23068_Sir Walter Gun Club_BAR_20201221

619
PREPARED FOR:
Merritt - MW1, LLC
2066 Lord Baltimore Drive
Baltimore, Maryland 21244-2501
S&ME, Inc.
3201 Spring Forest Road
Raleigh, NC 27616
Corporate Registration for Licensing of NC Geologists No. C-145
NC Engineering Firm No. F-0176
December 11, 2020
(Revised December 21, 2020)

=0
December 21, 2020
North Carolina Department of Environmental Quality
Division of Waste Management, Brownfields Program
217 West Jones Street
Raleigh, North Carolina 27605
Attention: Mr. Brad Atkinson
Brownfields Project Manager
Reference: Additional Soil Assessment Report - Revised
Sir Walter Gun Club
Hinton Oaks Blvd, Knightdale, North Carolina
NC Brownfields ID No. 23068-19-092
S&ME Project No. 4305-19-213
Dear Mr. Atkinson:
via email: [e-mail]
S&ME, Inc. (S&ME) is pleased to submit this Additional Soil Assessment Report for the proposed Merritt
Properties development in Knightdale, North Carolina. The work was completed in accordance with S&ME's Work
Plan for Environmental Assessment, dated November 10, 2020 and approved by the North Carolina Brownfields
Program (NCBP). This report has been revised from the previously submitted version to incorporate results from
additional laboratory analysis of samples using the Toxicity Characteristic Leaching Procedure (TCLP) method.
The purpose of this additional limited soil assessment was to provide additional information on the extent
(quantity) of soil contamination at the subject property to help prepare plans for the safe redevelopment of the
site, including future management of soil; preparing an EMP for site development; and preparing a Brownfields
Agreement between DEQ and Merritt. This report presents our understanding of the project, description of our
field activities, discussion of environmental conditions, relative to applicable North Carolina Department of
Environmental Quality (DEQ) regulatory standards, and our conclusions and recommendations.
If you have any questions about the information included in this report, please contact the undersigned.
Sincerely,
S&ME, Inc.
Bryan S.
Environmental Professional
[e-mail]
M: 336.816.3605
Enclosure
c: 5 �—/�*
Samuel P. Watts, PG
Senior Project Manager
[e-mail]
M: 919.801.4920
Cc: Nathan Robb ([e-mail]) — Merritt Properties
S&ME, Inc. 13201 Spring Forest Road I Raleigh, NC 276161 p 919.872.2660 1 www.smeinc.com

Additional Soil Assessment Report - Revised i
Sir Walter Gun Club_
NC Brownfields ID No. 23068-19-092
S&ME Project No. 4305-19-213
CERTIFICATION
Additional Soil Assessment Report — Revised
Sir Walter Gun Club
Hinton Oaks Blvd, Knightdale, North Carolina
NC Brownfields ID No. 23068-19-092
S&ME Project No. 4305-19-213
I, Samuel P. Watts , a Licensed Geologist for S&ME, Inc. , do hereby certify this report was prepared by me or
under my direct supervision.,i,a�ia,._.
Samuel P. Watts, P.G.
Senior Geologist
NC Licensed Geologist No. 1806
S&ME, Inc. is licensed to practice engineering in North Carolina. The firm's license number is C-145.
S&ME, Inc. is licensed to practice geology in North Carolina. The firm's license number is F-0176.
December 11, 2020 (Revised December 21, 2020)

Additional Soil Assessment Report - Revised
Sir Walter Gun Club
NC Brownfields ID No. 23068-19-092 I I I
S&ME Project No. 4305-19-213
Table of Contents
1.0 Introduction.......................................................................................................................1
2.0 Previous Assessment Activities.....................................................................................2
3.0 Additional Soil Assessment Activities.........................................................................3
3.1 Project Management, Health and Safety Plan, and Coordination...........................................3
3.2 Soil Sampling.................................................................................................................................. 4
3.3 Quality Assurance/Quality Control.............................................................................................4
4.0 Laboratory Testing............................................................................................................5
4.1 Soil Sample Results........................................................................................................................5
4.2 Quality Assurance/Quality Control Results...............................................................................5
4.3 Toxicity Characteristic Leaching Procedure (TCLP).................................................................5
5.0 Deviations from Approved Work Plan.........................................................................6
6.0 Conclusions and Recommendations.............................................................................6
List of Figures
Figure 1- Site Vicinity Map
Figure 2 - Sample Location Map
List of Tables
Table 1- Sample Location Coordinates
Table 2 - Summary of Analytical Results - June 2020 Soil Assessment
Table 3 - Summary of Analytical Results - November 2020 Soil Assessment
Table 4 - Summary of TCLP Results - November 2020 Soil Assessment
Appendices
Appendix I - Figures
Appendix II - Tables
Appendix III - Preliminary Grading Plans
Appendix IV - Laboratory Analytical Report and Chain -of -Custody Record
December 11, 2020 (Revised December 21, 2020)

Additional Soil Assessment Report - Revised
Sir Walter Gun Club
NC Brownfields ID No. 23068-19-092 111
S&ME Project No. 4305-19-213 E
1.0 Introduction
S&ME, Inc. (S&ME) has prepared this Additional Soil Assessment Report for the Sir Walter Gun Club (NC
Brownfields ID No. 23068-19-092) located northeast of the Hampton Inn & Suites at 405 Hinton Oaks Blvd. in
Knightdale, Wake County, North Carolina. (Hereafter referred to as the Site or subject Site.) A Site Vicinity Map,
depicting the subject Site, is provided as Figure 1.
The subject property consists of two parcels totaling approximately 45.50 acres. Parcel 1 is 5.35-acres, is identified
by Wake Co PIN 1744479093, and is located northeast of the Hampton Inn & Suites at 405 Hinton Oaks Blvd.
Knightdale, NC 27545. Parcel 2 is 40.15-acres, is identified by Wake Co PIN 1744566986 and is located north of
Target at 1000 Shoppes at Midway Dr, Knightdale, NC 27545. By way of recent correspondence with we
understand from the prospective developer (PD), Merritt - MW1, LLC, that a portion of Parcel 2 will be excluded
from the development. The excluded portion of Parcel 2 is referred to as Lot 3A and is identified on Figure 2.
The Site is listed as a State Inactive Hazardous Waste Site (SHWS) and is identified by the Inactive Hazardous Sites
Branch (IHSB) ID no. NONCD0000019. The site is currently wooded, undeveloped, and unoccupied. Three
dilapidated structures, soil berms, and soil stockpiles containing clay targets debris are still present on the site.
The structures, soil berms, and soil stockpiles were previously used as part of the former Sir Walter Gun Club,
which operated on a portion of the subject property from 1950-1988. Range facilities that were historically
operated by the Gun Club at the site consisted of two adjacent rifle ranges with nominal target distances of 100
yards and 200 yards; a 50-yard pistol range; and a combined skeet and trap field (refer to Figure 2). The rifle
ranges included earthen backstops (impact berms), which were approximately 10 feet high and appear to have
been constructed from soil obtained onsite. The skeet field was located immediately east of the 100-yard range,
from which it was separated by an earthen side berm approximately 80 feet long and 7 feet high. The pistol range,
which has been removed and covered by commercial development, was formerly located on a parcel immediately
south of the subject property, which was subdivided and sold during 2005.
The PD's proposed future development of the site will include five flex space buildings, along with associated
parking lots, access drives and stormwater ponds. Preliminary grading plans prepared by the PD are included in
Appendix III. Based on the plans, approximate finished floor elevations (FIFE) will be 288 feet (Building Al), 290
feet (Building A2), 296 feet (Building 131), 294 feet (Building 132), and 290 feet (Building 133). As shown on the
preliminary grading plans, the PD does not intend to develop the northeastern parcel (Lot 3A).
The overall objective of this additional soil assessment was to delineate areas of previously identified soil
contamination at the site to help prepare plans for the safe redevelopment of the site, including guiding future
management of soil; preparing an Environmental Management Plan (EMP) for site development; and preparing a
Brownfields Agreement between DEQ and the PD.
December 11, 2020 (Revised December 21, 2020)

Additional Soil Assessment Report - Revised
Sir Walter Gun Club
NC Brownfields ID No. 23068-19-092 I I I
S&ME Project No. 4305-19-213
2.0 Previous Assessment Activities
Prior to preparing the Work Plan for Environmental Assessment, dated June 6, 2020, S&ME reviewed the findings
of previous assessments, conducted at the subject site, and documented in by the following reports.
Memorandum — Sir Walter Gun Club, dated January 31, 1989, prepared by Stan Atwood, North Carolina
Department of Environmental and Natural Resources, Division of Waste Management, Superfund Branch
Removal of Lead Contaminants from the Soil on the Silver Plantations, dated March 10, 1992, prepared by
Paragon Environmental Group
Reconnaissance Investigation Results, Former Sir Walter Gun Club Site, Knightdale North Carolina, dated
February 14, 2013, prepared by AMEC Environment & Infrastructure, Inc.
Findings of Limited Soil Assessment - Abandoned Rifle Range Berms, dated November 18, 2010, prepared by
S&ME, Inc.
♦ Additional Soil Testing - Abandoned Rifle Range Berms, dated January 4, 2011, prepared by S&ME, Inc.
♦ Phase I Environmental Site Assessment, Multiple Parcels- Intersection of Hinton Oaks Blvd. and Knightdale Blvd.,
dated November 1, 2019, prepared by S&ME, Inc.
Sediment, Surface Water, and Groundwater Assessment, dated February 26, 2020, prepared by S&ME, Inc.
Limited Soil Assessment, dated August 4, 2020, prepared by S&ME, Inc.
The 1989 Atwood Memorandum documented high levels of lead in each of the three berms, and polyaromatic
hydrocarbons (PAHs) in the berms at the pistol range and the 100-yard rifle range.
The 1991 Paragon report documented limited excavation, removal, and screening of soils from the impact berms
by Paragon during August and September of 1991, on behalf of the Gun Club. Paragon reported removing soil
from the front (impact) face of each of the three impact berms (100-yard and 200-yard rifle ranges and the 50-
yard pistol range), which was processed through a mobile, vibratory screening plant. No field observations or
laboratory analytical results were provided in Paragon's report.
Results reported by the 2013 AMEC assessment indicated soil downgradient of the rifle range was not impacted.
Through sieve analysis, AMEC determined that shot concentration in the soil was estimated to be 770 to 3,500
milligrams per kilogram (mg/kg). But AMEC did not perform laboratory analysis of the soil samples for total
metals as part of their assessment.
The 2010 and 2011 reports by S&ME documented soil sampling and laboratory analysis of samples from the 100-
yard and 200-yard rifle range impact berms for total lead. Selected samples were also analyzed for total arsenic,
PAHs, and leachable lead using the Toxicity Characteristic Leaching Procedure (TCLP). Within the 100-yard impact
berm, total lead concentrations ranging from 35 to 5,100 mg/kg were detected in the soil, and within the 200-yard
impact berm total lead ranged from 100 to 8,200 mg/kg. Contamination in the soil berms exceeding the NCDEQ
Industrial/Commercial Health -Based Preliminary Soil Remediation Goal (PSRG) for lead of 800 mg/kg; the
Residential Health -Based PSRG of 400 mg/kg; and the Protection of Ground Water PSRG of 270 mg/kg were
reported at depths of up to 30 inches below grade. Samples from the 100-yard berm and the 200-tard berm were
also analyzed for Toxicity Characteristic Leaching Procedure (TCLP) for lead, and were found to exceed the federal
regulatory threshold of 5 milligrams per liter (mg/L) for disposal of solid waste as non -hazardous (40 CFR §
261.24). Traces of arsenic and PAH's were detected in the 100-yard berm. Arsenic and PAHs were not detected in
the soils collected from the 200-yard berm.
December 11, 2020 (Revised December 21, 2020)

Additional Soil Assessment Report - Revised
Sir Walter Gun Club
NC Brownfields ID No. 23068-19-092
S&ME Project No. 4305-19-213
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The February 2020 S&ME report documented environmental assessment of sediment, surface water, and
groundwater contamination at the subject property performed in November 2019. Based on the findings of
S&ME's November 2019 assessment, the sediment, surface water, and groundwater do not pose an unacceptable
risk to human health or the environment and should not hinder the redevelopment of the subject property.
The SVOC diethylphtalate was detected at an estimated concentration less than its respective 2L
Standard in the samples collected from MW-1 and MW-2. Lead and VOCs were not detected in any
of the groundwater samples submitted for laboratory analysis.
Several SVOCs were detected at estimated concentrations in one or more of the sediment samples
submitted for analysis at concentrations less than their respective PSRGs. Lead was also detected in
each of the sediment samples submitted for analysis at concentrations less than its respective PSRG.
VOCs were not detected in any of the sediment samples submitted for laboratory analysis.
The SVOC benzoic acid, which does not have a 2B Standard, was detected at an estimated
concentration in the samples collected from SW-2 and SW-3. Lead and VOCs were not detected in
any of the surface water samples submitted for laboratory analysis.
The August 2020 S&ME report documented the limited soil assessment at the subject property performed in June
2020. Results of the assessment activities performed at the site in June 2020, indicated the following:
Soil contaminated with lead and SVOCs was found at the site with contaminant concentrations
exceeding the Residential PSRGs. Based on review of prior assessment and the findings of this
assessment, soil with contamination exceeding PSRGs appears to be confined to a few specific areas
of the site, related to the prior use as a gun range. Contaminated soil is confined primarily to the
southern part of the site in the areas of the former impact berms, the low house and the trap house,
as indicated by detections of constituents greater than PSRGs in soil collected from hand auger
borings HA-16, HA-20, HA-27 and HA-28.
Contaminated soil also appears to be confined primarily to the surface. In most instances where
laboratory analysis detected constituents greater than the reporting limit in the 0 to 6-inch interval,
subsequent analysis of soil from the same boring location, from the 12 to 18 inches interval did not
detect constituents at concentrations greater than the laboratory reporting limit. Sample location
HA-27 was the only location where sample analysis of a sample from the 12 to 18-inch interval
detected a constituent at a concentration greater than its respective PSRG (benzo(a)pyrene at an
estimated concentration of 0.17 mg/kg).
3.0 Additional Soil Assessment Activities
3.1 Project Management, Health and Safety Plan, and Coordination
In November 2020 S&ME conducted an additional soil assessment in accordance with S&ME's Work Plan for
Environmental Assessment, dated November 10, 2020 and approved by the North Carolina Brownfields Program
(NCBP). Prior to mobilizing to the site to conduct the proposed sampling, S&ME performed the following:
December 11, 2020 (Revised December 21, 2020)

Additional Soil Assessment Report - Revised
Sir Walter Gun Club
NC Brownfields ID No. 23068-19-092
S&ME Project No. 4305-19-213
=0
Updated a previously prepared a health and safety plan to comply with currently proposed site
activities, in accordance with 29 CFR 1910.120 as required by the Occupational Safety and Health
Administration (OSHA);
Contacted NC 811, prior to mobilizing to the site, to locate public underground utilities at the
property boundaries.
Coordinated with a North Carolina certified laboratory for the proposed soil analyses with Level 2
Quality Assurance/Quality Control (QA/QC) data package.
3.2 Soil Sampling
S&ME mobilized to the site on November 17, 2020 to perform the soil sampling. Soil samples were collected
from 21 locations identified as HA-31 through HA-51 as depicted on Figure 2. Soil samples were collected using
a stainless -steel hand auger that was decontaminated before each sample was collected. At each location, S&ME
collected a soil sample from the ground surface to approximately six inches below the ground surface (bgs) and
from approximately 12 to 18 inches bgs.
After collection, the samples were placed in an ice -filled cooler and shipped under standard chain -of -custody
protocol to ENCO Laboratories for analysis of volatile organic compounds (VOCs) by EPA Method 8260B, semi -
volatile organic compounds (SVOCs) by EPA Method 8270E, and lead by EPA Method 6010D.
The samples collected from the 0 to 6-inch interval from borings HA-31 through HA-43 were submitted for
immediate analysis. The samples collected from the 12 to 18-inch interval from each boring were submitted to
the laboratory on hold, only to be analyzed if the results of the 0 to 6-inch interval indicated the presence of
contamination. Additionally, samples collected from the 0 to 6-inch interval and 12 to 18-inch interval from the
step -out delineation borings HA-44 through HA-51 were submitted to the laboratory on hold, only to be analyzed
if the corresponding interior borings indicated the presence of contamination. Coordinates of the hand auger soil
sample locations were logged with a TrimbleS GPS unit and are included in Table 1.
3.3 Quality Assurance/Quality Control
During the previous soil assessment in June 2020, S&ME collected a background soil sample in an area outside of
any previously developed areas of the site and outside the influence of the former Sir Walter Gun Club rifle ranges
and skeet and trap fields to document background VOCs, SVOCs, and lead concentrations.
To evaluate the precision of the analytical methods used by the laboratory, S&ME collected an additional sample
for Quality Assurance/Quality Control (QA/QC) purposes, consisting of a split or duplicate soil sample. The
duplicate sample, DUP-11-17-20, was a duplicate of the record sample HA-42.
To evaluate the possibility of contamination introduced to the samples through the sample equipment, an
equipment blank sample (Equipment Blank) was collected by pouring laboratory provided deionized water over
the bucket of the hand auger directly into laboratory supplied containers. The equipment blank sample was
submitted for the same constituents as the record samples. Additionally, to evaluate if the handling and transport
of the samples was contributing to contamination in the record sample, a trip blank sample (Trip Blank) was
submitted for analysis of VOCs by EPA Method 8260B.
December 11, 2020 (Revised December 21, 2020) 4

Additional Soil Assessment Report - Revised
Sir Walter Gun Club
NC Brownfields ID No. 23068-19-092 111
S&ME Project No. 4305-19-213 E
4.0 Laboratory Testing
4.1 Soil Sample Results
The laboratory analytical results of the soil samples indicated several VOCs and SVOCs were detected in one or
more of the samples submitted for analysis. Lead was also detected in each of the soil samples submitted for
analysis. Sample results were compared to the NCDEQ Division of Waste Management PSRGs. Tables 2 and 3
present a summary of the analytical results identified at the sample locations. A copy of the laboratory analytical
report and chain -of -custody record, for the November 2020 samples is provided in Appendix IV.
The detected concentrations of VOCs did not exceed their respective PSRGs in any of the samples submitted for
analysis.
Most of the detected SVOCs were polycyclic aromatic hydrocarbons (PAHs). One or more of the SVOCs
benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, and indeno(1,2,3-cd)pyrene
were detected at concentrations greater than their respective PSRGs in the 0 to 6-inch bgs sample interval from
HA-35, HA-36, HA-37, and HA-38. S&ME directed the laboratory to analyze the 12 to 18-inch interval samples for
these locations, which indicated no constituents in excess of their respective PSRGs, with the exception of
benzo(a)pyrene in HA-37 and dibenzo(a,h)anthracene in HA-37 and HA-38 at estimated concentrations.
Lead was detected at a concentration greater than its respective PSRG in the 0 to 6-inch interval sample from HA-
31, HA-42, HA-44, HA-46, and HA-51. S&ME directed the laboratory to analyze the 12 to 18-inch interval samples
for these locations, which indicated lead was not detected in excess of its PSRG.
4.2 Quality Assurance/Quality Control Results
Analysis of the background soil sample (BG), collected during the previous soil assessment in June 2020, detected
4-isopropyltoluene in the 12 to 18-inch bgs interval at a concentration less than its respective PSRG. No other
VOCs or SVOCs were detected in the BG samples. Lead was detected at in the background soil samples at 9.51
mg/kg and 6.69 mg/kg from the 0 to 6-inch and 12 to 18-inch intervals, respectively. These background
concentrations are less than the PSRG of 250 mg/kg for lead. This indicates some lead, at low concentrations, is
naturally present in soils at the subject site.
Analytical results of the duplicate soil sample indicated similar concentrations of constituents from the record
sample where the average relative percent difference (RPD) was 26.5%.
None of the targeted constituents were detected above their respective method detection limits in the equipment
blank sample or trip blank sample. This demonstrates the sample equipment used to collect the soil samples and
the sample handling and transportation did not contribute to contamination of the samples.
4.3 Toxicity Characteristic Leaching Procedure (TCLP)
To further evaluate the extent of lead contaminated soil at select locations, S&ME communicated with the
laboratory to analyze select samples using the toxicity characteristic leaching procedure (TCLP) method. Samples
analyzed using the TCLP method were the 0 to 6-inch intervals of soil samples where lead was previously detected
December 11, 2020 (Revised December 21, 2020)

Additional Soil Assessment Report - Revised
Sir Walter Gun Club
NC Brownfields ID No. 23068-19-092
S&ME Project No. 4305-19-213
=0
at concentrations greater than the NC DEQ Preliminary Soil Remediation Goal (PSRG) of 250 mg/kg for lead
(samples HA-31, HA-40, HA-42, HA-44, HA-46, and HA-51). Results of the TCLP analysis are summarized on Table
4 and a copy of the laboratory analytical report and chain -of -custody record for the TCLP samples is provided in
Appendix IV. Although the soils at the Sir Walter Gun Club are not considered waste subject to RCRA cleanup, 5
mg/L lead is the RCRA Regulatory Concentration for Characteristics of a Hazardous Waste, and soils with the TCLP
>5mg/L may require special handling or treatment as part of the Brownfields redevelopment. Results of the TCLP
analysis indicated that lead was detected at concentrations greater than 5 mg/L in the soil samples from HA-31
and HA-46. TCLP results from HA-40, HA-42, HA-44 and HA-51 were all less than 5mg/L. Contaminated soils
delineated at the site are depicted on Figure 2.
5.0 Deviations from Approved Work Plan
No deviations from the approved Work Plan occurred during the additional soil assessment performed at the
subject site, except for the following:
S&ME communicated with the laboratory to analyze select samples using the toxicity characteristic
leaching procedure (TCLP) method to further evaluate the lead contaminated soil at select locations.
6.0 Conclusions and Recommendations
S&ME has completed a Limited Soil Assessment Report for at the Sir Walter Gun Club Brownfields Site in
Knightdale, North Carolina. The assessment was completed in accordance with S&ME's Work Plan for
Environmental Assessment, dated November 10, 2020 and approved by the NCBP. Prior environmental
assessment activities at the subject site focused on the impact berms, groundwater, surface water, and sediment.
The overall objective of this additional limited soil assessment was to provide additional information on the extent
(quantity) of soil contamination at the subject property to help prepare plans for the safe redevelopment of the
site, including future management of soil; preparing an EMP for site development; and preparing a Brownfields
Agreement between DEQ and Merritt. Results of the assessment activities performed at the site in June 2020,
indicate the following:
Soil contaminated with lead and SVOCs was found at the site with contaminant concentrations
exceeding the PSRGs. Based on review of prior assessment and the findings of this assessment, soil
with contamination exceeding PSRGs appears to be confined to a few specific areas of the site, related
to the prior use as a gun range. Contaminated soil is confined primarily to the southern part of the
site in the areas of the former impact berms, the low house and the trap house.
Contaminated soil also appears to be confined primarily to the surface. In most instances where
laboratory analysis detected constituents greater than the reporting limit in the 0 to 6-inch interval,
subsequent analysis of soil from the same boring location, from the 12 to 18 inches interval did not
detect constituents at concentrations greater than the laboratory reporting limit.
Results of the TCLP analysis on select soil samples indicated that lead was detected above the RCRA
Regulatory Concentration for Characteristics of a Hazardous Waste of 5 mg/L in HA-31 and HA-46
and less than 5 mg/L HA-40, HA-42, HA-44 and HA-51. These TCLP results present a good show a
December 11, 2020 (Revised December 21, 2020)

Additional Soil Assessment Report - Revised
Sir Walter Gun Club
=0
NC Brownfields ID No. 23068-19-092 111
S&ME Project No. 4305-19-213 E
good correlation that soil with lead greater than 500 mg/kg will typically result in TCLP greater than
>5 mg/L, while soil with lead greater than 500 mg/kg will typically result in TCLP greater than >5
mg/L. Soil with lead concentrations greater than 500 mg/kg may require special handling or
treatment as part of the Brownfields redevelopment.
Topsoil and underlying shallow soils, contaminated with lead and SVOCs at concentrations greater
than PSRGs, have been delineated. These areas will be clearly marked prior to site development and
managed in a way to minimize mixing contaminated soil on -site with clean topsoil on -site. To
minimize future users of the site exposure to contaminated soil, the contaminated soil may be placed
at depths greater than one foot below design grade.
In the areas of topsoil/soil identified with constituents greater than PSRGs, we advise that surface
materials such as leaves, pine straw and root mat be removed from the near surface prior to site
grading, so that these materials are not present in quantities that will negatively impact the
geotechnical quality of the fill. A method of "blowing" or raking these near surface materials from the
ground surface prior to grading may be considered.
It may be necessary to excavate pits within proposed parking lot areas and use them as locations
where the blended contaminated soils can be placed at depth. After these materials have been
placed, clean on -site soils suitable for fill placement could be placed above them to design grade.
December 11, 2020 (Revised December 21, 2020)

Appendices

Appendix I - Figures

Appendix II - Tables

TABLE 1
Sample Location Coordinates
Sir Walter Gun Club
Knightdale, Wake County, North Carolina
Brownfields Project No. 23068-19-092
S&ME Project No. 4305-19-213
June 2020 Sample Locations
Sample ID
Northing
Easting
Latitude
Longitude
HA-1
747581.295
2145296.980
35.803094
-78.509993
HA-2
747581.295
2145596.980
35.803090
-78.508982
HA-3
747216.864
2144932.549
35.802098
-78.511228
HA-4
747281.295
2145296.980
35.802270
-78.509998
HA-5
747281.295
2145596.980
35.802266
-78.508987
HA-6
746981.295
2144996.980
35.801450
-78.511015
HA-7
746981.295
2145296.980
35.801445
-78.510003
HA-8
746981.295
2145596.980
35.801441
-78.508992
HA-9
746908.274
2145888.389
35.801237
-78.508010
HA-10
746833.582
2145986.725
35.801030
-78.507680
HA-11
746758.613
2145164.500
35.800836
-78.510454
HA-12
746681.295
2145596.980
35.800617
-78.508997
HA-13
746660.073
2145903.465
35.800555
-78.507963
HA-14
746736.499
2146126.246
35.800762
-78.507211
HA-15
746674.886
2146317.570
35.800590
-78.506567
HA-16
746595.387
2145266.912
35.800386
-78.510111
HA-17
746525.337
2145338.139
35.800192
-78.509872
HA-18
746525.717
2145753.325
35.800188
-78.508472
HA-19
746555.525
2145870.560
35.800268
-78.508076
HA-20
746595.218
2146157.014
35.800373
-78.507109
HA-21
746411.363
2145331.343
35.799879
-78.509897
HA-22
746430.839
2145527.137
35.799930
-78.509236
HA-23
746480.318
2145811.695
35.800062
-78.508276
HA-24
746492.380
2145921.076
35.800094
-78.507907
HA-25
746171.499
2145249.730
35.799221
-78.510176
HA-26
746338.341
2145639.934
35.799674
-78.508857
HA-27
746353.521
2145711.839
35.799715
-78.508615
HA-28
746408.977
2145821.423
35.799866
-78.508244
HA-29
1 746371.567
1 2145971.564
35.799761
1-78.507739
HA-30
746424.249
2146265.706
35.799902
-78.506746
November 2020 Sample Locations
Sample ID
Northing
Easting
Latitude
Longitude
HA-31
746637.636
2145232.821
35.800502
-78.510225
HA-32
746647.358
2145311.294
35.800528
-78.509961
HA-33
746548.747
2145277.266
35.800257
-78.510077
HA-34
746400.136
2145675.182
35.799844
-78.508738
HA-35
746426.525
2145758.516
35.799915
-78.508456
HA-36
746448.747
2145872.405
35.799975
-78.508072
HA-37
746383.469
2145877.266
35.799795
-78.508056
HA-38
746338.330
2145791.155
35.799672
-78.508347
HA-39
746300.136
2145710.599
35.799569
-78.508620
HA-40
746625.136
2146117.544
35.800456
-78.507242
HA-41
746641.108
2146202.960
35.800499
-78.506954
HA-42
746564.025
2146196.710
35.800287
-78.506976
HA-43
746552.914
2146114.071
35.800258
-78.507255
HA-44
746702.914
2146075.877
35.800670
-78.507381
HA-45
746515.414
2146283.516
35.800152
-78.506684
HA-46
746455.691
2146175.877
35.799990
-78.507048
HA-47
746494.580
2146053.655
35.800098
-78.507460
HA-48
746600.830
2146016.155
35.800390
-78.507584
HA-49
746235.553
2145680.044
35.799392
-78.508724
HA-50
746279.303
2145818.238
35.799510
-78.508257
HA-51
746310.553
2145927.960
35.799594
-78.507887
Notes:
Sample locations are in feet in the North Carolina State Plane Coordinate System (NAD83).
Latitude and longitude are reported in decimal degrees, measured with a Trimble GPS unit.
Hand auger borings were abandoned immediately after sample collection.
Tables for November 2020 Soil Assessment.xlsx

TABLE 2
Summary of Analytical Results - June 2020 Soil Assessment
Sir Walter Gun Club
Knightdale, Wake County, North Carolina
Brownfields Project No. 23068-19-092
S&ME Project No. 4305-19-213
Analytical Method
Volatile Organic Compounds by Method 8260D (mg/Kg)
Semi -Volatile Organic Compounds by EPA Method 8270E (mglKg)
Lead by EPA Method 6010D
(mg/Kg)
Analyte
d
q
C
d
'�
o
a.
°m
v
O
w
'v
°'
w
C
+
s
LL
v
w
'rJ
+
e
b
c
`>y
o
`�
w
0
`>y
v
_w
w
0
`�
s
wO
x
0
`>y
'o
`�
+
d
a
o
N
d
i
n
u+,
d
M
c
q
+
a,
Lead
Sample ID
Sample
Depth
(ft-bgs)
Date
Collected
HA-1
0-0.5
6/23/2020
<0.018
<0.00098
<0.0002
0.0067
<0.0012
<0.00030
<0.032
<0.043
<0.032
<0.037
<0.020
<0.053
<0.037
<0.17
<0.034
<0.030
<0.041
<0.033
<0.053
<0.030
<0.025
<0.043
4.87
HA-2
0-0.5
6/23/2020
0.033
<0.0011
<0.00024
<0.0011
<0.0014
<0.00035
<0.032
<0.044
<0.032
<0.038
<0.021
<0.054
<0.038
<0.17
<0.035
<0.031
<0.041
<0.033
<0.054
<0.031
<0.025
<0.044
8.78
HA-3
0-0.5
6/23/2020
0.079
1 <0.0011
<0.00023
I <0.0010
<0.0014
<0.00034
<0.032
<0.043
<0.032
<0.038
<0.020
<0.053
<0.038
<0.17
<0.034
<0.031
<0.041
I <0.033
<0.053
<0.031
<0.025
<0.043
4.41
HA-4
0-0.5
6/23/2020
0.084
<0.00079
<0.00016
<0.00074
<0.0010
<0.00024
<0.032
<0.045
<0.033
<0.039
<0.021
<0.055
<0.039
<0.18
<0.035
<0.032
<0.043
<0.034
<0.055
<0.032
<0.026
<0.045
6.15
HA-5
0-0.5
6/23/2020
<0.016
<0.00087
<0.00018
<0.00082
<0.0011
<0.00027
<0.031
<0.043
<0.031
<0.037
<0.020
<0.053
<0.037
<0.17
<0.034
<0.030
<0.040
<0.032
<0.053
<0.030
<0.025
<0.043
5.97
HA-6
0-0.5
6/23/2020
0.170
0.0039J
<0.00016
<0.00072
<0.00096
<0.00024
<0.032
<0.044
<0.032
<0.038
<0.021
<0.054
<0.038
<0.17
<0.035
<0.031
<0.041
<0.033
<0.054
<0.031
<0.025
<0.044
12.2
HA-7
0-0.5
6/23/2020
0.081
<0.0012
<0.00024
0.0072
<0.0015
<0.00036
<0.033
<0.044
<0.033
<0.038
<0.021
<0.055
<0.038
<0.17
<0.035
<0.031
<0.042
<0.034
<0.055
<0.031
<0.026
<0.044
9.26
HA-8
0-0.5
6/23/2020
<0.014
<0.00076
<0.00016
0.0065
1 <0.00095
I <0.00023
<0.031
I <0.042
<0.031
I <0.037
<0.020
<0.052
<0.037
<0.17
<0.033
<0.030
<0.040
<0.032
<0.052
<0.030
<0.025
<0.042
18.4
0-0.5
6/23/2020
<0.016
I <0.00090
<0.00019
<0.00084
<0.0011
<0.00028
<0.032
<0.044
<0.032
<0.038
<0.021
<0.054
<0.038
<0.17
<0.035
<0.031
<0.042
<0.034
<0.054
<0.031
<0.025
<0.044
236
HA-9
1.0-1.5
6/23/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
18.8
HA-10
0-0.5
6/23/2020
<0.016
<0.00088
<0.00018
<0.00083
<0.0011
<0.00027
<0.032
<0.043
<0.032
<0.037
<0.020
<0.053
<0.037
<0.17
<0.034
<0.031
<0.041
<0.033
<0.053
<0.031
<0.025
<0.043
32.6
HA-11
0-0.5
6/23/2020
<0.020
<0.0011
<0.00023
<0.0011
<0.0014
<0.00035
<0.031
<0.041
<0.031
<0.036
<0.020
<0.051
<0.036
<0.16
<0.033
<0.029
<0.039
<0.032
<0.051
<0.029
<0.024
<0.041
5.56
0-0.5
6/23/2020
0.013J
<0.00073
0.0045
<0.00068
<0.00091
<0.00022
I <0.033
<0.045
<0.033
<0.039
I <0.021
<0.055
<0.039
<0.18
<0.035
<0.032
<0.042
<0.034
<0.055
<0.032
<0.026
<0.045
13.4
HA-12
1.0-1.5
6/23/2020
<0.013
<0.00075
<0.00015
0.0076
<0.00094
<0.00023
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
4.69
0-0.5
6/23/2020
0.220
<0.00085
0.013
0.0073
<0.0011
<0.00026
<0.031
<0.042
<0.031
<0.036
<0.020
<0.051
<0.036
<0.16
<0.033
<0.030
<0.039
<0.032
<0.051
<0.030
<0.024
<0.042
35.4
HA-13
1.0-1.5
6/23/2020
<0.015
<0.00082
<0.00017
0.0100
<0.0010
<0.00025
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
7.05
HA-14
0-0.5
6/23/2020
<0.015
<0.00086
<0.00018
<0.00080
<0.0011
<0.00026
<0.031
<0.042
<0.031
<0.036
<0.020
<0.052
<0.036
0.69J
<0.033
<0.030
<0.040
<0.032
<0.052
<0.030
0.33J
<0.042
45.9
HA-15
0-0.5
6/23/2020
<0.016
<0.00087
<0.00018
<0.00081
<0.0011
<0.00027
<0.036
<0.049
<0.036
<0.043
<0.023
<0.061
<0.043
<0.19
<0.039
<0.035
<0.047
<0.038
<0.061
<0.035
<0.028
<0.049
35.2
HA-16
0-0.5
6/23/2020
<0.014
<0.00076
<0.00016
<0.00071
I <0.00095
<0.00023
I <0.031
<0.043
<0.031
I <0.037
<0.020
<0.053
<0.037
<0.17
<0.034
<0.030
<0.040
<0.032
<0.053
<0.030
<0.025
<0.043
323
HA-17
0-0.5
6/23/2020
<0.015
<0.00084
0.00091J
<0.00079
<0.0011
<0.00026
<0.030
<0.041
<0.030
<0.036
<0.019
<0.051
<0.036
<0.16
<0.032
<0.029
<0.039
<0.031
<0.051
<0.029
<0.024
<0.041
18.4
0-0.5
6/23/2020
<0.016
<0.00091
<0.00019
<0.00085
<0.0011
<0.00028
<0.032
<0.044
0.36
0.53
0.48
0.25 J
0.18 J
0.40 J
0.48
<0.031
0.24 J
<0.034
0.17 J
0.17 J
<0.026
0.34 J
14.7
HA-18
1.0-1.5
6/23/2020
NA
NA
NA
NA
NA
NA
<0.037
<0.051
<0.037
<0.044
<0.024
<0.063
<0.044
<0.20
<0.040
<0.036
<0.048
<0.039
<0.063
<0.036
<0.029
<0.051
21.6
HA-19
0-0.5
6/23/2020
<0.014
<0.00076
<0.00016
<0.00071
<0.00095
<0.00023
<0.031
<0.042
<0.031
<0.037
<0.020
<0.052
<0.037
0.53J
<0.033
<0.030
<0.040
<0.032
<0.052
<0.030
<0.024
<0.042
11.7
HA-20
0-0.5
6/23/2020
0.077
<0.00088
0.0028
<0.00082
0.032
<0.00027
<0.032
<0.043
<0.032
<0.037
<0.020
<0.053
<0.037
1.4J
<0.034
<0.030
<0.041
<0.033
<0.053
<0.030
<0.025
<0.043
274
1.0-1.5
6/23/2020
0.100
<0.0010
<0.00021
0.0037
<0.0013
<0.00031
<0.037
<0.050
<0.037
<0.043
<0.024
<0.061
<0.043
<0.20
<0.039
<0.035
<0.047
<0.038
<0.061
<0.035
<0.029
<0.050
30.5
Duplicate-1
0-0.5
6/23/2020
<0.016
<0.00088
0.0018
<0.00083
0.0027
<0.00027
<0.032
<0.043
<0.032
<0.037
<0.020
<0.053
<0.037
<0.17
<0.034
<0.031
<0.041
<0.033
<0.053
<0.031
<0.025
<0.043
310
HA-21
0-0.5
6/24/2020
<0.018
<0.0010
<0.00021
<0.00094
<0.0013
<0.00031
<0.032
<0.043
<0.032
<0.038
I <0.021
<0.054
I <0.038
0.40J
<0.034
<0.031
<0.041
<0.033
<0.054
<0.031
<0.025
<0.043
8.84
Duplicate-2
0-0.5
6/24/2020
<0.018
<0.0010
<0.00021
<0.00094
<0.0013
<0.00031
<0.032
<0.043
<0.032
<0.037
<0.020
<0.053
<0.037
0.51J
<0.034
<0.030
<0.041
<0.033
<0.053
<0.030
<0.025
<0.043
8.40
HA-22
0-0.5
6/24/2020
0.031
<0.00081
<0.00017
<0.00076
0.0015
<0.00025
<0.032
<0.044
<0.032
<0.038
<0.021
<0.054
<0.038
<0.17
<0.035
<0.031
<0.042
<0.034
<0.054
<0.031
<0.025
<0.044
9.60
HA-23
0-0.5
6/24/2020
<0.011
<0.00064
<0.00013
0.0014 J
<0.0008
<0.00020
<0.030
<0.041
0.082 J
0.12 J
0.14 J
0.077 J
0.049 J
<0.16
0.091 J
<0.029
0.073 J
<0.031
0.057 J
0.041 J
<0.024
0.075 J
13.1
1.0-1.5
6/24/2020
0.052
<0.0044
<0.00076
1 0.0025J
<0.00044
1 0.0020
<0.031
<0.042
1 <0.031
<0.037
<0.020
<0.052
<0.037
<0.17
1 <0.033
<0.030
<0.040
<0.032
<0.052
<0.030
<0.025
<0.042
NA
HA-24
0-0.5
6/24/2020
<0.015
<0.00082
<0.00017
<0.00077
<0.0010
<0.00025
<0.030
<0.040
<0.030
<0.035
<0.019
<0.050
<0.035
0.38J
<0.032
<0.029
<0.038
<0.031
<0.050
<0.029
<0.023
<0.040
18.2
0-0.5
6/24/2020
0.360
<0.00098
<0.00020
<0.00092
<0.0012
0.0021
<0.035
<0.048
<0.035
<0.042
<0.023
<0.059
<0.042
<0.19
<0.038
<0.034
<0.045
<0.037
<0.059
<0.034
<0.028
<0.048
11.1
HA-25
1.0-1.5
6/24/2020
0.280
<0.0010
<0.00021
<0.00096
<0.0013
<0.00032
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
16.3
0-0.5
6/24/2020
0.077
<0.00090
<0.00018
<0.00084
0.0017
<0.00028
<0.032
<0.044
<0.032
<0.038
<0.021
<0.054
<0.038
<0.17
<0.035
<0.031
<0.042
<0.033
<0.054
<0.031
<0.025
<0.044
26.5
HA-26
1.0-1.5
6/24/2020
<0.029
<0.0016
<0.00033
<0.0015
<0.0020
<0.00049
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
17.0
0-0.5
6/24/2020
0.330
<0.00097
0.0024
1 <0.00091
0.120
<0.00030
0.18 J
0.21 J
1 1.9
2.8*
3.4
1.3
1.6
0.41 J
2.1
0.054 J
2.2
0.080 J
1.0
1.1
<0.027
2.0
22.4
HA-27
1.0-1.5
6/24/2020
<0.015
<0.00084
<0.00017
<0.00079
<0.0011
<0.00026
<0.030
<0.041
0.13 J
0.17 T
0.29 J
0.098 J
0.11 J
<0.16
0.13 J
<0.029
0.19 J
<0.031
0.086 J
0.088 J
<0.024
0.17 J
7.43
0-0.5
6/24/2020
<0.016
<0.00089
<0.00018
<0.00083
<0.0011
<0.00027
7.6J
9.8J
55*
83*
110*
34
32
<6.8
55
2.5 J
60
4.2J
31*
38
<1.0
53
158
HA-28
1.0-1.5
6/24/2020
NA
NA
NA
NA
NA
NA
I <0.031
<0.042
0.041 J
0.053 J
0.086 J
<0.052
1 <0.037
<0.17
0.041 J
<0.030
0.048 J
<0.032
1 <0.052
<0.030
<0.024
0.046 J
8.18
0-0.5
6/24/2020
0.130
<0.00065
<0.00013
<0.00061
<0.00082
<0.00020
<0.033
<0.044
<0.033
<0.038
<0.021
<0.055
<0.038
0.75J
<0.035
<0.031
<0.042
<0.034
<0.055
<0.031
<0.026
<0.044
148
HA-29
1.0-1.5
6/24/2020
NA
NA
NA
NA
NA
NA
<0.035
<0.048
<0.035
<0.041
<0.023
<0.059
<0.041
<0.19
<0.038
<0.034
<0.045
<0.036
<0.059
<0.034
<0.028
<0.048
40.2
0-0.5
6/24/2020
<0.016
<0.00089
<0.00018
I <0.00083
<0.0011
<0.00027
<0.032
<0.043
I <0.032
<0.038
<0.020
<0.054
<0.038
3.3
<0.034
<0.031
<0.041
<0.033
<0.054
<0.031
<0.025
<0.043
176
HA-30
1.0-1.5
6/24/2020
NA
NA
NA
NA
NA
NA
<0.031
<0.042
<0.031
<0.037
<0.020
<0.052
<0.037
<0.17
<0.033
<0.030
<0.040
<0.032
<0.052
<0.030
<0.024
<0.042
18.5
BG
0-0.5
6/24/2020
<0.014
<0.00078
<0.00016
<0.00073
<0.00097
<0.00024
<0.032
<0.043
<0.032
<0.037
<0.020
<0.053
<0.037
<0.17
<0.034
<0.030
<0.041
<0.033
<0.053
<0.030
<0.025
<0.043
9.51
(Background)
1.0-1.5
6/24/2020
<0.012
<0.00067
0.0016
<0.00062
<0.00084
I <0.00020
I <0.032
<0.043
<0.032
<0.037
<0.020
I <0.053
I <0.037
<0.17
<0.034
<0.031
<0.041
I <0.033
I <0.053
<0.031
<0.025
<0.043
6.69
Protection of Groundwater PSRG
25
17
1.24
0.025
1.5
8.3
16
1,300
0.35
0.12
1.2
15,600
12
120
36
10
670
110
3.9
134
0.34
440
250
Residentail PSRG
12,000
5,500
NE
58
1,200
990
720
3,600
1.1
0.11
1.1
NE
11
51,000
110
15
480
480
1.1
NE
3,800
360
400
Industrial/Commercial PSRG
140,000
40,000
NE
650
7,300
9,700
9,000
45,000
21
2.1
21
NE
210
660,000
2,100
210
6,000
6,000
21
NE
49,000
4,500
800
Notes:
Soil sample concentrations are reported in mg/Kg.
mg/Kg - milligrams per kilogram.
NA - not analyzed.
NE - not established.
BG - Sample ID for background samples
+= Polycyclic aromatic hydrocarbons (PAHs)
J - indicates an estimated concentration above the method detection limit but below the reporting limit.
<- indicates the constituent was not detected above the method detection limit.
The soil sample Duplicate-1 is a duplicate sample of the record sample HA-20.
The soil sample Duplicate-2 is a duplicate sample of the record sample HA-21.
PSRG: Division of Waste Management Preliminary Soil Remediation Goals Only 2020).
Concentrations shown in BOLD exceed the laboratory detection limits.
Concentrations shown with an underline exceed the Protection of Groundwater PSRG.
Concentrations that exceed the Residential Health Based PSRG are shown with highlighted value.
Concentrations shown with an asterisk* exceed the Industrial/Commercial Health Based PSRG.
Tables for November 2020 Soil Assessment.xlsx

TABLE3
Summary of Analytical Results - November 2020 Soil Assessment
Sir Walter Gun Club
Knightdale, Wake County, North Carolina
Brownfields Project No. 23068-19-092
S&ME Project No. 4305-19-213
Volatile Organic Compounds by
Lead by EPA Method 6010D
Analytical Method
Semi -Volatile Organic Compounds by EPA Method 8270E (mg/Kg)
Method 8260D (mg/Kg)
(mg/Kg)
+
+
+
+
Analyte
+
,+
+
+
d
R
R
�r
Sample
r'
d
ii
iq
Q!
°
M
ti
r
+
„
'b
M
+
Lead
Sample ID
Depth
Date
c
m
a
u
y
V
x
Collected
o
a
c
o
0
0
0
0
0
d
$
c
o
a
+
d
(ft-bgs)
o
y�
1S
C
N
N
N
N
N
N
a
A
O
O
r
d
r
r
r
Z
rVi
/r
b
HA-31
0-0.5
11/17/2020
0.036
<0.00018
0.0047
<0.034
<0.031
<0.042
<0.031
<0.037
<0.020
<0.052
<0.037
1.4 J
<0.039
<0.033
<0.057
<0.040
<0.032
<0.052
<0.030
<0.042
695
1.0-1.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
6.34
HA-32
0-0.5
11/17/2020
0.035
<0.00018
<0.0011
<0.034
<0.031
<0.042
<0.031
<0.037
<0.037
<0.052
<0.037
<0.17
<0.039
<0.033
1 <0.056
<0.040
<0.032
<0.052
<0.030
<0.042
14.2
HA-33
0-0.5
11/17/2020
<0.013
<0.00015
<0.00092
<0.035
<0.032
<0.043
<0.032
<0.038
<0.021
<0.054
<0.038
0.43 J
<0.040
<0.034
<0.058
<0.041
<0.033
<0.054
<0.031
<0.043
13.7
HA-34
0-0.5
11/17/2020
<0.012
<0.00014
<0.00084
<0.036
<0.032
<0.044
<0.032
<0.032
<0.021
<0.054
<0.038
<0.17
<0.040
<0.034
<0.058
<0.041
<0.033
<0.054
<0.031
<0.044
7.07
HA-35
0-0.5
11/17/2020
<0.018
0.0008 J
<0.0012
<0.043
<0.039
<0.053
0.21 J
0.32
0.31 J
0.19 J
0.16 J
0.44 J
<0.048
0.23 J
<0.071
0.29 J
<0.040
0.35 J
0.18 J
0.23 J
38.4
1.0-1.5
11/17/2020
NA
NA
NA
<0.042
<0.028
<0.038
<0.028
<0.033
<0.018
<0.047
<0.033
<0.15
<0.035
<0.030
<0.069
<0.036
<0.029
<0.047
<0.027
<0.038
16.2
0-0.5
11/17/2020
<0.012
<0.00014
<0.00087
<0.035
<0.031
<0.042
0.89 J
0.13 L
0.13 J
0.083 J
0.066 J
<0.17
<0.039
0.097 J
<0.057
0.11 J
<0.032
0.23 J
0.069 J
0.10 J
12.0
HA-36
1.0-1.5
11/17/2020
NA
NA
NA
<0.037
<0.028
<0.038
<0.028
<0.033
<0.018
<0.047
<0.033
<0.15
<0.035
<0.030
<0.061
<0.036
<0.029
<0.047
<0.027
<0.038
7.86
HA-37
0-0.5
11/17/2020
<0.016
0.00058 J
<0.0011
<0.69
2.2 J
2.3 J
25*
37*
39*
32
15
<3.3
<0.78
30
<1.1
21
0.90 J
22*
13
20
20.0
1.0-1.5
11/17/2020
NA
NA
NA
<0.034
<0.028
<0.038
0.17 J
0.26 I
0.24 J
0.19 J
0.070 J
1 <0.15
<0.035
0.22 J
0.20 J
0.18 J
<0.029
0.25 J
0.097 J
0.22 J
6.45
HA-38
0-0.5
11/17/2020
<0.014
0.0007 J
0.0066
<0.036
0.044 J
0.056 J
0.38
0.61
0.63
0.59
0.23 J
1.6 J
0.072 J
0.42
<0.060
0.36 J
<0.034
0.56
0.27 J
0.30 J
48.5
1.0-1.5
11/17/2020
NA
NA
NA
<0.033
<0.028
<0.038
<0.028
<0.033
<0.018
<0.047
<0.033
<0.15
<0.035
<0.030
0.16 J
<0.036
<0.029
0.16 J
<0.027
<0.038
4.91
HA-39
0-0.5
11/17/2020
<0.012
<0.00014
<0.00087
<0.033
<0.030
<0.041
<0.030
<0.036
<0.019
<0.051
<0.036
<0.16
<0.038
<0.032
<0.055
<0.039
<0.031
<0.051
<0.029
<0.041
9.46
HA-40
0-0.5
11/17/2020
0.032
0.0021
<0.00087
<0.035
<0.031
<0.043
<0.031
<0.037
<0.020
<0.053
<0.037
<0.17
<0.039
<0.034
<0.057
<0.040
<0.032
<0.053
<0.030
0.043
244
1.0-1.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
14.5
HA-41
0-0.5
11/17/2020
0.080
0.0056
0.0047
<0.036
<0.032
<0.044
<0.032
<0.038
<0.021
<0.054
<0.038
0.49 J
<0.040
<0.035
<0.059
<0.042
<0.034
<0.054
<0.031
<0.044
65.6
1.0-1.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
17.0
HA-42
0-0.5
11/17/2020
0.017 J
0.011
<0.00091
<0.036
<0.032
<0.044
<0.032
<0.038
<0.021
<0.054
<0.038
0.20 J
<0.040
<0.035
<0.059
<0.042
<0.034
<0.054
<0.031
<0.044
276
1.0-1.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
21.7
HA-43
0-0.5
11/17/2020
0.036
0.00065 J
0.14
<0.042
<0.031
<0.042
<0.031
<0.037
<0.020
<0.052
<0.037
0.25 J
<0.039
<0.033
<0.057
<0.040
<0.032
<0.052
<0.030
<0.042
23.5
0-0.5
11/17/2020
1 NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
487
HA-44
1.0-1.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
23.8
HA-45
0-0.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
128
1.0-1.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
22.0
HA-46
0-0.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
535
1.0-1.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
7.38
HA-47
0-0.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
HA-48
0-0.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
207
1.0-1.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
6.30
HA-49
0-0.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
HA-50
0-0.5
11/17/2020
NA
NA
NA
0.067J
<0.028
<0.038
<0.028
<0.033
<0.018
<0.047
<0.033
<0.15
<0.035
<0.030
<0.051
<0.036
<0.029
<0.047
<0.027
<0.038
10.6
HA-51
0-0.5
11/17/2020
NA
NA
NA
<0.031
<0.028
<0.038
<0.028
<0.033
<0.018
<0.047
<0.033
<0.15
<0.035
<0.030
<0.051
<0.036
<0.029
<0.047
<0.027
<0.038
420
1.0-1.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
21.1
DLTP-11-17-20
0-0.5
11/17/2020
0.10
0.0048
0.00076
<0.034
<0.031
<0.042
<0.031
<0.036
<0.020
<0.052
<0.036
0.90 J
<0.039
<0.033
<0.056
<0.040
<0.032
<0.052
<0.030
<0.042
251
1.0-1.5
11/17/2020
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
43.8
of Groundwater PSRG
25
1.24
1.5
NE
16
1,300
0.35
0.12
1.2
15,600
12
120
NE
36
0.38
670
110
3.9
134
440
250
WProtection
Residentail PSRG
12,000
NE
1,200
NE
720
3,600
1.1
0.11
1.1
NE
11
51,000
NE
110
0.11
480
480
1.1
NE
360
400
Industrial/Commercial PSRG
140,000
1 NE
1 7,300
1 NE
1 9,000
1 45,000
1 21
1 2.1
21
1 NE
1 210
1 660,000
1 NE
2,100
2.1
6,000
6,000
21
NE
4,500
800
Notes:
Soil sample concentrations are reported in mg/Kg.
mg/Kg - milligrams per kilogram.
NA - not analyzed.
NE - not established.
+ = Polycyclic aromatic hydrocarbons (PAHs)
J - indicates an estimated concentration above the method detection limit but below the reporting limit.
< - indicates the constituent was not detected above the method detection limit.
The soil sample DUP-11-17-20 is a duplicate sample of the record sample HA-43.
PSRG: Division of Waste Management Preliminary Soil Remediation Goals (July 2020).
Concentrations shown in BOLD exceed the laboratory detection limits.
Concentrations shown with an underline exceed the Protection of Groundwater PSRG.
Concentrations that exceed the Residential Health Based PSRG are shown with highlighted value.
Concentrations shown with an asterisk* exceed the Industrial/Commercial Health Based PSRG.
Tables for November 2020 Soil AssessmentAu

� f
TABLE 4
s Summary of Soil TCLP Analytical Results - December 2020
I I' Sir Walter Gun Club
Knightdale, Wake County, North Carolina
Brownfields Project No. 23068-19-092
S&ME Project No. 4305-19-213
Analytical Method — 10
Lead by EPA Method 6010D
(mg/Kg)
Lead by EPA Method 6010D
(mg/L)
Analyte
Total Lead
Extractable Lead - TCLP
Sample ID
Sample
Depth
(ft-bgs)
Date Collected
HA-31
0-0.5
11/17/2020
695
10.7
HA-40
0-0.5
11/17/2020
244
2.00
HA-42
0-0.5
11/17/2020
276
1.84
HA-44
0-0.5
11/17/2020
487
4.35
HA-46
0-0.5
11/17/2020
535
5.72
HA-51
0-0.5
11/17/2020
420
2.74
Protection of Groundwater PSRG
250
NE
Residentail PSRG
400
NE
Industrial/Commercial PSRG
800
NE
RCRA Regulatory Concentration for
Characteristics Hazardous Waste by TCLP
NE
5
Notes:
TCLP - Toxicity Characteristic Leaching Procedure method
mg/Kg - milligrams per kilogram
mg/L - milligrams per liter
NA - not analyzed.
NE - not established.
Tables for November 2020 Assessmentxls

Appendix III - Preliminary Grading Plans

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Job No.
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Date
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PRELI M I NARY
NOT APPROVED FOR
CONSTRUCTION
Revisions
Sheet No.
C3.2

Appendix IV - Laboratory Analytical Report and Chain -of -Custody
Record

2�SQ pCCgF ENCO Laboratories
9e0
Accurate. Timely. Responsive. Innovative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Tuesday, December 15, 2020
S&ME, Inc. (SM001)
Attn: Bryan Wence
3201 Spring Forest Road
Raleigh, NC 27616
RE: Laboratory Results for
Project Number: 4305-19-213, Project Name/Desc: Sir Walter Gun Club
ENCO Workorder(s): CD18880
Dear Bryan Wence,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Tuesday, November 17, 2020.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
O"6LC'=-:;tA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 107

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: HA-31-6"
Lab ID: CD18880-01
Sampled: 11/17/20 08:30
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3010A
O5/16/21 06/12/21
12/14/20 15:26
12/15/20 12:15
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 12:08
11/18/20 22:02
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 15:12
Client ID: HA-31-6"
Lab ID: CD18880-01RE1
Sampled: 11/17/20 08:30
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/20/20 10:53
11/23/20 14:56
Client ID: HA-31-18"
Lab ID: CD18880-02
Sampled: 11/17/20 08:35
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 09:41
Client ID: HA-32-6"
Lab ID: CD18880-03
Sampled: 11/17/20 08:45
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/20/20 10:53
11/23/20 14:58
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 12:08
11/18/20 22:32
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 15:44
Client ID: HA-33-6"
Lab ID: CD18880-05
Sampled: 11/17/20 09:05
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time
EPA 6010D
EPA 3050B
05/16/21
11/20/20 10:53
11/23/20 14:59
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 12:08
11/18/20 23:02
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 16:15
Client ID: HA-34-6"
Lab ID: CD18880-07
Sampled: 11/17/20 09:25
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/20/20 10:53
11/23/20 15:01
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 12:08
11/18/20 23:32
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 16:47
Client ID: HA-35-6"
Lab ID: CD18880-09
Sampled: 11/17/20 09:40
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/20/20 10:53
11/23/20 15:03
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 12:08
11/19/20 00:02
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 17:18
Client ID: HA-35-18"
Lab ID: CD18880-10
Sampled: 11/17/20 09:45
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 09:52
EPA 8270E
EPA 3550C_MS
12/01/20 01/04/21
11/25/20 01:25
11/25/20 15:31
Client ID: HA-36-6"
Lab ID: CD18880-11
Sampled: 11/17/20 10:00
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O5/16/21
11/20/20 10:53
11/23/20 15:06
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 12:08
11/19/20 00:32
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 13:37
Client ID: HA-36-18"
Lab ID: CD18880-12
Sampled: 11/17/20 10:05
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 09:54
EPA 8270E
EPA 3550C_MS
12/01/20 01/04/21
11/25/20 01:25
11/25/20 16:03
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 107

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: HA-37-6"
Lab ID: CD18880-13
Sampled: 11/17/20 10:20
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O5/16/21
11/20/20 10:53
11/23/20 15:08
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 14:35
11/19/20 05:03
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 21:00
Client ID: HA-37-18"
Lab ID: CD18880-14
Sampled: 11/17/20 10:25
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 09:56
EPA 8270E
EPA 3550C_MS
12/01/20 01/04/21
11/25/20 01:25
11/25/20 16:34
Client ID: HA-38-6"
Lab ID: CD18880-15
Sampled: 11/17/20 10:40
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/20/20 10:53
11/23/20 15:15
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 14:35
11/19/20 05:33
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 22:04
Client ID: HA-38-18"
Lab ID: CD18880-16
Sampled: 11/17/20 10:45
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 10:05
EPA 8270E
EPA 3550C_MS
12/01/20 01/04/21
11/25/20 01:25
11/25/20 13:25
Client ID: HA-39-6"
Lab ID: CD18880-17
Sampled: 11/17/20 10:50
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/20/20 10:53
11/23/20 15:17
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 14:35
11/19/20 06:03
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 17:50
Client ID: HA-40-6"
Lab ID: CD18880-19
Sampled: 11/17/20 11:10
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O5/16/21
11/20/20 10:53
11/23/20 15:19
EPA 6010D
EPA 3010A
05/16/21 06/12/21
12/14/20 15:26
12/15/20 13:14
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 14:35
11/19/20 06:33
Client ID: HA-40-6"
Lab ID: CD18880-19RE1
Sampled: 11/17/20 11:10
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8270E
EPA 3550C_MS
12/01/20 01/04/21
11/25/20 01:25
11/25/20 15:00
Client ID: HA-40-18"
Lab ID: CD18880-20
Sampled: 11/17/20 11:15
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 10:07
Client ID: HA-41-6"
Lab ID: CD18880-21
Sampled: 11/17/20 11:30
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(sl
EPA 6010D
EPA 3050B
05/16/21
11/20/20 10:53
11/23/20 15:21
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 14:35
11/19/20 07:03
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 18:53
Client ID: HA-41-18"
Lab ID: CD18880-22
Sampled: 11/17/20 11:35
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 10:09
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 107

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: HA-42-6"
Lab ID: CD18880-23
Sampled: 11/17/20 11:40
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O5/16/21
11/20/20 10:53
11/23/20 15:23
EPA 6010D
EPA 3010A
05/16/21 06/12/21
12/14/20 15:26
12/15/20 13:16
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 14:35
11/19/20 07:33
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 19:25
Client ID: HA-42-18"
Lab ID: CD18880-24
Sampled: 11/17/20 11:45
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 10:11
Client ID: HA-43-6"
Lab ID: CD18880-25
Sampled: 11/17/20 11:55
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/20/20 10:53
11/23/20 15:25
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 14:35
11/19/20 08:03
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 19:57
Client ID: HA-44-6"
Lab ID: CD18880-27
Sampled: 11/17/20 13:30
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 10:13
EPA 6010D
EPA 3010A
05/16/21 06/12/21
12/14/20 15:26
12/15/20 13:19
Client ID: HA-44-18"
Lab ID: CD18880-28
Sampled: 11/17/20 13:35
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
12/04/20 11:44
12/07/20 10:47
Client ID: HA-45-6"
Lab ID: CD18880-29
Sampled: 11/17/20 13:45
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 10:15
Client ID: HA-45-18"
Lab ID: CD18880-30
Sampled: 11/17/20 13:50
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O5/16/21
12/04/20 11:44
12/07/20 11:17
Client ID: HA-46-6"
Lab ID: CD18880-31
Sampled: 11/17/20 14:00
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O5/16/21
11/30/20 08:59
12/01/20 10:17
EPA 6010D
EPA 3010A
05/16/21 06/12/21
12/14/20 15:26
12/15/20 13:21
Client ID: HA-46-18"
Lab ID: CD18880-32
Sampled: 11/17/20 14:05
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
12/04/20 11:44
12/07/20 11:19
Client ID: HA-48-6"
Lab ID: CD18880-35
Sampled: 11/17/20 14:40
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 10:19
Client ID: HA-48-18"
Lab ID: CD18880-36
Sampled: 11/17/20 14:45
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
12/04/20 11:44
12/07/20 11:21
Client ID: DUP-11-17-20-6"
Lab ID: CD18880-37
Sampled: 11/17/20 15:00
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O5/16/21
11/20/20 10:53
11/23/20 15:27
EPA 8260D
EPA 5035_MS
12/01/20
11/18/20 14:35
11/19/20 08:33
EPA 8270E
EPA 3550C_MS
12/01/20 12/29/20
11/19/20 03:48
11/23/20 20:28
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 107

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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: DUP-11-17-20-18"
Lab ID: CD18880-38
Sampled: 11/17/20 15:05
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O5/16/21
11/30/20 08:59
12/01/20 10:22
Client ID: HA-50-6"
Lab ID: CD18880-41
Sampled: 11/17/20 15:40
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O5/16/21
11/30/20 08:59
12/01/20 10:23
EPA 8270E
EPA 3550C_MS
12/01/20 01/04/21
11/25/20 01:25
11/25/20 17:06
Client ID: HA-51-6"
Lab ID: CD18880-43
Sampled: 11/17/20 15:50
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
05/16/21
11/30/20 08:59
12/01/20 10:32
EPA 6010D
EPA 3010A
05/16/21 06/12/21
12/14/20 15:26
12/15/20 13:23
EPA 8270E
EPA 3550C_MS
12/01/20 01/04/21
11/25/20 01:25
11/25/20 17:37
Client ID: HA-51-18"
Lab ID: CD18880-44
Sampled: 11/17/20 15:55
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3050B
O5/16/21
12/04/20 11:44
12/07/20 11:30
Client ID: Equipment Blank
Lab ID: CD18880-45
Sampled: 11/17/20 16:10
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
O5/16/21
11/18/20 09:37
11/20/20 14:28
EPA 8260D
EPA 503013_MS
12/01/20
11/18/20 15:12
11/19/20 18:22
Client ID: Equipment Blank
Lab ID: CD18880-45RE1
Sampled: 11/17/20 16:10
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8270E
EPA 3510C_MS
11/24/20 12/28/20
11/18/20 19:54
11/20/20 11:19
Client ID: Trip Blank
Lab ID: CD18880-46
Sampled: 11/17/20 16:10
Received: 11/17/20 17:10
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 8260D
EPA 503013_MS
12/01/20
11/18/20 15:12
11/19/20 17:54
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 107

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SAMPLE DETECTION SUMMARY
Client ID: HA-31-6"
Lab ID:
CD18880-01
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Acetone
0.036
0.016
0.022
mg/kg dry
EPA 8260D
Benzoic acid
1.4
J
0.17
1.9
mg/kg dry
EPA 8270E
Lead - TCLP
10.7
0.155
0.500
mg/L
EPA 6010D
Styrene
0.0047
0.0011
0.0011
mg/kg dry
EPA 8260D
Client ID: HA-31-6"
Lab ID:
CD18880-01RE1
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
695
D
0.667
2.78
mg/kg dry
EPA 6010D
Client ID: HA-31-18"
Lab ID:
CD18880-02
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
6.34
0.141
0.587
mg/kg dry
EPA 6010D
Client ID: HA-32-6"
Lab ID:
CD18880-03
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Acetone
0.035
0.016
0.022
mg/kg dry
EPA 8260D
Lead - Total
14.2
0.133
0.554
mg/kg dry
EPA 6010D
Client ID: HA-33-6"
Lab ID:
CD18880-05
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Benzoic acid
0.43
1
0.17
1.9
mg/kg dry
EPA 8270E
Lead - Total
13.7
0.137
0.570
mg/kg dry
EPA 6010D
Client ID: HA-34-6"
Lab ID:
CD18880-07
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
7.07
0.137
0.573
mg/kg dry
EPA 6010D
Client ID: HA-35-6"
Lab ID:
CD18880-09
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
4-Isopropyltoluene
0.00080
J
0.00020
0.0013
mg/kg dry
EPA 8260D
Benzo(a)anthracene
0.21
J
0.039
0.46
mg/kg dry
EPA 8270E
Benzo(a)pyrene
0.32
J
0.046
0.46
mg/kg dry
EPA 8270E
Benzo(b)fluoranthene
0.31
J
0.025
0.46
mg/kg dry
EPA 8270E
Benzo(g,h,i)perylene
0.19
J
0.065
0.46
mg/kg dry
EPA 8270E
QV-01
Benzo(k)fluoranthene
0.16
J
0.046
0.46
mg/kg dry
EPA 8270E
Benzoic acid
0.44
J
0.21
2.4
mg/kg dry
EPA 8270E
Chrysene
0.23
J
0.042
0.46
mg/kg dry
EPA 8270E
Fluoranthene
0.29
J
0.050
0.46
mg/kg dry
EPA 8270E
Indeno(1,2,3-cd)pyrene
0.35
J
0.065
0.46
mg/kg dry
EPA 8270E
Lead - Total
38.4
0.166
0.692
mg/kg dry
EPA 6010D
Phenanthrene
0.18
J
0.037
0.46
mg/kg dry
EPA 8270E
Pyrene
0.23
J
0.053
0.46
mg/kg dry
EPA 8270E
Client ID: HA-35-18"
Lab ID:
CD18880-10
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
16.2
0.163
0.679
mg/kg dry
EPA 6010D
Client ID: HA-36-6"
Lab ID:
CD18880-11
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Benzo(a)anthracene
0.089
J
0.031
0.37
mg/kg dry
EPA 8270E
Benzo(a)pyrene
0.13
J
0.037
0.37
mg/kg dry
EPA 8270E
Benzo(b)fluoranthene
0.13
J
0.020
0.37
mg/kg dry
EPA 8270E
Benzo(g,h,i)perylene
0.083
J
0.053
0.37
mg/kg dry
EPA 8270E
3-04
Benzo(k)fluoranthene
0.066
J
0.037
0.37
mg/kg dry
EPA 8270E
Chrysene
0.097
J
0.034
0.37
mg/kg dry
EPA 8270E
Fluoranthene
0.11
J
0.040
0.37
mg/kg dry
EPA 8270E
Indeno(1,2,3-cd)pyrene
0.23
J
0.053
0.37
mg/kg dry
EPA 8270E
Lead - Total
12.0
0.134
0.559
mg/kg dry
EPA 6010D
Phenanthrene
0.069
J
0.030
0.37
mg/kg dry
EPA 8270E
Pyrene
0.10
J
0.042
0.37
mg/kg dry
EPA 8270E
Client ID: HA-36-18"
Lab ID:
CD18880-12
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
7.86
0.159
0.661
mg/kg dry
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 107

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SAMPLE DETECTION SUMMARY
Client ID: HA-37-6"
Lab ID:
CD18880-13
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
4-Isopropyltoluene
0.00058
J
0.00018
0.0011
mg/kg dry
EPA 8260D
Acenaphthene
2.2
]D
0.62
7.3
mg/kg dry
EPA 8270E
R-05
Anthracene
2.3
]D
0.84
7.3
mg/kg dry
EPA 8270E
R-05
Benzo(a)anthracene
25
D
0.62
7.3
mg/kg dry
EPA 8270E
R-05
Benzo(a)pyrene
37
D
0.73
7.3
mg/kg dry
EPA 8270E
R-05
Benzo(b)fluoranthene
39
D
0.40
7.3
mg/kg dry
EPA 8270E
R-05
Benzo(g,h,i)perylene
32
D
1.0
7.3
mg/kg dry
EPA 8270E
3-04, R-05
Benzo(k)fluoranthene
15
D
0.73
7.3
mg/kg dry
EPA 8270E
R-05
Chrysene
30
D
0.67
7.3
mg/kg dry
EPA 8270E
R-05
Fluoranthene
21
D
0.80
7.3
mg/kg dry
EPA 8270E
R-05
Fluorene
0.90
]D
0.64
7.3
mg/kg dry
EPA 8270E
R-05
Indeno(1,2,3-cd)pyrene
22
D
1.0
7.3
mg/kg dry
EPA 8270E
R-05
Lead - Total
20.0
0.133
0.556
mg/kg dry
EPA 6010D
Phenanthrene
13
D
0.60
7.3
mg/kg dry
EPA 8270E
R-05
Pyrene
20
D
0.84
7.3
mg/kg dry
EPA 8270E
R-05
Client ID: HA-37-18"
Lab ID:
CD18880-14
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Benzo(a)anthracene
0.18
J
0.030
0.36
mg/kg dry
EPA 8270E
Benzo(a)pyrene
0.29
J
0.036
0.36
mg/kg dry
EPA 8270E
Benzo(b)fluoranthene
0.26
J
0.019
0.36
mg/kg dry
EPA 8270E
Benzo(g,h,i)perylene
0.20
J
0.051
0.36
mg/kg dry
EPA 8270E
Benzo(k)fluoranthene
0.076
J
0.036
0.36
mg/kg dry
EPA 8270E
Chrysene
0.24
J
0.032
0.36
mg/kg dry
EPA 8270E
Dibenzo(a,h)anth racene
0.21
J
0.055
0.36
mg/kg dry
EPA 8270E
Fluoranthene
0.19
J
0.039
0.36
mg/kg dry
EPA 8270E
Indeno(1,2,3-cd)pyrene
0.27
J
0.051
0.36
mg/kg dry
EPA 8270E
Lead - Total
6.45
0.130
0.541
mg/kg dry
EPA 6010D
Phenanthrene
0.10
J
0.029
0.36
mg/kg dry
EPA 8270E
Pyrene
0.23
J
0.041
0.36
mg/kg dry
EPA 8270E
Client ID: HA-38-6"
Lab ID:
CD18880-15
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
4-Isopropyltoluene
0.00070
J
0.00016
0.00098
mg/kg dry
EPA 8260D
Acenaphthene
0.044
1
0.033
0.39
mg/kg dry
EPA 8270E
Anthracene
0.056
J
0.045
0.39
mg/kg dry
EPA 8270E
Benzo(a)anthracene
0.38
J
0.033
0.39
mg/kg dry
EPA 8270E
Benzo(a)pyrene
0.61
0.039
0.39
mg/kg dry
EPA 8270E
Benzo(b)fluoranthene
0.63
0.021
0.39
mg/kg dry
EPA 8270E
Benzo(g,h,i)perylene
0.59
0.055
0.39
mg/kg dry
EPA 8270E
3-04
Benzo(k)fluoranthene
0.23
J
0.039
0.39
mg/kg dry
EPA 8270E
Benzoic acid
1.6
J
0.18
2.0
mg/kg dry
EPA 8270E
Bis(2-ethylhexyl)phthalate
0.072
J
0.041
0.39
mg/kg dry
EPA 8270E
Chrysene
0.42
0.035
0.39
mg/kg dry
EPA 8270E
Fluoranthene
0.36
J
0.042
0.39
mg/kg dry
EPA 8270E
Indeno(1,2,3-cd)pyrene
0.56
0.055
0.39
mg/kg dry
EPA 8270E
Lead - Total
48.5
0.141
0.588
mg/kg dry
EPA 6010D
Phenanthrene
0.27
J
0.032
0.39
mg/kg dry
EPA 8270E
Pyrene
0.30
J
0.045
0.39
mg/kg dry
EPA 8270E
Styrene
0.0066
0.00096
0.00098
mg/kg dry
EPA 8260D
Client ID: HA-38-18"
Lab ID:
CD18880-16
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Dibenzo(a,h)anth racene
0.17
J
0.054
0.35
mg/kg dry
EPA 8270E
Indeno(1,2,3-cd)pyrene
0.17
J
0.050
0.35
mg/kg dry
EPA 8270E
Lead - Total
4.91
0.128
0.534
mg/kg dry
EPA 6010D
Client ID: HA-39-6"
Lab ID:
CD18880-17
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
Lead - Total
9.46
0.130
0.540
mg/kg dry
EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 107

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SAMPLE DETECTION SUMMARY
Client ID: HA-40-6"
Lab ID:
CD18880-19
Analvte
Results
Flag
MDL
Q
Units
Method
Notes
4-Isopropyltoluene
0.0021
0.00014
0.00089
mg/kg dry
EPA 8260D
Acetone
0.032
0.012
0.018
mg/kg dry
EPA 8260D
Lead - Total
244
0.134
0.559
mg/kg dry
EPA 6010D
Lead - TCLP
2.00
0.155
0.500
mg/L
EPA 6010D
Client ID: HA-40-18"
Lab ID:
CD18880-20
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
14.5
0.139
0.579
mg/kg dry
EPA 6010D
Client ID: HA-41-6"
Lab ID:
CD18880-21
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
4-Isopropyltoluene
0.0056
0.00015
0.00096
mg/kg dry
EPA 8260D
Acetone
0.080
0.013
0.019
mg/kg dry
EPA 8260D
Benzoic acid
0.49
J
0.17
2.0
mg/kg dry
EPA 8270E
Lead - Total
65.6
0.139
0.578
mg/kg dry
EPA 6010D
Styrene
0.0047
0.00094
0.00096
mg/kg dry
EPA 8260D
Client ID: HA-41-18"
Lab ID:
CD18880-22
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
17.0
0.154
0.643
mg/kg dry
EPA 6010D
Client ID: HA-42-6"
Lab ID:
CD18880-23
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
4-Isopropyltoluene
0.011
0.00015
0.00093
mg/kg dry
EPA 8260D
Acetone
0.017
J
0.013
0.019
mg/kg dry
EPA 8260D
Benzoic acid
0.20
J
0.17
2.0
mg/kg dry
EPA 8270E
Lead - Total
276
0.138
0.575
mg/kg dry
EPA 6010D
Lead - TCLP
1.84
0.155
0.500
mg/L
EPA 6010D
Client ID: HA-42-18"
Lab ID:
CD18880-24
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
21.7
0.140
0.582
mg/kg dry
EPA 6010D
Client ID: HA-43-6"
Lab ID:
CD18880-25
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
4-Isopropyltoluene
0.00065
J
0.00014
0.00087
mg/kg dry
EPA 8260D
Acetone
0.036
0.012
0.017
mg/kg dry
EPA 8260D
Benzoic acid
0.25
J
0.17
1.9
mg/kg dry
EPA 8270E
Lead - Total
23.5
0.133
0.554
mg/kg dry
EPA 6010D
Styrene
0.14
0.00086
0.00087
mg/kg dry
EPA 8260D
Client ID: HA-44-6"
Lab ID:
CD18880-27
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
487
0.139
0.579
mg/kg dry
EPA 6010D
Lead - TCLP
4.35
0.155
0.500
mg/L
EPA 6010D
Client ID: HA-44-18"
Lab ID:
CD18880-28
Analvte
Results
Flag
MDL
PQL
Units
Method
Notes
Lead - Total
23.8
0.133
0.553
mq/kq dry
EPA 6010D
Client ID:
HA-45-6"
Lab ID:
CD18880-29
Analvte
Lead - Total
Results
128
Flag
MDL
0.141
PQL
0.586
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
HA-45-18"
Lab ID:
CD18880-30
Analvte
Lead - Total
Results
22.0
Flag
MDL
0.138
PQL
0.574
Units
mg/kg dry
Method
EPA 6010D
Notes
Client ID:
HA-46-6"
Lab ID:
CD18880-31
Analvte
Lead - Total
Lead - TCLP
Results
535
5.72
Flag
MDL
0.147
0.155
PQL
0.614
0.500
Units
mg/kg dry
mg/L
Method
EPA 6010D
EPA 6010D
Notes
Client ID:
HA-46-18"
Lab ID:
CD18880-32
Analvte
Lead - Total
Results
7.38
Flag
MDL
0.134
PQL
0.557
Units
mg/kg dry
Method
EPA 6010D
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 107

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SAMPLE DETECTION SUMMARY
Client ID: HA-48-6" Lab ID: CD18880-35
Analvte Results Flag MDL Q Units Method Notes
Lead - Total 207 0.146 0.608 mq/kq dry EPA 6010D
I Client ID: HA-48-18" Lab ID: CD18880-36
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Lead - Total
6.30
0.141
0.586
mg/kg dry
EPA 6010D
Client ID: DUP-11-17-20-6"
Lab ID:
CD18880-37
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
4-Isopropyltoluene
0.0048
0.00015
0.00094
mg/kg dry
EPA 8260D
Acetone
0.10
0.013
0.019
mg/kg dry
EPA 8260D
Benzoic acid
0.90
J
0.17
1.9
mg/kg dry
EPA 8270E
Lead - Total
251
0.132
0.551
mg/kg dry
EPA 6010D
0.0076 0.00092 0.00094 mq/kq dry EPA 8260D
I Client ID: DUP-11-17-20-18" Lab ID: CD18880-38
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Lead - Total
43.8
0.132
0.549
mg/kg dry
EPA 6010D
Client ID: HA-50-6"
Lab ID:
CD18880-41
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
4-Nitrophenol
0.074
J
0.035
0.37
mg/kg dry
EPA 8270E
Lead - Total
10.6
0.134
0.557
mg/kg dry
EPA 6010D
Client ID: HA-51-6"
Lab ID:
CD18880-43
Analvte
Results
Flag
MDL
PQL
Units
Method Notes
Lead - Total
420
0.139
0.580
mg/kg dry
EPA 6010D
Lead - TCLP
2.74 0.155
0.500
mg/L EPA 6010D
Client ID: HA-51-18"
Lab ID:
CD18880-44
Analvte
Lead - Total
Results Flag MDL
21.1 0.149
PQL
0.620
Units Method Notes
mg/kg dry EPA 6010D
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 107

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ANALYTICAL RESULTS
Description: HA-31-6" Lab Sample ID:CD18880-01 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 08:30 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.98
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00018
U
mg/kg
dry
1
0.00018
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,1,1-Trichloroethane [71-55-6]A
0.00028
U
mg/kg
dry
1
0.00028
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00022
U
mg/kg
dry
1
0.00022
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,1,2-Trichloroethane [79-00-5]A
0.00028
U
mg/kg
dry
1
0.00028
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,1-Dichloroethane [75-34-3]A
0.00028
U
mg/kg
dry
1
0.00028
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,1-Dichloroethene [75-35-4]A
0.00033
U
mg/kg
dry
1
0.00033
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,1-Dichloropropene [563-58-6]A
0.00018
U
mg/kg
dry
1
0.00018
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00031
U
mg/kg
dry
1
0.00031
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,2,3-Trichloropropane [96-18-4]A
0.00071
U
mg/kg
dry
1
0.00071
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00030
U
mg/kg
dry
1
0.00030
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00019
U
mg/kg
dry
1
0.00019
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00088
U
mg/kg
dry
1
0.00088
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,2-Dibromoethane [106-93-4]A
0.00051
U
mg/kg
dry
1
0.00051
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,2-Dichlorobenzene [95-50-1]A
0.00030
U
mg/kg
dry
1
0.00030
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,2-Dichloroethane [107-06-2]A
0.00046
U
mg/kg
dry
1
0.00046
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,2-Dichloropropane [78-87-5]A
0.00029
U
mg/kg
dry
1
0.00029
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00022
U
mg/kg
dry
1
0.00022
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,3-Dichlorobenzene [541-73-1]A
0.00024
U
mg/kg
dry
1
0.00024
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,3-Dichloropropane [142-28-9]A
0.00032
U
mg/kg
dry
1
0.00032
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
1,4-Dichlorobenzene [106-46-7]A
0.00022
U
mg/kg
dry
1
0.00022
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
2,2-Dichloropropane [594-20-7]A
0.00026
U
mg/kg
dry
1
0.00026
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
2-Butanone [78-93-3]A
0.00087
U
mg/kg
dry
1
0.00087
0.0056
OK18029
EPA
8260D
11/18/20
22:02
REF
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00018
U
mg/kg
dry
1
0.00018
0.0056
OK18029
EPA
8260D
11/18/20
22:02
REF
2-Chlorotoluene [95-49-8]A
0.00020
U
mg/kg
dry
1
0.00020
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
2-Hexanone [591-78-6]A
0.00083
U
mg/kg
dry
1
0.00083
0.0056
OK18029
EPA
8260D
11/18/20
22:02
REF
4-Chlorotoluene [106-43-4]A
0.00029
U
mg/kg
dry
1
0.00029
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
4-Isopropyltoluene [99-87-6]A
0.00018
U
mg/kg
dry
1
0.00018
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
4-Methyl-2-pentanone [108-10-1]A
0.00063
U
mg/kg
dry
1
0.00063
0.0056
OK18029
EPA
8260D
11/18/20
22:02
REF
Acetone [67-64-1]A
0.036
mg/kg
dry
1
0.016
0.022
OK18029
EPA
8260D
11/18/20
22:02
REF
Benzene [71-43-2]A
0.00019
U
mg/kg
dry
1
0.00019
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Bromobenzene [108-86-1]A
0.00024
U
mg/kg
dry
1
0.00024
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Bromochloromethane [74-97-5]A
0.00046
U
mg/kg
dry
1
0.00046
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Bromodichloromethane [75-27-4]A
0.00027
U
mg/kg
dry
1
0.00027
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Bromoform [75-25-2]A
0.00050
U
mg/kg
dry
1
0.00050
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Bromomethane [74-83-9]A
0.00036
U
mg/kg
dry
1
0.00036
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Carbon disulfide [75-15-0]A
0.00043
U
mg/kg
dry
1
0.00043
0.0056
OK18029
EPA
8260D
11/18/20
22:02
REF
Carbon Tetrachloride [56-23-5]A
0.00024
U
mg/kg
dry
1
0.00024
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Chlorobenzene [108-90-7]A
0.00019
U
mg/kg
dry
1
0.00019
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Chloroethane [75-00-3]A
0.00028
U
mg/kg
dry
1
0.00028
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Chloroform [67-66-3]A
0.00020
U
mg/kg
dry
1
0.00020
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Chloromethane [74-87-3]A
0.00023
U
mg/kg
dry
1
0.00023
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
cis-1,2-Dichloroethene [156-59-2]A
0.00026
U
mg/kg
dry
1
0.00026
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00019
U
mg/kg
dry
1
0.00019
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Dibromochloromethane [124-48-1]A
0.00039
U
mg/kg
dry
1
0.00039
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Dibromomethane [74-95-3]A
0.00037
U
mg/kg
dry
1
0.00037
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Dichlorodifluoromethane [75-71-8]A
0.00050
U
mg/kg
dry
1
0.00050
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
Ethylbenzene [100-41-4]A
0.00022
U
mg/kg
dry
1
0.00022
0.0011
OK18029
EPA
8260D
11/18/20
22:02
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 10 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-31-6" Lab Sample ID:CD18880-01 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 08:30 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.98
Volatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analvte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
Hexachlorobutadiene [87-68-3]A
0.00039
u
mg/kg
dry
1
0.00039
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
Isopropylbenzene [98-82-8]A
0.00017
u
mg/kg
dry
1
0.00017
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
m,p-Xylenes[108-38-3/106-42-3]A
0.00041
u
mg/kg
dry
1
0.00041
0.0022
OK18029
EPA 8260D
11/18/20
22:02
REF
Methylene Chloride [75-09-2]A
0.00081
u
mg/kg
dry
1
0.00081
0.0022
OK18029
EPA 8260D
11/18/20
22:02
REF
Methyl-tert-Butyl Ether [1634-04-4]A
0.00033
u
mg/kg
dry
1
0.00033
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
Naphthalene [91-20-3]A
0.00030
u
mg/kg
dry
1
0.00030
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
n-Butyl Benzene [104-51-8]A
0.00014
u
mg/kg
dry
1
0.00014
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
n-Propyl Benzene [103-65-1]A
0.00020
u
mg/kg
dry
1
0.00020
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
o-Xylene [95-47-6]A
0.00024
u
mg/kg
dry
1
0.00024
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
sec-Butylbenzene [135-98-8]A
0.0011
u
mg/kg
dry
1
0.0011
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
Styrene [500-42-5]A
0.0047
mg/kg
dry
1
0.0011
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
tert-Butyl benzene [98-06-6]A
0.00019
u
mg/kg
dry
1
0.00019
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
Tetrachloroethene [127-18-4]A
0.00031
u
mg/kg
dry
1
0.00031
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
Toluene [108-88-3]A
0.00027
u
mg/kg
dry
1
0.00027
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
trans-1,2-Dichloroethene [156-60-5]A
0.00041
u
mg/kg
dry
1
0.00041
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.00043
u
mg/kg
dry
1
0.00043
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
Trichloroethene [79-01-6]A
0.00036
u
mg/kg
dry
1
0.00036
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
Trichlorofluoromethane [75-69-4]A
0.00029
u
mg/kg
dry
1
0.00029
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
Vinyl chloride [75-01-4]A
0.00027
u
mg/kg
dry
1
0.00027
0.0011
OK18029
EPA 8260D
11/18/20
22:02
REF
Xylenes (Total) [1330-20-7]A
0.00062
u
mg/kg
dry
1
0.00062
0.0033
OK18029
EPA 8260D
11/18/20
22:02
REF
Surrogates
Results
DF
Spikev/
%Rec
%RecLimits
Batch
Method
Analvzed
" Notes
4-Bromofluorobenzene
30
1
50.0
59 %
50-127
OK18029
EPA 8260D
11118120 22.02
REF
Dibromofluoromethane
38
1
50.0
76 %
52-128
OK18029
EPA 8260D
11118120 22, 02
REF
Toluene-&
35
1
50.0
71 %
57-124
OK18029
EPA 8260D
11118120 22,02
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 5911
Analvte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]A
0.029
u
mg/kg dry
1
0.029
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
1,2-Dichlorobenzene [95-50-1]A
0.026
u
mg/kg dry
1
0.026
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
1,3-Dichlorobenzene [541-73-1]A
0.022
u
mg/kg dry
1
0.022
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
1,4-Dichlorobenzene [106-46-7]A
0.023
u
mg/kg dry
1
0.023
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
1-Methylnaphthalene [90-12-0]A
0.030
u
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2,4,5-Trichlorophenol[95-95-4]A
0.030
u
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2,4,6-Trichlorophenol[88-06-2]A
0.030
u
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2,4-Dichlorophenol [120-83-2]A
0.027
u
mg/kg dry
1
0.027
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2,4-Dimethylphenol [105-67-9]A
0.048
u
mg/kg dry
1
0.048
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2,4-Dinitrophenol [51-28-5]A
0.048
u
mg/kg dry
1
0.048
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2,4-Dinitrotoluene [121-14-2]A
0.031
u
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2,6-Dinitrotoluene [606-20-2]A
0.034
u
mg/kg dry
1
0.034
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2-Chloronaphthalene [91-58-7]A
0.031
u
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2-Chlorophenol [95-57-8]A
0.028
u
mg/kg dry
1
0.028
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]A
0.037
u
mg/kg dry
1
0.037
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM QV-01
2-Methylnaphthalene [91-57-6]A
0.031
u
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2-Methylphenol [95-48-7]A
0.028
u
mg/kg dry
1
0.028
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
2-Nitroaniline [88-74-4]A
0.033
U
mg/kg dry
1
0.033
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
FINAL
This report relates only to the
sample as received by the laboratory,
and may only
be reproduced in full.
Page 11 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-31-6" Lab Sample ID:CD18880-01 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 08:30 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.98
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]A
0.034
U
mg/kg
dry
1
0.034
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
U
mg/kg
dry
1
0.11
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
3-Nitroaniline [99-09-2]A
0.040
U
mg/kg
dry
1
0.040
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
4-Bromophenyl-phenylether[101-55-3]A
0.030
U
mg/kg
dry
1
0.030
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
4-Chloro-3-methylphenol[59-50-7]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
4-Chloroaniline [106-47-8]A
0.10
U
mg/kg
dry
1
0.10
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
4-Nitroaniline [100-01-6]A
0.059
U
mg/kg
dry
1
0.059
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
4-Nitrophenol [100-02-7]A
0.034
U
mg/kg
dry
1
0.034
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Acenaphthene [83-32-9]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Acenaphthylene [208-96-8]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Anthracene[120-12-7]A
0.042
U
mg/kg
dry
1
0.042
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Benzidine [92-87-5]A
0.12
U
mg/kg
dry
1
0.12
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Benzo(a)anthracene [56-55-3]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Benzo(a)pyrene [50-32-8]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Benzo(b)fluoranthene [205-99-2]A
0.020
U
mg/kg
dry
1
0.020
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.052
U
mg/kg
dry
1
0.052
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM QV-01
Benzo(k)fluoranthene [207-08-9]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Benzoic acid [65-85-O]A
1.4
J
mg/kg
dry
1
0.17
1.9
OK19001
EPA
8270E
11/23/20
15:12
DFM
Benzyl alcohol [100-51-6]A
0.026
U
mg/kg
dry
1
0.026
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.028
U
mg/kg
dry
1
0.028
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.048
U
mg/kg
dry
1
0.048
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.027
U
mg/kg
dry
1
0.027
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.039
U
mg/kg
dry
1
0.039
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Butylbenzylphthalate [85-68-7]A
0.044
U
mg/kg
dry
1
0.044
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Chrysene [218-01-9]A
0.033
U
mg/kg
dry
1
0.033
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.057
U
mg/kg
dry
1
0.057
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Dibenzofuran [132-64-9]A
0.030
U
mg/kg
dry
1
0.030
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Diethylphthalate [84-66-2]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Dimethylphthalate [131-11-3]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Di-n-butylphthalate [84-74-2]A
0.046
U
mg/kg
dry
1
0.046
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Di-n-octylphthalate [117-84-0]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Fluoranthene [206-44-0]A
0.040
U
mg/kg
dry
1
0.040
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Fluorene [86-73-7]A
0.032
U
mg/kg
dry
1
0.032
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Hexachlorobenzene [118-74-1]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Hexachlorobutadiene [87-68-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Hexachlorocyclopentadiene [77-47-4]A
0.043
U
mg/kg
dry
1
0.043
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Hexachloroethane [67-72-1]A
0.023
U
mg/kg
dry
1
0.023
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.052
U
mg/kg
dry
1
0.052
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Isophorone[78-59-1]A
0.033
U
mg/kg
dry
1
0.033
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Naphthalene [91-20-3]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
Nitrobenzene [98-95-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
N-Nitrosodimethylamine [62-75-9]A
0.023
U
mg/kg
dry
1
0.023
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.090
U
mg/kg
dry
1
0.090
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
N-nitrosodiphenylamine/Diphenylamine
0.060
U
mg/kg
dry
1
0.060
0.37
OK19001
EPA
8270E
11/23/20
15:12
DFM
[86-30-6/122-39-4]A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 107

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ANALYTICAL RESULTS
Description: HA-31-6" Lab Sample ID:CD18880-01 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 08:30 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.98
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.037
U
mg/kg dry
1
0.037
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
Phenanthrene[85-01-8]^
0.030
U
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
Phenol[108-95-2]^
0.024
U
mg/kg dry
1
0.024
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
Pyrene [129-00-0]^
0.042
U
mg/kg dry
1
0.042
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
Pyridine [110-86-1]^
0.091
U
mg/kg dry
1
0.091
0.37
OK19001
EPA 8270E
11/23/20 15:12
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,6-Tribromophenol
5.1
1
3.70
137 %
26-130
OK19001
EPA 8270E
11/23/2015:12
DFM
QS-03
2-Fluorobiphenyl
ZI
1
1.85
112 %
56-120
OK19001
EPA 8270E
1112312015:12
DFM
2-Fluorophenol
3.8
1
3.70
103 %
49-126
OK19001
EPA 8270E
1112312015:12
DFM
Nitrobenzene-d5
1.9
1
1.85
100 %
50-117
OK19001
EPA 8270E
11/23/2015:12
DFM
Phenol-d5
4.1
1
3.70
110 %
56-120
OK19001
EPA 8270E
11/23/2015:12
DFM
Terphenyl-d14
1.7
1
1.65
92 %
36-151
OK19001
EPA 8270E
11/23/2015:12
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
Lead [7439-92-1]^
695
D
mg/kg dry
5
0.667 2.78
OK20031
EPA 6010D
11/23/20 14:56
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
Lead [7439-92-1]^
10.7
mg/L
50
0.155 0.500
OL14039
EPA 6010D
12/15/20 12:15
JDH
Description: HA-31-18" Lab Sample ID:CD18880-02 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 08:35 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.23
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 6.34 mg/kg dry 1 0.141 0.587 OK30010 EPA 6010D 12/01/20 09:41 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-32-6" Lab Sample ID:CD18880-03 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 08:45 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.29
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00018
u
mg/kg
dry
1
0.00018
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,1,1-Trichloroethane [71-55-6]A
0.00028
u
mg/kg
dry
1
0.00028
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00022
u
mg/kg
dry
1
0.00022
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,1,2-Trichloroethane [79-00-5]A
0.00028
u
mg/kg
dry
1
0.00028
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,1-Dichloroethane [75-34-3]A
0.00028
u
mg/kg
dry
1
0.00028
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,1-Dichloroethene [75-35-4]A
0.00033
u
mg/kg
dry
1
0.00033
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,1-Dichloropropene [563-58-6]A
0.00018
u
mg/kg
dry
1
0.00018
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00031
u
mg/kg
dry
1
0.00031
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,2,3-Trichloropropane [96-18-4]A
0.00071
u
mg/kg
dry
1
0.00071
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00030
u
mg/kg
dry
1
0.00030
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00019
u
mg/kg
dry
1
0.00019
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00087
u
mg/kg
dry
1
0.00087
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,2-Dibromoethane [106-93-4]A
0.00051
u
mg/kg
dry
1
0.00051
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,2-Dichlorobenzene [95-50-1]A
0.00030
u
mg/kg
dry
1
0.00030
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,2-Dichloroethane [107-06-2]A
0.00045
u
mg/kg
dry
1
0.00045
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,2-Dichloropropane [78-87-5]A
0.00029
u
mg/kg
dry
1
0.00029
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00022
u
mg/kg
dry
1
0.00022
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,3-Dichlorobenzene [541-73-1]A
0.00024
u
mg/kg
dry
1
0.00024
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,3-Dichloropropane [142-28-9]A
0.00032
u
mg/kg
dry
1
0.00032
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
1,4-Dichlorobenzene [106-46-7]A
0.00022
u
mg/kg
dry
1
0.00022
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
2,2-Dichloropropane [594-20-7]A
0.00025
u
mg/kg
dry
1
0.00025
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
2-Butanone [78-93-3]A
0.00086
u
mg/kg
dry
1
0.00086
0.0055
OK18029
EPA
8260D
11/18/20
22:32
REF
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00018
u
mg/kg
dry
1
0.00018
0.0055
OK18029
EPA
8260D
11/18/20
22:32
REF
2-Chlorotoluene [95-49-8]A
0.00020
u
mg/kg
dry
1
0.00020
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
2-Hexanone [591-78-6]A
0.00083
u
mg/kg
dry
1
0.00083
0.0055
OK18029
EPA
8260D
11/18/20
22:32
REF
4-Chlorotoluene [106-43-4]A
0.00029
u
mg/kg
dry
1
0.00029
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
4-Isopropyltoluene [99-87-6]A
0.00018
u
mg/kg
dry
1
0.00018
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
4-Methyl-2-pentanone [108-10-1]A
0.00063
u
mg/kg
dry
1
0.00063
0.0055
OK18029
EPA
8260D
11/18/20
22:32
REF
Acetone [67-64-1]A
0.035
mg/kg
dry
1
0.016
0.022
OK18029
EPA
8260D
11/18/20
22:32
REF
Benzene [71-43-2]A
0.00019
u
mg/kg
dry
1
0.00019
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Bromobenzene [108-86-1]A
0.00024
u
mg/kg
dry
1
0.00024
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Bromochloromethane [74-97-5]A
0.00045
u
mg/kg
dry
1
0.00045
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Bromodichloromethane [75-27-4]A
0.00027
u
mg/kg
dry
1
0.00027
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Bromoform [75-25-2]A
0.00050
u
mg/kg
dry
1
0.00050
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Bromomethane [74-83-9]A
0.00035
u
mg/kg
dry
1
0.00035
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Carbon disulfide [75-15-0]A
0.00043
u
mg/kg
dry
1
0.00043
0.0055
OK18029
EPA
8260D
11/18/20
22:32
REF
Carbon Tetrachloride [56-23-5]A
0.00024
u
mg/kg
dry
1
0.00024
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Chlorobenzene [108-90-7]A
0.00019
u
mg/kg
dry
1
0.00019
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Chloroethane [75-00-3]A
0.00028
u
mg/kg
dry
1
0.00028
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Chloroform [67-66-3]A
0.00020
u
mg/kg
dry
1
0.00020
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Chloromethane [74-87-3]A
0.00023
u
mg/kg
dry
1
0.00023
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
cis-1,2-Dichloroethene [156-59-2]A
0.00025
u
mg/kg
dry
1
0.00025
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00019
u
mg/kg
dry
1
0.00019
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Dibromochloromethane [124-48-1]A
0.00039
u
mg/kg
dry
1
0.00039
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Dibromomethane [74-95-3]A
0.00037
u
mg/kg
dry
1
0.00037
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Dichlorodifluoromethane [75-71-8]A
0.00050
u
mg/kg
dry
1
0.00050
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
Ethylbenzene [100-41-4]A
0.00022
u
mg/kg
dry
1
0.00022
0.0011
OK18029
EPA
8260D
11/18/20
22:32
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 14 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-32-6 Lab Sample ID:CD18880-03 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 08:45 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.29
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Hexachlorobutadiene [87-68-3]^
0.00039
U
mg/kg
dry
1
0.00039
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
Isopropyl benzene [98-82-8]^
0.00017
U
mg/kg
dry
1
0.00017
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.00041
U
mg/kg
dry
1
0.00041
0.0022
OK18029
EPA 8260D
11/18/20
22:32
REF
Methylene Chloride [75-09-2]^
0.00081
U
mg/kg
dry
1
0.00081
0.0022
OK18029
EPA 8260D
11/18/20
22:32
REF
Methyl-tert-Butyl Ether [1634-04-4]^
0.00033
U
mg/kg
dry
1
0.00033
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
Naphthalene [91-20-3]^
0.00030
U
mg/kg
dry
1
0.00030
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
n-Butyl Benzene [104-51-8]^
0.00014
U
mg/kg
dry
1
0.00014
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
n-Propyl Benzene [103-65-1]^
0.00020
U
mg/kg
dry
1
0.00020
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
o-Xylene [95-47-6]^
0.00024
U
mg/kg
dry
1
0.00024
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
sec-Butylbenzene [135-98-8]^
0.0011
U
mg/kg
dry
1
0.0011
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
Styrene [100-42-5]^
0.0011
U
mg/kg
dry
1
0.0011
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
tert-Butylbenzene [98-06-6]^
0.00019
U
mg/kg
dry
1
0.00019
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
Tetrachloroethene [127-18-4]^
0.00031
U
mg/kg
dry
1
0.00031
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
Toluene [108-88-3]^
0.00027
U
mg/kg
dry
1
0.00027
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
trans-1,2-Dichloroethene [156-60-5]^
0.00041
U
mg/kg
dry
1
0.00041
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.00043
U
mg/kg
dry
1
0.00043
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
Trichloroethene [79-01-6]^
0.00035
U
mg/kg
dry
1
0.00035
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
Trichlorofluoromethane [75-69-4]^
0.00029
U
mg/kg
dry
1
0.00029
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
Vinyl chloride [75-01-4]^
0.00027
U
mg/kg
dry
1
0.00027
0.0011
OK18029
EPA 8260D
11/18/20
22:32
REF
Xylenes (Total) [1330-20-7]^
0.00062
U
mg/kg
dry
1
0.00062
0.0033
OK18029
EPA 8260D
11/18/20
22:32
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
31
1
50.0
61 %
50-127
OK18029
EPA 6260D
11118120 22:32
REF
Dlbromofluoromethane
38
1
50.0
76 %
52-128
OK18029
EPA 8260D
11116120 22:32
REF
Toluene-d8
36
1
50.0
72 %
57-124
OK18029
EPA 8260D
11/I6120 22:32
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.029
U
mg/kg dry
1
0.029
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
1,2-Dichlorobenzene [95-50-1]^
0.025
U
mg/kg dry
1
0.025
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
1,3-Dichlorobenzene [541-73-1]^
0.022
U
mg/kg dry
1
0.022
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
1,4-Dichlorobenzene [106-46-7]^
0.023
U
mg/kg dry
1
0.023
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
1- Methyl naphthalene [90-12-0]^
0.030
U
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2,4,5-Trichlorophenol[95-95-4]^
0.030
U
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2,4,6-Trichlorophenol[88-06-2]^
0.030
U
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2,4-Dichlorophenol [120-83-2]^
0.027
U
mg/kg dry
1
0.027
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2,4-Di methyl phenol [105-67-9]^
0.048
U
mg/kg dry
1
0.048
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2,4-Dinitrophenol [51-28-5]^
0.048
U
mg/kg dry
1
0.048
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2,4-Dinitrotoluene [121-14-2]^
0.031
U
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2,6-Dinitrotoluene [606-20-2]^
0.034
U
mg/kg dry
1
0.034
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2-Chloronaphthalene [91-58-7]^
0.031
U
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2-Chlorophenol [95-57-8]^
0.028
U
mg/kg dry
1
0.028
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
0.037
U
mg/kg dry
1
0.037
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM QV-01
2- Methyl naphthalene [91-57-6]^
0.031
U
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2-Methylphenol [95-48-7]^
0.028
U
mg/kg dry
1
0.028
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
2-Nitroaniline [88-74-4]^
0.033
U
mg/kg dry
1
0.033
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
FINAL
This report relates only
to the
sample as received by the laboratory,
and may only
be reproduced in full.
Page 15 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-32-6" Lab Sample ID:CD18880-03 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 08:45 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.29
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]A
0.034
U
mg/kg
dry
1
0.034
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
U
mg/kg
dry
1
0.11
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
3-Nitroaniline [99-09-2]A
0.040
U
mg/kg
dry
1
0.040
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.030
U
mg/kg
dry
1
0.030
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
4-Chloroaniline [106-47-8]A
0.10
U
mg/kg
dry
1
0.10
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
4-Nitroaniline [100-01-6]A
0.059
U
mg/kg
dry
1
0.059
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
4-Nitrophenol [100-02-7]A
0.034
U
mg/kg
dry
1
0.034
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Acenaphthene [83-32-9]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Acenaphthylene [208-96-8]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Anthracene[120-12-7]A
0.042
U
mg/kg
dry
1
0.042
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Benzidine [92-87-5]A
0.12
U
mg/kg
dry
1
0.12
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Benzo(a)anthracene [56-55-3]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Benzo(a)pyrene [50-32-8]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Benzo(b)fluoranthene [205-99-2]A
0.020
U
mg/kg
dry
1
0.020
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.052
U
mg/kg
dry
1
0.052
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM QV-01
Benzo(k)fluoranthene [207-08-9]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Benzoic acid [65-85-0]A
0.17
U
mg/kg
dry
1
0.17
1.9
OK19001
EPA
8270E
11/23/20
15:44
DFM
Benzyl alcohol [100-51-6]A
0.025
U
mg/kg
dry
1
0.025
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.028
U
mg/kg
dry
1
0.028
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.048
U
mg/kg
dry
1
0.048
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.027
U
mg/kg
dry
1
0.027
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.039
U
mg/kg
dry
1
0.039
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Butylbenzylphthalate [85-68-7]A
0.044
U
mg/kg
dry
1
0.044
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Chrysene [218-01-9]A
0.033
U
mg/kg
dry
1
0.033
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.056
U
mg/kg
dry
1
0.056
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Dibenzofuran [132-64-9]A
0.030
U
mg/kg
dry
1
0.030
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Diethylphthalate [84-66-2]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Dimethylphthalate [131-11-3]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Di-n-butylphthalate [84-74-2]A
0.045
U
mg/kg
dry
1
0.045
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Di-n-octylphthalate [117-84-0]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Fluoranthene [206-44-0]A
0.040
U
mg/kg
dry
1
0.040
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Fluorene [86-73-7]A
0.032
U
mg/kg
dry
1
0.032
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Hexachlorobenzene [118-74-1]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Hexachlorobutadiene [87-68-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Hexachlorocyclopentadiene [77-47-4]A
0.043
U
mg/kg
dry
1
0.043
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Hexachloroethane [67-72-1]A
0.023
U
mg/kg
dry
1
0.023
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.052
U
mg/kg
dry
1
0.052
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Isophorone[78-59-1]A
0.033
U
mg/kg
dry
1
0.033
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Naphthalene [91-20-3]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
Nitrobenzene [98-95-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
N-Nitrosodimethylamine [62-75-9]A
0.023
U
mg/kg
dry
1
0.023
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.090
U
mg/kg
dry
1
0.090
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
N-nitrosodiphenylamine/Diphenylamine
0.060
U
mg/kg
dry
1
0.060
0.37
OK19001
EPA
8270E
11/23/20
15:44
DFM
[86-30-6/122-39-4]A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-32-6 Lab Sample ID:CD18880-03 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 08:45 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.29
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.037
U
mg/kg dry
1
0.037
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
Phenanthrene[85-01-8]^
0.030
U
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
Phenol[108-95-2]^
0.024
U
mg/kg dry
1
0.024
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
Pyrene [129-00-0]^
0.042
U
mg/kg dry
1
0.042
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
Pyridine [110-86-1]^
0.091
U
mg/kg dry
1
0.091
0.37
OK19001
EPA 8270E
11/23/20 15:44
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.6
1
3.69
125 %
26-130
OK19001
EPA 8270E
11/23/2015:44
DFM
2-Fluorobiphenyl
1.9
1
1.85
105 %
56-120
OK19001
EPA 8270E
1112312015:44
DFM
2-Fluorophenol
3.7
1
3.69
99 %
49-126
OK19001
EPA 8270E
1112312015:44
DFM
Nitrobenzene-d5
1.7
1
1.85
94 %
50-117
OK19001
EPA 8270E
11/23/2015:44
DFM
Phenol-d5
4.1
1
3.69
110 %
56-120
OK19001
EPA 8270E
1112312015:44
DFM
Terphenyl-d14
1.5
1
1.65
79 %
36-151
OK19001
EPA 8270E
1112312015:44
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]1
14.2
mg/kg dry
1
0.133 0.554
OK20031
EPA 6010D
11/23/20 14:58
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-33-6" Lab Sample ID:CD18880-05 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:05 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.78
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00015
u
mg/kg
dry
0.828
0.00015
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,1,1-Trichloroethane [71-55-6]A
0.00024
u
mg/kg
dry
0.828
0.00024
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00019
u
mg/kg
dry
0.828
0.00019
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,1,2-Trichloroethane [79-00-5]A
0.00024
u
mg/kg
dry
0.828
0.00024
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,1-Dichloroethane [75-34-3]A
0.00024
u
mg/kg
dry
0.828
0.00024
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,1-Dichloroethene [75-35-4]A
0.00028
u
mg/kg
dry
0.828
0.00028
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,1-Dichloropropene [563-58-6]A
0.00015
u
mg/kg
dry
0.828
0.00015
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00026
u
mg/kg
dry
0.828
0.00026
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,2,3-Trichloropropane [96-18-4]A
0.00060
u
mg/kg
dry
0.828
0.00060
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00025
u
mg/kg
dry
0.828
0.00025
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00016
u
mg/kg
dry
0.828
0.00016
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00074
u
mg/kg
dry
0.828
0.00074
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,2-Dibromoethane [106-93-4]A
0.00043
u
mg/kg
dry
0.828
0.00043
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,2-Dichlorobenzene [95-50-1]A
0.00025
u
mg/kg
dry
0.828
0.00025
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,2-Dichloroethane [107-06-2]A
0.00039
u
mg/kg
dry
0.828
0.00039
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,2-Dichloropropane [78-87-5]A
0.00025
u
mg/kg
dry
0.828
0.00025
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00019
u
mg/kg
dry
0.828
0.00019
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,3-Dichlorobenzene [541-73-1]A
0.00021
u
mg/kg
dry
0.828
0.00021
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,3-Dichloropropane [142-28-9]A
0.00027
u
mg/kg
dry
0.828
0.00027
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
1,4-Dichlorobenzene [106-46-7]A
0.00019
u
mg/kg
dry
0.828
0.00019
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
2,2-Dichloropropane [594-20-7]A
0.00022
u
mg/kg
dry
0.828
0.00022
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
2-Butanone [78-93-3]A
0.00074
u
mg/kg
dry
0.828
0.00074
0.0047
OK18029
EPA
8260D
11/18/20
23:02
REF
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00015
u
mg/kg
dry
0.828
0.00015
0.0047
OK18029
EPA
8260D
11/18/20
23:02
REF
2-Chlorotoluene [95-49-8]A
0.00017
u
mg/kg
dry
0.828
0.00017
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
2-Hexanone [591-78-6]A
0.00071
u
mg/kg
dry
0.828
0.00071
0.0047
OK18029
EPA
8260D
11/18/20
23:02
REF
4-Chlorotoluene [106-43-4]A
0.00025
u
mg/kg
dry
0.828
0.00025
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
4-Isopropyltoluene [99-87-6]A
0.00015
u
mg/kg
dry
0.828
0.00015
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
4-Methyl-2-pentanone [108-10-1]A
0.00054
u
mg/kg
dry
0.828
0.00054
0.0047
OK18029
EPA
8260D
11/18/20
23:02
REF
Acetone [67-64-1]A
0.013
u
mg/kg
dry
0.828
0.013
0.019
OK18029
EPA
8260D
11/18/20
23:02
REF
Benzene [71-43-2]A
0.00016
u
mg/kg
dry
0.828
0.00016
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Bromobenzene [108-86-1]A
0.00021
u
mg/kg
dry
0.828
0.00021
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Bromochloromethane [74-97-5]A
0.00039
u
mg/kg
dry
0.828
0.00039
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Bromodichloromethane [75-27-4]A
0.00023
u
mg/kg
dry
0.828
0.00023
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Bromoform [75-25-2]A
0.00042
u
mg/kg
dry
0.828
0.00042
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Bromomethane [74-83-9]A
0.00030
u
mg/kg
dry
0.828
0.00030
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Carbon disulfide [75-15-0]A
0.00037
u
mg/kg
dry
0.828
0.00037
0.0047
OK18029
EPA
8260D
11/18/20
23:02
REF
Carbon Tetrachloride [56-23-5]A
0.00021
u
mg/kg
dry
0.828
0.00021
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Chlorobenzene [108-90-7]A
0.00016
u
mg/kg
dry
0.828
0.00016
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Chloroethane [75-00-3]A
0.00024
u
mg/kg
dry
0.828
0.00024
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Chloroform [67-66-3]A
0.00017
u
mg/kg
dry
0.828
0.00017
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Chloromethane [74-87-3]A
0.00020
u
mg/kg
dry
0.828
0.00020
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
cis-1,2-Dichloroethene [156-59-2]A
0.00022
u
mg/kg
dry
0.828
0.00022
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00016
u
mg/kg
dry
0.828
0.00016
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Dibromochloromethane [124-48-1]A
0.00033
u
mg/kg
dry
0.828
0.00033
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Dibromomethane [74-95-3]A
0.00031
u
mg/kg
dry
0.828
0.00031
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Dichlorodifluoromethane [75-71-8]A
0.00042
u
mg/kg
dry
0.828
0.00042
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
Ethylbenzene [100-41-4]A
0.00019
u
mg/kg
dry
0.828
0.00019
0.00094
OK18029
EPA
8260D
11/18/20
23:02
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 18 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-33-6 Lab Sample ID:CD18880-05 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:05 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.78
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Hexachlorobutadiene [87-68-3]^
0.00033
U
mg/kg
dry
0.828
0.00033
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
Isopropyl benzene [98-82-8]^
0.00014
U
mg/kg
dry
0.828
0.00014
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.00035
U
mg/kg
dry
0.828
0.00035
0.0019
OK18029
EPA 8260D
11/18/20
23:02
REF
Methylene Chloride [75-09-2]^
0.00069
U
mg/kg
dry
0.828
0.00069
0.0019
OK18029
EPA 8260D
11/18/20
23:02
REF
Methyl-tert-Butyl Ether [1634-04-4]^
0.00028
U
mg/kg
dry
0.828
0.00028
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
Naphthalene [91-20-3]^
0.00025
U
mg/kg
dry
0.828
0.00025
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
n-Butyl Benzene [104-51-8]^
0.00012
U
mg/kg
dry
0.828
0.00012
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
n-Propyl Benzene [103-65-1]^
0.00017
U
mg/kg
dry
0.828
0.00017
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
o-Xylene [95-47-6]^
0.00021
U
mg/kg
dry
0.828
0.00021
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
sec-Butylbenzene [135-98-8]^
0.00090
U
mg/kg
dry
0.828
0.00090
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
Styrene [100-42-5]^
0.00092
U
mg/kg
dry
0.828
0.00092
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
tert-Butylbenzene [98-06-6]^
0.00016
U
mg/kg
dry
0.828
0.00016
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
Tetrachloroethene [127-18-4]^
0.00026
U
mg/kg
dry
0.828
0.00026
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
Toluene [108-88-3]^
0.00023
U
mg/kg
dry
0.828
0.00023
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
trans-1,2-Dichloroethene [156-60-5]^
0.00035
U
mg/kg
dry
0.828
0.00035
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.00037
U
mg/kg
dry
0.828
0.00037
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
Trichloroethene [79-01-6]^
0.00030
U
mg/kg
dry
0.828
0.00030
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
Trichlorofluoromethane [75-69-4]^
0.00025
U
mg/kg
dry
0.828
0.00025
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
Vinyl chloride [75-01-4]^
0.00023
U
mg/kg
dry
0.828
0.00023
0.00094
OK18029
EPA 8260D
11/18/20
23:02
REF
Xylenes (Total) [1330-20-7]^
0.00053
U
mg/kg
dry
0.828
0.00053
0.0028
OK18029
EPA 8260D
11/18/20
23:02
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
30
0.828
50.0
60 %
50-127
OK18029
EPA 6260D
11118120 23:02
REF
Dlbromofluoromethane
38
0.828
50.0
75 %
52-128
OK18029
EPA 8260D
11116120 23:02
REF
Toluene-d8
38
0.828
50.0
76 %
57-124
OK18029
EPA 8260D
11/I6120 23:02
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.030
U
mg/kg dry
1
0.030
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
1,2-Dichlorobenzene [95-50-1]^
0.026
U
mg/kg dry
1
0.026
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
1,3-Dichlorobenzene [541-73-1]^
0.023
U
mg/kg dry
1
0.023
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
1,4-Dichlorobenzene [106-46-7]^
0.024
U
mg/kg dry
1
0.024
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
1- Methyl naphthalene [90-12-0]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2,4,5-Trichlorophenol[95-95-4]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2,4,6-Trichlorophenol[88-06-2]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2,4-Dichlorophenol [120-83-2]^
0.027
U
mg/kg dry
1
0.027
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2,4-Di methyl phenol[105-67-9]^
0.049
U
mg/kg dry
1
0.049
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2,4-Dinitrophenol[51-28-5]^
0.049
U
mg/kg dry
1
0.049
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2,4-Dinitrotoluene [121-14-2]^
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2,6-Dinitrotoluene [606-20-2]^
0.035
U
mg/kg dry
1
0.035
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2-Chloronaphthalene [91-58-7]^
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2-Chlorophenol [95-57-8]^
0.028
U
mg/kg dry
1
0.028
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM QV-01
2- Methyl naphthalene [91-57-6]^
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2-Methylphenol[95-48-7]^
0.028
U
mg/kg dry
1
0.028
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
2-Nitroaniline [88-74-4]^
0.034
U
mg/kg dry
1
0.034
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 19 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-33-6" Lab Sample ID:CD18880-05 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:05 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.78
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]A
0.035
U
mg/kg
dry
1
0.035
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
U
mg/kg
dry
1
0.11
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
3-Nitroaniline [99-09-2]A
0.041
U
mg/kg
dry
1
0.041
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
4-Bromophenyl-phenylether[101-55-3]A
0.031
U
mg/kg
dry
1
0.031
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
4-Chloro-3-methylphenol[59-50-7]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
4-Chloroaniline [106-47-8]A
0.11
U
mg/kg
dry
1
0.11
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
4-Nitroaniline [100-01-6]A
0.060
U
mg/kg
dry
1
0.060
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
4-Nitrophenol [100-02-7]A
0.035
U
mg/kg
dry
1
0.035
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Acenaphthene [83-32-9]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Acenaphthylene [208-96-8]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Anthracene[120-12-7]A
0.043
U
mg/kg
dry
1
0.043
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Benzidine [92-87-5]A
0.13
U
mg/kg
dry
1
0.13
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Benzo(a)anthracene [56-55-3]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Benzo(a)pyrene [50-32-8]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Benzo(b)fluoranthene [205-99-2]A
0.021
U
mg/kg
dry
1
0.021
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.054
U
mg/kg
dry
1
0.054
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM QV-01
Benzo(k)fluoranthene [207-08-9]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Benzoic acid [65-85-O]A
0.43
J
mg/kg
dry
1
0.17
1.9
OK19001
EPA
8270E
11/23/20
16:15
DFM
Benzyl alcohol [100-51-6]A
0.026
U
mg/kg
dry
1
0.026
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.028
U
mg/kg
dry
1
0.028
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.049
U
mg/kg
dry
1
0.049
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.027
U
mg/kg
dry
1
0.027
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.040
U
mg/kg
dry
1
0.040
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Butylbenzylphthalate [85-68-7]A
0.046
U
mg/kg
dry
1
0.046
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Chrysene [218-01-9]A
0.034
U
mg/kg
dry
1
0.034
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.058
U
mg/kg
dry
1
0.058
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Dibenzofuran [132-64-9]A
0.031
U
mg/kg
dry
1
0.031
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Diethylphthalate [84-66-2]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Dimethylphthalate [131-11-3]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Di-n-butylphthalate [84-74-2]A
0.047
U
mg/kg
dry
1
0.047
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Di-n-octylphthalate [117-84-O]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Fluoranthene [206-44-O]A
0.041
U
mg/kg
dry
1
0.041
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Fluorene [86-73-7]A
0.033
U
mg/kg
dry
1
0.033
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Hexachlorobenzene [118-74-1]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Hexachlorobutadiene [87-68-3]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Hexachlorocyclopentadiene [77-47-4]A
0.044
U
mg/kg
dry
1
0.044
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Hexachloroethane [67-72-1]A
0.024
U
mg/kg
dry
1
0.024
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.054
U
mg/kg
dry
1
0.054
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Isophorone[78-59-1]A
0.034
U
mg/kg
dry
1
0.034
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Naphthalene [91-20-3]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
Nitrobenzene [98-95-3]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
N-Nitrosodimethylamine [62-75-9]A
0.024
U
mg/kg
dry
1
0.024
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.092
U
mg/kg
dry
1
0.092
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
N-nitrosodiphenylamine/Diphenylamine
0.062
U
mg/kg
dry
1
0.062
0.38
OK19001
EPA
8270E
11/23/20
16:15
DFM
[86-30-6/122-39-4]A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 107

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ANALYTICAL RESULTS
Description: HA-33-6 Lab Sample ID:CD18880-05 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:05 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.78
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
Phenanthrene[85-01-8]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
Phenol[108-95-2]^
0.025
U
mg/kg dry
1
0.025
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
Pyrene [129-00-0]^
0.043
U
mg/kg dry
1
0.043
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
Pyridine [110-86-1]^
0.093
U
mg/kg dry
1
0.093
0.38
OK19001
EPA 8270E
11/23/20 16:15
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.7
1
3.80
123 %
26-130
OK19001
EPA 8270E
11/23/2016:15
DFM
2-Fluorobiphenyl
1.9
1
1.90
99 %
56-120
OK19001
EPA 8270E
11123120 16:15
DFM
2-Fluorophenol
3.7
1
3.80
98 %
49-126
OK19001
EPA 8270E
11123120 16:15
DFM
Nitrobenzene-d5
I.8
1
1.90
97 %
50-117
OK19001
EPA 8270E
11/23/2016:15
DFM
Phenol-d5
4.1
1
3.80
107 %
56-120
OK19001
EPA 8270E
11/23/2016:15
DFM
Terphenyl-d14
1.6
1
1.90
84 %
36-151
OK19001
EPA 8270E
11123120 16:15
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]1
13.7
mg/kg dry
1
0.137 0.570
OK20031
EPA 6010D
11/23/20 14:59
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-34-6" Lab Sample ID:CD18880-07 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:25 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.31
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00014
u
mg/kg
dry
0.751
0.00014
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,1,1-Trichloroethane [71-55-6]A
0.00021
u
mg/kg
dry
0.751
0.00021
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00017
u
mg/kg
dry
0.751
0.00017
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,1,2-Trichloroethane [79-00-5]A
0.00021
u
mg/kg
dry
0.751
0.00021
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,1-Dichloroethane [75-34-3]A
0.00021
u
mg/kg
dry
0.751
0.00021
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,1-Dichloroethene [75-35-4]A
0.00026
u
mg/kg
dry
0.751
0.00026
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,1-Dichloropropene [563-58-6]A
0.00014
u
mg/kg
dry
0.751
0.00014
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00024
u
mg/kg
dry
0.751
0.00024
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,2,3-Trichloropropane [96-18-4]A
0.00055
u
mg/kg
dry
0.751
0.00055
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00023
u
mg/kg
dry
0.751
0.00023
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00015
u
mg/kg
dry
0.751
0.00015
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00068
u
mg/kg
dry
0.751
0.00068
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,2-Dibromoethane [106-93-4]A
0.00040
u
mg/kg
dry
0.751
0.00040
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,2-Dichlorobenzene [95-50-1]A
0.00023
u
mg/kg
dry
0.751
0.00023
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,2-Dichloroethane [107-06-2]A
0.00035
u
mg/kg
dry
0.751
0.00035
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,2-Dichloropropane [78-87-5]A
0.00022
u
mg/kg
dry
0.751
0.00022
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00017
u
mg/kg
dry
0.751
0.00017
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,3-Dichlorobenzene [541-73-1]A
0.00019
u
mg/kg
dry
0.751
0.00019
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,3-Dichloropropane [142-28-9]A
0.00025
u
mg/kg
dry
0.751
0.00025
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
1,4-Dichlorobenzene [106-46-7]A
0.00017
u
mg/kg
dry
0.751
0.00017
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
2,2-Dichloropropane [594-20-7]A
0.00020
u
mg/kg
dry
0.751
0.00020
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
2-Butanone [78-93-3]A
0.00067
u
mg/kg
dry
0.751
0.00067
0.0043
OK18029
EPA
8260D
11/18/20
23:32
REF
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00014
u
mg/kg
dry
0.751
0.00014
0.0043
OK18029
EPA
8260D
11/18/20
23:32
REF
2-Chlorotoluene [95-49-8]A
0.00015
u
mg/kg
dry
0.751
0.00015
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
2-Hexanone [591-78-6]A
0.00064
u
mg/kg
dry
0.751
0.00064
0.0043
OK18029
EPA
8260D
11/18/20
23:32
REF
4-Chlorotoluene [106-43-4]A
0.00022
u
mg/kg
dry
0.751
0.00022
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
4-Isopropyltoluene [99-87-6]A
0.00014
u
mg/kg
dry
0.751
0.00014
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
4-Methyl-2-pentanone [108-10-1]A
0.00049
u
mg/kg
dry
0.751
0.00049
0.0043
OK18029
EPA
8260D
11/18/20
23:32
REF
Acetone [67-64-1]A
0.012
u
mg/kg
dry
0.751
0.012
0.017
OK18029
EPA
8260D
11/18/20
23:32
REF
Benzene [71-43-2]A
0.00015
u
mg/kg
dry
0.751
0.00015
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Bromobenzene [108-86-1]A
0.00019
u
mg/kg
dry
0.751
0.00019
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Bromochloromethane [74-97-5]A
0.00035
u
mg/kg
dry
0.751
0.00035
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Bromodichloromethane [75-27-4]A
0.00021
u
mg/kg
dry
0.751
0.00021
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Bromoform [75-25-2]A
0.00039
u
mg/kg
dry
0.751
0.00039
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Bromomethane [74-83-9]A
0.00028
u
mg/kg
dry
0.751
0.00028
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Carbon disulfide [75-15-0]A
0.00034
u
mg/kg
dry
0.751
0.00034
0.0043
OK18029
EPA
8260D
11/18/20
23:32
REF
Carbon Tetrachloride [56-23-5]A
0.00019
u
mg/kg
dry
0.751
0.00019
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Chlorobenzene [108-90-7]A
0.00015
u
mg/kg
dry
0.751
0.00015
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Chloroethane [75-00-3]A
0.00021
u
mg/kg
dry
0.751
0.00021
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Chloroform [67-66-3]A
0.00015
u
mg/kg
dry
0.751
0.00015
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Chloromethane [74-87-3]A
0.00018
u
mg/kg
dry
0.751
0.00018
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
cis-1,2-Dichloroethene [156-59-2]A
0.00020
u
mg/kg
dry
0.751
0.00020
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00015
u
mg/kg
dry
0.751
0.00015
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Dibromochloromethane [124-48-1]A
0.00030
u
mg/kg
dry
0.751
0.00030
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Dibromomethane [74-95-3]A
0.00028
u
mg/kg
dry
0.751
0.00028
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Dichlorodifluoromethane [75-71-8]A
0.00039
u
mg/kg
dry
0.751
0.00039
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
Ethylbenzene [100-41-4]A
0.00017
u
mg/kg
dry
0.751
0.00017
0.00086
OK18029
EPA
8260D
11/18/20
23:32
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 22 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-34-6 Lab Sample ID:CD18880-07 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:25 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.31
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Hexachlorobutadiene [87-68-3]^
0.00030
U
mg/kg
dry
0.751
0.00030
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
Isopropyl benzene [98-82-8]^
0.00013
U
mg/kg
dry
0.751
0.00013
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.00032
U
mg/kg
dry
0.751
0.00032
0.0017
OK18029
EPA 8260D
11/18/20
23:32
REF
Methylene Chloride [75-09-2]^
0.00063
U
mg/kg
dry
0.751
0.00063
0.0017
OK18029
EPA 8260D
11/18/20
23:32
REF
Methyl-tert-Butyl Ether [1634-04-4]^
0.00026
U
mg/kg
dry
0.751
0.00026
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
Naphthalene [91-20-3]^
0.00023
U
mg/kg
dry
0.751
0.00023
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
n-Butyl Benzene [104-51-8]^
0.00011
U
mg/kg
dry
0.751
0.00011
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
n-Propyl Benzene [103-65-1]^
0.00015
U
mg/kg
dry
0.751
0.00015
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
o-Xylene [95-47-6]^
0.00019
U
mg/kg
dry
0.751
0.00019
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
sec-Butylbenzene [135-98-8]^
0.00082
U
mg/kg
dry
0.751
0.00082
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
Styrene [100-42-5]^
0.00084
U
mg/kg
dry
0.751
0.00084
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
tert-Butylbenzene [98-06-6]^
0.00015
U
mg/kg
dry
0.751
0.00015
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
Tetrachloroethene [127-18-4]^
0.00024
U
mg/kg
dry
0.751
0.00024
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
Toluene [108-88-3]^
0.00021
U
mg/kg
dry
0.751
0.00021
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
trans-1,2-Dichloroethene [156-60-5]^
0.00032
U
mg/kg
dry
0.751
0.00032
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.00034
U
mg/kg
dry
0.751
0.00034
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
Trichloroethene [79-01-6]^
0.00028
U
mg/kg
dry
0.751
0.00028
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
Trichlorofluoromethane [75-69-4]^
0.00022
U
mg/kg
dry
0.751
0.00022
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
Vinyl chloride [75-01-4]^
0.00021
U
mg/kg
dry
0.751
0.00021
0.00086
OK18029
EPA 8260D
11/18/20
23:32
REF
Xylenes (Total) [1330-20-7]^
0.00048
U
mg/kg
dry
0.751
0.00048
0.0026
OK18029
EPA 8260D
11/18/20
23:32
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
30
0.751
50.0
60 %
50-127
OK18029
EPA 6260D
11118120 23:32
REF
Dlbromofluoromethane
37
0.751
50.0
73 %
52-128
OK18029
EPA 8260D
11116120 23:32
REF
Toluene-d8
36
0.751
50.0
72 %
57-124
OK18029
EPA 8260D
11/I6120 23:32
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.030
U
mg/kg dry
1
0.030
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
1,2-Dichlorobenzene [95-50-1]^
0.026
U
mg/kg dry
1
0.026
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
1,3-Dichlorobenzene [541-73-1]^
0.023
U
mg/kg dry
1
0.023
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
1,4-Dichlorobenzene [106-46-7]^
0.024
U
mg/kg dry
1
0.024
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
1- Methyl naphthalene [90-12-0]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2,4,5-Trichlorophenol[95-95-4]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2,4,6-Trichlorophenol[88-06-2]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2,4-Dichlorophenol [120-83-2]^
0.027
U
mg/kg dry
1
0.027
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2,4-Di methyl phenol[105-67-9]^
0.049
U
mg/kg dry
1
0.049
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2,4-Dinitrophenol[51-28-5]^
0.049
U
mg/kg dry
1
0.049
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2,4-Dinitrotoluene [121-14-2]^
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2,6-Dinitrotoluene [606-20-2]^
0.036
U
mg/kg dry
1
0.036
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2-Chloronaphthalene [91-58-7]^
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2-Chlorophenol [95-57-8]^
0.029
U
mg/kg dry
1
0.029
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM QV-01
2- Methyl naphthalene [91-57-6]^
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2-Methylphenol[95-48-7]^
0.029
U
mg/kg dry
1
0.029
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
2-Nitroaniline [88-74-4]^
0.034
U
mg/kg dry
1
0.034
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 23 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-34-6" Lab Sample ID:CD18880-07 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:25 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.31
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]A
0.036
U
mg/kg dry
1
0.036
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.030
U
mg/kg dry
1
0.030
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
U
mg/kg dry
1
0.11
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
3-Nitroaniline [99-09-2]A
0.041
U
mg/kg dry
1
0.041
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
4-Chloroaniline [106-47-8]A
0.11
U
mg/kg dry
1
0.11
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.030
U
mg/kg dry
1
0.030
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
4-Nitroaniline [100-01-6]A
0.061
U
mg/kg dry
1
0.061
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
4-Nitrophenol [100-02-7]A
0.036
U
mg/kg dry
1
0.036
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Acenaphthene [83-32-9]A
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Acenaphthylene [208-96-8]A
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Anthracene[120-12-7]A
0.044
U
mg/kg dry
1
0.044
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Benzidine [92-87-5]A
0.13
U
mg/kg dry
1
0.13
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Benzo(a)anthracene [56-55-3]A
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Benzo(a)pyrene[50-32-8]A
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Benzo(b)fluoranthene [205-99-2]A
0.021
U
mg/kg dry
1
0.021
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.054
U
mg/kg dry
1
0.054
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM QV-01
Benzo(k)fluoranthene [207-08-9]A
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Benzoic acid [65-85-0]A
0.17
U
mg/kg dry
1
0.17
1.9
OK19001
EPA 8270E
11/23/20 16:47
DFM
Benzyl alcohol [100-51-6]A
0.026
U
mg/kg dry
1
0.026
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.029
U
mg/kg dry
1
0.029
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.049
U
mg/kg dry
1
0.049
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.027
U
mg/kg dry
1
0.027
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.040
U
mg/kg dry
1
0.040
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Butylbenzylphthalate [85-68-7]A
0.046
U
mg/kg dry
1
0.046
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Chrysene [218-01-9]A
0.034
U
mg/kg dry
1
0.034
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.058
U
mg/kg dry
1
0.058
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Dibenzofuran [132-64-9]A
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Diethylphthalate [84-66-2]A
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Dimethylphthalate [131-11-3]A
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Di-n-butylphthalate [84-74-2]A
0.047
U
mg/kg dry
1
0.047
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Di-n-octylphthalate [117-84-0]A
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Fluoranthene [206-44-0]A
0.041
U
mg/kg dry
1
0.041
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Fluorene [86-73-7]A
0.033
U
mg/kg dry
1
0.033
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Hexachlorobenzene [118-74-1]A
0.030
U
mg/kg dry
1
0.030
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Hexachlorobutadiene [87-68-3]A
0.030
U
mg/kg dry
1
0.030
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Hexachlorocyclopentadiene [77-47-4]A
0.045
U
mg/kg dry
1
0.045
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Hexachloroethane [67-72-1]A
0.024
U
mg/kg dry
1
0.024
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.054
U
mg/kg dry
1
0.054
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Isophorone[78-59-1]A
0.034
U
mg/kg dry
1
0.034
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Naphthalene [91-20-3]A
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Nitrobenzene [98-95-3]A
0.030
U
mg/kg dry
1
0.030
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
N-Nitrosodimethylamine [62-75-9]A
0.024
U
mg/kg dry
1
0.024
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.093
U
mg/kg dry
1
0.093
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
N-nitrosodiphenylamine/Diphenylamine
0.062
U
mg/kg dry
1
0.062
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
86-30-6/122-39-4]A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-34-6 Lab Sample ID:CD18880-07 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:25 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.31
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Phenanthrene[85-01-8]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Phenol[108-95-2]^
0.025
U
mg/kg dry
1
0.025
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Pyrene [129-00-0]^
0.044
U
mg/kg dry
1
0.044
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Pyridine [110-86-1]^
0.094
U
mg/kg dry
1
0.094
0.38
OK19001
EPA 8270E
11/23/20 16:47
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.3
1
3.82
114 %
26-130
OK19001
EPA 8270E
11/23/2016:47
DFM
2-Fluorobiphenyl
20
1
1.91
104 %
56-120
OK19001
EPA 8270E
11123120 16:47
DFM
2-Fluorophenol
3.8
1
3.82
99 %
49-126
OK19001
EPA 8270E
11123120 16:47
DFM
Nitrobenzene-d5
I.8
1
1.91
96 %
50-117
OK19001
EPA 8270E
11/23/2016:47
DFM
Phenol-d5
4.0
1
3.82
105 %
56-120
OK19001
EPA 8270E
11/23/2016:47
DFM
Terphenyl-d14
1.7
1
1.91
90 %
36-151
OK19001
EPA 8270E
11123120 16:47
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]1
7.07
mg/kg dry
1
0.137 0.573
OK20031
EPA 6010D
11/23/20 15:01
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-35-6" Lab Sample ID:CD18880-09 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 72.28
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00020
u
mg/kg
dry
1
0.00020
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,1,1-Trichloroethane [71-55-6]A
0.00031
u
mg/kg
dry
1
0.00031
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00025
u
mg/kg
dry
1
0.00025
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,1,2-Trichloroethane [79-00-5]A
0.00031
u
mg/kg
dry
1
0.00031
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,1-Dichloroethane [75-34-3]A
0.00031
u
mg/kg
dry
1
0.00031
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,1-Dichloroethene [75-35-4]A
0.00038
u
mg/kg
dry
1
0.00038
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,1-Dichloropropene [563-58-6]A
0.00020
u
mg/kg
dry
1
0.00020
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00035
u
mg/kg
dry
1
0.00035
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,2,3-Trichloropropane [96-18-4]A
0.00080
u
mg/kg
dry
1
0.00080
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00034
u
mg/kg
dry
1
0.00034
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00021
u
mg/kg
dry
1
0.00021
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00099
u
mg/kg
dry
1
0.00099
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,2-Dibromoethane [106-93-4]A
0.00058
u
mg/kg
dry
1
0.00058
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,2-Dichlorobenzene [95-50-1]A
0.00034
u
mg/kg
dry
1
0.00034
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,2-Dichloroethane [107-06-2]A
0.00051
u
mg/kg
dry
1
0.00051
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,2-Dichloropropane [78-87-5]A
0.00033
u
mg/kg
dry
1
0.00033
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00025
u
mg/kg
dry
1
0.00025
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,3-Dichlorobenzene [541-73-1]A
0.00028
u
mg/kg
dry
1
0.00028
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,3-Dichloropropane [142-28-9]A
0.00036
u
mg/kg
dry
1
0.00036
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
1,4-Dichlorobenzene [106-46-7]A
0.00025
u
mg/kg
dry
1
0.00025
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
2,2-Dichloropropane [594-20-7]A
0.00029
u
mg/kg
dry
1
0.00029
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
2-Butanone [78-93-3]A
0.00098
u
mg/kg
dry
1
0.00098
0.0063
OK18029
EPA
8260D
11/19/20
00:02
REF
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00020
u
mg/kg
dry
1
0.00020
0.0063
OK18029
EPA
8260D
11/19/20
00:02
REF
2-Chlorotoluene [95-49-8]A
0.00023
u
mg/kg
dry
1
0.00023
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
2-Hexanone [591-78-6]A
0.00094
u
mg/kg
dry
1
0.00094
0.0063
OK18029
EPA
8260D
11/19/20
00:02
REF
4-Chlorotoluene [106-43-4]A
0.00033
u
mg/kg
dry
1
0.00033
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
4-Isopropyltoluene [99-87-6]A
0.00080
1
mg/kg
dry
1
0.00020
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
4-Methyl-2-pentanone [108-10-1]A
0.00071
u
mg/kg
dry
1
0.00071
0.0063
OK18029
EPA
8260D
11/19/20
00:02
REF
Acetone [67-64-1]A
0.018
u
mg/kg
dry
1
0.018
0.025
OK18029
EPA
8260D
11/19/20
00:02
REF
Benzene[71-43-2]A
0.00021
u
mg/kg
dry
1
0.00021
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Bromobenzene[108-86-1]A
0.00028
u
mg/kg
dry
1
0.00028
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Bromochloromethane [74-97-5]A
0.00051
u
mg/kg
dry
1
0.00051
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Bromodichloromethane [75-27-4]A
0.00030
u
mg/kg
dry
1
0.00030
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Bromoform [75-25-2]A
0.00056
u
mg/kg
dry
1
0.00056
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Bromomethane [74-83-9]A
0.00040
u
mg/kg
dry
1
0.00040
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Carbon disulfide [75-15-0]A
0.00049
u
mg/kg
dry
1
0.00049
0.0063
OK18029
EPA
8260D
11/19/20
00:02
REF
Carbon Tetrachloride [56-23-5]A
0.00028
u
mg/kg
dry
1
0.00028
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Chlorobenzene[108-90-7]A
0.00021
u
mg/kg
dry
1
0.00021
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Chloroethane [75-00-3]A
0.00031
u
mg/kg
dry
1
0.00031
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Chloroform [67-66-3]A
0.00023
u
mg/kg
dry
1
0.00023
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Chloromethane [74-87-3]A
0.00026
u
mg/kg
dry
1
0.00026
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
cis-1,2-Dichloroethene [156-59-2]A
0.00029
u
mg/kg
dry
1
0.00029
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00021
u
mg/kg
dry
1
0.00021
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Dibromochloromethane [124-48-1]A
0.00044
u
mg/kg
dry
1
0.00044
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Dibromomethane [74-95-3]A
0.00041
u
mg/kg
dry
1
0.00041
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Dichlorodifluoromethane [75-71-8]A
0.00056
u
mg/kg
dry
1
0.00056
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
Ethylbenzene[100-41-4]A
0.00025
u
mg/kg
dry
1
0.00025
0.0013
OK18029
EPA
8260D
11/19/20
00:02
REF
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 26 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-35-6 Lab Sample ID:CD18880-09 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 72.28
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Hexachlorobutadiene [87-68-3]^
0.00044
U
mg/kg
dry
1
0.00044
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
Isopropyl benzene [98-82-8]^
0.00019
U
mg/kg
dry
1
0.00019
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.00046
U
mg/kg
dry
1
0.00046
0.0025
OK18029
EPA 8260D
11/19/20
00:02
REF
Methylene Chloride [75-09-2]^
0.00091
U
mg/kg
dry
1
0.00091
0.0025
OK18029
EPA 8260D
11/19/20
00:02
REF
Methyl-tert-Butyl Ether [1634-04-4]^
0.00038
U
mg/kg
dry
1
0.00038
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
Naphthalene [91-20-3]^
0.00034
U
mg/kg
dry
1
0.00034
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
n-Butyl Benzene [104-51-8]^
0.00016
U
mg/kg
dry
1
0.00016
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
n-Propyl Benzene [103-65-1]^
0.00023
U
mg/kg
dry
1
0.00023
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
o-Xylene [95-47-6]^
0.00028
U
mg/kg
dry
1
0.00028
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
sec-Butylbenzene [135-98-8]^
0.0012
U
mg/kg
dry
1
0.0012
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
Styrene [100-42-5]^
0.0012
U
mg/kg
dry
1
0.0012
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
tert-Butylbenzene [98-06-6]^
0.00021
U
mg/kg
dry
1
0.00021
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
Tetrachloroethene [127-18-4]^
0.00035
U
mg/kg
dry
1
0.00035
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
Toluene [108-88-3]^
0.00030
U
mg/kg
dry
1
0.00030
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
trans-1,2-Dichloroethene [156-60-5]^
0.00046
U
mg/kg
dry
1
0.00046
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.00049
U
mg/kg
dry
1
0.00049
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
Trichloroethene [79-01-6]^
0.00040
U
mg/kg
dry
1
0.00040
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
Trichlorofluoromethane [75-69-4]^
0.00033
U
mg/kg
dry
1
0.00033
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
Vinyl chloride [75-01-4]^
0.00030
U
mg/kg
dry
1
0.00030
0.0013
OK18029
EPA 8260D
11/19/20
00:02
REF
Xylenes (Total) [1330-20-7]^
0.00070
U
mg/kg
dry
1
0.00070
0.0038
OK18029
EPA 8260D
11/19/20
00:02
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
31
1
50.0
62 %
50-127
OK18029
EPA 6260D
11119120 00:02
REF
Dibromofluoromethane
38
1
50.0
75 %
52-128
OK18029
EPA 8260D
11119120 00:02
REF
Toluene-d8
37
1
50.0
74 %
57-124
OK18029
EPA 8260D
11119120 00:02
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.036
U
mg/kg dry
1
0.036
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
1,2-Dichlorobenzene [95-50-1]^
0.032
U
mg/kg dry
1
0.032
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
1,3-Dichlorobenzene [541-73-1]^
0.028
U
mg/kg dry
1
0.028
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
1,4-Dichlorobenzene [106-46-7]^
0.029
U
mg/kg dry
1
0.029
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
1- Methyl naphthalene [90-12-0]^
0.037
U
mg/kg dry
1
0.037
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2,4,5-Trichlorophenol[95-95-4]^
0.037
U
mg/kg dry
1
0.037
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2,4,6-Trichlorophenol[88-06-2]^
0.037
U
mg/kg dry
1
0.037
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2,4-Dichlorophenol [120-83-2]^
0.033
U
mg/kg dry
1
0.033
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2,4-Di methyl phenol[105-67-9]^
0.059
U
mg/kg dry
1
0.059
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2,4-Dinitrophenol[51-28-5]^
0.059
U
mg/kg dry
1
0.059
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2,4-Dinitrotoluene [121-14-2]^
0.039
U
mg/kg dry
1
0.039
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2,6-Dinitrotoluene [606-20-2]^
0.043
U
mg/kg dry
1
0.043
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2-Chloronaphthalene [91-58-7]^
0.039
U
mg/kg dry
1
0.039
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2-Chlorophenol [95-57-8]^
0.035
U
mg/kg dry
1
0.035
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
0.046
U
mg/kg dry
1
0.046
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM QV-01
2- Methyl naphthalene [91-57-6]^
0.039
U
mg/kg dry
1
0.039
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2-Methylphenol [95-48-7]^
0.035
U
mg/kg dry
1
0.035
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
2-Nitroaniline [88-74-4]^
0.042
U
mg/kg dry
1
0.042
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
FINAL
This report relates only
to the
sample as received by the laboratory,
and may only
be reproduced in full.
Page 27 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-35-6" Lab Sample ID:CD18880-09 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 72.28
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
0.043
U
mg/kg
dry
1
0.043
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]^
0.036
U
mg/kg
dry
1
0.036
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
3,3'-Dichlorobenzidine [91-94-1]^
0.14
U
mg/kg
dry
1
0.14
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
3-Nitroaniline [99-09-2]^
0.050
U
mg/kg
dry
1
0.050
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
4-Bromophenyl-phenylether[101-55-3]^
0.037
U
mg/kg
dry
1
0.037
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
4-Chloro-3-methylphenol [59-50-7]^
0.046
U
mg/kg
dry
1
0.046
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
4-Chloroaniline [106-47-8]^
0.13
U
mg/kg
dry
1
0.13
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
4-Chlorophenyl-phenylether [7005-72-3]^
0.036
U
mg/kg
dry
1
0.036
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
4-Nitroaniline [100-01-6]^
0.073
U
mg/kg
dry
1
0.073
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
4-Nitrophenol [100-02-7]^
0.043
U
mg/kg
dry
1
0.043
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Acenaphthene [83-32-9]^
0.039
U
mg/kg
dry
1
0.039
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Acenaphthylene [208-96-8]^
0.039
U
mg/kg
dry
1
0.039
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Anthracene[120-12-7]^
0.053
U
mg/kg
dry
1
0.053
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Benzidine [92-87-5]^
0.15
U
mg/kg
dry
1
0.15
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Benzo(a)anthracene [56-55-3]^
0.21
J
mg/kg
dry
1
0.039
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Benzo(a)pyrene [50-32-8]^
0.32
J
mg/kg
dry
1
0.046
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Benzo(b)fluoranthene [205-99-2]^
0.31
J
mg/kg
dry
1
0.025
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Benzo(g,h,i)perylene [191-24-2]^
0.19
J
mg/kg
dry
1
0.065
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM QV-01
Benzo(k)fluoranthene [207-08-9]^
0.16
J
mg/kg
dry
1
0.046
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Benzoic acid [65-85-0] ^
0.44
J
mg/kg
dry
1
0.21
2.4
OK19001
EPA
8270E
11/23/20
17:18
DFM
Benzyl alcohol [100-51-6]^
0.032
U
mg/kg
dry
1
0.032
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
0.035
U
mg/kg
dry
1
0.035
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Bis(2-chloroethyl)ether [111-44-4]^
0.059
U
mg/kg
dry
1
0.059
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Bis(2-chloroisopropyl)ether [108-60-1]^
0.033
U
mg/kg
dry
1
0.033
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
0.048
U
mg/kg
dry
1
0.048
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Butylbenzylphthalate [85-68-7]^
0.055
U
mg/kg
dry
1
0.055
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Chrysene [218-01-9]^
0.23
J
mg/kg
dry
1
0.042
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Dibenzo(a,h)anthracene [53-70-3]^
0.071
U
mg/kg
dry
1
0.071
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Dibenzofuran [132-64-9]^
0.037
U
mg/kg
dry
1
0.037
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Diethylphthalate [84-66-2]^
0.039
U
mg/kg
dry
1
0.039
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Dimethylphthalate [131-11-3]^
0.046
U
mg/kg
dry
1
0.046
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Di-n-butylphthalate [84-74-2]^
0.057
U
mg/kg
dry
1
0.057
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Di-n-octylphthalate [117-84-O]^
0.046
U
mg/kg
dry
1
0.046
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Fluoranthene [206-44-O]^
0.29
J
mg/kg
dry
1
0.050
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Fluorene [86-73-7]^
0.040
U
mg/kg
dry
1
0.040
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Hexachlorobenzene [118-74-1]^
0.036
U
mg/kg
dry
1
0.036
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Hexachlorobutadiene [87-68-3]^
0.036
U
mg/kg
dry
1
0.036
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Hexachlorocyclopentadiene [77-47-4]^
0.054
U
mg/kg
dry
1
0.054
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Hexachloroethane [67-72-1]^
0.029
U
mg/kg
dry
1
0.029
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
0.35
J
mg/kg
dry
1
0.065
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Isophorone[78-59-1]^
0.042
U
mg/kg
dry
1
0.042
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Naphthalene [91-20-3]^
0.039
U
mg/kg
dry
1
0.039
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
Nitrobenzene [98-95-3]^
0.036
U
mg/kg
dry
1
0.036
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
N-Nitrosodimethylamine [62-75-9]^
0.029
U
mg/kg
dry
1
0.029
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
0.11
U
mg/kg
dry
1
0.11
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
N-nitrosodiphenylamine/Diphenylamine
0.075
U
mg/kg
dry
1
0.075
0.46
OK19001
EPA
8270E
11/23/20
17:18
DFM
[86-30-6/122-39-4]^
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-35-6 Lab Sample ID:CD18880-09 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 72.28
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.046
U
mg/kg dry
1
0.046
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
Phenanthrene [85-01-8]^
0.18
J
mg/kg dry
1
0.037
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
Phenol[108-95-2]^
0.030
U
mg/kg dry
1
0.030
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
Pyrene [129-00-0]^
0.23
J
mg/kg dry
1
0.053
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
Pyridine [110-86-1]^
0.11
U
mg/kg dry
1
0.11
0.46
OK19001
EPA 8270E
11/23/20 17:18
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
5.5
1
4.61
120 %
26-130
OK19001
EPA 8270E
11/23/2017:16
DFM
2-Fluorobiphenyl
24
1
231
102 %
56-120
OK19001
EPA 8270E
11123120 17:16
DFM
2-Fluorophenol
4.5
1
4.61
98 %
49-126
OK19001
EPA 8270E
11123120 17:16
DFM
Nitrobenzene-d5
23
1
231
99 %
50-117
OK19001
EPA 8270E
11/23/2017:18
DFM
Phenol-d5
5.0
1
4.61
108 %
56-120
OK19001
EPA 8270E
11/23/2017:18
DFM
Terphenyl-d14
1.8
1
2.31
80 %
36-151
OK19001
EPA 8270E
11/23/2017:18
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]1
38.4
mg/kg dry
1
0.166 0.692
OK20031
EPA 6010D
11/23/20 15:03
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 29 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-35-18" Lab Sample ID:CD18880-10 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:45 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 73.67
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]A
0.035
u
mg/kg dry
1
0.035
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
1,2-Dichlorobenzene [95-50-1]A
0.031
u
mg/kg dry
1
0.031
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
1,3-Dichlorobenzene [541-73-1]A
0.027
u
mg/kg dry
1
0.027
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
1,4-Dichlorobenzene [106-46-7]A
0.029
u
mg/kg dry
1
0.029
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
1-Methylnaphthalene [90-12-0]A
0.037
u
mg/kg dry
1
0.037
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2,4,5-Trichlorophenol [95-95-4]A
0.037
u
mg/kg dry
1
0.037
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2,4,6-Trichlorophenol [88-06-2]A
0.037
u
mg/kg dry
1
0.037
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2,4-Dichlorophenol [120-83-2]A
0.033
u
mg/kg dry
1
0.033
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2,4-Dimethylphenol [105-67-9]A
0.058
u
mg/kg dry
1
0.058
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2,4-Dinitrophenol [51-28-5]A
0.058
u
mg/kg dry
1
0.058
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2,4-Dinitrotoluene [121-14-2]A
0.038
u
mg/kg dry
1
0.038
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2,6-Dinitrotoluene [606-20-2]A
0.042
u
mg/kg dry
1
0.042
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2-Chloronaphthalene [91-58-7]A
0.038
u
mg/kg dry
1
0.038
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2-Chlorophenol [95-57-8]A
0.034
u
mg/kg dry
1
0.034
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]A
0.045
u
mg/kg dry
1
0.045
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2-Methylnaphthalene [91-57-6]A
0.038
u
mg/kg dry
1
0.038
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2-Methylphenol [95-48-7]A
0.034
u
mg/kg dry
1
0.034
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2-Nitroaniline [88-74-4]A
0.041
u
mg/kg dry
1
0.041
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
2-Nitrophenol [88-75-5]A
0.042
u
mg/kg dry
1
0.042
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.035
u
mg/kg dry
1
0.035
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.13
u
mg/kg dry
1
0.13
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
3-Nitroaniline [99-09-2]A
0.049
u
mg/kg dry
1
0.049
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.037
u
mg/kg dry
1
0.037
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.045
u
mg/kg dry
1
0.045
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
4-Chloroaniline [106-47-8]A
0.13
u
mg/kg dry
1
0.13
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.035
u
mg/kg dry
1
0.035
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
4-Nitroaniline [100-01-6]A
0.072
u
mg/kg dry
1
0.072
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
4-Nitrophenol [100-02-7]A
0.042
u
mg/kg dry
1
0.042
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Acenaphthene [83-32-9]A
0.038
u
mg/kg dry
1
0.038
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Acenaphthylene [208-96-8]A
0.038
u
mg/kg dry
1
0.038
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Anthracene[120-12-7]A
0.052
u
mg/kg dry
1
0.052
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Benzidine [92-87-5]A
0.15
u
mg/kg dry
1
0.15
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Benzo(a)anthracene [56-55-3]A
0.038
u
mg/kg dry
1
0.038
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Benzo(a)pyrene[50-32-8]A
0.045
u
mg/kg dry
1
0.045
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Benzo(b)fluoranthene [205-99-2]A
0.024
u
mg/kg dry
1
0.024
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.064
u
mg/kg dry
1
0.064
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Benzo(k)fluoranthene [207-08-9]A
0.045
u
mg/kg dry
1
0.045
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Benzoic acid [65-85-0]A
0.20
u
mg/kg dry
1
0.20
2.3
OK25001
EPA 8270E
11/25/20 15:31
DFM
Benzyl alcohol [100-51-6]A
0.031
u
mg/kg dry
1
0.031
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.034
u
mg/kg dry
1
0.034
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.058
u
mg/kg dry
1
0.058
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.033
u
mg/kg dry
1
0.033
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.048
u
mg/kg dry
1
0.048
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Butylbenzylphthalate [85-68-7]A
0.054
u
mg/kg dry
1
0.054
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Chrysene [218-01-9]A
0.041
u
mg/kg dry
1
0.041
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.069
u
mg/kg dry
1
0.069
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Dibenzofuran [132-64-9]A
0.037
u
mg/kg dry
1
0.037
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 30 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-35-18" Lab Sample ID:CD18880-10 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 09:45 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 73.67
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified anaiyte [NC 591]
Analvte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Diethylphthalate [84-66-2]A
0.038
U
mg/kg dry
1
0.038
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Dimethylphthalate [131-11-3]A
0.045
U
mg/kg dry
1
0.045
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Di-n-butylphthalate [84-74-2]A
0.056
U
mg/kg dry
1
0.056
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Di-n-octylphthalate [117-84-0]A
0.045
U
mg/kg dry
1
0.045
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM QV-01
Fluoranthene [206-44-0]A
0.049
U
mg/kg dry
1
0.049
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Fluorene [86-73-7]A
0.039
U
mg/kg dry
1
0.039
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Hexachlorobenzene [118-74-1]A
0.035
U
mg/kg dry
1
0.035
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Hexachlorobutadiene [87-68-3]A
0.035
U
mg/kg dry
1
0.035
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM QV-01
Hexachlorocyclopentadiene [77-47-4]A
0.053
U
mg/kg dry
1
0.053
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Hexachloroethane [67-72-1]A
0.029
U
mg/kg dry
1
0.029
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.064
U
mg/kg dry
1
0.064
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Isophorone[78-59-1]A
0.041
U
mg/kg dry
1
0.041
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Naphthalene [91-20-3]A
0.038
U
mg/kg dry
1
0.038
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Nitrobenzene [98-95-3]A
0.035
U
mg/kg dry
1
0.035
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
N-Nitrosodimethylamine [62-75-9]A
0.029
U
mg/kg dry
1
0.029
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.11
U
mg/kg dry
1
0.11
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
N-nitrosodiphenylamine/Diphenylamine
0.073
U
mg/kg dry
1
0.073
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
[86-30-6/122-39-4]A
Pentachlorophenol [87-86-5]A
0.045
U
mg/kg dry
1
0.045
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Phenanthrene [85-01-8]A
0.037
U
mg/kg dry
1
0.037
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Phenol[108-95-2]A
0.030
U
mg/kg dry
1
0.030
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Pyrene [129-00-0]A
0.052
U
mg/kg dry
1
0.052
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Pyridine [110-86-1]A
0.11
U
mg/kg dry
1
0.11
0.45
OK25001
EPA 8270E
11/25/20 15:31
DFM
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analyzed
fly Notes
2,4,6-Tribromophenol
4.0
1
4.52
88 %
28-130
OK25OO1
EPA 8270E
111251201531
DFM
2-Fluorobiphenyl
1.5
1
2.26
66 %
56-120
OK25OO1
EPA 8270E
111251201531
DFM
2-Fluorophenol
3.6
1
4.52
79 %
49-126
OK25OO1
EPA 8270E
111251201531
DFM
Nitrobenzene-d5
1.7
1
2.26
73 %
50-117
OK25OO1
EPA 8270E
111251201531
DFM
Phenol-d5
3.8
1
4.52
84 %
56-120
OK25OO1
EPA 8270E
111251201531
DFM
Terphenyl-d14
1.8
1
2.26
78 %
36-151
OK25OO1
EPA 8270E
111251201531
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified anaiyte [NC 591]
Analvte MAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]A
16.2
mg/kg dry
1
0.163 0.679
OK30010
EPA 6010D
12/01/20 09:52
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 31 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-36-6" Lab Sample ID:CD18880-11 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:00 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.42
Volatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00014
u
mg/kg
dry
0.792
0.00014
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,1,1-Trichloroethane [71-55-6]A
0.00022
u
mg/kg
dry
0.792
0.00022
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00018
u
mg/kg
dry
0.792
0.00018
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,1,2-Trichloroethane [79-00-5]A
0.00022
u
mg/kg
dry
0.792
0.00022
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,1-Dichloroethane [75-34-3]A
0.00022
u
mg/kg
dry
0.792
0.00022
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,1-Dichloroethene [75-35-4]A
0.00027
u
mg/kg
dry
0.792
0.00027
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,1-Dichloropropene [563-58-6]A
0.00014
u
mg/kg
dry
0.792
0.00014
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00025
u
mg/kg
dry
0.792
0.00025
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,2,3-Trichloropropane [96-18-4]A
0.00057
u
mg/kg
dry
0.792
0.00057
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00024
u
mg/kg
dry
0.792
0.00024
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00015
u
mg/kg
dry
0.792
0.00015
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00070
u
mg/kg
dry
0.792
0.00070
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,2-Dibromoethane [106-93-4]A
0.00041
u
mg/kg
dry
0.792
0.00041
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,2-Dichlorobenzene [95-50-1]A
0.00024
u
mg/kg
dry
0.792
0.00024
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,2-Dichloroethane [107-06-2]A
0.00036
u
mg/kg
dry
0.792
0.00036
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,2-Dichloropropane [78-87-5]A
0.00023
u
mg/kg
dry
0.792
0.00023
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00018
u
mg/kg
dry
0.792
0.00018
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,3-Dichlorobenzene [541-73-1]A
0.00019
u
mg/kg
dry
0.792
0.00019
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,3-Dichloropropane [142-28-9]A
0.00026
u
mg/kg
dry
0.792
0.00026
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
1,4-Dichlorobenzene [106-46-7]A
0.00018
u
mg/kg
dry
0.792
0.00018
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
2,2-Dichloropropane [594-20-7]A
0.00020
u
mg/kg
dry
0.792
0.00020
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
2-Butanone [78-93-3]A
0.00069
u
mg/kg
dry
0.792
0.00069
0.0044
OK18029
EPA
8260D
11/19/20
00:32
REF
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00014
u
mg/kg
dry
0.792
0.00014
0.0044
OK18029
EPA
8260D
11/19/20
00:32
REF
2-Chlorotoluene [95-49-8]A
0.00016
u
mg/kg
dry
0.792
0.00016
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
2-Hexanone [591-78-6]A
0.00066
u
mg/kg
dry
0.792
0.00066
0.0044
OK18029
EPA
8260D
11/19/20
00:32
REF
4-Chlorotoluene [106-43-4]A
0.00023
u
mg/kg
dry
0.792
0.00023
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
4-Isopropyltoluene [99-87-6]A
0.00014
u
mg/kg
dry
0.792
0.00014
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
4-Methyl-2-pentanone [108-10-1]A
0.00051
u
mg/kg
dry
0.792
0.00051
0.0044
OK18029
EPA
8260D
11/19/20
00:32
REF
Acetone [67-64-1]A
0.012
u
mg/kg
dry
0.792
0.012
0.018
OK18029
EPA
8260D
11/19/20
00:32
REF
Benzene [71-43-2]A
0.00015
u
mg/kg
dry
0.792
0.00015
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Bromobenzene [108-86-1]A
0.00019
u
mg/kg
dry
0.792
0.00019
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Bromochloromethane [74-97-5]A
0.00036
u
mg/kg
dry
0.792
0.00036
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Bromodichloromethane [75-27-4]A
0.00021
u
mg/kg
dry
0.792
0.00021
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Bromoform [75-25-2]A
0.00040
u
mg/kg
dry
0.792
0.00040
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Bromomethane [74-83-9]A
0.00028
u
mg/kg
dry
0.792
0.00028
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Carbon disulfide [75-15-0]A
0.00035
u
mg/kg
dry
0.792
0.00035
0.0044
OK18029
EPA
8260D
11/19/20
00:32
REF
Carbon Tetrachloride [56-23-5]A
0.00019
u
mg/kg
dry
0.792
0.00019
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Chlorobenzene [108-90-7]A
0.00015
u
mg/kg
dry
0.792
0.00015
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Chloroethane [75-00-3]A
0.00022
u
mg/kg
dry
0.792
0.00022
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Chloroform [67-66-3]A
0.00016
u
mg/kg
dry
0.792
0.00016
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Chloromethane [74-87-3]A
0.00019
u
mg/kg
dry
0.792
0.00019
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
cis-1,2-Dichloroethene [156-59-2]A
0.00020
u
mg/kg
dry
0.792
0.00020
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00015
u
mg/kg
dry
0.792
0.00015
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Dibromochloromethane [124-48-1]A
0.00031
u
mg/kg
dry
0.792
0.00031
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Dibromomethane [74-95-3]A
0.00029
u
mg/kg
dry
0.792
0.00029
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Dichlorodifluoromethane [75-71-8]A
0.00040
u
mg/kg
dry
0.792
0.00040
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
Ethylbenzene [100-41-4]A
0.00018
u
mg/kg
dry
0.792
0.00018
0.00089
OK18029
EPA
8260D
11/19/20
00:32
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 32 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-36-6 Lab Sample ID:CD18880-11 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:00 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.42
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Hexachlorobutadiene [87-68-3]^
0.00031
U
mg/kg
dry
0.792
0.00031
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
Isopropyl benzene [98-82-8]^
0.00013
U
mg/kg
dry
0.792
0.00013
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.00033
U
mg/kg
dry
0.792
0.00033
0.0018
OK18029
EPA 8260D
11/19/20
00:32
REF
Methylene Chloride [75-09-2]^
0.00065
U
mg/kg
dry
0.792
0.00065
0.0018
OK18029
EPA 8260D
11/19/20
00:32
REF
Methyl-tert-Butyl Ether [1634-04-4]^
0.00027
U
mg/kg
dry
0.792
0.00027
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
Naphthalene [91-20-3]^
0.00024
U
mg/kg
dry
0.792
0.00024
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
n-Butyl Benzene [104-51-8]^
0.00012
U
mg/kg
dry
0.792
0.00012
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
n-Propyl Benzene [103-65-1]^
0.00016
U
mg/kg
dry
0.792
0.00016
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
o-Xylene [95-47-6]^
0.00019
U
mg/kg
dry
0.792
0.00019
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
sec-Butylbenzene [135-98-8]^
0.00084
U
mg/kg
dry
0.792
0.00084
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
Styrene [100-42-5]^
0.00087
U
mg/kg
dry
0.792
0.00087
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
tert-Butylbenzene [98-06-6]^
0.00015
U
mg/kg
dry
0.792
0.00015
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
Tetrachloroethene [127-18-4]^
0.00025
U
mg/kg
dry
0.792
0.00025
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
Toluene [108-88-3]^
0.00021
U
mg/kg
dry
0.792
0.00021
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
trans-1,2-Dichloroethene [156-60-5]^
0.00033
U
mg/kg
dry
0.792
0.00033
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.00035
U
mg/kg
dry
0.792
0.00035
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
Trichloroethene [79-01-6]^
0.00028
U
mg/kg
dry
0.792
0.00028
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
Trichlorofluoromethane [75-69-4]^
0.00023
U
mg/kg
dry
0.792
0.00023
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
Vinyl chloride [75-01-4]^
0.00021
U
mg/kg
dry
0.792
0.00021
0.00089
OK18029
EPA 8260D
11/19/20
00:32
REF
Xylenes (Total) [1330-20-7]^
0.00050
U
mg/kg
dry
0.792
0.00050
0.0027
OK18029
EPA 8260D
11/19/20
00:32
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
32
0.792
50.0
64 %
50-127
OK18029
EPA 6260D
11119120 00:32
REF
Dlbromofluoromethane
38
0.792
50.0
77 %
52-128
OK18029
EPA 8260D
11119120 00:32
REF
Toluene-d8
36
0.792
50.0
72 %
57-124
OK18029
EPA 8260D
11119120 00:32
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.029
U
mg/kg dry
1
0.029
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
1,2-Dichlorobenzene [95-50-1]^
0.026
U
mg/kg dry
1
0.026
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
1,3-Dichlorobenzene [541-73-1]^
0.022
U
mg/kg dry
1
0.022
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
1,4-Dichlorobenzene [106-46-7]^
0.023
U
mg/kg dry
1
0.023
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
1- Methyl naphthalene [90-12-0]^
0.030
U
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2,4,5-Trichlorophenol[95-95-4]^
0.030
U
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2,4,6-Trichlorophenol[88-06-2]^
0.030
U
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2,4-Dichlorophenol [120-83-2]^
0.027
U
mg/kg dry
1
0.027
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2,4-Di methyl phenol[105-67-9]^
0.048
U
mg/kg dry
1
0.048
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2,4-Dinitrophenol [51-28-5]^
0.048
U
mg/kg dry
1
0.048
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2,4-Dinitrotoluene [121-14-2]^
0.031
U
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2,6-Dinitrotoluene [606-20-2]^
0.035
U
mg/kg dry
1
0.035
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2-Chloronaphthalene [91-58-7]^
0.031
U
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2-Chlorophenol [95-57-8]^
0.028
U
mg/kg dry
1
0.028
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
0.037
U
mg/kg dry
1
0.037
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM QV-01
2- Methyl naphthalene [91-57-6]^
0.031
U
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2-Methylphenol [95-48-7]^
0.028
U
mg/kg dry
1
0.028
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
2-Nitroaniline [88-74-4]^
0.034
U
mg/kg dry
1
0.034
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 33 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-36-6" Lab Sample ID:CD18880-11 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:00 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.42
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
0.035
U
mg/kg
dry
1
0.035
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]^
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
3,3'-Dichlorobenzidine [91-94-1]^
0.11
U
mg/kg
dry
1
0.11
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
3-Nitroaniline [99-09-2]^
0.040
U
mg/kg
dry
1
0.040
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
4-Bromophenyl-phenylether [101-55-3]^
0.030
U
mg/kg
dry
1
0.030
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
4-Chloro-3-methylphenol [59-50-7]^
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
4-Chloroaniline [106-47-8]^
0.10
U
mg/kg
dry
1
0.10
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
4-Chlorophenyl-phenylether [7005-72-3]^
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
4-Nitroaniline [100-01-6]^
0.059
U
mg/kg
dry
1
0.059
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
4-Nitrophenol [100-02-7]^
0.035
U
mg/kg
dry
1
0.035
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM QM-11
Acenaphthene [83-32-9]^
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Acenaphthylene [208-96-8]^
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Anthracene[120-12-7]^
0.042
U
mg/kg
dry
1
0.042
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Benzidine [92-87-5]^
0.12
U
mg/kg
dry
1
0.12
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Benzo(a)anthracene [56-55-3]^
0.089
J
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Benzo(a)pyrene [50-32-8]^
0.13
J
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Benzo(b)fluoranthene [205-99-2]^
0.13
J
mg/kg
dry
1
0.020
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Benzo(g,h,i)perylene [191-24-2]^
0.083
J
mg/kg
dry
1
0.053
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM 3-04
Benzo(k)fluoranthene [207-08-9]^
0.066
J
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Benzoic acid [65-85-0]^
0.17
U
mg/kg
dry
1
0.17
1.9
OK19001
EPA
8270E
11/23/20
13:37
DFM
Benzyl alcohol [100-51-6]^
0.026
U
mg/kg
dry
1
0.026
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
0.028
U
mg/kg
dry
1
0.028
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Bis(2-chloroethyl)ether [111-44-4]^
0.048
U
mg/kg
dry
1
0.048
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Bis(2-chloroisopropyl)ether [108-60-1]^
0.027
U
mg/kg
dry
1
0.027
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
0.039
U
mg/kg
dry
1
0.039
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Butylbenzylphthalate [85-68-7]^
0.045
U
mg/kg
dry
1
0.045
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Chrysene [218-01-9]^
0.097
J
mg/kg
dry
1
0.034
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Dibenzo(a,h)anthracene [53-70-3]^
0.057
U
mg/kg
dry
1
0.057
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Dibenzofuran [132-64-9]^
0.030
U
mg/kg
dry
1
0.030
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Diethylphthalate [84-66-2]^
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Dimethylphthalate [131-11-3]^
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Di-n-butylphthalate [84-74-2]^
0.046
U
mg/kg
dry
1
0.046
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Di-n-octylphthalate [117-84-O]^
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Fluoranthene [206-44-O]^
0.11
J
mg/kg
dry
1
0.040
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Fluorene [86-73-7]^
0.032
U
mg/kg
dry
1
0.032
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Hexachlorobenzene [118-74-1]^
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Hexachlorobutadiene [87-68-3]^
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Hexachlorocyclopentadiene [77-47-4]^
0.044
U
mg/kg
dry
1
0.044
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Hexachloroethane [67-72-1]^
0.023
U
mg/kg
dry
1
0.023
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
0.23
J
mg/kg
dry
1
0.053
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Isophorone[78-59-1]^
0.034
U
mg/kg
dry
1
0.034
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Naphthalene [91-20-3]^
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
Nitrobenzene [98-95-3]^
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
N-Nitrosodimethylamine [62-75-9]^
0.023
U
mg/kg
dry
1
0.023
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
0.091
U
mg/kg
dry
1
0.091
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
N-nitrosodiphenylamine/Diphenylamine
0.060
U
mg/kg
dry
1
0.060
0.37
OK19001
EPA
8270E
11/23/20
13:37
DFM
[86-30-6/122-39-4]^
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 34 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-36-6 Lab Sample ID:CD18880-11 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:00 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.42
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.037
U
mg/kg dry
1
0.037
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
Phenanthrene [85-01-8]^
0.069
J
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
Phenol[108-95-2]^
0.025
U
mg/kg dry
1
0.025
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
Pyrene [129-00-0]^
0.10
J
mg/kg dry
1
0.042
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
Pyridine [110-86-1]^
0.092
U
mg/kg dry
1
0.092
0.37
OK19001
EPA 8270E
11/23/20 13:37
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.4
1
3.73
119 %
26-130
OK19001
EPA 8270E
11/23/2013:37
DFM
2-Fluorobiphenyl
I.8
1
1.86
97 %
56-120
OK19001
EPA 8270E
1112312013:37
DFM
2-Fluorophenol
3.9
1
3.73
105 %
49-126
OK19001
EPA 8270E
1112312013:37
DFM
Nitrobenzene-d5
I.8
1
1.86
95 %
50-117
OK19001
EPA 8270E
11/23/2013:37
DFM
Phenol-d5
4.3
1
3.73
114 %
56-120
OK19001
EPA 8270E
11/23/2013:37
DFM
Terphenyl-d14
1.6
1
1.66
86 %
36-151
OK19001
EPA 8270E
11/23/2013:37
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]1
12.0
mg/kg dry
1
0.134 0.559
OK20031
EPA 6010D
11/23/20 15:06
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 35 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-36-18" Lab Sample ID:CD18880-12 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:05 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.03
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]A
0.031
u
mg/kg dry
1
0.031
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
1,2-Dichlorobenzene [95-50-1]A
0.027
u
mg/kg dry
1
0.027
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
1,3-Dichlorobenzene [541-73-1]A
0.024
u
mg/kg dry
1
0.024
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
1,4-Dichlorobenzene [106-46-7]A
0.025
u
mg/kg dry
1
0.025
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
1-Methylnaphthalene [90-12-0]A
0.032
u
mg/kg dry
1
0.032
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2,4,5-Trichlorophenol [95-95-4]A
0.032
u
mg/kg dry
1
0.032
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2,4,6-Trichlorophenol [88-06-2]A
0.032
u
mg/kg dry
1
0.032
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2,4-Dichlorophenol [120-83-2]A
0.029
u
mg/kg dry
1
0.029
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2,4-Dimethylphenol [105-67-9]A
0.051
u
mg/kg dry
1
0.051
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2,4-Dinitrophenol [51-28-5]A
0.051
u
mg/kg dry
1
0.051
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2,4-Dinitrotoluene [121-14-2]A
0.033
u
mg/kg dry
1
0.033
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2,6-Dinitrotoluene [606-20-2]A
0.037
u
mg/kg dry
1
0.037
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2-Chloronaphthalene [91-58-7]A
0.033
u
mg/kg dry
1
0.033
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2-Chlorophenol [95-57-8]A
0.030
u
mg/kg dry
1
0.030
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]A
0.039
u
mg/kg dry
1
0.039
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2-Methylnaphthalene [91-57-6]A
0.033
u
mg/kg dry
1
0.033
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2-Methylphenol [95-48-7]A
0.030
u
mg/kg dry
1
0.030
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2-Nitroaniline [88-74-4]A
0.036
u
mg/kg dry
1
0.036
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
2-Nitrophenol [88-75-5]A
0.037
u
mg/kg dry
1
0.037
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.031
u
mg/kg dry
1
0.031
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.12
u
mg/kg dry
1
0.12
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
3-Nitroaniline [99-09-2]A
0.043
u
mg/kg dry
1
0.043
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.032
u
mg/kg dry
1
0.032
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.039
u
mg/kg dry
1
0.039
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
4-Chloroaniline [106-47-8]A
0.11
u
mg/kg dry
1
0.11
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.031
u
mg/kg dry
1
0.031
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
4-Nitroaniline [100-01-6]A
0.063
u
mg/kg dry
1
0.063
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
4-Nitrophenol [100-02-7]A
0.037
u
mg/kg dry
1
0.037
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Acenaphthene [83-32-9]A
0.033
u
mg/kg dry
1
0.033
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Acenaphthylene [208-96-8]A
0.033
u
mg/kg dry
1
0.033
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Anthracene[120-12-7]A
0.045
u
mg/kg dry
1
0.045
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Benzidine [92-87-5]A
0.13
u
mg/kg dry
1
0.13
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Benzo(a)anthracene [56-55-3]A
0.033
u
mg/kg dry
1
0.033
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Benzo(a)pyrene[50-32-8]A
0.039
u
mg/kg dry
1
0.039
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Benzo(b)fluoranthene [205-99-2]A
0.021
u
mg/kg dry
1
0.021
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.056
u
mg/kg dry
1
0.056
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Benzo(k)fluoranthene [207-08-9]A
0.039
u
mg/kg dry
1
0.039
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Benzoic acid [65-85-0]A
0.18
u
mg/kg dry
1
0.18
2.0
OK25001
EPA 8270E
11/25/20 16:03
DFM
Benzyl alcohol [100-51-6]A
0.027
u
mg/kg dry
1
0.027
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.030
u
mg/kg dry
1
0.030
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.051
u
mg/kg dry
1
0.051
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.029
u
mg/kg dry
1
0.029
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.042
u
mg/kg dry
1
0.042
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Butylbenzylphthalate [85-68-7]A
0.048
u
mg/kg dry
1
0.048
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Chrysene [218-01-9]A
0.036
u
mg/kg dry
1
0.036
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.061
u
mg/kg dry
1
0.061
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Dibenzofuran [132-64-9]A
0.032
u
mg/kg dry
1
0.032
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 36 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-36-18" Lab Sample ID:CD18880-12 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:05 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 84.03
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified anaiyte [NC 591]
Analvte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Diethylphthalate [84-66-2]A
0.033
U
mg/kg dry
1
0.033
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Dimethylphthalate [131-11-3]A
0.039
U
mg/kg dry
1
0.039
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Di-n-butylphthalate [84-74-2]A
0.049
U
mg/kg dry
1
0.049
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Di-n-octylphthalate [117-84-0]A
0.039
U
mg/kg dry
1
0.039
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM QV-01
Fluoranthene [206-44-0]A
0.043
U
mg/kg dry
1
0.043
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Fluorene [86-73-7]A
0.035
U
mg/kg dry
1
0.035
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Hexachlorobenzene [118-74-1]A
0.031
U
mg/kg dry
1
0.031
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Hexachlorobutadiene [87-68-3]A
0.031
U
mg/kg dry
1
0.031
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM QV-01
Hexachlorocyclopentadiene [77-47-4]A
0.046
U
mg/kg dry
1
0.046
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Hexachloroethane [67-72-1]A
0.025
U
mg/kg dry
1
0.025
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.056
U
mg/kg dry
1
0.056
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Isophorone[78-59-1]A
0.036
U
mg/kg dry
1
0.036
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Naphthalene [91-20-3]A
0.033
U
mg/kg dry
1
0.033
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Nitrobenzene [98-95-3]A
0.031
U
mg/kg dry
1
0.031
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
N-Nitrosodimethylamine [62-75-9]A
0.025
U
mg/kg dry
1
0.025
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.096
U
mg/kg dry
1
0.096
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
N-nitrosodiphenylamine/Diphenylamine
0.064
U
mg/kg dry
1
0.064
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
[86-30-6/122-39-4]A
Pentachlorophenol [87-86-5]A
0.039
U
mg/kg dry
1
0.039
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Phenanthrene [85-01-8]A
0.032
U
mg/kg dry
1
0.032
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Phenol[108-95-2]A
0.026
U
mg/kg dry
1
0.026
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Pyrene [129-00-0]A
0.045
U
mg/kg dry
1
0.045
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Pyridine [110-86-1]A
0.098
U
mg/kg dry
1
0.098
0.39
OK25001
EPA 8270E
11/25/20 16:03
DFM
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analyzed
fly Notes
2,4,6-Tribromophenol
4.4
1
3.97
112 %
28-130
OK25OO1
EPA 8270E
1112512016:03
DFM
2-Fluorobiphenyl
1.7
1
1.98
85 %
56-120
OK25OO1
EPA 8270E
1112512016:03
DFM
2-Fluorophenol
3.5
1
3.97
89 %
49-126
OK25OO1
EPA 8270E
1112512016:03
DFM
Nitrobenzene-d5
1.8
1
1.98
89 %
50-117
OK25OO1
EPA 8270E
1112512016:03
DFM
Phenol-d5
3.8
1
3.97
95 %
56-120
OK25OO1
EPA 8270E
1112512016:03
DFM
Terphenyl-d14
2.1
1
1.98
104 %
36-151
OK25OO1
EPA 8270E
1112512016:03
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified anaiyte [NC 591]
Analvte MAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]A
7.86
mg/kg dry
1.11
0.159 0.661
OK30010
EPA 6010D
12/01/20 09:54
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 37 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-37-6" Lab Sample ID:CD18880-13 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:20 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.00
Volatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00018
u
mg/kg
dry
1
0.00018
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,1,1-Trichloroethane [71-55-6]A
0.00028
u
mg/kg
dry
1
0.00028
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00022
u
mg/kg
dry
1
0.00022
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,1,2-Trichloroethane [79-00-5]A
0.00028
u
mg/kg
dry
1
0.00028
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,1-Dichloroethane [75-34-3]A
0.00028
u
mg/kg
dry
1
0.00028
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
QV-01
1,1-Dichloroethene [75-35-4]A
0.00033
u
mg/kg
dry
1
0.00033
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,1-Dichloropropene [563-58-6]A
0.00018
u
mg/kg
dry
1
0.00018
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00031
u
mg/kg
dry
1
0.00031
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,2,3-Trichloropropane [96-18-4]A
0.00071
u
mg/kg
dry
1
0.00071
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00030
u
mg/kg
dry
1
0.00030
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00019
u
mg/kg
dry
1
0.00019
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00088
u
mg/kg
dry
1
0.00088
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,2-Dibromoethane [106-93-4]A
0.00051
u
mg/kg
dry
1
0.00051
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,2-Dichlorobenzene [95-50-1]A
0.00030
u
mg/kg
dry
1
0.00030
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,2-Dichloroethane [107-06-2]A
0.00046
u
mg/kg
dry
1
0.00046
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,2-Dichloropropane [78-87-5]A
0.00029
u
mg/kg
dry
1
0.00029
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00022
u
mg/kg
dry
1
0.00022
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,3-Dichlorobenzene [541-73-1]A
0.00024
u
mg/kg
dry
1
0.00024
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,3-Dichloropropane [142-28-9]A
0.00032
u
mg/kg
dry
1
0.00032
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
1,4-Dichlorobenzene [106-46-7]A
0.00022
u
mg/kg
dry
1
0.00022
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
2,2-Dichloropropane [594-20-7]A
0.00026
u
mg/kg
dry
1
0.00026
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
2-Butanone [78-93-3]A
0.00087
u
mg/kg
dry
1
0.00087
0.0056
OK18035
EPA
8260D
11/19/20
05:03
REF
QV-01
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00018
u
mg/kg
dry
1
0.00018
0.0056
OK18035
EPA
8260D
11/19/20
05:03
REF
2-Chlorotoluene [95-49-8]A
0.00020
u
mg/kg
dry
1
0.00020
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
2-Hexanone [591-78-6]A
0.00083
u
mg/kg
dry
1
0.00083
0.0056
OK18035
EPA
8260D
11/19/20
05:03
REF
4-Chlorotoluene [106-43-4]A
0.00029
u
mg/kg
dry
1
0.00029
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
4-Isopropyltoluene [99-87-6]A
0.00058
1
mg/kg
dry
1
0.00018
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
4-Methyl-2-pentanone [108-10-1]A
0.00063
u
mg/kg
dry
1
0.00063
0.0056
OK18035
EPA
8260D
11/19/20
05:03
REF
Acetone [67-64-1]A
0.016
u
mg/kg
dry
1
0.016
0.022
OK18035
EPA
8260D
11/19/20
05:03
REF
Benzene [71-43-2]A
0.00019
u
mg/kg
dry
1
0.00019
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
QV-01
Bromobenzene [108-86-1]A
0.00024
u
mg/kg
dry
1
0.00024
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Bromochloromethane [74-97-5]A
0.00046
u
mg/kg
dry
1
0.00046
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Bromodichloromethane [75-27-4]A
0.00027
u
mg/kg
dry
1
0.00027
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Bromoform [75-25-2]A
0.00050
u
mg/kg
dry
1
0.00050
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Bromomethane [74-83-9]A
0.00036
u
mg/kg
dry
1
0.00036
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Carbon disulfide [75-15-0]A
0.00043
u
mg/kg
dry
1
0.00043
0.0056
OK18035
EPA
8260D
11/19/20
05:03
REF
QV-01
Carbon Tetrachloride [56-23-5]A
0.00024
u
mg/kg
dry
1
0.00024
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Chlorobenzene [108-90-7]A
0.00019
u
mg/kg
dry
1
0.00019
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Chloroethane [75-00-3]A
0.00028
u
mg/kg
dry
1
0.00028
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Chloroform [67-66-3]A
0.00020
u
mg/kg
dry
1
0.00020
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Chloromethane [74-87-3]A
0.00023
u
mg/kg
dry
1
0.00023
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
QV-01
cis-1,2-Dichloroethene [156-59-2]A
0.00026
u
mg/kg
dry
1
0.00026
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00019
u
mg/kg
dry
1
0.00019
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Dibromochloromethane [124-48-1]A
0.00039
u
mg/kg
dry
1
0.00039
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Dibromomethane [74-95-3]A
0.00037
u
mg/kg
dry
1
0.00037
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Dichlorodifluoromethane [75-71-8]A
0.00050
u
mg/kg
dry
1
0.00050
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
Ethylbenzene [100-41-4]A
0.00022
u
mg/kg
dry
1
0.00022
0.0011
OK18035
EPA
8260D
11/19/20
05:03
REF
FINAL This
report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 38 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-37-6 Lab Sample ID:CD18880-13 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:20 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.00
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Hexachlorobutadiene [87-68-3]^
0.00039
U
mg/kg
dry
1
0.00039
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
Isopropyl benzene [98-82-8]^
0.00017
U
mg/kg
dry
1
0.00017
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.00041
U
mg/kg
dry
1
0.00041
0.0022
OK18035
EPA 8260D
11/19/20
05:03
REF
Methylene Chloride [75-09-2]^
0.00081
U
mg/kg
dry
1
0.00081
0.0022
OK18035
EPA 8260D
11/19/20
05:03
REF QV-01
Methyl-tert-Butyl Ether [1634-04-4]^
0.00033
U
mg/kg
dry
1
0.00033
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
Naphthalene [91-20-3]^
0.00030
U
mg/kg
dry
1
0.00030
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
n-Butyl Benzene [104-51-8]^
0.00014
U
mg/kg
dry
1
0.00014
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
n-Propyl Benzene [103-65-1]^
0.00020
U
mg/kg
dry
1
0.00020
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
o-Xylene [95-47-6]^
0.00024
U
mg/kg
dry
1
0.00024
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
sec-Butylbenzene [135-98-8]^
0.0011
U
mg/kg
dry
1
0.0011
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
Styrene [100-42-5]^
0.0011
U
mg/kg
dry
1
0.0011
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
tert-Butylbenzene [98-06-6]^
0.00019
U
mg/kg
dry
1
0.00019
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
Tetrachloroethene [127-18-4]^
0.00031
U
mg/kg
dry
1
0.00031
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
Toluene [108-88-3]^
0.00027
U
mg/kg
dry
1
0.00027
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
trans-1,2-Dichloroethene [156-60-5]^
0.00041
U
mg/kg
dry
1
0.00041
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF QV-01
trans-1,3-Dichloropropene [10061-02-6]^
0.00043
U
mg/kg
dry
1
0.00043
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
Trichloroethene [79-01-6]^
0.00036
U
mg/kg
dry
1
0.00036
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
Trichlorofluoromethane [75-69-4]^
0.00029
U
mg/kg
dry
1
0.00029
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
Vinyl chloride [75-01-4]^
0.00027
U
mg/kg
dry
1
0.00027
0.0011
OK18035
EPA 8260D
11/19/20
05:03
REF
Xylenes (Total) [1330-20-7]^
0.00062
U
mg/kg
dry
1
0.00062
0.0033
OK18035
EPA 8260D
11/19/20
05:03
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
4-Bromofluorobenzene
32
1
50.0
63 %
50-127
OK18035
EPA 6260D
11119120 05:03
REF
Dlbromofluoromethane
37
1
50.0
74 %
52-128
OK18035
EPA 8260D
11119120 05:03
REF
Toluene-d8
34
1
50.0
69 %
57-124
OK18035
EPA 8260D
11119120 05:03
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay
Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.58
UD
mg/kg dry
20
0.58
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
1,2-Dichlorobenzene [95-50-1]^
0.51
UD
mg/kg dry
20
0.51
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
1,3-Dichlorobenzene [541-73-1]^
0.44
UD
mg/kg dry
20
0.44
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
1,4-Dichlorobenzene [106-46-7]^
0.47
UD
mg/kg dry
20
0.47
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
1- Methyl naphthalene [90-12-0]^
0.60
UD
mg/kg dry
20
0.60
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2,4,5-Trichlorophenol[95-95-4]^
0.60
UD
mg/kg dry
20
0.60
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2,4,6-Trichlorophenol[88-06-2]^
0.60
UD
mg/kg dry
20
0.60
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2,4-Dichlorophenol [120-83-2]^
0.53
UD
mg/kg dry
20
0.53
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2,4-Di methyl phenol [105-67-9]^
0.96
UD
mg/kg dry
20
0.96
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2,4-Dinitrophenol [51-28-5]^
0.96
UD
mg/kg dry
20
0.96
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2,4-Dinitrotoluene [121-14-2]^
0.62
UD
mg/kg dry
20
0.62
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2,6-Dinitrotoluene [606-20-2]^
0.69
UD
mg/kg dry
20
0.69
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2-Chloronaphthalene [91-58-7]^
0.62
UD
mg/kg dry
20
0.62
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2-Chlorophenol [95-57-8]^
0.56
UD
mg/kg dry
20
0.56
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2-Methyl-4,6-dinitrophenol[534-52-1]^
0.73
UD
mg/kg dry
20
0.73
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
QV-01,
R-05
2- Methyl naphthalene [91-57-6]^
0.62
UD
mg/kg dry
20
0.62
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2-Methylphenol [95-48-7]^
0.56
UD
mg/kg dry
20
0.56
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
2-Nitroaniline [88-74-4]^
0.67
UD
mg/kg dry
20
0.67
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
FINAL
This report relates only
to the
sample as received by the laboratory,
and may only
be reproduced in full.
Page
39 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-37-6" Lab Sample ID:CD18880-13 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:20 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.00
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay
Notes
2-Nitrophenol [88-75-5]^
0.69
UD
mg/kg dry
20
0.69
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
3 & 4-Methylphenol[108-39-4/106-44-5]^
0.58
UD
mg/kg dry
20
0.58
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
3,3'-Dichlorobenzidine [91-94-1]^
2.2
UD
mg/kg dry
20
2.2
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
3-Nitroaniline [99-09-2]^
0.80
UD
mg/kg dry
20
0.80
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
4-Bromophenyl-phenylether[101-55-3]^
0.60
UD
mg/kg dry
20
0.60
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
4-Chloro-3-methylphenol[59-50-7]^
0.73
UD
mg/kg dry
20
0.73
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
4-Chloroaniline [106-47-8]^
2.1
UD
mg/kg dry
20
2.1
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
4-Chlorophenyl-phenylether[7005-72-3]^
0.58
UD
mg/kg dry
20
0.58
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
4-Nitroaniline [100-01-6]^
1.2
UD
mg/kg dry
20
1.2
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
4-Nitrophenol [100-02-7]^
0.69
UD
mg/kg dry
20
0.69
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Acenaphthene [83-32-9]^
2.2
JD
mg/kg dry
20
0.62
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Acenaphthylene [208-96-8]^
0.62
UD
mg/kg dry
20
0.62
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Anthracene [120-12-7]^
2.3
JD
mg/kg dry
20
0.84
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Benzidine [92-87-5]^
2.4
UD
mg/kg dry
20
2.4
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Benzo(a)anthracene [56-55-3]^
25
D
mg/kg dry
20
0.62
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Benzo(a)pyrene [50-32-8]^
37
D
mg/kg dry
20
0.73
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Benzo(b)fuoranthene [205-99-2]^
39
D
mg/kg dry
20
0.40
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Benzo(g,h,i)perylene [191-24-2]^
32
D
mg/kg dry
20
1.0
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
1-04,
R-05
Benzo(k)fluoranthene [207-08-9]^
15
D
mg/kg
dry
20
0.73
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Benzoic acid [65-85-O]^
3.3
UD
mg/kg
dry
20
3.3
38
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Benzyl alcohol [100-51-6]^
0.51
UD
mg/kg
dry
20
0.51
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Bis(2-chloroethoxy)methane [111-91-1]^
0.56
UD
mg/kg
dry
20
0.56
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Bis(2-chloroethyl)ether[111-44-4]^
0.96
UD
mg/kg
dry
20
0.96
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Bis(2-chloroisopropyl)ether[108-60-1]^
0.53
UD
mg/kg
dry
20
0.53
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Bis(2-ethylhexyl)phthalate [117-81-7]^
0.78
UD
mg/kg
dry
20
0.78
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Butyl benzylphtha late [85-68-7]^
0.89
UD
mg/kg
dry
20
0.89
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Chrysene [218-01-9]^
30
D
mg/kg
dry
20
0.67
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Dibenzo(a,h)anthracene [53-70-3]^
1.1
UD
mg/kg
dry
20
1.1
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Dibenzofuran [132-64-9]^
0.60
UD
mg/kg
dry
20
0.60
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Diethylphtha late [84-66-2]^
0.62
UD
mg/kg
dry
20
0.62
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Dimethylphtha late [131-11-3]^
0.73
UD
mg/kg
dry
20
0.73
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Di-n-butylphthalate [84-74-2]^
0.91
UD
mg/kg
dry
20
0.91
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Di-n-octylphthalate [117-84-O]^
0.73
UD
mg/kg
dry
20
0.73
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Fluoranthene [206-44-0]^
21
D
mg/kg
dry
20
0.80
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Fluorene [86-73-7]^
0.90
JD
mg/kg
dry
20
0.64
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Hexachlorobenzene [118-74-1]^
0.58
UD
mg/kg
dry
20
0.58
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Hexachlorobutadiene [87-68-3]^
0.58
UD
mg/kg
dry
20
0.58
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Hexachlorocyclopentadiene [77-47-4]^
0.87
UD
mg/kg
dry
20
0.87
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Hexachloroethane [67-72-1]^
0.47
UD
mg/kg
dry
20
0.47
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Indeno(1,2,3-cd)pyrene [193-39-5]^
22
D
mg/kg
dry
20
1.0
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Isophorone [78-59-1]^
0.67
UD
mg/kg
dry
20
0.67
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Naphthalene [91-20-3]^
0.62
UD
mg/kg
dry
20
0.62
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
Nitrobenzene [98-95-3]^
0.58
UD
mg/kg
dry
20
0.58
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
N-Nitrosodimethylamine [62-75-9]^
0.47
UD
mg/kg
dry
20
0.47
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
N-Nitroso-di-n-propylamine [621-64-7]^
1.8
UD
mg/kg
dry
20
1.8
7.3
OK19001
EPA
8270E
11/23/20 21:00
DFM
R-05
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 40 of 107

(� �Eo
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ANALYTICAL RESULTS
Description: HA-37-6 Lab Sample ID:CD18880-13 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:20 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.00
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX
Notes
N-nitrosodiphenylamine/Diphenylamine
1.2
UD
mg/kg dry
20
1.2
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
0.73
UD
mg/kg dry
20
0.73
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Phenanthrene [85-01-8]^
13
D
mg/kg dry
20
0.60
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Phenol [108-95-2]^
0.49
UD
mg/kg dry
20
0.49
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Pyrene [129-00-O]^
20
D
mg/kg dry
20
0.84
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Pyridine [110-86-1]^
1.8
UD
mg/kg dry
20
1.8
7.3
OK19001
EPA 8270E
11/23/20 21:00
DFM
R-05
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
2,4,6-Tribromophenol
4.1
20
3.70
112 %
28-130
OK19001
EPA 8270E
11123120 21:00
DFM
R-05
2-Fluorobiphenyl
1.9
20
1.65
104 %
56-120
OK19001
EPA 8270E
11123120 21:00
DFM
R-05
2-Fluorophenol
3.6
20
3.70
97 %
49-126
OK19001
EPA 8270E
11123120 21:00
DFM
R-05
Nitrobenzene-d5
1.7
20
1.65
90 %
50-117
OK19001
EPA 8270E
11123120 21:00
DFM
R-05
Phenol-d5
3.9
20
3.70
105 %
56-120
OK19001
EPA 8270E
11123120 21:00
DFM
R-05
Terphenyl-d14
1.3
20
1.65
69 %
36-151
OK19001
EPA 8270E
11123120 21:00
DFM
R-05
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
By
Notes
Lead [7439-92-1]^
20.0
mg/kg dry
1
0.133 0.556
OK20031
EPA 6010D
11/23/20 15:08
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 41 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-37-18" Lab Sample ID:CD18880-14 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:25 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.39
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certfied anaiyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.028
U
mg/kg dry
1
0.028
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
1,2-Dichlorobenzene [95-50-1]^
0.025
U
mg/kg dry
1
0.025
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
1,3-Dichlorobenzene [541-73-1]^
0.022
U
mg/kg dry
1
0.022
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
1,4-Dichlorobenzene [106-46-7]^
0.023
U
mg/kg dry
1
0.023
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
1-Methylnaphthalene [90-12-O]^
0.029
U
mg/kg dry
1
0.029
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2,4,5-Trichlorophenol [95-95-4]^
0.029
U
mg/kg dry
1
0.029
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2,4,6-Trichlorophenol [88-06-2]^
0.029
U
mg/kg dry
1
0.029
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2,4-Dichlorophenol [120-83-2]^
0.026
U
mg/kg dry
1
0.026
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2,4-Dimethylphenol [105-67-9]^
0.047
U
mg/kg dry
1
0.047
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2,4-Dinitrophenol [51-28-5]^
0.047
U
mg/kg dry
1
0.047
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2,4-Dinitrotoluene [121-14-2]^
0.030
U
mg/kg dry
1
0.030
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2,6-Dinitrotoluene [606-20-2]^
0.034
U
mg/kg dry
1
0.034
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2-Chloronaphthalene [91-58-7]^
0.030
U
mg/kg dry
1
0.030
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2-Chlorophenol [95-57-8]^
0.027
U
mg/kg dry
1
0.027
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]^
0.036
U
mg/kg dry
1
0.036
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2-Methylnaphthalene [91-57-6]^
0.030
U
mg/kg dry
1
0.030
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2-Methylphenol [95-48-7]^
0.027
U
mg/kg dry
1
0.027
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2-Nitroaniline [88-74-4]^
0.032
U
mg/kg dry
1
0.032
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
2-Nitrophenol [88-75-5]^
0.034
U
mg/kg dry
1
0.034
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]^
0.028
U
mg/kg dry
1
0.028
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
3,3'-Dichlorobenzidine [91-94-1]^
0.11
U
mg/kg dry
1
0.11
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
3-Nitroaniline [99-09-2]^
0.039
U
mg/kg dry
1
0.039
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
4-Bromophenyl-phenylether [101-55-3]^
0.029
U
mg/kg dry
1
0.029
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
4-Chloro-3-methylphenol [59-50-7]^
0.036
U
mg/kg dry
1
0.036
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
4-Chloroaniline [106-47-8]^
0.10
U
mg/kg dry
1
0.10
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
4-Chlorophenyl-phenylether [7005-72-3]^
0.028
U
mg/kg dry
1
0.028
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
4-Nitroaniline [100-01-6]^
0.057
U
mg/kg dry
1
0.057
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
4-Nitrophenol [100-02-7]^
0.034
U
mg/kg dry
1
0.034
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Acenaphthene [83-32-9]^
0.030
U
mg/kg dry
1
0.030
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Acenaphthylene [208-96-8]^
0.030
U
mg/kg dry
1
0.030
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Anthracene[120-12-7]^
0.041
U
mg/kg dry
1
0.041
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Benzidine [92-87-5]^
0.12
U
mg/kg dry
1
0.12
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Benzo(a)anthracene [56-55-3]^
0.18
J
mg/kg dry
1
0.030
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Benzo(a)pyrene [50-32-8]^
0.29
J
mg/kg dry
1
0.036
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Benzo(b)fluoranthene [205-99-2]^
0.26
J
mg/kg dry
1
0.019
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Benzo(g,h,i)perylene [191-24-2]^
0.20
J
mg/kg dry
1
0.051
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Benzo(k)fluoranthene [207-08-9]^
0.076
J
mg/kg dry
1
0.036
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Benzoic acid [65-85-O]^
0.16
U
mg/kg dry
1
0.16
1.8
OK25001
EPA 8270E
11/25/20 16:34
DFM
Benzyl alcohol [100-51-6]^
0.025
U
mg/kg dry
1
0.025
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
0.027
U
mg/kg dry
1
0.027
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Bis(2-chloroethyl)ether [111-44-4]^
0.047
U
mg/kg dry
1
0.047
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Bis(2-chloroisopropyl)ether [108-60-1]^
0.026
U
mg/kg dry
1
0.026
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]^
0.038
U
mg/kg dry
1
0.038
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Butylbenzylphthalate [85-68-7]^
0.043
U
mg/kg dry
1
0.043
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Chrysene [218-01-9]^
0.24
J
mg/kg dry
1
0.032
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Dibenzo(a,h)anthracene [53-70-3]^
0.21
J
mg/kg dry
1
0.055
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Dibenzofuran [132-64-9]^
0.029
U
mg/kg dry
1
0.029
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
FINAL
This report relates only
to the
sample as received by the laboratory,
and may only be reproduced in full.
Page 42 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-37-18" Lab Sample ID:CD18880-14 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:25 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.39
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified anaiyte [NC 591]
Analvte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Diethylphthalate [84-66-2]^
0.030
U
mg/kg dry
1
0.030
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Dimethylphthalate [131-11-3]^
0.036
U
mg/kg dry
1
0.036
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Di-n-butylphthalate [84-74-2]^
0.044
U
mg/kg dry
1
0.044
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Di-n-octylphthalate [117-84-O]^
0.036
U
mg/kg dry
1
0.036
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Fluoranthene [206-44-O]^
0.19
J
mg/kg dry
1
0.039
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Fluorene [86-73-7]^
0.031
U
mg/kg dry
1
0.031
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Hexachlorobenzene [118-74-1]^
0.028
U
mg/kg dry
1
0.028
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Hexachlorobutadiene [87-68-3]^
0.028
U
mg/kg dry
1
0.028
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Hexachlorocyclopentadiene [77-47-4]^
0.042
U
mg/kg dry
1
0.042
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Hexachloroethane [67-72-1]^
0.023
U
mg/kg dry
1
0.023
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
0.27
J
mg/kg dry
1
0.051
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Isophorone[78-59-1]^
0.032
U
mg/kg dry
1
0.032
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Naphthalene [91-20-3]^
0.030
U
mg/kg dry
1
0.030
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Nitrobenzene [98-95-3]^
0.028
U
mg/kg dry
1
0.028
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
N-Nitrosodimethylamine [62-75-9]^
0.023
U
mg/kg dry
1
0.023
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
0.088
U
mg/kg dry
1
0.088
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
N-nitrosodiphenylamine/Diphenylamine
0.058
U
mg/kg dry
1
0.058
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
0.036
U
mg/kg dry
1
0.036
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Phenanthrene [85-01-8]^
0.10
J
mg/kg dry
1
0.029
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Phenol[108-95-2]^
0.024
U
mg/kg dry
1
0.024
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Pyrene [129-00-O]^
0.23
J
mg/kg dry
1
0.041
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Pyridine [110-86-1]^
0.089
U
mg/kg dry
1
0.089
0.36
OK25001
EPA 8270E
11/25/20 16:34
DFM
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analyzed
fly Notes
2,4,6-Tribromophenol
3.8
1
3.61
106 %
28-130
OK25001
EPA 8270E
1112512016:34
DFM
2-Fluorobiphenyl
1.7
1
1.80
94 %
56-120
OK25001
EPA 8270E
1112512016:34
DFM
2-Fluorophenol
3.3
1
3.61
93 %
49-126
OK25001
EPA 8270E
1112512016:34
DFM
Nitrobenzene-d5
1.7
1
1.80
93 %
50-117
OK25001
EPA 8270E
11/25/2016:34
DFM
Phenol-d5
3.5
1
3.61
98 %
56-120
OK25001
EPA 8270E
11/25/2016:34
DFM
Terphenyl-d14
1.8
1
1.80
98 %
36-151
OK25001
EPA 8270E
111251201634
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified anaiyte [NC 591]
Analvte MAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^
6.45
mg/kg dry
1
0.130 0.541
OK30010
EPA 6010D
12/01/20 09:56
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 43 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-38-6" Lab Sample ID:CD18880-15 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.08
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00016
u
mg/kg
dry
0.833
0.00016
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,1,1-Trichloroethane [71-55-6]A
0.00024
u
mg/kg
dry
0.833
0.00024
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00020
u
mg/kg
dry
0.833
0.00020
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,1,2-Trichloroethane [79-00-5]A
0.00024
u
mg/kg
dry
0.833
0.00024
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,1-Dichloroethane [75-34-3]A
0.00024
u
mg/kg
dry
0.833
0.00024
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
QV-01
1,1-Dichloroethene [75-35-4]A
0.00029
u
mg/kg
dry
0.833
0.00029
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,1-Dichloropropene [563-58-6]A
0.00016
u
mg/kg
dry
0.833
0.00016
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00027
u
mg/kg
dry
0.833
0.00027
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,2,3-Trichloropropane [96-18-4]A
0.00063
u
mg/kg
dry
0.833
0.00063
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00026
u
mg/kg
dry
0.833
0.00026
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00017
u
mg/kg
dry
0.833
0.00017
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00077
u
mg/kg
dry
0.833
0.00077
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,2-Dibromoethane [106-93-4]A
0.00045
u
mg/kg
dry
0.833
0.00045
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,2-Dichlorobenzene [95-50-1]A
0.00026
u
mg/kg
dry
0.833
0.00026
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,2-Dichloroethane [107-06-2]A
0.00040
u
mg/kg
dry
0.833
0.00040
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,2-Dichloropropane [78-87-5]A
0.00025
u
mg/kg
dry
0.833
0.00025
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00020
u
mg/kg
dry
0.833
0.00020
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,3-Dichlorobenzene [541-73-1]A
0.00022
u
mg/kg
dry
0.833
0.00022
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,3-Dichloropropane [142-28-9]A
0.00028
u
mg/kg
dry
0.833
0.00028
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
1,4-Dichlorobenzene [106-46-7]A
0.00020
u
mg/kg
dry
0.833
0.00020
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
2,2-Dichloropropane [594-20-7]A
0.00023
u
mg/kg
dry
0.833
0.00023
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
2-Butanone [78-93-3]A
0.00076
u
mg/kg
dry
0.833
0.00076
0.0049
OK18035
EPA
8260D
11/19/20
05:33
REF
QV-01
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00016
u
mg/kg
dry
0.833
0.00016
0.0049
OK18035
EPA
8260D
11/19/20
05:33
REF
2-Chlorotoluene [95-49-8]A
0.00018
u
mg/kg
dry
0.833
0.00018
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
2-Hexanone [591-78-6]A
0.00073
u
mg/kg
dry
0.833
0.00073
0.0049
OK18035
EPA
8260D
11/19/20
05:33
REF
4-Chlorotoluene [106-43-4]A
0.00025
u
mg/kg
dry
0.833
0.00025
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
4-Isopropyltoluene [99-87-6]A
0.00070
1
mg/kg
dry
0.833
0.00016
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
4-Methyl-2-pentanone [108-10-1]A
0.00056
u
mg/kg
dry
0.833
0.00056
0.0049
OK18035
EPA
8260D
11/19/20
05:33
REF
Acetone [67-64-1]A
0.014
u
mg/kg
dry
0.833
0.014
0.020
OK18035
EPA
8260D
11/19/20
05:33
REF
Benzene [71-43-2]A
0.00017
u
mg/kg
dry
0.833
0.00017
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
QV-01
Bromobenzene [108-86-1]A
0.00022
u
mg/kg
dry
0.833
0.00022
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Bromochloromethane [74-97-5]A
0.00040
u
mg/kg
dry
0.833
0.00040
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Bromodichloromethane [75-27-4]A
0.00024
u
mg/kg
dry
0.833
0.00024
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Bromoform [75-25-2]A
0.00044
u
mg/kg
dry
0.833
0.00044
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Bromomethane [74-83-9]A
0.00031
u
mg/kg
dry
0.833
0.00031
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Carbon disulfide [75-15-0]A
0.00038
u
mg/kg
dry
0.833
0.00038
0.0049
OK18035
EPA
8260D
11/19/20
05:33
REF
QV-01
Carbon Tetrachloride [56-23-5]A
0.00022
u
mg/kg
dry
0.833
0.00022
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Chlorobenzene [108-90-7]A
0.00017
u
mg/kg
dry
0.833
0.00017
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Chloroethane [75-00-3]A
0.00024
u
mg/kg
dry
0.833
0.00024
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Chloroform [67-66-3]A
0.00018
u
mg/kg
dry
0.833
0.00018
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Chloromethane [74-87-3]A
0.00021
u
mg/kg
dry
0.833
0.00021
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
QV-01
cis-1,2-Dichloroethene [156-59-2]A
0.00023
u
mg/kg
dry
0.833
0.00023
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00017
u
mg/kg
dry
0.833
0.00017
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Dibromochloromethane [124-48-1]A
0.00034
u
mg/kg
dry
0.833
0.00034
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Dibromomethane [74-95-3]A
0.00032
u
mg/kg
dry
0.833
0.00032
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Dichlorodifluoromethane [75-71-8]A
0.00044
u
mg/kg
dry
0.833
0.00044
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
Ethylbenzene [100-41-4]A
0.00020
u
mg/kg
dry
0.833
0.00020
0.00098
OK18035
EPA
8260D
11/19/20
05:33
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 44 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-38-6" Lab Sample ID:CD18880-15 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.08
Volatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analvte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
Hexachlorobutadiene [87-68-3]A
0.00034
U
mg/kg
dry
0.833
0.00034
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
Isopropylbenzene [98-82-8]A
0.00015
U
mg/kg
dry
0.833
0.00015
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
m,p-Xylenes [108-38-3/106-42-3]A
0.00036
U
mg/kg
dry
0.833
0.00036
0.0020
OK18035
EPA 8260D
11/19/20
05:33
REF
Methylene Chloride [75-09-2]A
0.00072
U
mg/kg
dry
0.833
0.00072
0.0020
OK18035
EPA 8260D
11/19/20
05:33
REF QV-01
Methyl-tert-Butyl Ether [1634-04-4]A
0.00029
U
mg/kg
dry
0.833
0.00029
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
Naphthalene [91-20-3]A
0.00026
U
mg/kg
dry
0.833
0.00026
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
n-Butyl Benzene [104-51-8]A
0.00013
U
mg/kg
dry
0.833
0.00013
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
n-Propyl Benzene [503-65-1]A
0.00018
U
mg/kg
dry
0.833
0.00018
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
o-Xylene [95-47-6]A
0.00022
U
mg/kg
dry
0.833
0.00022
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
sec-Butylbenzene [135-98-8]A
0.00093
U
mg/kg
dry
0.833
0.00093
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
Styrene [500-42-5]A
0.0066
mg/kg
dry
0.833
0.00096
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
tert-Butyl benzene [98-06-6]A
0.00017
U
mg/kg
dry
0.833
0.00017
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
Tetrachloroethene [127-18-4]A
0.00027
U
mg/kg
dry
0.833
0.00027
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
Toluene [108-88-3]A
0.00024
U
mg/kg
dry
0.833
0.00024
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
trans-1,2-Dichloroethene [156-60-5]A
0.00036
U
mg/kg
dry
0.833
0.00036
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF QV-01
trans-1,3-Dichloropropene [10061-02-6]A
0.00038
U
mg/kg
dry
0.833
0.00038
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
Trichloroethene [79-01-6]A
0.00031
U
mg/kg
dry
0.833
0.00031
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
Trichlorofluoromethane [75-69-4]A
0.00025
U
mg/kg
dry
0.833
0.00025
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
Vinyl chloride [75-01-4]A
0.00024
U
mg/kg
dry
0.833
0.00024
0.00098
OK18035
EPA 8260D
11/19/20
05:33
REF
Xylenes (Total) [1330-20-7]A
0.00055
U
mg/kg
dry
0.833
0.00055
0.0029
OK18035
EPA 8260D
11/19/20
05:33
REF
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
" Notes
4-Bromofluorobenzene
32
0.833
50.0
65 %
50-127
OK18035
EPA 8260D
11119120 05:33
REF
Dibromofluoromethane
36
0.833
50.0
72 %
52-128
OK18035
EPA 8260D
11119120 05:33
REF
Toluene-&
35
0.833
50.0
70 %
57-124
OK18035
EPA 8260D
11119120 05:33
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 5911
Analvte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]A
0.031
U
mg/kg dry
1
0.031
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
1,2-Dichlorobenzene [95-50-1]A
0.027
U
mg/kg dry
1
0.027
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
1,3-Dichlorobenzene [541-73-1]A
0.024
U
mg/kg dry
1
0.024
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
1,4-Dichlorobenzene [106-46-7]A
0.025
U
mg/kg dry
1
0.025
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
1-Methylnaphthalene [90-12-0]A
0.032
U
mg/kg dry
1
0.032
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2,4,5-Trichlorophenol [95-95-4]A
0.032
U
mg/kg dry
1
0.032
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2,4,6-Trichlorophenol [88-06-2]A
0.032
U
mg/kg dry
1
0.032
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2,4-Dichlorophenol [120-83-2]A
0.028
U
mg/kg dry
1
0.028
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2,4-Dimethylphenol [105-67-9]A
0.051
U
mg/kg dry
1
0.051
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2,4-Dinitrophenol [51-28-5]A
0.051
U
mg/kg dry
1
0.051
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2,4-Dinitrotoluene [121-14-2]A
0.033
U
mg/kg dry
1
0.033
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2,6-Dinitrotoluene [606-20-2]A
0.036
U
mg/kg dry
1
0.036
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2-Chloronaphthalene [91-58-7]A
0.033
U
mg/kg dry
1
0.033
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2-Chlorophenol [95-57-8]A
0.029
U
mg/kg dry
1
0.029
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]A
0.039
U
mg/kg dry
1
0.039
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM QV-01
2-Methylnaphthalene [91-57-6]A
0.033
U
mg/kg dry
1
0.033
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2-Methylphenol [95-48-7]A
0.029
U
mg/kg dry
1
0.029
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
2-Nitroaniline [88-74-4]A
0.035
U
mg/kg dry
1
0.035
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 45 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-38-6" Lab Sample ID:CD18880-15 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.08
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]^
0.036
U
mg/kg dry
1
0.036
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]^
0.031
U
mg/kg dry
1
0.031
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
3,3'-Dichlorobenzidine [91-94-1]^
0.12
U
mg/kg dry
1
0.12
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
3-Nitroaniline [99-09-2]^
0.042
U
mg/kg dry
1
0.042
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
4-Bromophenyl-phenylether [101-55-3]^
0.032
U
mg/kg dry
1
0.032
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
4-Chloro-3-methylphenol [59-50-7]^
0.039
U
mg/kg dry
1
0.039
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
4-Chloroaniline [106-47-8]^
0.11
U
mg/kg dry
1
0.11
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
4-Chlorophenyl-phenylether [7005-72-3]^
0.031
U
mg/kg dry
1
0.031
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
4-Nitroaniline [100-01-6]^
0.062
U
mg/kg dry
1
0.062
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
4-Nitrophenol [100-02-7]^
0.036
U
mg/kg dry
1
0.036
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Acenaphthene [83-32-9]^
0.044
J
mg/kg dry
1
0.033
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Acenaphthylene [208-96-8]^
0.033
U
mg/kg dry
1
0.033
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Anthracene [120-12-7]^
0.056
J
mg/kg dry
1
0.045
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Benzidine [92-87-5]^
0.13
U
mg/kg dry
1
0.13
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Benzo(a)anthracene [56-55-3]^
0.38
J
mg/kg dry
1
0.033
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Benzo(a)pyrene [50-32-8]^
0.61
mg/kg dry
1
0.039
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Benzo(b)fluoranthene [205-99-2]^
0.63
mg/kg dry
1
0.021
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Benzo(g,h,i)perylene [191-24-2]^
0.59
mg/kg dry
1
0.055
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM 3-04
Benzo(k)fluoranthene [207-08-9]^
0.23
J
mg/kg dry
1
0.039
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Benzoic acid [65-85-0] ^
1.6
J
mg/kg dry
1
0.18
2.0
OK19001
EPA 8270E
11/23/20 22:04
DFM
Benzyl alcohol [100-51-6]^
0.027
U
mg/kg dry
1
0.027
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Bis(2-chloroethoxy)methane [111-91-1]^
0.029
U
mg/kg dry
1
0.029
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Bis(2-chloroethyl)ether [111-44-4]^
0.051
U
mg/kg dry
1
0.051
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Bis(2-chloroisopropyl)ether [108-60-1]^
0.028
U
mg/kg dry
1
0.028
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Bis(2-ethylhexyl)phthalate
0.072
J
mg/kg dry
1
0.041
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
[117-81-7]^
Butylbenzylphthalate [85-68-7]^
0.047
U
mg/kg dry
1
0.047
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Chrysene [218-01-9]1
0.42
mg/kg dry
1
0.035
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Dibenzo(a,h)anthracene [53-70-3]^
0.060
U
mg/kg dry
1
0.060
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Dibenzofuran [132-64-9]^
0.032
U
mg/kg dry
1
0.032
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Diethylphthalate [84-66-2]^
0.033
U
mg/kg dry
1
0.033
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Dimethylphthalate [131-11-3]^
0.039
U
mg/kg dry
1
0.039
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Di-n-butylphthalate [84-74-2]^
0.048
U
mg/kg dry
1
0.048
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Di-n-octylphthalate [117-84-O]^
0.039
U
mg/kg dry
1
0.039
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Fluoranthene [206-44-0]^
0.36
J
mg/kg dry
1
0.042
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Fluorene [86-73-7]^
0.034
U
mg/kg dry
1
0.034
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Hexachlorobenzene [118-74-1]^
0.031
U
mg/kg dry
1
0.031
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Hexachlorobutadiene [87-68-3]^
0.031
U
mg/kg dry
1
0.031
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Hexachlorocyclopentadiene [77-47-4]^
0.046
U
mg/kg dry
1
0.046
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Hexachloroethane [67-72-1]^
0.025
U
mg/kg dry
1
0.025
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
0.56
mg/kg dry
1
0.055
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Isophorone[78-59-1]^
0.035
U
mg/kg dry
1
0.035
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Naphthalene [91-20-3]^
0.033
U
mg/kg dry
1
0.033
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Nitrobenzene [98-95-3]^
0.031
U
mg/kg dry
1
0.031
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
N-Nitrosodimethylamine [62-75-9]^
0.025
U
mg/kg dry
1
0.025
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
0.095
U
mg/kg dry
1
0.095
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 46 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-38-6 Lab Sample ID:CD18880-15 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.08
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
N-nitrosodiphenylamine/Diphenylamine
0.063
U
mg/kg dry
1
0.063
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
0.039
U
mg/kg dry
1
0.039
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Phenanthrene [85-01-8]^
0.27
1
mg/kg dry
1
0.032
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Phenol[108-95-2]^
0.026
U
mg/kg dry
1
0.026
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Pyrene [129-00-O]^
0.30
1
mg/kg dry
1
0.045
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Pyridine [110-86-1]^
0.096
U
mg/kg dry
1
0.096
0.39
OK19001
EPA 8270E
11/23/20 22:04
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.5
1
3.92
116 %
28-130
OK19001
EPA 8270E
11123120 22:04
DFM
2-Fluorobiphenyl
2.0
1
1.96
102 %
56-120
OK19001
EPA 8270E
11123120 22:04
DFM
2-Fluorophenol
3.9
1
3,92
99 %
49-126
OK19001
EPA 8270E
11123120 22:04
DFM
Nitrobenzene-d5
1.9
1
1,96
97 %
50-117
OK19001
EPA 8270E
11123120 22:04
DFM
Phenol-d5
4.3
1
3,92
110 %
56-120
OK19001
EPA 8270E
11123120 22:04
DFM
Terphenyl-d14
1.2
1
1,96
63 %
36-151
OK19001
EPA 8270E
11123120 22:04
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^
48.5
mg/kg dry
1
0.141 0.588
OK20031
EPA 6010D
11/23/20 15:15
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 47 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-38-18" Lab Sample ID:CD18880-16 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:45 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.67
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]A
0.028
U
mg/kg
dry
1
0.028
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
1,2-Dichlorobenzene [95-50-1]A
0.025
U
mg/kg
dry
1
0.025
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
1,3-Dichlorobenzene [541-73-1]A
0.021
U
mg/kg
dry
1
0.021
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
1,4-Dichlorobenzene [106-46-7]A
0.022
U
mg/kg
dry
1
0.022
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
1-Methylnaphthalene [90-12-O]A
0.029
U
mg/kg
dry
1
0.029
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2,4,5-Trichlorophenol [95-95-4]A
0.029
U
mg/kg
dry
1
0.029
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2,4,6-Trichlorophenol [88-06-2]A
0.029
U
mg/kg
dry
1
0.029
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2,4-Dichlorophenol [120-83-2]A
0.026
U
mg/kg
dry
1
0.026
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2,4-Dimethylphenol [105-67-9]A
0.046
U
mg/kg
dry
1
0.046
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2,4-Dinitrophenol [51-28-5]A
0.046
U
mg/kg
dry
1
0.046
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2,4-Dinitrotoluene [121-14-2]A
0.030
U
mg/kg
dry
1
0.030
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2,6-Dinitrotoluene [606-20-2]A
0.033
U
mg/kg
dry
1
0.033
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2-Chloronaphthalene [91-58-7]A
0.030
U
mg/kg
dry
1
0.030
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2-Chlorophenol [95-57-8]A
0.027
U
mg/kg
dry
1
0.027
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]A
0.035
U
mg/kg
dry
1
0.035
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2-Methylnaphthalene [91-57-6]A
0.030
U
mg/kg
dry
1
0.030
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2-Methylphenol [95-48-7]A
0.027
U
mg/kg
dry
1
0.027
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2-Nitroaniline [88-74-4]A
0.032
U
mg/kg
dry
1
0.032
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
2-Nitrophenol [88-75-5]A
0.033
U
mg/kg
dry
1
0.033
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.028
U
mg/kg
dry
1
0.028
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.10
U
mg/kg
dry
1
0.10
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
3-Nitroaniline [99-09-2]A
0.038
U
mg/kg
dry
1
0.038
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.029
U
mg/kg
dry
1
0.029
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.035
U
mg/kg
dry
1
0.035
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
4-Chloroaniline [106-47-8]A
0.099
U
mg/kg
dry
1
0.099
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.028
U
mg/kg
dry
1
0.028
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
4-Nitroaniline [100-01-6]A
0.057
U
mg/kg
dry
1
0.057
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
4-Nitrophenol [100-02-7]A
0.033
U
mg/kg
dry
1
0.033
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Acenaphthene [83-32-9]A
0.030
U
mg/kg
dry
1
0.030
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Acenaphthylene [208-96-8]A
0.030
U
mg/kg
dry
1
0.030
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Anthracene[120-12-7]A
0.041
U
mg/kg
dry
1
0.041
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Benzidine [92-87-5]A
0.12
U
mg/kg
dry
1
0.12
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Benzo(a)anthracene [56-55-3]A
0.030
U
mg/kg
dry
1
0.030
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Benzo(a)pyrene [50-32-8]A
0.035
U
mg/kg
dry
1
0.035
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Benzo(b)fluoranthene [205-99-2]A
0.019
U
mg/kg
dry
1
0.019
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.050
U
mg/kg
dry
1
0.050
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Benzo(k)fluoranthene [207-08-9]A
0.035
U
mg/kg
dry
1
0.035
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Benzoic acid [65-85-O]A
0.16
U
mg/kg
dry
1
0.16
1.8
OK25001
EPA
8270E
11/25/20
13:25
DFM
Benzyl alcohol [100-51-6]A
0.025
U
mg/kg
dry
1
0.025
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.027
U
mg/kg
dry
1
0.027
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.046
U
mg/kg
dry
1
0.046
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.026
U
mg/kg
dry
1
0.026
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.037
U
mg/kg
dry
1
0.037
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Butylbenzylphthalate [85-68-7]A
0.043
U
mg/kg
dry
1
0.043
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Chrysene [218-01-9]A
0.032
U
mg/kg
dry
1
0.032
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.17
J
mg/kg
dry
1
0.054
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
Dibenzofuran [132-64-9]A
0.029
U
mg/kg
dry
1
0.029
0.35
OK25001
EPA
8270E
11/25/20
13:25
DFM
FINAL
This report relates only to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 48 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-38-18" Lab Sample ID:CD18880-16 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:45 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 93.67
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified anaiyte [NC 591]
Analvte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Diethylphthalate [84-66-2]^
0.030
U
mg/kg dry
1
0.030
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Dimethylphthalate [131-11-3]^
0.035
U
mg/kg dry
1
0.035
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Di-n-butylphthalate [84-74-2]^
0.044
U
mg/kg dry
1
0.044
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Di-n-octylphthalate [117-84-O]^
0.035
U
mg/kg dry
1
0.035
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM QV-01
Fluoranthene [206-44-O]^
0.038
U
mg/kg dry
1
0.038
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Fluorene [86-73-7]^
0.031
U
mg/kg dry
1
0.031
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Hexachlorobenzene [118-74-1]^
0.028
U
mg/kg dry
1
0.028
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Hexachlorobutadiene [87-68-3]^
0.028
U
mg/kg dry
1
0.028
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM QV-01
Hexachlorocyclopentadiene [77-47-4]^
0.042
U
mg/kg dry
1
0.042
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Hexachloroethane [67-72-1]^
0.022
U
mg/kg dry
1
0.022
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
0.17
J
mg/kg dry
1
0.050
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Isophorone[78-59-1]^
0.032
U
mg/kg dry
1
0.032
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Naphthalene [91-20-3]^
0.030
U
mg/kg dry
1
0.030
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Nitrobenzene [98-95-3]^
0.028
U
mg/kg dry
1
0.028
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
N-Nitrosodimethylamine [62-75-9]^
0.022
U
mg/kg dry
1
0.022
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
0.086
U
mg/kg dry
1
0.086
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
N-nitrosodiphenylamine/Diphenylamine
0.058
U
mg/kg dry
1
0.058
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
0.035
U
mg/kg dry
1
0.035
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Phenanthrene [85-01-8]^
0.029
U
mg/kg dry
1
0.029
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Phenol[108-95-2]^
0.023
U
mg/kg dry
1
0.023
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Pyrene [129-00-O]^
0.041
U
mg/kg dry
1
0.041
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Pyridine [110-86-1]^
0.088
U
mg/kg dry
1
0.088
0.35
OK25001
EPA 8270E
11/25/20 13:25
DFM
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analyzed
fly Notes
2,4,6-Tribromophenol
3.9
1
3.56
108 %
28-130
OK25001
EPA 8270E
1112512013:25
DFM
2-Fluorobiphenyl
1.6
1
1.78
90 %
56-120
OK25001
EPA 8270E
1112512013:25
DFM
2-Fluorophenol
3.2
1
3.56
89 %
49-126
OK25001
EPA 8270E
1112512013:25
DFM
Nitrobenzene-d5
1.5
1
1.78
87 %
50-117
OK25001
EPA 8270E
1112512013:25
DFM
Phenol-d5
3.4
1
3.56
94 %
56-120
OK25001
EPA 8270E
1112512013:25
DFM
Terphenyl-d14
2.0
1
1.78
111 %
36-151
OK25001
EPA 8270E
1112512013:25
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified anaiyte [NC 591]
Analvte MAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]A
4.91
mg/kg dry
1
0.128 0.534
OK30010
EPA 6010D
12/01/20 10:05
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 49 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-39-6" Lab Sample ID:CD18880-17 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:50 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.56
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00014
u
mg/kg
dry
0.821
0.00014
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,1,1-Trichloroethane [71-55-6]A
0.00022
u
mg/kg
dry
0.821
0.00022
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00018
u
mg/kg
dry
0.821
0.00018
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,1,2-Trichloroethane [79-00-5]A
0.00022
u
mg/kg
dry
0.821
0.00022
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,1-Dichloroethane [75-34-3]A
0.00022
u
mg/kg
dry
0.821
0.00022
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
QV-01
1,1-Dichloroethene [75-35-4]A
0.00027
u
mg/kg
dry
0.821
0.00027
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,1-Dichloropropene [563-58-6]A
0.00014
u
mg/kg
dry
0.821
0.00014
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00025
u
mg/kg
dry
0.821
0.00025
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,2,3-Trichloropropane [96-18-4]A
0.00057
u
mg/kg
dry
0.821
0.00057
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00024
u
mg/kg
dry
0.821
0.00024
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00015
u
mg/kg
dry
0.821
0.00015
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00070
u
mg/kg
dry
0.821
0.00070
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,2-Dibromoethane [506-93-4]A
0.00041
u
mg/kg
dry
0.821
0.00041
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,2-Dichlorobenzene [95-50-1]A
0.00024
u
mg/kg
dry
0.821
0.00024
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,2-Dichloroethane [507-06-2]A
0.00036
u
mg/kg
dry
0.821
0.00036
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,2-Dichloropropane [78-87-5]A
0.00023
u
mg/kg
dry
0.821
0.00023
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,3,5-Trimethylbenzene [508-67-8]A
0.00018
u
mg/kg
dry
0.821
0.00018
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,3-Dichlorobenzene [541-73-1]A
0.00020
u
mg/kg
dry
0.821
0.00020
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,3-Dichloropropane [142-28-9]A
0.00026
u
mg/kg
dry
0.821
0.00026
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
1,4-Dichlorobenzene [106-46-7]A
0.00018
u
mg/kg
dry
0.821
0.00018
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
2,2-Dichloropropane [594-20-7]A
0.00020
u
mg/kg
dry
0.821
0.00020
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
2-Butanone [78-93-3]A
0.00069
u
mg/kg
dry
0.821
0.00069
0.0044
OK18035
EPA
8260D
11/19/20
06:03
REF
QV-01
2-Chloroethyl Vinyl Ether [510-75-8]A
0.00014
u
mg/kg
dry
0.821
0.00014
0.0044
OK18035
EPA
8260D
11/19/20
06:03
REF
2-Chlorotoluene [95-49-8]A
0.00016
u
mg/kg
dry
0.821
0.00016
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
2-Hexanone [591-78-6]A
0.00067
u
mg/kg
dry
0.821
0.00067
0.0044
OK18035
EPA
8260D
11/19/20
06:03
REF
4-Chlorotoluene [106-43-4]A
0.00023
u
mg/kg
dry
0.821
0.00023
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
4-Isopropyltoluene [99-87-6]A
0.00014
u
mg/kg
dry
0.821
0.00014
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
4-Methyl-2-pentanone [108-10-1]A
0.00051
u
mg/kg
dry
0.821
0.00051
0.0044
OK18035
EPA
8260D
11/19/20
06:03
REF
Acetone [67-64-1]A
0.012
u
mg/kg
dry
0.821
0.012
0.018
OK18035
EPA
8260D
11/19/20
06:03
REF
Benzene [71-43-2]A
0.00015
u
mg/kg
dry
0.821
0.00015
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
QV-01
Bromobenzene [508-86-1]A
0.00020
u
mg/kg
dry
0.821
0.00020
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Bromochloromethane [74-97-5]A
0.00036
u
mg/kg
dry
0.821
0.00036
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Bromodichloromethane [75-27-4]A
0.00021
u
mg/kg
dry
0.821
0.00021
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Bromoform [75-25-2]A
0.00040
u
mg/kg
dry
0.821
0.00040
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Bromomethane [74-83-9]A
0.00028
u
mg/kg
dry
0.821
0.00028
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Carbon disulfide [75-15-0]A
0.00035
u
mg/kg
dry
0.821
0.00035
0.0044
OK18035
EPA
8260D
11/19/20
06:03
REF
QV-01
Carbon Tetrachloride [56-23-5]A
0.00020
u
mg/kg
dry
0.821
0.00020
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Chlorobenzene [508-90-7]A
0.00015
u
mg/kg
dry
0.821
0.00015
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Chloroethane [75-00-3]A
0.00022
u
mg/kg
dry
0.821
0.00022
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Chloroform [67-66-3]A
0.00016
u
mg/kg
dry
0.821
0.00016
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Chloromethane [74-87-3]A
0.00019
u
mg/kg
dry
0.821
0.00019
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
QV-01
cis-1,2-Dichloroethene [156-59-2]A
0.00020
u
mg/kg
dry
0.821
0.00020
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00015
u
mg/kg
dry
0.821
0.00015
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Dibromochloromethane [124-48-1]A
0.00031
u
mg/kg
dry
0.821
0.00031
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Dibromomethane [74-95-3]A
0.00029
u
mg/kg
dry
0.821
0.00029
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Dichlorodifluoromethane [75-71-8]A
0.00040
u
mg/kg
dry
0.821
0.00040
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
Ethylbenzene [100-41-4]A
0.00018
u
mg/kg
dry
0.821
0.00018
0.00089
OK18035
EPA
8260D
11/19/20
06:03
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 50 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-39-6 Lab Sample ID:CD18880-17 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:50 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.56
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Hexachlorobutadiene [87-68-3]^
0.00031
U
mg/kg
dry
0.821
0.00031
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
Isopropyl benzene [98-82-8]^
0.00013
U
mg/kg
dry
0.821
0.00013
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.00033
U
mg/kg
dry
0.821
0.00033
0.0018
OK18035
EPA 8260D
11/19/20
06:03
REF
Methylene Chloride [75-09-2]^
0.00065
U
mg/kg
dry
0.821
0.00065
0.0018
OK18035
EPA 8260D
11/19/20
06:03
REF QV-01
Methyl-tert-Butyl Ether [1634-04-4]^
0.00027
U
mg/kg
dry
0.821
0.00027
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
Naphthalene [91-20-3]^
0.00024
U
mg/kg
dry
0.821
0.00024
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
n-Butyl Benzene [104-51-8]^
0.00012
U
mg/kg
dry
0.821
0.00012
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
n-Propyl Benzene [103-65-1]^
0.00016
U
mg/kg
dry
0.821
0.00016
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
o-Xylene [95-47-6]^
0.00020
U
mg/kg
dry
0.821
0.00020
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
sec-Butylbenzene [135-98-8]^
0.00084
U
mg/kg
dry
0.821
0.00084
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
Styrene [100-42-5]^
0.00087
U
mg/kg
dry
0.821
0.00087
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
tert-Butylbenzene [98-06-6]^
0.00015
U
mg/kg
dry
0.821
0.00015
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
Tetrachloroethene [127-18-4]^
0.00025
U
mg/kg
dry
0.821
0.00025
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
Toluene [108-88-3]^
0.00021
U
mg/kg
dry
0.821
0.00021
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
trans-1,2-Dichloroethene [156-60-5]^
0.00033
U
mg/kg
dry
0.821
0.00033
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF QV-01
trans-1,3-Dichloropropene [10061-02-6]^
0.00035
U
mg/kg
dry
0.821
0.00035
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
Trichloroethene [79-01-6]^
0.00028
U
mg/kg
dry
0.821
0.00028
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
Trichlorofluoromethane [75-69-4]^
0.00023
U
mg/kg
dry
0.821
0.00023
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
Vinyl chloride [75-01-4]^
0.00021
U
mg/kg
dry
0.821
0.00021
0.00089
OK18035
EPA 8260D
11/19/20
06:03
REF
Xylenes (Total) [1330-20-7]^
0.00050
U
mg/kg
dry
0.821
0.00050
0.0027
OK18035
EPA 8260D
11/19/20
06:03
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
30
0.821
50.0
60 %
50-127
OK18035
EPA 6260D
11119120 06:03
REF
Dlbromofluoromethane
36
0.821
50.0
73 %
52-128
OK18035
EPA 8260D
11119120 06:03
REF
Toluene-d8
35
0.821
50.0
70 %
57-124
OK18035
EPA 8260D
11119120 06:03
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.028
U
mg/kg dry
1
0.028
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
1,2-Dichlorobenzene [95-50-1]^
0.025
U
mg/kg dry
1
0.025
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
1,3-Dichlorobenzene [541-73-1]^
0.022
U
mg/kg dry
1
0.022
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
1,4-Dichlorobenzene [106-46-7]^
0.023
U
mg/kg dry
1
0.023
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
1- Methyl naphthalene [90-12-0]^
0.029
U
mg/kg dry
1
0.029
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2,4,5-Trichlorophenol[95-95-4]^
0.029
U
mg/kg dry
1
0.029
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2,4,6-Trichlorophenol[88-06-2]^
0.029
U
mg/kg dry
1
0.029
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2,4-Dichlorophenol [120-83-2]^
0.026
U
mg/kg dry
1
0.026
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2,4-Di methyl phenol[105-67-9]^
0.046
U
mg/kg dry
1
0.046
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2,4-Dinitrophenol [51-28-5]^
0.046
U
mg/kg dry
1
0.046
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2,4-Dinitrotoluene [121-14-2]^
0.030
U
mg/kg dry
1
0.030
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2,6-Dinitrotoluene [606-20-2]^
0.033
U
mg/kg dry
1
0.033
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2-Chloronaphthalene [91-58-7]^
0.030
U
mg/kg dry
1
0.030
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2-Chlorophenol [95-57-8]^
0.027
U
mg/kg dry
1
0.027
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
0.036
U
mg/kg dry
1
0.036
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM QV-01
2- Methyl naphthalene [91-57-6]^
0.030
U
mg/kg dry
1
0.030
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2-Methylphenol [95-48-7]^
0.027
U
mg/kg dry
1
0.027
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
2-Nitroaniline [88-74-4]^
0.032
U
mg/kg dry
1
0.032
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 51 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-39-6" Lab Sample ID:CD18880-17 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:50 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.56
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]A
0.033
U
mg/kg
dry
1
0.033
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
3 & 4-Methylphenol [508-39-4/106-44-5]A
0.028
U
mg/kg
dry
1
0.028
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
U
mg/kg
dry
1
0.11
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
3-Nitroaniline [99-09-2]A
0.039
U
mg/kg
dry
1
0.039
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.029
U
mg/kg
dry
1
0.029
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.036
U
mg/kg
dry
1
0.036
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
4-Chloroaniline [106-47-8]A
0.10
U
mg/kg
dry
1
0.10
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.028
U
mg/kg
dry
1
0.028
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
4-Nitroaniline [100-01-6]A
0.057
U
mg/kg
dry
1
0.057
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
4-Nitrophenol [100-02-7]A
0.033
U
mg/kg
dry
1
0.033
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Acenaphthene [83-32-9]A
0.030
U
mg/kg
dry
1
0.030
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Acenaphthylene [208-96-8]A
0.030
U
mg/kg
dry
1
0.030
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Anthracene[120-12-7]A
0.041
U
mg/kg
dry
1
0.041
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Benzidine [92-87-5]A
0.12
U
mg/kg
dry
1
0.12
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Benzo(a)anthracene [56-55-3]A
0.030
U
mg/kg
dry
1
0.030
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Benzo(a)pyrene [50-32-8]A
0.036
U
mg/kg
dry
1
0.036
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Benzo(b)fluoranthene [205-99-2]A
0.019
U
mg/kg
dry
1
0.019
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.051
U
mg/kg
dry
1
0.051
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM QV-01
Benzo(k)fluoranthene [207-08-9]A
0.036
U
mg/kg
dry
1
0.036
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Benzoic acid [65-85-0]A
0.16
U
mg/kg
dry
1
0.16
1.8
OK19001
EPA
8270E
11/23/20
17:50
DFM
Benzyl alcohol [100-51-6]A
0.025
U
mg/kg
dry
1
0.025
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.027
U
mg/kg
dry
1
0.027
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.046
U
mg/kg
dry
1
0.046
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.026
U
mg/kg
dry
1
0.026
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.038
U
mg/kg
dry
1
0.038
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Butylbenzylphthalate [85-68-7]A
0.043
U
mg/kg
dry
1
0.043
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Chrysene [218-01-9]A
0.032
U
mg/kg
dry
1
0.032
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.055
U
mg/kg
dry
1
0.055
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Dibenzofuran [132-64-9]A
0.029
U
mg/kg
dry
1
0.029
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Diethylphthalate [84-66-2]A
0.030
U
mg/kg
dry
1
0.030
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Dimethylphthalate [131-11-3]A
0.036
U
mg/kg
dry
1
0.036
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Di-n-butylphthalate [84-74-2]A
0.044
U
mg/kg
dry
1
0.044
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Di-n-octylphthalate [117-84-0]A
0.036
U
mg/kg
dry
1
0.036
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Fluoranthene [206-44-0]A
0.039
U
mg/kg
dry
1
0.039
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Fluorene [86-73-7]A
0.031
U
mg/kg
dry
1
0.031
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Hexachlorobenzene [118-74-1]A
0.028
U
mg/kg
dry
1
0.028
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Hexachlorobutadiene [87-68-3]A
0.028
U
mg/kg
dry
1
0.028
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Hexachlorocyclopentadiene [77-47-4]A
0.042
U
mg/kg
dry
1
0.042
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Hexachloroethane [67-72-1]A
0.023
U
mg/kg
dry
1
0.023
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.051
U
mg/kg
dry
1
0.051
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Isophorone[78-59-1]A
0.032
U
mg/kg
dry
1
0.032
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Naphthalene [91-20-3]A
0.030
U
mg/kg
dry
1
0.030
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
Nitrobenzene [98-95-3]A
0.028
U
mg/kg
dry
1
0.028
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
N-Nitrosodimethylamine [62-75-9]A
0.023
U
mg/kg
dry
1
0.023
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.088
U
mg/kg
dry
1
0.088
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
N-nitrosodiphenylamine/Diphenylamine
0.058
U
mg/kg
dry
1
0.058
0.36
OK19001
EPA
8270E
11/23/20
17:50
DFM
[86-30-6/122-39-4]A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 52 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-39-6 Lab Sample ID:CD18880-17 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 10:50 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 92.56
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.036
U
mg/kg dry
1
0.036
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
Phenanthrene[85-01-8]^
0.029
U
mg/kg dry
1
0.029
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
Phenol[108-95-2]^
0.024
U
mg/kg dry
1
0.024
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
Pyrene [129-00-0]^
0.041
U
mg/kg dry
1
0.041
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
Pyridine [110-86-1]^
0.089
U
mg/kg dry
1
0.089
0.36
OK19001
EPA 8270E
11/23/20 17:50
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.2
1
3.60
116 %
26-130
OK19001
EPA 8270E
11/23/2017:50
DFM
2-Fluorobiphenyl
1.7
1
1.80
97 %
56-120
OK19001
EPA 8270E
11123120 17:50
DFM
2-Fluorophenol
3.7
1
3.60
102 %
49-126
OK19001
EPA 8270E
11123120 17:50
DFM
Nitrobenzene-d5
1.7
1
1.80
95 %
50-117
OK19001
EPA 8270E
11/23/2017:50
DFM
Phenol-d5
4.4
1
3.60
122 %
56-120
OK19001
EPA 8270E
11/23/2017:50
DFM QS-03
Terphenyl-d14
1.5
1
1.80
82 %
36-151
OK19001
EPA 8270E
11/23/2017:50
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]1
9.46
mg/kg dry
1
0.130 0.540
OK20031
EPA 6010D
11/23/20 15:17
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 53 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-40-6" Lab Sample ID:CD18880-19 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:10 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.40
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00014
U
mg/kg dry
0.797
0.00014 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,1,1-Trichloroethane [71-55-6]A
0.00022
U
mg/kg dry
0.797
0.00022 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00018
U
mg/kg dry
0.797
0.00018 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,1,2-Trichloroethane [79-00-5]A
0.00022
U
mg/kg dry
0.797
0.00022 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,1-Dichloroethane [75-34-3]A
0.00022
U
mg/kg dry
0.797
0.00022 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
QV-01
1,1-Dichloroethene [75-35-4]A
0.00027
U
mg/kg dry
0.797
0.00027 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,1-Dichloropropene [563-58-6]A
0.00014
U
mg/kg dry
0.797
0.00014 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00025
U
mg/kg dry
0.797
0.00025 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,2,3-Trichloropropane [96-18-4]A
0.00057
U
mg/kg dry
0.797
0.00057 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00024
U
mg/kg dry
0.797
0.00024 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00015
U
mg/kg dry
0.797
0.00015 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00070
U
mg/kg dry
0.797
0.00070 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,2-Dibromoethane [506-93-4]A
0.00041
U
mg/kg dry
0.797
0.00041 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,2-Dichlorobenzene [95-50-1]A
0.00024
U
mg/kg dry
0.797
0.00024 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,2-Dichloroethane [507-06-2]A
0.00037
U
mg/kg dry
0.797
0.00037 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,2-Dichloropropane [78-87-5]A
0.00023
U
mg/kg dry
0.797
0.00023 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,3,5-Trimethylbenzene [508-67-8]A
0.00018
U
mg/kg dry
0.797
0.00018 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,3-Dichlorobenzene [541-73-1]A
0.00020
U
mg/kg dry
0.797
0.00020 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,3-Dichloropropane [142-28-9]A
0.00026
U
mg/kg dry
0.797
0.00026 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
1,4-Dichlorobenzene [106-46-7]A
0.00018
U
mg/kg dry
0.797
0.00018 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
2,2-Dichloropropane [594-20-7]A
0.00021
U
mg/kg dry
0.797
0.00021 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
2-Butanone [78-93-3]A
0.00070
U
mg/kg dry
0.797
0.00070 0.0045
OK18035
EPA 8260D
11/19/20 06:33
REF
QV-01
2-Chloroethyl Vinyl Ether [510-75-8]A
0.00014
U
mg/kg dry
0.797
0.00014 0.0045
OK18035
EPA 8260D
11/19/20 06:33
REF
2-Chlorotoluene [95-49-8]A
0.00016
U
mg/kg dry
0.797
0.00016 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
2-Hexanone [591-78-6]A
0.00067
U
mg/kg dry
0.797
0.00067 0.0045
OK18035
EPA 8260D
11/19/20 06:33
REF
4-Chlorotoluene [106-43-4]A
0.00023
U
mg/kg dry
0.797
0.00023 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
4-Isopropyltoluene [99-87-6]A
0.0021
mg/kg dry
0.797
0.00014 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
4-Methyl-2-pentanone [108-10-1]A
0.00051
U
mg/kg dry
0.797
0.00051 0.0045
OK18035
EPA 8260D
11/19/20 06:33
REF
Acetone [67-64-1]A
0.032
mg/kg dry
0.797
0.012 0.018
OK18035
EPA 8260D
11/19/20 06:33
REF
Benzene [71-43-2]A
0.00015
U
mg/kg dry
0.797
0.00015 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
QV-01
Bromobenzene [508-86-1]A
0.00020
U
mg/kg dry
0.797
0.00020 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Bromochloromethane [74-97-5]A
0.00037
U
mg/kg dry
0.797
0.00037 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Bromodichloromethane [75-27-4]A
0.00021
U
mg/kg dry
0.797
0.00021 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Bromoform [75-25-2]A
0.00040
U
mg/kg dry
0.797
0.00040 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Bromomethane [74-83-9]A
0.00029
U
mg/kg dry
0.797
0.00029 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Carbon disulfide [75-15-0]A
0.00035
U
mg/kg dry
0.797
0.00035 0.0045
OK18035
EPA 8260D
11/19/20 06:33
REF
QV-01
Carbon Tetrachloride [56-23-5]A
0.00020
U
mg/kg dry
0.797
0.00020 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Chlorobenzene [508-90-7]A
0.00015
U
mg/kg dry
0.797
0.00015 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Chloroethane [75-00-3]A
0.00022
U
mg/kg dry
0.797
0.00022 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Chloroform [67-66-3]A
0.00016
U
mg/kg dry
0.797
0.00016 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Chloromethane [74-87-3]A
0.00019
U
mg/kg dry
0.797
0.00019 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
QV-01
cis-1,2-Dichloroethene [156-59-2]A
0.00021
U
mg/kg dry
0.797
0.00021 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00015
U
mg/kg dry
0.797
0.00015 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Dibromochloromethane [124-48-1]A
0.00031
U
mg/kg dry
0.797
0.00031 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Dibromomethane [74-95-3]A
0.00029
U
mg/kg dry
0.797
0.00029 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Dichlorodifluoromethane [75-71-8]A
0.00040
U
mg/kg dry
0.797
0.00040 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
Ethylbenzene [100-41-4]A
0.00018
U
mg/kg dry
0.797
0.00018 0.00089
OK18035
EPA 8260D
11/19/20 06:33
REF
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 54 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-40-6 Lab Sample ID:CD18880-19 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:10 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.40
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Hexachlorobutadiene [87-68-3]^
0.00031
U
mg/kg
dry
0.797
0.00031
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
Isopropyl benzene [98-82-8]^
0.00013
U
mg/kg
dry
0.797
0.00013
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.00033
U
mg/kg
dry
0.797
0.00033
0.0018
OK18035
EPA 8260D
11/19/20
06:33
REF
Methylene Chloride [75-09-2]^
0.00065
U
mg/kg
dry
0.797
0.00065
0.0018
OK18035
EPA 8260D
11/19/20
06:33
REF QV-01
Methyl-tert-Butyl Ether [1634-04-4]^
0.00027
U
mg/kg
dry
0.797
0.00027
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
Naphthalene [91-20-3]^
0.00024
U
mg/kg
dry
0.797
0.00024
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
n-Butyl Benzene [104-51-8]^
0.00012
U
mg/kg
dry
0.797
0.00012
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
n-Propyl Benzene [103-65-1]^
0.00016
U
mg/kg
dry
0.797
0.00016
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
o-Xylene [95-47-6]^
0.00020
U
mg/kg
dry
0.797
0.00020
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
sec-Butylbenzene [135-98-8]^
0.00085
U
mg/kg
dry
0.797
0.00085
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
Styrene [100-42-5]^
0.00087
U
mg/kg
dry
0.797
0.00087
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
tert-Butylbenzene [98-06-6]^
0.00015
U
mg/kg
dry
0.797
0.00015
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
Tetrachloroethene [127-18-4]^
0.00025
U
mg/kg
dry
0.797
0.00025
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
Toluene [108-88-3]^
0.00021
U
mg/kg
dry
0.797
0.00021
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
trans-1,2-Dichloroethene [156-60-5]^
0.00033
U
mg/kg
dry
0.797
0.00033
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF QV-01
trans-1,3-Dichloropropene [10061-02-6]^
0.00035
U
mg/kg
dry
0.797
0.00035
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
Trichloroethene [79-01-6]^
0.00029
U
mg/kg
dry
0.797
0.00029
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
Trichlorofluoromethane [75-69-4]^
0.00023
U
mg/kg
dry
0.797
0.00023
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
Vinyl chloride [75-01-4]^
0.00021
U
mg/kg
dry
0.797
0.00021
0.00089
OK18035
EPA 8260D
11/19/20
06:33
REF
Xylenes (Total) [1330-20-7]^
0.00050
U
mg/kg
dry
0.797
0.00050
0.0027
OK18035
EPA 8260D
11/19/20
06:33
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
32
0.797
50.0
63 %
50-127
OK18035
EPA 6260D
11119120 06:33
REF
Dlbromofluoromethane
36
0.797
50.0
72 %
52-128
OK18035
EPA 8260D
11119120 06:33
REF
Toluene-d8
36
0.797
50.0
73 %
57-124
OK18035
EPA 8260D
11119120 06:33
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.029
U
mg/kg dry
1
0.029
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
1,2-Dichlorobenzene [95-50-1]^
0.026
U
mg/kg dry
1
0.026
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
1,3-Dichlorobenzene [541-73-1]^
0.022
U
mg/kg dry
1
0.022
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
1,4-Dichlorobenzene [106-46-7]^
0.023
U
mg/kg dry
1
0.023
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
1- Methyl naphthalene [90-12-0]^
0.030
U
mg/kg dry
1
0.030
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2,4,5-Trichlorophenol[95-95-4]^
0.030
U
mg/kg dry
1
0.030
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2,4,6-Trichlorophenol[88-06-2]^
0.030
U
mg/kg dry
1
0.030
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2,4-Dichlorophenol [120-83-2]^
0.027
U
mg/kg dry
1
0.027
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2,4-Di methyl phenol [105-67-9]^
0.048
U
mg/kg dry
1
0.048
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2,4-Dinitrophenol [51-28-5]^
0.048
U
mg/kg dry
1
0.048
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2,4-Dinitrotoluene [121-14-2]^
0.031
U
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2,6-Dinitrotoluene [606-20-2]^
0.035
U
mg/kg dry
1
0.035
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2-Chloronaphthalene [91-58-7]^
0.031
U
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2-Chlorophenol [95-57-8]^
0.028
U
mg/kg dry
1
0.028
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
0.037
U
mg/kg dry
1
0.037
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2- Methyl naphthalene [91-57-6]^
0.031
U
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2-Methylphenol [95-48-7]^
0.028
U
mg/kg dry
1
0.028
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
2-Nitroaniline [88-74-4]^
0.034
U
mg/kg dry
1
0.034
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 55 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-40-6" Lab Sample ID:CD18880-19 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:10 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.40
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]A
0.035
U
mg/kg
dry
1
0.035
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
3 & 4-Methylphenol [508-39-4/106-44-5]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
U
mg/kg
dry
1
0.11
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
3-Nitroaniline [99-09-2]A
0.040
U
mg/kg
dry
1
0.040
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.030
U
mg/kg
dry
1
0.030
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
4-Chloroaniline [106-47-8]A
0.10
U
mg/kg
dry
1
0.10
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
4-Nitroaniline [100-01-6]A
0.059
U
mg/kg
dry
1
0.059
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
4-Nitrophenol [100-02-7]A
0.035
U
mg/kg
dry
1
0.035
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Acenaphthene [83-32-9]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Acenaphthylene [208-96-8]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Anthracene[120-12-7]A
0.043
U
mg/kg
dry
1
0.043
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Benzidine [92-87-5]A
0.12
U
mg/kg
dry
1
0.12
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Benzo(a)anthracene [56-55-3]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Benzo(a)pyrene [50-32-8]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Benzo(b)fluoranthene [205-99-2]A
0.020
U
mg/kg
dry
1
0.020
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.053
U
mg/kg
dry
1
0.053
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Benzo(k)fluoranthene [207-08-9]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Benzoic acid [65-85-0]A
0.17
U
mg/kg
dry
1
0.17
1.9
OK25001
EPA
8270E
11/25/20
15:00
DFM
Benzyl alcohol [100-51-6]A
0.026
U
mg/kg
dry
1
0.026
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.028
U
mg/kg
dry
1
0.028
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.048
U
mg/kg
dry
1
0.048
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.027
U
mg/kg
dry
1
0.027
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.039
U
mg/kg
dry
1
0.039
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Butylbenzylphthalate [85-68-7]A
0.045
U
mg/kg
dry
1
0.045
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Chrysene [218-01-9]A
0.034
U
mg/kg
dry
1
0.034
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.057
U
mg/kg
dry
1
0.057
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Dibenzofuran [132-64-9]A
0.030
U
mg/kg
dry
1
0.030
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Diethylphthalate [84-66-2]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Dimethylphthalate [131-11-3]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Di-n-butylphthalate [84-74-2]A
0.046
U
mg/kg
dry
1
0.046
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Di-n-octylphthalate [117-84-0]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM QV-01
Fluoranthene [206-44-0]A
0.040
U
mg/kg
dry
1
0.040
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Fluorene [86-73-7]A
0.032
U
mg/kg
dry
1
0.032
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Hexachlorobenzene [118-74-1]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Hexachlorobutadiene [87-68-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM QV-01
Hexachlorocyclopentadiene [77-47-4]A
0.044
U
mg/kg
dry
1
0.044
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Hexachloroethane [67-72-1]A
0.023
U
mg/kg
dry
1
0.023
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.053
U
mg/kg
dry
1
0.053
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Isophorone[78-59-1]A
0.034
U
mg/kg
dry
1
0.034
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Naphthalene [91-20-3]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
Nitrobenzene [98-95-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
N-Nitrosodimethylamine [62-75-9]A
0.023
U
mg/kg
dry
1
0.023
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.091
U
mg/kg
dry
1
0.091
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
N-nitrosodiphenylamine/Diphenylamine
0.060
U
mg/kg
dry
1
0.060
0.37
OK25001
EPA
8270E
11/25/20
15:00
DFM
[86-30-6/122-39-4]A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 56 of 107

(� �Eo
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ANALYTICAL RESULTS
Description: HA-40-6" Lab Sample ID:CD18880-19 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 11:10 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.40
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.037
U
mg/kg dry
1
0.037
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
Phenanthrene[85-01-8]^
0.030
U
mg/kg dry
1
0.030
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
Phenol[108-95-2]^
0.025
U
mg/kg dry
1
0.025
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
Pyrene [129-00-0]^
0.043
U
mg/kg dry
1
0.043
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
Pyridine [110-86-1]^
0.092
U
mg/kg dry
1
0.092
0.37
OK25001
EPA 8270E
11/25/20 15:00
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.3
1
3.73
115 %
26-130
OK25001
EPA 8270E
11/25/2015:00
DFM
2-Fluorobiphenyl
I.8
1
1.86
97 %
56-120
OK25001
EPA 8270E
1112512015:00
DFM
2-Fluorophenol
3.5
1
3.73
93 %
49-126
OK25001
EPA 8270E
1112512015:00
DFM
Nitrobenzene-d5
1.7
1
1.86
94 %
50-117
OK25001
EPA 8270E
11/25/2015:00
DFM
Phenol-d5
3.5
1
3.73
94 %
56-120
OK25001
EPA 8270E
11/25/2015:00
DFM
Terphenyl-d14
1.9
1
1.66
103 %
36-151
OK25001
EPA 8270E
11/25/2015:00
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]^
244
mg/kg dry
1
0.134 0.559
OK20031
EPA 6010D
11/23/20 15:19
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]^
2.00
mg/L
50
0.155 0.500
OL14039
EPA 6010D
12/15/20 13:14
JDH
Description: HA-40-18" Lab Sample ID:CD18880-20 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 11:15 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.43
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 14.5 mg/kg dry 1 0.139 0.579 OK30010 EPA 6010D 12/01/20 10:07 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 57 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-41-6" Lab Sample ID:CD18880-21 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:30 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.51
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00015
u
mg/kg
dry
0.828
0.00015
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,1,1-Trichloroethane [71-55-6]A
0.00024
u
mg/kg
dry
0.828
0.00024
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00019
u
mg/kg
dry
0.828
0.00019
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,1,2-Trichloroethane [79-00-5]A
0.00024
u
mg/kg
dry
0.828
0.00024
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,1-Dichloroethane [75-34-3]A
0.00024
u
mg/kg
dry
0.828
0.00024
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
QV-01
1,1-Dichloroethene [75-35-4]A
0.00029
u
mg/kg
dry
0.828
0.00029
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,1-Dichloropropene [563-58-6]A
0.00015
u
mg/kg
dry
0.828
0.00015
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00027
u
mg/kg
dry
0.828
0.00027
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,2,3-Trichloropropane [96-18-4]A
0.00061
u
mg/kg
dry
0.828
0.00061
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00026
u
mg/kg
dry
0.828
0.00026
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00016
u
mg/kg
dry
0.828
0.00016
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00076
u
mg/kg
dry
0.828
0.00076
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,2-Dibromoethane [506-93-4]A
0.00044
u
mg/kg
dry
0.828
0.00044
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,2-Dichlorobenzene [95-50-1]A
0.00026
u
mg/kg
dry
0.828
0.00026
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,2-Dichloroethane [507-06-2]A
0.00039
u
mg/kg
dry
0.828
0.00039
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,2-Dichloropropane [78-87-5]A
0.00025
u
mg/kg
dry
0.828
0.00025
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,3,5-Trimethylbenzene [508-67-8]A
0.00019
u
mg/kg
dry
0.828
0.00019
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,3-Dichlorobenzene [541-73-1]A
0.00021
u
mg/kg
dry
0.828
0.00021
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,3-Dichloropropane [142-28-9]A
0.00028
u
mg/kg
dry
0.828
0.00028
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
1,4-Dichlorobenzene [106-46-7]A
0.00019
u
mg/kg
dry
0.828
0.00019
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
2,2-Dichloropropane [594-20-7]A
0.00022
u
mg/kg
dry
0.828
0.00022
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
2-Butanone [78-93-3]A
0.00075
u
mg/kg
dry
0.828
0.00075
0.0048
OK18035
EPA
8260D
11/19/20
07:03
REF
QV-01
2-Chloroethyl Vinyl Ether [510-75-8]A
0.00015
u
mg/kg
dry
0.828
0.00015
0.0048
OK18035
EPA
8260D
11/19/20
07:03
REF
2-Chlorotoluene [95-49-8]A
0.00017
u
mg/kg
dry
0.828
0.00017
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
2-Hexanone [591-78-6]A
0.00072
u
mg/kg
dry
0.828
0.00072
0.0048
OK18035
EPA
8260D
11/19/20
07:03
REF
4-Chlorotoluene [106-43-4]A
0.00025
u
mg/kg
dry
0.828
0.00025
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
4-Isopropyltoluene [99-87-6]A
0.0056
mg/kg
dry
0.828
0.00015
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
4-Methyl-2-pentanone [108-10-1]A
0.00055
u
mg/kg
dry
0.828
0.00055
0.0048
OK18035
EPA
8260D
11/19/20
07:03
REF
Acetone [67-64-1]A
0.080
mg/kg
dry
0.828
0.013
0.019
OK18035
EPA
8260D
11/19/20
07:03
REF
Benzene [71-43-2]A
0.00016
u
mg/kg
dry
0.828
0.00016
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
QV-01
Bromobenzene [508-86-1]A
0.00021
u
mg/kg
dry
0.828
0.00021
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Bromochloromethane [74-97-5]A
0.00039
u
mg/kg
dry
0.828
0.00039
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Bromodichloromethane [75-27-4]A
0.00023
u
mg/kg
dry
0.828
0.00023
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Bromoform [75-25-2]A
0.00043
u
mg/kg
dry
0.828
0.00043
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Bromomethane [74-83-9]A
0.00031
u
mg/kg
dry
0.828
0.00031
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Carbon disulfide [75-15-0]A
0.00037
u
mg/kg
dry
0.828
0.00037
0.0048
OK18035
EPA
8260D
11/19/20
07:03
REF
QV-01
Carbon Tetrachloride [56-23-5]A
0.00021
u
mg/kg
dry
0.828
0.00021
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Chlorobenzene [508-90-7]A
0.00016
u
mg/kg
dry
0.828
0.00016
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Chloroethane [75-00-3]A
0.00024
u
mg/kg
dry
0.828
0.00024
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Chloroform [67-66-3]A
0.00017
u
mg/kg
dry
0.828
0.00017
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Chloromethane [74-87-3]A
0.00020
u
mg/kg
dry
0.828
0.00020
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
QV-01
cis-1,2-Dichloroethene [156-59-2]A
0.00022
u
mg/kg
dry
0.828
0.00022
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00016
u
mg/kg
dry
0.828
0.00016
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Dibromochloromethane [124-48-1]A
0.00033
u
mg/kg
dry
0.828
0.00033
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Dibromomethane [74-95-3]A
0.00032
u
mg/kg
dry
0.828
0.00032
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Dichlorodifluoromethane [75-71-8]A
0.00043
u
mg/kg
dry
0.828
0.00043
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
Ethylbenzene [100-41-4]A
0.00019
u
mg/kg
dry
0.828
0.00019
0.00096
OK18035
EPA
8260D
11/19/20
07:03
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 58 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-41-6" Lab Sample ID:CD18880-21 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:30 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.51
Volatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analvte rCAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
Hexachlorobutadiene [87-68-3]A
0.00033
U
mg/kg
dry
0.828
0.00033
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
Isopropylbenzene [98-82-8]A
0.00014
U
mg/kg
dry
0.828
0.00014
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
m,p-Xylenes[108-38-3/106-42-3]A
0.00035
U
mg/kg
dry
0.828
0.00035
0.0019
OK18035
EPA 8260D
11/19/20
07:03
REF
Methylene Chloride [75-09-2]A
0.00070
U
mg/kg
dry
0.828
0.00070
0.0019
OK18035
EPA 8260D
11/19/20
07:03
REF QV-01
Methyl-tert-Butyl Ether [1634-04-4]A
0.00029
U
mg/kg
dry
0.828
0.00029
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
Naphthalene [91-20-3]A
0.00026
U
mg/kg
dry
0.828
0.00026
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
n-Butyl Benzene [104-51-8]A
0.00012
U
mg/kg
dry
0.828
0.00012
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
n-Propyl Benzene [103-65-1]A
0.00017
U
mg/kg
dry
0.828
0.00017
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
o-Xylene [95-47-6]A
0.00021
U
mg/kg
dry
0.828
0.00021
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
sec-Butylbenzene [135-98-8]A
0.00091
U
mg/kg
dry
0.828
0.00091
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
Styrene [500-42-5]A
0.0047
mg/kg
dry
0.828
0.00094
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
tert-Butyl benzene [98-06-6]A
0.00016
U
mg/kg
dry
0.828
0.00016
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
Tetrachloroethene [127-18-4]A
0.00027
U
mg/kg
dry
0.828
0.00027
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
Toluene [108-88-3]A
0.00023
U
mg/kg
dry
0.828
0.00023
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
trans-1,2-Dichloroethene [156-60-5]A
0.00035
U
mg/kg
dry
0.828
0.00035
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF QV-01
trans-1,3-Dichloropropene [10061-02-6]A
0.00037
U
mg/kg
dry
0.828
0.00037
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
Trichloroethene [79-01-6]A
0.00031
U
mg/kg
dry
0.828
0.00031
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
Trichlorofluoromethane [75-69-4]A
0.00025
U
mg/kg
dry
0.828
0.00025
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
Vinyl chloride [75-01-4]A
0.00023
U
mg/kg
dry
0.828
0.00023
0.00096
OK18035
EPA 8260D
11/19/20
07:03
REF
Xylenes (Total) [1330-20-7]A
0.00054
U
mg/kg
dry
0.828
0.00054
0.0029
OK18035
EPA 8260D
11/19/20
07:03
REF
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
" Notes
4-Bromofluorobenzene
32
0,828
50.0
63 %
50-127
OK18035
EPA 8260D
11119120 07:03
REF
Dibromofluoromethane
38
0,828
50.0
77 %
52-128
OK18035
EPA 8260D
11119120 07:03
REF
Toluene-&
37
0.828
50.0
74 %
57-124
OK18035
EPA 8260D
11119120 07:03
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 5911
Analvte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]A
0.030
U
mg/kg dry
1
0.030
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
1,2-Dichlorobenzene [95-50-1]A
0.027
U
mg/kg dry
1
0.027
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
1,3-Dichlorobenzene [541-73-1]A
0.023
U
mg/kg dry
1
0.023
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
1,4-Dichlorobenzene [106-46-7]A
0.024
U
mg/kg dry
1
0.024
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
1-Methylnaphthalene [90-12-0]A
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2,4,5-Trichlorophenol [95-95-4]A
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2,4,6-Trichlorophenol [88-06-2]A
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2,4-Dichlorophenol [120-83-2]A
0.028
U
mg/kg dry
1
0.028
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2,4-Dimethylphenol [105-67-9]A
0.050
U
mg/kg dry
1
0.050
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2,4-Dinitrophenol [51-28-5]A
0.050
U
mg/kg dry
1
0.050
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2,4-Dinitrotoluene [121-14-2]A
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2,6-Dinitrotoluene [606-20-2]A
0.036
U
mg/kg dry
1
0.036
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2-Chloronaphthalene [91-58-7]A
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2-Chlorophenol [95-57-8]A
0.029
U
mg/kg dry
1
0.029
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]A
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM QV-01
2-Methylnaphthalene [91-57-6]A
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2-Methylphenol [95-48-7]A
0.029
U
mg/kg dry
1
0.029
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
2-Nitroaniline [88-74-4]A
0.035
U
mg/kg dry
1
0.035
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 59 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-41-6" Lab Sample ID:CD18880-21 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:30 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.51
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]A
0.036
U
mg/kg
dry
1
0.036
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
U
mg/kg
dry
1
0.11
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
3-Nitroaniline [99-09-2]A
0.042
U
mg/kg
dry
1
0.042
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.031
U
mg/kg
dry
1
0.031
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
4-Chloroaniline [106-47-8]A
0.11
U
mg/kg
dry
1
0.11
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
4-Nitroaniline [100-01-6]A
0.061
U
mg/kg
dry
1
0.061
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
4-Nitrophenol [100-02-7]A
0.036
U
mg/kg
dry
1
0.036
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Acenaphthene [83-32-9]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Acenaphthylene [208-96-8]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Anthracene[120-12-7]A
0.044
U
mg/kg
dry
1
0.044
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Benzidine [92-87-5]A
0.13
U
mg/kg
dry
1
0.13
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Benzo(a)anthracene [56-55-3]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Benzo(a)pyrene [50-32-8]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Benzo(b)fluoranthene [205-99-2]A
0.021
U
mg/kg
dry
1
0.021
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.054
U
mg/kg
dry
1
0.054
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM QV-01
Benzo(k)fluoranthene [207-08-9]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Benzoic acid [65-85-O]A
0.49
J
mg/kg
dry
1
0.17
2.0
OK19001
EPA
8270E
11/23/20
18:53
DFM
Benzyl alcohol [100-51-6]A
0.027
U
mg/kg
dry
1
0.027
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.029
U
mg/kg
dry
1
0.029
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.050
U
mg/kg
dry
1
0.050
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.028
U
mg/kg
dry
1
0.028
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.040
U
mg/kg
dry
1
0.040
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Butylbenzylphthalate [85-68-7]A
0.046
U
mg/kg
dry
1
0.046
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Chrysene [218-01-9]A
0.035
U
mg/kg
dry
1
0.035
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.059
U
mg/kg
dry
1
0.059
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Dibenzofuran [132-64-9]A
0.031
U
mg/kg
dry
1
0.031
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Diethylphthalate [84-66-2]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Dimethylphthalate [131-11-3]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Di-n-butylphthalate [84-74-2]A
0.047
U
mg/kg
dry
1
0.047
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Di-n-octylphthalate [117-84-O]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Fluoranthene [206-44-O]A
0.042
U
mg/kg
dry
1
0.042
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Fluorene [86-73-7]A
0.034
U
mg/kg
dry
1
0.034
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Hexachlorobenzene [118-74-1]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Hexachlorobutadiene [87-68-3]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Hexachlorocyclopentadiene [77-47-4]A
0.045
U
mg/kg
dry
1
0.045
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Hexachloroethane [67-72-1]A
0.024
U
mg/kg
dry
1
0.024
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.054
U
mg/kg
dry
1
0.054
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Isophorone[78-59-1]A
0.035
U
mg/kg
dry
1
0.035
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Naphthalene [91-20-3]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
Nitrobenzene [98-95-3]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
N-Nitrosodimethylamine [62-75-9]A
0.024
U
mg/kg
dry
1
0.024
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.094
U
mg/kg
dry
1
0.094
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
N-nitrosodiphenylamine/Diphenylamine
0.062
U
mg/kg
dry
1
0.062
0.38
OK19001
EPA
8270E
11/23/20
18:53
DFM
[86-30-6/122-39-4]A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 60 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-41-6 Lab Sample ID:CD18880-21 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 11:30 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.51
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
Phenanthrene[85-01-8]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
Phenol[108-95-2]^
0.025
U
mg/kg dry
1
0.025
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
Pyrene [129-00-0]^
0.044
U
mg/kg dry
1
0.044
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
Pyridine [110-86-1]^
0.095
U
mg/kg dry
1
0.095
0.38
OK19001
EPA 8270E
11/23/20 18:53
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.7
1
3.85
122 %
26-130
OK19001
EPA 8270E
11/23/2018:53
DFM
2-Fluorobiphenyl
ZI
1
1.93
107 %
56-120
OK19001
EPA 8270E
11123120 18:53
DFM
2-Fluorophenol
4.3
1
3.85
ill %
49-126
OK19001
EPA 8270E
11123120 18:53
DFM
Nitrobenzene-d5
1.9
1
1.93
96 %
50-117
OK19001
EPA 8270E
11/23/2018:53
DFM
Phenol-d5
4.4
1
3.85
114 %
56-120
OK19001
EPA 8270E
11/23/2018:53
DFM
Terphenyl-d14
1.2
1
1.93
64 %
36-151
OK19001
EPA 8270E
11/23/2018:53
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]1
65.6
mg/kg dry
1
0.139 0.578
OK20031
EPA 6010D
11/23/20 15:21
JDH
Description: HA-41-18" Lab Sample ID: CD18880-22 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 11:35 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 77.82
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 17.0 mg/kg dry 1 0.154 0.643 OK30010 EPA 6010D 12/01/20 10:09 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 61 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-42-6" Lab Sample ID:CD18880-23 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.91
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00015
u
mg/kg
dry
0.806
0.00015
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,1,1-Trichloroethane [71-55-6]A
0.00023
u
mg/kg
dry
0.806
0.00023
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00019
u
mg/kg
dry
0.806
0.00019
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,1,2-Trichloroethane [79-00-5]A
0.00023
u
mg/kg
dry
0.806
0.00023
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,1-Dichloroethane [75-34-3]A
0.00023
u
mg/kg
dry
0.806
0.00023
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
QV-01
1,1-Dichloroethene [75-35-4]A
0.00028
u
mg/kg
dry
0.806
0.00028
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,1-Dichloropropene [563-58-6]A
0.00015
u
mg/kg
dry
0.806
0.00015
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00026
u
mg/kg
dry
0.806
0.00026
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,2,3-Trichloropropane [96-18-4]A
0.00059
u
mg/kg
dry
0.806
0.00059
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00025
u
mg/kg
dry
0.806
0.00025
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00016
u
mg/kg
dry
0.806
0.00016
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00073
u
mg/kg
dry
0.806
0.00073
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,2-Dibromoethane [106-93-4]A
0.00043
u
mg/kg
dry
0.806
0.00043
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,2-Dichlorobenzene [95-50-1]A
0.00025
u
mg/kg
dry
0.806
0.00025
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,2-Dichloroethane [107-06-2]A
0.00038
u
mg/kg
dry
0.806
0.00038
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,2-Dichloropropane [78-87-5]A
0.00024
u
mg/kg
dry
0.806
0.00024
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00019
u
mg/kg
dry
0.806
0.00019
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,3-Dichlorobenzene [541-73-1]A
0.00020
u
mg/kg
dry
0.806
0.00020
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,3-Dichloropropane [142-28-9]A
0.00027
u
mg/kg
dry
0.806
0.00027
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
1,4-Dichlorobenzene [106-46-7]A
0.00019
u
mg/kg
dry
0.806
0.00019
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
2,2-Dichloropropane [594-20-7]A
0.00021
u
mg/kg
dry
0.806
0.00021
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
2-Butanone [78-93-3]A
0.00072
u
mg/kg
dry
0.806
0.00072
0.0046
OK18035
EPA
8260D
11/19/20
07:33
REF
QV-01
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00015
u
mg/kg
dry
0.806
0.00015
0.0046
OK18035
EPA
8260D
11/19/20
07:33
REF
2-Chlorotoluene [95-49-8]A
0.00017
u
mg/kg
dry
0.806
0.00017
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
2-Hexanone [591-78-6]A
0.00070
u
mg/kg
dry
0.806
0.00070
0.0046
OK18035
EPA
8260D
11/19/20
07:33
REF
4-Chlorotoluene [106-43-4]A
0.00024
u
mg/kg
dry
0.806
0.00024
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
4-Isopropyltoluene [99-87-6]A
0.011
mg/kg
dry
0.806
0.00015
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
4-Methyl-2-pentanone [108-10-1]A
0.00053
u
mg/kg
dry
0.806
0.00053
0.0046
OK18035
EPA
8260D
11/19/20
07:33
REF
Acetone [67-64-1]A
0.017
J
mg/kg
dry
0.806
0.013
0.019
OK18035
EPA
8260D
11/19/20
07:33
REF
Benzene [71-43-2]A
0.00016
u
mg/kg
dry
0.806
0.00016
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
QV-01
Bromobenzene [108-86-1]A
0.00020
u
mg/kg
dry
0.806
0.00020
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Bromochloromethane [74-97-5]A
0.00038
u
mg/kg
dry
0.806
0.00038
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Bromodichloromethane [75-27-4]A
0.00022
u
mg/kg
dry
0.806
0.00022
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Bromoform [75-25-2]A
0.00042
u
mg/kg
dry
0.806
0.00042
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Bromomethane [74-83-9]A
0.00030
u
mg/kg
dry
0.806
0.00030
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Carbon disulfide [75-15-0]A
0.00036
u
mg/kg
dry
0.806
0.00036
0.0046
OK18035
EPA
8260D
11/19/20
07:33
REF
QV-01
Carbon Tetrachloride [56-23-5]A
0.00020
u
mg/kg
dry
0.806
0.00020
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Chlorobenzene [108-90-7]A
0.00016
u
mg/kg
dry
0.806
0.00016
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Chloroethane [75-00-3]A
0.00023
u
mg/kg
dry
0.806
0.00023
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Chloroform [67-66-3]A
0.00017
u
mg/kg
dry
0.806
0.00017
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Chloromethane [74-87-3]A
0.00019
u
mg/kg
dry
0.806
0.00019
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
QV-01
cis-1,2-Dichloroethene [156-59-2]A
0.00021
u
mg/kg
dry
0.806
0.00021
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00016
u
mg/kg
dry
0.806
0.00016
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Dibromochloromethane [124-48-1]A
0.00032
u
mg/kg
dry
0.806
0.00032
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Dibromomethane [74-95-3]A
0.00031
u
mg/kg
dry
0.806
0.00031
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Dichlorodifluoromethane [75-71-8]A
0.00042
u
mg/kg
dry
0.806
0.00042
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
Ethylbenzene [100-41-4]A
0.00019
u
mg/kg
dry
0.806
0.00019
0.00093
OK18035
EPA
8260D
11/19/20
07:33
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 62 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-42-6 Lab Sample ID:CD18880-23 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.91
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Hexachlorobutadiene [87-68-3]^
0.00032
U
mg/kg
dry
0.806
0.00032
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
Isopropyl benzene [98-82-8]^
0.00014
U
mg/kg
dry
0.806
0.00014
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.00034
U
mg/kg
dry
0.806
0.00034
0.0019
OK18035
EPA 8260D
11/19/20
07:33
REF
Methylene Chloride [75-09-2]^
0.00068
U
mg/kg
dry
0.806
0.00068
0.0019
OK18035
EPA 8260D
11/19/20
07:33
REF QV-01
Methyl-tert-Butyl Ether [1634-04-4]^
0.00028
U
mg/kg
dry
0.806
0.00028
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
Naphthalene [91-20-3]^
0.00025
U
mg/kg
dry
0.806
0.00025
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
n-Butyl Benzene [104-51-8]^
0.00012
U
mg/kg
dry
0.806
0.00012
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
n-Propyl Benzene [103-65-1]^
0.00017
U
mg/kg
dry
0.806
0.00017
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
o-Xylene [95-47-6]^
0.00020
U
mg/kg
dry
0.806
0.00020
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
sec-Butylbenzene [135-98-8]^
0.00088
U
mg/kg
dry
0.806
0.00088
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
Styrene [100-42-5]^
0.00091
U
mg/kg
dry
0.806
0.00091
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
tert-Butylbenzene [98-06-6]^
0.00016
U
mg/kg
dry
0.806
0.00016
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
Tetrachloroethene [127-18-4]^
0.00026
U
mg/kg
dry
0.806
0.00026
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
Toluene [108-88-3]^
0.00022
U
mg/kg
dry
0.806
0.00022
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
trans-1,2-Dichloroethene [156-60-5]^
0.00034
U
mg/kg
dry
0.806
0.00034
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF QV-01
trans-1,3-Dichloropropene [10061-02-6]^
0.00036
U
mg/kg
dry
0.806
0.00036
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
Trichloroethene [79-01-6]^
0.00030
U
mg/kg
dry
0.806
0.00030
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
Trichlorofluoromethane [75-69-4]^
0.00024
U
mg/kg
dry
0.806
0.00024
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
Vinyl chloride [75-01-4]^
0.00022
U
mg/kg
dry
0.806
0.00022
0.00093
OK18035
EPA 8260D
11/19/20
07:33
REF
Xylenes (Total) [1330-20-7]^
0.00052
U
mg/kg
dry
0.806
0.00052
0.0028
OK18035
EPA 8260D
11/19/20
07:33
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
32
0.806
50.0
64 %
50-127
OK18035
EPA 6260D
11119120 0733
REF
Dlbromofluoromethane
38
0.806
50.0
76 %
52-128
OK18035
EPA 8260D
11119120 0733
REF
Toluene-d8
35
0.806
50.0
71 %
57-124
OK18035
EPA 8260D
11119120 0733
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.030
U
mg/kg dry
1
0.030
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
1,2-Dichlorobenzene [95-50-1]^
0.026
U
mg/kg dry
1
0.026
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
1,3-Dichlorobenzene [541-73-1]^
0.023
U
mg/kg dry
1
0.023
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
1,4-Dichlorobenzene [106-46-7]^
0.024
U
mg/kg dry
1
0.024
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
1- Methyl naphthalene [90-12-0]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2,4,5-Trichlorophenol[95-95-4]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2,4,6-Trichlorophenol[88-06-2]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2,4-Dichlorophenol [120-83-2]^
0.028
U
mg/kg dry
1
0.028
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2,4-Di methyl phenol[105-67-9]^
0.049
U
mg/kg dry
1
0.049
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2,4-Dinitrophenol[51-28-5]^
0.049
U
mg/kg dry
1
0.049
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2,4-Dinitrotoluene [121-14-2]^
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2,6-Dinitrotoluene [606-20-2]^
0.036
U
mg/kg dry
1
0.036
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2-Chloronaphthalene [91-58-7]^
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2-Chlorophenol [95-57-8]^
0.029
U
mg/kg dry
1
0.029
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM QV-01
2- Methyl naphthalene [91-57-6]^
0.032
U
mg/kg dry
1
0.032
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2-Methylphenol[95-48-7]^
0.029
U
mg/kg dry
1
0.029
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
2-Nitroaniline [88-74-4]^
0.035
U
mg/kg dry
1
0.035
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 63 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-42-6" Lab Sample ID:CD18880-23 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.91
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]A
0.036
U
mg/kg
dry
1
0.036
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
U
mg/kg
dry
1
0.11
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
3-Nitroaniline [99-09-2]A
0.041
U
mg/kg
dry
1
0.041
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.031
U
mg/kg
dry
1
0.031
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
4-Chloroaniline [106-47-8]A
0.11
U
mg/kg
dry
1
0.11
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
4-Nitroaniline [100-01-6]A
0.061
U
mg/kg
dry
1
0.061
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
4-Nitrophenol [100-02-7]A
0.036
U
mg/kg
dry
1
0.036
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Acenaphthene [83-32-9]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Acenaphthylene [208-96-8]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Anthracene[120-12-7]A
0.044
U
mg/kg
dry
1
0.044
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Benzidine [92-87-5]A
0.13
U
mg/kg
dry
1
0.13
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Benzo(a)anthracene [56-55-3]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Benzo(a)pyrene [50-32-8]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Benzo(b)fluoranthene [205-99-2]A
0.021
U
mg/kg
dry
1
0.021
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.054
U
mg/kg
dry
1
0.054
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM QV-01
Benzo(k)fluoranthene [207-08-9]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Benzoic acid [65-85-O]A
0.20
J
mg/kg
dry
1
0.17
2.0
OK19001
EPA
8270E
11/23/20
19:25
DFM
Benzyl alcohol [100-51-6]A
0.026
U
mg/kg
dry
1
0.026
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.029
U
mg/kg
dry
1
0.029
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.049
U
mg/kg
dry
1
0.049
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.028
U
mg/kg
dry
1
0.028
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.040
U
mg/kg
dry
1
0.040
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Butylbenzylphthalate [85-68-7]A
0.046
U
mg/kg
dry
1
0.046
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Chrysene [218-01-9]A
0.035
U
mg/kg
dry
1
0.035
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.059
U
mg/kg
dry
1
0.059
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Dibenzofuran [132-64-9]A
0.031
U
mg/kg
dry
1
0.031
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Diethylphthalate [84-66-2]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Dimethylphthalate [131-11-3]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Di-n-butylphthalate [84-74-2]A
0.047
U
mg/kg
dry
1
0.047
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Di-n-octylphthalate [117-84-O]A
0.038
U
mg/kg
dry
1
0.038
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Fluoranthene [206-44-O]A
0.041
U
mg/kg
dry
1
0.041
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Fluorene [86-73-7]A
0.033
U
mg/kg
dry
1
0.033
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Hexachlorobenzene [118-74-1]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Hexachlorobutadiene [87-68-3]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Hexachlorocyclopentadiene [77-47-4]A
0.045
U
mg/kg
dry
1
0.045
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Hexachloroethane [67-72-1]A
0.024
U
mg/kg
dry
1
0.024
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.054
U
mg/kg
dry
1
0.054
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Isophorone[78-59-1]A
0.035
U
mg/kg
dry
1
0.035
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Naphthalene [91-20-3]A
0.032
U
mg/kg
dry
1
0.032
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
Nitrobenzene [98-95-3]A
0.030
U
mg/kg
dry
1
0.030
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
N-Nitrosodimethylamine [62-75-9]A
0.024
U
mg/kg
dry
1
0.024
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.093
U
mg/kg
dry
1
0.093
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
N-nitrosodiphenylamine/Diphenylamine
0.062
U
mg/kg
dry
1
0.062
0.38
OK19001
EPA
8270E
11/23/20
19:25
DFM
[86-30-6/122-39-4]A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 64 of 107

(� �Eo
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ANALYTICAL RESULTS
Description: HA-42-6" Lab Sample ID:CD18880-23 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 11:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.91
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.038
U
mg/kg dry
1
0.038
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
Phenanthrene[85-01-8]^
0.031
U
mg/kg dry
1
0.031
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
Phenol[108-95-2]^
0.025
U
mg/kg dry
1
0.025
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
Pyrene [129-00-0]^
0.044
U
mg/kg dry
1
0.044
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
Pyridine [110-86-1]^
0.094
U
mg/kg dry
1
0.094
0.38
OK19001
EPA 8270E
11/23/20 19:25
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.7
1
3.84
123 %
26-130
OK19001
EPA 8270E
11/23/2019:25
DFM
2-Fluorobiphenyl
20
1
1.92
104 %
56-120
OK19001
EPA 8270E
11123120 19:25
DFM
2-Fluorophenol
3.8
1
3.84
100 %
49-126
OK19001
EPA 8270E
11123120 19:25
DFM
Nitrobenzene-d5
1.9
1
1.92
97 %
50-117
OK19001
EPA 8270E
11/23/2019:25
DFM
Phenol-d5
4.2
1
3.84
108 %
56-120
OK19001
EPA 8270E
11/23/2019:25
DFM
Terphenyl-d14
1.5
1
1.92
76 %
36-151
OK19001
EPA 8270E
11/23/2019:25
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]^
276
mg/kg dry
1
0.138 0.575
OK20031
EPA 6010D
11/23/20 15:23
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]^
1.84
mg/L
50
0.155 0.500
OL14039
EPA 6010D
12/15/20 13:16
JDH
Description: HA-42-18" Lab Sample ID:CD18880-24 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 11:45 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.87
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 21.7 mg/kg dry 1 0.140 0.582 OK30010 EPA 6010D 12/01/20 10:11 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 65 of 107

0Nk"q09
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ANALYTICAL RESULTS
Description: HA-43-6" Lab Sample ID:CD18880-25 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:55 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.20
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00014
U
mg/kg
dry
0.789
0.00014
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,1,1-Trichloroethane [71-55-6]A
0.00022
U
mg/kg
dry
0.789
0.00022
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00017
U
mg/kg
dry
0.789
0.00017
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,1,2-Trichloroethane [79-00-5]A
0.00022
U
mg/kg
dry
0.789
0.00022
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,1-Dichloroethane [75-34-3]A
0.00022
U
mg/kg
dry
0.789
0.00022
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
QV-01
1,1-Dichloroethene [75-35-4]A
0.00026
U
mg/kg
dry
0.789
0.00026
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,1-Dichloropropene [563-58-6]A
0.00014
U
mg/kg
dry
0.789
0.00014
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00024
U
mg/kg
dry
0.789
0.00024
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,2,3-Trichloropropane [96-18-4]A
0.00056
U
mg/kg
dry
0.789
0.00056
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00024
U
mg/kg
dry
0.789
0.00024
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00015
U
mg/kg
dry
0.789
0.00015
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00069
U
mg/kg
dry
0.789
0.00069
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,2-Dibromoethane [106-93-4]A
0.00040
U
mg/kg
dry
0.789
0.00040
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,2-Dichlorobenzene [95-50-1]A
0.00024
U
mg/kg
dry
0.789
0.00024
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,2-Dichloroethane [107-06-2]A
0.00036
U
mg/kg
dry
0.789
0.00036
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,2-Dichloropropane [78-87-5]A
0.00023
U
mg/kg
dry
0.789
0.00023
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00017
U
mg/kg
dry
0.789
0.00017
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,3-Dichlorobenzene [541-73-1]A
0.00019
U
mg/kg
dry
0.789
0.00019
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,3-Dichloropropane [142-28-9]A
0.00025
U
mg/kg
dry
0.789
0.00025
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
1,4-Dichlorobenzene [106-46-7]A
0.00017
U
mg/kg
dry
0.789
0.00017
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
2,2-Dichloropropane [594-20-7]A
0.00020
U
mg/kg
dry
0.789
0.00020
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
2-Butanone [78-93-3]A
0.00068
U
mg/kg
dry
0.789
0.00068
0.0044
OK18035
EPA
8260D
11/19/20
08:03
REF
QV-01
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00014
U
mg/kg
dry
0.789
0.00014
0.0044
OK18035
EPA
8260D
11/19/20
08:03
REF
2-Chlorotoluene [95-49-8]A
0.00016
U
mg/kg
dry
0.789
0.00016
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
2-Hexanone [591-78-6]A
0.00066
U
mg/kg
dry
0.789
0.00066
0.0044
OK18035
EPA
8260D
11/19/20
08:03
REF
4-Chlorotoluene [106-43-4]A
0.00023
U
mg/kg
dry
0.789
0.00023
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
4-Isopropyltoluene [99-87-6]A
0.00065
1
mg/kg
dry
0.789
0.00014
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
4-Methyl-2-pentanone [108-10-1]A
0.00050
U
mg/kg
dry
0.789
0.00050
0.0044
OK18035
EPA
8260D
11/19/20
08:03
REF
Acetone [67-64-1]A
0.036
mg/kg
dry
0.789
0.012
0.017
OK18035
EPA
8260D
11/19/20
08:03
REF
Benzene [71-43-2]A
0.00015
U
mg/kg
dry
0.789
0.00015
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
QV-01
Bromobenzene [108-86-1]A
0.00019
U
mg/kg
dry
0.789
0.00019
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Bromochloromethane [74-97-5]A
0.00036
U
mg/kg
dry
0.789
0.00036
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Bromodichloromethane [75-27-4]A
0.00021
U
mg/kg
dry
0.789
0.00021
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Bromoform [75-25-2]A
0.00039
U
mg/kg
dry
0.789
0.00039
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Bromomethane [74-83-9]A
0.00028
U
mg/kg
dry
0.789
0.00028
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Carbon disulfide [75-15-0]A
0.00034
U
mg/kg
dry
0.789
0.00034
0.0044
OK18035
EPA
8260D
11/19/20
08:03
REF
QV-01
Carbon Tetrachloride [56-23-5]A
0.00019
U
mg/kg
dry
0.789
0.00019
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Chlorobenzene [108-90-7]A
0.00015
U
mg/kg
dry
0.789
0.00015
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Chloroethane [75-00-3]A
0.00022
U
mg/kg
dry
0.789
0.00022
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Chloroform [67-66-3]A
0.00016
U
mg/kg
dry
0.789
0.00016
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Chloromethane [74-87-3]A
0.00018
U
mg/kg
dry
0.789
0.00018
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
QV-01
cis-1,2-Dichloroethene [156-59-2]A
0.00020
U
mg/kg
dry
0.789
0.00020
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00015
U
mg/kg
dry
0.789
0.00015
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Dibromochloromethane [124-48-1]A
0.00031
U
mg/kg
dry
0.789
0.00031
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Dibromomethane [74-95-3]A
0.00029
U
mg/kg
dry
0.789
0.00029
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Dichlorodifluoromethane [75-71-8]A
0.00039
U
mg/kg
dry
0.789
0.00039
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
Ethylbenzene [100-41-4]A
0.00017
U
mg/kg
dry
0.789
0.00017
0.00087
OK18035
EPA
8260D
11/19/20
08:03
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 66 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-43-6" Lab Sample ID:CD18880-25 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:55 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.20
Volatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analvte rCAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
Hexachlorobutadiene [87-68-3]A
0.00031
u
mg/kg
dry
0.789
0.00031
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
Isopropylbenzene [98-82-8]A
0.00013
u
mg/kg
dry
0.789
0.00013
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
m,p-Xylenes[108-38-3/106-42-3]A
0.00032
u
mg/kg
dry
0.789
0.00032
0.0017
OK18035
EPA 8260D
11/19/20
08:03
REF
Methylene Chloride [75-09-2]A
0.00064
u
mg/kg
dry
0.789
0.00064
0.0017
OK18035
EPA 8260D
11/19/20
08:03
REF QV-01
Methyl-tert-Butyl Ether [1634-04-4]A
0.00026
u
mg/kg
dry
0.789
0.00026
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
Naphthalene [91-20-3]A
0.00024
u
mg/kg
dry
0.789
0.00024
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
n-Butyl Benzene [104-51-8]A
0.00011
u
mg/kg
dry
0.789
0.00011
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
n-Propyl Benzene [103-65-1]A
0.00016
u
mg/kg
dry
0.789
0.00016
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
o-Xylene [95-47-6]A
0.00019
u
mg/kg
dry
0.789
0.00019
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
sec-Butylbenzene [135-98-8]A
0.00083
u
mg/kg
dry
0.789
0.00083
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
Styrene [500-42-5]A
0.14
mg/kg
dry
0.789
0.00086
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
tert-Butyl benzene [98-06-6]A
0.00015
u
mg/kg
dry
0.789
0.00015
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
Tetrachloroethene [127-18-4]A
0.00024
u
mg/kg
dry
0.789
0.00024
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
Toluene [108-88-3]A
0.00021
u
mg/kg
dry
0.789
0.00021
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
trans-1,2-Dichloroethene [156-60-5]A
0.00032
u
mg/kg
dry
0.789
0.00032
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF QV-01
trans-1,3-Dichloropropene [10061-02-6]A
0.00034
u
mg/kg
dry
0.789
0.00034
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
Trichloroethene [79-01-6]A
0.00028
u
mg/kg
dry
0.789
0.00028
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
Trichlorofluoromethane [75-69-4]A
0.00023
u
mg/kg
dry
0.789
0.00023
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
Vinyl chloride [75-01-4]A
0.00021
u
mg/kg
dry
0.789
0.00021
0.00087
OK18035
EPA 8260D
11/19/20
08:03
REF
Xylenes (Total) [1330-20-7]A
0.00049
u
mg/kg
dry
0.789
0.00049
0.0026
OK18035
EPA 8260D
11/19/20
08:03
REF
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
" Notes
4-Bromofluorobenzene
32
0.789
50.0
63 %
50-127
OK18035
EPA 8260D
11119120 08:03
REF
Dibromofluoromethane
34
0.789
50.0
68 %
52-128
OK18035
EPA 8260D
11119120 08:03
REF
Toluene-&
35
0.789
50.0
70 %
57-124
OK18035
EPA 8260D
11119120 08:03
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 5911
Analvte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]A
0.029
u
mg/kg dry
1
0.029
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
1,2-Dichlorobenzene [95-50-1]A
0.025
u
mg/kg dry
1
0.025
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
1,3-Dichlorobenzene [541-73-1]A
0.022
u
mg/kg dry
1
0.022
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
1,4-Dichlorobenzene [106-46-7]A
0.023
u
mg/kg dry
1
0.023
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
1-Methylnaphthalene [90-12-0]A
0.030
u
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2,4,5-Trichlorophenol [95-95-4]A
0.030
u
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2,4,6-Trichlorophenol [88-06-2]A
0.030
u
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2,4-Dichlorophenol [120-83-2]A
0.027
u
mg/kg dry
1
0.027
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2,4-Dimethylphenol [105-67-9]A
0.048
u
mg/kg dry
1
0.048
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2,4-Dinitrophenol [51-28-5]A
0.048
u
mg/kg dry
1
0.048
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2,4-Dinitrotoluene [121-14-2]A
0.031
u
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2,6-Dinitrotoluene [606-20-2]A
0.034
u
mg/kg dry
1
0.034
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2-Chloronaphthalene [91-58-7]A
0.031
u
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2-Chlorophenol [95-57-8]A
0.028
u
mg/kg dry
1
0.028
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]A
0.037
u
mg/kg dry
1
0.037
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM QV-01
2-Methylnaphthalene [91-57-6]A
0.031
u
mg/kg dry
1
0.031
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2-Methylphenol [95-48-7]A
0.028
u
mg/kg dry
1
0.028
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
2-Nitroaniline [88-74-4]A
0.033
u
mg/kg dry
1
0.033
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only
be reproduced in full.
Page 67 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-43-6" Lab Sample ID:CD18880-25 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 11:55 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.20
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]A
0.034
U
mg/kg
dry
1
0.034
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
U
mg/kg
dry
1
0.11
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
3-Nitroaniline [99-09-2]A
0.040
U
mg/kg
dry
1
0.040
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.030
U
mg/kg
dry
1
0.030
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
4-Chloroaniline [106-47-8]A
0.10
U
mg/kg
dry
1
0.10
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
4-Nitroaniline [100-01-6]A
0.059
U
mg/kg
dry
1
0.059
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
4-Nitrophenol [100-02-7]A
0.034
U
mg/kg
dry
1
0.034
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Acenaphthene [83-32-9]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Acenaphthylene [208-96-8]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Anthracene[120-12-7]A
0.042
U
mg/kg
dry
1
0.042
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Benzidine [92-87-5]A
0.12
U
mg/kg
dry
1
0.12
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Benzo(a)anthracene [56-55-3]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Benzo(a)pyrene [50-32-8]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Benzo(b)fluoranthene [205-99-2]A
0.020
U
mg/kg
dry
1
0.020
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.052
U
mg/kg
dry
1
0.052
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM QV-01
Benzo(k)fluoranthene [207-08-9]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Benzoic acid [65-85-O]A
0.25
J
mg/kg
dry
1
0.17
1.9
OK19001
EPA
8270E
11/23/20
19:57
DFM
Benzyl alcohol [100-51-6]A
0.025
U
mg/kg
dry
1
0.025
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.028
U
mg/kg
dry
1
0.028
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.048
U
mg/kg
dry
1
0.048
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.027
U
mg/kg
dry
1
0.027
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.039
U
mg/kg
dry
1
0.039
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Butylbenzylphthalate [85-68-7]A
0.044
U
mg/kg
dry
1
0.044
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Chrysene [218-01-9]A
0.033
U
mg/kg
dry
1
0.033
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.057
U
mg/kg
dry
1
0.057
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Dibenzofuran [132-64-9]A
0.030
U
mg/kg
dry
1
0.030
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Diethylphthalate [84-66-2]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Dimethylphthalate [131-11-3]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Di-n-butylphthalate [84-74-2]A
0.045
U
mg/kg
dry
1
0.045
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Di-n-octylphthalate [117-84-O]A
0.037
U
mg/kg
dry
1
0.037
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Fluoranthene [206-44-O]A
0.040
U
mg/kg
dry
1
0.040
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Fluorene [86-73-7]A
0.032
U
mg/kg
dry
1
0.032
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Hexachlorobenzene [118-74-1]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Hexachlorobutadiene [87-68-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Hexachlorocyclopentadiene [77-47-4]A
0.043
U
mg/kg
dry
1
0.043
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Hexachloroethane [67-72-1]A
0.023
U
mg/kg
dry
1
0.023
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.052
U
mg/kg
dry
1
0.052
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Isophorone[78-59-1]A
0.033
U
mg/kg
dry
1
0.033
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Naphthalene [91-20-3]A
0.031
U
mg/kg
dry
1
0.031
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
Nitrobenzene [98-95-3]A
0.029
U
mg/kg
dry
1
0.029
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
N-Nitrosodimethylamine [62-75-9]A
0.023
U
mg/kg
dry
1
0.023
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.090
U
mg/kg
dry
1
0.090
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
N-nitrosodiphenylamine/Diphenylamine
0.060
U
mg/kg
dry
1
0.060
0.37
OK19001
EPA
8270E
11/23/20
19:57
DFM
[86-30-6/122-39-4]A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 68 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-43-6" Lab Sample ID:CD18880-25 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 11:55 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.20
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.037
U
mg/kg dry
1
0.037
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
Phenanthrene[85-01-8]^
0.030
U
mg/kg dry
1
0.030
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
Phenol[108-95-2]^
0.024
U
mg/kg dry
1
0.024
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
Pyrene [129-00-0]^
0.042
U
mg/kg dry
1
0.042
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
Pyridine [110-86-1]^
0.091
U
mg/kg dry
1
0.091
0.37
OK19001
EPA 8270E
11/23/20 19:57
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.5
1
3.70
120 %
26-130
OK19001
EPA 8270E
11/23/2019:57
DFM
2-Fluorobiphenyl
1.9
1
1.85
100 %
56-120
OK19001
EPA 8270E
11123120 19:57
DFM
2-Fluorophenol
3.7
1
3.70
101 %
49-126
OK19001
EPA 8270E
11123120 19:57
DFM
Nitrobenzene-d5
I.8
1
1.85
98 %
50-117
OK19001
EPA 8270E
11/23/2019:57
DFM
Phenol-d5
4.1
1
3.70
112 %
56-120
OK19001
EPA 8270E
11/23/2019:57
DFM
Terphenyl-d14
1.6
1
1.65
87 %
36-151
OK19001
EPA 8270E
11/23/2019:57
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]1
23.5
mg/kg dry
1
0.133 0.554
OK20031
EPA 6010D
11/23/20 15:25
JDH
Description: HA-44-6" Lab Sample ID: CD18880-27 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 13:30 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.30
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^ 487
mg/kg dry
1
0.139
0.579
OK30010
EPA 6010D
12/01/20 10:13
JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]^ 4.35
mg/L
50
0.155
0.500
OL14039
EPA 6010D
12/15/20 13:19
JDH
Description: HA-44-18" Lab Sample ID:CD18880-28 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 13:35 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence a/o Solids: 90.49
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 23.8 mg/kg dry 1 0.133 0.553 OL04013 EPA 6010D 12/07/20 10:47 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 69 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-45-6 Lab Sample ID:CD18880-29 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 13:45 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.26
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Iy Notes
Lead [7439-92-1]^ 128 mg/kg dry 1 0.141 0.586 OK30010 EPA 6010D 12/01/20 10:15 JDH
Description: HA-45-18" Lab Sample ID:CD18880-30 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 13:50 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 87.15
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes
Lead [7439-92-1]^ 22.0 mg/kg dry 1 0.138 0.574 OL04013 EPA 6010D 12/07/20 11:17 JDH
Description: HA-46-6" Lab Sample ID:CD18880-31 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 14:00 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 81.50
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units DF MDL P L Batch
Method
Analyzed By Notes
Lead [7439-92-1]^ 535
mg/kg dry 1 0.147 0.614 OK30010
EPA 6010D
12/01/20 10:17 JDH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag
Units DF MDL P L Batch
Method
Analyzed By Notes
Lead [7439-92-1]^ 5.72
mg/L 50 0.155 0.500 OL14039
EPA 6010D
12/15/20 13:21 JDH
Description: HA-46-18"
Lab Sample ID:CD18880-32
Received: 11/17/20 17:10
Matrix: Soil
Sampled: 11/17/20 14:05
Work Order: CD18880
Project: Sir Walter Gun Club
Sampled By: Bryan S. Wence
% Solids: 89.74
(Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed Notes
Lead [7439-92-1]^ 7.38 mg/kg dry 1 0.134 0.557 OL04013 EPA 6010D 12/07/20 11:19 JDH
Description: HA-48-6" Lab Sample ID:CD18880-35 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 14:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 82.20
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL IQ Batch Method Analyzed I� Notes
Lead [7439-92-1]^ 207 mg/kg dry 1 0.146 0.608 OK30010 EPA 6010D 12/01/20 10:19 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 70 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-48-18" Lab Sample ID:CD1888O-36 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 14:45 Work Order: CD1888O
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 85.27
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL PDL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 6.30 mg/kg dry 1 0.141 0.586 OL04013 EPA 6010D 12/07/20 11:21 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 71 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: DUP-11-17-20-6 Lab Sample ID:CD18880-37 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 15:00 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.67
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.00015
u
mg/kg
dry
0.85
0.00015
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,1,1-Trichloroethane [71-55-6]A
0.00023
u
mg/kg
dry
0.85
0.00023
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.00019
u
mg/kg
dry
0.85
0.00019
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,1,2-Trichloroethane [79-00-5]A
0.00023
u
mg/kg
dry
0.85
0.00023
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,1-Dichloroethane [75-34-3]A
0.00023
u
mg/kg
dry
0.85
0.00023
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
QV-01
1,1-Dichloroethene [75-35-4]A
0.00028
u
mg/kg
dry
0.85
0.00028
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,1-Dichloropropene [563-58-6]A
0.00015
u
mg/kg
dry
0.85
0.00015
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,2,3-Trichlorobenzene [87-61-6]A
0.00026
u
mg/kg
dry
0.85
0.00026
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,2,3-Trichloropropane [96-18-4]A
0.00060
u
mg/kg
dry
0.85
0.00060
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,2,4-Trichlorobenzene [120-82-1]A
0.00025
u
mg/kg
dry
0.85
0.00025
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.00016
u
mg/kg
dry
0.85
0.00016
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,2-Dibromo-3-chloropropane [96-12-8]A
0.00074
u
mg/kg
dry
0.85
0.00074
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,2-Dibromoethane [106-93-4]A
0.00043
u
mg/kg
dry
0.85
0.00043
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,2-Dichlorobenzene [95-50-1]A
0.00025
u
mg/kg
dry
0.85
0.00025
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,2-Dichloroethane [107-06-2]A
0.00038
u
mg/kg
dry
0.85
0.00038
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,2-Dichloropropane [78-87-5]A
0.00024
u
mg/kg
dry
0.85
0.00024
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.00019
u
mg/kg
dry
0.85
0.00019
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,3-Dichlorobenzene [541-73-1]A
0.00021
u
mg/kg
dry
0.85
0.00021
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,3-Dichloropropane [142-28-9]A
0.00027
u
mg/kg
dry
0.85
0.00027
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
1,4-Dichlorobenzene [106-46-7]A
0.00019
u
mg/kg
dry
0.85
0.00019
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
2,2-Dichloropropane [594-20-7]A
0.00022
u
mg/kg
dry
0.85
0.00022
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
2-Butanone [78-93-3]A
0.00073
u
mg/kg
dry
0.85
0.00073
0.0047
OK18035
EPA
8260D
11/19/20
08:33
REF
QV-01
2-Chloroethyl Vinyl Ether [110-75-8]A
0.00015
u
mg/kg
dry
0.85
0.00015
0.0047
OK18035
EPA
8260D
11/19/20
08:33
REF
2-Chlorotoluene [95-49-8]A
0.00017
u
mg/kg
dry
0.85
0.00017
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
2-Hexanone [591-78-6]A
0.00070
u
mg/kg
dry
0.85
0.00070
0.0047
OK18035
EPA
8260D
11/19/20
08:33
REF
4-Chlorotoluene [106-43-4]A
0.00024
u
mg/kg
dry
0.85
0.00024
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
4-Isopropyltoluene [99-87-6]A
0.0048
mg/kg
dry
0.85
0.00015
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
4-Methyl-2-pentanone [108-10-1]A
0.00053
u
mg/kg
dry
0.85
0.00053
0.0047
OK18035
EPA
8260D
11/19/20
08:33
REF
Acetone [67-64-1]A
0.10
mg/kg
dry
0.85
0.013
0.019
OK18035
EPA
8260D
11/19/20
08:33
REF
Benzene[71-43-2]A
0.00016
u
mg/kg
dry
0.85
0.00016
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
QV-01
Bromobenzene [108-86-1]A
0.00021
u
mg/kg
dry
0.85
0.00021
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Bromochloromethane [74-97-5]A
0.00038
u
mg/kg
dry
0.85
0.00038
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Bromodichloromethane [75-27-4]A
0.00023
u
mg/kg
dry
0.85
0.00023
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Bromoform [75-25-2]A
0.00042
u
mg/kg
dry
0.85
0.00042
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Bromomethane [74-83-9]A
0.00030
u
mg/kg
dry
0.85
0.00030
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Carbon disulfide [75-15-0]A
0.00037
u
mg/kg
dry
0.85
0.00037
0.0047
OK18035
EPA
8260D
11/19/20
08:33
REF
QV-01
Carbon Tetrachloride [56-23-5]A
0.00021
u
mg/kg
dry
0.85
0.00021
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Chlorobenzene [108-90-7]A
0.00016
u
mg/kg
dry
0.85
0.00016
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Chloroethane [75-00-3]A
0.00023
u
mg/kg
dry
0.85
0.00023
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Chloroform [67-66-3]A
0.00017
u
mg/kg
dry
0.85
0.00017
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Chloromethane [74-87-3]A
0.00020
u
mg/kg
dry
0.85
0.00020
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
QV-01
cis-1,2-Dichloroethene [156-59-2]A
0.00022
u
mg/kg
dry
0.85
0.00022
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
cis-1,3-Dichloropropene [10061-01-5]A
0.00016
u
mg/kg
dry
0.85
0.00016
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Dibromochloromethane [124-48-1]A
0.00033
u
mg/kg
dry
0.85
0.00033
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Dibromomethane [74-95-3]A
0.00031
u
mg/kg
dry
0.85
0.00031
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Dichlorodifluoromethane [75-71-8]A
0.00042
u
mg/kg
dry
0.85
0.00042
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
Ethylbenzene [100-41-4]A
0.00019
u
mg/kg
dry
0.85
0.00019
0.00094
OK18035
EPA
8260D
11/19/20
08:33
REF
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page
72 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: DUP-11-17-20-6" Lab Sample ID:CD18880-37 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 15:00 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.67
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Hexachlorobutadiene [87-68-3]^
0.00033
U
mg/kg
dry
0.85
0.00033
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
Isopropyl benzene [98-82-8]^
0.00014
U
mg/kg
dry
0.85
0.00014
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.00035
U
mg/kg
dry
0.85
0.00035
0.0019
OK18035
EPA 8260D
11/19/20
08:33
REF
Methylene Chloride [75-09-2]^
0.00068
U
mg/kg
dry
0.85
0.00068
0.0019
OK18035
EPA 8260D
11/19/20
08:33
REF QV-01
Methyl-tert-Butyl Ether [1634-04-4]^
0.00028
U
mg/kg
dry
0.85
0.00028
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
Naphthalene [91-20-3]^
0.00025
U
mg/kg
dry
0.85
0.00025
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
n-Butyl Benzene [104-51-8]^
0.00012
U
mg/kg
dry
0.85
0.00012
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
n-Propyl Benzene [103-65-1]^
0.00017
U
mg/kg
dry
0.85
0.00017
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
o-Xylene [95-47-6]^
0.00021
U
mg/kg
dry
0.85
0.00021
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
sec-Butylbenzene [135-98-8]^
0.00089
U
mg/kg
dry
0.85
0.00089
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
Styrene [100-42-5]^
0.0076
mg/kg
dry
0.85
0.00092
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
tert-Butylbenzene [98-06-6]^
0.00016
U
mg/kg
dry
0.85
0.00016
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
Tetrachloroethene [127-18-4]^
0.00026
U
mg/kg
dry
0.85
0.00026
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
Toluene [108-88-3]^
0.00023
U
mg/kg
dry
0.85
0.00023
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
trans-1,2-Dichloroethene [156-60-5]^
0.00035
U
mg/kg
dry
0.85
0.00035
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF QV-01
trans-1,3-Dichloropropene [10061-02-6]^
0.00037
U
mg/kg
dry
0.85
0.00037
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
Trichloroethene [79-01-6]^
0.00030
U
mg/kg
dry
0.85
0.00030
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
Trichlorofluoromethane [75-69-4]^
0.00024
U
mg/kg
dry
0.85
0.00024
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
Vinyl chloride [75-01-4]^
0.00023
U
mg/kg
dry
0.85
0.00023
0.00094
OK18035
EPA 8260D
11/19/20
08:33
REF
Xylenes (Total) [1330-20-7]^
0.00053
U
mg/kg
dry
0.85
0.00053
0.0028
OK18035
EPA 8260D
11/19/20
08:33
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
31
0.85
50.0
62 %
50-127
OK18035
EPA 6260D
11119120 08:33
REF
Dlbromofluoromethane
37
0.85
50.0
75 %
52-128
OK18035
EPA 8260D
11119120 08:33
REF
Toluene-d8
35
0.85
50.0
69 %
57-124
OK18035
EPA 8260D
11119120 08:33
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4-Trichlorobenzene [120-82-1]^
0.029
U
mg/kg dry
1
0.029
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
1,2-Dichlorobenzene [95-50-1]^
0.025
U
mg/kg dry
1
0.025
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
1,3-Dichlorobenzene [541-73-1]^
0.022
U
mg/kg dry
1
0.022
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
1,4-Dichlorobenzene [106-46-7]^
0.023
U
mg/kg dry
1
0.023
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
1- Methyl naphthalene [90-12-0]^
0.030
U
mg/kg dry
1
0.030
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2,4,5-Trichlorophenol[95-95-4]^
0.030
U
mg/kg dry
1
0.030
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2,4,6-Trichlorophenol[88-06-2]^
0.030
U
mg/kg dry
1
0.030
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2,4-Dichlorophenol [120-83-2]^
0.026
U
mg/kg dry
1
0.026
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2,4-Di methyl phenol [105-67-9]^
0.047
U
mg/kg dry
1
0.047
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2,4-Dinitrophenol [51-28-5]^
0.047
U
mg/kg dry
1
0.047
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2,4-Dinitrotoluene [121-14-2]^
0.031
U
mg/kg dry
1
0.031
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2,6-Dinitrotoluene [606-20-2]^
0.034
U
mg/kg dry
1
0.034
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2-Chloronaphthalene [91-58-7]^
0.031
U
mg/kg dry
1
0.031
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2-Chlorophenol [95-57-8]^
0.028
U
mg/kg dry
1
0.028
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
0.036
U
mg/kg dry
1
0.036
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM QV-01
2- Methyl naphthalene [91-57-6]^
0.031
U
mg/kg dry
1
0.031
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2-Methylphenol [95-48-7]^
0.028
U
mg/kg dry
1
0.028
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
2-Nitroaniline [88-74-4]^
0.033
U
mg/kg dry
1
0.033
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
FINAL
This report relates only
to the
sample as received by the laboratory,
and may only
be reproduced in full.
Page 73 of 107

0Nk"q09
www.encolabs.com
ANALYTICAL RESULTS
Description: DUP-11-17-20-6" Lab Sample ID:CD18880-37 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 15:00 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.67
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
2-Nitrophenol [88-75-5]A
0.034
U
mg/kg
dry
1
0.034
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.029
U
mg/kg
dry
1
0.029
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
U
mg/kg
dry
1
0.11
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
3-Nitroaniline [99-09-2]A
0.040
U
mg/kg
dry
1
0.040
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.030
U
mg/kg
dry
1
0.030
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.036
U
mg/kg
dry
1
0.036
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
4-Chloroaniline [106-47-8]A
0.10
U
mg/kg
dry
1
0.10
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.029
U
mg/kg
dry
1
0.029
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
4-Nitroaniline [100-01-6]A
0.058
U
mg/kg
dry
1
0.058
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
4-Nitrophenol [100-02-7]A
0.034
U
mg/kg
dry
1
0.034
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Acenaphthene [83-32-9]A
0.031
U
mg/kg
dry
1
0.031
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Acenaphthylene [208-96-8]A
0.031
U
mg/kg
dry
1
0.031
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Anthracene[120-12-7]A
0.042
U
mg/kg
dry
1
0.042
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Benzidine [92-87-5]A
0.12
U
mg/kg
dry
1
0.12
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Benzo(a)anthracene [56-55-3]A
0.031
U
mg/kg
dry
1
0.031
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Benzo(a)pyrene[50-32-8]A
0.036
U
mg/kg
dry
1
0.036
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Benzo(b)fluoranthene [205-99-2]A
0.020
U
mg/kg
dry
1
0.020
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.052
U
mg/kg
dry
1
0.052
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM QV-01
Benzo(k)fluoranthene [207-08-9]A
0.036
U
mg/kg
dry
1
0.036
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Benzoic acid [65-85-O]A
0.90
J
mg/kg
dry
1
0.17
1.9
OK19001
EPA
8270E
11/23/20
20:28
DFM
Benzyl alcohol [100-51-6]A
0.025
U
mg/kg
dry
1
0.025
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.028
U
mg/kg
dry
1
0.028
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.047
U
mg/kg
dry
1
0.047
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.026
U
mg/kg
dry
1
0.026
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.039
U
mg/kg
dry
1
0.039
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Butylbenzylphthalate [85-68-7]A
0.044
U
mg/kg
dry
1
0.044
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Chrysene [218-01-9]A
0.033
U
mg/kg
dry
1
0.033
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.056
U
mg/kg
dry
1
0.056
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Dibenzofuran [132-64-9]A
0.030
U
mg/kg
dry
1
0.030
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Diethylphthalate [84-66-2]A
0.031
U
mg/kg
dry
1
0.031
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Dimethylphthalate [131-11-3]A
0.036
U
mg/kg
dry
1
0.036
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Di-n-butylphthalate [84-74-2]A
0.045
U
mg/kg
dry
1
0.045
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Di-n-octylphthalate [117-84-O]A
0.036
U
mg/kg
dry
1
0.036
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Fluoranthene [206-44-O]A
0.040
U
mg/kg
dry
1
0.040
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Fluorene [86-73-7]A
0.032
U
mg/kg
dry
1
0.032
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Hexachlorobenzene [118-74-1]A
0.029
U
mg/kg
dry
1
0.029
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Hexachlorobutadiene [87-68-3]A
0.029
U
mg/kg
dry
1
0.029
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Hexachlorocyclopentadiene [77-47-4]A
0.043
U
mg/kg
dry
1
0.043
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Hexachloroethane [67-72-1]A
0.023
U
mg/kg
dry
1
0.023
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.052
U
mg/kg
dry
1
0.052
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Isophorone[78-59-1]A
0.033
U
mg/kg
dry
1
0.033
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Naphthalene [91-20-3]A
0.031
U
mg/kg
dry
1
0.031
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
Nitrobenzene [98-95-3]A
0.029
U
mg/kg
dry
1
0.029
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
N-Nitrosodimethylamine [62-75-9]A
0.023
U
mg/kg
dry
1
0.023
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.089
U
mg/kg
dry
1
0.089
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
N-nitrosodiphenylamine/Diphenylamine
0.060
U
mg/kg
dry
1
0.060
0.36
OK19001
EPA
8270E
11/23/20
20:28
DFM
[86-30-6/122-39-4]A
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 74 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: DUP-11-17-20-6" Lab Sample ID:CD18880-37 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 15:00 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 90.67
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Pentachlorophenol [87-86-5]^
0.036
U
mg/kg dry
1
0.036
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
Phenanthrene[85-01-8]^
0.030
U
mg/kg dry
1
0.030
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
Phenol[108-95-2]^
0.024
U
mg/kg dry
1
0.024
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
Pyrene [129-00-0]^
0.042
U
mg/kg dry
1
0.042
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
Pyridine [110-86-1]^
0.090
U
mg/kg dry
1
0.090
0.36
OK19001
EPA 8270E
11/23/20 20:28
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
4.2
1
3.66
113 %
26-130
OK19001
EPA 8270E
11123120 20:28
DFM
2-Fluorobiphenyl
1.7
1
1.84
94 %
56-120
OK19001
EPA 8270E
11123120 20:28
DFM
2-Fluorophenol
3.5
1
3.66
95 %
49-126
OK19001
EPA 8270E
11123120 20:28
DFM
Nitrobenzene-d5
1.7
1
1.84
92 %
50-117
OK19001
EPA 8270E
11123120 20:28
DFM
Phenol-d5
3.8
1
3.66
103 %
56-120
OK19001
EPA 8270E
11123120 20:28
DFM
Terphenyl-d14
1.6
1
1.64
86 %
36-151
OK19001
EPA 8270E
11123120 20:28
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay Notes
Lead [7439-92-1]^
251
mg/kg dry
1
0.132 0.551
OK20031
EPA 6010D
11/23/20 15:27
JDH
Description: DUP-11-17-20-18" Lab Sample ID: CD18880-38 Received: 11/17/20 17:10
Matrix: Soil Sampled: 11/17/20 15:05 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 91.14
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flaa Units DF MDL PQL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 43.8 mg/kg dry 1 0.132 0.549 OK30010 EPA 6010D 12/01/20 10:22 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 75 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-50-6" Lab Sample ID:CD18880-41 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 15:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.72
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]A
0.029
u
mg/kg dry
1
0.029
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
1,2-Dichlorobenzene [95-50-1]A
0.026
u
mg/kg dry
1
0.026
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
1,3-Dichlorobenzene [541-73-1]A
0.022
u
mg/kg dry
1
0.022
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
1,4-Dichlorobenzene [106-46-7]A
0.023
u
mg/kg dry
1
0.023
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
1-Methylnaphthalene [90-12-O]A
0.030
u
mg/kg dry
1
0.030
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2,4,5-Trichlorophenol [95-95-4]A
0.030
u
mg/kg dry
1
0.030
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2,4,6-Trichlorophenol [88-06-2]A
0.030
u
mg/kg dry
1
0.030
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2,4-Dichlorophenol [120-83-2]A
0.027
u
mg/kg dry
1
0.027
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2,4-Dimethylphenol [105-67-9]A
0.048
u
mg/kg dry
1
0.048
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2,4-Dinitrophenol [51-28-5]A
0.048
u
mg/kg dry
1
0.048
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2,4-Dinitrotoluene [121-14-2]A
0.031
u
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2,6-Dinitrotoluene [606-20-2]A
0.035
u
mg/kg dry
1
0.035
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2-Chloronaphthalene [91-58-7]A
0.031
u
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2-Chlorophenol [95-57-8]A
0.028
u
mg/kg dry
1
0.028
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]A
0.037
u
mg/kg dry
1
0.037
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2-Methylnaphthalene [91-57-6]A
0.031
u
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2-Methylphenol [95-48-7]A
0.028
u
mg/kg dry
1
0.028
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2-Nitroaniline [88-74-4]A
0.033
u
mg/kg dry
1
0.033
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
2-Nitrophenol [88-75-5]A
0.035
u
mg/kg dry
1
0.035
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.029
u
mg/kg dry
1
0.029
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
u
mg/kg dry
1
0.11
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
3-Nitroaniline [99-09-2]A
0.040
u
mg/kg dry
1
0.040
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.030
u
mg/kg dry
1
0.030
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.037
u
mg/kg dry
1
0.037
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
4-Chloroaniline [106-47-8]A
0.10
u
mg/kg dry
1
0.10
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.029
u
mg/kg dry
1
0.029
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
4-Nitroaniline [100-01-6]A
0.059
u
mg/kg dry
1
0.059
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
4-Nitrophenol[100-02-7]A
0.074
J
mg/kg dry
1
0.035
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Acenaphthene [83-32-9]A
0.031
u
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Acenaphthylene [208-96-8]A
0.031
u
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Anthracene[120-12-7]A
0.042
u
mg/kg dry
1
0.042
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Benzidine [92-87-5]A
0.12
u
mg/kg dry
1
0.12
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Benzo(a)anthracene [56-55-3]A
0.031
u
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Benzo(a)pyrene [50-32-8]A
0.037
u
mg/kg dry
1
0.037
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Benzo(b)fluoranthene [205-99-2]A
0.020
u
mg/kg dry
1
0.020
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.052
u
mg/kg dry
1
0.052
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Benzo(k)fluoranthene [207-08-9]A
0.037
u
mg/kg dry
1
0.037
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Benzoic acid [65-85-O]A
0.17
u
mg/kg dry
1
0.17
1.9
OK25001
EPA 8270E
11/25/20 17:06
DFM
Benzyl alcohol [100-51-6]A
0.026
u
mg/kg dry
1
0.026
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.028
u
mg/kg dry
1
0.028
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.048
u
mg/kg dry
1
0.048
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.027
u
mg/kg dry
1
0.027
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.039
u
mg/kg dry
1
0.039
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Butylbenzylphthalate [85-68-7]A
0.045
u
mg/kg dry
1
0.045
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Chrysene [218-01-9]A
0.033
u
mg/kg dry
1
0.033
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.057
u
mg/kg dry
1
0.057
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Dibenzofuran [132-64-9]A
0.030
u
mg/kg dry
1
0.030
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 76 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-50-6" Lab Sample ID:CD18880-41 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 15:40 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 89.72
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified anaiyte [NC 591]
Analvte ICAS Numberl
Results
Flag
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Diethylphthalate [84-66-2]A
0.031
U
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Dimethylphthalate [131-11-3]A
0.037
U
mg/kg dry
1
0.037
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Di-n-butylphthalate [84-74-2]A
0.046
U
mg/kg dry
1
0.046
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Di-n-octylphthalate [117-84-0]A
0.037
U
mg/kg dry
1
0.037
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Fluoranthene [206-44-0]A
0.040
U
mg/kg dry
1
0.040
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Fluorene [86-73-7]A
0.032
U
mg/kg dry
1
0.032
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Hexachlorobenzene [118-74-1]A
0.029
U
mg/kg dry
1
0.029
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Hexachlorobutadiene [87-68-3]A
0.029
U
mg/kg dry
1
0.029
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Hexachlorocyclopentadiene [77-47-4]A
0.043
U
mg/kg dry
1
0.043
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Hexachloroethane [67-72-1]A
0.023
U
mg/kg dry
1
0.023
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
0.052
U
mg/kg dry
1
0.052
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Isophorone[78-59-1]A
0.033
U
mg/kg dry
1
0.033
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Naphthalene [91-20-3]A
0.031
U
mg/kg dry
1
0.031
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Nitrobenzene [98-95-3]A
0.029
U
mg/kg dry
1
0.029
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
N-Nitrosodimethylamine [62-75-9]A
0.023
U
mg/kg dry
1
0.023
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
0.090
U
mg/kg dry
1
0.090
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
N-nitrosodiphenylamine/Diphenylamine
0.060
U
mg/kg dry
1
0.060
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
[86-30-6/122-39-4]A
Pentachlorophenol [87-86-5]A
0.037
U
mg/kg dry
1
0.037
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Phenanthrene [85-01-8]A
0.030
U
mg/kg dry
1
0.030
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Phenol[108-95-2]A
0.025
U
mg/kg dry
1
0.025
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Pyrene [129-00-0]A
0.042
U
mg/kg dry
1
0.042
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Pyridine [110-86-1]A
0.091
U
mg/kg dry
1
0.091
0.37
OK25001
EPA 8270E
11/25/20 17:06
DFM
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analyzed
fly Notes
2,4,6-Tribromophenol
4.2
1
3.72
112 %
28-130
OK25OO1
EPA 8270E
1112512017:06
DFM
2-Fluorobiphenyl
1.8
1
1.86
99 %
56-120
OK25OO1
EPA 8270E
1112512017:06
DFM
2-Fluorophenol
3.5
1
3.72
95 %
49-126
OK25OO1
EPA 8270E
1112512017:06
DFM
Nitrobenzene-d5
1.8
1
1.86
95 %
50-117
OK25OO1
EPA 8270E
1112512017:06
DFM
Phenol-d5
3.7
1
3.72
100 %
56-120
OK25OO1
EPA 8270E
1112512017:06
DFM
Terphenyl-d14
2.1
1
1.86
112 %
36-151
OK25OO1
EPA 8270E
1112512017:06
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified anaiyte [NC 591]
Analvte MAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]A
10.6
mg/kg dry
1
0.134 0.557
OK30010
EPA 6010D
12/01/20 10:23
JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 77 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-51-6" Lab Sample ID:CD18880-43 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 15:50 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.26
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,2,4-Trichlorobenzene [120-82-1]A
0.030
u
mg/kg dry
1
0.030
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
1,2-Dichlorobenzene [95-50-1]A
0.027
u
mg/kg dry
1
0.027
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
1,3-Dichlorobenzene [541-73-1]A
0.023
u
mg/kg dry
1
0.023
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
1,4-Dichlorobenzene [106-46-7]A
0.024
u
mg/kg dry
1
0.024
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
1-Methylnaphthalene [90-12-0]A
0.031
u
mg/kg dry
1
0.031
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2,4,5-Trichlorophenol [95-95-4]A
0.031
u
mg/kg dry
1
0.031
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2,4,6-Trichlorophenol [88-06-2]A
0.031
u
mg/kg dry
1
0.031
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2,4-Dichlorophenol [120-83-2]A
0.028
u
mg/kg dry
1
0.028
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2,4-Dimethylphenol [105-67-9]A
0.050
u
mg/kg dry
1
0.050
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2,4-Dinitrophenol [51-28-5]A
0.050
u
mg/kg dry
1
0.050
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2,4-Dinitrotoluene [121-14-2]A
0.032
u
mg/kg dry
1
0.032
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2,6-Dinitrotoluene [606-20-2]A
0.036
u
mg/kg dry
1
0.036
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2-Chloronaphthalene [91-58-7]A
0.032
u
mg/kg dry
1
0.032
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2-Chlorophenol [95-57-8]A
0.029
u
mg/kg dry
1
0.029
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2-Methyl-4,6-dinitrophenol [534-52-1]A
0.038
u
mg/kg dry
1
0.038
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2-Methylnaphthalene [91-57-6]A
0.032
u
mg/kg dry
1
0.032
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2-Methylphenol [95-48-7]A
0.029
u
mg/kg dry
1
0.029
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2-Nitroaniline [88-74-4]A
0.035
u
mg/kg dry
1
0.035
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
2-Nitrophenol [88-75-5]A
0.036
u
mg/kg dry
1
0.036
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
3 & 4-Methylphenol [108-39-4/106-44-5]A
0.030
u
mg/kg dry
1
0.030
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
3,3'-Dichlorobenzidine [91-94-1]A
0.11
u
mg/kg dry
1
0.11
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
3-Nitroaniline [99-09-2]A
0.042
u
mg/kg dry
1
0.042
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
4-Bromophenyl-phenylether [101-55-3]A
0.031
u
mg/kg dry
1
0.031
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
4-Chloro-3-methylphenol [59-50-7]A
0.038
u
mg/kg dry
1
0.038
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
4-Chloroaniline [106-47-8]A
0.11
u
mg/kg dry
1
0.11
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
4-Chlorophenyl-phenylether [7005-72-3]A
0.030
u
mg/kg dry
1
0.030
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
4-Nitroaniline [100-01-6]A
0.061
u
mg/kg dry
1
0.061
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
4-Nitrophenol [100-02-7]A
0.036
u
mg/kg dry
1
0.036
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Acenaphthene [83-32-9]A
0.032
u
mg/kg dry
1
0.032
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Acenaphthylene [208-96-8]A
0.032
u
mg/kg dry
1
0.032
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Anthracene[120-12-7]A
0.044
u
mg/kg dry
1
0.044
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Benzidine [92-87-5]A
0.13
u
mg/kg dry
1
0.13
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Benzo(a)anthracene [56-55-3]A
0.032
u
mg/kg dry
1
0.032
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Benzo(a)pyrene [50-32-8]A
0.038
u
mg/kg dry
1
0.038
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Benzo(b)fluoranthene [205-99-2]A
0.021
u
mg/kg dry
1
0.021
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Benzo(g,h,i)perylene [191-24-2]A
0.054
u
mg/kg dry
1
0.054
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Benzo(k)fluoranthene [207-08-9]A
0.038
u
mg/kg dry
1
0.038
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Benzoic acid [65-85-0]A
0.17
u
mg/kg dry
1
0.17
2.0
OK25001
EPA 8270E
11/25/20 17:37
DFM
Benzyl alcohol [100-51-6]A
0.027
u
mg/kg dry
1
0.027
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
0.029
u
mg/kg dry
1
0.029
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Bis(2-chloroethyl)ether [111-44-4]A
0.050
u
mg/kg dry
1
0.050
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
0.028
u
mg/kg dry
1
0.028
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
0.041
u
mg/kg dry
1
0.041
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Butylbenzylphthalate [85-68-7]A
0.046
u
mg/kg dry
1
0.046
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Chrysene [218-01-9]A
0.035
u
mg/kg dry
1
0.035
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Dibenzo(a,h)anthracene [53-70-3]A
0.059
u
mg/kg dry
1
0.059
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
Dibenzofuran [132-64-9]A
0.031
u
mg/kg dry
1
0.031
0.38
OK25001
EPA 8270E
11/25/20 17:37
DFM
FINAL
This report relates only to the sample as received by the laboratory,
and may only be reproduced in full.
Page 78 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: HA-51-6 Lab Sample ID:CD18880-43 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 15:50 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 86.26
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
Diethylphtha late [84-66-2]^
0.032
U
mg/kg
dry
1
0.032
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Dirrethylphtha late [131-11-3]^
0.038
U
mg/kg
dry
1
0.038
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Di-n-butylphthalate [84-74-2]^
0.048
U
mg/kg
dry
1
0.048
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Di-n-octylphthalate [117-84-O]^
0.038
U
mg/kg
dry
1
0.038
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Fluoranthene [206-44-O]^
0.042
U
mg/kg
dry
1
0.042
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Fluorene [86-73-7]^
0.034
U
mg/kg
dry
1
0.034
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Hexachlorobenzene [118-74-1]1
0.030
U
mg/kg
dry
1
0.030
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Hexachlorobutadiene [87-68-3]^
0.030
U
mg/kg
dry
1
0.030
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Hexachlorocyclopentadiene [77-47-4]^
0.045
U
mg/kg
dry
1
0.045
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Hexachloroethane [67-72-1]^
0.024
U
mg/kg
dry
1
0.024
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]^
0.054
U
mg/kg
dry
1
0.054
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Isophorone[78-59-1]^
0.035
U
mg/kg
dry
1
0.035
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Naphthalene [91-20-3]^
0.032
U
mg/kg
dry
1
0.032
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Nitrobenzene [98-95-3]^
0.030
U
mg/kg
dry
1
0.030
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
N-Nitrosodimethylamine [62-75-9]^
0.024
U
mg/kg
dry
1
0.024
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
N-Nitroso-di-n-propylamine [621-64-7]^
0.094
U
mg/kg
dry
1
0.094
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
N-nitrosodiphenylamine/Diphenylamine
0.063
U
mg/kg
dry
1
0.063
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
[86-30-6/122-39-4]^
Pentachlorophenol [87-86-5]^
0.038
U
mg/kg
dry
1
0.038
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Phenanthrene[85-01-8]^
0.031
U
mg/kg
dry
1
0.031
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Phenol[108-95-2]^
0.026
U
mg/kg
dry
1
0.026
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Pyrene [129-00-O]^
0.044
U
mg/kg
dry
1
0.044
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Pyridine [110-86-1]^
0.095
U
mg/kg
dry
1
0.095
0.38
OK25001
EPA
8270E
11/25/20
17:37
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
2,4,6-Tribromophenol
4.2
1
3.66
110 %
28-130
OK25001
EPA 8270E
11/25/2017:37
DFM
2-Fluorobiphenyl
1.6
1
1.93
85 %
56-120
OK25001
EPA 8270E
111251201737
DFM
2-Fluorophenol
3.3
1
3,66
86 %
49-126
OK25001
EPA 8270E
111251201737
DFM
Nitrobenzene-d5
1.6
1
1,93
84 %
50-117
OK25001
EPA 8270E
11/25/2017:37
DFM
Phenol-d5
3.5
1
3,66
91 %
56-120
OK25001
EPA 8270E
11/25/2017:37
DFM
Terphenyl-d14
1.8
1
1,93
95 %
36-151
OK25001
EPA 8270E
11/25/2017:37
DFM
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]A
420
mg/kg dry
1
0.139 0.580
OK30010
EPA 6010D
12/01/20 10:32
]DH
TCLP Metals by 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]A
2.74
mg/L
50
0.155 0.500
OL14039
EPA 6010D
12/15/20 13:23
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 79 of 107

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ANALYTICAL RESULTS
Description: HA-51-18" Lab Sample ID:CD1888O-44 Received: 11/17/20 17:10
Matrix: Soil Sampled:11/17/20 15:55 Work Order: CD1888O
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence % Solids: 80.67
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte KAS Numberl Results Flaa Units DF MDL POLL Batch Method Analyzed Ay Notes
Lead [7439-92-1]^ 21.1 mg/kg dry 1 0.149 0.620 OL04013 EPA 6010D 12/07/20 11:30 JDH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 80 of 107

00�
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ANALYTICAL RESULTS
Description: Equipment Blank Lab Sample ID:CD18880-45 Received: 11/17/20 17:10
Matrix: Water Sampled:11/17/20 16:10 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
u
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
u
ug/L
1
0.12
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
u
ug/L
1
0.28
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
u
ug/L
1
0.14
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,1-Dichloropropene [563-58-6]^
0.15
u
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,2,3-Trichlorobenzene [87-61-6]^
0.012
u
ug/L
1
0.012
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,2,4-Trichlorobenzene [120-82-1]^
0.14
u
ug/L
1
0.14
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.10
u
ug/L
1
0.10
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.30
u
ug/L
1
0.30
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,3-Dichlorobenzene [541-73-1]^
0.15
u
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,3-Dichloropropane [142-28-9]^
0.16
u
ug/L
1
0.16
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
2,2-Dichloropropane [594-20-7]^
0.28
u
ug/L
1
0.28
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
2-Butanone [78-93-3]A
1.3
u
ug/L
1
1.3
5.0
OK19030
EPA 8260D
11/19/20
18:22
REF
2-ChloroethylVinyl Ether [110-75-8]^
1.1
u
ug/L
1
1.1
5.0
OK19030
EPA 8260D
11/19/20
18:22
REF
2-Chlorotoluene [95-49-8]^
0.081
u
ug/L
1
0.081
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
2-Hexanone [591-78-6]A
0.88
u
ug/L
1
0.88
5.0
OK19030
EPA 8260D
11/19/20
18:22
REF
4-Chlorotoluene [106-43-4]^
0.068
u
ug/L
1
0.068
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
4-Isopropyltoluene [99-87-6]^
0.085
u
ug/L
1
0.085
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Acetone [67-64-1]A
10
u
ug/L
1
10
20
OK19030
EPA 8260D
11/19/20
18:22
REF
Benzene[71-43-2]A
0.15
u
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Bromobenzene[108-86-1]^
0.16
u
ug/L
1
0.16
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Bromochloromethane [74-97-5]A
0.48
u
ug/L
1
0.48
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF QL-02,
QV-01
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Carbon disulfide [75-15-O]^
1.5
u
ug/L
1
1.5
5.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Chlorobenzene [108-90-7]^
0.17
u
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1
0.23
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
U
ug/L
1
0.20
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Dibromochloromethane [124-48-1]^
0.17
U
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Dibromomethane [74-95-3]^
0.27
U
ug/L
1
0.27
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Dichlorodifluoromethane [75-71-8]^
0.20
U
ug/L
1
0.20
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 81 of 107

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ANALYTICAL RESULTS
Description: Equipment Blank Lab Sample ID:CD18880-45 Received: 11/17/20 17:10
Matrix: Water Sampled:11/17/20 16:10 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
AX Notes
Ethylbenzene [100-41-4]^
0.13
U
ug/L
1
0.13
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Hexachlorobutadiene [87-68-3]^
0.22
U
ug/L
1
0.22
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Isopropyl benzene [98-82-8]^
0.14
U
ug/L
1
0.14
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
m,p-Xylenes [108-38-3/106-42-3]^
0.17
U
ug/L
1
0.17
2.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Methylene chloride [75-09-2]^
0.23
U
ug/L
1
0.23
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Methyl-tert-Butyl Ether [1634-04-4]^
0.16
U
ug/L
1
0.16
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Naphthalene [91-20-3]^
0.11
U
ug/L
1
0.11
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
n-Butyl Benzene [104-51-8]^
0.058
U
ug/L
1
0.058
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
n-Propyl Benzene [103-65-1]^
0.12
U
ug/L
1
0.12
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
sec-Butylbenzene [135-98-8]^
0.10
U
ug/L
1
0.10
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Styrene [100-42-5]^
0.11
U
ug/L
1
0.11
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
tert-Butylbenzene [98-06-6]^
0.17
U
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Tetrachloroethene [127-18-4]^
0.17
U
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Toluene [108-88-3]^
0.14
U
ug/L
1
0.14
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
U
ug/L
1
0.21
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
U
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Vinyl chloride [75-01-4]^
0.32
u
ug/L
1
0.32
1.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Xylenes(Total)[1330-20-7]^
0.45
u
ug/L
1
0.45
3.0
OK19030
EPA 8260D
11/19/20
18:22
REF
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
4-Bromofluorobenzene
42
1
50.0
84 %
53-136
OK19030
EPA 6260D
11/19/2018:22
REF
Dibromofluoromethane
44
1
50.0
88 %
67-129
OK19030
EPA 8260D
1111912018:22
REF
Toluene-c48
48
1
50.0
95 %
59-134
OK19030
EPA 8260D
1111912018:22
REF
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL
PQL
Batch
Method
Analyzed
Ay Notes
1,2,4-Trichlorobenzene [120-82-1]^
2.5
u
ug/L
1
2.5
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
1,2-Dichlorobenzene [95-50-1]^
2.5
u
ug/L
1
2.5
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
1,3-Dichlorobenzene [541-73-1]^
2.5
u
ug/L
1
2.5
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
1,4-Dichlorobenzene [106-46-7]^
2.4
u
ug/L
1
2.4
10
OK18042
EPA 8270E
11/20/20 11:19
DFM QL-02
1- Methyl naphthalene [90-12-0]^
2.7
u
ug/L
1
2.7
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2,4,5-Trichlorophenol[95-95-4]^
2.5
u
ug/L
1
2.5
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2,4,6-Trichlorophenol[88-06-2]^
2.6
u
ug/L
1
2.6
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2,4-Dichlorophenol[120-83-2]^
2.6
u
ug/L
1
2.6
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2,4-Di methyl phenol[105-67-9]^
2.3
u
ug/L
1
2.3
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2,4-Dinitrophenol[51-28-5]^
2.6
u
ug/L
1
2.6
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2,4-Dinitrotoluene [121-14-2]^
2.6
u
ug/L
1
2.6
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2,6-Dinitrotoluene [606-20-2]^
2.5
u
ug/L
1
2.5
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2-Chloronaphthalene [91-58-7]^
2.8
u
ug/L
1
2.8
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2-Chlorophenol[95-57-8]^
2.2
u
ug/L
1
2.2
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2-Methyl-4,6-dinitrophenol[534-52-1]^
3.3
u
ug/L
1
3.3
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2- Methyl naphthalene [91-57-6]^
2.8
u
ug/L
1
2.8
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
2-Methylphenol[95-48-7]^
2.0
u
ug/L
1
2.0
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
FINAL
This report relates only
to the
sample as received by the laboratory,
and may only
be reproduced in full.
Page 82 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: Equipment Blank Lab Sample ID:CD18880-45 Received: 11/17/20 17:10
Matrix: Water Sampled:11/17/20 16:10 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence
Semivolatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed
By Notes
2-Nitroaniline [88-74-4]A
2.5
U
ug/L
1
2.5
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
2-Nitrophenol[88-75-5]A
1.1
U
ug/L
1
1.1
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
3 & 4-Methylphenol[108-39-4/106-44-5]A
2.1
U
ug/L
1
2.1
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
3,3'-Dichlorobenzidine [91-94-1]A
3.5
U
ug/L
1
3.5
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
3-Nitroaniline [99-09-2]A
2.6
U
ug/L
1
2.6
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
4-Bromophenyl-phenylether[101-55-3]A
2.4
U
ug/L
1
2.4
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
4-Chloro-3-methylphenol[59-50-7]A
2.4
U
ug/L
1
2.4
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
4-Chloroaniline [106-47-8]A
2.0
U
ug/L
1
2.0
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
4-Chlorophenyl-phenylether[7005-72-3]A
2.6
U
ug/L
1
2.6
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
4-Nitroaniline [100-01-6]A
3.2
U
ug/L
1
3.2
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
4-Nitrophenol[100-02-7]A
2.8
U
ug/L
1
2.8
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Acenaphthene [83-32-9]A
2.7
U
ug/L
1
2.7
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Acenaphthylene [208-96-8]A
2.6
U
ug/L
1
2.6
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Anthracene[120-12-7]A
2.4
U
ug/L
1
2.4
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Benzidine [92-87-5]A
1.6
U
ug/L
1
1.6
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Benzo(a)anthracene [56-55-3]A
2.4
U
ug/L
1
2.4
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Benzo(a)pyrene [50-32-8]A
2.2
U
ug/L
1
2.2
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Benzo(b)fluoranthene [205-99-2]A
2.8
U
ug/L
1
2.8
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Benzo(g,h,i)perylene[191-24-2]A
2.4
U
ug/L
1
2.4
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Benzo(k)fluoranthene[207-08-9]A
2.4
U
ug/L
1
2.4
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Benzoic acid [65-85-0]A
1.0
U
ug/L
1
1.0
50
OK18042
EPA
8270E
11/20/20
11:19
DFM
Benzyl alcohol [100-51-6]A
2.4
U
ug/L
1
2.4
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Bis(2-chloroethoxy)methane [111-91-1]A
2.4
U
ug/L
1
2.4
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Bis(2-chloroethyl)ether [111-44-4]A
2.6
U
ug/L
1
2.6
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Bis(2-chloroisopropyl)ether [108-60-1]A
2.5
U
ug/L
1
2.5
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Bis(2-ethylhexyl)phthalate [117-81-7]A
1.9
U
ug/L
1
1.9
5.0
OK18042
EPA
8270E
11/20/20
11:19
DFM
Butylbenzylphthalate [85-68-7]A
3.8
U
ug/L
1
3.8
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Chrysene [218-01-9]A
2.2
U
ug/L
1
2.2
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Dibenzo(a,h)anthracene [53-70-3]A
2.3
U
ug/L
1
2.3
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Dibenzofuran [132-64-9]A
2.6
U
ug/L
1
2.6
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Diethylphthalate [84-66-2]A
2.4
U
ug/L
1
2.4
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Dimethylphthalate [131-11-3]A
2.5
U
ug/L
1
2.5
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Di-n-butylphthalate [84-74-2]A
2.8
U
ug/L
1
2.8
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Di-n-octylphthalate [117-84-0]A
3.1
U
ug/L
1
3.1
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Fluoranthene[206-44-0]A
3.1
U
ug/L
1
3.1
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Fluorene [86-73-7]A
2.5
U
ug/L
1
2.5
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Hexachlorobenzene[118-74-1]A
2.3
U
ug/L
1
2.3
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Hexachlorobutadiene [87-68-3]A
2.8
U
ug/L
1
2.8
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Hexachlorocyclopentadiene [77-47-4]A
2.7
U
ug/L
1
2.7
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Hexachloroethane [67-72-1]A
2.6
U
ug/L
1
2.6
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Indeno(1,2,3-cd)pyrene [193-39-5]A
2.2
U
ug/L
1
2.2
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Isophorone[78-59-1]A
2.5
U
ug/L
1
2.5
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Naphthalene [91-20-3]A
2.8
U
ug/L
1
2.8
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
Nitrobenzene [98-95-3]A
2.5
U
ug/L
1
2.5
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
N-Nitrosodimethylamine [62-75-9]A
1.9
U
ug/L
1
1.9
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
N-Nitroso-di-n-propylamine [621-64-7]A
2.3
U
ug/L
1
2.3
10
OK18042
EPA
8270E
11/20/20
11:19
DFM
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 83 of 107

(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: Equipment Blank Lab Sample ID:CD18880-45 Received: 11/17/20 17:10
Matrix: Water Sampled:11/17/20 16:10 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: Bryan S. Wence
Semivolatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flaa
Units
DF
MDL
POLL
Batch
Method
Analyzed
Ay Notes
N-nitrosodiphenylamine/Diphenylamine
2.5
U
ug/L
1
2.5
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
[86-30-6/122-39-4]^
Pentachlorophenol[87-86-5]^
2.1
U
ug/L
1
2.1
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
Phenanthrene[85-01-8]^
2.6
U
ug/L
1
2.6
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
Phenol[108-95-2]^
1.7
U
ug/L
1
1.7
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
Pyrene [129-00-O]^
3.5
U
ug/L
1
3.5
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
Pyridine [110-86-1]^
2.2
U
ug/L
1
2.2
10
OK18042
EPA 8270E
11/20/20 11:19
DFM
Surrogates
Results
DF
Spike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
2,4,6-Tribromophenol
86
1
100
86 %
10-179
OK18042
EPA 8270E
11120120 11:19
DFM
2-Fluorobiphenyl
42
1
50.0
84 %
10-149
OK18042
EPA 8270E
11120120 11:19
DFM
2-Fluorophenol
54
1
100
54 %
10-110
OK18042
EPA 8270E
11120120 11:19
DFM
Nitrobenzene-d5
38
1
50.0
76 %
10-149
OK18042
EPA 8270E
11120120 11:19
DFM
Phenol-d5
41
1
100
41 %
10-88
OK18042
EPA 8270E
11120120 11:19
DFM
Terphenyl-d14
31
1
50.0
62 %
10-186
OK18042
EPA 8270E
11120120 11:19
DFM
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 5911
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL P L
Batch
Method
Analyzed
By Notes
Lead [7439-92-1]^
3.10
U
ug/L
1
3.10 10.0
OK18012
EPA 6010D
11/20/20 14:28
]DH
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 84 of 107

00�
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ANALYTICAL RESULTS
Description: Trip Blank Lab Sample ID:CD18880-46 Received: 11/17/20 17:10
Matrix: Water Sampled:11/17/20 16:10 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
1,1,1,2-Tetrachloroethane [630-20-6]A
0.17
U
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,1,1-Trichloroethane [71-55-6]A
0.12
U
ug/L
1
0.12
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,1,2,2-Tetrachloroethane [79-34-5]A
0.28
U
ug/L
1
0.28
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,1,2-Trichloroethane [79-00-5]A
0.14
U
ug/L
1
0.14
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,1-Dichloroethane [75-34-3]^
0.13
U
ug/L
1
0.13
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,1-Dichloroethene [75-35-4]^
0.21
U
ug/L
1
0.21
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,1-Dichloropropene [563-58-6]^
0.15
U
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,2,3-Trichlorobenzene [87-61-6]^
0.012
U
ug/L
1
0.012
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
U
ug/L
1
0.23
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,2,4-Trichlorobenzene [120-82-1]^
0.14
U
ug/L
1
0.14
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,2,4-Trimethylbenzene [95-63-6]A
0.10
U
ug/L
1
0.10
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
U
ug/L
1
0.48
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,2-Dibromoethane [106-93-4]^
0.66
U
ug/L
1
0.66
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
U
ug/L
1
0.19
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,2-Dichloroethane [107-06-2]^
0.21
U
ug/L
1
0.21
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,2-Dichloropropane [78-87-5]^
0.10
U
ug/L
1
0.10
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,3,5-Trimethylbenzene [108-67-8]A
0.30
U
ug/L
1
0.30
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,3-Dichlorobenzene [541-73-1]^
0.15
U
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,3-Dichloropropane [142-28-9]^
0.16
U
ug/L
1
0.16
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
U
ug/L
1
0.19
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
2,2-Dichloropropane [594-20-7]^
0.28
U
ug/L
1
0.28
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
2-Butanone [78-93-3]A
1.3
U
ug/L
1
1.3
5.0
OK19030
EPA 8260D
11/19/20
17:54
REF
2-ChloroethylVinyl Ether [110-75-8]^
1.1
U
ug/L
1
1.1
5.0
OK19030
EPA 8260D
11/19/20
17:54
REF
2-Chlorotoluene [95-49-8]^
0.081
U
ug/L
1
0.081
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
2-Hexanone [591-78-6]A
0.88
U
ug/L
1
0.88
5.0
OK19030
EPA 8260D
11/19/20
17:54
REF
4-Chlorotoluene [106-43-4]^
0.068
U
ug/L
1
0.068
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
4-Isopropyltoluene [99-87-6]^
0.085
U
ug/L
1
0.085
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
U
ug/L
1
1.1
5.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Acetone [67-64-1]A
10
U
ug/L
1
10
20
OK19030
EPA 8260D
11/19/20
17:54
REF
Benzene[71-43-2]A
0.15
U
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Bromobenzene[108-86-1]^
0.16
U
ug/L
1
0.16
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Bromochloromethane [74-97-5]A
0.48
U
ug/L
1
0.48
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Bromodichloromethane [75-27-4]^
0.17
U
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Bromoform [75-25-2]^
0.22
U
ug/L
1
0.22
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF QL-02,
QV-01
Bromomethane [74-83-9]^
0.14
U
ug/L
1
0.14
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Carbon disulfide [75-15-O]^
1.5
U
ug/L
1
1.5
5.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Carbon tetrachloride [56-23-5]^
0.17
U
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Chlorobenzene [108-90-7]^
0.17
U
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Chloroethane [75-00-3]^
0.23
U
ug/L
1
0.23
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Chloroform [67-66-3]^
0.18
U
ug/L
1
0.18
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Chloromethane [74-87-3]^
0.13
U
ug/L
1
0.13
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
U
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
U
ug/L
1
0.20
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Dibromochloromethane [124-48-1]^
0.17
U
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Dibromomethane [74-95-3]^
0.27
U
ug/L
1
0.27
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Dichlorodifluoromethane [75-71-8]^
0.20
U
ug/L
1
0.20
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 85 of 107

00�
www.encolabs.com
ANALYTICAL RESULTS
Description: Trip Blank Lab Sample ID:CD18880-46 Received: 11/17/20 17:10
Matrix: Water Sampled:11/17/20 16:10 Work Order: CD18880
Project: Sir Walter Gun Club Sampled By: ENCO
Volatile Organic Compounds
by GCMS
^ - ENCO Cary rertified analyte [NC 591]
Analyte ICAS Numberl
Results
Flaa
Units
DF
MDL
P L
Batch
Method
Analyzed
By Notes
Ethylbenzene [100-41-4]A
0.13
U
ug/L
1
0.13
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Hexachlorobutadiene [87-68-3]A
0.22
U
ug/L
1
0.22
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Isopropylbenzene [98-82-8]A
0.14
U
ug/L
1
0.14
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
m,p-Xylenes[108-38-3/106-42-3]A
0.17
U
ug/L
1
0.17
2.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Methylene chloride [75-09-2]A
0.23
U
ug/L
1
0.23
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Methyl-tert-Butyl Ether [1634-04-4]A
0.16
U
ug/L
1
0.16
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Naphthalene [91-20-3]A
0.11
U
ug/L
1
0.11
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
n-Butyl Benzene [104-51-8]A
0.058
U
ug/L
1
0.058
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
n-Propyl Benzene [103-65-1]A
0.12
U
ug/L
1
0.12
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
o-Xylene [95-47-6]A
0.065
U
ug/L
1
0.065
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
sec-Butylbenzene [135-98-8]A
0.10
U
ug/L
1
0.10
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Styrene [100-42-5]A
0.11
U
ug/L
1
0.11
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
tert-Butyl benzene [98-06-6]A
0.17
U
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Tetrachloroethene [127-18-4]A
0.17
U
ug/L
1
0.17
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Toluene [108-88-3]A
0.14
U
ug/L
1
0.14
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
trans-1,2-Dichloroethene [156-60-5]A
0.21
U
ug/L
1
0.21
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
trans-1,3-Dichloropropene [10061-02-6]A
0.15
U
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Trichloroethene [79-01-6]A
0.15
U
ug/L
1
0.15
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Trichlorofluoromethane [75-69-4]A
0.24
U
ug/L
1
0.24
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Vinyl chloride [75-01-4]A
0.32
U
ug/L
1
0.32
1.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Xylenes (Total) [1330-20-7]A
0.45
U
ug/L
1
0.45
3.0
OK19030
EPA 8260D
11/19/20
17:54
REF
Surrogates
Results
DF
Spike L v/
% Rec
% Rec Limits
Batch
Method
Analyzed
" Notes
4-Bromofluorobenzene
43
1
50.0
86 %
53-136
OK19030
EPA 8260D
1111912017.-54
REF
Dibromofluoromethane
45
1
50.0
89 %
67-129
OK19030
EPA 8260D
1111912017.-54
REF
Toluene-&
48
1
50.0
96 %
59-134
OK19030
EPA 8260D
11119120 17.-54
REF
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 86 of 107

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch OKIBO29 - EPA 5030E MS
Blank (OK18029-BLKS) Prepared: 11/18/2020 12:08 Analyzed: 11/18/2020 16:01
Spike
Analvte
Result
Flaq
POL
Units Level
1, 1, 1,2-Tetrachloroethane
0.00016
U
0.0010
mg/kg wet
1,1,1-Trichloroethane
0.00025
U
0.0010
mg/kg wet
1,1,2,2-Tetrachloroethane
0.00020
U
0.0010
mg/kg wet
1,1,2-Trichloroethane
0.00025
U
0.0010
mg/kg wet
1,1-Dichloroethane
0.00025
U
0.0010
mg/kg wet
1,1-Dichloroethene
0.00030
U
0.0010
mg/kg wet
1,1-Dichloropropene
0.00016
U
0.0010
mg/kg wet
1,2,3-Trichlorobenzene
0.00028
U
0.0010
mg/kg wet
1,2,3-Trichloropropane
0.00064
U
0.0010
mg/kg wet
1,2,4-Trichlorobenzene
0.00027
U
0.0010
mg/kg wet
1,2,4-Trimethylbenzene
0.00017
U
0.0010
mg/kg wet
1,2-Dibromo-3-chloropropane
0.00079
U
0.0010
mg/kg wet
1,2-Dibromoethane
0.00046
U
0.0010
mg/kg wet
1,2-Dichlorobenzene
0.00027
U
0.0010
mg/kg wet
1,2-Dichloroethane
0.00041
U
0.0010
mg/kg wet
1,2-Dichloropropane
0.00026
U
0.0010
mg/kg wet
1,3,5-Trimethylbenzene
0.00020
U
0.0010
mg/kg wet
1,3-Dichlorobenzene
0.00022
U
0.0010
mg/kg wet
1,3-Dichloropropane
0.00029
U
0.0010
mg/kg wet
1,4-Dichlorobenzene
0.00020
U
0.0010
mg/kg wet
2,2-Dichloropropane
0.00023
U
0.0010
mg/kg wet
2-Butanone
0.00078
U
0.0050
mg/kg wet
2-Chloroethyl Vinyl Ether
0.00016
U
0.0050
mg/kg wet
2-Chlorotoluene
0.00018
U
0.0010
mg/kg wet
2-Hexanone
0.00075
U
0.0050
mg/kg wet
4-Chlorotoluene
0.00026
U
0.0010
mg/kg wet
4-Isopropyltoluene
0.00016
U
0.0010
mg/kg wet
4-Methyl-2-pentanone
0.00057
U
0.0050
mg/kg wet
Acetone
0.014
U
0.020
mg/kg wet
Benzene
0.00017
U
0.0010
mg/kg wet
Bromobenzene
0.00022
U
0.0010
mg/kg wet
Bromochloromethane
0.00041
U
0.0010
mg/kg wet
Bromodichloromethane
0.00024
U
0.0010
mg/kg wet
Bromoform
0.00045
U
0.0010
mg/kg wet
Bromomethane
0.00032
U
0.0010
mg/kg wet
Carbon disulfide
0.00039
U
0.0050
mg/kg wet
Carbon Tetrachloride
0.00022
U
0.0010
mg/kg wet
Chlorobenzene
0.00017
U
0.0010
mg/kg wet
Chloroethane
0.00025
U
0.0010
mg/kg wet
Chloroform
0.00018
U
0.0010
mg/kg wet
Chloromethane
0.00021
U
0.0010
mg/kg wet
cis- 1,2-Dichloroethene
0.00023
U
0.0010
mg/kg wet
cis- 1,3-Dichloropropene
0.00017
U
0.0010
mg/kg wet
Dibromochloromethane
0.00035
U
0.0010
mg/kg wet
Dibromomethane
0.00033
U
0.0010
mg/kg wet
Dichlorodifluoromethane
0.00045
U
0.0010
mg/kg wet
Ethylbenzene
0.00020
U
0.0010
mg/kg wet
Hexachlorobutadiene
0.00035
U
0.0010
mg/kg wet
Isopropyl benzene
0.00015
U
0.0010
mg/kg wet
Source %REC RPD
Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 87 of 107

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch OK18O29 - EPA 5030E MS - Continued
Blank (OK18029-BLK1) Continued Prepared: 11/18/2020 12:08 Analyzed: 11/18/2020 16:01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
m,p-Xylenes
0.00037
U
0.0020
mg/kg wet
Methylene Chloride
0.00073
U
0.0020
mg/kg wet
Methyl-tert-Butyl Ether
0.00030
U
0.0010
mg/kg wet
Naphthalene
0.00027
U
0.0010
mg/kg wet
n-Butyl Benzene
0.00013
U
0.0010
mg/kg wet
n-Propyl Benzene
0.00018
U
0.0010
mg/kg wet
o-Xylene
0.00022
U
0.0010
mg/kg wet
sec-Butylbenzene
0.00095
U
0.0010
mg/kg wet
Styrene
0.00098
U
0.0010
mg/kg wet
tert-Butylbenzene
0.00017
U
0.0010
mg/kg wet
Tetrachloroethene
0.00028
U
0.0010
mg/kg wet
Toluene
0.00024
U
0.0010
mg/kg wet
trans-1,2-Dichloroethene
0.00037
U
0.0010
mg/kg wet
trans-1,3-Dichloropropene
0.00039
U
0.0010
mg/kg wet
Trichloroethene
0.00032
U
0.0010
mg/kg wet
Trichlorofluoromethane
0.00026
U
0.0010
mg/kg wet
Vinyl chloride
0.00024
U
0.0010
mg/kg wet
Xylenes (Total)
0.00056
U
0.0030
mg/kg wet
4-Bromofluorobenzene
35
u9/L
50.0
69
50-127
Dibromofluoromethane
37
u9/L
50.0
75
52-128
Toluene-d8
37
u9/L
50.0
74
57-124
LCS (OK18029-BSI)
Prepared: 11/18/2020 12:08 Analyzed: 11/18/2020 14:30
Spike
Source
%REC
RPD
Analvte
Result
Flaa
POL
Uni
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
0.020
0.0010
mg/kg wet
0.0200
102
64-133
Benzene
0.025
0.0010
mg/kg wet
0.0200
123
79-129
Chlorobenzene
0.020
0.0010
mg/kg wet
0.0200
98
79-121
Toluene
0.024
0.0010
mg/kg wet
0.0200
119
77-120
Trichloroethene
0.021
0.0010
mg/kg wet
0.0200
107
78-120
4-8romofluorobenzene
32
u9/L
50.0
63
50-127
Dibromofluoromethane
35
u9/L
50.0
70
52-128
Toluene-d8
35
u9/L
50.0
70
57-124
Matrix Spike (OK18029-MS1)
Prepared: 11/18/2020 12:08 Analyzed: 11/18/2020 14:00
Source: CD19195-03
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
0.022
0.0010
mg/kg wet
0.0200
0.00030 U
112
64-133
Benzene
0.026
0.0010
mg/kg wet
0.0200
0.00017 U
129
79-129
Chlorobenzene
0.021
0.0010
mg/kg wet
0.0200
0.00017 U
105
79-121
Toluene
0.025
0.0010
mg/kg wet
0.0200
0.00024 U
124
77-120
QM-07
Trichloroethene
0.022
0.0010
mg/kg wet
0.0200
0.00032 U
109
78-120
4-8romofluorobenzene
33
u9/L
50.0
67
50-127
Dibromofluoromethane
37
u9/L
50.0
75
52-128
Toluene-d8
37
u9/L
50.0
74
57-124
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 88 of 107

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch OK18O29 - EPA 5O3OB MS - Continued
Matrix Spike Dup (OK18029-MSD1) Prepared: 11/18/2020 12:08 Analyzed: 11/18/2020 15:01
Source: CD19195-03
Spike
Source
%REC
RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
0.022
0.0010
mg/kg wet
0.0200
0.00030 U
111
64-133
2
23
Benzene
0.026
0.0010
mg/kg wet
0.0200
0.00017 U
128
79-129
1
23
Chlorobenzene
0.021
0.0010
mg/kg wet
0.0200
0.00017 U
107
79-121
2
25
Toluene
0.026
0.0010
mg/kg wet
0.0200
0.00024 U
128
77-120
3
23 QM-07
Trichloroethene
0.021
0.0010
mg/kg wet
0.0200
0.00032 U
106
78-120
3
24
4-Bromofluorobenzene 35 u91L 50.0 69 50-127
Dibromofluoromethane 36 u91L 50.0 72 52-128
Toluene-d8 36 u91L 50.0 73 57-124
Batch OK18O35 - EPA 5030E MS
Blank (OK18035-BLK1) Prepared: 11/18/2020 14:35 Analyzed: 11/19/2020 04:32
Spike
Analvte
Result
Flaq
Q
Units Level
1,1,1,2-Tetrachloroethane
0.00016
U
0.0010
mg/kg wet
1,1,1-Trichloroethane
0.00025
U
0.0010
mg/kg wet
1,1,2,2-Tetrachloroethane
0.00020
U
0.0010
mg/kg wet
1,1,2-Trichloroethane
0.00025
U
0.0010
mg/kg wet
1,1-Dichloroethane
0.00025
U
0.0010
mg/kg wet
1,1-Dichloroethene
0.00030
U
0.0010
mg/kg wet
1,1-Dichloropropene
0.00016
U
0.0010
mg/kg wet
1,2,3-Trichlorobenzene
0.00028
U
0.0010
mg/kg wet
1,2,3-Trichloropropane
0.00064
U
0.0010
mg/kg wet
1,2,4-Trichlorobenzene
0.00027
U
0.0010
mg/kg wet
1,2,4-Trimethylbenzene
0.00017
U
0.0010
mg/kg wet
1,2-Dibromo-3-chloropropane
0.00079
U
0.0010
mg/kg wet
1,2-Dibromoethane
0.00046
U
0.0010
mg/kg wet
1,2-Dichlorobenzene
0.00027
U
0.0010
mg/kg wet
1,2-Dichloroethane
0.00041
U
0.0010
mg/kg wet
1,2-Dichloropropane
0.00026
U
0.0010
mg/kg wet
1,3,5-Trimethylbenzene
0.00020
U
0.0010
mg/kg wet
1,3-Dichlorobenzene
0.00022
U
0.0010
mg/kg wet
1,3-Dichloropropane
0.00029
U
0.0010
mg/kg wet
1,4-Dichlorobenzene
0.00020
U
0.0010
mg/kg wet
2,2-Dichloropropane
0.00023
U
0.0010
mg/kg wet
2-Butanone
0.00078
U
0.0050
mg/kg wet
2-Chloroethyl Vinyl Ether
0.00016
U
0.0050
mg/kg wet
2-Chlorotoluene
0.00018
U
0.0010
mg/kg wet
2-Hexanone
0.00075
U
0.0050
mg/kg wet
4-Chlorotoluene
0.00026
U
0.0010
mg/kg wet
4-Isopropyltoluene
0.00016
U
0.0010
mg/kg wet
4-Methyl-2-pentanone
0.00057
U
0.0050
mg/kg wet
Acetone
0.014
U
0.020
mg/kg wet
Benzene
0.00017
U
0.0010
mg/kg wet
Bromobenzene
0.00022
U
0.0010
mg/kg wet
Bromochloromethane
0.00041
U
0.0010
mg/kg wet
Bromodichloromethane
0.00024
U
0.0010
mg/kg wet
Bromoform
0.00045
U
0.0010
mg/kg wet
Bromomethane
0.00032
U
0.0010
mg/kg wet
Source %REC RPD
Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 89 of 107

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch OKI B035 - EPA 5O3OB MS - Continued
Blank (OK18035-BLKS) Continued Prepared: 11/18/2020 14:35 Analyzed: 11/19/2020 04:32
Spike
Analvte
Result
Flaq
POL
Units Level
Carbon disulfide
0.00039
U
0.0050
mg/kg wet
Carbon Tetrachloride
0.00022
U
0.0010
mg/kg wet
Chlorobenzene
0.00017
U
0.0010
mg/kg wet
Chloroethane
0.00025
U
0.0010
mg/kg wet
Chloroform
0.00018
U
0.0010
mg/kg wet
Chloromethane
0.00021
U
0.0010
mg/kg wet
cis- 1,2-Dichloroethene
0.00023
U
0.0010
mg/kg wet
cis- 1,3-Dichloropropene
0.00017
U
0.0010
mg/kg wet
Dibromochloromethane
0.00035
U
0.0010
mg/kg wet
Dibromomethane
0.00033
U
0.0010
mg/kg wet
Dichlorodifluoromethane
0.00045
U
0.0010
mg/kg wet
Ethylbenzene
0.00020
U
0.0010
mg/kg wet
Hexachlorobutadiene
0.00035
U
0.0010
mg/kg wet
Isopropyl benzene
0.00015
U
0.0010
mg/kg wet
m,p-Xylenes
0.00037
U
0.0020
mg/kg wet
Methylene Chloride
0.00073
U
0.0020
mg/kg wet
Methyl-tert-Butyl Ether
0.00030
U
0.0010
mg/kg wet
Naphthalene
0.00027
U
0.0010
mg/kg wet
n-Butyl Benzene
0.00013
U
0.0010
mg/kg wet
n-Propyl Benzene
0.00018
U
0.0010
mg/kg wet
o-Xylene
0.00022
U
0.0010
mg/kg wet
sec-Butylbenzene
0.00095
U
0.0010
mg/kg wet
Styrene
0.00098
U
0.0010
mg/kg wet
tert-Butyl benzene
0.00017
U
0.0010
mg/kg wet
Tetrachloroethene
0.00028
U
0.0010
mg/kg wet
Toluene
0.00024
U
0.0010
mg/kg wet
trans-1,2-Dichloroethene
0.00037
U
0.0010
mg/kg wet
trans-1,3-Dichloropropene
0.00039
U
0.0010
mg/kg wet
Trichloroethene
0.00032
U
0.0010
mg/kg wet
Trichlorofluoromethane
0.00026
U
0.0010
mg/kg wet
Vinyl chloride
0.00024
U
0.0010
mg/kg wet
Xylenes (Total)
0.00056
U
0.0030
mg/kg wet
Source %REC RPD
Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene
30
u91L
50.0
61
50-127
Dibromofluoromethane
36
u91L
50.0
71
52-128
Toluene-d8
37
u91L
50.0
74
57-124
LCS (OK18035-BS1)
Prepared: 11/18/2020 14:35 Analyzed: 11/19/2020 02:32
Spike
Source
%REC RPD
Analvte
Result
Flaq Q
Units
Level
Result %REC
Limits RPD Limit Notes
1,1-Dichloroethene
0.020
0.0010
mg/kg wet
0.0200
102
64-133
Benzene
0.025
0.0010
mg/kg wet
0.0200
127
79-129
Chlorobenzene
0.019
0.0010
mg/kg wet
0.0200
96
79-121
Toluene
0.024
0.0010
mg/kg wet
0.0200
120
77-120
Trichloroethene
0.019
0.0010
mg/kg wet
0.0200
97
78-120
4-Bromofluorobenzene
32
u91L
50.0
63
50-127
Dibromofluoromethane
35
u91L
50.0
70
52-128
Toluene-d8
34
u91L
50.0
69
57-124
FINAL
This report relates only to the sample as received by the laboratory, and
may only be reproduced in
full. Page 90 of 107

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch OKI B035 - EPA 5O3OB MS - Continued
Matrix Spike (OK38035-MS1) Prepared: 11/18/2020 14:35 Analyzed: 11/19/2020 03:02
Source: CD19267-04
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
1,1-Dichloroethene
0.021
0.0010
mg/kg wet
0.0200
0.00030 U
104
64-133
Benzene
0.026
0.0010
mg/kg wet
0.0200
0.00017 U
129
79-129
Chlorobenzene
0.019
0.0010
mg/kg wet
0.0200
0.00017 U
95
79-121
Toluene
0.024
0.0010
mg/kg wet
0.0200
0.00024 U
121
77-120
QM-07
Trichloroethene
0.021
0.0010
mg/kg wet
0.0200
0.00032 U
103
78-120
4-Bromofluorobenzene
33
u91L
50.0
66
50-127
Dibromofluoromethane
35
u91L
50.0
69
52-128
Toluene-d8
35
u91L
50.0
70
57-124
Matrix Spike Dup (OK18035-MSD1)
Prepared: 11/18/2020 14:35 Analyzed: 11/19/2020 03:32
Source: CD19267-04
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
1,1-Dichloroethene
0.021
0.0010
mg/kg wet
0.0200
0.00030 U
106
64-133
2
23
Benzene
0.026
0.0010
mg/kg wet
0.0200
0.00017 U
130
79-129
0.8
23
QM-07
Chlorobenzene
0.019
0.0010
mg/kg wet
0.0200
0.00017 U
93
79-121
3
25
Toluene
0.023
0.0010
mg/kg wet
0.0200
0.00024 U
115
77-120
4
23
Trichloroethene
0.021
0.0010
mg/kg wet
0.0200
0.00032 U
104
78-120
1
24
4-Bromofluorobenzene
31
u91L
50.0
63
50-127
Dibromofluoromethane
35
u91L
50.0
71
52-128
Toluene-d8
35
u91L
50.0
70
57-124
Batch OK19O3O - EPA 5O3OB MS
Blank (OK19030-BLK1)
Prepared: 11/19/2020 10:41 Analyzed: 11/19/2020 17:27
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit
Notes
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,1-Dichloropropene
0.15
U
1.0
ug/L
1,2,3-Trichlorobenzene
0.012
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2,4-Trichlorobenzene
0.14
U
1.0
ug/L
1,2,4-Trimethylbenzene
0.10
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,3,5-Trimethylbenzene
0.30
U
1.0
ug/L
1,3-Dichlorobenzene
0.15
U
1.0
ug/L
1,3-Dichloropropane
0.16
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2,2-Dichloropropane
0.28
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
FINAL This
report relates only to the sample as received by the laboratory, and may only be reproduced
in
full.
Page 91 of 107

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch OK19O3O - EPA 5O3OB MS - Continued
Blank (OK19030-BLKS) Continued Prepared: 11/19/2020 10:41 Analyzed: 11/19/2020 17:27
Analvte
Result
Flaq
POL
Units
2-Chloroethyl Vinyl Ether
1.1
U
5.0
ug/L
2-Chlorotoluene
0.081
U
1.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Chlorotoluene
0.068
U
1.0
ug/L
4-Isopropyltoluene
0.085
U
1.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Benzene
0.15
U
1.0
ug/L
Bromobenzene
0.16
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Dichlorodifluoromethane
0.20
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Hexachlorobutadiene
0.22
U
1.0
ug/L
Isopropyl benzene
0.14
U
1.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
Methyl-tert-Butyl Ether
0.16
U
1.0
ug/L
Naphthalene
0.11
U
1.0
ug/L
n-Butyl Benzene
0.058
U
1.0
ug/L
n-Propyl Benzene
0.12
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
sec-Butylbenzene
0.10
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
tert-Butyl benzene
0.17
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene 43 u91L 50.0 87 53-136
Dibromofluoromethane 45 u91L 50.0 89 67-129
Toluene-d8 49 u91L 50.0 98 59-134
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 92 of 107

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QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch OK19O3O - EPA 5O3OB MS - Continued
LCS (OK19030-BS1) Prepared: 11/19/2020 10:41 Analyzed: 11/19/2020 15:36
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
89
75-133
Benzene
20
1.0
ug/L
20.0
100
80-134
Chlorobenzene
19
1.0
ug/L
20.0
97
80-120
Toluene
18
1.0
ug/L
20.0
90
71-120
Trichloroethene
24
1.0
ug/L
20.0
119
74-120
4-Bromofluorobenzene
43
u91L
50.0
86
53-136
Dibromofluoromethane
43
u91L
50.0
87
67-129
Toluene-d8
48
u91L
50.0
96
59-134
Matrix Spike (OK19030-MS1)
Prepared: 11/19/2020 10:41 Analyzed: 11/19/2020 16:04
Source: CD19195-07
Spike
Source
%REC
RPD
Analvte
Result Flaq
Q
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
19
1.0
ug/L
20.0
0.21 U
96
75-133
Benzene
21
1.0
ug/L
20.0
0.15 U
104
80-134
Chlorobenzene
20
1.0
ug/L
20.0
0.17 U
100
80-120
Toluene
19
1.0
ug/L
20.0
0.14 U
94
71-120
Trichloroethene
25
1.0
ug/L
20.0
0.15 U
124
74-120
QM-07
4-Bromofluorobenzene
42
u91L
50.0
85
53-136
Dibromofluoromethane
44
u91L
50.0
88
67-129
Toluene-d8
48
u91L
50.0
97
59-134
Matrix Spike Dup (OK19030-MSD1)
Prepared: 11/19/2020 10:41 Analyzed: 11/19/2020 16:32
Source: CD19195-07
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene
18
1.0
ug/L
20.0
0.21 U
90
75-133
6
20
Benzene
20
1.0
ug/L
20.0
0.15 U
99
80-134
6
17
Chlorobenzene
19
1.0
ug/L
20.0
0.17 U
96
80-120
4
16
Toluene
18
1.0
ug/L
20.0
0.14 U
89
71-120
5
17
Trichloroethene
23
1.0
ug/L
20.0
0.15 U
116
74-120
7
22
4-Bromofluorobenzene 42 u91L 50.0 84 53-136
Dibromofluoromethane 43 u91L 50.0 87 67-129
Toluene-d8 48 u91L 50.0 97 59-134
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OK18O42 -EPA 351OC MS
Blank (OK18042-BLKS) Prepared: 11/18/2020 19:54 Analyzed: 11/19/2020 16:10
Analvte
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1- Methyl naphthalene
2,4, 5-Trich t o rop hen o f
2,4, 6-Trich t o rop hen o f
2,4-Dichlorophenol
FINAL
Result
Flaq
POL
Units
2.5
U
10
ug/L
2.5
U
10
ug/L
2.5
U
10
ug/L
2.4
U
10
ug/L
2.7
U
10
ug/L
2.5
U
10
ug/L
2.6
U
10
ug/L
2.6
U
10
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Notes
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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OK18042 - EPA 3510C MS - Continued
Blank (OK18042-BLK1) Continued Prepared: 11/18/2020 19:54 Analyzed: 11/19/2020 16:10
Analvte
Result
Flaq
POL
Units
2,4-Dimethylphenol
2.3
U
10
ug/L
2,4-Dinitrophenol
2.6
U
10
ug/L
2,4-Dinitrotoluene
2.6
U
10
ug/L
2,6-Dinitrotoluene
2.5
U
10
ug/L
2-Chloronaphthalene
2.8
U
10
ug/L
2-Chlorophenol
2.2
U
10
ug/L
2-Methyl-4,6-dinitrophenol
3.3
U
10
ug/L
2-Methylnaphthalene
2.8
U
10
ug/L
2-Methylphenol
2.0
U
10
ug/L
2-Nitroaniline
2.5
U
10
ug/L
2-Nitrophenol
1.1
U
10
ug/L
3 & 4-Methylphenol
2.1
U
10
ug/L
3,3'-Dichlorobenzidine
3.5
U
10
ug/L
3-Nitroaniline
2.6
U
10
ug/L
4-Bromophenyl-phenylether
2.4
U
10
ug/L
4-Chloro-3-methylphenol
2.4
U
10
ug/L
4-Chloroaniline
2.0
U
10
ug/L
4-Chlorophenyl-phenylether
2.6
U
10
ug/L
4-Nitroaniline
3.2
U
10
ug/L
4-Nitrophenol
2.8
U
10
ug/L
Acenaphthene
2.7
U
10
ug/L
Acenaphthylene
2.6
U
10
ug/L
Anthracene
2.4
U
10
ug/L
Benzidine
1.6
U
10
ug/L
Benzo(a)anthracene
2.4
U
10
ug/L
Benzo(a)pyrene
2.2
U
10
ug/L
Benzo(b)fluoranthene
2.8
U
10
ug/L
Benzo(g,h,i)perylene
2.4
U
10
ug/L
Benzo(k)fluoranthene
2.4
U
10
ug/L
Benzoic acid
1.0
U
50
ug/L
Benzyl alcohol
2.4
U
10
ug/L
Bis(2-chloroethoxy)methane
2.4
U
10
ug/L
Bis(2-chloroethyl)ether
2.6
U
10
ug/L
Bis(2-chloroisopropyl)ether
2.5
U
10
ug/L
Bis(2-ethylhexyl)phthalate
1.9
U
5.0
ug/L
Butylbenzylphthalate
3.8
U
10
ug/L
Chrysene
2.2
U
10
ug/L
Dibenzo(a,h)anthracene
2.3
U
10
ug/L
Dibenzofuran
2.6
U
10
ug/L
Diethylphthalate
2.4
U
10
ug/L
Dimethylphthalate
2.5
U
10
ug/L
Di-n-butylphthalate
2.8
U
10
ug/L
Di-n-octylphthalate
3.1
U
10
ug/L
Fluoranthene
3.1
U
10
ug/L
Fluorene
2.5
U
10
ug/L
Hexachlorobenzene
2.3
U
10
ug/L
Hexachlorobutadiene
2.8
U
10
ug/L
Hexachlorocyclopentadiene
2.7
U
10
ug/L
Hexachloroethane
2.6
U
10
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 94 of 107

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QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OKI B042 - EPA 351OC MS - Continued
Blank (OK18042-BLKS) Continued Prepared: 11/18/2020 19:54 Analyzed: 11/19/2020 16:10
Analvte
Result
Flaq
POL
Units
Indeno(1,2,3-cd)pyrene
2.2
U
10
ug/L
Isophorone
2.5
U
10
ug/L
Naphthalene
2.8
U
10
ug/L
Nitrobenzene
2.5
U
10
ug/L
N-Nitrosodimethylamine
1.9
U
10
ug/L
N-Nitroso-di-n-propylamine
2.3
U
10
ug/L
N-nitrosodiphenylamine/Diphenylamine
2.5
U
10
ug/L
Pentachlorophenol
2.1
U
10
ug/L
Phenanthrene
2.6
U
10
ug/L
Phenol
1.7
U
10
ug/L
Pyrene
3.5
U
10
ug/L
Pyridine
2.2
U
10
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
2,4,6-Tribromophenol
99
u91L
100 99 10-179
2-Fluorobiphenyl
46
u91L
50.0 92 10-149
2-Fluorophenol
59
u91L
100 59 10-110
Nitrobenzene-d5
42
u91L
50.0 83 10-149
Phenohd5
46
u91L
100 46 10-88
Terphenyl-d14
40
u91L
50.0 80 10-188
LCS (OK38042-BSI)
Prepared: 11/18/2020 19:54 Analyzed: 11/19/2020 16:39
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,2,4-Trichlorobenzene
44
10
ug/L
50.0
87
27-90
1,4-Dichlorobenzene
42
10
ug/L
50.0
85
23-84 3-02
2,4-Dinitrotoluene
50
10
ug/L
50.0
99
67-132
2-Chlorophenol
36
10
ug/L
50.0
73
40-109
4-Chloro-3-methylphenol
41
10
ug/L
50.0
82
58-121
4-Nitrophenol
24
10
ug/L
50.0
49
33-105
Acenaphthene
48
10
ug/L
50.0
95
39-125
N-Nitroso-di-n-propylamine
47
10
ug/L
50.0
93
48-126
Pentachlorophenol
50
10
ug/L
50.0
100
51-135
Phenol
20
10
ug/L
50.0
40
19-78
Pyrene
52
10
ug/L
50.0
104
44-137
2,4,6-Tribromophenol
120
u91L
100 124 10-179
2-Fluorobiphenyl
51
u91L
50.0 102 10-149
2-Fluorophenol
62
u91L
100 62 10-110
Nitrobenzene-d5
52
u91L
50.0 103 10-149
Phenol-d5
50
u91L
100 50 10-88
Terphenyl-d14
47
u91L
50.0 95 10-188
Matrix Spike (OK18042-MS1)
Prepared: 11/18/2020 19:54 Analyzed: 11/19/2020 17:07
Source: CD19195-08
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,2,4-Trichlorobenzene
45
10
ug/L
50.0
2.5 U
90
27-90
1,4-Dichlorobenzene
43
10
ug/L
50.0
2.4 U
86
23-84 J-02
2,4-Dinitrotoluene
52
10
ug/L
50.0
2.6 U
105
67-132
2-Chlorophenol
39
10
ug/L
50.0
2.2 U
78
40-109
4-Chloro-3-methylphenol
47
10
ug/L
50.0
2.4 U
94
58-121
FINAL
This report relates only to
the sample as received by the
laboratory, and
may only be
reproduced in
full. Page 95 of 107

0Nk"q09
www.encolabs.com
QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OK18O42 - EPA 351OC MS - Continued
Matrix Spike (OK18042-MSI) Continued Prepared: 11/18/2020 19:54 Analyzed: 11/19/2020 17:07
Source: CD19195-08
Spike
Source
%REC RPD
Analvte
Result Flaa
POL
Units
Level
Result
%REC
Limi RPD Limit Notes
4-Nitrophenol
29
10
ug/L
50.0
2.8 U
58
33-105
Acenaphthene
49
10
ug/L
50.0
2.7 U
97
39-125
N-Nitroso-di-n-propylamine
48
10
ug/L
50.0
2.3 U
96
48-126
Pentachlorophenol
54
10
ug/L
50.0
2.1 U
108
51-135
Phenol
23
10
ug/L
50.0
1.7 U
46
19-78
Pyrene
50
10
ug/L
50.0
3.5 U
100
44-137
2,4,6-Tribromophenol
130
u91L
100
129
10-179
2-Fluorobiphenyl
51
u91L
50.0
102
10-149
2-Fluorophenol
62
u91L
100
62
10-110
Nitrobenzene-d5
52
u91L
50.0
103
10-149
Phenol-d5
52
u91L
100
52
10-88
Terphenyl-d14
45
u91L
50.0
90
10-188
Matrix Spike Dup (OK18042-MSD1)
Prepared: 11/18/2020 19:54 Analyzed: 11/19/2020 17:36
Source: CD19195-08
Spike
Source
%REC
RPD
Analvte
Result Flaa
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,2,4-Trichlorobenzene
45
10
ug/L
50.0
2.5 U
91
27-90
0.2
43
1,4-Dichlorobenzene
43
10
ug/L
50.0
2.4 U
86
23-84
0.7
39 J-02
2,4-Dinitrotoluene
47
10
ug/L
50.0
2.6 U
94
67-132
11
17
2-Chlorophenol
37
10
ug/L
50.0
2.2 U
74
40-109
4
22
4-Chloro-3-methylphenol
43
10
ug/L
50.0
2.4 U
86
58-121
10
22
4-Nitrophenol
21
10
ug/L
50.0
2.8 U
42
33-105
32
27 QM-11
Acenaphthene
49
10
ug/L
50.0
2.7 U
99
39-125
2
25
N-Nitroso-di-n-propylamine
43
10
ug/L
50.0
2.3 U
86
48-126
11
23
Pentachlorophenol
51
10
ug/L
50.0
2.1 U
101
51-135
7
11
Phenol
19
10
ug/L
50.0
1.7 U
38
19-78
18
18
Pyrene
44
10
ug/L
50.0
3.5 U
89
44-137
11
24
2,4,6-Tribromophenol
110
u91L
100
114
10-179
2-Fluorobiphenyl
51
u9/L
50.0
102
10-149
2-Fluorophenol
60
u91L
100
60
10-110
Nitrobenzene-d5
52
u91L
50.0
103
10-149
Phenol-d5
44
u91L
100
44
10-88
Terphenyl-d14
39
u91L
50.0
79
10-188
Batch OK19OO1 - SOP EXSV-33
Blank (OK19001-BLK1)
Prepared: 11/19/2020 03:48 Analyzed: 11/23/2020 12:33
Spike Source %REC RPD
Analvte
Result
Flaci
POL
Units Level Result %REC Limits RPD Limit Notes
1,2,4-Trichlorobenzene
0.026
U
0.33
mg/kg wet
1,2-Dichlorobenzene
0.023
U
0.33
mg/kg wet
1,3-Dichlorobenzene
0.020
U
0.33
mg/kg wet
1,4-Dichlorobenzene
0.021
U
0.33
mg/kg wet
1-Methylnaphthalene
0.027
U
0.33
mg/kg wet
2,4,5-Trichlorophenol
0.027
U
0.33
mg/kg wet
2,4,6-Trichlorophenol
0.027
U
0.33
mg/kg wet
2,4-Dichlorophenol
0.024
U
0.33
mg/kg wet
2,4-Dimethylphenol
0.043
U
0.33
mg/kg wet
FINAL
This report relates only to
the sample
as received by the laboratory, and may only be reproduced in full. Page 96 of 107

0Nk"q09
www.encolabs.com
QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OK19OO1 - SOP EXSV-33 - Continued
Blank (OK19001-BLK1) Continued Prepared: 11/19/2020 03:48 Analyzed: 11/23/2020 12:33
Spike
Analvte
Result
Flaq
POL
Units Level
2,4-Dinitrophenol
0.043
U
0.33
mg/kg wet
2,4-Dinitrotoluene
0.028
U
0.33
mg/kg wet
2,6-Dinitrotoluene
0.031
U
0.33
mg/kg wet
2-Chloronaphthalene
0.028
U
0.33
mg/kg wet
2-Chlorophenol
0.025
U
0.33
mg/kg wet
2-Methyl-4,6-dinitrophenol
0.033
U
0.33
mg/kg wet
2-Methylnaphthalene
0.028
U
0.33
mg/kg wet
2-Methylphenol
0.025
U
0.33
mg/kg wet
2-Nitroaniline
0.030
U
0.33
mg/kg wet
2-Nitrophenol
0.031
U
0.33
mg/kg wet
3 & 4-Methylphenol
0.026
U
0.33
mg/kg wet
3,3'-Dichlorobenzidine
0.098
U
0.33
mg/kg wet
3-Nitroaniline
0.036
U
0.33
mg/kg wet
4-Bromophenyl-phenylether
0.027
U
0.33
mg/kg wet
4-Chloro-3-methylphenol
0.033
U
0.33
mg/kg wet
4-Chloroaniline
0.093
U
0.33
mg/kg wet
4-Chlorophenyl-phenylether
0.026
U
0.33
mg/kg wet
4-Nitroaniline
0.053
U
0.33
mg/kg wet
4-Nitrophenol
0.031
U
0.33
mg/kg wet
Acenaphthene
0.028
U
0.33
mg/kg wet
Acenaphthylene
0.028
U
0.33
mg/kg wet
Anthracene
0.038
U
0.33
mg/kg wet
Benzidine
0.11
U
0.33
mg/kg wet
Benzo(a)anthracene
0.028
U
0.33
mg/kg wet
Benzo(a)pyrene
0.033
U
0.33
mg/kg wet
Benzo(b)fluoranthene
0.018
U
0.33
mg/kg wet
Benzo(g,h,i)perylene
0.047
U
0.33
mg/kg wet
Benzo(k)fluoranthene
0.033
U
0.33
mg/kg wet
Benzoic acid
0.15
U
1.7
mg/kg wet
Benzyl alcohol
0.023
U
0.33
mg/kg wet
Bis(2-chloroethoxy)methane
0.025
U
0.33
mg/kg wet
Bis(2-chloroethyl)ether
0.043
U
0.33
mg/kg wet
Bis(2-chloroisopropyl)ether
0.024
U
0.33
mg/kg wet
Bis(2-ethylhexyl)phthalate
0.035
U
0.33
mg/kg wet
Butylbenzylphthalate
0.040
U
0.33
mg/kg wet
Chrysene
0.030
U
0.33
mg/kg wet
Dibenzo(a,h)anthracene
0.051
U
0.33
mg/kg wet
Dibenzofuran
0.027
U
0.33
mg/kg wet
Diethylphthalate
0.028
U
0.33
mg/kg wet
Dimethylphthalate
0.033
U
0.33
mg/kg wet
Di-n-butylphthalate
0.041
U
0.33
mg/kg wet
Di-n-octylphthalate
0.033
U
0.33
mg/kg wet
Fluoranthene
0.036
U
0.33
mg/kg wet
Fluorene
0.029
U
0.33
mg/kg wet
Hexachlorobenzene
0.026
U
0.33
mg/kg wet
Hexachlorobutadiene
0.026
U
0.33
mg/kg wet
Hexachlorocyclopentadiene
0.039
U
0.33
mg/kg wet
Hexachloroethane
0.021
U
0.33
mg/kg wet
Indeno(1,2,3-cd)pyrene
0.047
U
0.33
mg/kg wet
Source %REC RPD
Result %REC Limits RPD Limit
Notes
QV-01
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 97 of 107

0Nk"q09
www.encolabs.com
QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OK19OO1 - SOP EXSV-33 - Continued
Blank (OK19001-BLK1) Continued Prepared: 11/19/2020 03:48 Analyzed: 11/23/2020 12:33
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
Isophorone
0.030
U
0.33
mg/kg wet
Naphthalene
0.028
U
0.33
mg/kg wet
Nitrobenzene
0.026
U
0.33
mg/kg wet
N-Nitrosodimethylamine
0.021
U
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
0.081
U
0.33
mg/kg wet
N-nitrosodiphenylamine/Diphenylamine
0.054
U
0.33
mg/kg wet
Pentachlorophenol
0.033
U
0.33
mg/kg wet
Phenanthrene
0.027
U
0.33
mg/kg wet
Phenol
0.022
U
0.33
mg/kg wet
Pyrene
0.038
U
0.33
mg/kg wet
Pyridine
0.082
U
0.33
mg/kg wet
2,4,6-Tribromophenol
3.6
mg/kg wet
3,33
107
28-130
2-Fluo-biphenyl
1.6
mg/kg wet
1.67
96
56-120
2-Fluorophenol
4.0
mg/kg wet
3.33
120
49-126
Nitrobenzene-d5
1.4
mg/kg wet
1.67
81
50-117
Phenohd5
3.6
mg/kg wet
3.33
107
56-120
Terphenyl-d14
2.0
mg/kg wet
1.67
119
36-151
LCS (OK39001-BS1)
Prepared: 11/19/2020 03:48 Analyzed: 11/23/2020 13:06
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
1,2,4-Trichlorobenzene
1.6
0.33
mg/kg wet
1.67
96
51-121
1,4-Dichlorobenzene
1.6
0.33
mg/kg wet
1.67
94
48-118
2,4-Dinitrotoluene
1.8
0.33
mg/kg wet
1.67
106
63-127
2-Chlorophenol
1.6
0.33
mg/kg wet
1.67
93
56-120
4-Chloro-3-methylphenol
1.7
0.33
mg/kg wet
1.67
105
59-121
4-Nitrophenol
1.9
0.33
mg/kg wet
1.67
115
73-147
Acenaphthene
1.7
0.33
mg/kg wet
1.67
100
64-131
N-Nitroso-di-n-propylamine
1.8
0.33
mg/kg wet
1.67
107
55-135
Pentachlorophenol
1.8
0.33
mg/kg wet
1.67
108
45-117
Phenol
1.5
0.33
mg/kg wet
1.67
92
54-121
Pyrene
1.7
0.33
mg/kg wet
1.67
100
65-146
2,4,6-Tribromophenol
4.3
mg/kg wet
3.33
129
28-130
2-Fluorobiphenyl
1.8
mg/kg wet
1.67
106
56-120
2-Fiuorophenol
3.5
mg/kg wet
333
106
49-126
Nitrobenzene-d5
1.7
mg/kg wet
1.67
101
50-117
Phenol-d5
3.8
mg/kg wet
3.33
114
56-120
Terphenyl-d14
1.8
mg/kg wet
1.67
109
36-151
Matrix Spike (OK39001-MS1)
Prepared: 11/19/2020 03:48 Analyzed: 11/23/2020 14:09
Source: CD18880-11
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
1,2,4-Trichlorobenzene
1.8
0.37
mg/kg dry
1.86
0.029 U
95
51-121
1,4-Dichlorobenzene
1.7
0.37
mg/kg dry
1.86
0.023 U
93
48-118
2,4-Dinitrotoluene
2.0
0.37
mg/kg dry
1.86
0.031 U
105
63-127
2-Chlorophenol
1.7
0.37
mg/kg dry
1.86
0.028 U
94
56-120
4-Chloro-3-methylphenol
2.0
0.37
mg/kg dry
1.86
0.037 U
107
59-121
4-Nitrophenol
2.3
0.37
mg/kg dry
1.86
0.035 U
122
73-147
FINAL
This report relates only to
the sample
as received by the laboratory, and
may only be
reproduced in
full. Page 98 of 107

0 F. Nk"q 09)
www.encolabs.com
QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OK19OO1 - SOP EXSV-33 - Continued
Matrix Spike (OK19001-MSI) Continued
Prepared: 11/19/2020 03:48 Analyzed: 11/23/2020 14:09
Source: CD18880-11
Spike
Source
%REC RPD
Analvte Result Flaa
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Acenaphthene 1.9
0.37
mg/kg dry
1.86
0.031 U
99
64-131
N-Nitroso-di-n-propylamine 2.0
0.37
mg/kg dry
1.86
0.091 U
106
55-135
Pentachlorophenol 2.1
0.37
mg/kg dry
1.86
0.037 U
114
45-117
Phenol 1.7
0.37
mg/kg dry
1.86
0.025 U
91
54-121
Pyrene 1.7
0.37
mg/kg dry
1.86
0.10
85
65-146
2,4,6-Tribromophenol
4.7
mg/kg dry
3.73
126
28-130
2-Fluorobiphenyl
1.9
mg/kg dry
1.86
104
56-120
2-Fluorophenol
3.8
mg/kg dry
3.73
102
49-126
Nitrobenzene-d5
1.8
mg/kg dry
1.86
97
50-117
Phenohd5
4.1
mg/kg dry
373
111
56-120
Terphenyhd14
1.7
mg/kg dry
1.86
89
36-151
Matrix Spike Dup (OK19001-MSD1)
Prepared: 11/19/2020 03:48 Analyzed: 11/23/2020 14:40
Source: CD18880-11
Spike
Source
%REC
RPD
Analvte
Result Flaa
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,2,4-Trichlorobenzene
1.7
0.37
mg/kg dry
1.86
0.029 U
92
51-121
4
10
1,4-Dichlorobenzene
1.7
0.37
mg/kg dry
1.86
0.023 U
92
48-118
0.4
13
2,4-Dinitrotoluene
1.9
0.37
mg/kg dry
1.86
0.031 U
103
63-127
2
10
2-Chlorophenol
1.7
0.37
mg/kg dry
1.86
0.028 U
90
56-120
4
11
4-Chloro-3-methylphenol
1.9
0.37
mg/kg dry
1.86
0.037 U
102
59-121
5
10
4-Nitrophenol
2.0
0.37
mg/kg dry
1.86
0.035 U
108
73-147
12
10 QM-11
Acenaphthene
1.8
0.37
mg/kg dry
1.86
0.031 U
99
64-131
0.6
19
N-Nitroso-di-n-propylamine
2.0
0.37
mg/kg dry
1.86
0.091 U
108
55-135
1
10
Pentachlorophenol
2.1
0.37
mg/kg dry
1.86
0.037 U
112
45-117
2
10
Phenol
1.6
0.37
mg/kg dry
1.86
0.025 U
86
54-121
6
13
Pyrene
1.8
0.37
mg/kg dry
1.86
0.10
88
65-146
4
50
2,4,6-Tribromophenol
4.7
mg/kg dry
3.73
125
28-130
2-Fluorobiphenyl
1.9
mg/kg dry
1,86
102
56-120
2-Fiuorophenol
3.7
mg/kg dry
373
98
49-126
Nitrobenzene-d5
1.8
mg/kg dry
1.86
94
50-117
Phenohd5
4.0
mg/kg dry
3.73
106
56-120
Terphenyl-d14
1.7
mg/kg dry
1.86
92
36-151
Batch OK25OO1 - SOP EXSV-33
Blank (OK25001-BLKI) Prepared: 11/25/2020 01:25 Analyzed: 11/25/2020 12:22
Spike Source %REC RPD
Analvte
Result
Flag
POL
Units Level Result %REC Limits RPD Limit Notes
1,2,4-Trichlorobenzene
0.026
U
0.33
mg/kg wet
1,2-Dichlorobenzene
0.023
U
0.33
mg/kg wet
1,3-Dichlorobenzene
0.020
U
0.33
mg/kg wet
1,4-Dichlorobenzene
0.021
U
0.33
mg/kg wet
1-Methylnaphthalene
0.027
U
0.33
mg/kg wet
2,4,5-Trichlorophenol
0.027
U
0.33
mg/kg wet
2,4,6-Trichlorophenol
0.027
U
0.33
mg/kg wet
2,4-Dichlorophenol
0.024
U
0.33
mg/kg wet
2,4-Dimethylphenol
0.043
U
0.33
mg/kg wet
2,4-Dinitrophenol
0.043
U
0.33
mg/kg wet
FINAL
This report relates only to
the sample
as received by the laboratory, and may only be reproduced in full. Page 99 of 107

(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OK25OO1 - SOP EXSV-33 - Continued
Blank (OK25001-BLKS) Continued Prepared: 11/25/2020 01:25 Analyzed: 11/25/2020 12:22
Spike
Analvte
Result
Flaq
POL
Units Level
2,4-Dinitrotoluene
0.028
U
0.33
mg/kg wet
2,6-Dinitrotoluene
0.031
U
0.33
mg/kg wet
2-Chloronaphthalene
0.028
U
0.33
mg/kg wet
2-Chlorophenol
0.025
U
0.33
mg/kg wet
2-Methyl-4,6-dinitrophenol
0.033
U
0.33
mg/kg wet
2- Methyl naphthalene
0.028
U
0.33
mg/kg wet
2-Methylphenol
0.025
U
0.33
mg/kg wet
2-Nitroaniline
0.030
U
0.33
mg/kg wet
2-Nitrophenol
0.031
U
0.33
mg/kg wet
3 & 4-Methylphenol
0.026
U
0.33
mg/kg wet
3,3'-Dichlorobenzidine
0.098
U
0.33
mg/kg wet
3-Nitroaniline
0.036
U
0.33
mg/kg wet
4-Bromophenyl-phenylether
0.027
U
0.33
mg/kg wet
4-Chloro-3-methylphenol
0.033
U
0.33
mg/kg wet
4-Chloroaniline
0.093
U
0.33
mg/kg wet
4-Chlorophenyl-phenylether
0.026
U
0.33
mg/kg wet
4-Nitroaniline
0.053
U
0.33
mg/kg wet
4-Nitrophenol
0.031
U
0.33
mg/kg wet
Acenaphthene
0.028
U
0.33
mg/kg wet
Acenaphthylene
0.028
U
0.33
mg/kg wet
Anthracene
0.038
U
0.33
mg/kg wet
Benzidine
0.11
U
0.33
mg/kg wet
Benzo(a)anthracene
0.028
U
0.33
mg/kg wet
Benzo(a)pyrene
0.033
U
0.33
mg/kg wet
Benzo(b)fluoranthene
0.018
U
0.33
mg/kg wet
Benzo(g,h,i)perylene
0.047
U
0.33
mg/kg wet
Benzo(k)fluoranthene
0.033
U
0.33
mg/kg wet
Benzoic acid
0.15
U
1.7
mg/kg wet
Benzyl alcohol
0.023
U
0.33
mg/kg wet
Bis(2-chloroethoxy)methane
0.025
U
0.33
mg/kg wet
Bis(2-chloroethyl)ether
0.043
U
0.33
mg/kg wet
Bis(2-chloroisopropyl)ether
0.024
U
0.33
mg/kg wet
Bis(2-ethylhexyl)phthalate
0.035
U
0.33
mg/kg wet
Butyl benzylphtha late
0.040
U
0.33
mg/kg wet
Chrysene
0.030
U
0.33
mg/kg wet
Dibenzo(a,h)anthracene
0.051
U
0.33
mg/kg wet
Dibenzofuran
0.027
U
0.33
mg/kg wet
Diethylphtha late
0.028
U
0.33
mg/kg wet
Dimethylphthalate
0.033
U
0.33
mg/kg wet
Di-n-butylphthalate
0.041
U
0.33
mg/kg wet
Di-n-octylphthalate
0.033
U
0.33
mg/kg wet
Fluoranthene
0.036
U
0.33
mg/kg wet
Fluorene
0.029
U
0.33
mg/kg wet
Hexachlorobenzene
0.026
U
0.33
mg/kg wet
Hexachlorobutadiene
0.026
U
0.33
mg/kg wet
Hexachlorocyclopentadiene
0.039
U
0.33
mg/kg wet
Hexachloroethane
0.021
U
0.33
mg/kg wet
Indeno(1,2,3-cd)pyrene
0.047
U
0.33
mg/kg wet
Isophorone
0.030
U
0.33
mg/kg wet
Source %REC RPD
Result %REC Limits RPD Limit
Notes
QV-01
QV-01
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 100 of 107

0Nk"q09
www.encolabs.com
QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OK25OO1 - SOP EXSV-33 - Continued
Blank (OK25001-BLK1) Continued Prepared: 11/25/2020 01:25 Analyzed: 11/25/2020 12:22
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units Level Result %REC Limits RPD Limit Notes
Naphthalene
0.028
U
0.33
mg/kg wet
Nitrobenzene
0.026
U
0.33
mg/kg wet
N-Nitrosodimethylamine
0.021
U
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
0.081
U
0.33
mg/kg wet
N-nitrosodiphenylamine/Diphenylamine
0.054
U
0.33
mg/kg wet
Pentachlorophenol
0.033
U
0.33
mg/kg wet
Phenanthrene
0.027
U
0.33
mg/kg wet
Phenol
0.022
U
0.33
mg/kg wet
Pyrene
0.038
U
0.33
mg/kg wet
Pyridine
0.082
U
0.33
mg/kg wet
2,4,6-Tribromophenol
3.4
mg/kg wet
3.33
103
28-130
2-Fluorobiphenyl
1.6
mg/kg wet
1.67
99
56-120
2-Fluo-phenol
3.1
mg/kg wet
3.33
94
49-126
Nitrobenzene-d5
1.6
mg/kg wet
1.67
94
50-117
Phenol-d5
3.4
mg/kg wet
3.33
101
56-120
Terphenyl-d14
1.9
mg/kg wet
1.67
114
36-151
LCS (OK25001-BS1)
Prepared: 11/25/2020 01:25 Analyzed: 11/25/2020 12:54
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limi RPD iiina Notes
1,2,4-Trichlorobenzene
1.6
0.33
mg/kg wet
1.67
98
51-121
1,4-Dichlorobenzene
1.5
0.33
mg/kg wet
1.67
91
48-118
2,4-Dinitrotoluene
1.8
0.33
mg/kg wet
1.67
106
63-127
2-Chlorophenol
1.5
0.33
mg/kg wet
1.67
89
56-120
4-Chloro-3-methylphenol
1.7
0.33
mg/kg wet
1.67
100
59-121
4-Nitrophenol
2.0
0.33
mg/kg wet
1.67
121
73-147
Acenaphthene
1.6
0.33
mg/kg wet
1.67
97
64-131
N-Nitroso-di-n-propylamine
1.5
0.33
mg/kg wet
1.67
92
55-135
Pentachlorophenol
1.7
0.33
mg/kg wet
1.67
102
45-117
Phenol
1.3
0.33
mg/kg wet
1.67
81
54-121
Pyrene
1.6
0.33
mg/kg wet
1.67
95
65-146
2,4,6-Tribromophenol
4.2
mg/kg wet
3.33
125
28-130
2-Fluorobiphenyl
1.8
mg/kg wet
1.67
106
56-120
2-Fluorophenol
3.2
mg/kg wet
3.33
96
49-126
Nitrobenzene-d5
1.6
mg/kg wet
1.67
97
50-117
Phenohd5
3.4
mg/kg wet
3.33
101
56-120
Terphenyhd14
1.7
mg/kg wet
1.67
105
36-151
Matrix Spike (OK25001-MS1)
Prepared: 11/25/2020 01:25 Analyzed: 11/25/2020 13:57
Source: CD18880-16
Spike
Source
%REC RPD
Analvte
Result Flaa
iQ
Units
Level
Result
%REC
Limits RPD Limit Notes
1,2,4-Trichlorobenzene
1.6
0.35
mg/kg dry
1.78
0.028 U
91
51-121
1,4-Dichlorobenzene
1.5
0.35
mg/kg dry
1.78
0.022 U
86
48-118
2,4-Dinitrotoluene
1.8
0.35
mg/kg dry
1.78
0.030 U
99
63-127
2-Chlorophenol
1.5
0.35
mg/kg dry
1.78
0.027 U
86
56-120
4-Chloro-3-methylphenol
1.6
0.35
mg/kg dry
1.78
0.035 U
91
59-121
4-Nitrophenol
2.0
0.35
mg/kg dry
1.78
0.033 U
113
73-147
Acenaphthene
1.7
0.35
mg/kg dry
1.78
0.030 U
93
64-131
FINAL
This report relates only to the sample
as received by the laboratory, and
may only be
reproduced in
full. Page 101 of 107

0 F. Nk"q 09)
www.encolabs.com
QUALITY CONTROL DATA
Semivolatile Organic Compounds by GCMS - Quality Control
Batch OK25OO1 - SOP EXSV-33 - Continued
Matrix Spike (OK25001-MSI) Continued
Prepared: 11/25/2020 01:25 Analyzed: 11/25/2020 13:57
Source: CD18880-16
Spike
Source
%REC RPD
Analvte Result Flaq
POL
Units
Level
Result
%REC
Limits RPD Limit Notes
N-Nitroso-di-n-propylamine 1.6
0.35
mg/kg dry
1.78
0.086 U
90
55-135
Pentachlorophenol 1.8
0.35
mg/kg dry
1.78
0.035 U
101
45-117
Phenol 1.4
0.35
mg/kg dry
1.78
0.023 U
78
54-121
Pyrene 1.6
0.35
mg/kg dry
1.78
0.041 U
92
65-146
2,4,6-Tribromophenol
39
mg/kg dry
3.56
111
28-130
2-Fluorobiphenyl
1.7
mg/kg dry
1.78
97
56-120
2-Fluo-phenol
3.1
mg/kg dry
3.56
87
49-126
Nitrobenzene-d5
1.6
mg/kg dry
1.78
88
50-117
Phenohd5
3.3
mg/kg dry
3.56
92
56-120
Terphenyl-d14
1.7
mg/kg dry
1.78
97
36-151
Matrix Spike Dup (OK25001-MSD1)
Prepared: 11/25/2020 01:25 Analyzed: 11/25/2020 14:28
Source: CD18880-16
Spike
Source
%REC
RPD
Analvte
Result Flag
POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,2,4-Trichlorobenzene
1.7
0.35
mg/kg dry
1.78
0.028 U
96
51-121
5
10
1,4-Dichlorobenzene
1.6
0.35
mg/kg dry
1.78
0.022 U
92
48-118
6
13
2,4-Dinitrotoluene
1.9
0.35
mg/kg dry
1.78
0.030 U
105
63-127
6
10
2-Chlorophenol
1.6
0.35
mg/kg dry
1.78
0.027 U
89
56-120
4
11
4-Chloro-3-methylphenol
1.8
0.35
mg/kg dry
1.78
0.035 U
100
59-121
10
10
4-Nitrophenol
2.2
0.35
mg/kg dry
1.78
0.033 U
126
73-147
10
10
Acenaphthene
1.8
0.35
mg/kg dry
1.78
0.030 U
99
64-131
6
19
N-Nitroso-di-n-propylamine
1.6
0.35
mg/kg dry
1.78
0.086 U
91
55-135
1
10
Pentachlorophenol
1.9
0.35
mg/kg dry
1.78
0.035 U
107
45-117
6
10
Phenol
1.4
0.35
mg/kg dry
1.78
0.023 U
81
54-121
3
13
Pyrene
1.7
0.35
mg/kg dry
1.78
0.041 U
97
65-146
5
50
2,4,6-Tribromophenol
4.3
mg/kg dry
3.56
121
28-130
2-Fluorobiphenyl
1.8
mg/kg dry
1.78
99
56-120
2-Fluorophenol
3.2
mg/kg dry
3.56
91
49-126
Nitrobenzene-d5
1.6
mg/kg dry
1.78
91
50-117
Phenohd5
3.4
mg/kg dry
3.56
95
56-120
Terphenyhd14
1.8
mg/kg dry
1.78
103
36-151
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OK20031 - EPA 3O5OB
Blank (OK20031-BLK1)
Prepared: 11/20/2020 10:53 Analyzed: 11/23/2020 12:29
Spike Source %REC
RPD
Analvte
Result Flaq
POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
0.120 U
0.500
mg/kg wet
LCS (OK20031-BSI)
Prepared: 11/20/2020 10:53 Analyzed: 11/23/2020 14:33
Spike Source %REC
RPD
Analvte
Result Flaa
POL
Units
Level Result %REC Limits RPD
Limit Notes
Lead
9.12
0.500
mg/kg wet
9.80 93 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 102 of 107

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OK20031 - EPA 3O5OB - Continued
Matrix Spike (OK20031-MS1)
Prepared: 11/20/2020 10:53 Analyzed: 11/23/2020 14:49
Source: CD18880-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
1040
0.556
mg/kg dry
11.2 675 NR 75-125
QM-07
Matrix Spike Dup (OK20031-MSD3)
Prepared: 11/20/2020 10:53 Analyzed: 11/23/2020 14:51
Source: CD18880-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
883
0.556
mg/kg dry
11.5 675 NR 75-125 17
20
QM-07
Post Spike (OK20031-PSI)
Prepared: 11/20/2020 10:53 Analyzed: 11/23/2020 14:53
Source: CD18880-01
Spike Source %REC
RPD
Analvte
Result
Flaq POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
12.8
0.0100
mg/L
0.200 13.0 NR 80-120
QM-08
Batch OK3OO1O - EPA 3O5OB
Blank (OK30010-BLKI) Prepared: 11/30/2020 08:59 Analyzed: 12/01/2020 09:34
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
LCS (OK30010-BS1) Prepared: 11/30/2020 08:59 Analyzed: 12/01/2020 09:38
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
10.2
0.500
mg/kg wet
10.0 102 80-120
Matrix Spike (OK30010-MSI)
Prepared: 11/30/2020 08:59 Analyzed: 12/01/2020 09:43
Source: CD18880-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
18.5
0.587
mg/kg dry
12.0 6.34 101 75-125
Matrix Spike Dup (OK30010-MSD1)
Prepared: 11/30/2020 08:59 Analyzed: 12/01/2020 09:45
Source: CD18880-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
17.8
0.587
mg/kg dry
11.7 6.34 98 75-125 4
20
Post Spike (OK30030-PS1)
Prepared: 11/30/2020 08:59 Analyzed: 12/01/2020 09:48
Source: CD18880-02
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.300
0.0100
mg/L
0.200 0.105 98 80-120
Batch OLO4O13 - EPA 3050E
Blank (OL04013-BLKI) Prepared: 12/04/2020 11:44 Analyzed: 12/07/2020 09:53
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.120 U 0.500 mg/kg wet
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 103 of 107

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QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch OLO4O13 - EPA 3050E - Continued
LCS (OL04013-BS3) Prepared: 12/04/2020 11:44 Analyzed: 12/07/2020 10:44
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
9.38
0.500
mg/kg wet
10.4
90
80-120
Matrix Spike (OL04013-MS1)
Prepared: 12/04/2020 11:44 Analyzed: 12/07/2020 10:49
Source: CD18880-28
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
64.2
0.553
mg/kg dry
11.8
23.8
344
75-125
QM-07
Matrix Spike Dup (OL04013-MSD1)
Prepared: 12/04/2020 11:44 Analyzed: 12/07/2020 10:51
Source: CD18880-28
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
65.0
0.553
mg/kg dry
11.6
23.8
354
75-125 1
20
QM-07
Post Spike (OL04013-PSI)
Prepared: 12/04/2020 11:44 Analyzed: 12/07/2020 10:54
Source: CD18880-28
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
0.570
0.0100
mg/L
0.200
0.405
82
80-120
Metals (total recoverable) by EPA 6000/7000
Series Methods - Quality Control
Batch OKISO12 - EPA 3OO5A
Blank (OK18012-BLK1) Prepared: 11/18/2020 09:37 Analyzed: 11/20/2020 11:15
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 3.10 U 10.0 ug/L
LCS (OK18012-BS1) Prepared: 11/18/2020 09:37 Analyzed: 11/20/2020 13:30
Spike
Source
%REC
RPD
Analvte
Result
Flaa
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
209
10.0
ug/L
200
105
80-120
Matrix Spike (OK18012-MS1)
Prepared: 11/18/2020 09:37 Analyzed: 11/20/2020 13:37
Source: CD18064-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
168
10.0
ug/L
200
3.10 U
84
75-125
Matrix Spike Dup (OK18012-MSD1)
Prepared: 11/18/2020 09:37 Analyzed: 11/20/2020 13:40
Source: CD18064-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
166
10.0
ug/L
200
3.10 U
83
75-125 1
20
Post Spike (OK18012-PS1)
Prepared: 11/18/2020 09:37 Analyzed: 11/20/2020 13:42
Source: CD18064-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Lead
0.183
0.0100
mg/L
0.200
0.000308
91
80-120
TCLP Metals by 6000/7000 Series Methods - Quality Control
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 104 of 107

(� �Eo
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QUALITY CONTROL DATA
TCLP Metals by 6000/7000 Series Methods - Quality Control
Batch OL14039 - EPA 3010A
Blank (OL34039-BLK3) Prepared: 12/14/2020 15:26 Analyzed: 12/15/2020 12:12
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
Lead 0.155 U 0.500 mg/L
LCS (OL14039-BSI) Prepared: 12/14/2020 15:26 Analyzed: 12/15/2020 13:00
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.198
0.0100
mg/L
0.200 99 80-120
Matrix Spike (OL14039-MS1)
Prepared: 12/14/2020 15:26 Analyzed: 12/15/2020 13:04
Source: CD18880-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
22.7
0.500
mg/L
10.0 10.7 120 75-125
Matrix Spike Dup (OL14039-MSD1)
Prepared: 12/14/2020 15:26 Analyzed: 12/15/2020 13:07
Source: CD18880-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
23.1
0.500
mg/L
10.0 10.7 124 75-125 2
20
Post Spike (OL14039-PSI)
Prepared: 12/14/2020 15:26 Analyzed: 12/15/2020 13:09
Source: CD18880-01
Spike Source %REC
RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD
Limit
Notes
Lead
0.413
0.0100
mg/L
0.200 0.215 99 80-120
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 105 of 107

(� �Eo
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
3-02 Result may be biased high. Associated laboratory control sample (LCS) exceeded the upper control limit.
3-04 Result may be biased high. Associated calibration verification standard exceeded the upper control limit.
QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test).
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QS-03 Surrogate recovery outside acceptance limits
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
R-05 The sample was diluted due to the presence of high levels of non -target analytes resulting in elevated
reporting limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 106 of 107

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