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HomeMy WebLinkAbout06001_Alamac American_GWMR_20200124Draper Aden Associates V Engineering • Surveying • Environmental Services 114 Edinburgh South Drive Suite 200 Cary, North Caroiina 27511 919.827.0864 www.daa.com January 24, 2020 Mr. Kelly Johnson, LG Via email to: kelly.*ohnson@ncdenr.gov North Carolina Brownfields Program NC Department of Environmental Quality 1646 Mail Service Center Raleigh, NC 27699-1646 RE: Lumberton Energy Holdings, LLC (former Alamac American Knits Site) Transmittal of Annual Groundwater Report and Request to Increase Interval between Groundwater Sampling Events 188S Alamac Road, Lumberton, Robeson County; BF#06001-02-048 Draper Aden Associates Project No.19080294-010103 Dear Mr. Johnson: Draper Aden Associates (DAA) is pleased to submit the attached annual groundwater monitoring report on behalf of the new owner of the facility, Lumberton Energy Holdings LLC (LEH) for the above - referenced site. This work was completed in accordance with the requirements of the March 2006 brownfields agreement (BFA). Paragraph 16 of the BFA states that for three years the Prospective Developer shall sample water from the residential water supply well located at 2237 Alamac Road. Following three years of sampling, DENR or its successor in function (DEQ) shall determine, what if any, ongoing or additional sampling is required. Paragraph 17 of the BFA lists five monitoring wells and three recovery wells and states that after the first two years of operation, DENR or its successor in function shall determine what, if any, ongoing or additional groundwater monitoring is required. On September 18, 2008, Ms. Lisa Taber of the NCBP agreed to allow Alamac to discontinue the sampling of five monitoring wells during the annual sampling event. Since 2006, the three recovery wells and one water supply well located on the private property that the owner uses for irrigation, have been sampled annually. No constituents associated with the former Alamac groundwater contaminant plume have been detected in the private water supply well in the 14 years of sampling (see Table 3-2 of the attached report). Blacksburg • Charlottesville • Manassas • Newport News • Richmond • Vrginia Beach Fayetteville • Raleigh Mr. Kelly Johnson, LG January 24, 2020 Page 2 of 3 LEH understands the need to operate the pump & treat (P&T) system based on the contaminant concentrations still being removed by the three recovery wells. LEH would like to ask the NCBP to consider their request to continue to operate the pump & treat system but decrease the sampling/reporting of the recovery wells to every four years and the private water supply well to every two years. AERP will maintain the P&T system and repair/replace malfunctioning pumps in the three recovery wells as quickly as possible. The rationale for LEH's request to reduce the well sampling frequency is as follows: The above ground storage tank and ancillary piping for tetrachloroethene (PCE) for the dry- cleaning machine was used at the site between 1978 and 1997. Contamination was discovered during due diligence activities conducted in 1997. Except for the aerosol silicon release agent that contained PCE used by a tenant of Alamac for a short period of time prior to the January 2005 indoor air sampling event, PCE and other chlorinated solvents have not been used at the site since 1997. 2. The remediation of the PCE-contaminated soil through excavation and treatment occurred in 1999 along with enhanced in situ groundwater bioremediation. The currently operating P&T system for groundwater containment/remediation was initiated in 1999. 3. The 2019 calculated mass removal of contaminants from groundwater associated with the three recovery wells indicates the P&T system continues to be effective in removing groundwater contaminants at the site. 4. In 14 years, no contaminants associated with the groundwater contaminant plume have been detected in the groundwater samples collected from the private water supply well (WSW) located at 2237 Alamac Road, approximately 750 feet south of the main manufacturing building. The residence is connected to the municipal water supply but uses well water for irrigation. Jacob's Branch, a perennial stream and possible groundwater divide lies between the site and this residential property. With 14 years of annual sampling data and LEH's commitment to continue the operation of the P&T system, please consider their request to modify the current annual schedule of groundwater sampling and reporting. If approved, LEH would schedule the next sampling/reporting of the residential well in December 2021 and the recovery well sampling/reporting event in December 2023. If approved, LEH will notify the owner of the property of 2237 Alamac Road of this change in sampling schedule. Finally, DAA has been emailing a copy of the annual report to Sean Boyles of the Inactive Hazardous Sites Branch (IHSB) in the Fayetteville Regional office each year. Because Mr. Boyles is no longer listed Transmittal of December 2019 Annual Groundwater Monitoring Report Request to Increase Interval Between Groundwater Sampling Events Lumberton Energy Holdings (Former Alamac) Site Lumberton, North Carolina Mr. Kelly Johnson, LG January 24, 2019 Page 3 of 3 on the IHSB contact list, we are transmitting this report to Mr. John Walch, the Eastern Regional supervisor for the so he can forward this report to the correct person. Sincerely, Draper Aden Associates Daphne M. Jones, LG Senior Geologist, Project Manager Attachment: 2019 Annual Groundwater Monitoring Report ec: John Walch, john.walch@ncdenr.gov Antonio Esposito antonio.esposito@aegplc.com Doris Sampson doris.sampson@aegplc.com Chuck Pakala cvpakala@carolina.rr.com Doris Sampson doris.sampson@aegplc.com Transmittal of December 2019 Annual Groundwater Monitoring Report Request to Increase Interval Between Groundwater Sampling Events Lumberton Energy Holdings (Former Alamac) Site Lumberton, North Carolina 2019 ANNUAL GROUNDWATER MONITORING REPORT LUMBERTON ENERGY HOLDINGS, LLC (FORMER ALAMAC AMERICAN KNITS SITE) 1885 ALAMAC ROAD, LUMBERTON ROBESON COUNTY, NORTH CAROLINA 28359 BROWNFIELDS NO. 06001-02-78 Groundwater Incident No. 18926 Latitude 34°35'19.84" N Longitude 79°00'22.35" W Prepared for: Active Energy Renewable Power, LLC 1885 Alamac Road (P.O. Box 1347) Lumberton, North Carolina 28359 Prepared by: Draper Aden Associates 114 Edinburgh South Drive Cary, NC 27511 Phone: 919-827-0864 www.daa.com Draper Aden Project No. 19080294-010103 January 24, 2020 N O i+ Sc�AL 229❑ Sean Jarvah Environmental Specialist i Daphne M. Jones, LG Senior Geologist/Project Manager 3RD PARTY REVIEW This Report has been subjected to technical and quality reviews by: faa SeanJarvah 1/09/2020 Name: Printed Signature Date Project Manager Daphne Jones 1/16/2020 Name: Printed Signature Date Sr. Reviewer Jim Hurley 1/10/2020 Name: Printed Signature Date Quality Reviewer 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 TABLE OF CONTENTS 1.0 INTRODUCTION............................................................................................................................... 1 2.0 BACKGROUND................................................................................................................................. 2 3.0 ENVIRONMENTAL MONITORING.................................................................................................. 3 3.1 Groundwater Sampling Methods.......................................................................................................................3 3.2 Groundwater Results..............................................................................................................................................3 3.2.1 Biogeochemical Parameters.................................................................................................................3 3.2.2 Volatile Organic Compounds in Recovery Wells.......................................................................... 3 3.2.3 Discussion of Groundwater Results................................................................................................... 5 3.3 Residential Water Supply Well............................................................................................................................6 4.0 GROUNDWATER RECOVERY SYSTEM OPERATION & MAINTENANCE ...................................... 8 4.1 Hydraulic Performance...........................................................................................................................................8 4.2 Volatile Organic Compound Removal and Disposal..................................................................................9 5.0 CONCLUSIONS............................................................................................................................... 11 6.0 REFERENCES................................................................................................................................... 12 TABLES Table 3-1 Historical Summary of Selected Bio-Geochemical Parameters in Groundwater Table 3-2 Historical Summary of Volatile Organic Compounds in Groundwater from Recovery Wells Table 4-1 Operational Data Summary for Groundwater Recovery Wells Table 4-2 Calculation of Mass of Volatile Organic Compounds Removed from Groundwater by the Recovery Well Network Table 4-3 Historical Summary of Volatile Organic Compounds in On -Site Wastewater Treatment Plant Effluent 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 i FIGURES Figure 1 Site Location Figure 2 Facility Layout and Groundwater Sampling Locations Figure 3 Performance Monitoring in RW-1 Figure 4 Performance Monitoring in RW-2 Figure 5 Performance Monitoring in RW-3 APPENDICES Appendix A Field Notes Appendix B Laboratory Analytical Reports Appendix C Monthly Recovery Well Flow Reports 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 1.0 INTRODUCTION Draper Aden Associates (DAA), formerly Solutions-IES a division of DAA, prepared this 2079 Annual Groundwater Monitoring Report for the North Carolina Department of Environmental Quality (NCDEQ), Division of Waste Management (DWM), Brownfields Program (NCBP), on behalf of Lumberton Energy Holdings, LLC (LEH), located in Lumberton, North Carolina. LEH is the current owner of the former Alamac American Knits LLC (Alamac) site. Except in the references, we are using DAA throughout this report instead of differentiating between the three entities that worked at this site. Alamac is used when referring to activities performed prior to the sale of the site to LEH or in reference to former Alamac personnel who continue to maintain operation of their groundwater extraction and treatment system. This is the 14t" annual report prepared in accordance with the Brownfields Agreement (BFA) entered into by the NCDEQ and Alamac on February 24, 2006 (BF# 06001-02-78). 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 1 The former Alamac textile manufacturing facility is located in Lumberton, Robeson County, North Carolina (Figure 1). Figure 2 provides the current facility layout with groundwater sampling locations. Until the December 2006 Groundwater Monitoring Report, DAA prepared previous reports in accordance with the Water Quality Monitoring Plan (WQMP) originally submitted to the NCDEQ Division of Water Quality, Aquifer Protection Section, Fayetteville Regional Office, approved on August 16, 1999 and modified January 29, 2001. Based on the requirements of the WQMP, Alamac conducted quarterly sampling and semi-annual reporting through the first quarter of 2004. On June 7, 2004, DEQ reduced quarterly to annual sampling and reporting. Sampling and reporting proceeded under these guidelines until the approval of the BFA in February 2006. On September 18, 2008, Ms. Lisa Taber of the NCBP agreed to reduce the number of wells being sampled by eliminating the requirement to collect samples from source area wells MW-1, MW-11 and MW-15, downgradient well MW-23, and offsite well MW-19 (Figure 2). The remaining monitoring program consists of sampling and analysis of the three recovery wells (RW-1, RW-2 and RW-3) and one offsite residential water supply well at 2237 Alamac Road, located approximately 750 feet south of the LEH manufacturing building. Hurricane Matthew caused severe damage to the former Alamac facility in 2016. As a result, all manufacturing and most of shipping operations ceased. Although manufacturing operations ceased in July 2017, the former Alamac facility operated on a skeleton crew pending the distribution of the manufacturing goods currently in stock. The plant was subsequently affected by two hurricanes in 2018 (Hurricane Michael and Hurricane Florence). Although Alamac has continued to maintain operation of their groundwater extraction and treatment system, the property was sold to LEH, a subsidiary of Active Energy Group PLC, a London listed renewable energy company in 2019. As the current owner LEH has taken over requirements associated with maintaining the protections of the Brownfields agreement. This 2079 Annual Groundwater Monitoring Report includes the monitoring activities conducted during the annual groundwater sampling event completed on December 05, 2019. 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 3.0 ENVIRONMENTAL MONITORING 3.1 Groundwater Sampling Methods The groundwater sampling protocol for the December 2019 event included sampling the three recovery wells (RW-1, RW-2 and RW-3) for volatile organic compounds (VOCs) and bio-geochemical parameters' and the water supply well located at 2237 Alamac Road for VOCs. DAA collected samples directly from sampling ports located on the former treatment system pad for recovery wells RW-1, RW-2 and RW-3. DAA collected the sample from 2237 Alamac Road directly from the water stream after letting the faucet run for approximately 15 minutes. DAA personnel measured the temperature, pH, specific conductivity, oxidation-reduction potential (ORP) and dissolved oxygen (DO) in the field (see Field Notes in Appendix A). DAA collected the samples in laboratory -supplied glassware, packaged and shipped under chain -of -custody control to Waypoint Analytical (formerly Prism Laboratories, Inc.) in Charlotte, NC, NCDEQ Certification #402 to analyze for VOCs by EPA Method 8260B. 3.2 Groundwater Results 3.2.1 Biogeochemical Parameters Field parameters recorded during the December 2019 sampling event are consistent with historical values summarized in the historical groundwater bio-geochemical parameter data for recovery wells RW-1, RW-2, and RW-3 (Table 3-1). The current data indicates a continuing reducing environment, which assists with the remediation process, aided by the groundwater extraction system. 3.2.2 Volatile Organic Compounds in Recovery Wells Table 3-2 provides a summary of the historical VOC data, including the December 2019 samples. The laboratory analytical report is included as Appendix B. Graphs depicting the historical concentrations of tetrachloroethene (PCE), trichloroethene (TCE), cis-1,2-dichloroethene (cis-1,2-DCE), vinyl chloride (VC) and total VOCs in the recovery wells are provided in Figures 3, 4 and 5. Increases and decreases Bio-geochemical parameter analysis includes field measurements of temperature, pH, conductivity, oxidation- reduction potential (ORP) and dissolved oxygen (DO). 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 3 of PCE, TCE, cis-1,2-DCE and VC in the recovery wells can result from a combination of different factors simultaneously influencing concentrations. Anaerobic reductive dechlorination of PCE sequentially results in the formation of TCE, then cis-1,2-DCE from degradation of TCE, and then VC from the breakdown of cis-1,2-DCE. These transformations appear as increases followed by decreases in concentrations over time, eventually leading to cleanup as long as groundwater conditions remain conducive to biological activity. Additionally, recovery wells physically remove contaminant mass independent of biodegradation. The drawdown around each well continues to capture new contaminants into the well that the remediation system will then process. The increase seen is the result of the physical capture of the contaminant, not biotransformation. The PCE and TCE concentrations in RW-1 have continued to slowly increase over time and continues to be several orders of magnitude above the NC 2L Standards since system startup in 1999 (Table 3-2). In 2015, DAA reported PCE and TCE concentrations below their respective laboratory analytical method detection limits. Based on the recent data, it seems that the abrupt decrease in chlorinated VOC (cVOC) concentrations in RW-1 in 2015 was an anomaly, likely a result of faulty pump operation and being off- line between April and December 2015. In November 2017, the PCE, TCE, cis-1,2-DCE and vinyl chloride concentrations in RW-1 increased to the highest level since system startup. During the 2019 reporting season, the pump in RW-1 was offline from July 13th through December 4t". Similar to 2015, all historically reported VOC concentrations are approximately 75% lower than historical averages. Although there was a significant decrease in reported concentrations, all exceedances in RW-1 are still between one and three orders of magnitude higher than their respective NC 2L standard. Naphthalene was reported at an estimated concentration of 3.3 pg/L, which is below its NC 2L standard of 6 pg/L. Naphthalene has been reported above NC 2L standard since 2016 and was thought to be an increasing trend. Continuous operation of the remediation pump should help to evaluate any trends in naphthalene concentrations. All reported VOC's in RW-2 have decreased in concentration since the beginning of pumping, with fluctuations along the way. Since pumping began in 1999, the reported concentrations of PCE and TCE decreased by over 95%. Both PCE and TCE are at their second -lowest historical concentrations since November 2006. Additionally, VC concentration also decreased to their second lowest concentrations 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 4 since sampling began, the lowest concentration of VC in RW-2 occurred in 2018. Future events will clarify if there is a significant trend in VC degradation. Naphthalene concentrations were also lower in 2019 and appear to be part of a reducing trend in groundwater collected from RW-2. Naphthalene exceeded the NC 2L standard for the past three sampling events prior to 2019. PCE and TCE have decreased by close to 98% and VC by 90% in RW-2 since pumping began in 1999. Since 2001, RW-3 (located approximately 100 ft downgradient of the primary PCE release area), has reported between 5.6 and 16 pg/L TCE, with a current concentration being the upper limit at 16 pg/L. RW-3 has shown a slow but steady decline in cis-1,2-DCE concentrations from 1999 to 2009. Although there has been a 72% decrease in cis-1,2-DCE since 2000, concentrations seemed relatively stable from 2008 to 2019. The 2019 result for cis-1,2-DCE (1,800 pg/L) was the highest reported since November 2004. Vinyl chloride concentrations have also increased in 2019, with a current concentration of 240 pg/L, which is the highest reported concentration of VC since 2011. This increase is likely as a result of anaerobic reductive dechlorination of the chlorinated contaminants, breaking down to VC. VC concentrations have ranged from 94 pg/L to 290 pg/L since 2005 and significantly exceed the NC 2L standard of 0.03 pg/L. 3.2.3 Discussion of Groundwater Results The continuing presence of elevated concentrations of cis-1,2-DCE and VC in all three recovery wells suggests that at least a portion of the observed PCE and TCE reductions are a result of biodegradation via anaerobic reductive dechlorination. Although the biogeochemical conditions in the immediate vicinity of the pumping wells are not optimal for enhanced reductive dechlorination (i.e., elevated DO, mildly reducing ORP, and acidic pH), the data suggest that aquifer conditions away from active pumping may support modest bioactivity. ♦ In RW-1, the historic concentrations of cis-1,2-DCE have increased gradually since pumping began in 1999. DAA believes the large decrease in 2015 and 2019 were related to the pump malfunctions, which occurred during much of 2015 and this reporting period. ♦ Since pumping of recovery well RW-2 began in 1999, cis-1,2-DCE concentrations have decreased close to 78% from the 1999 concentration of 31,000 pg/L. Concentrations have remained relatively stable since 2014, ranging from 6,300 pg/L to 8,200 pg/L with the current cis-1,2-DCE levels in RW-2 were reported at 7,100 pg/L, which is the third lowest concentration of DCE since sampling began. 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 ♦ RW-3 showed steady decline in cis-1,2-DCE concentrations from 2000 through 2008, but has remained relatively stable since 2008. The current concentration of cis-1,2-DCE (1,800 pg/L) in RW-3 remains above the NC 2L Standard of 70 pg/L. This is also true for RW-1 and RW-2. VC also remains elevated in each of the recovery wells. The reported concentration of VC in recovery well RW-1 has remained stable from the beginning of pumping through 2018 but decreased sharply in 2015 and again in 2019 compared to historical range of concentrations. As with cis-1,2-DCE, it is likely that the large decrease is an artifact of the pump malfunction. The continued presence of VC in recovery well RW-2 suggests complete reductive dechlorination may be occurring. The reported VC concentration in RW-2 is at its second lowest concentration since 1999 (310 pg/L) but appears to be part of an overall stable VC trend. VC concentrations in RW-3 have decreased 78% between 2000 and 2019. The average concentration over the past 10 years is approximately 175 pg/L. Current concentrations of VC in all three wells remain several orders of magnitude above the NC 2L Standard of 0.03 pg/L. The sub -optimal removal of these biodegradation daughter products may be a result of several factors including: 1) groundwater pH is below the optimal range (pH range of 6.0-8.0) for enhanced reductive dechlorination; 2) elevated DO which limits anaerobic metabolism; 3) absence of the appropriate microflora in the aquifer to carry out these reactions; or 4) insufficient bioavailable organic carbon to sustain bioactivity. 3.3 Residential Water Supply Well On December 5, 2019, DAA sampled the water supply well located at 2237 Alamac Road. The field staff opened the spigot closest to the well house allowing the water to flow for approximately 15 minutes. According to the property owner, municipal water connects to the residence, while water from the supply well is used for irrigation. DAA measured and recorded the bio-geochemical parameters in the field book, then collected the water sample directly into laboratory -supplied containers and placed them in on ice in coolers. DAA then shipped the coolers using standard chain -of -custody protocol to Waypoint Analytical for analysis. Prism analyzed the submitted samples for VOCs by EPA Method 8260B. 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 6 The laboratory analytical results of the groundwater sample collected from the water supply well located at 2237 Alamac Road indicated that both acetone (13 pg/L), 2-butanone (12 pg/L), chloroform (0.23 J pg/L) and methylene chloride (0.50 J pg/L) were present but did not exceed their respective NC 2L standards. The ketone compounds are common laboratory contaminants (U.S. Environmental Protection Agency, 1999) and chloroform is a disinfectant byproduct that has been detected in this water supply well previously. Table 3.2 provides a summary of the current and historical water supply well analytical results, and a copy of the laboratory analytical report and chain -of -custody record is located in Appendix B. 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 7 4.0 GROUNDWATER RECOVERY SYSTEM OPERATION & MAINTENANCE 4.1 Hydraulic Performance Except for RW-1 being offline for five months during the reporting period, the groundwater recovery system operated with minimal interruption during 2019. Alamac reported a malfunction in RW-1 on July 13t". The pump was repaired and returned to service on December 4t". Alamac plant personnel periodically inspected the three recovery wells that comprise the groundwater extraction system in 2019 and recorded system performance measurements including the pumping rate and the cumulative volume of groundwater recovered from each well. Monthly reporting sheets are included in Appendix C. Table 4-1 provides a summary of the historical and current operational data through December 2019. Alamac personnel periodically had to reset or replace the integrator on RW-1. Since 2012, DAA used the readings from the RW-1 flowmeter to calculate the volume removed in each period, which they add to the cumulative volume totals. Due to a meter replacement for RW-2, DAA added the previous flow meter reading of 11,484,819 gallons to each monthly totalizer reading for the 2018 and 2019 reporting period to calculate the cumulative volume for all recovery wells. Extraction flow rates during 2019 were recorded in two ways: (1) from instantaneous flow rate readings from meters assigned to each recovery well, and (2) by dividing the totalizer flow meter reading for each well by the number of days (converted to minutes) of operation (i.e., average annual flow rate). As shown in Table 4-1, during the 2019, the average instantaneous flow rate for RW-1 was 1.64 gallons per minute (gpm); the average instantaneous flow rate in extraction well RW-2 was calculated to be 2.70 gpm; and the average instantaneous flow rate from extraction well RW-3 was 5.05 gpm. From startup in 1999 through December 5, 2019, approximately 112.10 million gallons of groundwater have been extracted, treated in the on -site wastewater treatment plant (WWTP), and discharged through a permitted NPDES point. This total volume includes approximately 4.20 million gallons extracted in 2019, which is a 0.84 million gallon decrease from the total volume extracted in 2018. The total recovery amount is typically higher. Reduced recovery was a result of RW-1 being off-line for five months during the reporting period. The average instantaneous flow rate for all three recovery wells during 2019 was 9.39, down from 11.28 gpm in 2018 gpm. The instantaneous and average annual 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 8 recovery rates at the recovery wells in 2019 are similar to those recorded in preceding years, indicating consistent operation throughout the reporting period. 4.2 Volatile Organic Compound Removal and Disposal To estimate the mass of VOCs removed from groundwater via the recovery system, the volume of water extracted from each well during the reporting period was multiplied by the concentration of total VOCs in the groundwater recovered from the well on the sampling date. During the 2019 reporting period from December 4, 2018 through December 5, 2019 (based on sampling dates), a total of approximately 117 pounds (Ibs) of VOCs were removed from the groundwater (Table 4-2). This is a 34% decrease from the previous year. Individually, since pumping began, RW-1 has collected and discharged 1,199 Ibs; RW-2 has collected and discharged 1,730 Ibs and, RW-3 has extracted and discharged 1,644 Ibs of VOCs. Altogether since pumping began on November 8, 1999, a conservative estimate of approximately 4,574 Ibs of VOCs have been removed from the treatment area via the recovery well network. Figures 3b, 4b and 5b plot the mass of cVOCs removed each year from RW-1, RW-2 and RW-3, respectively, and the cumulative total mass removed by each well since startup. The data in Tables 3-2 and 4-1 indicate that the decreased cVOCs and lower extraction rates in RW-1 in 2019 (from 1.77 gpm in 2018 to 1.64 gpm in 2019) resulted in decreased removal of cVOCs. As mentioned, this is due to do RW-1 being out of service for approximately five months. RW-2 has continued to extract groundwater at pumping rate of 0.92 to 3.65 gpm since pumping began, with an average of 2.70 gpm during 2019. In RW-2, the effectiveness of the mass removal of cVOCs has remained steady. RW-3 has continued to extract groundwater at a pumping rate from approximately 2.6 to 9.97 gpm since pumping began and had an average of 5.05 gpm during this reporting period. The higher pumping rate in RW-3 has resulted in effective extraction of contaminant mass from this well even though the total cVOC concentration in the groundwater pumped from it is historically much lower than in RW-1 and RW-2. During the 2019 reporting period, RW-3 showed the only increase in contaminated mass removal when compared to the previous reporting period (Table 4-2). 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 The groundwater pumped from the three recovery wells discharges directly to the on -site wastewater treatment plant (WWTP). AEGP operates the WWTP under a National Pollutant Discharge Elimination System (NPDES) permit and monitors the effluent quality at the outfall in accordance with the permit. Alamac collected and analyzed effluent samples that discharge to the outfall since 1999, even though it was not required by the WQMP or under the current BFA. Alamac provided DAA with the wastewater analyses provided by Microbac Laboratory in Fayetteville, NC on samples collected on March 12, June 25, September 24 and December 5, 2019. No PCE, TCE, cis-1,2-DCE or VC was detected in the WWTP effluent during the four quarterly sampling events (Table 4-3). See Appendix B for copies of Microbac's analytical reports for the WWTP effluent reporting period. 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 10 5.0 CONCLUSIONS The groundwater recovery and discharge system is the only active remediation approach in the source area. Natural attenuation is also likely occurring to some degree. The pumping regimen continues to effectively capture and remove contamination from the aquifer. During the 2019 reporting period, total VOC removal was the second lowest total since 2004. The average removed per period since 2004 is 188 per period. The system removed approximately 117 pounds during 2019. RW-1 removed a total of 16 Ibs of VOCs during this reporting period (77% decrease). In RW-2, a decrease in total VOCs continues slowly, likely a result of the combination of some in situ bioactivity and physical extraction by pumping, but concentrations of the target VOCs remain far above the NC 2L standards. Pumping RW-2 in 2019 removed approximately 55 Ibs of VOCs (12% decrease). Concentrations of chlorinated solvents remained stable in RW-3 since 2009. PCE and TCE concentrations in this well are already close to the target NC 2L standards, but cis-1,2-DCE and VC remain elevated. This well extracted approximately 46 Ibs of VOCs from groundwater in 2019 (3% increase). The increase in performance of RW-3 was due to a higher concentration of total VOCs reported when compared to the previous reporting period. Based on the volume of groundwater extracted and the concentrations measured in the recovered water over time, it has been estimated that the recovery system has removed approximately 4,574 Ibs of VOCs since it began operation November 1999. Combined with the removal of an estimated 732 Ibs of VOCs via other remediation activities that were implemented previously (Ref. 2), the total amount of VOCs removed from the site is calculated to be approximately 5,306 lbs. 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 11 6.0 REFERENCES 1. Proposed Remedial Action Report, S&ME, Inc., April 1999. 2. Report of Excavation and Disposal of PCE-Contaminated Soil, Soil Solutions, Inc., April 1999. 3. Water Quality Monitoring Plan, S&ME, Inc., July 1999. 4. Injection Well Permit Application, S&ME, Inc., September 29, 1999. 5. Groundwater Monitoring Report, S&ME, Inc., March 28, 2000; September 5, 2000; February 2, 2001. 6. Evaluation Report for Injection of Liquid Soybean Oil, S&ME, Inc., March 21, 2001. 7. Groundwater Monitoring Report, Solutions-IES, June 2001; January 2002; June 2002; January 2003; June 2003; January 2004; January 2005; January 2006. 8. Brownfields Agreement between NCDEQ and Alamac American Knits, LLC, February 24, 2006. 9. Groundwater Monitoring Report, Solutions-IES, January 2007; January 2008; January 2009; January 2010; January 2011; January 2012; January 2013; January 2014; January 2015; January 2016. 10. Groundwater Monitoring Report, SIES/DAA January 2017, January 2018. 11. Groundwater Monitoring Report, DAA January 2019 11. U.S. Environmental Protection Agency, 1999a, Data validation standard operating procedures for contact laboratory program routine analytical services (rev. 2.1): Athens, Ga., U.S. Environmental Protection Agency, Region IV, 32 p. 2019 Annual Groundwater Monitoring Report Lumberton Energy Holdings LLC (Former Alamac Site) Lumberton, NC Draper Aden Project No. 19080294-010103 January 24, 2020 12 TABLES TABLE 3-1 HISTORICAL SUMMARY OF SELECTED BIO-GEOCHEMICAL PARAMETERS IN GROUNDWATER LUMBERTON ENERGY HOLDINGS, LLC (FORMER ALAMAC AMERICAN KNITS SITE) LUMBERTON, NORTH CAROLINA DAA PROJECT NO: 19080294 Well ID Sampling Date Daysafter PH (SU) DO ( g/L) ORP (mv) Specific Conductance (VS/cm) Recovery Wells RW-1 11/03/99 -5 5.8 0.40 5 NA 11/08/99 0 Startup 10/24/00 351 NA 0.23 NA NA 11/14/01 737 6.7 1.21 <-100 203 11/13/02 1101 5.7 1.30 -56 230 11/03/03 1456 5.9 1.19 25 134 11 /01 /04 1820 5.5 1.14 18 108 10/25/05 2178 5.0 1.10 -5 212 11/28/06 2577 5.4 1.51 -178 91 10/25/07 2908 5.5 3.32 53 117 11/06/08 3286 4.9 4.96 38 129 10/30/09 3644 5.8 5.18 13 96 11/02/10 4012 5.0 5.11 -36 171 11/01/11 4376 5.2 3.67 196 151 11/02/12 4743 4.9 3.72 96 70 11/06/13 5112 5.3 2.01 38 116 12/09/14 5510 5.0 3.96 100 76 11/11/15 5847 5.9 0.51 -68 77 11/03/16 6205 5.8 0.68 -25 75 11/27/17 6594 5.6 0.81 -46 163 12/04/18 6966 5.1 0.90 -36 155 12/05/19 7332 5.5 1.09 -113 178 RW-2 11/03/99 -5 5.2 0.26 0 NA 11/08/99 0 Startup 10/24/00 351 NA 0.78 NA NA 11/14/01 737 6.4 1.40 -60 343 11/13/02 1101 5.6 1.26 -42 330 11/03/03 1456 5.8 1.23 20 346 11/01/04 1820 5.3 1.23 0.2 355 10/25/05 2178 5.4 1.48 -74 265 11/28/06 2577 5.8 1.78 -199 207 10/25/07 2908 5.3 5.73 39 237 11/06/08 3286 5.1 2.15 38 194 10/30/09 3644 6.0 6.32 -16 222 11/02/10 4012 5.5 6.20 -67 254 11/01/11 4376 5.3 4.98 183 165 11/02/12 4743 5.2 1 3.68 50 160 11/06/13 5112 5.7 2.39 27 197 12/09/14 5510 5.4 2.86 43 206 11/10/15 5846 5.6 2.44 -50 209 11/03/16 6205 5.6 1.61 -33 198 11/27/17 6594 5.9 1.17 -79 219 12/04/18 6966 5.6 0.89 -27 166 12/05/19 7332 5.9 0.93 -72 137 Page 1 of 2 TABLE 3-1 HISTORICAL SUMMARY OF SELECTED BIO-GEOCHEMICAL PARAMETERS IN GROUNDWATER LUMBERTON ENERGY HOLDINGS, LLC (FORMER ALAMAC AMERICAN KNITS SITE) LUMBERTON, NORTH CAROLINA DAA PROJECT NO: 19080294 Well ID Sampling Date Daysafter PH (SU) DO ( g/L) ORP (mv) Specific Conductance (PS/cm) Recovery Well RW-3 11/03/99 -5 5.2 5.22 40 NA 11/08/99 0 Startup 10/24/00 351 NA 1.98 NA NA 11/14/01 737 6.6 1.71 -82 125 11/13/02 1101 5.5 1.27 -43 120 11/03/03 1456 5.6 1.26 52 96 11/01/04 1820 5.5 1.10 -1 118 10/25/05 2178 5.3 2.41 42 120 11/28/06 2577 5.6 2.62 -197 91 10/25/07 2908 5.4 3.24 34 105 11/06/08 3286 5.5 4.73 68 118 10/30/09 3644 6.0 5.08 38 110 11/02/10 4012 5.6 5.20 -40 119 11/01/11 4376 5.4 5.01 184 107 11/02/12 4743 5.2 3.81 106 75 11/06/13 5112 5.6 2.71 43 112 12/09/14 5510 5.8 2.68 61 121 11/10/15 5846 5.7 2.00 -87 112 11/03/16 6205 6.0 1.41 -68 115 11/27/17 6594 6.0 1.34 -66 103 12/04/18 6966 5.7 0.70 -52 100 12/05/19 1 7332 1 5.9 1 0.85 1 -86 1 97 Residential Water Supply Well 2237 Alamac Rd 11/28/06 0) a Q z 1 6.0 0.16 -137 82 10/25/07 5.7 0.52 109 107 11/6/08 5.5 3.93 157 105 10/30/09 5.6 1.85 118 119 1112110 5.2 4.04 28 98 11/1/11 4.6 5.29 252 169 1112112 4.2 3.40 240 156 11/6/13 5.3 4.24 103 85 12/9/14 5.5 4.10 169 142 11/10/15 5.4 1 4.10 59 96 11/3/16 5.5 6.51 173 181 11/27/17 5.6 1.20 78 112 12/4/18 5.4 2.40 108 95 12/5/19 5.6 3.56 1 20 1 117 Notes: NA = Not analyzed Days after startup = number of days groundwater recovery system has been in operation since system was started on November 8, 1999. SU - Standard Units mg/L = milligrams per liter my = millivolts pS/cm = microSiemens per centimeter Page 2 of 2 TABLE 3-2 HISTORICAL SUMMARY OF VOLATILE ORGANIC COMPOUNDS IN GROUNDWATER FROM RECOVERY WELLS LUMBERTON ENERGY HOLDINGS, LLC (FORMER ALAMAC AMERICAN KNITS SITE) LUMBERTON, NORTH CAROLINA DAA PROJECT NO: 19080294 Well ID Sample Date Days after Startup Tetrachloroethene (N9/L) Trichloroethene (N9/L) 1,1,1- Trichloroethane (Pg/L) 1,1,2- Trichloroethane (N9/L) 1,1- Dichloroethane (p9/L) 1,1- Dichloroethene (Pg/L) cis-1,2- Dichloroethene (N9/L) trans-1,2- Dichloroethene (Pg/L) Vinyl Chloride (N9/L) Toluene (N9/L) Naphthalene (N9/L) Other VOCs (Ng/L) TOTAL VOCs (ug/L) 15A NCAC 2L Standards 0.70 3.0 200 Not listed 6* 350*** 70 100 0.03** 600 6 Compound Specific 11/03/99 -5 15 170 <5 <5 32 7.4 2,000 32 200 <5 15 Benzene (8.0) 2,479 10/24/00 351 360 1,300 <5 <5 17 <5 4,800 66 200 26 160 Benzene (12) 6,945 11/14/01 737 200 840 8.3 <5 14 6.7 3,200 12 70 <5 83 BDL 4,434 11/13/02 1101 210 820 16 <5 7.3 6.4 3,800 15 130 <5 47 1,2-Dichloropropane (61) 5,113 11/3/03 1456 180 750 <5 <5 <5 7.8 4,000 11 130 <5 26 BDL 5,105 11/01/04 1820 270 800 <5 <5 <5 8.3 4,200 37 170 <5 <5 BDL 5,485 10/25/05 2178 380 790 <5 <5 <5 11 3,700 21 160 <5 31 BDL 5,093 11/28/06 2577 560 1,100 <10 <10 <10 <10 4,600 8.7 J 180 <10 <10 BDL 6,449 10/25/07 2908 470 1,400 <10 <10 5.1 J 5.2 J 3,100 19 J 200 <10 <10 BDL 5,199 11/06/08 3286 600 860 <10 <10 7.2 J 10 5,200 32 180 <10 <10 BDL 6,889 RW-1 10/30/09 3644 460 960 <10 <10 6.7 J 8.6 J 5,500 34 200 <10 9.6 J BDL 7,179 11/02/10 4012 470 1,100 <100 <100 <100 <100 5,600 <100 120J <100 <100 BDL 7,290 11/01/11 4376 180 480 <100 <100 <100 <100 5,100 <200 170J <100 <100 BDL 5,930 11/02/12 4743 970 1,500 <100 <100 <100 <100 5,900 <200 170J <100 <100 BDL 8,540 11/06/13 5112 1,500 2,400 <100 <100 <100 <100 6,900 51 J 220 <100 <100 BDL 11,071 12/09/14 5510 1,000 2,100 <50 <50 <50 <50 5,500 <50 180 <50 <100 BDL 8,780 11/11/15 5847 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 80 <5.0 20 <5.0 <10.0 BDL 100 11/03/16 6205 2,400 2,300 <5.0 <5.0 <5.0 12 5,800 52 180 <5.0 23 BDL 10,767 11/27/17 6594 2,600 4,100 <5.0 <5.0 <5.0 13 7,200 74 240 5.4 29 BDL 14,261 12/04/18 6966 970 2,600 <0.61 <0.66 <0.83 19 5,700 50 140 4.1 J 20 BDL 9,503 12/05/19 7332 530 690 <0.61 <0.66 <0.83 3.6 J 1,500 50 63 <0.44 3.3 J Benzene (2.0 J), 2-Butanone (8.6 J) 2,851 11/03/99 8,200 7,700 <5 <5 22 120 31,000 430 2,700 96 660 Benzene (61), Ethylbenzene (22), Xylenes (57), 12-Dichlorobenzene 73 51,020 10/24/00 351 1,200 3,900 <5 <5 16 33 30,000 410 2,700 45 140 1,2-Dichlorobenzene (5.9), Benzene 8.5 38,480 11/14/01 737 1,200 1,800 <50 <50 <50 <50 17,000 83 740 <50 90 BRL 20,913 11/13/02 1101 290 830 <50 <50 <50 <50 34,000 160 2,200 <50 83 1,2-Dichloropropane (98); 1,1-Dichloro ro ene (130) 37,791 11/3/03 1456 320 2,500 <50 <50 <50 <50 25,000 73 1,300 <50 <50 BDL 29,193 11/01/04 1820 630 4,800 <50 <50 <50 55 22,000 160 1,100 <50 <50 Benzene (8.0) 28,698 10/25/05 2178 93 300 <50 <50 <50 <50 21,000 130 2,200 1 <50 <50 BDL 23,723 11/28/06 2577 <100 170J <100 <100 <100 <100 19,000 <200 1,700 <100 <100 BDL 20,870 RW-2 10/25/07 2908 140 470 <100 <100 <100 <100 18,000 110J 2,000 <100 <100 BDL 20,720 11/06/08 3286 280 1,500 <100 <100 <100 <100 16,000 1101 920 <100 <100 BDL 18,810 10/30/09 3644 190 830 <100 <100 <100 <100 14,000 88J 1,200 <100 <100 BDL 16,308 11/02/10 4012 150 660 <100 <100 <100 <100 13,000 84J 830 <100 <100 BDL 14,724 11/01/11 4376 150 570 <100 <100 <100 <100 12,000 74J 960 <100 <100 BDL 13,754 11/02/12 4743 180 570 <100 <100 <100 <100 11,000 73J 930 <100 <100 BDL 12,680 11/06/13 5112 230 410 <100 <100 <100 <100 9,200 60J 730 <100 <100 BDL 10,630 12/09/14 5510 210 350 <50 <50 <50 <50 8,200 76 1,300 <50 <100 BDL 10,136 11/10/15 5846 350 820 <5.0 <5.0 <5.0 12 7,900 43 330 <5.0 5.8 J BDL 9,449 11/03/16 6205 160 260 <5.0 <5.0 <5.0 12 6,300 38 310 13 BDL 7,093 11/27/17 6594 120 220 <5.0 <5.0 <5.0 16 8,100 50 550 17 BDL 9,073 12/04/18 6966 140 250 <0.61 <0.66 <0.83 22 6,600 33 250 E<5. 9.1 J BDL 7,304 12/05/19 7332 130 240 <0.61 <0.66 2.5 J 14 7,100 40 310 4.8 J BDL 7,841 Page 1 of 2 TABLE 3-2 HISTORICAL SUMMARY OF VOLATILE ORGANIC COMPOUNDS IN GROUNDWATER FROM RECOVERY WELLS LUMBERTON ENERGY HOLDINGS, LLC (FORMER ALAMAC AMERICAN KNITS SITE) LUMBERTON, NORTH CAROLINA DAA PROJECT NO: 19080294 Well ID Sample Date Days after Startup Tetrachloroethene (pg/L) Trichloroethene (pg/L) 1,1,1- Trichloroethane (pg/L) 1,1,2- Trichloroethane (Ng/L) 1,1- Dichloroethane (pg/L) 1,1- Dichloroethene (pg/L) cis-1,2- Dichloroethene (pg/L) trans-1,2- Dichloroethene (pg/L) Vinyl Chloride (pg/L) Toluene (pg/L) Naphthalene (pg/L) Other VOCs (pg/L) TOTAL VOCs (ug/L) 1SA NCAC 2L Standards 0.70 3.0 200 Not listed 6* 350*** 70 100 0.03** 600 6 Compound Specific 11/03/99 -5 110 68 <5 <5 8.5 <5 330 <5 <10 <5 <25 BDL 517 10/24/00 351 <5 19 <5 <5 6.1 6.7 6,500 67 1100 8.5 26 BDL 7,733 11/14/01 737 <5 6.8 6.7 <5 <5 <5 2,000 8.8 320 <5 14 BDL 2,356 11/13/02 1101 <50 <50 <50 <50 <50 <50 2,800 <50 610 <50 <50 BDL 3,410 11/03/03 1456 <5 8.8 <5 <5 <5 <5 3,100 8.7 350 <5 6.8 BDL 3,474 11/01/04 1820 <5 15.0 <5 <5 <5 <5 2,700 16 330 <5 <5 BDL 3,061 10/25/05 2178 <5 6.2 <5 <5 <5 <5 1,700 7.6 250 <5 <5 BDL 1,964 11/28/06 2577 <10 <20 <10 <20 <10 <10 1,800 <20 290 <10 <10 BDL 2,090 10/25/07 2908 <10 5.6 J <10 <10 <10 <10 960 5.3 J 140 <10 <10 BDL 1,111 11/06/08 3286 <10 115.1 <10 <10 <10 <10 1,600 12J 240 <10 <10 BDL 1,867 10/30/09 3644 <10 8.0 J <10 <10 <10 <10 1,100 5.3 J 140 <10 <10 BDL 1,253 11/02/10 4012 <10 12 J <10 <10 <10 <10 1,300 8.9 J 150 <10 <10 BDL 1,471 11/01/11 4376 <10 5.9 J <10 <10 <10 <10 1,200 7.6 J 280 <10 <10 BDL 1,494 RW-3 11/02/12 4743 <10 6.0 J <10 <10 <10 <10 1,100 6.3 J 230 <10 <10 BDL 1,342 11/06/13 5112 <20 <40 <20 <20 <20 <20 1,100 <40 220 <20 <20 BDL 1,320 12/09/14 5510 <10 <10 <10 <10 <10 <10 690 <10 92 <10 <20 BDL 782 11/10/15 5846 2.8 9.3 <5.0 <5.0 1.0 2.5 1,300 8.1 160 <5.0 2.9 1,4-Dichlorobenzene (0.61), 2- Chlorotoluene (0.66), Benzene (0.55) 1,488 11/03/16 6205 <5.0 9.0 <5.0 <5.0 <5.0 <5.0 1,100 5.8 140 <5.0 5.4 J BDL 1,260 11/27/17 6594 <5.0 5.9 <5.0 <5.0 0.92 2.2 840 6.5 94 <5.0 4.3 1,4-Dichlorobenzene (0.73), Benzene (0.54), Chlorobenzene (1.0) 956 12/04/18 6966 7.2 11 1.2 <0.66 0.70 4.3 1,500 10 180 0.37 J 5.2 1,2,4-Trichlorobenzene (0.34J) 1,4- Dichlorobenzene (0.82), 2- Chlorotoluene (0.51), Benzene (0.71), Chlorobenzene (0.89), Xylenes (0.901) 1,724 12/05/19 7332 6.1 16 <0.61 <0.66 <0.83 3.6 J 1,800 10 240 <0.44 2.3 J BDL 2,078 11/28/06 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0 BDL 0 10/25/07 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0 BDL 0 11/06/08 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0 BDL 0 10/30/09 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0 romo orm , Chlorodibromomethane (0.57 J) 3.07 11/02/10 -2 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0 BDL 0 11/01/11 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0 BDL 0 2237 Alamac 11/02/12 ° Q <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0 BDL 0 11/06/13 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 Chloroform (0.51) 0.51 Road 12/09/14 0 z <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 BDL 0 11/10/15 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 BDL 0 11/03/16 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 Acetone (8.4), 2-Butanone (15) 23.4 11/27/17 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0 BDL 0 12/04/18 <0.098 <0.078 <0.061 <0.066 <0.083 <0.083 <0.056 <0.094 <0.097 <0.044 <0.19 Acetone (37), 2-Butanone (33) 70 12/05/19 <0.098 <0.078 <0.061 <0.066 <0.083 <0.083 <0.056 <0.094 <0.097 <0.044 <0.19 Acetone (13), 2-Butanone (12), Chloroform (0.23 J) 25.23 Notes: pg/L = micrograms per liter NC 2L Standards = 15A NCAC 2L Groundwater Quality Standards (April 1, 2013) NS = Not Sampled BDL = Below Detection Limit Shaded cells represent concentrations exceeding the 15A NCAC 2L Standard Values in bold represent concetrations exceeding the detection limit. J = Estimated value between the Reporting Limit and the Method Detection Limit. = NC 2L Standard changed in Jan 2010 from 70 pg/L to 6 pg/L. *= NC 2L Standard changed in Jan 2010 from 0.015 pg/L to 0.03 pg/L. = NC 2L Standard changed in April 2013 from 7 pg/L to 350 pg/L. < = Constituent concentration less than the detection limit shown Days after startup indicate number of days groundwater recovery system has been in operation since system was started on November 8, 1999. N/A = Not Applicable Page 2of2 TABLE 4-1 OPERATIONAL DATA SUMMARY FOR GROUNDWATER RECOVERY WELLS LUMBERTON ENERGY HOLDINGS, LLC (FORMER ALAMAC AMERICAN KNITS SITE) LUMBERTON, NORTH CAROLINA DAA PROJECT NO: 19080294 Rec very Well Data Flow Rates m Cumulative Volume al Date Days of Operation RW-1 RW-2 RW-3 Total from all RWs RW-1 Meter Reading RW-1 RW-2 RW-3 Total from all RWs Avg. Instantaneous Flow Rate Reading (gpm)-1999-2005 ca Q 0 Z Avg. Flow Rate (gpm) for 1999 - 2005 2.35 1 0.92 1 7.63 1 10.9 1.52 0.75 1 8.49 T 10.76 Avg. Instantaneous Flow Rate Reading (gpm) - 2006 Avg. Flow Rate (gpm) for year 2006 2.01 1.06 7.17 10.24 1.46 1.03 7.37 9.85 Avg. Instantaneous Flow Rate Reading (gpm) - 2007 Avg. Flow Rate (gpm) for year 2007 2.18 1.38 7.73 11.28 1.19 1.38 7.66 10.23 Avg. Instantaneous Flow Rate Reading (gpm) - 2008 Avg. Flow Rate (gpm) for year 2008 1.35 1.32 8.07 10.74 0.97 1.28 8.09 T 10.34 Avg. Instantaneous Flow Rate Reading (gpm) - 2009 Avg. Flow Rate (gpm) for year 2009 1.46 1.45 8.33 11.12 1.05 1.34 8.21 10.60 01/01/10 3707 1.45 1.40 8.60 11.5 @ @ a' 0 z 7,342,062 5,100,890 43,955,425 56,398,377 02/01/10 3738 1.37 1.47 8.51 11.4 7,388,086 5,165,365 44,334,467 56,887,918 03/01/10 3766 1.71 1.99 8.92 12.6 7,425,792 5,225,243 44,661,950 57,312,985 04/01/10 3797 1.43 1.33 8.31 11.1 7,464,876 5,287,751 45,042,637 57,795,264 05/01/10 3827 1.52 1.29 7.45 10.3 7,508,624 5,345,077 45,400,963 58,254,664 06/01/10 3858 1.55 1.33 8.50 11.4 7,559,139 5,392,209 45,742,796 58,694,144 07/01/10 3888 1.60 1.43 8.37 11.4 7,608,764 5,450,720 46,103,208 59,162,692 08/01/10 3919 1.32 1.37 8.41 11.1 7,656,330 5,510,839 46,467,111 59,634,280 09/01/10 3950 1.71 1.27 9.61 12.6 7,702,429 5,568,519 46,852,245 60,123,193 10/01/10 3980 1.64 1.30 7.55 10.5 7,754,455 5,623,672 47,246,402 60,624,529 11/01/10 4011 1.55 1.32 9.23 12.1 7,806,155 5,682,554 47,632,579 61,121,288 12/01/10 4041 1.23 1.26 8.00 10.5 7,844,010 5,733,056 47,986,685 61,563,751 2010 Avg. Instantaneous Flow Rate Reading (gpm) - 2010 Avg. Flow Rate (gpm) for year 2010 1.51 1.40 8.46 11.36 1.05 1.33 8.39 10.77 01/01/11 4072 1.23 1.43 8.02 10.7 a) M < 0 Z 7,881,904 5,791,701 48,336,780 62,010,385 02/01/11 4103 1.22 1.37 9.53 12.1 7,920,407 5,852,064 48,713,585 62,486,056 03/01/11 4131 1.57 1.30 8.99 11.9 7,955,505 5,904,817 49,076,488 62,936,810 04/01/11 4162 1.59 1.59 8.86 12.0 8,005,792 5,962,539 49,455,019 63,423,350 05/01/11 4192 1.60 1.20 8.36 11.2 8,055,020 6,015,670 49,817,677 63,888,367 06/01/11 4223 1.48 1.15 8.08 10.7 8,102,989 6,067,589 50,205,623 64,376,201 07/01/11 4253 1.42 1.61 7.69 10.7 8,147,336 6,131,828 50,570,575 64,849,739 08/01/11 4284 1.39 1.72 8.01 11.1 8,191,167 6,207,959 50,947,697 65,346,823 09/01/11 4315 1.36 1.53 8.87 11.8 8,234,854 6,280,082 51,308,976 65,823,912 10/01/11 4345 1.59 1.50 8.32 11.4 8,282,127 6,346,046 51,666,952 66,295,125 11/01/11 4376 1.70 1.43 7.70 10.8 8,335,752 6,412,079 51,992,167 66,739,998 12/01/11 4406 1.22 1.46 7.39 10.1 8,388,578 6,474,994 1 52,311,543 67,175,115 2011 Avg. Instantaneous Flow Rate Reading (gpm) - 2011 Avg. Flow Rate (gpm) for year 2011 1.45 1.44 8.32 11.21 1.04 1.41 8.23 10.68 01/01/12 4437 1.52 1.50 8.38 11.4 a) m < 0 z 8,440,248 6,541,093 52,666,916 67,648,257 02/01/12 4468 1.45 1.58 8.56 11.6 8,523,580 6,606,462 53,048,874 68,178,916 03/01/12 4497 1.35 1.63 8.77 11.9 8,644,583 6,668,241 53,384,479 68,697,303 04/01/12 4528 1.17 1.52 9.15 11.8 8,724,975 6,736,965 53,797,932 69,259,872 05/01/12 4558 1.29 1.46 9.00 11.8 8,763,365 6,800,509 54,195,559 69,759,433 06/01/12 4589 1.11 1.42 9.06 11.6 8,849,796 6,862,724 54,588,741 70,301,261 07/01/12 4619 1.03 1.33 9.43 11.8 8,883,163 6,922,435 54,984,102 70,789,700 08/01/12 4650 1.33 1.60 8.13 11.1 8,962,072 6,983,797 55,379,577 71,325,446 09/01/12 4681 1.30 1.76 8.04 11.1 9,004,641 7,055,241 55,724,287 71,784,169 10/01/12 4711 1.24 1.61 8.78 11.6 9,043,657 7,123,051 55,982,283 72,148,991 11/01/12 4742 1.24 1.57 6.51 9.3 9,081,834 7,202,089 56,325,888 72,609,811 12/01/12 4772 1.17 1.56 7.91 10.6 9,120,157 7,275,594 56,631,219 73,026,970 2012 Avg. Instantaneous Flow Rate Reading pm - 2012 Avg. Flow Rate (gpm) for year 2012 1.27 1.55 8.48 11.30 1.39 1.52 8.20 11.10 01/01/13 4803 1.23 2.72 8.52 12.5 9,957,993 9,957,993 7,349,106 56,964,491 74,271,590 02/01/13 4834 1.75 1.47 8.37 11.6 9,996,772 9,996,772 7,427,642 57,343,383 74,767,797 03/01/13 4862 1.33 1.62 8.67 11.6 10,034,260 10,034,260 7,490,303 57,684,356 75,208,919 04/01/13 4893 1.45 1.61 8.42 11.5 10,074,226 10,074,226 7,559,998 58,064,904 75,699,128 05/01/13 4923 1.37 1.68 8.24 11.3 10,038,990 10,038,990 7,629,268 58,422,405 76,090,663 06/01/13 4954 1.34 1.49 8.40 11.2 10,082,973 10,082,973 7,698,122 58,806,001 76,587,096 07/01/13 4984 1.48 1.63 8.13 11.2 10,047,309 10,047,309 7,764,930 59,165,099 76,977,338 07/24/13 5007 1.36 1.65 7.60 10.6 10,081,376 10,081,376 7,818,785 59,444,656 77,344,817 07/25/13 5008 off - reset 1.69 8.68 10.4 90,882,823 10,081,376 7,821,168 59,457,161 77,359,705 08/01/13 5015 1.39 1.60 8.51 11.5 90,892,895 10,091,448 7,838,103 59,542,874 77,472,425 09/01/13 5046 1.29 1.66 8.34 11.3 90,937,199 10,135,752 7,912,433 59,914,826 77,963,011 10/01/13 5076 1.12 1.69 7.41 10.2 90,974,086 10,172,639 7,983,116 1 60,251,240 1 78,406,995 11/01/13 5107 1.32 1.56 6.72 9.6 91,014,083 10,212,636 8,060,326 60,533,019 78,805,981 12/01/13 5137 1.16 1.59 6.51 9.3 91,053,606 10,252,159 8,127,392 60,786,729 79,166,280 2013 Avg. Instantaneous Flow Rate Reading (gpm) - 2013 Avg. Flow Rate (gpm) for year 2013 1.35 1.69 8.04 10.98 2.15 1.62 7.91 11.68 01/01/14 5168 1.37 1.78 8.43 11.6 91,884,677 11,083,230 8,203,889 61,089,774 80,376,893 02/01/14 5199 1.31 1.85 9.03 12.2 91,927,944 11,126,497 8,283,445 61,450,102 80,860,044 03/01/14 5227 1.22 1.73 8.03 11.0 93,005,327 12,203,880 8,351,045 61,775,099 82,330,024 03/12/14 5238 1.28 1.69 7.95 10.9 93,019,145 12,217,698 8,377,901 61,905,552 82,501,151 03/13/14 5239 off - reset 1.60 8.49 10.1 13,264,273 12,217,698 8,380,256 61,917,205 82,515,159 03/21/14 5247 1.04 1.68 9.61 12.3 13,272,862 12,226,287 8,399,904 62,018,261 82,644,452 03/22/14 5248 off - reset 1.70 8.81 10.5 999,756 12,226,287 8,402,259 62,031,040 82,659,586 04/01/14 5258 1.67 1.56 8.63 11.9 1,028,895 12,255,426 8,425,898 62,155,314 82,836,638 05/01/14 5288 1.36 1.68 9.31 12.4 1,091,349 12,317,880 8,495,272 62,554,218 83,367,370 06/01/14 5319 0.93 1.47 8.99 11.4 1,147,219 12,373,750 8,564,461 62,970,849 83,909,060 07/01/14 5349 1.83 1.57 6.23 9.6 1,237,785 12,464,316 8,632,416 63,284,007 84,380,739 08/01/14 5380 2.37 1.93 8.90 13.2 1,304,965 12,531,496 8,703,545 63,564,385 84,799,426 09/01/14 5411 2.42 1.89 8.11 12.4 1,410,254 12,636,785 8,787,912 63,907,799 85,332,496 10/01/14 5441 2.28 1.92 7.52 11.7 1,505,963 12,732,494 8,868,461 64,231,610 85,832,565 11/01/14 5472 2.49 1.83 7.12 11.4 1,686,671 12,913,202 8,951,247 64,532,604 86,397,053 12/01/14 5502 2.15 1.84 6.91 10.9 1,783,980 13,010,511 9,030,272 64,806,070 86,846,853 2014 Avg. Instantaneous Flow Rate Reading (gpm) - 2014 Avg. Flow Rate (gpm) for year 2014 1.69 1.73 8.25 11.47 5.25 1.72 7.65 14.61 01/01/15 5533 2.04 1.87 8.47 12.4 1,879,450 13,105,981 9,114,129 65,119,618 87,339,728 02/01/15 5564 2.36 1.54 8.55 12.5 1,976,329 13,202,860 9,197,473 65,492,729 87,893,062 03/01/15 5592 2.99 1.64 9.51 14.1 2,064,626 13,291,157 9,260,960 65,832,354 88,384,471 04/01/15 5623 0.06 1.51 9.97 11.5 2,067,123 13,293,654 9,331,994 66,254,329 88,879,977 05/01/15 5653 0.11 1.53 9.47 11.1 2,071,889 13,298,420 9,398,153 66,672,485 89,369,058 06/01/15 5684 0.15 1.47 8.61 10.2 2,078,786 13,305,317 9,464,636 67,084,530 89,854,483 07/01/15 5714 0.10 1.54 7.96 9.6 2,083,005 13,309,536 9,530,699 67,384,958 90,225,193 08/01/15 5745 0.05 1.54 6.58 8.2 2,085,050 13,311,581 9,599,640 67,706,925 90,618,146 09/01/15 5776 0.03 1.57 6.35 8.0 2,086,486 13,313,017 9,668,736 68,004,536 90,986,289 10/01/15 5806 0.00 1.54 6.85 8.4 2,086,487 13,313,018 9,736,047 68,278,076 91,327,141 11/01/15 5837 0.00 1.52 7.15 8.7 2,086,542 13,313,073 9,804,333 68,609,326 91,726,732 12/01/15 5867 0.00 1.58 7.88 9.5 2,086,543 13,313,074 1 9,872,666 68,984,922 92,170,662 Page 1 of 2 TABLE 4-1 OPERATIONAL DATA SUMMARY FOR GROUNDWATER RECOVERY WELLS LUMBERTON ENERGY HOLDINGS, LLC (FORMER ALAMAC AMERICAN KNITS SITE) LUMBERTON, NORTH CAROLINA DAA PROJECT NO: 19080294 Date Days of Operation Rec very Well Data Flow Rates m Cumulative Volume al RW-1 RW-2 RW-3 Total from all RWs RW-1 Meter Reading RW-1 RW-2 RW-3 Total from all RWs 2015 Avg. Instantaneous Flow Rate Reading (gpm) - 2015 Avg. Flow Rate pm for year 2015 0.66 1.57 8.11 10.34 0.58 1.34 6.61 8.52 01/01/16 5898 2.19 1.73 9.92 13.8 2,151,351 13,377,882 9,949,910 69,392,733 92,720,525 02/01/16 5929 1.91 1.63 9.89 13.4 2,253,366 13,479,897 10,024,621 69,830,431 93,334,949 03/01/16 5958 2.61 1.68 9.40 13.7 2,353,947 13,580,478 10,096,062 70,245,846 93,922,386 04/01/16 5989 2.33 1.67 10.33 14.3 2,442,383 13,668,914 10,171,801 70,688,001 94,528,716 05/01/16 6019 2.24 1.82 10.54 14.6 2,533,003 13,759,534 10,245,507 71,130,249 95,135,290 06/01/16 6050 2.07 1.76 8.89 12.7 2,625,046 13,851,577 10,324,299 71,509,233 95,685,109 07/01/16 6080 1.70 1.64 8.34 11.7 2,705,668 13,932,199 10,396,730 71,893,326 96,222,255 08/01/16 6111 2.36 1.55 7.84 11.8 2,785,924 1 14,012,455 10,467,663 72,286,242 96,766,360 09/01/16 6142 2.31 1.47 7.04 10.8 2,908,133 14,134,664 10,535,304 72,613,757 97,283,725 10/01/16 6172 2.04 1.53 7.21 10.8 2,990,641 14,217,172 10,599,752 72,919,702 97,736,626 11/01/16 6203 2.19 1.23 7.67 11.1 3,058,422 14,284,953 10,641,854 73,157,298 98,084,105 12/01/16 6233 1.19 1.90 7.07 10.2 3,147,039 14,373,570 10,719,264 1 73,477,860 1 98,570,694 2016 Avg. Instantaneous Flow Rate Reading (gpm) - 2016 Avg. Flow Rate (gpm) for year 2016 2.10 1.63 8.68 12.41 2.01 1.61 8.52 12.14 01/01/17 6264 2.97 1.86 5.98 10.8 3,244,281 14,470,812 10,803,604 73,782,146 99,056,562 02/01/17 6295 2.77 2.04 3.36 8.2 3,357,696 14,584,227 10,874,680 73,984,218 99,443,125 03/01/17 6323 2.35 2.44 2.73 7.5 3,455,097 14,681,628 10,950,508 74,113,414 99,745,550 04/01/17 6354 2.05 2.30 2.75 7.1 3,553,508 14,780,039 11,038,565 74,241,062 100,059,666 05/01/17 6384 2.16 1.59 2.63 6.4 3,604,422 14,830,953 11,139,653 74,361,418 100,332,024 06/01/17 6415 2.26 1.64 2.91 6.8 3,679,341 14,905,872 11,214,653 74,482,929 100,603,454 07/01/17 6445 1.38 1.95 4.15 7.5 3,770,922 14,997,453 11,289,653 74,633,745 100,920,851 08/01/17 6476 2.18 1.99 4.52 8.7 3,850,643 15,077,174 11,364,653 74,840,785 101,282,612 09/01/17 6507 2.49 1.95 4.79 9.2 3,948,548 15,175,079 11,439,653 75,042,853 101,657,585 10/01/17 6537 1.83 3.05 5.67 10.6 4,042,217 15,268,748 11,514,653 75,276,759 102,060,160 11/01/17 6568 2.28 3.54 5.35 11.2 4,150,395 15,376,926 11,589,653 75,529,663 102,496,242 12/01/17 6598 2.31 3.65 5.49 11.5 4,258,325 15,484,856 11,664,653 1 75,763,937 1 102,913,446 2017 Avg. Instantaneous Flow Rate Reading (gpm) - 2017 Avg. Flow Rate (gpm) for year 2017 2.25 2.33 4.19 8.78 2.11 1.80 4.35 8.26 01/01/18 6629 1.55 4.03 6.06 11.6 4,344,915 15,571,446 11,769,482 76,025,468 103,366,396 02/01/18 6660 1.72 4.02 5.97 11.7 4,436,060 15,662,591 11,877,975 76,293,700 103,834,266 03/01/18 6688 2.16 3.71 6.01 11.9 4,521,559 15,748,090 11,969,954 76,534,834 104,252,878 04/01/18 6719 0.00 3.69 5.86 9.6 4,540,473 15,767,004 12,071,442 76,797,660 104,636,106 05/01/18 6749 0.00 3.14 5.83 9.0 4,540,473 15,767,004 12,159,266 77,050,381 104,976,651 06/01/18 6780 0.00 3.14 5.84 9.0 4,540,473 15,767,004 12,241,690 77,313,879 105,322,573 07/01/18 6810 0.00 4.31 5.92 10.2 4,540,475 15,767,006 12,305,252 77,571,332 105,643,590 08/01/18 6841 3.77 2.77 6.29 12.8 4,655,935 15,882,466 12,392,326 77,843,588 106,118,380 09/01/18 6872 2.80 4.67 5.98 13.5 4,806,626 16,033,157 12,504,858 78,116,560 106,654,575 10/01/18 6902 3.41 2.55 6.80 12.8 4,855,539 16,082,070 12,555,400 78,231,197 106,868,667 11/01/18 6933 3.21 2.21 6.71 12.1 5,020,270 16,246,801 12,610,050 78,534,353 107,391,204 12/01/18 6963 2.66 2.04 6.47 11.2 5,140,462 16,366,993 12,669,889 78,818,339 107,855,221 2018 Avg. Instantaneous Flow Rate Reading (gpm) - 2018 Avg. Flow Rate (gpm) for year 2018 1.77 3.36 6.15 11.28 1.65 1.87 5.81 9.33 01/01/19 6994 2.39 2.25 5.53 10.2 5,253,460 16,479,991 12,747,051 79,103,617 108,330,655 02/01/19 7025 2.07 2.67 3.53 8.3 5,355,846 16,582,377 12,816,838 79,290,212 108,689,427 03/01/19 7053 1.85 2.52 4.35 8.7 5,437,089 16,663,620 12,879,303 79,453,164 108,996,087 04/01/19 7084 1.74 2.25 4.38 8.4 5,523,442 16,749,973 12,943,260 79,644,739 109,337,972 05/01/19 7114 2.89 2.25 4.77 9.9 5,606,354 16,832,885 13,005,293 79,848,964 109,687,142 06/01/19 7145 2.12 1.84 4.93 8.9 5,713,270 16,939,801 13,059,305 80,061,043 110,060,149 07/01/19 7175 2.21 1.92 5.44 9.6 5,804,497 17,031,028 13,112,224 80,285,083 110,428,335 08/01/19 7206 0.63 3.00 5.40 9.0 5,832,814 17,059,345 13,182,919 80,522,323 110,764,587 09/01/19 7237 0.00 3.01 5.53 8.5 5,832,819 17,059,350 13,264,234 80,767,458 111,091,042 10/01/19 7267 0.00 2.13 5.61 7.7 5,832,819 17,059,350 13,322,424 81,000,751 111,382,525 11/01/19 7298 2.64 5.54 8.2 5,832,819 17,059,350 13,395,089 81,252,517 111,706,956 12/05/19 7332 5.92 5.58 15.3 5,839,632 17,066,163 13,514,749 81,525,275 112,106,187 2019 EjEAvg.Instantaneous Flow Rate Reading (gpm) - 2019 Avg. Flow Rate (gpm) for year 2019 2.70 5.05 1 9.39 1.20 1.58 4.98 7.76 11,484,819 gallons added to monthly totals In "Total from all HW's" due to meter change In HW-2. Page 2 of 2 TABLE 4-2 CALCULATION OF MASS OF VOLATILE ORGANIC COMPOUNDS REMOVED FROM GROUNDWATER BY THE RECOVERY WELL NETWORK LUMBERTON ENERGY HOLDINGS, LLC (FORMER ALAMAC AMERICAN KNITS SITE) LUMBERTON, NORTH CAROLINA DAA PROJECT NO: 19080294 Sampling Date Days after Startup Total VOCs Recovery Wells Calculated Mass Removal (Ng/L) (Gallons) Pounds (Ibs) Removed RW-1 RW-2 RW-3 RW-1 RW-2** RW-3 Recovered Per Period Cumulative Total RW-1 RW-2 RW-3 Removed Per Period Cumulative Total 11/03/99 -5 2,479 51,020 517 0 0 0 0 0 11/08/99 0 NA NA NA 583 728 1,584 2,895 2,895 0.0 0.3 0.0 0.3 0.3 02/03/00 87 4,562 44,255 6,837 178,297 224,078 1,454,751 1,854,231 1,857,126 6.7 82.2 82.6 172.0 171.9 04/26/00 170 3,863 41,256 7,127 296,738 314,213 2,879,623 1,633,448 3,490,574 3.8 30.9 84.4 119.0 291.1 07/24/00 259 NA NA NA 390,980 375,625 4,454,671 1,730,702 5,221,276 07/25/00 260 5,330 34,977 5,820 4.2 17.9 76.2 98.0 389.3 10/24/00 351 6,945 34,480 7,733 02/15/01 465 10,155 43,171 9,346 872,959 557,930 7,366,871 3,576,484 8,797,760 34.3 58.9 206.8 300.0 689.3 05/22/01 561 2,385 34,140 6,519 1,010,268 574,573 8,468,793 1,255,874 10,053,634 2.7 4.7 59.7 67.0 756.5 08/28/01 659 3,145 17,771 5,930 1,168,399 609,243 9,659,466 1,383,474 11,437,108 4.1 5.1 58.7 68.0 824.4 11/14/01 737 4,434 20,913 2,536 11/15/01 738 NA NA NA 1,301,866 693,357 10,525,149 1,083,264 12,520,372 4.9 14.6 18.3 38.0 862.2 02/13/02 828 5,844 24,033 3,938 1,465,100 803,303 11,598,264 1,346,295 13,866,667 7.9 22.0 35.1 65.0 927.3 05/20/02 924 NA NA NA 1,652,612 902,321 12,813,585 1,501,851 15,368,518 8.2 24.5 44.1 77.0 1,004.0 05/21/02 925 5,234 29,700 4,364 08/05/02 1001 NA NA NA 1,806,428 981,799 13,821,493 1,241,202 16,609,720 6.3 18.6 32.7 58.0 1,061.6 08/06/02 1002 4,920 28,136 3,900 11/13/02 1101 5,113 37,791 3,410 2,001,703 1,120,943 14,950,240 1,463,166 18,072,886 8.3 43.7 32.0 84.0 1,145.6 02/11/03 1191 6,372 28,468 3,079 02/12/03 1192 NA NA NA 2,186,278 1,236,577 15,988,242 1,338,211 19,411,097 9.8 27.4 26.6 64.0 1,209.4 05/13/03 1282 5,010 24,850 2,292 5/14/2003 1283 NA NA NA 2,422,769 1,342,694 17,035,269 1,389,635 20,800,732 9.9 21.9 20.0 52.0 1261.1 8/26/2003 1387 4,630 24,350 3,318 8/27/2003 1388 NA NA NA 2,727,875 1,453,090 18,205,959 1,586,192 22,386,924 11.7 22.4 32.3 66.0 1,327.5 11/3/2003 1456 5,105 29,193 3,474 11/7/2003 1460 NA NA NA 2,930,785 1,536,824 18,971,934 1,052,619 23,439,543 8.6 20.3 22.1 51.1 1,378.6 2/20/2004 1565 5,864 33,969 2,523 3,225,285 1,655,701 20,113,454 1,554,897 24,994,440 14.4 33.6 24.0 71.9 1,450.5 11/1/2004 1820 5,485 28,698 3,061 3,865,038 1,928,465 22,797,606 3,596,669 28,591,109 29.2 65.1 68.3 162.6 1,613.1 10/25/2005 2178 5,093 23,723 1,964 4,834,285 2,390,003 27,092,242 5,725,421 34,316,530 41.1 91.1 70.1 202.2 1,815.3 11/28/2006 2577 6,449 20,870 2,090 5,601,019 2,930,821 30,964,147 5,179,457 39,495,987 41.1 93.9 67.3 202.3 2,017.6 10/25/2007 2908 5,199 20,720 1,111 6,189,583 3,596,820 34,647,851 4,938,267 44,434,254 25.4 114.8 34.0 174.2 2,191.8 11/30/2008 3310 6,889 18,810 1,867 6,736,628 4,340,176 39,236,323 5,878,873 50,313,127 31.3 116.3 71.2 218.9 2,410.7 10/30/2009 3644 7,179 16,308 1,253 7,243,173 4,969,241 43,208,854 5,108,141 55,421,268 30.2 85.3 41.4 156.9 2,567.6 11/2/2010 4012 7,290 14,724 1,471 7,806,155 5,682,554 47,632,579 5,700,020 61,121,288 34.1 87.3 54.1 175.6 2,743.2 11/1/2011 4376 5,930 13,754 1,494 8,335,752 6,412,079 51,992,167 5,618,710 66,739,998 26.1 83.4 54.2 163.7 2,906.9 11/2/2012 4743 8,540 12,680 1,342 9,083,145 7,204,409 56,334,951 5,882,507 72,622,505 53.1 83.5 48.5 185.1 3,092.0 11/6/2013 5112 11,071 10,630 1,320 10,219,624 8,071,379 60,571,451 6,239,949 78,862,454 104.6 76.6 46.5 227.8 3,319.8 12/9/2014 5510 8,780 10,136 782 13,032,819 9,052,141 64,880,526 8,103,032 86,965,486 205.4 82.7 28.0 316.1 3,635.9 11/1/2015 5837 100 9,449 1,488 2,086,542* 9,804,333 68,609,326 4,759,246 91,724,732 0.231 59.1 46.2 105.5 3,741.4 11/3/2016 6205 10,767 7,093 1,260 3,064,750 10,645,398 73,179,273 6,389,220 98,113,952 87.6 49.6 47.9 185.1 3,926.5 11/27/2017 6594 14,261 9,073 956 4,242,969 11,651,232 75,731,396 4,736,176 102,850,128 255.7 75.9 20.3 351.9 4,278.4 12/4/2018 6966 9,503 7,304 1,724 5,151,201 12,677,120 78,845,535 5,048,259 107,898,387 71.8 62.3 44.6 178.7 4,457.1 12/5/2019 7332 2,851 7,841 2,078 5,839,632 13,514,749 81,525,275 4,205,800 112,104,187 16.3 54.6 46.3 117.2 4,574.4 Total Pounds Removed Since Startup by Recovery Well 1,199.2 1,730.5 1,644.E Cumulative of 1 All RWs 4,574 NA = Not analyzed. *Totalizer changed. Value subtracted from initial reading of 1,808,288 ** 11,484,819 gallons added to each reading for RW-2 in 2018 due to meter change Page 1 of 1 TABLE 4-3 HISTORICAL SUMMARY OF VOLATILE ORGANIC COMPOUNDS IN ON -SITE WASTEWATER TREATMENT PLANT EFFLUENT LUMBERTON ENERGY HOLDINGS, LLC (FORMER ALAMAC AMERICAN KNITS SITE) LUMBERTON, NORTH CAROLINA DAA PROJECT NO: 19080294 WWTP Effluent Sample Date Tetrachloroethene (Ng/L) Trichloroethene (Ng/L) cis -1,2- Dichloroethene (Ng/L) Vinyl Chloride (Ng/L) 1999 11/09/99 <5 <5 <5 <5 2000 1 04/13/00 <5 <5 <5 <10 2001 09/04/01 <5 <5 <5 <10 2002 11/05/02 <5 <5 <5 <10 2003 12/01/03 <5 <5 <5 <10 2004 12/07/04 <5 <5 0.8 <10 2005 10/04/05 <0.01 <0.01 <0.01 <0.01 2006 12/11/06 <1.0 <1.0 <1.0 <2.0 2007 12/04/07 < 5.0 < 5.0 < 5.0 < 10.0 2008 09/16/08 <2.0 <1.0 <1.0 <2.0 2009 12/15/09 < 1.0 < 1.0 < 1.0 < 2.0 2010 12/14/10 <1.0 <1.0 <1.0 <2.0 N 03/11/11 <1.0 <1.0 <1.0 <2.0 06/14/11 <1.0 <1.0 <1.0 <2.0 09/13/11 <1.0 <1.0 <1.0 <2.0 12/13/11 <1.0 <1.0 <1.0 <2.0 N N 03/12/12 <1.0 <1.0 <1.0 <2.0 06/12/12 <1.0 <1.0 <1.0 <2.0 09/11/12 <1.0 <1.0 <1.0 <2.0 12/04/12 <1.0 <1.0 <1.0 <2.0 ^� N 03/05/13 <1.0 <1.0 <1.0 <2.0 06/11/13 <1.0 <1.0 <1.0 <2.0 09/10/13 <1.0 <1.0 <1.0 <2.0 12/10/13 <1.0 <1.0 <1.0 <2.0 N 03/11/14 <1.0 <1.0 <1.0 <2.0 06/10/14 <1.0 <1.0 <1.0 <2.0 09/23/14 <1.0 <1.0 <1.0 <2.0 12/17/14 <1.0 <1.0 <1.0 <2.0 Ln N 03/17/15 <1.0 <1.0 <1.0 <2.0 06/09/15 <0.250 <0.250 <0.250 <0.250 09/15/15 <0.250 <0.250 <0.250 <0.250 12/08/15 <0.250 <0.250 <0.250 <0.250 N 03/15/16 <0.250 <0.250 <0.250 <0.250 06/07/16 <0.250 <0.250 <0.250 <0.250 09/13/16 <0.250 <0.250 <0.250 <0.250 12/13/16 <0.250 <0.250 0.335 <0.250 Page 1 of 2 TABLE 4-3 HISTORICAL SUMMARY OF VOLATILE ORGANIC COMPOUNDS IN ON -SITE WASTEWATER TREATMENT PLANT EFFLUENT LUMBERTON ENERGY HOLDINGS, LLC (FORMER ALAMAC AMERICAN KNITS SITE) LUMBERTON, NORTH CAROLINA DAA PROJECT NO: 19080294 WWTP Sample Tetrachloroethene Trichloroethene cis -1,2- Vinyl Chloride Effluent Date (Ng/L) (Ng/L) Dichloroethene (Ng/L) (Ng/L) 03/14/17 <0.250 <0.250 <0.250 <0.250 n 06/20/17 <0.250 <0.250 <0.250 <0.250 N 09/26/17 <0.250 <0.250 <0.250 <0.250 12/12/17 <0.250 <0.250 <0.250 <0.250 03/20/18 <0.250 <0.250 <0.250 <0.250 00 06/19/18 <0.250 <0.250 <0.250 <0.250 N 10/23/18 <0.250 <0.250 <0.250 <0.250 12/04/18 <0.250 <0.250 <0.250 <0.250 03/12/19 <0.250 <0.250 <0.250 <0.250 06/25/19 <1.0 <1.0 <1.0 <1.0 N 09/24/19 <0.250 <0.250 <0.250 <0.250 12/17/19 <0.250 <0.250 <0.250 <0.250 Bold indicates value exceeded laboratory method detection limit. < = Constituentdid not exceed the method detection limit shown Page 2 of 2 FIGURES FILE DATE PROJECT MANAGER CHECKED BY DRAFTER PROJECT NUMBER AERP Former Alamac..dwg 1/16/2020 SKJ SKJ KTS 19080294-010103 0. ff .�Q�x;C1:'• �r r• r � � Sit AL ' = �; 4_ Manufacturing Q Building �` s �. •' 0 400 800 r, SCALE IN FEET aDraper Aden Associates SITE LOCATION FIGURE: Engineering . Surveying • Environmental Services LUMBERTON ENERGY HOLDINGS, LLC FORMER ALAMAC AMERICAN KNITS SITE C 114 Edinbu gRichmondVA South Drive, 9uiie 200 • Hampton Roads, VA LUMBERTON, NC caIs, NC 27511 •, 919.873.1060 Fa.- 919.873-1074 • Blacksburg, VA •Fayetteville, INC ww.daa.com • Charlottesville, VA ' Northern Virginia NC Firm License # C-0861 Virginia Beach, VA T:\\Env-NC\CAD Files\Project Fileswtrtr rormer Alamac\Current Drawings\AERP Former Alamac.dwg FILE DATE PROJECT MANAGER I CHECKED BY DRAFTER PROJECT NUMBER AERP Former Alamac.dwg1/16/2020 SKJ SKJ KTS 19080294-010103 POND I qq WATERPARKDS LOCATION OF FORMER PCE < TANK TANK CONTAINMENT PAD 5 RW-3 O FORMERLY USED INFILTRATION GALLERY WATER V� � Px' M -15 r PA%00 -1 M -16 0 a W 11-RV El coNc• ""MPS RW-1 SOURCE AREA MANUFACTURING BUILDING FIRE HOUSE qq 6 O I.P. GAS TA!'"mumO MW-3 UNPAVED DRIVE 1W-14 O O MW- MW- WATER FUEi TMIIC TANK 0 t MW-1 n ❑ oRRKrc� O ® M 4-21 O o MW-23 - MW-22 PAD PAD ❑ MW-6EI _ MW-12 STA. 7 3 O MW-19 LEGEND O TYPE II MONITORING WELL (SHALLOW 0-20 FT EIGS) 13 TYPE III MONITORING WELL (DEEP 20-75 FT EIGS) (D RECOVERY WELL CIE RESIDENTIAL SUPPLY WELL too q too GRAPHIC SCALE IN FEEF 3 RESIDENTIAL SUPPLY WELL (APPROXIMATE LOCATION) OFFICES ASPtLNT PA11wIG Am ALAMAC ROAD NOTES: 1) BASE MAP FROM S&ME, FEBRUARY 2001. 2) LOCATIONS OF MW-21, MW-22, AND MW-23 ARE ESTIMATED FROM 4p1PLT PARKING rRTw I _ ENVIRONMENTAL STRATEGIES CORP (FIGURE 1, FEBRUARY 2002.) = Draper Aden Associates FACILITY LAYOUT AND GROUNDWATER SAMPLING LOCATIONS FIGURE: Engineering • Surveying • Environmental Services LUMBERTON ENERGY HOLDINGS, LLC FORMER ALAMAC AMERICAN KNITS SITE 2 114 Edinburgh South Drive, Suite 200 •Hampton Roads, VA Cary, NC 27511 •Richmond, VA , Fayetteville, NC LUMBERTON, NC 919-873-1060 Fax: 919-873-1074 • Blacksburg, VA wwwcenseom • Charlottesville, VA Northern Virginia NC Firm License # C-O861 Virginia • Beach, VA 16, 000 14,000 J 12,000 10,000 c 8,000 c� L = 6,000 d v 4,000 0 2,000 0 0 1400 1200 1000 u 800 O IA 600 400 200 0 0 Figure 3. Performance Monitoring in RW-1 Figure 3a. Chlorinated Ethene Concentrations 1,000 2,000 3,000 4,000 5,000 6,000 7,000 8,000 Days Since Startup --o—PCE fTCE —*—cis-1,2- VC --*—TOTAL VOCs DCE Figure 3b. VOC Removal 1,000 2,000 3,000 4,000 5,000 6,000 7,000 8,000 Days Since Start Up TRW-1 fRW-1 Cumul. Lbs VOCs Figure 4. Performance Monitoring in RW-2 Figure 4a. Chlorinated Ethene Concentrations 60,000 50,000 J ':"40,000 c 0 v 30,000 L Ar 0 20,000 V 10,000 0 1,000 2,000 3,000 4,000 5,000 6,000 7,000 8,000 Days Since Startup tPCE fTCE fcis-1,2- VC --)K--TOTAL VOCs DCE Figure 4b. VOC Removal 2,000 1,800 1,600 1,400 1,200 V j 1,000 a = 800 600 400 200 0 0 1,000 2,000 3,000 4,000 5,000 6,000 7,000 8,000 Days Since Start Up TRW-2 fRW-2 Cumul. Lbs VOCs Figure 5. Performance Monitoring in RW-3 Figure 5a. Chlorinated Ethene Concentrations 10,000 9,000 8,000 J a, 7,000 c 6,000 0 5,000 4,000 c 0 3,000 2,000 1,000 0 0 1,000 2,000 3,000 4,000 5,000 6,000 7,000 8,000 Days Since Startup --*-PCE fTCE fcis-1,2-DCE VC --X--Total VOCs Figure 5b. VOC Removal 1,800 1,600 1,400 1,200 0 1,000 800 600 400 200 0IF 0 1,000 2,000 3,000 4,000 5,000 6,000 7,000 8,000 Days Since Start Up TRW-3 fRW-3 Cumul. Lbs VOCs APPENDIX A FIELD NOTES APPENDIX B LABORATORY ANALYTICAL REPORTS Case Narrative Waypolnt(z) 4\1AI r I K Al Draper Arden & Associates Sean Jarvah 114 Edinburg South Drive Ste 200 Cary, NC 27511 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: ALAMAC Lab Submittal Date: 12/06/2019 Work Order: 9120098 12/19/19 13:36 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL a,j Angela D. Overcash Project Management Manager Data Qualifiers Key Reference: Reviewed By Angela D. Overcash Project Management Manager A Probable lab contaminant. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 20 Sample Receipt Summary Wapoi nt 12/19/2019 4'+lil'r II[ Al Work Order: 9120098 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received RW-1 9120098-01 Water 12/05/19 9:40 12/06/19 17:10 RW-2 9120098-02 Water 12/05/19 9:50 12/06/19 17:10 RW-3 9120098-03 Water 12/05/19 10:00 12/06/19 17:10 2237 Alamac 9120098-04 Water 12/05/19 10:30 12/06/19 17:10 Trip Blank 9120098-05 Water 12/05/19 0:00 12/06/19 17:10 Samples were received in good condition at 2.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 20 Waypoint.0 4vaI V I ICAI Summary of Detections 12/19/2019 Work Order: 9120098 Waypoint ID Client ID Parameter Method Result Units 9120098-01 RW-1 1,1-Dichloroethylene 8260D 3.6 J ug/L 9120098-01 RW-1 Benzene 8260D 2.0 J ug/L 9120098-01 RW-1 cis- 1,2-Dichloroethylene 8260D 1500 ug/L 9120098-01 RW-1 Methyl Ethyl Ketone (2-Butanone) 8260D 8.6 J ug/L 9120098-01 RW-1 Naphthalene 8260D 3.3 J ug/L 9120098-01 RW-1 Tetrachloroethylene 8260D 530 ug/L 9120098-01 RW-1 trans- 1,2-Dichloroethylene 8260D 50 ug/L 9120098-01 RW-1 Trichloroethylene 8260D 690 ug/L 9120098-01 RW-1 Vinyl chloride 8260D 63 ug/L 9120098-02 RW-2 1,1-Dichloroethane 8260D 2.5 J ug/L 9120098-02 RW-2 1,1-Dichloroethylene 8260D 14 ug/L 9120098-02 RW-2 cis- 1,2-Dichloroethylene 8260D 7100 ug/L 9120098-02 RW-2 Naphthalene 8260D 4.8 J ug/L 9120098-02 RW-2 Tetrachloroethylene 8260D 130 ug/L 9120098-02 RW-2 trans- 1,2-Dichloroethylene 8260D 40 ug/L 9120098-02 RW-2 Trichloroethylene 8260D 240 ug/L 9120098-02 RW-2 Vinyl chloride 8260D 310 ug/L 9120098-03 RW-3 1,1-Dichloroethylene 8260D 3.6 J ug/L 9120098-03 RW-3 cis- 1,2-Dichloroethylene 8260D 1800 ug/L 9120098-03 RW-3 Naphthalene 8260D 2.3 J ug/L 9120098-03 RW-3 Tetrachloroethylene 8260D 6.1 ug/L 9120098-03 RW-3 trans- 1,2-Dichloroethylene 8260D 10 ug/L 9120098-03 RW-3 Trichloroethylene 8260D 16 ug/L 9120098-03 RW-3 Vinyl chloride 8260D 240 ug/L 9120098-04 2237 Alamac Acetone 8260D 13 ug/L 9120098-04 2237 Alamac Chloroform 8260D 0.23 J ug/L 9120098-04 2237 Alamac Methyl Ethyl Ketone (2-Butanone) 8260D 12 ug/L 9120098-05 Trip Blank Methylene Chloride 8260D 0.50 A, J ug/L This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 20 Laboratory Report Way p of 1 1 12/19/2019 a 3IAI r I K Al Draper Arden & Associates Project: ALAMAC Client Sample ID: RW-1 Attn: Sean Jarvah Sample ID: 9120098-01 114 Edinburg South Drive Ste 200 Work Order: 9120098 Cary, NC 27511 Sample Matrix: Water Time Collected: 12/05/19 09:40 Time Submitted: 12/06/19 17:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL ug/L 5.0 1.1 10 8260D 12/13/19 6:55 ANG P9L0237 1,1,1-Trichloroethane BRL ug/L 5.0 0.61 10 8260D 12/13/19 6:55 ANG P9L0237 1,1,2,2-Tetrachloroethane BRL ug/L 5.0 0.36 10 8260D 12/13/19 6:55 ANG P9L0237 1,1,2-Trichloroethane BRL ug/L 5.0 0.66 10 8260D 12/13/19 6:55 ANG P9L0237 1,1-Dichloroethane BRL ug/L 5.0 0.83 10 8260D 12/13/19 6:55 ANG P9L0237 1,1-Dichloroethylene 3.6 J ug/L 5.0 0.83 10 8260D 12/13/19 6:55 ANG P9L0237 1,1-Dichloropropylene BRL ug/L 5.0 0.51 10 8260D 12/13/19 6:55 ANG P9L0237 1,2,3-Trichlorobenzene BRL ug/L 20 4.0 10 8260D 12/13/19 6:55 ANG P9L0237 1,2,3-Trichloropropane BRL ug/L 10 1.4 10 8260D 12/13/19 6:55 ANG P9L0237 1,2,4-Trichlorobenzene BRL ug/L 10 1.3 10 8260D 12/13/19 6:55 ANG P9L0237 1,2,4-Trimethyl benzene BRL ug/L 5.0 0.54 10 8260D 12/13/19 6:55 ANG P9L0237 1,2-Dibromo-3-chloropropane BRL ug/L 20 1.7 10 8260D 12/13/19 6:55 ANG P9L0237 1,2-Dibromoethane BRL ug/L 5.0 0.51 10 8260D 12/13/19 6:55 ANG P9L0237 1,2-Dichlorobenzene BRL ug/L 5.0 0.76 10 8260D 12/13/19 6:55 ANG P9L0237 1,2-Dichloroethane BRL ug/L 5.0 0.66 10 8260D 12/13/19 6:55 ANG P9L0237 1,2-Dichloropropane BRL ug/L 5.0 1.1 10 8260D 12/13/19 6:55 ANG P9L0237 1,3,5-Trimethyl benzene BRL ug/L 5.0 0.76 10 8260D 12/13/19 6:55 ANG P9L0237 1,3-Dichlorobenzene BRL ug/L 5.0 0.54 10 8260D 12/13/19 6:55 ANG P9L0237 1,3-Dichloropropane BRL ug/L 5.0 0.43 10 8260D 12/13/19 6:55 ANG P9L0237 1,4-Dichlorobenzene BRL ug/L 5.0 0.50 10 8260D 12/13/19 6:55 ANG P9L0237 2,2-Dichloropropane BRL ug/L 20 1.1 10 8260D 12/13/19 6:55 ANG P9L0237 2-Chlorotoluene BRL ug/L 5.0 0.66 10 8260D 12/13/19 6:55 ANG P9L0237 4-Chlorotoluene BRL ug/L 5.0 0.50 10 8260D 12/13/19 6:55 ANG P9L0237 4-Isopropyltoluene BRL ug/L 5.0 0.89 10 8260D 12/13/19 6:55 ANG P9L0237 Acetone BRL ug/L 50 3.1 10 8260D 12/13/19 6:55 ANG P9L0237 Acrolein BRL ug/L 200 2.0 10 8260D 12/13/19 6:55 ANG P9L0237 Acrylonitrile BRL ug/L 200 2.0 10 8260D 12/13/19 6:55 ANG P9L0237 Benzene 2.0 J ug/L 5.0 0.48 10 8260D 12/13/19 6:55 ANG P9L0237 Bromobenzene BRL ug/L 5.0 0.57 10 8260D 12/13/19 6:55 ANG P9L0237 Bromochloromethane BRL ug/L 5.0 1.4 10 8260D 12/13/19 6:55 ANG P9L0237 Bromodichloromethane BRL ug/L 5.0 0.62 10 8260D 12/13/19 6:55 ANG P9L0237 Bromoform BRL ug/L 10 0.40 10 8260D 12/13/19 6:55 ANG P9L0237 Bromomethane BRL ug/L 10 1.8 10 8260D 12/13/19 6:55 ANG P9L0237 Carbon disulfide BRL ug/L 50 0.75 10 8260D 12/13/19 6:55 ANG P9L0237 Carbon Tetrachloride BRL ug/L 5.0 1.1 10 8260D 12/13/19 6:55 ANG P9L0237 Chlorobenzene BRL ug/L 5.0 0.62 10 8260D 12/13/19 6:55 ANG P9L0237 Chloroethane BRL ug/L 5.0 2.2 10 8260D 12/13/19 6:55 ANG P9L0237 Chloroform BRL ug/L 5.0 0.76 10 8260D 12/13/19 6:55 ANG P9L0237 Chloromethane BRL ug/L 5.0 0.79 10 8260D 12/13/19 6:55 ANG P9L0237 cis-1,2-Dichloroethylene 1500 ug/L 50 5.6 100 8260D 12/13/19 7:21 ANG P9L0237 cis-1,3-Dichloropropylene BRL ug/L 5.0 0.79 10 8260D 12/13/19 6:55 ANG P9L0237 Dibromochloromethane BRL ug/L 5.0 0.81 10 8260D 12/13/19 6:55 ANG P9L0237 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 20 Laboratory Report Way p of 1 1 12/19/2019 4 +141 r I I[ Al Draper Arden & Associates Project: ALAMAC Client Sample ID: RW-1 Attn: Sean Jarvah Sample ID: 9120098-01 114 Edinburg South Drive Ste 200 Work Order: 9120098 Cary, NC 27511 Sample Matrix: Water Time Collected: 12/05/19 09:40 Time Submitted: 12/06/19 17:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dibromomethane BRL ug/L 5.0 0.65 10 8260D 12/13/19 6:55 ANG P9L0237 Dichlorodifluoromethane BRL ug/L 50 1.1 10 8260D 12/13/19 6:55 ANG P9L0237 Ethylbenzene BRL ug/L 5.0 0.61 10 8260D 12/13/19 6:55 ANG P9L0237 Hexachlorobutadiene BRL ug/L 20 1.6 10 8260D 12/13/19 6:55 ANG P9L0237 Isopropyl Ether BRL ug/L 5.0 0.50 10 8260D 12/13/19 6:55 ANG P9L0237 Isopropylbenzene (Cumene) BRL ug/L 5.0 0.54 10 8260D 12/13/19 6:55 ANG P9L0237 m,p-Xylenes BRL ug/L 10 1.2 10 8260D 12/13/19 6:55 ANG P9L0237 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 50 0.65 10 8260D 12/13/19 6:55 ANG P9L0237 Methyl Ethyl Ketone (2-Butanone) 8.6 J ug/L 50 2.4 10 8260D 12/13/19 6:55 ANG P9L0237 Methyl Isobutyl Ketone BRL ug/L 50 0.78 10 8260D 12/13/19 6:55 ANG P9L0237 Methylene Chloride BRL ug/L 10 0.83 10 8260D 12/13/19 6:55 ANG P9L0237 Methyl-tert-Butyl Ether BRL ug/L 5.0 0.42 10 8260D 12/13/19 6:55 ANG P9L0237 Naphthalene 3.3 J ug/L 10 1.9 10 8260D 12/13/19 6:55 ANG P9L0237 n-Butylbenzene BRL ug/L 10 0.76 10 8260D 12/13/19 6:55 ANG P9L0237 n-Propylbenzene BRL ug/L 5.0 0.87 10 8260D 12/13/19 6:55 ANG P9L0237 o-Xylene BRL ug/L 5.0 0.44 10 8260D 12/13/19 6:55 ANG P9L0237 sec-Butylbenzene BRL ug/L 5.0 0.76 10 8260D 12/13/19 6:55 ANG P9L0237 Styrene BRL ug/L 5.0 0.47 10 8260D 12/13/19 6:55 ANG P9L0237 tert-Butylbenzene BRL ug/L 5.0 0.88 10 8260D 12/13/19 6:55 ANG P9L0237 Tetrachloroethylene 530 ug/L 5.0 0.98 10 8260D 12/13/19 6:55 ANG P9L0237 Toluene BRL ug/L 5.0 0.44 10 8260D 12/13/19 6:55 ANG P9L0237 trans-1,2-Dichloroethylene 50 ug/L 5.0 0.94 10 8260D 12/13/19 6:55 ANG P9L0237 trans- 1,3-Dichloropropylene BRL ug/L 5.0 0.70 10 8260D 12/13/19 6:55 ANG P9L0237 Trichloroethylene 690 ug/L 5.0 0.78 10 8260D 12/13/19 6:55 ANG P9L0237 Trichlorofluoromethane BRL ug/L 5.0 0.62 10 8260D 12/13/19 6:55 ANG P9L0237 Vinyl acetate BRL ug/L 20 0.60 10 8260D 12/13/19 6:55 ANG P9L0237 Vinyl chloride 63 ug/L 5.0 0.97 10 8260D 12/13/19 6:55 ANG P9L0237 Xylenes, total BRL ug/L 15 1.5 10 8260D 12/13/19 6:55 ANG P9L0237 Surrogate Recovery Control Limits 4-Bromofluorobenzene 98 % 80-124 Dibromofluoromethane 96 % 75-129 Toluene-d8 85 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 20 Laboratory Report Way p of 1 1 12/19/2019 a 3IAI r I K Al Draper Arden & Associates Project: ALAMAC Client Sample ID: RW-2 Attn: Sean Jarvah Sample ID: 9120098-02 114 Edinburg South Drive Ste 200 Work Order: 9120098 Cary, NC 27511 Sample Matrix: Water Time Collected: 12/05/19 09:50 Time Submitted: 12/06/19 17:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL ug/L 5.0 1.1 10 8260D 12/13/19 7:47 ANG P9L0237 1,1,1-Trichloroethane BRL ug/L 5.0 0.61 10 8260D 12/13/19 7:47 ANG P9L0237 1,1,2,2-Tetrachloroethane BRL ug/L 5.0 0.36 10 8260D 12/13/19 7:47 ANG P9L0237 1,1,2-Trichloroethane BRL ug/L 5.0 0.66 10 8260D 12/13/19 7:47 ANG P9L0237 1,1-Dichloroethane 2.5 J ug/L 5.0 0.83 10 8260D 12/13/19 7:47 ANG P9L0237 1,1-Dichloroethylene 14 ug/L 5.0 0.83 10 8260D 12/13/19 7:47 ANG P9L0237 1,1-Dichloropropylene BRL ug/L 5.0 0.51 10 8260D 12/13/19 7:47 ANG P9L0237 1,2,3-Trichlorobenzene BRL ug/L 20 4.0 10 8260D 12/13/19 7:47 ANG P9L0237 1,2,3-Trichloropropane BRL ug/L 10 1.4 10 8260D 12/13/19 7:47 ANG P9L0237 1,2,4-Trichlorobenzene BRL ug/L 10 1.3 10 8260D 12/13/19 7:47 ANG P9L0237 1,2,4-Trimethyl benzene BRL ug/L 5.0 0.54 10 8260D 12/13/19 7:47 ANG P9L0237 1,2-Dibromo-3-chloropropane BRL ug/L 20 1.7 10 8260D 12/13/19 7:47 ANG P9L0237 1,2-Dibromoethane BRL ug/L 5.0 0.51 10 8260D 12/13/19 7:47 ANG P9L0237 1,2-Dichlorobenzene BRL ug/L 5.0 0.76 10 8260D 12/13/19 7:47 ANG P9L0237 1,2-Dichloroethane BRL ug/L 5.0 0.66 10 8260D 12/13/19 7:47 ANG P9L0237 1,2-Dichloropropane BRL ug/L 5.0 1.1 10 8260D 12/13/19 7:47 ANG P9L0237 1,3,5-Trimethyl benzene BRL ug/L 5.0 0.76 10 8260D 12/13/19 7:47 ANG P9L0237 1,3-Dichlorobenzene BRL ug/L 5.0 0.54 10 8260D 12/13/19 7:47 ANG P9L0237 1,3-Dichloropropane BRL ug/L 5.0 0.43 10 8260D 12/13/19 7:47 ANG P9L0237 1,4-Dichlorobenzene BRL ug/L 5.0 0.50 10 8260D 12/13/19 7:47 ANG P9L0237 2,2-Dichloropropane BRL ug/L 20 1.1 10 8260D 12/13/19 7:47 ANG P9L0237 2-Chlorotoluene BRL ug/L 5.0 0.66 10 8260D 12/13/19 7:47 ANG P9L0237 4-Chlorotoluene BRL ug/L 5.0 0.50 10 8260D 12/13/19 7:47 ANG P9L0237 4-Isopropyltoluene BRL ug/L 5.0 0.89 10 8260D 12/13/19 7:47 ANG P9L0237 Acetone BRL ug/L 50 3.1 10 8260D 12/13/19 7:47 ANG P9L0237 Acrolein BRL ug/L 200 2.0 10 8260D 12/13/19 7:47 ANG P9L0237 Acrylonitrile BRL ug/L 200 2.0 10 8260D 12/13/19 7:47 ANG P9L0237 Benzene BRL ug/L 5.0 0.48 10 8260D 12/13/19 7:47 ANG P9L0237 Bromobenzene BRL ug/L 5.0 0.57 10 8260D 12/13/19 7:47 ANG P9L0237 Bromochloromethane BRL ug/L 5.0 1.4 10 8260D 12/13/19 7:47 ANG P9L0237 Bromodichloromethane BRL ug/L 5.0 0.62 10 8260D 12/13/19 7:47 ANG P9L0237 Bromoform BRL ug/L 10 0.40 10 8260D 12/13/19 7:47 ANG P9L0237 Bromomethane BRL ug/L 10 1.8 10 8260D 12/13/19 7:47 ANG P9L0237 Carbon disulfide BRL ug/L 50 0.75 10 8260D 12/13/19 7:47 ANG P9L0237 Carbon Tetrachloride BRL ug/L 5.0 1.1 10 8260D 12/13/19 7:47 ANG P9L0237 Chlorobenzene BRL ug/L 5.0 0.62 10 8260D 12/13/19 7:47 ANG P9L0237 Chloroethane BRL ug/L 5.0 2.2 10 8260D 12/13/19 7:47 ANG P9L0237 Chloroform BRL ug/L 5.0 0.76 10 8260D 12/13/19 7:47 ANG P9L0237 Chloromethane BRL ug/L 5.0 0.79 10 8260D 12/13/19 7:47 ANG P9L0237 cis-1,2-Dichloroethylene 7100 ug/L 50 5.6 100 8260D 12/13/19 8:13 ANG P9L0237 cis-1,3-Dichloropropylene BRL ug/L 5.0 0.79 10 8260D 12/13/19 7:47 ANG P9L0237 Dibromochloromethane BRL ug/L 5.0 0.81 10 8260D 12/13/19 7:47 ANG P9L0237 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 20 Laboratory Report Way p of 1 1 12/19/2019 4 +141 r I I[ Al Draper Arden & Associates Project: ALAMAC Client Sample ID: RW-2 Attn: Sean Jarvah Sample ID: 9120098-02 114 Edinburg South Drive Ste 200 Work Order: 9120098 Cary, NC 27511 Sample Matrix: Water Time Collected: 12/05/19 09:50 Time Submitted: 12/06/19 17:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dibromomethane BRL ug/L 5.0 0.65 10 8260D 12/13/19 7:47 ANG P91-0237 Dichlorodifluoromethane BRL ug/L 50 1.1 10 8260D 12/13/19 7:47 ANG P91-0237 Ethylbenzene BRL ug/L 5.0 0.61 10 8260D 12/13/19 7:47 ANG P91-0237 Hexachlorobutadiene BRL ug/L 20 1.6 10 8260D 12/13/19 7:47 ANG P91-0237 Isopropyl Ether BRL ug/L 5.0 0.50 10 8260D 12/13/19 7:47 ANG P91-0237 Isopropylbenzene (Cumene) BRL ug/L 5.0 0.54 10 8260D 12/13/19 7:47 ANG P91-0237 m,p-Xylenes BRL ug/L 10 1.2 10 8260D 12/13/19 7:47 ANG P91-0237 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 50 0.65 10 8260D 12/13/19 7:47 ANG P91-0237 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 50 2.4 10 8260D 12/13/19 7:47 ANG P91-0237 Methyl Isobutyl Ketone BRL ug/L 50 0.78 10 8260D 12/13/19 7:47 ANG P91-0237 Methylene Chloride BRL ug/L 10 0.83 10 8260D 12/13/19 7:47 ANG P91-0237 Methyl-tert-Butyl Ether BRL ug/L 5.0 0.42 10 8260D 12/13/19 7:47 ANG P91-0237 Naphthalene 4.8 J ug/L 10 1.9 10 8260D 12/13/19 7:47 ANG P91-0237 n-Butylbenzene BRL ug/L 10 0.76 10 8260D 12/13/19 7:47 ANG P91-0237 n-Propylbenzene BRL ug/L 5.0 0.87 10 8260D 12/13/19 7:47 ANG P91-0237 o-Xylene BRL ug/L 5.0 0.44 10 8260D 12/13/19 7:47 ANG P91-0237 sec-Butylbenzene BRL ug/L 5.0 0.76 10 8260D 12/13/19 7:47 ANG P91-0237 Styrene BRL ug/L 5.0 0.47 10 8260D 12/13/19 7:47 ANG P91-0237 tert-Butylbenzene BRL ug/L 5.0 0.88 10 8260D 12/13/19 7:47 ANG P91-0237 Tetrachloroethylene 130 ug/L 5.0 0.98 10 8260D 12/13/19 7:47 ANG P91-0237 Toluene BRL ug/L 5.0 0.44 10 8260D 12/13/19 7:47 ANG P91-0237 trans-1,2-Dichloroethylene 40 ug/L 5.0 0.94 10 8260D 12/13/19 7:47 ANG P91-0237 trans-1,3-Dichloropropylene BRL ug/L 5.0 0.70 10 8260D 12/13/19 7:47 ANG P91-0237 Trichloroethylene 240 ug/L 5.0 0.78 10 8260D 12/13/19 7:47 ANG P91-0237 Trichlorofluoromethane BRL ug/L 5.0 0.62 10 8260D 12/13/19 7:47 ANG P91-0237 Vinyl acetate BRL ug/L 20 0.60 10 8260D 12/13/19 7:47 ANG P91-0237 Vinyl chloride 310 ug/L 5.0 0.97 10 8260D 12/13/19 7:47 ANG P91-0237 Xylenes, total BRL ug/L 15 1.5 10 8260D 12/13/19 7:47 ANG P91-0237 Surrogate Recovery Control Limits 4-Bromofluorobenzene 96 % 80-124 Dibromofluoromethane 97 % 75-129 Toluene-d8 85 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 20 Laboratory Report Way p of 1 1 12/19/2019 4 +IAI r I K Al Draper Arden & Associates Project: ALAMAC Client Sample ID: RW-3 Attn: Sean Jarvah Sample ID: 9120098-03 114 Edinburg South Drive Ste 200 Work Order: 9120098 Cary, NC 27511 Sample Matrix: Water Time Collected: 12/05/19 10:00 Time Submitted: 12/06/19 17:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL ug/L 5.0 1.1 10 8260D 12/13/19 8:39 ANG P9L0237 1,1,1-Trichloroethane BRL ug/L 5.0 0.61 10 8260D 12/13/19 8:39 ANG P9L0237 1,1,2,2-Tetrachloroethane BRL ug/L 5.0 0.36 10 8260D 12/13/19 8:39 ANG P9L0237 1,1,2-Trichloroethane BRL ug/L 5.0 0.66 10 8260D 12/13/19 8:39 ANG P9L0237 1,1-Dichloroethane BRL ug/L 5.0 0.83 10 8260D 12/13/19 8:39 ANG P9L0237 1,1-Dichloroethylene 3.6 J ug/L 5.0 0.83 10 8260D 12/13/19 8:39 ANG P9L0237 1,1-Dichloropropylene BRL ug/L 5.0 0.51 10 8260D 12/13/19 8:39 ANG P9L0237 1,2,3-Trichlorobenzene BRL ug/L 20 4.0 10 8260D 12/13/19 8:39 ANG P9L0237 1,2,3-Trichloropropane BRL ug/L 10 1.4 10 8260D 12/13/19 8:39 ANG P9L0237 1,2,4-Trichlorobenzene BRL ug/L 10 1.3 10 8260D 12/13/19 8:39 ANG P9L0237 1,2,4-Trimethyl benzene BRL ug/L 5.0 0.54 10 8260D 12/13/19 8:39 ANG P9L0237 1,2-Dibromo-3-chloropropane BRL ug/L 20 1.7 10 8260D 12/13/19 8:39 ANG P9L0237 1,2-Dibromoethane BRL ug/L 5.0 0.51 10 8260D 12/13/19 8:39 ANG P9L0237 1,2-Dichlorobenzene BRL ug/L 5.0 0.76 10 8260D 12/13/19 8:39 ANG P9L0237 1,2-Dichloroethane BRL ug/L 5.0 0.66 10 8260D 12/13/19 8:39 ANG P9L0237 1,2-Dichloropropane BRL ug/L 5.0 1.1 10 8260D 12/13/19 8:39 ANG P9L0237 1,3,5-Trimethyl benzene BRL ug/L 5.0 0.76 10 8260D 12/13/19 8:39 ANG P9L0237 1,3-Dichlorobenzene BRL ug/L 5.0 0.54 10 8260D 12/13/19 8:39 ANG P9L0237 1,3-Dichloropropane BRL ug/L 5.0 0.43 10 8260D 12/13/19 8:39 ANG P9L0237 1,4-Dichlorobenzene BRL ug/L 5.0 0.50 10 8260D 12/13/19 8:39 ANG P9L0237 2,2-Dichloropropane BRL ug/L 20 1.1 10 8260D 12/13/19 8:39 ANG P9L0237 2-Chlorotoluene BRL ug/L 5.0 0.66 10 8260D 12/13/19 8:39 ANG P9L0237 4-Chlorotoluene BRL ug/L 5.0 0.50 10 8260D 12/13/19 8:39 ANG P9L0237 4-Isopropyltoluene BRL ug/L 5.0 0.89 10 8260D 12/13/19 8:39 ANG P9L0237 Acetone BRL ug/L 50 3.1 10 8260D 12/13/19 8:39 ANG P9L0237 Acrolein BRL ug/L 200 2.0 10 8260D 12/13/19 8:39 ANG P9L0237 Acrylonitrile BRL ug/L 200 2.0 10 8260D 12/13/19 8:39 ANG P9L0237 Benzene BRL ug/L 5.0 0.48 10 8260D 12/13/19 8:39 ANG P9L0237 Bromobenzene BRL ug/L 5.0 0.57 10 8260D 12/13/19 8:39 ANG P9L0237 Bromochloromethane BRL ug/L 5.0 1.4 10 8260D 12/13/19 8:39 ANG P9L0237 Bromodichloromethane BRL ug/L 5.0 0.62 10 8260D 12/13/19 8:39 ANG P9L0237 Bromoform BRL ug/L 10 0.40 10 8260D 12/13/19 8:39 ANG P9L0237 Bromomethane BRL ug/L 10 1.8 10 8260D 12/13/19 8:39 ANG P9L0237 Carbon disulfide BRL ug/L 50 0.75 10 8260D 12/13/19 8:39 ANG P9L0237 Carbon Tetrachloride BRL ug/L 5.0 1.1 10 8260D 12/13/19 8:39 ANG P9L0237 Chlorobenzene BRL ug/L 5.0 0.62 10 8260D 12/13/19 8:39 ANG P9L0237 Chloroethane BRL ug/L 5.0 2.2 10 8260D 12/13/19 8:39 ANG P9L0237 Chloroform BRL ug/L 5.0 0.76 10 8260D 12/13/19 8:39 ANG P9L0237 Chloromethane BRL ug/L 5.0 0.79 10 8260D 12/13/19 8:39 ANG P9L0237 cis-1,2-Dichloroethylene 1800 ug/L 50 5.6 100 8260D 12/13/19 9:05 ANG P9L0237 cis-1,3-Dichloropropylene BRL ug/L 5.0 0.79 10 8260D 12/13/19 8:39 ANG P9L0237 Dibromochloromethane BRL ug/L 5.0 0.81 10 8260D 12/13/19 8:39 ANG P9L0237 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 20 Laboratory Report Way p of 1 1 12/19/2019 4 +141 r I I[ Al Draper Arden & Associates Project: ALAMAC Client Sample ID: RW-3 Attn: Sean Jarvah Sample ID: 9120098-03 114 Edinburg South Drive Ste 200 Work Order: 9120098 Cary, NC 27511 Sample Matrix: Water Time Collected: 12/05/19 10:00 Time Submitted: 12/06/19 17:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dibromomethane BRL ug/L 5.0 0.65 10 8260D 12/13/19 8:39 ANG P91-0237 Dichlorodifluoromethane BRL ug/L 50 1.1 10 8260D 12/13/19 8:39 ANG P91-0237 Ethylbenzene BRL ug/L 5.0 0.61 10 8260D 12/13/19 8:39 ANG P91-0237 Hexachlorobutadiene BRL ug/L 20 1.6 10 8260D 12/13/19 8:39 ANG P91-0237 Isopropyl Ether BRL ug/L 5.0 0.50 10 8260D 12/13/19 8:39 ANG P91-0237 Isopropylbenzene (Cumene) BRL ug/L 5.0 0.54 10 8260D 12/13/19 8:39 ANG P91-0237 m,p-Xylenes BRL ug/L 10 1.2 10 8260D 12/13/19 8:39 ANG P91-0237 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 50 0.65 10 8260D 12/13/19 8:39 ANG P91-0237 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 50 2.4 10 8260D 12/13/19 8:39 ANG P91-0237 Methyl Isobutyl Ketone BRL ug/L 50 0.78 10 8260D 12/13/19 8:39 ANG P91-0237 Methylene Chloride BRL ug/L 10 0.83 10 8260D 12/13/19 8:39 ANG P91-0237 Methyl-tert-Butyl Ether BRL ug/L 5.0 0.42 10 8260D 12/13/19 8:39 ANG P91-0237 Naphthalene 2.3 J ug/L 10 1.9 10 8260D 12/13/19 8:39 ANG P91-0237 n-Butylbenzene BRL ug/L 10 0.76 10 8260D 12/13/19 8:39 ANG P91-0237 n-Propylbenzene BRL ug/L 5.0 0.87 10 8260D 12/13/19 8:39 ANG P91-0237 o-Xylene BRL ug/L 5.0 0.44 10 8260D 12/13/19 8:39 ANG P91-0237 sec-Butylbenzene BRL ug/L 5.0 0.76 10 8260D 12/13/19 8:39 ANG P91-0237 Styrene BRL ug/L 5.0 0.47 10 8260D 12/13/19 8:39 ANG P91-0237 tert-Butylbenzene BRL ug/L 5.0 0.88 10 8260D 12/13/19 8:39 ANG P91-0237 Tetrachloroethylene 6.1 ug/L 5.0 0.98 10 8260D 12/13/19 8:39 ANG P91-0237 Toluene BRL ug/L 5.0 0.44 10 8260D 12/13/19 8:39 ANG P91-0237 trans-1,2-Dichloroethylene 10 ug/L 5.0 0.94 10 8260D 12/13/19 8:39 ANG P91-0237 trans-1,3-Dichloropropylene BRL ug/L 5.0 0.70 10 8260D 12/13/19 8:39 ANG P91-0237 Trichloroethylene 16 ug/L 5.0 0.78 10 8260D 12/13/19 8:39 ANG P91-0237 Trichlorofluoromethane BRL ug/L 5.0 0.62 10 8260D 12/13/19 8:39 ANG P91-0237 Vinyl acetate BRL ug/L 20 0.60 10 8260D 12/13/19 8:39 ANG P91-0237 Vinyl chloride 240 ug/L 5.0 0.97 10 8260D 12/13/19 8:39 ANG P91-0237 Xylenes, total BRL ug/L 15 1.5 10 8260D 12/13/19 8:39 ANG P91-0237 Surrogate Recovery Control Limits 4-Bromofluorobenzene 97 % 80-124 Dibromofluoromethane 97 % 75-129 Toluene-d8 86 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 20 Laboratory Report Way p of 1 1 12/19/2019 4 +IAI r I K Al Draper Arden & Associates Project: ALAMAC Client Sample ID: 2237 Alamac Attn: Sean Jarvah Sample ID: 9120098-04 114 Edinburg South Drive Ste 200 Work Order: 9120098 Cary, NC 27511 Sample Matrix: Water Time Collected: 12/05/19 10:30 Time Submitted: 12/06/19 17:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 12/13/19 3:28 ANG P9L0237 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 12/13/19 3:28 ANG P9L0237 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 12/13/19 3:28 ANG P9L0237 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 12/13/19 3:28 ANG P9L0237 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 12/13/19 3:28 ANG P9L0237 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 12/13/19 3:28 ANG P9L0237 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 12/13/19 3:28 ANG P9L0237 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 12/13/19 3:28 ANG P9L0237 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 12/13/19 3:28 ANG P9L0237 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 12/13/19 3:28 ANG P9L0237 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 12/13/19 3:28 ANG P9L0237 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 12/13/19 3:28 ANG P9L0237 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 12/13/19 3:28 ANG P9L0237 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 12/13/19 3:28 ANG P9L0237 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 12/13/19 3:28 ANG P9L0237 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 12/13/19 3:28 ANG P9L0237 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 12/13/19 3:28 ANG P9L0237 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 12/13/19 3:28 ANG P9L0237 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 12/13/19 3:28 ANG P9L0237 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 12/13/19 3:28 ANG P9L0237 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 12/13/19 3:28 ANG P9L0237 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 12/13/19 3:28 ANG P9L0237 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 12/13/19 3:28 ANG P9L0237 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 12/13/19 3:28 ANG P9L0237 Acetone 13 ug/L 5.0 0.31 1 8260D 12/13/19 3:28 ANG P9L0237 Acrolein BRL ug/L 20 0.20 1 8260D 12/13/19 3:28 ANG P9L0237 Acrylonitrile BRL ug/L 20 0.20 1 8260D 12/13/19 3:28 ANG P9L0237 Benzene BRL ug/L 0.50 0.048 1 8260D 12/13/19 3:28 ANG P9L0237 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 12/13/19 3:28 ANG P9L0237 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 12/13/19 3:28 ANG P9L0237 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 12/13/19 3:28 ANG P9L0237 Bromoform BRL ug/L 1.0 0.040 1 8260D 12/13/19 3:28 ANG P9L0237 Bromomethane BRL ug/L 1.0 0.18 1 8260D 12/13/19 3:28 ANG P9L0237 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 12/13/19 3:28 ANG P9L0237 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 12/13/19 3:28 ANG P9L0237 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 12/13/19 3:28 ANG P9L0237 Chloroethane BRL ug/L 0.50 0.22 1 8260D 12/13/19 3:28 ANG P9L0237 Chloroform 0.23 J ug/L 0.50 0.076 1 8260D 12/13/19 3:28 ANG P9L0237 Chloromethane BRL ug/L 0.50 0.079 1 8260D 12/13/19 3:28 ANG P9L0237 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 12/13/19 3:28 ANG P9L0237 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 12/13/19 3:28 ANG P9L0237 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 12/13/19 3:28 ANG P9L0237 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 20 Laboratory Report Way p of 1 1 12/19/2019 4 +1.J r I I[ Al Draper Arden & Associates Project: ALAMAC Client Sample ID: 2237 Alamac Attn: Sean Jarvah Sample ID: 9120098-04 114 Edinburg South Drive Ste 200 Work Order: 9120098 Cary, NC 27511 Sample Matrix: Water Time Collected: 12/05/19 10:30 Time Submitted: 12/06/19 17:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dibromomethane BRL ug/L 0.50 0.065 1 8260D 12/13/19 3:28 ANG P9L0237 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 12/13/19 3:28 ANG P9L0237 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 12/13/19 3:28 ANG P9L0237 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 12/13/19 3:28 ANG P9L0237 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260D 12/13/19 3:28 ANG P9L0237 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 12/13/19 3:28 ANG P9L0237 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 12/13/19 3:28 ANG P9L0237 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 12/13/19 3:28 ANG P9L0237 Methyl Ethyl Ketone (2-Butanone) 12 ug/L 5.0 0.24 1 8260D 12/13/19 3:28 ANG P9L0237 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260D 12/13/19 3:28 ANG P9L0237 Methylene Chloride BRL ug/L 1.0 0.083 1 8260D 12/13/19 3:28 ANG P9L0237 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 12/13/19 3:28 ANG P9L0237 Naphthalene BRL ug/L 1.0 0.19 1 8260D 12/13/19 3:28 ANG P9L0237 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 12/13/19 3:28 ANG P9L0237 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 12/13/19 3:28 ANG P9L0237 o-Xylene BRL ug/L 0.50 0.044 1 8260D 12/13/19 3:28 ANG P9L0237 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 12/13/19 3:28 ANG P9L0237 Styrene BRL ug/L 0.50 0.047 1 8260D 12/13/19 3:28 ANG P9L0237 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 12/13/19 3:28 ANG P9L0237 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260D 12/13/19 3:28 ANG P9L0237 Toluene BRL ug/L 0.50 0.044 1 8260D 12/13/19 3:28 ANG P9L0237 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 12/13/19 3:28 ANG P9L0237 trans- 1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 12/13/19 3:28 ANG P9L0237 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 12/13/19 3:28 ANG P9L0237 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 12/13/19 3:28 ANG P9L0237 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 12/13/19 3:28 ANG P9L0237 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 12/13/19 3:28 ANG P9L0237 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 12/13/19 3:28 ANG P9L0237 Surrogate Recovery Control Limits 4-Bromofluorobenzene 97 % 80-124 Dibromofluoromethane 98 % 75-129 Toluene-d8 86 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 20 Laboratory Report Way p of 1 1 12/19/2019 4 +IAI r I K Al Draper Arden & Associates Project: ALAMAC Client Sample ID: Trip Blank Attn: Sean Jarvah Sample ID: 9120098-05 114 Edinburg South Drive Ste 200 Work Order: 9120098 Cary, NC 27511 Sample Matrix: Water Time Collected: 12/05/19 00:00 Time Submitted: 12/06/19 17:10 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260D 12/13/19 3:02 ANG P9L0237 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260D 12/13/19 3:02 ANG P9L0237 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260D 12/13/19 3:02 ANG P9L0237 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260D 12/13/19 3:02 ANG P9L0237 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260D 12/13/19 3:02 ANG P9L0237 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260D 12/13/19 3:02 ANG P9L0237 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260D 12/13/19 3:02 ANG P9L0237 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260D 12/13/19 3:02 ANG P9L0237 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260D 12/13/19 3:02 ANG P9L0237 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260D 12/13/19 3:02 ANG P9L0237 1,2,4-Trimethyl benzene BRL ug/L 0.50 0.054 1 8260D 12/13/19 3:02 ANG P9L0237 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260D 12/13/19 3:02 ANG P9L0237 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260D 12/13/19 3:02 ANG P9L0237 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260D 12/13/19 3:02 ANG P9L0237 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260D 12/13/19 3:02 ANG P9L0237 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260D 12/13/19 3:02 ANG P9L0237 1,3,5-Trimethyl benzene BRL ug/L 0.50 0.076 1 8260D 12/13/19 3:02 ANG P9L0237 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260D 12/13/19 3:02 ANG P9L0237 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260D 12/13/19 3:02 ANG P9L0237 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260D 12/13/19 3:02 ANG P9L0237 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260D 12/13/19 3:02 ANG P9L0237 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260D 12/13/19 3:02 ANG P9L0237 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260D 12/13/19 3:02 ANG P9L0237 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260D 12/13/19 3:02 ANG P9L0237 Acetone BRL ug/L 5.0 0.31 1 8260D 12/13/19 3:02 ANG P9L0237 Acrolein BRL ug/L 20 0.20 1 8260D 12/13/19 3:02 ANG P9L0237 Acrylonitrile BRL ug/L 20 0.20 1 8260D 12/13/19 3:02 ANG P9L0237 Benzene BRL ug/L 0.50 0.048 1 8260D 12/13/19 3:02 ANG P9L0237 Bromobenzene BRL ug/L 0.50 0.057 1 8260D 12/13/19 3:02 ANG P9L0237 Bromochloromethane BRL ug/L 0.50 0.14 1 8260D 12/13/19 3:02 ANG P9L0237 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260D 12/13/19 3:02 ANG P9L0237 Bromoform BRL ug/L 1.0 0.040 1 8260D 12/13/19 3:02 ANG P9L0237 Bromomethane BRL ug/L 1.0 0.18 1 8260D 12/13/19 3:02 ANG P9L0237 Carbon disulfide BRL ug/L 5.0 0.075 1 8260D 12/13/19 3:02 ANG P9L0237 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260D 12/13/19 3:02 ANG P9L0237 Chlorobenzene BRL ug/L 0.50 0.062 1 8260D 12/13/19 3:02 ANG P9L0237 Chloroethane BRL ug/L 0.50 0.22 1 8260D 12/13/19 3:02 ANG P9L0237 Chloroform BRL ug/L 0.50 0.076 1 8260D 12/13/19 3:02 ANG P9L0237 Chloromethane BRL ug/L 0.50 0.079 1 8260D 12/13/19 3:02 ANG P9L0237 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260D 12/13/19 3:02 ANG P9L0237 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260D 12/13/19 3:02 ANG P9L0237 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260D 12/13/19 3:02 ANG P9L0237 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 0f 20 Laboratory Report Way p of 1 1 12/19/2019 4 +1.J r I I[ Al Draper Arden & Associates Project: ALAMAC Client Sample ID: Trip Blank Attn: Sean Jarvah Sample ID: 9120098-05 114 Edinburg South Drive Ste 200 Work Order: 9120098 Cary, NC 27511 Sample Matrix: Water Time Collected: 12/05/19 00:00 Time Submitted: 12/06/19 17:10 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dibromomethane BRL ug/L 0.50 0.065 1 8260D 12/13/19 3:02 ANG P91-0237 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260D 12/13/19 3:02 ANG P91-0237 Ethylbenzene BRL ug/L 0.50 0.061 1 8260D 12/13/19 3:02 ANG P91-0237 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260D 12/13/19 3:02 ANG P91-0237 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260D 12/13/19 3:02 ANG P91-0237 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260D 12/13/19 3:02 ANG P91-0237 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260D 12/13/19 3:02 ANG P91-0237 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260D 12/13/19 3:02 ANG P91-0237 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260D 12/13/19 3:02 ANG P91-0237 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260D 12/13/19 3:02 ANG P91-0237 Methylene Chloride 0.50 A, J ug/L 1.0 0.083 1 8260D 12/13/19 3:02 ANG P91-0237 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260D 12/13/19 3:02 ANG P91-0237 Naphthalene BRL ug/L 1.0 0.19 1 8260D 12/13/19 3:02 ANG P91-0237 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 12/13/19 3:02 ANG P91-0237 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260D 12/13/19 3:02 ANG P91-0237 o-Xylene BRL ug/L 0.50 0.044 1 8260D 12/13/19 3:02 ANG P91-0237 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260D 12/13/19 3:02 ANG P91-0237 Styrene BRL ug/L 0.50 0.047 1 8260D 12/13/19 3:02 ANG P91-0237 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260D 12/13/19 3:02 ANG P91-0237 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260D 12/13/19 3:02 ANG P91-0237 Toluene BRL ug/L 0.50 0.044 1 8260D 12/13/19 3:02 ANG P91-0237 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260D 12/13/19 3:02 ANG P91-0237 trans- 1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260D 12/13/19 3:02 ANG P91-0237 Trichloroethylene BRL ug/L 0.50 0.078 1 8260D 12/13/19 3:02 ANG P91-0237 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260D 12/13/19 3:02 ANG P91-0237 Vinyl acetate BRL ug/L 2.0 0.060 1 8260D 12/13/19 3:02 ANG P91-0237 Vinyl chloride BRL ug/L 0.50 0.097 1 8260D 12/13/19 3:02 ANG P91-0237 Xylenes, total BRL ug/L 1.5 0.15 1 8260D 12/13/19 3:02 ANG P91-0237 Surrogate Recovery Control Limits 4-Bromofluorobenzene 98 % 80-124 Dibromofluoromethane 96 % 75-129 Toluene-d8 88 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 20 Waypoint. ANALYTICAL Level II QC Report 12/19/19 Draper Arden & Associates Project: ALAMAC Attn: Sean Jarvah 114 Edinburg South Drive Ste 200 Cary, NC 27511 Volatile Organic Compounds by GC/MS - Quality Control Work Order: 9120098 Time Submitted: 12/6/2019 5:10:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P91-0237 - 5030B Blank (P91-0237-131-K1) Prepared: 12/12/19 Analyzed: 12/13/19 1,1,1,2-Tetrachloroethane BRL 0.50 ug/L 1,1,1-Trichloroethane BRL 0.50 ug/L 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 1,1,2-Trichloroethane BRL 0.50 ug/L 1,1-Dichloroethane BRL 0.50 ug/L 1,1-Dichloroethylene BRL 0.50 ug/L 1,1-Dichloropropylene BRL 0.50 ug/L 1,2,3-Trichlorobenzene BRL 2.0 ug/L 1,2,3-Trichloropropane BRL 1.0 ug/L 1,2,4-Trichlorobenzene BRL 1.0 ug/L 1,2,4-Trimethyl benzene BRL 0.50 ug/L 1,2-Dibromo-3-chloropropane BRL 2.0 ug/L 1,2-Dibromoethane BRL 0.50 ug/L 1,2-Dichlorobenzene BRL 0.50 ug/L 1,2-Dichloroethane BRL 0.50 ug/L 1,2-Dichloropropane BRL 0.50 ug/L 1,3,5-Trimethyl benzene BRL 0.50 ug/L 1,3-Dichlorobenzene BRL 0.50 ug/L 1,3-Dichloropropane BRL 0.50 ug/L 1,4-Dichlorobenzene BRL 0.50 ug/L 2,2-Dichloropropane BRL 2.0 ug/L 2-Chlorotoluene BRL 0.50 ug/L 4-Chlorotoluene BRL 0.50 ug/L 4-Isopropyltoluene BRL 0.50 ug/L Acetone BRL 5.0 ug/L Acrolein BRL 20 ug/L Acrylonitrile BRL 20 ug/L Benzene BRL 0.50 ug/L Bromobenzene BRL 0.50 ug/L Bromochloromethane BRL 0.50 ug/L Bromodichloromethane BRL 0.50 ug/L Bromoform BRL 1.0 ug/L Bromomethane BRL 1.0 ug/L Carbon disulfide BRL 5.0 ug/L Carbon Tetrachloride BRL 0.50 ug/L Chlorobenzene BRL 0.50 ug/L Chloroethane BRL 0.50 ug/L Chloroform BRL 0.50 ug/L Chloromethane BRL 0.50 ug/L cis-1,2-Dichloroethylene BRL 0.50 ug/L cis-1,3-Dichloropropylene BRL 0.50 ug/L Dibromochloromethane BRL 0.50 ug/L Dibromomethane BRL 0.50 ug/L Dichlorodifluoromethane BRL 5.0 ug/L Ethylbenzene BRL 0.50 ug/L Hexachlorobutadiene BRL 2.0 ug/L This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 20 Waypoint.0 ANALYTICAL Level II QC Report 12/19/19 Draper Arden & Associates Project: ALAMAC Work Order: 9120098 Attn: Sean Jarvah Time Submitted: 12/6/2019 5:10:OOPM 114 Edinburg South Drive Ste 200 Cary, NC 27511 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9LO237 - 5030B Blank (1291-0237-BLM) Prepared: 12/12/19 Analyzed: 12/13/19 Isopropyl Ether BRL 0.50 ug/L Isopropylbenzene (Cumene) BRL 0.50 ug/L m,p-Xylenes BRL 1.0 ug/L Methyl Butyl Ketone (2-Hexanone) BRL 5.0 ug/L Methyl Ethyl Ketone (2-Butanone) BRL 5.0 ug/L Methyl Isobutyl Ketone BRL 5.0 ug/L Methylene Chloride BRL 1.0 ug/L Methyl-tert-Butyl Ether BRL 0.50 ug/L Naphthalene 0.220 1.0 ug/L J n-Butylbenzene BRL 1.0 ug/L n-Propylbenzene BRL 0.50 ug/L o-Xylene BRL 0.50 ug/L sec-Butylbenzene BRL 0.50 ug/L Styrene BRL 0.50 ug/L tert-Butylbenzene BRL 0.50 ug/L Tetrachloroethylene BRL 0.50 ug/L Toluene BRL 0.50 ug/L trans-1,2-Dichloroethylene BRL 0.50 ug/L trans-1,3-Dichloropropylene BRL 0.50 ug/L Trichloroethylene BRL 0.50 ug/L Trichlorofluoromethane BRL 0.50 ug/L Vinyl acetate BRL 2.0 ug/L Vinyl chloride BRL 0.50 ug/L Xylenes, total BRL 1.5 ug/L Surrogate:4-Bromofluorobenzene 49.8 ug/L 50.00 100 80-124 Surrogate: Dibromofluoromethane 47.7 ug/L 50.00 95 75-129 Surrogate: Toluene-d8 42.7 ug/L 50.00 85 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 20 Waypoint_0 ANALYTICAL Level II QC Report 12/19/19 Draper Arden & Associates Project: ALAMAC Work Order: 9120098 Attn: Sean Jarvah Time Submitted: 12/6/2019 5:10:OOPM 114 Edinburg South Drive Ste 200 Cary, NC 27511 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9L0237 - 5030B LCS (P9L0237-BS1) Prepared: 12/12/19 Analyzed: 12/13/19 1,1,1,2-Tetrachloroethane 19.8 0.50 ug/L 20.00 99 79-134 1,1,1-Trichloroethane 22.6 0.50 ug/L 20.00 113 75-136 1,1,2,2-Tetrachloroethane 18.7 0.50 ug/L 20.00 93 62-127 1,1,2-Trichloroethane 23.6 0.50 ug/L 20.00 118 70-140 1,1-Dichloroethane 23.3 0.50 ug/L 20.00 116 78-130 1,1-Dichloroethylene 22.7 0.50 ug/L 20.00 114 70-154 1, 1 -Dichloropropylene 23.6 0.50 ug/L 20.00 118 71-136 1,2,3-Trichlorobenzene 19.0 2.0 ug/L 20.00 95 58-144 1,2,3-Trichloropropane 18.4 1.0 ug/L 20.00 92 71-127 1,2,4-Trichlorobenzene 18.0 1.0 ug/L 20.00 90 66-139 1,2,4-Trimethylbenzene 18.8 0.50 ug/L 20.00 94 75-133 1,2-Dibromo-3-chloropropane 18.4 2.0 ug/L 20.00 92 63-134 1,2-Dibromoethane 20.4 0.50 ug/L 20.00 102 77-135 1,2-Dichlorobenzene 18.7 0.50 ug/L 20.00 93 78-128 1,2-Dichloroethane 22.0 0.50 ug/L 20.00 110 68-131 1,2-Dichloropropane 23.4 0.50 ug/L 20.00 117 77-130 1,3,5-Trimethylbenzene 19.0 0.50 ug/L 20.00 95 75-131 1,3-Dichlorobenzene 18.5 0.50 ug/L 20.00 93 77-125 1,3-Dichloropropane 20.4 0.50 ug/L 20.00 102 76-132 1,4-Dichlorobenzene 18.4 0.50 ug/L 20.00 92 75-126 2,2-Dichloropropane 22.8 2.0 ug/L 20.00 114 29-149 2-Chlorotoluene 18.5 0.50 ug/L 20.00 93 74-126 4-Chlorotoluene 18.5 0.50 ug/L 20.00 92 78-129 4-Isopropyltoluene 18.8 0.50 ug/L 20.00 94 69-132 Acetone 44.8 5.0 ug/L 40.00 112 40-166 Acrolein 48.7 20 ug/L 40.00 122 70-130 Acrylonitrile 44.4 20 ug/L 40.00 111 81-127 Benzene 23.2 0.50 ug/L 20.00 116 77-128 Bromobenzene 19.2 0.50 ug/L 20.00 96 78-129 Bromochloromethane 23.7 0.50 ug/L 20.00 119 78-135 Bromodichloromethane 23.2 0.50 ug/L 20.00 116 76-138 Bromoform 19.8 1.0 ug/L 20.00 99 71-135 Bromomethane 18.4 1.0 ug/L 20.00 92 41-168 Carbon disulfide 24.7 5.0 ug/L 20.00 123 59-135 Carbon Tetrachloride 22.7 0.50 ug/L 20.00 114 72-142 Chlorobenzene 19.9 0.50 ug/L 20.00 100 78-119 Chloroethane 23.5 0.50 ug/L 20.00 118 57-142 Chloroform 23.5 0.50 ug/L 20.00 117 77-130 Chloromethane 21.8 0.50 ug/L 20.00 109 47-145 cis-1,2-Dichloroethylene 22.4 0.50 ug/L 20.00 112 76-141 cis-1,3-Dichloropropylene 24.3 0.50 ug/L 20.00 121 65-140 Dibromochloromethane 20.4 0.50 ug/L 20.00 102 75-134 Dibromomethane 22.9 0.50 ug/L 20.00 115 76-138 Dichlorodifluoromethane 21.4 5.0 ug/L 20.00 107 28-163 Ethylbenzene 19.8 0.50 ug/L 20.00 99 80-127 Hexachlorobutadiene 18.6 2.0 ug/L 20.00 93 61-134 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 Of 20 Waypoint.0 ANALYTICAL Level II QC Report 12/19/19 Draper Arden & Associates Project: ALAMAC Attn: Sean Jarvah 114 Edinburg South Drive Ste 200 Cary, NC 27511 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9LO237 - 5030B Reporting Result Limit Units Work Order: 9120098 Time Submitted: 12/6/2019 5:10:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P91-0237-BSI) Prepared: 12/12/19 Analyzed: 12/13/19 Isopropyl Ether 22.3 0.50 ug/L 20.00 112 60-154 Isopropylbenzene (Cumene) 19.1 0.50 ug/L 20.00 96 70-130 m,p-Xylenes 40.1 1.0 ug/L 40.00 100 77-133 Methyl Butyl Ketone (2-Hexanone) 20.0 5.0 ug/L 20.00 100 64-137 Methyl Ethyl Ketone (2-Butanone) 24.4 5.0 ug/L 20.00 122 71-134 Methyl Isobutyl Ketone 22.4 5.0 ug/L 20.00 112 69-134 Methylene Chloride 22.2 1.0 ug/L 20.00 ill 73-131 Methyl-tert-Butyl Ether 23.8 0.50 ug/L 20.00 119 68-135 Naphthalene 17.7 1.0 ug/L 20.00 89 64-136 n-Butylbenzene 18.8 1.0 ug/L 20.00 94 68-134 n-Propylbenzene 18.7 0.50 ug/L 20.00 93 72-132 o-Xylene 20.4 0.50 ug/L 20.00 102 78-128 sec-Butylbenzene 18.9 0.50 ug/L 20.00 94 71-131 Styrene 20.7 0.50 ug/L 20.00 104 78-129 tert-Butylbenzene 19.0 0.50 ug/L 20.00 95 70-132 Tetrachloroethylene 19.9 0.50 ug/L 20.00 100 80-129 Toluene 23.1 0.50 ug/L 20.00 116 76-131 trans-1,2-Dichloroethylene 22.4 0.50 ug/L 20.00 112 76-135 trans- 1,3-Dichloropropylene 24.3 0.50 ug/L 20.00 121 67-140 Trichloroethylene 22.7 0.50 ug/L 20.00 113 77-133 Trichlorofluoromethane 24.3 0.50 ug/L 20.00 122 62-148 Vinyl acetate 25.3 2.0 ug/L 20.00 126 34-167 Vinyl chloride 24.1 0.50 ug/L 20.00 121 57-141 Xylenes, total 60.5 1.5 ug/L 60.00 101 77-133 Surrogate:4-Bromofluorobenzene 49.3 ug/L 50.00 99 80-124 Surrogate: Dibromofluoromethane 48.0 ug/L 50.00 96 75-129 Surrogate: Toluene-d8 43.7 ug/L 50.00 87 77-123 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 20 Waypoint_0 ANALYTICAL Level II QC Report 12/19/19 Draper Arden & Associates Project: ALAMAC Work Order: 9120098 Attn: Sean Jarvah Time Submitted: 12/6/2019 5:10:OOPM 114 Edinburg South Drive Ste 200 Cary, NC 27511 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9L0237 - 5030B LCS Dup (P91-0237-13SD1) Prepared: 12/12/19 Analyzed: 12/13/19 1,1,1,2-Tetrachloroethane 19.4 0.50 ug/L 20.00 97 79-134 2 20 1,1,1-Trichloroethane 22.5 0.50 ug/L 20.00 113 75-136 0.4 20 1,1,2,2-Tetrachloroethane 19.0 0.50 ug/L 20.00 95 62-127 2 20 1,1,2-Trichloroethane 23.3 0.50 ug/L 20.00 116 70-140 2 20 1,1-Dichloroethane 23.1 0.50 ug/L 20.00 116 78-130 0.9 20 1,1-Dichloroethylene 22.2 0.50 ug/L 20.00 111 70-154 2 20 1, 1 -Dichloropropylene 22.9 0.50 ug/L 20.00 115 71-136 3 20 1,2,3-Trichlorobenzene 19.7 2.0 ug/L 20.00 99 58-144 4 20 1,2,3-Trichloropropane 19.3 1.0 ug/L 20.00 96 71-127 5 20 1,2,4-Trichlorobenzene 18.8 1.0 ug/L 20.00 94 66-139 4 20 1,2,4-Trimethylbenzene 18.2 0.50 ug/L 20.00 91 75-133 3 20 1,2-Dibromo-3-chloropropane 19.7 2.0 ug/L 20.00 98 63-134 7 20 1,2-Dibromoethane 20.7 0.50 ug/L 20.00 104 77-135 2 20 1,2-Dichlorobenzene 18.8 0.50 ug/L 20.00 94 78-128 0.7 20 1,2-Dichloroethane 22.3 0.50 ug/L 20.00 111 68-131 1 20 1,2-Dichloropropane 23.0 0.50 ug/L 20.00 115 77-130 2 20 1,3,5-Trimethylbenzene 18.4 0.50 ug/L 20.00 92 75-131 3 20 1,3-Dichlorobenzene 18.0 0.50 ug/L 20.00 90 77-125 3 20 1,3-Dichloropropane 20.9 0.50 ug/L 20.00 105 76-132 2 20 1,4-Dichlorobenzene 18.0 0.50 ug/L 20.00 90 75-126 3 20 2,2-Dichloropropane 22.6 2.0 ug/L 20.00 113 29-149 0.7 20 2-Chlorotoluene 18.0 0.50 ug/L 20.00 90 74-126 3 20 4-Chlorotoluene 18.0 0.50 ug/L 20.00 90 78-129 3 20 4-Isopropyltoluene 18.4 0.50 ug/L 20.00 92 69-132 2 20 Acetone 46.7 5.0 ug/L 40.00 117 40-166 4 20 Acrolein 49.3 20 ug/L 40.00 123 70-130 1 20 Acrylonitrile 45.1 20 ug/L 40.00 113 81-127 2 20 Benzene 22.7 0.50 ug/L 20.00 114 77-128 2 20 Bromobenzene 18.8 0.50 ug/L 20.00 94 78-129 2 20 Bromochloromethane 23.5 0.50 ug/L 20.00 117 78-135 1 20 Bromodichloromethane 23.2 0.50 ug/L 20.00 116 76-138 0.2 20 Bromoform 20.5 1.0 ug/L 20.00 103 71-135 3 20 Bromomethane 18.6 1.0 ug/L 20.00 93 41-168 1 20 Carbon disulfide 23.8 5.0 ug/L 20.00 119 59-135 4 20 Carbon Tetrachloride 22.3 0.50 ug/L 20.00 111 72-142 2 20 Chlorobenzene 19.6 0.50 ug/L 20.00 98 78-119 2 20 Chloroethane 22.6 0.50 ug/L 20.00 113 57-142 4 20 Chloroform 23.4 0.50 ug/L 20.00 117 77-130 0.5 20 Chloromethane 21.8 0.50 ug/L 20.00 109 47-145 0.2 20 cis-1,2-Dichloroethylene 21.9 0.50 ug/L 20.00 109 76-141 2 20 cis-1,3-Dichloropropylene 24.0 0.50 ug/L 20.00 120 65-140 1 20 Dibromochloromethane 20.6 0.50 ug/L 20.00 103 75-134 0.7 20 Dibromomethane 23.0 0.50 ug/L 20.00 115 76-138 0.6 20 Dichlorodifluoromethane 20.9 5.0 ug/L 20.00 105 28-163 2 20 Ethylbenzene 19.9 0.50 ug/L 20.00 99 80-127 0.05 20 Hexachlorobutadiene 18.4 2.0 ug/L 20.00 92 61-134 1 20 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 Of 20 Waypoint_0 ANALYTICAL Level II QC Report 12/19/19 Draper Arden & Associates Project: ALAMAC Attn: Sean Jarvah 114 Edinburg South Drive Ste 200 Cary, NC 27511 Volatile Organic Compounds by GC/MS - Quality Control Work Order: 9120098 Time Submitted: 12/6/2019 5:10:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9LO237 - 5030B LCS Dup (P9L0237-BSD1) Prepared: 12/12/19 Analyzed: 12/13/19 Isopropyl Ether 22.1 0.50 ug/L 20.00 ill 60-154 0.9 20 Isopropylbenzene (Cumene) 18.6 0.50 ug/L 20.00 93 70-130 3 20 m,p-Xylenes 39.4 1.0 ug/L 40.00 98 77-133 2 20 Methyl Butyl Ketone (2-Hexanone) 20.7 5.0 ug/L 20.00 103 64-137 3 20 Methyl Ethyl Ketone (2-Butanone) 24.4 5.0 ug/L 20.00 122 71-134 0.3 20 Methyl Isobutyl Ketone 23.4 5.0 ug/L 20.00 117 69-134 5 20 Methylene Chloride 21.9 1.0 ug/L 20.00 110 73-131 1 20 Methyl-tert-Butyl Ether 23.9 0.50 ug/L 20.00 119 68-135 0.08 20 Naphthalene 18.7 1.0 ug/L 20.00 94 64-136 6 20 n-Butylbenzene 18.5 1.0 ug/L 20.00 93 68-134 1 20 n-Propylbenzene 18.3 0.50 ug/L 20.00 92 72-132 2 20 o-Xylene 20.1 0.50 ug/L 20.00 100 78-128 1 20 sec-Butylbenzene 18.6 0.50 ug/L 20.00 93 71-131 1 20 Styrene 20.4 0.50 ug/L 20.00 102 78-129 1 20 tert-Butyl benzene 18.6 0.50 ug/L 20.00 93 70-132 3 20 Tetrachloroethylene 19.9 0.50 ug/L 20.00 99 80-129 0.3 20 Toluene 22.6 0.50 ug/L 20.00 113 76-131 2 20 trans- 1,2-Dichloroethylene 21.7 0.50 ug/L 20.00 109 76-135 3 20 trans- 1,3-Dichloropropylene 24.6 0.50 ug/L 20.00 123 67-140 1 20 Trichloroethylene 22.2 0.50 ug/L 20.00 ill 77-133 2 20 Trichlorofluoromethane 23.8 0.50 ug/L 20.00 119 62-148 2 20 Vinyl acetate 25.5 2.0 ug/L 20.00 127 34-167 0.7 20 Vinyl chloride 23.4 0.50 ug/L 20.00 117 57-141 3 20 Xylenes, total 59.5 1.5 ug/L 60.00 99 77-133 2 20 Surrogate:4-Bromofluorobenzene 48.8 ug/L 50.00 98 80-124 Surrogate: Dibromofluoromethane 48.4 ug/L 50.00 97 75-129 Surrogate: Toluene-d8 44.1 ug/L 50.00 88 77-123 Sample Extraction Data Prep Method: 5030E Lab Number Batch Initial Final Daterrime 9120098-01 P91-0237 10 mL 10 mL 12/12/19 17:33 9120098-01 P91-0237 10 mL 10 mL 12/12/19 17:33 9120098-02 P91-0237 10 mL 10 mL 12/12/19 17:33 9120098-02 P91-0237 10 mL 10 mL 12/12/19 17:33 9120098-03 P91-0237 10 mL 10 mL 12/12/19 17:33 9120098-03 P91-0237 10 mL 10 mL 12/12/19 17:33 9120098-04 P91-0237 10 mL 10 mL 12/12/19 17:33 9120098-05 P91-0237 10 mL 10 mL 12/12/19 17:33 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 20 PRISo n Full -Service Analytical & I V I Environmental Solutions :--. LARORATORIFF INC 449 Springbrook Road • Charlotte, NC 28217 Phone 704/52-9-6364 Fax: 7041552-5-0. 409 1,J Client Company Name: [L•a�e,. Al_ Report To/Contact Name Reporting Address: I jq I ly, A'h *.11- -,- 2aall CHAIN OF CUSTODY RECORD PAGE OF�_ QUOTE # TO ENSURE PROPER BILLING: Project Name: Occ ,' UL (,ow ,A l:) YLy _ Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) *Please ATTACH any project specific reporting (QC LEVEL 1 II III IV) provisions a dlor QC Requ'rements Invoice To: Address: Samples INTACT upon arrival? Received ON WET ICE? PROPER PRESERVATIVES indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES rec'd W/OUT HEADSPACE? PROPER CONTAINERS used? TEMP: Themt IDa _/4 Observed: Y NO NIA CD O CD CV �� CD cts d "C f Corm! _0C ` - t"+3 tax (Yes) (No): (�- »A �''Ot`�1 Purchase Order No./Billing Reference _J S � 029 4 -171C�G 3 TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email dress:in_ Email Address: . EDD Type: ✓Excel ✓Other Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC_ PDF "Working Days" ❑ 6-9 Days ❑Standard 10 days L7 Rush Work Must Be �1 Site Location Name: �� f-+1%�� Pre -Approved Samples received after 14:00 will be processed next business day. SC OTHER NIA Site Location Physical Address: LV1'rbs-AVY Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ Nd__L (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES NO TIME MATRIX `` SAMPLE CONTAINER ANALYSIS REQUESTED CLIENT DATE COLLECTED (SOIL, I PRESERVA- PRISM SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE TIVES f REMARKS LAB HOURS SLUDGE) SEE BELOW NO. SIZE ID NO. 3 pt- L -- X, W 50 E MOW— 3 L Sampler's Signature Sampled By (Print Name) " ��� ,L'1 Affiliation Upon reli quishing, th' haf ofd stody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be 72 submitt6 in writing a rim roject Manager. There will be charges for any changes after analyses have been initialized. ahnqurs y:(Slnnatu : (sf sure) Date ilitary ours Additional Comments: l6ls 777- Roll + d S' I coined gy; re} Date 1d6lsli� y .!� r� S ..Ilrs u" lure Recei rism Laboratories By: Date Field Tech Fee: iti 1?LO Mol of Shipment NOTE: ALL SAMPLE COOLERS SHDULD BE TAPED SHUT wiTA CUSTODY SEALS FOR TRANSPORTATIOT THE LABORATORY. COC Group No. Mileage: SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. ( fj nn, l ❑ Fed Ex El UPS El Hand -delivered ❑ Prism Field Service ❑ Other k ll Io1 NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: ' ❑NC❑Sl ❑NC ❑SC NC ❑SC ❑NC ❑SC ❑NC ❑SC oNC❑SC ❑NC El❑NC ❑SCI ❑NC ❑SC ❑ _ El❑ El *CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORIGINAL I O AC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9C0061 Alamac American Knits - Lumb Project Name: WW samples - Monthly/Qrtly Mr. Cleve Collins Project / PO Number: 2041451 Post Office Box 1347 Received: 03/12/2019 Lumberton, NC 28359 Reported: 03/25/2019 Analytical Testing Parameters Client Sample ID: Effluent 00-1, Composite Sample Matrix: Aqueous Lab Sample ID: K9C0061-01 Wet Chemistry Result Method: EPA 300.0, Rev. 2.1 (1993) MDL Nitrate as N 0.335 0.0300 Nitrite as N 0.0327 0.0300 Method: SM 4500-Norg C-2011 Total Kjeldahl Nitrogen 2.18 Collected By: Collins Collection Date: 03/12/20'19 8:15 RL Units Note Prepared Analyzed Analyst 0.0300 mg/L 03/13/19 0928 03/13/19 1415 DSK 0.0500 mg/L 03/13/19 0928 03/13/19 1415 DSK 1.00 mg/L 03/19/19 0844 DC Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley Result MDL RL Units Note Prepared Analyzed Analyst Method: EPA200.7 Chromium, Total <0.00250 0.00250 0.00500 mg/L 03/19/19 0713 03/19/19 1922 KKB Client Sample ID: Effluent 001, Grab Sample Matrix: Aqueous Collected By: Collins Lab Sample ID: K9C0061--02 Collection Date: 03/12/2019 8:30 Method: EPA200.7 Copper, Total Zinc, Total Method: EPA420.1 Phenolics, Total Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley Result MDL RL Units Note Prepared Analyzed Analyst 0.0108 0.00250 0.00500 mg/L 03/19/19 0713 03/19/19 1926 KKB 0.0102 0.0100 0.0200 mg/L J 03/19/19 0713 03/19/19 1926 KKB <3.33 3.33 5.56 ug/L 03/20/19 1425 DLP Volatile Organics-Spec/MS Result MDL RL Units Note Prepared Analyzed Analyst Method: EPA624.1 1,1,1-Trichloroethane <0.250 0.250 1.00 ug/L 03/19/19 1439 JDS Carbon tetrachloride <0.250 0.250 1.00 ug/L 03/19/19 1439 JDS cis-1,2-Dichloroethene <0.250 0.250 1.00 ug/L 03/19/19 1439 JDS Tetrachloroethene <0.250 0.250 1.00 ug/L 03/19/19 1439 JDS Trichloroethene <0.250 0.250 1.00 ug/L 03/19/19 1439 JDS Vinyl chloride <0.250 0.250 1.00 ug/L 03/19/19 1439 JDS Surrogate: 1,2-Dichloroethane-d4 101 Limit: 63-140 % Rec 03/19/19 1439 JDS Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com Page 1 of 4 OMICRO AC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9F0228 Analytical Testing Parameters Client Sample ID: Effluent 001, Composite Sample Matrix: Aqueous Lab Sample ID: K9F0228.01 Wet Chemistry Result MDL RL Units Method: EPA 300.0, Rev. 2.1 (1993) Nitrate as N 0.306 0.0300 0.0300 mg/L Nitrite as N 0.275 0.0300 0.0500 mg/L Collected By: Collins Collection Date: 06/25/2019 8:20 Dilution Note Prepared Analyzed Analyst 1 06/26/19 0946 06/26/19 1653 DSK 1 06/26/19 0946 06/26/19 1653 DSK Method: SM 4500-Norg C-2011 Total Kjeldahl Nitrogen 2.88 1.00 mg/L 1 07/02/19 0858 TBM Metals Result MDL RL Units Dilution Note Prepared Analyzed Analyst Method: Metals Aqueous/EPA 200.7 Rev 4.4 1994 Chromium <0.013 0.013 0.050 mg/L 1 07/10/19 1710 07/10/19 1710 TAB Client Sample ID: Effluent 001, Grab Sample Matrix: Aqueous Lab Sample ID: K9F0228-02 Metals Result MDL RL Units Method: Metals Aqueous/EPA 200.7 Rev 4.4 1994 Copper <0.017 0.017 0.050 mg/L Zinc <0.004 0.004 0.005 mg/L Inorganics Method: EPA 420.1, Rv 1978 Phenols - 4AAP Volatile Organic Compounds - GC/MS Method: EPA 624.1 Acrolein Acrylonitrile Benzene Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane (Ethyl chloride) 2-Chloroethyl vinyl ether Collected By: Collins Collection Date: 06/25/2019 9:30 Dilution Note Prepared Analyzed Analyst 1 07/10/19 1714 07/10/19 1714 TAB 1 07/10/19 1714 07/10/19 1714 TAB Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Result MDL RL Units Dilution Note Prepared Analyzed Analyst: <0.0055 0.0055 mg/L 1 07/02/19 0853 07/02/19 1725 APH Result MDL RL Units Dilution Note Prepared Analyzed Analyst <10.0 10.0 ug/L 1 A9, Q2 <5.00 5.00 ug/L 1 A9 <1.00 1.00 ug/L 1 <1.00 1.00 ug/L 1 <1.00 1.00 ug/L 1 <1.00 1.00 ug/L 1 <1.00 1.00 ug/L 1 <1.00 1.00 ug/L 1 <1.00 1.00 ug/L 1 <1.00 1.00 ug/L 1 <5.00 5.00 ug/L 1 Microbac Laboratories, Inc. 2592 Hope Mills Rd Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com 07/02/19 2230 JDS 07/02/19 2230 JDS 07/02/19 2230 JDS 07/02/19 2230 JDS 07/02/19 2230 JDS 07/02/19 2230 JDS 07/02/19 2230 JDS 07/02/19 2230 JDS 07/02/19 2230 JDS 07/02/19 2230 JDS 07/02/19 2230 JDS Page 2 of 6 Client Sample ID: Effluent 001, Grab Sample Matrix: Aqueous Lab Sample ID: K9F0228-02 Volatile Organic Compounds - GC/MS Chloroform Chloromethane 1,3-Dichlorobenzene 1,2-Dichlorobenzene 1,1-Dichloroethane 1,2-Dichloroethane cis-1,2-Dichloroethene 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene Ethylbenzene Methylene chloride 1,1,2,2-Tetrachloroethane Tetra chi oroethene Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Vinyl chloride Surrogate: 4-Bromofluorobenzene Surrogate: 1,2-Dichloroethane-d4 Surrogate: Toluene-d8 Wet Chemistry Method: *** DEFAULT SPECIFIC METHOD *** Sulfide 0.12 Definitions VM I C O AC.o Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K9F0228 Collected By: Collins Collection Date: 06/25/2019 9:30 Result MDL RL Units Dilution Note Prepared Analyzed Analyst <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS <1.00 1.00 ug/L 1 07/02/19 2230 JDS 103 Limit: 60-140 % Rec 1 07/02/19 2230 JDS 96.7 Limit: 63-140 % Rec 1 07/02/19 2230 JDS 102 Limit: 60-140 % Rec 1 07/02/19 2230 JDS Analyses Subcontracted to: Pace Analytical ( Huntersville) Result MDL RL Units Dilution Note 0.1 0.1 mg/L 1 A9: Sample was improperly preserved. MDL: Minimum Detection Limit Q2: LCS recovery is above acceptance limits. However there is no impact on the reported value. RL: Reporting Limit Cooler Receipt Log Cooler ID: Default Cooler Temp: 9.7°C Prepared Analyzed Analyst 07/01/19 0000 TB Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 6 M i C FCC] AC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K910241 Analytical Testing Parameters Client Sample ID: Effluent 001, Composite Sample Matrix: Aqueous Lab Sample ID: K910241-•01 Wet Chemistry Result Method: EPA 300.0, Rev. 2.1 (1993) Nitrate as N 0.308 Nitrite as N 0.0722 Method: SM 4500-Norg C-2011 Total Kjeldahl Nitrogen 2.46 MDL RL Units 0.0300 0.0300 mg/L 0.0300 0.0500 mg/L Collected By: Collins Collection Date: 09/24/2019 8:30 Dilution Note Prepared Analyzed Analyst 1 09/24/19 0954 09/25/19 0857 DSK 1 09/24/19 0954 09/25/19 0857 DSK 1.00 mg/L 1. 10/01/19 0848 TBM Metals Result MDL RL Units Dilution Note Prepared Analyzed Analyst Method: Metals Aqueous/EPA 200.7 Rev 4.4 1994 Chromium <0.013 0.013 0.050 mg/L 1,. 09/25/19 1259 09/25/19 1259 TAB Client Sample ID: Effluent 001, Grab Sample Matrix: Aqueous Collected By: Collins Lab Sample ID_ K910241-02 L Collection Date: 09/24/2019 8:30 Metals Result MDL RL Units Dilution Note Prepared Analyzed Analyst Method: Metals Aqueous/EPA 200.7 Rev 4.4 1994 Copper <0.017 0.017 0.050 mg/L 1 09/25/19 1303 09/25/19 1303 TAB Zinc 0.010 0.004 0.005 mg/L 1 09/25/19 1303 09/25/19 1303 TAB Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Inorganics Result MDL RL Units Dilution Note Prepared Analyzed Analyst Method: EPA 420.1, Rv 1978 Phenols - 4AAP <0.0056 0.0056 mg/L 1 y 09/30/19 1618 09/30/19 1624 TB Volatile Organic Compounds - Result MDL RL Units Dilution Note Prepared Analyzed Analyst GC/MS Method: EPA 624.1 Carbon tetrachloride <0.250 0.250 1.00 ug/L 1 09/26/19 2138 EEA cis- 1,2-Dichloroethene <0.250 0.250 1.00 ug/L 1 09/26/19 2138 EEA Tetra chloroethene <0.250 0.250 1.00 ug/L 1 09/26/19 2138 EEA 1,1,1-Trichloroethane <0.250 0.250 1.00 ug/L 1 09/26/19 2138 EEA Trichloroethene <0.250 0.250 1.00 ug/L 1 09/26/19 2138 EEA Vinyl chloride <0.500 0.500 1.00 ug/L 1 09/26/19 2138 EEA Surrogate: 4-Bromofluorobenzene 106 Limit: 60-140 % Rec 1 09/26/19 2138 EEA Surrogate: 1,2-Dichloroethane-d4 101 Limit: 63-140 % Rec 1 09/26/19 2138 EEA Surrogate: Toluene-d8 101 Limit: 60-140 % Rec 1 09/26/19 2138 EEA Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 10 ViviiCRoBAC- Microbac Laboratories, Inc, - Fayetteville CERTIFICATE OF ANALYSIS K9L0336 Anatytical Testing Parameters Client Sample ID: Eiilueni 001, Cornposile Sample Matrix: Aqueays Collected By: C ollinz, Lab Sample ID_ K91_033&C11 Collection Date: 12117(2019 8:22 Wet Chemistry _ Method. EPA 300.0, Rev, 2.111993) Nitrate as N Nitrite as N Method: SM 4300-Norg C-2011 Total Kjeldahl Nhrogen Resutt MDL RL Units Dilution Nola Prepared Analyzed Analys[ 0.0690 0,0300 0,0300 mq& 1 12119r19 2100 VAA <0,0300 0.0300 0.0500 mglL 1 12119r19 2100 VAA 2.32 1.00 mg1l. 1 12127119 0522 rang Client Sample ID: Effluerll 001, Grab Sample Matrix: Aqueous Collected By: Collins Lab Sample ID: K91.0336-02 Collection Date: 1211717.019 0-,30 Metals Result MDL RL Units_ _Dilution Moto - Prepared Analyzed Analyst Method: Metals AqueouslEPA 200.7 Rev 4.4 1994 Chromium <0.013 0.013 0.060 m91L 1 12119119 1702 121191lg 1702 TBM Copper <0.017 0.017 0.060 mg1L 1 12119119 1702 12A9119 1702 Tom Zinc 0.012 0.004 0.005 mg1L 1 12119/19 1702 12119119 1702 TBM Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH Inorganics Result MDL RL -Units � Dilution Note Prepared - Analyzed _ _ Analyst — Method: EPA 420.1, Rv 1978 Phenols - 4AAP <0.0056 0,0056 mgiL 1 y 12128;19 1250 120119 1450 EPT VolatileClrganiaCompounds- Result MDL RL Units Dilution Note Prepared Analyzed Analyst GCtMS -- - - - -- _— - - Method: EPA 624.1 Carbon tetrachloride <0.250 0.250 1.00 ug1L 1 1217119 1930 EEA ci-1,2-Dichloroelhene <0-250 0.250 1.00 ug1L 1 12127119 t930 EEA Tetrachloroethene <0.250 0 250 1.00 41L 1 1212P19 1930 EEA 1,1,1-TrIcNoroelhane <0.250 0.250 1.00 uglL 1 12127r19 1030 EEA Trichloroethene <0.250 0.250 1.00 uglL 1 12127119 1030 EEA limyl chloride <0.500 0,500 1.00 ug1L 1 12127119 1930 EEA Surrogate:4-Bromofluorobenzene 104 Limit: 60-140 °% Rec 1 1V27119 1930 EEA Surrogate: 1,2-Dichloroelhane-l4 110 Limit: 63-140 °% Rec 1 12127119 1930 EEA Surrogate, Toluene-d8 102 Limil: 60-140 % Rec 1 12127119 1930 EF_A Analyses Subcontracted to: Pace Analytical ( Huntersville) Wet Chemistry Result MDL RL Units Dilution Note Prepared Analyzed Analyst Microbac Laboratories, h1c. 2592 Hope Mills Rd I Fayetteville, INC 28306 1 910,864,1920 p I www.microbac.corn Page 3 of 9 APPENDIX C MONTHLY RECOVERY WELL FLOW REPORTS ALAMAC INVESTORS, LLC REMEDIATION WELL REPORT 2019 MONTH: January DATE TIME WELL #1 WELL #1 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GIRD / GPM INTEGRAT. GIRD / GPM INTEGRAT. GPD / GPM 5249428 1260006 79094190 01 1050 5253460 4032 / 2.39 1262232 2226 / 2.25 79103617 09427 / 5.53 02 0758 5256554 3094 / 2.44 1263944 1712 / 2.24 79110804 07187 / 5.55 03 0800 5260119 3565 / 2.42 1265858 1914 / 2.11 79118831 08027 / 5.45 04 0801 5263839 3720 / 2.52 1267825 1967 / 2.25 79126972 08141 / 5.32 05 1240 5267731 3892 / 2.36 1269894 2069 / 2.10 79135348 08376 / 5.21 06 1200 5271156 3425 / 2.43 1271723 1829 / 2.18 79142544 07196 / 5.03 07 0800 5274058 2902 / 2.42 1273495 1772 / 2.61 79148560 06016 / 4.69 08 0805 5277494 3436 / 2.44 1275749 2254 / 2.65 79155505 06945 / 4.77 09 0800 5281215 3721/2.39 1278149 2400/2.64 79162678 07173/4.66 10 0801 5284693 3478 / 2.37 1280411 2262 / 2.71 79169209 06531 / 4.47 11 0758 5288061 3368 / 2.41 1282675 2264 / 2.85 79175358 06149 / 4.32 12 1250 5292132 4071 / 2.39 1285475 2800 / 2.79 79182564 07206 / 4.18 13 1146 5295380 3248 / 2.39 1287728 2253 / 2.76 79188150 05587 / 4.11 14 0800 5298385 3005 / 2.41 1289841 2113 / 2.70 79193246 05096 / 4.05 15 0800 5301799 3414 / 2.44 1292257 2416 / 2.82 79198982 05736 / 3.98 16 0800 5305473 3674 / 2.32 1294864 2607 / 2.79 79205150 06168 / 3.95 17 0805 5308771 3298 / 2.32 1297191 2327 / 2.82 79210659 05509 / 3.92 18 0750 5311998 3227 / 2.36 1299469 2278 / 2.77 79216012 05353 / 3.94 19 1120 5315847 3849 / 2.35 1302162 2693 / 2.76 79222342 06330 / 3.91 20 1300 5319465 3618 / 2.18 1304782 2620 / 2.75 79228425 06083 / 3.77 21 0800 5322312 2847 / 2, 27 1306942 2160 / 2.94 79233257 04832 / 3.78 22 0801 5325072 2760 / 2.14 1309159 2217 / 3.08 79238088 04831 / 3.74 23 0800 5328098 3026 / 2.09 1311615 2456 / 2.71 79243409 05321 / 3.68 24 0801 5331075 2977 / 2.16 1313923 2308 / 2.64 79248556 05147 / 3.65 25 0801 5334259 3184 / 2.13 1316227 2304 / 2.67 79254063 05507 / 3.64 26 1150 5337870 3611 / 2.16 1318839 2612 / 2.76 79260284 06221 / 3.65 27 1150 5340887 3017 / 2.17 1321014 2175 / 2.65 79265346 06062 / 3.61 28 0800 5343501 2614 / 2.01 1322939 1925 / 2.61 79269796 04450 / 3.57 29 0801 5346730 3229 / 2.20 1325311 2372 / 2.63 79275203 05407 / 3.56 30 0759 5349959 3229 / 2.13 1327684 2373 / 2.63 79280610 05407 / 3.50 31 0800 5352583 2624 / 2.11 1329577 1893 / 2.56 79284864 04254 / 3.49 COMMENTS: ANALYST: ALAMAC INVESTORS, LLC REMEDIATION WELL REPORT 2019 MONTH: February DATE TIME WELL #1 WELL #1 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GPD / GPM INTEGRAT. GPD / GPM INTEGRAT. GPD / GPM 5352583 1329577 79284864 01 0800 5355846 3263 / 2.07 1332019 2442 / 2 67 79290212 05348 / 3.53 02 1257 5359568 3722 / 2.08 1334803 2784 / 2.49 79296391 06179 / 3.64 03 1110 5362398 2830 / 2.09 1336906 2103 / 2.55 79301235 04844 / 3.61 04 0800 5365196 2798 / 2 10 1338981 2075 / 2.63 79306062 04827 / 3.60 05 0801 5367994 2798 / 2.04 1341056 2075 / 2.63 79310888 04826 / 3.64 06 0800 5371203 3209 / 2.24 1343402 2346 / 2.52 79316397 05509 / 3.64 07 0800 5374267 3064 / 2.15 1345490 2088 / 2.48 79321564 05167 / 3.67 08 0801 5377330 3063 / 2.14 1347577 2087 / 2.47 79326954 05390 / 3.86 09 1355 5381282 3952 / 2.10 1350237 2660 / 2.31 79334018 07064 / 3.88 10 1150 5383890 2608 / 2.12 1352026 1789 / 2.47 79338776 04758 / 3.89 11 0801 5386716 2826 / 2.09 1354042 2016 / 2.48 79344032 05256 / 3.91 12 0801 5389580 2864 / 2.01 1356096 2054 / 2.54 79349565 05533 / 4.13 13 0802 5392516 2936 / 2.17 1358193 2097 / 2.47 79355426 05861 / 4.23 14 0804 5395773 3257 / 2.10 1360473 2280 / 2.56 79361851 06425 / 4.23 15 0802 5398921 3148 / 2.16 1362703 2230 / 2.46 79368113 06262 / 4.21 16 1050 5401982 3061 / 2.09 1364878 2175 / 2.57 79374413 06300 / 4.40 17 1140 5405022 3040 / 2.07 1367088 2210 / 2.54 79380921 06508 / 4.48 18 0801 5407519 2497 / 1.99 1368947 1859 / 2.53 79386259 05338 / 4 32 19 0800 5410464 2945 / 2.86 1371081 2134 / 2.39 79392527 06268 / 4.25 20 0801 5413387 2923 / 2.04 1373366 2285 / 2.93 79398716 6189 / 4.27 21 0801 5416393 3006 / 1.91 1376024 2658 / 2 94 79405083 06367 / 4.18 22 1058 5419521 3128 / 1.97 1378751 2727 / 2.91 79411782 06699 / 4.23 23 1152 5422132 2611 / 1.89 1381192 2441 / 2.84 79417855 06073 / 4.22 24 1057 5424492 2360 / 1.66 1383516 2324 / 2.69 79423560 05705 / 4.21 25 0802 5426801 2309 / 1.70 1385826 2310 / 2.76 79429353 05793 / 4.21 26 0802 5429070 2269 / 1.60 1387973 2147 / 2.62 79435098 05745 / 4.18 27 0802 5431678 2608 / 1.84 1390114 2141 / 2.61 79440960 05862 / 4.22 28 0801 5434366 2688 / 1.88 1392320 2206 / 2.44 79447026 06066 / 4.21 COMMENTS: ANALYST: ALAMAC INVESTORS, LLC REMEDIATION WELL REPORT 2019 MONTH: March DATE TIME WELL #1 WELL #1 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GPD / GPM INTEGRAT. GPD / GPM INTEGRAT. GPD / GPM 5434366 1392320 79447026 01 0800 5437089 2723 / 1.85 1394484 2164 / 2.52 79453164 06138 / 4.35 02 1058 5440191 3102 / 1.90 1396947 2463 / 2.57 79460274 07110 / 4.28 03 0957 5442733 2542 / 1.89 1398950 2003 / 2.54 79466074 05800 / 4.30 04 0800 5445611 2878 / 1.91 1401214 2264 / 2.58 79472635 06561 / 4.32 05 0800 5448021 2410/2.47 1403127 1913/2.47 79478146 05511/4.32 06 0801 5450704 2683 / 1.84 1405332 2205 / 2 59 79484296 06150 / 4.30 07 0804 5453377 2673 / 1 92 1407513 2181 / 2.65 79490353 06057 / 4.29 08 0801 5456090 2713 / 1.87 1409696 2183 / 2.32 79496470 06117 / 4.25 09 1020 5459137 3047 / 1.85 1412117 2421 / 2.52 79503277 06807 / 4.22 10 1028 5461911 2774 / 1.99 1414308 2191 / 2.72 79509468 06191 / 4.30 11 0802 5464429 2518 / 1.89 1416239 1931 / 2.46 79515079 05611 / 4.24 12 0800 5467186 2757 / 1.86 1418316 2077 / 2.43 79521310 06231 / 4.34 13 0801 5469843 2657 / 1.85 1420321 2005 / 2.33 79527365 06055 / 4.31 14 0802 5472959 3116 / 2.13 1422360 2039 / 2.44 79533524 06159 / 4.34 15 0800 5475957 2998 / 2.11 1424303 1943 / 2.32 79539463 05939 / 4.27 16 1157 5479670 3713 / 2.07 1426668 2365 / 2.33 79546790 07327 / 4.27 17 1200 5482741 3071 / 2.08 1428634 1966 / 2.36 79552892 06102 / 4.25 18 0801 5485228 2487 / 2.11 1430264 16630 / 2.37 79557910 05018 / 4.25 19 0800 5488336 3108 / 2.00 1432371 2107 / 2.30 79564382 06472 / 4.28 20 0802 5491169 2833 / 1.99 1434339 1968 / 2.39 79570368 05986 / 4.25 21 0800 5494056 28887 / 1.91 1436419 2080 / 2.32 79576497 06129 / 4.24 22 0802 5497066 3010 / 1.95 1438620 2201 / 2.43 79582977 06480 / 4.24 23 1150 5500131 3065 / 1.94 1440834 2214 / 2.36 79589664 06687 / 4.32 24 1150 5502901 2770 / 1.93 1442857 2023 / 2.29 79595843 06179 / 4.24 25 0803 5505473 2572 / 1.97 1444729 1872 / 2.38 79601647 05804 / 4.31 26 0804 5507871 2398 / 1.94 1446471 1742 / 2 34 79607115 05468 / 4.36 27 0802 5510783 2912 / 1.93 1448634 2163 / 2.40 79613853 06738 / 4.37 28 0800 5513634 2851 / 1.84 1450828 2194 / 2.22 79620582 06729 / 4.35 29 0800 5516046 2412 / 1.74 1452676 1848 / 2.31 79626372 05790 / 4.34 30 1158 5518868 2822 / 1.77 1454871 2195 / 2.28 79633308 06936 / 4.31 31 1358 5521509 2641 11.75 1456935 2064 / 2.28 79639904 06596 / 4.30 COMMENTS: ANALYST: ALAMAC INVESTORS, LLC REMEDIATION WELL REPORT 2019 MONTH: April DATE TIME WELL #1 WELL #1 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GPD / GPM INTEGRAT. GPD I GPM INTEGRAT. GPD / GPM 5521509 1456935 79639904 01 0801 5523442 1933 / 1 74 1458441 1506 / 2.25 79644739 04835 / 4.38 02 0804 5525814 2372 / 2.25 1460336 1895 / 2.25 79650870 6131 / 4.38 03 0800 5528525 2711 / 1.69 1462616 2280 / 2.47 79657958 7088 / 4.44 04 0801 5530952 2427 / 1.71 1464633 2017 / 2.35 79664372 6414 / 4.42 05 0800 5533465 2513 / 1.64 1466664 2031 / 2.15 79671017 6645 / 4.45 06 0840 5535593 2128 / 1.65 1468363 1699 / 2.04 79676758 5741 / 4.57 07 1140 5538304 2711 / 1.72 1470239 1876 / 1.92 79684017 7259 / 4.53 08 0801 5540579 2275 / 1 66 1471756 1517 / 1.79 79690184 6167 / 4.51 09 0800 5542754 2175 / 1.62 1473187 1422 / 1.92 79696095 5911 / 4.49 10 0800 5545164 2410 / 1.69 1474778 1591 / 1.89 79702636 6541 / 4.45 11 0800 5547582 2418 / 1.69 1476313 1535 / 1.89 79709067 6431 / 4.45 12 0800 5550248 2666 / 1.78 1477931 1618 / 1.68 79716042 6975 / 4.44 13 1155 5553122 2874 / 1.74 1480245 2314 / 2.51 79723576 7534 / 4.52 14 1210 5555418 2296 / 1.78 1482217 1972 / 2.50 79729558 5982 / 4.57 15 0802 5557513 2095 / 1.74 1483999 1782 / 2.42 79735017 5459 / 4.54 16 0800 5560137 2624 / 1.71 1486201 2202 / 2.46 79741809 6792 / 4.50 17 0802 5562656 2519 / 1 88 1488296 2095 / 2.44 79748249 6440 / 4.48 18 0800 5565285 2629 / 1.82 1490390 2094 / 2.36 79754764 6515 / 4.48 19 0825 5567917 2632 / 1.71 1492460 2070 / 2.38 79761217 6453 / 4.42 20 0958 5570279 2362 / 1.95 1494540 2080 / 2.99 79766790 5573 / 4.57 21 1155 5573469 3190 / 2.04 1497529 2989 / 3.16 79774141 7351 / 4.52 22 0801 5575924 2455 / 1.97 1499776 2247 / 2.82 79779853 5712 / 4.55 23 0800 5578793 2869 / 1.97 1502249 2473 / 2.82 79786604 6751 / 4.59 24 0802 5581370 2577 / 1.94 1504624 2375 / 3.21 79792690 6086 / 4.62 25 0800 5584169 2799 / 1.91 1507210 2586 / 3.09 79799299 6609 / 4.63 26 0800 5587094 2925 / 1.94 1509868 2658 / 3.11 79806146 6847 / 4.62 27 1125 5588059 0965 / 0.00 1512354 2486 / 2.19 79813717 7571 / 4.64 28 1030 5592435 4376 / 3.26 1514286 1932 / 2.33 79819927 6210 / 4.66 29 0800 5597074 4639 / 2.89 1516349 2063 / 2.30 79829606 9679 / 4.99 30 0805 5601713 4639 / 3 00 1518412 2063 / 3.00 79839285 9679 / 4.92 COMMENTS: ANALYST: ALAMAC INVESTORS, LLC REMEDIATION WELL REPORT 2019 MONTH: May DATE TIME WELL #1 WELL #1 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GPD / GPM INTEGRAT. GPD / GPM INTEGRAT. GPD / GPM 5601713 1518412 79839285 01 0801 5606354 4641 / 2.89 1520474 2062 / 2.25 79848964 9679 / 4.77 02 0801 5609591 3237 / 2.79 1521988 1514 79846257 2707 / 4.74 03 0801 5613677 4086 / 2.79 1523967 1979 / 2.29 79853240 6983 / 4.78 04 0810 5617597 3920 / 2.65 1525902 1935 / 2.16 79860100 6860 / 4.77 05 1140 5621823 4226 / 2.44 1528099 2197 / 2.34 79867978 7878 / 4.83 06 0802 5625049 3226 / 2.34 1529083 0984 / 2.22 79874255 6277 / 4.88 07 0801 5628429 3380 / 2.38 1531671 2588 / 2.17 79880999 6744 / 4.84 08 0800 5631789 3360 / 2.17 1533605 1934 / 2.15 79888199 7200 / 4.90 09 0802 5634481 2692 / 1.87 1535372 1767 / 2.14 79894843 6644 / 4.87 10 0800 5634983 0502 / 0.00 1537216 1844 / 2.14 79901879 7036 / 4.91 11 1155 5639736 4753 / 2.17 1539040 1824 / 2.15 79909102 7223 / 4.84 12 1410 5644489 4753 / 2.79 1540864 1824 / 2.29 79916325 7223 / 4.70 13 0800 5649242 4753 / 2.17 1542688 1824 / 2.29 79923548 7223 / 4.80 14 0800 5653993 5249 / 2.76 1544513 1825 / 2.10 79930720 7172 / 5.02 15 0801 5658287 4294 / 2,54 1546515 2002 / 2.09 79938779 8059 / 4.98 16 0800 5662042 3755 / 2.53 1548292 1777 / 2.12 79945947 7168 / 5.04 17 0801 5665386 3344 / 2.53 1549873 1581 / 1.95 79952419 6472 / 4.97 18 1135 5669521 4135 / 2.49 1551823 1950 / 1.95 79960475 8056 / 4.99 19 1125 5673358 3837 / 2.47 1553678 1855 / 1.96 79968236 7761 / 5.02 20 0800 5676118 2760 / 2.33 1555038 1360 / 1.93 79973971 5735 / 4.96 21 0800 5679240 3122 / 2.26 1556681 1643 / 1.92 79980879 6908 / 4.97 22 0800 5682495 3255 / 2.16 1558372 1691 / 1.93 79988034 7155 / 5.86 23 0800 5685672 3177 / 2.16 1560082 1710 / 2.04 79995258 7224 / 5.00 24 0800 5688628 2956 / 1.88 1561738 1656 / 1.92 80002658 7400 / 5.04 25 1155 5691921 3293 / 1.88 1563598 1860 / 1.76 80011054 8396 / 4.91 26 1225 5694969 3048 / 2.20 1565093 1495 / 1.74 80017993 6939 / 4.91 27 0801 5698021 3952 / 2.12 1566598 1505 / 1.79 80024886 6893 / 4.93 28 0750 5700546 2525 / 2.06 1567952 1354 / 1.92 80030791 5905 / 4.93 29 0800 5703519 2973 / 2.02 1669533 1581 / 1.85 80037943 7152 / 4.94 30 0800 5706477 2958 / 1.94 1571093 1560 / 1.78 80045144 7201 / 4.92 31 0800 5709560 3083 / 2.03 1572678 1585 / 1.68 80052633 7489 / 4.97 COMMENTS: ANALYST: ALAMAC INVESTORS, LLC REMEDIATION WELL REPORT 2019 MONTH: June DATE TIME WELL #1 WELL #1 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GPD / GPM INTEGRAT. GPD / GPM INTEGRAT. GPD / GPM 01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 5709560 1572678 80052633 1350 5713270 3710 / 2.12 1574486 1808 / 1.84 80061043 10218 / 4.93 1330 5716367 3097 / 2.35 1575960 1474 / 1.60 80067859 6816 / 4.90 0800 5719103 2736 / 2.21 1577134 1174 / 1.69 80073725 5866 / 4.91 0800 5722248 3145/2.21 1578486 1352/162 80080630 6905/4.97 0800 5725331 3083 / 2.11 1579860 1374 / 1 67 80087707 7077 / 5.03 0800 5728170 2829 / 2.01 1581225 1365 / 1.67 80094633 6926 / 5.04 0800 5731065 2895 / 1.94 1582736 1511 / 1.66 80102216 7583 / 5.07 1225 5734010 2945 / 1.93 1584488 1752 / 1.71 80110929 9128 / 5.64 1245 5736876 2866 / 1.95 1585986 1498 / 1.67 80118436 7507 / 5.18 0800 5739667 2791 / 2.06 1587303 1317 / 2.13 80124738 6302 / 5.14 0800 5742390 2723 / 2.15 1588964 1661 / 2.17 80131449 6711 / 5.15 0735 5745371 2981 / 2.16 1590966 2002 / 2.42 80138773 7324 / 5.13 0745 5748453 3082 / 2.12 1593100 2134 / 2 61 80146233 7460 / 5.21 7545 5751562 3109 / 2.07 1595260 2160 / 2.49 80153747 7514 / 5.19 1140 5754896 3334 / 2.20 1597550 2290 / 2.50 80161839 8092 / 5.31 1357 5758730 3834 / 2.18 1600104 2554 / 2.38 80171255 9416 / 5.27 0810 5761157 2787 / 2.26 1601683 1579 / 2.36 80177173 5918 / 5.33 0740 5764019 2862 / 2.19 1603495 1812 / 2.42 80184100 6927 / 5.34 0740 5767111 3092 / 2.14 1605467 1972 / 2.31 80191723 7623 / 5.27 0740 5770508 3397 / 2 13 1607625 2158 / 2.14 80200191 8468 / 5 25 0755 5773284 2776 / 2.07 1609439 1814 / 2.33 80207426 7235 / 5.36 1100 5776554 3270 / 1.97 1611581 2142 / 2.15 80216110 8684 / 5.37 1300 5779758 3204 / 2.21 1613426 1845 / 1.93 80224371 8261 / 5.39 0740 5782090 2332 / 2.14 1614667 1241 / 2.04 80230160 5789 / 5.42 0729 5785200 3110 / 2.10 1616553 1886 / 2.16 80238027 7867 / 5.40 0750 5788412 3212 / 2.20 1618447 1894 / 2.07 80246032 8005 / 5.33 0749 5791559 3147 / 2.37 1620276 1829 / 2.01 80253892 7860 / 5.40 0730 5794793 3234 / 2.35 1621995 1719 / 2.14 80261373 7481 / 5.44 1110 5798610 3817 / 2.15 1624099 2104 / 1.99 80278528 7155 / 5.43 1200 5801938 3328 / 2.17 1625973 1874 / 1.98 80278702 0174 / 5.44 COMMENTS: ANALYST: LUMBERTON ENERGY HOLDINGS, LLC REMEDIATION WELL REPORT 2019 MONTH: July DATE TIME WELL #1 WELL #1 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GPD / GPM INTEGRAT. GPD / GPM INTEGRAT. GPD / GPM 5801938 1625973 80278702 01 0745 5804497 2559 / 2.21 1627405 1432 / 1 92 80285083 6381 / 5.44 02 0750 5808005 3508 / 2.25 1629390 1985 / 2.21 80293765 8682 / 5.41 03 0733 5810801 2796 / 2.28 1630684 1294 / 1.22 80300564 6799 / 5.15 04 0810 5813353 2552 / 1.62 1631956 1272 / 1.26 80309000 8436 / 5.43 05 0750 5815584 2231 / 1.68 1632373 0417 / 0.00 80316638 7638 / 5.52 06 1425 5818623 3039 / 1.79 1635334 2961 12.27 80326737 10099 / 5.51 07 1450 5819848 1225 / 0.00 1637575 2241 / 2.74 80334351 7614 / 5.51 08 0750 5824969 5121 / 2.66 1639531 1956 / 2.96 80340587 6236 / 5.48 09 0751 5828751 3782 / 2.53 1641766 2235 / 2.67 80348261 7674 / 5.54 10 0750 5832118 3367 / 2.00 1644127 2361 / 2 79 80356203 7942 / 5.49 11 0758 5832812 0694 / 0.00 1646758 2631 / 3.02 80364463 8260 / 5.57 12 0747 5832813 0001 / 0.00 1649234 2476 / 2.87 80372362 7899 / 5.56 13 0858 5832813 MALFUNCTION 1651775 2541 / 2.93 80380474 8112 / 5.46 14 1425 5832813 MALFUNCTION 1654797 3022 / 2.78 80390252 9778 / 5.47 15 0750 5832813 MALFUNCTION 1656444 1647 / 3.06 80395804 5552 / 5.49 16 0747 5832813 MALFUNCTION 1659207 2763 / 2 95 80404164 8360 / 5.52 17 0750 5832813 MALFUNCTION 1661843 2636 / 3.04 80412160 7996 / 5.49 18 0750 5832813 MALFUNCTION 1664322 2479 / 3.07 80419714 7554 / 5.51 19 0754 5832813 MALFUNCTION 1667203 2881 / 3.02 80428500 8786 / 5.45 20 0820 5832813 MALFUNCTION 1669750 2547 / 2.89 80436216 7716 / 553 21 1115 5832813 MALFUNCTION 1672297 2547 / 3.03 80443931 7715 / 5.53 22 0740 5832813 MALFUNCTION 1674844 2547 / 3.03 80451647 7716 / 5.53 23 0752 5832813 MALFUNCTION 1677391 2547 / 3.12 80459362 7715 / 5.47 24 0751 5832813 MALFUNCTION 1680032 2641 / 3.04 80467404 8042 / 5.47 25 0750 5832813 MALFUNCTION 1682833 2801 / 3.21 80475739 8335 / 5.47 26 0756 5832813 MALFUNCTION 1684874 2041 / 2.96 80482410 6671 / 5.46 27 1200 5832813 MALFUNCTION 1687845 2971 / 3.11 80490828 8418 / 5.42 28 1250 5832813 MALFUNCTION 1690397 2552 / 2.99 80498034 7206 / 5.30 29 0751 5832813 MALFUNCTION 1692502 2105 / 2.80 80505241 7207 / 5.30 30 0750 5832813 MALFUNCTION 1694894 2392 / 2.85 80512654 7413 / 5.34 31 0750 5832813 MALFUNCTION 1695633 0739 / 2.17 80514928 2274 / 5.97 COMMENTS: REMEDIATION SYSTEM MALFUNCTIONED ON 7130/19 AND CORRECTED ON 7/31/19. ANALYST: Lumberton Energy Holdings, LLC REMEDIATION WELL REPORT 2019 MONTH: August DATE TIME WELL #1 WELL #1 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GIRD / GPM INTEGRAT. GPD / GPM INTEGRAT. GIRD / GPM 5832814 1695633 80514928 01 0740 5832814 MALFUNCTION 1698100 2467 / 3.00 80522323 7395 / 5.40 02 0735 5832814 MALFUNCTION 1700567 2467 / 3.19 80529718 7395 / 5.46 03 1057 5832814 MALFUNCTION 1703720 3153 / 3.40 80538108 8390 / 3.40 04 1245 5832814 MALFUNCTION 1706823 3103 / 3.38 80546499 8391 / 5.43 05 0750 5832814 MALFUNCTION 1709266 2443 / 3.43 80553064 6565 / 5.45 06 0755 5832814 MALFUNCTION 1712264 2998 / 3.45 80561216 8152 / 5.41 07 0750 5832814 MALFUNCTION 1715115 2851 / 3.31 80568960 7744 / 5.42 08 0756 5832814 MALFUNCTION 1718010 2895 / 3.31 80576968 8008 / 5.46 09 0756 5832814 MALFUNCTION 1720550 2540 / 3.05 80584417 7449 / 5.46 10 1158 5832814 MALFUNCTION 1723395 2645 / 2.93 80593293 8876 / 5.41 11 1225 5832814 MALFUNCTION 1725976 2581 / 3.02 80601279 7986 / 5.94 12 0756 5832814 MALFUNCTION 1728433 2457 / 3.15 80608326 7047 / 5.44 13 0755 5832814 MALFUNCTION 1731182 2749 / 3.21 80616154 7828 / 5.50 14 0758 5832814 MALFUNCTION 1733732 2550 / 3.28 80623444 7290 / 5.47 15 0750 5832814 MALFUNCTION 1736701 2969 / 3.12 80631956 8512 / 5.46 16 0758 5832814 MALFUNCTION 1739463 2762 / 3.36 80639813 7857 / 5.51 17 1200 5832814 MALFUNCTION 1742678 3215 / 3.33 80648962 9149 / 5.49 18 1300 5832814 MALFUNCTION 1745306 2628 / 3.13 80656762 7800 / 5.54 19 0757 5832814 MALFUNCTION 1747412 2106 / 3.04 80663123 6361 / 5.51 20 0757 5832814 MALFUNCTION 1750028 2616 / 2.97 80671231 8108 / 5.54 21 0752 5832814 MALFUNCTION 1752219 2191 / 2.41 80679544 8313 / 5.51 22 0745 5832814 MALFUNCTION 1754059 1840 / 2.28 80686803 7259 / 5.54 23 0751 5832814 MALFUNCTION 1756516 2457 / 2.42 80696427 9624 / 5.59 24 1450 5832814 MALFUNCTION 1758756 2240 / 2.82 80704914 8487 / 5.47 25 1326 5832814 MALFUNCTION 1761147 2391 / 3.15 80712335 7421 15.54 26 0758 5832814 MALFUNCTION 1763407 2260 / 3.14 80719019 6684 / 5.51 27 0752 5832814 MALFUNCTION 1766011 2604 / 3.04 80726796 7777 / 5.49 28 0758 5832814 MALFUNCTION 1768547 2536 / 3.09 80734394 7598 / 5.54 29 0755 5832814 MALFUNCTION 1771194 2647 / 3.11 80742310 7516 / 5.55 30 0758 5832819 MALFUNCTION 1773897 2703 / 3.11 80750523 8213 / 5.54 31 1257 5832814 MALFUNCTION 1776925 3028 / 2.97 80759793 9270 / 5.57 COMMENTS: ANALYST: LUMBERTON ENERGY HOLDINGS, LLC REMEDIATION WELL REPORT 2019 MONTH: September DATE TIME WELL #1 WELL #1 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GPD / GPM INTEGRAT, GPD / GPM INTEGRAT. GPD / GPM 5832819 1776925 80759793 01 1158 5832819 MALFUNCTION 1779415 2490 / 3.01 80767458 7665 / 5.53 02 1158 5832819 MALFUNCTION 1782008 2593 / 3.01 80775500 8042 / 5.46 03 0800 5832819 MALFUNCTION 1784505 2497 / 2.92 80783286 7786 / 5.44 04 0754 5832819 MALFUNCTION 1786557 2052 / 2 87 80789730 6444 / 5.45 05 0755 5832819 MALFUNCTION 1789514 2957 / 2.92 80799019 9289 / 5.53 06 0800 ELECTRICAL MALFUNCTION ELECTRICAL POWER FAILURE 07 1256 5832819 MALFUNCTION 1791792 2278 / 2.33 80807952 8933 / 5.64 08 1258 5832819 MALFUNCTION 1793038 1246 / 2.31 80816306 8354 / 5.65 09 0757 5832819 MALFUNCTION 1795427 2389 / 2.38 80822719 6413 / 5.65 10 0758 5832819 MALFUNCTION 1797383 1956 / 2.15 80830634 7915 / 5.64 11 0750 5832819 MALFUNCTION 1799517 2134 / 2.51 80839387 8753 / 5.61 12 0757 5832819 MALFUNCTION 1801458 1941 / 2.27 80847353 7966 / 5.45 13 0758 5832819 MALFUNCTION 1803307 1849 / 2.30 80855061 7708 / 5.67 14 0957 5832819 MALFUNCTION 1805432 2125 / 2.38 80863937 8876 / 5.60 15 1238 5832819 MALFUNCTION 1807560 2128 / 2.17 80872827 8890 / 5.61 16 0758 5832819 MALFUNCTION 1809179 1619 / 2.36 80879568 6741 / 5.67 17 0800 5832819 MALFUNCTION 1811139 1960 / 2.29 80887664 8096 / 5.67 18 0800 5832819 MALFUNCTION 1813094 1955 / 2.19 80895857 8193 / 5.64 19 0755 5832819 MALFUNCTION 1815081 1987 / 2.33 80902430 6573 / 5.62 20 0757 5832819 MALFUNCTION 1816979 1898 / 2 41 80910268 7838 / 5.64 21 0958 5832819 MALFUNCTION 1819053 2074 /. 2.20 80920659 10391 / 5.68 22 1147 5832819 MALFUNCTION 1821121 2068 / 2.28 80929442 8783 / 5.60 23 0756 5832819 MALFUNCTION 1822779 1658 / 2.25 80936541 7099 / 5.68 24 0758 5832819 MALFUNCTION 1824646 1867 / 2.11 80944549 8008 / 5.59 25 0757 5832819 MALFUNCTION 1826524 1878 / 2.17 80952670 8121 / 5.64 26 0757 5832819 MALFUNCTION 1828388 1864 / 2.15 80960711 8041 / 5.60 27 0758 5832819 MALFUNCTION 1830251 1863 / 2.14 80968752 8041 / 5.61 28 1020 5832819 MALFUNCTION 1832208 1957 / 2.11 80977374 8622 / 5.62 29 1200 5832819 MALFUNCTION 1834106 1898 / 2.16 80985709 8335 / 5.60 30 0757 5832819 MALFUNCTION 1835727 1621 / 2.33 80992719 7010 / 5.60 COMMENTS: ELECTRICAL POWER FAILURE 9106/19 ANALYST: LUMBERTON ENERGY HOLDINGS, LLC REMEDIATION WELL REPORT 2019 MONTH: October DATE TIME WELL #1 WELL 41 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GPD 1 GPM INTEGRAT. GPD 1 GPM INTEGRAT. GPD 1 GPM 5832819 1835727 80992719 01 0755 5832819 MALFUNCTION 1837605 187812.13 81000751 803215.61 02 0756 5832819 MALFUNCTION 1839609 200412.37 81009226 847415.62 03 0755 5832819 MALFUNCTION 1941547 193812.31 81017375 8150 / 5.61 04 0756 5832819 MALFUNCTION 1943610 206312.74 81025254 7879 / 5.57 05 1157 5032019 MALFUNCTION 1846208 26012.80 81034282 902015.02 06 1157 5832819 MALFUNCTION 1848516 2306 f 2.70 51042086 780616.52 07 0758 5832819 MALFUNCTION 1850825 230912.69 81049694 780615.62 08 0758 5832819 MALFUNCTION 1853277 245212.78 81058224 833015,60 09 0758 5832819 MALFUNCTION 1855729 245212.91 B1066554 8330 / 5.65 10 0755 6832819 MALFUNCTION 1857974 224512.07 81074024 747015.65 11 0758 5832819 MALFUNCTION 1860506 253212.87 81082429 8405 / 5.64 12 1158 5832019 MALFUNCTION 1863219 2713 f 2.88 81091448 901915.67 13 1258 6832919 MALFUNCTION 1866744 2525 f 2.74 61099900 846215.64 14 0758 5832819 MALFUNCTION 1867789 204512.84 81106739 683915.71 15 0757 5832819 MALFUNCTION 1870327 253812.98 81115212 847315.69 16 0759 5832819 MALFUNCTION 1872713 2306 / 2.85 81123091 78791 5.65 17 0757 5832819 MALFUNCTION 1875239 252612.94 81131329 8238/5.67 18 0758 5832819 MALFUNCTION 1877685 244612.96 81139184 785515.65 19 1212 5832819 MALFUNCTION 1880212 252712.90 81/41574 839015.65 20 1158 5832819 MALFUNCTION 1882739 252712.91 61155984 839015.59 21 0758 5832819 MALFUNCTION 1885266 252712,73 81164356 839215,59 22 0759 5832819 MALFUNCTION 1887260 199412.76 81171226 687015.67 23 0758 5832819 MALFUNCTION 1889703 244312.75 81179641 841515.62 24 0758 5832819 MALFUNCTION 1892079 237612 83 81187778 81371 5.63 25 0755 5832819 MALFUNCTION 1894395 231612.78 81195702 792415.65 26 1067 $632819 MALFUNCTION 1897005 261012.75 81204704 900215.54 27 1100 $832819 MALFUNCTION 1899307 230212.71 81212880 817615.66 28 0755 5832819 MALFUNCTION 1901404 2097 / 2.67 81220358 747815,57 29 0758 5832819 MALFUNCTION 1903592 2188 / 2.67 81228157 779915.60 30 0769 5832819 MALFUNCTION 1906909 231712.76 81236336 817915.51 31 0758 5832819 MALFUNCTION 1906089 218012.54 81244349 801315.60 COMMENT& � ANALYST`L>'11JLQ� LUMBERTON ENERGY HOLDINGS, LLC REMEDIATION WELL REPORT 2019 MONTH: November DATE TIME WELL #1 WELL #1 WELL #2 WELL #2 WELL #3 WELL #3 INTEGRAT. GPD I GPM INTEGRAT. GPD I GPM INTEGRAT. GPD 1 GPM 5832819 1908089 81244349 01 0758 5832819 MALFUNCTION 1910270 218112.64 81252517 816815.54 02 1155 SB32819 MALFUNCTION 1912156 248512.60 81261664 914715.56 03 1055 5832819 MALFUNCTION 1914984 222912.66 81269685 802115.52 04 0748 5832819 MALFUNCTION 1917101 211712.64 81277218 753315.54 05 0800 5832819 MALFUNCTION 1919217 211612.56 81284750 753215-50 06 0756 5832819 MALFUNCTION 1921484 226712.50 61292931 818115-50 07 0755 5832819 MALFUNCTION 1923751 2267 / 2.62 81301112 8181 1 5.56 08 0757 5832819 MALFUNCTION 1926024 227312.51 81309311 819915,62 09 0700 5832819 MALFUNCTION 1927940 191612.75 81317449 813815.50 10 1o18 5832819 MALFUNCTION 1929783 194310.00 81325686 813715.64 11 0758 5832819 MALFUNCTION 1831972 218912.77 81333266 768015,57 12 0758 5832819 MALFUNCTION 1934479 250713.27 81341567 829115.57 13 0758 5832819 MALFUNCTION 1936967 248813.27 81349198 764115.62 14 0758 5832619 MALFUNCTION 1939770 2803 / 3.60 81357419 8221 15.56 15 0758 5832819 MALFUNCTION 1944504 47341 &57 81365303 788415.70 i6 0910 6832819 MALFUNCTION 1948260 374614.13 81373573 827016.65 17 1211 5832819 MALFUNCTION 1952349 409914.12 81302712 913915.61 18 0758 5832819 MALFUNCTION 1955467 311814.31 81389677 896516.67 19 0758 5832819 MALFUNCTION 1958965 349814.23 81397457 778016.54 20 0757 5832819 MALFUNCTION 1962597 363214.21 81405507 805015.54 21 0755 5832819 MALFUNCTION 1966042 344514.20 81413123 781615.51 22 0800 5832819 MALFUNCTION 1969987 394514.99 81421896 8773 f 6.89 23 1040 5832619 MALFUNCTION 1973849 386214.50 81430093 819715.55 24 1115 5832999 MALFUNCTION 1977424 357514.98 81437536 744315.60 25 0800 5832999 MALFUNCTION 1980999 3576 f 4.13 81444979 744315.54 26 0800 5832999 MALFUNCTION 1984574 357514.36 81452421 744215.52 27 0800 5832999 MALFUNCTION 1988840 426615.36 81460664 8243I6.01 28 0828 5832999 MALFUNCTION 1994632 5792 f 5.98 81469797 913315.60 29 0820 5832999 MALFUNCTION 1999197 4565 f 5.82 81477019 722215.62 30 1158 5832999 MALFUNCTION 2005232 6035 / 6.06 81486482 946315.61 COMMENTS: ANALYST: -911/n LUMBERTON ENERGY HOLDINGS, LLC REMEDIATION WELL REPORT 2019 MONTH: December DATE TIME WELL #1 INTEGRAT. WELL #1 GPDIGPM WELL #2 INTEGRAT. WELL #2 GPDIGPM WELL #3 INTEGRAT WELL #3 GPDIGPM 5832999 2005232 81486492 01 1344 5832999 MALFUNCTION 2010486 525415.79 81494706 822415.72 02 0759 5832999 MALFUNCTION 2014496 401016.02 81501016 6310 / 5.67 03 0800 5832999 MALFUNCTION 2020047 555116,14 81509710 869415.64 04 0800 5832999 MALFUNCTION 2025025 497815.96 $1517515 780515.62 05 0804 5839632 663313 80 2029930 490515.92 81525275 776015.58 06 0805 5845305 567313.69 2035330 540016- 4 81533728 845315.64 07 07SS 58N049 47" 13,29 2040192 486215.86 81541414 7686 f 5.54 08 1168 5855157 510812.75 2046381 618916.01 81551349 993515.73 09 0758 5658536 3379 / 2.87 2060612 4231 18,03 81558129 678016.65 10 0758 5562467 3931 12,90 2055580 496816.15 81586059 7930 / 5.69 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 COMMENTS: 1101 REMEDIATION WELL RETURNED TO SERVICE 12M4M9 ® 1030 HOURS. ANALYST: 1,2za a - ,