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HomeMy WebLinkAboutAlamac_Lumberton_VOC_Data_0110138_FINAL_11_17_10_1116Case Narrative PRI S M Full -Service Analytical & JI I Environmental Solutions LABORATORIES, INC. Solutions-IES, Inc. Sean K. Jarvah 1101 Nowell Road Raleigh, NC 27607 NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert No. 37735 Project: Alamac Lab Submittal Date: 11/03/2010 Prism Work Order: 0110138 11 /17/2010 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a-,--.1 VP Laboratory Services Data Qualifiers Key Reference: Reviewed By J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 18 Sample Receipt Summary &GIE R I IS M Full -Service Analytical R Environmental Solutions 11/17/2010 LABORATORIES, INC. Prism Work Order: 0110138 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received RW-1 0110138-01 Water 11/02/10 11/03/10 RW-2 0110138-02 Water 11/02/10 11/03/10 RW-3 0110138-03 Water 11/02/10 11/03/10 2237 0110138-04 Water 11/02/10 11/03/10 TRIP BLANK 0110138-05 Water 11/02/10 11/03/10 Samples received in good condition at 3.1 degrees C unless otherwise noted. Summary of Detections R I S M Full -Service Analytical & �P Environmental Solutions 11/17/2010 LABORATORIES, INa Prism Work Order: 0110138 Prism ID Client ID Parameter Method Result Units 0110138-01 RW-1 cis- 1,2-Dichloroethylene 8260E 5600 ug/L 0110138-01 RW-1 Tetrachloroethylene 8260B 470 ug/L 0110138-01 RW-1 Trichloroethylene 8260B 1100 ug/L 0110138-01 RW-1 Vinyl chloride 8260E 120 .1 ug/L 0110138-02 RW-2 cis- 1,2-Dichloroethylene 8260E 13000 ug/L 0110138-02 RW-2 Tetrachloroethylene 8260E 150 ug/L 0110138-02 RW-2 trans- 1,2-Dichloroethylene 8260E 84 1 ug/L 0110138-02 RW-2 Trichloroethylene 8260E 660 ug/L 0110138-02 RW-2 Vinyl chloride 8260B 830 ug/L 0110138-03 RW-3 cis- 1,2-Dichloroethylene 8260B 1300 ug/L 0110138-03 RW-3 trans- 1,2-Dichloroethylene 8260B 8.9 J ug/L 0110138-03 RW-3 Trichloroethylene 8260E 12 .1 ug/L 0110138-03 RW-3 Vinyl chloride 8260E 150 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 18 PRISM Fun -Service Analytical & Laboratory Report Environmental Solutions 11/17/2010 & I LABORATORIES, INC. Solutions-IES, Inc. Project: Alamac Client Sample ID: RW-1 Attn: Sean K. Jarvah Prism Sample ID: 0110138-01 1101 Nowell Road Prism Work Order: 0110138 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:02 Time Submitted: 11/03/10 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL ug/L 100 15 100 8260B 11/9/10 13:58 LMW POK0222 1,1,1-Trichloroethane BRL ug/L 100 6.3 100 8260B 11/9/10 13:58 LMW POK0222 1,1,2,2-Tetrachloroethane BRL ug/L 100 7.1 100 8260B 11/9/10 13:58 LMW POK0222 1,1,2-Trichloroethane BRL ug/L 100 17 100 8260B 11/9/10 13:58 LMW POK0222 1,1-Dichloroethane BRL ug/L 100 9.6 100 8260B 11/9/10 13:58 LMW POK0222 1,1-Dichloroethylene BRL ug/L 100 7.8 100 8260E 11/9/10 13:58 LMW POK0222 1,1-Dichloropropylene BRL ug/L 100 6.1 100 8260E 11/9/10 13:58 LMW POK0222 1,2,3-Trichlorobenzene BRL ug/L 200 20 100 8260E 11/9/10 13:58 LMW POK0222 1,2,3-Trichloropropane BRL ug/L 100 8.1 100 8260B 11/9/10 13:58 LMW POK0222 1,2,4-Trichlorobenzene BRL ug/L 100 10 100 8260E 11/9/10 13:58 LMW POK0222 1,2,4-Trimethyl benzene BRL ug/L 100 4.8 100 8260E 11/9/10 13:58 LMW POK0222 1,2-Dibromo-3-chloropropane BRL ug/L 200 59 100 8260E 11/9/10 13:58 LMW POK0222 1,2-Dibromoethane BRL ug/L 100 14 100 8260B 11/9/10 13:58 LMW POK0222 1,2-Dichlorobenzene BRL ug/L 100 7.6 100 8260B 11/9/10 13:58 LMW POK0222 1,2-Dichloroethane BRL ug/L 100 14 100 8260B 11/9/10 13:58 LMW POK0222 1,2-Dichloropropane BRL ug/L 100 13 100 8260B 11/9/10 13:58 LMW POK0222 1,3,5-Trimethyl benzene BRL ug/L 100 5.7 100 8260B 11/9/10 13:58 LMW POK0222 1,3-Dichlorobenzene BRL ug/L 100 7.4 100 8260E 11/9/10 13:58 LMW POK0222 1,3-Dichloropropane BRL ug/L 100 11 100 8260E 11/9/10 13:58 LMW POK0222 1,4-Dichlorobenzene BRL ug/L 100 6.8 100 8260E 11/9/10 13:58 LMW POK0222 2,2-Dichloropropane BRL ug/L 200 11 100 8260B 11/9/10 13:58 LMW POK0222 2-Chloroethyl Vinyl Ether BRL ug/L 200 22 100 8260E 11/9/10 13:58 LMW POK0222 2-Chlorotoluene BRL ug/L 100 3.8 100 8260E 11/9/10 13:58 LMW POK0222 4-Chlorotoluene BRL ug/L 100 5.3 100 8260E 11/9/10 13:58 LMW POK0222 4-Isopropyltoluene BRL ug/L 100 6.5 100 8260B 11/9/10 13:58 LMW POK0222 Acetone BRL ug/L 1000 62 100 8260B 11/9/10 13:58 LMW POK0222 Acrolein BRL ug/L 10000 110 100 8260B 11/9/10 13:58 LMW POK0222 Acrylonitrile BRL ug/L 10000 86 100 8260B 11/9/10 13:58 LMW POK0222 Benzene BRL ug/L 100 7.2 100 8260B 11/9/10 13:58 LMW POK0222 Bromobenzene BRL ug/L 100 6.4 100 8260E 11/9/10 13:58 LMW POK0222 Bromochloromethane BRL ug/L 100 13 100 8260E 11/9/10 13:58 LMW POK0222 Bromodichloromethane BRL ug/L 100 6.2 100 8260E 11/9/10 13:58 LMW POK0222 Bromoform BRL ug/L 100 27 100 8260B 11/9/10 13:58 LMW POK0222 Bromomethane BRL ug/L 300 47 100 8260E 11/9/10 13:58 LMW POK0222 Carbon disulfide BRL ug/L 500 140 100 8260E 11/9/10 13:58 LMW POK0222 Carbon Tetrachloride BRL ug/L 200 12 100 8260E 11/9/10 13:58 LMW POK0222 Chlorobenzene BRL ug/L 100 6.1 100 8260B 11/9/10 13:58 LMW POK0222 Chloroethane BRL ug/L 500 13 100 8260B 11/9/10 13:58 LMW POK0222 Chloroform BRL ug/L 100 8.9 100 8260B 11/9/10 13:58 LMW POK0222 Chloromethane BRL ug/L 200 11 100 8260B 11/9/10 13:58 LMW POK0222 cis-1,2-Dichloroethylene 5600 ug/L 100 7.6 100 8260B 1119/10 13:58 LMW POK0222 cis-1,3-Dichloropropylene BRL ug/L 100 10 100 8260B 11/9/10 13:58 LMW POK0222 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 18 P R S M Laboratory Report Full -Service Analytical & Environmental Solutions 11/17/2010 LABORATORIES INC. Solutions-IES, Inc. Project: Alamac Client Sample ID: RW-1 Attn: Sean K. Jarvah Prism Sample ID: 0110138-01 1101 Nowell Road Prism Work Order: 0110138 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:02 Time Submitted: 11/03/10 15:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dibromochloromethane BRL ug/L 100 30 100 8260E 11/9/10 13:58 LMW POK0222 Dibromomethane BRL ug/L 100 13 100 8260E 11/9/10 13:58 LMW POK0222 Dichlorodifluoromethane BRL ug/L 200 11 100 8260E 11/9/10 13:58 LMW POK0222 Ethylbenzene BRL ug/L 100 6.7 100 8260B 11/9/10 13:58 LMW POK0222 Hexachlorobutadiene BRL ug/L 200 36 100 8260E 11/9/10 13:58 LMW POK0222 Isopropyl Ether BRL ug/L 100 4.3 100 8260E 11/9/10 13:58 LMW POK0222 Isopropylbenzene (Cumene) BRL ug/L 100 7.2 100 8260E 11/9/10 13:58 LMW POK0222 m,p-Xylenes BRL ug/L 200 8.1 100 8260B 11/9/10 13:58 LMW POK0222 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 500 19 100 8260B 11/9/10 13:58 LMW POK0222 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 500 90 100 8260B 11/9/10 13:58 LMW POK0222 Methyl Isobutyl Ketone BRL ug/L 500 12 100 8260B 11/9/10 13:58 LMW POK0222 Methylene Chloride BRL ug/L 200 44 100 8260B 11/9/10 13:58 LMW POK0222 Methyl-tert-Butyl Ether BRL ug/L 100 7.0 100 8260E 11/9/10 13:58 LMW POK0222 Naphthalene BRL ug/L 100 9.8 100 8260E 11/9/10 13:58 LMW POK0222 n-Butylbenzene BRL ug/L 100 11 100 8260E 11/9/10 13:58 LMW POK0222 n-Propylbenzene BRL ug/L 100 6.0 100 8260B 11/9/10 13:58 LMW POK0222 o-Xylene BRL ug/L 100 4.6 100 8260E 11/9/10 13:58 LMW POK0222 sec-Butylbenzene BRL ug/L 100 8.7 100 8260E 11/9/10 13:58 LMW POK0222 Styrene BRL ug/L 100 4.7 100 8260E 11/9/10 13:58 LMW POK0222 tert-Butylbenzene BRL ug/L 100 8.0 100 8260B 11/9/10 13:58 LMW POK0222 Tetrachloroethylene 470 ug/L 100 6.9 100 8260B 11/9/10 13:58 LMW POK0222 Toluene BRL ug/L 100 4.2 100 8260E 11/9/10 13:58 LMW POK0222 trans-1,2-Dichloroethylene BRL ug/L 200 12 100 8260E 11/9/10 13:58 LMW POK0222 trans-1,3-Dichloropropylene BRL ug/L 100 4.3 100 8260B 11/9/10 13:58 LMW POK0222 Trichloroethylene 1100 ug/L 200 5.4 100 8260B 11/9/10 13:58 LMW POK0222 Trichlorofluoromethane BRL ug/L 200 8.8 100 8260E 11/9/10 13:58 LMW POK0222 Vinyl acetate BRL ug/L 2000 10 100 8260E 11/9/10 13:58 LMW POK0222 Vinyl chloride 120 J ug/L 200 16 100 8260B 11/9/10 13:58 LMW POK0222 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 80-124 Dibromofluoromethane 100 % 75-129 Toluene-d8 94 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 18 P R S M Laboratory Report Full -Service Analytical & Environmental Solutions 11/17/2010 LABORATORIES INC. Solutions-IES, Inc. Project: Alamac Client Sample ID: RW-2 Attn: Sean K. Jarvah Prism Sample ID: 0110138-02 1101 Nowell Road Prism Work Order: 0110138 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:04 Time Submitted: 11/03/10 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 100 15 100 8260B 11/9/10 10:54 LMW POK0222 1,1,1-Trichloroethane BRL ug/L 100 6.3 100 8260B 11/9/10 10:54 LMW POK0222 1,1,2,2-Tetrachloroethane BRL ug/L 100 7.1 100 8260E 11/9/10 10:54 LMW POK0222 1,1,2-Trichloroethane BRL ug/L 100 17 100 8260E 11/9/10 10:54 LMW POK0222 1,1-Dichloroethane BRL ug/L 100 9.6 100 8260E 11/9/10 10:54 LMW POK0222 1,1-Dichloroethylene BRL ug/L 100 7.8 100 8260E 11/9/10 10:54 LMW POK0222 1,1-Dichloropropylene BRL ug/L 100 6.1 100 8260E 11/9/10 10:54 LMW POK0222 1,2,3-Trichlorobenzene BRL ug/L 200 20 100 8260E 11/9/10 10:54 LMW POK0222 1,2,3-Trichloropropane BRL ug/L 100 8.1 100 8260B 11/9/10 10:54 LMW POK0222 1,2,4-Trichlorobenzene BRL ug/L 100 10 100 8260B 11/9/10 10:54 LMW POK0222 1,2,4-Trimethyl benzene BRL ug/L 100 4.8 100 8260B 11/9/10 10:54 LMW POK0222 1,2-Dibromo-3-chloropropane BRL ug/L 200 59 100 8260B 11/9/10 10:54 LMW POK0222 1,2-Dibromoethane BRL ug/L 100 14 100 8260B 11/9/10 10:54 LMW POK0222 1,2-Dichlorobenzene BRL ug/L 100 7.6 100 8260B 11/9/10 10:54 LMW POK0222 1,2-Dichloroethane BRL ug/L 100 14 100 8260E 11/9/10 10:54 LMW POK0222 1,2-Dichloropropane BRL ug/L 100 13 100 8260E 11/9/10 10:54 LMW POK0222 1,3,5-Trimethyl benzene BRL ug/L 100 5.7 100 8260E 11/9/10 10:54 LMW POK0222 1,3-Dichlorobenzene BRL ug/L 100 7.4 100 8260E 11/9/10 10:54 LMW POK0222 1,3-Dichloropropane BRL ug/L 100 11 100 8260E 11/9/10 10:54 LMW POK0222 1,4-Dichlorobenzene BRL ug/L 100 6.8 100 8260E 11/9/10 10:54 LMW POK0222 2,2-Dichloropropane BRL ug/L 200 11 100 8260B 11/9/10 10:54 LMW POK0222 2-Chloroethyl Vinyl Ether BRL ug/L 200 22 100 8260B 11/9/10 10:54 LMW POK0222 2-Chlorotoluene BRL ug/L 100 3.8 100 8260B 11/9/10 10:54 LMW POK0222 4-Chlorotoluene BRL ug/L 100 5.3 100 8260B 11/9/10 10:54 LMW POK0222 4-Isopropyltoluene BRL ug/L 100 6.5 100 8260B 11/9/10 10:54 LMW POK0222 Acetone BRL ug/L 1000 62 100 8260B 11/9/10 10:54 LMW POK0222 Acrolein BRL ug/L 10000 110 100 8260E 11/9/10 10:54 LMW POK0222 Acrylonitrile BRL ug/L 10000 86 100 8260E 11/9/10 10:54 LMW POK0222 Benzene BRL ug/L 100 7.2 100 8260E 11/9/10 10:54 LMW POK0222 Bromobenzene BRL ug/L 100 6.4 100 8260E 11/9/10 10:54 LMW POK0222 Bromochloromethane BRL ug/L 100 13 100 8260E 11/9/10 10:54 LMW POK0222 Bromodichloromethane BRL ug/L 100 6.2 100 8260E 11/9/10 10:54 LMW POK0222 Bromoform BRL ug/L 100 27 100 8260B 11/9/10 10:54 LMW POK0222 Bromomethane BRL ug/L 300 47 100 8260B 11/9/10 10:54 LMW POK0222 Carbon disulfide BRL ug/L 500 140 100 8260B 11/9/10 10:54 LMW POK0222 Carbon Tetrachloride BRL ug/L 200 12 100 8260B 11/9/10 10:54 LMW POK0222 Chlorobenzene BRL ug/L 100 6.1 100 8260B 11/9/10 10:54 LMW POK0222 Chloroethane BRL ug/L 500 13 100 8260B 11/9/10 10:54 LMW POK0222 Chloroform BRL ug/L 100 8.9 100 8260E 11/9/10 10:54 LMW POK0222 Chloromethane BRL ug/L 200 11 100 8260E 11/9/10 10:54 LMW POK0222 cis-1,2-Dichloroethylene 13000 ug/L 1000 76 1000 8260B 11/9/10 14:24 LMW POK0222 cis-1,3-Dichloropropylene BRL ug/L 100 10 100 8260B 11/9/10 10:54 LMW POK0222 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 18 P R S M Laboratory Report Full -Service Analytical & Environmental Solutions 11/17/2010 LABORATORIES INC. Solutions-IES, Inc. Project: Alamac Client Sample ID: RW-2 Attn: Sean K. Jarvah Prism Sample ID: 0110138-02 1101 Nowell Road Prism Work Order: 0110138 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:04 Time Submitted: 11/03/10 15:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dibromochloromethane BRL ug/L 100 30 100 8260E 11/9/10 10:54 LMW POK0222 Dibromomethane BRL ug/L 100 13 100 8260E 11/9/10 10:54 LMW POK0222 Dichlorodifluoromethane BRL ug/L 200 11 100 8260E 11/9/10 10:54 LMW POK0222 Ethylbenzene BRL ug/L 100 6.7 100 8260B 11/9/10 10:54 LMW POK0222 Hexachlorobutadiene BRL ug/L 200 36 100 8260E 11/9/10 10:54 LMW POK0222 Isopropyl Ether BRL ug/L 100 4.3 100 8260E 11/9/10 10:54 LMW POK0222 Isopropylbenzene (Cumene) BRL ug/L 100 7.2 100 8260E 11/9/10 10:54 LMW POK0222 m,p-Xylenes BRL ug/L 200 8.1 100 8260B 11/9/10 10:54 LMW POK0222 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 500 19 100 8260B 11/9/10 10:54 LMW POK0222 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 500 90 100 8260B 11/9/10 10:54 LMW POK0222 Methyl Isobutyl Ketone BRL ug/L 500 12 100 8260B 11/9/10 10:54 LMW POK0222 Methylene Chloride BRL ug/L 200 44 100 8260B 11/9/10 10:54 LMW POK0222 Methyl-tert-Butyl Ether BRL ug/L 100 7.0 100 8260E 11/9/10 10:54 LMW POK0222 Naphthalene BRL ug/L 100 9.8 100 8260E 11/9/10 10:54 LMW POK0222 n-Butylbenzene BRL ug/L 100 11 100 8260E 11/9/10 10:54 LMW POK0222 n-Propylbenzene BRL ug/L 100 6.0 100 8260B 11/9/10 10:54 LMW POK0222 o-Xylene BRL ug/L 100 4.6 100 8260E 11/9/10 10:54 LMW POK0222 sec-Butylbenzene BRL ug/L 100 8.7 100 8260E 11/9/10 10:54 LMW POK0222 Styrene BRL ug/L 100 4.7 100 8260E 11/9/10 10:54 LMW POK0222 tert-Butylbenzene BRL ug/L 100 8.0 100 8260B 11/9/10 10:54 LMW POK0222 Tetrachloroethylene 150 ug/L 100 6.9 100 8260B 11/9/10 10:54 LMW POK0222 Toluene BRL ug/L 100 4.2 100 8260E 11/9/10 10:54 LMW POK0222 trans-1,2-Dichloroethylene 84 J ug/L 200 12 100 8260E 11/9/10 10:54 LMW POK0222 trans-1,3-Dichloropropylene BRL ug/L 100 4.3 100 8260B 11/9/10 10:54 LMW POK0222 Trichloroethylene 660 ug/L 200 5.4 100 8260B 11/9/10 10:54 LMW POK0222 Trichlorofluoromethane BRL ug/L 200 8.8 100 8260E 11/9/10 10:54 LMW POK0222 Vinyl acetate BRL ug/L 2000 10 100 8260E 11/9/10 10:54 LMW POK0222 Vinyl chloride 830 ug/L 200 16 100 8260B 11/9/10 10:54 LMW POK0222 Surrogate Recovery Control Limits 4-Bromofluorobenzene 98 % 80-124 Dibromofluoromethane 107 % 75-129 Toluene-d8 94 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 18 P R S M Laboratory Report Full -Service Analytical & Environmental Solutions 11/17/2010 LABORATORIES INC. Solutions-IES, Inc. Project: Alamac Client Sample ID: RW-3 Attn: Sean K. Jarvah Prism Sample ID: 0110138-03 1101 Nowell Road Prism Work Order: 0110138 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:06 Time Submitted: 11/03/10 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 10 1.5 10 8260B 11/9/10 10:28 LMW POK0222 1,1,1-Trichloroethane BRL ug/L 10 0.63 10 8260B 11/9/10 10:28 LMW POK0222 1,1,2,2-Tetrachloroethane BRL ug/L 10 0.71 10 8260B 11/9/10 10:28 LMW POK0222 1,1,2-Trichloroethane BRL ug/L 10 1.7 10 8260B 11/9/10 10:28 LMW POK0222 1,1-Dichloroethane BRL ug/L 10 0.96 10 8260B 11/9/10 10:28 LMW POK0222 1,1-Dichloroethylene BRL ug/L 10 0.78 10 8260B 11/9/10 10:28 LMW POK0222 1,1-Dichloropropylene BRL ug/L 10 0.61 10 8260B 11/9/10 10:28 LMW POK0222 1,2,3-Trichlorobenzene BRL ug/L 20 2.0 10 8260B 11/9/10 10:28 LMW POK0222 1,2,3-Trichloropropane BRL ug/L 10 0.81 10 8260B 11/9/10 10:28 LMW POK0222 1,2,4-Trichlorobenzene BRL ug/L 10 1.0 10 8260B 11/9/10 10:28 LMW POK0222 1,2,4-Trimethyl benzene BRL ug/L 10 0.48 10 8260B 11/9/10 10:28 LMW POK0222 1,2-Dibromo-3-chloropropane BRL ug/L 20 5.9 10 8260B 11/9/10 10:28 LMW POK0222 1,2-Dibromoethane BRL ug/L 10 1.4 10 8260B 11/9/10 10:28 LMW POK0222 1,2-Dichlorobenzene BRL ug/L 10 0.76 10 8260B 11/9/10 10:28 LMW POK0222 1,2-Dichloroethane BRL ug/L 10 1.4 10 8260B 11/9/10 10:28 LMW POK0222 1,2-Dichloropropane BRL ug/L 10 1.3 10 8260B 11/9/10 10:28 LMW POK0222 1,3,5-Trimethyl benzene BRL ug/L 10 0.57 10 8260B 11/9/10 10:28 LMW POK0222 1,3-Dichlorobenzene BRL ug/L 10 0.74 10 8260B 11/9/10 10:28 LMW POK0222 1,3-Dichloropropane BRL ug/L 10 1.1 10 8260B 11/9/10 10:28 LMW POK0222 1,4-Dichlorobenzene BRL ug/L 10 0.68 10 8260B 11/9/10 10:28 LMW POK0222 2,2-Dichloropropane BRL ug/L 20 1.1 10 8260B 11/9/10 10:28 LMW POK0222 2-Chloroethyl Vinyl Ether BRL ug/L 20 2.2 10 8260B 11/9/10 10:28 LMW POK0222 2-Chlorotoluene BRL ug/L 10 0.38 10 8260B 11/9/10 10:28 LMW POK0222 4-Chlorotoluene BRL ug/L 10 0.53 10 8260B 11/9/10 10:28 LMW POK0222 4-Isopropyltoluene BRL ug/L 10 0.65 10 8260B 11/9/10 10:28 LMW POK0222 Acetone BRL ug/L 100 6.2 10 8260B 11/9/10 10:28 LMW POK0222 Acrolein BRL ug/L 1000 11 10 8260E 11/9/10 10:28 LMW POK0222 Acrylonitrile BRL ug/L 1000 8.6 10 8260E 11/9/10 10:28 LMW POK0222 Benzene BRL ug/L 10 0.72 10 8260B 11/9/10 10:28 LMW POK0222 Bromobenzene BRL ug/L 10 0.64 10 8260B 11/9/10 10:28 LMW POK0222 Bromochloromethane BRL ug/L 10 1.3 10 8260B 11/9/10 10:28 LMW POK0222 Bromodichloromethane BRL ug/L 10 0.62 10 8260B 11/9/10 10:28 LMW POK0222 Bromoform BRL ug/L 10 2.7 10 8260B 11/9/10 10:28 LMW POK0222 Bromomethane BRL ug/L 30 4.7 10 8260B 11/9/10 10:28 LMW POK0222 Carbon disulfide BRL ug/L 50 14 10 8260B 11/9/10 10:28 LMW POK0222 Carbon Tetrachloride BRL ug/L 20 1.2 10 8260B 11/9/10 10:28 LMW POK0222 Chlorobenzene BRL ug/L 10 0.61 10 8260B 11/9/10 10:28 LMW POK0222 Chloroethane BRL ug/L 50 1.3 10 8260B 11/9/10 10:28 LMW POK0222 Chloroform BRL ug/L 10 0.89 10 8260B 11/9/10 10:28 LMW POK0222 Chloromethane BRL ug/L 20 1.1 10 8260B 11/9/10 10:28 LMW POK0222 cis-1,2-Dichloroethylene 1300 ug/L 100 7.6 100 8260B 11/9/10 7:48 LMW POK0222 cis-1,3-Dichloropropylene BRL ug/L 10 1.0 10 8260B 11/9/10 10:28 LMW POK0222 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 18 P R S M Laboratory Report Full -Service Analytical & Environmental Solutions 11/17/2010 LABORATORIES INC. Solutions-IES, Inc. Project: Alamac Client Sample ID: RW-3 Attn: Sean K. Jarvah Prism Sample ID: 0110138-03 1101 Nowell Road Prism Work Order: 0110138 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:06 Time Submitted: 11/03/10 15:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dibromochloromethane BRL ug/L 10 3.0 10 8260B 11/9/10 10:28 LMW POK0222 Dibromomethane BRL ug/L 10 1.3 10 8260B 11/9/10 10:28 LMW POK0222 Dichlorodifluoromethane BRL ug/L 20 1.1 10 8260B 11/9/10 10:28 LMW POK0222 Ethylbenzene BRL ug/L 10 0.67 10 8260B 11/9/10 10:28 LMW POK0222 Hexachlorobutadiene BRL ug/L 20 3.6 10 8260B 11/9/10 10:28 LMW POK0222 Isopropyl Ether BRL ug/L 10 0.43 10 8260B 11/9/10 10:28 LMW POK0222 Isopropylbenzene (Cumene) BRL ug/L 10 0.72 10 8260B 11/9/10 10:28 LMW POK0222 m,p-Xylenes BRL ug/L 20 0.81 10 8260B 11/9/10 10:28 LMW POK0222 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 50 1.9 10 8260B 11/9/10 10:28 LMW POK0222 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 50 9.0 10 8260B 11/9/10 10:28 LMW POK0222 Methyl Isobutyl Ketone BRL ug/L 50 1.2 10 8260B 11/9/10 10:28 LMW POK0222 Methylene Chloride BRL ug/L 20 4.4 10 8260B 11/9/10 10:28 LMW POK0222 Methyl-tert-Butyl Ether BRL ug/L 10 0.70 10 8260B 11/9/10 10:28 LMW POK0222 Naphthalene BRL ug/L 10 0.98 10 8260B 11/9/10 10:28 LMW POK0222 n-Butylbenzene BRL ug/L 10 1.1 10 8260B 11/9/10 10:28 LMW POK0222 n-Propylbenzene BRL ug/L 10 0.60 10 8260B 11/9/10 10:28 LMW POK0222 o-Xylene BRL ug/L 10 0.46 10 8260B 11/9/10 10:28 LMW POK0222 sec-Butylbenzene BRL ug/L 10 0.87 10 8260B 11/9/10 10:28 LMW POK0222 Styrene BRL ug/L 10 0.47 10 8260B 11/9/10 10:28 LMW POK0222 tert-Butylbenzene BRL ug/L 10 0.80 10 8260B 11/9/10 10:28 LMW POK0222 Tetrachloroethylene BRL ug/L 10 0.69 10 8260B 11/9/10 10:28 LMW POK0222 Toluene BRL ug/L 10 0.42 10 8260B 11/9/10 10:28 LMW POK0222 trans-1,2-Dichloroethylene 8.9 J ug/L 20 1.2 10 8260B 1119/10 10:28 LMW POK0222 trans-1,3-Dichloropropylene BRL ug/L 10 0.43 10 8260B 11/9/10 10:28 LMW POK0222 Trichloroethylene 12 J ug/L 20 0.54 10 8260B 11/9/10 10:28 LMW POK0222 Trichlorofluoromethane BRL ug/L 20 0.88 10 8260B 11/9/10 10:28 LMW POK0222 Vinyl acetate BRL ug/L 200 1.0 10 8260E 11/9/10 10:28 LMW POK0222 Vinyl chloride 150 ug/L 20 1.6 10 8260B 11/9/10 10:28 LMW POK0222 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 80-124 Dibromofluoromethane 106 % 75-129 Toluene-d8 94 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 18 P R S M Laboratory Report Full -Service Analytical & Environmental Solutions 11/17/2010 LABORATORIES INC. Solutions-IES, Inc. Project: Alamac Client Sample ID: 2237 Attn: Sean K. Jarvah Prism Sample ID: 0110138-04 1101 Nowell Road Prism Work Order: 0110138 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:35 Time Submitted: 11/03/10 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 1.0 0.15 1 8260B 11/11/10 18:09 LMW POK0338 1,1,1-Trichloroethane BRL ug/L 1.0 0.063 1 8260B 11/11/10 18:09 LMW POK0338 1,1,2,2-Tetrachloroethane BRL ug/L 1.0 0.071 1 8260B 11/11/10 18:09 LMW POK0338 1,1,2-Trichloroethane BRL ug/L 1.0 0.17 1 8260B 11/11/10 18:09 LMW POK0338 1,1-Dichloroethane BRL ug/L 1.0 0.096 1 8260B 11/11/10 18:09 LMW POK0338 1,1-Dichloroethylene BRL ug/L 1.0 0.078 1 8260B 11/11/10 18:09 LMW POK0338 1,1-Dichloropropylene BRL ug/L 1.0 0.061 1 8260B 11/11/10 18:09 LMW POK0338 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.20 1 8260B 11/11/10 18:09 LMW POK0338 1,2,3-Trichloropropane BRL ug/L 1.0 0.081 1 8260B 11/11/10 18:09 LMW POK0338 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.10 1 8260B 11/11/10 18:09 LMW POK0338 1,2,4-Trimethyl benzene BRL ug/L 1.0 0.048 1 8260B 11/11/10 18:09 LMW POK0338 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.59 1 8260B 11/11/10 18:09 LMW POK0338 1,2-Dibromoethane BRL ug/L 1.0 0.14 1 8260B 11/11/10 18:09 LMW POK0338 1,2-Dichlorobenzene BRL ug/L 1.0 0.076 1 8260B 11/11/10 18:09 LMW POK0338 1,2-Dichloroethane BRL ug/L 1.0 0.14 1 8260B 11/11/10 18:09 LMW POK0338 1,2-Dichloropropane BRL ug/L 1.0 0.13 1 8260B 11/11/10 18:09 LMW POK0338 1,3,5-Trimethyl benzene BRL ug/L 1.0 0.057 1 8260B 11/11/10 18:09 LMW POK0338 1,3-Dichlorobenzene BRL ug/L 1.0 0.074 1 8260B 11/11/10 18:09 LMW POK0338 1,3-Dichloropropane BRL ug/L 1.0 0.11 1 8260B 11/11/10 18:09 LMW POK0338 1,4-Dichlorobenzene BRL ug/L 1.0 0.068 1 8260B 11/11/10 18:09 LMW POK0338 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 11/11/10 18:09 LMW POK0338 2-Chloroethyl Vinyl Ether BRL ug/L 2.0 0.22 1 8260B 11/11/10 18:09 LMW POK0338 2-Chlorotoluene BRL ug/L 1.0 0.038 1 8260B 11/11/10 18:09 LMW POK0338 4-Chlorotoluene BRL ug/L 1.0 0.053 1 8260B 11/11/10 18:09 LMW POK0338 4-Isopropyltoluene BRL ug/L 1.0 0.065 1 8260B 11/11/10 18:09 LMW POK0338 Acetone BRL ug/L 10 0.62 1 8260B 11/11/10 18:09 LMW POK0338 Acrolein BRL ug/L 100 1.1 1 8260E 11/11/10 18:09 LMW POK0338 Acrylonitrile BRL ug/L 100 0.86 1 8260B 11/11/10 18:09 LMW POK0338 Benzene BRL ug/L 1.0 0.072 1 8260B 11/11/10 18:09 LMW POK0338 Bromobenzene BRL ug/L 1.0 0.064 1 8260B 11/11/10 18:09 LMW POK0338 Bromochloromethane BRL ug/L 1.0 0.13 1 8260B 11/11/10 18:09 LMW POK0338 Bromodichloromethane BRL ug/L 1.0 0.062 1 8260B 11/11/10 18:09 LMW POK0338 Bromoform BRL ug/L 1.0 0.27 1 8260B 11/11/10 18:09 LMW POK0338 Bromomethane BRL ug/L 3.0 0.47 1 8260B 11/11/10 18:09 LMW POK0338 Carbon disulfide BRL ug/L 5.0 1.4 1 8260B 11/11/10 18:09 LMW POK0338 Carbon Tetrachloride BRL ug/L 2.0 0.12 1 8260B 11/11/10 18:09 LMW POK0338 Chlorobenzene BRL ug/L 1.0 0.061 1 8260B 11/11/10 18:09 LMW POK0338 Chloroethane BRL ug/L 5.0 0.13 1 8260B 11/11/10 18:09 LMW POK0338 Chloroform BRL ug/L 1.0 0.089 1 8260B 11/11/10 18:09 LMW POK0338 Chloromethane BRL ug/L 2.0 0.11 1 8260B 11/11/10 18:09 LMW POK0338 cis-1,2-Dichloroethylene BRL ug/L 1.0 0.076 1 8260B 11/11/10 18:09 LMW POK0338 cis-1,3-Dichloropropylene BRL ug/L 1.0 0.10 1 8260B 11/11/10 18:09 LMW POK0338 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 18 P R S M Laboratory Report Full -Service Analytical & Environmental Solutions 11/17/2010 LABORATORIES INC. Solutions-IES, Inc. Project: Alamac Client Sample ID: 2237 Attn: Sean K. Jarvah Prism Sample ID: 0110138-04 1101 Nowell Road Prism Work Order: 0110138 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:35 Time Submitted: 11/03/10 15:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dibromochloromethane BRL ug/L 1.0 0.30 1 8260B 11/11/10 18:09 LMW POK0338 Dibromomethane BRL ug/L 1.0 0.13 1 8260B 11/11/10 18:09 LMW POK0338 Dichlorodifluoromethane BRL ug/L 2.0 0.11 1 8260B 11/11/10 18:09 LMW POK0338 Ethylbenzene BRL ug/L 1.0 0.067 1 8260B 11/11/10 18:09 LMW POK0338 Hexachlorobutadiene BRL ug/L 2.0 0.36 1 8260B 11/11/10 18:09 LMW POK0338 Isopropyl Ether BRL ug/L 1.0 0.043 1 8260B 11/11/10 18:09 LMW POK0338 Isopropylbenzene (Cumene) BRL ug/L 1.0 0.072 1 8260B 11/11/10 18:09 LMW POK0338 m,p-Xylenes BRL ug/L 2.0 0.081 1 8260B 11/11/10 18:09 LMW POK0338 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.19 1 8260B 11/11/10 18:09 LMW POK0338 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.90 1 8260B 11/11/10 18:09 LMW POK0338 Methyl Isobutyl Ketone BRL ug/L 5.0 0.12 1 8260B 11/11/10 18:09 LMW POK0338 Methylene Chloride BRL ug/L 2.0 0.44 1 8260B 11/11/10 18:09 LMW POK0338 Methyl-tert-Butyl Ether BRL ug/L 1.0 0.070 1 8260B 11/11/10 18:09 LMW POK0338 Naphthalene BRL ug/L 1.0 0.098 1 8260B 11/11/10 18:09 LMW POK0338 n-Butylbenzene BRL ug/L 1.0 0.11 1 8260B 11/11/10 18:09 LMW POK0338 n-Propylbenzene BRL ug/L 1.0 0.060 1 8260B 11/11/10 18:09 LMW POK0338 o-Xylene BRL ug/L 1.0 0.046 1 8260B 11/11/10 18:09 LMW POK0338 sec-Butylbenzene BRL ug/L 1.0 0.087 1 8260B 11/11/10 18:09 LMW POK0338 Styrene BRL ug/L 1.0 0.047 1 8260B 11/11/10 18:09 LMW POK0338 tert-Butylbenzene BRL ug/L 1.0 0.080 1 8260B 11/11/10 18:09 LMW POK0338 Tetrachloroethylene BRL ug/L 1.0 0.069 1 8260B 11/11/10 18:09 LMW POK0338 Toluene BRL ug/L 1.0 0.042 1 8260B 11/11/10 18:09 LMW POK0338 trans-1,2-Dichloroethylene BRL ug/L 2.0 0.12 1 8260B 11/11/10 18:09 LMW POK0338 trans-1,3-Dichloropropylene BRL ug/L 1.0 0.043 1 8260B 11/11/10 18:09 LMW POK0338 Trichloroethylene BRL ug/L 2.0 0.054 1 8260B 11/11/10 18:09 LMW POK0338 Trichlorofluoromethane BRL ug/L 2.0 0.088 1 8260B 11/11/10 18:09 LMW POK0338 Vinyl acetate BRL ug/L 20 0.10 1 8260B 11/11/10 18:09 LMW POK0338 Vinyl chloride BRL ug/L 2.0 0.16 1 8260B 11/11/10 18:09 LMW POK0338 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 80-124 Dibromofluoromethane 105 % 75-129 Toluene-d8 89 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 18 P R S M Laboratory Report Full -Service Analytical & Environmental Solutions 11/17/2010 LABORATORIES INC. Solutions-IES, Inc. Project: Alamac Client Sample ID: TRIP BLANK Attn: Sean K. Jarvah Prism Sample ID: 0110138-05 1101 Nowell Road Prism Work Order: 0110138 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:35 Time Submitted: 11/03/10 15:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 1.0 0.15 1 8260B 11/9/10 4:15 LMW POK0222 1,1,1-Trichloroethane BRL ug/L 1.0 0.063 1 8260B 11/9/10 4:15 LMW POK0222 1,1,2,2-Tetrachloroethane BRL ug/L 1.0 0.071 1 8260B 11/9/10 4:15 LMW POK0222 1,1,2-Trichloroethane BRL ug/L 1.0 0.17 1 8260B 11/9/10 4:15 LMW POK0222 1,1-Dichloroethane BRL ug/L 1.0 0.096 1 8260B 11/9/10 4:15 LMW POK0222 1,1-Dichloroethylene BRL ug/L 1.0 0.078 1 8260B 11/9/10 4:15 LMW POK0222 1,1-Dichloropropylene BRL ug/L 1.0 0.061 1 8260B 11/9/10 4:15 LMW POK0222 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.20 1 8260B 11/9/10 4:15 LMW POK0222 1,2,3-Trichloropropane BRL ug/L 1.0 0.081 1 8260B 11/9/10 4:15 LMW POK0222 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.10 1 8260B 11/9/10 4:15 LMW POK0222 1,2,4-Trimethyl benzene BRL ug/L 1.0 0.048 1 8260B 11/9/10 4:15 LMW POK0222 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.59 1 8260B 11/9/10 4:15 LMW POK0222 1,2-Dibromoethane BRL ug/L 1.0 0.14 1 8260B 11/9/10 4:15 LMW POK0222 1,2-Dichlorobenzene BRL ug/L 1.0 0.076 1 8260B 11/9/10 4:15 LMW POK0222 1,2-Dichloroethane BRL ug/L 1.0 0.14 1 8260B 11/9/10 4:15 LMW POK0222 1,2-Dichloropropane BRL ug/L 1.0 0.13 1 8260B 11/9/10 4:15 LMW POK0222 1,3,5-Trimethyl benzene BRL ug/L 1.0 0.057 1 8260B 11/9/10 4:15 LMW POK0222 1,3-Dichlorobenzene BRL ug/L 1.0 0.074 1 8260B 11/9/10 4:15 LMW POK0222 1,3-Dichloropropane BRL ug/L 1.0 0.11 1 8260B 11/9/10 4:15 LMW POK0222 1,4-Dichlorobenzene BRL ug/L 1.0 0.068 1 8260B 11/9/10 4:15 LMW POK0222 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 11/9/10 4:15 LMW POK0222 2-Chloroethyl Vinyl Ether BRL ug/L 2.0 0.22 1 8260B 11/9/10 4:15 LMW POK0222 2-Chlorotoluene BRL ug/L 1.0 0.038 1 8260B 11/9/10 4:15 LMW POK0222 4-Chlorotoluene BRL ug/L 1.0 0.053 1 8260B 11/9/10 4:15 LMW POK0222 4-Isopropyltoluene BRL ug/L 1.0 0.065 1 8260B 11/9/10 4:15 LMW POK0222 Acetone BRL ug/L 10 0.62 1 8260B 11/9/10 4:15 LMW POK0222 Acrolein BRL ug/L 100 1.1 1 8260E 11/9/10 4:15 LMW POK0222 Acrylonitrile BRL ug/L 100 0.86 1 8260B 11/9/10 4:15 LMW POK0222 Benzene BRL ug/L 1.0 0.072 1 8260B 11/9/10 4:15 LMW POK0222 Bromobenzene BRL ug/L 1.0 0.064 1 8260B 11/9/10 4:15 LMW POK0222 Bromochloromethane BRL ug/L 1.0 0.13 1 8260B 11/9/10 4:15 LMW POK0222 Bromodichloromethane BRL ug/L 1.0 0.062 1 8260B 11/9/10 4:15 LMW POK0222 Bromoform BRL ug/L 1.0 0.27 1 8260B 11/9/10 4:15 LMW POK0222 Bromomethane BRL ug/L 3.0 0.47 1 8260B 11/9/10 4:15 LMW POK0222 Carbon disulfide BRL ug/L 5.0 1.4 1 8260B 11/9/10 4:15 LMW POK0222 Carbon Tetrachloride BRL ug/L 2.0 0.12 1 8260B 11/9/10 4:15 LMW POK0222 Chlorobenzene BRL ug/L 1.0 0.061 1 8260B 11/9/10 4:15 LMW POK0222 Chloroethane BRL ug/L 5.0 0.13 1 8260B 11/9/10 4:15 LMW POK0222 Chloroform BRL ug/L 1.0 0.089 1 8260B 11/9/10 4:15 LMW POK0222 Chloromethane BRL ug/L 2.0 0.11 1 8260B 11/9/10 4:15 LMW POK0222 cis-1,2-Dichloroethylene BRL ug/L 1.0 0.076 1 8260B 11/9/10 4:15 LMW POK0222 cis-1,3-Dichloropropylene BRL ug/L 1.0 0.10 1 8260B 11/9/10 4:15 LMW POK0222 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 18 P R S M Laboratory Report Full -Service Analytical & Environmental Solutions 11/17/2010 LABORATORIES INC. Solutions-IES, Inc. Project: Alamac Client Sample ID: TRIP BLANK Attn: Sean K. Jarvah Prism Sample ID: 0110138-05 1101 Nowell Road Prism Work Order: 0110138 Raleigh, NC 27607 Sample Matrix: Water Time Collected: 11/02/10 11:35 Time Submitted: 11/03/10 15:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Dibromochloromethane BRL ug/L 1.0 0.30 1 8260B 11/9/10 4:15 LMW POK0222 Dibromomethane BRL ug/L 1.0 0.13 1 8260B 11/9/10 4:15 LMW POK0222 Dichlorodifluoromethane BRL ug/L 2.0 0.11 1 8260B 11/9/10 4:15 LMW POK0222 Ethylbenzene BRL ug/L 1.0 0.067 1 8260B 11/9/10 4:15 LMW POK0222 Hexachlorobutadiene BRL ug/L 2.0 0.36 1 8260B 11/9/10 4:15 LMW POK0222 Isopropyl Ether BRL ug/L 1.0 0.043 1 8260B 11/9/10 4:15 LMW POK0222 Isopropylbenzene (Cumene) BRL ug/L 1.0 0.072 1 8260B 11/9/10 4:15 LMW POK0222 m,p-Xylenes BRL ug/L 2.0 0.081 1 8260B 11/9/10 4:15 LMW POK0222 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.19 1 8260B 11/9/10 4:15 LMW POK0222 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.90 1 8260B 11/9/10 4:15 LMW POK0222 Methyl Isobutyl Ketone BRL ug/L 5.0 0.12 1 8260B 11/9/10 4:15 LMW POK0222 Methylene Chloride BRL ug/L 2.0 0.44 1 8260B 11/9/10 4:15 LMW POK0222 Methyl-tert-Butyl Ether BRL ug/L 1.0 0.070 1 8260B 11/9/10 4:15 LMW POK0222 Naphthalene BRL ug/L 1.0 0.098 1 8260B 11/9/10 4:15 LMW POK0222 n-Butylbenzene BRL ug/L 1.0 0.11 1 8260B 11/9/10 4:15 LMW POK0222 n-Propylbenzene BRL ug/L 1.0 0.060 1 8260B 11/9/10 4:15 LMW POK0222 o-Xylene BRL ug/L 1.0 0.046 1 8260B 11/9/10 4:15 LMW POK0222 sec-Butylbenzene BRL ug/L 1.0 0.087 1 8260B 11/9/10 4:15 LMW POK0222 Styrene BRL ug/L 1.0 0.047 1 8260B 11/9/10 4:15 LMW POK0222 tert-Butylbenzene BRL ug/L 1.0 0.080 1 8260B 11/9/10 4:15 LMW POK0222 Tetrachloroethylene BRL ug/L 1.0 0.069 1 8260B 11/9/10 4:15 LMW POK0222 Toluene BRL ug/L 1.0 0.042 1 8260B 11/9/10 4:15 LMW POK0222 trans-1,2-Dichloroethylene BRL ug/L 2.0 0.12 1 8260B 11/9/10 4:15 LMW POK0222 trans-1,3-Dichloropropylene BRL ug/L 1.0 0.043 1 8260B 11/9/10 4:15 LMW POK0222 Trichloroethylene BRL ug/L 2.0 0.054 1 8260B 11/9/10 4:15 LMW POK0222 Trichlorofluoromethane BRL ug/L 2.0 0.088 1 8260B 11/9/10 4:15 LMW POK0222 Vinyl acetate BRL ug/L 20 0.10 1 8260B 11/9/10 4:15 LMW POK0222 Vinyl chloride BRL ug/L 2.0 0.16 1 8260B 11/9/10 4:15 LMW POK0222 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 80-124 Dibromofluoromethane 103 % 75-129 Toluene-d8 96 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 18 ,ot P R I IS M EService Analytical s Environmental Solutions LABORATORIES, INC. Level II QC Report 11/17/10 Solutions-IES, Inc. Project: Alamac Attn: Sean K. Jarvah 1101 Nowell Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 0110138 Time Submitted: 11/3/10 3:40:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POK0222 - 5030B Blank (POK0222-BLK1) Prepared: 11/08/10 Analyzed: 11/09/10 1,1,1,2-Tetrachloroethane BRL 1.0 ug/L 1,1,1-Trichloroethane BRL 1.0 ug/L 1,1,2,2-Tetrachloroethane BRL 1.0 ug/L 1,1,2-Trichloroethane BRL 1.0 ug/L 1,1-Dichloroethane BRL 1.0 ug/L 1,1-Dichloroethylene BRL 1.0 ug/L 1,1-Dichloropropylene BRL 1.0 ug/L 1,2,3-Trichlorobenzene BRL 2.0 ug/L 1,2,3-Trichloropropane BRL 1.0 ug/L 1,2,4-Trichlorobenzene BRL 1.0 ug/L 1,2,4-Trimethyl benzene BRL 1.0 ug/L 1,2-Dibromo-3-chloropropane BRL 2.0 ug/L 1,2-Dibromoethane BRL 1.0 ug/L 1,2-Dichlorobenzene BRL 1.0 ug/L 1,2-Dichloroethane BRL 1.0 ug/L 1,2-Dichloropropane BRL 1.0 ug/L 1,3,5-Trimethyl benzene BRL 1.0 ug/L 1,3-Dichlorobenzene BRL 1.0 ug/L 1,3-Dichloropropane BRL 1.0 ug/L 1,4-Dichlorobenzene BRL 1.0 ug/L 2,2-Dichloropropane BRL 2.0 ug/L 2-Chloroethyl Vinyl Ether BRL 2.0 ug/L 2-Chlorotoluene BRL 1.0 ug/L 4-Chlorotoluene BRL 1.0 ug/L 4-Isopropyltoluene BRL 1.0 ug/L Acetone BRL 10 ug/L Acrolein BRL 100 ug/L Acrylonitrile BRL 100 ug/L Benzene BRL 1.0 ug/L Bromobenzene BRL 1.0 ug/L Bromochloromethane BRL 1.0 ug/L Bromodichloromethane BRL 1.0 ug/L Bromoform BRL 1.0 ug/L Bromomethane BRL 3.0 ug/L Carbon disulfide BRL 5.0 ug/L Carbon Tetrachloride BRL 2.0 ug/L Chlorobenzene BRL 1.0 ug/L Chloroethane BRL 5.0 ug/L Chloroform BRL 1.0 ug/L Chloromethane BRL 2.0 ug/L cis-1,2-Dichloroethylene BRL 1.0 ug/L cis-1,3-Dichloropropylene BRL 1.0 ug/L Dibromochloromethane BRL 1.0 ug/L Dibromomethane BRL 1.0 ug/L Dichlorodifluoromethane BRL 2.0 ug/L Ethylbenzene BRL 1.0 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 18 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Solutions-IES, Inc. Project: Alamac Attn: Sean K. Jarvah 1101 Nowell Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 11/17/10 Prism Work Order: 0110138 Time Submitted: 11/3/10 3:40:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POK0222 - 5030B Blank (POK0222-BLK1) Prepared: 11/08/10 Analyzed: 11/09/10 Hexachlorobutadiene BRL 2.0 ug/L Isopropyl Ether BRL 1.0 ug/L Isopropylbenzene (Cumene) BRL 1.0 ug/L m,p-Xylenes BRL 2.0 ug/L Methyl Butyl Ketone (2-Hexanone) BRL 5.0 ug/L Methyl Ethyl Ketone (2-Butanone) BRL 5.0 ug/L Methyl Isobutyl Ketone BRL 5.0 ug/L Methylene Chloride BRL 2.0 ug/L Methyl-tert-Butyl Ether BRL 1.0 ug/L Naphthalene BRL 1.0 ug/L n-Butylbenzene BRL 1.0 ug/L n-Propylbenzene BRL 1.0 ug/L o-Xylene BRL 1.0 ug/L sec-Butylbenzene BRL 1.0 ug/L Styrene BRL 1.0 ug/L tert-Butylbenzene BRL 1.0 ug/L Tetrachloroethylene BRL 1.0 ug/L Toluene BRL 1.0 ug/L trans-1,2-Dichloroethylene BRL 2.0 ug/L trans-1,3-Dichloropropylene BRL 1.0 ug/L Trichloroethylene BRL 2.0 ug/L Trichlorofluoromethane BRL 2.0 ug/L Vinyl acetate BRL 20 ug/L Vinyl chloride BRL 2.0 ug/L Surrogate:4-Bromofluorobenzene 24.7 ug/L 25.0 99 80-124 Surrogate: Dibromofluoromethane 26.1 ug/L 25.0 105 75-129 Surrogate: Toluene-d8 23.5 ug/L 25.0 94 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 18 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Level II QC Report 11/17/10 Solutions-IES, Inc. Project: Alamac Attn: Sean K. Jarvah 1101 Nowell Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 0110138 Time Submitted: 11/3/10 3:40:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POK0222 - 5030B LCS (POK0222-BSI) Prepared: 11/08/10 Analyzed: 11/09/10 1,1-Dichloroethylene 59.3 1.0 ug/L 50.0 119 70-154 Benzene 51.7 1.0 ug/L 50.0 103 77-128 Chlorobenzene 50.8 1.0 ug/L 50.0 102 78-119 Toluene 52.6 1.0 ug/L 50.0 105 76-131 Trichloroethylene 55.6 2.0 ug/L 50.0 ill 77-133 Surrogate:4-Bromofluorobenzene 25.9 ug/L 25.0 103 80-124 Surrogate: Dibromofluoromethane 24.7 ug/L 25.0 99 75-129 Surrogate: Toluene-d8 24.1 ug/L 25.0 96 77-123 LCS Dup (POK0222-BSD1) Prepared: 11/08/10 Analyzed: 11/09/10 1,1-Dichloroethylene 54.6 1.0 ug/L 50.0 109 70-154 8 200 Benzene 49.1 1.0 ug/L 50.0 98 77-128 5 200 Chlorobenzene 48.0 1.0 ug/L 50.0 96 78-119 6 200 Toluene 49.2 1.0 ug/L 50.0 98 76-131 7 200 Trichloroethylene 51.8 2.0 ug/L 50.0 104 77-133 7 200 Surrogate:4-Bromofluorobenzene 26.1 ug/L 25.0 104 80-124 Surrogate: Dibromofluoromethane 24.4 ug/L 25.0 98 75-129 Surrogate: Toluene-d8 24.2 ug/L 25.0 97 77-123 Batch POK0338 - 5030B Blank (POK0338-BLK1) Prepared & Analyzed: 11 /11 /10 1,1,1,2-Tetrachloroethane BRL 1.0 ug/L 1,1,1-Trichloroethane BRL 1.0 ug/L 1,1,2,2-Tetrachloroethane BRL 1.0 ug/L 1,1,2-Trichloroethane BRL 1.0 ug/L 1,1-Dichloroethane BRL 1.0 ug/L 1,1-Dichloroethylene BRL 1.0 ug/L 1,1-Dichloropropylene BRL 1.0 ug/L 1,2,3-Trichlorobenzene BRL 2.0 ug/L 1,2,3-Trichloropropane BRL 1.0 ug/L 1,2,4-Trichlorobenzene BRL 1.0 ug/L 1,2,4-Trimethyl benzene BRL 1.0 ug/L 1,2-Dibromo-3-chloropropane BRL 2.0 ug/L 1,2-Dibromoethane BRL 1.0 ug/L 1,2-Dichlorobenzene BRL 1.0 ug/L 1,2-Dichloroethane BRL 1.0 ug/L 1,2-Dichloropropane BRL 1.0 ug/L 1,3,5-Trimethyl benzene BRL 1.0 ug/L 1,3-Dichlorobenzene BRL 1.0 ug/L 1,3-Dichloropropane BRL 1.0 ug/L 1,4-Dichlorobenzene BRL 1.0 ug/L 2,2-Dichloropropane BRL 2.0 ug/L 2-Chloroethyl Vinyl Ether BRL 2.0 ug/L 2-Chlorotoluene BRL 1.0 ug/L 4-Chlorotoluene BRL 1.0 ug/L 4-Isopropyltoluene BRL 1.0 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 18 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Level II QC Report 11/17/10 Solutions-IES, Inc. Project: Alamac Attn: Sean K. Jarvah 1101 Nowell Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 0110138 Time Submitted: 11/3/10 3:40:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POK0338 - 5030B Blank (POK0338-BLK1) Prepared & Analyzed: 11 /11 /10 Acetone BRL 10 ug/L Acrolein BRL 100 ug/L Acrylonitrile BRL 100 ug/L Benzene BRL 1.0 ug/L Bromobenzene BRL 1.0 ug/L Bromochloromethane BRL 1.0 ug/L Bromodichloromethane BRL 1.0 ug/L Bromoform BRL 1.0 ug/L Bromomethane BRL 3.0 ug/L Carbon disulfide BRL 5.0 ug/L Carbon Tetrachloride BRL 2.0 ug/L Chlorobenzene BRL 1.0 ug/L Chloroethane BRL 5.0 ug/L Chloroform BRL 1.0 ug/L Chloromethane BRL 2.0 ug/L cis-1,2-Dichloroethylene BRL 1.0 ug/L cis-1,3-Dichloropropylene BRL 1.0 ug/L Dibromochloromethane BRL 1.0 ug/L Dibromomethane BRL 1.0 ug/L Dichlorodifluoromethane BRL 2.0 ug/L Ethylbenzene BRL 1.0 ug/L Hexachlorobutadiene BRL 2.0 ug/L Isopropyl Ether BRL 1.0 ug/L Isopropylbenzene (Cumene) BRL 1.0 ug/L m,p-Xylenes BRL 2.0 ug/L Methyl Butyl Ketone (2-Hexanone) BRL 5.0 ug/L Methyl Ethyl Ketone (2-Butanone) BRL 5.0 ug/L Methyl Isobutyl Ketone BRL 5.0 ug/L Methylene Chloride BRL 2.0 ug/L Methyl-tert-Butyl Ether BRL 1.0 ug/L Naphthalene BRL 1.0 ug/L n-Butylbenzene BRL 1.0 ug/L n-Propylbenzene BRL 1.0 ug/L o-Xylene BRL 1.0 ug/L sec-Butylbenzene BRL 1.0 ug/L Styrene BRL 1.0 ug/L tert-Butylbenzene BRL 1.0 ug/L Tetrachloroethylene BRL 1.0 ug/L Toluene BRL 1.0 ug/L trans-1,2-Dichloroethylene BRL 2.0 ug/L trans-1,3-Dichloropropylene BRL 1.0 ug/L Trichloroethylene BRL 2.0 ug/L Trichlorofluoromethane BRL 2.0 ug/L Vinyl acetate BRL 20 ug/L Vinyl chloride BRL 2.0 ug/L Surrogate:4-Bromofluorobenzene 25.1 ug/L 25.0 100 80-124 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 18 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Solutions-IES, Inc. Project: Alamac Attn: Sean K. Jarvah 1101 Nowell Road Raleigh, NC 27607 Volatile Organic Compounds by GC/MS - Quality Control Level II QC Report 11/17/10 Prism Work Order: 0110138 Time Submitted: 11/3/10 3:4O:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POK0338 - 5030B Blank (POK0338-BLK1) Prepared & Analyzed: 11 /11 /10 Surrogate: Dibromofluoromethane 26.1 ug/L 25.0 104 75-129 Surrogate: Toluene-d8 22.4 ug/L 25.0 89 77-123 LCS (POK0338-BSI) Prepared & Analyzed: 11 /11 /10 1,1-Dichloroethylene 57.2 1.0 ug/L 50.0 114 70-154 Benzene 50.2 1.0 ug/L 50.0 100 77-128 Chlorobenzene 46.0 1.0 ug/L 50.0 92 78-119 Toluene 49.8 1.0 ug/L 50.0 100 76-131 Trichloroethylene 51.8 2.0 ug/L 50.0 104 77-133 Surrogate:4-Bromofluorobenzene 25.0 ug/L 25.0 100 80-124 Surrogate: Dibromofluoromethane 24.6 ug/L 25.0 99 75-129 Surrogate: Toluene-d8 22.9 ug/L 25.0 92 77-123 LCS Dup (POK0338-BSD1) Prepared & Analyzed: 11 /11 /10 1,1-Dichloroethylene 57.5 1.0 ug/L 50.0 115 70-154 0.5 200 Benzene 51.2 1.0 ug/L 50.0 102 77-128 2 200 Chlorobenzene 46.4 1.0 ug/L 50.0 93 78-119 0.9 200 Toluene 51.1 1.0 ug/L 50.0 102 76-131 3 200 Trichloroethylene 52.9 2.0 ug/L 50.0 106 77-133 2 200 Surrogate:4-Bromofluorobenzene 24.9 ug/L 25.0 99 80-124 Surrogate: Dibromofluoromethane 25.6 ug/L 25.0 102 75-129 Surrogate: Toluene-d8 23.0 ug/L 25.0 92 77-123 Sample Extraction Data Prep Method: 5030B Lab Number Batch Initial Final Date 0110138-01 POK0222 10 mL 10 mL 11/08/10 0110138-02 POK0222 10 mL 10 mL 11/08/10 0110138-02 POK0222 10 mL 10 mL 11/08/10 0110138-03 POK0222 10 mL 10 mL 11/08/10 0110138-03 POK0222 10 mL 10 mL 11/08/10 0110138-04 POK0338 10 mL 10 mL 11/11/10 0110138-05 POK0222 10 mL 10 mL 11/08/10 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 18 CHAIN OF CUSTODY RECORD PAGE --/ OF —/— QUOTE # TO ENSURE PROPER BILLING: Project Name: 19 ,1 6 MA C- Short Hold Analysis: (Yes) " UST Project: (Yes) lam *Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) provisions and/or OC Requirements Invoice To: ��v ''j ALA," Ayo ^ , e t Address: Phone: 'I )11- 3' I.S-) QW2. Fax (Yes) I"o "— Purchase Order No./Billing Reference A mt- ©R A 3 TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email (Yes) (No) Email Addres5$:y cyr-l.G4al .❑ Requested Due Date Q 1 Day ❑ 2 Days 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC� EDD Type: " Excel— Other "Working ,_PDF� Days" ❑ 6-9 Days ❑ Standard 10 days Sc— OTHER N/A Site Location Name: Samples received after 15:00 will be processed next business day. X- Site Location Physical Address: U,"l, 00-o n . A) L Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES NO Sample Iced Upon Collection: YES_)( RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) TIME MATRIX SAMPLE CONTAINER ANALYSES REQUESTED � PRISM CLIENT DATE COLLECTED (SOIL, PRESERVA- LAB *TYPE SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR TIVES (��fl REMARKS ID NO. HOURS SLUDGE) SEE BELOW NO. SIZE ML RNN-3 o� o VQ3 I3� d O Af 7 Sampler' Signatur Sampled By (Print Name)L A4 Affiliation »J Uponquishi , his Chain o tody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be .re submftt in wrl in to the Prist oject Manager. There will be charges f r any changes after analyses have been initialized. Relinquis ey: (i na re) Received 8 nature) Date Military/Hours Additional Comments: Sfte Arrnral Ttme lSs I �� 10 Re q ed By: i ature) Receive ? t $tte Departure Time Field Tech Fee Relinquishe B ecew La ratori Date _ -hod of -pmenCO S S BE TAPED SHUT WITH CUSTODY SEALS OR T SPOR TION TO THE LABORATORY. 'Log- Group No. SAMPLES OT�CEPTEDD VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORAT RY.❑ Fed Ex ❑ UPS ❑ Hand-deliveredervice ❑ Other NPDES: UST: GR UNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: O NC ❑ SC ❑ NC ❑ SC )(NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC I ❑ NC ❑ SCI ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ q Page 18 of 18 *CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (ZerO:Head Space)