23053 Final Redevelopment Summary Report_Cotton Seed Oil Mill 20210412

Via Email

April 12, 2021

NCDEQ – Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attention: Ms. Jordan Thompson

Re: Redevelopment Summary Report
Former Cotton Seed Oil Mill
300 Rampart Street
Charlotte, North Carolina
Brownfields Project No. 23053-19-060
H&H Job No. JMC-011

Dear Jordan:

1.0 Introduction

On behalf of 300 Rampart Owner, LLC (Prospective Developer or PD), Hart & Hickman, PC
(H&H) is submitting this report to summarize environmental-related activities associated with
redevelopment of the Former Cotton Seed Oil Mill Brownfields property (Brownfields Project
No. 23053-19-060) located at 300 Rampart Street in Charlotte, Mecklenburg County, North
Carolina (Site). In addition, this report documents methods and results associated with final
grade soil assessment activities completed. The Site is comprised of one parcel of land that is
approximately 2.4 acres. A Site location map is provided as Figure 1, and the Site and
surrounding area are depicted on Figure 2.

The current phase of construction (identified as Phase 1) involves adaptive reuse of the central
and eastern warehouse buildings for commercial office and retail use. During Phase 1 of
redevelopment, partial demolition of the western warehouse occurred (building slab remains) to
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provide a location for additional parking spaces. Future phases of construction may include the
potential future vertical build-out for high-density residential development.

A Notice of Brownfields Property, including the Land Use Restrictions (LURs) and the
Brownfields Agreement between the North Carolina Department of Environmental Quality
(DEQ) and the PD, was recorded on August 28, 2020. LUR “h” generally states that a final
report documenting environmental-related activities during redevelopment will be submitted
upon completion of physical redevelopment of the Brownfields property. The previous
redevelopment summary report for the Site was submitted to DEQ on January 21, 2021 and this
report covers Brownfields-related activities since January 2021.

LUR “e” generally states that for each phase of redevelopment completion, representative final
grade soil sampling will be completed in areas within the Brownfields property that are not
covered by demonstrably clean fill soil, building foundations, sidewalks, or asphaltic or concrete
parking areas and driveways pursuant to a plan approved in writing by DEQ. The Final Grade
Soil Sampling Work Plan (Revision 1) was submitted to the DEQ Brownfields Program on
January 20, 2021 and received DEQ-approval in a letter dated February 4, 2021.

This report has been prepared in accordance with LUR No. h and LUR No. e in the recorded
Brownfields agreement for the Site. Details of environmental-related redevelopment activities
are provided in Section 2.0; final grade soil assessment activities are discussed in Section 3.0;
and a summary is provided in Section 4.0.
Ms. Jordan Thompson
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2.0 Recent Environmental-Related Redevelopment Activities

The first phase of redevelopment activities at the Site has been completed and included building
perimeter grading activities, utility installations, partial demolition of the western warehouse
building, and interior renovation of the central and eastern warehouse buildings. The slab of the
western building remains for use as a parking surface. Remaining portions of the Site have been
improved with concrete-paved access drives, parking areas, sidewalks, landscaped areas, and a
concrete drainage channel. Redevelopment activities at the Site were conducted in accordance
with the DEQ-approved Environmental Management Plan (EMP) signed January 14, 2020.

As part of grading and redevelopment activities completed at the Site, approximately 783 tons of
excess soil were loaded onto trucks and transported to the Republic Services CMS Landfill in
Concord, North Carolina for disposal. Export soil amounts and manifests provided by the
landfill are included in Appendix A.

3.0 Final Grade Soil Assessment

The final grade soil sampling activities were conducted in general accordance with the DEQ
Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup dated January
2020, the most recent versions of the U.S. Environmental Protection Agency (EPA) Region IV
Science and Ecosystem Support Division (SESD) Field Branches Quality System and Technical
Procedures guidance, and the DEQ-approved Work Plan.

3.1 Soil Sampling Methodologies

Results of visual observations and conversations with Site personnel indicate that the Site is
predominately covered with hardscape surfaces with the exception of three distinct portions of
the Site. Unpaved areas at the Site include 1) a landscaped and grass-covered area west of the
parking ramp in the southwestern portion of the Site; 2) landscaped and grass-covered areas east
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of the parking ramp between the Site building and Rampart Street; and 3) a relatively long
landscaped and grass-covered area along the northern Site property boundary.

Landscaped and/or grass-covered areas were divided into four discrete final grade evaluation
areas (FG-1 through FG-4). The four final grade areas are shown on Figure 3 and are described
below:

 Final grade area FG-1 includes landscaped and grass-covered areas located west of the
parking ramp in the southwestern portion of the Site;
 Final grade area FG-2 includes landscaped and grass-covered areas located east of the
parking ramp between the Site building and Rampart Street;
 Final grade area FG-3 includes the western portion of landscaped and grass-covered areas
located along the northern Site property boundary; and
 Final grade area FG-4 includes the eastern portion of landscaped and grass-covered areas
located along the northern Site property boundary.

Multiple soil borings were advanced in each final grade evaluation area for collection of soil
samples to represent shallow soil conditions in unpaved areas at the Site. The soil boring
locations for each final grade evaluation area are shown in Figure 3.

Each final grade soil boring was advanced to approximately 2 feet below the ground surface (ft
bgs) utilizing a decontaminated stainless-steel hand auger. Continuous aliquot soil samples were
collected from the center of the hand auger bucket at each boring and observed for the presence
of staining or odors and field screened for elevated volatile organic vapors using a calibrated
photo-ionization detector (PID). Field personnel did not observe the presence of staining or
odors in the sample aliquots and PID readings did not indicate the presence of organic vapors.
Boring logs showing PID readings are provided in Appendix B.

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Following boring advancement, soil sample aliquots collected in each final grade evaluation area
were combined and homogenized to form one composite soil sample representative of that
evaluation area for a total of four (4) composite final grade soil samples (FG-1 through FG-4).
In addition to the composite soil samples, one representative grab soil sample was collected from
each final grade evaluation area at the aliquot location that exhibited the highest PID reading.
The grab soil samples were collected from undisturbed portions of the aliquot soil sample.

Soil samples selected for laboratory analysis were collected directly into dedicated laboratory
supplied sample containers, labeled with the sample identification, date, time, and requested
analyses, and placed in a dedicated laboratory supplied cooler with ice. The samples were
delivered to Waypoint Analytical under standard chain of custody protocols for analysis of
volatile organic compounds (VOCs) by EPA Method 8260, semi-VOCs (SVOCs) by EPA
Method 8270, and Resource Conservation and Recovery Act (RCRA) metals plus hexavalent
chromium by EPA Methods 6020/7471/7199.

For quality assurance and quality control purposes, H&H collected one duplicate composite
sample from FG-2 for analysis of SVOCs and RCRA metals plus hexavalent chromium analysis.
H&H also collected a duplicate sample for VOC analysis from the FG2-AL1 grab sample
aliquot.

Following sampling activities, the soil borings were properly abandoned and the surfaces were
repaired similar to pre-drilling conditions.

3.2 Final Grade Soil Sample Results

A tabular summary of final grade soil sample analytical results is presented in Table 1, and
copies of the laboratory analytical report and chain of custody record are provided in Appendix
C. The laboratory analytical results were compared to the DEQ IHSB Residential and
Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) dated January 2021. In
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addition to the PSRGs, metals results were compared to published concentrations for naturally
occurring metals.

Arsenic concentrations (up to 16.5 mg/kg) in two areas exceed the Non-Residential and
Residential PSRGs and appear to also exceed background concentrations. However, the detected
concentrations of arsenic are below EPA’s Site-Specific Action Level for lead of 27 mg/kg. In
addition, the SVOC benzo(a)pyrene (0.143 estimated or “J” mg/kg) was detected in the FG-4
composite soil sample at a concentration above the DEQ IHSB Residential PSRG of 0.11 mg/kg.
Additionally, detected concentrations of hexavalent chromium (up to 0.71 J mg/kg) exceeded
DEQ IHSB Residential PSRGs and were above the mean background metals concentrations in
North Carolina soils in soil samples FG-2/FG-DUP, FG-3, and FG-4. Mean background metals
concentrations for North Carolina soils were obtained from Elements in North American Soils by
Dragun and Chekiri, 2005. Several additional VOCs, SVOCs, and metals were detected in soil
samples at concentrations above the laboratory method detection limit, but below PSRGs or the
mean background metals concentrations.

The DEQ IHSB PSRGs are conservative and based upon a lifetime incremental cancer risk
(LICR) for potential carcinogenic risks of 1 x 10-6 and a non-carcinogenic hazard quotient (HQ)
of 0.2 for potential non-carcinogenic risks. The DEQ and EPA acceptable risk level for
cumulative carcinogenic risks is 1 x 10-4 and the acceptable level for cumulative non-
carcinogenic risks is a hazard index (HI) less than 1.

H&H completed the DEQ Risk Calculator (January 2021 version) to confirm there are no
unacceptable exposure risks in soil located in unpaved areas at the Site. To model a hypothetical
worst-case residential exposure scenario, the highest concentrations of each compound detected
in the final grade soil samples was utilized in the calculator.

Although the Site is currently redeveloped for commercial purposes, hypothetical worst-case
residential risk calculator results indicate that the cumulative LICR is 2.8 x 10-5 and the
calculated cumulative HI is 0.51. The results of worst-case scenario final grade soil sample risk
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calculations indicate that cumulative carcinogenic and noncarcinogenic risks do not exceed the
DEQ and EPA acceptable levels, even for residential use. A copy of the completed Risk
Calculator is included as Appendix D.

4.0 Summary and Conclusions

The first phase of redevelopment activities at the former Cotton Seed Oil Mill Brownfields
property located at 300 Rampart Street in Charlotte, Mecklenburg County, NC has been
completed. The redevelopment activities were performed in accordance with the DEQ-approved
EMP. H&H has completed final grade soil sampling activities in accordance with the DEQ-
approved Work Plan. During redevelopment activities, approximately 783 tons of soil were
exported from the Site and disposed at the Republic Services CMS Landfill in Concord, North
Carolina.

Final grade soil sampling activities were also conducted at the Site and included collection of
soil samples to evaluate the potential for impacts in areas at the Site that are not covered by
demonstrably clean fill soil, building foundations, sidewalks, or asphaltic or concrete parking
areas and driveways. Arsenic concentrations (up to 16.5 mg/kg) in two areas exceed the Non-
Residential and Residential PSRGs and appear to also exceed background concentrations. In
addition, the SVOC benzo(a)pyrene (0.143 estimated or “J” mg/kg) was detected in the FG-4
composite soil sample at a concentration above the DEQ IHSB Residential PSRG. Additionally,
detected concentrations of hexavalent chromium (up to 0.71 J mg/kg) exceeded DEQ IHSB
Residential PSRGs and were above the mean background metals concentrations in North
Carolina soils in three composite soil sample areas. Although the Site is currently redeveloped
for commercial purposes, to further evaluate potential cumulative risks for a residential occupant
at the Site, H&H calculated cumulative risks using the conservatively highest concentrations of
compounds detected in the final grade soil samples. The results of the risk calculations indicate
that the calculated cumulative LICR (2.8 x 10-5) and the calculated cumulative HI (0.51) are
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within the DEQ and EPA acceptable levels for cumulative carcinogenic and noncarcinogenic
exposure risks, even for residential use.

Should you have any questions or need additional information, please do not hesitate to call us at
[phone].

Very truly yours,
Hart & Hickman, PC

Matt Bramblett, PE Robert Sorgel
Principal and Project Manager Project Geologist

Attachments:

Table 1 Summary of Final Grade Soil Sample Analytical Results

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Final Grade Soil Sample Location Map

Appendix A Export Soil Summary
Appendix B Soil Boring Logs
Appendix C Laboratory Analytical Report
Appendix D DEQ Risk Calculator

cc: Mr. Chris Deppoliti, Acram (Via Email)
Ms. Mary Katherine Stukes, MVA (Via Email)
Mr. Robert Sorgel, H&H (Via Email)

Table 1 Summary of Final Grade Soil Analytical ResultsFormer Cotton Seed Oil MillCharlotte, North CarolinaH&H Job No. JMC-011Sample IDFG-1 FG1-AL4 FG-2 FG2-AL1 FG-DUP (FG-2/FG2-AL1) FG-3 FG3-AL3 FG-4 FG4-AL3Sample Date3/8/2021 3/8/2021 3/8/2021 3/8/2021 3/8/2021 3/8/2021 3/8/2021 3/8/2021 3/8/2021Sample TypeComposite Grab Composite Grab Composite / Grab Composite Grab Composite GrabSample Depth (ft bgs)0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 0-2 Range MeanVOCs (8260B)AcetoneNA <0.018 NA <0.018 <0.018 NA <0.018 NA0.022 J 12,000 140,000 -- --Methyl Ethyl Ketone (2-Butanone)NA <0.001 NA <0.001 <0.001 NA <0.001 NA0.002 J 5,500 40,000 -- --SVOCs (8270D)Acenapthylene<0.016 NA <0.018 NA <0.018 <0.016 NA0.026 JNA720 9,000 -- --Anthracene<0.009 NA <0.009 NA <0.009 <0.008 NA0.028 JNA3,600 45,000 -- --Benzo(a)anthracene0.026 JNA <0.009 NA <0.0090.023 JNA0.113 JNA1.1 21 -- --Benzo(a)pyrene0.021 JNA <0.007 NA <0.0070.021 JNA0.143 JNA0.11 2.1 -- --Benzo(b)fluoranthene<0.007 NA <0.007 NA <0.0070.034 JNA0.219 JNA1.1 21 -- --Benzo(g,h,i)perylene<0.008 NA <0.008 NA <0.008 <0.008 NA0.123 JNANE NE -- --Benzo(k)fluoranthene<0.008 NA <0.008 NA <0.008 <0.008 NA0.075 JNA11 210 -- --Chrysene<0.009 NA <0.009 NA <0.0090.022 JNA0.154 JNA110 2,100 -- --Fluoranthene<0.009 NA <0.009 NA <0.0090.033 JNA0.274 JNA480 6,000 -- --Indeno(1,2,3-cd)pyrene<0.023 NA <0.023 NA <0.023 <0.022 NA0.128 JNA1.1 21 -- --1-Methylnaphthalene<0.012 NA <0.012 NA <0.012 <0.012 NA0.020 JNA18 73 -- --2-Methylnaphthalene<0.015 NA <0.016 NA <0.016 <0.015 NA0.024 JNA48 600 -- --Naphthalene<0.017 NA <0.017 NA <0.017 <0.017 NA0.022 JNA2.1 8.8 -- --Phenanthrene<0.008 NA <0.009 NA <0.009 <0.008 NA0.143 JNANE NE -- --Pyrene<0.011 NA <0.012 NA <0.0120.038 JNA0.295 JNA360 4,500 -- --Metals (6020/7471/7199)Arsenic3.61NA3.39NA3.5312.8NA16.5NA0.68 3.01.0 - 18 4.8Barium78.2NA65.5NA72.6 81.2NA123NA3,100 47,000 50 - 1,000 356Cadmium0.0524 JNA <0.0463 NA <0.04640.0935 JNA0.226 JNA14 200 1.0 - 10 4.3Total Chromium40.4NA58.6NA58.6 42.9NA44.9NA-- --7.0 - 300 65Hexavalent Chromium<0.26 NA0.71 JNA0.41 J<0.23 NA <0.24 NA0.31 6.5 NE NETrivalent Chromium40.4NA57.9NA58.2 42.9NA44.9NA23,000 350,000 NE NELead11.8NA19.0NA18.4 46.1NA78.7NA400 8000 - 50 16Mercury0.0723NA0.107NA0.106 0.116NA0.086NA2.3 9.70.03 - 0.52 0.121Selenium2.93NA2.44NA1.89 2.29NA2.32NA78 1,200 <0.1 - 0.8 0.4Silver<0.0632 NA <0.0638 NA <0.06390.0717 JNA0.0784 JNA78 1,2000 - 5.0 NENotes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (January 2021).2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Background Cd and Ag concentrations were taken from Southeastern and Conterminous US soils.Bold indicates concentration exceeds DEQ IHSB Residential PSRG and above the mean background metals in North Carolina soils for metals as preliminary comparison.Underlined indicates concentration exceeds DEQ IHSB Industrial/Commercial PSRGs and above the mean background metals in North Carolina soils for metals as preliminary comparison.Soil concentrations are reported in milligrams per kilogram (mg/kg). Laboratory analytical methods are shown in parentheses.Compound concentrations are reported to the laboratory method detection limit.With the exception of metals, only those compounds detected in at least one sample are shown.Residential PSRG (1)Industrial/Commercial PSRG (1)Regional Background Metals in Soil (2)ft bgs = feet below ground surface; VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; NA = not analyzed; -- = not applicable; NE = Not EstablishedJ = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in an estimated concentration. S:\AAA-Master Projects\JMC Holdings\JMC.011 Rampart BFs Implementation\Final Grade Soil Sampling\Tables\Final Grade Sampling (JMC.011)3/22/2021Table 1 (Page 1 of 1)Hart & Hickman, PC
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NORTH CAROLINA 1991
TITLE
PROJECT
SITE LOCATION MAP
FORMER COTTON SEED OIL MILL 300 RAMPART STREET CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
8-23-2019 0
1JMC-011
SITE
REVISION NO. 0
JOB NO. JMC-011
DATE: 12-10-19
FIGURE NO. 2
CHARLOTTE SALVAGE COMPANY
300 RAMPART STREET
CHARLOTTE, NORTH CAROLINA
SITE AND SURROUNDING AREA MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
FLOOR DRAIN
POLE-MOUNTED TRANSFORMER
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
RAMPART ST
R
E
E
T
RAMPART S
T
R
E
E
T
HAW
KI
N
S
S
T
R
E
E
T
HAW
KI
N
S
S
T
R
E
E
TS. TRYON STREETS.TRYON STREETTHE PENROSE APARTMENTS / FORMER
VCC CHARLOTTE (349 W. TREMONT AVENUE)
THE PENROSE APARTMENTS / FORMER
VCC CHARLOTTE (349 W. TREMONT AVENUE)
VACANT
(2129 S. TRYON STREET)
VACANT
(2129 S. TRYON STREET)
K9 PLAYLAND
(2139 S. TRYON STREET)
K9 PLAYLAND
(2139 S. TRYON STREET)
MUTLI-TENANT COMMERCIAL BUILDINGS
(2204-2228 HAWKINS STREET)
MUTLI-TENANT COMMERCIAL BUILDINGS
(2204-2228 HAWKINS STREET)
KEG N CUE
(2131 S. TRYON STREET)
KEG N CUE
(2131 S. TRYON STREET)
MAACO FLEET SOLUTIONS
(2217 S. TRYON STREET)
MAACO FLEET SOLUTIONS
(2217 S. TRYON STREET)
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS (2019).
GMI
(222 RAMPART STREET)
GMI
(222 RAMPART STREET)S:\AAA-Master Projects\JMC Holdings\JMC.009 300 Rampart Brownfields\Brownfields Assessment\Figures\Site Map.dwg, FIG 2, 1/6/2020 10:31:45 PM, sperry
REVISION NO. 0
JOB NO. JMC-011
DATE: 3-8-21
FIGURE NO. 3
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
BUILDING FOOTPRINT
UNPAVED AREAS
FG-1 ALIQUOT SOIL SAMPLE LOCATION
FG-2 ALIQUOT SOIL SAMPLE LOCATION
FG-3 ALIQUOT SOIL SAMPLE LOCATION
FG-4 ALIQUOT SOIL SAMPLE LOCATION
FORMER COTTON SEED OIL MILL
300 RAMPART STREET
CHARLOTTE, NORTH CAROLINA
FINAL GRADE SOIL SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
MULTI-TENANT COMMERCIAL BUILDINGS(2204-2228 HAWKINS STREET)
HAW
KI
N
S
S
T
R
E
E
T
RAMPART S
T
R
E
E
TS. TRYON STREETGMI(222 RAMPART STREET)
THE PENROSE APARTMENTS
(349 W. TREMONT AVENUE)
VACANT(2129 S. TRYON STREET)
MAACO FLEET SOLUTIONS(2217 S. TRYON STREET)
KEG N CUE(2131 S. TRYON STREET)
K9 PLAYLAND(2139 S. TRYON STREET)S:\AAA-Master Projects\JMC Holdings\JMC.011 Rampart BFs Implementation\Final Grade Soil Sampling\Figures\JMC-011.Figures 20210108.dwg, FIG 3, 1/12/2021 8:42:37 AM, shaynesFG1-AL1
FG1-AL3
FG1-AL2
FG1-AL4
FG3-AL1 FG3-AL2 FG3-AL3 FG3-AL4 FG3-AL5 FG4-AL1 FG4-AL2 FG4-AL3 FG4-AL4 FG4-AL5
FG2-AL1
FG2-AL2 FG2-AL3 FG2-AL4
FG2-AL5

Appendix A

Export Soil Summary
Ticket Number Tonnage Total to Date
Friday, January 29, 2021
1789147 12.50 783.43
1789172 16.78
1789185 10.83
1789204 14.89
1789205 13.28
1789227 18.04
1789234 13.03
1789238 16.52
1789255 17.20
1789269 15.72
1789272 17.97
1789277 19.34
1789295 13.99
1789301 15.77
1789306 13.98
1789323 17.23
1789326 18.20
1789337 20.71
1789353 17.00
Saturday, January 30, 2021
1789381 17.16
1789384 17.11
1789385 13.90
1789388 16.05
1789391 13.69
1789394 14.35
1789399 17.15
1789400 14.25
1789406 18.90
Monday, February 01, 2021
1789460 11.37
1789465 9.90
1789469 9.51
1789489 10.14
1789494 13.43
1789506 12.41
1789507 10.65
1789513 12.25
1789518 15.92
1789542 12.71
1789545 11.04
1789552 11.15
1789560 9.92
1789572 14.30
1789575 11.54
1789577 10.38
1789581 11.91
1789597 14.18
1789615 14.05
1789616 12.50
1789620 11.23
1789629 13.98
1789645 14.33
Tuesday, February 02, 2021
1789710 14.24
1789752 14.53
1789763 15.87
1789789 14.45
300 Rampart Hauling to Republic

Appendix B

Soil Boring Logs
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG1-AL1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') SILT (ML); few fine-medium sand, some clay, medium stiff, moist, reddish-brown
(2') Boring terminated
0.9 FG-1
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG1-AL2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Sandy SILT (ML); little clay, medium stiff, dry, reddish-brown
(2') Boring terminated
0.3 FG-1
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG1-AL3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Sandy SILT (ML); little clay, medium stiff, dry, reddish-brown
(2') Boring terminated
0.4 FG-1
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG1-AL4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Sandy SILT (ML); little clay, medium stiff, dry, reddish-brown
(2') Boring terminated
1.3 FG1-AL4
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG2-AL1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') SILT with sand (ML); few fine gravel, medium stiff, moist, reddish-brown, fill
(2') Boring terminated
2.2 FG2-AL1
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG2-AL2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') SILT (ML); few fine sand, little clay, stiff, dry, reddish-brown
(2') Boring terminated
1.2 FG-2/DUP
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG2-AL3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') SILT (ML); few fine-medium sand, little clay, stiff, dry, reddish-brown
(2') Boring terminated
2.0 FG-2/DUP
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG2-AL4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') SILT (ML); trace fine-medium sand, little clay, stiff, moist, reddish-brown, some
gravel fill
(2') Boring terminated
1.8 FG-2/DUP
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG2-AL5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') SILT (ML); few fine sand, little clay, medium stiff, moist, reddish-brown, some
gravel fill
(2') Boring terminated
1.2 FG-2/DUP
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG3-AL1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Lean CLAY (CL); few fine sand, few silt, medium plasticity, soft, moist,
reddish-brown
(2') Boring terminated
1.0 FG-3
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG3-AL2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Fat CLAY (CH); trace fine gravel, trace fine sand, some silt, high plasticity, soft,
saturated, reddish-brown
(2') Boring terminated
1.4 FG-3
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG3-AL3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Sandy SILT (ML); stiff, dry, brown, some gravel fill
(2') Boring terminated
2.1 FG3-AL3
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG3-AL4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Sandy SILT (ML); stiff, dry, brown, some gravel fill
(2') Boring terminated
2.0 FG-3
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG3-AL5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Sandy SILT (ML); stiff, dry, brown, some gravel fill
(2') Boring terminated
1.2 FG-3
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG4-AL1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Sandy SILT (ML); few clay, soft, moist, reddish-brown, some gravel fill
(2') Boring terminated
1.1 FG-4
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG4-AL2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Sandy SILT (ML); few clay, soft, moist, reddish-brown, some gravel fill
(2') Boring terminated
1.5 FG-4
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG4-AL3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') SILT (ML); trace fine sand, little clay, medium stiff, moist, reddish-brown
(2') Boring terminated
1.7 FG4-AL3
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG4-AL4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Sandy SILT (ML); soft, moist, reddish-brown
(2') Boring terminated
1.3 FG-4
0
1
2
3
4
5
NOTES: Hole precleared to 2.0' on 3/8/2021 by Hart & Hickman, PC using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
JMC Holdings
JMC-011
300 Rampart Street, Charlotte, NC
BORING LOG
Boring No.
Page:
FG4-AL5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/8/2021
3/8/2021
Hart & Hickman, PC
Other
Hand Auger
KAM
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.30
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 2.00 (0') Sandy SILT (ML); medium stiff, moist, reddish-brown
(2') Boring terminated
0.7 FG-4
0
1
2
3
4
5
NOTES:
BORING AND WELL LOG LEGEND
LITHOLOGYWATER LEVELWELL/BORINGCOMPLETIONSample TypeDESCRIPTION

GR
EN
SS
SH
CO
DP
ID
ASPHALT
CONCRETE
BEDROCK
IGNEOUS Rock
METAMORPHIC Rock
SEDIMENTARY Rock
Well-graded GRAVEL (GW)
Poorly graded GRAVEL (GP)
Silty GRAVEL (GM)
Clayey GRAVEL (GC)
Well-graded GRAVEL with silt (GW-GM)
Poorly graded GRAVEL with silt (GP-GM)
Well-graded GRAVEL with clay (GW-GC)
Poorly graded GRAVEL with clay (GP-GC)
Well-graded SAND (SW)
Poorly graded SAND (SP)
Silty SAND (SM)
Clayey SAND (SC)
Well-graded SAND with silt (SW-SM)
Poorly graded SAND with silt (SP-SM)
Well-graded SAND with clay (SW-SC)
Poorly graded SAND with clay (SP-SC)
SILT (ML)
Lean CLAY (CL)
Organic SOIL (OL)
Elastic SILT (MH)
Fat CLAY (CH)
Organic SOIL (OH)
Organic SOIL (OL/OH)
PEAT (PT)
Volume Descriptors:
Trace = <5%
Few = 5-10%
Little = 15-25%
Some = 30-45%
Mostly = >=50%
Water Level During Drilling
Water Level at End of Drilling/in Completed Well
Cap
Riser
Screen
End Plug
Annular Seal (Bentonite-Cement Grout, Bentonite Slurry/Chips/Pellets/Powder, Other)
Sanitary Seal (Bentonite Slurry/Chips/Pellets/Powder, Other)
Filter Pack (Sand, Gravel, Other)
Backfill
Grab
Encore
Split Spoon
Shelby Tube
Core Barrel
Direct Push
Lab Sample and ID

Appendix C

Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

3/16/2021
Hart & Hickman (Charlotte) Robert Sorgel
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 21-068-0001 Client Project Description: JMC.011
Dear Robert Sorgel:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/8/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 110
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202137735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202199012State ProgramSouth Carolina
12/31/202099012State ProgramSouth Carolina
Page 1 of 1 00016/21-068-0001
Page 2 of 110
Report Number:
Sample Summary Table
Client Project Description:
21-068-0001
JMC.011
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
03/08/2021 12:15Solids 94144 FG-1 03/08/2021 15:57 7199
03/08/2021 12:15Solids 94144 FG-1 03/08/2021 15:57
03/08/2021 14:00Solids 94145 FG-2 03/08/2021 15:57 7199
03/08/2021 14:00Solids 94145 FG-2 03/08/2021 15:57
03/08/2021 09:15Solids 94146 FG-3 03/08/2021 15:57 7199
03/08/2021 09:15Solids 94146 FG-3 03/08/2021 15:57
03/08/2021 11:00Solids 94147 FG-4 03/08/2021 15:57 7199
03/08/2021 11:00Solids 94147 FG-4 03/08/2021 15:57
03/08/2021 12:20Solids 94148 FG1-AL4 03/08/2021 15:57
03/08/2021 14:05Solids 94149 FG2-AL1 03/08/2021 15:57
03/08/2021 09:20Solids 94150 FG3-AL3 03/08/2021 15:57
03/08/2021 11:05Solids 94151 FG4-AL3 03/08/2021 15:57
03/08/2021Solids 94152 FG-Dup 03/08/2021 15:57 7199
03/08/2021Solids 94152 FG-Dup 03/08/2021 15:57
03/08/2021Aqueous 94153 Trip Blank 03/08/2021 15:57
: Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 110
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-068-0001
Report Limit
Project:JMC.011
V 94144FG-1
3.61 03/10/2021 16:126020BArsenicmg/Kg - dry 0.104
78.2 03/10/2021 16:126020BBariummg/Kg - dry 0.446
J0.0524 03/10/2021 16:126020BCadmiummg/Kg - dry 0.0459
40.4 03/10/2021 16:126020BChromiummg/Kg - dry 0.297
11.8 03/10/2021 16:126020BLeadmg/Kg - dry 0.0942
2.93 03/10/2021 16:126020BSeleniummg/Kg - dry 0.285
0.0723 03/10/2021 12:477471BMercury (Total)mg/Kg - dry 0.0186
J0.026 03/10/2021 16:198270EBenzo(a)anthracene mg/Kg - dry 0.009
J0.021 03/10/2021 16:198270EBenzo(a)pyrene mg/Kg - dry 0.007
19.4 03/09/2021 15:20SW-DRYWT Moisture %
V 94145FG-2
3.39 03/10/2021 16:196020BArsenicmg/Kg - dry 0.105
65.5 03/10/2021 16:196020BBariummg/Kg - dry 0.450
58.6 03/10/2021 16:196020BChromiummg/Kg - dry 0.300
19.0 03/10/2021 16:196020BLeadmg/Kg - dry 0.0951
2.44 03/10/2021 16:196020BSeleniummg/Kg - dry 0.287
0.107 03/10/2021 12:517471BMercury (Total)mg/Kg - dry 0.0188
20.1 03/09/2021 15:20SW-DRYWT Moisture %
V 94146FG-3
12.8 03/10/2021 16:256020BArsenicmg/Kg - dry 0.103
81.2 03/10/2021 16:256020BBariummg/Kg - dry 0.443
J0.0935 03/10/2021 16:256020BCadmiummg/Kg - dry 0.0455
42.9 03/10/2021 16:256020BChromiummg/Kg - dry 0.295
46.1 03/10/2021 16:256020BLeadmg/Kg - dry 0.0935
2.29 03/10/2021 16:256020BSeleniummg/Kg - dry 0.283
J0.0717 03/10/2021 16:256020BSilvermg/Kg - dry 0.0628
0.116 03/10/2021 12:567471BMercury (Total)mg/Kg - dry 0.0185
J0.023 03/10/2021 17:038270EBenzo(a)anthracene mg/Kg - dry 0.009
J0.021 03/10/2021 17:038270EBenzo(a)pyrene mg/Kg - dry 0.007
J0.034 03/10/2021 17:038270EBenzo(b)fluoranthene mg/Kg - dry 0.007
J0.022 03/10/2021 17:038270EChrysenemg/Kg - dry 0.009
J0.033 03/10/2021 17:038270EFluoranthenemg/Kg - dry 0.009
J0.038 03/10/2021 17:038270EPyrenemg/Kg - dry 0.011
18.8 03/09/2021 15:20SW-DRYWT Moisture %
Page 4 of 110
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-068-0001
Report Limit
Project:JMC.011
V 94147FG-4
16.5 03/10/2021 16:326020BArsenicmg/Kg - dry 0.102
123 03/10/2021 16:326020BBariummg/Kg - dry 0.439
J0.226 03/10/2021 16:326020BCadmiummg/Kg - dry 0.0451
44.9 03/10/2021 16:326020BChromiummg/Kg - dry 0.292
78.7 03/10/2021 16:326020BLeadmg/Kg - dry 0.0926
2.32 03/10/2021 16:326020BSeleniummg/Kg - dry 0.280
J0.0784 03/10/2021 16:326020BSilvermg/Kg - dry 0.0621
0.0860 03/10/2021 13:017471BMercury (Total)mg/Kg - dry 0.0183
J0.026 03/10/2021 17:268270EAcenaphthylenemg/Kg - dry 0.015
J0.028 03/10/2021 17:268270EAnthracenemg/Kg - dry 0.008
J0.113 03/10/2021 17:268270EBenzo(a)anthracene mg/Kg - dry 0.009
J0.143 03/10/2021 17:268270EBenzo(a)pyrene mg/Kg - dry 0.007
J0.219 03/10/2021 17:268270EBenzo(b)fluoranthene mg/Kg - dry 0.007
J0.123 03/10/2021 17:268270EBenzo(g,h,i)perylene mg/Kg - dry 0.007
J0.075 03/10/2021 17:268270EBenzo(k)fluoranthene mg/Kg - dry 0.008
J0.154 03/10/2021 17:268270EChrysenemg/Kg - dry 0.009
J0.274 03/10/2021 17:268270EFluoranthenemg/Kg - dry 0.009
J0.128 03/10/2021 17:268270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.022
J0.020 03/10/2021 17:268270E1-Methylnaphthalene mg/Kg - dry 0.012
J0.024 03/10/2021 17:268270E2-Methylnaphthalene mg/Kg - dry 0.015
J0.022 03/10/2021 17:268270ENaphthalenemg/Kg - dry 0.017
J0.143 03/10/2021 17:268270EPhenanthrenemg/Kg - dry 0.008
J0.295 03/10/2021 17:268270EPyrenemg/Kg - dry 0.011
18.0 03/09/2021 15:20SW-DRYWT Moisture %
V 94148FG1-AL4
19.4 03/09/2021 15:20SW-DRYWT Moisture %
V 94149FG2-AL1
20.1 03/09/2021 15:20SW-DRYWT Moisture %
V 94150FG3-AL3
18.8 03/09/2021 15:20SW-DRYWT Moisture %
V 94151FG4-AL3
J0.022 03/11/2021 16:178260DAcetonemg/Kg - dry 0.018
J0.002 03/11/2021 16:178260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.001
18.0 03/09/2021 15:20SW-DRYWT Moisture %
Page 5 of 110
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-068-0001
Report Limit
Project:JMC.011
V 94152FG-Dup
3.53 03/10/2021 16:386020BArsenicmg/Kg - dry 0.105
72.6 03/10/2021 16:386020BBariummg/Kg - dry 0.451
58.6 03/10/2021 16:386020BChromiummg/Kg - dry 0.301
18.4 03/10/2021 16:386020BLeadmg/Kg - dry 0.0953
1.89 03/10/2021 16:386020BSeleniummg/Kg - dry 0.288
0.106 03/10/2021 13:057471BMercury (Total)mg/Kg - dry 0.0188
20.3 03/09/2021 15:20SW-DRYWT Moisture %
V 94153Trip Blank
JB1.63 03/10/2021 15:348260DAcetoneµg/L 0.310
Page 6 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-1
94144 Matrix:
3/8/2021 12:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.4 %Moisture 1 03/09/21 15:20 SW-DRYWTEDV
3.61 mg/Kg - dry 0.104 0.124Arsenic 10 03/10/21 16:12 6020BMMR
78.2 mg/Kg - dry 0.446 12.4Barium 10 03/10/21 16:12 6020BMMR
0.0524 J mg/Kg - dry 0.0459 0.620Cadmium 10 03/10/21 16:12 6020BMMR
40.4 mg/Kg - dry 0.297 1.24Chromium 10 03/10/21 16:12 6020BMMR
11.8 mg/Kg - dry 0.0942 1.24
Lead 10 03/10/21 16:12 6020BMMR
0.0723 mg/Kg - dry 0.0186 0.0620Mercury (Total)1 03/10/21 12:47 7471BEDV
2.93 mg/Kg - dry 0.285 1.24Selenium 10 03/10/21 16:12 6020BMMR
<0.0632 mg/Kg - dry 0.0632 0.620Silver 10 03/10/21 16:12 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 7 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-1
94144 Matrix:
3/8/2021 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.018 mg/Kg - dry 0.018 0.818Acenaphthene 1 03/10/21 16:19 V1707JMV
<0.016 mg/Kg - dry 0.016 0.818Acenaphthylene 1 03/10/21 16:19 V1707JMV
<0.202 mg/Kg - dry 0.202 0.818Aniline 1 03/10/21 16:19 V1707JMV
<0.009 mg/Kg - dry 0.009 0.818Anthracene 1 03/10/21 16:19 V1707JMV
0.026 J mg/Kg - dry 0.009 0.818Benzo(a)anthracene 1 03/10/21 16:19 V1707JMV
0.021 J mg/Kg - dry 0.007 0.818Benzo(a)pyrene 1 03/10/21 16:19 V1707JMV
<0.007 mg/Kg - dry 0.007 0.818Benzo(b)fluoranthene 1 03/10/21 16:19 V1707JMV
<0.008 mg/Kg - dry 0.008 0.818Benzo(g,h,i)perylene 1 03/10/21 16:19 V1707JMV
<0.008 mg/Kg - dry 0.008 0.818
Benzo(k)fluoranthene 1 03/10/21 16:19 V1707JMV
<0.679 mg/Kg - dry 0.679 2.48Benzoic Acid 1 03/10/21 16:19 V1707JMV
<0.153 mg/Kg - dry 0.153 0.818Benzyl alcohol 1 03/10/21 16:19 V1707JMV
<0.156 mg/Kg - dry 0.156 0.818Bis(2-Chloroethoxy)methane 1 03/10/21 16:19 V1707JMV
<0.131 mg/Kg - dry 0.131 0.818Bis(2-Chloroethyl)ether 1 03/10/21 16:19 V1707JMV
<0.146 mg/Kg - dry 0.146 0.409Bis(2-Chloroisopropyl)ether 1 03/10/21 16:19 V1707JMV
<0.184 mg/Kg - dry 0.184 0.818Bis(2-ethylhexyl)phthalate 1 03/10/21 16:19 V1707JMV
<0.192 mg/Kg - dry 0.192 0.818
4-Bromophenyl phenyl ether 1 03/10/21 16:19 V1707JMV
<0.141 mg/Kg - dry 0.141 0.409Butyl benzyl phthalate 1 03/10/21 16:19 V1707JMV
<0.156 mg/Kg - dry 0.156 0.8184-Chloro-3-methylphenol 1 03/10/21 16:19 V1707JMV
<0.099 mg/Kg - dry 0.099 0.4094-Chloroaniline 1 03/10/21 16:19 V1707JMV
<0.199 mg/Kg - dry 0.199 0.8182-Chloronaphthalene 1 03/10/21 16:19 V1707JMV
<0.156 mg/Kg - dry 0.156 0.8182-Chlorophenol 1 03/10/21 16:19 V1707JMV
<0.250 mg/Kg - dry 0.250 1.244-Chlorophenyl phenyl ether 1 03/10/21 16:19 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-1
94144 Matrix:
3/8/2021 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.009 mg/Kg - dry 0.009 0.818Chrysene 1 03/10/21 16:19 V1707JMV
<0.023 mg/Kg - dry 0.023 0.818Dibenz(a,h)anthracene 1 03/10/21 16:19 V1707JMV
<0.022 mg/Kg - dry 0.022 0.818Dibenzofuran 1 03/10/21 16:19 V1707JMV
<0.132 mg/Kg - dry 0.132 0.8181,2-Dichlorobenzene 1 03/10/21 16:19 V1707JMV
<0.120 mg/Kg - dry 0.120 0.8181,3-Dichlorobenzene 1 03/10/21 16:19 V1707JMV
<0.129 mg/Kg - dry 0.129 0.4091,4-Dichlorobenzene 1 03/10/21 16:19 V1707JMV
<0.162 mg/Kg - dry 0.162 0.8183,3'-Dichlorobenzidine 1 03/10/21 16:19 V1707JMV
<0.160 mg/Kg - dry 0.160 0.8182,4-Dichlorophenol 1 03/10/21 16:19 V1707JMV
<0.210 mg/Kg - dry 0.210 0.818
Diethyl phthalate 1 03/10/21 16:19 V1707JMV
<0.196 mg/Kg - dry 0.196 0.818Dimethyl phthalate 1 03/10/21 16:19 V1707JMV
<0.169 mg/Kg - dry 0.169 0.4092,4-Dimethylphenol 1 03/10/21 16:19 V1707JMV
<0.203 mg/Kg - dry 0.203 0.818Di-n-butyl phthalate 1 03/10/21 16:19 V1707JMV
<0.451 mg/Kg - dry 0.451 1.864,6-Dinitro-2-methylphenol 1 03/10/21 16:19 V1707JMV
<0.480 mg/Kg - dry 0.480 1.862,4-Dinitrophenol 1 03/10/21 16:19 V1707JMV
<0.217 mg/Kg - dry 0.217 0.8182,4-Dinitrotoluene 1 03/10/21 16:19 V1707JMV
<0.212 mg/Kg - dry 0.212 0.818
2,6-Dinitrotoluene 1 03/10/21 16:19 V1707JMV
<0.212 mg/Kg - dry 0.212 0.409Di-n-Octyl Phthalate 1 03/10/21 16:19 V1707JMV
<0.009 mg/Kg - dry 0.009 0.818Fluoranthene 1 03/10/21 16:19 V1707JMV
<0.017 mg/Kg - dry 0.017 0.818Fluorene 1 03/10/21 16:19 V1707JMV
<0.179 mg/Kg - dry 0.179 0.818Hexachlorobenzene 1 03/10/21 16:19 V1707JMV
<0.184 mg/Kg - dry 0.184 0.818Hexachlorobutadiene 1 03/10/21 16:19 V1707JMV
<0.281 mg/Kg - dry 0.281 0.818Hexachlorocyclopentadiene 1 03/10/21 16:19 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-1
94144 Matrix:
3/8/2021 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.129 mg/Kg - dry 0.129 0.818Hexachloroethane 1 03/10/21 16:19 V1707JMV
<0.023 mg/Kg - dry 0.023 0.818Indeno(1,2,3-cd)pyrene 1 03/10/21 16:19 V1707JMV
<0.176 mg/Kg - dry 0.176 0.818Isophorone 1 03/10/21 16:19 V1707JMV
<0.012 mg/Kg - dry 0.012 0.8181-Methylnaphthalene 1 03/10/21 16:19 V1707JMV
<0.015 mg/Kg - dry 0.015 0.8182-Methylnaphthalene 1 03/10/21 16:19 V1707JMV
<0.156 mg/Kg - dry 0.156 0.8182-Methylphenol 1 03/10/21 16:19 V1707JMV
<0.177 mg/Kg - dry 0.177 0.8183&4 Methylphenol 1 03/10/21 16:19 V1707JMV
<0.017 mg/Kg - dry 0.017 0.818Naphthalene 1 03/10/21 16:19 V1707JMV
<0.176 mg/Kg - dry 0.176 0.818
2-Nitroaniline 1 03/10/21 16:19 V1707JMV
<0.148 mg/Kg - dry 0.148 0.8183-Nitroaniline 1 03/10/21 16:19 V1707JMV
<0.127 mg/Kg - dry 0.127 0.4094-Nitroaniline 1 03/10/21 16:19 V1707JMV
<0.173 mg/Kg - dry 0.173 0.409Nitrobenzene 1 03/10/21 16:19 V1707JMV
<0.136 mg/Kg - dry 0.136 0.8182-Nitrophenol 1 03/10/21 16:19 V1707JMV
<0.202 mg/Kg - dry 0.202 0.8184-Nitrophenol 1 03/10/21 16:19 V1707JMV
<0.006 mg/Kg - dry 0.006 0.210N-Nitrosodimethylamine 1 03/10/21 16:19 V1707JMV
<0.224 mg/Kg - dry 0.224 0.818
N-Nitrosodiphenylamine 1 03/10/21 16:19 V1707JMV
<0.188 mg/Kg - dry 0.188 0.818N-Nitroso-di-n-propylamine 1 03/10/21 16:19 V1707JMV
<0.522 mg/Kg - dry 0.522 1.24Pentachlorophenol 1 03/10/21 16:19 V1707JMV
<0.008 mg/Kg - dry 0.008 0.818Phenanthrene 1 03/10/21 16:19 V1707JMV
<0.133 mg/Kg - dry 0.133 0.818Phenol 1 03/10/21 16:19 V1707JMV
<0.011 mg/Kg - dry 0.011 0.818Pyrene 1 03/10/21 16:19 V1707JMV
<0.078 mg/Kg - dry 0.078 0.409Pyridine 1 03/10/21 16:19 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-1
94144 Matrix:
3/8/2021 12:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.145 mg/Kg - dry 0.145 0.8181,2,4-Trichlorobenzene 1 03/10/21 16:19 V1707JMV
<0.173 mg/Kg - dry 0.173 0.8182,4,5-Trichlorophenol 1 03/10/21 16:19 V1707JMV
<0.198 mg/Kg - dry 0.198 0.8182,4,6-Trichlorophenol 1 03/10/21 16:19 V1707JMV
Surrogate: 2-Fluorobiphenyl 89.2 Limits: 44-115%03/10/21 16:191 JMV V1707
Surrogate: 2-Fluorophenol 72.4 Limits: 35-115%03/10/21 16:191 JMV V1707
Surrogate: Nitrobenzene-d5 80.7 Limits: 37-122%03/10/21 16:191 JMV V1707
Surrogate: 4-Terphenyl-d14 94.0 Limits: 54-127%03/10/21 16:191 JMV V1707
Surrogate: 2,4,6-Tribromophenol 72.1 Limits: 39-132%03/10/21 16:191 JMV V1707
Surrogate: Phenol-d5 73.9 Limits: 34-121%03/10/21 16:191 JMV V1707
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-2
94145 Matrix:
3/8/2021 14:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.1 %Moisture 1 03/09/21 15:20 SW-DRYWTEDV
3.39 mg/Kg - dry 0.105 0.125Arsenic 10 03/10/21 16:19 6020BMMR
65.5 mg/Kg - dry 0.450 12.5Barium 10 03/10/21 16:19 6020BMMR
<0.0463 mg/Kg - dry 0.0463 0.626Cadmium 10 03/10/21 16:19 6020BMMR
58.6 mg/Kg - dry 0.300 1.25Chromium 10 03/10/21 16:19 6020BMMR
19.0 mg/Kg - dry 0.0951 1.25
Lead 10 03/10/21 16:19 6020BMMR
0.107 mg/Kg - dry 0.0188 0.0626Mercury (Total)1 03/10/21 12:51 7471BEDV
2.44 mg/Kg - dry 0.287 1.25Selenium 10 03/10/21 16:19 6020BMMR
<0.0638 mg/Kg - dry 0.0638 0.626Silver 10 03/10/21 16:19 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 12 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-2
94145 Matrix:
3/8/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.018 mg/Kg - dry 0.018 0.826Acenaphthene 1 03/10/21 16:41 V1707JMV
<0.016 mg/Kg - dry 0.016 0.826Acenaphthylene 1 03/10/21 16:41 V1707JMV
<0.204 mg/Kg - dry 0.204 0.826Aniline 1 03/10/21 16:41 V1707JMV
<0.009 mg/Kg - dry 0.009 0.826Anthracene 1 03/10/21 16:41 V1707JMV
<0.009 mg/Kg - dry 0.009 0.826Benzo(a)anthracene 1 03/10/21 16:41 V1707JMV
<0.007 mg/Kg - dry 0.007 0.826Benzo(a)pyrene 1 03/10/21 16:41 V1707JMV
<0.007 mg/Kg - dry 0.007 0.826Benzo(b)fluoranthene 1 03/10/21 16:41 V1707JMV
<0.008 mg/Kg - dry 0.008 0.826Benzo(g,h,i)perylene 1 03/10/21 16:41 V1707JMV
<0.008 mg/Kg - dry 0.008 0.826
Benzo(k)fluoranthene 1 03/10/21 16:41 V1707JMV
<0.685 mg/Kg - dry 0.685 2.50Benzoic Acid 1 03/10/21 16:41 V1707JMV
<0.155 mg/Kg - dry 0.155 0.826Benzyl alcohol 1 03/10/21 16:41 V1707JMV
<0.157 mg/Kg - dry 0.157 0.826Bis(2-Chloroethoxy)methane 1 03/10/21 16:41 V1707JMV
<0.132 mg/Kg - dry 0.132 0.826Bis(2-Chloroethyl)ether 1 03/10/21 16:41 V1707JMV
<0.147 mg/Kg - dry 0.147 0.413Bis(2-Chloroisopropyl)ether 1 03/10/21 16:41 V1707JMV
<0.186 mg/Kg - dry 0.186 0.826Bis(2-ethylhexyl)phthalate 1 03/10/21 16:41 V1707JMV
<0.193 mg/Kg - dry 0.193 0.826
4-Bromophenyl phenyl ether 1 03/10/21 16:41 V1707JMV
<0.142 mg/Kg - dry 0.142 0.413Butyl benzyl phthalate 1 03/10/21 16:41 V1707JMV
<0.157 mg/Kg - dry 0.157 0.8264-Chloro-3-methylphenol 1 03/10/21 16:41 V1707JMV
<0.100 mg/Kg - dry 0.100 0.4134-Chloroaniline 1 03/10/21 16:41 V1707JMV
<0.201 mg/Kg - dry 0.201 0.8262-Chloronaphthalene 1 03/10/21 16:41 V1707JMV
<0.157 mg/Kg - dry 0.157 0.8262-Chlorophenol 1 03/10/21 16:41 V1707JMV
<0.252 mg/Kg - dry 0.252 1.254-Chlorophenyl phenyl ether 1 03/10/21 16:41 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-2
94145 Matrix:
3/8/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.009 mg/Kg - dry 0.009 0.826Chrysene 1 03/10/21 16:41 V1707JMV
<0.023 mg/Kg - dry 0.023 0.826Dibenz(a,h)anthracene 1 03/10/21 16:41 V1707JMV
<0.022 mg/Kg - dry 0.022 0.826Dibenzofuran 1 03/10/21 16:41 V1707JMV
<0.133 mg/Kg - dry 0.133 0.8261,2-Dichlorobenzene 1 03/10/21 16:41 V1707JMV
<0.121 mg/Kg - dry 0.121 0.8261,3-Dichlorobenzene 1 03/10/21 16:41 V1707JMV
<0.130 mg/Kg - dry 0.130 0.4131,4-Dichlorobenzene 1 03/10/21 16:41 V1707JMV
<0.163 mg/Kg - dry 0.163 0.8263,3'-Dichlorobenzidine 1 03/10/21 16:41 V1707JMV
<0.161 mg/Kg - dry 0.161 0.8262,4-Dichlorophenol 1 03/10/21 16:41 V1707JMV
<0.212 mg/Kg - dry 0.212 0.826
Diethyl phthalate 1 03/10/21 16:41 V1707JMV
<0.197 mg/Kg - dry 0.197 0.826Dimethyl phthalate 1 03/10/21 16:41 V1707JMV
<0.171 mg/Kg - dry 0.171 0.4132,4-Dimethylphenol 1 03/10/21 16:41 V1707JMV
<0.205 mg/Kg - dry 0.205 0.826Di-n-butyl phthalate 1 03/10/21 16:41 V1707JMV
<0.455 mg/Kg - dry 0.455 1.884,6-Dinitro-2-methylphenol 1 03/10/21 16:41 V1707JMV
<0.484 mg/Kg - dry 0.484 1.882,4-Dinitrophenol 1 03/10/21 16:41 V1707JMV
<0.219 mg/Kg - dry 0.219 0.8262,4-Dinitrotoluene 1 03/10/21 16:41 V1707JMV
<0.214 mg/Kg - dry 0.214 0.826
2,6-Dinitrotoluene 1 03/10/21 16:41 V1707JMV
<0.214 mg/Kg - dry 0.214 0.413Di-n-Octyl Phthalate 1 03/10/21 16:41 V1707JMV
<0.009 mg/Kg - dry 0.009 0.826Fluoranthene 1 03/10/21 16:41 V1707JMV
<0.018 mg/Kg - dry 0.018 0.826Fluorene 1 03/10/21 16:41 V1707JMV
<0.181 mg/Kg - dry 0.181 0.826Hexachlorobenzene 1 03/10/21 16:41 V1707JMV
<0.186 mg/Kg - dry 0.186 0.826Hexachlorobutadiene 1 03/10/21 16:41 V1707JMV
<0.284 mg/Kg - dry 0.284 0.826Hexachlorocyclopentadiene 1 03/10/21 16:41 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-2
94145 Matrix:
3/8/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.130 mg/Kg - dry 0.130 0.826Hexachloroethane 1 03/10/21 16:41 V1707JMV
<0.023 mg/Kg - dry 0.023 0.826Indeno(1,2,3-cd)pyrene 1 03/10/21 16:41 V1707JMV
<0.177 mg/Kg - dry 0.177 0.826Isophorone 1 03/10/21 16:41 V1707JMV
<0.012 mg/Kg - dry 0.012 0.8261-Methylnaphthalene 1 03/10/21 16:41 V1707JMV
<0.016 mg/Kg - dry 0.016 0.8262-Methylnaphthalene 1 03/10/21 16:41 V1707JMV
<0.157 mg/Kg - dry 0.157 0.8262-Methylphenol 1 03/10/21 16:41 V1707JMV
<0.178 mg/Kg - dry 0.178 0.8263&4 Methylphenol 1 03/10/21 16:41 V1707JMV
<0.017 mg/Kg - dry 0.017 0.826Naphthalene 1 03/10/21 16:41 V1707JMV
<0.177 mg/Kg - dry 0.177 0.826
2-Nitroaniline 1 03/10/21 16:41 V1707JMV
<0.150 mg/Kg - dry 0.150 0.8263-Nitroaniline 1 03/10/21 16:41 V1707JMV
<0.128 mg/Kg - dry 0.128 0.4134-Nitroaniline 1 03/10/21 16:41 V1707JMV
<0.175 mg/Kg - dry 0.175 0.413Nitrobenzene 1 03/10/21 16:41 V1707JMV
<0.137 mg/Kg - dry 0.137 0.8262-Nitrophenol 1 03/10/21 16:41 V1707JMV
<0.204 mg/Kg - dry 0.204 0.8264-Nitrophenol 1 03/10/21 16:41 V1707JMV
<0.007 mg/Kg - dry 0.007 0.212N-Nitrosodimethylamine 1 03/10/21 16:41 V1707JMV
<0.226 mg/Kg - dry 0.226 0.826
N-Nitrosodiphenylamine 1 03/10/21 16:41 V1707JMV
<0.190 mg/Kg - dry 0.190 0.826N-Nitroso-di-n-propylamine 1 03/10/21 16:41 V1707JMV
<0.526 mg/Kg - dry 0.526 1.25Pentachlorophenol 1 03/10/21 16:41 V1707JMV
<0.009 mg/Kg - dry 0.009 0.826Phenanthrene 1 03/10/21 16:41 V1707JMV
<0.135 mg/Kg - dry 0.135 0.826Phenol 1 03/10/21 16:41 V1707JMV
<0.012 mg/Kg - dry 0.012 0.826Pyrene 1 03/10/21 16:41 V1707JMV
<0.078 mg/Kg - dry 0.078 0.413Pyridine 1 03/10/21 16:41 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-2
94145 Matrix:
3/8/2021 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.146 mg/Kg - dry 0.146 0.8261,2,4-Trichlorobenzene 1 03/10/21 16:41 V1707JMV
<0.175 mg/Kg - dry 0.175 0.8262,4,5-Trichlorophenol 1 03/10/21 16:41 V1707JMV
<0.200 mg/Kg - dry 0.200 0.8262,4,6-Trichlorophenol 1 03/10/21 16:41 V1707JMV
Surrogate: 2-Fluorobiphenyl 99.4 Limits: 44-115%03/10/21 16:411 JMV V1707
Surrogate: 2-Fluorophenol 79.9 Limits: 35-115%03/10/21 16:411 JMV V1707
Surrogate: Nitrobenzene-d5 91.6 Limits: 37-122%03/10/21 16:411 JMV V1707
Surrogate: 4-Terphenyl-d14 102 Limits: 54-127%03/10/21 16:411 JMV V1707
Surrogate: 2,4,6-Tribromophenol 78.1 Limits: 39-132%03/10/21 16:411 JMV V1707
Surrogate: Phenol-d5 80.5 Limits: 34-121%03/10/21 16:411 JMV V1707
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-3
94146 Matrix:
3/8/2021 9:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.8 %Moisture 1 03/09/21 15:20 SW-DRYWTEDV
12.8 mg/Kg - dry 0.103 0.123Arsenic 10 03/10/21 16:25 6020BMMR
81.2 mg/Kg - dry 0.443 12.3Barium 10 03/10/21 16:25 6020BMMR
0.0935 J mg/Kg - dry 0.0455 0.616Cadmium 10 03/10/21 16:25 6020BMMR
42.9 mg/Kg - dry 0.295 1.23Chromium 10 03/10/21 16:25 6020BMMR
46.1 mg/Kg - dry 0.0935 1.23
Lead 10 03/10/21 16:25 6020BMMR
0.116 mg/Kg - dry 0.0185 0.0616Mercury (Total)1 03/10/21 12:56 7471BEDV
2.29 mg/Kg - dry 0.283 1.23Selenium 10 03/10/21 16:25 6020BMMR
0.0717 J mg/Kg - dry 0.0628 0.616Silver 10 03/10/21 16:25 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 17 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-3
94146 Matrix:
3/8/2021 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.018 mg/Kg - dry 0.018 0.812Acenaphthene 1 03/10/21 17:03 V1707JMV
<0.016 mg/Kg - dry 0.016 0.812Acenaphthylene 1 03/10/21 17:03 V1707JMV
<0.200 mg/Kg - dry 0.200 0.812Aniline 1 03/10/21 17:03 V1707JMV
<0.008 mg/Kg - dry 0.008 0.812Anthracene 1 03/10/21 17:03 V1707JMV
0.023 J mg/Kg - dry 0.009 0.812Benzo(a)anthracene 1 03/10/21 17:03 V1707JMV
0.021 J mg/Kg - dry 0.007 0.812Benzo(a)pyrene 1 03/10/21 17:03 V1707JMV
0.034 J mg/Kg - dry 0.007 0.812Benzo(b)fluoranthene 1 03/10/21 17:03 V1707JMV
<0.008 mg/Kg - dry 0.008 0.812Benzo(g,h,i)perylene 1 03/10/21 17:03 V1707JMV
<0.008 mg/Kg - dry 0.008 0.812
Benzo(k)fluoranthene 1 03/10/21 17:03 V1707JMV
<0.674 mg/Kg - dry 0.674 2.46Benzoic Acid 1 03/10/21 17:03 V1707JMV
<0.152 mg/Kg - dry 0.152 0.812Benzyl alcohol 1 03/10/21 17:03 V1707JMV
<0.155 mg/Kg - dry 0.155 0.812Bis(2-Chloroethoxy)methane 1 03/10/21 17:03 V1707JMV
<0.130 mg/Kg - dry 0.130 0.812Bis(2-Chloroethyl)ether 1 03/10/21 17:03 V1707JMV
<0.145 mg/Kg - dry 0.145 0.406Bis(2-Chloroisopropyl)ether 1 03/10/21 17:03 V1707JMV
<0.183 mg/Kg - dry 0.183 0.812Bis(2-ethylhexyl)phthalate 1 03/10/21 17:03 V1707JMV
<0.190 mg/Kg - dry 0.190 0.812
4-Bromophenyl phenyl ether 1 03/10/21 17:03 V1707JMV
<0.140 mg/Kg - dry 0.140 0.406Butyl benzyl phthalate 1 03/10/21 17:03 V1707JMV
<0.155 mg/Kg - dry 0.155 0.8124-Chloro-3-methylphenol 1 03/10/21 17:03 V1707JMV
<0.098 mg/Kg - dry 0.098 0.4064-Chloroaniline 1 03/10/21 17:03 V1707JMV
<0.198 mg/Kg - dry 0.198 0.8122-Chloronaphthalene 1 03/10/21 17:03 V1707JMV
<0.155 mg/Kg - dry 0.155 0.8122-Chlorophenol 1 03/10/21 17:03 V1707JMV
<0.248 mg/Kg - dry 0.248 1.234-Chlorophenyl phenyl ether 1 03/10/21 17:03 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-3
94146 Matrix:
3/8/2021 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
0.022 J mg/Kg - dry 0.009 0.812Chrysene 1 03/10/21 17:03 V1707JMV
<0.023 mg/Kg - dry 0.023 0.812Dibenz(a,h)anthracene 1 03/10/21 17:03 V1707JMV
<0.021 mg/Kg - dry 0.021 0.812Dibenzofuran 1 03/10/21 17:03 V1707JMV
<0.131 mg/Kg - dry 0.131 0.8121,2-Dichlorobenzene 1 03/10/21 17:03 V1707JMV
<0.119 mg/Kg - dry 0.119 0.8121,3-Dichlorobenzene 1 03/10/21 17:03 V1707JMV
<0.128 mg/Kg - dry 0.128 0.4061,4-Dichlorobenzene 1 03/10/21 17:03 V1707JMV
<0.161 mg/Kg - dry 0.161 0.8123,3'-Dichlorobenzidine 1 03/10/21 17:03 V1707JMV
<0.158 mg/Kg - dry 0.158 0.8122,4-Dichlorophenol 1 03/10/21 17:03 V1707JMV
<0.209 mg/Kg - dry 0.209 0.812
Diethyl phthalate 1 03/10/21 17:03 V1707JMV
<0.194 mg/Kg - dry 0.194 0.812Dimethyl phthalate 1 03/10/21 17:03 V1707JMV
<0.168 mg/Kg - dry 0.168 0.4062,4-Dimethylphenol 1 03/10/21 17:03 V1707JMV
<0.201 mg/Kg - dry 0.201 0.812Di-n-butyl phthalate 1 03/10/21 17:03 V1707JMV
<0.448 mg/Kg - dry 0.448 1.854,6-Dinitro-2-methylphenol 1 03/10/21 17:03 V1707JMV
<0.476 mg/Kg - dry 0.476 1.852,4-Dinitrophenol 1 03/10/21 17:03 V1707JMV
<0.215 mg/Kg - dry 0.215 0.8122,4-Dinitrotoluene 1 03/10/21 17:03 V1707JMV
<0.210 mg/Kg - dry 0.210 0.812
2,6-Dinitrotoluene 1 03/10/21 17:03 V1707JMV
<0.210 mg/Kg - dry 0.210 0.406Di-n-Octyl Phthalate 1 03/10/21 17:03 V1707JMV
0.033 J mg/Kg - dry 0.009 0.812Fluoranthene 1 03/10/21 17:03 V1707JMV
<0.017 mg/Kg - dry 0.017 0.812Fluorene 1 03/10/21 17:03 V1707JMV
<0.178 mg/Kg - dry 0.178 0.812Hexachlorobenzene 1 03/10/21 17:03 V1707JMV
<0.183 mg/Kg - dry 0.183 0.812Hexachlorobutadiene 1 03/10/21 17:03 V1707JMV
<0.279 mg/Kg - dry 0.279 0.812Hexachlorocyclopentadiene 1 03/10/21 17:03 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-3
94146 Matrix:
3/8/2021 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.128 mg/Kg - dry 0.128 0.812Hexachloroethane 1 03/10/21 17:03 V1707JMV
<0.022 mg/Kg - dry 0.022 0.812Indeno(1,2,3-cd)pyrene 1 03/10/21 17:03 V1707JMV
<0.174 mg/Kg - dry 0.174 0.812Isophorone 1 03/10/21 17:03 V1707JMV
<0.012 mg/Kg - dry 0.012 0.8121-Methylnaphthalene 1 03/10/21 17:03 V1707JMV
<0.015 mg/Kg - dry 0.015 0.8122-Methylnaphthalene 1 03/10/21 17:03 V1707JMV
<0.155 mg/Kg - dry 0.155 0.8122-Methylphenol 1 03/10/21 17:03 V1707JMV
<0.176 mg/Kg - dry 0.176 0.8123&4 Methylphenol 1 03/10/21 17:03 V1707JMV
<0.017 mg/Kg - dry 0.017 0.812Naphthalene 1 03/10/21 17:03 V1707JMV
<0.174 mg/Kg - dry 0.174 0.812
2-Nitroaniline 1 03/10/21 17:03 V1707JMV
<0.147 mg/Kg - dry 0.147 0.8123-Nitroaniline 1 03/10/21 17:03 V1707JMV
<0.126 mg/Kg - dry 0.126 0.4064-Nitroaniline 1 03/10/21 17:03 V1707JMV
<0.172 mg/Kg - dry 0.172 0.406Nitrobenzene 1 03/10/21 17:03 V1707JMV
<0.135 mg/Kg - dry 0.135 0.8122-Nitrophenol 1 03/10/21 17:03 V1707JMV
<0.200 mg/Kg - dry 0.200 0.8124-Nitrophenol 1 03/10/21 17:03 V1707JMV
<0.006 mg/Kg - dry 0.006 0.209N-Nitrosodimethylamine 1 03/10/21 17:03 V1707JMV
<0.222 mg/Kg - dry 0.222 0.812
N-Nitrosodiphenylamine 1 03/10/21 17:03 V1707JMV
<0.187 mg/Kg - dry 0.187 0.812N-Nitroso-di-n-propylamine 1 03/10/21 17:03 V1707JMV
<0.518 mg/Kg - dry 0.518 1.23Pentachlorophenol 1 03/10/21 17:03 V1707JMV
<0.008 mg/Kg - dry 0.008 0.812Phenanthrene 1 03/10/21 17:03 V1707JMV
<0.133 mg/Kg - dry 0.133 0.812Phenol 1 03/10/21 17:03 V1707JMV
0.038 J mg/Kg - dry 0.011 0.812Pyrene 1 03/10/21 17:03 V1707JMV
<0.077 mg/Kg - dry 0.077 0.406Pyridine 1 03/10/21 17:03 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-3
94146 Matrix:
3/8/2021 9:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.144 mg/Kg - dry 0.144 0.8121,2,4-Trichlorobenzene 1 03/10/21 17:03 V1707JMV
<0.172 mg/Kg - dry 0.172 0.8122,4,5-Trichlorophenol 1 03/10/21 17:03 V1707JMV
<0.197 mg/Kg - dry 0.197 0.8122,4,6-Trichlorophenol 1 03/10/21 17:03 V1707JMV
Surrogate: 2-Fluorobiphenyl 103 Limits: 44-115%03/10/21 17:031 JMV V1707
Surrogate: 2-Fluorophenol 81.4 Limits: 35-115%03/10/21 17:031 JMV V1707
Surrogate: Nitrobenzene-d5 93.4 Limits: 37-122%03/10/21 17:031 JMV V1707
Surrogate: 4-Terphenyl-d14 103 Limits: 54-127%03/10/21 17:031 JMV V1707
Surrogate: 2,4,6-Tribromophenol 79.0 Limits: 39-132%03/10/21 17:031 JMV V1707
Surrogate: Phenol-d5 83.2 Limits: 34-121%03/10/21 17:031 JMV V1707
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-4
94147 Matrix:
3/8/2021 11:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.0 %Moisture 1 03/09/21 15:20 SW-DRYWTEDV
16.5 mg/Kg - dry 0.102 0.122Arsenic 10 03/10/21 16:32 6020BMMR
123 mg/Kg - dry 0.439 12.2Barium 10 03/10/21 16:32 6020BMMR
0.226 J mg/Kg - dry 0.0451 0.610Cadmium 10 03/10/21 16:32 6020BMMR
44.9 mg/Kg - dry 0.292 1.22Chromium 10 03/10/21 16:32 6020BMMR
78.7 mg/Kg - dry 0.0926 1.22
Lead 10 03/10/21 16:32 6020BMMR
0.0860 mg/Kg - dry 0.0183 0.0610Mercury (Total)1 03/10/21 13:01 7471BEDV
2.32 mg/Kg - dry 0.280 1.22Selenium 10 03/10/21 16:32 6020BMMR
0.0784 J mg/Kg - dry 0.0621 0.610Silver 10 03/10/21 16:32 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 22 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-4
94147 Matrix:
3/8/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.018 mg/Kg - dry 0.018 0.804Acenaphthene 1 03/10/21 17:26 V1707JMV
0.026 J mg/Kg - dry 0.015 0.804Acenaphthylene 1 03/10/21 17:26 V1707JMV
<0.198 mg/Kg - dry 0.198 0.804Aniline 1 03/10/21 17:26 V1707JMV
0.028 J mg/Kg - dry 0.008 0.804Anthracene 1 03/10/21 17:26 V1707JMV
0.113 J mg/Kg - dry 0.009 0.804Benzo(a)anthracene 1 03/10/21 17:26 V1707JMV
0.143 J mg/Kg - dry 0.007 0.804Benzo(a)pyrene 1 03/10/21 17:26 V1707JMV
0.219 J mg/Kg - dry 0.007 0.804Benzo(b)fluoranthene 1 03/10/21 17:26 V1707JMV
0.123 J mg/Kg - dry 0.007 0.804Benzo(g,h,i)perylene 1 03/10/21 17:26 V1707JMV
0.075 J
mg/Kg - dry 0.008 0.804
Benzo(k)fluoranthene 1 03/10/21 17:26 V1707JMV
<0.668 mg/Kg - dry 0.668 2.44Benzoic Acid 1 03/10/21 17:26 V1707JMV
<0.151 mg/Kg - dry 0.151 0.804Benzyl alcohol 1 03/10/21 17:26 V1707JMV
<0.153 mg/Kg - dry 0.153 0.804Bis(2-Chloroethoxy)methane 1 03/10/21 17:26 V1707JMV
<0.129 mg/Kg - dry 0.129 0.804Bis(2-Chloroethyl)ether 1 03/10/21 17:26 V1707JMV
<0.143 mg/Kg - dry 0.143 0.402Bis(2-Chloroisopropyl)ether 1 03/10/21 17:26 V1707JMV
<0.181 mg/Kg - dry 0.181 0.804Bis(2-ethylhexyl)phthalate 1 03/10/21 17:26 V1707JMV
<0.189 mg/Kg - dry 0.189 0.804
4-Bromophenyl phenyl ether 1 03/10/21 17:26 V1707JMV
<0.139 mg/Kg - dry 0.139 0.402Butyl benzyl phthalate 1 03/10/21 17:26 V1707JMV
<0.153 mg/Kg - dry 0.153 0.8044-Chloro-3-methylphenol 1 03/10/21 17:26 V1707JMV
<0.097 mg/Kg - dry 0.097 0.4024-Chloroaniline 1 03/10/21 17:26 V1707JMV
<0.196 mg/Kg - dry 0.196 0.8042-Chloronaphthalene 1 03/10/21 17:26 V1707JMV
<0.153 mg/Kg - dry 0.153 0.8042-Chlorophenol 1 03/10/21 17:26 V1707JMV
<0.246 mg/Kg - dry 0.246 1.224-Chlorophenyl phenyl ether 1 03/10/21 17:26 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-4
94147 Matrix:
3/8/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
0.154 J mg/Kg - dry 0.009 0.804Chrysene 1 03/10/21 17:26 V1707JMV
<0.023 mg/Kg - dry 0.023 0.804Dibenz(a,h)anthracene 1 03/10/21 17:26 V1707JMV
<0.021 mg/Kg - dry 0.021 0.804Dibenzofuran 1 03/10/21 17:26 V1707JMV
<0.130 mg/Kg - dry 0.130 0.8041,2-Dichlorobenzene 1 03/10/21 17:26 V1707JMV
<0.118 mg/Kg - dry 0.118 0.8041,3-Dichlorobenzene 1 03/10/21 17:26 V1707JMV
<0.126 mg/Kg - dry 0.126 0.4021,4-Dichlorobenzene 1 03/10/21 17:26 V1707JMV
<0.159 mg/Kg - dry 0.159 0.8043,3'-Dichlorobenzidine 1 03/10/21 17:26 V1707JMV
<0.157 mg/Kg - dry 0.157 0.8042,4-Dichlorophenol 1 03/10/21 17:26 V1707JMV
<0.207 mg/Kg - dry 0.207 0.804
Diethyl phthalate 1 03/10/21 17:26 V1707JMV
<0.192 mg/Kg - dry 0.192 0.804Dimethyl phthalate 1 03/10/21 17:26 V1707JMV
<0.167 mg/Kg - dry 0.167 0.4022,4-Dimethylphenol 1 03/10/21 17:26 V1707JMV
<0.200 mg/Kg - dry 0.200 0.804Di-n-butyl phthalate 1 03/10/21 17:26 V1707JMV
<0.443 mg/Kg - dry 0.443 1.834,6-Dinitro-2-methylphenol 1 03/10/21 17:26 V1707JMV
<0.471 mg/Kg - dry 0.471 1.832,4-Dinitrophenol 1 03/10/21 17:26 V1707JMV
<0.213 mg/Kg - dry 0.213 0.8042,4-Dinitrotoluene 1 03/10/21 17:26 V1707JMV
<0.208 mg/Kg - dry 0.208 0.804
2,6-Dinitrotoluene 1 03/10/21 17:26 V1707JMV
<0.208 mg/Kg - dry 0.208 0.402Di-n-Octyl Phthalate 1 03/10/21 17:26 V1707JMV
0.274 J mg/Kg - dry 0.009 0.804Fluoranthene 1 03/10/21 17:26 V1707JMV
<0.017 mg/Kg - dry 0.017 0.804Fluorene 1 03/10/21 17:26 V1707JMV
<0.176 mg/Kg - dry 0.176 0.804Hexachlorobenzene 1 03/10/21 17:26 V1707JMV
<0.181 mg/Kg - dry 0.181 0.804Hexachlorobutadiene 1 03/10/21 17:26 V1707JMV
<0.276 mg/Kg - dry 0.276 0.804Hexachlorocyclopentadiene 1 03/10/21 17:26 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-4
94147 Matrix:
3/8/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.126 mg/Kg - dry 0.126 0.804Hexachloroethane 1 03/10/21 17:26 V1707JMV
0.128 J mg/Kg - dry 0.022 0.804Indeno(1,2,3-cd)pyrene 1 03/10/21 17:26 V1707JMV
<0.173 mg/Kg - dry 0.173 0.804Isophorone 1 03/10/21 17:26 V1707JMV
0.020 J mg/Kg - dry 0.012 0.8041-Methylnaphthalene 1 03/10/21 17:26 V1707JMV
0.024 J mg/Kg - dry 0.015 0.8042-Methylnaphthalene 1 03/10/21 17:26 V1707JMV
<0.153 mg/Kg - dry 0.153 0.8042-Methylphenol 1 03/10/21 17:26 V1707JMV
<0.174 mg/Kg - dry 0.174 0.8043&4 Methylphenol 1 03/10/21 17:26 V1707JMV
0.022 J mg/Kg - dry 0.017 0.804Naphthalene 1 03/10/21 17:26 V1707JMV
<0.173 mg/Kg - dry 0.173 0.804
2-Nitroaniline 1 03/10/21 17:26 V1707JMV
<0.146 mg/Kg - dry 0.146 0.8043-Nitroaniline 1 03/10/21 17:26 V1707JMV
<0.125 mg/Kg - dry 0.125 0.4024-Nitroaniline 1 03/10/21 17:26 V1707JMV
<0.170 mg/Kg - dry 0.170 0.402Nitrobenzene 1 03/10/21 17:26 V1707JMV
<0.134 mg/Kg - dry 0.134 0.8042-Nitrophenol 1 03/10/21 17:26 V1707JMV
<0.198 mg/Kg - dry 0.198 0.8044-Nitrophenol 1 03/10/21 17:26 V1707JMV
<0.006 mg/Kg - dry 0.006 0.207N-Nitrosodimethylamine 1 03/10/21 17:26 V1707JMV
<0.220 mg/Kg - dry 0.220 0.804
N-Nitrosodiphenylamine 1 03/10/21 17:26 V1707JMV
<0.185 mg/Kg - dry 0.185 0.804N-Nitroso-di-n-propylamine 1 03/10/21 17:26 V1707JMV
<0.513 mg/Kg - dry 0.513 1.22Pentachlorophenol 1 03/10/21 17:26 V1707JMV
0.143 J mg/Kg - dry 0.008 0.804Phenanthrene 1 03/10/21 17:26 V1707JMV
<0.131 mg/Kg - dry 0.131 0.804Phenol 1 03/10/21 17:26 V1707JMV
0.295 J mg/Kg - dry 0.011 0.804Pyrene 1 03/10/21 17:26 V1707JMV
<0.076 mg/Kg - dry 0.076 0.402Pyridine 1 03/10/21 17:26 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-4
94147 Matrix:
3/8/2021 11:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.142 mg/Kg - dry 0.142 0.8041,2,4-Trichlorobenzene 1 03/10/21 17:26 V1707JMV
<0.170 mg/Kg - dry 0.170 0.8042,4,5-Trichlorophenol 1 03/10/21 17:26 V1707JMV
<0.195 mg/Kg - dry 0.195 0.8042,4,6-Trichlorophenol 1 03/10/21 17:26 V1707JMV
Surrogate: 2-Fluorobiphenyl 92.8 Limits: 44-115%03/10/21 17:261 JMV V1707
Surrogate: 2-Fluorophenol 77.4 Limits: 35-115%03/10/21 17:261 JMV V1707
Surrogate: Nitrobenzene-d5 87.3 Limits: 37-122%03/10/21 17:261 JMV V1707
Surrogate: 4-Terphenyl-d14 100 Limits: 54-127%03/10/21 17:261 JMV V1707
Surrogate: 2,4,6-Tribromophenol 74.7 Limits: 39-132%03/10/21 17:261 JMV V1707
Surrogate: Phenol-d5 77.7 Limits: 34-121%03/10/21 17:261 JMV V1707
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG1-AL4
94148 Matrix:
3/8/2021 12:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
19.4 %Moisture 1 03/09/21 15:20 SW-DRYWTEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 27 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG1-AL4
94148 Matrix:
3/8/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.018 mg/Kg - dry 0.018 0.024Acetone 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.024Acrylonitrile 1 03/11/21 14:46 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Benzene 1 03/11/21 14:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/11/21 14:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromodichloromethane 1 03/11/21 14:46 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 03/11/21 14:46 V1590TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 03/11/21 14:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/11/21 14:46 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Chlorobenzene 1 03/11/21 14:46 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.006
Chlorodibromomethane 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/11/21 14:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chloroform 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Chloromethane 1 03/11/21 14:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0062-Chlorotoluene 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0064-Chlorotoluene 1 03/11/21 14:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/11/21 14:46 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG1-AL4
94148 Matrix:
3/8/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0121,2-Dibromo-3-Chloropropane 1 03/11/21 14:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dichlorobenzene 1 03/11/21 14:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 03/11/21 14:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dichloroethane 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 03/11/21 14:46 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/11/21 14:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2-Dichloropropane 1 03/11/21 14:46 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichloropropane 1 03/11/21 14:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 03/11/21 14:46 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 03/11/21 14:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 03/11/21 14:46 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.006trans-1,3-Dichloropropene 1 03/11/21 14:46 V1590TBL
<0.022 mg/Kg - dry 0.022 0.310Ethanol 1 03/11/21 14:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Ethylbenzene 1 03/11/21 14:46 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.062Ethyl Tertiary Butyl Ether (ETBE)1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 03/11/21 14:46 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG1-AL4
94148 Matrix:
3/8/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.012n-Hexane 1 03/11/21 14:46 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.0242-Hexanone 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Isopropylbenzene 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.024Methyl Ethyl Ketone (MEK)1 03/11/21 14:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 03/11/21 14:46 V1590TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 03/11/21 14:46 V1590TBL
<0.006 mg/Kg - dry 0.006 0.012Methylene Chloride 1 03/11/21 14:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Naphthalene 1 03/11/21 14:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006n-Propylbenzene 1 03/11/21 14:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006Styrene 1 03/11/21 14:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 03/11/21 14:46 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/11/21 14:46 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Toluene 1 03/11/21 14:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.012
1,2,3-Trichlorobenzene 1 03/11/21 14:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,4-Trichlorobenzene 1 03/11/21 14:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1,1-Trichloroethane 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Trichlorofluoromethane 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2,3-Trichloropropane 1 03/11/21 14:46 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG1-AL4
94148 Matrix:
3/8/2021 12:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.012Vinyl Acetate 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Vinyl Chloride 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 03/11/21 14:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/11/21 14:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/11/21 14:46 V1590
Surrogate: 4-Bromofluorobenzene 97.0 Limits: 70-130%03/11/21 14:461 TBL V1590
Surrogate: Dibromofluoromethane 100 Limits: 84-123%03/11/21 14:461 TBL V1590
Surrogate: Toluene-d8 82.1 Limits: 76-129%03/11/21 14:461 TBL V1590
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG2-AL1
94149 Matrix:
3/8/2021 14:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.1 %Moisture 1 03/09/21 15:20 SW-DRYWTEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 32 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG2-AL1
94149 Matrix:
3/8/2021 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.018 mg/Kg - dry 0.018 0.025Acetone 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.025Acrylonitrile 1 03/11/21 15:16 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Benzene 1 03/11/21 15:16 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/11/21 15:16 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromodichloromethane 1 03/11/21 15:16 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 03/11/21 15:16 V1590TBL
<0.003 mg/Kg - dry 0.003 0.012
Bromomethane 1 03/11/21 15:16 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/11/21 15:16 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Chlorobenzene 1 03/11/21 15:16 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.006
Chlorodibromomethane 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/11/21 15:16 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chloroform 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Chloromethane 1 03/11/21 15:16 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0062-Chlorotoluene 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0064-Chlorotoluene 1 03/11/21 15:16 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/11/21 15:16 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 33 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG2-AL1
94149 Matrix:
3/8/2021 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0121,2-Dibromo-3-Chloropropane 1 03/11/21 15:16 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dichlorobenzene 1 03/11/21 15:16 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 03/11/21 15:16 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/11/21 15:16 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dichloroethane 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 03/11/21 15:16 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/11/21 15:16 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2-Dichloropropane 1 03/11/21 15:16 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichloropropane 1 03/11/21 15:16 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 03/11/21 15:16 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 03/11/21 15:16 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 03/11/21 15:16 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.006trans-1,3-Dichloropropene 1 03/11/21 15:16 V1590TBL
<0.022 mg/Kg - dry 0.022 0.312Ethanol 1 03/11/21 15:16 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Ethylbenzene 1 03/11/21 15:16 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.062Ethyl Tertiary Butyl Ether (ETBE)1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 03/11/21 15:16 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 34 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG2-AL1
94149 Matrix:
3/8/2021 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.012n-Hexane 1 03/11/21 15:16 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.0252-Hexanone 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Isopropylbenzene 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.025Methyl Ethyl Ketone (MEK)1 03/11/21 15:16 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 03/11/21 15:16 V1590TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 03/11/21 15:16 V1590TBL
<0.006 mg/Kg - dry 0.006 0.012Methylene Chloride 1 03/11/21 15:16 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Naphthalene 1 03/11/21 15:16 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006n-Propylbenzene 1 03/11/21 15:16 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006Styrene 1 03/11/21 15:16 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 03/11/21 15:16 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,1,2,2-Tetrachloroethane 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Toluene 1 03/11/21 15:16 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.012
1,2,3-Trichlorobenzene 1 03/11/21 15:16 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,4-Trichlorobenzene 1 03/11/21 15:16 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1,1-Trichloroethane 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Trichlorofluoromethane 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2,3-Trichloropropane 1 03/11/21 15:16 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 35 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG2-AL1
94149 Matrix:
3/8/2021 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.012Vinyl Acetate 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Vinyl Chloride 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 03/11/21 15:16 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/11/21 15:16 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/11/21 15:16 V1590
Surrogate: 4-Bromofluorobenzene 94.9 Limits: 70-130%03/11/21 15:161 TBL V1590
Surrogate: Dibromofluoromethane 98.5 Limits: 84-123%03/11/21 15:161 TBL V1590
Surrogate: Toluene-d8 81.8 Limits: 76-129%03/11/21 15:161 TBL V1590
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 36 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG3-AL3
94150 Matrix:
3/8/2021 9:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.8 %Moisture 1 03/09/21 15:20 SW-DRYWTEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 37 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG3-AL3
94150 Matrix:
3/8/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.018 mg/Kg - dry 0.018 0.024Acetone 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.024Acrylonitrile 1 03/11/21 15:46 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Benzene 1 03/11/21 15:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.006Bromobenzene 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/11/21 15:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromodichloromethane 1 03/11/21 15:46 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 03/11/21 15:46 V1590TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 03/11/21 15:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/11/21 15:46 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Chlorobenzene 1 03/11/21 15:46 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.006
Chlorodibromomethane 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/11/21 15:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chloroform 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Chloromethane 1 03/11/21 15:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0062-Chlorotoluene 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0064-Chlorotoluene 1 03/11/21 15:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/11/21 15:46 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 38 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG3-AL3
94150 Matrix:
3/8/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0121,2-Dibromo-3-Chloropropane 1 03/11/21 15:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dichlorobenzene 1 03/11/21 15:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 03/11/21 15:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dichloroethane 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 03/11/21 15:46 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/11/21 15:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2-Dichloropropane 1 03/11/21 15:46 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichloropropane 1 03/11/21 15:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 03/11/21 15:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 03/11/21 15:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 03/11/21 15:46 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.006trans-1,3-Dichloropropene 1 03/11/21 15:46 V1590TBL
<0.022 mg/Kg - dry 0.022 0.307Ethanol 1 03/11/21 15:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Ethylbenzene 1 03/11/21 15:46 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.061Ethyl Tertiary Butyl Ether (ETBE)1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 03/11/21 15:46 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 39 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG3-AL3
94150 Matrix:
3/8/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.012n-Hexane 1 03/11/21 15:46 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.0242-Hexanone 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Isopropylbenzene 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.024Methyl Ethyl Ketone (MEK)1 03/11/21 15:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 03/11/21 15:46 V1590TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 03/11/21 15:46 V1590TBL
<0.006 mg/Kg - dry 0.006 0.012Methylene Chloride 1 03/11/21 15:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Naphthalene 1 03/11/21 15:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006n-Propylbenzene 1 03/11/21 15:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006Styrene 1 03/11/21 15:46 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 03/11/21 15:46 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/11/21 15:46 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Toluene 1 03/11/21 15:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.012
1,2,3-Trichlorobenzene 1 03/11/21 15:46 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,4-Trichlorobenzene 1 03/11/21 15:46 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1,1-Trichloroethane 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Trichlorofluoromethane 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2,3-Trichloropropane 1 03/11/21 15:46 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 40 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG3-AL3
94150 Matrix:
3/8/2021 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.012Vinyl Acetate 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Vinyl Chloride 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 03/11/21 15:46 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/11/21 15:46 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/11/21 15:46 V1590
Surrogate: 4-Bromofluorobenzene 96.3 Limits: 70-130%03/11/21 15:461 TBL V1590
Surrogate: Dibromofluoromethane 98.2 Limits: 84-123%03/11/21 15:461 TBL V1590
Surrogate: Toluene-d8 83.3 Limits: 76-129%03/11/21 15:461 TBL V1590
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 41 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG4-AL3
94151 Matrix:
3/8/2021 11:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.0 %Moisture 1 03/09/21 15:20 SW-DRYWTEDV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 42 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG4-AL3
94151 Matrix:
3/8/2021 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
0.022 J mg/Kg - dry 0.018 0.024Acetone 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.024Acrylonitrile 1 03/11/21 16:17 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Benzene 1 03/11/21 16:17 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.006Bromobenzene 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/11/21 16:17 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromodichloromethane 1 03/11/21 16:17 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 03/11/21 16:17 V1590TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 03/11/21 16:17 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/11/21 16:17 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Chlorobenzene 1 03/11/21 16:17 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.006
Chlorodibromomethane 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Chloroform 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Chloromethane 1 03/11/21 16:17 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0062-Chlorotoluene 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0064-Chlorotoluene 1 03/11/21 16:17 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/11/21 16:17 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 43 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG4-AL3
94151 Matrix:
3/8/2021 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0121,2-Dibromo-3-Chloropropane 1 03/11/21 16:17 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dibromoethane 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dichlorobenzene 1 03/11/21 16:17 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 03/11/21 16:17 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dichloroethane 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 03/11/21 16:17 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/11/21 16:17 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2-Dichloropropane 1 03/11/21 16:17 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichloropropane 1 03/11/21 16:17 V1590TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 03/11/21 16:17 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 03/11/21 16:17 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 03/11/21 16:17 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.006trans-1,3-Dichloropropene 1 03/11/21 16:17 V1590TBL
<0.021 mg/Kg - dry 0.021 0.304Ethanol 1 03/11/21 16:17 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Ethylbenzene 1 03/11/21 16:17 V1590TBL
<0.0005 mg/Kg - dry 0.0005 0.060Ethyl Tertiary Butyl Ether (ETBE)1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 03/11/21 16:17 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 44 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG4-AL3
94151 Matrix:
3/8/2021 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.012n-Hexane 1 03/11/21 16:17 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.0242-Hexanone 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.006Isopropylbenzene 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/11/21 16:17 V1590TBL
0.002 J mg/Kg - dry 0.001 0.024Methyl Ethyl Ketone (MEK)1 03/11/21 16:17 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 03/11/21 16:17 V1590TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 03/11/21 16:17 V1590TBL
<0.006 mg/Kg - dry 0.006 0.012Methylene Chloride 1 03/11/21 16:17 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Naphthalene 1 03/11/21 16:17 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.006n-Propylbenzene 1 03/11/21 16:17 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006Styrene 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,1,2-Tetrachloroethane 1 03/11/21 16:17 V1590TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/11/21 16:17 V1590TBL
<0.0010 mg/Kg - dry 0.0010 0.006Toluene 1 03/11/21 16:17 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.012
1,2,3-Trichlorobenzene 1 03/11/21 16:17 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,4-Trichlorobenzene 1 03/11/21 16:17 V1590TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1,1-Trichloroethane 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Trichlorofluoromethane 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2,3-Trichloropropane 1 03/11/21 16:17 V1590TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 45 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG4-AL3
94151 Matrix:
3/8/2021 11:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1588 03/11/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 03/11/21 16:17 V1590TBL
<0.0007 mg/Kg - dry 0.0007 0.012Vinyl Acetate 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012Vinyl Chloride 1 03/11/21 16:17 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 03/11/21 16:17 V1590TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/11/21 16:17 V1590TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 03/11/21 16:17 V1590
Surrogate: 4-Bromofluorobenzene 93.9 Limits: 70-130%03/11/21 16:171 TBL V1590
Surrogate: Dibromofluoromethane 101 Limits: 84-123%03/11/21 16:171 TBL V1590
Surrogate: Toluene-d8 81.1 Limits: 76-129%03/11/21 16:171 TBL V1590
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 46 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-Dup
94152 Matrix:
3/8/2021 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.3 %Moisture 1 03/09/21 15:20 SW-DRYWTEDV
3.53 mg/Kg - dry 0.105 0.125Arsenic 10 03/10/21 16:38 6020BMMR
72.6 mg/Kg - dry 0.451 12.5Barium 10 03/10/21 16:38 6020BMMR
<0.0464 mg/Kg - dry 0.0464 0.627Cadmium 10 03/10/21 16:38 6020BMMR
58.6 mg/Kg - dry 0.301 1.25Chromium 10 03/10/21 16:38 6020BMMR
18.4 mg/Kg - dry 0.0953 1.25
Lead 10 03/10/21 16:38 6020BMMR
0.106 mg/Kg - dry 0.0188 0.0627Mercury (Total)1 03/10/21 13:05 7471BEDV
1.89 mg/Kg - dry 0.288 1.25Selenium 10 03/10/21 16:38 6020BMMR
<0.0639 mg/Kg - dry 0.0639 0.627Silver 10 03/10/21 16:38 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 47 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-Dup
94152 Matrix:
3/8/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1656 03/12/21 08:00
<0.018 mg/Kg - dry 0.018 0.025Acetone 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.025Acrylonitrile 1 03/12/21 13:16 V1657TBL
<0.0010 mg/Kg - dry 0.0010 0.006Benzene 1 03/12/21 13:16 V1657TBL
<0.0009 mg/Kg - dry 0.0009 0.006Bromobenzene 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/12/21 13:16 V1657TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromodichloromethane 1 03/12/21 13:16 V1657TBL
<0.0005 mg/Kg - dry 0.0005 0.006Bromoform 1 03/12/21 13:16 V1657TBL
<0.003 mg/Kg - dry 0.003 0.012
Bromomethane 1 03/12/21 13:16 V1657TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Disulfide 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/12/21 13:16 V1657TBL
<0.0010 mg/Kg - dry 0.0010 0.006Chlorobenzene 1 03/12/21 13:16 V1657TBL
<0.0004 mg/Kg - dry 0.0004 0.006
Chlorodibromomethane 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/12/21 13:16 V1657TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chloroform 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.012Chloromethane 1 03/12/21 13:16 V1657TBL
<0.0008 mg/Kg - dry 0.0008 0.0062-Chlorotoluene 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.0064-Chlorotoluene 1 03/12/21 13:16 V1657TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/12/21 13:16 V1657TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 48 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-Dup
94152 Matrix:
3/8/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1656 03/12/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0121,2-Dibromo-3-Chloropropane 1 03/12/21 13:16 V1657TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dibromoethane 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dichlorobenzene 1 03/12/21 13:16 V1657TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichlorobenzene 1 03/12/21 13:16 V1657TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/12/21 13:16 V1657TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dichloroethane 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 03/12/21 13:16 V1657TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/12/21 13:16 V1657TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2-Dichloropropane 1 03/12/21 13:16 V1657TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichloropropane 1 03/12/21 13:16 V1657TBL
<0.0008 mg/Kg - dry 0.0008 0.0062,2-Dichloropropane 1 03/12/21 13:16 V1657TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 03/12/21 13:16 V1657TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 03/12/21 13:16 V1657TBL
<0.0005 mg/Kg - dry 0.0005 0.006trans-1,3-Dichloropropene 1 03/12/21 13:16 V1657TBL
<0.022 mg/Kg - dry 0.022 0.313Ethanol 1 03/12/21 13:16 V1657TBL
<0.0009 mg/Kg - dry 0.0009 0.006Ethylbenzene 1 03/12/21 13:16 V1657TBL
<0.0005 mg/Kg - dry 0.0005 0.062Ethyl Tertiary Butyl Ether (ETBE)1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 03/12/21 13:16 V1657TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 49 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-Dup
94152 Matrix:
3/8/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1656 03/12/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.012n-Hexane 1 03/12/21 13:16 V1657TBL
<0.0004 mg/Kg - dry 0.0004 0.0252-Hexanone 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.006Isopropylbenzene 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.025Methyl Ethyl Ketone (MEK)1 03/12/21 13:16 V1657TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 03/12/21 13:16 V1657TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 03/12/21 13:16 V1657TBL
<0.006 mg/Kg - dry 0.006 0.012Methylene Chloride 1 03/12/21 13:16 V1657TBL
<0.0006 mg/Kg - dry 0.0006 0.012
Naphthalene 1 03/12/21 13:16 V1657TBL
<0.0009 mg/Kg - dry 0.0009 0.006n-Propylbenzene 1 03/12/21 13:16 V1657TBL
<0.0006 mg/Kg - dry 0.0006 0.006Styrene 1 03/12/21 13:16 V1657TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,1,1,2-Tetrachloroethane 1 03/12/21 13:16 V1657TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,1,2,2-Tetrachloroethane 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.006Toluene 1 03/12/21 13:16 V1657TBL
<0.0009 mg/Kg - dry 0.0009 0.012
1,2,3-Trichlorobenzene 1 03/12/21 13:16 V1657TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,4-Trichlorobenzene 1 03/12/21 13:16 V1657TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1,1-Trichloroethane 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.012Trichlorofluoromethane 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2,3-Trichloropropane 1 03/12/21 13:16 V1657TBL
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 50 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-Dup
94152 Matrix:
3/8/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V1656 03/12/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.012Vinyl Acetate 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.012Vinyl Chloride 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 03/12/21 13:16 V1657TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/12/21 13:16 V1657TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/12/21 13:16 V1657
Surrogate: 4-Bromofluorobenzene 92.0 Limits: 70-130%03/12/21 13:161 TBL V1657
Surrogate: Dibromofluoromethane 97.6 Limits: 84-123%03/12/21 13:161 TBL V1657
Surrogate: Toluene-d8 81.8 Limits: 76-129%03/12/21 13:161 TBL V1657
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.018 mg/Kg - dry 0.018 0.828Acenaphthene 1 03/10/21 17:48 V1707JMV
<0.016 mg/Kg - dry 0.016 0.828Acenaphthylene 1 03/10/21 17:48 V1707JMV
<0.204 mg/Kg - dry 0.204 0.828Aniline 1 03/10/21 17:48 V1707JMV
<0.009 mg/Kg - dry 0.009 0.828Anthracene 1 03/10/21 17:48 V1707JMV
<0.009 mg/Kg - dry 0.009 0.828Benzo(a)anthracene 1 03/10/21 17:48 V1707JMV
<0.007 mg/Kg - dry 0.007 0.828
Benzo(a)pyrene 1 03/10/21 17:48 V1707JMV
<0.007 mg/Kg - dry 0.007 0.828Benzo(b)fluoranthene 1 03/10/21 17:48 V1707JMV
<0.008 mg/Kg - dry 0.008 0.828Benzo(g,h,i)perylene 1 03/10/21 17:48 V1707JMV
<0.008 mg/Kg - dry 0.008 0.828Benzo(k)fluoranthene 1 03/10/21 17:48 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 51 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-Dup
94152 Matrix:
3/8/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.687 mg/Kg - dry 0.687 2.51Benzoic Acid 1 03/10/21 17:48 V1707JMV
<0.155 mg/Kg - dry 0.155 0.828Benzyl alcohol 1 03/10/21 17:48 V1707JMV
<0.158 mg/Kg - dry 0.158 0.828Bis(2-Chloroethoxy)methane 1 03/10/21 17:48 V1707JMV
<0.132 mg/Kg - dry 0.132 0.828Bis(2-Chloroethyl)ether 1 03/10/21 17:48 V1707JMV
<0.148 mg/Kg - dry 0.148 0.414Bis(2-Chloroisopropyl)ether 1 03/10/21 17:48 V1707JMV
<0.186 mg/Kg - dry 0.186 0.828Bis(2-ethylhexyl)phthalate 1 03/10/21 17:48 V1707JMV
<0.194 mg/Kg - dry 0.194 0.8284-Bromophenyl phenyl ether 1 03/10/21 17:48 V1707JMV
<0.143 mg/Kg - dry 0.143 0.414Butyl benzyl phthalate 1 03/10/21 17:48 V1707JMV
<0.158 mg/Kg - dry 0.158 0.828
4-Chloro-3-methylphenol 1 03/10/21 17:48 V1707JMV
<0.100 mg/Kg - dry 0.100 0.4144-Chloroaniline 1 03/10/21 17:48 V1707JMV
<0.202 mg/Kg - dry 0.202 0.8282-Chloronaphthalene 1 03/10/21 17:48 V1707JMV
<0.158 mg/Kg - dry 0.158 0.8282-Chlorophenol 1 03/10/21 17:48 V1707JMV
<0.253 mg/Kg - dry 0.253 1.254-Chlorophenyl phenyl ether 1 03/10/21 17:48 V1707JMV
<0.009 mg/Kg - dry 0.009 0.828Chrysene 1 03/10/21 17:48 V1707JMV
<0.023 mg/Kg - dry 0.023 0.828Dibenz(a,h)anthracene 1 03/10/21 17:48 V1707JMV
<0.022 mg/Kg - dry 0.022 0.828
Dibenzofuran 1 03/10/21 17:48 V1707JMV
<0.134 mg/Kg - dry 0.134 0.8281,2-Dichlorobenzene 1 03/10/21 17:48 V1707JMV
<0.121 mg/Kg - dry 0.121 0.8281,3-Dichlorobenzene 1 03/10/21 17:48 V1707JMV
<0.130 mg/Kg - dry 0.130 0.4141,4-Dichlorobenzene 1 03/10/21 17:48 V1707JMV
<0.164 mg/Kg - dry 0.164 0.8283,3'-Dichlorobenzidine 1 03/10/21 17:48 V1707JMV
<0.161 mg/Kg - dry 0.161 0.8282,4-Dichlorophenol 1 03/10/21 17:48 V1707JMV
<0.213 mg/Kg - dry 0.213 0.828Diethyl phthalate 1 03/10/21 17:48 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 52 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-Dup
94152 Matrix:
3/8/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.198 mg/Kg - dry 0.198 0.828Dimethyl phthalate 1 03/10/21 17:48 V1707JMV
<0.171 mg/Kg - dry 0.171 0.4142,4-Dimethylphenol 1 03/10/21 17:48 V1707JMV
<0.205 mg/Kg - dry 0.205 0.828Di-n-butyl phthalate 1 03/10/21 17:48 V1707JMV
<0.456 mg/Kg - dry 0.456 1.884,6-Dinitro-2-methylphenol 1 03/10/21 17:48 V1707JMV
<0.485 mg/Kg - dry 0.485 1.882,4-Dinitrophenol 1 03/10/21 17:48 V1707JMV
<0.219 mg/Kg - dry 0.219 0.8282,4-Dinitrotoluene 1 03/10/21 17:48 V1707JMV
<0.214 mg/Kg - dry 0.214 0.8282,6-Dinitrotoluene 1 03/10/21 17:48 V1707JMV
<0.214 mg/Kg - dry 0.214 0.414Di-n-Octyl Phthalate 1 03/10/21 17:48 V1707JMV
<0.009 mg/Kg - dry 0.009 0.828
Fluoranthene 1 03/10/21 17:48 V1707JMV
<0.018 mg/Kg - dry 0.018 0.828Fluorene 1 03/10/21 17:48 V1707JMV
<0.181 mg/Kg - dry 0.181 0.828Hexachlorobenzene 1 03/10/21 17:48 V1707JMV
<0.186 mg/Kg - dry 0.186 0.828Hexachlorobutadiene 1 03/10/21 17:48 V1707JMV
<0.284 mg/Kg - dry 0.284 0.828Hexachlorocyclopentadiene 1 03/10/21 17:48 V1707JMV
<0.130 mg/Kg - dry 0.130 0.828Hexachloroethane 1 03/10/21 17:48 V1707JMV
<0.023 mg/Kg - dry 0.023 0.828Indeno(1,2,3-cd)pyrene 1 03/10/21 17:48 V1707JMV
<0.178 mg/Kg - dry 0.178 0.828
Isophorone 1 03/10/21 17:48 V1707JMV
<0.012 mg/Kg - dry 0.012 0.8281-Methylnaphthalene 1 03/10/21 17:48 V1707JMV
<0.016 mg/Kg - dry 0.016 0.8282-Methylnaphthalene 1 03/10/21 17:48 V1707JMV
<0.158 mg/Kg - dry 0.158 0.8282-Methylphenol 1 03/10/21 17:48 V1707JMV
<0.179 mg/Kg - dry 0.179 0.8283&4 Methylphenol 1 03/10/21 17:48 V1707JMV
<0.017 mg/Kg - dry 0.017 0.828Naphthalene 1 03/10/21 17:48 V1707JMV
<0.178 mg/Kg - dry 0.178 0.8282-Nitroaniline 1 03/10/21 17:48 V1707JMV
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 53 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:FG-Dup
94152 Matrix:
3/8/2021 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V1480 03/10/21 10:45
<0.150 mg/Kg - dry 0.150 0.8283-Nitroaniline 1 03/10/21 17:48 V1707JMV
<0.129 mg/Kg - dry 0.129 0.4144-Nitroaniline 1 03/10/21 17:48 V1707JMV
<0.175 mg/Kg - dry 0.175 0.414Nitrobenzene 1 03/10/21 17:48 V1707JMV
<0.138 mg/Kg - dry 0.138 0.8282-Nitrophenol 1 03/10/21 17:48 V1707JMV
<0.204 mg/Kg - dry 0.204 0.8284-Nitrophenol 1 03/10/21 17:48 V1707JMV
<0.007 mg/Kg - dry 0.007 0.213N-Nitrosodimethylamine 1 03/10/21 17:48 V1707JMV
<0.227 mg/Kg - dry 0.227 0.828N-Nitrosodiphenylamine 1 03/10/21 17:48 V1707JMV
<0.190 mg/Kg - dry 0.190 0.828N-Nitroso-di-n-propylamine 1 03/10/21 17:48 V1707JMV
<0.528 mg/Kg - dry 0.528 1.25
Pentachlorophenol 1 03/10/21 17:48 V1707JMV
<0.009 mg/Kg - dry 0.009 0.828Phenanthrene 1 03/10/21 17:48 V1707JMV
<0.135 mg/Kg - dry 0.135 0.828Phenol 1 03/10/21 17:48 V1707JMV
<0.012 mg/Kg - dry 0.012 0.828Pyrene 1 03/10/21 17:48 V1707JMV
<0.079 mg/Kg - dry 0.079 0.414Pyridine 1 03/10/21 17:48 V1707JMV
<0.146 mg/Kg - dry 0.146 0.8281,2,4-Trichlorobenzene 1 03/10/21 17:48 V1707JMV
<0.175 mg/Kg - dry 0.175 0.8282,4,5-Trichlorophenol 1 03/10/21 17:48 V1707JMV
<0.200 mg/Kg - dry 0.200 0.828
2,4,6-Trichlorophenol 1 03/10/21 17:48 V1707JMV
Surrogate: 2-Fluorobiphenyl 92.2 Limits: 44-115%03/10/21 17:481 JMV V1707
Surrogate: 2-Fluorophenol 74.5 Limits: 35-115%03/10/21 17:481 JMV V1707
Surrogate: Nitrobenzene-d5 86.2 Limits: 37-122%03/10/21 17:481 JMV V1707
Surrogate: 4-Terphenyl-d14 93.4 Limits: 54-127%03/10/21 17:481 JMV V1707
Surrogate: 2,4,6-Tribromophenol 71.2 Limits: 39-132%03/10/21 17:481 JMV V1707
Surrogate: Phenol-d5 75.4 Limits: 34-121%03/10/21 17:481 JMV V1707
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 54 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:Trip Blank
94153 Matrix:
3/8/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V1542 03/10/21 09:00
1.63 JB µg/L 0.310 5.00Acetone 1 03/10/21 15:34 V1543JLB
<0.200 µg/L 0.200 20.0Acrolein 1 03/10/21 15:34 V1543JLB
<0.200 µg/L 0.200 20.0Acrylonitrile 1 03/10/21 15:34 V1543JLB
<0.048 µg/L 0.048 0.500Benzene 1 03/10/21 15:34 V1543JLB
<0.057 µg/L 0.057 0.500Bromobenzene 1 03/10/21 15:34 V1543JLB
<0.140 µg/L 0.140 0.500Bromochloromethane 1 03/10/21 15:34 V1543JLB
<0.062 µg/L 0.062 0.500Bromodichloromethane 1 03/10/21 15:34 V1543JLB
<0.040 µg/L 0.040 1.00Bromoform 1 03/10/21 15:34 V1543JLB
<0.180 µg/L 0.180 1.00
Bromomethane 1 03/10/21 15:34 V1543JLB
<0.076 µg/L 0.076 1.00n-Butylbenzene 1 03/10/21 15:34 V1543JLB
<0.076 µg/L 0.076 0.500sec-Butyl benzene 1 03/10/21 15:34 V1543JLB
<0.088 µg/L 0.088 0.500tert-Butyl benzene 1 03/10/21 15:34 V1543JLB
<0.075 µg/L 0.075 5.00Carbon Disulfide 1 03/10/21 15:34 V1543JLB
<0.110 µg/L 0.110 0.500Carbon Tetrachloride 1 03/10/21 15:34 V1543JLB
<0.062 µg/L 0.062 0.500Chlorobenzene 1 03/10/21 15:34 V1543JLB
<0.081 µg/L 0.081 0.500
Chlorodibromomethane 1 03/10/21 15:34 V1543JLB
<0.220 µg/L 0.220 0.500Chloroethane 1 03/10/21 15:34 V1543JLB
<0.076 µg/L 0.076 0.500Chloroform 1 03/10/21 15:34 V1543JLB
<0.079 µg/L 0.079 0.500Chloromethane 1 03/10/21 15:34 V1543JLB
<0.066 µg/L 0.066 0.5002-Chlorotoluene 1 03/10/21 15:34 V1543JLB
<0.050 µg/L 0.050 0.5004-Chlorotoluene 1 03/10/21 15:34 V1543JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 03/10/21 15:34 V1543JLB
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 55 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:Trip Blank
94153 Matrix:
3/8/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V1542 03/10/21 09:00
<0.170 µg/L 0.170 2.001,2-Dibromo-3-Chloropropane 1 03/10/21 15:34 V1543JLB
<0.051 µg/L 0.051 0.5001,2-Dibromoethane 1 03/10/21 15:34 V1543JLB
<0.065 µg/L 0.065 0.500Dibromomethane 1 03/10/21 15:34 V1543JLB
<0.076 µg/L 0.076 0.5001,2-Dichlorobenzene 1 03/10/21 15:34 V1543JLB
<0.054 µg/L 0.054 0.5001,3-Dichlorobenzene 1 03/10/21 15:34 V1543JLB
<0.050 µg/L 0.050 0.5001,4-Dichlorobenzene 1 03/10/21 15:34 V1543JLB
<0.110 µg/L 0.110 5.00Dichlorodifluoromethane 1 03/10/21 15:34 V1543JLB
<0.083 µg/L 0.083 0.5001,1-Dichloroethane 1 03/10/21 15:34 V1543JLB
<0.066 µg/L 0.066 0.500
1,2-Dichloroethane 1 03/10/21 15:34 V1543JLB
<0.083 µg/L 0.083 0.5001,1-Dichloroethene 1 03/10/21 15:34 V1543JLB
<0.056 µg/L 0.056 0.500cis-1,2-Dichloroethene 1 03/10/21 15:34 V1543JLB
<0.094 µg/L 0.094 0.500trans-1,2-Dichloroethene 1 03/10/21 15:34 V1543JLB
<0.110 µg/L 0.110 0.5001,2-Dichloropropane 1 03/10/21 15:34 V1543JLB
<0.043 µg/L 0.043 0.5001,3-Dichloropropane 1 03/10/21 15:34 V1543JLB
<0.110 µg/L 0.110 2.002,2-Dichloropropane 1 03/10/21 15:34 V1543JLB
<0.051 µg/L 0.051 0.500
1,1-Dichloropropene 1 03/10/21 15:34 V1543JLB
<0.079 µg/L 0.079 0.500cis-1,3-Dichloropropene 1 03/10/21 15:34 V1543JLB
<0.070 µg/L 0.070 0.500trans-1,3-Dichloropropene 1 03/10/21 15:34 V1543JLB
<27.0 µg/L 27.0 200Ethanol 1 03/10/21 15:34 V1543JLB
<0.061 µg/L 0.061 0.500Ethylbenzene 1 03/10/21 15:34 V1543JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 03/10/21 15:34 V1543JLB
<0.160 µg/L 0.160 2.00Hexachlorobutadiene 1 03/10/21 15:34 V1543JLB
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 56 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:Trip Blank
94153 Matrix:
3/8/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V1542 03/10/21 09:00
<0.760 µg/L 0.760 10.0n-Hexane 1 03/10/21 15:34 V1543JLB
<0.065 µg/L 0.065 5.002-Hexanone 1 03/10/21 15:34 V1543JLB
<0.330 µg/L 0.330 5.00Isopropylbenzene 1 03/10/21 15:34 V1543JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 03/10/21 15:34 V1543JLB
<0.240 µg/L 0.240 5.00Methyl Ethyl Ketone (MEK)1 03/10/21 15:34 V1543JLB
<0.042 µg/L 0.042 0.500Methyl tert-butyl ether (MTBE)1 03/10/21 15:34 V1543JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 03/10/21 15:34 V1543JLB
<0.083 µg/L 0.083 1.00Methylene Chloride 1 03/10/21 15:34 V1543JLB
<0.300 µg/L 0.300 1.00
Naphthalene 1 03/10/21 15:34 V1543JLB
<0.087 µg/L 0.087 0.500n-Propylbenzene 1 03/10/21 15:34 V1543JLB
<0.047 µg/L 0.047 0.500Styrene 1 03/10/21 15:34 V1543JLB
<0.110 µg/L 0.110 0.5001,1,1,2-Tetrachloroethane 1 03/10/21 15:34 V1543JLB
<0.036 µg/L 0.036 0.5001,1,2,2-Tetrachloroethane 1 03/10/21 15:34 V1543JLB
<0.098 µg/L 0.098 0.500Tetrachloroethene 1 03/10/21 15:34 V1543JLB
<0.044 µg/L 0.044 0.500Toluene 1 03/10/21 15:34 V1543JLB
<0.400 µg/L 0.400 2.00
1,2,3-Trichlorobenzene 1 03/10/21 15:34 V1543JLB
<0.130 µg/L 0.130 1.001,2,4-Trichlorobenzene 1 03/10/21 15:34 V1543JLB
<0.061 µg/L 0.061 0.5001,1,1-Trichloroethane 1 03/10/21 15:34 V1543JLB
<0.066 µg/L 0.066 0.5001,1,2-Trichloroethane 1 03/10/21 15:34 V1543JLB
<0.078 µg/L 0.078 0.500Trichloroethene 1 03/10/21 15:34 V1543JLB
<0.062 µg/L 0.062 0.500Trichlorofluoromethane 1 03/10/21 15:34 V1543JLB
<0.140 µg/L 0.140 1.001,2,3-Trichloropropane 1 03/10/21 15:34 V1543JLB
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 57 of 110
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
21-068-0001
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Robert Sorgel
Charlotte
Angela D Overcash
Senior Project Manager
Received : 03/08/2021
JMC.011
Report Date : 03/16/2021
Sample ID :
Lab No :
Sampled:Trip Blank
94153 Matrix:
3/8/2021 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V1542 03/10/21 09:00
<0.076 µg/L 0.076 0.5001,3,5-Trimethylbenzene 1 03/10/21 15:34 V1543JLB
<0.060 µg/L 0.060 2.00Vinyl Acetate 1 03/10/21 15:34 V1543JLB
<0.097 µg/L 0.097 0.500Vinyl Chloride 1 03/10/21 15:34 V1543JLB
<0.044 µg/L 0.044 0.500o-Xylene 1 03/10/21 15:34 V1543JLB
<0.120 µg/L 0.120 1.00m,p-Xylene 1 03/10/21 15:34 V1543JLB
<0.044 µg/L 0.044 0.500Xylene (Total)1 03/10/21 15:34 V1543
Surrogate: 4-Bromofluorobenzene 98.4 Limits: 80-124%03/10/21 15:341 JLB V1543
Surrogate: Dibromofluoromethane 101 Limits: 75-129%03/10/21 15:341 JLB V1543
Surrogate: 1,2-Dichloroethane - d4 97.4 Limits: 63-136%03/10/21 15:341 JLB V1543
Surrogate: Toluene-d8 95.6 Limits: 77-123%03/10/21 15:341 JLB V1543
Qualifiers/
Definitions
Dilution FactorDFAnalyte detected in blankB
Method Quantitation LimitMQLEstimated valueJ
Page 58 of 110
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172Tel: [phone] Fax: [phone] www.pacelabs.com
Report of Analysis
Waypoint Analytical
PO Box 240543Charlotte, NC 28224Attention: Angela Overcash
Project Name: 21-068-0001
Lot Number:WC11049
Date Completed:03/15/2021
03/15/2021 7:49 PMApproved and released by:
Project Manager II:Lucas Odom
Page 1 of 16
Page 59 of 110
PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Waypoint Analytical
Lot Number: WC11049
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header informationassociated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page ordiscussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on thecover page.
Page 2 of 16
Page 60 of 110
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WC11049

Sample Number Sample ID Matrix Date Sampled Date Received
001 03/08/2021 1215FG-1 Solid 03/11/2021
002 03/08/2021 1400FG-2 Solid 03/11/2021
003 03/08/2021 0915FG-3 Solid 03/11/2021
004 03/08/2021 1100FG-4 Solid 03/11/2021
005 03/08/2021FG-Dup Solid 03/11/2021
(5 samples)
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 16
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WC11049

Sample Sample ID Matrix Parameter Method Result Q Units Page
002 FG-2 Solid Hexavalent Chromium 7199 0.71 J mg/kg 6
005 FG-Dup Solid Hexavalent Chromium 7199 0.41 J mg/kg 9
(2 detections)
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 16
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
FG-1
WC11049-001
03/08/2021 1215
03/11/2021
Solid
% Solids:77.7 03/11/2021 2358
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 03/15/2021 1022 AMR 03/12/2021 1144 85529
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.261.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 16
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
FG-2
WC11049-002
03/08/2021 1400
03/11/2021
Solid
% Solids:83.6 03/11/2021 2358
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 03/15/2021 1035 AMR 03/12/2021 1144 85529
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.71 J 1mg/kg0.241.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 16
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
FG-3
WC11049-003
03/08/2021 0915
03/11/2021
Solid
% Solids:85.7 03/11/2021 2358
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 03/15/2021 1048 AMR 03/12/2021 1144 85529
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.231.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 16
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
FG-4
WC11049-004
03/08/2021 1100
03/11/2021
Solid
% Solids:82.2 03/11/2021 2358
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 03/15/2021 1101 AMR 03/12/2021 1144 85529
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.241.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 16
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
FG-Dup
WC11049-005
03/08/2021
03/11/2021
Solid
% Solids:82.7 03/11/2021 2358
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 03/15/2021 1126 AMR 03/12/2021 1144 85529
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.41 J 1mg/kg0.241.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 16
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 16
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ85529-001
85529 3060A
03/12/2021 1144Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 03/15/2021 09431.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
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Page 11 of 16
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ85529-002
85529 3060A
03/12/2021 1144Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 9.2 03/15/2021 0956921080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
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Page 12 of 16
Inorganic non-metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:WC11049-004MS
85529 3060A
03/12/2021 1144Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/kg) (mg/kg) (mg/kg)
Hexavalent Chromium 1200 03/15/2021 111393130075-125ND50
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 16
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 16
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 15 of 16
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 16 of 16
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Metals Analyses
6020B
V1529QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V1459
Associated Lab Samples: 94144, 94145, 94146, 94147, 94152
LRB-V1459 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/10/21 14:550.1000.0840<0.0840mg/KgArsenic
03/10/21 14:5510.00.360<0.360mg/KgBarium
03/10/21 14:550.5000.0370<0.0370mg/KgCadmium
03/10/21 14:551.000.240<0.240mg/KgChromium
03/10/21 14:551.000.0760<0.0760mg/KgLead
03/10/21 14:551.000.230<0.230mg/KgSelenium
03/10/21 14:550.5000.0510<0.0510mg/KgSilver
LCS-V1459Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.011.812.5mg/KgArsenic 80-120
10112.612.5mg/KgBarium 80-120
98.012.212.5mg/KgCadmium 80-120
95.011.912.5mg/KgChromium 80-120
98.012.312.5mg/KgLead 80-120
99.012.412.5mg/KgSelenium 80-120
94.04.725.00mg/KgSilver 80-120
V 93663-MS-V1459 V 93663-MSD-V1459Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
10.9 79.010.812.512.51.06mg/KgArsenic 78.0 75-125 0.9 20
64.7 11864.512.512.550.0mg/KgBarium 116 75-125 0.3 20
12.2 98.012.112.512.50.0428mg/KgCadmium 97.0 75-125 0.8 20
17.7 89.017.312.512.56.58mg/KgChromium 86.0 75-125 2.2 20
Page 1 of 34Date:03/16/2021 03:25 PM
Page 75 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Metals Analyses
6020B
V1529QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V1459
V 93663-MS-V1459 V 93663-MSD-V1459Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
20.9 97.020.412.512.58.76mg/KgLead 93.0 75-125 2.4 20
12.6 84.012.712.512.52.06mg/KgSelenium 85.0 75-125 0.7 20
4.75 95.04.745.005.00<0.0510mg/KgSilver 95.0 75-125 0.2 20
V 93663-PDS-V1459Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
03/10/21 15:2795.012.4mg/KgArsenic
03/10/21 15:2710238.3mg/KgBarium
03/10/21 15:2797.012.1mg/KgCadmium
03/10/21 15:2794.014.9mg/KgChromium
03/10/21 15:2797.016.4mg/KgLead
03/10/21 15:2798.013.2mg/KgSelenium
03/10/21 15:2797.012.1mg/KgSilver
Page 2 of 34Date:03/16/2021 03:25 PM
Page 76 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V1511QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V1467
Associated Lab Samples: 94144, 94145, 94146, 94147, 94152
LRB-V1467 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/10/21 11:430.05000.0150<0.0150mg/KgMercury (Total)
LCS-V1467Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1010.4220.417mg/KgMercury (Total)80-120
V 94184-MS-V1467 V 94184-MSD-V1467Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.431 1030.4250.4170.417<0.0150mg/KgMercury (Total)102 80-120 1.4 20
V 94184-PDS-V1467Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
03/10/21 12:061030.214mg/KgMercury (Total)
Page 3 of 34Date:03/16/2021 03:25 PM
Page 77 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V1542
Associated Lab Samples: 94153
LRB-V1542 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/10/21 14:425.000.3101.26µg/LAcetone
03/10/21 14:4220.00.200<0.200µg/LAcrolein
03/10/21 14:4220.00.200<0.200µg/LAcrylonitrile
03/10/21 14:420.5000.048<0.048µg/LBenzene
03/10/21 14:420.5000.057<0.057µg/LBromobenzene
03/10/21 14:420.5000.140<0.140µg/LBromochloromethane
03/10/21 14:420.5000.062<0.062µg/LBromodichloromethane
03/10/21 14:421.000.040<0.040µg/LBromoform
03/10/21 14:421.000.180<0.180µg/LBromomethane
03/10/21 14:421.000.076<0.076µg/Ln-Butylbenzene
03/10/21 14:420.5000.076<0.076µg/Lsec-Butyl benzene
03/10/21 14:420.5000.088<0.088µg/Ltert-Butyl benzene
03/10/21 14:425.000.075<0.075µg/LCarbon Disulfide
03/10/21 14:420.5000.110<0.110µg/LCarbon Tetrachloride
03/10/21 14:420.5000.062<0.062µg/LChlorobenzene
03/10/21 14:420.5000.081<0.081µg/LChlorodibromomethane
03/10/21 14:420.5000.220<0.220µg/LChloroethane
03/10/21 14:420.5000.076<0.076µg/LChloroform
03/10/21 14:420.5000.079<0.079µg/LChloromethane
03/10/21 14:420.5000.066<0.066µg/L2-Chlorotoluene
03/10/21 14:420.5000.050<0.050µg/L4-Chlorotoluene
03/10/21 14:425.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
03/10/21 14:422.000.170<0.170µg/L1,2-Dibromo-3-Chloropropane
03/10/21 14:420.5000.051<0.051µg/L1,2-Dibromoethane
03/10/21 14:420.5000.065<0.065µg/LDibromomethane
03/10/21 14:420.5000.076<0.076µg/L1,2-Dichlorobenzene
03/10/21 14:420.5000.054<0.054µg/L1,3-Dichlorobenzene
Page 4 of 34Date:03/16/2021 03:25 PM
Page 78 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V1542
Associated Lab Samples: 94153
LRB-V1542 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/10/21 14:420.5000.050<0.050µg/L1,4-Dichlorobenzene
03/10/21 14:425.000.110<0.110µg/LDichlorodifluoromethane
03/10/21 14:420.5000.083<0.083µg/L1,1-Dichloroethane
03/10/21 14:420.5000.066<0.066µg/L1,2-Dichloroethane
03/10/21 14:420.5000.083<0.083µg/L1,1-Dichloroethene
03/10/21 14:420.5000.056<0.056µg/Lcis-1,2-Dichloroethene
03/10/21 14:420.5000.094<0.094µg/Ltrans-1,2-Dichloroethene
03/10/21 14:420.5000.110<0.110µg/L1,2-Dichloropropane
03/10/21 14:420.5000.043<0.043µg/L1,3-Dichloropropane
03/10/21 14:422.000.110<0.110µg/L2,2-Dichloropropane
03/10/21 14:420.5000.051<0.051µg/L1,1-Dichloropropene
03/10/21 14:420.5000.079<0.079µg/Lcis-1,3-Dichloropropene
03/10/21 14:420.5000.070<0.070µg/Ltrans-1,3-Dichloropropene
03/10/21 14:4220027.0<27.0µg/LEthanol
03/10/21 14:420.5000.061<0.061µg/LEthylbenzene
03/10/21 14:4210.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
03/10/21 14:422.000.160<0.160µg/LHexachlorobutadiene
03/10/21 14:4210.00.760<0.760µg/Ln-Hexane
03/10/21 14:425.000.065<0.065µg/L2-Hexanone
03/10/21 14:425.000.330<0.330µg/LIsopropylbenzene
03/10/21 14:420.5000.089<0.089µg/L4-Isopropyl toluene
03/10/21 14:425.000.240<0.240µg/LMethyl Ethyl Ketone (MEK)
03/10/21 14:420.5000.042<0.042µg/LMethyl tert-butyl ether (MTBE)
03/10/21 14:425.001.00<1.00µg/L4-Methyl-2-Pentanone
03/10/21 14:421.000.083<0.083µg/LMethylene Chloride
03/10/21 14:421.000.300<0.300µg/LNaphthalene
03/10/21 14:420.5000.087<0.087µg/Ln-Propylbenzene
Page 5 of 34Date:03/16/2021 03:25 PM
Page 79 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V1542
Associated Lab Samples: 94153
LRB-V1542 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/10/21 14:420.5000.047<0.047µg/LStyrene
03/10/21 14:420.5000.110<0.110µg/L1,1,1,2-Tetrachloroethane
03/10/21 14:420.5000.036<0.036µg/L1,1,2,2-Tetrachloroethane
03/10/21 14:420.5000.098<0.098µg/LTetrachloroethene
03/10/21 14:420.5000.044<0.044µg/LToluene
03/10/21 14:422.000.400<0.400µg/L1,2,3-Trichlorobenzene
03/10/21 14:421.000.130<0.130µg/L1,2,4-Trichlorobenzene
03/10/21 14:420.5000.061<0.061µg/L1,1,1-Trichloroethane
03/10/21 14:420.5000.066<0.066µg/L1,1,2-Trichloroethane
03/10/21 14:420.5000.078<0.078µg/LTrichloroethene
03/10/21 14:420.5000.062<0.062µg/LTrichlorofluoromethane
03/10/21 14:421.000.140<0.140µg/L1,2,3-Trichloropropane
03/10/21 14:420.5000.076<0.076µg/L1,3,5-Trimethylbenzene
03/10/21 14:422.000.060<0.060µg/LVinyl Acetate
03/10/21 14:420.5000.097<0.097µg/LVinyl Chloride
03/10/21 14:420.5000.044<0.044µg/Lo-Xylene
03/10/21 14:421.000.120<0.120µg/Lm,p-Xylene
03/10/21 14:424-Bromofluorobenzene (S)97.4 80-124
03/10/21 14:42Dibromofluoromethane (S)98.8 75-129
03/10/21 14:421,2-Dichloroethane - d4 (S)99.6 63-136
03/10/21 14:42Toluene-d8 (S)94.6 77-123
LCS-V1542 LCSD-V1542Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.7 91.793.737.540.0µg/LAcetone 40-166 2.1 20
Page 6 of 34Date:03/16/2021 03:25 PM
Page 80 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V1542
LCS-V1542 LCSD-V1542Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
43.9 11012851.240.0µg/LAcrolein 70-130 15.3 20
43.0 10811144.340.0µg/LAcrylonitrile 81-127 2.9 20
19.5 97.510120.220.0µg/LBenzene 77-128 3.5 20
17.7 88.593.018.620.0µg/LBromobenzene 78-129 4.9 20
20.6 10310020.020.0µg/LBromochloromethane 78-135 2.9 20
20.1 10110921.720.0µg/LBromodichloromethane 76-138 7.6 20
20.2 10110520.920.0µg/LBromoform 71-135 3.4 20
20.4 10210220.320.0µg/LBromomethane 41-168 0.4 20
18.2 91.092.518.520.0µg/Ln-Butylbenzene 68-134 1.6 20
17.9 89.593.518.720.0µg/Lsec-Butyl benzene 71-131 4.3 20
17.5 87.594.518.920.0µg/Ltert-Butyl benzene 70-132 7.6 20
18.8 94.010020.020.0µg/LCarbon Disulfide 59-135 6.1 20
21.1 10611422.720.0µg/LCarbon Tetrachloride 72-142 7.3 20
18.9 94.598.019.620.0µg/LChlorobenzene 78-119 3.6 20
19.6 98.010020.020.0µg/LChlorodibromomethane 75-134 2.0 20
20.1 10110220.420.0µg/LChloroethane 57-142 1.4 20
20.3 10210420.720.0µg/LChloroform 77-130 1.9 20
19.1 95.510520.920.0µg/LChloromethane 47-145 9.0 20
17.7 88.592.018.420.0µg/L2-Chlorotoluene 74-126 3.8 20
17.4 87.092.018.420.0µg/L4-Chlorotoluene 78-129 5.5 20
20.3 10210521.020.0µg/LDi-Isopropyl Ether (DIPE)60-154 3.3 20
18.7 93.598.019.620.0µg/L1,2-Dibromo-3-Chloropropane 63-134 4.6 20
19.8 99.010120.120.0µg/L1,2-Dibromoethane 77-135 1.5 20
21.1 10611021.920.0µg/LDibromomethane 76-138 3.7 20
18.3 91.594.518.920.0µg/L1,2-Dichlorobenzene 78-128 3.2 20
18.3 91.594.018.820.0µg/L1,3-Dichlorobenzene 77-125 2.6 20
Page 7 of 34Date:03/16/2021 03:25 PM
Page 81 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V1542
LCS-V1542 LCSD-V1542Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.9 89.588.517.720.0µg/L1,4-Dichlorobenzene 75-126 1.1 20
26.1 13113226.420.0µg/LDichlorodifluoromethane 28-163 1.1 20
19.9 99.596.519.320.0µg/L1,1-Dichloroethane 70-130 3.0 20
20.6 10310420.720.0µg/L1,2-Dichloroethane 68-131 0.4 20
19.3 96.510520.920.0µg/L1,1-Dichloroethene 70-154 7.9 20
19.1 95.599.519.920.0µg/Lcis-1,2-Dichloroethene 76-141 4.1 20
18.8 94.010220.420.0µg/Ltrans-1,2-Dichloroethene 76-135 8.1 20
19.5 97.597.019.420.0µg/L1,2-Dichloropropane 77-130 0.5 20
19.2 96.098.519.720.0µg/L1,3-Dichloropropane 76-132 2.5 20
20.4 10211022.020.0µg/L2,2-Dichloropropane 29-149 7.5 20
19.0 95.010220.320.0µg/L1,1-Dichloropropene 71-136 6.6 20
20.2 10110120.220.0µg/Lcis-1,3-Dichloropropene 65-140 0.0 20
21.1 10610721.320.0µg/Ltrans-1,3-Dichloropropene 67-140 0.9 20
497 99.4108539500µg/LEthanol 70-130 8.1 20
18.7 93.597.019.420.0µg/LEthylbenzene 80-127 3.6 20
42.7 10710943.540.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 1.8 20
19.1 95.510020.020.0µg/LHexachlorobutadiene 61-134 4.6 20
18.0 90.010420.720.0µg/Ln-Hexane 70-130 13.9 20
19.8 99.099.519.920.0µg/L2-Hexanone 64-137 0.5 20
17.9 89.591.518.320.0µg/LIsopropylbenzene 70-130 2.2 20
17.6 88.093.018.620.0µg/L4-Isopropyl toluene 69-132 5.5 20
18.3 91.599.519.920.0µg/LMethyl Ethyl Ketone (MEK)71-134 8.3 20
20.9 10511122.120.0µg/LMethyl tert-butyl ether (MTBE)68-135 5.5 20
20.2 10110821.520.0µg/L4-Methyl-2-Pentanone 69-134 6.2 20
19.4 97.010220.320.0µg/LMethylene Chloride 73-131 4.5 20
16.8 84.082.016.420.0µg/LNaphthalene 64-136 2.4 20
Page 8 of 34Date:03/16/2021 03:25 PM
Page 82 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1543QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V1542
LCS-V1542 LCSD-V1542Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.9 89.594.018.820.0µg/Ln-Propylbenzene 72-132 4.9 20
18.6 93.097.019.420.0µg/LStyrene 78-129 4.2 20
19.3 96.597.019.420.0µg/L1,1,1,2-Tetrachloroethane 79-134 0.5 20
17.5 87.592.018.420.0µg/L1,1,2,2-Tetrachloroethane 62-127 5.0 20
19.8 99.010420.720.0µg/LTetrachloroethene 80-129 4.4 20
19.9 99.510521.020.0µg/LToluene 76-131 5.3 20
18.0 90.088.517.720.0µg/L1,2,3-Trichlorobenzene 58-144 1.6 20
18.4 92.092.018.420.0µg/L1,2,4-Trichlorobenzene 66-139 0.0 20
20.3 10210921.720.0µg/L1,1,1-Trichloroethane 75-135 6.6 20
19.9 99.510320.520.0µg/L1,1,2-Trichloroethane 70-140 2.9 20
19.1 95.510120.220.0µg/LTrichloroethene 77-133 5.5 20
21.5 10811222.420.0µg/LTrichlorofluoromethane 62-148 4.1 20
19.1 95.596.519.320.0µg/L1,2,3-Trichloropropane 71-127 1.0 20
18.7 93.593.518.720.0µg/L1,3,5-Trimethylbenzene 75-131 0.0 20
21.8 10911522.920.0µg/LVinyl Acetate 34-167 4.9 20
21.1 10611122.120.0µg/LVinyl Chloride 57-141 4.6 20
18.9 94.597.019.420.0µg/Lo-Xylene 78-128 2.6 20
39.8 99.510441.640.0µg/Lm,p-Xylene 77-133 4.4 20
96.496.84-Bromofluorobenzene (S)80-124
98.498.4Dibromofluoromethane (S)75-129
99.61071,2-Dichloroethane - d4 (S)63-136
95.296.2Toluene-d8 (S)77-123
Page 9 of 34Date:03/16/2021 03:25 PM
Page 83 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1590QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1588
Associated Lab Samples: 94148, 94149, 94150, 94151
LRB-V1588 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/11/21 10:150.0200.015<0.015mg/KgAcetone
03/11/21 10:150.0200.0009<0.0009mg/KgAcrolein
03/11/21 10:150.0200.001<0.001mg/KgAcrylonitrile
03/11/21 10:150.0050.0008<0.0008mg/KgBenzene
03/11/21 10:150.0050.0007<0.0007mg/KgBromobenzene
03/11/21 10:150.0050.0008<0.0008mg/KgBromochloromethane
03/11/21 10:150.0050.0005<0.0005mg/KgBromodichloromethane
03/11/21 10:150.0050.0004<0.0004mg/KgBromoform
03/11/21 10:150.0100.002<0.002mg/KgBromomethane
03/11/21 10:150.0050.0005<0.0005mg/Kgn-Butylbenzene
03/11/21 10:150.0050.0005<0.0005mg/Kgsec-Butyl benzene
03/11/21 10:150.0050.0006<0.0006mg/Kgtert-Butyl benzene
03/11/21 10:150.0050.0009<0.0009mg/KgCarbon Disulfide
03/11/21 10:150.0050.0010<0.0010mg/KgCarbon Tetrachloride
03/11/21 10:150.0050.0008<0.0008mg/KgChlorobenzene
03/11/21 10:150.0050.0003<0.0003mg/KgChlorodibromomethane
03/11/21 10:150.0100.0010<0.0010mg/KgChloroethane
03/11/21 10:150.0050.0006<0.0006mg/KgChloroform
03/11/21 10:150.0100.001<0.001mg/KgChloromethane
03/11/21 10:150.0050.0007<0.0007mg/Kg2-Chlorotoluene
03/11/21 10:150.0050.0006<0.0006mg/Kg4-Chlorotoluene
03/11/21 10:150.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
03/11/21 10:150.0100.0006<0.0006mg/Kg1,2-Dibromo-3-Chloropropane
03/11/21 10:150.0050.0005<0.0005mg/Kg1,2-Dibromoethane
03/11/21 10:150.0050.0006<0.0006mg/KgDibromomethane
03/11/21 10:150.0050.0006<0.0006mg/Kg1,2-Dichlorobenzene
03/11/21 10:150.0050.0006<0.0006mg/Kg1,3-Dichlorobenzene
Page 10 of 34Date:03/16/2021 03:25 PM
Page 84 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1590QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1588
Associated Lab Samples: 94148, 94149, 94150, 94151
LRB-V1588 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/11/21 10:150.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
03/11/21 10:150.0100.001<0.001mg/KgDichlorodifluoromethane
03/11/21 10:150.0050.0009<0.0009mg/Kg1,1-Dichloroethane
03/11/21 10:150.0050.0006<0.0006mg/Kg1,2-Dichloroethane
03/11/21 10:150.0050.0009<0.0009mg/Kg1,1-Dichloroethene
03/11/21 10:150.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
03/11/21 10:150.0050.0010<0.0010mg/Kgtrans-1,2-Dichloroethene
03/11/21 10:150.0050.0008<0.0008mg/Kg1,2-Dichloropropane
03/11/21 10:150.0050.0004<0.0004mg/Kg1,3-Dichloropropane
03/11/21 10:150.0050.0006<0.0006mg/Kg2,2-Dichloropropane
03/11/21 10:150.0050.0008<0.0008mg/Kg1,1-Dichloropropene
03/11/21 10:150.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
03/11/21 10:150.0050.0004<0.0004mg/Kgtrans-1,3-Dichloropropene
03/11/21 10:150.2500.018<0.018mg/KgEthanol
03/11/21 10:150.0050.0008<0.0008mg/KgEthylbenzene
03/11/21 10:150.0500.0004<0.0004mg/KgEthyl Tertiary Butyl Ether (ETBE)
03/11/21 10:150.0100.0008<0.0008mg/KgHexachlorobutadiene
03/11/21 10:150.0100.0006<0.0006mg/Kgn-Hexane
03/11/21 10:150.0200.0004<0.0004mg/Kg2-Hexanone
03/11/21 10:150.0050.0006<0.0006mg/KgIsopropylbenzene
03/11/21 10:150.0050.001<0.001mg/Kg4-Isopropyl toluene
03/11/21 10:150.0200.001<0.001mg/KgMethyl Ethyl Ketone (MEK)
03/11/21 10:150.0050.0007<0.0007mg/KgMethyl tert-butyl ether (MTBE)
03/11/21 10:150.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
03/11/21 10:150.0100.005<0.005mg/KgMethylene Chloride
03/11/21 10:150.0100.0005<0.0005mg/KgNaphthalene
03/11/21 10:150.0050.0007<0.0007mg/Kgn-Propylbenzene
Page 11 of 34Date:03/16/2021 03:25 PM
Page 85 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1590QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1588
Associated Lab Samples: 94148, 94149, 94150, 94151
LRB-V1588 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/11/21 10:150.0050.0005<0.0005mg/KgStyrene
03/11/21 10:150.0050.0006<0.0006mg/Kg1,1,1,2-Tetrachloroethane
03/11/21 10:150.0050.0004<0.0004mg/Kg1,1,2,2-Tetrachloroethane
03/11/21 10:150.0050.0009<0.0009mg/KgTetrachloroethene
03/11/21 10:150.0050.0008<0.0008mg/KgToluene
03/11/21 10:150.0100.0007<0.0007mg/Kg1,2,3-Trichlorobenzene
03/11/21 10:150.0100.0005<0.0005mg/Kg1,2,4-Trichlorobenzene
03/11/21 10:150.0050.0007<0.0007mg/Kg1,1,1-Trichloroethane
03/11/21 10:150.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
03/11/21 10:150.0050.0010<0.0010mg/KgTrichloroethene
03/11/21 10:150.0100.001<0.001mg/KgTrichlorofluoromethane
03/11/21 10:150.0050.0006<0.0006mg/Kg1,2,3-Trichloropropane
03/11/21 10:150.0050.0006<0.0006mg/Kg1,3,5-Trimethylbenzene
03/11/21 10:150.0100.0005<0.0005mg/KgVinyl Acetate
03/11/21 10:150.0100.0010<0.0010mg/KgVinyl Chloride
03/11/21 10:150.0050.0005<0.0005mg/Kgo-Xylene
03/11/21 10:150.0100.001<0.001mg/Kgm,p-Xylene
03/11/21 10:154-Bromofluorobenzene (S)93.0 70-130
03/11/21 10:15Dibromofluoromethane (S)98.0 84-123
03/11/21 10:15Toluene-d8 (S)82.0 76-129
LCS-V1588 LCSD-V1588Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.109 1091120.1120.100mg/KgAcetone 29-198 2.7 20
0.103 10399.40.0990.100mg/KgAcrolein 70-130 3.5 20
Page 12 of 34Date:03/16/2021 03:25 PM
Page 86 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1590QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1588
LCS-V1588 LCSD-V1588Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.107 1071020.1020.100mg/KgAcrylonitrile 65-134 4.7 20
0.051 1041100.0550.050mg/KgBenzene 74-127 6.1 20
0.041 82.286.60.0430.050mg/KgBromobenzene 73-125 5.2 20
0.056 1141160.0580.050mg/KgBromochloromethane 72-134 2.2 20
0.059 119124*0.0620.050mg/KgBromodichloromethane 75-122 4.2 20
0.053 1061070.0530.050mg/KgBromoform 66-135 0.9 20
0.044 88.895.60.0470.050mg/KgBromomethane 20-180 7.3 20
0.044 89.296.60.0480.050mg/Kgn-Butylbenzene 65-135 7.9 20
0.043 87.293.00.0460.050mg/Kgsec-Butyl benzene 66-131 6.4 20
0.043 87.492.40.0460.050mg/Kgtert-Butyl benzene 67-132 5.5 20
0.050 1021140.0570.050mg/KgCarbon Disulfide 61-129 11.6 20
0.063 1261400.0690.050mg/KgCarbon Tetrachloride 64-143 10.2 20
0.048 97.699.00.0490.050mg/KgChlorobenzene 74-118 1.4 20
0.049 99.41010.0500.050mg/KgChlorodibromomethane 73-122 1.7 20
0.042 85.090.80.0450.050mg/KgChloroethane 33-149 6.5 20
0.056 1121190.0590.050mg/KgChloroform 73-127 5.7 20
0.047 94.81010.0500.050mg/KgChloromethane 45-143 6.5 20
0.042 84.891.00.0450.050mg/Kg2-Chlorotoluene 67-124 7.0 20
0.042 84.891.00.0450.050mg/Kg4-Chlorotoluene 71-126 7.0 20
0.052 1061110.0550.050mg/KgDi-Isopropyl Ether (DIPE)59-159 4.4 20
0.043 86.883.40.0410.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.9 20
0.048 96.497.40.0480.050mg/Kg1,2-Dibromoethane 70-132 1.0 20
0.055 1121180.0590.050mg/KgDibromomethane 74-133 5.9 20
0.042 85.088.60.0440.050mg/Kg1,2-Dichlorobenzene 72-123 4.1 20
0.043 87.691.20.0450.050mg/Kg1,3-Dichlorobenzene 71-120 4.0 20
0.043 87.494.00.0470.050mg/Kg1,4-Dichlorobenzene 71-123 7.2 20
Page 13 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 87 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1590QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1588
LCS-V1588 LCSD-V1588Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.054 1081210.0600.050mg/KgDichlorodifluoromethane 26-146 11.3 20
0.053 1081140.0570.050mg/Kg1,1-Dichloroethane 74-127 5.9 20
0.061 1221260.0620.050mg/Kg1,2-Dichloroethane 68-128 2.5 20
0.053 1081180.0590.050mg/Kg1,1-Dichloroethene 67-149 9.3 20
0.054 1091130.0560.050mg/Kgcis-1,2-Dichloroethene 76-134 3.7 20
0.052 1051130.0560.050mg/Kgtrans-1,2-Dichloroethene 73-132 7.3 20
0.052 1051080.0530.050mg/Kg1,2-Dichloropropane 73-130 2.4 20
0.047 95.294.40.0470.050mg/Kg1,3-Dichloropropane 75-124 0.8 20
0.059 1201280.0640.050mg/Kg2,2-Dichloropropane 50-142 6.9 20
0.056 1131190.0590.050mg/Kg1,1-Dichloropropene 71-130 5.5 20
0.055 1121150.0570.050mg/Kgcis-1,3-Dichloropropene 71-125 2.8 20
0.057 1161200.0600.050mg/Kgtrans-1,3-Dichloropropene 68-123 3.7 20
1.21 96.888.01.101.25mg/KgEthanol 70-130 9.5 20
0.049 98.21040.0510.050mg/KgEthylbenzene 74-128 5.5 20
0.115 1151180.1180.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 2.5 20
0.048 97.01070.0530.050mg/KgHexachlorobutadiene 64-125 9.4 20
0.058 1161250.0620.050mg/Kgn-Hexane 70-130 6.8 20
0.049 98.896.80.0480.050mg/Kg2-Hexanone 61-157 2.0 20
0.042 85.291.80.0450.050mg/KgIsopropylbenzene 68-126 7.4 20
0.044 89.094.00.0470.050mg/Kg4-Isopropyl toluene 68-129 5.4 20
0.055 1111070.0530.050mg/KgMethyl Ethyl Ketone (MEK)63-149 2.9 20
0.056 1121140.0560.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.2 20
0.053 1071070.0530.050mg/Kg4-Methyl-2-Pentanone 57-162 0.0 20
0.046 93.097.00.0480.050mg/KgMethylene Chloride 74-129 4.2 20
0.043 86.685.60.0420.050mg/KgNaphthalene 57-157 1.1 20
0.043 86.291.80.0450.050mg/Kgn-Propylbenzene 67-130 6.2 20
Page 14 of 34Date:03/16/2021 03:25 PM
Page 88 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1590QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1588
LCS-V1588 LCSD-V1588Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.049 99.81020.0510.050mg/KgStyrene 77-121 2.1 20
0.051 1031070.0530.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.1 20
0.038 77.477.00.0380.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.5 20
0.058 1171280.0630.050mg/KgTetrachloroethene 68-130 8.6 20
0.054 1081140.0570.050mg/KgToluene 71-129 5.7 20
0.045 91.095.20.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 4.5 20
0.046 92.295.40.0470.050mg/Kg1,2,4-Trichlorobenzene 66-125 3.4 20
0.061 123133*0.0660.050mg/Kg1,1,1-Trichloroethane 67-131 7.9 20
0.046 93.493.40.0460.050mg/Kg1,1,2-Trichloroethane 70-133 0.0 20
0.055 1121190.0590.050mg/KgTrichloroethene 75-133 6.2 20
0.063 1261400.0700.050mg/KgTrichlorofluoromethane 44-146 10.3 20
0.042 85.886.20.0430.050mg/Kg1,2,3-Trichloropropane 60-137 0.4 20
0.042 85.291.80.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 7.4 20
0.054 1081050.0520.050mg/KgVinyl Acetate 85-161 3.5 20
0.047 95.61070.0530.050mg/KgVinyl Chloride 48-147 10.8 20
0.049 98.61030.0510.050mg/Kgo-Xylene 74-126 4.3 20
0.102 1021060.1060.100mg/Kgm,p-Xylene 75-124 3.8 20
92.693.44-Bromofluorobenzene (S)70-130
96.698.6Dibromofluoromethane (S)84-123
84.283.6Toluene-d8 (S)76-129
Page 15 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 89 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1657QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1656
Associated Lab Samples: 94152
LRB-V1656 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/12/21 12:160.0200.015<0.015mg/KgAcetone
03/12/21 12:160.0200.0009<0.0009mg/KgAcrolein
03/12/21 12:160.0200.001<0.001mg/KgAcrylonitrile
03/12/21 12:160.0050.0008<0.0008mg/KgBenzene
03/12/21 12:160.0050.0007<0.0007mg/KgBromobenzene
03/12/21 12:160.0050.0008<0.0008mg/KgBromochloromethane
03/12/21 12:160.0050.0005<0.0005mg/KgBromodichloromethane
03/12/21 12:160.0050.0004<0.0004mg/KgBromoform
03/12/21 12:160.0100.002<0.002mg/KgBromomethane
03/12/21 12:160.0050.0005<0.0005mg/Kgn-Butylbenzene
03/12/21 12:160.0050.0005<0.0005mg/Kgsec-Butyl benzene
03/12/21 12:160.0050.0006<0.0006mg/Kgtert-Butyl benzene
03/12/21 12:160.0050.0009<0.0009mg/KgCarbon Disulfide
03/12/21 12:160.0050.0010<0.0010mg/KgCarbon Tetrachloride
03/12/21 12:160.0050.0008<0.0008mg/KgChlorobenzene
03/12/21 12:160.0050.0003<0.0003mg/KgChlorodibromomethane
03/12/21 12:160.0100.0010<0.0010mg/KgChloroethane
03/12/21 12:160.0050.0006<0.0006mg/KgChloroform
03/12/21 12:160.0100.001<0.001mg/KgChloromethane
03/12/21 12:160.0050.0007<0.0007mg/Kg2-Chlorotoluene
03/12/21 12:160.0050.0006<0.0006mg/Kg4-Chlorotoluene
03/12/21 12:160.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
03/12/21 12:160.0100.0006<0.0006mg/Kg1,2-Dibromo-3-Chloropropane
03/12/21 12:160.0050.0005<0.0005mg/Kg1,2-Dibromoethane
03/12/21 12:160.0050.0006<0.0006mg/KgDibromomethane
03/12/21 12:160.0050.0006<0.0006mg/Kg1,2-Dichlorobenzene
03/12/21 12:160.0050.0006<0.0006mg/Kg1,3-Dichlorobenzene
Page 16 of 34Date:03/16/2021 03:25 PM
Page 90 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1657QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1656
Associated Lab Samples: 94152
LRB-V1656 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/12/21 12:160.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
03/12/21 12:160.0100.001<0.001mg/KgDichlorodifluoromethane
03/12/21 12:160.0050.0009<0.0009mg/Kg1,1-Dichloroethane
03/12/21 12:160.0050.0006<0.0006mg/Kg1,2-Dichloroethane
03/12/21 12:160.0050.0009<0.0009mg/Kg1,1-Dichloroethene
03/12/21 12:160.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
03/12/21 12:160.0050.0010<0.0010mg/Kgtrans-1,2-Dichloroethene
03/12/21 12:160.0050.0008<0.0008mg/Kg1,2-Dichloropropane
03/12/21 12:160.0050.0004<0.0004mg/Kg1,3-Dichloropropane
03/12/21 12:160.0050.0006<0.0006mg/Kg2,2-Dichloropropane
03/12/21 12:160.0050.0008<0.0008mg/Kg1,1-Dichloropropene
03/12/21 12:160.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
03/12/21 12:160.0050.0004<0.0004mg/Kgtrans-1,3-Dichloropropene
03/12/21 12:160.2500.018<0.018mg/KgEthanol
03/12/21 12:160.0050.0008<0.0008mg/KgEthylbenzene
03/12/21 12:160.0500.0004<0.0004mg/KgEthyl Tertiary Butyl Ether (ETBE)
03/12/21 12:160.0100.0008<0.0008mg/KgHexachlorobutadiene
03/12/21 12:160.0100.0006<0.0006mg/Kgn-Hexane
03/12/21 12:160.0200.0004<0.0004mg/Kg2-Hexanone
03/12/21 12:160.0050.0006<0.0006mg/KgIsopropylbenzene
03/12/21 12:160.0050.001<0.001mg/Kg4-Isopropyl toluene
03/12/21 12:160.0200.001<0.001mg/KgMethyl Ethyl Ketone (MEK)
03/12/21 12:160.0050.0007<0.0007mg/KgMethyl tert-butyl ether (MTBE)
03/12/21 12:160.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
03/12/21 12:160.0100.005<0.005mg/KgMethylene Chloride
03/12/21 12:160.0100.0005<0.0005mg/KgNaphthalene
03/12/21 12:160.0050.0007<0.0007mg/Kgn-Propylbenzene
Page 17 of 34Date:03/16/2021 03:25 PM
Page 91 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1657QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1656
Associated Lab Samples: 94152
LRB-V1656 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/12/21 12:160.0050.0005<0.0005mg/KgStyrene
03/12/21 12:160.0050.0006<0.0006mg/Kg1,1,1,2-Tetrachloroethane
03/12/21 12:160.0050.0004<0.0004mg/Kg1,1,2,2-Tetrachloroethane
03/12/21 12:160.0050.0009<0.0009mg/KgTetrachloroethene
03/12/21 12:160.0050.0008<0.0008mg/KgToluene
03/12/21 12:160.0100.0007<0.0007mg/Kg1,2,3-Trichlorobenzene
03/12/21 12:160.0100.0005<0.0005mg/Kg1,2,4-Trichlorobenzene
03/12/21 12:160.0050.0007<0.0007mg/Kg1,1,1-Trichloroethane
03/12/21 12:160.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
03/12/21 12:160.0050.0010<0.0010mg/KgTrichloroethene
03/12/21 12:160.0100.001<0.001mg/KgTrichlorofluoromethane
03/12/21 12:160.0050.0006<0.0006mg/Kg1,2,3-Trichloropropane
03/12/21 12:160.0050.0006<0.0006mg/Kg1,3,5-Trimethylbenzene
03/12/21 12:160.0100.0005<0.0005mg/KgVinyl Acetate
03/12/21 12:160.0100.0010<0.0010mg/KgVinyl Chloride
03/12/21 12:160.0050.0005<0.0005mg/Kgo-Xylene
03/12/21 12:160.0100.001<0.001mg/Kgm,p-Xylene
03/12/21 12:164-Bromofluorobenzene (S)98.0 70-130
03/12/21 12:16Dibromofluoromethane (S)99.0 84-123
03/12/21 12:16Toluene-d8 (S)83.4 76-129
LCS-V1656Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
84.30.0840.100mg/KgAcetone 29-198
1010.1010.100mg/KgAcrolein 70-130
1080.1080.100mg/KgAcrylonitrile 65-134
Page 18 of 34Date:03/16/2021 03:25 PM
Page 92 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1657QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1656
LCS-V1656Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
99.40.0490.050mg/KgBenzene 74-127
81.80.0400.050mg/KgBromobenzene 73-125
1120.0560.050mg/KgBromochloromethane 72-134
1170.0580.050mg/KgBromodichloromethane 75-122
1080.0530.050mg/KgBromoform 66-135
94.00.0470.050mg/KgBromomethane 20-180
84.20.0420.050mg/Kgn-Butylbenzene 65-135
81.80.0400.050mg/Kgsec-Butyl benzene 66-131
81.20.0400.050mg/Kgtert-Butyl benzene 67-132
92.20.0460.050mg/KgCarbon Disulfide 61-129
1160.0580.050mg/KgCarbon Tetrachloride 64-143
92.20.0460.050mg/KgChlorobenzene 74-118
1010.0500.050mg/KgChlorodibromomethane 73-122
83.00.0410.050mg/KgChloroethane 33-149
1100.0540.050mg/KgChloroform 73-127
94.20.0470.050mg/KgChloromethane 45-143
84.00.0420.050mg/Kg2-Chlorotoluene 67-124
84.00.0420.050mg/Kg4-Chlorotoluene 71-126
1030.0510.050mg/KgDi-Isopropyl Ether (DIPE)59-159
85.60.0420.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157
98.40.0490.050mg/Kg1,2-Dibromoethane 70-132
1140.0560.050mg/KgDibromomethane 74-133
85.80.0420.050mg/Kg1,2-Dichlorobenzene 72-123
85.80.0420.050mg/Kg1,3-Dichlorobenzene 71-120
86.40.0430.050mg/Kg1,4-Dichlorobenzene 71-123
1040.0520.050mg/KgDichlorodifluoromethane 26-146
1010.0500.050mg/Kg1,1-Dichloroethane 74-127
Page 19 of 34Date:03/16/2021 03:25 PM
Page 93 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1657QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1656
LCS-V1656Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1220.0600.050mg/Kg1,2-Dichloroethane 68-128
94.00.0470.050mg/Kg1,1-Dichloroethene 67-149
1040.0520.050mg/Kgcis-1,2-Dichloroethene 76-134
99.00.0490.050mg/Kgtrans-1,2-Dichloroethene 73-132
1040.0510.050mg/Kg1,2-Dichloropropane 73-130
95.20.0470.050mg/Kg1,3-Dichloropropane 75-124
1070.0530.050mg/Kg2,2-Dichloropropane 50-142
1010.0500.050mg/Kg1,1-Dichloropropene 71-130
1090.0540.050mg/Kgcis-1,3-Dichloropropene 71-125
1180.0590.050mg/Kgtrans-1,3-Dichloropropene 68-123
91.21.141.25mg/KgEthanol 70-130
92.40.0460.050mg/KgEthylbenzene 74-128
1150.1150.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130
92.80.0460.050mg/KgHexachlorobutadiene 64-125
96.40.0480.050mg/Kgn-Hexane 70-130
92.60.0460.050mg/Kg2-Hexanone 61-157
81.20.0400.050mg/KgIsopropylbenzene 68-126
83.20.0410.050mg/Kg4-Isopropyl toluene 68-129
94.20.0470.050mg/KgMethyl Ethyl Ketone (MEK)63-149
1120.0550.050mg/KgMethyl tert-butyl ether (MTBE)70-130
1080.0530.050mg/Kg4-Methyl-2-Pentanone 57-162
89.40.0440.050mg/KgMethylene Chloride 74-129
87.40.0430.050mg/KgNaphthalene 57-157
81.00.0400.050mg/Kgn-Propylbenzene 67-130
96.20.0480.050mg/KgStyrene 77-121
99.80.0490.050mg/Kg1,1,1,2-Tetrachloroethane 72-115
79.00.0390.050mg/Kg1,1,2,2-Tetrachloroethane 56-126
Page 20 of 34Date:03/16/2021 03:25 PM
Page 94 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1657QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1656
LCS-V1656Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1100.0550.050mg/KgTetrachloroethene 68-130
1030.0510.050mg/KgToluene 71-129
94.00.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130
92.80.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125
1130.0560.050mg/Kg1,1,1-Trichloroethane 67-131
94.00.0470.050mg/Kg1,1,2-Trichloroethane 70-133
1040.0520.050mg/KgTrichloroethene 75-133
1140.0560.050mg/KgTrichlorofluoromethane 44-146
84.80.0420.050mg/Kg1,2,3-Trichloropropane 60-137
81.20.0400.050mg/Kg1,3,5-Trimethylbenzene 69-128
1100.0550.050mg/KgVinyl Acetate 85-161
89.60.0440.050mg/KgVinyl Chloride 48-147
94.80.0470.050mg/Kgo-Xylene 74-126
96.10.0960.100mg/Kgm,p-Xylene 75-124
92.84-Bromofluorobenzene (S)70-130
97.4Dibromofluoromethane (S)84-123
82.2Toluene-d8 (S)76-129
V 94266-MS-V1656 V 94266-MSD-V1656Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.077 77.10.0890.1000.100<0.015mg/KgAcetone 89.1 34-143 14.4 49
0.018 0.0*0.0250.1000.100<0.0009mg/KgAcrolein 25.1*70-130 22.6*20
0.057 57.9*0.0630.1000.100<0.001mg/KgAcrylonitrile 63.9*65-134 9.8 30
0.033 66.20.0350.0500.050<0.0008mg/KgBenzene 71.0 60-135 6.9 20
0.017 34.0*0.0170.0500.050<0.0007mg/KgBromobenzene 34.4*45-135 1.1 25
Page 21 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 95 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1657QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1656
V 94266-MS-V1656 V 94266-MSD-V1656Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.029 58.80.0320.0500.050<0.0008mg/KgBromochloromethane 65.4 55-136 10.6 18
0.033 66.80.0360.0500.050<0.0005mg/KgBromodichloromethane 72.6 55-127 8.3 17
0.025 50.00.0260.0500.050<0.0004mg/KgBromoform 53.0 40-136 5.8 35
0.024 48.80.0290.0500.050<0.002mg/KgBromomethane 58.2 30-137 17.5 30
0.016 33.40.0160.0500.050<0.0005mg/Kgn-Butylbenzene 33.6 23-148 0.5 39
0.021 43.20.0210.0500.050<0.0005mg/Kgsec-Butyl benzene 43.8 34-144 1.3 28
0.024 48.40.0250.0500.050<0.0006mg/Kgtert-Butyl benzene 51.0 36-150 5.2 29
0.025 50.20.0260.0500.050<0.0009mg/KgCarbon Disulfide 53.2 49-139 5.8 26
0.045 90.80.0480.0500.050<0.0010mg/KgCarbon Tetrachloride 96.8 48-153 6.3 23
0.022 44.4*0.0230.0500.050<0.0008mg/KgChlorobenzene 46.4*57-125 4.4 14
0.026 52.80.0280.0500.050<0.0003mg/KgChlorodibromomethane 56.8 49-127 7.2 24
0.025 51.60.0290.0500.050<0.0010mg/KgChloroethane 58.4 16-177 12.3 47
0.037 74.00.0380.0500.050<0.0006mg/KgChloroform 77.8 56-137 5.0 18
0.032 64.00.0340.0500.050<0.001mg/KgChloromethane 68.8 40-145 7.2 26
0.017 34.8*0.0170.0500.050<0.0007mg/Kg2-Chlorotoluene 34.6*46-132 0.5 29
0.017 34.8*0.0170.0500.050<0.0006mg/Kg4-Chlorotoluene 34.6*44-135 0.5 23
0.038 76.20.0400.0500.050<0.0007mg/KgDi-Isopropyl Ether (DIPE)81.8 51-155 7.0 13
0.018 36.40.0200.0500.050<0.0006mg/Kg1,2-Dibromo-3-Chloropropane 40.2 27-132 9.9 25
0.019 39.2*0.0220.0500.050<0.0005mg/Kg1,2-Dibromoethane 44.4*49-132 12.4 15
0.026 53.0*0.0270.0500.050<0.0006mg/KgDibromomethane 55.2*59-133 4.0 15
0.016 32.8*0.0160.0500.050<0.0006mg/Kg1,2-Dichlorobenzene 32.6*42-130 0.6 21
0.016 32.6*0.0160.0500.050<0.0006mg/Kg1,3-Dichlorobenzene 32.2*41-129 1.2 24
0.015 30.0*0.0140.0500.050<0.0006mg/Kg1,4-Dichlorobenzene 29.8*44-134 0.6 21
0.026 52.60.0290.0500.050<0.001mg/KgDichlorodifluoromethane 58.0 25-151 9.7 37
0.037 74.80.0400.0500.050<0.0009mg/Kg1,1-Dichloroethane 81.4 59-137 8.4 21
0.033 66.20.0350.0500.050<0.0006mg/Kg1,2-Dichloroethane 71.4 51-131 7.5 13
Page 22 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 96 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1657QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1656
V 94266-MS-V1656 V 94266-MSD-V1656Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.033 67.80.0370.0500.050<0.0009mg/Kg1,1-Dichloroethene 74.2 54-162 9.0 22
0.027 55.0*0.0290.0500.050<0.0008mg/Kgcis-1,2-Dichloroethene 59.4 58-140 7.6 28
0.027 55.2*0.0280.0500.050<0.0010mg/Kgtrans-1,2-Dichloroethene 56.6*57-141 2.5 18
0.034 68.20.0360.0500.050<0.0008mg/Kg1,2-Dichloropropane 72.0 55-138 5.4 16
0.023 46.0*0.0250.0500.050<0.0004mg/Kg1,3-Dichloropropane 50.4*53-129 9.1 15
0.044 88.40.0470.0500.050<0.0006mg/Kg2,2-Dichloropropane 94.8 30-147 6.9 20
0.030 61.00.0310.0500.050<0.0008mg/Kg1,1-Dichloropropene 63.0 55-137 3.2 19
0.024 48.20.0260.0500.050<0.0005mg/Kgcis-1,3-Dichloropropene 52.0 42-135 7.5 32
0.019 39.2*0.0210.0500.050<0.0004mg/Kgtrans-1,3-Dichloropropene 42.0 41-124 6.8 20
0.741 59.2*0.8281.251.250.050mg/KgEthanol 66.2*70-130 11.0 20
0.024 49.80.0260.0500.050<0.0008mg/KgEthylbenzene 52.6 44-144 5.4 19
0.083 83.70.0900.1000.100<0.0004mg/KgEthyl Tertiary Butyl Ether (ETBE)90.8 70-130 8.1 20
0.020 40.40.0200.0500.050<0.0008mg/KgHexachlorobutadiene 41.0 30-126 1.4 26
0.027 54.0*0.0310.0500.050<0.0006mg/Kgn-Hexane 63.2*70-130 15.6 20
0.024 48.60.0270.0500.050<0.0004mg/Kg2-Hexanone 54.0 30-147 10.5 42
0.023 46.80.0240.0500.050<0.0006mg/KgIsopropylbenzene 49.2 41-140 5.0 27
0.020 41.60.0210.0500.050<0.001mg/Kg4-Isopropyl toluene 42.2 32-144 1.4 22
0.035 70.60.0410.0500.050<0.001mg/KgMethyl Ethyl Ketone (MEK)82.6 24-160 15.6 42
0.039 79.60.0440.0500.050<0.0007mg/KgMethyl tert-butyl ether (MTBE)89.2 49-135 11.3 22
0.034 68.00.0370.0500.050<0.015mg/Kg4-Methyl-2-Pentanone 75.6 25-163 10.5 44
0.027 55.60.0290.0500.050<0.005mg/KgMethylene Chloride 58.8 53-144 5.5 14
0.011 22.8*0.0100.0500.050<0.0005mg/KgNaphthalene 21.2*32-127 7.2 44
0.020 40.00.0200.0500.050<0.0007mg/Kgn-Propylbenzene 40.6 35-144 1.4 27
0.019 38.6*0.0200.0500.050<0.0005mg/KgStyrene 41.6*42-132 7.4 28
0.031 62.80.0340.0500.050<0.0006mg/Kg1,1,1,2-Tetrachloroethane 68.0 60-120 7.9 15
0.020 41.20.0220.0500.050<0.0004mg/Kg1,1,2,2-Tetrachloroethane 44.2 39-135 7.0 22
Page 23 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 97 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V1657QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V1656
V 94266-MS-V1656 V 94266-MSD-V1656Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.030 61.00.0320.0500.050<0.0009mg/KgTetrachloroethene 64.4 47-142 5.4 26
0.029 59.20.0310.0500.050<0.0008mg/KgToluene 63.4 57-135 6.8 22
0.011 23.0*0.0100.0500.050<0.0007mg/Kg1,2,3-Trichlorobenzene 20.4*34-120 11.9 41
0.011 22.0*0.0100.0500.050<0.0005mg/Kg1,2,4-Trichlorobenzene 20.0*35-116 9.5 62
0.044 89.40.0490.0500.050<0.0007mg/Kg1,1,1-Trichloroethane 98.2 52-139 9.3 21
0.027 54.20.0290.0500.050<0.0005mg/Kg1,1,2-Trichloroethane 58.2 44-140 7.1 21
0.030 60.00.0300.0500.050<0.0010mg/KgTrichloroethene 60.8 38-164 1.3 18
0.043 86.60.0470.0500.050<0.001mg/KgTrichlorofluoromethane 95.4 30-157 9.6 27
0.023 47.60.0250.0500.050<0.0006mg/Kg1,2,3-Trichloropropane 50.4 45-139 5.7 25
0.023 46.80.0240.0500.050<0.0006mg/Kg1,3,5-Trimethylbenzene 49.2 44-140 5.0 29
0.009 0.0*0.0050.0500.050<0.0005mg/KgVinyl Acetate 0.0*61-154 0.0 35
0.025 50.20.0260.0500.050<0.0010mg/KgVinyl Chloride 53.6 40-156 6.5 35
0.026 52.60.0270.0500.050<0.0005mg/Kgo-Xylene 54.8 43-143 4.0 17
0.050 50.00.0530.1000.100<0.001mg/Kgm,p-Xylene 53.0 36-148 5.8 20
94.44-Bromofluorobenzene (S)93.8 70-130
98.0Dibromofluoromethane (S)97.6 84-123
83.4Toluene-d8 (S)82.2 76-129
Page 24 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 98 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V1707QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V1480
Associated Lab Samples: 94144, 94145, 94146, 94147, 94152
LRB-V1480 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/10/21 14:270.6600.015<0.015mg/KgAcenaphthene
03/10/21 14:270.6600.013<0.013mg/KgAcenaphthylene
03/10/21 14:270.6600.163<0.163mg/KgAniline
03/10/21 14:270.6600.007<0.007mg/KgAnthracene
03/10/21 14:270.6600.007<0.007mg/KgBenzo(a)anthracene
03/10/21 14:270.6600.005<0.005mg/KgBenzo(a)pyrene
03/10/21 14:270.6600.006<0.006mg/KgBenzo(b)fluoranthene
03/10/21 14:270.6600.006<0.006mg/KgBenzo(g,h,i)perylene
03/10/21 14:270.6600.007<0.007mg/KgBenzo(k)fluoranthene
03/10/21 14:272.000.548<0.548mg/KgBenzoic Acid
03/10/21 14:270.6600.124<0.124mg/KgBenzyl alcohol
03/10/21 14:270.6600.126<0.126mg/KgBis(2-Chloroethoxy)methane
03/10/21 14:270.6600.106<0.106mg/KgBis(2-Chloroethyl)ether
03/10/21 14:270.3300.118<0.118mg/KgBis(2-Chloroisopropyl)ether
03/10/21 14:270.6600.149<0.149mg/KgBis(2-ethylhexyl)phthalate
03/10/21 14:270.6600.155<0.155mg/Kg4-Bromophenyl phenyl ether
03/10/21 14:270.3300.114<0.114mg/KgButyl benzyl phthalate
03/10/21 14:270.6600.126<0.126mg/Kg4-Chloro-3-methylphenol
03/10/21 14:270.3300.080<0.080mg/Kg4-Chloroaniline
03/10/21 14:270.6600.161<0.161mg/Kg2-Chloronaphthalene
03/10/21 14:270.6600.126<0.126mg/Kg2-Chlorophenol
03/10/21 14:271.000.202<0.202mg/Kg4-Chlorophenyl phenyl ether
03/10/21 14:270.6600.007<0.007mg/KgChrysene
03/10/21 14:270.6600.019<0.019mg/KgDibenz(a,h)anthracene
03/10/21 14:270.6600.017<0.017mg/KgDibenzofuran
03/10/21 14:270.6600.107<0.107mg/Kg1,2-Dichlorobenzene
03/10/21 14:270.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 25 of 34Date:03/16/2021 03:25 PM
Page 99 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V1707QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V1480
Associated Lab Samples: 94144, 94145, 94146, 94147, 94152
LRB-V1480 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/10/21 14:270.3300.104<0.104mg/Kg1,4-Dichlorobenzene
03/10/21 14:270.6600.131<0.131mg/Kg3,3'-Dichlorobenzidine
03/10/21 14:270.6600.129<0.129mg/Kg2,4-Dichlorophenol
03/10/21 14:270.6600.170<0.170mg/KgDiethyl phthalate
03/10/21 14:270.6600.158<0.158mg/KgDimethyl phthalate
03/10/21 14:270.3300.137<0.137mg/Kg2,4-Dimethylphenol
03/10/21 14:270.6600.164<0.164mg/KgDi-n-butyl phthalate
03/10/21 14:271.500.364<0.364mg/Kg4,6-Dinitro-2-methylphenol
03/10/21 14:271.500.387<0.387mg/Kg2,4-Dinitrophenol
03/10/21 14:270.6600.175<0.175mg/Kg2,4-Dinitrotoluene
03/10/21 14:270.6600.171<0.171mg/Kg2,6-Dinitrotoluene
03/10/21 14:270.3300.171<0.171mg/KgDi-n-Octyl Phthalate
03/10/21 14:270.6600.007<0.007mg/KgFluoranthene
03/10/21 14:270.6600.014<0.014mg/KgFluorene
03/10/21 14:270.6600.145<0.145mg/KgHexachlorobenzene
03/10/21 14:270.6600.149<0.149mg/KgHexachlorobutadiene
03/10/21 14:270.6600.227<0.227mg/KgHexachlorocyclopentadiene
03/10/21 14:270.6600.104<0.104mg/KgHexachloroethane
03/10/21 14:270.6600.018<0.018mg/KgIndeno(1,2,3-cd)pyrene
03/10/21 14:270.6600.142<0.142mg/KgIsophorone
03/10/21 14:270.6600.010<0.010mg/Kg1-Methylnaphthalene
03/10/21 14:270.6600.012<0.012mg/Kg2-Methylnaphthalene
03/10/21 14:270.6600.126<0.126mg/Kg2-Methylphenol
03/10/21 14:270.6600.143<0.143mg/Kg3&4 Methylphenol
03/10/21 14:270.6600.014<0.014mg/KgNaphthalene
03/10/21 14:270.6600.142<0.142mg/Kg2-Nitroaniline
03/10/21 14:270.6600.120<0.120mg/Kg3-Nitroaniline
Page 26 of 34Date:03/16/2021 03:25 PM
Page 100 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V1707QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V1480
Associated Lab Samples: 94144, 94145, 94146, 94147, 94152
LRB-V1480 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/10/21 14:270.3300.103<0.103mg/Kg4-Nitroaniline
03/10/21 14:270.3300.140<0.140mg/KgNitrobenzene
03/10/21 14:270.6600.110<0.110mg/Kg2-Nitrophenol
03/10/21 14:270.6600.163<0.163mg/Kg4-Nitrophenol
03/10/21 14:270.1700.005<0.005mg/KgN-Nitrosodimethylamine
03/10/21 14:270.6600.181<0.181mg/KgN-Nitrosodiphenylamine
03/10/21 14:270.6600.152<0.152mg/KgN-Nitroso-di-n-propylamine
03/10/21 14:271.000.421<0.421mg/KgPentachlorophenol
03/10/21 14:270.6600.007<0.007mg/KgPhenanthrene
03/10/21 14:270.6600.108<0.108mg/KgPhenol
03/10/21 14:270.6600.009<0.009mg/KgPyrene
03/10/21 14:270.3300.063<0.063mg/KgPyridine
03/10/21 14:270.6600.117<0.117mg/Kg1,2,4-Trichlorobenzene
03/10/21 14:270.6600.140<0.140mg/Kg2,4,5-Trichlorophenol
03/10/21 14:270.6600.160<0.160mg/Kg2,4,6-Trichlorophenol
03/10/21 14:272-Fluorobiphenyl (S)114 44-115
03/10/21 14:272-Fluorophenol (S)92.7 35-115
03/10/21 14:27Nitrobenzene-d5 (S)102 37-122
03/10/21 14:274-Terphenyl-d14 (S)124 54-127
03/10/21 14:272,4,6-Tribromophenol (S)89.7 39-132
03/10/21 14:27Phenol-d5 (S)94.8 34-121
LCS-V1480Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1041.741.67mg/KgAcenaphthene 40-123
1141.901.67mg/KgAcenaphthylene 32-132
Page 27 of 34Date:03/16/2021 03:25 PM
Page 101 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V1707QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V1480
LCS-V1480Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1222.041.67mg/KgAniline 12-197
1131.891.67mg/KgAnthracene 47-123
1141.911.67mg/KgBenzo(a)anthracene 49-126
141*2.351.67mg/KgBenzo(a)pyrene 45-129
1191.991.67mg/KgBenzo(b)fluoranthene 45-132
1191.981.67mg/KgBenzo(g,h,i)perylene 43-134
1212.021.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.071.67mg/KgBenzoic Acid 10-83
1071.781.67mg/KgBenzyl alcohol 29-122
1101.841.67mg/KgBis(2-Chloroethoxy)methane 36-121
92.21.541.67mg/KgBis(2-Chloroethyl)ether 31-120
1031.721.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1181.971.67mg/KgBis(2-ethylhexyl)phthalate 51-133
1051.761.67mg/Kg4-Bromophenyl phenyl ether 46-124
1171.961.67mg/KgButyl benzyl phthalate 48-132
76.61.281.67mg/Kg4-Chloro-3-methylphenol 45-122
82.61.381.67mg/Kg4-Chloroaniline 17-106
92.81.551.67mg/Kg2-Chloronaphthalene 41-114
86.21.441.67mg/Kg2-Chlorophenol 34-121
1021.701.67mg/Kg4-Chlorophenyl phenyl ether 45-121
1191.991.67mg/KgChrysene 50-124
65.81.101.67mg/KgDibenz(a,h)anthracene 45-134
1021.701.67mg/KgDibenzofuran 44-120
80.81.351.67mg/Kg1,2-Dichlorobenzene 33-117
80.21.341.67mg/Kg1,3-Dichlorobenzene 30-115
78.41.311.67mg/Kg1,4-Dichlorobenzene 31-115
1011.681.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 28 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 102 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V1707QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V1480
LCS-V1480Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
80.21.341.67mg/Kg2,4-Dichlorophenol 40-122
98.81.651.67mg/KgDiethyl phthalate 50-124
1011.681.67mg/KgDimethyl phthalate 48-124
82.61.381.67mg/Kg2,4-Dimethylphenol 30-127
1081.801.67mg/KgDi-n-butyl phthalate 51-128
0.0*1.241.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
0.0*1.161.67mg/Kg2,4-Dinitrophenol 27-129
1111.851.67mg/Kg2,4-Dinitrotoluene 48-126
1141.911.67mg/Kg2,6-Dinitrotoluene 46-124
1171.961.67mg/KgDi-n-Octyl Phthalate 45-140
1101.831.67mg/KgFluoranthene 50-127
1071.781.67mg/KgFluorene 43-125
92.81.551.67mg/KgHexachlorobenzene 45-122
75.41.261.67mg/KgHexachlorobutadiene 32-123
75.41.261.67mg/KgHexachlorocyclopentadiene 32-117
76.61.281.67mg/KgHexachloroethane 28-117
1131.891.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
71.21.191.67mg/KgIsophorone 30-122
94.01.571.67mg/Kg1-Methylnaphthalene 40-119
89.21.491.67mg/Kg2-Methylnaphthalene 38-122
89.21.491.67mg/Kg2-Methylphenol 32-122
78.41.311.67mg/Kg3&4 Methylphenol 34-119
86.21.441.67mg/KgNaphthalene 35-123
1101.841.67mg/Kg2-Nitroaniline 44-127
1041.741.67mg/Kg3-Nitroaniline 33-119
1011.681.67mg/Kg4-Nitroaniline 63-147
81.41.361.67mg/KgNitrobenzene 34-122
Page 29 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 103 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V1707QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V1480
LCS-V1480Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
77.21.291.67mg/Kg2-Nitrophenol 36-123
88.01.471.67mg/Kg4-Nitrophenol 30-132
99.41.661.67mg/KgN-Nitrosodimethylamine 10-146
129*2.151.67mg/KgN-Nitrosodiphenylamine 38-127
95.21.591.67mg/KgN-Nitroso-di-n-propylamine 36-120
1021.701.67mg/KgPentachlorophenol 25-133
1121.871.67mg/KgPhenanthrene 50-121
84.41.411.67mg/KgPhenol 34-121
128*2.141.67mg/KgPyrene 47-127
71.2*1.191.67mg/KgPyridine 10-60
74.81.251.67mg/Kg1,2,4-Trichlorobenzene 34-118
90.41.511.67mg/Kg2,4,5-Trichlorophenol 41-124
84.41.411.67mg/Kg2,4,6-Trichlorophenol 39-126
1022-Fluorobiphenyl (S)44-115
86.72-Fluorophenol (S)35-115
83.2Nitrobenzene-d5 (S)37-122
1084-Terphenyl-d14 (S)54-127
82.82,4,6-Tribromophenol (S)39-132
85.5Phenol-d5 (S)34-121
V 93113-MS-V1480 V 93113-MSD-V1480Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.64 98.71.601.661.66<0.015mg/KgAcenaphthene 96.3 40-123 2.4 20
1.76 1061.731.661.660.017mg/KgAcenaphthylene 104 32-132 1.7 20
1.50 90.31.541.661.66<0.163mg/KgAniline 92.7 12-197 2.6 20
Page 30 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 104 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V1707QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V1480
V 93113-MS-V1480 V 93113-MSD-V1480Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.75 1051.741.661.660.017mg/KgAnthracene 105 47-123 0.5 20
2.23 134*1.751.661.660.084mg/KgBenzo(a)anthracene 105 49-126 24.1*20
2.55 154*2.181.661.660.108mg/KgBenzo(a)pyrene 131*45-129 15.6 20
2.46 148*1.841.661.660.132mg/KgBenzo(b)fluoranthene 111 45-132 28.8*20
2.07 1251.821.661.66<0.006mg/KgBenzo(g,h,i)perylene 110 43-134 12.8 20
1.86 1121.831.661.660.045mg/KgBenzo(k)fluoranthene 110 47-132 1.6 20
1.47 0.0*1.181.661.66<0.548mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.62 97.51.601.661.66<0.124mg/KgBenzyl alcohol 96.3 29-122 1.2 20
1.68 1011.671.661.66<0.126mg/KgBis(2-Chloroethoxy)methane 101 36-121 0.5 20
1.41 84.91.371.661.66<0.106mg/KgBis(2-Chloroethyl)ether 82.5 31-120 2.8 20
1.60 96.31.511.661.66<0.118mg/KgBis(2-Chloroisopropyl)ether 90.9 33-131 5.7 20
1.83 1101.821.661.66<0.149mg/KgBis(2-ethylhexyl)phthalate 110 51-133 0.5 20
1.64 98.71.661.661.66<0.155mg/Kg4-Bromophenyl phenyl ether 100 46-124 1.2 20
1.85 1111.841.661.66<0.114mg/KgButyl benzyl phthalate 111 48-132 0.5 20
1.20 72.21.191.661.66<0.126mg/Kg4-Chloro-3-methylphenol 71.6 45-122 0.8 20
1.26 75.91.271.661.66<0.080mg/Kg4-Chloroaniline 76.5 17-106 0.7 20
1.43 86.11.421.661.66<0.161mg/Kg2-Chloronaphthalene 85.5 41-114 0.7 20
1.30 78.31.261.661.66<0.126mg/Kg2-Chlorophenol 75.9 34-121 3.1 20
1.57 94.51.541.661.66<0.202mg/Kg4-Chlorophenyl phenyl ether 92.7 45-121 1.9 20
2.15 130*1.831.661.660.102mg/KgChrysene 110 50-124 16.0 20
1.40 84.31.251.661.66<0.019mg/KgDibenz(a,h)anthracene 75.3 45-134 11.3 20
1.59 95.71.551.661.660.020mg/KgDibenzofuran 93.3 44-120 2.5 20
1.21 72.81.181.661.66<0.107mg/Kg1,2-Dichlorobenzene 71.0 33-117 2.5 20
1.19 71.61.161.661.66<0.097mg/Kg1,3-Dichlorobenzene 69.8 30-115 2.5 20
1.16 69.81.151.661.66<0.104mg/Kg1,4-Dichlorobenzene 69.2 31-115 0.8 20
1.40 84.31.661.661.66<0.131mg/Kg3,3'-Dichlorobenzidine 100 22-121 16.9 20
Page 31 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 105 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V1707QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V1480
V 93113-MS-V1480 V 93113-MSD-V1480Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.24 74.61.231.661.66<0.129mg/Kg2,4-Dichlorophenol 74.0 40-122 0.8 20
1.53 92.11.501.661.66<0.170mg/KgDiethyl phthalate 90.3 50-124 1.9 20
1.55 93.31.521.661.66<0.158mg/KgDimethyl phthalate 91.5 48-124 1.9 30
1.24 74.61.241.661.66<0.137mg/Kg2,4-Dimethylphenol 74.6 30-127 0.0 20
1.66 1001.661.661.66<0.164mg/KgDi-n-butyl phthalate 100 51-128 0.0 20
1.23 0.0*1.231.661.66<0.364mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
1.25 0.0*1.181.661.66<0.387mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.73 1041.681.661.66<0.175mg/Kg2,4-Dinitrotoluene 101 48-126 2.9 20
1.75 1051.711.661.66<0.171mg/Kg2,6-Dinitrotoluene 103 46-124 2.3 20
1.81 1091.831.661.66<0.171mg/KgDi-n-Octyl Phthalate 110 45-140 1.0 20
2.62 158*1.671.661.660.180mg/KgFluoranthene 101 50-127 44.2*20
1.65 99.31.631.661.66<0.014mg/KgFluorene 98.1 43-125 1.2 20
1.44 86.71.431.661.66<0.145mg/KgHexachlorobenzene 86.1 45-122 0.6 20
1.14 68.61.131.661.66<0.149mg/KgHexachlorobutadiene 68.0 32-123 0.8 20
1.19 71.61.131.661.66<0.227mg/KgHexachlorocyclopentadiene 68.0 32-117 5.1 20
1.13 68.01.101.661.66<0.104mg/KgHexachloroethane 66.2 28-117 2.6 20
1.99 1201.761.661.660.073mg/KgIndeno(1,2,3-cd)pyrene 106 45-133 12.2 20
1.22 73.41.101.661.66<0.142mg/KgIsophorone 66.2 30-122 10.3 20
1.47 88.51.451.661.660.041mg/Kg1-Methylnaphthalene 87.3 40-119 1.3 20
1.38 83.11.341.661.660.045mg/Kg2-Methylnaphthalene 80.7 38-122 2.9 20
1.34 80.71.321.661.66<0.126mg/Kg2-Methylphenol 79.5 32-122 1.5 20
1.20 72.21.181.661.66<0.143mg/Kg3&4 Methylphenol 71.0 34-119 1.6 20
1.34 80.71.311.661.660.032mg/KgNaphthalene 78.9 35-123 2.2 20
1.77 1071.731.661.66<0.142mg/Kg2-Nitroaniline 104 44-127 2.2 20
1.57 94.51.601.661.66<0.120mg/Kg3-Nitroaniline 96.3 33-119 1.8 20
1.60 96.31.561.661.66<0.103mg/Kg4-Nitroaniline 93.9 63-147 2.5 20
Page 32 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 106 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V1707QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V1480
V 93113-MS-V1480 V 93113-MSD-V1480Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.27 76.51.231.661.66<0.140mg/KgNitrobenzene 74.0 34-122 3.2 20
1.19 71.61.151.661.66<0.110mg/Kg2-Nitrophenol 69.2 32-123 3.4 20
1.44 86.71.361.661.66<0.163mg/Kg4-Nitrophenol 81.9 30-132 5.7 20
1.35 81.31.281.661.66<0.005mg/KgN-Nitrosodimethylamine 77.1 10-146 5.3 30
1.98 1192.001.661.66<0.181mg/KgN-Nitrosodiphenylamine 120 38-127 1.0 20
1.46 87.91.431.661.66<0.152mg/KgN-Nitroso-di-n-propylamine 86.1 36-120 2.0 20
1.61 96.91.611.661.66<0.421mg/KgPentachlorophenol 96.9 25-133 0.0 20
2.31 139*1.721.661.660.133mg/KgPhenanthrene 104 50-121 29.2*20
1.29 77.71.241.661.66<0.108mg/KgPhenol 74.6 34-121 3.9 20
2.95 178*1.951.661.660.184mg/KgPyrene 117 47-127 40.8*20
0.957 57.60.8951.661.66<0.063mg/KgPyridine 53.9 10-60 6.6 20
1.15 69.21.121.661.66<0.117mg/Kg1,2,4-Trichlorobenzene 67.4 34-118 2.6 20
1.36 81.91.401.661.66<0.140mg/Kg2,4,5-Trichlorophenol 84.3 41-124 2.8 20
1.32 79.51.311.661.66<0.160mg/Kg2,4,6-Trichlorophenol 78.9 39-126 0.7 20
94.52-Fluorobiphenyl (S)93.3 44-115
76.42-Fluorophenol (S)74.1 35-115
77.1Nitrobenzene-d5 (S)75.3 37-122
1024-Terphenyl-d14 (S)101 54-127
77.62,4,6-Tribromophenol (S)75.9 39-132
77.9Phenol-d5 (S)75.3 34-121
Page 33 of 34* QC Fail Date:03/16/2021 03:25 PM
Page 107 of 110
Quality Control Data
21-068-0001Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
JMC.011
Dry Weight Determination
SW-DRYWT
V1445QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94151-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/09/21 15:202.217.618.0%Moisture
V 94147-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/09/21 15:202.217.618.0%Moisture
Page 34 of 34Date:03/16/2021 03:25 PM
Page 108 of 110
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-068-0001
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 5.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Talon J Yelton Date & Time:03/09/2021 07:49:36
Special precautions or instructions included?
Comments:
Page 109 of 110
Page 110 of 110

Appendix D

DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
Former Cotton Seed Oil Mill
300 Rampart Street Charlotte, NC
Brownfields
23053-19-060
January 2021
November 2020 EPA RSL Table
Prepared By:RHS
MRB
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 23053-19-060
Exposure Unit ID: Worst Case
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration to Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 23053-19-060
Exposure Unit ID: Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Factors and Target Risks
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 23053-19-060
Exposure Parameter Site Specific Value Justification
Target Cancer Risk (individual) 1.0E-06
Target Cancer Risk (cumulative) 1.0E-04
Target Hazard Index (individual) 2.0E-01
Target Hazard Index (cumulative) 1.0E+00
Lifetime (LT) (years)70
Body Weight (BW) (kg) 15
Exposure Duration (ED) (yr) 6
Exposure Frequency (EF) (d/yr) 350
Exposure Time (ET) (hr) 24
Skin Surface Area - Soil Exposure (SAs) (cm2)2373
Soil Adherence Factor (AF) (mg/cm2)0.2
Soil Ingestion Rate (IRS) (mg/day) 200
Skin Surface Area - Water Exposure (SAw) (cm2)6365
Water Ingestion Rate (IRW) (L/d) 0.78
Water Exposure Time (ETevent) (hr/event)0.54
Water Event Frequency (EV) (events/day) 1
Lifetime (LT) (years)70
Body Weight (BW) (kg) 80
Exposure Duration (ED) (yr) 20
Exposure Frequency (EF) (d/yr) 350
Exposure Time (ET) (hr) 24
Skin Surface Area - Soil Exposure (SAs) (cm2)6032
Soil Adherence Factor (AF) (mg/cm2)0.07
Soil Ingestion Rate (IRS) (mg/day) 100
Skin Surface Area - Water Exposure (SAw) (cm2)19652
Water Ingestion Rate (IRW) (L/d) 2.5
Water Exposure Time (ETevent) (hr/event)0.71
Water Event Frequency (EV) (events/day) 1
Lifetime (LT) (years)70
Body Weight (BW) (kg) 80
Exposure Duration (ED) (yr) 25
Exposure Frequency (EF) (d/yr) 250
Exposure Time (ET) (hr) 8
Skin Surface Area - Soil Exposure (SAs) (cm2)3527
Soil Adherence Factor (AF) (mg/cm2)0.12
Soil Ingestion Rate (IR) (mg/day) 100
Skin Surface Area - Water Exposure (SAw) (cm2)19652
Water Ingestion Rate (IRW) (L/d) 0.83
Water Exposure Time (ETevent) (hr/event)0.67
Water Event Frequency (EV) (events/day) 1
Lifetime (LT) (years)70
Body Weight (BW) (kg) 80
Working Weeks (EW) (wk/yr) 50
Exposure Duration (ED) (yr) 1
Exposure Frequency (EF) (d/yr) 250
Exposure Time (ET) (hr) 8
Skin Surface Area - Soil Exposure (SAs) (cm2)3527
Soil Adherence Factor (AF) (mg/cm2)0.3
Soil Ingestion Rate (IR) (mg/day) 330
Non-Residential Worker
Construction Worker
70
80
25
250
8
3527
0.12
100
19652
0.83
0.67
Input Form 1B
Exposure Unit ID: Worst Case
Residential Child
General
Residential Adult
Default Value
1.0E-06
1.0E-04
2.0E-01
1.0E+00
70
15
6
350
24
2373
0.2
200
6365
0.78
0.54
1
70
80
20
350
24
6032
0.07
100
19652
2.5
0.71
1
1
70
80
330
1
250
8
3527
0.3
50
North Carolina DEQ Risk Calculator
Exposure Factors and Target Risks
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 23053-19-060
Exposure Parameter Site Specific Value Justification
Input Form 1B
Exposure Unit ID: Worst Case
Default Value
Recreator Trespasser
Lifetime (LT) (years)70 NA 70
Averaging Time (AT) (days/yr) 365 NA 365
Body Weight (BW) (kg) 15 NA 15
Exposure Duration 0-2 (ED) (yr) 2 NA 2
Exposure Duration 2-6 (ED) (yr) 4 NA 4
Exposure Frequency (EF) (d/yr) 195 NA 195
Exposure Time (ET) (hr) 2 NA 2
Skin Surface Area - Soil Exposure (SAs) (cm2)2373 NA 2373
Soil Adherence Factor (AF) (mg/cm2)0.2 NA 0.2
Soil Ingestion Rate (IRS) (mg/day) 200 NA 200
Skin Surface Area - Water Exposure (SAw) (cm2)6365 NA 6365
Water Ingestion Rate (IRW) (L/hr) 0.124 NA 0.124
Water Exposure Time (ETevent) (hr/event)2NA 2
Water Event Frequency (EV) (events/day) 1 NA 1
Recreator Trespasser
Lifetime (LT) (years)70 70 70
Body Weight (BW) (kg) 80 45 80
Exposure Duration 6-16 (ED) (yr) 10 10 10
Exposure Duration 16-26 (ED) (yr) 10 0 10
Exposure Frequency (EF) (d/yr) 195 90 195
Exposure Time (ET) (hr) 2 2 2
Skin Surface Area - Soil Exposure (SAs) (cm2)6032 6032 6032
Soil Adherence Factor (AF) (mg/cm2)0.07 0.2 0.07
Soil Ingestion Rate (IRS) (mg/day) 100 200 100
Skin Surface Area - Water Exposure (SAw) (cm2)19652 19652 19652
Water Ingestion Rate (IRW) (L/hr) 0.0985 0.071 0.0985
Water Exposure Time (ETevent) (hr/event)22 2
Water Event Frequency (EV) (events/day) 1 1 1
User Defined Child
User Defined Adult
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: January 2021Basis: November 2020 EPA RSL TableSite ID: 23053-19-060Exposure Unit ID: Worst CaseNOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsExposure Point Concentration (mg/kg)Notes: CAS NumberChemicalFor the chemicals highlighted in blue, data entry notes are provided in the PSRG Table link on the Main MenuMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion0.022 67-64-1Acetonemg/kg16.5 7440-38-2Arsenic, Inorganicmg/kg123 7440-39-3Bariummg/kg0.226 7440-43-9Cadmium (Diet)mg/kg58.2 16065-83-1Chromium(III), Insoluble Saltsmg/kg0.71 18540-29-9Chromium(VI)mg/kg78.7 7439-92-1~Lead and Compoundsmg/kg0.116 7439-97-6~Mercury (elemental)mg/kg0.002 78-93-3Methyl Ethyl Ketone (2-Butanone)mg/kg0.026 83-32-9~Acenaphthenemg/kg0.028 120-12-7~Anthracenemg/kg0.113 56-55-3~Benz[a]anthracenemg/kg0.143 50-32-8~Benzo[a]pyrenemg/kg0.219 205-99-2~Benzo[b]fluoranthenemg/kg0.075 207-08-9~Benzo[k]fluoranthenemg/kg0.154 218-01-9~Chrysenemg/kg0.274 206-44-0~Fluoranthenemg/kg0.128 193-39-5~Indeno[1,2,3-cd]pyrenemg/kg0.02 90-12-0~Methylnaphthalene, 1-mg/kg0.024 91-57-6~Methylnaphthalene, 2-mg/kg0.022 91-20-3~Naphthalenemg/kg0.295 129-00-0~Pyrenemg/kg2.93 7782-49-2Seleniummg/kg0.0717 7440-22-4Silvermg/kgInput Form 2ASoil Exposure Point Concentration TableDescription of Exposure Point Concentration Selection:North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 23053-19-060
Exposure Unit ID: Worst Case
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 2.8E-05 5.1E-01 NO
Groundwater Use* NC NC NC
Soil NC NC NC
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Sitewide RiskOutput Form 1BVersion Date: January 2021Basis: November 2020 EPA RSL TableSite ID: 23053-19-060Exposure Unit ID: Worst CaseReceptor PathwayCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexSoil 2.8E-05 5.1E-01 2.8E-05 5.1E-01Groundwater Use* NM NM NM NMSoil NM NM NM NMGroundwater Use*NM NM NM NMConstruction Worker Soil NM NMSoil NM NMSurface Water Use*NM NMGroundwater to Indoor Air NM NM NM NMSoil Gas to Indoor Air NM NM NM NMIndoor Air NMNM NMNMGroundwater to Indoor AirNM NM NM NMSoil Gas to Indoor AirNM NM NM NMIndoor AirNM NM NM NM2.8E-05 5.1E-01 2.8E-05 5.1E-01 0.0E+00 0.0E+00 0.0E+00 0.0E+00 0.0E+00 0.0E+00 0.0E+00 0.0E+003. NM = Not Modeled4. NC = Pathway not calculatedResidentNon-Residential WorkerRecreator/TrespasserVAPOR INTRUSION CALCULATORSDIRECT CONTACT SOIL AND WATER CALCULATORSNon-Residential Worker - Future Scenario Construction Worker Recreator/TrespasserResident - Current Scenario Resident - Future Scenario Non-Residential Worker - Current ScenarioTOTAL SITEWIDE RISK FOR EACH RECEPTORNotes:1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure.ResidentNon-Residential WorkerNorth Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 23053-19-060
Exposure Unit ID: Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.022 0.022 0.022 3.1E-07 4.7E-08 3.6E-07
7440-38-2 Arsenic, Inorganic 16.5 16.5 16.5 2.1E-05 3.0E-06 4.3E-10 2.4E-05 4.2E-01 5.0E-02 1.8E-05 4.7E-01
7440-39-3 Barium 123 123 123 7.9E-03 4.0E-06 7.9E-03
7440-43-9 Cadmium (Diet) 0.226 0.226 0.226 2.4E-12 2.4E-12 2.9E-03 2.7E-04 3.7E-07 3.2E-03
16065-83-1 Chromium(III), Insoluble Salts 58.2 58.2 58.2 5.0E-04 5.0E-04
18540-29-9 Chromium(VI) 0.71 0.71 0.71 2.3E-06 9.9E-10 2.3E-06 3.0E-03 1.1E-07 3.0E-03
7439-92-1 ~Lead and Compounds 78.7 78.7 78.7 <SL** <SL** <SL**
7439-97-6 ~Mercury (elemental) 0.116 0.116 0.116 1.0E-02 1.0E-02
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.002 0.002 0.002 4.3E-08 3.0E-08 7.2E-08
83-32-9 ~Acenaphthene 0.026 0.026 0.026 5.5E-06 1.7E-06 7.2E-06
120-12-7 ~Anthracene 0.028 0.028 0.028 1.2E-06 3.7E-07 1.6E-06
56-55-3 ~Benz[a]anthracene 0.113 0.113 0.113 7.4E-08 2.5E-08 1.4E-09 1.0E-07
50-32-8 ~Benzo[a]pyrene 0.143 0.143 0.143 9.3E-07 3.1E-07 1.4E-12 1.2E-06 6.1E-03 1.9E-03 1.2E-06 8.0E-03
205-99-2 ~Benzo[b]fluoranthene 0.219 0.219 0.219 1.4E-07 4.8E-08 2.2E-13 1.9E-07
207-08-9 ~Benzo[k]fluoranthene 0.075 0.075 0.075 4.9E-09 1.6E-09 7.5E-15 6.5E-09
218-01-9 ~Chrysene 0.154 0.154 0.154 1.0E-09 3.4E-10 1.5E-15 1.3E-09
206-44-0 ~Fluoranthene 0.274 0.274 0.274 8.8E-05 2.7E-05 1.1E-04
193-39-5 ~Indeno[1,2,3-cd]pyrene 0.128 0.128 0.128 8.4E-08 2.8E-08 1.3E-13 1.1E-07
90-12-0 ~Methylnaphthalene, 1- 0.02 0.02 0.02 8.3E-10 3.1E-10 1.1E-09 3.7E-06 1.1E-06 4.8E-06
91-57-6 ~Methylnaphthalene, 2- 0.024 0.024 0.024 7.7E-05 2.4E-05 1.0E-04
91-20-3 ~Naphthalene 0.022 0.022 0.022 3.8E-09 1.4E-09 5.4E-09 1.1E-08 1.4E-05 4.3E-06 1.4E-04 1.6E-04
129-00-0 ~Pyrene 0.295 0.295 0.295 1.3E-04 3.9E-05 1.6E-04
7782-49-2 Selenium 2.93 2.93 2.93 7.5E-03 2.4E-09 7.5E-03
7440-22-4 Silver 0.0717 0.0717 0.0717 1.8E-04 1.8E-04
Cumulative: 2.8E-05 5.1E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator