dry Result
Det. Limit Units Method
Date Dil.
Total Solids
93.4
%- 2540G
12/15/10 1
Lead
260
0.27 mg/kg 6010B
12/19/10 1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 4 of 15

12065 Lebanon Rd.
Mt. Juliet, TN 37122
OESC
[phone]
1-800-767-5859
Fax [phone]
I
Tax I.D. 62-0814289
• •
Est. 1970
REPORT OF ANALYSIS
David Wells
December 20,2010
S&ME Inc. - Raleigh NC
3201 Spring Forest
Road
Raleigh, NC 27616
Date Received
October 14, 2010
ESC Sample # L493179-04
Description
Sir Walter Gun Club
Site ID
Sample ID
S-2 COMP 24-30 IN
Project # 1054-10-252
Collected By
Collection Date
10/12/10 13:45
Parameter
Dry Result Det. Limit
Units Method Date Dil.
Total Solids
92.5
% 2540G 12/15/10 1
Lead
35. 0.27
mg/kg 6010B 12/19/10 1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 5 of 15

OESC
I
K]
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
David Wells
December 20,2010
S&ME Inc. - Raleigh
NC
3201 Spring Forest Road
Raleigh, NC 27616
Date Received
October 14, 2010
ESC Sample #
L493179-05
Description
Sir Walter Gun Club
Site ID
Sample ID
S-3 COMP 12-18 IN
Collected By
Project # : 1054-10-252
Collection Date
10/12/10 14:30
Parameter
Dry Result Det. Limit
Units Method
Date Dil.
Total Solids
86.4
% 254OG
12/15/10 1
Lead
1
3200 0.29
mg/kg 6010B
12/19/10 1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 6 of 15

12065 Lebanon Rd.
Mt. Juliet, TN 37122
JOESC
[phone]
1-800-767-5859
Fax [phone]
1-•A•8 5•C-I-E-N•C, E•5
Tax I_D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
David Wells
December 20,2010
S&NE Inc. - Raleigh
NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample # : L493179-06
Date Received
October 14, 2010
Description
Sir Walter Gun Club
Site ID
Sample ID
S-3 COMP 24-30 IN
Project # 1054-10-252
Collected By
Collection Date
10/12/10 14:30
Parameter
Dry
Result Det. Limit
Units Method Date Dil.
Total Solids
93.6
% 254OG 12/15/10 1
Lead
220 0.27
mg/kg 6010B 12/19/10 1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 7 of 15

12065 Lebanon Rd.
akA
Mt. Juliet, TN 37122
[phone]
y
i
1-800-767-5859
Fax [phone]
L-A•B 5•C-i•E•N C•E•S
Tax I.D. 62-0814289
•
Est. 1970
REPORT OF ANALYSIS
David Wells
December 20,2010
S&ME Inc. - Raleigh
NC
3201 Spring Forest Road
Raleigh, NC 27616
i
ESC Sample # L493179-07
Date Received
October 14, 2010
Description
Sir Walter Gun Club
Site ID
Sample ID
S-4 COMP 12-18 IN
Project # 1054-10-252
Collected By
Collection Date
10/12/10 15:15
Parameter
Dry Result Det. Limit
units Method Date Dil.
Total Solids
88.5
%- 254OG 12/15/10 1
1
I Lead
8200 1.4
mg/kg 6010B 12/19/10 5
K
Results listed are dry weight basis,
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 8 of 15

OESC
f
REPORT OF ANALYSIS
David Wells
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Pax [phone]
Tax I.D. 62-0814289
Est. 1970
December 20,2010
ESC Sample #
:
L493179-08
Date Received
October 14, 2010
Description
Sir Walter Gun Club
Site ID
Sample ID
S-4 COMP 24-30 IN
Project #
1054-10-252
Collected By
Collection Date
10/12/10 15:15
Parameter
Dry Result
Det. Limit Units Method
Date Dil.
Total Solids
88.8
g 254OG
12/15/10 1
Lead
440
0.28 mg/kg 6010B
12/19/10 1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 9 of 15

1kl
12065 Lebanon Rd,
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Pax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
David Wells
December 20,2010
S&ME Inc. - Raleigh
NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample#
L493179-09
Date Received
October 14, 2010
Description
Sir Walter Gun Club
Site ID
Sample ID
S-5 COMP 12-18 IN
Project # 1054-10-252
Collected By
Collection Date
10/12/10 15:50
Parameter
Dry
Result Det. Limit
Units Method
Date Dil.
Total Solids
87.7
% 254OG
12/15/10 1
Lead
3500 0.28
mg/kg 6010B
12/19/10 1
Results.listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 10 of 15

OESC
k
mampuln.22MIMMMM
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
David Wells
December 20,2010
S&ME Inc. - Raleigh
NC
a 3201 Spring Forest Road
Raleigh, NC 27616
'
ESC Sample #
L493379-lo
Date Received
October 14, 2010
Description
Sir Walter Gun Club
Site ID
Sample ID
S-5 COMP 24-30 IN
Project # 1054-10-252
Collected By
Collection Date
10/12/10 15:50
Parameter
Dry Result Det. Limit
Units Method
Date Dil.
Total Solids
89.2
%- 254OG
12/15/10 1
Lead
560 0.28
mg/kg 6010B
12/19/10 1
U
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 11 of 15

WAEi OF CHO1Cr
REPORT OF ANALYSIS
David Wells
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
12063 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I_D. 62-0814289
Est. 1970
December 20,2010
ESC Sample #
L493179-11
Date Received
October 14, 2010
Description
Sir Walter Gun Club
Site ID
Sample ID
S-6 COMP 12-18 IN
Project #
1054-10-252
Collected By
Collection Date
10/12/10 16:15
Parameter
Dry Result
Det. Limit Units Method
Date Dil.
Total Solids
90.0
% 2540G
12/15/10 1
Lead
100
0.28 mg/kg 6010B
12/19/10 1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
► This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 12 of 15
J

4
I
a
W.", A 6. , "C H O I C C
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est, 1970
REPORT OF ANALYSIS
David Wells
December 20,2010
S&ME Inc. - Raleigh NC
3201 Spring Forest
Road
Raleigh, NC 27616
ESC Sample #
L493179-12
Date Received
October 14, 2010
Description
Sir Walter Gun Club
Site ID
Sample ID
S-6 COMP 24-30 IN
Project # 1054-10-252
Collected By
Collection Date
10/12/10 16:15
Parameter
Dry
Result Det. Limit
Units Method
Date Dil.
Total Solids
90.7
254OG
12/15/10 1
Lead
280 0.28
mg/kg 601OB
12/19/10 1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
This report shall not be reproduced, except in full, without the written approval from ESC
The reported analytical results relate only to the sample submitted
Reported: 12/20/10 09:16 Printed: 12/20/10 12:20
Page 13 of 15

12065 Lebanon Rd:
Mt. Juliet, TN 37122
*ESC-
[phone]
1-800-767-5859
Fax [phone]
L•A•B S-Gi•E•N•C•E•S
a •
Tax I.D. 62 0814289
S&ME Inc. -
•
Raleigh NC
Est. 1970
David Wells
3201 Spring
Forest Road
Quality Assurance Report
Level II
Raleigh, NC
27616
�
December 20, 2010
L493179
Laboratory Blank
Analyte
Result
Units % Rec
Limit
Batch Date Analyzed
Total Solids
< .1
WG513139 12/15/10 06:11
Total Solids
< .1
WG513138 12/15/10 07:47
7 Lead
< .25
mg/kq
--
WG513833 12/19/10 17:35
Duplicate
Analyte
Units
Result Duplicate RPD
Limit
Ref Samp Batch
Total Solids
%
78.0 78.0 0.296
5
L493316-05 WG513139
Total Solids
90.0 89.2 0.623
5
L493179-10 WG513138
Laboratory Control Sample
Analyte
Units
Known Val Result
% Rec
Limit Batch
Total Solids
%
50 50.0
100.
85-115 WG513139
Total Solids
%
50 50.0
100.
85-115 WG513138
Lead
- mg/kg
113 109.
96.5
77.3-122.1 WG513833
Batch number /Run number / Sample number cross
t
reference
WG513139:
R1505110: L493179-11
12
WG513138:
R1505134: L493179-01
02
03 04 05 06
07 08 09 10
WG512797:
R1506749: L493179-01
02
03 04 05 06
07 08 09 10 11 12
WG513833:
R1509371: L493179-01
02
03 04 05 06
07 08 09 10 11 12
* * Calculations are performed prior to rounding of reported values.
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.,
Page 14 of 15

.y
*ESC
S&ME Inc. -Raleigh NC
David Wells
3201 Spring Forest Road
Raleigh, NC 27616
Quality Assurance Report
Level II
L493179
The data package includes a summary of the analytic results of the quality
control samples required by the SW-846 or CWA methods. The quality control
samples include a method blank, a laboratory control sample, and the matrix
spike/matrix spike duplicate analysis. If a target parameter is outside
the method limits, every sample that is effected is flagged with the
appropriate qualifier in Appendix B of the analytic report.
Method Blank - an aliquot of reagent water carried through the
entire analytic process. The method blank results indicate if
any possible contamination exposure during the sample handling,
digestion or extraction process, and analysis. Concentrations of
target analytes above the reporting limit in the method blank are
qualified with the "9" qualifier.
Laboratory Control Sample - is a sample of known concentration
that is carried through the digestion/extraction and analysis
process. The percent recovery, expressed as a percentage of the
theoretical concentration, has statistical control limits
indicating that the analytic process is "in control". If a
target analyte is outside the control limits for the laboratory
control sample or any other control sample, the parameter is
flagged with a "J4" qualifier for all effected samples.
Matrix Spike and Matrix Spike Duplicate - is two aliquots of an
environmental sample that is spiked with known concentrations of
target analytes. The percent recovery of the target analytes
also has statistical control limits. If any recoveries that are
outside the method control limits, the sample that was selected
for matrix spike/matrix spike duplicate analysis is flagged with
either a "J5" or a "J6". The relative percent difference (%RPD)
between the matrix spike and the matrix spike duplicate
recoveries is all calculated. If the RPD is above the method
limit, the effected samples are flagged with a 11J3" qualifier.
Page 15 of 15
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax 1.D. 62-0814289
Est. 1970
December 20, 2010

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Eat. 1970
David Wells
S&KE Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
Report Suumnary
Monday December 20, 2010
Report Number: L493471
Samples Received: 12/14/10
Client Project: 1054-10-252
Description: Sir Walter Gun Club
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have an
questions regarding this data package, please do not hesitate to caly
l.
Entire Report Reviewed By:.
M 4
Tom Mellette , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT - PH-0197, FL - E87487
GA - 923, IN - C-TN-01, KY 90010, KYUST - 0016, NC - ENV375/DW21704, ND - R-140
NJ - TN002,NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 00109, WV - 233
AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032008A,
TX - T104704245, OK-9915
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
Note: The use of the preparatory EPA Method 3511 is not approved or endorsed by the CA ELAP.
This report may not be reproduced, except in full, Without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 5

i
L-A- B S•C-I•E•M•C-E-S
s a • �
T
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-167-5859
Fax [phone]
Tax E.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
David Wells December 20,2010
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
` Date Received December 14, 2010 ESC Sample # L493471-01
Description Sir Walter Gun Club
Sample ID S-1 COMP 0-6 IN Site ID
Collected By Project 1054-10-252
Collection Date 10/12/10 13:00
Parameter Result Det. Limit Units Limit Method Date/Time By Dil
TCLP Extraction - 1311 12/17/10 0850 MVE 1
Lead 91. 0.050 mg/l S.0 6010E 12/19/10 1001 ALT 1
IL
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Limit - Maximum Contaminant Level as established by the US EPA
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 12/20/10 16:35 Printed: 12/20/10 16:35
Page 2 of 5
I

12065 Lebanon Rd
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
David Wells December 20,2010
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample # L493471-02
Date Received December 14, 2010
Description Sir Walter Gun Club
Site ID
Sample ID S-4 C-1 GRAB 0-6 IN
Collected By Project 1054-10-252
Collection Date 10/12/10 15:15
Parameter Result Det. Limit Units Limit Method Date/Time By Dil
TCLP Extraction - 1311 12/17/10 0850 MVE 1
Lead 720 0.50 mg/1 5.0 6010B 12/19/10 1404 ALT 10
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Limit - Maximum Contaminant Level as established by the US EPA
Note -
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 12/20/10 16:35 Printed: 12/20/10 16:35
Page 3 of 5

Summary of Remarks For Samples Printed
12/20/10 at 16:35:50
6'1
TSR Signing Reports: 690
R5 - Desired TAT
GW -Arsenic always needs ASG
Sample: L493471-01 Account: SMERLNC Received: 12/14/10 07:15 Due Date: 12/20/10 00:00 RPT Date: 12/20/10 16:35
Sample: L493471-02 Account: SMERLNC Received: 12/14/10 07:15 Due Date: 12/20/10 00:00 RPT Date: 12/20/10 16:35
i

"y
*ESC
J
s •
S&ME Inc. - Raleigh NC
David Wells
3201 Spring Forest Road
Raleigh, NC 27616
Quality Assurance Report
Level II
L493471
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62 0814289
Est. 1970
December 20, 2010
Laboratory Blank
Analyte
Result
Units Rec
Limit
Batch Date Analyzed
Lead
< .05
mg/1
WG513916 12/19/10 08:57
Duplicate
Analyte
Y
Units
Result Duplicate RPD
Limit
Ref Samp Batch
Lead
mg/1
0 0 0
20
L493922 01 WG513916
Laboratory Control Sample
Analyte
Units
Known Val Result
Rec
Limit Batch
Lead
mg/l
1.13 1.10
97.3
85-115
WG513916
Analyte
Units
Matrix Spike
MS Res Ref Res TV
% Rec
Limit
Ref Samp
Batch
Lead
mg/1
1.13 0 1.13
100.
75-125
L493922-01
WG513916
Analyte
Units
Matrix Spike Duplicate
MSD Ref %Rec
Limit
RPD Limit
Ref Samp
Batch
Lead
mg/l
1.16 1.13 103.
75-125
2.62 20
L493922-01
WG513916
Batch number /Run number / Sample number cross reference
WG513599: R1508075. L493471•-01 02
WG513916: R1510293: L493471-01 02
* Calculations are performed prior to rounding of reported values.
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers
Page 4 of 5

JOESC
L•A•B S-C-I-E-N•C-E•S
S&ME Inc. - Raleigh NC
David Wells
3201 Spring Forest Road
Raleigh, NC 27616
Quality Assurance Report
Level II
L493471
The data package includes a summary of the analytic results of the quality
control samples required by the SW-846 or CWA methods. The quality control
samples include a method blank, a laboratory control sample, and the matrix
spike/matrix spike duplicate analysis. If a target parameter is outside
the method limits, every sample that is effected is flagged with the
appropriate qualifier in Appendix B of the analytic report.
Method Blank - an aliquot of reagent water carried through the
entire analytic process. The method blank results indicate if
any possible contamination exposure during the sample handling,
digestion or extraction process, and analysis. Concentrations of
target analytes above the reporting limit in the method blank are
qualified with the "B" qualifier.
Laboratory Control Sample - is a sample of known concentration
that is carried through the digestion/extraction and analysis
process. The percent recovery, expressed as a percentage of the
theoretical concentration, has statistical control limits
indicating that the analytic process is "in control". If a
target analyte is outside the control limits for the laboratory
control sample or any other control sample, the parameter is
flagged with a "J4" qualifier for all effected samples.
Matrix Spike and Matrix Spike Duplicate - is two aliquots of an
environmental sample that is spiked with known concentrations of
target analytes. The percent recovery of the target analytes
also has statistical control limits. If any recoveries that are
outside the method control limits, the sample that was selected
for matrix spike/matrix spike duplicate analysis is flagged with
either a "J5" or a "J6". The relative percent difference (%RPD)
between the matrix spike and the matrix spike duplicate
recoveries is all calculated. If the RPD is above the method
limit, the effected samples are flagged with a 11J3" qualifier.
Page 5 of 5
12065 Lebanon Pd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
December 20, 2010

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Appendix D
October 2000 Memorandurn by
NCDENR Site Evaluation and Removal Branch

4
Oct(.-)ber 5: 2000
ficad
fin.1101.1ve Bazard atis Sites Branch
Throuorl): Dem
Site tvaluaTion aiW Removal BraD�--:7�
T 4.
Site Evffa`and Rernov, Branch
Re; Sir WaItcr G.un cju,,�,
US Tlvvy 64 Eal.st
KajghtdMe,'Wa'kt County
&-j

0i0i £!, �' S�; :fit ' IP;.
Site Photographs

Photo 9: Soil stockpile located immediately east of 200 yard impact
berm containing remnants of former target frames.
Photo 10. Sieving a surface soil sample collected from the forest
floor behind the 200 yard impact berm.
amen
AMEC Environment & Infrastructure, Inc.
285 Davidson Avenue, Suite 405
Somerset, NJ 08873
Former Sir Walter Gun Club Site
Knightdale, North Carolina
Appendix E
Site Photographs
21 February 2012

Photo 11: lest pit RR 100-6 excavated into the front of the 100
yard impact berm.
Photo 12: Rear of the 100-yard impact berm.
amec Appendix E
Former Sir Walter Gun Club Site
AMEC Environment & Infrastructure, Inc, Knightdale, North Carolina Site Ph
285 Davidson Avenue, Suite 405 e Photographs
Somerset, NJ 08873
21 February 2012

4
.
�T.�rpt. - V4,
�,
. � � •,`F�. .� ' -""� ,fir !".=..,. , _

0

4r
ilk
116

1' �.t_ fir ,., _ - . ♦ 1
Sli
_ 4-+ I 1 i°"lr Et, i I
r �� � yu r� '^z•A�,�yyTtrt1�t��A_I�. 'Sh � � 'e'i�r. r � e,t�'.'��
�����` h:4'3.w t'r••g-Yf 1.,s. •� y.f�! 7v4.\ i�� �� ..r�t � .�.�•-d �Af .fit+'
r i,tP
I-
Ap
r
bd
one

1 inch owl
04
i
t
00o • ,• 0
Photo 21: Lead shot collected 250 feet downrange of Skeet Field station
No. S.
Photo 22: Magnified view of the same lead shot sample, showing evidence of
dissolution (corrosion) and weathering of the grains.
ame& Appendix E
Former Sir Walter Gun Club Site
AMEG Environment& infrastructure, Inc. Knightdale, North Carolina Site Photographs
285 Davidson Avenue, Suite 405
Somerset, NJ 08873
21 February 2012

• 1 . inch 01
C:
I
Cl
.- -
Photo 23: Lead shot collected 400 feet downrange of Skeet Field station
No. 8.
Photo 24: Magnified view of the same sample showing varying degrees of
dissolution and weathering (note the faceted surfaces on some grains).
am Appendix E
Former Sir Walter Gun Club Site
AMEC Environment & Infrastructure, Inc.
285 Davidson Avenue, Suite 405 Knightciale, North Carolina Site Photographs
Somerset, NJ 08873
21 February 2012

I j� `j`j.�•. i I �.� ' i � 1
44
pe
I!
�. iv 2. _ /
a' ^' V i" L 1 t � y j"�+� `;'f»(1� -f 1.4 t'i. ""'"f'�p y�, k� ! r'�� - t•
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y t ylr ` q'� 5 .. ' �rR, - r �1 �r�,`i7af„✓ r r/}�'� �% •4� ,� e� 4''�, �\\`
r�� .. -.��� lt'x F _raC�ti}u4A'�. '�'�'" �4 �•e� 'i t'-�'-'��.��Ai'.'�:��,:.

Laboratory Reports

P R I S M I FullService Analytical &
Environmental Solutions
F�ABORATORIES, INC
AMEC Env. & Infrastructure Inc (tree)
David Treadway
7347-E West Friendly Avenue
Greensboro, NC 27410
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 1287
Project: Sir Walter Gun Club
Lab Submittal Date: 02/27/2012
Prism Work Order: 2020605
Case Narrative
03/06/2012
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 10

i��I `- ORgTOR1E$ INCI Full -Service Analytical & Sample Receipt Summary
�s J environmental Solutions 03/06/2012
P LAB
Prism Work Order: 2020605
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
WP-1
2020605-01
Solid
02/21/12
02/27/12
WP-3
2020605-02
Solid
02/21/12
02/27/12
WP-2A
2020605-03
Solid
02/22/12
02/27/12
WP-4A
2020605-04
Solid
02/22/12
02/27/12
Samples received in good condition at 4.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 2 of 10

&KIR1 Full Service Analytical &
Environmental Solutions
v7L 80RATORIES. INC.
Summary of Detections
03/06/2012
Prism Work Order: 2020605
Prism ID
Client ID
Parameter
Method
Result
Units
2020605-01
WP-1
Arsenic
*6010C
1.5
mg/kg dry
2020605-01
WP-1
Copper
*601 OC
0.99
mg/kg dry
2020605-01
WP-1
Lead
*6010C
14
mg/kg dry
2020605-02
WP-3
Arsenic
*601 OC
2.1
mg/kg dry
2020605-02
WP-3
Copper
*601 OC
0.93
mg/kg dry
2020605-02
WP-3
Lead
*6010C
6.3
mg/kg dry
2020605-03
WP-2A
Arsenic
*6010C
1.6
mg/kg dry
2020605-03
WP-2A
Copper
*6010C
1.3
mg/kg dry
2020605-03
WP-2A
Lead
*6010C
8.3
mg/kg dry
2020605-04
WP-4A
Arsenic
*6010C
1.5
mg/kg dry
2020605-04
WP-4A
Copper
*601 OC
1.2
mg/kg dry
2020605-04
WP-4A
Lead
*601 OC
6.6
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 3 of 10

ei Full -Service Analytical R
V I Environmental Solutions
_. �LA00RATORIE$ ING
Laboratory Report
03/06/2012
AMEC Env. & Infrastructure Inc (Gree)
Attn: David Treadway
7347-E West Friendly Avenue
Greensboro, NC 27410
Client Sample ID: WP-1
Prism Sample ID: 2020605-01
Prism Work Order: 2020605
Time Collected: 02/21/12 17:45
Time Submitted: 02/27/12 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Project: Sir Walter Gun Club
Sample Matrix: Solid
General Chemistry Parameters
% Solids
84.0
% by
0.100
0.100
1
*SM2540 G
2/28/12
14:30
JAB
P2130549
Weight
Total Metals
Antimony
BRL
mg/kg dry
0.23
0.042
1
*6010C
2/29/12
2:27
BGM
P260541
Arsenic
1.5
mg/kg dry
0.29
0.066
1
*6010C
2/29112
2:27
BGM
P280541
Copper
0.99
mg/kg dry
0.59
0.25
1
*6010C
2/29/12
2:27
BGM
P2130541
Lead
14
mg/kg dry
0.29
0.072
1
*6010C
2129/12
2:27
BGM
P2130541
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 10

LA 11101, Full -Service Analytical &
R I S, Y � I Environmental Solutions
07"LABORATORIE6 INC.
Laboratory Report
03/06/2012
AMEC Env. & Infrastructure Inc (Gree)
Attn: David Treadway
7347-E West Friendly Avenue
Greensboro, NC 27410
Client Sample ID: WP-3
Prism Sample ID: 2020605-02
Prism Work Order: 2020605
Time Collected: 02/21/12 17:55
Time Submitted: 02/27/12 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Project: Sir Walter Gun Club
Sample Matrix: Solid
General Chemistry Parameters
% Solids
83.9
% by
0.100
0.100
1
*SM2540 G
2/28/12 14:30
JAB
P260549
Weight
Total Metals
Antimony
BRL
mg/kg dry
0.23
0.043
1
*6010C
2/29/12 2:35
BGM
P260541
Arsenic
2.1
mg/kg dry
0.29
0.066
1
*6010C
2/29112 2:35
BGM
P2B0541
Copper
0.93
mg/kg dry
0.59
0.26
1
*6010C
2/29/12 2:35
BGM
P2B0541
Lead
6.3
mg/kg dry
0.29
0.072
1
*6010C
2/29/12 2:35
BGM
P2130541
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 10

'El I `- Service Analytical &
�� J Environmental Solutions
�LABORATORIE$ INC.
Laboratory Report
03/06/2012
AMEC Env. & Infrastructure Inc (Gree)
Attn: David Treadway
7347-E West Friendly Avenue
Greensboro, NC 27410
Client Sample ID: WP-2A
Prism Sample ID: 2020605-03
Prism Work Order: 2020605
Time Collected: 02/22/12 08:35
Time Submitted: 02/27/12 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Project: Sir Walter Gun Club
Sample Matrix: Solid
% Solids
83.0
% by
0.100
0.100
1
*SM2540 G
2128/12 14:30
JAB
P2B0549
Weight
Total Metals
Antimony
BRL
mg/kg dry
0.24
0.043
1
*6010C
2/29/12 2:42
BGM
P260541
Arsenic
1.6
mg/kg dry
0.30
0.067
1
*6010C
2/29112 2:42
BGM
P2130541
Copper
1.3
mg/kg dry
0.60
0.26
1
*6010C
2/29/12 2:42
BGM
P2130541
Lead
8.3
mg/kg dry
0.30
0.074
1
*6010C
2/29/12 2:42
BGM
P2130541
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 10

Arou
n Full -Service Analytical S
R' S Environmental Solutions
_. UV"-so—ORIE o.a
Laboratory Report
03/06/2012
AMEC Env. & Infrastructure Inc (tree) Project: Sir Walter Gun Club Client Sample ID: WP-4A
Attn: David Treadway Prism Sample ID: 2020605-04
7347-E West Friendly Avenue Prism Work Order: 2020605
Greensboro, NC 27410 Sample Matrix: Solid Time Collected: 02/22/12 08:40
Time Submitted: 02/27/12 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
84.8
% by
0.100
0.100
1
*SM2540 G
2/28/12 14:30
JAB
P2130549
Weight
Total Metals
Antimony
BRL
mg/kg dry
0.24
0.043
1
*6010C
2/29/12 2:50
BGM
1`260541
Arsenic
1.5
mg/kg dry
0.30
0.067
1
*6010C
2129/12 2:50
BGM
P2130541
Copper
1.2
mg/kg dry
0.59
0.26
1
*6010C
2/29/12 2:50
BGM
P2130541
Lead
6.6
mg/kg dry
0.30
0.073
1
*6010C
2/29112 2:50
BGM
P2130541
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 10

&R'F-,
IIFull-Service Analytical R
Environmental Solutions
! IP:BORATORiFS, ING
AMEC Env. & Infrastructure Inc (Gree) Project: Sir Walter Gun Club
Attn: David Treadway
7347-E West Friendly Avenue
Greensboro, NC 27410
Total Metals - Quality Control
Level II QC Report
3/6/12
Prism Work Order: 2020605
Time Submitted: 2/27/2012 4:00:OOPM
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P2BO541 - 3050B
Blank (P2130541-131-K1)
Prepared: _0_2_/28/12 Analyzed: 02/29/12
Antimony
BRL
0.20
mg/kg wet
Arsenic
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
gH
LCS (P2B0541-BS1)
Prepared: 02/28/12 Analyzed: 02/29/12
Antimony
21.6
0.20
mg/kg wet
24.75 87 80-120
Arsenic
22.5
0.25
mg/kg wet
24.75 91 80-120
Copper
23.6
0.50
mg/kg wet
24.75 95 80-120
Lead
21.8
0.25
mg/kg wet
24.75 88 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 8 of 10

AAR
�`. �LABORANRIE$ INC I S M I Full -Service Analytical &
Environmental Solutions
Level If QC Report
3/6/12
AMEC Env. & Infrastructure Inc (Gree) Project: Sir Walter Gun Club
Attn: David Treadway
7347-E West Friendly Avenue
Greensboro, NC 27410
General Chemistry Parameters - Quality Control
Prism Work Order: 2020605
Time Submitted: 2/27/2012 4:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P2130549 - NO PREP
Blank (P2130549-BLK1) Prepared &Analyzed: 02/28/12 _
% Solids 100 0.100 % by Weight
Sample Extraction Data
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
2020605-01
P2B0541
2.03 g
50 mL
02/28/12 7:40
2020605-02
P2B0541
2.03 g
50 mL
02/28/12 7:40
2020605-03
P2B0541
2.02 g
50 mL
02/28/12 7:40
2020605-04
P2130541
1.99 g
50 mL
02/28/12 7:40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 10

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�iPRISM
'U180RATORIES, kNG
Full -Service Analytical &
Environmental Solutions
AMEC Env. & Infrastructure Inc (Gree)
David Treadway
7347-E West Friendly Avenue
Greensboro, NC 27410
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
VA Certification No. 1287
Project: Sir Walter Gun Club
Lab Submittal Date: 03/07/2012
Prism Work Order: 2030185
Case Narrative
03/13/2012
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Data Qualifiers Key Reference:
1�; �'_ a - - &. I —
Reviewed By
HT Sample received and analyzed outside of the hold time.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 8

�} I S I Full -Service Analytical Environmental Solutions
W"BOBATOBIES. INC
Sample Receipt Summary
03/13/2012
Prism Work Order: 2030185
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
WP-2 2030185-01 Solid 02/21/12 03/07/12
WP-4 2030185-02 Solid 02/21/12 03/07/12
Samples received in good condition at 1.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of

IB ISM Environmental
Analytical
J Environmental Solutions
LABORATORIES, ING
Summary of Detections
03/13/2012
Prism Work Order: 2030185
Prism ID
Client ID
Parameter
Method
Result
Units
2030185-01
WP-2
Arsenic
'6010C
2.0
mg/kg dry
2030185-01
WP-2
Copper
*6010C
1.0
mg/kg dry
2030185-01
WP-2
Lead
'6010C
7.2
mg/kg dry
2030185-02
WP-4
Arsenic
'6010C
2.9
mg/kg dry
2030185-02
WP-4
Copper
`6010C
2.0
mg/kg dry
2030185-02
WP-4
Lead
'6010C
22
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 8

F
® I `- I Fun -Service Analytical 8
n J Environmental Solutions
�WRORATORIE6, INC.
Laboratory Report
03/13/2012
AMEC Env. & Infrastructure Inc (Gree)
Attn: David Treadway
7347-E West Friendly Avenue
Greensboro, NC 27410
Client Sample ID: WP-2
Prism Sample ID: 2030185-01
Prism Work Order: 2030185
Time Collected: 02/21/12 17:50
Time Submitted: 03/07/12 14:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Project: Sir Walter Gun Club
Sample Matrix: Solid
General Chemistry Parameters
Solids
84.7 HT
% by
0.100
0.100
1
*SM2540 G
3/9112 15:00
JAB
P2C0197
Weight
Total Metals
Antimony
BRL
mg/kg dry
0.24
0.043
1
*6010C
3/9/12 23:07
BGM
P2C0184
Arsenic
2.0
mg/kg dry
0.30
0.067
1
*6010C
319112 23:07
BGM
P2C0184
Copper
1.0
mg/kg dry
0.60
0.26
1
*6010C
3/9/12 23:07
BGM
P2C0184
Lead
7.2
mg/kg dry
0.30
0.074
1
*6010C
319112 23:07
BGM
P2C0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 8

�FD
I` -Full -Service Analytical &
JEnvironmental Solutions
ABORATORIES INC
Laboratory Report
03/13/2012
AMEC Env. & Infrastructure Inc (Gree) Project: Sir Walter Gun Club Client Sample ID: WP-4
Attn: David Treadway Prism Sample ID: 2030185-02
7347-E West Friendly Avenue Prism Work Order: 2030185
Greensboro, NC 27410 Sample Matrix: Solid Time Collected: 02/21/12 18:00
Time Submitted: 03/07/12 14:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
83.9 HT
% by
0.100
0.100
1
*SM2540 G
3/9/12 15:00
JAB
P2C0197
Weight
Total Metals
Antimony
BRL
mg/kg dry
0.24
0.044
1
*6010C
3/9/12 23:14
BGM
P2C0184
Arsenic
2.9
mg/kg dry
0.30
0.068
1
*6010C
3/9/12 23:14
BGM
P2C0184
Copper
2.0
mg/kg dry
0.60
0.26
1
*6010C
3/9112 23:14
BGM
P2C0184
Lead
22
mg/kg dry
0.30
0.074
1
*6010C
319/12 23:14
BGM
P2C0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 5 of 8

Full -Service Analytical &
I SM I Environmental Solutions
vi-RATORIZa INC.
AMEC Env. & Infrastructure Inc (Gree) Project: Sir Walter Gun Club
Attn: David Treadway
7347-E West Friendly Avenue
Greensboro, NC 27410
Total Metals - Quality Control
Level II QC Report
3/13/12
Prism Work Order: 2030185
Time Submitted: 3/7/2012 2:15:00PM
Reporting
Spike Source
%REC RPD
Analyte
Result
Limit
Units
Level Result %REC
Limits RPD Limit Notes
Batch P2C0184 - 3050B
Blank (P2C0184-BLK1)
Prepared & Analyzed: 03/09/12
Antimony
BRL
0.20
mg/kg wet
Arsenic
BRL
0.26
mg/kg wet
Copper
BRL
0.51
mg/kg wet
Lead
BRL
0.26
mg/kg wet
LCS (P2C0184-BS1)
Prepared &Analyzed: 03/09/12
Antimony
22.5
0.20
mg/kg wet
24.51 92
80-120
Arsenic
22.3
0.25
mg/kg wet
24.51 91
80-120
Copper
24.0
0.49
mg/kg wet
24.51 98
80-120
Lead
21.7
0.25
mg/kg wet
24.51 89
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 8

AFull-Service
I51�&r',L
'v u IS n � Analytical s
Environmental Solutions
ABORATORIES, INC
Level II QC Report
3/13/12
AMEC Env. & Infrastructure Inc (Gree) Project: Sir Walter Gun Club
Attn: David Treadway
7347-E West Friendly Avenue
Greensboro, NC 27410
General Chemistry Parameters - Quality Control
Prism Work Order: 2030185
Time Submitted: 3/7/2012 2:15:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOM - NO PREP
Blank (P2C0197-BLK1) Prepared & Analyzed: 03/09/12
% Solids 100 0.100 % by Weight
Sample Extraction Data
Prep Method: 3050B
Lab Number Batch Initial Final Date/Time
2030185-01 P2C0184 1.98 g 50 mL 03/09/12 9:30
2030185-02 P2C0184 1.98 g 50 mL 03/09/12 9:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 8

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