Stork Rotary_Soil Sampling Activities Report_10.21.2022

Tower Engineering Professionals, Inc. ∙ 326 Tryon Road ∙ Charlotte, NC 27603 ∙ T 919.661.6351 ∙ tepgroup.net
October 21, 2022
Ms. Carolyn Minnich
Brownfields Project Manager
North Carolina Department of Environmental Quality
Division of Waste Management
217 West Jones Street
Raleigh, North Carolina 27699
Re: Soil Sampling Activities Report
Stork Rotary RFRU (RN)
3201 Rotary Drive
Charlotte, Mecklenburg County, NC
Brownfields Project No. 19059-15-060
Dear Ms. Minnich:
Please find the enclosed Soil Sampling Activities Report for the Stork Rotary RFRU (RN) property
(Brownfields Project Number 19059-15-060) located at 3201 Rotary Drive, in Charlotte, Mecklenburg
County, North Carolina.
Please do not hesitate to call if you have any questions or require additional information.
Sincerely,
Tower Engineering Professionals, Inc.
Clint E. Sorrell, P.G. Graham M. Andres, P.E.
Environmental Due Diligence Manager Executive Vice President
SOIL SAMPLING ACTIVITES REPORT
STORK ROTARY RFRU (RN)
3201 ROTARY DRIVE
CHARLOTTE, NORTH CAROLINA 28269
BROWNFIELDS PROJECT NO. 19059-15-060
Prepared For:
No Bull Properties, LLC
326 Tryon Road
Raleigh, NC 27603
Prepared By:
Tower Engineering Professionals, Inc.
326 Tryon Road
Raleigh, NC 27603
October 21, 2022
Prepared by:
______________________________
Graham M. Andres, P.E.
Executive Vice President
Tower Engineering Professionals, Inc. ∙ 326 Tryon Road ∙ Charlotte, NC 27603 ∙ T 919.661.6351 ∙ tepgroup.net
Soil Sampling Activities Report
Stork Rotary RFRU (RN)
3201 Rotary Drive
Charlotte, North Carolina
Brownfields Project No. 19059-15-060
TEP Job No. 246684.740348
Table of Contents
Section Page No.
1.0 Introduction…………..……….……………………………………………………………………………………………1
2.0 Background Information……….……………………………………………………………………………………..1
2.1 Site History.………………………………..………………………………………………………………………..1
2.2 Summary of Previous Environmental Activities ……………………………………………………2
3.0 Soil Sampling Activities………………………………………………………………..……………………………...3
3.1 Soil Sampling………………………………………………………………………………………………………..3
3.2 Soil Sampling Results……………………………………………………………………………………..….…4
3.3 Quality Assurance/Quality Control………………………………………………………………….……5
3.4 Boring Abandonment/Investigation Derived Wase……………………………………….……..4
4.0 Summary and Conclusions…………………………………………………………………………………….…….5
Tables
Table 1 Summary of Soil Sampling Analytical Results
Figures
Figure 1 Site Location Map
Figure 2 Soil Sample Location Map
Appendices
Appendix A Soil Boring Logs
Appendix B Laboratory Analytical Report
Soil Sampling Activities Report October 21, 2022
Stork Rotary RFRU (RN) 1

Soil Sampling Activities Report
Stork Rotary RFRU (RN)
3201 Rotary Drive
Charlotte, North Carolina
Brownfields Project No. 19059-15-060
TEP Job No. 246684.740348

1.0 INTRODUCTION
On behalf of No Bull Properties, LLC, Tower Engineering Professionals, Inc. (TEP) has prepared this Soil
Sampling Activities Report summarizing the soil sampling performed at the Stork Rotary RFRU (RN)
Brownfields property (Brownfields Project No. 19059-15-060) located at 3201 Rotary Drive, in
Charlotte, Mecklenburg County, North Carolina (Site). Please see Figure 1 for a provided Site Location
Map.
The Site is approximately 6.9-acres and is located along the northern side of Rotary Drive,
approximately 1,400 feet west of its intersection with Starita Road in Charlotte, North Carolina. The
Site is identified as Mecklenburg County Tax Parcel ID No. 04501312 and has a physical address of 3201
Rotary Drive. An existing single—story building occupies the central portion of the Site. The building
(approximately 46,800 square feet) was reportedly constructed in 1968 and is currently used as office
and warehouse space. The portion of the Site surrounding the existing building generally consists of
paved parking areas, landscaped area, and grass lawns. However, the northern portion of the subject
property (approximately 2 acres) was formerly wooded land and has recently been cleared/graded.
The soil sampling activities were conducted in general accordance with the methods stated in the DEQ-
approved Soil Sampling Activities Work Plan dated September 21, 2022. The purpose of the soil
sampling was to evaluate potential risks to future Site residents and/or workers from direct contact
exposure to soil at the Site. A brief summary of background information is presented in Section 2.0,
and the methods and results of the soil sampling assessment are provided in Section 3.0.
2.0 BACKGROUND INFORMATION
2.1 Site History
Historically, the Site was owned by Covington Diesel from 1968 until 1985. Covington Diesel operated
the Site as an automotive engine repair facility and truck garage. In 1985, SPG Prints purchased the
Site from Covington Diesel. SPG Prints also owned the western adjoining property (3001 Boxmeer
Drive) and operated both facilities as a single campus. The 3001 Boxmeer Drive property is also subject
to a Brownfields Agreement (19051—15—060).
Primary production work by SPG Prints on the Site was production of nickel sleeves from the operation
of nickel-plating baths. Other key activities included production of mandrels and rollers out of copper
Soil Sampling Activities Report October 21, 2022
Stork Rotary RFRU (RN) 2

and chromium plating baths. In addition, SEAMEX polymer production that was initially performed at
the adjoining 3001 Boxmeer Drive property was moved to the Site. The polymer process involved the
use of tetrachloroethylene (PCE) and trichloroethylene (TCE). SEAMEX polymer production reportedly
ceased in 1990.
It is our understanding that the Site was placed under a Ready-for-Reuse Brownfields Agreement in
October of 2016.
2.2 Summary of Previous Environmental Activities
Soil Impact
Previous assessments at the Site identified minor impacts from metals. However, only arsenic
was detected at concentrations exceeding North Carolina remediation goals. Arsenic detections
on the Site ranged from 3 to 10 mg/kg, but background samples exhibited concentrations of 4.1
and 4.6 mg/kg. With no known sources of arsenic from Site operations, the on-Site arsenic was
deemed to be naturally occurring.
Groundwater Impact
Previous assessments identified chlorinated solvent contamination in the shallow groundwater
across the central portion of the Site. Specifically, PCE was detected at concentrations exceeding
North Carolina Groundwater (2L) Standards. In addition, TCE was detected at a concentration
exceeding its 2L Standard. The concentrations of PCE and TCE detected also exceeded their
respective non-residential vapor intrusion screening levels. Although chlorinated solvent
contaminants were also detected in the groundwater at the western adjoining 3001 Boxmeer
Drive property, the assessments conducted to date suggest that the plumes are separate.
Therefore, it is presumed that the chlorinated solvent contamination at the Site is the result of
historic Site operations.
Potential Vapor Intrusion
Previous assessments revealed the presence of several VOCs in the soil gas beneath the building.
Specifically, PCE was detected at all sample locations during sampling events, with one (1)
sampling location exceeding its nonresidential vapor intrusion screening level. TCE was also
detected in the samples at concentrations that do not exceed the TCE nonresidential vapor
intrusion screening level. None of the remaining degradation products of PCE (cis-l,2-
dichloroethylene, trans-l,2-dichloroethylene, 1,1-dichloroethylene, and vinyl chloride) were
detected in the sub-slab vapor samples. No other VOCs were detected at concentrations
exceeding non—residential screening levels.

Soil Sampling Activities Report October 21, 2022
Stork Rotary RFRU (RN) 3

Ambient Air Sampling
In order to further assess vapor intrusion, multiple rounds of indoor air samples were collected
close to the sampling location exceeding its nonresidential vapor intrusion screen level for PCE.
These sampling events demonstrated that PCE concentrations inside that portion of the building
did not exceed non—residential indoor air screening levels.
3.0 SOIL SAMPLING ACTIVITIES
3.1 Soil Sampling
Front Lawn Area Soil Sampling
On October 3, 2022, TEP advanced a total of six (6) soil borings (HA-1A, HA-2A, HA-3A, HA-1B, HA-
2B, and HA-3B) from two (2) designated composite sample areas (A and B) in the front lawn area
parallel to Highway 85 and Rotary Drive where the installation of utility poles, fiber handholes, and
fiber conduit are proposed. TEP notes that the installation of these items is for training exercises
only. Soil borings were advanced to approximately 5 feet below ground surface (BGS) at each boring
location utilizing a decontaminated stainless-steel hand auger. Continuous soil samples were
collected from the center of the hand auger bucket at each soil boring and described for lithologic
purposes, observed for the presence of staining, and field screened for the presence of organic
vapors using a calibrated photoionization detector (PID). Soil boring logs with lithologic and field
screening information are included in Appendix A. Aliquots of soil from each area boring were placed
into a stainless-steel bowl and homogenized to form one (1) composite soil sample per sample area.
No obvious evidence of impacts was observed in the soil at the boring locations during field
screening activities. In accordance with the Work Plan, TEP selected the soil boring from each area
with the highest field screening result to collect a grab sample for laboratory analysis of volatile
organic compounds (VOCs). TEP selected a random soil boring from each area for VOC analysis
where field screening results did not indicate substantive indication of VOC impact. Grab samples
were collected from soil borings HA-3A and HA-1B (Figure2).
The soil samples selected for laboratory analysis were collected directly into laboratory supplied
glassware, labeled with the sample identification, date, time, and requested analysis and placed on
ice in a laboratory supplied cooler. The samples were delivered to Pace Analytical Laboratories
(Pace) under standard chain of custody protocols. The grab samples (HA-3A and HA-1B) were
collected and submitted for analysis of VOCs by EPA Method 8260. The composite samples (HA-A
and HA-B) were collected and submitted for analysis of semi-volatile organic compounds (SVOCs)
by EPA 8270, and RCRA metals by EPA Methods 6010/7471. The laboratory analytical report and the
chain of custody are included in Appendix B, and the analytical data is summarized on Table 1.

Soil Sampling Activities Report October 21, 2022
Stork Rotary RFRU (RN) 4

Back Graded Area Soil Sampling
On October 3, 2022, TEP advanced ten (10) soil borings (HA-1C, HA-2C, HA-3C, HA-4C, HA-5C, HA-
1D, HA-2D, HA-3D, HA-4D, and HA-5D) from two (2) designated composite sample areas (C and D)
in the back area that has recently been cleared, grubbed, and graded. Soil borings were advanced
to approximately 2 feet below ground surface (BGS) at each boring location utilizing a
decontaminated stainless-steel hand auger. Continuous soil samples were collected from the center
of the hand auger bucket at each soil boring and described for lithologic purposes, observed for the
presence of staining, and field screened for the presence of organic vapors using a calibrated PID.
Soil boring logs with lithologic and field screening information are included as Appendix A. Aliquots
of soil from each boring were placed into a stainless-steel bowl and homogenized to form one (1)
composite soil sample per sample area. No obvious evidence of impacts was observed in the soil at
the boring locations during field screening activities. In accordance with the Work Plan, TEP selected
the soil boring from each area with the highest field screening result to collect a grab sample for
laboratory analysis of VOCs. TEP selected a random soil boring from each area for VOC analysis
where field screening results did not indicate substantive indication of VOC impact. Grab samples
were collected from soil borings HA-3C and HA-5D (Figure2).
The soil samples selected for laboratory analysis were collected directly into laboratory supplied
glassware, labeled with the sample identification, date, time, and requested analysis and placed on
ice in a laboratory supplied cooler. The samples were delivered to Pace under standard chain of
custody protocols. The grab samples (HA-3C and HA-5D) were collected and submitted for analysis
of VOCs by EPA Method 8260. The composite samples (HA-C and HA-D) were collected and
submitted for analysis of SVOCs by EPA 8270, and RCRA metals by EPA Methods 6010/7471. The
laboratory analytical report and the chain of custody are included in Appendix B, and the analytical
data is summarized on Table 1.
3.2 Soil Sampling Results
VOCs
Laboratory analytical results indicate that no VOCs were detected at concentrations above Residential
PSRGs. Five (5) low-level VOCs (acetone, 2-butanone (MEK), n-butylbenzene, p-isopropyltoluene, and
o-xylene) were detected at concentrations above laboratory method detection limits in one or more
samples and associated duplicate sample, but at concentrations well below their respective PSRG
values.
SVOCs
Laboratory analytical results indicate that no SVOCs were detected at concentrations above laboratory
method detection limits.
Soil Sampling Activities Report October 21, 2022
Stork Rotary RFRU (RN) 5

Metals
Analytical results indicate the presence of several metals at concentrations above laboratory method
detection limits in the samples and associated duplicate sample, but below the Residential PSRGs or
regional background levels (in the absence of PSRGs).
3.3 Quality Assurance/Quality Control
For quality assurance/quality control (QA/QC) purposes, TEP collected one duplicate soil sample (DUP)
from HA-D (the VOC sample was collected from HA-5D) for laboratory analysis. The duplicate sample
was analyzed for the same laboratory analysis as the parent sample. The results of the analytical data
from the duplicate sample indicated that similar constituents and concentrations were detected in
both the parent and duplicate soil sample. Therefore, the duplicate sample results indicated good
laboratory repeatability.
Additionally, TEP collected an equipment blank (EQ Blank) to evaluate the effectiveness of the field
equipment decontamination methods. To collect the equipment blank, laboratory supplied analyte
free water was poured over the decontaminated stainless-steel hand auger. The water was collected
off the hand auger directly into laboratory supplied sample containers. The equipment blank sample
was analyzed for the same laboratory analysis. The analytical data for the equipment blank sample
indicated that VOC, SVOC, or metal constituents were not detected above laboratory MDLs, with the
exception of acetone, which was detected a low estimated J-flag concentration. Acetone was also
detected in the trip blank at a similar low estimated J-flag concentration. Acetone is a common
ingredient in cleaning solutions and thus is a common laboratory contaminant. The low concentration
of acetone detected could be attributed to laboratory contamination. Therefore, the results of the
equipment blank indicate that effective field equipment decontamination methods were performed
and did not appear to impact the analytical results of the soil samples. The laboratory analytical report
and the chain of custody are included in Appendix B, and the analytical data is summarized on Table 1.
3.4 Boring Abandonment and Investigation Derived Waste
During boring advancement and sampling, field screening indicated no evidence of significant impact.
Therefore, the investigation derived waste (IDW) generated during the sampling activities was thin
spread in the areas of generation. Following sampling activities, the soil borings were abandoned using
excess soils generated from the sampling activities, and the surface was repaired to match pre-
sampling conditions with grass cover.
4.0 REPORTING
TEP has completed soil sampling activities at the Stork Rotary RFRU (RN) Brownfields property (BF #
19059-15-060) located at 3201 Rotary Drive in Charlotte, Mecklenburg County, North Carolina. The
Soil Sampling Activities Report October 21, 2022
Stork Rotary RFRU (RN) 6

purpose of the soil sampling activities was to evaluate potential risks to future Site residents and/or
workers from direct contact exposure to soil at the Site. The results of the soil sampling indicated the
following:
• No VOCs were detected at concentrations above Residential PSRGs in any of the soil samples.
• No SVOCs were detected at concentrations above laboratory method detection limits in any of
the soil samples.
• No metals were detected at concentrations above Residential PSRGs or regional background
levels (in the absence of PSRGs) in any of the soil samples.
HA-A HA-B HA-C
VOC Sample Aliquot HA-3A HA-1B HA-3C
Sample Date
Units
VOCs by EPA Method 8260
Acetone ND ND ND 2.57 1.99 14,000 210,000 --
2-Butanone (MEK)ND ND ND 0.24 0.182 5,500 40,000 --
n-Butylbenzene ND ND ND 0.177 0.104 780 12,000 --
p-Isopropyltoluene ND ND ND 0.375 0.277 1.24 (pgw)1.24 (pgw)--
o-Xylene ND ND 0.0043J ND ND 140 590 --
SVOCs by EPA Method 8270 ND ND ND ND ND ----
Metals by EPA Method 6010/7471
Arsenic ND ND 0.95 ND ND 1 3.0 1.0-18.0 4.8
Barium 47.1 34 82.2 116 162 3,100 47,000 50-1,000 356
Cadmium ND 0.48 0.48 ND ND 1.4 20 1.0-10.0*4.3
Total Chromium ND 30.3 13.2 14.4 18.7 NE NE 7.0-300 65
Lead 7.2 8 14.1 17.9 18.5 400 800 ND-50 16
Mercury 0.014 0.019 0.12 0.039 0.052 2.3 9.7 0.03-0.52 0.121
Selenium ND ND ND ND ND 78 1,200 <0.1-0.8 0.42
Silver ND ND ND ND ND 78 1,200 ND-5.0 NS
Notes:
SVOCs = Semi-Volatile Organic Compounds
PSRG = Preliminary Soil Remediation Goal
NS = Not Specified
NE = Not Established
ND = Not Detected
(1) = Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005
* = Range and mean values of background metals for Southeastern USA soils
J = estimated value between the laboratory detection limit and the laboratory reporting limit
VOC sample collected as grab sample
Soil samples for analysis of SVOCs and metals collected as composite samples
(pgw) = protection of groundwater PSRG. No residential or industrial/commercial PSRG exists
Table1
VOCs = Volatile Organic Compounds
TEP Project No. 246684.740348
Brownfields Project No. 19059-15-060
Stork Rotary RFRU (RN)Summary of Soil Sampling Analytical Results
Sample ID
Composite Sample Areas
HA-D/DUP
HA-5D
10/3/2022
mg/kg
PSRGs
Residential Industrial/Commercial
mg/kg
Regional Background Metals in Soil (1)
Range Mean
mg/kg
Figure #1
North
Client:
Project:Location:TEP Project No:
Source:Date: October 2022
SITE LOCAITON MAP
TOWER ENGINEERING PROFESSIONALS,
INC.
326 Tryon Road
Raleigh, North Carolina 27603919-661-6351
No Bull Properties, LLC
Stork Rotary RFRU (RN)3201 Rotary Drive, Charlotte, NC
246694.740348EDR
Figure #2
North
Client:
Project:
Location:
TEP Project No:
Source:
Date: October 2022
SOIL SAMPLE LOCATION MAP
TOWER ENGINEERING PROFESSIONALS,
INC.
326 Tryon Road
Raleigh, North Carolina  27603
919‐661‐6351
No Bull Properties, LLC
Stork Rotary RFRU (RN)
3201 Rotary Drive, Charlotte, NC
246694.740348
Google Earth
Legend
Proposed Utility Pole
Proposed Fiber Hand Hole
Proposed Underground Conduit
Approximate Clearing Limits
Area A
Area BArea C
Area D
HA-3B
HA-2B
HA-1B
HA-3AHA-1A HA-2A
HA-1D HA-2D
HA-3D
HA-5D
HA-4D
HA-1C HA-2C
HA-4C
HA-3C
HA-5C
GB
GB
GB
PID = 0 ppm
PID = 0 ppm
PID = 0 ppm
CL-
ML
5.0
(CL-ML) Dry, brown, silty CLAY
Bottom of borehole at 5.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
3
4
5
PAGE 1 OF 1
BORING NUMBER HA-1A
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB
GB
GB
PID = 0 ppm
PID = 0 ppm
PID = 0 ppm
CL-
ML
5.0
(CL-ML) Dry, tan to pink, silty CLAY
Bottom of borehole at 5.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
3
4
5
PAGE 1 OF 1
BORING NUMBER HA-2A
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB
GB
GB
PID = 0 ppm
PID = 0 ppm
PID = 0 ppm
CL-
ML
5.0
(CL-ML) Dry, tan to pink, silty CLAY
Bottom of borehole at 5.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
3
4
5
PAGE 1 OF 1
BORING NUMBER HA-3A
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB
GB
GB
PID = 0 ppm
PID = 0 ppm
PID = 0 ppm
CL-
ML
5.0
(CL-ML) Dry, brown, silty CLAY
Bottom of borehole at 5.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
3
4
5
PAGE 1 OF 1
BORING NUMBER HA-1B
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB
GB
GB
PID = 0 ppm
PID = 0 ppm
PID = 0 ppm
CL-
ML
5.0
(CL-ML) Dry, brown, silty CLAY
Bottom of borehole at 5.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
3
4
5
PAGE 1 OF 1
BORING NUMBER HA-2B
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB
GB
GB
PID = 0 ppm
PID = 0 ppm
PID = 0 ppm
CL-
ML
5.0
(CL-ML) Dry, tan-pink, silty CLAY
Bottom of borehole at 5.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
3
4
5
PAGE 1 OF 1
BORING NUMBER HA-3B
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB PID = 2 ppm CL
2.0
(CL) Moist, brown-orange, sandy CLAY
Bottom of borehole at 2.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
PAGE 1 OF 1
BORING NUMBER HA-1C
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB PID = 0.8 ppm CL
2.0
(CL) Moist, brown-orange, sandy CLAY
Bottom of borehole at 2.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
PAGE 1 OF 1
BORING NUMBER HA-2C
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB PID = 6.7 ppm CL
2.0
(CL) Moist, brown-orange, sandy CLAY
Bottom of borehole at 2.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
PAGE 1 OF 1
BORING NUMBER HA-3C
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB PID = 0 ppm SC
2.0
(SC) Dry, orange-brown, clayey SAND
Bottom of borehole at 2.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
PAGE 1 OF 1
BORING NUMBER HA-4C
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB PID = 0 ppm SC
2.0
(SC) Dry, orange-brown, clayey SAND
Bottom of borehole at 2.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
PAGE 1 OF 1
BORING NUMBER HA-5C
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB PID = 2.4 ppm CL
2.0
(CL) Moist, brown-orange, sandy CLAY
Bottom of borehole at 2.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
PAGE 1 OF 1
BORING NUMBER HA-1D
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB
PID = 15.4 ppm
(pine needles androots in sample)CL
2.0
(CL) Moist, brown-orange, sandy CLAY
Bottom of borehole at 2.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
PAGE 1 OF 1
BORING NUMBER HA-2D
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB PID = 1.3 ppm CL
2.0
(CL) Moist, brown-orange, sandy CLAY
Bottom of borehole at 2.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
PAGE 1 OF 1
BORING NUMBER HA-3D
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB PID = 0 ppm CL
2.0
(CL) Moist, brown-orange, sandy CLAY
Bottom of borehole at 2.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
PAGE 1 OF 1
BORING NUMBER HA-4D
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
GB
PID = 17 ppm
(pine needles androots in sample)CL
2.0
(CL) Moist, brown-orange, sandy CLAY
Bottom of borehole at 2.0 feet.
NOTES
GROUND ELEVATION
LOGGED BY CS
DRILLING METHOD Hand Auger
DRILLING CONTRACTOR TEP GROUND WATER LEVELS:
CHECKED BY RM
DATE STARTED 10/3/22 COMPLETED 10/3/22
AT TIME OF DRILLING ---
AT END OF DRILLING ---
AFTER DRILLING ---
HOLE SIZE 3.25 inches
SAMPLE TYPENUMBERDEPTH(ft)0
1
2
PAGE 1 OF 1
BORING NUMBER HA-5D
CLIENT No Bull Properties, LLC
PROJECT NUMBER 246684.740348
PROJECT NAME Stork Rotary RFRU (RN)
PROJECT LOCATION 3201 Rotary Drive, Charlotte, NC
GENERAL BH / TP / WELL - GINT STD US LAB.GDT - 10/21/22 14:11 - G:\SHARED DRIVES\245780 - 247073\246684\P-223677_L-740348__3201 ROTARY DRIVE_SOIL SAMPLING\SOIL SAMPLING REPORT\BORING LOGS.GPJTower Engineering Professionals, Inc.
REMARKS
U.S.C.S.GRAPHICLOGMATERIAL DESCRIPTION
#=CL#
October 18, 2022
LIMS USE: FR - CLINT SORRELL
LIMS OBJECT ID: 92629052
92629052
Project:
Pace Project No.:
RE:
Clint Sorrell
Tower Engineering Professionals, Inc
326 Tryon Road
Raleigh, NC 27603
ROTARY DRIVE
Dear Clint Sorrell:
Enclosed are the analytical results for sample(s) received by the laboratory on October 04, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
• Pace Analytical Services - Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 72
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Pace Analytical Services Ormond Beach
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maine Certification #: FL01264
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Ohio DEP 87780
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 72
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Lab ID Sample ID Matrix Date Collected Date Received
92629052001 HA-C Solid 10/03/22 13:00 10/04/22 13:17
92629052002 HA-D Solid 10/03/22 15:30 10/04/22 13:17
92629052003 HA-D-DUP Solid 10/03/22 15:35 10/04/22 13:17
92629052004 HA-A Solid 10/03/22 16:30 10/04/22 13:17
92629052005 HA-B Solid 10/03/22 17:20 10/04/22 13:17
92629052006 HA-3C Solid 10/03/22 13:00 10/04/22 13:17
92629052007 HA-5D Solid 10/03/22 15:30 10/04/22 13:17
92629052008 HA-5D-DUP Solid 10/03/22 15:35 10/04/22 13:17
92629052009 HA-3A Solid 10/03/22 16:35 10/04/22 13:17
92629052010 HA-1B Solid 10/03/22 17:25 10/04/22 13:17
92629052011 EQ BLANK Water 10/03/22 13:30 10/04/22 13:17
92629052012 TRIP BLANK Water 10/03/22 00:00 10/04/22 13:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 72
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92629052001 HA-C EPA 6010 7 PASI-OAME, KC2
EPA 7471 1 PASI-OJNK
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92629052002 HA-D EPA 6010 7 PASI-OAME
EPA 7471 1 PASI-OJNK
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92629052003 HA-D-DUP EPA 6010 7 PASI-OAME
EPA 7471 1 PASI-OJNK
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92629052004 HA-A EPA 6010 7 PASI-OAME
EPA 7471 1 PASI-OJNK
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92629052005 HA-B EPA 6010 7 PASI-OAME, KC2
EPA 7471 1 PASI-OJNK
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92629052006 HA-3C EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92629052007 HA-5D EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92629052008 HA-5D-DUP EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92629052009 HA-3A EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92629052010 HA-1B EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92629052011 EQ BLANK EPA 6010D 7 PASI-GADRB
EPA 7470A 1 PASI-ANMP
EPA 8270E 74 PASI-CPKS
EPA 8260D 71 PASI-CSAS
92629052012 TRIP BLANK EPA 8260D 71 PASI-CSAS
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 72
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
PASI-O = Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-C Lab ID: 92629052001 Collected: 10/03/22 13:00 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Ormond Beach
6010 MET ICP
Arsenic 0.95 mg/kg 10/15/22 19:47 7440-38-210/11/22 21:260.71 0.35 1
Barium 82.2 mg/kg 10/15/22 19:47 7440-39-310/11/22 21:260.71 0.12 1
Cadmium 0.48 mg/kg 10/15/22 19:47 7440-43-910/11/22 21:260.071 0.035 1
Chromium 13.2 mg/kg 10/15/22 19:47 7440-47-310/11/22 21:260.35 0.18 1
Lead 14.1 mg/kg 10/15/22 19:47 7439-92-110/11/22 21:260.71 0.35 1
Selenium ND mg/kg 10/17/22 11:44 7782-49-2 D310/11/22 21:265.3 2.7 5
Silver ND mg/kg 10/17/22 11:44 7440-22-4 D310/11/22 21:261.8 0.39 5
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
7471 Mercury
Mercury 0.12 mg/kg 10/13/22 09:31 7439-97-610/12/22 07:340.012 0.0059 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 10/14/22 09:50 83-32-910/12/22 17:09424 149 1
Acenaphthylene ND ug/kg 10/14/22 09:50 208-96-810/12/22 17:09424 149 1
Aniline ND ug/kg 10/14/22 09:50 62-53-310/12/22 17:09424 166 1
Anthracene ND ug/kg 10/14/22 09:50 120-12-710/12/22 17:09424 139 1
Benzo(a)anthracene ND ug/kg 10/14/22 09:50 56-55-310/12/22 17:09424 141 1
Benzo(a)pyrene ND ug/kg 10/14/22 09:50 50-32-810/12/22 17:09424 146 1
Benzo(b)fluoranthene ND ug/kg 10/14/22 09:50 205-99-210/12/22 17:09424 141 1
Benzo(g,h,i)perylene ND ug/kg 10/14/22 09:50 191-24-210/12/22 17:09424 164 1
Benzo(k)fluoranthene ND ug/kg 10/14/22 09:50 207-08-910/12/22 17:09424 149 1
Benzoic Acid ND ug/kg 10/14/22 09:50 65-85-010/12/22 17:092120 911 1
Benzyl alcohol ND ug/kg 10/14/22 09:50 100-51-610/12/22 17:09848 321 1
4-Bromophenylphenyl ether ND ug/kg 10/14/22 09:50 101-55-310/12/22 17:09424 163 1
Butylbenzylphthalate ND ug/kg 10/14/22 09:50 85-68-710/12/22 17:09424 179 1
4-Chloro-3-methylphenol ND ug/kg 10/14/22 09:50 59-50-710/12/22 17:09848 298 1
4-Chloroaniline ND ug/kg 10/14/22 09:50 106-47-810/12/22 17:09848 333 1
bis(2-Chloroethoxy)methane ND ug/kg 10/14/22 09:50 111-91-110/12/22 17:09424 176 1
bis(2-Chloroethyl) ether ND ug/kg 10/14/22 09:50 111-44-410/12/22 17:09424 159 1
2-Chloronaphthalene ND ug/kg 10/14/22 09:50 91-58-710/12/22 17:09424 168 1
2-Chlorophenol ND ug/kg 10/14/22 09:50 95-57-810/12/22 17:09424 159 1
4-Chlorophenylphenyl ether ND ug/kg 10/14/22 09:50 7005-72-310/12/22 17:09424 158 1
Chrysene ND ug/kg 10/14/22 09:50 218-01-910/12/22 17:09424 154 1
Dibenz(a,h)anthracene ND ug/kg 10/14/22 09:50 53-70-310/12/22 17:09424 163 1
Dibenzofuran ND ug/kg 10/14/22 09:50 132-64-910/12/22 17:09424 153 1
1,2-Dichlorobenzene ND ug/kg 10/14/22 09:50 95-50-110/12/22 17:09424 153 1
1,3-Dichlorobenzene ND ug/kg 10/14/22 09:50 541-73-110/12/22 17:09424 150 1
1,4-Dichlorobenzene ND ug/kg 10/14/22 09:50 106-46-710/12/22 17:09424 162 1
3,3'-Dichlorobenzidine ND ug/kg 10/14/22 09:50 91-94-110/12/22 17:09848 287 1
2,4-Dichlorophenol ND ug/kg 10/14/22 09:50 120-83-210/12/22 17:09424 166 1
Diethylphthalate ND ug/kg 10/14/22 09:50 84-66-210/12/22 17:09424 155 1
2,4-Dimethylphenol ND ug/kg 10/14/22 09:50 105-67-910/12/22 17:09424 176 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-C Lab ID: 92629052001 Collected: 10/03/22 13:00 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 10/14/22 09:50 131-11-310/12/22 17:09424 154 1
Di-n-butylphthalate ND ug/kg 10/14/22 09:50 84-74-210/12/22 17:09424 143 1
4,6-Dinitro-2-methylphenol ND ug/kg 10/14/22 09:50 534-52-110/12/22 17:09848 396 1
2,4-Dinitrophenol ND ug/kg 10/14/22 09:50 51-28-510/12/22 17:092120 1310 1
2,4-Dinitrotoluene ND ug/kg 10/14/22 09:50 121-14-210/12/22 17:09424 163 1
2,6-Dinitrotoluene ND ug/kg 10/14/22 09:50 606-20-210/12/22 17:09424 155 1
Di-n-octylphthalate ND ug/kg 10/14/22 09:50 117-84-010/12/22 17:09424 167 1
bis(2-Ethylhexyl)phthalate ND ug/kg 10/14/22 09:50 117-81-710/12/22 17:09424 164 1
Fluoranthene ND ug/kg 10/14/22 09:50 206-44-010/12/22 17:09424 145 1
Fluorene ND ug/kg 10/14/22 09:50 86-73-710/12/22 17:09424 149 1
Hexachloro-1,3-butadiene ND ug/kg 10/14/22 09:50 87-68-3 v110/12/22 17:09424 184 1
Hexachlorobenzene ND ug/kg 10/14/22 09:50 118-74-110/12/22 17:09424 166 1
Hexachlorocyclopentadiene ND ug/kg 10/14/22 09:50 77-47-410/12/22 17:09424 243 1
Hexachloroethane ND ug/kg 10/14/22 09:50 67-72-110/12/22 17:09424 162 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/14/22 09:50 193-39-510/12/22 17:09424 167 1
Isophorone ND ug/kg 10/14/22 09:50 78-59-110/12/22 17:09424 189 1
1-Methylnaphthalene ND ug/kg 10/14/22 09:50 90-12-010/12/22 17:09424 149 1
2-Methylnaphthalene ND ug/kg 10/14/22 09:50 91-57-610/12/22 17:09424 170 1
2-Methylphenol(o-Cresol)ND ug/kg 10/14/22 09:50 95-48-710/12/22 17:09424 173 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/14/22 09:50 15831-10-410/12/22 17:09424 171 1
Naphthalene ND ug/kg 10/14/22 09:50 91-20-310/12/22 17:09424 144 1
2-Nitroaniline ND ug/kg 10/14/22 09:50 88-74-410/12/22 17:092120 347 1
3-Nitroaniline ND ug/kg 10/14/22 09:50 99-09-210/12/22 17:092120 333 1
4-Nitroaniline ND ug/kg 10/14/22 09:50 100-01-610/12/22 17:09848 323 1
Nitrobenzene ND ug/kg 10/14/22 09:50 98-95-310/12/22 17:09424 197 1
2-Nitrophenol ND ug/kg 10/14/22 09:50 88-75-510/12/22 17:09424 184 1
4-Nitrophenol ND ug/kg 10/14/22 09:50 100-02-710/12/22 17:092120 820 1
N-Nitrosodimethylamine ND ug/kg 10/14/22 09:50 62-75-910/12/22 17:09424 143 1
N-Nitroso-di-n-propylamine ND ug/kg 10/14/22 09:50 621-64-710/12/22 17:09424 159 1
N-Nitrosodiphenylamine ND ug/kg 10/14/22 09:50 86-30-610/12/22 17:09424 150 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/14/22 09:50 108-60-1 v210/12/22 17:09424 202 1
Pentachlorophenol ND ug/kg 10/14/22 09:50 87-86-510/12/22 17:09848 415 1
Phenanthrene ND ug/kg 10/14/22 09:50 85-01-810/12/22 17:09424 139 1
Phenol ND ug/kg 10/14/22 09:50 108-95-210/12/22 17:09424 189 1
Pyrene ND ug/kg 10/14/22 09:50 129-00-010/12/22 17:09424 172 1
Pyridine ND ug/kg 10/14/22 09:50 110-86-110/12/22 17:09424 134 1
1,2,4-Trichlorobenzene ND ug/kg 10/14/22 09:50 120-82-110/12/22 17:09424 167 1
2,4,5-Trichlorophenol ND ug/kg 10/14/22 09:50 95-95-410/12/22 17:09424 194 1
2,4,6-Trichlorophenol ND ug/kg 10/14/22 09:50 88-06-210/12/22 17:09424 175 1
Surrogates
Nitrobenzene-d5 (S)65 %10/14/22 09:50 4165-60-010/12/22 17:0910-130 1
2-Fluorobiphenyl (S)56 %10/14/22 09:50 321-60-810/12/22 17:0910-130 1
Terphenyl-d14 (S)62 %10/14/22 09:50 1718-51-010/12/22 17:0910-130 1
Phenol-d6 (S)51 %10/14/22 09:50 13127-88-310/12/22 17:0910-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-C Lab ID: 92629052001 Collected: 10/03/22 13:00 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)51 %10/14/22 09:50 367-12-410/12/22 17:0910-130 1
2,4,6-Tribromophenol (S)64 %10/14/22 09:50 118-79-610/12/22 17:0910-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.4 %10/04/22 17:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-D Lab ID: 92629052002 Collected: 10/03/22 15:30 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Ormond Beach
6010 MET ICP
Arsenic ND mg/kg 10/17/22 11:55 7440-38-2 D310/11/22 21:265.3 2.6 10
Barium 116 mg/kg 10/17/22 11:55 7440-39-310/11/22 21:265.3 0.89 10
Cadmium ND mg/kg 10/17/22 11:55 7440-43-9 D310/11/22 21:260.53 0.26 10
Chromium 14.4 mg/kg 10/17/22 11:55 7440-47-310/11/22 21:262.6 1.3 10
Lead 17.9 mg/kg 10/17/22 11:55 7439-92-110/11/22 21:265.3 2.6 10
Selenium ND mg/kg 10/17/22 11:55 7782-49-2 D310/11/22 21:267.9 4.0 10
Silver ND mg/kg 10/17/22 11:55 7440-22-4 D310/11/22 21:262.6 0.58 10
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
7471 Mercury
Mercury 0.039 mg/kg 10/13/22 09:38 7439-97-610/12/22 07:340.010 0.0051 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 10/14/22 14:49 83-32-910/12/22 17:09408 143 1
Acenaphthylene ND ug/kg 10/14/22 14:49 208-96-810/12/22 17:09408 143 1
Aniline ND ug/kg 10/14/22 14:49 62-53-310/12/22 17:09408 159 1
Anthracene ND ug/kg 10/14/22 14:49 120-12-710/12/22 17:09408 133 1
Benzo(a)anthracene ND ug/kg 10/14/22 14:49 56-55-310/12/22 17:09408 136 1
Benzo(a)pyrene ND ug/kg 10/14/22 14:49 50-32-810/12/22 17:09408 141 1
Benzo(b)fluoranthene ND ug/kg 10/14/22 14:49 205-99-210/12/22 17:09408 136 1
Benzo(g,h,i)perylene ND ug/kg 10/14/22 14:49 191-24-210/12/22 17:09408 158 1
Benzo(k)fluoranthene ND ug/kg 10/14/22 14:49 207-08-910/12/22 17:09408 143 1
Benzoic Acid ND ug/kg 10/14/22 14:49 65-85-010/12/22 17:092040 876 1
Benzyl alcohol ND ug/kg 10/14/22 14:49 100-51-610/12/22 17:09815 309 1
4-Bromophenylphenyl ether ND ug/kg 10/14/22 14:49 101-55-310/12/22 17:09408 157 1
Butylbenzylphthalate ND ug/kg 10/14/22 14:49 85-68-710/12/22 17:09408 172 1
4-Chloro-3-methylphenol ND ug/kg 10/14/22 14:49 59-50-710/12/22 17:09815 287 1
4-Chloroaniline ND ug/kg 10/14/22 14:49 106-47-810/12/22 17:09815 320 1
bis(2-Chloroethoxy)methane ND ug/kg 10/14/22 14:49 111-91-110/12/22 17:09408 169 1
bis(2-Chloroethyl) ether ND ug/kg 10/14/22 14:49 111-44-410/12/22 17:09408 153 1
2-Chloronaphthalene ND ug/kg 10/14/22 14:49 91-58-710/12/22 17:09408 162 1
2-Chlorophenol ND ug/kg 10/14/22 14:49 95-57-810/12/22 17:09408 153 1
4-Chlorophenylphenyl ether ND ug/kg 10/14/22 14:49 7005-72-310/12/22 17:09408 152 1
Chrysene ND ug/kg 10/14/22 14:49 218-01-910/12/22 17:09408 148 1
Dibenz(a,h)anthracene ND ug/kg 10/14/22 14:49 53-70-310/12/22 17:09408 157 1
Dibenzofuran ND ug/kg 10/14/22 14:49 132-64-910/12/22 17:09408 147 1
1,2-Dichlorobenzene ND ug/kg 10/14/22 14:49 95-50-110/12/22 17:09408 147 1
1,3-Dichlorobenzene ND ug/kg 10/14/22 14:49 541-73-110/12/22 17:09408 145 1
1,4-Dichlorobenzene ND ug/kg 10/14/22 14:49 106-46-710/12/22 17:09408 156 1
3,3'-Dichlorobenzidine ND ug/kg 10/14/22 14:49 91-94-110/12/22 17:09815 275 1
2,4-Dichlorophenol ND ug/kg 10/14/22 14:49 120-83-210/12/22 17:09408 159 1
Diethylphthalate ND ug/kg 10/14/22 14:49 84-66-210/12/22 17:09408 149 1
2,4-Dimethylphenol ND ug/kg 10/14/22 14:49 105-67-910/12/22 17:09408 169 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-D Lab ID: 92629052002 Collected: 10/03/22 15:30 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 10/14/22 14:49 131-11-310/12/22 17:09408 148 1
Di-n-butylphthalate ND ug/kg 10/14/22 14:49 84-74-210/12/22 17:09408 137 1
4,6-Dinitro-2-methylphenol ND ug/kg 10/14/22 14:49 534-52-110/12/22 17:09815 380 1
2,4-Dinitrophenol ND ug/kg 10/14/22 14:49 51-28-510/12/22 17:092040 1260 1
2,4-Dinitrotoluene ND ug/kg 10/14/22 14:49 121-14-210/12/22 17:09408 157 1
2,6-Dinitrotoluene ND ug/kg 10/14/22 14:49 606-20-210/12/22 17:09408 149 1
Di-n-octylphthalate ND ug/kg 10/14/22 14:49 117-84-010/12/22 17:09408 161 1
bis(2-Ethylhexyl)phthalate ND ug/kg 10/14/22 14:49 117-81-710/12/22 17:09408 158 1
Fluoranthene ND ug/kg 10/14/22 14:49 206-44-010/12/22 17:09408 140 1
Fluorene ND ug/kg 10/14/22 14:49 86-73-710/12/22 17:09408 143 1
Hexachloro-1,3-butadiene ND ug/kg 10/14/22 14:49 87-68-3 v110/12/22 17:09408 177 1
Hexachlorobenzene ND ug/kg 10/14/22 14:49 118-74-110/12/22 17:09408 159 1
Hexachlorocyclopentadiene ND ug/kg 10/14/22 14:49 77-47-410/12/22 17:09408 233 1
Hexachloroethane ND ug/kg 10/14/22 14:49 67-72-110/12/22 17:09408 156 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/14/22 14:49 193-39-510/12/22 17:09408 161 1
Isophorone ND ug/kg 10/14/22 14:49 78-59-110/12/22 17:09408 182 1
1-Methylnaphthalene ND ug/kg 10/14/22 14:49 90-12-010/12/22 17:09408 143 1
2-Methylnaphthalene ND ug/kg 10/14/22 14:49 91-57-610/12/22 17:09408 163 1
2-Methylphenol(o-Cresol)ND ug/kg 10/14/22 14:49 95-48-710/12/22 17:09408 167 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/14/22 14:49 15831-10-410/12/22 17:09408 164 1
Naphthalene ND ug/kg 10/14/22 14:49 91-20-310/12/22 17:09408 138 1
2-Nitroaniline ND ug/kg 10/14/22 14:49 88-74-410/12/22 17:092040 334 1
3-Nitroaniline ND ug/kg 10/14/22 14:49 99-09-210/12/22 17:092040 320 1
4-Nitroaniline ND ug/kg 10/14/22 14:49 100-01-610/12/22 17:09815 310 1
Nitrobenzene ND ug/kg 10/14/22 14:49 98-95-310/12/22 17:09408 189 1
2-Nitrophenol ND ug/kg 10/14/22 14:49 88-75-510/12/22 17:09408 177 1
4-Nitrophenol ND ug/kg 10/14/22 14:49 100-02-710/12/22 17:092040 788 1
N-Nitrosodimethylamine ND ug/kg 10/14/22 14:49 62-75-910/12/22 17:09408 137 1
N-Nitroso-di-n-propylamine ND ug/kg 10/14/22 14:49 621-64-710/12/22 17:09408 153 1
N-Nitrosodiphenylamine ND ug/kg 10/14/22 14:49 86-30-610/12/22 17:09408 145 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/14/22 14:49 108-60-1 v210/12/22 17:09408 194 1
Pentachlorophenol ND ug/kg 10/14/22 14:49 87-86-510/12/22 17:09815 399 1
Phenanthrene ND ug/kg 10/14/22 14:49 85-01-810/12/22 17:09408 133 1
Phenol ND ug/kg 10/14/22 14:49 108-95-210/12/22 17:09408 182 1
Pyrene ND ug/kg 10/14/22 14:49 129-00-010/12/22 17:09408 166 1
Pyridine ND ug/kg 10/14/22 14:49 110-86-110/12/22 17:09408 128 1
1,2,4-Trichlorobenzene ND ug/kg 10/14/22 14:49 120-82-110/12/22 17:09408 161 1
2,4,5-Trichlorophenol ND ug/kg 10/14/22 14:49 95-95-410/12/22 17:09408 187 1
2,4,6-Trichlorophenol ND ug/kg 10/14/22 14:49 88-06-210/12/22 17:09408 168 1
Surrogates
Nitrobenzene-d5 (S)58 %10/14/22 14:49 4165-60-010/12/22 17:0910-130 1
2-Fluorobiphenyl (S)42 %10/14/22 14:49 321-60-810/12/22 17:0910-130 1
Terphenyl-d14 (S)57 %10/14/22 14:49 1718-51-010/12/22 17:0910-130 1
Phenol-d6 (S)43 %10/14/22 14:49 13127-88-310/12/22 17:0910-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-D Lab ID: 92629052002 Collected: 10/03/22 15:30 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)36 %10/14/22 14:49 367-12-410/12/22 17:0910-130 1
2,4,6-Tribromophenol (S)45 %10/14/22 14:49 118-79-610/12/22 17:0910-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.8 %10/04/22 17:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-D-DUP Lab ID: 92629052003 Collected: 10/03/22 15:35 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Ormond Beach
6010 MET ICP
Arsenic ND mg/kg 10/17/22 11:59 7440-38-2 D310/11/22 21:265.0 2.5 5
Barium 162 mg/kg 10/17/22 11:59 7440-39-310/11/22 21:265.0 0.84 5
Cadmium ND mg/kg 10/17/22 11:59 7440-43-9 D310/11/22 21:260.50 0.25 5
Chromium 18.7 mg/kg 10/17/22 11:59 7440-47-310/11/22 21:262.5 1.2 5
Lead 18.5 mg/kg 10/17/22 11:59 7439-92-110/11/22 21:265.0 2.5 5
Selenium ND mg/kg 10/17/22 11:59 7782-49-2 D310/11/22 21:267.5 3.7 5
Silver ND mg/kg 10/17/22 11:59 7440-22-4 D310/11/22 21:262.5 0.55 5
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
7471 Mercury
Mercury 0.052 mg/kg 10/13/22 09:40 7439-97-610/12/22 07:340.016 0.0080 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 10/14/22 15:16 83-32-910/12/22 17:09562 198 1
Acenaphthylene ND ug/kg 10/14/22 15:16 208-96-810/12/22 17:09562 198 1
Aniline ND ug/kg 10/14/22 15:16 62-53-310/12/22 17:09562 220 1
Anthracene ND ug/kg 10/14/22 15:16 120-12-710/12/22 17:09562 184 1
Benzo(a)anthracene ND ug/kg 10/14/22 15:16 56-55-310/12/22 17:09562 187 1
Benzo(a)pyrene ND ug/kg 10/14/22 15:16 50-32-810/12/22 17:09562 194 1
Benzo(b)fluoranthene ND ug/kg 10/14/22 15:16 205-99-210/12/22 17:09562 187 1
Benzo(g,h,i)perylene ND ug/kg 10/14/22 15:16 191-24-210/12/22 17:09562 218 1
Benzo(k)fluoranthene ND ug/kg 10/14/22 15:16 207-08-910/12/22 17:09562 198 1
Benzoic Acid ND ug/kg 10/14/22 15:16 65-85-010/12/22 17:092810 1210 1
Benzyl alcohol ND ug/kg 10/14/22 15:16 100-51-610/12/22 17:091120 426 1
4-Bromophenylphenyl ether ND ug/kg 10/14/22 15:16 101-55-310/12/22 17:09562 216 1
Butylbenzylphthalate ND ug/kg 10/14/22 15:16 85-68-710/12/22 17:09562 237 1
4-Chloro-3-methylphenol ND ug/kg 10/14/22 15:16 59-50-710/12/22 17:091120 395 1
4-Chloroaniline ND ug/kg 10/14/22 15:16 106-47-810/12/22 17:091120 441 1
bis(2-Chloroethoxy)methane ND ug/kg 10/14/22 15:16 111-91-110/12/22 17:09562 233 1
bis(2-Chloroethyl) ether ND ug/kg 10/14/22 15:16 111-44-410/12/22 17:09562 211 1
2-Chloronaphthalene ND ug/kg 10/14/22 15:16 91-58-710/12/22 17:09562 223 1
2-Chlorophenol ND ug/kg 10/14/22 15:16 95-57-810/12/22 17:09562 211 1
4-Chlorophenylphenyl ether ND ug/kg 10/14/22 15:16 7005-72-310/12/22 17:09562 209 1
Chrysene ND ug/kg 10/14/22 15:16 218-01-910/12/22 17:09562 204 1
Dibenz(a,h)anthracene ND ug/kg 10/14/22 15:16 53-70-310/12/22 17:09562 216 1
Dibenzofuran ND ug/kg 10/14/22 15:16 132-64-910/12/22 17:09562 203 1
1,2-Dichlorobenzene ND ug/kg 10/14/22 15:16 95-50-110/12/22 17:09562 203 1
1,3-Dichlorobenzene ND ug/kg 10/14/22 15:16 541-73-110/12/22 17:09562 199 1
1,4-Dichlorobenzene ND ug/kg 10/14/22 15:16 106-46-710/12/22 17:09562 215 1
3,3'-Dichlorobenzidine ND ug/kg 10/14/22 15:16 91-94-110/12/22 17:091120 380 1
2,4-Dichlorophenol ND ug/kg 10/14/22 15:16 120-83-210/12/22 17:09562 220 1
Diethylphthalate ND ug/kg 10/14/22 15:16 84-66-210/12/22 17:09562 206 1
2,4-Dimethylphenol ND ug/kg 10/14/22 15:16 105-67-910/12/22 17:09562 233 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-D-DUP Lab ID: 92629052003 Collected: 10/03/22 15:35 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 10/14/22 15:16 131-11-310/12/22 17:09562 204 1
Di-n-butylphthalate ND ug/kg 10/14/22 15:16 84-74-210/12/22 17:09562 189 1
4,6-Dinitro-2-methylphenol ND ug/kg 10/14/22 15:16 534-52-110/12/22 17:091120 524 1
2,4-Dinitrophenol ND ug/kg 10/14/22 15:16 51-28-510/12/22 17:092810 1740 1
2,4-Dinitrotoluene ND ug/kg 10/14/22 15:16 121-14-210/12/22 17:09562 216 1
2,6-Dinitrotoluene ND ug/kg 10/14/22 15:16 606-20-210/12/22 17:09562 206 1
Di-n-octylphthalate ND ug/kg 10/14/22 15:16 117-84-010/12/22 17:09562 221 1
bis(2-Ethylhexyl)phthalate ND ug/kg 10/14/22 15:16 117-81-710/12/22 17:09562 218 1
Fluoranthene ND ug/kg 10/14/22 15:16 206-44-010/12/22 17:09562 192 1
Fluorene ND ug/kg 10/14/22 15:16 86-73-710/12/22 17:09562 198 1
Hexachloro-1,3-butadiene ND ug/kg 10/14/22 15:16 87-68-3 v110/12/22 17:09562 244 1
Hexachlorobenzene ND ug/kg 10/14/22 15:16 118-74-110/12/22 17:09562 220 1
Hexachlorocyclopentadiene ND ug/kg 10/14/22 15:16 77-47-410/12/22 17:09562 322 1
Hexachloroethane ND ug/kg 10/14/22 15:16 67-72-110/12/22 17:09562 215 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/14/22 15:16 193-39-510/12/22 17:09562 221 1
Isophorone ND ug/kg 10/14/22 15:16 78-59-110/12/22 17:09562 250 1
1-Methylnaphthalene ND ug/kg 10/14/22 15:16 90-12-010/12/22 17:09562 198 1
2-Methylnaphthalene ND ug/kg 10/14/22 15:16 91-57-610/12/22 17:09562 225 1
2-Methylphenol(o-Cresol)ND ug/kg 10/14/22 15:16 95-48-710/12/22 17:09562 230 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/14/22 15:16 15831-10-410/12/22 17:09562 226 1
Naphthalene ND ug/kg 10/14/22 15:16 91-20-310/12/22 17:09562 191 1
2-Nitroaniline ND ug/kg 10/14/22 15:16 88-74-410/12/22 17:092810 460 1
3-Nitroaniline ND ug/kg 10/14/22 15:16 99-09-210/12/22 17:092810 441 1
4-Nitroaniline ND ug/kg 10/14/22 15:16 100-01-610/12/22 17:091120 427 1
Nitrobenzene ND ug/kg 10/14/22 15:16 98-95-310/12/22 17:09562 261 1
2-Nitrophenol ND ug/kg 10/14/22 15:16 88-75-510/12/22 17:09562 244 1
4-Nitrophenol ND ug/kg 10/14/22 15:16 100-02-710/12/22 17:092810 1090 1
N-Nitrosodimethylamine ND ug/kg 10/14/22 15:16 62-75-910/12/22 17:09562 189 1
N-Nitroso-di-n-propylamine ND ug/kg 10/14/22 15:16 621-64-710/12/22 17:09562 211 1
N-Nitrosodiphenylamine ND ug/kg 10/14/22 15:16 86-30-610/12/22 17:09562 199 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/14/22 15:16 108-60-1 v210/12/22 17:09562 267 1
Pentachlorophenol ND ug/kg 10/14/22 15:16 87-86-510/12/22 17:091120 550 1
Phenanthrene ND ug/kg 10/14/22 15:16 85-01-810/12/22 17:09562 184 1
Phenol ND ug/kg 10/14/22 15:16 108-95-210/12/22 17:09562 250 1
Pyrene ND ug/kg 10/14/22 15:16 129-00-010/12/22 17:09562 228 1
Pyridine ND ug/kg 10/14/22 15:16 110-86-110/12/22 17:09562 177 1
1,2,4-Trichlorobenzene ND ug/kg 10/14/22 15:16 120-82-110/12/22 17:09562 221 1
2,4,5-Trichlorophenol ND ug/kg 10/14/22 15:16 95-95-410/12/22 17:09562 257 1
2,4,6-Trichlorophenol ND ug/kg 10/14/22 15:16 88-06-210/12/22 17:09562 232 1
Surrogates
Nitrobenzene-d5 (S)54 %10/14/22 15:16 4165-60-010/12/22 17:0910-130 1
2-Fluorobiphenyl (S)25 %10/14/22 15:16 321-60-810/12/22 17:0910-130 1
Terphenyl-d14 (S)27 %10/14/22 15:16 1718-51-010/12/22 17:0910-130 1
Phenol-d6 (S)43 %10/14/22 15:16 13127-88-310/12/22 17:0910-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-D-DUP Lab ID: 92629052003 Collected: 10/03/22 15:35 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)47 %10/14/22 15:16 367-12-410/12/22 17:0910-130 1
2,4,6-Tribromophenol (S)35 %10/14/22 15:16 118-79-610/12/22 17:0910-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 40.9 %10/04/22 17:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-A Lab ID: 92629052004 Collected: 10/03/22 16:30 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Ormond Beach
6010 MET ICP
Arsenic ND mg/kg 10/17/22 12:10 7440-38-2 D310/11/22 21:266.2 3.1 10
Barium 47.1 mg/kg 10/17/22 12:10 7440-39-310/11/22 21:266.2 1.0 10
Cadmium ND mg/kg 10/17/22 12:10 7440-43-9 D310/11/22 21:260.62 0.31 10
Chromium ND mg/kg 10/17/22 12:10 7440-47-3 D310/11/22 21:263.1 1.6 10
Lead 7.2 mg/kg 10/17/22 12:10 7439-92-110/11/22 21:266.2 3.1 10
Selenium ND mg/kg 10/17/22 12:10 7782-49-2 D310/11/22 21:269.3 4.7 10
Silver ND mg/kg 10/17/22 12:10 7440-22-4 D310/11/22 21:263.1 0.68 10
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
7471 Mercury
Mercury 0.014 mg/kg 10/13/22 09:42 7439-97-610/12/22 07:340.0095 0.0048 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 10/14/22 15:43 83-32-910/12/22 17:09384 135 1
Acenaphthylene ND ug/kg 10/14/22 15:43 208-96-810/12/22 17:09384 135 1
Aniline ND ug/kg 10/14/22 15:43 62-53-310/12/22 17:09384 150 1
Anthracene ND ug/kg 10/14/22 15:43 120-12-710/12/22 17:09384 126 1
Benzo(a)anthracene ND ug/kg 10/14/22 15:43 56-55-310/12/22 17:09384 128 1
Benzo(a)pyrene ND ug/kg 10/14/22 15:43 50-32-810/12/22 17:09384 133 1
Benzo(b)fluoranthene ND ug/kg 10/14/22 15:43 205-99-210/12/22 17:09384 128 1
Benzo(g,h,i)perylene ND ug/kg 10/14/22 15:43 191-24-210/12/22 17:09384 149 1
Benzo(k)fluoranthene ND ug/kg 10/14/22 15:43 207-08-910/12/22 17:09384 135 1
Benzoic Acid ND ug/kg 10/14/22 15:43 65-85-010/12/22 17:091920 825 1
Benzyl alcohol ND ug/kg 10/14/22 15:43 100-51-610/12/22 17:09768 291 1
4-Bromophenylphenyl ether ND ug/kg 10/14/22 15:43 101-55-310/12/22 17:09384 148 1
Butylbenzylphthalate ND ug/kg 10/14/22 15:43 85-68-710/12/22 17:09384 162 1
4-Chloro-3-methylphenol ND ug/kg 10/14/22 15:43 59-50-710/12/22 17:09768 270 1
4-Chloroaniline ND ug/kg 10/14/22 15:43 106-47-810/12/22 17:09768 301 1
bis(2-Chloroethoxy)methane ND ug/kg 10/14/22 15:43 111-91-110/12/22 17:09384 159 1
bis(2-Chloroethyl) ether ND ug/kg 10/14/22 15:43 111-44-410/12/22 17:09384 144 1
2-Chloronaphthalene ND ug/kg 10/14/22 15:43 91-58-710/12/22 17:09384 152 1
2-Chlorophenol ND ug/kg 10/14/22 15:43 95-57-810/12/22 17:09384 144 1
4-Chlorophenylphenyl ether ND ug/kg 10/14/22 15:43 7005-72-310/12/22 17:09384 143 1
Chrysene ND ug/kg 10/14/22 15:43 218-01-910/12/22 17:09384 140 1
Dibenz(a,h)anthracene ND ug/kg 10/14/22 15:43 53-70-310/12/22 17:09384 148 1
Dibenzofuran ND ug/kg 10/14/22 15:43 132-64-910/12/22 17:09384 138 1
1,2-Dichlorobenzene ND ug/kg 10/14/22 15:43 95-50-110/12/22 17:09384 138 1
1,3-Dichlorobenzene ND ug/kg 10/14/22 15:43 541-73-110/12/22 17:09384 136 1
1,4-Dichlorobenzene ND ug/kg 10/14/22 15:43 106-46-710/12/22 17:09384 147 1
3,3'-Dichlorobenzidine ND ug/kg 10/14/22 15:43 91-94-110/12/22 17:09768 259 1
2,4-Dichlorophenol ND ug/kg 10/14/22 15:43 120-83-210/12/22 17:09384 150 1
Diethylphthalate ND ug/kg 10/14/22 15:43 84-66-210/12/22 17:09384 141 1
2,4-Dimethylphenol ND ug/kg 10/14/22 15:43 105-67-910/12/22 17:09384 159 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-A Lab ID: 92629052004 Collected: 10/03/22 16:30 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 10/14/22 15:43 131-11-310/12/22 17:09384 140 1
Di-n-butylphthalate ND ug/kg 10/14/22 15:43 84-74-210/12/22 17:09384 129 1
4,6-Dinitro-2-methylphenol ND ug/kg 10/14/22 15:43 534-52-110/12/22 17:09768 358 1
2,4-Dinitrophenol ND ug/kg 10/14/22 15:43 51-28-510/12/22 17:091920 1190 1
2,4-Dinitrotoluene ND ug/kg 10/14/22 15:43 121-14-210/12/22 17:09384 148 1
2,6-Dinitrotoluene ND ug/kg 10/14/22 15:43 606-20-210/12/22 17:09384 141 1
Di-n-octylphthalate ND ug/kg 10/14/22 15:43 117-84-010/12/22 17:09384 151 1
bis(2-Ethylhexyl)phthalate ND ug/kg 10/14/22 15:43 117-81-710/12/22 17:09384 149 1
Fluoranthene ND ug/kg 10/14/22 15:43 206-44-010/12/22 17:09384 131 1
Fluorene ND ug/kg 10/14/22 15:43 86-73-710/12/22 17:09384 135 1
Hexachloro-1,3-butadiene ND ug/kg 10/14/22 15:43 87-68-3 v110/12/22 17:09384 166 1
Hexachlorobenzene ND ug/kg 10/14/22 15:43 118-74-110/12/22 17:09384 150 1
Hexachlorocyclopentadiene ND ug/kg 10/14/22 15:43 77-47-410/12/22 17:09384 220 1
Hexachloroethane ND ug/kg 10/14/22 15:43 67-72-110/12/22 17:09384 147 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/14/22 15:43 193-39-510/12/22 17:09384 151 1
Isophorone ND ug/kg 10/14/22 15:43 78-59-110/12/22 17:09384 171 1
1-Methylnaphthalene ND ug/kg 10/14/22 15:43 90-12-010/12/22 17:09384 135 1
2-Methylnaphthalene ND ug/kg 10/14/22 15:43 91-57-610/12/22 17:09384 154 1
2-Methylphenol(o-Cresol)ND ug/kg 10/14/22 15:43 95-48-710/12/22 17:09384 157 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/14/22 15:43 15831-10-410/12/22 17:09384 155 1
Naphthalene ND ug/kg 10/14/22 15:43 91-20-310/12/22 17:09384 130 1
2-Nitroaniline ND ug/kg 10/14/22 15:43 88-74-410/12/22 17:091920 314 1
3-Nitroaniline ND ug/kg 10/14/22 15:43 99-09-210/12/22 17:091920 301 1
4-Nitroaniline ND ug/kg 10/14/22 15:43 100-01-610/12/22 17:09768 292 1
Nitrobenzene ND ug/kg 10/14/22 15:43 98-95-310/12/22 17:09384 178 1
2-Nitrophenol ND ug/kg 10/14/22 15:43 88-75-510/12/22 17:09384 166 1
4-Nitrophenol ND ug/kg 10/14/22 15:43 100-02-710/12/22 17:091920 742 1
N-Nitrosodimethylamine ND ug/kg 10/14/22 15:43 62-75-910/12/22 17:09384 129 1
N-Nitroso-di-n-propylamine ND ug/kg 10/14/22 15:43 621-64-710/12/22 17:09384 144 1
N-Nitrosodiphenylamine ND ug/kg 10/14/22 15:43 86-30-610/12/22 17:09384 136 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/14/22 15:43 108-60-1 v210/12/22 17:09384 183 1
Pentachlorophenol ND ug/kg 10/14/22 15:43 87-86-510/12/22 17:09768 376 1
Phenanthrene ND ug/kg 10/14/22 15:43 85-01-810/12/22 17:09384 126 1
Phenol ND ug/kg 10/14/22 15:43 108-95-210/12/22 17:09384 171 1
Pyrene ND ug/kg 10/14/22 15:43 129-00-010/12/22 17:09384 156 1
Pyridine ND ug/kg 10/14/22 15:43 110-86-110/12/22 17:09384 121 1
1,2,4-Trichlorobenzene ND ug/kg 10/14/22 15:43 120-82-110/12/22 17:09384 151 1
2,4,5-Trichlorophenol ND ug/kg 10/14/22 15:43 95-95-410/12/22 17:09384 176 1
2,4,6-Trichlorophenol ND ug/kg 10/14/22 15:43 88-06-210/12/22 17:09384 158 1
Surrogates
Nitrobenzene-d5 (S)20 %10/14/22 15:43 4165-60-010/12/22 17:0910-130 1
2-Fluorobiphenyl (S)20 %10/14/22 15:43 321-60-810/12/22 17:0910-130 1
Terphenyl-d14 (S)27 %10/14/22 15:43 1718-51-010/12/22 17:0910-130 1
Phenol-d6 (S)17 %10/14/22 15:43 13127-88-310/12/22 17:0910-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-A Lab ID: 92629052004 Collected: 10/03/22 16:30 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)20 %10/14/22 15:43 367-12-410/12/22 17:0910-130 1
2,4,6-Tribromophenol (S)22 %10/14/22 15:43 118-79-610/12/22 17:0910-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.2 %10/04/22 17:35 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-B Lab ID: 92629052005 Collected: 10/03/22 17:20 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Pace Analytical Services - Ormond Beach
6010 MET ICP
Arsenic ND mg/kg 10/15/22 20:05 7440-38-210/11/22 21:260.61 0.31 1
Barium 34.0 mg/kg 10/15/22 20:05 7440-39-310/11/22 21:260.61 0.10 1
Cadmium 0.48 mg/kg 10/15/22 20:05 7440-43-910/11/22 21:260.061 0.031 1
Chromium 30.3 mg/kg 10/15/22 20:05 7440-47-310/11/22 21:260.31 0.15 1
Lead 8.0 mg/kg 10/15/22 20:05 7439-92-110/11/22 21:260.61 0.31 1
Selenium ND mg/kg 10/17/22 12:14 7782-49-2 D310/11/22 21:264.6 2.3 5
Silver ND mg/kg 10/17/22 12:14 7440-22-4 D310/11/22 21:261.5 0.34 5
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Pace Analytical Services - Ormond Beach
7471 Mercury
Mercury 0.019 mg/kg 10/13/22 09:44 7439-97-610/12/22 07:340.011 0.0056 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 10/14/22 16:11 83-32-910/12/22 17:09392 138 1
Acenaphthylene ND ug/kg 10/14/22 16:11 208-96-810/12/22 17:09392 138 1
Aniline ND ug/kg 10/14/22 16:11 62-53-310/12/22 17:09392 153 1
Anthracene ND ug/kg 10/14/22 16:11 120-12-710/12/22 17:09392 128 1
Benzo(a)anthracene ND ug/kg 10/14/22 16:11 56-55-310/12/22 17:09392 131 1
Benzo(a)pyrene ND ug/kg 10/14/22 16:11 50-32-810/12/22 17:09392 135 1
Benzo(b)fluoranthene ND ug/kg 10/14/22 16:11 205-99-210/12/22 17:09392 131 1
Benzo(g,h,i)perylene ND ug/kg 10/14/22 16:11 191-24-210/12/22 17:09392 152 1
Benzo(k)fluoranthene ND ug/kg 10/14/22 16:11 207-08-910/12/22 17:09392 138 1
Benzoic Acid ND ug/kg 10/14/22 16:11 65-85-010/12/22 17:091960 842 1
Benzyl alcohol ND ug/kg 10/14/22 16:11 100-51-610/12/22 17:09784 297 1
4-Bromophenylphenyl ether ND ug/kg 10/14/22 16:11 101-55-310/12/22 17:09392 151 1
Butylbenzylphthalate ND ug/kg 10/14/22 16:11 85-68-710/12/22 17:09392 165 1
4-Chloro-3-methylphenol ND ug/kg 10/14/22 16:11 59-50-710/12/22 17:09784 276 1
4-Chloroaniline ND ug/kg 10/14/22 16:11 106-47-810/12/22 17:09784 308 1
bis(2-Chloroethoxy)methane ND ug/kg 10/14/22 16:11 111-91-110/12/22 17:09392 163 1
bis(2-Chloroethyl) ether ND ug/kg 10/14/22 16:11 111-44-410/12/22 17:09392 147 1
2-Chloronaphthalene ND ug/kg 10/14/22 16:11 91-58-710/12/22 17:09392 156 1
2-Chlorophenol ND ug/kg 10/14/22 16:11 95-57-810/12/22 17:09392 147 1
4-Chlorophenylphenyl ether ND ug/kg 10/14/22 16:11 7005-72-310/12/22 17:09392 146 1
Chrysene ND ug/kg 10/14/22 16:11 218-01-910/12/22 17:09392 143 1
Dibenz(a,h)anthracene ND ug/kg 10/14/22 16:11 53-70-310/12/22 17:09392 151 1
Dibenzofuran ND ug/kg 10/14/22 16:11 132-64-910/12/22 17:09392 141 1
1,2-Dichlorobenzene ND ug/kg 10/14/22 16:11 95-50-110/12/22 17:09392 141 1
1,3-Dichlorobenzene ND ug/kg 10/14/22 16:11 541-73-110/12/22 17:09392 139 1
1,4-Dichlorobenzene ND ug/kg 10/14/22 16:11 106-46-710/12/22 17:09392 150 1
3,3'-Dichlorobenzidine ND ug/kg 10/14/22 16:11 91-94-110/12/22 17:09784 265 1
2,4-Dichlorophenol ND ug/kg 10/14/22 16:11 120-83-210/12/22 17:09392 153 1
Diethylphthalate ND ug/kg 10/14/22 16:11 84-66-210/12/22 17:09392 144 1
2,4-Dimethylphenol ND ug/kg 10/14/22 16:11 105-67-910/12/22 17:09392 163 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-B Lab ID: 92629052005 Collected: 10/03/22 17:20 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 10/14/22 16:11 131-11-310/12/22 17:09392 143 1
Di-n-butylphthalate ND ug/kg 10/14/22 16:11 84-74-210/12/22 17:09392 132 1
4,6-Dinitro-2-methylphenol ND ug/kg 10/14/22 16:11 534-52-110/12/22 17:09784 366 1
2,4-Dinitrophenol ND ug/kg 10/14/22 16:11 51-28-510/12/22 17:091960 1210 1
2,4-Dinitrotoluene ND ug/kg 10/14/22 16:11 121-14-210/12/22 17:09392 151 1
2,6-Dinitrotoluene ND ug/kg 10/14/22 16:11 606-20-210/12/22 17:09392 144 1
Di-n-octylphthalate ND ug/kg 10/14/22 16:11 117-84-010/12/22 17:09392 154 1
bis(2-Ethylhexyl)phthalate ND ug/kg 10/14/22 16:11 117-81-710/12/22 17:09392 152 1
Fluoranthene ND ug/kg 10/14/22 16:11 206-44-010/12/22 17:09392 134 1
Fluorene ND ug/kg 10/14/22 16:11 86-73-710/12/22 17:09392 138 1
Hexachloro-1,3-butadiene ND ug/kg 10/14/22 16:11 87-68-3 v110/12/22 17:09392 170 1
Hexachlorobenzene ND ug/kg 10/14/22 16:11 118-74-110/12/22 17:09392 153 1
Hexachlorocyclopentadiene ND ug/kg 10/14/22 16:11 77-47-410/12/22 17:09392 225 1
Hexachloroethane ND ug/kg 10/14/22 16:11 67-72-110/12/22 17:09392 150 1
Indeno(1,2,3-cd)pyrene ND ug/kg 10/14/22 16:11 193-39-510/12/22 17:09392 154 1
Isophorone ND ug/kg 10/14/22 16:11 78-59-110/12/22 17:09392 175 1
1-Methylnaphthalene ND ug/kg 10/14/22 16:11 90-12-010/12/22 17:09392 138 1
2-Methylnaphthalene ND ug/kg 10/14/22 16:11 91-57-610/12/22 17:09392 157 1
2-Methylphenol(o-Cresol)ND ug/kg 10/14/22 16:11 95-48-710/12/22 17:09392 160 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 10/14/22 16:11 15831-10-410/12/22 17:09392 158 1
Naphthalene ND ug/kg 10/14/22 16:11 91-20-310/12/22 17:09392 133 1
2-Nitroaniline ND ug/kg 10/14/22 16:11 88-74-410/12/22 17:091960 321 1
3-Nitroaniline ND ug/kg 10/14/22 16:11 99-09-210/12/22 17:091960 308 1
4-Nitroaniline ND ug/kg 10/14/22 16:11 100-01-610/12/22 17:09784 298 1
Nitrobenzene ND ug/kg 10/14/22 16:11 98-95-310/12/22 17:09392 182 1
2-Nitrophenol ND ug/kg 10/14/22 16:11 88-75-510/12/22 17:09392 170 1
4-Nitrophenol ND ug/kg 10/14/22 16:11 100-02-710/12/22 17:091960 758 1
N-Nitrosodimethylamine ND ug/kg 10/14/22 16:11 62-75-910/12/22 17:09392 132 1
N-Nitroso-di-n-propylamine ND ug/kg 10/14/22 16:11 621-64-710/12/22 17:09392 147 1
N-Nitrosodiphenylamine ND ug/kg 10/14/22 16:11 86-30-610/12/22 17:09392 139 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 10/14/22 16:11 108-60-1 v210/12/22 17:09392 187 1
Pentachlorophenol ND ug/kg 10/14/22 16:11 87-86-510/12/22 17:09784 384 1
Phenanthrene ND ug/kg 10/14/22 16:11 85-01-810/12/22 17:09392 128 1
Phenol ND ug/kg 10/14/22 16:11 108-95-210/12/22 17:09392 175 1
Pyrene ND ug/kg 10/14/22 16:11 129-00-010/12/22 17:09392 159 1
Pyridine ND ug/kg 10/14/22 16:11 110-86-110/12/22 17:09392 124 1
1,2,4-Trichlorobenzene ND ug/kg 10/14/22 16:11 120-82-110/12/22 17:09392 154 1
2,4,5-Trichlorophenol ND ug/kg 10/14/22 16:11 95-95-410/12/22 17:09392 179 1
2,4,6-Trichlorophenol ND ug/kg 10/14/22 16:11 88-06-210/12/22 17:09392 162 1
Surrogates
Nitrobenzene-d5 (S)27 %10/14/22 16:11 4165-60-010/12/22 17:0910-130 1
2-Fluorobiphenyl (S)26 %10/14/22 16:11 321-60-810/12/22 17:0910-130 1
Terphenyl-d14 (S)32 %10/14/22 16:11 1718-51-010/12/22 17:0910-130 1
Phenol-d6 (S)24 %10/14/22 16:11 13127-88-310/12/22 17:0910-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-B Lab ID: 92629052005 Collected: 10/03/22 17:20 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)24 %10/14/22 16:11 367-12-410/12/22 17:0910-130 1
2,4,6-Tribromophenol (S)30 %10/14/22 16:11 118-79-610/12/22 17:0910-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.7 %10/04/22 17:36 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-3C Lab ID: 92629052006 Collected: 10/03/22 13:00 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 10/04/22 20:01 67-64-110/04/22 16:34154 49.5 1
Benzene ND ug/kg 10/04/22 20:01 71-43-210/04/22 16:347.7 3.1 1
Bromobenzene ND ug/kg 10/04/22 20:01 108-86-110/04/22 16:347.7 2.5 1
Bromochloromethane ND ug/kg 10/04/22 20:01 74-97-510/04/22 16:347.7 2.3 1
Bromodichloromethane ND ug/kg 10/04/22 20:01 75-27-410/04/22 16:347.7 3.0 1
Bromoform ND ug/kg 10/04/22 20:01 75-25-210/04/22 16:347.7 2.7 1
Bromomethane ND ug/kg 10/04/22 20:01 74-83-9 v210/04/22 16:3415.4 12.2 1
2-Butanone (MEK)ND ug/kg 10/04/22 20:01 78-93-310/04/22 16:34154 37.0 1
n-Butylbenzene ND ug/kg 10/04/22 20:01 104-51-810/04/22 16:347.7 3.6 1
sec-Butylbenzene ND ug/kg 10/04/22 20:01 135-98-810/04/22 16:347.7 3.4 1
tert-Butylbenzene ND ug/kg 10/04/22 20:01 98-06-610/04/22 16:347.7 2.7 1
Carbon tetrachloride ND ug/kg 10/04/22 20:01 56-23-510/04/22 16:347.7 2.9 1
Chlorobenzene ND ug/kg 10/04/22 20:01 108-90-710/04/22 16:347.7 1.5 1
Chloroethane ND ug/kg 10/04/22 20:01 75-00-310/04/22 16:3415.4 6.0 1
Chloroform ND ug/kg 10/04/22 20:01 67-66-310/04/22 16:347.7 4.7 1
Chloromethane ND ug/kg 10/04/22 20:01 74-87-310/04/22 16:3415.4 6.5 1
2-Chlorotoluene ND ug/kg 10/04/22 20:01 95-49-810/04/22 16:347.7 2.7 1
4-Chlorotoluene ND ug/kg 10/04/22 20:01 106-43-410/04/22 16:347.7 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/04/22 20:01 96-12-810/04/22 16:347.7 3.0 1
Dibromochloromethane ND ug/kg 10/04/22 20:01 124-48-110/04/22 16:347.7 4.3 1
1,2-Dibromoethane (EDB)ND ug/kg 10/04/22 20:01 106-93-410/04/22 16:347.7 3.4 1
Dibromomethane ND ug/kg 10/04/22 20:01 74-95-310/04/22 16:347.7 1.7 1
1,2-Dichlorobenzene ND ug/kg 10/04/22 20:01 95-50-110/04/22 16:347.7 2.8 1
1,3-Dichlorobenzene ND ug/kg 10/04/22 20:01 541-73-110/04/22 16:347.7 2.4 1
1,4-Dichlorobenzene ND ug/kg 10/04/22 20:01 106-46-710/04/22 16:347.7 2.0 1
Dichlorodifluoromethane ND ug/kg 10/04/22 20:01 75-71-810/04/22 16:3415.4 3.3 1
1,1-Dichloroethane ND ug/kg 10/04/22 20:01 75-34-310/04/22 16:347.7 3.2 1
1,2-Dichloroethane ND ug/kg 10/04/22 20:01 107-06-210/04/22 16:347.7 5.1 1
1,1-Dichloroethene ND ug/kg 10/04/22 20:01 75-35-410/04/22 16:347.7 3.2 1
cis-1,2-Dichloroethene ND ug/kg 10/04/22 20:01 156-59-210/04/22 16:347.7 2.6 1
trans-1,2-Dichloroethene ND ug/kg 10/04/22 20:01 156-60-510/04/22 16:347.7 2.7 1
1,2-Dichloropropane ND ug/kg 10/04/22 20:01 78-87-510/04/22 16:347.7 2.3 1
1,3-Dichloropropane ND ug/kg 10/04/22 20:01 142-28-910/04/22 16:347.7 2.4 1
2,2-Dichloropropane ND ug/kg 10/04/22 20:01 594-20-7 v210/04/22 16:347.7 2.5 1
1,1-Dichloropropene ND ug/kg 10/04/22 20:01 563-58-610/04/22 16:347.7 3.7 1
cis-1,3-Dichloropropene ND ug/kg 10/04/22 20:01 10061-01-510/04/22 16:347.7 2.1 1
trans-1,3-Dichloropropene ND ug/kg 10/04/22 20:01 10061-02-610/04/22 16:347.7 2.7 1
Diisopropyl ether ND ug/kg 10/04/22 20:01 108-20-310/04/22 16:347.7 2.1 1
Ethylbenzene ND ug/kg 10/04/22 20:01 100-41-410/04/22 16:347.7 3.6 1
Hexachloro-1,3-butadiene ND ug/kg 10/04/22 20:01 87-68-3 v210/04/22 16:3415.4 12.6 1
2-Hexanone ND ug/kg 10/04/22 20:01 591-78-610/04/22 16:3477.2 7.4 1
Isopropylbenzene (Cumene)ND ug/kg 10/04/22 20:01 98-82-810/04/22 16:347.7 2.6 1
p-Isopropyltoluene ND ug/kg 10/04/22 20:01 99-87-610/04/22 16:347.7 3.8 1
Methylene Chloride ND ug/kg 10/04/22 20:01 75-09-2 v210/04/22 16:3430.9 21.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-3C Lab ID: 92629052006 Collected: 10/03/22 13:00 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/04/22 20:01 108-10-110/04/22 16:3477.2 7.4 1
Methyl-tert-butyl ether ND ug/kg 10/04/22 20:01 1634-04-410/04/22 16:347.7 2.9 1
Naphthalene ND ug/kg 10/04/22 20:01 91-20-310/04/22 16:347.7 4.1 1
n-Propylbenzene ND ug/kg 10/04/22 20:01 103-65-110/04/22 16:347.7 2.7 1
Styrene ND ug/kg 10/04/22 20:01 100-42-510/04/22 16:347.7 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/04/22 20:01 630-20-610/04/22 16:347.7 3.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/04/22 20:01 79-34-510/04/22 16:347.7 2.0 1
Tetrachloroethene ND ug/kg 10/04/22 20:01 127-18-410/04/22 16:347.7 2.4 1
Toluene ND ug/kg 10/04/22 20:01 108-88-310/04/22 16:347.7 2.2 1
1,2,3-Trichlorobenzene ND ug/kg 10/04/22 20:01 87-61-610/04/22 16:347.7 6.2 1
1,2,4-Trichlorobenzene ND ug/kg 10/04/22 20:01 120-82-110/04/22 16:347.7 6.5 1
1,1,1-Trichloroethane ND ug/kg 10/04/22 20:01 71-55-610/04/22 16:347.7 4.0 1
1,1,2-Trichloroethane ND ug/kg 10/04/22 20:01 79-00-510/04/22 16:347.7 2.6 1
Trichloroethene ND ug/kg 10/04/22 20:01 79-01-610/04/22 16:347.7 2.0 1
Trichlorofluoromethane ND ug/kg 10/04/22 20:01 75-69-410/04/22 16:347.7 4.2 1
1,2,3-Trichloropropane ND ug/kg 10/04/22 20:01 96-18-410/04/22 16:347.7 3.9 1
1,2,4-Trimethylbenzene ND ug/kg 10/04/22 20:01 95-63-610/04/22 16:347.7 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 10/04/22 20:01 108-67-810/04/22 16:347.7 2.6 1
Vinyl acetate ND ug/kg 10/04/22 20:01 108-05-410/04/22 16:3477.2 5.6 1
Vinyl chloride ND ug/kg 10/04/22 20:01 75-01-410/04/22 16:3415.4 3.9 1
Xylene (Total)ND ug/kg 10/04/22 20:01 1330-20-710/04/22 16:3415.4 4.4 1
m&p-Xylene ND ug/kg 10/04/22 20:01 179601-23-110/04/22 16:3415.4 5.3 1
o-Xylene 4.3J ug/kg 10/04/22 20:01 95-47-610/04/22 16:347.7 3.4 1
Surrogates
Toluene-d8 (S)99 %10/04/22 20:01 2037-26-510/04/22 16:3470-130 1
4-Bromofluorobenzene (S)101 %10/04/22 20:01 460-00-410/04/22 16:3470-130 1
1,2-Dichloroethane-d4 (S)94 %10/04/22 20:01 17060-07-010/04/22 16:3470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.9 %10/04/22 17:36 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-5D Lab ID: 92629052007 Collected: 10/03/22 15:30 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 2570 ug/kg 10/04/22 20:18 67-64-1 C710/04/22 16:34153 49.1 1
Benzene ND ug/kg 10/04/22 20:18 71-43-210/04/22 16:347.7 3.0 1
Bromobenzene ND ug/kg 10/04/22 20:18 108-86-110/04/22 16:347.7 2.5 1
Bromochloromethane ND ug/kg 10/04/22 20:18 74-97-510/04/22 16:347.7 2.3 1
Bromodichloromethane ND ug/kg 10/04/22 20:18 75-27-410/04/22 16:347.7 3.0 1
Bromoform ND ug/kg 10/04/22 20:18 75-25-210/04/22 16:347.7 2.7 1
Bromomethane ND ug/kg 10/04/22 20:18 74-83-9 v210/04/22 16:3415.3 12.1 1
2-Butanone (MEK)240 ug/kg 10/04/22 20:18 78-93-3 C710/04/22 16:34153 36.7 1
n-Butylbenzene 177 ug/kg 10/04/22 20:18 104-51-810/04/22 16:347.7 3.6 1
sec-Butylbenzene ND ug/kg 10/04/22 20:18 135-98-810/04/22 16:347.7 3.4 1
tert-Butylbenzene ND ug/kg 10/04/22 20:18 98-06-610/04/22 16:347.7 2.7 1
Carbon tetrachloride ND ug/kg 10/04/22 20:18 56-23-510/04/22 16:347.7 2.9 1
Chlorobenzene ND ug/kg 10/04/22 20:18 108-90-710/04/22 16:347.7 1.5 1
Chloroethane ND ug/kg 10/04/22 20:18 75-00-310/04/22 16:3415.3 5.9 1
Chloroform ND ug/kg 10/04/22 20:18 67-66-310/04/22 16:347.7 4.7 1
Chloromethane ND ug/kg 10/04/22 20:18 74-87-310/04/22 16:3415.3 6.4 1
2-Chlorotoluene ND ug/kg 10/04/22 20:18 95-49-810/04/22 16:347.7 2.7 1
4-Chlorotoluene ND ug/kg 10/04/22 20:18 106-43-410/04/22 16:347.7 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/04/22 20:18 96-12-810/04/22 16:347.7 3.0 1
Dibromochloromethane ND ug/kg 10/04/22 20:18 124-48-110/04/22 16:347.7 4.3 1
1,2-Dibromoethane (EDB)ND ug/kg 10/04/22 20:18 106-93-410/04/22 16:347.7 3.4 1
Dibromomethane ND ug/kg 10/04/22 20:18 74-95-310/04/22 16:347.7 1.6 1
1,2-Dichlorobenzene ND ug/kg 10/04/22 20:18 95-50-110/04/22 16:347.7 2.8 1
1,3-Dichlorobenzene ND ug/kg 10/04/22 20:18 541-73-110/04/22 16:347.7 2.4 1
1,4-Dichlorobenzene ND ug/kg 10/04/22 20:18 106-46-710/04/22 16:347.7 2.0 1
Dichlorodifluoromethane ND ug/kg 10/04/22 20:18 75-71-810/04/22 16:3415.3 3.3 1
1,1-Dichloroethane ND ug/kg 10/04/22 20:18 75-34-310/04/22 16:347.7 3.2 1
1,2-Dichloroethane ND ug/kg 10/04/22 20:18 107-06-210/04/22 16:347.7 5.1 1
1,1-Dichloroethene ND ug/kg 10/04/22 20:18 75-35-410/04/22 16:347.7 3.2 1
cis-1,2-Dichloroethene ND ug/kg 10/04/22 20:18 156-59-210/04/22 16:347.7 2.6 1
trans-1,2-Dichloroethene ND ug/kg 10/04/22 20:18 156-60-510/04/22 16:347.7 2.7 1
1,2-Dichloropropane ND ug/kg 10/04/22 20:18 78-87-510/04/22 16:347.7 2.3 1
1,3-Dichloropropane ND ug/kg 10/04/22 20:18 142-28-910/04/22 16:347.7 2.4 1
2,2-Dichloropropane ND ug/kg 10/04/22 20:18 594-20-7 v210/04/22 16:347.7 2.5 1
1,1-Dichloropropene ND ug/kg 10/04/22 20:18 563-58-610/04/22 16:347.7 3.7 1
cis-1,3-Dichloropropene ND ug/kg 10/04/22 20:18 10061-01-510/04/22 16:347.7 2.1 1
trans-1,3-Dichloropropene ND ug/kg 10/04/22 20:18 10061-02-610/04/22 16:347.7 2.6 1
Diisopropyl ether ND ug/kg 10/04/22 20:18 108-20-310/04/22 16:347.7 2.1 1
Ethylbenzene ND ug/kg 10/04/22 20:18 100-41-410/04/22 16:347.7 3.6 1
Hexachloro-1,3-butadiene ND ug/kg 10/04/22 20:18 87-68-3 v210/04/22 16:3415.3 12.5 1
2-Hexanone ND ug/kg 10/04/22 20:18 591-78-610/04/22 16:3476.5 7.4 1
Isopropylbenzene (Cumene)ND ug/kg 10/04/22 20:18 98-82-810/04/22 16:347.7 2.6 1
p-Isopropyltoluene 375 ug/kg 10/04/22 20:18 99-87-610/04/22 16:347.7 3.8 1
Methylene Chloride ND ug/kg 10/04/22 20:18 75-09-2 v210/04/22 16:3430.6 21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-5D Lab ID: 92629052007 Collected: 10/03/22 15:30 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/04/22 20:18 108-10-110/04/22 16:3476.5 7.4 1
Methyl-tert-butyl ether ND ug/kg 10/04/22 20:18 1634-04-410/04/22 16:347.7 2.9 1
Naphthalene ND ug/kg 10/04/22 20:18 91-20-310/04/22 16:347.7 4.0 1
n-Propylbenzene ND ug/kg 10/04/22 20:18 103-65-110/04/22 16:347.7 2.7 1
Styrene ND ug/kg 10/04/22 20:18 100-42-510/04/22 16:347.7 2.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/04/22 20:18 630-20-610/04/22 16:347.7 2.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/04/22 20:18 79-34-510/04/22 16:347.7 2.0 1
Tetrachloroethene ND ug/kg 10/04/22 20:18 127-18-410/04/22 16:347.7 2.4 1
Toluene ND ug/kg 10/04/22 20:18 108-88-310/04/22 16:347.7 2.2 1
1,2,3-Trichlorobenzene ND ug/kg 10/04/22 20:18 87-61-610/04/22 16:347.7 6.2 1
1,2,4-Trichlorobenzene ND ug/kg 10/04/22 20:18 120-82-110/04/22 16:347.7 6.4 1
1,1,1-Trichloroethane ND ug/kg 10/04/22 20:18 71-55-610/04/22 16:347.7 4.0 1
1,1,2-Trichloroethane ND ug/kg 10/04/22 20:18 79-00-510/04/22 16:347.7 2.5 1
Trichloroethene ND ug/kg 10/04/22 20:18 79-01-610/04/22 16:347.7 2.0 1
Trichlorofluoromethane ND ug/kg 10/04/22 20:18 75-69-410/04/22 16:347.7 4.2 1
1,2,3-Trichloropropane ND ug/kg 10/04/22 20:18 96-18-410/04/22 16:347.7 3.9 1
1,2,4-Trimethylbenzene ND ug/kg 10/04/22 20:18 95-63-610/04/22 16:347.7 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 10/04/22 20:18 108-67-810/04/22 16:347.7 2.6 1
Vinyl acetate ND ug/kg 10/04/22 20:18 108-05-410/04/22 16:3476.5 5.6 1
Vinyl chloride ND ug/kg 10/04/22 20:18 75-01-410/04/22 16:3415.3 3.9 1
Xylene (Total)ND ug/kg 10/04/22 20:18 1330-20-710/04/22 16:3415.3 4.4 1
m&p-Xylene ND ug/kg 10/04/22 20:18 179601-23-110/04/22 16:3415.3 5.2 1
o-Xylene ND ug/kg 10/04/22 20:18 95-47-610/04/22 16:347.7 3.4 1
Surrogates
Toluene-d8 (S)98 %10/04/22 20:18 2037-26-510/04/22 16:3470-130 1
4-Bromofluorobenzene (S)100 %10/04/22 20:18 460-00-410/04/22 16:3470-130 1
1,2-Dichloroethane-d4 (S)96 %10/04/22 20:18 17060-07-010/04/22 16:3470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.6 %10/04/22 17:36 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-5D-DUP Lab ID: 92629052008 Collected: 10/03/22 15:35 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 1990 ug/kg 10/04/22 20:35 67-64-1 C710/04/22 16:34174 56.0 1
Benzene ND ug/kg 10/04/22 20:35 71-43-210/04/22 16:348.7 3.5 1
Bromobenzene ND ug/kg 10/04/22 20:35 108-86-110/04/22 16:348.7 2.8 1
Bromochloromethane ND ug/kg 10/04/22 20:35 74-97-510/04/22 16:348.7 2.6 1
Bromodichloromethane ND ug/kg 10/04/22 20:35 75-27-410/04/22 16:348.7 3.4 1
Bromoform ND ug/kg 10/04/22 20:35 75-25-210/04/22 16:348.7 3.1 1
Bromomethane ND ug/kg 10/04/22 20:35 74-83-9 v210/04/22 16:3417.4 13.8 1
2-Butanone (MEK)182 ug/kg 10/04/22 20:35 78-93-3 C710/04/22 16:34174 41.8 1
n-Butylbenzene 104 ug/kg 10/04/22 20:35 104-51-810/04/22 16:348.7 4.1 1
sec-Butylbenzene ND ug/kg 10/04/22 20:35 135-98-810/04/22 16:348.7 3.8 1
tert-Butylbenzene ND ug/kg 10/04/22 20:35 98-06-610/04/22 16:348.7 3.1 1
Carbon tetrachloride ND ug/kg 10/04/22 20:35 56-23-510/04/22 16:348.7 3.3 1
Chlorobenzene ND ug/kg 10/04/22 20:35 108-90-710/04/22 16:348.7 1.7 1
Chloroethane ND ug/kg 10/04/22 20:35 75-00-310/04/22 16:3417.4 6.7 1
Chloroform ND ug/kg 10/04/22 20:35 67-66-310/04/22 16:348.7 5.3 1
Chloromethane ND ug/kg 10/04/22 20:35 74-87-310/04/22 16:3417.4 7.3 1
2-Chlorotoluene ND ug/kg 10/04/22 20:35 95-49-810/04/22 16:348.7 3.1 1
4-Chlorotoluene ND ug/kg 10/04/22 20:35 106-43-410/04/22 16:348.7 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/04/22 20:35 96-12-810/04/22 16:348.7 3.4 1
Dibromochloromethane ND ug/kg 10/04/22 20:35 124-48-110/04/22 16:348.7 4.9 1
1,2-Dibromoethane (EDB)ND ug/kg 10/04/22 20:35 106-93-410/04/22 16:348.7 3.8 1
Dibromomethane ND ug/kg 10/04/22 20:35 74-95-310/04/22 16:348.7 1.9 1
1,2-Dichlorobenzene ND ug/kg 10/04/22 20:35 95-50-110/04/22 16:348.7 3.1 1
1,3-Dichlorobenzene ND ug/kg 10/04/22 20:35 541-73-110/04/22 16:348.7 2.7 1
1,4-Dichlorobenzene ND ug/kg 10/04/22 20:35 106-46-710/04/22 16:348.7 2.3 1
Dichlorodifluoromethane ND ug/kg 10/04/22 20:35 75-71-810/04/22 16:3417.4 3.8 1
1,1-Dichloroethane ND ug/kg 10/04/22 20:35 75-34-310/04/22 16:348.7 3.6 1
1,2-Dichloroethane ND ug/kg 10/04/22 20:35 107-06-210/04/22 16:348.7 5.8 1
1,1-Dichloroethene ND ug/kg 10/04/22 20:35 75-35-410/04/22 16:348.7 3.6 1
cis-1,2-Dichloroethene ND ug/kg 10/04/22 20:35 156-59-210/04/22 16:348.7 3.0 1
trans-1,2-Dichloroethene ND ug/kg 10/04/22 20:35 156-60-510/04/22 16:348.7 3.1 1
1,2-Dichloropropane ND ug/kg 10/04/22 20:35 78-87-510/04/22 16:348.7 2.6 1
1,3-Dichloropropane ND ug/kg 10/04/22 20:35 142-28-910/04/22 16:348.7 2.7 1
2,2-Dichloropropane ND ug/kg 10/04/22 20:35 594-20-7 v210/04/22 16:348.7 2.8 1
1,1-Dichloropropene ND ug/kg 10/04/22 20:35 563-58-610/04/22 16:348.7 4.2 1
cis-1,3-Dichloropropene ND ug/kg 10/04/22 20:35 10061-01-510/04/22 16:348.7 2.4 1
trans-1,3-Dichloropropene ND ug/kg 10/04/22 20:35 10061-02-610/04/22 16:348.7 3.0 1
Diisopropyl ether ND ug/kg 10/04/22 20:35 108-20-310/04/22 16:348.7 2.4 1
Ethylbenzene ND ug/kg 10/04/22 20:35 100-41-410/04/22 16:348.7 4.1 1
Hexachloro-1,3-butadiene ND ug/kg 10/04/22 20:35 87-68-3 v210/04/22 16:3417.4 14.3 1
2-Hexanone ND ug/kg 10/04/22 20:35 591-78-610/04/22 16:3487.2 8.4 1
Isopropylbenzene (Cumene)ND ug/kg 10/04/22 20:35 98-82-810/04/22 16:348.7 3.0 1
p-Isopropyltoluene 277 ug/kg 10/04/22 20:35 99-87-610/04/22 16:348.7 4.3 1
Methylene Chloride ND ug/kg 10/04/22 20:35 75-09-2 v210/04/22 16:3434.9 23.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-5D-DUP Lab ID: 92629052008 Collected: 10/03/22 15:35 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/04/22 20:35 108-10-110/04/22 16:3487.2 8.4 1
Methyl-tert-butyl ether ND ug/kg 10/04/22 20:35 1634-04-410/04/22 16:348.7 3.3 1
Naphthalene ND ug/kg 10/04/22 20:35 91-20-310/04/22 16:348.7 4.6 1
n-Propylbenzene ND ug/kg 10/04/22 20:35 103-65-110/04/22 16:348.7 3.1 1
Styrene ND ug/kg 10/04/22 20:35 100-42-510/04/22 16:348.7 2.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/04/22 20:35 630-20-610/04/22 16:348.7 3.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/04/22 20:35 79-34-510/04/22 16:348.7 2.3 1
Tetrachloroethene ND ug/kg 10/04/22 20:35 127-18-410/04/22 16:348.7 2.8 1
Toluene ND ug/kg 10/04/22 20:35 108-88-310/04/22 16:348.7 2.5 1
1,2,3-Trichlorobenzene ND ug/kg 10/04/22 20:35 87-61-610/04/22 16:348.7 7.0 1
1,2,4-Trichlorobenzene ND ug/kg 10/04/22 20:35 120-82-110/04/22 16:348.7 7.3 1
1,1,1-Trichloroethane ND ug/kg 10/04/22 20:35 71-55-610/04/22 16:348.7 4.5 1
1,1,2-Trichloroethane ND ug/kg 10/04/22 20:35 79-00-510/04/22 16:348.7 2.9 1
Trichloroethene ND ug/kg 10/04/22 20:35 79-01-610/04/22 16:348.7 2.2 1
Trichlorofluoromethane ND ug/kg 10/04/22 20:35 75-69-410/04/22 16:348.7 4.8 1
1,2,3-Trichloropropane ND ug/kg 10/04/22 20:35 96-18-410/04/22 16:348.7 4.4 1
1,2,4-Trimethylbenzene ND ug/kg 10/04/22 20:35 95-63-610/04/22 16:348.7 2.4 1
1,3,5-Trimethylbenzene ND ug/kg 10/04/22 20:35 108-67-810/04/22 16:348.7 2.9 1
Vinyl acetate ND ug/kg 10/04/22 20:35 108-05-410/04/22 16:3487.2 6.3 1
Vinyl chloride ND ug/kg 10/04/22 20:35 75-01-410/04/22 16:3417.4 4.4 1
Xylene (Total)ND ug/kg 10/04/22 20:35 1330-20-710/04/22 16:3417.4 5.0 1
m&p-Xylene ND ug/kg 10/04/22 20:35 179601-23-110/04/22 16:3417.4 6.0 1
o-Xylene ND ug/kg 10/04/22 20:35 95-47-610/04/22 16:348.7 3.9 1
Surrogates
Toluene-d8 (S)99 %10/04/22 20:35 2037-26-510/04/22 16:3470-130 1
4-Bromofluorobenzene (S)99 %10/04/22 20:35 460-00-410/04/22 16:3470-130 1
1,2-Dichloroethane-d4 (S)91 %10/04/22 20:35 17060-07-010/04/22 16:3470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.7 %10/04/22 17:36 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-3A Lab ID: 92629052009 Collected: 10/03/22 16:35 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 10/04/22 20:53 67-64-110/04/22 16:34177 56.9 1
Benzene ND ug/kg 10/04/22 20:53 71-43-210/04/22 16:348.9 3.5 1
Bromobenzene ND ug/kg 10/04/22 20:53 108-86-110/04/22 16:348.9 2.9 1
Bromochloromethane ND ug/kg 10/04/22 20:53 74-97-510/04/22 16:348.9 2.6 1
Bromodichloromethane ND ug/kg 10/04/22 20:53 75-27-410/04/22 16:348.9 3.4 1
Bromoform ND ug/kg 10/04/22 20:53 75-25-210/04/22 16:348.9 3.1 1
Bromomethane ND ug/kg 10/04/22 20:53 74-83-9 v210/04/22 16:3417.7 14.0 1
2-Butanone (MEK)ND ug/kg 10/04/22 20:53 78-93-310/04/22 16:34177 42.6 1
n-Butylbenzene ND ug/kg 10/04/22 20:53 104-51-810/04/22 16:348.9 4.2 1
sec-Butylbenzene ND ug/kg 10/04/22 20:53 135-98-810/04/22 16:348.9 3.9 1
tert-Butylbenzene ND ug/kg 10/04/22 20:53 98-06-610/04/22 16:348.9 3.2 1
Carbon tetrachloride ND ug/kg 10/04/22 20:53 56-23-510/04/22 16:348.9 3.3 1
Chlorobenzene ND ug/kg 10/04/22 20:53 108-90-710/04/22 16:348.9 1.7 1
Chloroethane ND ug/kg 10/04/22 20:53 75-00-310/04/22 16:3417.7 6.8 1
Chloroform ND ug/kg 10/04/22 20:53 67-66-310/04/22 16:348.9 5.4 1
Chloromethane ND ug/kg 10/04/22 20:53 74-87-310/04/22 16:3417.7 7.4 1
2-Chlorotoluene ND ug/kg 10/04/22 20:53 95-49-810/04/22 16:348.9 3.1 1
4-Chlorotoluene ND ug/kg 10/04/22 20:53 106-43-410/04/22 16:348.9 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/04/22 20:53 96-12-810/04/22 16:348.9 3.4 1
Dibromochloromethane ND ug/kg 10/04/22 20:53 124-48-110/04/22 16:348.9 5.0 1
1,2-Dibromoethane (EDB)ND ug/kg 10/04/22 20:53 106-93-410/04/22 16:348.9 3.9 1
Dibromomethane ND ug/kg 10/04/22 20:53 74-95-310/04/22 16:348.9 1.9 1
1,2-Dichlorobenzene ND ug/kg 10/04/22 20:53 95-50-110/04/22 16:348.9 3.2 1
1,3-Dichlorobenzene ND ug/kg 10/04/22 20:53 541-73-110/04/22 16:348.9 2.7 1
1,4-Dichlorobenzene ND ug/kg 10/04/22 20:53 106-46-710/04/22 16:348.9 2.3 1
Dichlorodifluoromethane ND ug/kg 10/04/22 20:53 75-71-810/04/22 16:3417.7 3.8 1
1,1-Dichloroethane ND ug/kg 10/04/22 20:53 75-34-310/04/22 16:348.9 3.7 1
1,2-Dichloroethane ND ug/kg 10/04/22 20:53 107-06-210/04/22 16:348.9 5.9 1
1,1-Dichloroethene ND ug/kg 10/04/22 20:53 75-35-410/04/22 16:348.9 3.7 1
cis-1,2-Dichloroethene ND ug/kg 10/04/22 20:53 156-59-210/04/22 16:348.9 3.0 1
trans-1,2-Dichloroethene ND ug/kg 10/04/22 20:53 156-60-510/04/22 16:348.9 3.1 1
1,2-Dichloropropane ND ug/kg 10/04/22 20:53 78-87-510/04/22 16:348.9 2.7 1
1,3-Dichloropropane ND ug/kg 10/04/22 20:53 142-28-910/04/22 16:348.9 2.8 1
2,2-Dichloropropane ND ug/kg 10/04/22 20:53 594-20-7 v210/04/22 16:348.9 2.9 1
1,1-Dichloropropene ND ug/kg 10/04/22 20:53 563-58-610/04/22 16:348.9 4.3 1
cis-1,3-Dichloropropene ND ug/kg 10/04/22 20:53 10061-01-510/04/22 16:348.9 2.4 1
trans-1,3-Dichloropropene ND ug/kg 10/04/22 20:53 10061-02-610/04/22 16:348.9 3.1 1
Diisopropyl ether ND ug/kg 10/04/22 20:53 108-20-310/04/22 16:348.9 2.4 1
Ethylbenzene ND ug/kg 10/04/22 20:53 100-41-410/04/22 16:348.9 4.1 1
Hexachloro-1,3-butadiene ND ug/kg 10/04/22 20:53 87-68-3 v210/04/22 16:3417.7 14.5 1
2-Hexanone ND ug/kg 10/04/22 20:53 591-78-610/04/22 16:3488.7 8.5 1
Isopropylbenzene (Cumene)ND ug/kg 10/04/22 20:53 98-82-810/04/22 16:348.9 3.0 1
p-Isopropyltoluene ND ug/kg 10/04/22 20:53 99-87-610/04/22 16:348.9 4.4 1
Methylene Chloride ND ug/kg 10/04/22 20:53 75-09-2 v210/04/22 16:3435.5 24.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-3A Lab ID: 92629052009 Collected: 10/03/22 16:35 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/04/22 20:53 108-10-110/04/22 16:3488.7 8.5 1
Methyl-tert-butyl ether ND ug/kg 10/04/22 20:53 1634-04-410/04/22 16:348.9 3.3 1
Naphthalene ND ug/kg 10/04/22 20:53 91-20-310/04/22 16:348.9 4.7 1
n-Propylbenzene ND ug/kg 10/04/22 20:53 103-65-110/04/22 16:348.9 3.2 1
Styrene ND ug/kg 10/04/22 20:53 100-42-510/04/22 16:348.9 2.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/04/22 20:53 630-20-610/04/22 16:348.9 3.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/04/22 20:53 79-34-510/04/22 16:348.9 2.3 1
Tetrachloroethene ND ug/kg 10/04/22 20:53 127-18-410/04/22 16:348.9 2.8 1
Toluene ND ug/kg 10/04/22 20:53 108-88-310/04/22 16:348.9 2.5 1
1,2,3-Trichlorobenzene ND ug/kg 10/04/22 20:53 87-61-610/04/22 16:348.9 7.2 1
1,2,4-Trichlorobenzene ND ug/kg 10/04/22 20:53 120-82-110/04/22 16:348.9 7.4 1
1,1,1-Trichloroethane ND ug/kg 10/04/22 20:53 71-55-610/04/22 16:348.9 4.6 1
1,1,2-Trichloroethane ND ug/kg 10/04/22 20:53 79-00-510/04/22 16:348.9 2.9 1
Trichloroethene ND ug/kg 10/04/22 20:53 79-01-610/04/22 16:348.9 2.3 1
Trichlorofluoromethane ND ug/kg 10/04/22 20:53 75-69-410/04/22 16:348.9 4.9 1
1,2,3-Trichloropropane ND ug/kg 10/04/22 20:53 96-18-410/04/22 16:348.9 4.5 1
1,2,4-Trimethylbenzene ND ug/kg 10/04/22 20:53 95-63-610/04/22 16:348.9 2.4 1
1,3,5-Trimethylbenzene ND ug/kg 10/04/22 20:53 108-67-810/04/22 16:348.9 3.0 1
Vinyl acetate ND ug/kg 10/04/22 20:53 108-05-410/04/22 16:3488.7 6.5 1
Vinyl chloride ND ug/kg 10/04/22 20:53 75-01-410/04/22 16:3417.7 4.5 1
Xylene (Total)ND ug/kg 10/04/22 20:53 1330-20-710/04/22 16:3417.7 5.1 1
m&p-Xylene ND ug/kg 10/04/22 20:53 179601-23-110/04/22 16:3417.7 6.1 1
o-Xylene ND ug/kg 10/04/22 20:53 95-47-610/04/22 16:348.9 3.9 1
Surrogates
Toluene-d8 (S)99 %10/04/22 20:53 2037-26-510/04/22 16:3470-130 1
4-Bromofluorobenzene (S)100 %10/04/22 20:53 460-00-410/04/22 16:3470-130 1
1,2-Dichloroethane-d4 (S)92 %10/04/22 20:53 17060-07-010/04/22 16:3470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.7 %10/04/22 17:36 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-1B Lab ID: 92629052010 Collected: 10/03/22 17:25 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 10/04/22 21:10 67-64-110/04/22 16:34166 53.2 1
Benzene ND ug/kg 10/04/22 21:10 71-43-210/04/22 16:348.3 3.3 1
Bromobenzene ND ug/kg 10/04/22 21:10 108-86-110/04/22 16:348.3 2.7 1
Bromochloromethane ND ug/kg 10/04/22 21:10 74-97-510/04/22 16:348.3 2.5 1
Bromodichloromethane ND ug/kg 10/04/22 21:10 75-27-410/04/22 16:348.3 3.2 1
Bromoform ND ug/kg 10/04/22 21:10 75-25-210/04/22 16:348.3 2.9 1
Bromomethane ND ug/kg 10/04/22 21:10 74-83-9 v210/04/22 16:3416.6 13.1 1
2-Butanone (MEK)ND ug/kg 10/04/22 21:10 78-93-310/04/22 16:34166 39.8 1
n-Butylbenzene ND ug/kg 10/04/22 21:10 104-51-810/04/22 16:348.3 3.9 1
sec-Butylbenzene ND ug/kg 10/04/22 21:10 135-98-810/04/22 16:348.3 3.6 1
tert-Butylbenzene ND ug/kg 10/04/22 21:10 98-06-610/04/22 16:348.3 2.9 1
Carbon tetrachloride ND ug/kg 10/04/22 21:10 56-23-510/04/22 16:348.3 3.1 1
Chlorobenzene ND ug/kg 10/04/22 21:10 108-90-710/04/22 16:348.3 1.6 1
Chloroethane ND ug/kg 10/04/22 21:10 75-00-310/04/22 16:3416.6 6.4 1
Chloroform ND ug/kg 10/04/22 21:10 67-66-310/04/22 16:348.3 5.0 1
Chloromethane ND ug/kg 10/04/22 21:10 74-87-310/04/22 16:3416.6 7.0 1
2-Chlorotoluene ND ug/kg 10/04/22 21:10 95-49-810/04/22 16:348.3 2.9 1
4-Chlorotoluene ND ug/kg 10/04/22 21:10 106-43-410/04/22 16:348.3 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 10/04/22 21:10 96-12-810/04/22 16:348.3 3.2 1
Dibromochloromethane ND ug/kg 10/04/22 21:10 124-48-110/04/22 16:348.3 4.7 1
1,2-Dibromoethane (EDB)ND ug/kg 10/04/22 21:10 106-93-410/04/22 16:348.3 3.6 1
Dibromomethane ND ug/kg 10/04/22 21:10 74-95-310/04/22 16:348.3 1.8 1
1,2-Dichlorobenzene ND ug/kg 10/04/22 21:10 95-50-110/04/22 16:348.3 3.0 1
1,3-Dichlorobenzene ND ug/kg 10/04/22 21:10 541-73-110/04/22 16:348.3 2.6 1
1,4-Dichlorobenzene ND ug/kg 10/04/22 21:10 106-46-710/04/22 16:348.3 2.2 1
Dichlorodifluoromethane ND ug/kg 10/04/22 21:10 75-71-810/04/22 16:3416.6 3.6 1
1,1-Dichloroethane ND ug/kg 10/04/22 21:10 75-34-310/04/22 16:348.3 3.4 1
1,2-Dichloroethane ND ug/kg 10/04/22 21:10 107-06-210/04/22 16:348.3 5.5 1
1,1-Dichloroethene ND ug/kg 10/04/22 21:10 75-35-410/04/22 16:348.3 3.4 1
cis-1,2-Dichloroethene ND ug/kg 10/04/22 21:10 156-59-210/04/22 16:348.3 2.8 1
trans-1,2-Dichloroethene ND ug/kg 10/04/22 21:10 156-60-510/04/22 16:348.3 2.9 1
1,2-Dichloropropane ND ug/kg 10/04/22 21:10 78-87-510/04/22 16:348.3 2.5 1
1,3-Dichloropropane ND ug/kg 10/04/22 21:10 142-28-910/04/22 16:348.3 2.6 1
2,2-Dichloropropane ND ug/kg 10/04/22 21:10 594-20-7 v210/04/22 16:348.3 2.7 1
1,1-Dichloropropene ND ug/kg 10/04/22 21:10 563-58-610/04/22 16:348.3 4.0 1
cis-1,3-Dichloropropene ND ug/kg 10/04/22 21:10 10061-01-510/04/22 16:348.3 2.3 1
trans-1,3-Dichloropropene ND ug/kg 10/04/22 21:10 10061-02-610/04/22 16:348.3 2.8 1
Diisopropyl ether ND ug/kg 10/04/22 21:10 108-20-310/04/22 16:348.3 2.2 1
Ethylbenzene ND ug/kg 10/04/22 21:10 100-41-410/04/22 16:348.3 3.9 1
Hexachloro-1,3-butadiene ND ug/kg 10/04/22 21:10 87-68-3 v210/04/22 16:3416.6 13.6 1
2-Hexanone ND ug/kg 10/04/22 21:10 591-78-610/04/22 16:3482.8 8.0 1
Isopropylbenzene (Cumene)ND ug/kg 10/04/22 21:10 98-82-810/04/22 16:348.3 2.8 1
p-Isopropyltoluene ND ug/kg 10/04/22 21:10 99-87-610/04/22 16:348.3 4.1 1
Methylene Chloride ND ug/kg 10/04/22 21:10 75-09-2 v210/04/22 16:3433.1 22.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: HA-1B Lab ID: 92629052010 Collected: 10/03/22 17:25 Received: 10/04/22 13:17 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 10/04/22 21:10 108-10-110/04/22 16:3482.8 8.0 1
Methyl-tert-butyl ether ND ug/kg 10/04/22 21:10 1634-04-410/04/22 16:348.3 3.1 1
Naphthalene ND ug/kg 10/04/22 21:10 91-20-310/04/22 16:348.3 4.4 1
n-Propylbenzene ND ug/kg 10/04/22 21:10 103-65-110/04/22 16:348.3 2.9 1
Styrene ND ug/kg 10/04/22 21:10 100-42-510/04/22 16:348.3 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 10/04/22 21:10 630-20-610/04/22 16:348.3 3.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 10/04/22 21:10 79-34-510/04/22 16:348.3 2.2 1
Tetrachloroethene ND ug/kg 10/04/22 21:10 127-18-410/04/22 16:348.3 2.6 1
Toluene ND ug/kg 10/04/22 21:10 108-88-310/04/22 16:348.3 2.4 1
1,2,3-Trichlorobenzene ND ug/kg 10/04/22 21:10 87-61-610/04/22 16:348.3 6.7 1
1,2,4-Trichlorobenzene ND ug/kg 10/04/22 21:10 120-82-110/04/22 16:348.3 7.0 1
1,1,1-Trichloroethane ND ug/kg 10/04/22 21:10 71-55-610/04/22 16:348.3 4.3 1
1,1,2-Trichloroethane ND ug/kg 10/04/22 21:10 79-00-510/04/22 16:348.3 2.7 1
Trichloroethene ND ug/kg 10/04/22 21:10 79-01-610/04/22 16:348.3 2.1 1
Trichlorofluoromethane ND ug/kg 10/04/22 21:10 75-69-410/04/22 16:348.3 4.6 1
1,2,3-Trichloropropane ND ug/kg 10/04/22 21:10 96-18-410/04/22 16:348.3 4.2 1
1,2,4-Trimethylbenzene ND ug/kg 10/04/22 21:10 95-63-610/04/22 16:348.3 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 10/04/22 21:10 108-67-810/04/22 16:348.3 2.8 1
Vinyl acetate ND ug/kg 10/04/22 21:10 108-05-410/04/22 16:3482.8 6.0 1
Vinyl chloride ND ug/kg 10/04/22 21:10 75-01-410/04/22 16:3416.6 4.2 1
Xylene (Total)ND ug/kg 10/04/22 21:10 1330-20-710/04/22 16:3416.6 4.7 1
m&p-Xylene ND ug/kg 10/04/22 21:10 179601-23-110/04/22 16:3416.6 5.7 1
o-Xylene ND ug/kg 10/04/22 21:10 95-47-610/04/22 16:348.3 3.7 1
Surrogates
Toluene-d8 (S)98 %10/04/22 21:10 2037-26-510/04/22 16:3470-130 1
4-Bromofluorobenzene (S)102 %10/04/22 21:10 460-00-410/04/22 16:3470-130 1
1,2-Dichloroethane-d4 (S)91 %10/04/22 21:10 17060-07-010/04/22 16:3470-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.8 %10/05/22 00:24 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: EQ BLANK Lab ID: 92629052011 Collected: 10/03/22 13:30 Received: 10/04/22 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND ug/L 10/11/22 19:10 7440-38-210/11/22 11:2630.0 26.2 1
Barium ND ug/L 10/11/22 19:10 7440-39-310/11/22 11:2610.0 1.3 1
Cadmium ND ug/L 10/11/22 19:10 7440-43-910/11/22 11:2610.0 2.7 1
Chromium ND ug/L 10/11/22 19:10 7440-47-310/11/22 11:2610.0 3.6 1
Silver ND ug/L 10/11/22 19:10 7440-22-410/11/22 11:2610.0 4.6 1
Lead ND ug/L 10/11/22 19:10 7439-92-110/11/22 11:2620.0 19.0 1
Selenium ND ug/L 10/11/22 19:10 7782-49-210/11/22 11:2640.0 31.1 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
7470 Mercury
Mercury ND ug/L 10/18/22 12:59 7439-97-610/18/22 09:250.20 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 10/11/22 19:46 83-32-910/10/22 17:039.1 1.8 1
Acenaphthylene ND ug/L 10/11/22 19:46 208-96-810/10/22 17:039.1 1.8 1
Aniline ND ug/L 10/11/22 19:46 62-53-310/10/22 17:039.1 1.5 1
Anthracene ND ug/L 10/11/22 19:46 120-12-710/10/22 17:039.1 2.1 1
Benzo(a)anthracene ND ug/L 10/11/22 19:46 56-55-310/10/22 17:039.1 2.4 1
Benzo(a)pyrene ND ug/L 10/11/22 19:46 50-32-810/10/22 17:039.1 2.5 1
Benzo(b)fluoranthene ND ug/L 10/11/22 19:46 205-99-210/10/22 17:039.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 10/11/22 19:46 191-24-210/10/22 17:039.1 2.6 1
Benzo(k)fluoranthene ND ug/L 10/11/22 19:46 207-08-910/10/22 17:039.1 2.5 1
Benzoic Acid ND ug/L 10/11/22 19:46 65-85-010/10/22 17:0345.5 20.0 1
Benzyl alcohol ND ug/L 10/11/22 19:46 100-51-610/10/22 17:0318.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 10/11/22 19:46 101-55-310/10/22 17:039.1 1.6 1
Butylbenzylphthalate ND ug/L 10/11/22 19:46 85-68-710/10/22 17:039.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 10/11/22 19:46 59-50-710/10/22 17:039.1 3.0 1
4-Chloroaniline ND ug/L 10/11/22 19:46 106-47-810/10/22 17:0318.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 10/11/22 19:46 111-91-110/10/22 17:039.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 10/11/22 19:46 111-44-410/10/22 17:039.1 1.7 1
2-Chloronaphthalene ND ug/L 10/11/22 19:46 91-58-710/10/22 17:039.1 1.6 1
2-Chlorophenol ND ug/L 10/11/22 19:46 95-57-810/10/22 17:039.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 10/11/22 19:46 7005-72-310/10/22 17:039.1 1.8 1
Chrysene ND ug/L 10/11/22 19:46 218-01-910/10/22 17:039.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 10/11/22 19:46 53-70-310/10/22 17:039.1 2.7 1
Dibenzofuran ND ug/L 10/11/22 19:46 132-64-910/10/22 17:039.1 1.9 1
1,2-Dichlorobenzene ND ug/L 10/11/22 19:46 95-50-110/10/22 17:039.1 1.6 1
1,3-Dichlorobenzene ND ug/L 10/11/22 19:46 541-73-110/10/22 17:039.1 1.5 1
1,4-Dichlorobenzene ND ug/L 10/11/22 19:46 106-46-710/10/22 17:039.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 10/11/22 19:46 91-94-110/10/22 17:0318.2 7.4 1
2,4-Dichlorophenol ND ug/L 10/11/22 19:46 120-83-210/10/22 17:039.1 1.3 1
Diethylphthalate ND ug/L 10/11/22 19:46 84-66-210/10/22 17:039.1 1.9 1
2,4-Dimethylphenol ND ug/L 10/11/22 19:46 105-67-910/10/22 17:039.1 1.5 1
Dimethylphthalate ND ug/L 10/11/22 19:46 131-11-310/10/22 17:039.1 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: EQ BLANK Lab ID: 92629052011 Collected: 10/03/22 13:30 Received: 10/04/22 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 10/11/22 19:46 84-74-210/10/22 17:039.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 10/11/22 19:46 534-52-110/10/22 17:0318.2 7.1 1
2,4-Dinitrophenol ND ug/L 10/11/22 19:46 51-28-510/10/22 17:0345.5 23.6 1
2,4-Dinitrotoluene ND ug/L 10/11/22 19:46 121-14-210/10/22 17:039.1 1.5 1
2,6-Dinitrotoluene ND ug/L 10/11/22 19:46 606-20-210/10/22 17:039.1 1.6 1
Di-n-octylphthalate ND ug/L 10/11/22 19:46 117-84-010/10/22 17:039.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 10/11/22 19:46 117-81-710/10/22 17:035.5 3.4 1
Fluoranthene ND ug/L 10/11/22 19:46 206-44-010/10/22 17:039.1 2.0 1
Fluorene ND ug/L 10/11/22 19:46 86-73-710/10/22 17:039.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 10/11/22 19:46 87-68-310/10/22 17:039.1 1.6 1
Hexachlorobenzene ND ug/L 10/11/22 19:46 118-74-110/10/22 17:039.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 10/11/22 19:46 77-47-410/10/22 17:039.1 1.4 1
Hexachloroethane ND ug/L 10/11/22 19:46 67-72-110/10/22 17:039.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 10/11/22 19:46 193-39-510/10/22 17:039.1 2.6 1
Isophorone ND ug/L 10/11/22 19:46 78-59-110/10/22 17:039.1 1.5 1
1-Methylnaphthalene ND ug/L 10/11/22 19:46 90-12-010/10/22 17:039.1 1.8 1
2-Methylnaphthalene ND ug/L 10/11/22 19:46 91-57-610/10/22 17:039.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 10/11/22 19:46 95-48-710/10/22 17:039.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 10/11/22 19:46 15831-10-410/10/22 17:039.1 1.1 1
Naphthalene ND ug/L 10/11/22 19:46 91-20-310/10/22 17:039.1 1.9 1
2-Nitroaniline ND ug/L 10/11/22 19:46 88-74-410/10/22 17:0318.2 2.7 1
3-Nitroaniline ND ug/L 10/11/22 19:46 99-09-210/10/22 17:0318.2 3.4 1
4-Nitroaniline ND ug/L 10/11/22 19:46 100-01-610/10/22 17:0318.2 4.6 1
Nitrobenzene ND ug/L 10/11/22 19:46 98-95-310/10/22 17:039.1 1.7 1
2-Nitrophenol ND ug/L 10/11/22 19:46 88-75-510/10/22 17:039.1 1.3 1
4-Nitrophenol ND ug/L 10/11/22 19:46 100-02-710/10/22 17:0345.5 6.0 1
N-Nitrosodimethylamine ND ug/L 10/11/22 19:46 62-75-910/10/22 17:039.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 10/11/22 19:46 621-64-710/10/22 17:039.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 10/11/22 19:46 86-30-610/10/22 17:039.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 10/11/22 19:46 108-60-110/10/22 17:039.1 1.0 1
Pentachlorophenol ND ug/L 10/11/22 19:46 87-86-510/10/22 17:0318.2 3.4 1
Phenanthrene ND ug/L 10/11/22 19:46 85-01-810/10/22 17:039.1 1.8 1
Phenol ND ug/L 10/11/22 19:46 108-95-210/10/22 17:039.1 1.2 1
Pyrene ND ug/L 10/11/22 19:46 129-00-010/10/22 17:039.1 2.0 1
1,2,4-Trichlorobenzene ND ug/L 10/11/22 19:46 120-82-110/10/22 17:039.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 10/11/22 19:46 95-95-410/10/22 17:039.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 10/11/22 19:46 88-06-210/10/22 17:039.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)45 %10/11/22 19:46 4165-60-010/10/22 17:0310-144 1
2-Fluorobiphenyl (S)19 %10/11/22 19:46 321-60-810/10/22 17:0310-130 1
Terphenyl-d14 (S)116 %10/11/22 19:46 1718-51-010/10/22 17:0334-163 1
Phenol-d6 (S)27 %10/11/22 19:46 13127-88-310/10/22 17:0310-130 1
2-Fluorophenol (S)35 %10/11/22 19:46 367-12-410/10/22 17:0310-130 1
2,4,6-Tribromophenol (S)84 %10/11/22 19:46 118-79-610/10/22 17:0310-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: EQ BLANK Lab ID: 92629052011 Collected: 10/03/22 13:30 Received: 10/04/22 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV
Acetone 13.8J ug/L 10/07/22 00:01 67-64-1 C025.0 3.0 1
Benzene ND ug/L 10/07/22 00:01 71-43-25.0 1.7 1
Bromobenzene ND ug/L 10/07/22 00:01 108-86-15.0 1.9 1
Bromochloromethane ND ug/L 10/07/22 00:01 74-97-55.0 2.1 1
Bromodichloromethane ND ug/L 10/07/22 00:01 75-27-45.0 1.1 1
Bromoform ND ug/L 10/07/22 00:01 75-25-25.0 1.0 1
Bromomethane ND ug/L 10/07/22 00:01 74-83-910.0 6.0 1
2-Butanone (MEK)ND ug/L 10/07/22 00:01 78-93-310.0 2.6 1
tert-Butyl Alcohol ND ug/L 10/07/22 00:01 75-65-0100 11.6 1
n-Butylbenzene ND ug/L 10/07/22 00:01 104-51-85.0 2.3 1
sec-Butylbenzene ND ug/L 10/07/22 00:01 135-98-85.0 2.2 1
tert-Butylbenzene ND ug/L 10/07/22 00:01 98-06-65.0 0.98 1
Carbon tetrachloride ND ug/L 10/07/22 00:01 56-23-55.0 2.2 1
Chlorobenzene ND ug/L 10/07/22 00:01 108-90-75.0 1.8 1
Chloroethane ND ug/L 10/07/22 00:01 75-00-310.0 4.1 1
Chloroform ND ug/L 10/07/22 00:01 67-66-35.0 1.3 1
Chloromethane ND ug/L 10/07/22 00:01 74-87-35.0 2.8 1
2-Chlorotoluene ND ug/L 10/07/22 00:01 95-49-85.0 1.8 1
4-Chlorotoluene ND ug/L 10/07/22 00:01 106-43-45.0 2.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/07/22 00:01 96-12-85.0 1.0 1
Dibromochloromethane ND ug/L 10/07/22 00:01 124-48-15.0 2.3 1
1,2-Dibromoethane (EDB)ND ug/L 10/07/22 00:01 106-93-45.0 1.9 1
Dibromomethane ND ug/L 10/07/22 00:01 74-95-35.0 1.0 1
1,2-Dichlorobenzene ND ug/L 10/07/22 00:01 95-50-15.0 1.9 1
1,3-Dichlorobenzene ND ug/L 10/07/22 00:01 541-73-15.0 1.7 1
1,4-Dichlorobenzene ND ug/L 10/07/22 00:01 106-46-75.0 1.9 1
Dichlorodifluoromethane ND ug/L 10/07/22 00:01 75-71-85.0 1.8 1
1,1-Dichloroethane ND ug/L 10/07/22 00:01 75-34-35.0 2.3 1
1,2-Dichloroethane ND ug/L 10/07/22 00:01 107-06-25.0 2.1 1
1,2-Dichloroethene (Total)ND ug/L 10/07/22 00:01 540-59-05.0 5.0 1
1,1-Dichloroethene ND ug/L 10/07/22 00:01 75-35-45.0 2.2 1
cis-1,2-Dichloroethene ND ug/L 10/07/22 00:01 156-59-25.0 2.2 1
trans-1,2-Dichloroethene ND ug/L 10/07/22 00:01 156-60-55.0 2.2 1
1,2-Dichloropropane ND ug/L 10/07/22 00:01 78-87-55.0 2.1 1
1,3-Dichloropropane ND ug/L 10/07/22 00:01 142-28-95.0 1.9 1
2,2-Dichloropropane ND ug/L 10/07/22 00:01 594-20-75.0 2.4 1
1,1-Dichloropropene ND ug/L 10/07/22 00:01 563-58-65.0 2.8 1
cis-1,3-Dichloropropene ND ug/L 10/07/22 00:01 10061-01-55.0 2.0 1
trans-1,3-Dichloropropene ND ug/L 10/07/22 00:01 10061-02-65.0 2.2 1
Diisopropyl ether ND ug/L 10/07/22 00:01 108-20-35.0 1.4 1
Ethylbenzene ND ug/L 10/07/22 00:01 100-41-45.0 1.8 1
Hexachloro-1,3-butadiene ND ug/L 10/07/22 00:01 87-68-35.0 4.8 1
2-Hexanone ND ug/L 10/07/22 00:01 591-78-610.0 4.2 1
Isopropylbenzene (Cumene)ND ug/L 10/07/22 00:01 98-82-85.0 2.1 1
p-Isopropyltoluene ND ug/L 10/07/22 00:01 99-87-65.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: EQ BLANK Lab ID: 92629052011 Collected: 10/03/22 13:30 Received: 10/04/22 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV
Methylene Chloride ND ug/L 10/07/22 00:01 75-09-25.0 3.3 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/07/22 00:01 108-10-110.0 4.7 1
Methyl-tert-butyl ether ND ug/L 10/07/22 00:01 1634-04-45.0 3.1 1
Naphthalene ND ug/L 10/07/22 00:01 91-20-35.0 2.1 1
n-Propylbenzene ND ug/L 10/07/22 00:01 103-65-15.0 2.0 1
Styrene ND ug/L 10/07/22 00:01 100-42-55.0 1.9 1
1,1,1,2-Tetrachloroethane ND ug/L 10/07/22 00:01 630-20-65.0 1.1 1
1,1,2,2-Tetrachloroethane ND ug/L 10/07/22 00:01 79-34-55.0 2.0 1
Tetrachloroethene ND ug/L 10/07/22 00:01 127-18-45.0 1.8 1
Toluene ND ug/L 10/07/22 00:01 108-88-35.0 2.0 1
1,2,3-Trichlorobenzene ND ug/L 10/07/22 00:01 87-61-65.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 10/07/22 00:01 120-82-15.0 2.3 1
1,1,1-Trichloroethane ND ug/L 10/07/22 00:01 71-55-65.0 2.1 1
1,1,2-Trichloroethane ND ug/L 10/07/22 00:01 79-00-55.0 2.0 1
Trichloroethene ND ug/L 10/07/22 00:01 79-01-65.0 1.8 1
Trichlorofluoromethane ND ug/L 10/07/22 00:01 75-69-410.0 1.5 1
1,2,3-Trichloropropane ND ug/L 10/07/22 00:01 96-18-45.0 1.1 1
1,2,4-Trimethylbenzene ND ug/L 10/07/22 00:01 95-63-65.0 2.0 1
1,3,5-Trimethylbenzene ND ug/L 10/07/22 00:01 108-67-85.0 2.1 1
Vinyl acetate ND ug/L 10/07/22 00:01 108-05-410.0 5.6 1
Vinyl chloride ND ug/L 10/07/22 00:01 75-01-45.0 1.8 1
m&p-Xylene ND ug/L 10/07/22 00:01 179601-23-110.0 4.1 1
o-Xylene ND ug/L 10/07/22 00:01 95-47-65.0 2.0 1
Surrogates
4-Bromofluorobenzene (S)101 %10/07/22 00:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/07/22 00:01 17060-07-070-130 1
Toluene-d8 (S)104 %10/07/22 00:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: TRIP BLANK Lab ID: 92629052012 Collected: 10/03/22 00:00 Received: 10/04/22 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV
Acetone 13.4J ug/L 10/07/22 00:19 67-64-1 C025.0 3.0 1
Benzene ND ug/L 10/07/22 00:19 71-43-25.0 1.7 1
Bromobenzene ND ug/L 10/07/22 00:19 108-86-15.0 1.9 1
Bromochloromethane ND ug/L 10/07/22 00:19 74-97-55.0 2.1 1
Bromodichloromethane ND ug/L 10/07/22 00:19 75-27-45.0 1.1 1
Bromoform ND ug/L 10/07/22 00:19 75-25-25.0 1.0 1
Bromomethane ND ug/L 10/07/22 00:19 74-83-910.0 6.0 1
2-Butanone (MEK)ND ug/L 10/07/22 00:19 78-93-310.0 2.6 1
tert-Butyl Alcohol ND ug/L 10/07/22 00:19 75-65-0100 11.6 1
n-Butylbenzene ND ug/L 10/07/22 00:19 104-51-85.0 2.3 1
sec-Butylbenzene ND ug/L 10/07/22 00:19 135-98-85.0 2.2 1
tert-Butylbenzene ND ug/L 10/07/22 00:19 98-06-65.0 0.98 1
Carbon tetrachloride ND ug/L 10/07/22 00:19 56-23-55.0 2.2 1
Chlorobenzene ND ug/L 10/07/22 00:19 108-90-75.0 1.8 1
Chloroethane ND ug/L 10/07/22 00:19 75-00-310.0 4.1 1
Chloroform ND ug/L 10/07/22 00:19 67-66-35.0 1.3 1
Chloromethane ND ug/L 10/07/22 00:19 74-87-35.0 2.8 1
2-Chlorotoluene ND ug/L 10/07/22 00:19 95-49-85.0 1.8 1
4-Chlorotoluene ND ug/L 10/07/22 00:19 106-43-45.0 2.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/07/22 00:19 96-12-85.0 1.0 1
Dibromochloromethane ND ug/L 10/07/22 00:19 124-48-15.0 2.3 1
1,2-Dibromoethane (EDB)ND ug/L 10/07/22 00:19 106-93-45.0 1.9 1
Dibromomethane ND ug/L 10/07/22 00:19 74-95-35.0 1.0 1
1,2-Dichlorobenzene ND ug/L 10/07/22 00:19 95-50-15.0 1.9 1
1,3-Dichlorobenzene ND ug/L 10/07/22 00:19 541-73-15.0 1.7 1
1,4-Dichlorobenzene ND ug/L 10/07/22 00:19 106-46-75.0 1.9 1
Dichlorodifluoromethane ND ug/L 10/07/22 00:19 75-71-85.0 1.8 1
1,1-Dichloroethane ND ug/L 10/07/22 00:19 75-34-35.0 2.3 1
1,2-Dichloroethane ND ug/L 10/07/22 00:19 107-06-25.0 2.1 1
1,2-Dichloroethene (Total)ND ug/L 10/07/22 00:19 540-59-05.0 5.0 1
1,1-Dichloroethene ND ug/L 10/07/22 00:19 75-35-45.0 2.2 1
cis-1,2-Dichloroethene ND ug/L 10/07/22 00:19 156-59-25.0 2.2 1
trans-1,2-Dichloroethene ND ug/L 10/07/22 00:19 156-60-55.0 2.2 1
1,2-Dichloropropane ND ug/L 10/07/22 00:19 78-87-55.0 2.1 1
1,3-Dichloropropane ND ug/L 10/07/22 00:19 142-28-95.0 1.9 1
2,2-Dichloropropane ND ug/L 10/07/22 00:19 594-20-75.0 2.4 1
1,1-Dichloropropene ND ug/L 10/07/22 00:19 563-58-65.0 2.8 1
cis-1,3-Dichloropropene ND ug/L 10/07/22 00:19 10061-01-55.0 2.0 1
trans-1,3-Dichloropropene ND ug/L 10/07/22 00:19 10061-02-65.0 2.2 1
Diisopropyl ether ND ug/L 10/07/22 00:19 108-20-35.0 1.4 1
Ethylbenzene ND ug/L 10/07/22 00:19 100-41-45.0 1.8 1
Hexachloro-1,3-butadiene ND ug/L 10/07/22 00:19 87-68-35.0 4.8 1
2-Hexanone ND ug/L 10/07/22 00:19 591-78-610.0 4.2 1
Isopropylbenzene (Cumene)ND ug/L 10/07/22 00:19 98-82-85.0 2.1 1
p-Isopropyltoluene ND ug/L 10/07/22 00:19 99-87-65.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 72
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Sample: TRIP BLANK Lab ID: 92629052012 Collected: 10/03/22 00:00 Received: 10/04/22 13:17 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV
Methylene Chloride ND ug/L 10/07/22 00:19 75-09-25.0 3.3 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/07/22 00:19 108-10-110.0 4.7 1
Methyl-tert-butyl ether ND ug/L 10/07/22 00:19 1634-04-45.0 3.1 1
Naphthalene ND ug/L 10/07/22 00:19 91-20-35.0 2.1 1
n-Propylbenzene ND ug/L 10/07/22 00:19 103-65-15.0 2.0 1
Styrene ND ug/L 10/07/22 00:19 100-42-55.0 1.9 1
1,1,1,2-Tetrachloroethane ND ug/L 10/07/22 00:19 630-20-65.0 1.1 1
1,1,2,2-Tetrachloroethane ND ug/L 10/07/22 00:19 79-34-55.0 2.0 1
Tetrachloroethene ND ug/L 10/07/22 00:19 127-18-45.0 1.8 1
Toluene ND ug/L 10/07/22 00:19 108-88-35.0 2.0 1
1,2,3-Trichlorobenzene ND ug/L 10/07/22 00:19 87-61-65.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 10/07/22 00:19 120-82-15.0 2.3 1
1,1,1-Trichloroethane ND ug/L 10/07/22 00:19 71-55-65.0 2.1 1
1,1,2-Trichloroethane ND ug/L 10/07/22 00:19 79-00-55.0 2.0 1
Trichloroethene ND ug/L 10/07/22 00:19 79-01-65.0 1.8 1
Trichlorofluoromethane ND ug/L 10/07/22 00:19 75-69-410.0 1.5 1
1,2,3-Trichloropropane ND ug/L 10/07/22 00:19 96-18-45.0 1.1 1
1,2,4-Trimethylbenzene ND ug/L 10/07/22 00:19 95-63-65.0 2.0 1
1,3,5-Trimethylbenzene ND ug/L 10/07/22 00:19 108-67-85.0 2.1 1
Vinyl acetate ND ug/L 10/07/22 00:19 108-05-410.0 5.6 1
Vinyl chloride ND ug/L 10/07/22 00:19 75-01-45.0 1.8 1
m&p-Xylene ND ug/L 10/07/22 00:19 179601-23-110.0 4.1 1
o-Xylene ND ug/L 10/07/22 00:19 95-47-65.0 2.0 1
Surrogates
4-Bromofluorobenzene (S)98 %10/07/22 00:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/07/22 00:19 17060-07-070-130 1
Toluene-d8 (S)107 %10/07/22 00:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729336
EPA 3010A
EPA 6010D
6010D ATL
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92629052011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3797992
Associated Lab Samples:92629052011
Matrix: Water
AnalyzedMDL
Arsenic ug/L ND 30.0 10/11/22 19:0126.2
Barium ug/L ND 10.0 10/11/22 19:011.3
Cadmium ug/L ND 10.0 10/11/22 19:012.7
Chromium ug/L ND 10.0 10/11/22 19:013.6
Lead ug/L ND 20.0 10/11/22 19:0119.0
Selenium ug/L ND 40.0 10/11/22 19:0131.1
Silver ug/L ND 10.0 10/11/22 19:014.6
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3797993LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 10701000 107 80-120
Barium ug/L 10401000 104 80-120
Cadmium ug/L 10601000 106 80-120
Chromium ug/L 10901000 109 80-120
Lead ug/L 10901000 109 80-120
Selenium ug/L 11101000 111 80-120
Silver ug/L 10501000 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3797994MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92629507002
3797995
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 1000 106 75-125107 1 201000ND1060 1070
Barium ug/L 1000 101 75-125104 2 2010004491460 1480
Cadmium ug/L 1000 103 75-125105 1 201000ND1030 1050
Chromium ug/L 1000 103 75-125105 1 201000ND1030 1050
Lead ug/L 1000 105 75-125105 1 201000ND1060 1070
Selenium ug/L 1000 105 75-125105 0 201000ND1050 1050
Silver ug/L 1000 99 75-125100 1 201000ND989 1000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
730879
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples: 92629052011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3805310
Associated Lab Samples:92629052011
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.20 10/18/22 12:550.12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3805311LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.42.5 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3805312MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92629052011
3805313
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 103 75-125107 4 252.5ND 2.6 2.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
862776
EPA 7471
EPA 7471
7471 Mercury
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92629052001, 92629052002, 92629052003, 92629052004, 92629052005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4748768
Associated Lab Samples:92629052001, 92629052002, 92629052003, 92629052004, 92629052005
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.0096 10/13/22 09:050.0048
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4748769LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0990.098 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4748770MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35750030001
4748771
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.407 87 80-12081 4 200.4120.26 0.62 0.60
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
862699
EPA 3050
EPA 6010
6010 MET Solid
Laboratory:Pace Analytical Services - Ormond Beach
Associated Lab Samples: 92629052001, 92629052002, 92629052003, 92629052004, 92629052005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 4748166
Associated Lab Samples:92629052001, 92629052002, 92629052003, 92629052004, 92629052005
Matrix: Solid
AnalyzedMDL
Arsenic mg/kg ND 0.57 10/15/22 19:250.28
Barium mg/kg ND 0.57 10/15/22 19:250.095
Cadmium mg/kg ND 0.057 10/15/22 19:250.028
Chromium mg/kg ND 0.28 10/15/22 19:250.14
Lead mg/kg ND 0.57 10/15/22 19:250.28
Selenium mg/kg ND 0.85 10/15/22 19:250.43
Silver mg/kg ND 0.28 10/15/22 19:250.062
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4748167LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 14.315.3 94 80-120
Barium mg/kg 16.615.3 109 80-120
Cadmium mg/kg 1.51.5 101 80-120
Chromium mg/kg 16.115.3 105 80-120
Lead mg/kg 15.615.3 102 80-120
Selenium mg/kg 14.315.3 94 80-120
Silver mg/kg 1.51.5 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4748168MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35751256007
4748169
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 18.2 89 75-12593 13 2019.70.43U 16.6 18.8
Barium mg/kg 18.2 106 75-125113 12 2019.75.2 24.4 27.6
Cadmium mg/kg 1.81 101 75-125103 10 201.950.043U 1.9 2.1
Chromium mg/kg 18.2 106 75-125109 10 2019.71.1 20.5 22.7
Lead mg/kg 18.2 101 75-125104 10 2019.71.2 19.6 21.8
Selenium mg/kg 18.2 91 75-12595 12 2019.70.65U 16.9 19.1
Silver mg/kg 1.81 98 75-125101 11 201.950.095U 1.8 2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
727781
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92629052006, 92629052007, 92629052008, 92629052009, 92629052010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3790081
Associated Lab Samples:92629052006, 92629052007, 92629052008, 92629052009, 92629052010
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 10/04/22 15:581.9
1,1,1-Trichloroethane ug/kg ND 5.0 10/04/22 15:582.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 10/04/22 15:581.3
1,1,2-Trichloroethane ug/kg ND 5.0 10/04/22 15:581.7
1,1-Dichloroethane ug/kg ND 5.0 10/04/22 15:582.1
1,1-Dichloroethene ug/kg ND 5.0 10/04/22 15:582.1
1,1-Dichloropropene ug/kg ND 5.0 10/04/22 15:582.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 10/04/22 15:584.0
1,2,3-Trichloropropane ug/kg ND 5.0 10/04/22 15:582.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 10/04/22 15:584.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 10/04/22 15:581.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 10/04/22 15:581.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 10/04/22 15:582.2
1,2-Dichlorobenzene ug/kg ND 5.0 10/04/22 15:581.8
1,2-Dichloroethane ug/kg ND 5.0 10/04/22 15:583.3
1,2-Dichloropropane ug/kg ND 5.0 10/04/22 15:581.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 10/04/22 15:581.7
1,3-Dichlorobenzene ug/kg ND 5.0 10/04/22 15:581.6
1,3-Dichloropropane ug/kg ND 5.0 10/04/22 15:581.6
1,4-Dichlorobenzene ug/kg ND 5.0 10/04/22 15:581.3
2,2-Dichloropropane ug/kg ND 5.0 v210/04/22 15:581.6
2-Butanone (MEK)ug/kg ND 100 10/04/22 15:5824.0
2-Chlorotoluene ug/kg ND 5.0 10/04/22 15:581.8
2-Hexanone ug/kg ND 50.0 10/04/22 15:584.8
4-Chlorotoluene ug/kg ND 5.0 10/04/22 15:580.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 10/04/22 15:584.8
Acetone ug/kg ND 100 10/04/22 15:5832.1
Benzene ug/kg ND 5.0 10/04/22 15:582.0
Bromobenzene ug/kg ND 5.0 10/04/22 15:581.6
Bromochloromethane ug/kg ND 5.0 10/04/22 15:581.5
Bromodichloromethane ug/kg ND 5.0 10/04/22 15:581.9
Bromoform ug/kg ND 5.0 10/04/22 15:581.8
Bromomethane ug/kg ND 10.0 v210/04/22 15:587.9
Carbon tetrachloride ug/kg ND 5.0 10/04/22 15:581.9
Chlorobenzene ug/kg ND 5.0 10/04/22 15:580.96
Chloroethane ug/kg ND 10.0 10/04/22 15:583.9
Chloroform ug/kg ND 5.0 10/04/22 15:583.0
Chloromethane ug/kg ND 10.0 10/04/22 15:584.2
cis-1,2-Dichloroethene ug/kg ND 5.0 10/04/22 15:581.7
cis-1,3-Dichloropropene ug/kg ND 5.0 10/04/22 15:581.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3790081
Associated Lab Samples:92629052006, 92629052007, 92629052008, 92629052009, 92629052010
Matrix: Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 10/04/22 15:582.8
Dibromomethane ug/kg ND 5.0 10/04/22 15:581.1
Dichlorodifluoromethane ug/kg ND 10.0 10/04/22 15:582.2
Diisopropyl ether ug/kg ND 5.0 10/04/22 15:581.4
Ethylbenzene ug/kg ND 5.0 10/04/22 15:582.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 v210/04/22 15:588.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 10/04/22 15:581.7
m&p-Xylene ug/kg ND 10.0 10/04/22 15:583.4
Methyl-tert-butyl ether ug/kg ND 5.0 10/04/22 15:581.9
Methylene Chloride ug/kg ND 20.0 v210/04/22 15:5813.7
n-Butylbenzene ug/kg ND 5.0 10/04/22 15:582.4
n-Propylbenzene ug/kg ND 5.0 10/04/22 15:581.8
Naphthalene ug/kg ND 5.0 10/04/22 15:582.6
o-Xylene ug/kg ND 5.0 10/04/22 15:582.2
p-Isopropyltoluene ug/kg ND 5.0 10/04/22 15:582.5
sec-Butylbenzene ug/kg ND 5.0 10/04/22 15:582.2
Styrene ug/kg ND 5.0 10/04/22 15:581.3
tert-Butylbenzene ug/kg ND 5.0 10/04/22 15:581.8
Tetrachloroethene ug/kg ND 5.0 10/04/22 15:581.6
Toluene ug/kg ND 5.0 10/04/22 15:581.4
trans-1,2-Dichloroethene ug/kg ND 5.0 10/04/22 15:581.8
trans-1,3-Dichloropropene ug/kg ND 5.0 10/04/22 15:581.7
Trichloroethene ug/kg ND 5.0 10/04/22 15:581.3
Trichlorofluoromethane ug/kg ND 5.0 10/04/22 15:582.8
Vinyl acetate ug/kg ND 50.0 10/04/22 15:583.6
Vinyl chloride ug/kg ND 10.0 10/04/22 15:582.5
Xylene (Total)ug/kg ND 10.0 10/04/22 15:582.8
1,2-Dichloroethane-d4 (S)%95 70-130 10/04/22 15:58
4-Bromofluorobenzene (S)%101 70-130 10/04/22 15:58
Toluene-d8 (S)%98 70-130 10/04/22 15:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3790082LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11001250 88 70-130
1,1,1-Trichloroethane ug/kg 10201250 82 70-130
1,1,2,2-Tetrachloroethane ug/kg 11101250 89 70-130
1,1,2-Trichloroethane ug/kg 11501250 92 70-130
1,1-Dichloroethane ug/kg 10401250 83 70-130
1,1-Dichloroethene ug/kg 10601250 85 70-130
1,1-Dichloropropene ug/kg 10901250 87 70-130
1,2,3-Trichlorobenzene ug/kg 11501250 92 70-130
1,2,3-Trichloropropane ug/kg 10601250 85 70-130
1,2,4-Trichlorobenzene ug/kg 11001250 88 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3790082LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 10501250 84 70-130
1,2-Dibromo-3-chloropropane ug/kg 12201250 98 67-130
1,2-Dibromoethane (EDB)ug/kg 11401250 91 70-130
1,2-Dichlorobenzene ug/kg 11301250 90 70-130
1,2-Dichloroethane ug/kg 10501250 84 70-130
1,2-Dichloropropane ug/kg 11101250 88 70-130
1,3,5-Trimethylbenzene ug/kg 10801250 86 70-130
1,3-Dichlorobenzene ug/kg 11201250 90 70-130
1,3-Dichloropropane ug/kg 10801250 87 70-130
1,4-Dichlorobenzene ug/kg 10901250 87 70-130
2,2-Dichloropropane ug/kg 853 v3125068 67-130
2-Butanone (MEK)ug/kg 23702500 95 66-130
2-Chlorotoluene ug/kg 10901250 87 70-130
2-Hexanone ug/kg 25102500 100 70-130
4-Chlorotoluene ug/kg 10601250 85 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24902500 100 70-130
Acetone ug/kg 22502500 90 67-130
Benzene ug/kg 10101250 81 70-130
Bromobenzene ug/kg 11201250 89 70-130
Bromochloromethane ug/kg 11001250 88 70-130
Bromodichloromethane ug/kg 11001250 88 70-130
Bromoform ug/kg 12001250 96 70-130
Bromomethane ug/kg 905 v3125072 53-175
Carbon tetrachloride ug/kg 10301250 83 70-130
Chlorobenzene ug/kg 10801250 87 70-130
Chloroethane ug/kg 11201250 90 70-135
Chloroform ug/kg 10201250 82 70-130
Chloromethane ug/kg 11001250 88 64-130
cis-1,2-Dichloroethene ug/kg 10201250 82 70-130
cis-1,3-Dichloropropene ug/kg 11001250 88 70-130
Dibromochloromethane ug/kg 11201250 90 70-130
Dibromomethane ug/kg 11901250 95 70-130
Dichlorodifluoromethane ug/kg 11201250 89 63-145
Diisopropyl ether ug/kg 10701250 86 68-130
Ethylbenzene ug/kg 11101250 89 70-130
Hexachloro-1,3-butadiene ug/kg 968 v3125077 70-130
Isopropylbenzene (Cumene)ug/kg 10201250 82 70-130
m&p-Xylene ug/kg 20802500 83 70-130
Methyl-tert-butyl ether ug/kg 12201250 98 70-130
Methylene Chloride ug/kg 961 v3125077 67-130
n-Butylbenzene ug/kg 10401250 83 70-130
n-Propylbenzene ug/kg 10501250 84 70-130
Naphthalene ug/kg 12601250 101 70-130
o-Xylene ug/kg 10401250 83 70-130
p-Isopropyltoluene ug/kg 11001250 88 70-130
sec-Butylbenzene ug/kg 10101250 81 70-130
Styrene ug/kg 10801250 86 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3790082LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 10401250 83 64-130
Tetrachloroethene ug/kg 11401250 91 70-130
Toluene ug/kg 10701250 85 70-130
trans-1,2-Dichloroethene ug/kg 10501250 84 70-130
trans-1,3-Dichloropropene ug/kg 11401250 91 70-130
Trichloroethene ug/kg 11001250 88 70-130
Trichlorofluoromethane ug/kg 10001250 80 70-130
Vinyl acetate ug/kg 23402500 94 70-134
Vinyl chloride ug/kg 11701250 94 68-130
Xylene (Total)ug/kg 31103750 83 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3790083MATRIX SPIKE SAMPLE:
MSSpike
Result
92628827001
1,1,1,2-Tetrachloroethane ug/kg 747740 101 58-140ND
1,1,1-Trichloroethane ug/kg 720740 97 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 729740 98 52-139ND
1,1,2-Trichloroethane ug/kg 774740 105 56-140ND
1,1-Dichloroethane ug/kg 726740 98 58-145ND
1,1-Dichloroethene ug/kg 755740 102 57-158ND
1,1-Dichloropropene ug/kg 753740 102 58-151ND
1,2,3-Trichlorobenzene ug/kg 646740 87 48-149ND
1,2,3-Trichloropropane ug/kg 686740 93 54-132ND
1,2,4-Trichlorobenzene ug/kg 641740 87 51-151ND
1,2,4-Trimethylbenzene ug/kg 689740 93 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 634740 86 44-134ND
1,2-Dibromoethane (EDB)ug/kg 755740 102 60-138ND
1,2-Dichlorobenzene ug/kg 739740 100 59-147ND
1,2-Dichloroethane ug/kg 714740 97 57-139ND
1,2-Dichloropropane ug/kg 790740 107 62-145ND
1,3,5-Trimethylbenzene ug/kg 718740 97 47-159ND
1,3-Dichlorobenzene ug/kg 705740 95 58-144ND
1,3-Dichloropropane ug/kg 749740 101 60-142ND
1,4-Dichlorobenzene ug/kg 722740 98 57-143ND
2,2-Dichloropropane ug/kg 658 v274089 37-144ND
2-Butanone (MEK)ug/kg 14201470 96 28-146ND
2-Chlorotoluene ug/kg 735740 99 55-158ND
2-Hexanone ug/kg 14901470 101 44-141ND
4-Chlorotoluene ug/kg 697740 94 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 15101470 102 50-138ND
Acetone ug/kg 12201470 82 20-136ND
Benzene ug/kg 740740 100 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3790083MATRIX SPIKE SAMPLE:
MSSpike
Result
92628827001
Bromobenzene ug/kg 754740 102 59-145ND
Bromochloromethane ug/kg 721740 97 57-143ND
Bromodichloromethane ug/kg 706740 95 53-133ND
Bromoform ug/kg 653740 88 48-133ND
Bromomethane ug/kg 99.6 v274013 10-167ND
Carbon tetrachloride ug/kg 698740 94 57-147ND
Chlorobenzene ug/kg 774740 105 61-144ND
Chloroethane ug/kg 93.9740 13 10-153ND
Chloroform ug/kg 705740 95 58-141ND
Chloromethane ug/kg 779740 105 54-165ND
cis-1,2-Dichloroethene ug/kg 722740 98 59-144ND
cis-1,3-Dichloropropene ug/kg 749740 101 56-137ND
Dibromochloromethane ug/kg 664740 90 53-139ND
Dibromomethane ug/kg 794740 107 60-136ND
Dichlorodifluoromethane ug/kg 791740 107 49-177ND
Diisopropyl ether ug/kg 710740 96 53-136ND
Ethylbenzene ug/kg 794740 107 53-150ND
Hexachloro-1,3-butadiene ug/kg 613 v274082 42-186ND
Isopropylbenzene (Cumene)ug/kg 732740 99 62-154ND
m&p-Xylene ug/kg 14701470 99 49-156ND
Methyl-tert-butyl ether ug/kg 783740 106 54-133ND
Methylene Chloride ug/kg 615 v274083 50-153ND
n-Butylbenzene ug/kg 630740 85 44-174ND
n-Propylbenzene ug/kg 694740 94 52-157ND
Naphthalene ug/kg 679740 92 37-150ND
o-Xylene ug/kg 751740 101 54-150ND
p-Isopropyltoluene ug/kg 711740 96 50-164ND
sec-Butylbenzene ug/kg 680740 92 58-161ND
Styrene ug/kg 758740 102 60-148ND
tert-Butylbenzene ug/kg 711740 96 44-151ND
Tetrachloroethene ug/kg 712740 96 53-151ND
Toluene ug/kg 762740 103 52-148ND
trans-1,2-Dichloroethene ug/kg 733740 99 60-148ND
trans-1,3-Dichloropropene ug/kg 752740 102 55-133ND
Trichloroethene ug/kg 776740 105 60-148ND
Trichlorofluoromethane ug/kg 89.5740 12 10-154ND
Vinyl acetate ug/kg 14601470 99 50-149ND
Vinyl chloride ug/kg 886740 120 57-157ND
Xylene (Total)ug/kg 22202220 100 52-153ND
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92628827002
3790084SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND v230ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND v230ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND v230ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92628827002
3790084SAMPLE DUPLICATE:
m&p-Xylene ug/kg 6.8J 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND v230ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg 7.0 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 3.7J 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg 7.0J 30ND
1,2-Dichloroethane-d4 (S)%9594
4-Bromofluorobenzene (S)%102103
Toluene-d8 (S)%9899
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
728501
EPA 8260D
EPA 8260D
8260D MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92629052011, 92629052012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3793963
Associated Lab Samples:92629052011, 92629052012
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 10/06/22 23:071.1
1,1,1-Trichloroethane ug/L ND 5.0 10/06/22 23:072.1
1,1,2,2-Tetrachloroethane ug/L ND 5.0 10/06/22 23:072.0
1,1,2-Trichloroethane ug/L ND 5.0 10/06/22 23:072.0
1,1-Dichloroethane ug/L ND 5.0 10/06/22 23:072.3
1,1-Dichloroethene ug/L ND 5.0 10/06/22 23:072.2
1,1-Dichloropropene ug/L ND 5.0 10/06/22 23:072.8
1,2,3-Trichlorobenzene ug/L ND 5.0 10/06/22 23:072.2
1,2,3-Trichloropropane ug/L ND 5.0 10/06/22 23:071.1
1,2,4-Trichlorobenzene ug/L ND 5.0 10/06/22 23:072.3
1,2,4-Trimethylbenzene ug/L ND 5.0 10/06/22 23:072.0
1,2-Dibromo-3-chloropropane ug/L ND 5.0 10/06/22 23:071.0
1,2-Dibromoethane (EDB)ug/L ND 5.0 10/06/22 23:071.9
1,2-Dichlorobenzene ug/L ND 5.0 10/06/22 23:071.9
1,2-Dichloroethane ug/L ND 5.0 10/06/22 23:072.1
1,2-Dichloroethene (Total)ug/L ND 5.0 10/06/22 23:075.0
1,2-Dichloropropane ug/L ND 5.0 10/06/22 23:072.1
1,3,5-Trimethylbenzene ug/L ND 5.0 10/06/22 23:072.1
1,3-Dichlorobenzene ug/L ND 5.0 10/06/22 23:071.7
1,3-Dichloropropane ug/L ND 5.0 10/06/22 23:071.9
1,4-Dichlorobenzene ug/L ND 5.0 10/06/22 23:071.9
2,2-Dichloropropane ug/L ND 5.0 10/06/22 23:072.4
2-Butanone (MEK)ug/L ND 10.0 10/06/22 23:072.6
2-Chlorotoluene ug/L ND 5.0 10/06/22 23:071.8
2-Hexanone ug/L ND 10.0 10/06/22 23:074.2
4-Chlorotoluene ug/L ND 5.0 10/06/22 23:072.0
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 10/06/22 23:074.7
Acetone ug/L ND 25.0 10/06/22 23:073.0
Benzene ug/L ND 5.0 10/06/22 23:071.7
Bromobenzene ug/L ND 5.0 10/06/22 23:071.9
Bromochloromethane ug/L ND 5.0 10/06/22 23:072.1
Bromodichloromethane ug/L ND 5.0 10/06/22 23:071.1
Bromoform ug/L ND 5.0 10/06/22 23:071.0
Bromomethane ug/L ND 10.0 10/06/22 23:076.0
Carbon tetrachloride ug/L ND 5.0 10/06/22 23:072.2
Chlorobenzene ug/L ND 5.0 10/06/22 23:071.8
Chloroethane ug/L ND 10.0 10/06/22 23:074.1
Chloroform ug/L ND 5.0 10/06/22 23:071.3
Chloromethane ug/L ND 5.0 10/06/22 23:072.8
cis-1,2-Dichloroethene ug/L ND 5.0 10/06/22 23:072.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3793963
Associated Lab Samples:92629052011, 92629052012
Matrix: Water
AnalyzedMDL
cis-1,3-Dichloropropene ug/L ND 5.0 10/06/22 23:072.0
Dibromochloromethane ug/L ND 5.0 10/06/22 23:072.3
Dibromomethane ug/L ND 5.0 10/06/22 23:071.0
Dichlorodifluoromethane ug/L ND 5.0 10/06/22 23:071.8
Diisopropyl ether ug/L ND 5.0 10/06/22 23:071.4
Ethylbenzene ug/L ND 5.0 10/06/22 23:071.8
Hexachloro-1,3-butadiene ug/L ND 5.0 10/06/22 23:074.8
Isopropylbenzene (Cumene)ug/L ND 5.0 10/06/22 23:072.1
m&p-Xylene ug/L ND 10.0 10/06/22 23:074.1
Methyl-tert-butyl ether ug/L ND 5.0 10/06/22 23:073.1
Methylene Chloride ug/L ND 5.0 10/06/22 23:073.3
n-Butylbenzene ug/L ND 5.0 10/06/22 23:072.3
n-Propylbenzene ug/L ND 5.0 10/06/22 23:072.0
Naphthalene ug/L ND 5.0 10/06/22 23:072.1
o-Xylene ug/L ND 5.0 10/06/22 23:072.0
p-Isopropyltoluene ug/L ND 5.0 10/06/22 23:071.0
sec-Butylbenzene ug/L ND 5.0 10/06/22 23:072.2
Styrene ug/L ND 5.0 10/06/22 23:071.9
tert-Butyl Alcohol ug/L ND 100 10/06/22 23:0711.6
tert-Butylbenzene ug/L ND 5.0 10/06/22 23:070.98
Tetrachloroethene ug/L ND 5.0 10/06/22 23:071.8
Toluene ug/L ND 5.0 10/06/22 23:072.0
trans-1,2-Dichloroethene ug/L ND 5.0 10/06/22 23:072.2
trans-1,3-Dichloropropene ug/L ND 5.0 10/06/22 23:072.2
Trichloroethene ug/L ND 5.0 10/06/22 23:071.8
Trichlorofluoromethane ug/L ND 10.0 10/06/22 23:071.5
Vinyl acetate ug/L ND 10.0 10/06/22 23:075.6
Vinyl chloride ug/L ND 5.0 10/06/22 23:071.8
1,2-Dichloroethane-d4 (S)%96 70-130 10/06/22 23:07
4-Bromofluorobenzene (S)%98 70-130 10/06/22 23:07
Toluene-d8 (S)%107 70-130 10/06/22 23:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3793964LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.250 100 70-130
1,1,1-Trichloroethane ug/L 51.250 102 70-130
1,1,2,2-Tetrachloroethane ug/L 47.950 96 70-130
1,1,2-Trichloroethane ug/L 48.350 97 70-130
1,1-Dichloroethane ug/L 47.650 95 70-130
1,1-Dichloroethene ug/L 51.350 103 70-130
1,1-Dichloropropene ug/L 53.750 107 70-130
1,2,3-Trichlorobenzene ug/L 50.650 101 70-130
1,2,3-Trichloropropane ug/L 49.550 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3793964LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 50.550 101 70-130
1,2,4-Trimethylbenzene ug/L 50.450 101 70-130
1,2-Dibromo-3-chloropropane ug/L 51.250 102 70-131
1,2-Dibromoethane (EDB)ug/L 49.450 99 70-130
1,2-Dichlorobenzene ug/L 50.450 101 70-130
1,2-Dichloroethane ug/L 48.850 98 70-130
1,2-Dichloroethene (Total)ug/L 102
1,2-Dichloropropane ug/L 48.650 97 70-130
1,3,5-Trimethylbenzene ug/L 50.950 102 70-130
1,3-Dichlorobenzene ug/L 51.150 102 70-130
1,3-Dichloropropane ug/L 49.650 99 70-130
1,4-Dichlorobenzene ug/L 50.750 101 70-130
2,2-Dichloropropane ug/L 48.550 97 68-135
2-Butanone (MEK)ug/L 90.0100 90 70-134
2-Chlorotoluene ug/L 48.250 96 70-130
2-Hexanone ug/L 94.5100 94 70-131
4-Chlorotoluene ug/L 48.250 96 70-130
4-Methyl-2-pentanone (MIBK)ug/L 91.0100 91 70-130
Acetone ug/L 96.0100 96 70-133
Benzene ug/L 45.050 90 70-130
Bromobenzene ug/L 48.350 97 70-130
Bromochloromethane ug/L 50.850 102 70-130
Bromodichloromethane ug/L 48.650 97 70-130
Bromoform ug/L 52.050 104 70-130
Bromomethane ug/L 47.850 96 45-151
Carbon tetrachloride ug/L 50.950 102 70-130
Chlorobenzene ug/L 50.550 101 70-130
Chloroethane ug/L 49.150 98 39-152
Chloroform ug/L 49.250 98 70-130
Chloromethane ug/L 52.750 105 58-130
cis-1,2-Dichloroethene ug/L 49.850 100 70-130
cis-1,3-Dichloropropene ug/L 49.150 98 70-130
Dibromochloromethane ug/L 50.550 101 70-130
Dibromomethane ug/L 44.750 89 70-130
Dichlorodifluoromethane ug/L 47.450 95 54-133
Diisopropyl ether ug/L 53.450 107 70-130
Ethylbenzene ug/L 50.450 101 70-130
Hexachloro-1,3-butadiene ug/L 52.750 105 70-135
Isopropylbenzene (Cumene)ug/L 51.150 102 70-130
m&p-Xylene ug/L 100100 100 70-130
Methyl-tert-butyl ether ug/L 52.350 105 70-130
Methylene Chloride ug/L 46.650 93 66-130
n-Butylbenzene ug/L 54.450 109 70-130
n-Propylbenzene ug/L 50.950 102 70-130
Naphthalene ug/L 49.750 99 70-130
o-Xylene ug/L 48.450 97 70-130
p-Isopropyltoluene ug/L 53.650 107 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3793964LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene ug/L 51.850 104 70-130
Styrene ug/L 49.250 98 70-130
tert-Butyl Alcohol ug/L 482500 96 68-134
tert-Butylbenzene ug/L 44.050 88 63-130
Tetrachloroethene ug/L 52.150 104 70-130
Toluene ug/L 46.550 93 70-130
trans-1,2-Dichloroethene ug/L 51.850 104 70-130
trans-1,3-Dichloropropene ug/L 49.550 99 70-130
Trichloroethene ug/L 49.750 99 70-130
Trichlorofluoromethane ug/L 45.550 91 62-130
Vinyl acetate ug/L 104100 104 70-144
Vinyl chloride ug/L 48.450 97 62-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3793965MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92628720001
3793966
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 83 70-14184 2 3020ND16.6 16.9
1,1,1-Trichloroethane ug/L 20 92 70-15098 6 3020ND18.3 19.6
1,1,2,2-Tetrachloroethane ug/L 20 79 69-14283 5 3020ND15.8 16.6
1,1,2-Trichloroethane ug/L 20 82 70-13887 6 3020ND16.3 17.4
1,1-Dichloroethane ug/L 20 83 70-15090 8 3020ND16.6 18.0
1,1-Dichloroethene ug/L 20 92 70-156101 10 3020ND18.4 20.3
1,1-Dichloropropene ug/L 20 97 70-150103 6 3020ND19.4 20.6
1,2,3-Trichlorobenzene ug/L 20 83 70-14894 12 3020ND16.7 18.8
1,2,3-Trichloropropane ug/L 20 81 70-14088 8 3020ND16.1 17.5
1,2,4-Trichlorobenzene ug/L 20 84 70-14689 6 3020ND16.8 17.8
1,2,4-Trimethylbenzene ug/L 20 82 70-14986 4 3020ND16.4 17.1
1,2-Dibromo-3-chloropropane ug/L 20 78 68-14685 9 3020ND15.7 17.1
1,2-Dibromoethane (EDB) ug/L 20 81 70-13887 7 3020ND16.1 17.4
1,2-Dichlorobenzene ug/L 20 77 70-14183 7 3020ND15.5 16.6
1,2-Dichloroethane ug/L 20 83 69-14388 5 3020ND16.7 17.6
1,2-Dichloroethene (Total) ug/L 7 30ND36.0 38.4
1,2-Dichloropropane ug/L 20 85 68-15690 6 3020ND17.0 18.0
1,3,5-Trimethylbenzene ug/L 20 86 70-15390 4 3020ND17.2 17.9
1,3-Dichlorobenzene ug/L 20 84 70-14387 4 3020ND16.8 17.5
1,3-Dichloropropane ug/L 20 79 70-13886 8 3020ND15.8 17.2
1,4-Dichlorobenzene ug/L 20 80 70-14285 6 3020ND16.0 16.9
2,2-Dichloropropane ug/L 20 91 52-17094 4 3020ND18.1 18.8
2-Butanone (MEK)ug/L 40 76 60-15790 17 3040ND30.6 36.1
2-Chlorotoluene ug/L 20 89 70-14784 6 3020ND17.8 16.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3793965MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92628720001
3793966
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Hexanone ug/L 40 83 68-14692 10 3040ND33.3 36.9
4-Chlorotoluene ug/L 20 89 70-14284 6 3020ND17.8 16.7
4-Methyl-2-pentanone
(MIBK)ug/L 40 77 70-14185 10 3040ND30.8 34.1
Acetone ug/L R1409458-157131 33 3040ND37.5 52.4
Benzene ug/L 20 80 70-14283 4 3020ND16.1 16.7
Bromobenzene ug/L 20 81 70-14384 5 3020ND16.1 16.9
Bromochloromethane ug/L 20 84 70-14691 9 3020ND16.7 18.2
Bromodichloromethane ug/L M1208070-13965 14 30206.0 22.0 19.1
Bromoform ug/L 20 80 64-14087 9 3020ND16.0 17.5
Bromomethane ug/L 20 73 28-19290 20 3020ND14.6 17.9
Carbon tetrachloride ug/L 20 92 70-14895 3 3020ND18.3 18.9
Chlorobenzene ug/L 20 85 70-14189 4 3020ND17.1 17.8
Chloroethane ug/L 20 92 58-19197 5 3020ND18.4 19.4
Chloroform ug/L M1,R1205970-148-7 33 302035.2 47.1 33.7
Chloromethane ug/L 20 97 43-162103 7 3020ND19.4 20.7
cis-1,2-Dichloroethene ug/L 20 88 68-15193 5 3020ND17.7 18.6
cis-1,3-Dichloropropene ug/L 20 83 70-13987 5 3020ND16.6 17.5
Dibromochloromethane ug/L 20 81 70-14488 9 3020ND16.7 18.2
Dibromomethane ug/L 20 75 70-13980 6 3020ND15.1 15.9
Dichlorodifluoromethane ug/L 20 91 39-17198 7 3020ND18.3 19.6
Diisopropyl ether ug/L 20 82 67-14294 13 3020ND16.4 18.7
Ethylbenzene ug/L 20 86 70-14392 7 3020ND17.2 18.4
Hexachloro-1,3-butadiene ug/L 20 95 64-163100 5 3020ND18.9 19.9
Isopropylbenzene
(Cumene)ug/L 20 88 70-14590 2 3020ND17.6 18.0
m&p-Xylene ug/L 40 85 70-14490 7 3040ND33.9 36.2
Methyl-tert-butyl ether ug/L 20 85 65-14394 10 3020ND17.0 18.8
Methylene Chloride ug/L 20 84 62-14990 6 3020ND16.9 17.9
n-Butylbenzene ug/L 20 90 65-16397 7 3020ND18.1 19.5
n-Propylbenzene ug/L 20 87 70-15291 4 3020ND17.4 18.2
Naphthalene ug/L 20 79 67-14787 10 3020ND15.8 17.4
o-Xylene ug/L 20 84 70-14590 8 3020ND16.7 18.0
p-Isopropyltoluene ug/L 20 90 70-14797 7 3020ND18.0 19.3
sec-Butylbenzene ug/L 20 89 70-14493 4 3020ND17.8 18.5
Styrene ug/L 20 81 70-14386 6 3020ND16.2 17.2
tert-Butyl Alcohol ug/L 200 84 35-200108 23 30200ND187 235
tert-Butylbenzene ug/L 20 76 62-13377 2 3020ND15.1 15.5
Tetrachloroethene ug/L 20 84 70-14594 10 3020ND16.9 18.7
Toluene ug/L 20 79 70-14288 10 3020ND15.9 17.6
trans-1,2-Dichloroethene ug/L 20 91 70-15199 8 3020ND18.3 19.8
trans-1,3-Dichloropropene ug/L 20 82 70-13989 8 3020ND16.4 17.8
Trichloroethene ug/L 20 88 62-14693 6 3020ND17.6 18.6
Trichlorofluoromethane ug/L 20 85 63-15394 11 3020ND16.9 18.8
Vinyl acetate ug/L 40 83 61-16291 9 3040ND33.1 36.3
Vinyl chloride ug/L 20 88 61-163102 15 3020ND17.7 20.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3793965MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92628720001
3793966
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dichloroethane-d4 (S) %97 70-13099
4-Bromofluorobenzene (S) %101 70-130100
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729070
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92629052011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3796752
Associated Lab Samples:92629052011
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 10/11/22 08:561.7
1,2-Dichlorobenzene ug/L ND 10.0 10/11/22 08:561.8
1,3-Dichlorobenzene ug/L ND 10.0 10/11/22 08:561.6
1,4-Dichlorobenzene ug/L ND 10.0 10/11/22 08:561.7
1-Methylnaphthalene ug/L ND 10.0 10/11/22 08:562.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 10/11/22 08:561.2
2,4,5-Trichlorophenol ug/L ND 10.0 10/11/22 08:561.4
2,4,6-Trichlorophenol ug/L ND 10.0 10/11/22 08:561.6
2,4-Dichlorophenol ug/L ND 10.0 10/11/22 08:561.4
2,4-Dimethylphenol ug/L ND 10.0 10/11/22 08:561.7
2,4-Dinitrophenol ug/L ND 50.0 10/11/22 08:5626.0
2,4-Dinitrotoluene ug/L ND 10.0 10/11/22 08:561.6
2,6-Dinitrotoluene ug/L ND 10.0 10/11/22 08:561.7
2-Chloronaphthalene ug/L ND 10.0 10/11/22 08:561.7
2-Chlorophenol ug/L ND 10.0 10/11/22 08:561.2
2-Methylnaphthalene ug/L ND 10.0 10/11/22 08:561.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 10/11/22 08:561.9
2-Nitroaniline ug/L ND 20.0 10/11/22 08:563.0
2-Nitrophenol ug/L ND 10.0 10/11/22 08:561.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 10/11/22 08:561.2
3,3'-Dichlorobenzidine ug/L ND 20.0 10/11/22 08:568.1
3-Nitroaniline ug/L ND 20.0 10/11/22 08:563.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 10/11/22 08:567.8
4-Bromophenylphenyl ether ug/L ND 10.0 10/11/22 08:561.8
4-Chloro-3-methylphenol ug/L ND 10.0 10/11/22 08:563.3
4-Chloroaniline ug/L ND 20.0 10/11/22 08:563.6
4-Chlorophenylphenyl ether ug/L ND 10.0 10/11/22 08:562.0
4-Nitroaniline ug/L ND 20.0 10/11/22 08:565.1
4-Nitrophenol ug/L ND 50.0 10/11/22 08:566.6
Acenaphthene ug/L ND 10.0 10/11/22 08:562.0
Acenaphthylene ug/L ND 10.0 10/11/22 08:562.0
Aniline ug/L ND 10.0 10/11/22 08:561.6
Anthracene ug/L ND 10.0 10/11/22 08:562.3
Benzo(a)anthracene ug/L ND 10.0 10/11/22 08:562.7
Benzo(a)pyrene ug/L ND 10.0 10/11/22 08:562.8
Benzo(b)fluoranthene ug/L ND 10.0 10/11/22 08:562.6
Benzo(g,h,i)perylene ug/L ND 10.0 10/11/22 08:562.8
Benzo(k)fluoranthene ug/L ND 10.0 10/11/22 08:562.7
Benzoic Acid ug/L ND 50.0 10/11/22 08:5622.0
Benzyl alcohol ug/L ND 20.0 10/11/22 08:562.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3796752
Associated Lab Samples:92629052011
Matrix: Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 10/11/22 08:561.8
bis(2-Chloroethyl) ether ug/L ND 10.0 10/11/22 08:561.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 10/11/22 08:563.7
Butylbenzylphthalate ug/L ND 10.0 10/11/22 08:563.1
Chrysene ug/L ND 10.0 10/11/22 08:562.8
Di-n-butylphthalate ug/L ND 10.0 10/11/22 08:562.2
Di-n-octylphthalate ug/L ND 10.0 10/11/22 08:563.9
Dibenz(a,h)anthracene ug/L ND 10.0 10/11/22 08:563.0
Dibenzofuran ug/L ND 10.0 10/11/22 08:562.1
Diethylphthalate ug/L ND 10.0 10/11/22 08:562.0
Dimethylphthalate ug/L ND 10.0 10/11/22 08:562.1
Fluoranthene ug/L ND 10.0 10/11/22 08:562.2
Fluorene ug/L ND 10.0 10/11/22 08:562.1
Hexachloro-1,3-butadiene ug/L ND 10.0 10/11/22 08:561.8
Hexachlorobenzene ug/L ND 10.0 10/11/22 08:562.2
Hexachlorocyclopentadiene ug/L ND 10.0 10/11/22 08:561.6
Hexachloroethane ug/L ND 10.0 10/11/22 08:561.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 10/11/22 08:562.9
Isophorone ug/L ND 10.0 10/11/22 08:561.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 10/11/22 08:561.3
N-Nitrosodimethylamine ug/L ND 10.0 10/11/22 08:561.9
N-Nitrosodiphenylamine ug/L ND 10.0 10/11/22 08:563.0
Naphthalene ug/L ND 10.0 10/11/22 08:562.1
Nitrobenzene ug/L ND 10.0 10/11/22 08:561.9
Pentachlorophenol ug/L ND 20.0 10/11/22 08:563.8
Phenanthrene ug/L ND 10.0 10/11/22 08:562.0
Phenol ug/L ND 10.0 10/11/22 08:561.4
Pyrene ug/L ND 10.0 10/11/22 08:562.2
2,4,6-Tribromophenol (S)%84 10-144 10/11/22 08:56
2-Fluorobiphenyl (S)%52 10-130 10/11/22 08:56
2-Fluorophenol (S)%52 10-130 10/11/22 08:56
Nitrobenzene-d5 (S)%75 10-144 10/11/22 08:56
Phenol-d6 (S)%42 10-130 10/11/22 08:56
Terphenyl-d14 (S)%102 34-163 10/11/22 08:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3796753LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 24.050 48 18-130
1,2-Dichlorobenzene ug/L 18.150 36 20-130
1,3-Dichlorobenzene ug/L 14.250 28 18-130
1,4-Dichlorobenzene ug/L 15.150 30 18-130
1-Methylnaphthalene ug/L 37.950 76 29-130
2,2'-Oxybis(1-chloropropane)ug/L 34.650 69 28-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3796753LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 44.250 88 35-130
2,4,6-Trichlorophenol ug/L 42.350 85 31-130
2,4-Dichlorophenol ug/L 40.950 82 35-130
2,4-Dimethylphenol ug/L 47.450 95 34-130
2,4-Dinitrophenol ug/L 199250 80 10-153
2,4-Dinitrotoluene ug/L 48.550 97 37-136
2,6-Dinitrotoluene ug/L 47.350 95 33-136
2-Chloronaphthalene ug/L 40.250 80 26-130
2-Chlorophenol ug/L 35.350 71 37-130
2-Methylnaphthalene ug/L 34.450 69 29-130
2-Methylphenol(o-Cresol)ug/L 36.250 72 35-130
2-Nitroaniline ug/L 86.8100 87 37-130
2-Nitrophenol ug/L 39.050 78 32-130
3&4-Methylphenol(m&p Cresol)ug/L 34.950 70 34-130
3,3'-Dichlorobenzidine ug/L 90.6100 91 34-136
3-Nitroaniline ug/L 94.2100 94 37-138
4,6-Dinitro-2-methylphenol ug/L 90.4100 90 21-157
4-Bromophenylphenyl ether ug/L 41.850 84 38-130
4-Chloro-3-methylphenol ug/L 86.3100 86 37-130
4-Chloroaniline ug/L 82.7100 83 38-130
4-Chlorophenylphenyl ether ug/L 41.350 83 33-130
4-Nitroaniline ug/L 94.4100 94 42-137
4-Nitrophenol ug/L 135250 54 10-130
Acenaphthene ug/L 43.750 87 33-130
Acenaphthylene ug/L 42.750 85 35-130
Aniline ug/L 29.650 59 22-130
Anthracene ug/L 43.650 87 48-130
Benzo(a)anthracene ug/L 45.950 92 48-137
Benzo(a)pyrene ug/L 46.950 94 49-138
Benzo(b)fluoranthene ug/L 46.750 93 52-138
Benzo(g,h,i)perylene ug/L 49.750 99 48-140
Benzo(k)fluoranthene ug/L 48.850 98 48-139
Benzoic Acid ug/L 138250 55 10-130
Benzyl alcohol ug/L 75.3100 75 35-130
bis(2-Chloroethoxy)methane ug/L 38.950 78 34-130
bis(2-Chloroethyl) ether ug/L 35.450 71 36-130
bis(2-Ethylhexyl)phthalate ug/L 49.250 98 32-165
Butylbenzylphthalate ug/L 48.750 97 34-161
Chrysene ug/L 46.950 94 47-131
Di-n-butylphthalate ug/L 44.450 89 39-144
Di-n-octylphthalate ug/L 49.550 99 30-170
Dibenz(a,h)anthracene ug/L 48.750 97 49-138
Dibenzofuran ug/L 43.950 88 33-130
Diethylphthalate ug/L 46.650 93 38-131
Dimethylphthalate ug/L 45.050 90 37-130
Fluoranthene ug/L 46.750 93 46-137
Fluorene ug/L 45.350 91 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3796753LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 18.050 36 11-130
Hexachlorobenzene ug/L 43.050 86 38-130
Hexachlorocyclopentadiene ug/L 23.850 48 10-130
Hexachloroethane ug/L 14.150 28 14-130
Indeno(1,2,3-cd)pyrene ug/L 48.150 96 41-130
Isophorone ug/L 41.750 83 33-130
N-Nitroso-di-n-propylamine ug/L 41.350 83 36-130
N-Nitrosodimethylamine ug/L 32.350 65 34-130
N-Nitrosodiphenylamine ug/L 45.050 90 37-130
Naphthalene ug/L 28.450 57 30-130
Nitrobenzene ug/L 35.750 71 36-130
Pentachlorophenol ug/L 88.4100 88 23-149
Phenanthrene ug/L 45.750 91 44-130
Phenol ug/L 24.150 48 18-130
Pyrene ug/L 48.650 97 47-134
2,4,6-Tribromophenol (S)%90 10-144
2-Fluorobiphenyl (S)%61 10-130
2-Fluorophenol (S)%55 10-130
Nitrobenzene-d5 (S)%72 10-144
Phenol-d6 (S)%47 10-130
Terphenyl-d14 (S)%98 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3796754MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92629875004
3796755
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L R190.9 21 10-13032 40 3090.9ND 19.5 29.4
1,2-Dichlorobenzene ug/L 90.9 15 10-13020 3090.9ND 13.5J 18.0J
1,3-Dichlorobenzene ug/L 90.9 10 10-13016 3090.9ND 9.5J 14.3J
1,4-Dichlorobenzene ug/L 90.9 12 10-13017 3090.9ND 11.0J 15.6J
1-Methylnaphthalene ug/L 90.9 51 10-13065 24 3090.9ND 46.2 59.0
2,2'-Oxybis(1-chloropropane)ug/L 90.9 61 12-14266 8 3090.9ND 55.3 60.0
2,4,5-Trichlorophenol ug/L 90.9 78 10-14390 14 3090.9ND 71.3 81.6
2,4,6-Trichlorophenol ug/L 90.9 77 10-14787 13 3090.9ND 69.6 79.0
2,4-Dichlorophenol ug/L 90.9 68 10-13878 13 3090.9ND 62.1 70.9
2,4-Dimethylphenol ug/L 90.9 80 25-13094 16 3090.9ND 72.7 85.4
2,4-Dinitrophenol ug/L 455 54 10-16563 15 30455ND247 286
2,4-Dinitrotoluene ug/L 90.9 88 29-148103 16 3090.9ND 79.7 93.9
2,6-Dinitrotoluene ug/L 90.9 85 26-146102 18 3090.9ND 77.3 92.4
2-Chloronaphthalene ug/L 90.9 60 11-13072 17 3090.9ND 54.9 65.2
2-Chlorophenol ug/L 90.9 60 10-13365 10 3090.9ND 54.1 59.5
2-Methylnaphthalene ug/L 90.9 45 13-13059 26 3090.9ND 40.8 53.2
2-Methylphenol(o-Cresol) ug/L 90.9 63 20-13070 11 3090.9ND 57.0 63.4
2-Nitroaniline ug/L 182 76 24-13690 16 30182ND139 163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3796754MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92629875004
3796755
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitrophenol ug/L 90.9 65 10-15376 15 3090.9ND 59.1 69.0
3&4-Methylphenol(m&p
Cresol)ug/L 90.9 58 16-13065 11 3090.9ND 53.0 59.2
3,3'-Dichlorobenzidine ug/L 182 88 10-15399 11 30182ND160 179
3-Nitroaniline ug/L 182 86 22-151103 18 30182ND157 188
4,6-Dinitro-2-methylphenol ug/L 182 82 10-18098 18 30182ND149 178
4-Bromophenylphenyl ether ug/L 90.9 77 25-13089 15 3090.9ND 69.7 81.0
4-Chloro-3-methylphenol ug/L 182 72 25-13387 19 30182ND131 159
4-Chloroaniline ug/L 182 73 14-13283 13 30182ND133 151
4-Chlorophenylphenyl ether ug/L 90.9 73 19-13084 15 3090.9ND 66.3 76.7
4-Nitroaniline ug/L 182 88 29-150100 13 30182ND160 182
4-Nitrophenol ug/L 455 44 10-13052 16 30455ND202 238
Acenaphthene ug/L 90.9 73 16-13085 14 3090.9ND 66.7 76.9
Acenaphthylene ug/L 90.9 72 15-13783 14 3090.9ND 65.3 75.5
Aniline ug/L 90.9 54 10-13059 10 3090.9ND 48.6 53.7
Anthracene ug/L 90.9 79 37-13693 16 3090.9ND 72.2 84.4
Benzo(a)anthracene ug/L 90.9 91 40-145101 11 3090.9ND 82.4 91.7
Benzo(a)pyrene ug/L 90.9 88 41-146101 14 3090.9ND 79.7 91.7
Benzo(b)fluoranthene ug/L 90.9 88 39-151103 16 3090.9ND 80.2 94.0
Benzo(g,h,i)perylene ug/L 90.9 92 40-147107 14 3090.9ND 84.0 96.8
Benzo(k)fluoranthene ug/L 90.9 89 40-146104 15 3090.9ND 81.3 94.9
Benzoic Acid ug/L 455 23 10-13024 5 30455ND105 111
Benzyl alcohol ug/L 182 63 25-13071 12 30182ND114 129
bis(2-Chloroethoxy)methane ug/L 90.9 67 23-13078 16 3090.9ND 60.8 71.1
bis(2-Chloroethyl) ether ug/L 90.9 65 25-13070 9 3090.9ND 58.8 64.0
bis(2-Ethylhexyl)phthalate ug/L 90.9 97 28-166110 13 3090.9ND 87.9 100
Butylbenzylphthalate ug/L 90.9 99 33-165112 12 3090.9ND 89.8 102
Chrysene ug/L 90.9 92 38-141101 10 3090.9ND 83.3 92.0
Di-n-butylphthalate ug/L 90.9 86 32-15399 14 3090.9ND 78.5 90.2
Di-n-octylphthalate ug/L 90.9 100 30-175114 13 3090.9ND 90.9 104
Dibenz(a,h)anthracene ug/L 90.9 95 39-148107 12 3090.9ND 86.6 97.6
Dibenzofuran ug/L 90.9 76 20-13087 13 3090.9ND 68.9 78.7
Diethylphthalate ug/L 90.9 84 28-14299 17 3090.9ND 75.9 90.0
Dimethylphthalate ug/L 90.9 80 26-13694 15 3090.9ND 73.1 85.2
Fluoranthene ug/L 90.9 90 39-143103 14 3090.9ND 81.6 93.5
Fluorene ug/L 90.9 80 24-13292 14 3090.9ND 72.3 83.3
Hexachloro-1,3-butadiene ug/L M190.9 9 10-13017 3090.9ND 8.3J 15.3J
Hexachlorobenzene ug/L 90.9 80 29-13093 14 3090.9ND 73.1 84.2
Hexachlorocyclopentadiene ug/L R190.9 22 10-13032 38 3090.9ND 19.7 28.8
Hexachloroethane ug/L M190.9 6 10-13011 3090.9ND 5.2J 10.2J
Indeno(1,2,3-cd)pyrene ug/L 90.9 92 39-148106 14 3090.9ND 84.0 96.6
Isophorone ug/L 90.9 73 23-13084 14 3090.9ND 66.7 76.6
N-Nitroso-di-n-propylamine ug/L 90.9 72 25-13079 9 3090.9ND 65.2 71.5
N-Nitrosodimethylamine ug/L 90.9 59 22-13064 7 3090.9ND 53.7 57.9
N-Nitrosodiphenylamine ug/L 90.9 82 26-13496 16 3090.9ND 74.5 87.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3796754MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92629875004
3796755
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Naphthalene ug/L R190.9 32 14-13045 34 3090.9ND 29.3 41.4
Nitrobenzene ug/L 90.9 63 25-13074 15 3090.9ND 57.7 66.9
Pentachlorophenol ug/L 182 78 10-17599 23 30182ND142 179
Phenanthrene ug/L 90.9 84 36-13399 16 3090.9ND 76.6 90.3
Phenol ug/L 90.9 40 10-13043 7 3090.9ND 35.9 38.7
Pyrene ug/L 90.9 94 40-143106 12 3090.9ND 85.2 96.0
2,4,6-Tribromophenol (S) %80 10-14496
2-Fluorobiphenyl (S)%51 10-13053
2-Fluorophenol (S)%43 10-13048
Nitrobenzene-d5 (S)%64 10-14468
Phenol-d6 (S)%38 10-13042
Terphenyl-d14 (S)%92 34-163102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
729746
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92629052001, 92629052002, 92629052003, 92629052004, 92629052005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3799933
Associated Lab Samples:92629052001, 92629052002, 92629052003, 92629052004, 92629052005
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 325 10/13/22 15:07128
1,2-Dichlorobenzene ug/kg ND 325 10/13/22 15:07117
1,3-Dichlorobenzene ug/kg ND 325 10/13/22 15:07115
1,4-Dichlorobenzene ug/kg ND 325 10/13/22 15:07124
1-Methylnaphthalene ug/kg ND 325 10/13/22 15:07114
2,2'-Oxybis(1-chloropropane)ug/kg ND 325 v210/13/22 15:07154
2,4,5-Trichlorophenol ug/kg ND 325 10/13/22 15:07149
2,4,6-Trichlorophenol ug/kg ND 325 10/13/22 15:07134
2,4-Dichlorophenol ug/kg ND 325 10/13/22 15:07127
2,4-Dimethylphenol ug/kg ND 325 10/13/22 15:07135
2,4-Dinitrophenol ug/kg ND 1620 10/13/22 15:071000
2,4-Dinitrotoluene ug/kg ND 325 10/13/22 15:07125
2,6-Dinitrotoluene ug/kg ND 325 10/13/22 15:07119
2-Chloronaphthalene ug/kg ND 325 10/13/22 15:07129
2-Chlorophenol ug/kg ND 325 10/13/22 15:07122
2-Methylnaphthalene ug/kg ND 325 10/13/22 15:07130
2-Methylphenol(o-Cresol)ug/kg ND 325 10/13/22 15:07133
2-Nitroaniline ug/kg ND 1620 10/13/22 15:07266
2-Nitrophenol ug/kg ND 325 10/13/22 15:07141
3&4-Methylphenol(m&p Cresol)ug/kg ND 325 10/13/22 15:07131
3,3'-Dichlorobenzidine ug/kg ND 649 10/13/22 15:07219
3-Nitroaniline ug/kg ND 1620 10/13/22 15:07255
4,6-Dinitro-2-methylphenol ug/kg ND 649 10/13/22 15:07303
4-Bromophenylphenyl ether ug/kg ND 325 v110/13/22 15:07125
4-Chloro-3-methylphenol ug/kg ND 649 10/13/22 15:07228
4-Chloroaniline ug/kg ND 649 10/13/22 15:07255
4-Chlorophenylphenyl ether ug/kg ND 325 10/13/22 15:07121
4-Nitroaniline ug/kg ND 649 v210/13/22 15:07247
4-Nitrophenol ug/kg ND 1620 10/13/22 15:07628
Acenaphthene ug/kg ND 325 10/13/22 15:07114
Acenaphthylene ug/kg ND 325 10/13/22 15:07114
Aniline ug/kg ND 325 10/13/22 15:07127
Anthracene ug/kg ND 325 10/13/22 15:07106
Benzo(a)anthracene ug/kg ND 325 10/13/22 15:07108
Benzo(a)pyrene ug/kg ND 325 10/13/22 15:07112
Benzo(b)fluoranthene ug/kg ND 325 10/13/22 15:07108
Benzo(g,h,i)perylene ug/kg ND 325 10/13/22 15:07126
Benzo(k)fluoranthene ug/kg ND 325 10/13/22 15:07114
Benzoic Acid ug/kg ND 1620 10/13/22 15:07697
Benzyl alcohol ug/kg ND 649 10/13/22 15:07246
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3799933
Associated Lab Samples:92629052001, 92629052002, 92629052003, 92629052004, 92629052005
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 325 10/13/22 15:07135
bis(2-Chloroethyl) ether ug/kg ND 325 10/13/22 15:07122
bis(2-Ethylhexyl)phthalate ug/kg ND 325 10/13/22 15:07126
Butylbenzylphthalate ug/kg ND 325 10/13/22 15:07137
Chrysene ug/kg ND 325 10/13/22 15:07118
Di-n-butylphthalate ug/kg ND 325 10/13/22 15:07109
Di-n-octylphthalate ug/kg ND 325 10/13/22 15:07128
Dibenz(a,h)anthracene ug/kg ND 325 10/13/22 15:07125
Dibenzofuran ug/kg ND 325 10/13/22 15:07117
Diethylphthalate ug/kg ND 325 10/13/22 15:07119
Dimethylphthalate ug/kg ND 325 10/13/22 15:07118
Fluoranthene ug/kg ND 325 10/13/22 15:07111
Fluorene ug/kg ND 325 10/13/22 15:07114
Hexachloro-1,3-butadiene ug/kg ND 325 v110/13/22 15:07141
Hexachlorobenzene ug/kg ND 325 10/13/22 15:07127
Hexachlorocyclopentadiene ug/kg ND 325 10/13/22 15:07186
Hexachloroethane ug/kg ND 325 10/13/22 15:07124
Indeno(1,2,3-cd)pyrene ug/kg ND 325 10/13/22 15:07128
Isophorone ug/kg ND 325 10/13/22 15:07145
N-Nitroso-di-n-propylamine ug/kg ND 325 10/13/22 15:07122
N-Nitrosodimethylamine ug/kg ND 325 10/13/22 15:07109
N-Nitrosodiphenylamine ug/kg ND 325 10/13/22 15:07115
Naphthalene ug/kg ND 325 10/13/22 15:07110
Nitrobenzene ug/kg ND 325 10/13/22 15:07150
Pentachlorophenol ug/kg ND 649 10/13/22 15:07318
Phenanthrene ug/kg ND 325 10/13/22 15:07106
Phenol ug/kg ND 325 10/13/22 15:07145
Pyrene ug/kg ND 325 10/13/22 15:07132
Pyridine ug/kg ND 325 10/13/22 15:07102
2,4,6-Tribromophenol (S)%70 10-131 10/13/22 15:07
2-Fluorobiphenyl (S)%60 10-130 10/13/22 15:07
2-Fluorophenol (S)%56 10-130 10/13/22 15:07
Nitrobenzene-d5 (S)%63 10-130 10/13/22 15:07
Phenol-d6 (S)%55 10-130 10/13/22 15:07
Terphenyl-d14 (S)%69 10-130 10/13/22 15:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799934LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13601650 82 43-130
1,2-Dichlorobenzene ug/kg 11401650 69 43-130
1,3-Dichlorobenzene ug/kg 11001650 66 43-130
1,4-Dichlorobenzene ug/kg 11001650 67 44-130
1-Methylnaphthalene ug/kg 12701650 77 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799934LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 674 v2165041 29-130
2,4,5-Trichlorophenol ug/kg 12601650 77 47-130
2,4,6-Trichlorophenol ug/kg 13601650 82 47-130
2,4-Dichlorophenol ug/kg 13501650 82 45-130
2,4-Dimethylphenol ug/kg 14901650 90 45-130
2,4-Dinitrophenol ug/kg 61608250 75 27-140
2,4-Dinitrotoluene ug/kg 13001650 79 46-130
2,6-Dinitrotoluene ug/kg 12901650 78 48-130
2-Chloronaphthalene ug/kg 12401650 75 46-130
2-Chlorophenol ug/kg 10701650 65 43-130
2-Methylnaphthalene ug/kg 12201650 74 47-130
2-Methylphenol(o-Cresol)ug/kg 11301650 68 42-130
2-Nitroaniline ug/kg 25103300 76 41-130
2-Nitrophenol ug/kg 12001650 73 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 11101650 67 39-130
3,3'-Dichlorobenzidine ug/kg 23903300 72 41-130
3-Nitroaniline ug/kg 20703300 63 37-130
4,6-Dinitro-2-methylphenol ug/kg 26603300 81 38-141
4-Bromophenylphenyl ether ug/kg 1470 v1165089 47-130
4-Chloro-3-methylphenol ug/kg 27303300 83 44-130
4-Chloroaniline ug/kg 22703300 69 41-130
4-Chlorophenylphenyl ether ug/kg 14601650 89 45-130
4-Nitroaniline ug/kg 2070 v2330063 42-130
4-Nitrophenol ug/kg 71508250 87 39-131
Acenaphthene ug/kg 12401650 75 49-130
Acenaphthylene ug/kg 12901650 78 50-130
Aniline ug/kg 9511650 58 38-130
Anthracene ug/kg 12101650 73 49-130
Benzo(a)anthracene ug/kg 13401650 81 51-130
Benzo(a)pyrene ug/kg 14101650 86 51-130
Benzo(b)fluoranthene ug/kg 13401650 81 49-130
Benzo(g,h,i)perylene ug/kg 11401650 69 48-140
Benzo(k)fluoranthene ug/kg 12801650 78 51-130
Benzoic Acid ug/kg 33508250 41 22-130
Benzyl alcohol ug/kg 24103300 73 43-130
bis(2-Chloroethoxy)methane ug/kg 11801650 71 43-130
bis(2-Chloroethyl) ether ug/kg 10601650 65 42-130
bis(2-Ethylhexyl)phthalate ug/kg 12301650 74 43-130
Butylbenzylphthalate ug/kg 12301650 74 44-131
Chrysene ug/kg 13301650 80 51-130
Di-n-butylphthalate ug/kg 11801650 71 46-130
Di-n-octylphthalate ug/kg 12501650 75 45-130
Dibenz(a,h)anthracene ug/kg 11901650 72 48-130
Dibenzofuran ug/kg 13901650 84 10-130
Diethylphthalate ug/kg 12701650 77 48-130
Dimethylphthalate ug/kg 12601650 76 48-130
Fluoranthene ug/kg 13201650 80 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3799934LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 13201650 80 48-130
Hexachloro-1,3-butadiene ug/kg 1330 v1165080 39-130
Hexachlorobenzene ug/kg 13901650 85 47-130
Hexachlorocyclopentadiene ug/kg 12001650 73 17-130
Hexachloroethane ug/kg 10901650 66 40-130
Indeno(1,2,3-cd)pyrene ug/kg 11901650 72 50-130
Isophorone ug/kg 12001650 73 41-130
N-Nitroso-di-n-propylamine ug/kg 12601650 76 36-130
N-Nitrosodimethylamine ug/kg 11101650 67 34-130
N-Nitrosodiphenylamine ug/kg 12801650 78 48-130
Naphthalene ug/kg 11501650 70 46-130
Nitrobenzene ug/kg 13401650 81 39-130
Pentachlorophenol ug/kg 23803300 72 42-130
Phenanthrene ug/kg 12801650 78 50-130
Phenol ug/kg 10801650 66 42-130
Pyrene ug/kg 13801650 84 50-130
Pyridine ug/kg 9571650 58 26-130
2,4,6-Tribromophenol (S)%80 10-131
2-Fluorobiphenyl (S)%75 10-130
2-Fluorophenol (S)%68 10-130
Nitrobenzene-d5 (S)%77 10-130
Phenol-d6 (S)%70 10-130
Terphenyl-d14 (S)%77 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629052001
3799936SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND v230ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629052001
3799936SAMPLE DUPLICATE:
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND v130ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629052001
3799936SAMPLE DUPLICATE:
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6064
2-Fluorobiphenyl (S)%6256
2-Fluorophenol (S)%6451
Nitrobenzene-d5 (S)%7765
Phenol-d6 (S)%6351
Terphenyl-d14 (S)%6062
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
727841
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92629052001, 92629052002, 92629052003, 92629052004, 92629052005, 92629052006, 92629052007,
92629052008, 92629052009
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92628385001
3790423SAMPLE DUPLICATE:
Percent Moisture %15.7 N212515.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92629052009
3790424SAMPLE DUPLICATE:
Percent Moisture %14.8 N272513.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 72
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
727882
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92629052010
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92627255001
3790586SAMPLE DUPLICATE:
Percent Moisture %26.0 N2132529.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 72
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92629052
ROTARY DRIVE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Result confirmed by second analysis.C0
Analyte is a possible laboratory contaminant (not present in method blank).C7
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 72
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92629052
ROTARY DRIVE
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92629052011 729336 729409EQ BLANK EPA 3010A EPA 6010D
92629052001 862699 862743HA-C EPA 3050 EPA 6010
92629052002 862699 862743HA-D EPA 3050 EPA 6010
92629052003 862699 862743HA-D-DUP EPA 3050 EPA 6010
92629052004 862699 862743HA-A EPA 3050 EPA 6010
92629052005 862699 862743HA-B EPA 3050 EPA 6010
92629052011 730879 730958EQ BLANK EPA 7470A EPA 7470A
92629052001 862776 862870HA-C EPA 7471 EPA 7471
92629052002 862776 862870HA-D EPA 7471 EPA 7471
92629052003 862776 862870HA-D-DUP EPA 7471 EPA 7471
92629052004 862776 862870HA-A EPA 7471 EPA 7471
92629052005 862776 862870HA-B EPA 7471 EPA 7471
92629052011 729070 729274EQ BLANK EPA 3510C EPA 8270E
92629052001 729746 730025HA-C EPA 3546 EPA 8270E
92629052002 729746 730025HA-D EPA 3546 EPA 8270E
92629052003 729746 730025HA-D-DUP EPA 3546 EPA 8270E
92629052004 729746 730025HA-A EPA 3546 EPA 8270E
92629052005 729746 730025HA-B EPA 3546 EPA 8270E
92629052006 727781 727926HA-3C EPA 5035A/5030B EPA 8260D
92629052007 727781 727926HA-5D EPA 5035A/5030B EPA 8260D
92629052008 727781 727926HA-5D-DUP EPA 5035A/5030B EPA 8260D
92629052009 727781 727926HA-3A EPA 5035A/5030B EPA 8260D
92629052010 727781 727926HA-1B EPA 5035A/5030B EPA 8260D
92629052011 728501EQ BLANK EPA 8260D
92629052012 728501TRIP BLANK EPA 8260D
92629052001 727841HA-C SW-846
92629052002 727841HA-D SW-846
92629052003 727841HA-D-DUP SW-846
92629052004 727841HA-A SW-846
92629052005 727841HA-B SW-846
92629052006 727841HA-3C SW-846
92629052007 727841HA-5D SW-846
92629052008 727841HA-5D-DUP SW-846
92629052009 727841HA-3A SW-846
92629052010 727882HA-1B SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/18/2022 06:19 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 72
Page 70 of 72
Page 71 of 72
Page 72 of 72