24003 Final Grade Soil Sampling Report_North Davidson II 20220407

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Final Grade Soil Sampling Report
North Davidson II Brownfields Property
2315 N. Davidson Street and 421 E. 26th Street
Charlotte, North Carolina
Brownfields Project No. 24003-20-060
H&H Job No. PAM-003

Table of Contents
1.0 Introduction ............................................................................................................................ 1 
2.0 Final Grade Soil Sampling .................................................................................................... 2 
2.1 Final Grade Soil Sampling Methodologies ....................................................................... 2 
2.2 Soil Sample Results ............................................................................................................. 3 
2.3 Exposure Risk Evaluation ................................................................................................. 5 
3.0 Summary ................................................................................................................................. 6 

List of Tables

Table 1 Soil Lithology Summary
Table 2 Summary of Soil Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Final Grade Soil Sample Location Map

List of Appendices

Appendix A Laboratory Analytical Report
Appendix B DEQ Risk Calculator

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Final Grade Soil Sampling Report
North Davidson II Brownfields Property
2315 N. Davidson Street and 421 E. 26th Street
Charlotte, North Carolina
Brownfields Project No. 24003-20-060
H&H Job No. PAM-003

1.0 Introduction

On behalf of Mill District Partners, LLC, Hart & Hickman, PC (H&H) has prepared this report to
document final grade soil sampling activities completed at the North Davidson II Brownfields
property (Brownfields Project No. 24003-20-060) located at 2315 N. Davidson Street and 421 E.
26th Street in Charlotte, Mecklenburg County, North Carolina (Site). A Site location map is
provided as Figure 1.

The Site consists of two parcels of land (Parcel Identification Numbers 08305204 and 08305206)
that total approximately 3.8 acres. The southeastern parcel (2315 N. Davidson Street) is developed
with an approximate 28,675-square foot (sq ft) vacant commercial building, and the northwestern
parcel (421 E. 26th Street) is developed with an approximate 12,960-sq ft vacant commercial
building. An inactive rail corridor that is owned by the City of Charlotte separates the two Site
parcels. Redevelopment at the Site includes adaptive re-use of the Site buildings for mixed-
commercial purposes including retail, office, and restaurants, with landscaped areas and an outdoor
patio on the eastern portion of the northwestern Site parcel. The building locations are shown on
Figure 2.

An Environmental Management Plan (EMP) for the Site was approved by the North Carolina
Department of Environmental Quality (DEQ) Brownfields Program on October 27, 2020. The
EMP includes a requirement for collection of final grade soil samples in areas that are not covered
with a minimum of 2 ft of clean fill soil or topsoil from a landscaping company, building
foundations, sidewalks, asphalt or concrete parking areas, driveways, or other impervious surfaces
following completion of redevelopment activities. H&H prepared a Final Grade Soil Sampling
Work Plan (Work Plan), dated March 10, 2022. The Work Plan was approved by the DEQ
Brownfields Program on March 16, 2022.

The following sections describe final grade soil sampling activities conducted at the Site.
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2.0 Final Grade Soil Sampling

On March 21, 2022, H&H conducted final grade soil sampling activities at the Site to evaluate the
potential for impacts in shallow soil that may pose unacceptable exposure risks to
industrial/commercial occupants. The soil sampling activities were performed in general
accordance with the DEQ-approved Work Plan, the DEQ Inactive Hazardous Sites Branch
Guidelines for Assessment and Cleanup dated July 2021, and the most recent versions of the U.S.
Environmental Protection Agency Region IV Lab Services and Applied Sciences Division Field
Branches Quality System and Technical Procedures guidance.

2.1 Final Grade Soil Sampling Methodologies

Based on review of the Site landscaping plan, conversations with the prospective developer and
Site superintendent, and observations at the Site, proposed areas of grass, artificial turf, crushed
stone, and landscaping were divided into five final grade evaluation areas (FG-1 through FG-5).
Soil borings were advanced in each final grade evaluation area for collection of aliquot soil
samples. The final grade evaluation areas and soil boring locations are shown in Figure 2.

To collect representative soil samples, three to five shallow soil borings were advanced within
each final grade evaluation area. Each soil boring was advanced to approximately 2 feet below
ground surface (ft bgs) utilizing a decontaminated stainless-steel hand auger. Continuous soil
samples were collected from the center of the hand auger bucket at each boring and observed for
lithologic description, the presence of obvious staining or unusual odors, and field screened for
volatile organic vapors using a calibrated photo-ionization detector (PID). A maximum PID
reading of 94.1 parts per million (ppm) was observed during the sampling activities at boring FG-
2A. The elevated PID reading is believed to be a result of asphalt mixed with the sandy silt that
was observed in the FG-2 final grade evaluation area. Field personnel did not observe the presence
of staining or odors in the aliquot soil samples. A summary of final grade soil lithology is provided
in Table 1.

Based on field screening results, one representative grab soil sample was collected for laboratory
analysis from an undisturbed portion of an aliquot soil sample in each final grade evaluation area.
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In addition, soil sample aliquots from each area were combined and homogenized to form one
composite soil sample representative of that evaluation area for a total of five composite soil
samples (FG-1 through FG-5). Soil samples selected for laboratory analysis from each evaluation
area were collected directly into dedicated laboratory-supplied sample containers, labeled with the
sample identification, date, time, and requested analysis and placed in a laboratory-supplied cooler
with ice. The samples were delivered to Waypoint Analytical (Waypoint) under standard chain-
of-custody protocols for analysis.

Composite soil samples were submitted to Waypoint for analysis of semi-volatile organic
compounds (SVOCs) by EPA Method 8270 and Resource Conservation and Recovery Act
(RCRA) metals plus hexavalent chromium by EPA Methods 6010/7471/7199. The grab soil
samples were submitted to Waypoint for analysis of VOCs by EPA Method 8260.

For quality assurance and quality control purposes, H&H collected one duplicate composite and
one duplicate grab sample (FG-DUP) from final grade evaluation area FG-2. The duplicate soil
sample was submitted for the same analyses as the parent samples as described above.

Following sampling activities, the soil borings were properly abandoned and the surfaces were
repaired similar to pre-drilling conditions. Additionally, the soil boring locations were estimated
using a hand-held global positioning system unit. A discussion of the results of the laboratory
analyses is provided below.

2.2 Soil Sample Results

A tabular summary of final grade soil sample laboratory analytical results is presented in Table 2,
and a copy of the laboratory analytical report and chain-of-custody record is provided in
Appendix A. The laboratory analytical results were compared to the DEQ Residential and
Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) dated January 2022. In
addition to the PSRGs, metals results were compared to published concentrations for naturally
occurring metals in soil. A brief summary of the final grade soil sampling results is provided
below.
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VOCs
Low levels of the VOCs acetone, carbon disulfide, ethanol, methyl ethyl ketone, and methylene
chloride were detected at estimated (J-flag) concentrations above the laboratory method detection
limits but below the reporting limits in one or more final grade soil evaluation area. No VOCs
were detected above DEQ Residential or Industrial/Commercial PSRGs.

SVOCs
Low levels of polynuclear aromatic hydrocarbons (PAHs) were detected at estimated (J-flag)
concentrations above the laboratory method detection limits in final grade soil sample FG-4. The
concentration of benzo(a)pyrene [0.290 J milligrams per kilogram (mg/kg)] detected in final grade
soil sample FG-4 slightly exceeds the Residential PSRG of 0.11 mg/kg, but is below the
Industrial/Commercial PSRG of 2.1 mg/kg. No other SVOCs were detected at concentrations
above the PSRGs in the final grade soil samples.

Metals
Due to the presence of naturally occurring metals in soil, several metals were detected at
concentrations above laboratory method detection limits in the final grade samples collected at the
Site. Arsenic was detected at concentrations above the Residential PSRG of 0.68 mg/kg in each
final grade evaluation area, and the arsenic concentration (3.02 mg/kg) in sample FG-2 also
slightly exceeded the Industrial/Commercial PSRG of 3.0 mg/kg. However, the arsenic
concentrations are consistent with naturally occurring levels in North Carolina soils and are
considered representative of background conditions.

Low concentrations of hexavalent chromium (ranging from 1.2 to 2.7 mg/kg) were detected in
each of the final grade soil samples at concentrations above the Residential PSRG of 0.31 mg/kg.
However, the concentrations were below the Industrial/Commercial PSRG of 6.5 mg/kg.
Additionally, because hexavalent chromium was detected at relatively consistent concentrations
in each of the final grade soil samples collected across the Site, H&H concludes that the hexavalent
chromium is likely naturally occurring.

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2.3 Exposure Risk Evaluation

The DEQ health-based PSRGs are very conservative and based on the lower of a Target
Carcinogenic Risk (TCR) of 1 x 10-6 for potential carcinogenic risks and a Target Hazard Quotient
(THQ) of 0.2 for potential non-carcinogenic risks. The DEQ and EPA acceptable risks for
potential carcinogenic risks is a cumulative lifetime incremental carcinogenic risk (LICR) of
1 x 10-4 and a cumulative hazard index (HI) of 1.0 for non-carcinogenic risks. Therefore, H&H
utilized the DEQ Risk Calculator (January 2022) to further evaluate cumulative risks to occupants
and workers based on the final grade soil sample analytical results.

The highest concentration of each compound detected in any final grade soil sample was used to
model a hypothetical worst-case exposure risk under the residential, non-residential worker, and
construction worker scenarios. Results of risk calculations are presented in the table below:

Exposure Scenario Cumulative LICR Cumulative HI Risk Exceeded?
Residential 1.7 x 10-5 0.16 No
Non-Residential Worker 1.6 x 10-6 0.012 No
Construction Worker 9.4 x 10-7 0.12 No

As shown in the table above, the results of the risk calculations indicate that the calculated
cumulative carcinogenic and non-carcinogenic risks are below the DEQ and EPA acceptable levels
for residential, non-residential worker, and construction worker scenarios. A copy of the
completed DEQ Risk Calculator is provided as Appendix B.
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3.0 Summary

Redevelopment activities at the North Davidson II Brownfields property located at 2315 N.
Davidson Street and 421 E. 26th Street in Charlotte, Mecklenburg County, North Carolina are
nearing completion. Redevelopment activities include adaptive re-use of two existing Site
buildings with landscaped areas and an outdoor patio on the eastern portion of the northwestern
Site parcel. In March 2022, H&H conducted final grade soil sampling activities at the Site in
accordance with the DEQ Brownfields-approved Work Plan dated March 10, 2022. Final grade
soil sampling activities included the collection of soil samples to evaluate the potential for impacts
in areas at the Site that would not be covered by impervious surfaces following redevelopment.

Laboratory analytical results indicate the presence of benzo(a)pyrene, arsenic, and hexavalent
chromium at concentrations above the DEQ Residential PSRGs. The concentration of arsenic in
one composite soil sample also slightly exceeded the Industrial/Commercial PSRG. However, the
detected arsenic concentrations in the final grade soil samples are consistent with naturally
occurring levels in North Carolina soils. Based on the similar concentrations detected across the
Site, the hexavalent chromium concentrations reported in the final grade soil samples are also
likely naturally occurring.

H&H utilized the DEQ Risk Calculator to further evaluate cumulative risks to occupants and
workers based on the highest concentration of each compound detected in any final grade
evaluation area at the Site. Results of the hypothetical worst-case risk calculations indicate that
cumulative carcinogenic and non-carcinogenic risks are below the DEQ and EPA acceptable levels
for the residential, non-residential worker, and construction worker exposure scenarios.

The Site has been redeveloped for its intended use in accordance with the DEQ-approved EMP
and the recorded Brownfields Agreement.

.
Table 1Soil Lithology SummaryNorth Davidson II Brownfields Property2315 N. Davidson Street and 421 E. 26th StreetCharlotte, North CarolinaBrownfields Project No.: 24003-20-060H&H Job No. PAM-003Sample ID Sample Date Sample Time Depth(ft bgs)Moisture Content Stiffness Color LithologyPID Reading(ppm)NotesFG-1A0-1moist medium stiff red brown sandy SILT w tr gravel0.0FG-1A1-2moist medium stiff red brown sandy SILT w gravel0.0FG-1B0-1moist soft brown sandy SILT w gravel0.7FG-1B1-2moist soft brown sandy SILT w gravel0.2FG-1C0-1moist medium dense dark brown silty SAND w gravel0.2FG-1C1-2moist medium stiff red and orange sandy SILT w tr clay0.1FG-1D0-1moist loose dark brown and gray gravel w silty sand0.1FG-1D1-2moist medium stiff red and orange clayey SILT w tr sand0.2FG-1E0-1moist soft red brown sandy SILT0.1FG-1E1-2moist soft brown clayey SILT 7.4VOC grab sampleFG-2A0-1moist medium stiff brown sandy SILT w gravel94.1VOC grab sampleFG-2A1-2moist medium stiff brown and gray sandy SILT w gravel65.9FG-2B0-1moist medium stiff red, orange and brown sandy SILT w gravel0.0FG-2B1-2moist medium stiff red, orange and brown sandy SILT w gravel0.0FG-2C0-1moist medium stiff brown and blacksandy SILT w gravel and asphalt64.0FG-2C1-2N/A N/A N/A N/A N/A no recovery (asphalt)FG-2D0-1moist medium stiff brown clayey SILT w tr sand0.0FG-2D1-2moist medium stiff red and orange sandy SILT w gravel0.0FG-2E0-1moist medium stiff brown clayey SILT w gravel0.5FG-2E1-2moist medium stiff brown clayey SILT w gravel0.2FG-3A0-1moist medium stiff red and orange sandy SILT w gravel0.0FG-3A1-2moist medium stiff red and orange sandy SILT w gravel0.0FG-3B0-1 moist medium stiff brown CLAY tr sand 0.5FG-3B1-2 moist medium stiff brown and gray clayey SILT w sand 2.4 VOC grab sampleFG-3C0-1 moist medium stiff red and orangesandy SILT w gravel and tr clay0.0FG-3C1-2 moist medium stiff red and orangesandy SILT w gravel and tr clay0.0FG-3D0-1 moist medium stiff red brown sandy CLAY w gravel 0.0FG-3D1-2 moist medium stiff red brown sandy CLAY w gravel 0.4FG-3E0-1 moist medium stiff red and orangesandy SILT w gravel and tr clay0.1FG-3E1-2 moist medium stiff red and orangesandy SILT w gravel and tr clay0.0FG-4A0-1 moist medium stiff red and orange silty SAND w gravel 1.3FG-4A1-2 moist medium stiff red and orange silty SAND w gravel 4.0FG-4B0-1 dry stiff brown sandy SILT w tr gravel 5.6FG-4B1-2 dry stiff dark brown sandy SILT w tr gravel 24.2 VOC grab SampleFG-4C0-1 dry medium stiff brown sandy SILT w tr gravel 22.9FG-4C1-2 dry medium stiff brown sandy SILT w tr gravel 4.7FG-4D0-1 dry stiff brown sandy SILT w gravel 0.2FG-4D1-2 dry stiff brown sandy SILT w gravel 0.0FG-5A0-1 moist loose orange and brown silty SAND 4.4 VOC grab sampleFG-5A1-2 moist loose orange and brown silty SAND 4.2FG-5B0-1moist loose orange and brown silty SAND0.7FG-5B1-2moist loose orange and brown silty SAND3.1FG-5C0-1moist medium stiff red clayey SILT w tr sand3.3FG-5C1-2moist medium stiff red clayey SILT w tr sand3.3Notes:parts per million = ppm; ft bgs = feet below ground surface3/21/2022 11:453/21/2022 15:053/21/2022 15:153/21/2022 10:353/21/2022 12:55https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/PAMAKA - PAM/PAM-003 N. Davidson & E. 26th/Final Grade Sampling/Tables/Tables.xlsx4/7/2022Table 1 (Page 1 of 1)Hart & Hickman, PC
Table 2Summary of Soil Analytical DataNorth Davidson II Brownfields Property2315 N. Davidson Street and 421 E. 26th StreetCharlotte, North CarolinaBrownfields Project No.: 24003-20-060H&H Job No. PAM-003Sample IDSample TypeComposite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite GrabSample Depth (ft bgs)0-2 1-2 0-2 0-1 0-2 0-1 0-2 1-2 0-2 1-2 0-2 0-1Sample DateRange MeanUnitsVOCs (8260D)AcetoneNA0.018 JNA0.037NA0.017 JNA0.012 JNA0.012 JNA0.018 J 14,000 210,000 -- --Carbon DisulfideNA <0.0007 NA <0.0007 NA <0.0007 NA <0.0008 NA0.0009 JNA <0.0008160 740 -- --EthanolNA0.047 JNA <0.016 NA <0.014 NA <0.016 NA0.032 JNA <0.017NE NE -- --Methyl Ethyl KetoneNA0.002 JNA0.004 JNA0.001 JNA0.001 JNA0.002 JNA0.002 J 5,500 40,000 -- --Methylene ChlorideNA <0.001 NA0.001 JNA <0.001 NA <0.001 NA <0.001 NA <0.00158 650-- --SVOCs (8270E)Benzo(a)anthracene<0.159 NA <0.161 NA <0.161 NA <0.167 NA0.315 JNA <0.169 NA1.1 21-- --Benzo(a)pyrene<0.168 NA <0.170 NA <0.170 NA <0.176 NA0.290 JNA <0.179 NA0.11 2.1-- --Benzo(b)fluoranthene<0.167 NA <0.169 NA <0.169 NA <0.175 NA0.535 JNA <0.178 NA1.1 21-- --Chrysene<0.162 NA <0.165 NA <0.165 NA <0.170 NA0.411 JNA <0.173 NA110 2,100-- --Fluoranthene<0.140 NA <0.143 NA <0.143 NA <0.148 NA0.718 JNA <0.150 NA480 6,000-- --Pyrene<0.153 NA <0.155 NA <0.155 NA <0.161 NA0.654 JNA <0.163 NA360 4,500-- --Metals (6010D/7471B/7199)Arsenic 2.79NA2.95NA3.02NA1.88NA1.99NA2.35NA0.68 3.0 1.0 - 18 4.8Barium 80.3NA84.9NA86.2NA102NA109NA107NA3,100 47,000 50 - 1,000 356Cadmium 0.106 JNA0.0479 JNA0.126NA0.0243 JNA0.256NA <0.0098 NA1.4 20 1.0 - 10 4.3Chromium (total) 61.6NA55.1NA54.7NA44.9NA40.6NA54.8NANE NE 7.0 - 300 65Chromium (trivalent) 59.7NA53.3NA53.3NA43.4NA39.4NA52.1NA23,000 350,000 NS NSChromium (hexavalent)1.9NA1.8NA1.4NA1.5NA1.2NA2.7NA0.31 6.5 NS NSLead 33.0NA17.8NA23.1NA14.0NA59.1NA11.1NA400 800 ND - 50 16Mercury 0.0368NA0.0819NA0.0404NA0.0548NA0.0530NA0.0445NA4.7 70 0.03 - 0.52 0.121Selenium 0.342 JNA <0.220 NA <0.201 NA <0.228 NA <0.207 NA <0.231 NA78 1,200 <0.1 - 0.8 0.42Silver<0.0332 NA <0.0337 NA <0.0307 NA <0.0348 NA <0.0316 NA <0.0353 NA78 1,200 ND - 5.0 NSNotes:2) Range and mean values of background metals for North Carolina soils published in Elements in North American Soils by Dragun and Chekiri, 2005. North Carolina values are generally shown; however, southeastern and conterminous US soil values are shown for cadmium and silver.With the exception of metals, only compounds detected in at least one sample are shown in the table above.Compound concentrations are reported to the laboratory method detection limit.Soil concentrations are reported in milligrams per kilogram (mg/kg). Laboratory analytical methods are shown in parentheses.Bold indicates concentration is above the Residential PSRG and regional background levels in the case of metals.Trivalent chromium value was calculated by subtracting the hexavalent chromium concentration from the total chromium concentration.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Actft bgs = feet below ground surface; NE = not established; NA = not analyzed; -- = not applicable; NS = not specifiedJ = compound was detected above the laboratory method detection limit but below the laboratory reporting limit, resulting in an estimated concentration.Residential PSRGs(1)1) North Carolina Department of Environmental Quality (DEQ) Residential and Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) (January 2022)Industrial/Commercial PSRGs(1)Regional Background Metals in Soil(2)mg/kgFG-53/21/20223/21/2022 3/21/2022 3/21/20223/21/2022FG-2 / FG-DUPFG-1FG-3 FG-4https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/PAMAKA - PAM/PAM-003 N. Davidson & E. 26th/Final Grade Sampling/Tables/Tables.xlsx4/7/2022Table 2 (Page 1 of 1)Hart & Hickman, PC
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NORTH CAROLINA 1991
TITLE
PROJECT
SITE LOCATION MAP
1257+'$9,'621,,%52:1),(/'63523(57<
2315 N. DAVIDSON STREET & 421 E. 26TH STREET
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
0
1PAM-003
SITE
FG-4A
FG-4B
FG-4C
FG-4D
FG-2E
FG-2D
FG-2C
FG-2B
FG-2A
FG-3A
FG-3B
FG-3C
FG-3D
FG-3E
FG-1A
FG-1B
FG-1C
FG-1D
FG-1E
REVISION NO. 0
JOB NO. PAM-003
DATE: 3-31-22
FIGURE NO. 2
NORTH DAVIDSON II BROWNFIELDS PROPERTY
2315 N. DAVIDSON STREET & 421 E. 26TH STREET
CHARLOTTE, NORTH CAROLINA
FINAL GRADE SOIL SAMPLE
LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
LITTLE SUGAR CREEK
DRAINAGE FEATURE
COMPOSITE SOIL SAMPLE AREA
FG-1 SOIL ALIQUOT SAMPLE LOCATION
FG-2 SOIL ALIQUOT SAMPLE LOCATION
FG-3 SOIL ALIQUOT SAMPLE LOCATION
FG-4 SOIL ALIQUOT SAMPLE LOCATION
FG-5 SOIL ALIQUOT SAMPLE LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 GeologyLYNX
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NOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS (2021).
2.COMPOSITE SOIL SAMPLE AREAS INCLUDE GRASS,
ARTIFICIAL TURF, CRUSHED STONE, AND LANDSCAPED
AREAS.
FG-5A
FG-5B
FG-5C
S:\AAA-Master Projects\PAMAKA - PAM\PAM-003 N. Davidson & E. 26th\Final Grade Sampling\Figures\Site Map 20220309.dwg, FIG 2, 3/31/2022 10:38:58 AM, sperry

Appendix A
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

3/31/2022
Hart & Hickman (Charlotte) Bo Cappleman
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-080-0034 Client Project Description: PAM-003
Dear Bo Cappleman:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/21/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 92
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-080-0034
Page 2 of 92
Report Number:
Sample Summary Table
Client Project Description:
22-080-0034
PAM-003
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
03/21/2022 12:55Solids 96591 FG-1 03/21/2022 16:30 7199
03/21/2022 12:55Solids 96591 FG-1 03/21/2022 16:30
03/21/2022 10:35Solids 96592 FG-2 03/21/2022 16:30 7199
03/21/2022 10:35Solids 96592 FG-2 03/21/2022 16:30
03/21/2022 11:45Solids 96593 FG-3 03/21/2022 16:30 7199
03/21/2022 11:45Solids 96593 FG-3 03/21/2022 16:30
03/21/2022 15:05Solids 96594 FG-4 03/21/2022 16:30 7199
03/21/2022 15:05Solids 96594 FG-4 03/21/2022 16:30
03/21/2022 15:15Solids 96595 FG-5 03/21/2022 16:30 7199
03/21/2022 15:15Solids 96595 FG-5 03/21/2022 16:30
03/21/2022Solids 96596 FG-DUP 03/21/2022 16:30 7199
03/21/2022Solids 96596 FG-DUP 03/21/2022 16:30
: Eurofins Eaton Analytical, Inc. - PA Lab, Lancaster, PA
Page 3 of 92
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-080-0034
Report Limit
Project:PAM-003
V 96591FG-1
2.79 03/24/2022 12:006010DArsenicmg/Kg - dry 0.171
80.3 03/24/2022 12:006010DBariummg/Kg - dry 0.032
J0.106 03/24/2022 12:006010DCadmiummg/Kg - dry 0.0092
61.6 03/24/2022 12:006010DChromiummg/Kg - dry 0.194
33.0 03/24/2022 12:006010DLeadmg/Kg - dry 0.090
J0.342 03/24/2022 12:006010DSeleniummg/Kg - dry 0.217
0.0368 03/23/2022 16:477471BMercury (Total)mg/Kg - dry 0.0137
J0.018 03/25/2022 15:428260DAcetonemg/Kg - dry 0.002
J0.047 03/25/2022 15:428260DEthanolmg/Kg - dry 0.016
J0.002 03/25/2022 15:428260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
12.7 03/24/2022 10:33SW-DRYWT Moisture %
V 96592FG-2
2.95 03/24/2022 12:046010DArsenicmg/Kg - dry 0.174
84.9 03/24/2022 12:046010DBariummg/Kg - dry 0.032
J0.0479 03/24/2022 12:046010DCadmiummg/Kg - dry 0.0094
55.1 03/24/2022 12:046010DChromiummg/Kg - dry 0.197
17.8 03/24/2022 12:046010DLeadmg/Kg - dry 0.091
0.0819 03/23/2022 16:507471BMercury (Total)mg/Kg - dry 0.0140
0.037 03/25/2022 16:098260DAcetonemg/Kg - dry 0.002
J0.004 03/25/2022 16:098260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.001 03/25/2022 16:098260DMethylene Chloride mg/Kg - dry 0.001
14.0 03/24/2022 10:33SW-DRYWT Moisture %
V 96593FG-3
1.88 03/24/2022 12:286010DArsenicmg/Kg - dry 0.180
102 03/24/2022 12:286010DBariummg/Kg - dry 0.033
J0.0243 03/24/2022 12:286010DCadmiummg/Kg - dry 0.0097
44.9 03/24/2022 12:286010DChromiummg/Kg - dry 0.204
14.0 03/24/2022 12:286010DLeadmg/Kg - dry 0.095
0.0548 03/23/2022 16:317471BMercury (Total)mg/Kg - dry 0.0144
J0.012 03/25/2022 16:378260DAcetonemg/Kg - dry 0.002
J0.001 03/25/2022 16:378260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
16.9 03/24/2022 10:33SW-DRYWT Moisture %
V 96594FG-4
1.99 03/24/2022 12:086010DArsenicmg/Kg - dry 0.163
109 03/24/2022 12:086010DBariummg/Kg - dry 0.030
Page 4 of 92
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-080-0034
Report Limit
Project:PAM-003
V 96594FG-4
0.256 03/24/2022 12:086010DCadmiummg/Kg - dry 0.0088
40.6 03/24/2022 12:086010DChromiummg/Kg - dry 0.185
59.1 03/24/2022 12:086010DLeadmg/Kg - dry 0.086
0.0530 03/23/2022 16:527471BMercury (Total)mg/Kg - dry 0.0131
J0.012 03/25/2022 17:058260DAcetonemg/Kg - dry 0.002
J0.0009 03/25/2022 17:058260DCarbon Disulfide mg/Kg - dry 0.0007
J0.032 03/25/2022 17:058260DEthanolmg/Kg - dry 0.015
J0.002 03/25/2022 17:058260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.315 03/24/2022 18:258270EBenzo(a)anthracene mg/Kg - dry 0.151
J0.290 03/24/2022 18:258270EBenzo(a)pyrene mg/Kg - dry 0.160
J0.535 03/24/2022 18:258270EBenzo(b)fluoranthene mg/Kg - dry 0.159
J0.411 03/24/2022 18:258270EChrysenemg/Kg - dry 0.155
J0.718 03/24/2022 18:258270EFluoranthenemg/Kg - dry 0.134
J0.654 03/24/2022 18:258270EPyrenemg/Kg - dry 0.146
8.45 03/24/2022 10:33SW-DRYWT Moisture %
V 96595FG-5
2.35 03/24/2022 12:126010DArsenicmg/Kg - dry 0.182
107 03/24/2022 12:126010DBariummg/Kg - dry 0.034
54.8 03/24/2022 12:126010DChromiummg/Kg - dry 0.207
11.1 03/24/2022 12:126010DLeadmg/Kg - dry 0.096
0.0445 03/23/2022 17:027471BMercury (Total)mg/Kg - dry 0.0146
J0.018 03/25/2022 17:338260DAcetonemg/Kg - dry 0.002
J0.002 03/25/2022 17:338260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
18.0 03/24/2022 10:33SW-DRYWT Moisture %
V 96596FG-DUP
3.02 03/24/2022 12:246010DArsenicmg/Kg - dry 0.159
86.2 03/24/2022 12:246010DBariummg/Kg - dry 0.029
0.126 03/24/2022 12:246010DCadmiummg/Kg - dry 0.0085
54.7 03/24/2022 12:246010DChromiummg/Kg - dry 0.180
23.1 03/24/2022 12:246010DLeadmg/Kg - dry 0.083
0.0404 03/23/2022 17:047471BMercury (Total)mg/Kg - dry 0.0127
J0.017 03/25/2022 18:008260DAcetonemg/Kg - dry 0.002
J0.001 03/25/2022 18:008260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
5.68 03/24/2022 10:33SW-DRYWT Moisture %
Page 5 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-1
96591 Matrix:
3/21/2022 12:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.7 %Moisture 1 03/24/22 10:33 SW-DRYWTSJL
2.79 mg/Kg - dry 0.171 0.572Arsenic 1 03/24/22 12:00 6010DEDV
80.3 mg/Kg - dry 0.032 0.572Barium 1 03/24/22 12:00 6010DEDV
0.106 J mg/Kg - dry 0.0092 0.115Cadmium 1 03/24/22 12:00 6010DEDV
61.6 mg/Kg - dry 0.194 0.572Chromium 1 03/24/22 12:00 6010DEDV
33.0 mg/Kg - dry 0.090 0.343
Lead 1 03/24/22 12:00 6010DEDV
0.0368 mg/Kg - dry 0.0137 0.0344Mercury (Total)1 03/23/22 16:47 7471BEDV
0.342 J mg/Kg - dry 0.217 0.572Selenium 1 03/24/22 12:00 6010DEDV
<0.0332 mg/Kg - dry 0.0332 0.286Silver 1 03/24/22 12:00 6010DEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-1
96591 Matrix:
3/21/2022 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
0.018 J mg/Kg - dry 0.002 0.022Acetone 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 03/25/22 15:42 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 03/25/22 15:42 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 03/25/22 15:42 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 03/25/22 15:42 V16630TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 03/25/22 15:42 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 03/25/22 15:42 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 03/25/22 15:42 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 03/25/22 15:42 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 03/25/22 15:42 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 03/25/22 15:42 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-1
96591 Matrix:
3/21/2022 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 03/25/22 15:42 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 03/25/22 15:42 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 03/25/22 15:42 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 03/25/22 15:42 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 03/25/22 15:42 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 03/25/22 15:42 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 03/25/22 15:42 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 03/25/22 15:42 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 03/25/22 15:42 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 03/25/22 15:42 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 03/25/22 15:42 V16630TBL
0.047 J mg/Kg - dry 0.016 0.286Ethanol 1 03/25/22 15:42 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 03/25/22 15:42 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 03/25/22 15:42 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 03/25/22 15:42 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-1
96591 Matrix:
3/21/2022 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 03/25/22 15:42 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 03/25/22 15:42 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 03/25/22 15:42 V16630TBL
0.002 J mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 03/25/22 15:42 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 03/25/22 15:42 V16630TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 03/25/22 15:42 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 03/25/22 15:42 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 03/25/22 15:42 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 03/25/22 15:42 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 03/25/22 15:42 V16630TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 03/25/22 15:42 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 03/25/22 15:42 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-1
96591 Matrix:
3/21/2022 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 03/25/22 15:42 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 03/25/22 15:42 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 03/25/22 15:42 V16630TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 03/25/22 15:42 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 03/25/22 15:42 V16630
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%03/25/22 15:421 TBL V16630
Surrogate: Dibromofluoromethane 102 Limits: 84-123%03/25/22 15:421 TBL V16630
Surrogate: Toluene-d8 96.1 Limits: 76-129%03/25/22 15:421 TBL V16630
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.132 mg/Kg - dry 0.132 0.756Acenaphthene 1 03/24/22 17:19 V16588JMV
<0.120 mg/Kg - dry 0.120 0.756Acenaphthylene 1 03/24/22 17:19 V16588JMV
<0.174 mg/Kg - dry 0.174 0.756Aniline 1 03/24/22 17:19 V16588JMV
<0.163 mg/Kg - dry 0.163 0.756Anthracene 1 03/24/22 17:19 V16588JMV
<0.159 mg/Kg - dry 0.159 0.756
Benzo(a)anthracene 1 03/24/22 17:19 V16588JMV
<0.168 mg/Kg - dry 0.168 0.756Benzo(a)pyrene 1 03/24/22 17:19 V16588JMV
<0.167 mg/Kg - dry 0.167 0.756Benzo(b)fluoranthene 1 03/24/22 17:19 V16588JMV
<0.155 mg/Kg - dry 0.155 0.756Benzo(g,h,i)perylene 1 03/24/22 17:19 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-1
96591 Matrix:
3/21/2022 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.156 mg/Kg - dry 0.156 0.756Benzo(k)fluoranthene 1 03/24/22 17:19 V16588JMV
<0.664 mg/Kg - dry 0.664 2.29Benzoic Acid 1 03/24/22 17:19 V16588JMV
<0.120 mg/Kg - dry 0.120 0.756Benzyl alcohol 1 03/24/22 17:19 V16588JMV
<0.135 mg/Kg - dry 0.135 0.756Bis(2-Chloroethoxy)methane 1 03/24/22 17:19 V16588JMV
<0.122 mg/Kg - dry 0.122 0.756Bis(2-Chloroethyl)ether 1 03/24/22 17:19 V16588JMV
<0.155 mg/Kg - dry 0.155 0.378Bis(2-Chloroisopropyl)ether 1 03/24/22 17:19 V16588JMV
<0.137 mg/Kg - dry 0.137 0.756Bis(2-ethylhexyl)phthalate 1 03/24/22 17:19 V16588JMV
<0.124 mg/Kg - dry 0.124 0.7564-Bromophenyl phenyl ether 1 03/24/22 17:19 V16588JMV
<0.129 mg/Kg - dry 0.129 0.378
Butyl benzyl phthalate 1 03/24/22 17:19 V16588JMV
<0.105 mg/Kg - dry 0.105 0.7564-Chloro-3-methylphenol 1 03/24/22 17:19 V16588JMV
<0.128 mg/Kg - dry 0.128 0.3784-Chloroaniline 1 03/24/22 17:19 V16588JMV
<0.132 mg/Kg - dry 0.132 0.7562-Chloronaphthalene 1 03/24/22 17:19 V16588JMV
<0.112 mg/Kg - dry 0.112 0.7562-Chlorophenol 1 03/24/22 17:19 V16588JMV
<0.144 mg/Kg - dry 0.144 1.154-Chlorophenyl phenyl ether 1 03/24/22 17:19 V16588JMV
<0.162 mg/Kg - dry 0.162 0.756Chrysene 1 03/24/22 17:19 V16588JMV
<0.263 mg/Kg - dry 0.263 0.756
Dibenz(a,h)anthracene 1 03/24/22 17:19 V16588JMV
<0.136 mg/Kg - dry 0.136 0.756Dibenzofuran 1 03/24/22 17:19 V16588JMV
<0.108 mg/Kg - dry 0.108 0.7561,2-Dichlorobenzene 1 03/24/22 17:19 V16588JMV
<0.111 mg/Kg - dry 0.111 0.7561,3-Dichlorobenzene 1 03/24/22 17:19 V16588JMV
<0.111 mg/Kg - dry 0.111 0.3781,4-Dichlorobenzene 1 03/24/22 17:19 V16588JMV
<0.168 mg/Kg - dry 0.168 0.7563,3'-Dichlorobenzidine 1 03/24/22 17:19 V16588JMV
<0.109 mg/Kg - dry 0.109 0.7562,4-Dichlorophenol 1 03/24/22 17:19 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-1
96591 Matrix:
3/21/2022 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.206 mg/Kg - dry 0.206 0.756Diethyl phthalate 1 03/24/22 17:19 V16588JMV
<0.199 mg/Kg - dry 0.199 0.756Dimethyl phthalate 1 03/24/22 17:19 V16588JMV
<0.123 mg/Kg - dry 0.123 0.3782,4-Dimethylphenol 1 03/24/22 17:19 V16588JMV
<0.122 mg/Kg - dry 0.122 0.756Di-n-butyl phthalate 1 03/24/22 17:19 V16588JMV
<0.274 mg/Kg - dry 0.274 1.724,6-Dinitro-2-methylphenol 1 03/24/22 17:19 V16588JMV
<0.595 mg/Kg - dry 0.595 1.722,4-Dinitrophenol 1 03/24/22 17:19 V16588JMV
<0.110 mg/Kg - dry 0.110 0.7562,4-Dinitrotoluene 1 03/24/22 17:19 V16588JMV
<0.123 mg/Kg - dry 0.123 0.7562,6-Dinitrotoluene 1 03/24/22 17:19 V16588JMV
<0.163 mg/Kg - dry 0.163 0.378
Di-n-Octyl Phthalate 1 03/24/22 17:19 V16588JMV
<0.140 mg/Kg - dry 0.140 0.756Fluoranthene 1 03/24/22 17:19 V16588JMV
<0.146 mg/Kg - dry 0.146 0.756Fluorene 1 03/24/22 17:19 V16588JMV
<0.121 mg/Kg - dry 0.121 0.756Hexachlorobenzene 1 03/24/22 17:19 V16588JMV
<0.111 mg/Kg - dry 0.111 0.756Hexachlorobutadiene 1 03/24/22 17:19 V16588JMV
<0.179 mg/Kg - dry 0.179 0.756Hexachlorocyclopentadiene 1 03/24/22 17:19 V16588JMV
<0.090 mg/Kg - dry 0.090 0.756Hexachloroethane 1 03/24/22 17:19 V16588JMV
<0.205 mg/Kg - dry 0.205 0.756
Indeno(1,2,3-cd)pyrene 1 03/24/22 17:19 V16588JMV
<0.218 mg/Kg - dry 0.218 0.756Isophorone 1 03/24/22 17:19 V16588JMV
<0.121 mg/Kg - dry 0.121 0.7561-Methylnaphthalene 1 03/24/22 17:19 V16588JMV
<0.114 mg/Kg - dry 0.114 0.7562-Methylnaphthalene 1 03/24/22 17:19 V16588JMV
<0.111 mg/Kg - dry 0.111 0.7562-Methylphenol 1 03/24/22 17:19 V16588JMV
<0.097 mg/Kg - dry 0.097 0.7563&4 Methylphenol 1 03/24/22 17:19 V16588JMV
<0.164 mg/Kg - dry 0.164 0.756Naphthalene 1 03/24/22 17:19 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-1
96591 Matrix:
3/21/2022 12:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.110 mg/Kg - dry 0.110 0.7562-Nitroaniline 1 03/24/22 17:19 V16588JMV
<0.137 mg/Kg - dry 0.137 0.7563-Nitroaniline 1 03/24/22 17:19 V16588JMV
<0.106 mg/Kg - dry 0.106 0.3784-Nitroaniline 1 03/24/22 17:19 V16588JMV
<0.132 mg/Kg - dry 0.132 0.378Nitrobenzene 1 03/24/22 17:19 V16588JMV
<0.101 mg/Kg - dry 0.101 0.7562-Nitrophenol 1 03/24/22 17:19 V16588JMV
<0.134 mg/Kg - dry 0.134 0.7564-Nitrophenol 1 03/24/22 17:19 V16588JMV
<0.301 mg/Kg - dry 0.301 0.756N-Nitrosodimethylamine 1 03/24/22 17:19 V16588JMV
<0.207 mg/Kg - dry 0.207 0.756N-Nitrosodiphenylamine 1 03/24/22 17:19 V16588JMV
<0.135 mg/Kg - dry 0.135 0.756
N-Nitroso-di-n-propylamine 1 03/24/22 17:19 V16588JMV
<0.397 mg/Kg - dry 0.397 1.15Pentachlorophenol 1 03/24/22 17:19 V16588JMV
<0.238 mg/Kg - dry 0.238 0.756Phenanthrene 1 03/24/22 17:19 V16588JMV
<0.128 mg/Kg - dry 0.128 0.756Phenol 1 03/24/22 17:19 V16588JMV
<0.153 mg/Kg - dry 0.153 0.756Pyrene 1 03/24/22 17:19 V16588JMV
<0.090 mg/Kg - dry 0.090 0.378Pyridine 1 03/24/22 17:19 V16588JMV
<0.122 mg/Kg - dry 0.122 0.7561,2,4-Trichlorobenzene 1 03/24/22 17:19 V16588JMV
<0.110 mg/Kg - dry 0.110 0.756
2,4,5-Trichlorophenol 1 03/24/22 17:19 V16588JMV
<0.110 mg/Kg - dry 0.110 0.7562,4,6-Trichlorophenol 1 03/24/22 17:19 V16588JMV
8270ESurrogate: Phenol-d5 72.4 Limits: 34-121%03/24/22 17:191 JMV
Surrogate: 2-Fluorobiphenyl 79.0 Limits: 44-115%03/24/22 17:191 JMV V16588
Surrogate: 2-Fluorophenol 74.5 Limits: 35-115%03/24/22 17:191 JMV V16588
Surrogate: Nitrobenzene-d5 72.5 Limits: 37-122%03/24/22 17:191 JMV V16588
Surrogate: 4-Terphenyl-d14 81.4 Limits: 54-127%03/24/22 17:191 JMV V16588
Surrogate: 2,4,6-Tribromophenol 82.3 Limits: 39-132%03/24/22 17:191 JMV V16588
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-2
96592 Matrix:
3/21/2022 10:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.0 %Moisture 1 03/24/22 10:33 SW-DRYWTSJL
2.95 mg/Kg - dry 0.174 0.581Arsenic 1 03/24/22 12:04 6010DEDV
84.9 mg/Kg - dry 0.032 0.581Barium 1 03/24/22 12:04 6010DEDV
0.0479 J mg/Kg - dry 0.0094 0.116Cadmium 1 03/24/22 12:04 6010DEDV
55.1 mg/Kg - dry 0.197 0.581Chromium 1 03/24/22 12:04 6010DEDV
17.8 mg/Kg - dry 0.091 0.348
Lead 1 03/24/22 12:04 6010DEDV
0.0819 mg/Kg - dry 0.0140 0.0349Mercury (Total)1 03/23/22 16:50 7471BEDV
<0.220 mg/Kg - dry 0.220 0.581Selenium 1 03/24/22 12:04 6010DEDV
<0.0337 mg/Kg - dry 0.0337 0.291Silver 1 03/24/22 12:04 6010DEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-2
96592 Matrix:
3/21/2022 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
0.037 mg/Kg - dry 0.002 0.023Acetone 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 03/25/22 16:09 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 03/25/22 16:09 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 03/25/22 16:09 V16630TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 03/25/22 16:09 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 03/25/22 16:09 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 03/25/22 16:09 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 03/25/22 16:09 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-2
96592 Matrix:
3/21/2022 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 03/25/22 16:09 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 03/25/22 16:09 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 03/25/22 16:09 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 03/25/22 16:09 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 03/25/22 16:09 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 03/25/22 16:09 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 03/25/22 16:09 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 03/25/22 16:09 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 03/25/22 16:09 V16630TBL
<0.016 mg/Kg - dry 0.016 0.290Ethanol 1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 03/25/22 16:09 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 03/25/22 16:09 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 03/25/22 16:09 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-2
96592 Matrix:
3/21/2022 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 03/25/22 16:09 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 03/25/22 16:09 V16630TBL
0.004 J mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 03/25/22 16:09 V16630TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 03/25/22 16:09 V16630TBL
0.001 J mg/Kg - dry 0.001 0.011Methylene Chloride 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 03/25/22 16:09 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 03/25/22 16:09 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 03/25/22 16:09 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 03/25/22 16:09 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 03/25/22 16:09 V16630TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 03/25/22 16:09 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 03/25/22 16:09 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-2
96592 Matrix:
3/21/2022 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 03/25/22 16:09 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 03/25/22 16:09 V16630TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 03/25/22 16:09 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 03/25/22 16:09 V16630
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%03/25/22 16:091 TBL V16630
Surrogate: Dibromofluoromethane 102 Limits: 84-123%03/25/22 16:091 TBL V16630
Surrogate: Toluene-d8 94.7 Limits: 76-129%03/25/22 16:091 TBL V16630
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.134 mg/Kg - dry 0.134 0.767Acenaphthene 1 03/24/22 17:41 V16588JMV
<0.122 mg/Kg - dry 0.122 0.767Acenaphthylene 1 03/24/22 17:41 V16588JMV
<0.176 mg/Kg - dry 0.176 0.767Aniline 1 03/24/22 17:41 V16588JMV
<0.166 mg/Kg - dry 0.166 0.767Anthracene 1 03/24/22 17:41 V16588JMV
<0.161 mg/Kg - dry 0.161 0.767
Benzo(a)anthracene 1 03/24/22 17:41 V16588JMV
<0.170 mg/Kg - dry 0.170 0.767Benzo(a)pyrene 1 03/24/22 17:41 V16588JMV
<0.169 mg/Kg - dry 0.169 0.767Benzo(b)fluoranthene 1 03/24/22 17:41 V16588JMV
<0.158 mg/Kg - dry 0.158 0.767Benzo(g,h,i)perylene 1 03/24/22 17:41 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-2
96592 Matrix:
3/21/2022 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.159 mg/Kg - dry 0.159 0.767Benzo(k)fluoranthene 1 03/24/22 17:41 V16588JMV
<0.674 mg/Kg - dry 0.674 2.33Benzoic Acid 1 03/24/22 17:41 V16588JMV
<0.122 mg/Kg - dry 0.122 0.767Benzyl alcohol 1 03/24/22 17:41 V16588JMV
<0.137 mg/Kg - dry 0.137 0.767Bis(2-Chloroethoxy)methane 1 03/24/22 17:41 V16588JMV
<0.124 mg/Kg - dry 0.124 0.767Bis(2-Chloroethyl)ether 1 03/24/22 17:41 V16588JMV
<0.158 mg/Kg - dry 0.158 0.383Bis(2-Chloroisopropyl)ether 1 03/24/22 17:41 V16588JMV
<0.139 mg/Kg - dry 0.139 0.767Bis(2-ethylhexyl)phthalate 1 03/24/22 17:41 V16588JMV
<0.126 mg/Kg - dry 0.126 0.7674-Bromophenyl phenyl ether 1 03/24/22 17:41 V16588JMV
<0.131 mg/Kg - dry 0.131 0.383
Butyl benzyl phthalate 1 03/24/22 17:41 V16588JMV
<0.107 mg/Kg - dry 0.107 0.7674-Chloro-3-methylphenol 1 03/24/22 17:41 V16588JMV
<0.130 mg/Kg - dry 0.130 0.3834-Chloroaniline 1 03/24/22 17:41 V16588JMV
<0.134 mg/Kg - dry 0.134 0.7672-Chloronaphthalene 1 03/24/22 17:41 V16588JMV
<0.114 mg/Kg - dry 0.114 0.7672-Chlorophenol 1 03/24/22 17:41 V16588JMV
<0.146 mg/Kg - dry 0.146 1.164-Chlorophenyl phenyl ether 1 03/24/22 17:41 V16588JMV
<0.165 mg/Kg - dry 0.165 0.767Chrysene 1 03/24/22 17:41 V16588JMV
<0.267 mg/Kg - dry 0.267 0.767
Dibenz(a,h)anthracene 1 03/24/22 17:41 V16588JMV
<0.138 mg/Kg - dry 0.138 0.767Dibenzofuran 1 03/24/22 17:41 V16588JMV
<0.109 mg/Kg - dry 0.109 0.7671,2-Dichlorobenzene 1 03/24/22 17:41 V16588JMV
<0.113 mg/Kg - dry 0.113 0.7671,3-Dichlorobenzene 1 03/24/22 17:41 V16588JMV
<0.113 mg/Kg - dry 0.113 0.3831,4-Dichlorobenzene 1 03/24/22 17:41 V16588JMV
<0.170 mg/Kg - dry 0.170 0.7673,3'-Dichlorobenzidine 1 03/24/22 17:41 V16588JMV
<0.111 mg/Kg - dry 0.111 0.7672,4-Dichlorophenol 1 03/24/22 17:41 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-2
96592 Matrix:
3/21/2022 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.209 mg/Kg - dry 0.209 0.767Diethyl phthalate 1 03/24/22 17:41 V16588JMV
<0.202 mg/Kg - dry 0.202 0.767Dimethyl phthalate 1 03/24/22 17:41 V16588JMV
<0.125 mg/Kg - dry 0.125 0.3832,4-Dimethylphenol 1 03/24/22 17:41 V16588JMV
<0.124 mg/Kg - dry 0.124 0.767Di-n-butyl phthalate 1 03/24/22 17:41 V16588JMV
<0.279 mg/Kg - dry 0.279 1.744,6-Dinitro-2-methylphenol 1 03/24/22 17:41 V16588JMV
<0.604 mg/Kg - dry 0.604 1.742,4-Dinitrophenol 1 03/24/22 17:41 V16588JMV
<0.112 mg/Kg - dry 0.112 0.7672,4-Dinitrotoluene 1 03/24/22 17:41 V16588JMV
<0.125 mg/Kg - dry 0.125 0.7672,6-Dinitrotoluene 1 03/24/22 17:41 V16588JMV
<0.166 mg/Kg - dry 0.166 0.383
Di-n-Octyl Phthalate 1 03/24/22 17:41 V16588JMV
<0.143 mg/Kg - dry 0.143 0.767Fluoranthene 1 03/24/22 17:41 V16588JMV
<0.148 mg/Kg - dry 0.148 0.767Fluorene 1 03/24/22 17:41 V16588JMV
<0.123 mg/Kg - dry 0.123 0.767Hexachlorobenzene 1 03/24/22 17:41 V16588JMV
<0.113 mg/Kg - dry 0.113 0.767Hexachlorobutadiene 1 03/24/22 17:41 V16588JMV
<0.182 mg/Kg - dry 0.182 0.767Hexachlorocyclopentadiene 1 03/24/22 17:41 V16588JMV
<0.092 mg/Kg - dry 0.092 0.767Hexachloroethane 1 03/24/22 17:41 V16588JMV
<0.208 mg/Kg - dry 0.208 0.767
Indeno(1,2,3-cd)pyrene 1 03/24/22 17:41 V16588JMV
<0.222 mg/Kg - dry 0.222 0.767Isophorone 1 03/24/22 17:41 V16588JMV
<0.123 mg/Kg - dry 0.123 0.7671-Methylnaphthalene 1 03/24/22 17:41 V16588JMV
<0.116 mg/Kg - dry 0.116 0.7672-Methylnaphthalene 1 03/24/22 17:41 V16588JMV
<0.112 mg/Kg - dry 0.112 0.7672-Methylphenol 1 03/24/22 17:41 V16588JMV
<0.098 mg/Kg - dry 0.098 0.7673&4 Methylphenol 1 03/24/22 17:41 V16588JMV
<0.167 mg/Kg - dry 0.167 0.767Naphthalene 1 03/24/22 17:41 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-2
96592 Matrix:
3/21/2022 10:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.112 mg/Kg - dry 0.112 0.7672-Nitroaniline 1 03/24/22 17:41 V16588JMV
<0.139 mg/Kg - dry 0.139 0.7673-Nitroaniline 1 03/24/22 17:41 V16588JMV
<0.108 mg/Kg - dry 0.108 0.3834-Nitroaniline 1 03/24/22 17:41 V16588JMV
<0.134 mg/Kg - dry 0.134 0.383Nitrobenzene 1 03/24/22 17:41 V16588JMV
<0.103 mg/Kg - dry 0.103 0.7672-Nitrophenol 1 03/24/22 17:41 V16588JMV
<0.136 mg/Kg - dry 0.136 0.7674-Nitrophenol 1 03/24/22 17:41 V16588JMV
<0.305 mg/Kg - dry 0.305 0.767N-Nitrosodimethylamine 1 03/24/22 17:41 V16588JMV
<0.210 mg/Kg - dry 0.210 0.767N-Nitrosodiphenylamine 1 03/24/22 17:41 V16588JMV
<0.137 mg/Kg - dry 0.137 0.767
N-Nitroso-di-n-propylamine 1 03/24/22 17:41 V16588JMV
<0.403 mg/Kg - dry 0.403 1.16Pentachlorophenol 1 03/24/22 17:41 V16588JMV
<0.241 mg/Kg - dry 0.241 0.767Phenanthrene 1 03/24/22 17:41 V16588JMV
<0.130 mg/Kg - dry 0.130 0.767Phenol 1 03/24/22 17:41 V16588JMV
<0.155 mg/Kg - dry 0.155 0.767Pyrene 1 03/24/22 17:41 V16588JMV
<0.092 mg/Kg - dry 0.092 0.383Pyridine 1 03/24/22 17:41 V16588JMV
<0.124 mg/Kg - dry 0.124 0.7671,2,4-Trichlorobenzene 1 03/24/22 17:41 V16588JMV
<0.111 mg/Kg - dry 0.111 0.767
2,4,5-Trichlorophenol 1 03/24/22 17:41 V16588JMV
<0.112 mg/Kg - dry 0.112 0.7672,4,6-Trichlorophenol 1 03/24/22 17:41 V16588JMV
8270ESurrogate: Phenol-d5 73.9 Limits: 34-121%03/24/22 17:411 JMV
Surrogate: 2-Fluorobiphenyl 80.2 Limits: 44-115%03/24/22 17:411 JMV V16588
Surrogate: 2-Fluorophenol 77.8 Limits: 35-115%03/24/22 17:411 JMV V16588
Surrogate: Nitrobenzene-d5 76.0 Limits: 37-122%03/24/22 17:411 JMV V16588
Surrogate: 4-Terphenyl-d14 82.6 Limits: 54-127%03/24/22 17:411 JMV V16588
Surrogate: 2,4,6-Tribromophenol 81.1 Limits: 39-132%03/24/22 17:411 JMV V16588
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-3
96593 Matrix:
3/21/2022 11:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.9 %Moisture 1 03/24/22 10:33 SW-DRYWTSJL
1.88 mg/Kg - dry 0.180 0.601Arsenic 1 03/24/22 12:28 6010DEDV
102 mg/Kg - dry 0.033 0.601Barium 1 03/24/22 12:28 6010DEDV
0.0243 J mg/Kg - dry 0.0097 0.120Cadmium 1 03/24/22 12:28 6010DEDV
44.9 mg/Kg - dry 0.204 0.601Chromium 1 03/24/22 12:28 6010DEDV
14.0 mg/Kg - dry 0.095 0.361
Lead 1 03/24/22 12:28 6010DEDV
0.0548 mg/Kg - dry 0.0144 0.0361Mercury (Total)1 03/23/22 16:31 7471BEDV
<0.228 mg/Kg - dry 0.228 0.601Selenium 1 03/24/22 12:28 6010DEDV
<0.0348 mg/Kg - dry 0.0348 0.301Silver 1 03/24/22 12:28 6010DEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-3
96593 Matrix:
3/21/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
0.012 J mg/Kg - dry 0.002 0.024Acetone 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 03/25/22 16:37 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 03/25/22 16:37 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 03/25/22 16:37 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/25/22 16:37 V16630TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/25/22 16:37 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 03/25/22 16:37 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/25/22 16:37 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/25/22 16:37 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 03/25/22 16:37 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/25/22 16:37 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/25/22 16:37 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-3
96593 Matrix:
3/21/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 03/25/22 16:37 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 03/25/22 16:37 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/25/22 16:37 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/25/22 16:37 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/25/22 16:37 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/25/22 16:37 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 03/25/22 16:37 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 03/25/22 16:37 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/25/22 16:37 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 03/25/22 16:37 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/25/22 16:37 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 03/25/22 16:37 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 03/25/22 16:37 V16630TBL
<0.016 mg/Kg - dry 0.016 0.300Ethanol 1 03/25/22 16:37 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 03/25/22 16:37 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.060Ethyl Tertiary Butyl Ether (ETBE)1 03/25/22 16:37 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 03/25/22 16:37 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-3
96593 Matrix:
3/21/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 03/25/22 16:37 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0242-Hexanone 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/25/22 16:37 V16630TBL
0.001 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 03/25/22 16:37 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 03/25/22 16:37 V16630TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Propylbenzene 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/25/22 16:37 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/25/22 16:37 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.012
1,2,3-Trichlorobenzene 1 03/25/22 16:37 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/25/22 16:37 V16630TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 03/25/22 16:37 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 03/25/22 16:37 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-3
96593 Matrix:
3/21/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3,5-Trimethylbenzene 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 03/25/22 16:37 V16630TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/25/22 16:37 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 03/25/22 16:37 V16630
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%03/25/22 16:371 TBL V16630
Surrogate: Dibromofluoromethane 104 Limits: 84-123%03/25/22 16:371 TBL V16630
Surrogate: Toluene-d8 95.5 Limits: 76-129%03/25/22 16:371 TBL V16630
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.139 mg/Kg - dry 0.139 0.794Acenaphthene 1 03/24/22 18:03 V16588JMV
<0.126 mg/Kg - dry 0.126 0.794Acenaphthylene 1 03/24/22 18:03 V16588JMV
<0.182 mg/Kg - dry 0.182 0.794Aniline 1 03/24/22 18:03 V16588JMV
<0.172 mg/Kg - dry 0.172 0.794Anthracene 1 03/24/22 18:03 V16588JMV
<0.167 mg/Kg - dry 0.167 0.794
Benzo(a)anthracene 1 03/24/22 18:03 V16588JMV
<0.176 mg/Kg - dry 0.176 0.794Benzo(a)pyrene 1 03/24/22 18:03 V16588JMV
<0.175 mg/Kg - dry 0.175 0.794Benzo(b)fluoranthene 1 03/24/22 18:03 V16588JMV
<0.163 mg/Kg - dry 0.163 0.794Benzo(g,h,i)perylene 1 03/24/22 18:03 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-3
96593 Matrix:
3/21/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.164 mg/Kg - dry 0.164 0.794Benzo(k)fluoranthene 1 03/24/22 18:03 V16588JMV
<0.697 mg/Kg - dry 0.697 2.41Benzoic Acid 1 03/24/22 18:03 V16588JMV
<0.126 mg/Kg - dry 0.126 0.794Benzyl alcohol 1 03/24/22 18:03 V16588JMV
<0.141 mg/Kg - dry 0.141 0.794Bis(2-Chloroethoxy)methane 1 03/24/22 18:03 V16588JMV
<0.128 mg/Kg - dry 0.128 0.794Bis(2-Chloroethyl)ether 1 03/24/22 18:03 V16588JMV
<0.163 mg/Kg - dry 0.163 0.397Bis(2-Chloroisopropyl)ether 1 03/24/22 18:03 V16588JMV
<0.144 mg/Kg - dry 0.144 0.794Bis(2-ethylhexyl)phthalate 1 03/24/22 18:03 V16588JMV
<0.131 mg/Kg - dry 0.131 0.7944-Bromophenyl phenyl ether 1 03/24/22 18:03 V16588JMV
<0.135 mg/Kg - dry 0.135 0.397
Butyl benzyl phthalate 1 03/24/22 18:03 V16588JMV
<0.111 mg/Kg - dry 0.111 0.7944-Chloro-3-methylphenol 1 03/24/22 18:03 V16588JMV
<0.134 mg/Kg - dry 0.134 0.3974-Chloroaniline 1 03/24/22 18:03 V16588JMV
<0.139 mg/Kg - dry 0.139 0.7942-Chloronaphthalene 1 03/24/22 18:03 V16588JMV
<0.118 mg/Kg - dry 0.118 0.7942-Chlorophenol 1 03/24/22 18:03 V16588JMV
<0.151 mg/Kg - dry 0.151 1.204-Chlorophenyl phenyl ether 1 03/24/22 18:03 V16588JMV
<0.170 mg/Kg - dry 0.170 0.794Chrysene 1 03/24/22 18:03 V16588JMV
<0.276 mg/Kg - dry 0.276 0.794
Dibenz(a,h)anthracene 1 03/24/22 18:03 V16588JMV
<0.143 mg/Kg - dry 0.143 0.794Dibenzofuran 1 03/24/22 18:03 V16588JMV
<0.113 mg/Kg - dry 0.113 0.7941,2-Dichlorobenzene 1 03/24/22 18:03 V16588JMV
<0.117 mg/Kg - dry 0.117 0.7941,3-Dichlorobenzene 1 03/24/22 18:03 V16588JMV
<0.117 mg/Kg - dry 0.117 0.3971,4-Dichlorobenzene 1 03/24/22 18:03 V16588JMV
<0.176 mg/Kg - dry 0.176 0.7943,3'-Dichlorobenzidine 1 03/24/22 18:03 V16588JMV
<0.115 mg/Kg - dry 0.115 0.7942,4-Dichlorophenol 1 03/24/22 18:03 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-3
96593 Matrix:
3/21/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.216 mg/Kg - dry 0.216 0.794Diethyl phthalate 1 03/24/22 18:03 V16588JMV
<0.209 mg/Kg - dry 0.209 0.794Dimethyl phthalate 1 03/24/22 18:03 V16588JMV
<0.129 mg/Kg - dry 0.129 0.3972,4-Dimethylphenol 1 03/24/22 18:03 V16588JMV
<0.128 mg/Kg - dry 0.128 0.794Di-n-butyl phthalate 1 03/24/22 18:03 V16588JMV
<0.288 mg/Kg - dry 0.288 1.814,6-Dinitro-2-methylphenol 1 03/24/22 18:03 V16588JMV
<0.625 mg/Kg - dry 0.625 1.812,4-Dinitrophenol 1 03/24/22 18:03 V16588JMV
<0.116 mg/Kg - dry 0.116 0.7942,4-Dinitrotoluene 1 03/24/22 18:03 V16588JMV
<0.129 mg/Kg - dry 0.129 0.7942,6-Dinitrotoluene 1 03/24/22 18:03 V16588JMV
<0.172 mg/Kg - dry 0.172 0.397
Di-n-Octyl Phthalate 1 03/24/22 18:03 V16588JMV
<0.148 mg/Kg - dry 0.148 0.794Fluoranthene 1 03/24/22 18:03 V16588JMV
<0.154 mg/Kg - dry 0.154 0.794Fluorene 1 03/24/22 18:03 V16588JMV
<0.127 mg/Kg - dry 0.127 0.794Hexachlorobenzene 1 03/24/22 18:03 V16588JMV
<0.117 mg/Kg - dry 0.117 0.794Hexachlorobutadiene 1 03/24/22 18:03 V16588JMV
<0.188 mg/Kg - dry 0.188 0.794Hexachlorocyclopentadiene 1 03/24/22 18:03 V16588JMV
<0.095 mg/Kg - dry 0.095 0.794Hexachloroethane 1 03/24/22 18:03 V16588JMV
<0.215 mg/Kg - dry 0.215 0.794
Indeno(1,2,3-cd)pyrene 1 03/24/22 18:03 V16588JMV
<0.229 mg/Kg - dry 0.229 0.794Isophorone 1 03/24/22 18:03 V16588JMV
<0.127 mg/Kg - dry 0.127 0.7941-Methylnaphthalene 1 03/24/22 18:03 V16588JMV
<0.120 mg/Kg - dry 0.120 0.7942-Methylnaphthalene 1 03/24/22 18:03 V16588JMV
<0.116 mg/Kg - dry 0.116 0.7942-Methylphenol 1 03/24/22 18:03 V16588JMV
<0.102 mg/Kg - dry 0.102 0.7943&4 Methylphenol 1 03/24/22 18:03 V16588JMV
<0.173 mg/Kg - dry 0.173 0.794Naphthalene 1 03/24/22 18:03 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-3
96593 Matrix:
3/21/2022 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.116 mg/Kg - dry 0.116 0.7942-Nitroaniline 1 03/24/22 18:03 V16588JMV
<0.144 mg/Kg - dry 0.144 0.7943-Nitroaniline 1 03/24/22 18:03 V16588JMV
<0.112 mg/Kg - dry 0.112 0.3974-Nitroaniline 1 03/24/22 18:03 V16588JMV
<0.139 mg/Kg - dry 0.139 0.397Nitrobenzene 1 03/24/22 18:03 V16588JMV
<0.106 mg/Kg - dry 0.106 0.7942-Nitrophenol 1 03/24/22 18:03 V16588JMV
<0.140 mg/Kg - dry 0.140 0.7944-Nitrophenol 1 03/24/22 18:03 V16588JMV
<0.316 mg/Kg - dry 0.316 0.794N-Nitrosodimethylamine 1 03/24/22 18:03 V16588JMV
<0.217 mg/Kg - dry 0.217 0.794N-Nitrosodiphenylamine 1 03/24/22 18:03 V16588JMV
<0.141 mg/Kg - dry 0.141 0.794
N-Nitroso-di-n-propylamine 1 03/24/22 18:03 V16588JMV
<0.417 mg/Kg - dry 0.417 1.20Pentachlorophenol 1 03/24/22 18:03 V16588JMV
<0.250 mg/Kg - dry 0.250 0.794Phenanthrene 1 03/24/22 18:03 V16588JMV
<0.134 mg/Kg - dry 0.134 0.794Phenol 1 03/24/22 18:03 V16588JMV
<0.161 mg/Kg - dry 0.161 0.794Pyrene 1 03/24/22 18:03 V16588JMV
<0.095 mg/Kg - dry 0.095 0.397Pyridine 1 03/24/22 18:03 V16588JMV
<0.128 mg/Kg - dry 0.128 0.7941,2,4-Trichlorobenzene 1 03/24/22 18:03 V16588JMV
<0.115 mg/Kg - dry 0.115 0.794
2,4,5-Trichlorophenol 1 03/24/22 18:03 V16588JMV
<0.116 mg/Kg - dry 0.116 0.7942,4,6-Trichlorophenol 1 03/24/22 18:03 V16588JMV
8270ESurrogate: Phenol-d5 78.7 Limits: 34-121%03/24/22 18:031 JMV
Surrogate: 2-Fluorobiphenyl 84.4 Limits: 44-115%03/24/22 18:031 JMV V16588
Surrogate: 2-Fluorophenol 80.8 Limits: 35-115%03/24/22 18:031 JMV V16588
Surrogate: Nitrobenzene-d5 76.6 Limits: 37-122%03/24/22 18:031 JMV V16588
Surrogate: 4-Terphenyl-d14 89.8 Limits: 54-127%03/24/22 18:031 JMV V16588
Surrogate: 2,4,6-Tribromophenol 87.7 Limits: 39-132%03/24/22 18:031 JMV V16588
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-4
96594 Matrix:
3/21/2022 15:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
8.45 %Moisture 1 03/24/22 10:33 SW-DRYWTSJL
1.99 mg/Kg - dry 0.163 0.546Arsenic 1 03/24/22 12:08 6010DEDV
109 mg/Kg - dry 0.030 0.546Barium 1 03/24/22 12:08 6010DEDV
0.256 mg/Kg - dry 0.0088 0.109Cadmium 1 03/24/22 12:08 6010DEDV
40.6 mg/Kg - dry 0.185 0.546Chromium 1 03/24/22 12:08 6010DEDV
59.1 mg/Kg - dry 0.086 0.327
Lead 1 03/24/22 12:08 6010DEDV
0.0530 mg/Kg - dry 0.0131 0.0328Mercury (Total)1 03/23/22 16:52 7471BEDV
<0.207 mg/Kg - dry 0.207 0.546Selenium 1 03/24/22 12:08 6010DEDV
<0.0316 mg/Kg - dry 0.0316 0.273Silver 1 03/24/22 12:08 6010DEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-4
96594 Matrix:
3/21/2022 15:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
0.012 J mg/Kg - dry 0.002 0.021Acetone 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 03/25/22 17:05 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 03/25/22 17:05 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 03/25/22 17:05 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.010
Bromomethane 1 03/25/22 17:05 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 03/25/22 17:05 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 03/25/22 17:05 V16630TBL
0.0009 J mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 03/25/22 17:05 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 03/25/22 17:05 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.005
Chlorodibromomethane 1 03/25/22 17:05 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 03/25/22 17:05 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 03/25/22 17:05 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 03/25/22 17:05 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 03/25/22 17:05 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-4
96594 Matrix:
3/21/2022 15:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 03/25/22 17:05 V16630TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 03/25/22 17:05 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 03/25/22 17:05 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 03/25/22 17:05 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 03/25/22 17:05 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 03/25/22 17:05 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 03/25/22 17:05 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 03/25/22 17:05 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloropropene 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 03/25/22 17:05 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 03/25/22 17:05 V16630TBL
0.032 J mg/Kg - dry 0.015 0.273Ethanol 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 03/25/22 17:05 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.054Ethyl Tertiary Butyl Ether (ETBE)1 03/25/22 17:05 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.010Hexachlorobutadiene 1 03/25/22 17:05 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-4
96594 Matrix:
3/21/2022 15:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 03/25/22 17:05 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 03/25/22 17:05 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 03/25/22 17:05 V16630TBL
0.002 J mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 03/25/22 17:05 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 03/25/22 17:05 V16630TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.010
Naphthalene 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 03/25/22 17:05 V16630TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 03/25/22 17:05 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 03/25/22 17:05 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.010
1,2,3-Trichlorobenzene 1 03/25/22 17:05 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 03/25/22 17:05 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 03/25/22 17:05 V16630TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 03/25/22 17:05 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 03/25/22 17:05 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-4
96594 Matrix:
3/21/2022 15:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 03/25/22 17:05 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 03/25/22 17:05 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 03/25/22 17:05 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 03/25/22 17:05 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 03/25/22 17:05 V16630TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 03/25/22 17:05 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 03/25/22 17:05 V16630
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%03/25/22 17:051 TBL V16630
Surrogate: Dibromofluoromethane 103 Limits: 84-123%03/25/22 17:051 TBL V16630
Surrogate: Toluene-d8 95.6 Limits: 76-129%03/25/22 17:051 TBL V16630
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.126 mg/Kg - dry 0.126 0.720Acenaphthene 1 03/24/22 18:25 V16588JMV
<0.114 mg/Kg - dry 0.114 0.720Acenaphthylene 1 03/24/22 18:25 V16588JMV
<0.166 mg/Kg - dry 0.166 0.720Aniline 1 03/24/22 18:25 V16588JMV
<0.156 mg/Kg - dry 0.156 0.720Anthracene 1 03/24/22 18:25 V16588JMV
0.315 J
mg/Kg - dry 0.151 0.720
Benzo(a)anthracene 1 03/24/22 18:25 V16588JMV
0.290 J mg/Kg - dry 0.160 0.720Benzo(a)pyrene 1 03/24/22 18:25 V16588JMV
0.535 J mg/Kg - dry 0.159 0.720Benzo(b)fluoranthene 1 03/24/22 18:25 V16588JMV
<0.148 mg/Kg - dry 0.148 0.720Benzo(g,h,i)perylene 1 03/24/22 18:25 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-4
96594 Matrix:
3/21/2022 15:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.149 mg/Kg - dry 0.149 0.720Benzo(k)fluoranthene 1 03/24/22 18:25 V16588JMV
<0.633 mg/Kg - dry 0.633 2.18Benzoic Acid 1 03/24/22 18:25 V16588JMV
<0.114 mg/Kg - dry 0.114 0.720Benzyl alcohol 1 03/24/22 18:25 V16588JMV
<0.128 mg/Kg - dry 0.128 0.720Bis(2-Chloroethoxy)methane 1 03/24/22 18:25 V16588JMV
<0.116 mg/Kg - dry 0.116 0.720Bis(2-Chloroethyl)ether 1 03/24/22 18:25 V16588JMV
<0.148 mg/Kg - dry 0.148 0.360Bis(2-Chloroisopropyl)ether 1 03/24/22 18:25 V16588JMV
<0.131 mg/Kg - dry 0.131 0.720Bis(2-ethylhexyl)phthalate 1 03/24/22 18:25 V16588JMV
<0.119 mg/Kg - dry 0.119 0.7204-Bromophenyl phenyl ether 1 03/24/22 18:25 V16588JMV
<0.123 mg/Kg - dry 0.123 0.360
Butyl benzyl phthalate 1 03/24/22 18:25 V16588JMV
<0.100 mg/Kg - dry 0.100 0.7204-Chloro-3-methylphenol 1 03/24/22 18:25 V16588JMV
<0.122 mg/Kg - dry 0.122 0.3604-Chloroaniline 1 03/24/22 18:25 V16588JMV
<0.126 mg/Kg - dry 0.126 0.7202-Chloronaphthalene 1 03/24/22 18:25 V16588JMV
<0.107 mg/Kg - dry 0.107 0.7202-Chlorophenol 1 03/24/22 18:25 V16588JMV
<0.137 mg/Kg - dry 0.137 1.094-Chlorophenyl phenyl ether 1 03/24/22 18:25 V16588JMV
0.411 J mg/Kg - dry 0.155 0.720Chrysene 1 03/24/22 18:25 V16588JMV
<0.251 mg/Kg - dry 0.251 0.720
Dibenz(a,h)anthracene 1 03/24/22 18:25 V16588JMV
<0.129 mg/Kg - dry 0.129 0.720Dibenzofuran 1 03/24/22 18:25 V16588JMV
<0.103 mg/Kg - dry 0.103 0.7201,2-Dichlorobenzene 1 03/24/22 18:25 V16588JMV
<0.106 mg/Kg - dry 0.106 0.7201,3-Dichlorobenzene 1 03/24/22 18:25 V16588JMV
<0.106 mg/Kg - dry 0.106 0.3601,4-Dichlorobenzene 1 03/24/22 18:25 V16588JMV
<0.160 mg/Kg - dry 0.160 0.7203,3'-Dichlorobenzidine 1 03/24/22 18:25 V16588JMV
<0.104 mg/Kg - dry 0.104 0.7202,4-Dichlorophenol 1 03/24/22 18:25 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-4
96594 Matrix:
3/21/2022 15:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.196 mg/Kg - dry 0.196 0.720Diethyl phthalate 1 03/24/22 18:25 V16588JMV
<0.190 mg/Kg - dry 0.190 0.720Dimethyl phthalate 1 03/24/22 18:25 V16588JMV
<0.117 mg/Kg - dry 0.117 0.3602,4-Dimethylphenol 1 03/24/22 18:25 V16588JMV
<0.116 mg/Kg - dry 0.116 0.720Di-n-butyl phthalate 1 03/24/22 18:25 V16588JMV
<0.262 mg/Kg - dry 0.262 1.644,6-Dinitro-2-methylphenol 1 03/24/22 18:25 V16588JMV
<0.567 mg/Kg - dry 0.567 1.642,4-Dinitrophenol 1 03/24/22 18:25 V16588JMV
<0.105 mg/Kg - dry 0.105 0.7202,4-Dinitrotoluene 1 03/24/22 18:25 V16588JMV
<0.117 mg/Kg - dry 0.117 0.7202,6-Dinitrotoluene 1 03/24/22 18:25 V16588JMV
<0.156 mg/Kg - dry 0.156 0.360
Di-n-Octyl Phthalate 1 03/24/22 18:25 V16588JMV
0.718 J mg/Kg - dry 0.134 0.720Fluoranthene 1 03/24/22 18:25 V16588JMV
<0.139 mg/Kg - dry 0.139 0.720Fluorene 1 03/24/22 18:25 V16588JMV
<0.115 mg/Kg - dry 0.115 0.720Hexachlorobenzene 1 03/24/22 18:25 V16588JMV
<0.106 mg/Kg - dry 0.106 0.720Hexachlorobutadiene 1 03/24/22 18:25 V16588JMV
<0.171 mg/Kg - dry 0.171 0.720Hexachlorocyclopentadiene 1 03/24/22 18:25 V16588JMV
<0.086 mg/Kg - dry 0.086 0.720Hexachloroethane 1 03/24/22 18:25 V16588JMV
<0.195 mg/Kg - dry 0.195 0.720
Indeno(1,2,3-cd)pyrene 1 03/24/22 18:25 V16588JMV
<0.208 mg/Kg - dry 0.208 0.720Isophorone 1 03/24/22 18:25 V16588JMV
<0.115 mg/Kg - dry 0.115 0.7201-Methylnaphthalene 1 03/24/22 18:25 V16588JMV
<0.109 mg/Kg - dry 0.109 0.7202-Methylnaphthalene 1 03/24/22 18:25 V16588JMV
<0.105 mg/Kg - dry 0.105 0.7202-Methylphenol 1 03/24/22 18:25 V16588JMV
<0.092 mg/Kg - dry 0.092 0.7203&4 Methylphenol 1 03/24/22 18:25 V16588JMV
<0.157 mg/Kg - dry 0.157 0.720Naphthalene 1 03/24/22 18:25 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-4
96594 Matrix:
3/21/2022 15:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.105 mg/Kg - dry 0.105 0.7202-Nitroaniline 1 03/24/22 18:25 V16588JMV
<0.131 mg/Kg - dry 0.131 0.7203-Nitroaniline 1 03/24/22 18:25 V16588JMV
<0.101 mg/Kg - dry 0.101 0.3604-Nitroaniline 1 03/24/22 18:25 V16588JMV
<0.126 mg/Kg - dry 0.126 0.360Nitrobenzene 1 03/24/22 18:25 V16588JMV
<0.096 mg/Kg - dry 0.096 0.7202-Nitrophenol 1 03/24/22 18:25 V16588JMV
<0.127 mg/Kg - dry 0.127 0.7204-Nitrophenol 1 03/24/22 18:25 V16588JMV
<0.287 mg/Kg - dry 0.287 0.720N-Nitrosodimethylamine 1 03/24/22 18:25 V16588JMV
<0.197 mg/Kg - dry 0.197 0.720N-Nitrosodiphenylamine 1 03/24/22 18:25 V16588JMV
<0.128 mg/Kg - dry 0.128 0.720
N-Nitroso-di-n-propylamine 1 03/24/22 18:25 V16588JMV
<0.379 mg/Kg - dry 0.379 1.09Pentachlorophenol 1 03/24/22 18:25 V16588JMV
<0.227 mg/Kg - dry 0.227 0.720Phenanthrene 1 03/24/22 18:25 V16588JMV
<0.122 mg/Kg - dry 0.122 0.720Phenol 1 03/24/22 18:25 V16588JMV
0.654 J mg/Kg - dry 0.146 0.720Pyrene 1 03/24/22 18:25 V16588JMV
<0.086 mg/Kg - dry 0.086 0.360Pyridine 1 03/24/22 18:25 V16588JMV
<0.116 mg/Kg - dry 0.116 0.7201,2,4-Trichlorobenzene 1 03/24/22 18:25 V16588JMV
<0.105 mg/Kg - dry 0.105 0.720
2,4,5-Trichlorophenol 1 03/24/22 18:25 V16588JMV
<0.105 mg/Kg - dry 0.105 0.7202,4,6-Trichlorophenol 1 03/24/22 18:25 V16588JMV
8270ESurrogate: Phenol-d5 75.7 Limits: 34-121%03/24/22 18:251 JMV
Surrogate: 2-Fluorobiphenyl 82.0 Limits: 44-115%03/24/22 18:251 JMV V16588
Surrogate: 2-Fluorophenol 77.8 Limits: 35-115%03/24/22 18:251 JMV V16588
Surrogate: Nitrobenzene-d5 74.3 Limits: 37-122%03/24/22 18:251 JMV V16588
Surrogate: 4-Terphenyl-d14 86.8 Limits: 54-127%03/24/22 18:251 JMV V16588
Surrogate: 2,4,6-Tribromophenol 86.2 Limits: 39-132%03/24/22 18:251 JMV V16588
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-5
96595 Matrix:
3/21/2022 15:15
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.0 %Moisture 1 03/24/22 10:33 SW-DRYWTSJL
2.35 mg/Kg - dry 0.182 0.609Arsenic 1 03/24/22 12:12 6010DEDV
107 mg/Kg - dry 0.034 0.609Barium 1 03/24/22 12:12 6010DEDV
<0.0098 mg/Kg - dry 0.0098 0.122Cadmium 1 03/24/22 12:12 6010DEDV
54.8 mg/Kg - dry 0.207 0.609Chromium 1 03/24/22 12:12 6010DEDV
11.1 mg/Kg - dry 0.096 0.365
Lead 1 03/24/22 12:12 6010DEDV
0.0445 mg/Kg - dry 0.0146 0.0366Mercury (Total)1 03/23/22 17:02 7471BEDV
<0.231 mg/Kg - dry 0.231 0.609Selenium 1 03/24/22 12:12 6010DEDV
<0.0353 mg/Kg - dry 0.0353 0.305Silver 1 03/24/22 12:12 6010DEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-5
96595 Matrix:
3/21/2022 15:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
0.018 J mg/Kg - dry 0.002 0.024Acetone 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 03/25/22 17:33 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 03/25/22 17:33 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 03/25/22 17:33 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/25/22 17:33 V16630TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 03/25/22 17:33 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/25/22 17:33 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 03/25/22 17:33 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/25/22 17:33 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/25/22 17:33 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 03/25/22 17:33 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 03/25/22 17:33 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/25/22 17:33 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/25/22 17:33 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-5
96595 Matrix:
3/21/2022 15:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/25/22 17:33 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/25/22 17:33 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 03/25/22 17:33 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 03/25/22 17:33 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/25/22 17:33 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/25/22 17:33 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 03/25/22 17:33 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 03/25/22 17:33 V16630TBL
<0.017 mg/Kg - dry 0.017 0.304Ethanol 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 03/25/22 17:33 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 03/25/22 17:33 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-5
96595 Matrix:
3/21/2022 15:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 03/25/22 17:33 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 03/25/22 17:33 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/25/22 17:33 V16630TBL
0.002 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 03/25/22 17:33 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 03/25/22 17:33 V16630TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/25/22 17:33 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/25/22 17:33 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 03/25/22 17:33 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/25/22 17:33 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/25/22 17:33 V16630TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 03/25/22 17:33 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 03/25/22 17:33 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-5
96595 Matrix:
3/21/2022 15:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 03/25/22 17:33 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 03/25/22 17:33 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 03/25/22 17:33 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 03/25/22 17:33 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 03/25/22 17:33 V16630TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/25/22 17:33 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 03/25/22 17:33 V16630
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%03/25/22 17:331 TBL V16630
Surrogate: Dibromofluoromethane 102 Limits: 84-123%03/25/22 17:331 TBL V16630
Surrogate: Toluene-d8 95.3 Limits: 76-129%03/25/22 17:331 TBL V16630
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.141 mg/Kg - dry 0.141 0.804Acenaphthene 1 03/24/22 18:48 V16588JMV
<0.128 mg/Kg - dry 0.128 0.804Acenaphthylene 1 03/24/22 18:48 V16588JMV
<0.185 mg/Kg - dry 0.185 0.804Aniline 1 03/24/22 18:48 V16588JMV
<0.174 mg/Kg - dry 0.174 0.804Anthracene 1 03/24/22 18:48 V16588JMV
<0.169 mg/Kg - dry 0.169 0.804
Benzo(a)anthracene 1 03/24/22 18:48 V16588JMV
<0.179 mg/Kg - dry 0.179 0.804Benzo(a)pyrene 1 03/24/22 18:48 V16588JMV
<0.178 mg/Kg - dry 0.178 0.804Benzo(b)fluoranthene 1 03/24/22 18:48 V16588JMV
<0.165 mg/Kg - dry 0.165 0.804Benzo(g,h,i)perylene 1 03/24/22 18:48 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-5
96595 Matrix:
3/21/2022 15:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.167 mg/Kg - dry 0.167 0.804Benzo(k)fluoranthene 1 03/24/22 18:48 V16588JMV
<0.707 mg/Kg - dry 0.707 2.44Benzoic Acid 1 03/24/22 18:48 V16588JMV
<0.128 mg/Kg - dry 0.128 0.804Benzyl alcohol 1 03/24/22 18:48 V16588JMV
<0.143 mg/Kg - dry 0.143 0.804Bis(2-Chloroethoxy)methane 1 03/24/22 18:48 V16588JMV
<0.130 mg/Kg - dry 0.130 0.804Bis(2-Chloroethyl)ether 1 03/24/22 18:48 V16588JMV
<0.165 mg/Kg - dry 0.165 0.402Bis(2-Chloroisopropyl)ether 1 03/24/22 18:48 V16588JMV
<0.146 mg/Kg - dry 0.146 0.804Bis(2-ethylhexyl)phthalate 1 03/24/22 18:48 V16588JMV
<0.132 mg/Kg - dry 0.132 0.8044-Bromophenyl phenyl ether 1 03/24/22 18:48 V16588JMV
<0.137 mg/Kg - dry 0.137 0.402
Butyl benzyl phthalate 1 03/24/22 18:48 V16588JMV
<0.112 mg/Kg - dry 0.112 0.8044-Chloro-3-methylphenol 1 03/24/22 18:48 V16588JMV
<0.136 mg/Kg - dry 0.136 0.4024-Chloroaniline 1 03/24/22 18:48 V16588JMV
<0.141 mg/Kg - dry 0.141 0.8042-Chloronaphthalene 1 03/24/22 18:48 V16588JMV
<0.119 mg/Kg - dry 0.119 0.8042-Chlorophenol 1 03/24/22 18:48 V16588JMV
<0.153 mg/Kg - dry 0.153 1.224-Chlorophenyl phenyl ether 1 03/24/22 18:48 V16588JMV
<0.173 mg/Kg - dry 0.173 0.804Chrysene 1 03/24/22 18:48 V16588JMV
<0.280 mg/Kg - dry 0.280 0.804
Dibenz(a,h)anthracene 1 03/24/22 18:48 V16588JMV
<0.145 mg/Kg - dry 0.145 0.804Dibenzofuran 1 03/24/22 18:48 V16588JMV
<0.115 mg/Kg - dry 0.115 0.8041,2-Dichlorobenzene 1 03/24/22 18:48 V16588JMV
<0.118 mg/Kg - dry 0.118 0.8041,3-Dichlorobenzene 1 03/24/22 18:48 V16588JMV
<0.118 mg/Kg - dry 0.118 0.4021,4-Dichlorobenzene 1 03/24/22 18:48 V16588JMV
<0.179 mg/Kg - dry 0.179 0.8043,3'-Dichlorobenzidine 1 03/24/22 18:48 V16588JMV
<0.116 mg/Kg - dry 0.116 0.8042,4-Dichlorophenol 1 03/24/22 18:48 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-5
96595 Matrix:
3/21/2022 15:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.219 mg/Kg - dry 0.219 0.804Diethyl phthalate 1 03/24/22 18:48 V16588JMV
<0.212 mg/Kg - dry 0.212 0.804Dimethyl phthalate 1 03/24/22 18:48 V16588JMV
<0.131 mg/Kg - dry 0.131 0.4022,4-Dimethylphenol 1 03/24/22 18:48 V16588JMV
<0.130 mg/Kg - dry 0.130 0.804Di-n-butyl phthalate 1 03/24/22 18:48 V16588JMV
<0.292 mg/Kg - dry 0.292 1.834,6-Dinitro-2-methylphenol 1 03/24/22 18:48 V16588JMV
<0.634 mg/Kg - dry 0.634 1.832,4-Dinitrophenol 1 03/24/22 18:48 V16588JMV
<0.117 mg/Kg - dry 0.117 0.8042,4-Dinitrotoluene 1 03/24/22 18:48 V16588JMV
<0.131 mg/Kg - dry 0.131 0.8042,6-Dinitrotoluene 1 03/24/22 18:48 V16588JMV
<0.174 mg/Kg - dry 0.174 0.402
Di-n-Octyl Phthalate 1 03/24/22 18:48 V16588JMV
<0.150 mg/Kg - dry 0.150 0.804Fluoranthene 1 03/24/22 18:48 V16588JMV
<0.156 mg/Kg - dry 0.156 0.804Fluorene 1 03/24/22 18:48 V16588JMV
<0.129 mg/Kg - dry 0.129 0.804Hexachlorobenzene 1 03/24/22 18:48 V16588JMV
<0.119 mg/Kg - dry 0.119 0.804Hexachlorobutadiene 1 03/24/22 18:48 V16588JMV
<0.191 mg/Kg - dry 0.191 0.804Hexachlorocyclopentadiene 1 03/24/22 18:48 V16588JMV
<0.096 mg/Kg - dry 0.096 0.804Hexachloroethane 1 03/24/22 18:48 V16588JMV
<0.218 mg/Kg - dry 0.218 0.804
Indeno(1,2,3-cd)pyrene 1 03/24/22 18:48 V16588JMV
<0.232 mg/Kg - dry 0.232 0.804Isophorone 1 03/24/22 18:48 V16588JMV
<0.129 mg/Kg - dry 0.129 0.8041-Methylnaphthalene 1 03/24/22 18:48 V16588JMV
<0.121 mg/Kg - dry 0.121 0.8042-Methylnaphthalene 1 03/24/22 18:48 V16588JMV
<0.118 mg/Kg - dry 0.118 0.8042-Methylphenol 1 03/24/22 18:48 V16588JMV
<0.103 mg/Kg - dry 0.103 0.8043&4 Methylphenol 1 03/24/22 18:48 V16588JMV
<0.175 mg/Kg - dry 0.175 0.804Naphthalene 1 03/24/22 18:48 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-5
96595 Matrix:
3/21/2022 15:15
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.117 mg/Kg - dry 0.117 0.8042-Nitroaniline 1 03/24/22 18:48 V16588JMV
<0.146 mg/Kg - dry 0.146 0.8043-Nitroaniline 1 03/24/22 18:48 V16588JMV
<0.113 mg/Kg - dry 0.113 0.4024-Nitroaniline 1 03/24/22 18:48 V16588JMV
<0.141 mg/Kg - dry 0.141 0.402Nitrobenzene 1 03/24/22 18:48 V16588JMV
<0.108 mg/Kg - dry 0.108 0.8042-Nitrophenol 1 03/24/22 18:48 V16588JMV
<0.142 mg/Kg - dry 0.142 0.8044-Nitrophenol 1 03/24/22 18:48 V16588JMV
<0.320 mg/Kg - dry 0.320 0.804N-Nitrosodimethylamine 1 03/24/22 18:48 V16588JMV
<0.220 mg/Kg - dry 0.220 0.804N-Nitrosodiphenylamine 1 03/24/22 18:48 V16588JMV
<0.143 mg/Kg - dry 0.143 0.804
N-Nitroso-di-n-propylamine 1 03/24/22 18:48 V16588JMV
<0.423 mg/Kg - dry 0.423 1.22Pentachlorophenol 1 03/24/22 18:48 V16588JMV
<0.253 mg/Kg - dry 0.253 0.804Phenanthrene 1 03/24/22 18:48 V16588JMV
<0.136 mg/Kg - dry 0.136 0.804Phenol 1 03/24/22 18:48 V16588JMV
<0.163 mg/Kg - dry 0.163 0.804Pyrene 1 03/24/22 18:48 V16588JMV
<0.096 mg/Kg - dry 0.096 0.402Pyridine 1 03/24/22 18:48 V16588JMV
<0.130 mg/Kg - dry 0.130 0.8041,2,4-Trichlorobenzene 1 03/24/22 18:48 V16588JMV
<0.117 mg/Kg - dry 0.117 0.804
2,4,5-Trichlorophenol 1 03/24/22 18:48 V16588JMV
<0.117 mg/Kg - dry 0.117 0.8042,4,6-Trichlorophenol 1 03/24/22 18:48 V16588JMV
8270ESurrogate: Phenol-d5 74.2 Limits: 34-121%03/24/22 18:481 JMV
Surrogate: 2-Fluorobiphenyl 80.2 Limits: 44-115%03/24/22 18:481 JMV V16588
Surrogate: 2-Fluorophenol 77.2 Limits: 35-115%03/24/22 18:481 JMV V16588
Surrogate: Nitrobenzene-d5 73.7 Limits: 37-122%03/24/22 18:481 JMV V16588
Surrogate: 4-Terphenyl-d14 88.6 Limits: 54-127%03/24/22 18:481 JMV V16588
Surrogate: 2,4,6-Tribromophenol 88.6 Limits: 39-132%03/24/22 18:481 JMV V16588
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-DUP
96596 Matrix:
3/21/2022 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
5.68 %Moisture 1 03/24/22 10:33 SW-DRYWTSJL
3.02 mg/Kg - dry 0.159 0.530Arsenic 1 03/24/22 12:24 6010DEDV
86.2 mg/Kg - dry 0.029 0.530Barium 1 03/24/22 12:24 6010DEDV
0.126 mg/Kg - dry 0.0085 0.106Cadmium 1 03/24/22 12:24 6010DEDV
54.7 mg/Kg - dry 0.180 0.530Chromium 1 03/24/22 12:24 6010DEDV
23.1 mg/Kg - dry 0.083 0.318
Lead 1 03/24/22 12:24 6010DEDV
0.0404 mg/Kg - dry 0.0127 0.0318Mercury (Total)1 03/23/22 17:04 7471BEDV
<0.201 mg/Kg - dry 0.201 0.530Selenium 1 03/24/22 12:24 6010DEDV
<0.0307 mg/Kg - dry 0.0307 0.265Silver 1 03/24/22 12:24 6010DEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-DUP
96596 Matrix:
3/21/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
0.017 J mg/Kg - dry 0.002 0.021Acetone 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 03/25/22 18:00 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 03/25/22 18:00 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005Bromochloromethane 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.010
Bromomethane 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 03/25/22 18:00 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 03/25/22 18:00 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 03/25/22 18:00 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.005
Chlorodibromomethane 1 03/25/22 18:00 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.010Chloroethane 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 03/25/22 18:00 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0052-Chlorotoluene 1 03/25/22 18:00 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 03/25/22 18:00 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 03/25/22 18:00 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-DUP
96596 Matrix:
3/21/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 03/25/22 18:00 V16630TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 03/25/22 18:00 V16630TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,4-Dichlorobenzene 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 03/25/22 18:00 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 03/25/22 18:00 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 03/25/22 18:00 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005cis-1,2-Dichloroethene 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 03/25/22 18:00 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloropropene 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 03/25/22 18:00 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.005trans-1,3-Dichloropropene 1 03/25/22 18:00 V16630TBL
<0.014 mg/Kg - dry 0.014 0.265Ethanol 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 03/25/22 18:00 V16630TBL
<0.0009 mg/Kg - dry 0.0009 0.053Ethyl Tertiary Butyl Ether (ETBE)1 03/25/22 18:00 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.010Hexachlorobutadiene 1 03/25/22 18:00 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-DUP
96596 Matrix:
3/21/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 03/25/22 18:00 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 03/25/22 18:00 V16630TBL
0.001 J mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 03/25/22 18:00 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 03/25/22 18:00 V16630TBL
<0.015 mg/Kg - dry 0.015 0.0214-Methyl-2-Pentanone 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.010
Naphthalene 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 03/25/22 18:00 V16630TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 03/25/22 18:00 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 03/25/22 18:00 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.010
1,2,3-Trichlorobenzene 1 03/25/22 18:00 V16630TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 03/25/22 18:00 V16630TBL
<0.0010 mg/Kg - dry 0.0010 0.005Trichloroethene 1 03/25/22 18:00 V16630TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 03/25/22 18:00 V16630TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 03/25/22 18:00 V16630TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-DUP
96596 Matrix:
3/21/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V16629 03/25/22 08:00
<0.0005 mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 03/25/22 18:00 V16630TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 03/25/22 18:00 V16630TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 03/25/22 18:00 V16630TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 03/25/22 18:00 V16630
Surrogate: 4-Bromofluorobenzene 99.5 Limits: 70-130%03/25/22 18:001 TBL V16630
Surrogate: Dibromofluoromethane 102 Limits: 84-123%03/25/22 18:001 TBL V16630
Surrogate: Toluene-d8 95.7 Limits: 76-129%03/25/22 18:001 TBL V16630
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.122 mg/Kg - dry 0.122 0.700Acenaphthene 1 03/24/22 19:10 V16588JMV
<0.111 mg/Kg - dry 0.111 0.700Acenaphthylene 1 03/24/22 19:10 V16588JMV
<0.161 mg/Kg - dry 0.161 0.700Aniline 1 03/24/22 19:10 V16588JMV
<0.151 mg/Kg - dry 0.151 0.700Anthracene 1 03/24/22 19:10 V16588JMV
<0.147 mg/Kg - dry 0.147 0.700
Benzo(a)anthracene 1 03/24/22 19:10 V16588JMV
<0.155 mg/Kg - dry 0.155 0.700Benzo(a)pyrene 1 03/24/22 19:10 V16588JMV
<0.154 mg/Kg - dry 0.154 0.700Benzo(b)fluoranthene 1 03/24/22 19:10 V16588JMV
<0.144 mg/Kg - dry 0.144 0.700Benzo(g,h,i)perylene 1 03/24/22 19:10 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-DUP
96596 Matrix:
3/21/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.145 mg/Kg - dry 0.145 0.700Benzo(k)fluoranthene 1 03/24/22 19:10 V16588JMV
<0.614 mg/Kg - dry 0.614 2.12Benzoic Acid 1 03/24/22 19:10 V16588JMV
<0.111 mg/Kg - dry 0.111 0.700Benzyl alcohol 1 03/24/22 19:10 V16588JMV
<0.125 mg/Kg - dry 0.125 0.700Bis(2-Chloroethoxy)methane 1 03/24/22 19:10 V16588JMV
<0.113 mg/Kg - dry 0.113 0.700Bis(2-Chloroethyl)ether 1 03/24/22 19:10 V16588JMV
<0.144 mg/Kg - dry 0.144 0.349Bis(2-Chloroisopropyl)ether 1 03/24/22 19:10 V16588JMV
<0.127 mg/Kg - dry 0.127 0.700Bis(2-ethylhexyl)phthalate 1 03/24/22 19:10 V16588JMV
<0.115 mg/Kg - dry 0.115 0.7004-Bromophenyl phenyl ether 1 03/24/22 19:10 V16588JMV
<0.119 mg/Kg - dry 0.119 0.349
Butyl benzyl phthalate 1 03/24/22 19:10 V16588JMV
<0.098 mg/Kg - dry 0.098 0.7004-Chloro-3-methylphenol 1 03/24/22 19:10 V16588JMV
<0.118 mg/Kg - dry 0.118 0.3494-Chloroaniline 1 03/24/22 19:10 V16588JMV
<0.122 mg/Kg - dry 0.122 0.7002-Chloronaphthalene 1 03/24/22 19:10 V16588JMV
<0.104 mg/Kg - dry 0.104 0.7002-Chlorophenol 1 03/24/22 19:10 V16588JMV
<0.133 mg/Kg - dry 0.133 1.064-Chlorophenyl phenyl ether 1 03/24/22 19:10 V16588JMV
<0.150 mg/Kg - dry 0.150 0.700Chrysene 1 03/24/22 19:10 V16588JMV
<0.243 mg/Kg - dry 0.243 0.700
Dibenz(a,h)anthracene 1 03/24/22 19:10 V16588JMV
<0.126 mg/Kg - dry 0.126 0.700Dibenzofuran 1 03/24/22 19:10 V16588JMV
<0.100 mg/Kg - dry 0.100 0.7001,2-Dichlorobenzene 1 03/24/22 19:10 V16588JMV
<0.103 mg/Kg - dry 0.103 0.7001,3-Dichlorobenzene 1 03/24/22 19:10 V16588JMV
<0.103 mg/Kg - dry 0.103 0.3491,4-Dichlorobenzene 1 03/24/22 19:10 V16588JMV
<0.155 mg/Kg - dry 0.155 0.7003,3'-Dichlorobenzidine 1 03/24/22 19:10 V16588JMV
<0.101 mg/Kg - dry 0.101 0.7002,4-Dichlorophenol 1 03/24/22 19:10 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 92
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-DUP
96596 Matrix:
3/21/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.190 mg/Kg - dry 0.190 0.700Diethyl phthalate 1 03/24/22 19:10 V16588JMV
<0.184 mg/Kg - dry 0.184 0.700Dimethyl phthalate 1 03/24/22 19:10 V16588JMV
<0.114 mg/Kg - dry 0.114 0.3492,4-Dimethylphenol 1 03/24/22 19:10 V16588JMV
<0.113 mg/Kg - dry 0.113 0.700Di-n-butyl phthalate 1 03/24/22 19:10 V16588JMV
<0.254 mg/Kg - dry 0.254 1.594,6-Dinitro-2-methylphenol 1 03/24/22 19:10 V16588JMV
<0.551 mg/Kg - dry 0.551 1.592,4-Dinitrophenol 1 03/24/22 19:10 V16588JMV
<0.102 mg/Kg - dry 0.102 0.7002,4-Dinitrotoluene 1 03/24/22 19:10 V16588JMV
<0.114 mg/Kg - dry 0.114 0.7002,6-Dinitrotoluene 1 03/24/22 19:10 V16588JMV
<0.151 mg/Kg - dry 0.151 0.349
Di-n-Octyl Phthalate 1 03/24/22 19:10 V16588JMV
<0.130 mg/Kg - dry 0.130 0.700Fluoranthene 1 03/24/22 19:10 V16588JMV
<0.135 mg/Kg - dry 0.135 0.700Fluorene 1 03/24/22 19:10 V16588JMV
<0.112 mg/Kg - dry 0.112 0.700Hexachlorobenzene 1 03/24/22 19:10 V16588JMV
<0.103 mg/Kg - dry 0.103 0.700Hexachlorobutadiene 1 03/24/22 19:10 V16588JMV
<0.166 mg/Kg - dry 0.166 0.700Hexachlorocyclopentadiene 1 03/24/22 19:10 V16588JMV
<0.084 mg/Kg - dry 0.084 0.700Hexachloroethane 1 03/24/22 19:10 V16588JMV
<0.189 mg/Kg - dry 0.189 0.700
Indeno(1,2,3-cd)pyrene 1 03/24/22 19:10 V16588JMV
<0.202 mg/Kg - dry 0.202 0.700Isophorone 1 03/24/22 19:10 V16588JMV
<0.112 mg/Kg - dry 0.112 0.7001-Methylnaphthalene 1 03/24/22 19:10 V16588JMV
<0.106 mg/Kg - dry 0.106 0.7002-Methylnaphthalene 1 03/24/22 19:10 V16588JMV
<0.102 mg/Kg - dry 0.102 0.7002-Methylphenol 1 03/24/22 19:10 V16588JMV
<0.090 mg/Kg - dry 0.090 0.7003&4 Methylphenol 1 03/24/22 19:10 V16588JMV
<0.152 mg/Kg - dry 0.152 0.700Naphthalene 1 03/24/22 19:10 V16588JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
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,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-080-0034
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 03/21/2022
PAM-003
Report Date : 03/31/2022
Sample ID :
Lab No :
Sampled:FG-DUP
96596 Matrix:
3/21/2022 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V16465 03/23/22 08:11
<0.102 mg/Kg - dry 0.102 0.7002-Nitroaniline 1 03/24/22 19:10 V16588JMV
<0.127 mg/Kg - dry 0.127 0.7003-Nitroaniline 1 03/24/22 19:10 V16588JMV
<0.098 mg/Kg - dry 0.098 0.3494-Nitroaniline 1 03/24/22 19:10 V16588JMV
<0.122 mg/Kg - dry 0.122 0.349Nitrobenzene 1 03/24/22 19:10 V16588JMV
<0.094 mg/Kg - dry 0.094 0.7002-Nitrophenol 1 03/24/22 19:10 V16588JMV
<0.124 mg/Kg - dry 0.124 0.7004-Nitrophenol 1 03/24/22 19:10 V16588JMV
<0.278 mg/Kg - dry 0.278 0.700N-Nitrosodimethylamine 1 03/24/22 19:10 V16588JMV
<0.191 mg/Kg - dry 0.191 0.700N-Nitrosodiphenylamine 1 03/24/22 19:10 V16588JMV
<0.125 mg/Kg - dry 0.125 0.700
N-Nitroso-di-n-propylamine 1 03/24/22 19:10 V16588JMV
<0.367 mg/Kg - dry 0.367 1.06Pentachlorophenol 1 03/24/22 19:10 V16588JMV
<0.220 mg/Kg - dry 0.220 0.700Phenanthrene 1 03/24/22 19:10 V16588JMV
<0.118 mg/Kg - dry 0.118 0.700Phenol 1 03/24/22 19:10 V16588JMV
<0.142 mg/Kg - dry 0.142 0.700Pyrene 1 03/24/22 19:10 V16588JMV
<0.083 mg/Kg - dry 0.083 0.349Pyridine 1 03/24/22 19:10 V16588JMV
<0.113 mg/Kg - dry 0.113 0.7001,2,4-Trichlorobenzene 1 03/24/22 19:10 V16588JMV
<0.102 mg/Kg - dry 0.102 0.700
2,4,5-Trichlorophenol 1 03/24/22 19:10 V16588JMV
<0.102 mg/Kg - dry 0.102 0.7002,4,6-Trichlorophenol 1 03/24/22 19:10 V16588JMV
8270ESurrogate: Phenol-d5 72.8 Limits: 34-121%03/24/22 19:101 JMV
Surrogate: 2-Fluorobiphenyl 76.6 Limits: 44-115%03/24/22 19:101 JMV V16588
Surrogate: 2-Fluorophenol 76.0 Limits: 35-115%03/24/22 19:101 JMV V16588
Surrogate: Nitrobenzene-d5 71.3 Limits: 37-122%03/24/22 19:101 JMV V16588
Surrogate: 4-Terphenyl-d14 78.4 Limits: 54-127%03/24/22 19:101 JMV V16588
Surrogate: 2,4,6-Tribromophenol 77.8 Limits: 39-132%03/24/22 19:101 JMV V16588
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
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




 

 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 

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















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



 


     




 


     




 


     







     







     







     



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





 
    
  




 
    
  




 
    
  




 
    
  




 
    
  




 
    
  




 
    
  

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


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

 
    
  




 
    
  




 
    
  




 
    
  




 
    
  

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

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

 
      
 
 



 
      
 
 



    

 
  







   

 
  







   

 
  







    

 
  





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



    
  
  
  
  
  
  
  
  
  

    
   
   
   
   
   
   
   
   
   
   
   
   
   
   
   
   
   
   


    
  
  
  
  
  
  

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




    

 

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

   

 

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     
    
     



    
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 

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
   
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 

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     
    
     

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    
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 

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
   
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 
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

     
    
     

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


    

 











   

 








     
    
     



    

 











   

 








     
    
     



    

 











   

 








     
    
     

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



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



 
  


   
 

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
 
 
 
 






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
   
   
   
   
   
   
   

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

 











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







Page 71 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Metals Analysis
6010D
V16555QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V16472
Associated Lab Samples: 96591, 96592, 96593, 96594, 96595, 96596
LRB-V16472 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/24/22 11:520.5000.150<0.150mg/KgArsenic
03/24/22 11:520.5000.028<0.028mg/KgBarium
03/24/22 11:520.1000.0081<0.0081mg/KgCadmium
03/24/22 11:520.5000.170<0.170mg/KgChromium
03/24/22 11:520.3000.079<0.079mg/KgLead
03/24/22 11:520.5000.190<0.190mg/KgSelenium
03/24/22 11:520.2500.0290<0.0290mg/KgSilver
LCS-V16472Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.04.595.00mg/KgArsenic 80-120
10351.550.0mg/KgBarium 80-120
1004.995.00mg/KgCadmium 80-120
10351.450.0mg/KgChromium 80-120
1045.205.00mg/KgLead 80-120
91.04.575.00mg/KgSelenium 80-120
97.04.835.00mg/KgSilver 80-120
V 96593-MS-V16472 V 96593-MSD-V16472Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
10.0 169*5.045.005.001.56mg/KgArsenic 70.0*75-125 65.9*20
129 89.015650.050.084.4mg/KgBarium 143*75-125 18.9 20
4.06 81.03.965.005.000.0202mg/KgCadmium 79.0 75-125 2.4 20
104 133*11350.050.037.3mg/KgChromium 151*75-125 8.2 20
Page 1 of 19* QC Fail Date:03/31/2022 02:15 PM
Page 72 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Metals Analysis
6010D
V16555QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V16472
V 96593-MS-V16472 V 96593-MSD-V16472Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
12.0 8.0*13.65.005.0011.6mg/KgLead 40.0*75-125 12.5 20
4.04 81.03.825.005.00<0.190mg/KgSelenium 76.0 75-125 5.5 20
4.36 87.04.165.005.00<0.0290mg/KgSilver 83.0 75-125 4.6 20
V 96593-PDS-V16472Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
03/24/22 12:3991.012.0mg/KgArsenic
03/24/22 12:3997.0162mg/KgBarium
03/24/22 12:3991.011.4mg/KgCadmium
03/24/22 12:3996.0137mg/KgChromium
03/24/22 12:3996.017.6mg/KgLead
03/24/22 12:3990.011.3mg/KgSelenium
03/24/22 12:3994.011.7mg/KgSilver
Page 2 of 19* QC Fail Date:03/31/2022 02:15 PM
Page 73 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V16510QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V16470
Associated Lab Samples: 96591, 96592, 96593, 96594, 96595, 96596
LRB-V16470 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/23/22 16:250.03000.0120<0.0120mg/KgMercury (Total)
LCS-V16470Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1010.4210.417mg/KgMercury (Total)80-120
V 96593-MS-V16470 V 96593-MSD-V16470Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.489 1060.4460.4170.4170.0455mg/KgMercury (Total)96.0 80-120 9.1 20
V 96593-PDS-V16470Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
03/23/22 16:4294.00.218mg/KgMercury (Total)
Page 3 of 19Date:03/31/2022 02:15 PM
Page 74 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V16630QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V16629
Associated Lab Samples: 96591, 96592, 96593, 96594, 96595, 96596
LRB-V16629 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/25/22 09:590.0200.002<0.002mg/KgAcetone
03/25/22 09:590.0200.001<0.001mg/KgAcrolein
03/25/22 09:590.0200.0008<0.0008mg/KgAcrylonitrile
03/25/22 09:590.0050.0006<0.0006mg/KgBenzene
03/25/22 09:590.0050.0005<0.0005mg/KgBromobenzene
03/25/22 09:590.0050.0008<0.0008mg/KgBromochloromethane
03/25/22 09:590.0050.001<0.001mg/KgBromodichloromethane
03/25/22 09:590.0050.001<0.001mg/KgBromoform
03/25/22 09:590.0100.001<0.001mg/KgBromomethane
03/25/22 09:590.0050.0005<0.0005mg/Kgn-Butylbenzene
03/25/22 09:590.0050.0006<0.0006mg/Kgsec-Butyl benzene
03/25/22 09:590.0050.0005<0.0005mg/Kgtert-Butyl benzene
03/25/22 09:590.0050.0006<0.0006mg/KgCarbon Disulfide
03/25/22 09:590.0050.001<0.001mg/KgCarbon Tetrachloride
03/25/22 09:590.0050.0007<0.0007mg/KgChlorobenzene
03/25/22 09:590.0050.0009<0.0009mg/KgChlorodibromomethane
03/25/22 09:590.0100.0009<0.0009mg/KgChloroethane
03/25/22 09:590.0050.001<0.001mg/KgChloroform
03/25/22 09:590.0100.0006<0.0006mg/KgChloromethane
03/25/22 09:590.0050.0005<0.0005mg/Kg2-Chlorotoluene
03/25/22 09:590.0050.0004<0.0004mg/Kg4-Chlorotoluene
03/25/22 09:590.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
03/25/22 09:590.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
03/25/22 09:590.0050.0006<0.0006mg/Kg1,2-Dibromoethane
03/25/22 09:590.0050.0006<0.0006mg/KgDibromomethane
03/25/22 09:590.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
03/25/22 09:590.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 19Date:03/31/2022 02:15 PM
Page 75 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V16630QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V16629
Associated Lab Samples: 96591, 96592, 96593, 96594, 96595, 96596
LRB-V16629 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/25/22 09:590.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
03/25/22 09:590.0100.001<0.001mg/KgDichlorodifluoromethane
03/25/22 09:590.0050.0008<0.0008mg/Kg1,1-Dichloroethane
03/25/22 09:590.0050.001<0.001mg/Kg1,2-Dichloroethane
03/25/22 09:590.0050.0007<0.0007mg/Kg1,1-Dichloroethene
03/25/22 09:590.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
03/25/22 09:590.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
03/25/22 09:590.0050.0004<0.0004mg/Kg1,2-Dichloropropane
03/25/22 09:590.0050.0006<0.0006mg/Kg1,3-Dichloropropane
03/25/22 09:590.0050.001<0.001mg/Kg2,2-Dichloropropane
03/25/22 09:590.0050.0008<0.0008mg/Kg1,1-Dichloropropene
03/25/22 09:590.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
03/25/22 09:590.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
03/25/22 09:590.2500.014<0.014mg/KgEthanol
03/25/22 09:590.0050.0006<0.0006mg/KgEthylbenzene
03/25/22 09:590.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
03/25/22 09:590.0100.0008<0.0008mg/KgHexachlorobutadiene
03/25/22 09:590.0100.0007<0.0007mg/Kgn-Hexane
03/25/22 09:590.0200.0006<0.0006mg/Kg2-Hexanone
03/25/22 09:590.0050.0005<0.0005mg/KgIsopropylbenzene
03/25/22 09:590.0050.001<0.001mg/Kg4-Isopropyl toluene
03/25/22 09:590.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
03/25/22 09:590.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
03/25/22 09:590.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
03/25/22 09:590.0100.001<0.001mg/KgMethylene Chloride
03/25/22 09:590.0100.0010<0.0010mg/KgNaphthalene
03/25/22 09:590.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 19Date:03/31/2022 02:15 PM
Page 76 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V16630QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V16629
Associated Lab Samples: 96591, 96592, 96593, 96594, 96595, 96596
LRB-V16629 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/25/22 09:590.0050.001<0.001mg/KgStyrene
03/25/22 09:590.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
03/25/22 09:590.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
03/25/22 09:590.0050.0009<0.0009mg/KgTetrachloroethene
03/25/22 09:590.0050.0007<0.0007mg/KgToluene
03/25/22 09:590.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
03/25/22 09:590.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
03/25/22 09:590.0050.001<0.001mg/Kg1,1,1-Trichloroethane
03/25/22 09:590.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
03/25/22 09:590.0050.0009<0.0009mg/KgTrichloroethene
03/25/22 09:590.0100.002<0.002mg/KgTrichlorofluoromethane
03/25/22 09:590.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
03/25/22 09:590.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
03/25/22 09:590.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
03/25/22 09:590.0100.0005<0.0005mg/KgVinyl Acetate
03/25/22 09:590.0100.0005<0.0005mg/KgVinyl Chloride
03/25/22 09:590.0050.0005<0.0005mg/Kgo-Xylene
03/25/22 09:590.0100.001<0.001mg/Kgm,p-Xylene
03/25/22 09:594-Bromofluorobenzene (S)99.2 70-130
03/25/22 09:59Dibromofluoromethane (S)99.8 84-123
03/25/22 09:59Toluene-d8 (S)96.4 76-129
LCS-V16629 LCSD-V16629Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.116 1161240.1240.100mg/KgAcetone 29-198 6.6 20
Page 6 of 19Date:03/31/2022 02:15 PM
Page 77 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V16630QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V16629
LCS-V16629 LCSD-V16629Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.103 1031110.1110.100mg/KgAcrolein 70-130 7.4 20
0.102 1021070.1070.100mg/KgAcrylonitrile 65-134 4.7 20
0.048 97.699.40.0490.050mg/KgBenzene 74-127 1.8 20
0.047 94.895.40.0470.050mg/KgBromobenzene 73-125 0.6 20
0.050 1011020.0510.050mg/KgBromochloromethane 72-134 0.9 20
0.050 1011030.0510.050mg/KgBromodichloromethane 75-122 1.9 20
0.049 99.01040.0510.050mg/KgBromoform 66-135 4.7 20
0.051 1041120.0560.050mg/KgBromomethane 20-180 7.7 20
0.045 91.093.00.0460.050mg/Kgn-Butylbenzene 65-135 2.1 20
0.044 88.892.40.0460.050mg/Kgsec-Butyl benzene 66-131 3.9 20
0.045 90.291.40.0450.050mg/Kgtert-Butyl benzene 67-132 1.3 20
0.046 92.095.60.0470.050mg/KgCarbon Disulfide 61-129 3.8 20
0.044 88.492.80.0460.050mg/KgCarbon Tetrachloride 64-143 4.8 20
0.048 96.098.00.0490.050mg/KgChlorobenzene 74-118 2.0 20
0.049 99.61010.0500.050mg/KgChlorodibromomethane 73-122 1.5 20
0.047 95.299.00.0490.050mg/KgChloroethane 33-149 3.9 20
0.049 99.01010.0500.050mg/KgChloroform 73-127 2.3 20
0.048 97.21020.0510.050mg/KgChloromethane 45-143 4.8 20
0.046 93.895.20.0470.050mg/Kg2-Chlorotoluene 67-124 1.4 20
0.046 92.694.80.0470.050mg/Kg4-Chlorotoluene 71-126 2.3 20
0.051 1031040.0520.050mg/KgDi-Isopropyl Ether (DIPE)59-159 1.5 20
0.049 99.01030.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 3.9 20
0.049 98.81010.0500.050mg/Kg1,2-Dibromoethane 70-132 1.8 20
0.052 1051060.0530.050mg/KgDibromomethane 74-133 1.1 20
0.047 95.495.80.0470.050mg/Kg1,2-Dichlorobenzene 72-123 0.4 20
0.047 94.295.80.0470.050mg/Kg1,3-Dichlorobenzene 71-120 1.6 20
Page 7 of 19Date:03/31/2022 02:15 PM
Page 78 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V16630QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V16629
LCS-V16629 LCSD-V16629Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 93.694.80.0470.050mg/Kg1,4-Dichlorobenzene 71-123 1.2 20
0.044 88.895.40.0470.050mg/KgDichlorodifluoromethane 26-146 7.1 20
0.049 99.61020.0510.050mg/Kg1,1-Dichloroethane 74-127 2.5 20
0.050 1011030.0510.050mg/Kg1,2-Dichloroethane 68-128 1.7 20
0.045 90.494.20.0470.050mg/Kg1,1-Dichloroethene 67-149 4.1 20
0.049 99.01020.0510.050mg/Kgcis-1,2-Dichloroethene 76-134 2.9 20
0.047 95.899.00.0490.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.2 20
0.051 1031040.0510.050mg/Kg1,2-Dichloropropane 73-130 0.5 20
0.049 98.21010.0500.050mg/Kg1,3-Dichloropropane 75-124 2.8 20
0.045 91.296.20.0480.050mg/Kg2,2-Dichloropropane 50-142 5.3 20
0.045 90.492.80.0460.050mg/Kg1,1-Dichloropropene 71-130 2.6 20
0.050 1021040.0520.050mg/Kgcis-1,3-Dichloropropene 71-125 2.3 20
0.050 1011050.0520.050mg/Kgtrans-1,3-Dichloropropene 68-123 3.8 20
1.34 1071101.371.25mg/KgEthanol 70-130 2.2 20
0.046 92.695.00.0470.050mg/KgEthylbenzene 74-128 2.5 20
0.103 1031040.1040.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.045 90.892.40.0460.050mg/KgHexachlorobutadiene 64-125 1.7 20
0.043 87.889.40.0440.050mg/Kgn-Hexane 70-130 1.8 20
0.053 1081150.0570.050mg/Kg2-Hexanone 61-157 6.8 20
0.044 89.891.00.0450.050mg/KgIsopropylbenzene 68-126 1.3 20
0.045 91.293.40.0460.050mg/Kg4-Isopropyl toluene 68-129 2.3 20
0.056 1131180.0590.050mg/KgMethyl Ethyl Ketone (MEK)63-149 4.1 20
0.051 1031060.0520.050mg/KgMethyl tert-butyl ether (MTBE)70-130 2.6 20
0.052 1061110.0550.050mg/Kg4-Methyl-2-Pentanone 57-162 4.7 20
0.049 98.299.60.0490.050mg/KgMethylene Chloride 74-129 1.4 20
0.046 93.496.20.0480.050mg/KgNaphthalene 57-157 2.9 20
Page 8 of 19Date:03/31/2022 02:15 PM
Page 79 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V16630QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V16629
LCS-V16629 LCSD-V16629Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 90.692.40.0460.050mg/Kgn-Propylbenzene 67-130 1.9 20
0.049 98.61010.0500.050mg/KgStyrene 77-121 2.6 20
0.048 96.81000.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 3.6 20
0.047 95.697.80.0480.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.2 20
0.045 91.096.40.0480.050mg/KgTetrachloroethene 68-130 5.7 20
0.048 96.099.20.0490.050mg/KgToluene 71-129 3.2 20
0.048 97.298.00.0490.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.8 20
0.048 96.698.80.0490.050mg/Kg1,2,4-Trichlorobenzene 66-125 2.2 20
0.045 90.895.40.0470.050mg/Kg1,1,1-Trichloroethane 67-131 4.9 20
0.049 98.81020.0500.050mg/Kg1,1,2-Trichloroethane 70-133 2.7 20
0.048 97.099.80.0490.050mg/KgTrichloroethene 75-133 2.8 20
0.047 94.099.40.0490.050mg/KgTrichlorofluoromethane 44-146 5.5 20
0.048 97.098.20.0490.050mg/Kg1,2,3-Trichloropropane 60-137 1.2 20
0.046 93.495.80.0470.050mg/Kg1,2,4-Trimethylbenzene 69-129 2.5 20
0.046 93.293.80.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 0.6 20
0.053 1061120.0550.050mg/KgVinyl Acetate 60-140 5.1 20
0.046 92.498.00.0490.050mg/KgVinyl Chloride 48-147 5.8 20
0.047 95.097.40.0480.050mg/Kgo-Xylene 74-126 2.4 20
0.094 94.297.80.0970.100mg/Kgm,p-Xylene 75-124 3.7 20
99.298.24-Bromofluorobenzene (S)70-130
101101Dibromofluoromethane (S)84-123
96.697.6Toluene-d8 (S)76-129
Page 9 of 19Date:03/31/2022 02:15 PM
Page 80 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V16588QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V16465
Associated Lab Samples: 96591, 96592, 96593, 96594, 96595, 96596
LRB-V16465 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/24/22 12:020.6600.116<0.116mg/KgAcenaphthene
03/24/22 12:020.6600.105<0.105mg/KgAcenaphthylene
03/24/22 12:020.6600.152<0.152mg/KgAniline
03/24/22 12:020.6600.143<0.143mg/KgAnthracene
03/24/22 12:020.6600.139<0.139mg/KgBenzo(a)anthracene
03/24/22 12:020.6600.147<0.147mg/KgBenzo(a)pyrene
03/24/22 12:020.6600.146<0.146mg/KgBenzo(b)fluoranthene
03/24/22 12:020.6600.136<0.136mg/KgBenzo(g,h,i)perylene
03/24/22 12:020.6600.137<0.137mg/KgBenzo(k)fluoranthene
03/24/22 12:022.000.580<0.580mg/KgBenzoic Acid
03/24/22 12:020.6600.105<0.105mg/KgBenzyl alcohol
03/24/22 12:020.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
03/24/22 12:020.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
03/24/22 12:020.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
03/24/22 12:020.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
03/24/22 12:020.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
03/24/22 12:020.3300.113<0.113mg/KgButyl benzyl phthalate
03/24/22 12:020.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
03/24/22 12:020.3300.112<0.112mg/Kg4-Chloroaniline
03/24/22 12:020.6600.116<0.116mg/Kg2-Chloronaphthalene
03/24/22 12:020.6600.098<0.098mg/Kg2-Chlorophenol
03/24/22 12:021.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
03/24/22 12:020.6600.142<0.142mg/KgChrysene
03/24/22 12:020.6600.230<0.230mg/KgDibenz(a,h)anthracene
03/24/22 12:020.6600.119<0.119mg/KgDibenzofuran
03/24/22 12:020.6600.094<0.094mg/Kg1,2-Dichlorobenzene
03/24/22 12:020.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 10 of 19Date:03/31/2022 02:15 PM
Page 81 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V16588QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V16465
Associated Lab Samples: 96591, 96592, 96593, 96594, 96595, 96596
LRB-V16465 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/24/22 12:020.3300.097<0.097mg/Kg1,4-Dichlorobenzene
03/24/22 12:020.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
03/24/22 12:020.6600.095<0.095mg/Kg2,4-Dichlorophenol
03/24/22 12:020.6600.180<0.180mg/KgDiethyl phthalate
03/24/22 12:020.6600.174<0.174mg/KgDimethyl phthalate
03/24/22 12:020.3300.108<0.108mg/Kg2,4-Dimethylphenol
03/24/22 12:020.6600.107<0.107mg/KgDi-n-butyl phthalate
03/24/22 12:021.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
03/24/22 12:021.500.520<0.520mg/Kg2,4-Dinitrophenol
03/24/22 12:020.6600.096<0.096mg/Kg2,4-Dinitrotoluene
03/24/22 12:020.6600.108<0.108mg/Kg2,6-Dinitrotoluene
03/24/22 12:020.3300.143<0.143mg/KgDi-n-Octyl Phthalate
03/24/22 12:020.6600.123<0.123mg/KgFluoranthene
03/24/22 12:020.6600.128<0.128mg/KgFluorene
03/24/22 12:020.6600.106<0.106mg/KgHexachlorobenzene
03/24/22 12:020.6600.097<0.097mg/KgHexachlorobutadiene
03/24/22 12:020.6600.157<0.157mg/KgHexachlorocyclopentadiene
03/24/22 12:020.6600.079<0.079mg/KgHexachloroethane
03/24/22 12:020.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
03/24/22 12:020.6600.191<0.191mg/KgIsophorone
03/24/22 12:020.6600.106<0.106mg/Kg1-Methylnaphthalene
03/24/22 12:020.6600.100<0.100mg/Kg2-Methylnaphthalene
03/24/22 12:020.6600.097<0.097mg/Kg2-Methylphenol
03/24/22 12:020.6600.084<0.084mg/Kg3&4 Methylphenol
03/24/22 12:020.6600.144<0.144mg/KgNaphthalene
03/24/22 12:020.6600.096<0.096mg/Kg2-Nitroaniline
03/24/22 12:020.6600.120<0.120mg/Kg3-Nitroaniline
Page 11 of 19Date:03/31/2022 02:15 PM
Page 82 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V16588QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V16465
Associated Lab Samples: 96591, 96592, 96593, 96594, 96595, 96596
LRB-V16465 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/24/22 12:020.3300.093<0.093mg/Kg4-Nitroaniline
03/24/22 12:020.3300.116<0.116mg/KgNitrobenzene
03/24/22 12:020.6600.088<0.088mg/Kg2-Nitrophenol
03/24/22 12:020.6600.117<0.117mg/Kg4-Nitrophenol
03/24/22 12:020.6600.263<0.263mg/KgN-Nitrosodimethylamine
03/24/22 12:020.6600.181<0.181mg/KgN-Nitrosodiphenylamine
03/24/22 12:020.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
03/24/22 12:021.000.347<0.347mg/KgPentachlorophenol
03/24/22 12:020.6600.208<0.208mg/KgPhenanthrene
03/24/22 12:020.6600.112<0.112mg/KgPhenol
03/24/22 12:020.6600.134<0.134mg/KgPyrene
03/24/22 12:020.3300.079<0.079mg/KgPyridine
03/24/22 12:020.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
03/24/22 12:020.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
03/24/22 12:020.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
03/24/22 12:022-Fluorobiphenyl (S)86.8 44-115
03/24/22 12:022-Fluorophenol (S)85.5 35-115
03/24/22 12:02Nitrobenzene-d5 (S)79.0 37-122
03/24/22 12:024-Terphenyl-d14 (S)89.2 54-127
03/24/22 12:022,4,6-Tribromophenol (S)95.7 39-132
03/24/22 12:02Phenol-d5 (S)81.6 34-121
LCS-V16465Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
79.61.331.67mg/KgAcenaphthene 40-123
84.41.411.67mg/KgAcenaphthylene 32-132
Page 12 of 19Date:03/31/2022 02:15 PM
Page 83 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V16588QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V16465
LCS-V16465Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
86.81.451.67mg/KgAniline 12-197
87.41.461.67mg/KgAnthracene 47-123
84.41.411.67mg/KgBenzo(a)anthracene 49-126
1021.701.67mg/KgBenzo(a)pyrene 45-129
91.61.531.67mg/KgBenzo(b)fluoranthene 45-132
88.01.471.67mg/KgBenzo(g,h,i)perylene 43-134
87.41.461.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.081.67mg/KgBenzoic Acid 10-83
77.81.301.67mg/KgBenzyl alcohol 29-122
80.21.341.67mg/KgBis(2-Chloroethoxy)methane 36-121
76.61.281.67mg/KgBis(2-Chloroethyl)ether 31-120
77.81.301.67mg/KgBis(2-Chloroisopropyl)ether 33-131
94.01.571.67mg/KgBis(2-ethylhexyl)phthalate 51-133
86.81.451.67mg/Kg4-Bromophenyl phenyl ether 46-124
87.41.461.67mg/KgButyl benzyl phthalate 48-132
80.81.351.67mg/Kg4-Chloro-3-methylphenol 45-122
70.01.171.67mg/Kg4-Chloroaniline 17-106
81.41.361.67mg/Kg2-Chloronaphthalene 41-114
80.81.351.67mg/Kg2-Chlorophenol 34-121
85.61.431.67mg/Kg4-Chlorophenyl phenyl ether 45-121
85.01.421.67mg/KgChrysene 50-124
82.01.371.67mg/KgDibenz(a,h)anthracene 45-134
82.01.371.67mg/KgDibenzofuran 44-120
72.41.211.67mg/Kg1,2-Dichlorobenzene 33-117
71.81.201.67mg/Kg1,3-Dichlorobenzene 30-115
70.61.181.67mg/Kg1,4-Dichlorobenzene 31-115
62.21.041.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 13 of 19* QC Fail Date:03/31/2022 02:15 PM
Page 84 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V16588QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V16465
LCS-V16465Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
78.41.311.67mg/Kg2,4-Dichlorophenol 40-122
86.21.441.67mg/KgDiethyl phthalate 50-124
83.81.401.67mg/KgDimethyl phthalate 48-124
83.81.401.67mg/Kg2,4-Dimethylphenol 30-127
94.61.581.67mg/KgDi-n-butyl phthalate 51-128
0.0*1.411.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
0.0*1.441.67mg/Kg2,4-Dinitrophenol 27-129
88.61.481.67mg/Kg2,4-Dinitrotoluene 48-126
91.01.521.67mg/Kg2,6-Dinitrotoluene 46-124
94.01.571.67mg/KgDi-n-Octyl Phthalate 45-140
85.01.421.67mg/KgFluoranthene 50-127
86.21.441.67mg/KgFluorene 43-125
87.41.461.67mg/KgHexachlorobenzene 45-122
71.81.201.67mg/KgHexachlorobutadiene 32-123
67.01.121.67mg/KgHexachlorocyclopentadiene 32-117
70.01.171.67mg/KgHexachloroethane 28-117
89.21.491.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
67.61.131.67mg/KgIsophorone 30-122
70.61.181.67mg/Kg1-Methylnaphthalene 40-119
70.01.171.67mg/Kg2-Methylnaphthalene 38-122
82.01.371.67mg/Kg2-Methylphenol 32-122
71.21.191.67mg/Kg3&4 Methylphenol 34-119
67.61.131.67mg/KgNaphthalene 35-123
84.41.411.67mg/Kg2-Nitroaniline 44-127
82.01.371.67mg/Kg3-Nitroaniline 33-119
83.81.401.67mg/Kg4-Nitroaniline 63-147
68.21.141.67mg/KgNitrobenzene 34-122
Page 14 of 19* QC Fail Date:03/31/2022 02:15 PM
Page 85 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V16588QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V16465
LCS-V16465Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
71.21.191.67mg/Kg2-Nitrophenol 36-123
91.61.531.67mg/Kg4-Nitrophenol 30-132
53.00.8861.67mg/KgN-Nitrosodimethylamine 10-146
1021.701.67mg/KgN-Nitrosodiphenylamine 38-127
76.61.281.67mg/KgN-Nitroso-di-n-propylamine 36-120
1101.841.67mg/KgPentachlorophenol 25-133
85.61.431.67mg/KgPhenanthrene 50-121
79.01.321.67mg/KgPhenol 34-121
86.21.441.67mg/KgPyrene 47-127
40.30.6741.67mg/KgPyridine 10-80
68.21.141.67mg/Kg1,2,4-Trichlorobenzene 34-118
85.01.421.67mg/Kg2,4,5-Trichlorophenol 41-124
89.81.501.67mg/Kg2,4,6-Trichlorophenol 39-126
82.02-Fluorobiphenyl (S)44-115
83.12-Fluorophenol (S)35-115
67.6Nitrobenzene-d5 (S)37-122
89.24-Terphenyl-d14 (S)54-127
96.02,4,6-Tribromophenol (S)39-132
79.5Phenol-d5 (S)34-121
V 96592-MS-V16465 V 96592-MSD-V16465Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.26 75.41.061.671.67<0.116mg/KgAcenaphthene 63.4 40-123 17.2 20
1.36 81.41.161.671.67<0.105mg/KgAcenaphthylene 69.4 32-132 15.8 20
1.08 64.61.021.671.67<0.152mg/KgAniline 61.0 12-197 5.7 20
Page 15 of 19Date:03/31/2022 02:15 PM
Page 86 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V16588QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V16465
V 96592-MS-V16465 V 96592-MSD-V16465Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.35 80.81.151.671.67<0.143mg/KgAnthracene 68.8 47-123 16.0 20
1.29 77.21.121.671.67<0.139mg/KgBenzo(a)anthracene 67.0 49-126 14.1 20
1.52 91.01.301.671.67<0.147mg/KgBenzo(a)pyrene 77.8 45-129 15.6 20
1.42 85.01.231.671.67<0.146mg/KgBenzo(b)fluoranthene 73.6 45-132 14.3 20
1.08 64.60.8861.671.67<0.136mg/KgBenzo(g,h,i)perylene 53.0 43-134 19.7 20
1.30 77.81.111.671.67<0.137mg/KgBenzo(k)fluoranthene 66.4 47-132 15.7 20
<0.580 0.0*<0.5801.671.67<0.580mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.32 79.01.151.671.67<0.105mg/KgBenzyl alcohol 68.8 29-122 13.7 20
1.32 79.01.151.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 68.8 36-121 13.7 20
1.25 74.81.071.671.67<0.107mg/KgBis(2-Chloroethyl)ether 64.0 31-120 15.5 20
1.32 79.01.141.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 68.2 33-131 14.6 20
1.53 91.61.281.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 76.6 51-133 17.7 20
1.37 82.01.151.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 68.8 46-124 17.4 20
1.40 83.81.201.671.67<0.113mg/KgButyl benzyl phthalate 71.8 48-132 15.3 20
1.21 72.41.031.671.67<0.092mg/Kg4-Chloro-3-methylphenol 61.6 45-122 16.0 20
1.00 59.80.9051.671.67<0.112mg/Kg4-Chloroaniline 54.1 17-106 9.9 20
1.34 80.21.161.671.67<0.116mg/Kg2-Chloronaphthalene 69.4 41-114 14.4 20
1.31 78.41.151.671.67<0.098mg/Kg2-Chlorophenol 68.8 34-121 13.0 20
1.32 79.01.101.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 65.8 45-121 18.1 20
1.31 78.41.111.671.67<0.142mg/KgChrysene 66.4 50-124 16.5 20
1.11 66.40.9091.671.67<0.230mg/KgDibenz(a,h)anthracene 54.4 45-134 19.9 20
1.32 79.01.121.671.67<0.119mg/KgDibenzofuran 67.0 44-120 16.3 20
1.18 70.61.031.671.67<0.094mg/Kg1,2-Dichlorobenzene 61.6 33-117 13.5 20
1.15 68.80.9961.671.67<0.097mg/Kg1,3-Dichlorobenzene 59.6 30-115 14.3 20
1.13 67.60.9951.671.67<0.097mg/Kg1,4-Dichlorobenzene 59.5 31-115 12.7 20
0.590 0.0*0.5591.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 0.0*22-121 0.0 20
Page 16 of 19* QC Fail Date:03/31/2022 02:15 PM
Page 87 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V16588QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V16465
V 96592-MS-V16465 V 96592-MSD-V16465Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.22 73.01.061.671.67<0.095mg/Kg2,4-Dichlorophenol 63.4 40-122 14.0 20
1.33 79.61.141.671.67<0.180mg/KgDiethyl phthalate 68.2 50-124 15.3 20
1.30 77.81.111.671.67<0.174mg/KgDimethyl phthalate 66.4 48-124 15.7 30
1.01 60.40.9021.671.67<0.108mg/Kg2,4-Dimethylphenol 54.0 30-127 11.2 20
1.47 88.01.271.671.67<0.107mg/KgDi-n-butyl phthalate 76.0 51-128 14.5 20
0.630 0.0*0.5311.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
0.529 0.0*<0.5201.671.67<0.520mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.34 80.21.141.671.67<0.096mg/Kg2,4-Dinitrotoluene 68.2 48-126 16.1 20
1.40 83.81.171.671.67<0.108mg/Kg2,6-Dinitrotoluene 70.0 46-124 17.8 20
1.52 91.01.291.671.67<0.143mg/KgDi-n-Octyl Phthalate 77.2 45-140 16.3 20
1.29 77.21.121.671.67<0.123mg/KgFluoranthene 67.0 50-127 14.1 20
1.34 80.21.141.671.67<0.128mg/KgFluorene 68.2 43-125 16.1 20
1.27 76.01.071.671.67<0.106mg/KgHexachlorobenzene 64.0 45-122 17.0 20
1.17 70.01.021.671.67<0.097mg/KgHexachlorobutadiene 61.0 32-123 13.6 20
0.203 0.0*0.1751.671.67<0.157mg/KgHexachlorocyclopentadiene 0.0*32-117 0.0 20
1.03 61.60.8851.671.67<0.079mg/KgHexachloroethane 52.9 28-117 15.1 20
1.16 69.40.9581.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 57.3 45-133 19.0 20
1.09 65.20.9401.671.67<0.191mg/KgIsophorone 56.2 30-122 14.7 20
1.13 67.60.9901.671.67<0.106mg/Kg1-Methylnaphthalene 59.2 40-119 13.2 20
1.14 68.20.9991.671.67<0.100mg/Kg2-Methylnaphthalene 59.8 38-122 13.1 20
1.19 71.21.061.671.67<0.097mg/Kg2-Methylphenol 63.4 32-122 11.5 20
1.06 63.40.9161.671.67<0.084mg/Kg3&4 Methylphenol 54.8 34-119 14.5 20
1.13 67.60.9721.671.67<0.144mg/KgNaphthalene 58.2 35-123 15.0 20
1.37 82.01.181.671.67<0.096mg/Kg2-Nitroaniline 70.6 44-127 14.9 20
1.29 77.21.091.671.67<0.120mg/Kg3-Nitroaniline 65.2 33-119 16.8 20
1.30 77.81.111.671.67<0.093mg/Kg4-Nitroaniline 66.4 63-147 15.7 20
Page 17 of 19* QC Fail Date:03/31/2022 02:15 PM
Page 88 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V16588QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V16465
V 96592-MS-V16465 V 96592-MSD-V16465Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.14 68.20.9991.671.67<0.116mg/KgNitrobenzene 59.8 34-122 13.1 20
1.16 69.41.031.671.67<0.088mg/Kg2-Nitrophenol 61.6 32-123 11.8 20
1.33 79.61.161.671.67<0.117mg/Kg4-Nitrophenol 69.4 30-132 13.6 20
0.877 52.50.7231.671.67<0.263mg/KgN-Nitrosodimethylamine 43.2 10-146 19.2 30
1.53 91.61.311.671.67<0.181mg/KgN-Nitrosodiphenylamine 78.4 38-127 15.4 20
1.26 75.41.091.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 65.2 36-120 14.4 20
1.48 88.61.241.671.67<0.347mg/KgPentachlorophenol 74.2 25-133 17.6 20
1.34 80.21.161.671.67<0.208mg/KgPhenanthrene 69.4 50-121 14.4 20
1.26 75.41.111.671.67<0.112mg/KgPhenol 66.4 34-121 12.6 20
1.39 83.21.181.671.67<0.134mg/KgPyrene 70.6 47-127 16.3 20
0.732 43.80.6321.671.67<0.079mg/KgPyridine 37.8 10-80 14.6 20
1.12 67.00.9731.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 58.2 34-118 14.0 20
1.28 76.61.111.671.67<0.096mg/Kg2,4,5-Trichlorophenol 66.4 41-124 14.2 20
1.35 80.81.161.671.67<0.096mg/Kg2,4,6-Trichlorophenol 69.4 39-126 15.1 20
80.82-Fluorobiphenyl (S)68.8 44-115
79.52-Fluorophenol (S)68.2 35-115
68.8Nitrobenzene-d5 (S)58.9 37-122
82.04-Terphenyl-d14 (S)68.8 54-127
80.12,4,6-Tribromophenol (S)68.5 39-132
75.0Phenol-d5 (S)64.6 34-121
Page 18 of 19Date:03/31/2022 02:15 PM
Page 89 of 92
Quality Control Data
22-080-0034Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
PAM-003
Dry Weight Determination
SW-DRYWT
V16532QC Analytical Batch:
Analysis Method:
Analysis Description:
V 96592-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/24/22 10:330.714.114.0%Moisture
Page 19 of 19Date:03/31/2022 02:15 PM
Page 90 of 92
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-080-0034
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 4.2C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Sarah J. Locklear Date & Time:03/21/2022 16:32:53
Special precautions or instructions included?
Comments:
Page 91 of 92
Page 92 of 92

Appendix B
DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
hypothetical worst-case final grade soil
North Carolina Department of Environmental Quality
Risk Calculator
North Davidson II Brownfields Property
2315 N. Davidson Street and 421 E. 26th Street
Brownfields Program
24003-20-060
January 2022
November 2021 EPA RSL Table
4/1/2022
Prepared By:Hart & Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC 28203
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: 24003-20-060
Exposure Unit ID: hypothetical worst-case final grade soil
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: 24003-20-060
Exposure Unit ID: hypothetical worst-case final grade soil
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: January 2022Basis: November 2021 EPA RSL TableSite ID: 24003-20-060Exposure Unit ID: hypothetical worst-case final grade soilNOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsExposure Point Concentration (mg/kg)Notes: CAS NumberChemicalFor the chemicals highlighted in blue, data entry notes are provided in the PSRG Table link on the Main MenuMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion0.037 67-64-1Acetonemg/kg3.02 7440-38-2Arsenic, Inorganicmg/kg109 7440-39-3Bariummg/kg0.256 7440-43-9Cadmium (Diet)mg/kg0.0009 75-15-0Carbon Disulfidemg/kg59.7 16065-83-1Chromium(III), Insoluble Saltsmg/kg2.7 18540-29-9Chromium(VI)mg/kg59.1 7439-92-1~Lead and Compoundsmg/kg0.0819 7487-94-7~Mercuric Chloride (and other Mercury salts)mg/kg0.004 78-93-3Methyl Ethyl Ketone (2-Butanone)mg/kg0.001 75-09-2Methylene Chloridemg/kg0.315 56-55-3~Benz[a]anthracenemg/kg0.29 50-32-8~Benzo[a]pyrenemg/kg0.535 205-99-2~Benzo[b]fluoranthenemg/kg0.411 218-01-9~Chrysenemg/kg0.718 206-44-0~Fluoranthenemg/kg0.654 129-00-0~Pyrenemg/kg0.342 7782-49-2Seleniummg/kgInput Form 2ASoil Exposure Point Concentration TableDescription of Exposure Point Concentration Selection:North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: 24003-20-060
Exposure Unit ID: hypothetical worst-case final grade soil
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 1.7E-05 1.6E-01 NO
Groundwater Use* NC NC NC
Soil 1.6E-06 1.2E-02 NO
Groundwater Use* NC NC NC
Construction Worker Soil 9.4E-07 1.2E-01 NO
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: 24003-20-060
Exposure Unit ID: hypothetical worst-case final grade soil
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.037 0.037 0.037 5.3E-07 5.3E-07
7440-38-2 Arsenic, Inorganic 3.02 3.02 3.02 3.9E-06 5.5E-07 7.8E-11 4.5E-06 7.7E-02 9.2E-03 3.3E-06 8.6E-02
7440-39-3 Barium 109 109 109 7.0E-03 3.5E-06 7.0E-03
7440-43-9 Cadmium (Diet) 0.256 0.256 0.256 2.8E-12 2.8E-12 3.3E-02 3.1E-03 4.1E-07 3.6E-02
75-15-0 Carbon Disulfide 0.0009 0.0009 0.0009 1.2E-07 3.9E-07 5.1E-07
16065-83-1 Chromium(III), Insoluble Salts 59.7 59.7 59.7 5.1E-04 5.1E-04
18540-29-9 Chromium(VI) 2.7 2.7 2.7 8.8E-06 3.8E-09 8.8E-06 1.2E-02 4.4E-07 1.2E-02
7439-92-1 ~Lead and Compounds 59.1 59.1 59.1 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.0819 0.0819 0.0819 3.5E-03 4.4E-09 3.5E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.004 0.004 0.004 8.5E-08 5.9E-08 1.4E-07
75-09-2 Methylene Chloride 0.001 0.001 0.001 1.3E-11 3.1E-12 1.6E-11 2.1E-06 5.1E-07 2.6E-06
56-55-3 ~Benz[a]anthracene 0.315 0.315 0.315 2.1E-07 6.9E-08 4.0E-09 2.8E-07
50-32-8 ~Benzo[a]pyrene 0.29 0.29 0.29 1.9E-06 6.3E-07 2.9E-12 2.5E-06 1.2E-02 3.8E-03 2.3E-06 1.6E-02
205-99-2 ~Benzo[b]fluoranthene 0.535 0.535 0.535 3.5E-07 1.2E-07 5.3E-13 4.7E-07
218-01-9 ~Chrysene 0.411 0.411 0.411 2.7E-09 9.0E-10 4.1E-15 3.6E-09
206-44-0 ~Fluoranthene 0.718 0.718 0.718 2.3E-04 7.1E-05 3.0E-04
129-00-0 ~Pyrene 0.654 0.654 0.654 2.8E-04 8.6E-05 3.6E-04
7782-49-2 Selenium 0.342 0.342 0.342 8.7E-04 2.8E-10 8.7E-04
Cumulative: 1.7E-05 1.6E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: 24003-20-060
Exposure Unit ID: hypothetical worst-case final grade soil
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.037 0.037 0.037 3.5E-08 3.5E-08
7440-38-2 Arsenic, Inorganic 3.02 3.02 3.02 8.3E-07 1.8E-07 1.8E-11 1.0E-06 5.2E-03 1.1E-03 7.7E-07 6.3E-03
7440-39-3 Barium 109 109 109 4.7E-04 8.4E-07 4.7E-04
7440-43-9 Cadmium (Diet) 0.256 0.256 0.256 6.3E-13 6.3E-13 2.2E-03 3.7E-04 9.9E-08 2.6E-03
75-15-0 Carbon Disulfide 0.0009 0.0009 0.0009 7.7E-09 9.3E-08 1.0E-07
16065-83-1 Chromium(III), Insoluble Salts 59.7 59.7 59.7 3.4E-05 3.4E-05
18540-29-9 Chromium(VI) 2.7 2.7 2.7 4.1E-07 3.1E-10 4.1E-07 7.7E-04 1.0E-07 7.7E-04
7439-92-1 ~Lead and Compounds 59.1 59.1 59.1 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.0819 0.0819 0.0819 2.3E-04 1.1E-09 2.3E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.004 0.004 0.004 5.7E-09 1.4E-08 2.0E-08
75-09-2 Methylene Chloride 0.001 0.001 0.001 6.1E-13 2.6E-13 8.7E-13 1.4E-07 1.2E-07 2.6E-07
56-55-3 ~Benz[a]anthracene 0.315 0.315 0.315 9.6E-09 5.3E-09 3.3E-10 1.5E-08
50-32-8 ~Benzo[a]pyrene 0.29 0.29 0.29 8.9E-08 4.9E-08 2.4E-13 1.4E-07 8.3E-04 4.6E-04 5.6E-07 1.3E-03
205-99-2 ~Benzo[b]fluoranthene 0.535 0.535 0.535 1.6E-08 9.0E-09 4.4E-14 2.5E-08
218-01-9 ~Chrysene 0.411 0.411 0.411 1.3E-10 6.9E-11 3.4E-16 1.9E-10
206-44-0 ~Fluoranthene 0.718 0.718 0.718 1.5E-05 8.5E-06 2.4E-05
129-00-0 ~Pyrene 0.654 0.654 0.654 1.9E-05 1.0E-05 2.9E-05
7782-49-2 Selenium 0.342 0.342 0.342 5.9E-05 6.6E-11 5.9E-05
Cumulative: 1.6E-06 1.2E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID: 24003-20-060
Exposure Unit ID: hypothetical worst-case final grade soil
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.037 0.037 0.037 1.1E-07 1.1E-07
7440-38-2 Arsenic, Inorganic 3.02 3.02 3.02 1.1E-07 1.8E-08 4.0E-08 1.7E-07 1.8E-02 2.9E-03 4.5E-02 6.6E-02
7440-39-3 Barium 109 109 109 1.6E-03 4.9E-03 6.5E-03
7440-43-9 Cadmium (Diet) 0.256 0.256 0.256 1.4E-09 1.4E-09 1.5E-03 1.9E-04 5.8E-03 7.5E-03
75-15-0 Carbon Disulfide 0.0009 0.0009 0.0009 2.7E-08 1.2E-06 1.2E-06
16065-83-1 Chromium(III), Insoluble Salts 59.7 59.7 59.7 1.2E-04 2.7E-03 2.8E-03
18540-29-9 Chromium(VI) 2.7 2.7 2.7 5.4E-08 7.0E-07 7.5E-07 1.6E-03 2.0E-03 3.6E-03
7439-92-1 ~Lead and Compounds 59.1 59.1 59.1 <SL** <SL** <SL**7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.0819 0.0819 0.0819 1.2E-04 6.1E-05 1.8E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone) 0.004 0.004 0.004 5.9E-09 3.5E-07 3.5E-07
75-09-2 Methylene Chloride 0.001 0.001 0.001 8.1E-14 6.6E-14 1.5E-13 4.9E-08 4.7E-07 5.1E-07
56-55-3 ~Benz[a]anthracene 0.315 0.315 0.315 1.3E-09 5.3E-10 1.2E-10 1.9E-09
50-32-8 ~Benzo[a]pyrene 0.29 0.29 0.29 1.2E-08 4.9E-09 5.4E-10 1.7E-08 2.8E-03 1.2E-03 3.3E-02 3.7E-02
205-99-2 ~Benzo[b]fluoranthene 0.535 0.535 0.535 2.2E-09 9.0E-10 9.9E-11 3.2E-09
218-01-9 ~Chrysene 0.411 0.411 0.411 1.7E-11 6.9E-12 7.6E-13 2.4E-11
206-44-0 ~Fluoranthene 0.718 0.718 0.718 2.1E-05 8.8E-06 3.0E-05
129-00-0 ~Pyrene 0.654 0.654 0.654 6.4E-06 2.7E-06 9.1E-06
7782-49-2 Selenium 0.342 0.342 0.342 2.0E-04 3.8E-06 2.1E-04
Cumulative: 9.4E-07 1.2E-01
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800 mg/kg
for commercial/industrial soil.
North Carolina DEQ Risk Calculator