25006_Maaco Fleet_Final Grade Sample Report Review Pkg_20211112

November 12, 2021
Sent Via E-mail
Eric Nichols
FHN Holdings, LLC c/o Providence Group Capital
300 W. Summit Avenue, Suite 250 Charlotte, NC 28203 [e-mail]
Subject: Final Grade Soil Sampling Report Review Maaco Fleet Solutions, 2217 S. Tryon Street Charlotte, Mecklenburg County Brownfields Project Number 25006-21-060
Dear Mr. Nichols: The North Carolina Department of Environmental Quality Brownfields Program (DEQ Brownfields)
received and reviewed the Final Grade Soil Sampling Report (Report) dated November 2, 2021.
Following review, the Report was found to be compliant with the previously approved final grade soil sampling work plan for the Brownfields Property. Based on the sampling results and risk calculations included in the Report, DEQ Brownfields concurs that the 0-2 ft soil interval at the property is acceptable for the proposed use as a food court and beer hall.
Please be aware that DEQ Brownfields will need to be notified of any activities that disturb site soils, and such notification procedures will need to be included in the project’s Environmental Management Plan (EMP). Changes in the intended use of the property or discovery of previously unknown
contaminant sources may require additional data collection.
Please be advised that this review from DEQ Brownfields does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local entities. If you have any questions, please contact me at [phone], or via e-mail at
[e-mail].
Sincerely,
Peter L. Doorn, Project Manager Brownfields Program ec: Tracy Wahl, DEQ
J.Q. Freeman, Providence Group Capital Matt Ingalls, Hart & Hickman, PC
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Final Grade Soil Sampling Report
Former Maaco Fleet Solutions Site
2217 S. Tryon Street
Charlotte, Mecklenburg County, North Carolina
Brownfields Project ID: 25006-21-060
H&H Job No. PRO-014

Table of Contents

Section Page No.

1.0 Introduction ............................................................................................................................ 1
2.0 Background Information....................................................................................................... 3
2.1 Site History ........................................................................................................................... 3
2.2 Summary of Previous Environmental Assessment and Brownfields Activities ................... 3
3.0 Final Grade Soil Sampling Activities ................................................................................... 8
3.1 Soil Sampling ....................................................................................................................... 8
3.2 Soil Sampling Results ........................................................................................................... 9
3.3 Risk Calculations ................................................................................................................ 11
4.0 Summary and Conclusions .................................................................................................. 13

List of Attachments

Table 1 Summary of Final Grade Soil Analytical Results

Figure 1 Site Location Map
Figure 2 Final Grade Soil Sample Location Map

Appendix A Site Plan
Appendix B Laboratory Analytical Report
Appendix C NC DEQ Risk Calculator
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Former Maaco Fleet Solutions Site
2217 S. Tryon Street
Charlotte, Mecklenburg County, North Carolina
Brownfields Project ID: 25006-21-060
H&H Job No. PRO-014

1.0 Introduction

On behalf of FHN Holdings, LLC c/o Providence Group Capital (the Prospective Developer or
PD), Hart & Hickman, PC (H&H) has prepared this report to document final grade soil sampling
activities at the former Maaco Fleet Solutions Brownfields property (Brownfields Project Number
25006-21-060) located at 2217 S. Tryon Street in Charlotte, Mecklenburg County, North Carolina
(Site). Brownfields eligibility was granted to the PD by the North Carolina Department of
Environmental Quality (DEQ) in a letter dated April 15, 2021. A Site location map is included as
Figure 1.

The subject Site consists of an approximate 1.14-acre parcel of land (Parcel Identification Number
12104401) that is developed with an approximate 8,540-square foot (sq ft) vacant one-story light
industrial warehouse building comprised of former office, storage, and service shop areas. The
building was previously occupied by Maaco Fleet Solutions and was previously utilized as a
vehicle service facility, which consisted of oil/fluid changing, vehicle body work, and vehicle
painting activities. The building and property have remained vacant since early 2021 and the PD’s
plans include adaptive re-use of the existing building and property as a food court and beer hall.

H&H understands that the PD does not plan to significantly alter the grade of the property and
intends to utilize the outdoors spaces for patron seating, walkway areas, and dog walk areas. The
purpose of the final grade sampling was to further characterize surficial soil (0-2 ft) for planning
purposes and to determine the appropriate engineering controls to protect workers and future
occupants of the property. A conceptual Site plan which shows redevelopment features is included
as Figure 2.

The soil sampling activities were conducted in general accordance with the methods stated in the
DEQ-approved Final Grade Soil Sampling Work Plan dated July 30, 2021. The purpose of the

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final grade sampling was to evaluate potential risks to future Site residents and/or workers from
direct contact exposure to surficial soil at the Site during and after completion of an adaptive reuse
development. A summary of background information is presented in Section 2.0, and the methods
and results of the final grade assessment are provided in Section 3.0.

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2.0 Background Information

2.1 Site History

Historically, the Brownfields Site appears to have been undeveloped in the earliest historical
source reviewed, an 1890 Sanborn Map. In 1929, a building (depicted on the Sanborn Map utilized
for machinery storage), and a rail spur existed in the northern portion of the Site. In the 1950s, a
building depicted as a small office building (thought to be occupied by Blankenship Brothers
grading contractor) and a building depicted as an auto repair shop/oil storage facility (thought to
be occupied by Queen City Oil) were located in the southern and northeastern portions of the Site,
respectively. In the late 1950s to the 1970s, a gas station with four gasoline tanks (occupied by
Queen City Oil and Mustang Oil service station) operated in the northern portion of the Site. In
the 1980s, B&B Contracting appears to have utilized the Site buildings for office and storage.

The previous structures were demolished, and existing Site building was constructed in 1987.
HyrdaStar, a distributor/installer of trailer braking systems, was the original Site occupant. B&B
Automotive and Capstone Builders occupied the Site building in the 2000s and early 2010s,
respectively. Maaco Fleet Solutions operated in the existing Site building from the mid-2010s
until they vacated the building in late 2020/early 2021.

2.2 Summary of Previous Environmental Assessment and Brownfields Activities

Phase I ESA
H&H conducted a Phase I ESA at the Site in September 2020 and identified the following
Recognized Environmental Conditions (RECs) in connection with the Site:

 H&H identified a paint booth, a paint gun cleaner, and solvent recycling unit located
indoors within the central and eastern portions of the service garage. H&H observed paint
stains and paint dust to the concrete floor in the service garage near the vehicle painting
operations. The concrete floor in these areas appeared to be in good condition without
evidence of significant cracks. Paint dust was reportedly cleaned up by staff and placed in

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garbage bags prior to disposal in the facility dumpster. However, it appeared that some of
paint dust entered the floor drains (and into a potential sump covered by a steel plate)
located in the service garage, which mixed with fluids and discharged into to an oil water
separator (located southwest of the Site building) prior to discharge into the municipal
sanitary sewage system. Due to potential for impacts to the subject Site, H&H considered
current and previous auto painting activities conducted in the service garage including
collection of paint dust in the floor drains and oil/water separator to be a REC.

 H&H did not observe evidence of storage tanks during the Site visit. However, four (4)
former gasoline tanks were identified on a Sanborn Map associated with a former gas
station that operated in the northern portion of the Site from the late 1950s until the 1970s.
H&H did not locate records associated with the former tanks in the EDR report or during
review of documents on the NC Department of Environmental Quality (DEQ) Laserfiche
web-portal. Due to the lack of assessment activities performed to date at the Site, H&H
considered the potential for a release to the Site associated with former gas station
operations and/or the USTs to be a REC.

 H&H identified two former in-ground hydraulic lifts located in the northern portion of the
service garage. Site contact Mr. McGee reported that Maaco Fleet Solutions had not
operated the lifts since he began managing the facility in 2015 and he was not aware of a
previous release associated with the lifts. H&H did not locate records associated with the
hydraulic lifts in the EDR report or during review of documents on the DEQ Laserfiche
web-portal. Due to the lack of assessment activities performed to date at the Site, H&H
considered the potential for a release to the Site associated with the former hydraulic lifts
to be a REC.

Phase II ESA
H&H conducted a Phase II ESA Site in October 2020 that included the collection of soil and
groundwater samples for laboratory analysis. The assessment activities were conducted to assess
the potential for impact to the subject Site from historical Site operations, upgradient contaminant

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sources, and to evaluate potential risks associated with future Site development. A summary of
the results of the Phase II ESA is provided below.

Soil
 Analytical data indicate that soil in the area of the former gas station (SB-1) located on the
northern portion of the Site is impacted by petroleum constituents at concentrations above
Residential Maximum Soil Contaminant Concentrations (MSCCs) and Preliminary Soil
Remediation Goals (PSRGs).

 Analytical data indicate that soil below an oil/water separator (OWS; SB-2) is impacted by
petroleum constituents at concentrations above soil to groundwater MSCCs and protection
of groundwater (POG) PSRGs. Analytical data indicate that soil below one of the two
subgrade hydraulic lifts (SB-6) is impacted by petroleum constituents at concentrations
above soil to groundwater MSCCs.

 Soil sampled underneath the trench and floor drains, one of the subgrade hydraulic lifts,
and subgrade vault were not impacted with volatile organic compounds (VOCs) or
polycyclic aromatic hydrocarbons (PAHs) above MSCCs or PSRGs.

 Arsenic (ranging from 2.2 to 3.9 mg/kg) was detected in soil at the Site at concentrations
above the Industrial/Commercial PSRG of 3.0 mg/kg. However, the detected arsenic
concentrations are within the published range of background concentrations for North
Carolina soil and were consistent with the arsenic concentration reported in the SB-BG
background sample.

Hexavalent chromium (ranging from 0.6 to 1.5 mg/kg) was detected at concentrations
above the Residential PSRG of 0.31 mg/kg. However, the detected hexavalent chromium
concentrations are consistent with the concentration reported in the SB-BG background
sample. Additional metals, including barium, cadmium, lead, mercury, and selenium, were
detected at concentrations below MSCCs, PSRGs, background concentrations, and/or were
generally consistent with published average background levels for North Carolina soils.

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Groundwater
 VOCs (naphthalene, n-propylbenzene, and 1,2,4-trimethylbenzene) and PAHs (indeno
[1,2,3-cd] pyrene and naphthalene) were detected at concentrations above 2L Standards
and Residential/Non-Residential GWSLs in the area of the former gas station (TMW-1).

 Cumulative risk calculations indicate that the non-carcinogenic and carcinogenic risk
levels are above acceptable risk levels for both Residential and Non-Residential exposure
scenarios for groundwater in the northern portion of the Site near TWM-1, but not in the
southern portion of the Site near TMW-2. Therefore, vapor intrusion appears to pose a
potential risk to future residents and Non-Residential workers at the Site should a building
be developed on the northern portion of the Site.

Brownfields Eligibility
The Site received a letter of eligibility for entry into the DEQ Brownfields Program (Brownfields
Project No. 25006-21-060) on April 15, 2021. During an initial kick-off meeting and follow up
email correspondence, the DEQ Brownfields Project Manager Pete Doorn reported that soil and
groundwater appears to have been adequately assessed at the Site. However, Mr. Doorn requested
that additional sub-slab soil vapor sampling be completed at the Site to further evaluate current
environmental conditions at the Site.

Brownfields Assessment
H&H completed sub-slab vapor assessment activities at the Site in May 2021. The assessment
activities included the collection and analysis of two sub-slab vapor (SSV) samples. The results
of the assessment activities are summarized below.

 SSV-2, advanced in the garage portion of the existing building, contained trichloroethylene
(TCE) concentrations above the Residential Soil Gas Screening Level (SGSL) but below
the Non-Residential SGSL. No other VOCs exceeded SGSLs in the samples collected.

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 Calculated cancer risks did not exceed a lifetime incremental cancer risk (LICR) of 1.0 x
10-5 and calculated non-carcinogenic HIs were less than 1 in sub-slab vapor sample
locations and the worst-case Site wide scenario. Therefore, vapor intrusion does not appear
to pose a risk to the Site building.

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3.0 Final Grade Soil Sampling Activities

Final grade soil sampling activities were performed in general accordance with the DEQ-approved
Final Grade Soil Sampling Work Plan dated July 30, 2021, the DEQ Inactive Hazardous Sites
Branch’s (IHSB’s) Guidelines for Assessment and Cleanup (Guidelines) dated July 2021, and the
most recent version of the U.S. Environmental Protection Agency (EPA) Region IV Science and
Ecosystem Support Division’s (SESD’s) Field Branches Quality System and Technical
Procedures guidance.

3.1 Soil Sampling

On August 6, 2021, H&H collected shallow composite soil samples to evaluate potential risks to
future Site residents and/or workers from direct contact exposure to surficial soil at the Site. The
samples were collected from areas on the Brownfields Property not covered by impervious surface
(e.g., building foundations, sidewalks, hardscaping, asphalt surface parking, etc.). The soil borings
were advanced to a depth of 0 to 2 feet below ground surface (ft bgs) from four (4) designated
composite sample areas (CS-1 through CS-4) referenced on Figure 2. Each area included five (5)
soil borings per composite sample for a total of 20 soil boring locations.

The shallow soil borings were advanced using a decontaminated hand auger and the soil from the
borings was field screened for the presence of odor, staining, and elevated photoionization detector
(PID) readings. As indicated on Table 1, the range of PID readings from the soil samples collected
in each composite area were detected as follows:

 Composite Area 1- from 0.0 to 6.7 parts per million per volume (ppmv);
 Composite Area 2 - from 0.0 to 1.0 ppmv;
 Composite Area 3 - from 4.0 to 6.4 ppmv, and
 Composite Area 4 - from 0.0 to 0.6 ppmv.

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Based on the highest field screening results, H&H collected one grab soil sample from each of the
four composite areas for laboratory analysis of VOCs by EPA Method 8260.

H&H also generated a composite soil sample from aliquots collected from each of the soil borings
within a designated composite sample area (for a total of four samples). The soil sample aliquots
were homogenized using a decontaminated stainless-steel bowl and spoon prior to placement into
laboratory-supplied glassware. The composite soil samples were analyzed for semi-VOCs
(SVOCs) by EPA Method 8270, Resource Conservation and Recovery Act (RCRA) metals by
EPA Methods 6020/7471 and hexavalent chromium by EPA Method 7199. The RCRA metals
include arsenic, barium, cadmium, chromium, lead, selenium, and silver by EPA Method 6020,
and mercury by EPA Method 7471.

The soil samples were placed in dedicated laboratory-supplied sample containers, labeled with the
sample identification, date, time, and requested analyses then placed in a laboratory supplied
cooler and covered with ice. The grab and composite soil samples were delivered to Waypoint
Analytical, LLC (Waypoint), a North Carolina-certified laboratory, under chain of custody
protocols.

For quality assurance/quality control (QA/QC) purposes, H&H collected one duplicate soil sample
(DUP) from S-3 (the VOC sample was collected from S-3-E) for laboratory analysis. The
duplicate sample was analyzed for the same laboratory analysis as the parent sample. The results
of analysis of the duplicate sample indicates good analytical repeatability.

3.2 Soil Sampling Results

The analytical laboratory results for the final grade soil samples are summarized in Table 1 and
the laboratory report is included in Appendix B. The analytical results were compared to the DEQ
Residential and Industrial/Commercial PSRGs dated May 2021. Metal concentrations were
compared to Site-specific background samples collected during Phase II ESA activities in October

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2020 and published background metal concentrations in North Carolina soil for comparison
purposes.

VOCs
Laboratory analytical results indicate that VOCs were not detected at concentrations above
Residential PSRGs in the S-1 through the S-4 soil samples. Four low-level VOCs (acetone,
acrolein, benzene, and methyl ethyl ketone) were detected at low or estimated concentrations
above laboratory method detection limits in one or more samples, but at concentrations well below
their respective PSRG values.

SVOCs
Laboratory analytical results indicate that benzo(a)pyrene was detected in the S-2 and S-4
composite samples at estimated concentrations of 0.159 J and 0.287 J mg/kg, respectively, which
is slightly above the Residential PSRG of 0.11 mg/kg, but below the Industrial/Commercial PSRG
of 2.1 mg/kg. The SVOCs benzo(b)fluoranthene, benzo(g,h,i)perylene, chrysene, fluoranthene,
indeno(1,23-cd)pyrene, and pyrene were also detected in the SB-2 and/or the SB-4 soil samples at
low or estimated concentrations above laboratory method detection limits, but at concentrations
well below their respective PSRG values.

Metals
The results of the metals analyses indicate that arsenic was detected above the Residential PSRG
of 0.68 mg/kg in the S-1 and the S-3 soil samples (and associated duplicate sample) at
concentrations ranging from 2.21 mg/kg to 2.50 mg/kg. Arsenic was also detected in the SB-2 and
SB-4 soil samples at concentrations of 4.81 and 7.36, which are above the Industrial/Commercial
PSRG of 3 mg/kg. Although detected at concentrations above PSRGs, the arsenic concentrations
detected in the SB-1 through SB-4 soil samples are generally consistent with the range of arsenic
concentrations detected during previous Phase II ESA sampling activities conducted at the Site
(2.9 to 3.9 mg/kg) in October 2020, and within the range of published regional background arsenic
concentrations reported for North Carolina soils (1.0 mg/kg to 18.0 mg/kg).

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Analytical results indicate that hexavalent chromium was detected in soil samples S-1, S-2, and
the S-3 soil samples (and associated duplicate sample) at concentrations ranging from the
estimated value of 0.75 J mg/kg to 3.8 mg/kg, which are above the Residential PSRG of 0.31
mg/kg but below the Industrial/Commercial PSRG of 6.5 mg/kg. Although detected at
concentrations above PSRGs, the hexavalent chromium concentrations detected in the SB-1
through SB-4 soil samples are generally consistent with those detected during previous Phase II
ESA sampling activities conducted at the Site (0.6 to 1.5 mg/kg) in October 2020.

Although the presence of hexavalent chromium in the environment may be the result of
anthropogenic activity, hexavalent chromium is potentially present in background soil. For
example, the New Jersey Department of Environmental Protection (NJ DEP) conducted a study of
background levels of hexavalent chromium in soil. Results indicated that of the 258 samples
analyzed, 36% contained detectable concentrations of hexavalent chromium, with a 75th percentile
concentration of 1.4 mg/kg and a 99th percentile concentration of 5.5 mg/kg1.

No other metals were detected above PSRGs.

3.3 Risk Calculations

To further evaluate the detected compounds, H&H input the highest concentration of each
compound detected in the soil samples (to simulate a worst-case scenario) into the DEQ Risk
Calculator (June 2021 version). Calculations were completed for both a Residential and Non-
Residential use scenario of the direct contact soil exposure pathway to calculate cumulative
potential carcinogenic and non-carcinogenic risks for the soil samples. The completed risk
calculator is provided in Appendix B.

The soil risk calculator indicated that the non-carcinogenic HI for residents is 0.28 and the HI for
Non-Residential workers is 0.023, which are below the risk threshold of 1. Additionally, the soil
risk calculator indicated that the LICR for a resident is 2.5 x 10-5 and the LICR for Non-Residential

1 http://nemc.us/docs/2011/presentations/Presentation-NagourneyS-8-16-11-Tue-
PM%20[Compatibility%20Mode].pdf

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workers is 3.2 x 10-6, which are below the acceptable risk of 1x10-4. Therefore, exposed surficial
soil at the Site does not appear to pose an unacceptable risk to future Site residents or Non-
Residential workers.

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4.0 Summary and Conclusions

H&H has completed final grade soil sampling activities at the former Maaco Fleet Solutions
Brownfields property (Brownfields Project Number 25006-21-060) located at 2217 S. Tryon Street
in Charlotte, Mecklenburg County, North Carolina. The purpose of the final grade sampling was
to evaluate potential risks to future Site residents and/or workers from direct contact exposure to
surficial soil at the Site during and after completion of an adaptive reuse development. The results
of the final grade soil assessment activities indicated the following:

 VOCs were not detected at concentrations above Residential PSRGs in any of the soil
samples.

 The SVOC benzo(a)pyrene was detected in the S-2 and S-4 composite samples as estimated
concentrations slightly above the Residential PSRG, but below the Industrial/Commercial
PSRG.

 Arsenic was detected above the Residential PSRG of 0.68 mg/kg in the S-1 and the S-3
soil samples (and associated duplicate sample) at concentrations ranging from 2.21 mg/kg
to 2.50 mg/kg. Arsenic was also detected in the SB-2 and SB-4 soil samples at
concentrations of 4.81 and 7.36, which are above the Industrial/Commercial PSRG of 3
mg/kg.

Low-levels of hexavalent chromium were detected in the S-1, S-2, and the S-3 soil samples
(and associated duplicate sample) at concentrations ranging from the estimated value of
0.75 J mg/kg to 3.8 mg/kg, which are above the Residential PSRG of 0.31 mg/kg but below
the Industrial/Commercial PSRG of 6.5 mg/kg. However, the results of the metals analysis
indicate that metals concentrations in shallow soil at the Site are generally consistent with
Site-specific background levels and/or within published background concentrations in
North Carolina soil for the arsenic detections.

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 The results of the cumulative risk calculations indicate that potential carcinogenic and non-
carcinogenic risks associated with the soil detections are within the range of acceptable
limits for a direct contact soil exposure pathway under both Residential and Non-
Residential use scenarios. Therefore, shallow soil at the Site does not appear to pose a
direct contact exposure concern for future Site residents or workers.

Tables

Table 1Summary of Final Grade Soil Analytical ResultsFormer Maaco Fleet Solutions Property2217 S. Tryon StreetCharlotte, North CarolinaH&H Job No. PRO-014Evaluation AreaComposite Area 1 Composite Area 2 Composite Area 4Sample IDS-1 S-2 S-4Date8/6/2021 8/6/2021 8/6/2021Depth (ft bgs)0-2 0-2 0-2Range of PID Readings (ppmv)0.0-6.7* 0.0-1.0* 0.0-0.6*UnitsVOCs (8260D)Acetone 0.024 J 0.0910.009 J 0.041 0.10412,000 140,000-- -- --Acrolein<0.001 <0.001<0.001 <0.001 0.001 J0.031 0.13-- -- --Benzene 0.0009 J<0.0006<0.0007 <0.0007 <0.00061.2 5.4-- -- --Methyl Ethyl Ketone (MEK) 0.001 J 0.005 J<0.0008 0.003 J 0.006 J5,500 40,000-- -- --SVOCs (8270E)Benzo(a)pyrene<0.2050.159 J<0.173 <0.1870.287 J0.11 2.1-- -- --Benzo(b)fluoranthene<0.2040.257 J<0.172 <0.186 0.456 J1.1 21-- -- --Benzo(g,h,i)perylene<0.190 <0.148<0.160 <0.173 0.215 JNE NE-- -- --Chrysene<0.198 <0.154<0.168 <0.181 0.178 J110 2,100-- -- --Fluoranthene<0.1720.171 J<0.145 <0.156 0.193 J480 6,000-- -- --Indeno(1,2,3-cd)pyrene)<0.250 <0.195<0.211 <0.227 0.226 J1.1 21-- -- --Pyrene<0.1870.180 J<0.158 <0.170 0.220 J360 4,500-- -- --RCRA Metals (6020B/7471B/7199)Arsenic 2.50 4.812.21 2.27 7.36 0.68 3 2.2-3.9 1.0 - 18 4.8Barium 35.8 99.426.5 50 101 3,100 47,000 33-180 50 - 1,000 356Cadmium<0.07690.275 J<0.0650 <0.0696 0.399 J 14 200 <0.047--0.28 J 1.0 - 10 4.3Chromium 176 40.2120 134 34.5 NE NE 37-170 7.0 - 300 65Hexavalent Chromium 3.8 0.75 J0.81 J 0.96 J <0.25 0.31 6.5 0.6-1.1 NS NSTrivalent Chromium 172.2 39.45119.19 133.04 34.5 23,000 350,000 35.9-169.4 NS NSLead 13.3 83.121.9 11.4 71.5 400 800 3.7-160 ND - 50 16Selenium<1.261.65 J1.29 J <1.14 1.97 J 78 1,200 2.5-12 <0.1 - 0.8 0.42Silver<0.05730.0988 J0.0707 J <0.0518 0.105 J 78 1,200 <0.065-0.091 J ND - 5.0 NSMercury 0.106 0.05010.0637 0.0405 0.0789 4.7 70 0.029 J - 0.13 0.03 - 0.52 0.121Notes:1) NC Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) dated June 20212) Metal concentrations detected during Phase II ESA activities conducted at the Site in October 20203) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils. Soil concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits.With the exception of metals, only those compounds detected in at least one sample are shown in the table above. Laboratory analytical methods are shown in parentheses.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Act; ft bgs= feet below ground surface; ND = not detectedBDL = below laboratory method detection limits; NE = not established; NS= not specified; -- = not applicableJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. mg/kgS-3/DUP-1Screening CriteriaRegional Background Metals in Soil (3)Composite Area 38/6/20210-24.0-6.4*Range MeanResidential PSRGs (1)Site-Specficic Background Metals (2)Industrial/ Commercial PSRGs (1)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Providence Group (PRO)/PRO‐014 2217 S Tryon Street (Maaco Service)/Final Grade/Soil Analytical11/1/2021Table 1 (Page 1 of 1)Hart & Hickman, PC

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U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NORTH CAROLINA 1991
TITLE
PROJECT
SITE LOCATION MAP
MAACO FLEET SOLUTIONS
2217 S. TRYON STREET
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
9-24-20 0
1PRO-014
SITE
73
0
7
2
5
730725 RAMPART STREET50' PUBLIC R/W(M.B. 62, PG. 890)DUNAVANT STREET50' PUBLIC R/W(M.B. 62, PG. 890)SOUTH TRYON STREET60' PUBLIC R/WFOOD STALL 120'X25'FOOD STALL 220'X25'FOOD STALL 320'X25'FOOD STALL 420'X25'FOOD STALL 520'X25'FOOD STALL QUEUEORDER/PICKUPDUTCHDOORWALK UP WINDOWWALK UP COUNTERWALK UP COUNTERUP4' DELIVERY /TRASH OPENING4' DELIVERY /TRASH DOORWALK UP COUNTERWALK UP COUNTERWALK UP COUNTERWALK UP COUNTERMENDININGBAREXISTDOORNEWDOORDUTCHDOOR INPLACEOF EXISTDOORCOOLER6'X5'COOLER6'X5'COOLER6'X5'COOLER6'X5'COOLER6'X5'FOOD STALL 612'X11'FOOD STALL 726'X9'LOCKERSCANWASH8' PICNIC TABLE TYP.8' PICNIC TABLE TYP.8' PICNIC TABLE TYP.2217 SOUTH TRYON8,595 TOTAL SF(304 SF FINISHED MEZZAREA NOT INCLUDED)36X3636X3636X3636X3636X3636X36POTENTIAL UNDERGROUND DETENTION
STORAGE AREA : OPTION 1 - STORMTANK
SYSTEM
EXISTING 727.87
CURRENTLY 3.5%
CROSS-SLOPE. NEED TO
POUR NEW
CONTINUOUS, ADA
COMPLIANT CONCRETE
PATHWAYS 1.5%EXISTING
728.13EXISTING
727.84
EXISTING
727.69
EXISTING
728.10
EXISTING
728.08
EXISTING
728.22 @
RECESSED
DOORWAY
NEW DRAINAGE PIPE UNDER
NEW SIDEWALK (8" OR LARGER) - WATER
TAKEN TO STORM BOX CLOSER TO
INTERSECTION
EXISTING STORM DRAINS IN STREET - RUN NEW
PIPE AND -UNCTION BOX TO THIS POINT / TIE-IN
NEW -UNCTION BOX TIED INTO DRAINS/BOX AT
STREET - -UNCTION BOX WILL SERVE NEW PIPE
AS WELL AS DETENTION SYSTEM
NEW DRAIN INLET AT HIGH END
OF DRAINAGE RUN ALONG RAMPART
POTENTIAL UNDERGROUND DETENTION
STORAGE AREA : OPTION 2 - OLD CASTLE
PRECAST VAULT
DETENTION STORAGE TO BE WATERTIGHT.
LINER NEEDED IF NOT A VAULT SYSTEM.1.5%1.5%1.5%
TC 723.50
BC 723.00
TC 722.50
BC 722.00
TC 724.50
BC 724.00
TC 726.50
BC 726.00
TC 727.50
BC 727.00
TC 729.50
BC 729.00
TC 722.50
BC 722.00
TC 723.50
BC 723.00
TC 724.50
BC 724.00
LP 721.29
EXISTING STORM DRAINS
TC 725.50
BC 725.00
EXISTING
728.00
EXISTING
724.09
EXISTING
724.22
EXISTING
721.85
ALL CONCRETE
WALKWAYS TO BE ADA
COMPLIANT - PART OF
ACCESSIBLE ROUTE 1.5%1.5%727.56
1.5%3.4%1.5%
1.5%
1.5%
1.5%
1.5%
727.14
1.5%
727.02 TC 726.68
BC 726.184.25%
1.5%GRAVEL AREA 2-3% SLOPE TOWARD PERIMETER PLANTING AREAEXISTING
724.00
EXISTING
725.00
EXISTING
726.00
STREET TREE TO
REMAIN, TYP.
STREET TREE TO
REMAIN, TYP.
STREET TREE TO
REMAIN, TYP.
1
.
5%1.
5%1.
5%1.5%
EXISTING
724.12
EXISTING
725.12
EXISTING
726.12
EXISTING
723.40
EXISTING
723.86
1
.5%
723.52
EXISTING
724.28
EXISTING
727.26
EXISTING
727.241.5%
0.8%
0.8%
EXISTING
725.53
725.65
1
.5%
725.65
727.53
727.84
EXISTING
727.56
727.68
1.5%2.6%
727.66
1.5%
EXISTING
RETAINING
WALL TO
REMAIN
727.66
1
.
8%1.1%725.93
725.98 727.57
4.25%
725.99
726.111.5%
1.5%
727.51
1.5%
1.5%
727.51
RIM 727.40
RIM 727.00
4
.
8%
725.84
4.0%726.45
2.0%1.15%2.0% - 3.0%FRENCH DRAINAGE
ALONG EDGE OF
GRAVEL AND
PLANTING AREA
FRENCH DRAINAGE
ALONG EDGE OF
GRAVEL AND
PLANTING AREA
FRENCH DRAINAGE
ALONG EDGE OF
GRAVEL AND
PLANTING AREA
FRENCH DRAINAGE
ALONG EDGE OF
GRAVEL AND
PLANTING AREA
FRENCH DRAINAGE (AND/OR ANY AREA
DRAINS) ROUTED TO UNDERGROUND
DETENTION
UNDERGROUND DETENTION - 4,000 CU YDS
LANDSCAPE
DRAINS NEEDED
FOR PLANTING
AREAS
1.5%1.8%6/4/2021 10:51 PM HPREITER N:\_2020\1020308\CAD\DOCUMENTATION\1020308_PLN_GRAD.DWG
PN 1020308 | PROVIDENCE GROUP CAPITAL
2117 S. TRYON ▪ CHARLOTTE, NC ▪ PRELIMINARY GRADING AND DRAINAGE
SCALE:1" = 20'
0 20 4010

Appendix A

Site Plan
2217 S TRYON CHARLOTTE, NC •
PN 1020308 | 04.07.2021 | PROVIDENCE GROUP CAPITAL
SITE PLAN RAMPART STREET DUNAVANT STREETS TRYON ST
REET
73
0
7
2
5
730725 RAMPART STREET50' PUBLIC R/W(M.B. 62, PG. 890)DUNAVANT STREET50' PUBLIC R/W(M.B. 62, PG. 890)SOUTH TRYON STREET60' PUBLIC R/WFOOD STALL 120'X25'FOOD STALL 220'X25'FOOD STALL 320'X25'FOOD STALL 420'X25'FOOD STALL 520'X25'FOOD STALL QUEUEORDER/PICKUPDUTCHDOORWALK UP WINDOWWALK UP COUNTERWALK UP COUNTERUP4' DELIVERY /TRASH OPENING4' DELIVERY /TRASH DOORWALK UP COUNTERWALK UP COUNTERWALK UP COUNTERWALK UP COUNTERMENDININGBAREXISTDOORNEWDOORDUTCHDOOR INPLACEOF EXISTDOORCOOLER6'X5'COOLER6'X5'COOLER6'X5'COOLER6'X5'COOLER6'X5'FOOD STALL 612'X11'FOOD STALL 726'X9'LOCKERSCANWASH8' PICNIC TABLE TYP.8' PICNIC TABLE TYP.8' PICNIC TABLE TYP.2217 SOUTH TRYON8,595 TOTAL SF(304 SF FINISHED MEZZAREA NOT INCLUDED)36X3636X3636X3636X3636X3636X36POTENTIAL UNDERGROUND DETENTION
STORAGE AREA : OPTION 1 - STORMTANK
SYSTEM
EXISTING 727.87
CURRENTLY 3.5%
CROSS-SLOPE. NEED TO
POUR NEW
CONTINUOUS, ADA
COMPLIANT CONCRETE
PATHWAYS 1.5%EXISTING
728.13EXISTING
727.84
EXISTING
727.69
EXISTING
728.10
EXISTING
728.08
EXISTING
728.22 @
RECESSED
DOORWAY
NEW DRAINAGE PIPE UNDER
NEW SIDEWALK (8" OR LARGER) - WATER
TAKEN TO STORM BOX CLOSER TO
INTERSECTION
EXISTING STORM DRAINS IN STREET - RUN NEW
PIPE AND -UNCTION BOX TO THIS POINT / TIE-IN
NEW -UNCTION BOX TIED INTO DRAINS/BOX AT
STREET - -UNCTION BOX WILL SERVE NEW PIPE
AS WELL AS DETENTION SYSTEM
NEW DRAIN INLET AT HIGH END
OF DRAINAGE RUN ALONG RAMPART
POTENTIAL UNDERGROUND DETENTION
STORAGE AREA : OPTION 2 - OLD CASTLE
PRECAST VAULT
DETENTION STORAGE TO BE WATERTIGHT.
LINER NEEDED IF NOT A VAULT SYSTEM.1.5%1.5%1.5%
TC 723.50
BC 723.00
TC 722.50
BC 722.00
TC 724.50
BC 724.00
TC 726.50
BC 726.00
TC 727.50
BC 727.00
TC 729.50
BC 729.00
TC 722.50
BC 722.00
TC 723.50
BC 723.00
TC 724.50
BC 724.00
LP 721.29
EXISTING STORM DRAINS
TC 725.50
BC 725.00
EXISTING
728.00
EXISTING
724.09
EXISTING
724.22
EXISTING
721.85
ALL CONCRETE
WALKWAYS TO BE ADA
COMPLIANT - PART OF
ACCESSIBLE ROUTE 1.5%1.5%727.56
1.5%3.4%1.5%
1.5%
1.5%
1.5%
1.5%
727.14
1.5%
727.02 TC 726.68
BC 726.184.25%
1.5%GRAVEL AREA 2-3% SLOPE TOWARD PERIMETER PLANTING AREAEXISTING
724.00
EXISTING
725.00
EXISTING
726.00
STREET TREE TO
REMAIN, TYP.
STREET TREE TO
REMAIN, TYP.
STREET TREE TO
REMAIN, TYP.
1
.
5%1.
5%1.
5%1.5%
EXISTING
724.12
EXISTING
725.12
EXISTING
726.12
EXISTING
723.40
EXISTING
723.86
1
.5%
723.52
EXISTING
724.28
EXISTING
727.26
EXISTING
727.241.5%
0.8%
0.8%
EXISTING
725.53
725.65
1
.5%
725.65
727.53
727.84
EXISTING
727.56
727.68
1.5%2.6%
727.66
1.5%
EXISTING
RETAINING
WALL TO
REMAIN
727.66
1
.
8%1.1%725.93
725.98 727.57
4.25%
725.99
726.111.5%
1.5%
727.51
1.5%
1.5%
727.51
RIM 727.40
RIM 727.00
4
.
8%
725.84
4.0%726.45
2.0%1.15%2.0% - 3.0%FRENCH DRAINAGE
ALONG EDGE OF
GRAVEL AND
PLANTING AREA
FRENCH DRAINAGE
ALONG EDGE OF
GRAVEL AND
PLANTING AREA
FRENCH DRAINAGE
ALONG EDGE OF
GRAVEL AND
PLANTING AREA
FRENCH DRAINAGE
ALONG EDGE OF
GRAVEL AND
PLANTING AREA
FRENCH DRAINAGE (AND/OR ANY AREA
DRAINS) ROUTED TO UNDERGROUND
DETENTION
UNDERGROUND DETENTION - 4,000 CU YDS
LANDSCAPE
DRAINS NEEDED
FOR PLANTING
AREAS
1.5%1.8%6/4/2021 10:51 PM HPREITER N:\_2020\1020308\CAD\DOCUMENTATION\1020308_PLN_GRAD.DWG
PN 1020308 | PROVIDENCE GROUP CAPITAL
2117 S. TRYON ▪ CHARLOTTE, NC ▪ PRELIMINARY GRADING AND DRAINAGE
SCALE:1" = 20'
0 20 4010

Appendix B

Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

8/17/2021
Hart & Hickman (Charlotte) Matt Ingalls
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 21-218-0030 Client Project Description: PRO-014
Dear Matt Ingalls:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/6/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 87
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202199012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-218-0030
Page 2 of 87
Report Number:
Sample Summary Table
Client Project Description:
21-218-0030
PRO-014
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
08/06/2021 09:05Solids 93188 S-1 08/06/2021 15:25 7199
08/06/2021 09:05Solids 93188 S-1 08/06/2021 15:25
08/06/2021 09:50Solids 93189 S-2 08/06/2021 15:25 7199
08/06/2021 09:50Solids 93189 S-2 08/06/2021 15:25
08/06/2021 11:45Solids 93190 S-3 08/06/2021 15:25 7199
08/06/2021 11:45Solids 93190 S-3 08/06/2021 15:25
08/06/2021 10:45Solids 93191 S-4 08/06/2021 15:25 7199
08/06/2021 10:45Solids 93191 S-4 08/06/2021 15:25
08/06/2021Solids 93192 Dup-1 08/06/2021 15:25 7199
08/06/2021Solids 93192 Dup-1 08/06/2021 15:25
: Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 87
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-218-0030
Report Limit
Project:PRO-014
V 93188S-1
2.50 08/10/2021 20:056020BArsenicmg/Kg - dry 0.131
35.8 08/10/2021 20:056020BBariummg/Kg - dry 1.96
176 08/10/2021 20:056020BChromiummg/Kg - dry 0.405
13.3 08/10/2021 20:056020BLeadmg/Kg - dry 0.196
0.106 08/10/2021 16:347471BMercury (Total)mg/Kg - dry 0.0168
J0.024 08/10/2021 19:328260DAcetonemg/Kg - dry 0.003
J0.0009 08/10/2021 19:328260DBenzenemg/Kg - dry 0.0008
J0.001 08/10/2021 19:328260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
28.5 08/12/2021 17:20SW-DRYWT Moisture %
V 93189S-2
4.81 08/10/2021 20:126020BArsenicmg/Kg - dry 0.102
99.4 08/10/2021 20:126020BBariummg/Kg - dry 1.51
J0.275 08/10/2021 20:126020BCadmiummg/Kg - dry 0.0594
40.2 08/10/2021 20:126020BChromiummg/Kg - dry 0.313
83.1 08/10/2021 20:126020BLeadmg/Kg - dry 0.151
J1.65 08/10/2021 20:126020BSeleniummg/Kg - dry 0.972
J0.0988 08/10/2021 20:126020BSilvermg/Kg - dry 0.0442
0.0501 08/10/2021 16:367471BMercury (Total)mg/Kg - dry 0.0130
0.091 08/10/2021 20:028260DAcetonemg/Kg - dry 0.002
J0.005 08/10/2021 20:028260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.159 08/13/2021 14:378270EBenzo(a)pyrene mg/Kg - dry 0.159
J0.257 08/13/2021 14:378270EBenzo(b)fluoranthene mg/Kg - dry 0.158
J0.171 08/13/2021 14:378270EFluoranthenemg/Kg - dry 0.133
J0.180 08/13/2021 14:378270EPyrenemg/Kg - dry 0.145
7.44 08/12/2021 17:20SW-DRYWT Moisture %
V 93190S-3
2.21 08/10/2021 20:186020BArsenicmg/Kg - dry 0.111
26.5 08/10/2021 20:186020BBariummg/Kg - dry 1.66
120 08/10/2021 20:186020BChromiummg/Kg - dry 0.343
21.9 08/10/2021 20:186020BLeadmg/Kg - dry 0.166
J1.29 08/10/2021 20:186020BSeleniummg/Kg - dry 1.07
J0.0707 08/10/2021 20:186020BSilvermg/Kg - dry 0.0485
0.0637 08/10/2021 16:397471BMercury (Total)mg/Kg - dry 0.0142
J0.009 08/10/2021 20:318260DAcetonemg/Kg - dry 0.002
15.5 08/12/2021 17:20SW-DRYWT Moisture %
Page 4 of 87
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-218-0030
Report Limit
Project:PRO-014
V 93191S-4
7.36 08/10/2021 20:386020BArsenicmg/Kg - dry 0.104
101 08/10/2021 20:386020BBariummg/Kg - dry 1.55
J0.399 08/10/2021 20:386020BCadmiummg/Kg - dry 0.0610
34.5 08/10/2021 20:386020BChromiummg/Kg - dry 0.322
71.5 08/10/2021 20:386020BLeadmg/Kg - dry 0.155
J1.97 08/10/2021 20:386020BSeleniummg/Kg - dry 0.999
J0.105 08/10/2021 20:386020BSilvermg/Kg - dry 0.0455
0.0789 08/12/2021 15:307471BMercury (Total)mg/Kg - dry 0.0133
0.104 08/10/2021 21:018260DAcetonemg/Kg - dry 0.002
J0.001 08/10/2021 21:018260DAcroleinmg/Kg - dry 0.001
J0.006 08/10/2021 21:018260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.287 08/13/2021 15:008270EBenzo(a)pyrene mg/Kg - dry 0.163
J0.456 08/13/2021 15:008270EBenzo(b)fluoranthene mg/Kg - dry 0.162
J0.215 08/13/2021 15:008270EBenzo(g,h,i)perylene mg/Kg - dry 0.151
J0.178 08/13/2021 15:008270EChrysenemg/Kg - dry 0.157
J0.193 08/13/2021 15:008270EFluoranthenemg/Kg - dry 0.136
J0.226 08/13/2021 15:008270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.198
J0.220 08/13/2021 15:008270EPyrenemg/Kg - dry 0.148
9.94 08/12/2021 17:20SW-DRYWT Moisture %
V 93192Dup-1
2.27 08/10/2021 20:446020BArsenicmg/Kg - dry 0.119
50.0 08/10/2021 20:446020BBariummg/Kg - dry 1.77
134 08/10/2021 20:446020BChromiummg/Kg - dry 0.367
11.4 08/10/2021 20:446020BLeadmg/Kg - dry 0.177
0.0405 08/10/2021 16:417471BMercury (Total)mg/Kg - dry 0.0152
0.041 08/10/2021 21:318260DAcetonemg/Kg - dry 0.003
J0.003 08/10/2021 21:318260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
21.0 08/12/2021 17:20SW-DRYWT Moisture %
Page 5 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-1
93188 Matrix:
8/6/2021 9:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.5 %Moisture 1 08/12/21 17:20 SW-DRYWTEDV
2.50 mg/Kg - dry 0.131 1.40Arsenic 10 08/10/21 20:05 6020BEDV
35.8 mg/Kg - dry 1.96 14.0Barium 10 08/10/21 20:05 6020BEDV
<0.0769 mg/Kg - dry 0.0769 0.699Cadmium 10 08/10/21 20:05 6020BEDV
176 mg/Kg - dry 0.405 1.40Chromium 10 08/10/21 20:05 6020BEDV
13.3 mg/Kg - dry 0.196 1.40
Lead 10 08/10/21 20:05 6020BEDV
0.106 mg/Kg - dry 0.0168 0.0420Mercury (Total)1 08/10/21 16:34 7471BEDV
<1.26 mg/Kg - dry 1.26 2.80Selenium 10 08/10/21 20:05 6020BEDV
<0.0573 mg/Kg - dry 0.0573 0.699Silver 10 08/10/21 20:05 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 6 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-1
93188 Matrix:
8/6/2021 9:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
0.024 J mg/Kg - dry 0.003 0.027Acetone 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 08/10/21 19:32 V7457TBL
0.0009 J mg/Kg - dry 0.0008 0.006Benzene 1 08/10/21 19:32 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 08/10/21 19:32 V7457TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 08/10/21 19:32 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 08/10/21 19:32 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 08/10/21 19:32 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 08/10/21 19:32 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 08/10/21 19:32 V7457TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 08/10/21 19:32 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 08/10/21 19:32 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 08/10/21 19:32 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 08/10/21 19:32 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 08/10/21 19:32 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-1
93188 Matrix:
8/6/2021 9:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 08/10/21 19:32 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 08/10/21 19:32 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 08/10/21 19:32 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 08/10/21 19:32 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 08/10/21 19:32 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 08/10/21 19:32 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 08/10/21 19:32 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 08/10/21 19:32 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.006cis-1,3-Dichloropropene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 08/10/21 19:32 V7457TBL
<0.019 mg/Kg - dry 0.019 0.349Ethanol 1 08/10/21 19:32 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 08/10/21 19:32 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-1
93188 Matrix:
8/6/2021 9:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 08/10/21 19:32 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 08/10/21 19:32 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 08/10/21 19:32 V7457TBL
0.001 J mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 08/10/21 19:32 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 08/10/21 19:32 V7457TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 08/10/21 19:32 V7457TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 08/10/21 19:32 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.006n-Propylbenzene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 08/10/21 19:32 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 08/10/21 19:32 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 08/10/21 19:32 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.013
1,2,3-Trichlorobenzene 1 08/10/21 19:32 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 08/10/21 19:32 V7457TBL
<0.002 mg/Kg - dry 0.002 0.0061,1,1-Trichloroethane 1 08/10/21 19:32 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 08/10/21 19:32 V7457TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0061,2,3-Trichloropropane 1 08/10/21 19:32 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-1
93188 Matrix:
8/6/2021 9:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 08/10/21 19:32 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 08/10/21 19:32 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 08/10/21 19:32 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 08/10/21 19:32 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 08/10/21 19:32 V7457TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 08/10/21 19:32 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 08/10/21 19:32 V7457
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%08/10/21 19:321 TBL V7457
Surrogate: Dibromofluoromethane 103 Limits: 84-123%08/10/21 19:321 TBL V7457
Surrogate: Toluene-d8 96.4 Limits: 76-129%08/10/21 19:321 TBL V7457
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.162 mg/Kg - dry 0.162 0.923Acenaphthene 1 08/13/21 13:28 V7647JMV
<0.146 mg/Kg - dry 0.146 0.923Acenaphthylene 1 08/13/21 13:28 V7647JMV
<0.212 mg/Kg - dry 0.212 0.923Aniline 1 08/13/21 13:28 V7647JMV
<0.200 mg/Kg - dry 0.200 0.923Anthracene 1 08/13/21 13:28 V7647JMV
<0.194 mg/Kg - dry 0.194 0.923
Benzo(a)anthracene 1 08/13/21 13:28 V7647JMV
<0.205 mg/Kg - dry 0.205 0.923Benzo(a)pyrene 1 08/13/21 13:28 V7647JMV
<0.204 mg/Kg - dry 0.204 0.923Benzo(b)fluoranthene 1 08/13/21 13:28 V7647JMV
<0.190 mg/Kg - dry 0.190 0.923Benzo(g,h,i)perylene 1 08/13/21 13:28 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-1
93188 Matrix:
8/6/2021 9:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.191 mg/Kg - dry 0.191 0.923Benzo(k)fluoranthene 1 08/13/21 13:28 V7647JMV
<0.811 mg/Kg - dry 0.811 2.80Benzoic Acid 1 08/13/21 13:28 V7647JMV
<0.146 mg/Kg - dry 0.146 0.923Benzyl alcohol 1 08/13/21 13:28 V7647JMV
<0.165 mg/Kg - dry 0.165 0.923Bis(2-Chloroethoxy)methane 1 08/13/21 13:28 V7647JMV
<0.149 mg/Kg - dry 0.149 0.923Bis(2-Chloroethyl)ether 1 08/13/21 13:28 V7647JMV
<0.190 mg/Kg - dry 0.190 0.461Bis(2-Chloroisopropyl)ether 1 08/13/21 13:28 V7647JMV
<0.167 mg/Kg - dry 0.167 0.923Bis(2-ethylhexyl)phthalate 1 08/13/21 13:28 V7647JMV
<0.152 mg/Kg - dry 0.152 0.9234-Bromophenyl phenyl ether 1 08/13/21 13:28 V7647JMV
<0.158 mg/Kg - dry 0.158 0.461
Butyl benzyl phthalate 1 08/13/21 13:28 V7647JMV
<0.129 mg/Kg - dry 0.129 0.9234-Chloro-3-methylphenol 1 08/13/21 13:28 V7647JMV
<0.156 mg/Kg - dry 0.156 0.4614-Chloroaniline 1 08/13/21 13:28 V7647JMV
<0.162 mg/Kg - dry 0.162 0.9232-Chloronaphthalene 1 08/13/21 13:28 V7647JMV
<0.137 mg/Kg - dry 0.137 0.9232-Chlorophenol 1 08/13/21 13:28 V7647JMV
<0.176 mg/Kg - dry 0.176 1.404-Chlorophenyl phenyl ether 1 08/13/21 13:28 V7647JMV
<0.198 mg/Kg - dry 0.198 0.923Chrysene 1 08/13/21 13:28 V7647JMV
<0.321 mg/Kg - dry 0.321 0.923
Dibenz(a,h)anthracene 1 08/13/21 13:28 V7647JMV
<0.166 mg/Kg - dry 0.166 0.923Dibenzofuran 1 08/13/21 13:28 V7647JMV
<0.132 mg/Kg - dry 0.132 0.9231,2-Dichlorobenzene 1 08/13/21 13:28 V7647JMV
<0.136 mg/Kg - dry 0.136 0.9231,3-Dichlorobenzene 1 08/13/21 13:28 V7647JMV
<0.136 mg/Kg - dry 0.136 0.4611,4-Dichlorobenzene 1 08/13/21 13:28 V7647JMV
<0.205 mg/Kg - dry 0.205 0.9233,3'-Dichlorobenzidine 1 08/13/21 13:28 V7647JMV
<0.133 mg/Kg - dry 0.133 0.9232,4-Dichlorophenol 1 08/13/21 13:28 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-1
93188 Matrix:
8/6/2021 9:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.251 mg/Kg - dry 0.251 0.923Diethyl phthalate 1 08/13/21 13:28 V7647JMV
<0.243 mg/Kg - dry 0.243 0.923Dimethyl phthalate 1 08/13/21 13:28 V7647JMV
<0.151 mg/Kg - dry 0.151 0.4612,4-Dimethylphenol 1 08/13/21 13:28 V7647JMV
<0.149 mg/Kg - dry 0.149 0.923Di-n-butyl phthalate 1 08/13/21 13:28 V7647JMV
<0.335 mg/Kg - dry 0.335 2.104,6-Dinitro-2-methylphenol 1 08/13/21 13:28 V7647JMV
<0.727 mg/Kg - dry 0.727 2.102,4-Dinitrophenol 1 08/13/21 13:28 V7647JMV
<0.135 mg/Kg - dry 0.135 0.9232,4-Dinitrotoluene 1 08/13/21 13:28 V7647JMV
<0.151 mg/Kg - dry 0.151 0.9232,6-Dinitrotoluene 1 08/13/21 13:28 V7647JMV
<0.200 mg/Kg - dry 0.200 0.461
Di-n-Octyl Phthalate 1 08/13/21 13:28 V7647JMV
<0.172 mg/Kg - dry 0.172 0.923Fluoranthene 1 08/13/21 13:28 V7647JMV
<0.179 mg/Kg - dry 0.179 0.923Fluorene 1 08/13/21 13:28 V7647JMV
<0.148 mg/Kg - dry 0.148 0.923Hexachlorobenzene 1 08/13/21 13:28 V7647JMV
<0.136 mg/Kg - dry 0.136 0.923Hexachlorobutadiene 1 08/13/21 13:28 V7647JMV
<0.219 mg/Kg - dry 0.219 0.923Hexachlorocyclopentadiene 1 08/13/21 13:28 V7647JMV
<0.110 mg/Kg - dry 0.110 0.923Hexachloroethane 1 08/13/21 13:28 V7647JMV
<0.250 mg/Kg - dry 0.250 0.923
Indeno(1,2,3-cd)pyrene 1 08/13/21 13:28 V7647JMV
<0.267 mg/Kg - dry 0.267 0.923Isophorone 1 08/13/21 13:28 V7647JMV
<0.148 mg/Kg - dry 0.148 0.9231-Methylnaphthalene 1 08/13/21 13:28 V7647JMV
<0.139 mg/Kg - dry 0.139 0.9232-Methylnaphthalene 1 08/13/21 13:28 V7647JMV
<0.135 mg/Kg - dry 0.135 0.9232-Methylphenol 1 08/13/21 13:28 V7647JMV
<0.118 mg/Kg - dry 0.118 0.9233&4 Methylphenol 1 08/13/21 13:28 V7647JMV
<0.201 mg/Kg - dry 0.201 0.923Naphthalene 1 08/13/21 13:28 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-1
93188 Matrix:
8/6/2021 9:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.135 mg/Kg - dry 0.135 0.9232-Nitroaniline 1 08/13/21 13:28 V7647JMV
<0.167 mg/Kg - dry 0.167 0.9233-Nitroaniline 1 08/13/21 13:28 V7647JMV
<0.130 mg/Kg - dry 0.130 0.4614-Nitroaniline 1 08/13/21 13:28 V7647JMV
<0.162 mg/Kg - dry 0.162 0.461Nitrobenzene 1 08/13/21 13:28 V7647JMV
<0.124 mg/Kg - dry 0.124 0.9232-Nitrophenol 1 08/13/21 13:28 V7647JMV
<0.163 mg/Kg - dry 0.163 0.9234-Nitrophenol 1 08/13/21 13:28 V7647JMV
<0.367 mg/Kg - dry 0.367 0.923N-Nitrosodimethylamine 1 08/13/21 13:28 V7647JMV
<0.253 mg/Kg - dry 0.253 0.923N-Nitrosodiphenylamine 1 08/13/21 13:28 V7647JMV
<0.165 mg/Kg - dry 0.165 0.923
N-Nitroso-di-n-propylamine 1 08/13/21 13:28 V7647JMV
<0.485 mg/Kg - dry 0.485 1.40Pentachlorophenol 1 08/13/21 13:28 V7647JMV
<0.290 mg/Kg - dry 0.290 0.923Phenanthrene 1 08/13/21 13:28 V7647JMV
<0.156 mg/Kg - dry 0.156 0.923Phenol 1 08/13/21 13:28 V7647JMV
<0.187 mg/Kg - dry 0.187 0.923Pyrene 1 08/13/21 13:28 V7647JMV
<0.110 mg/Kg - dry 0.110 0.461Pyridine 1 08/13/21 13:28 V7647JMV
<0.149 mg/Kg - dry 0.149 0.9231,2,4-Trichlorobenzene 1 08/13/21 13:28 V7647JMV
<0.134 mg/Kg - dry 0.134 0.923
2,4,5-Trichlorophenol 1 08/13/21 13:28 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-1
93188 Matrix:
8/6/2021 9:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.135 mg/Kg - dry 0.135 0.9232,4,6-Trichlorophenol 1 08/13/21 13:28 V7647JMV
Surrogate: Phenol-d5 65.1 Limits: 34-121%08/13/21 13:281 JMV V7647
Surrogate: 2-Fluorobiphenyl 74.7 Limits: 44-115%08/13/21 13:281 JMV V7647
Surrogate: 2-Fluorophenol 66.0 Limits: 35-115%08/13/21 13:281 JMV V7647
Surrogate: Nitrobenzene-d5 67.5 Limits: 37-122%08/13/21 13:281 JMV V7647
Surrogate: 4-Terphenyl-d14 76.5 Limits: 54-127%08/13/21 13:281 JMV V7647
Surrogate: 2,4,6-Tribromophenol 68.7 Limits: 39-132%08/13/21 13:281 JMV V7647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-2
93189 Matrix:
8/6/2021 9:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
7.44 %Moisture 1 08/12/21 17:20 SW-DRYWTEDV
4.81 mg/Kg - dry 0.102 1.08Arsenic 10 08/10/21 20:12 6020BEDV
99.4 mg/Kg - dry 1.51 10.8Barium 10 08/10/21 20:12 6020BEDV
0.275 J mg/Kg - dry 0.0594 0.540Cadmium 10 08/10/21 20:12 6020BEDV
40.2 mg/Kg - dry 0.313 1.08Chromium 10 08/10/21 20:12 6020BEDV
83.1 mg/Kg - dry 0.151 1.08
Lead 10 08/10/21 20:12 6020BEDV
0.0501 mg/Kg - dry 0.0130 0.0324Mercury (Total)1 08/10/21 16:36 7471BEDV
1.65 J mg/Kg - dry 0.972 2.16Selenium 10 08/10/21 20:12 6020BEDV
0.0988 J mg/Kg - dry 0.0442 0.540Silver 10 08/10/21 20:12 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 15 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-2
93189 Matrix:
8/6/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
0.091 mg/Kg - dry 0.002 0.021Acetone 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 08/10/21 20:02 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 08/10/21 20:02 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 08/10/21 20:02 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.010
Bromomethane 1 08/10/21 20:02 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 08/10/21 20:02 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 08/10/21 20:02 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 08/10/21 20:02 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 08/10/21 20:02 V7457TBL
<0.0010 mg/Kg - dry 0.0010 0.005
Chlorodibromomethane 1 08/10/21 20:02 V7457TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 08/10/21 20:02 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 08/10/21 20:02 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 08/10/21 20:02 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 08/10/21 20:02 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-2
93189 Matrix:
8/6/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 08/10/21 20:02 V7457TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 08/10/21 20:02 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,4-Dichlorobenzene 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 08/10/21 20:02 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 08/10/21 20:02 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 08/10/21 20:02 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 08/10/21 20:02 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 08/10/21 20:02 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloropropene 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 08/10/21 20:02 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 08/10/21 20:02 V7457TBL
<0.015 mg/Kg - dry 0.015 0.270Ethanol 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 08/10/21 20:02 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.054Ethyl Tertiary Butyl Ether (ETBE)1 08/10/21 20:02 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.010Hexachlorobutadiene 1 08/10/21 20:02 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-2
93189 Matrix:
8/6/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 08/10/21 20:02 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 08/10/21 20:02 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 08/10/21 20:02 V7457TBL
0.005 J mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 08/10/21 20:02 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 08/10/21 20:02 V7457TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.010
Naphthalene 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 08/10/21 20:02 V7457TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 08/10/21 20:02 V7457TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 08/10/21 20:02 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.010
1,2,3-Trichlorobenzene 1 08/10/21 20:02 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 08/10/21 20:02 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 08/10/21 20:02 V7457TBL
<0.0010 mg/Kg - dry 0.0010 0.005Trichloroethene 1 08/10/21 20:02 V7457TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 08/10/21 20:02 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 08/10/21 20:02 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-2
93189 Matrix:
8/6/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 08/10/21 20:02 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 08/10/21 20:02 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 08/10/21 20:02 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 08/10/21 20:02 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 08/10/21 20:02 V7457TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 08/10/21 20:02 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 08/10/21 20:02 V7457
Surrogate: 4-Bromofluorobenzene 99.3 Limits: 70-130%08/10/21 20:021 TBL V7457
Surrogate: Dibromofluoromethane 101 Limits: 84-123%08/10/21 20:021 TBL V7457
Surrogate: Toluene-d8 95.4 Limits: 76-129%08/10/21 20:021 TBL V7457
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.126 mg/Kg - dry 0.126 0.719Acenaphthene 1 08/13/21 14:37 V7647JMV
<0.114 mg/Kg - dry 0.114 0.719Acenaphthylene 1 08/13/21 14:37 V7647JMV
<0.165 mg/Kg - dry 0.165 0.719Aniline 1 08/13/21 14:37 V7647JMV
<0.155 mg/Kg - dry 0.155 0.719Anthracene 1 08/13/21 14:37 V7647JMV
<0.151 mg/Kg - dry 0.151 0.719
Benzo(a)anthracene 1 08/13/21 14:37 V7647JMV
0.159 J mg/Kg - dry 0.159 0.719Benzo(a)pyrene 1 08/13/21 14:37 V7647JMV
0.257 J mg/Kg - dry 0.158 0.719Benzo(b)fluoranthene 1 08/13/21 14:37 V7647JMV
<0.148 mg/Kg - dry 0.148 0.719Benzo(g,h,i)perylene 1 08/13/21 14:37 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-2
93189 Matrix:
8/6/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.149 mg/Kg - dry 0.149 0.719Benzo(k)fluoranthene 1 08/13/21 14:37 V7647JMV
<0.633 mg/Kg - dry 0.633 2.18Benzoic Acid 1 08/13/21 14:37 V7647JMV
<0.114 mg/Kg - dry 0.114 0.719Benzyl alcohol 1 08/13/21 14:37 V7647JMV
<0.128 mg/Kg - dry 0.128 0.719Bis(2-Chloroethoxy)methane 1 08/13/21 14:37 V7647JMV
<0.116 mg/Kg - dry 0.116 0.719Bis(2-Chloroethyl)ether 1 08/13/21 14:37 V7647JMV
<0.148 mg/Kg - dry 0.148 0.359Bis(2-Chloroisopropyl)ether 1 08/13/21 14:37 V7647JMV
<0.130 mg/Kg - dry 0.130 0.719Bis(2-ethylhexyl)phthalate 1 08/13/21 14:37 V7647JMV
<0.118 mg/Kg - dry 0.118 0.7194-Bromophenyl phenyl ether 1 08/13/21 14:37 V7647JMV
<0.123 mg/Kg - dry 0.123 0.359
Butyl benzyl phthalate 1 08/13/21 14:37 V7647JMV
<0.100 mg/Kg - dry 0.100 0.7194-Chloro-3-methylphenol 1 08/13/21 14:37 V7647JMV
<0.122 mg/Kg - dry 0.122 0.3594-Chloroaniline 1 08/13/21 14:37 V7647JMV
<0.126 mg/Kg - dry 0.126 0.7192-Chloronaphthalene 1 08/13/21 14:37 V7647JMV
<0.107 mg/Kg - dry 0.107 0.7192-Chlorophenol 1 08/13/21 14:37 V7647JMV
<0.137 mg/Kg - dry 0.137 1.094-Chlorophenyl phenyl ether 1 08/13/21 14:37 V7647JMV
<0.154 mg/Kg - dry 0.154 0.719Chrysene 1 08/13/21 14:37 V7647JMV
<0.250 mg/Kg - dry 0.250 0.719
Dibenz(a,h)anthracene 1 08/13/21 14:37 V7647JMV
<0.129 mg/Kg - dry 0.129 0.719Dibenzofuran 1 08/13/21 14:37 V7647JMV
<0.102 mg/Kg - dry 0.102 0.7191,2-Dichlorobenzene 1 08/13/21 14:37 V7647JMV
<0.106 mg/Kg - dry 0.106 0.7191,3-Dichlorobenzene 1 08/13/21 14:37 V7647JMV
<0.106 mg/Kg - dry 0.106 0.3591,4-Dichlorobenzene 1 08/13/21 14:37 V7647JMV
<0.159 mg/Kg - dry 0.159 0.7193,3'-Dichlorobenzidine 1 08/13/21 14:37 V7647JMV
<0.104 mg/Kg - dry 0.104 0.7192,4-Dichlorophenol 1 08/13/21 14:37 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-2
93189 Matrix:
8/6/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.196 mg/Kg - dry 0.196 0.719Diethyl phthalate 1 08/13/21 14:37 V7647JMV
<0.190 mg/Kg - dry 0.190 0.719Dimethyl phthalate 1 08/13/21 14:37 V7647JMV
<0.117 mg/Kg - dry 0.117 0.3592,4-Dimethylphenol 1 08/13/21 14:37 V7647JMV
<0.116 mg/Kg - dry 0.116 0.719Di-n-butyl phthalate 1 08/13/21 14:37 V7647JMV
<0.261 mg/Kg - dry 0.261 1.634,6-Dinitro-2-methylphenol 1 08/13/21 14:37 V7647JMV
<0.565 mg/Kg - dry 0.565 1.632,4-Dinitrophenol 1 08/13/21 14:37 V7647JMV
<0.105 mg/Kg - dry 0.105 0.7192,4-Dinitrotoluene 1 08/13/21 14:37 V7647JMV
<0.117 mg/Kg - dry 0.117 0.7192,6-Dinitrotoluene 1 08/13/21 14:37 V7647JMV
<0.155 mg/Kg - dry 0.155 0.359
Di-n-Octyl Phthalate 1 08/13/21 14:37 V7647JMV
0.171 J mg/Kg - dry 0.133 0.719Fluoranthene 1 08/13/21 14:37 V7647JMV
<0.139 mg/Kg - dry 0.139 0.719Fluorene 1 08/13/21 14:37 V7647JMV
<0.115 mg/Kg - dry 0.115 0.719Hexachlorobenzene 1 08/13/21 14:37 V7647JMV
<0.106 mg/Kg - dry 0.106 0.719Hexachlorobutadiene 1 08/13/21 14:37 V7647JMV
<0.170 mg/Kg - dry 0.170 0.719Hexachlorocyclopentadiene 1 08/13/21 14:37 V7647JMV
<0.086 mg/Kg - dry 0.086 0.719Hexachloroethane 1 08/13/21 14:37 V7647JMV
<0.195 mg/Kg - dry 0.195 0.719
Indeno(1,2,3-cd)pyrene 1 08/13/21 14:37 V7647JMV
<0.208 mg/Kg - dry 0.208 0.719Isophorone 1 08/13/21 14:37 V7647JMV
<0.115 mg/Kg - dry 0.115 0.7191-Methylnaphthalene 1 08/13/21 14:37 V7647JMV
<0.109 mg/Kg - dry 0.109 0.7192-Methylnaphthalene 1 08/13/21 14:37 V7647JMV
<0.105 mg/Kg - dry 0.105 0.7192-Methylphenol 1 08/13/21 14:37 V7647JMV
<0.092 mg/Kg - dry 0.092 0.7193&4 Methylphenol 1 08/13/21 14:37 V7647JMV
<0.156 mg/Kg - dry 0.156 0.719Naphthalene 1 08/13/21 14:37 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-2
93189 Matrix:
8/6/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.105 mg/Kg - dry 0.105 0.7192-Nitroaniline 1 08/13/21 14:37 V7647JMV
<0.130 mg/Kg - dry 0.130 0.7193-Nitroaniline 1 08/13/21 14:37 V7647JMV
<0.101 mg/Kg - dry 0.101 0.3594-Nitroaniline 1 08/13/21 14:37 V7647JMV
<0.126 mg/Kg - dry 0.126 0.359Nitrobenzene 1 08/13/21 14:37 V7647JMV
<0.096 mg/Kg - dry 0.096 0.7192-Nitrophenol 1 08/13/21 14:37 V7647JMV
<0.127 mg/Kg - dry 0.127 0.7194-Nitrophenol 1 08/13/21 14:37 V7647JMV
<0.286 mg/Kg - dry 0.286 0.719N-Nitrosodimethylamine 1 08/13/21 14:37 V7647JMV
<0.197 mg/Kg - dry 0.197 0.719N-Nitrosodiphenylamine 1 08/13/21 14:37 V7647JMV
<0.128 mg/Kg - dry 0.128 0.719
N-Nitroso-di-n-propylamine 1 08/13/21 14:37 V7647JMV
<0.378 mg/Kg - dry 0.378 1.09Pentachlorophenol 1 08/13/21 14:37 V7647JMV
<0.226 mg/Kg - dry 0.226 0.719Phenanthrene 1 08/13/21 14:37 V7647JMV
<0.122 mg/Kg - dry 0.122 0.719Phenol 1 08/13/21 14:37 V7647JMV
0.180 J mg/Kg - dry 0.145 0.719Pyrene 1 08/13/21 14:37 V7647JMV
<0.086 mg/Kg - dry 0.086 0.359Pyridine 1 08/13/21 14:37 V7647JMV
<0.116 mg/Kg - dry 0.116 0.7191,2,4-Trichlorobenzene 1 08/13/21 14:37 V7647JMV
<0.104 mg/Kg - dry 0.104 0.719
2,4,5-Trichlorophenol 1 08/13/21 14:37 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-2
93189 Matrix:
8/6/2021 9:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.105 mg/Kg - dry 0.105 0.7192,4,6-Trichlorophenol 1 08/13/21 14:37 V7647JMV
Surrogate: Phenol-d5 58.6 Limits: 34-121%08/13/21 14:371 JMV V7647
Surrogate: 2-Fluorobiphenyl 69.6 Limits: 44-115%08/13/21 14:371 JMV V7647
Surrogate: 2-Fluorophenol 58.3 Limits: 35-115%08/13/21 14:371 JMV V7647
Surrogate: Nitrobenzene-d5 62.5 Limits: 37-122%08/13/21 14:371 JMV V7647
Surrogate: 4-Terphenyl-d14 73.2 Limits: 54-127%08/13/21 14:371 JMV V7647
Surrogate: 2,4,6-Tribromophenol 58.0 Limits: 39-132%08/13/21 14:371 JMV V7647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-3
93190 Matrix:
8/6/2021 11:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.5 %Moisture 1 08/12/21 17:20 SW-DRYWTEDV
2.21 mg/Kg - dry 0.111 1.18Arsenic 10 08/10/21 20:18 6020BEDV
26.5 mg/Kg - dry 1.66 11.8Barium 10 08/10/21 20:18 6020BEDV
<0.0650 mg/Kg - dry 0.0650 0.592Cadmium 10 08/10/21 20:18 6020BEDV
120 mg/Kg - dry 0.343 1.18Chromium 10 08/10/21 20:18 6020BEDV
21.9 mg/Kg - dry 0.166 1.18
Lead 10 08/10/21 20:18 6020BEDV
0.0637 mg/Kg - dry 0.0142 0.0355Mercury (Total)1 08/10/21 16:39 7471BEDV
1.29 J mg/Kg - dry 1.07 2.37Selenium 10 08/10/21 20:18 6020BEDV
0.0707 J mg/Kg - dry 0.0485 0.592Silver 10 08/10/21 20:18 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 24 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-3
93190 Matrix:
8/6/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
0.009 J mg/Kg - dry 0.002 0.023Acetone 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 08/10/21 20:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 08/10/21 20:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 08/10/21 20:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 08/10/21 20:31 V7457TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 08/10/21 20:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 08/10/21 20:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 08/10/21 20:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 08/10/21 20:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 08/10/21 20:31 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 08/10/21 20:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 08/10/21 20:31 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-3
93190 Matrix:
8/6/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 08/10/21 20:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 08/10/21 20:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 08/10/21 20:31 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 08/10/21 20:31 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 08/10/21 20:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 08/10/21 20:31 V7457TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 08/10/21 20:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 08/10/21 20:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 08/10/21 20:31 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 08/10/21 20:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,3-Dichloropropane 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 08/10/21 20:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 08/10/21 20:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 08/10/21 20:31 V7457TBL
<0.016 mg/Kg - dry 0.016 0.295Ethanol 1 08/10/21 20:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 08/10/21 20:31 V7457TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 08/10/21 20:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 08/10/21 20:31 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-3
93190 Matrix:
8/6/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 08/10/21 20:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 08/10/21 20:31 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 08/10/21 20:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 08/10/21 20:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 08/10/21 20:31 V7457TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 08/10/21 20:31 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 08/10/21 20:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 08/10/21 20:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 08/10/21 20:31 V7457TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 08/10/21 20:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 08/10/21 20:31 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-3
93190 Matrix:
8/6/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 08/10/21 20:31 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 08/10/21 20:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 08/10/21 20:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 08/10/21 20:31 V7457
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%08/10/21 20:311 TBL V7457
Surrogate: Dibromofluoromethane 102 Limits: 84-123%08/10/21 20:311 TBL V7457
Surrogate: Toluene-d8 94.9 Limits: 76-129%08/10/21 20:311 TBL V7457
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.137 mg/Kg - dry 0.137 0.781Acenaphthene 1 08/13/21 14:14 V7647JMV
<0.124 mg/Kg - dry 0.124 0.781Acenaphthylene 1 08/13/21 14:14 V7647JMV
<0.179 mg/Kg - dry 0.179 0.781Aniline 1 08/13/21 14:14 V7647JMV
<0.169 mg/Kg - dry 0.169 0.781Anthracene 1 08/13/21 14:14 V7647JMV
<0.164 mg/Kg - dry 0.164 0.781
Benzo(a)anthracene 1 08/13/21 14:14 V7647JMV
<0.173 mg/Kg - dry 0.173 0.781Benzo(a)pyrene 1 08/13/21 14:14 V7647JMV
<0.172 mg/Kg - dry 0.172 0.781Benzo(b)fluoranthene 1 08/13/21 14:14 V7647JMV
<0.160 mg/Kg - dry 0.160 0.781Benzo(g,h,i)perylene 1 08/13/21 14:14 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-3
93190 Matrix:
8/6/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.162 mg/Kg - dry 0.162 0.781Benzo(k)fluoranthene 1 08/13/21 14:14 V7647JMV
<0.686 mg/Kg - dry 0.686 2.37Benzoic Acid 1 08/13/21 14:14 V7647JMV
<0.124 mg/Kg - dry 0.124 0.781Benzyl alcohol 1 08/13/21 14:14 V7647JMV
<0.139 mg/Kg - dry 0.139 0.781Bis(2-Chloroethoxy)methane 1 08/13/21 14:14 V7647JMV
<0.126 mg/Kg - dry 0.126 0.781Bis(2-Chloroethyl)ether 1 08/13/21 14:14 V7647JMV
<0.160 mg/Kg - dry 0.160 0.390Bis(2-Chloroisopropyl)ether 1 08/13/21 14:14 V7647JMV
<0.142 mg/Kg - dry 0.142 0.781Bis(2-ethylhexyl)phthalate 1 08/13/21 14:14 V7647JMV
<0.128 mg/Kg - dry 0.128 0.7814-Bromophenyl phenyl ether 1 08/13/21 14:14 V7647JMV
<0.133 mg/Kg - dry 0.133 0.390
Butyl benzyl phthalate 1 08/13/21 14:14 V7647JMV
<0.109 mg/Kg - dry 0.109 0.7814-Chloro-3-methylphenol 1 08/13/21 14:14 V7647JMV
<0.132 mg/Kg - dry 0.132 0.3904-Chloroaniline 1 08/13/21 14:14 V7647JMV
<0.137 mg/Kg - dry 0.137 0.7812-Chloronaphthalene 1 08/13/21 14:14 V7647JMV
<0.116 mg/Kg - dry 0.116 0.7812-Chlorophenol 1 08/13/21 14:14 V7647JMV
<0.149 mg/Kg - dry 0.149 1.184-Chlorophenyl phenyl ether 1 08/13/21 14:14 V7647JMV
<0.168 mg/Kg - dry 0.168 0.781Chrysene 1 08/13/21 14:14 V7647JMV
<0.272 mg/Kg - dry 0.272 0.781
Dibenz(a,h)anthracene 1 08/13/21 14:14 V7647JMV
<0.140 mg/Kg - dry 0.140 0.781Dibenzofuran 1 08/13/21 14:14 V7647JMV
<0.111 mg/Kg - dry 0.111 0.7811,2-Dichlorobenzene 1 08/13/21 14:14 V7647JMV
<0.115 mg/Kg - dry 0.115 0.7811,3-Dichlorobenzene 1 08/13/21 14:14 V7647JMV
<0.115 mg/Kg - dry 0.115 0.3901,4-Dichlorobenzene 1 08/13/21 14:14 V7647JMV
<0.173 mg/Kg - dry 0.173 0.7813,3'-Dichlorobenzidine 1 08/13/21 14:14 V7647JMV
<0.113 mg/Kg - dry 0.113 0.7812,4-Dichlorophenol 1 08/13/21 14:14 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-3
93190 Matrix:
8/6/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.213 mg/Kg - dry 0.213 0.781Diethyl phthalate 1 08/13/21 14:14 V7647JMV
<0.205 mg/Kg - dry 0.205 0.781Dimethyl phthalate 1 08/13/21 14:14 V7647JMV
<0.127 mg/Kg - dry 0.127 0.3902,4-Dimethylphenol 1 08/13/21 14:14 V7647JMV
<0.126 mg/Kg - dry 0.126 0.781Di-n-butyl phthalate 1 08/13/21 14:14 V7647JMV
<0.284 mg/Kg - dry 0.284 1.784,6-Dinitro-2-methylphenol 1 08/13/21 14:14 V7647JMV
<0.615 mg/Kg - dry 0.615 1.782,4-Dinitrophenol 1 08/13/21 14:14 V7647JMV
<0.114 mg/Kg - dry 0.114 0.7812,4-Dinitrotoluene 1 08/13/21 14:14 V7647JMV
<0.127 mg/Kg - dry 0.127 0.7812,6-Dinitrotoluene 1 08/13/21 14:14 V7647JMV
<0.169 mg/Kg - dry 0.169 0.390
Di-n-Octyl Phthalate 1 08/13/21 14:14 V7647JMV
<0.145 mg/Kg - dry 0.145 0.781Fluoranthene 1 08/13/21 14:14 V7647JMV
<0.151 mg/Kg - dry 0.151 0.781Fluorene 1 08/13/21 14:14 V7647JMV
<0.125 mg/Kg - dry 0.125 0.781Hexachlorobenzene 1 08/13/21 14:14 V7647JMV
<0.115 mg/Kg - dry 0.115 0.781Hexachlorobutadiene 1 08/13/21 14:14 V7647JMV
<0.185 mg/Kg - dry 0.185 0.781Hexachlorocyclopentadiene 1 08/13/21 14:14 V7647JMV
<0.093 mg/Kg - dry 0.093 0.781Hexachloroethane 1 08/13/21 14:14 V7647JMV
<0.211 mg/Kg - dry 0.211 0.781
Indeno(1,2,3-cd)pyrene 1 08/13/21 14:14 V7647JMV
<0.226 mg/Kg - dry 0.226 0.781Isophorone 1 08/13/21 14:14 V7647JMV
<0.125 mg/Kg - dry 0.125 0.7811-Methylnaphthalene 1 08/13/21 14:14 V7647JMV
<0.118 mg/Kg - dry 0.118 0.7812-Methylnaphthalene 1 08/13/21 14:14 V7647JMV
<0.114 mg/Kg - dry 0.114 0.7812-Methylphenol 1 08/13/21 14:14 V7647JMV
<0.100 mg/Kg - dry 0.100 0.7813&4 Methylphenol 1 08/13/21 14:14 V7647JMV
<0.170 mg/Kg - dry 0.170 0.781Naphthalene 1 08/13/21 14:14 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-3
93190 Matrix:
8/6/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.114 mg/Kg - dry 0.114 0.7812-Nitroaniline 1 08/13/21 14:14 V7647JMV
<0.142 mg/Kg - dry 0.142 0.7813-Nitroaniline 1 08/13/21 14:14 V7647JMV
<0.110 mg/Kg - dry 0.110 0.3904-Nitroaniline 1 08/13/21 14:14 V7647JMV
<0.137 mg/Kg - dry 0.137 0.390Nitrobenzene 1 08/13/21 14:14 V7647JMV
<0.105 mg/Kg - dry 0.105 0.7812-Nitrophenol 1 08/13/21 14:14 V7647JMV
<0.138 mg/Kg - dry 0.138 0.7814-Nitrophenol 1 08/13/21 14:14 V7647JMV
<0.311 mg/Kg - dry 0.311 0.781N-Nitrosodimethylamine 1 08/13/21 14:14 V7647JMV
<0.214 mg/Kg - dry 0.214 0.781N-Nitrosodiphenylamine 1 08/13/21 14:14 V7647JMV
<0.139 mg/Kg - dry 0.139 0.781
N-Nitroso-di-n-propylamine 1 08/13/21 14:14 V7647JMV
<0.410 mg/Kg - dry 0.410 1.18Pentachlorophenol 1 08/13/21 14:14 V7647JMV
<0.246 mg/Kg - dry 0.246 0.781Phenanthrene 1 08/13/21 14:14 V7647JMV
<0.132 mg/Kg - dry 0.132 0.781Phenol 1 08/13/21 14:14 V7647JMV
<0.158 mg/Kg - dry 0.158 0.781Pyrene 1 08/13/21 14:14 V7647JMV
<0.093 mg/Kg - dry 0.093 0.390Pyridine 1 08/13/21 14:14 V7647JMV
<0.126 mg/Kg - dry 0.126 0.7811,2,4-Trichlorobenzene 1 08/13/21 14:14 V7647JMV
<0.113 mg/Kg - dry 0.113 0.781
2,4,5-Trichlorophenol 1 08/13/21 14:14 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-3
93190 Matrix:
8/6/2021 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.114 mg/Kg - dry 0.114 0.7812,4,6-Trichlorophenol 1 08/13/21 14:14 V7647JMV
Surrogate: Phenol-d5 69.5 Limits: 34-121%08/13/21 14:141 JMV V7647
Surrogate: 2-Fluorobiphenyl 78.3 Limits: 44-115%08/13/21 14:141 JMV V7647
Surrogate: 2-Fluorophenol 71.0 Limits: 35-115%08/13/21 14:141 JMV V7647
Surrogate: Nitrobenzene-d5 68.7 Limits: 37-122%08/13/21 14:141 JMV V7647
Surrogate: 4-Terphenyl-d14 79.5 Limits: 54-127%08/13/21 14:141 JMV V7647
Surrogate: 2,4,6-Tribromophenol 68.0 Limits: 39-132%08/13/21 14:141 JMV V7647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-4
93191 Matrix:
8/6/2021 10:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.94 %Moisture 1 08/12/21 17:20 SW-DRYWTEDV
7.36 mg/Kg - dry 0.104 1.11Arsenic 10 08/10/21 20:38 6020BEDV
101 mg/Kg - dry 1.55 11.1Barium 10 08/10/21 20:38 6020BEDV
0.399 J mg/Kg - dry 0.0610 0.555Cadmium 10 08/10/21 20:38 6020BEDV
34.5 mg/Kg - dry 0.322 1.11Chromium 10 08/10/21 20:38 6020BEDV
71.5 mg/Kg - dry 0.155 1.11
Lead 10 08/10/21 20:38 6020BEDV
0.0789 mg/Kg - dry 0.0133 0.0333Mercury (Total)1 08/12/21 15:30 7471BEDV
1.97 J mg/Kg - dry 0.999 2.22Selenium 10 08/10/21 20:38 6020BEDV
0.105 J mg/Kg - dry 0.0455 0.555Silver 10 08/10/21 20:38 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 33 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-4
93191 Matrix:
8/6/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
0.104 mg/Kg - dry 0.002 0.022Acetone 1 08/10/21 21:01 V7457TBL
0.001 J mg/Kg - dry 0.001 0.022Acrolein 1 08/10/21 21:01 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 08/10/21 21:01 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 08/10/21 21:01 V7457TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 08/10/21 21:01 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 08/10/21 21:01 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 08/10/21 21:01 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 08/10/21 21:01 V7457TBL
<0.0010 mg/Kg - dry 0.0010 0.005
Chlorodibromomethane 1 08/10/21 21:01 V7457TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 08/10/21 21:01 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 08/10/21 21:01 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 08/10/21 21:01 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 08/10/21 21:01 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-4
93191 Matrix:
8/6/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 08/10/21 21:01 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 08/10/21 21:01 V7457TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 08/10/21 21:01 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 08/10/21 21:01 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 08/10/21 21:01 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 08/10/21 21:01 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 08/10/21 21:01 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 08/10/21 21:01 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 08/10/21 21:01 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloropropene 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 08/10/21 21:01 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 08/10/21 21:01 V7457TBL
<0.015 mg/Kg - dry 0.015 0.277Ethanol 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 08/10/21 21:01 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 08/10/21 21:01 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 08/10/21 21:01 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-4
93191 Matrix:
8/6/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 08/10/21 21:01 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 08/10/21 21:01 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 08/10/21 21:01 V7457TBL
0.006 J mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 08/10/21 21:01 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 08/10/21 21:01 V7457TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 08/10/21 21:01 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 08/10/21 21:01 V7457TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 08/10/21 21:01 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 08/10/21 21:01 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 08/10/21 21:01 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 08/10/21 21:01 V7457TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 08/10/21 21:01 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 08/10/21 21:01 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-4
93191 Matrix:
8/6/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 08/10/21 21:01 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 08/10/21 21:01 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 08/10/21 21:01 V7457TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 08/10/21 21:01 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 08/10/21 21:01 V7457
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%08/10/21 21:011 TBL V7457
Surrogate: Dibromofluoromethane 101 Limits: 84-123%08/10/21 21:011 TBL V7457
Surrogate: Toluene-d8 96.8 Limits: 76-129%08/10/21 21:011 TBL V7457
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.128 mg/Kg - dry 0.128 0.732Acenaphthene 1 08/13/21 15:00 V7647JMV
<0.116 mg/Kg - dry 0.116 0.732Acenaphthylene 1 08/13/21 15:00 V7647JMV
<0.168 mg/Kg - dry 0.168 0.732Aniline 1 08/13/21 15:00 V7647JMV
<0.158 mg/Kg - dry 0.158 0.732Anthracene 1 08/13/21 15:00 V7647JMV
<0.154 mg/Kg - dry 0.154 0.732
Benzo(a)anthracene 1 08/13/21 15:00 V7647JMV
0.287 J mg/Kg - dry 0.163 0.732Benzo(a)pyrene 1 08/13/21 15:00 V7647JMV
0.456 J mg/Kg - dry 0.162 0.732Benzo(b)fluoranthene 1 08/13/21 15:00 V7647JMV
0.215 J mg/Kg - dry 0.151 0.732Benzo(g,h,i)perylene 1 08/13/21 15:00 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-4
93191 Matrix:
8/6/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.152 mg/Kg - dry 0.152 0.732Benzo(k)fluoranthene 1 08/13/21 15:00 V7647JMV
<0.644 mg/Kg - dry 0.644 2.22Benzoic Acid 1 08/13/21 15:00 V7647JMV
<0.116 mg/Kg - dry 0.116 0.732Benzyl alcohol 1 08/13/21 15:00 V7647JMV
<0.131 mg/Kg - dry 0.131 0.732Bis(2-Chloroethoxy)methane 1 08/13/21 15:00 V7647JMV
<0.118 mg/Kg - dry 0.118 0.732Bis(2-Chloroethyl)ether 1 08/13/21 15:00 V7647JMV
<0.151 mg/Kg - dry 0.151 0.366Bis(2-Chloroisopropyl)ether 1 08/13/21 15:00 V7647JMV
<0.133 mg/Kg - dry 0.133 0.732Bis(2-ethylhexyl)phthalate 1 08/13/21 15:00 V7647JMV
<0.121 mg/Kg - dry 0.121 0.7324-Bromophenyl phenyl ether 1 08/13/21 15:00 V7647JMV
<0.125 mg/Kg - dry 0.125 0.366
Butyl benzyl phthalate 1 08/13/21 15:00 V7647JMV
<0.102 mg/Kg - dry 0.102 0.7324-Chloro-3-methylphenol 1 08/13/21 15:00 V7647JMV
<0.124 mg/Kg - dry 0.124 0.3664-Chloroaniline 1 08/13/21 15:00 V7647JMV
<0.128 mg/Kg - dry 0.128 0.7322-Chloronaphthalene 1 08/13/21 15:00 V7647JMV
<0.109 mg/Kg - dry 0.109 0.7322-Chlorophenol 1 08/13/21 15:00 V7647JMV
<0.139 mg/Kg - dry 0.139 1.114-Chlorophenyl phenyl ether 1 08/13/21 15:00 V7647JMV
0.178 J mg/Kg - dry 0.157 0.732Chrysene 1 08/13/21 15:00 V7647JMV
<0.255 mg/Kg - dry 0.255 0.732
Dibenz(a,h)anthracene 1 08/13/21 15:00 V7647JMV
<0.132 mg/Kg - dry 0.132 0.732Dibenzofuran 1 08/13/21 15:00 V7647JMV
<0.104 mg/Kg - dry 0.104 0.7321,2-Dichlorobenzene 1 08/13/21 15:00 V7647JMV
<0.108 mg/Kg - dry 0.108 0.7321,3-Dichlorobenzene 1 08/13/21 15:00 V7647JMV
<0.108 mg/Kg - dry 0.108 0.3661,4-Dichlorobenzene 1 08/13/21 15:00 V7647JMV
<0.163 mg/Kg - dry 0.163 0.7323,3'-Dichlorobenzidine 1 08/13/21 15:00 V7647JMV
<0.106 mg/Kg - dry 0.106 0.7322,4-Dichlorophenol 1 08/13/21 15:00 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-4
93191 Matrix:
8/6/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.199 mg/Kg - dry 0.199 0.732Diethyl phthalate 1 08/13/21 15:00 V7647JMV
<0.193 mg/Kg - dry 0.193 0.732Dimethyl phthalate 1 08/13/21 15:00 V7647JMV
<0.119 mg/Kg - dry 0.119 0.3662,4-Dimethylphenol 1 08/13/21 15:00 V7647JMV
<0.118 mg/Kg - dry 0.118 0.732Di-n-butyl phthalate 1 08/13/21 15:00 V7647JMV
<0.266 mg/Kg - dry 0.266 1.674,6-Dinitro-2-methylphenol 1 08/13/21 15:00 V7647JMV
<0.577 mg/Kg - dry 0.577 1.672,4-Dinitrophenol 1 08/13/21 15:00 V7647JMV
<0.107 mg/Kg - dry 0.107 0.7322,4-Dinitrotoluene 1 08/13/21 15:00 V7647JMV
<0.119 mg/Kg - dry 0.119 0.7322,6-Dinitrotoluene 1 08/13/21 15:00 V7647JMV
<0.158 mg/Kg - dry 0.158 0.366
Di-n-Octyl Phthalate 1 08/13/21 15:00 V7647JMV
0.193 J mg/Kg - dry 0.136 0.732Fluoranthene 1 08/13/21 15:00 V7647JMV
<0.142 mg/Kg - dry 0.142 0.732Fluorene 1 08/13/21 15:00 V7647JMV
<0.117 mg/Kg - dry 0.117 0.732Hexachlorobenzene 1 08/13/21 15:00 V7647JMV
<0.108 mg/Kg - dry 0.108 0.732Hexachlorobutadiene 1 08/13/21 15:00 V7647JMV
<0.174 mg/Kg - dry 0.174 0.732Hexachlorocyclopentadiene 1 08/13/21 15:00 V7647JMV
<0.087 mg/Kg - dry 0.087 0.732Hexachloroethane 1 08/13/21 15:00 V7647JMV
0.226 J
mg/Kg - dry 0.198 0.732
Indeno(1,2,3-cd)pyrene 1 08/13/21 15:00 V7647JMV
<0.212 mg/Kg - dry 0.212 0.732Isophorone 1 08/13/21 15:00 V7647JMV
<0.117 mg/Kg - dry 0.117 0.7321-Methylnaphthalene 1 08/13/21 15:00 V7647JMV
<0.111 mg/Kg - dry 0.111 0.7322-Methylnaphthalene 1 08/13/21 15:00 V7647JMV
<0.107 mg/Kg - dry 0.107 0.7322-Methylphenol 1 08/13/21 15:00 V7647JMV
<0.094 mg/Kg - dry 0.094 0.7323&4 Methylphenol 1 08/13/21 15:00 V7647JMV
<0.159 mg/Kg - dry 0.159 0.732Naphthalene 1 08/13/21 15:00 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-4
93191 Matrix:
8/6/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.107 mg/Kg - dry 0.107 0.7322-Nitroaniline 1 08/13/21 15:00 V7647JMV
<0.133 mg/Kg - dry 0.133 0.7323-Nitroaniline 1 08/13/21 15:00 V7647JMV
<0.103 mg/Kg - dry 0.103 0.3664-Nitroaniline 1 08/13/21 15:00 V7647JMV
<0.128 mg/Kg - dry 0.128 0.366Nitrobenzene 1 08/13/21 15:00 V7647JMV
<0.098 mg/Kg - dry 0.098 0.7322-Nitrophenol 1 08/13/21 15:00 V7647JMV
<0.129 mg/Kg - dry 0.129 0.7324-Nitrophenol 1 08/13/21 15:00 V7647JMV
<0.292 mg/Kg - dry 0.292 0.732N-Nitrosodimethylamine 1 08/13/21 15:00 V7647JMV
<0.200 mg/Kg - dry 0.200 0.732N-Nitrosodiphenylamine 1 08/13/21 15:00 V7647JMV
<0.131 mg/Kg - dry 0.131 0.732
N-Nitroso-di-n-propylamine 1 08/13/21 15:00 V7647JMV
<0.385 mg/Kg - dry 0.385 1.11Pentachlorophenol 1 08/13/21 15:00 V7647JMV
<0.230 mg/Kg - dry 0.230 0.732Phenanthrene 1 08/13/21 15:00 V7647JMV
<0.124 mg/Kg - dry 0.124 0.732Phenol 1 08/13/21 15:00 V7647JMV
0.220 J mg/Kg - dry 0.148 0.732Pyrene 1 08/13/21 15:00 V7647JMV
<0.087 mg/Kg - dry 0.087 0.366Pyridine 1 08/13/21 15:00 V7647JMV
<0.118 mg/Kg - dry 0.118 0.7321,2,4-Trichlorobenzene 1 08/13/21 15:00 V7647JMV
<0.106 mg/Kg - dry 0.106 0.732
2,4,5-Trichlorophenol 1 08/13/21 15:00 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:S-4
93191 Matrix:
8/6/2021 10:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.107 mg/Kg - dry 0.107 0.7322,4,6-Trichlorophenol 1 08/13/21 15:00 V7647JMV
Surrogate: Phenol-d5 66.2 Limits: 34-121%08/13/21 15:001 JMV V7647
Surrogate: 2-Fluorobiphenyl 77.1 Limits: 44-115%08/13/21 15:001 JMV V7647
Surrogate: 2-Fluorophenol 64.7 Limits: 35-115%08/13/21 15:001 JMV V7647
Surrogate: Nitrobenzene-d5 67.5 Limits: 37-122%08/13/21 15:001 JMV V7647
Surrogate: 4-Terphenyl-d14 80.7 Limits: 54-127%08/13/21 15:001 JMV V7647
Surrogate: 2,4,6-Tribromophenol 65.6 Limits: 39-132%08/13/21 15:001 JMV V7647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:Dup-1
93192 Matrix:
8/6/2021 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.0 %Moisture 1 08/12/21 17:20 SW-DRYWTEDV
2.27 mg/Kg - dry 0.119 1.27Arsenic 10 08/10/21 20:44 6020BEDV
50.0 mg/Kg - dry 1.77 12.7Barium 10 08/10/21 20:44 6020BEDV
<0.0696 mg/Kg - dry 0.0696 0.633Cadmium 10 08/10/21 20:44 6020BEDV
134 mg/Kg - dry 0.367 1.27Chromium 10 08/10/21 20:44 6020BEDV
11.4 mg/Kg - dry 0.177 1.27
Lead 10 08/10/21 20:44 6020BEDV
0.0405 mg/Kg - dry 0.0152 0.0380Mercury (Total)1 08/10/21 16:41 7471BEDV
<1.14 mg/Kg - dry 1.14 2.53Selenium 10 08/10/21 20:44 6020BEDV
<0.0518 mg/Kg - dry 0.0518 0.633Silver 10 08/10/21 20:44 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQLLimit ExceededL
Page 42 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:Dup-1
93192 Matrix:
8/6/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
0.041 mg/Kg - dry 0.003 0.025Acetone 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 08/10/21 21:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 08/10/21 21:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 08/10/21 21:31 V7457TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 08/10/21 21:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 08/10/21 21:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 08/10/21 21:31 V7457TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 08/10/21 21:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 08/10/21 21:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 08/10/21 21:31 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 08/10/21 21:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 08/10/21 21:31 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:Dup-1
93192 Matrix:
8/6/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 08/10/21 21:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 08/10/21 21:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 08/10/21 21:31 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 08/10/21 21:31 V7457TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 08/10/21 21:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 08/10/21 21:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 08/10/21 21:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 08/10/21 21:31 V7457TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 08/10/21 21:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 08/10/21 21:31 V7457TBL
<0.017 mg/Kg - dry 0.017 0.316Ethanol 1 08/10/21 21:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 08/10/21 21:31 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:Dup-1
93192 Matrix:
8/6/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 08/10/21 21:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 08/10/21 21:31 V7457TBL
0.003 J mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 08/10/21 21:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 08/10/21 21:31 V7457TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 08/10/21 21:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 08/10/21 21:31 V7457TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 08/10/21 21:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 08/10/21 21:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 08/10/21 21:31 V7457TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 08/10/21 21:31 V7457TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 08/10/21 21:31 V7457TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 08/10/21 21:31 V7457TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:Dup-1
93192 Matrix:
8/6/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V7456 08/10/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 08/10/21 21:31 V7457TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 08/10/21 21:31 V7457TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 08/10/21 21:31 V7457TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 08/10/21 21:31 V7457
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%08/10/21 21:311 TBL V7457
Surrogate: Dibromofluoromethane 102 Limits: 84-123%08/10/21 21:311 TBL V7457
Surrogate: Toluene-d8 95.5 Limits: 76-129%08/10/21 21:311 TBL V7457
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.148 mg/Kg - dry 0.148 0.841Acenaphthene 1 08/13/21 13:51 V7647JMV
<0.134 mg/Kg - dry 0.134 0.841Acenaphthylene 1 08/13/21 13:51 V7647JMV
<0.193 mg/Kg - dry 0.193 0.841Aniline 1 08/13/21 13:51 V7647JMV
<0.182 mg/Kg - dry 0.182 0.841Anthracene 1 08/13/21 13:51 V7647JMV
<0.177 mg/Kg - dry 0.177 0.841
Benzo(a)anthracene 1 08/13/21 13:51 V7647JMV
<0.187 mg/Kg - dry 0.187 0.841Benzo(a)pyrene 1 08/13/21 13:51 V7647JMV
<0.186 mg/Kg - dry 0.186 0.841Benzo(b)fluoranthene 1 08/13/21 13:51 V7647JMV
<0.173 mg/Kg - dry 0.173 0.841Benzo(g,h,i)perylene 1 08/13/21 13:51 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:Dup-1
93192 Matrix:
8/6/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.174 mg/Kg - dry 0.174 0.841Benzo(k)fluoranthene 1 08/13/21 13:51 V7647JMV
<0.741 mg/Kg - dry 0.741 2.56Benzoic Acid 1 08/13/21 13:51 V7647JMV
<0.134 mg/Kg - dry 0.134 0.841Benzyl alcohol 1 08/13/21 13:51 V7647JMV
<0.150 mg/Kg - dry 0.150 0.841Bis(2-Chloroethoxy)methane 1 08/13/21 13:51 V7647JMV
<0.136 mg/Kg - dry 0.136 0.841Bis(2-Chloroethyl)ether 1 08/13/21 13:51 V7647JMV
<0.173 mg/Kg - dry 0.173 0.421Bis(2-Chloroisopropyl)ether 1 08/13/21 13:51 V7647JMV
<0.153 mg/Kg - dry 0.153 0.841Bis(2-ethylhexyl)phthalate 1 08/13/21 13:51 V7647JMV
<0.139 mg/Kg - dry 0.139 0.8414-Bromophenyl phenyl ether 1 08/13/21 13:51 V7647JMV
<0.144 mg/Kg - dry 0.144 0.421
Butyl benzyl phthalate 1 08/13/21 13:51 V7647JMV
<0.117 mg/Kg - dry 0.117 0.8414-Chloro-3-methylphenol 1 08/13/21 13:51 V7647JMV
<0.143 mg/Kg - dry 0.143 0.4214-Chloroaniline 1 08/13/21 13:51 V7647JMV
<0.148 mg/Kg - dry 0.148 0.8412-Chloronaphthalene 1 08/13/21 13:51 V7647JMV
<0.125 mg/Kg - dry 0.125 0.8412-Chlorophenol 1 08/13/21 13:51 V7647JMV
<0.160 mg/Kg - dry 0.160 1.284-Chlorophenyl phenyl ether 1 08/13/21 13:51 V7647JMV
<0.181 mg/Kg - dry 0.181 0.841Chrysene 1 08/13/21 13:51 V7647JMV
<0.293 mg/Kg - dry 0.293 0.841
Dibenz(a,h)anthracene 1 08/13/21 13:51 V7647JMV
<0.151 mg/Kg - dry 0.151 0.841Dibenzofuran 1 08/13/21 13:51 V7647JMV
<0.120 mg/Kg - dry 0.120 0.8411,2-Dichlorobenzene 1 08/13/21 13:51 V7647JMV
<0.124 mg/Kg - dry 0.124 0.8411,3-Dichlorobenzene 1 08/13/21 13:51 V7647JMV
<0.124 mg/Kg - dry 0.124 0.4211,4-Dichlorobenzene 1 08/13/21 13:51 V7647JMV
<0.187 mg/Kg - dry 0.187 0.8413,3'-Dichlorobenzidine 1 08/13/21 13:51 V7647JMV
<0.122 mg/Kg - dry 0.122 0.8412,4-Dichlorophenol 1 08/13/21 13:51 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:Dup-1
93192 Matrix:
8/6/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.229 mg/Kg - dry 0.229 0.841Diethyl phthalate 1 08/13/21 13:51 V7647JMV
<0.221 mg/Kg - dry 0.221 0.841Dimethyl phthalate 1 08/13/21 13:51 V7647JMV
<0.137 mg/Kg - dry 0.137 0.4212,4-Dimethylphenol 1 08/13/21 13:51 V7647JMV
<0.136 mg/Kg - dry 0.136 0.841Di-n-butyl phthalate 1 08/13/21 13:51 V7647JMV
<0.306 mg/Kg - dry 0.306 1.914,6-Dinitro-2-methylphenol 1 08/13/21 13:51 V7647JMV
<0.662 mg/Kg - dry 0.662 1.912,4-Dinitrophenol 1 08/13/21 13:51 V7647JMV
<0.123 mg/Kg - dry 0.123 0.8412,4-Dinitrotoluene 1 08/13/21 13:51 V7647JMV
<0.137 mg/Kg - dry 0.137 0.8412,6-Dinitrotoluene 1 08/13/21 13:51 V7647JMV
<0.182 mg/Kg - dry 0.182 0.421
Di-n-Octyl Phthalate 1 08/13/21 13:51 V7647JMV
<0.156 mg/Kg - dry 0.156 0.841Fluoranthene 1 08/13/21 13:51 V7647JMV
<0.163 mg/Kg - dry 0.163 0.841Fluorene 1 08/13/21 13:51 V7647JMV
<0.135 mg/Kg - dry 0.135 0.841Hexachlorobenzene 1 08/13/21 13:51 V7647JMV
<0.124 mg/Kg - dry 0.124 0.841Hexachlorobutadiene 1 08/13/21 13:51 V7647JMV
<0.200 mg/Kg - dry 0.200 0.841Hexachlorocyclopentadiene 1 08/13/21 13:51 V7647JMV
<0.101 mg/Kg - dry 0.101 0.841Hexachloroethane 1 08/13/21 13:51 V7647JMV
<0.227 mg/Kg - dry 0.227 0.841
Indeno(1,2,3-cd)pyrene 1 08/13/21 13:51 V7647JMV
<0.243 mg/Kg - dry 0.243 0.841Isophorone 1 08/13/21 13:51 V7647JMV
<0.135 mg/Kg - dry 0.135 0.8411-Methylnaphthalene 1 08/13/21 13:51 V7647JMV
<0.127 mg/Kg - dry 0.127 0.8412-Methylnaphthalene 1 08/13/21 13:51 V7647JMV
<0.123 mg/Kg - dry 0.123 0.8412-Methylphenol 1 08/13/21 13:51 V7647JMV
<0.108 mg/Kg - dry 0.108 0.8413&4 Methylphenol 1 08/13/21 13:51 V7647JMV
<0.183 mg/Kg - dry 0.183 0.841Naphthalene 1 08/13/21 13:51 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:Dup-1
93192 Matrix:
8/6/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.123 mg/Kg - dry 0.123 0.8412-Nitroaniline 1 08/13/21 13:51 V7647JMV
<0.153 mg/Kg - dry 0.153 0.8413-Nitroaniline 1 08/13/21 13:51 V7647JMV
<0.119 mg/Kg - dry 0.119 0.4214-Nitroaniline 1 08/13/21 13:51 V7647JMV
<0.148 mg/Kg - dry 0.148 0.421Nitrobenzene 1 08/13/21 13:51 V7647JMV
<0.113 mg/Kg - dry 0.113 0.8412-Nitrophenol 1 08/13/21 13:51 V7647JMV
<0.149 mg/Kg - dry 0.149 0.8414-Nitrophenol 1 08/13/21 13:51 V7647JMV
<0.335 mg/Kg - dry 0.335 0.841N-Nitrosodimethylamine 1 08/13/21 13:51 V7647JMV
<0.230 mg/Kg - dry 0.230 0.841N-Nitrosodiphenylamine 1 08/13/21 13:51 V7647JMV
<0.150 mg/Kg - dry 0.150 0.841
N-Nitroso-di-n-propylamine 1 08/13/21 13:51 V7647JMV
<0.443 mg/Kg - dry 0.443 1.28Pentachlorophenol 1 08/13/21 13:51 V7647JMV
<0.265 mg/Kg - dry 0.265 0.841Phenanthrene 1 08/13/21 13:51 V7647JMV
<0.143 mg/Kg - dry 0.143 0.841Phenol 1 08/13/21 13:51 V7647JMV
<0.170 mg/Kg - dry 0.170 0.841Pyrene 1 08/13/21 13:51 V7647JMV
<0.101 mg/Kg - dry 0.101 0.421Pyridine 1 08/13/21 13:51 V7647JMV
<0.136 mg/Kg - dry 0.136 0.8411,2,4-Trichlorobenzene 1 08/13/21 13:51 V7647JMV
<0.122 mg/Kg - dry 0.122 0.841
2,4,5-Trichlorophenol 1 08/13/21 13:51 V7647JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 87
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-218-0030
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 08/06/2021
PRO-014
Report Date : 08/17/2021
Sample ID :
Lab No :
Sampled:Dup-1
93192 Matrix:
8/6/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7552 08/12/21 12:00
<0.123 mg/Kg - dry 0.123 0.8412,4,6-Trichlorophenol 1 08/13/21 13:51 V7647JMV
Surrogate: Phenol-d5 57.7 Limits: 34-121%08/13/21 13:511 JMV V7647
Surrogate: 2-Fluorobiphenyl 66.1 Limits: 44-115%08/13/21 13:511 JMV V7647
Surrogate: 2-Fluorophenol 58.9 Limits: 35-115%08/13/21 13:511 JMV V7647
Surrogate: Nitrobenzene-d5 60.1 Limits: 37-122%08/13/21 13:511 JMV V7647
Surrogate: 4-Terphenyl-d14 66.7 Limits: 54-127%08/13/21 13:511 JMV V7647
Surrogate: 2,4,6-Tribromophenol 58.6 Limits: 39-132%08/13/21 13:511 JMV V7647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 87
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172Tel: [phone] Fax: [phone] www.pacelabs.com
Report of Analysis
Waypoint Analytical
PO Box 240543Charlotte, NC 28224Attention: Angela Overcash
Project Name: 21-218-0030
Lot Number:WH09054
Date Completed:08/12/2021
08/12/2021 4:49 PMApproved and released by:
Project Manager II:Lucas Odom
Page 1 of 15
Page 51 of 87
PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Waypoint Analytical
Lot Number: WH09054
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header informationassociated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page ordiscussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on thecover page.
Page 2 of 15
Page 52 of 87
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WH09054

Sample Number Sample ID Matrix Date Sampled Date Received
001 08/06/2021 0905S-1 Solid 08/09/2021
002 08/06/2021 0950S-2 Solid 08/09/2021
003 08/06/2021 1145S-3 Solid 08/09/2021
004 08/06/2021 1045S-4 Solid 08/09/2021
005 08/06/2021Dup-1 Solid 08/09/2021
(5 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 15
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WH09054

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 S-1 Solid Hexavalent Chromium 7199 3.8 mg/kg 5
002 S-2 Solid Hexavalent Chromium 7199 0.75 J mg/kg 6
003 S-3 Solid Hexavalent Chromium 7199 0.81 J mg/kg 7
005 Dup-1 Solid Hexavalent Chromium 7199 0.96 J mg/kg 9
(4 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 15
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S-1
WH09054-001
08/06/2021 0905
08/09/2021
Solid
% Solids:72.3 08/09/2021 2237
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 3060A (Hexavalent C) 7199 1 08/11/2021 1932 AMR 08/10/2021 1218 11546
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 3.8 2mg/kg0.281.4
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 15
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S-2
WH09054-002
08/06/2021 0950
08/09/2021
Solid
% Solids:87.0 08/09/2021 2237
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 08/11/2021 0337 AMR 08/10/2021 1218 11546
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.75 J 1mg/kg0.231.1
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 15
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S-3
WH09054-003
08/06/2021 1145
08/09/2021
Solid
% Solids:82.8 08/09/2021 2237
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 08/11/2021 0350 AMR 08/10/2021 1218 11546
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.81 J 1mg/kg0.241.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 15
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S-4
WH09054-004
08/06/2021 1045
08/09/2021
Solid
% Solids:81.1 08/09/2021 2237
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 08/11/2021 0428 AMR 08/10/2021 1218 11546
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.251.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 15
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
Dup-1
WH09054-005
08/06/2021
08/09/2021
Solid
% Solids:77.5 08/09/2021 2237
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 08/11/2021 0441 AMR 08/10/2021 1218 11546
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.96 J 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 15
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 15
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ11546-001
11546 3060A
08/10/2021 1218Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 08/10/2021 22001.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 15
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ11546-002
11546 3060A
08/10/2021 1218Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 9.6 08/10/2021 2213961080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 15
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 15
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 15
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 15 of 15
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Metals Analyses
6020B
V7484QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V7439
Associated Lab Samples: 93188, 93189, 93190, 93191, 93192
LRB-V7439 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
08/10/21 19:201.000.0940<0.0940mg/KgArsenic
08/10/21 19:2010.01.40<1.40mg/KgBarium
08/10/21 19:200.5000.0550<0.0550mg/KgCadmium
08/10/21 19:201.000.290<0.290mg/KgChromium
08/10/21 19:201.000.140<0.140mg/KgLead
08/10/21 19:202.000.900<0.900mg/KgSelenium
08/10/21 19:200.5000.0410<0.0410mg/KgSilver
LCS-V7439Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
99.012.412.5mg/KgArsenic 80-120
10212.712.5mg/KgBarium 80-120
10012.512.5mg/KgCadmium 80-120
98.012.312.5mg/KgChromium 80-120
10112.612.5mg/KgLead 80-120
10012.512.5mg/KgSelenium 80-120
1025.115.00mg/KgSilver 80-120
V 91972-MS-V7439 V 91972-MSD-V7439Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
12.2 78.011.912.512.52.44mg/KgArsenic 76.0 75-125 2.4 20
103 286*99.512.512.567.2mg/KgBarium 258*75-125 3.4 20
12.7 10212.112.512.5<0.0550mg/KgCadmium 97.0 75-125 4.8 20
34.5 10432.912.512.521.5mg/KgChromium 91.0 75-125 4.7 20
Page 1 of 20* QC Fail Date:08/17/2021 11:31 AM
Page 66 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Metals Analyses
6020B
V7484QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V7439
V 91972-MS-V7439 V 91972-MSD-V7439Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
30.1 11928.512.512.515.2mg/KgLead 106 75-125 5.4 20
11.2 90.011.012.512.51.16mg/KgSelenium 88.0 75-125 1.8 20
5.13 1034.925.005.00<0.0410mg/KgSilver 98.0 75-125 4.1 20
V 91972-PDS-V7439Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
08/10/21 19:5210013.8mg/KgArsenic
08/10/21 19:5210347.6mg/KgBarium
08/10/21 19:5210012.4mg/KgCadmium
08/10/21 19:5299.023.0mg/KgChromium
08/10/21 19:5298.019.7mg/KgLead
08/10/21 19:5210212.7mg/KgSelenium
08/10/21 19:5210212.7mg/KgSilver
Page 2 of 20Date:08/17/2021 11:31 AM
Page 67 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V7481QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V7437
Associated Lab Samples: 93188, 93189, 93190, 93192
LRB-V7437 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
08/10/21 15:400.03000.0120<0.0120mg/KgMercury (Total)
LCS-V7437Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.00.4010.417mg/KgMercury (Total)80-120
V 93065-MS-V7437 V 93065-MSD-V7437Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.460 1000.4440.4170.4170.0452mg/KgMercury (Total)96.0 80-120 3.5 20
V 93065-PDS-V7437Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
08/10/21 16:0293.00.215mg/KgMercury (Total)
Page 3 of 20Date:08/17/2021 11:31 AM
Page 68 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V7550QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V7543
Associated Lab Samples: 93191
LRB-V7543 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
08/12/21 14:570.03000.0120<0.0120mg/KgMercury (Total)
LCS-V7543Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
97.00.4060.417mg/KgMercury (Total)80-120
V 92846-MS-V7543 V 92846-MSD-V7543Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.427 93.00.4360.4170.4170.0380mg/KgMercury (Total)96.0 80-120 2.0 20
V 92846-PDS-V7543Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
08/12/21 15:121000.227mg/KgMercury (Total)
Page 4 of 20Date:08/17/2021 11:31 AM
Page 69 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V7457QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V7456
Associated Lab Samples: 93188, 93189, 93190, 93191, 93192
LRB-V7456 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/10/21 12:050.0200.002<0.002mg/KgAcetone
08/10/21 12:050.0200.001<0.001mg/KgAcrolein
08/10/21 12:050.0200.0008<0.0008mg/KgAcrylonitrile
08/10/21 12:050.0050.0006<0.0006mg/KgBenzene
08/10/21 12:050.0050.0005<0.0005mg/KgBromobenzene
08/10/21 12:050.0050.0008<0.0008mg/KgBromochloromethane
08/10/21 12:050.0050.001<0.001mg/KgBromodichloromethane
08/10/21 12:050.0050.001<0.001mg/KgBromoform
08/10/21 12:050.0100.001<0.001mg/KgBromomethane
08/10/21 12:050.0050.0005<0.0005mg/Kgn-Butylbenzene
08/10/21 12:050.0050.0006<0.0006mg/Kgsec-Butyl benzene
08/10/21 12:050.0050.0005<0.0005mg/Kgtert-Butyl benzene
08/10/21 12:050.0050.0006<0.0006mg/KgCarbon Disulfide
08/10/21 12:050.0050.001<0.001mg/KgCarbon Tetrachloride
08/10/21 12:050.0050.0007<0.0007mg/KgChlorobenzene
08/10/21 12:050.0050.0009<0.0009mg/KgChlorodibromomethane
08/10/21 12:050.0100.0009<0.0009mg/KgChloroethane
08/10/21 12:050.0050.001<0.001mg/KgChloroform
08/10/21 12:050.0100.0006<0.0006mg/KgChloromethane
08/10/21 12:050.0050.0005<0.0005mg/Kg2-Chlorotoluene
08/10/21 12:050.0050.0004<0.0004mg/Kg4-Chlorotoluene
08/10/21 12:050.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
08/10/21 12:050.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
08/10/21 12:050.0050.0006<0.0006mg/Kg1,2-Dibromoethane
08/10/21 12:050.0050.0006<0.0006mg/KgDibromomethane
08/10/21 12:050.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
08/10/21 12:050.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 5 of 20Date:08/17/2021 11:31 AM
Page 70 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V7457QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V7456
Associated Lab Samples: 93188, 93189, 93190, 93191, 93192
LRB-V7456 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/10/21 12:050.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
08/10/21 12:050.0100.001<0.001mg/KgDichlorodifluoromethane
08/10/21 12:050.0050.0008<0.0008mg/Kg1,1-Dichloroethane
08/10/21 12:050.0050.001<0.001mg/Kg1,2-Dichloroethane
08/10/21 12:050.0050.0007<0.0007mg/Kg1,1-Dichloroethene
08/10/21 12:050.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
08/10/21 12:050.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
08/10/21 12:050.0050.0004<0.0004mg/Kg1,2-Dichloropropane
08/10/21 12:050.0050.0006<0.0006mg/Kg1,3-Dichloropropane
08/10/21 12:050.0050.001<0.001mg/Kg2,2-Dichloropropane
08/10/21 12:050.0050.0008<0.0008mg/Kg1,1-Dichloropropene
08/10/21 12:050.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
08/10/21 12:050.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
08/10/21 12:050.2500.014<0.014mg/KgEthanol
08/10/21 12:050.0050.0006<0.0006mg/KgEthylbenzene
08/10/21 12:050.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
08/10/21 12:050.0100.0008<0.0008mg/KgHexachlorobutadiene
08/10/21 12:050.0100.0007<0.0007mg/Kgn-Hexane
08/10/21 12:050.0200.0006<0.0006mg/Kg2-Hexanone
08/10/21 12:050.0050.0005<0.0005mg/KgIsopropylbenzene
08/10/21 12:050.0050.001<0.001mg/Kg4-Isopropyl toluene
08/10/21 12:050.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
08/10/21 12:050.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
08/10/21 12:050.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
08/10/21 12:050.0100.001<0.001mg/KgMethylene Chloride
08/10/21 12:050.0100.0010<0.0010mg/KgNaphthalene
08/10/21 12:050.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 6 of 20Date:08/17/2021 11:31 AM
Page 71 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V7457QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V7456
Associated Lab Samples: 93188, 93189, 93190, 93191, 93192
LRB-V7456 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/10/21 12:050.0050.001<0.001mg/KgStyrene
08/10/21 12:050.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
08/10/21 12:050.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
08/10/21 12:050.0050.0009<0.0009mg/KgTetrachloroethene
08/10/21 12:050.0050.0007<0.0007mg/KgToluene
08/10/21 12:050.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
08/10/21 12:050.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
08/10/21 12:050.0050.001<0.001mg/Kg1,1,1-Trichloroethane
08/10/21 12:050.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
08/10/21 12:050.0050.0009<0.0009mg/KgTrichloroethene
08/10/21 12:050.0100.002<0.002mg/KgTrichlorofluoromethane
08/10/21 12:050.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
08/10/21 12:050.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
08/10/21 12:050.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
08/10/21 12:050.0100.0005<0.0005mg/KgVinyl Acetate
08/10/21 12:050.0100.0005<0.0005mg/KgVinyl Chloride
08/10/21 12:050.0050.0005<0.0005mg/Kgo-Xylene
08/10/21 12:050.0100.001<0.001mg/Kgm,p-Xylene
08/10/21 12:054-Bromofluorobenzene (S)99.0 70-130
08/10/21 12:05Dibromofluoromethane (S)100 84-123
08/10/21 12:05Toluene-d8 (S)97.2 76-129
LCS-V7456 LCSD-V7456Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.082 82.585.40.0850.100mg/KgAcetone 29-198 3.4 20
Page 7 of 20Date:08/17/2021 11:31 AM
Page 72 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V7457QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V7456
LCS-V7456 LCSD-V7456Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.105 1051060.1060.100mg/KgAcrolein 70-130 0.9 20
0.106 1061070.1070.100mg/KgAcrylonitrile 65-134 0.9 20
0.045 90.295.60.0470.050mg/KgBenzene 74-127 5.8 20
0.045 90.092.20.0460.050mg/KgBromobenzene 73-125 2.4 20
0.046 93.296.00.0480.050mg/KgBromochloromethane 72-134 2.9 20
0.046 93.096.40.0480.050mg/KgBromodichloromethane 75-122 3.5 20
0.048 97.698.20.0490.050mg/KgBromoform 66-135 0.6 20
0.041 82.480.40.0400.050mg/KgBromomethane 20-180 2.4 20
0.044 89.495.00.0470.050mg/Kgn-Butylbenzene 65-135 6.0 20
0.044 88.693.20.0460.050mg/Kgsec-Butyl benzene 66-131 5.0 20
0.044 88.092.40.0460.050mg/Kgtert-Butyl benzene 67-132 4.8 20
0.041 83.490.40.0450.050mg/KgCarbon Disulfide 61-129 8.0 20
0.043 86.293.80.0460.050mg/KgCarbon Tetrachloride 64-143 8.4 20
0.045 90.292.00.0460.050mg/KgChlorobenzene 74-118 1.9 20
0.047 95.295.20.0470.050mg/KgChlorodibromomethane 73-122 0.0 20
0.037 75.880.00.0400.050mg/KgChloroethane 33-149 5.3 20
0.044 89.093.60.0460.050mg/KgChloroform 73-127 5.0 20
0.042 85.290.20.0450.050mg/KgChloromethane 45-143 5.7 20
0.045 90.093.00.0460.050mg/Kg2-Chlorotoluene 67-124 3.2 20
0.045 90.093.40.0460.050mg/Kg4-Chlorotoluene 71-126 3.7 20
0.046 93.497.20.0480.050mg/KgDi-Isopropyl Ether (DIPE)59-159 3.9 20
0.048 97.61000.0500.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 2.6 20
0.047 94.695.60.0470.050mg/Kg1,2-Dibromoethane 70-132 1.0 20
0.047 94.296.80.0480.050mg/KgDibromomethane 74-133 2.7 20
0.045 91.092.20.0460.050mg/Kg1,2-Dichlorobenzene 72-123 1.3 20
0.044 89.691.80.0450.050mg/Kg1,3-Dichlorobenzene 71-120 2.4 20
Page 8 of 20Date:08/17/2021 11:31 AM
Page 73 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V7457QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V7456
LCS-V7456 LCSD-V7456Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.692.20.0460.050mg/Kg1,4-Dichlorobenzene 71-123 2.8 20
0.040 80.687.80.0430.050mg/KgDichlorodifluoromethane 26-146 8.5 20
0.044 89.894.20.0470.050mg/Kg1,1-Dichloroethane 74-127 4.7 20
0.046 92.894.80.0470.050mg/Kg1,2-Dichloroethane 68-128 2.1 20
0.042 85.493.00.0460.050mg/Kg1,1-Dichloroethene 67-149 8.5 20
0.044 89.895.60.0470.050mg/Kgcis-1,2-Dichloroethene 76-134 6.2 20
0.044 88.293.00.0460.050mg/Kgtrans-1,2-Dichloroethene 73-132 5.2 20
0.046 92.895.00.0470.050mg/Kg1,2-Dichloropropane 73-130 2.3 20
0.047 94.495.20.0470.050mg/Kg1,3-Dichloropropane 75-124 0.8 20
0.043 87.692.00.0460.050mg/Kg2,2-Dichloropropane 50-142 4.8 20
0.044 88.293.80.0460.050mg/Kg1,1-Dichloropropene 71-130 6.1 20
0.046 93.296.20.0480.050mg/Kgcis-1,3-Dichloropropene 71-125 3.1 20
0.048 96.699.20.0490.050mg/Kgtrans-1,3-Dichloropropene 68-123 2.6 20
1.29 1031051.311.25mg/KgEthanol 70-130 1.5 20
0.045 90.093.00.0460.050mg/KgEthylbenzene 74-128 3.2 20
0.096 96.898.60.0980.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.8 20
0.043 87.092.80.0460.050mg/KgHexachlorobutadiene 64-125 6.4 20
0.043 87.493.80.0460.050mg/Kgn-Hexane 70-130 7.0 20
0.051 1021010.0500.050mg/Kg2-Hexanone 61-157 1.1 20
0.044 89.092.40.0460.050mg/KgIsopropylbenzene 68-126 3.7 20
0.044 89.093.60.0460.050mg/Kg4-Isopropyl toluene 68-129 5.0 20
0.032 65.063.60.0310.050mg/KgMethyl Ethyl Ketone (MEK)63-149 2.1 20
0.048 96.098.40.0490.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.4 20
0.051 1041050.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 1.5 20
0.040 80.283.40.0410.050mg/KgMethylene Chloride 74-129 3.9 20
0.048 97.495.40.0470.050mg/KgNaphthalene 57-157 2.0 20
Page 9 of 20Date:08/17/2021 11:31 AM
Page 74 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V7457QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V7456
LCS-V7456 LCSD-V7456Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 90.494.40.0470.050mg/Kgn-Propylbenzene 67-130 4.3 20
0.046 92.495.80.0470.050mg/KgStyrene 77-121 3.6 20
0.046 93.694.60.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.0 20
0.049 98.897.60.0480.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.2 20
0.043 86.895.40.0470.050mg/KgTetrachloroethene 68-130 9.4 20
0.045 90.094.80.0470.050mg/KgToluene 71-129 5.1 20
0.046 93.093.00.0460.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.0 20
0.046 92.892.60.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.2 20
0.044 88.093.20.0460.050mg/Kg1,1,1-Trichloroethane 67-131 5.7 20
0.047 94.896.60.0480.050mg/Kg1,1,2-Trichloroethane 70-133 1.8 20
0.044 88.893.80.0460.050mg/KgTrichloroethene 75-133 5.4 20
0.041 83.090.20.0450.050mg/KgTrichlorofluoromethane 44-146 8.3 20
0.048 96.696.00.0480.050mg/Kg1,2,3-Trichloropropane 60-137 0.6 20
0.045 90.493.40.0460.050mg/Kg1,2,4-Trimethylbenzene 69-129 3.2 20
0.044 89.092.40.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.7 20
0.055 1121150.0570.050mg/KgVinyl Acetate 85-161 2.4 20
0.042 84.692.00.0460.050mg/KgVinyl Chloride 48-147 8.3 20
0.045 90.092.80.0460.050mg/Kgo-Xylene 74-126 3.0 20
0.092 92.695.90.0950.100mg/Kgm,p-Xylene 75-124 3.5 20
99.299.24-Bromofluorobenzene (S)70-130
99.899.2Dibromofluoromethane (S)84-123
98.497.4Toluene-d8 (S)76-129
Page 10 of 20Date:08/17/2021 11:31 AM
Page 75 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7552
Associated Lab Samples: 93188, 93189, 93190, 93191, 93192
LRB-V7552 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/12/21 18:390.6600.116<0.116mg/KgAcenaphthene
08/12/21 18:390.6600.105<0.105mg/KgAcenaphthylene
08/12/21 18:390.6600.152<0.152mg/KgAniline
08/12/21 18:390.6600.143<0.143mg/KgAnthracene
08/12/21 18:390.6600.139<0.139mg/KgBenzo(a)anthracene
08/12/21 18:390.6600.147<0.147mg/KgBenzo(a)pyrene
08/12/21 18:390.6600.146<0.146mg/KgBenzo(b)fluoranthene
08/12/21 18:390.6600.136<0.136mg/KgBenzo(g,h,i)perylene
08/12/21 18:390.6600.137<0.137mg/KgBenzo(k)fluoranthene
08/12/21 18:392.000.580<0.580mg/KgBenzoic Acid
08/12/21 18:390.6600.105<0.105mg/KgBenzyl alcohol
08/12/21 18:390.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
08/12/21 18:390.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
08/12/21 18:390.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
08/12/21 18:390.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
08/12/21 18:390.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
08/12/21 18:390.3300.113<0.113mg/KgButyl benzyl phthalate
08/12/21 18:390.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
08/12/21 18:390.3300.112<0.112mg/Kg4-Chloroaniline
08/12/21 18:390.6600.116<0.116mg/Kg2-Chloronaphthalene
08/12/21 18:390.6600.098<0.098mg/Kg2-Chlorophenol
08/12/21 18:391.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
08/12/21 18:390.6600.142<0.142mg/KgChrysene
08/12/21 18:390.6600.230<0.230mg/KgDibenz(a,h)anthracene
08/12/21 18:390.6600.119<0.119mg/KgDibenzofuran
08/12/21 18:390.6600.094<0.094mg/Kg1,2-Dichlorobenzene
08/12/21 18:390.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 11 of 20Date:08/17/2021 11:31 AM
Page 76 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7552
Associated Lab Samples: 93188, 93189, 93190, 93191, 93192
LRB-V7552 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/12/21 18:390.3300.097<0.097mg/Kg1,4-Dichlorobenzene
08/12/21 18:390.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
08/12/21 18:390.6600.095<0.095mg/Kg2,4-Dichlorophenol
08/12/21 18:390.6600.180<0.180mg/KgDiethyl phthalate
08/12/21 18:390.6600.174<0.174mg/KgDimethyl phthalate
08/12/21 18:390.3300.108<0.108mg/Kg2,4-Dimethylphenol
08/12/21 18:390.6600.107<0.107mg/KgDi-n-butyl phthalate
08/12/21 18:391.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
08/12/21 18:391.500.520<0.520mg/Kg2,4-Dinitrophenol
08/12/21 18:390.6600.096<0.096mg/Kg2,4-Dinitrotoluene
08/12/21 18:390.6600.108<0.108mg/Kg2,6-Dinitrotoluene
08/12/21 18:390.3300.143<0.143mg/KgDi-n-Octyl Phthalate
08/12/21 18:390.6600.123<0.123mg/KgFluoranthene
08/12/21 18:390.6600.128<0.128mg/KgFluorene
08/12/21 18:390.6600.106<0.106mg/KgHexachlorobenzene
08/12/21 18:390.6600.097<0.097mg/KgHexachlorobutadiene
08/12/21 18:390.6600.157<0.157mg/KgHexachlorocyclopentadiene
08/12/21 18:390.6600.079<0.079mg/KgHexachloroethane
08/12/21 18:390.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
08/12/21 18:390.6600.191<0.191mg/KgIsophorone
08/12/21 18:390.6600.106<0.106mg/Kg1-Methylnaphthalene
08/12/21 18:390.6600.100<0.100mg/Kg2-Methylnaphthalene
08/12/21 18:390.6600.097<0.097mg/Kg2-Methylphenol
08/12/21 18:390.6600.084<0.084mg/Kg3&4 Methylphenol
08/12/21 18:390.6600.144<0.144mg/KgNaphthalene
08/12/21 18:390.6600.096<0.096mg/Kg2-Nitroaniline
08/12/21 18:390.6600.120<0.120mg/Kg3-Nitroaniline
Page 12 of 20Date:08/17/2021 11:31 AM
Page 77 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7552
Associated Lab Samples: 93188, 93189, 93190, 93191, 93192
LRB-V7552 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/12/21 18:390.3300.093<0.093mg/Kg4-Nitroaniline
08/12/21 18:390.3300.116<0.116mg/KgNitrobenzene
08/12/21 18:390.6600.088<0.088mg/Kg2-Nitrophenol
08/12/21 18:390.6600.117<0.117mg/Kg4-Nitrophenol
08/12/21 18:390.6600.263<0.263mg/KgN-Nitrosodimethylamine
08/12/21 18:390.6600.181<0.181mg/KgN-Nitrosodiphenylamine
08/12/21 18:390.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
08/12/21 18:391.000.347<0.347mg/KgPentachlorophenol
08/12/21 18:390.6600.208<0.208mg/KgPhenanthrene
08/12/21 18:390.6600.112<0.112mg/KgPhenol
08/12/21 18:390.6600.134<0.134mg/KgPyrene
08/12/21 18:390.3300.079<0.079mg/KgPyridine
08/12/21 18:390.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
08/12/21 18:390.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
08/12/21 18:390.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
08/12/21 18:392-Fluorobiphenyl (S)86.2 44-115
08/12/21 18:392-Fluorophenol (S)87.9 35-115
08/12/21 18:39Nitrobenzene-d5 (S)81.4 37-122
08/12/21 18:394-Terphenyl-d14 (S)94.0 54-127
08/12/21 18:392,4,6-Tribromophenol (S)88.5 39-132
08/12/21 18:39Phenol-d5 (S)87.3 34-121
LCS-V7552Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
87.41.461.67mg/KgAcenaphthene 40-123
92.81.551.67mg/KgAcenaphthylene 32-132
Page 13 of 20Date:08/17/2021 11:31 AM
Page 78 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7552
LCS-V7552Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.21.391.67mg/KgAniline 12-197
92.81.551.67mg/KgAnthracene 47-123
90.41.511.67mg/KgBenzo(a)anthracene 49-126
1011.691.67mg/KgBenzo(a)pyrene 45-129
95.21.591.67mg/KgBenzo(b)fluoranthene 45-132
88.61.481.67mg/KgBenzo(g,h,i)perylene 43-134
85.01.421.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.311.67mg/KgBenzoic Acid 10-83
85.61.431.67mg/KgBenzyl alcohol 29-122
95.81.601.67mg/KgBis(2-Chloroethoxy)methane 36-121
80.21.341.67mg/KgBis(2-Chloroethyl)ether 31-120
83.81.401.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1031.721.67mg/KgBis(2-ethylhexyl)phthalate 51-133
87.41.461.67mg/Kg4-Bromophenyl phenyl ether 46-124
97.61.631.67mg/KgButyl benzyl phthalate 48-132
99.41.661.67mg/Kg4-Chloro-3-methylphenol 45-122
83.81.401.67mg/Kg4-Chloroaniline 17-106
85.61.431.67mg/Kg2-Chloronaphthalene 41-114
86.81.451.67mg/Kg2-Chlorophenol 34-121
90.41.511.67mg/Kg4-Chlorophenyl phenyl ether 45-121
92.81.551.67mg/KgChrysene 50-124
82.61.381.67mg/KgDibenz(a,h)anthracene 45-134
88.01.471.67mg/KgDibenzofuran 44-120
78.41.311.67mg/Kg1,2-Dichlorobenzene 33-117
76.61.281.67mg/Kg1,3-Dichlorobenzene 30-115
76.61.281.67mg/Kg1,4-Dichlorobenzene 31-115
85.01.421.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 14 of 20* QC Fail Date:08/17/2021 11:31 AM
Page 79 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7552
LCS-V7552Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
95.81.601.67mg/Kg2,4-Dichlorophenol 40-122
94.01.571.67mg/KgDiethyl phthalate 50-124
89.21.491.67mg/KgDimethyl phthalate 48-124
96.41.611.67mg/Kg2,4-Dimethylphenol 30-127
1041.731.67mg/KgDi-n-butyl phthalate 51-128
0.0*1.391.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
0.0*1.361.67mg/Kg2,4-Dinitrophenol 27-129
95.81.601.67mg/Kg2,4-Dinitrotoluene 48-126
95.21.591.67mg/Kg2,6-Dinitrotoluene 46-124
97.61.631.67mg/KgDi-n-Octyl Phthalate 45-140
92.81.551.67mg/KgFluoranthene 50-127
92.81.551.67mg/KgFluorene 43-125
89.21.491.67mg/KgHexachlorobenzene 45-122
81.41.361.67mg/KgHexachlorobutadiene 32-123
62.21.041.67mg/KgHexachlorocyclopentadiene 32-117
76.01.271.67mg/KgHexachloroethane 28-117
87.41.461.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
75.41.261.67mg/KgIsophorone 30-122
86.21.441.67mg/Kg1-Methylnaphthalene 40-119
86.21.441.67mg/Kg2-Methylnaphthalene 38-122
92.21.541.67mg/Kg2-Methylphenol 32-122
80.81.351.67mg/Kg3&4 Methylphenol 34-119
83.81.401.67mg/KgNaphthalene 35-123
93.41.561.67mg/Kg2-Nitroaniline 44-127
91.01.521.67mg/Kg3-Nitroaniline 33-119
96.41.611.67mg/Kg4-Nitroaniline 63-147
82.01.371.67mg/KgNitrobenzene 34-122
Page 15 of 20* QC Fail Date:08/17/2021 11:31 AM
Page 80 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7552
LCS-V7552Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.81.401.67mg/Kg2-Nitrophenol 36-123
1081.801.67mg/Kg4-Nitrophenol 30-132
68.81.151.67mg/KgN-Nitrosodimethylamine 10-146
1081.811.67mg/KgN-Nitrosodiphenylamine 38-127
81.41.361.67mg/KgN-Nitroso-di-n-propylamine 36-120
93.41.561.67mg/KgPentachlorophenol 25-133
93.41.561.67mg/KgPhenanthrene 50-121
86.21.441.67mg/KgPhenol 34-121
97.01.621.67mg/KgPyrene 47-127
55.90.9341.67mg/KgPyridine 10-80
80.81.351.67mg/Kg1,2,4-Trichlorobenzene 34-118
88.01.471.67mg/Kg2,4,5-Trichlorophenol 41-124
90.41.511.67mg/Kg2,4,6-Trichlorophenol 39-126
85.02-Fluorobiphenyl (S)44-115
88.82-Fluorophenol (S)35-115
80.8Nitrobenzene-d5 (S)37-122
93.44-Terphenyl-d14 (S)54-127
94.82,4,6-Tribromophenol (S)39-132
85.5Phenol-d5 (S)34-121
V 93140-MS-V7552 V 93140-MSD-V7552Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.38 83.11.291.661.66<0.116mg/KgAcenaphthene 77.7 40-123 6.7 20
1.45 87.31.371.661.66<0.105mg/KgAcenaphthylene 82.5 32-132 5.6 20
1.23 74.01.241.661.66<0.152mg/KgAniline 74.6 12-197 0.8 20
Page 16 of 20Date:08/17/2021 11:31 AM
Page 81 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7552
V 93140-MS-V7552 V 93140-MSD-V7552Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.40 84.31.321.661.66<0.143mg/KgAnthracene 79.5 47-123 5.8 20
1.41 84.91.301.661.66<0.139mg/KgBenzo(a)anthracene 78.3 49-126 8.1 20
1.57 94.51.431.661.66<0.147mg/KgBenzo(a)pyrene 86.1 45-129 9.3 20
1.45 87.31.391.661.66<0.146mg/KgBenzo(b)fluoranthene 83.7 45-132 4.2 20
1.35 81.31.251.661.66<0.136mg/KgBenzo(g,h,i)perylene 75.3 43-134 7.6 20
1.31 78.91.201.661.66<0.137mg/KgBenzo(k)fluoranthene 72.2 47-132 8.7 20
0.832 0.0*1.001.661.66<0.580mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.37 82.51.321.661.66<0.105mg/KgBenzyl alcohol 79.5 29-122 3.7 20
1.43 86.11.381.661.66<0.118mg/KgBis(2-Chloroethoxy)methane 83.1 36-121 3.5 20
1.16 69.81.121.661.66<0.107mg/KgBis(2-Chloroethyl)ether 67.4 31-120 3.5 20
1.26 75.91.231.661.66<0.136mg/KgBis(2-Chloroisopropyl)ether 74.0 33-131 2.4 20
1.62 97.51.471.661.66<0.120mg/KgBis(2-ethylhexyl)phthalate 88.5 51-133 9.7 20
1.34 80.71.241.661.66<0.109mg/Kg4-Bromophenyl phenyl ether 74.6 46-124 7.7 20
1.52 91.51.391.661.66<0.113mg/KgButyl benzyl phthalate 83.7 48-132 8.9 20
1.44 86.71.341.661.66<0.092mg/Kg4-Chloro-3-methylphenol 80.7 45-122 7.1 20
1.14 68.61.141.661.66<0.112mg/Kg4-Chloroaniline 68.6 17-106 0.0 20
1.37 82.51.291.661.66<0.116mg/Kg2-Chloronaphthalene 77.7 41-114 6.0 20
1.36 81.91.321.661.66<0.098mg/Kg2-Chlorophenol 79.5 34-121 2.9 20
1.42 85.51.301.661.66<0.126mg/Kg4-Chlorophenyl phenyl ether 78.3 45-121 8.8 20
1.42 85.51.321.661.66<0.142mg/KgChrysene 79.5 50-124 7.2 20
1.24 74.61.151.661.66<0.230mg/KgDibenz(a,h)anthracene 69.2 45-134 7.5 20
1.40 84.31.311.661.66<0.119mg/KgDibenzofuran 78.9 44-120 6.6 20
1.20 72.21.161.661.66<0.094mg/Kg1,2-Dichlorobenzene 69.8 33-117 3.3 20
1.17 70.41.141.661.66<0.097mg/Kg1,3-Dichlorobenzene 68.6 30-115 2.5 20
1.15 69.21.111.661.66<0.097mg/Kg1,4-Dichlorobenzene 66.8 31-115 3.5 20
1.25 75.31.181.661.66<0.147mg/Kg3,3'-Dichlorobenzidine 71.0 22-121 5.7 20
Page 17 of 20* QC Fail Date:08/17/2021 11:31 AM
Page 82 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7552
V 93140-MS-V7552 V 93140-MSD-V7552Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.41 84.91.321.661.66<0.095mg/Kg2,4-Dichlorophenol 79.5 40-122 6.5 20
1.45 87.31.321.661.66<0.180mg/KgDiethyl phthalate 79.5 50-124 9.3 20
1.39 83.71.291.661.66<0.174mg/KgDimethyl phthalate 77.7 48-124 7.4 30
1.49 89.71.381.661.66<0.108mg/Kg2,4-Dimethylphenol 83.1 30-127 7.6 20
1.54 92.71.461.661.66<0.107mg/KgDi-n-butyl phthalate 87.9 51-128 5.3 20
<0.240 0.0*<0.2401.661.66<0.240mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
<0.520 0.0*<0.5201.661.66<0.520mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.45 87.31.331.661.66<0.096mg/Kg2,4-Dinitrotoluene 80.1 48-126 8.6 20
1.46 87.91.351.661.66<0.108mg/Kg2,6-Dinitrotoluene 81.3 46-124 7.8 20
1.83 1101.711.661.66<0.143mg/KgDi-n-Octyl Phthalate 103 45-140 6.7 20
1.45 87.31.351.661.66<0.123mg/KgFluoranthene 81.3 50-127 7.1 20
1.44 86.71.341.661.66<0.128mg/KgFluorene 80.7 43-125 7.1 20
1.35 81.31.271.661.66<0.106mg/KgHexachlorobenzene 76.5 45-122 6.1 20
1.22 73.41.191.661.66<0.097mg/KgHexachlorobutadiene 71.6 32-123 2.4 20
0.588 0.0*0.5291.661.66<0.157mg/KgHexachlorocyclopentadiene 0.0*32-117 0.0 20
1.16 69.81.141.661.66<0.079mg/KgHexachloroethane 68.6 28-117 1.7 20
1.36 81.91.261.661.66<0.179mg/KgIndeno(1,2,3-cd)pyrene 75.9 45-133 7.6 20
1.11 66.81.051.661.66<0.191mg/KgIsophorone 63.2 30-122 5.5 20
1.27 76.51.231.661.66<0.106mg/Kg1-Methylnaphthalene 74.0 40-119 3.2 20
1.30 78.31.241.661.66<0.100mg/Kg2-Methylnaphthalene 74.6 38-122 4.7 20
1.40 84.31.361.661.66<0.097mg/Kg2-Methylphenol 81.9 32-122 2.8 20
1.23 74.01.191.661.66<0.084mg/Kg3&4 Methylphenol 71.6 34-119 3.3 20
1.26 75.91.211.661.66<0.144mg/KgNaphthalene 72.8 35-123 4.0 20
1.47 88.51.361.661.66<0.096mg/Kg2-Nitroaniline 81.9 44-127 7.7 20
1.40 84.31.291.661.66<0.120mg/Kg3-Nitroaniline 77.7 33-119 8.1 20
1.40 84.31.251.661.66<0.093mg/Kg4-Nitroaniline 75.3 63-147 11.3 20
Page 18 of 20* QC Fail Date:08/17/2021 11:31 AM
Page 83 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7552
V 93140-MS-V7552 V 93140-MSD-V7552Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.20 72.21.181.661.66<0.116mg/KgNitrobenzene 71.0 34-122 1.6 20
1.23 74.01.171.661.66<0.088mg/Kg2-Nitrophenol 70.4 32-123 5.0 20
1.51 90.91.411.661.66<0.117mg/Kg4-Nitrophenol 84.9 30-132 6.8 20
1.00 60.20.9771.661.66<0.263mg/KgN-Nitrosodimethylamine 58.8 10-146 2.3 30
1.67 1011.551.661.66<0.181mg/KgN-Nitrosodiphenylamine 93.3 38-127 7.4 20
1.28 77.11.211.661.66<0.118mg/KgN-Nitroso-di-n-propylamine 72.8 36-120 5.6 20
1.15 69.21.081.661.66<0.347mg/KgPentachlorophenol 65.0 25-133 6.2 20
1.42 85.51.331.661.66<0.208mg/KgPhenanthrene 80.1 50-121 6.5 20
1.36 81.91.321.661.66<0.112mg/KgPhenol 79.5 34-121 2.9 20
1.51 90.91.411.661.66<0.134mg/KgPyrene 84.9 47-127 6.8 20
0.794 47.80.7881.661.66<0.079mg/KgPyridine 47.4 10-80 0.7 20
1.18 71.01.151.661.66<0.107mg/Kg1,2,4-Trichlorobenzene 69.2 34-118 2.5 20
1.36 81.91.261.661.66<0.096mg/Kg2,4,5-Trichlorophenol 75.9 41-124 7.6 20
1.41 84.91.311.661.66<0.096mg/Kg2,4,6-Trichlorophenol 78.9 39-126 7.3 20
80.12-Fluorobiphenyl (S)75.3 44-115
82.52-Fluorophenol (S)78.9 35-115
72.2Nitrobenzene-d5 (S)69.2 37-122
85.54-Terphenyl-d14 (S)78.9 54-127
85.52,4,6-Tribromophenol (S)78.0 39-132
79.2Phenol-d5 (S)75.6 34-121
Page 19 of 20Date:08/17/2021 11:31 AM
Page 84 of 87
Quality Control Data
21-218-0030Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PRO-014
Dry Weight Determination
SW-DRYWT
V7556QC Analytical Batch:
Analysis Method:
Analysis Description:
V 92912-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 08/12/21 17:202.721.722.3%Moisture
V 93180-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 08/12/21 17:202.217.618.0%Moisture
Page 20 of 20Date:08/17/2021 11:31 AM
Page 85 of 87
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-218-0030
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 6.0
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Terri W Cole Date & Time:08/06/2021 16:17:38
Special precautions or instructions included?
Comments:
Page 86 of 87
Page 87 of 87

Appendix C

NC DEQ Risk Calculator

Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
Former Fleet Maco Solutions Site
2217 South Tryon
Brownfields
25006-21-060
June 2021
May 2021 EPA RSL Table
Prepared By:Vanessa Hunter
Hart and Hickman
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 25006-21-060
Exposure Unit ID: Worst Case
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 25006-21-060
Exposure Unit ID: Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Factors and Target Risks
Version Date: June 2021
Basis: May 2021 EPA RSL TableSite ID: 25006-21-060
Exposure Parameter Site Specific Value Justification
Target Cancer Risk (individual)1.0E-06
Target Cancer Risk (cumulative)1.0E-04
Target Hazard Index (individual)2.0E-01
Target Hazard Index (cumulative)1.0E+00
Lifetime (LT) (years)70
Body Weight (BW) (kg)15
Exposure Duration (ED) (yr)6
Exposure Frequency (EF) (d/yr)350
Exposure Time (ET) (hr)24
Skin Surface Area - Soil Exposure (SAs) (cm2)2373
Soil Adherence Factor (AF) (mg/cm2)0.2
Soil Ingestion Rate (IRS) (mg/day)200
Skin Surface Area - Water Exposure (SAw) (cm2)6365
Water Ingestion Rate (IRW) (L/d)0.78
Water Exposure Time (ETevent) (hr/event)0.54
Water Event Frequency (EV) (events/day)1
Lifetime (LT) (years)70
Body Weight (BW) (kg)80
Exposure Duration (ED) (yr)20
Exposure Frequency (EF) (d/yr)350
Exposure Time (ET) (hr)24
Skin Surface Area - Soil Exposure (SAs) (cm2)6032
Soil Adherence Factor (AF) (mg/cm2)0.07
Soil Ingestion Rate (IRS) (mg/day)100
Skin Surface Area - Water Exposure (SAw) (cm2)19652
Water Ingestion Rate (IRW) (L/d)2.5
Water Exposure Time (ETevent) (hr/event)0.71
Water Event Frequency (EV) (events/day)1
Lifetime (LT) (years)70
Body Weight (BW) (kg)80
Exposure Duration (ED) (yr)25
Exposure Frequency (EF) (d/yr)250
Exposure Time (ET) (hr)8
Skin Surface Area - Soil Exposure (SAs) (cm2)3527
Soil Adherence Factor (AF) (mg/cm2)0.12
Soil Ingestion Rate (IR) (mg/day)100
Skin Surface Area - Water Exposure (SAw) (cm2)19652
Water Ingestion Rate (IRW) (L/d)0.83
Water Exposure Time (ETevent) (hr/event)0.67
Water Event Frequency (EV) (events/day)1
Lifetime (LT) (years)70
Body Weight (BW) (kg)80
Working Weeks (EW) (wk/yr)50
Exposure Duration (ED) (yr)1
Exposure Frequency (EF) (d/yr)250
Exposure Time (ET) (hr)8
Skin Surface Area - Soil Exposure (SAs) (cm2)3527
Soil Adherence Factor (AF) (mg/cm2)0.3
Soil Ingestion Rate (IR) (mg/day)330
Non-Residential Worker
Construction Worker
70
80
25
250
8
3527
0.12
100
19652
0.83
0.67
Input Form 1B
Exposure Unit ID: Worst Case
Residential Child
General
Residential Adult
Default Value
1.0E-06
1.0E-04
2.0E-01
1.0E+00
70
15
6
350
24
2373
0.2
200
6365
0.78
0.54
1
70
80
20
350
24
6032
0.07
100
19652
2.5
0.71
1
1
70
80
330
1
250
8
3527
0.3
50
North Carolina DEQ Risk Calculator
Exposure Factors and Target Risks
Version Date: June 2021
Basis: May 2021 EPA RSL TableSite ID: 25006-21-060
Exposure Parameter Site Specific Value Justification
Input Form 1B
Exposure Unit ID: Worst Case
Default Value
Recreator Trespasser
Lifetime (LT) (years)70 NA 70
Averaging Time (AT) (days/yr)365 NA 365
Body Weight (BW) (kg)15 NA 15
Exposure Duration 0-2 (ED) (yr)2 NA 2
Exposure Duration 2-6 (ED) (yr)4 NA 4
Exposure Frequency (EF) (d/yr)195 NA 195
Exposure Time (ET) (hr)2 NA 2
Skin Surface Area - Soil Exposure (SAs) (cm2)2373 NA 2373
Soil Adherence Factor (AF) (mg/cm2)0.2 NA 0.2
Soil Ingestion Rate (IRS) (mg/day)200 NA 200
Skin Surface Area - Water Exposure (SAw) (cm2)6365 NA 6365
Water Ingestion Rate (IRW) (L/hr)0.124 NA 0.124
Water Exposure Time (ETevent) (hr/event)2 NA 2
Water Event Frequency (EV) (events/day)1 NA 1
Recreator Trespasser
Lifetime (LT) (years)70 70 70
Body Weight (BW) (kg)80 45 80
Exposure Duration 6-16 (ED) (yr)10 10 10
Exposure Duration 16-26 (ED) (yr)10 0 10
Exposure Frequency (EF) (d/yr)195 90 195
Exposure Time (ET) (hr)2 2 2
Skin Surface Area - Soil Exposure (SAs) (cm2)6032 6032 6032
Soil Adherence Factor (AF) (mg/cm2)0.07 0.2 0.07
Soil Ingestion Rate (IRS) (mg/day)100 200 100
Skin Surface Area - Water Exposure (SAw) (cm2)19652 19652 19652
Water Ingestion Rate (IRW) (L/hr)0.0985 0.071 0.0985
Water Exposure Time (ETevent) (hr/event)2 2 2
Water Event Frequency (EV) (events/day)1 1 1
User Defined Child
User Defined Adult
North Carolina DEQ Risk Calculator
Contaminant Migration Parameters Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 25006-21-060
Exposure Unit ID: Worst Case
Parameter Default Value Site Specific
Value Justification
Distance to Protection of
Groundwater Point of
Exposure (POEgw) (feet)
0 0
Distance to Protection of
Surface Water Point of
Exposure (POEsw) (feet)
0 0
Depth to Base of Affected
Soils (ds) (cm)1244 1,244
Length of Affected Soil
Parallel to Assumed GW Flow Direction (L) (cm)
Site-specific
value required
Areal extent of soil contamination
range 0.5-500 (As) (acres)0.5 0.5
Fraction of vegetative cover
(V) (unitless)0.5 0.5
0.15 (soil to
outdoor air pathway)0.15
0.3 (soil to
groundwater
pathway)
0.3
Provide justification for the contaminant migration parameters used.
Water Filled Soil Porosity
(θw) (unitless)
Input Form 1C
North Carolina DEQ Risk Calculator
Contaminant Migration Parameters Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 25006-21-060
Exposure Unit ID: Worst Case
Parameter Default Value Site Specific
Value Justification
Provide justification for the contaminant migration parameters used.
Input Form 1C
0.28 (soil to
outdoor air
pathway)
0.28
0.13 (soil to
groundwater
pathway)
0.13
Total Soil Porosity (n) (unitless)0.43 0.43
Dry Soil Bulk Density (ρb)
(g/cm3)1.5 1.5
Net Infiltration Rate (I)
(cm/yr)66 66
0.006 (soil to outdoor air
pathway)
0.006
0.002 (soil
leaching to
groundwater
pathway)
0.002
Aquifer Hydraulic
Conductivity (K) (cm/d)
Site-specific
value required
Hydraulic Gradient (i)
(unitless)
Site-specific
value required
Average Groundwater
Temperature (Tgw) (°C)25 25
Fraction Organic Carbon
(foc) (unitless)
Air Filled Soil Porosity (θa)
(unitless)
North Carolina DEQ Risk Calculator
Contaminant Migration Parameters Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 25006-21-060
Exposure Unit ID: Worst Case
Parameter Default Value Site Specific
Value Justification
Provide justification for the contaminant migration parameters used.
Input Form 1C
Aquifer Thickness (da) (cm)Site-specific value required
Groundwater Source
Thickness (Sd) (cm)Site-specific value required
Groundwater Source Width
(Sw) (cm)Site-specific value required
Plume Thickness at GW/SW
Discharge (δsw) (cm)
Site-specific value required
Plume Width at GW/SW
Discharge (Wgwsw) (cm)Site-specific
value required
Surface Water Flowrate at
GW/SW Discharge (Qsw)
(cm3/d)
Site-specific
value required
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: June 2021Basis: May 2021 EPA RSL TableSite ID: 25006-21-060
Exposure Unit ID: Worst Case
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point Concentration (mg/kg)Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the PSRG Table link on the Main Menu
Minimum Concentration (Qualifier)
Maximum Concentration (Qualifier)
Units Location of Maximum Concentration
Detection Frequency Range of Detection Limits
Concentration Used for Screening
Background Value
Screening Toxicity Value (Screening Level) (n/c)
Potential ARAR/TBC Value
Potential ARAR/TBC Source
COPC Flag (Y/N)
Rationale for Selection or Deletion
0.104 67-64-1 Acetone mg/kg0.001 107-02-8 Acrolein mg/kg7.36 7440-38-2 Arsenic, Inorganic mg/kg1017440-39-3 Barium mg/kg0.0009 71-43-2 Benzene mg/kg0.399 7440-43-9 Cadmium (Diet)mg/kg172.2 16065-83-1 Chromium(III), Insoluble Salts mg/kg3.8 18540-29-9 Chromium(VI)mg/kg83.1 7439-92-1 ~Lead and Compounds mg/kg0.106 7439-97-6 ~Mercury (elemental)mg/kg0.006 78-93-3 Methyl Ethyl Ketone (2-Butanone)mg/kg0.287 50-32-8 ~Benzo[a]pyrene mg/kg0.456 205-99-2 ~Benzo[b]fluoranthene mg/kg0.178 218-01-9 ~Chrysene mg/kg0.193 206-44-0 ~Fluoranthene mg/kg0.226 193-39-5 ~Indeno[1,2,3-cd]pyrene mg/kg0.22 129-00-0 ~Pyrene mg/kg1.97 7782-49-2 Selenium mg/kg0.105 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 25006-21-060
Exposure Unit ID: Worst Case
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 2.6E-05 2.8E-01 NO
Groundwater Use*NC NC NC
Soil 3.2E-06 2.3E-02 NO
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 25006-21-060
Exposure Unit ID: Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:Ingestion Concentration (mg/kg)
Dermal Concentration (mg/kg)
Inhalation Concentration (mg/kg)*
Ingestion Carcinogenic Risk
Dermal Carcinogenic Risk
Inhalation Carcinogenic Risk*
Calculated Carcinogenic Risk
Ingestion Hazard Quotient
Dermal Hazard Quotient
Inhalation Hazard Quotient*
Calculated Non-Carcinogenic Hazard Quotient67-64-1 Acetone 0.104 0.104 0.104 1.5E-06 2.2E-07 1.7E-06
107-02-8 Acrolein 0.001 0.001 0.001 2.6E-05 6.5E-03 6.5E-037440-38-2 Arsenic, Inorganic 7.36 7.36 7.36 9.5E-06 1.3E-06 1.9E-10 1.1E-05 1.9E-01 2.2E-02 7.9E-06 2.1E-017440-39-3 Barium 101 101 101 6.5E-03 3.3E-06 6.5E-0371-43-2 Benzene 0.0009 0.0009 0.0009 7.1E-11 6.6E-10 7.4E-10 2.9E-06 7.6E-06 1.1E-057440-43-9 Cadmium (Diet)0.399 0.399 0.399 4.3E-12 4.3E-12 5.1E-03 4.8E-04 6.4E-07 5.6E-03
16065-83-1 Chromium(III), Insoluble Salts 172.2 172.2 172.2 1.5E-03 1.5E-0318540-29-9 Chromium(VI)3.8 3.8 3.8 1.2E-05 5.3E-09 1.2E-05 1.6E-02 6.1E-07 1.6E-027439-92-1 ~Lead and Compounds 83.1 83.1 83.1 <SL**<SL**<SL**7439-97-6 ~Mercury (elemental)0.106 0.106 0.106 9.2E-03 9.2E-0378-93-3 Methyl Ethyl Ketone (2-Butanone)0.006 0.006 0.006 1.3E-07 8.9E-08 2.2E-07
50-32-8 ~Benzo[a]pyrene 0.287 0.287 0.287 1.9E-06 6.3E-07 2.9E-12 2.5E-06 1.2E-02 3.8E-03 2.3E-06 1.6E-02205-99-2 ~Benzo[b]fluoranthene 0.456 0.456 0.456 3.0E-07 9.9E-08 4.5E-13 4.0E-07218-01-9 ~Chrysene 0.178 0.178 0.178 1.2E-09 3.9E-10 1.8E-15 1.6E-09206-44-0 ~Fluoranthene 0.193 0.193 0.193 6.2E-05 1.9E-05 8.1E-05193-39-5 ~Indeno[1,2,3-cd]pyrene 0.226 0.226 0.226 1.5E-07 4.9E-08 2.3E-13 2.0E-07
129-00-0 ~Pyrene 0.22 0.22 0.22 9.4E-05 2.9E-05 1.2E-047782-49-2 Selenium 1.97 1.97 1.97 5.0E-03 1.6E-09 5.0E-037440-22-4 Silver 0.105 0.105 0.105 2.7E-04 2.7E-04
Cumulative:2.6E-05 2.8E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: 25006-21-060Exposure Unit ID: Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:Ingestion Concentration (mg/kg)
Dermal Concentration (mg/kg)
Inhalation Concentration (mg/kg)*
Ingestion Carcinogenic Risk
Dermal Carcinogenic Risk
Inhalation Carcinogenic Risk
Calculated Carcinogenic Risk
Ingestion Hazard Quotient
Dermal Hazard Quotient
Inhalation Hazard Quotient
Calculated
Non-Carcinogenic Hazard Quotient67-64-1 Acetone 0.104 0.104 0.104 9.9E-08 5.3E-08 1.5E-07
107-02-8 Acrolein 0.001 0.001 0.001 1.7E-06 1.6E-03 1.6E-037440-38-2 Arsenic, Inorganic 7.36 7.36 7.36 2.0E-06 4.3E-07 4.3E-11 2.5E-06 1.3E-02 2.7E-03 1.9E-06 1.5E-027440-39-3 Barium 101 101 101 4.3E-04 7.8E-07 4.3E-0471-43-2 Benzene 0.0009 0.0009 0.0009 1.5E-11 1.5E-10 1.7E-10 1.9E-07 1.8E-06 2.0E-06
7440-43-9 Cadmium (Diet)0.399 0.399 0.399 9.9E-13 9.9E-13 3.4E-04 5.8E-05 1.5E-07 4.0E-0416065-83-1 Chromium(III), Insoluble Salts 172.2 172.2 172.2 9.8E-05 9.8E-0518540-29-9 Chromium(VI)3.8 3.8 3.8 5.8E-07 4.4E-10 5.8E-07 1.1E-03 1.5E-07 1.1E-037439-92-1 ~Lead and Compounds 83.1 83.1 83.1 <SL**<SL**<SL**7439-97-6 ~Mercury (elemental)0.106 0.106 0.106 2.2E-03 2.2E-0378-93-3 Methyl Ethyl Ketone (2-Butanone)0.006 0.006 0.006 8.6E-09 2.1E-08 3.0E-0850-32-8 ~Benzo[a]pyrene 0.287 0.287 0.287 8.8E-08 4.8E-08 2.4E-13 1.4E-07 8.2E-04 4.5E-04 5.5E-07 1.3E-03205-99-2 ~Benzo[b]fluoranthene 0.456 0.456 0.456 1.4E-08 7.7E-09 3.8E-14 2.2E-08218-01-9 ~Chrysene 0.178 0.178 0.178 5.4E-11 3.0E-11 1.5E-16 8.4E-11206-44-0 ~Fluoranthene 0.193 0.193 0.193 4.1E-06 2.3E-06 6.4E-06193-39-5 ~Indeno[1,2,3-cd]pyrene 0.226 0.226 0.226 6.9E-09 3.8E-09 1.9E-14 1.1E-08129-00-0 ~Pyrene 0.22 0.22 0.22 6.3E-06 3.5E-06 9.7E-067782-49-2 Selenium 1.97 1.97 1.97 3.4E-04 3.8E-10 3.4E-047440-22-4 Silver 0.105 0.105 0.105 1.8E-05 1.8E-05
Cumulative:3.2E-06 2.3E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator