19025_AMI_OAR_20140519

SOIL VAPOR AND
WATER SUPPLY WELL SAMPLING REPORT
AM19 INC. SITE
NCD0001259
2609 TUCKER STREET
BURLINGTON, ALAMANCE COUNTY, NORTH CAROLINA
S&ME PROJECT NO. 1054-14-2086
Prepared for:
North Carolina Department of Environment and Natural Resources
Division of Waste Management
Inactive Hazardous Sites Branch
Superfund Section
Green Square Complex
217 West Jones Street
Raleigh, North Carolina 27603
Candy E. i tt, P.G.
Staff Geoldgist
Prepared by:
#S&ME
3201 Spring Forest Road
Raleigh, North Carolina 27616
[phone]
S&ME PROJECT NO. 1054-14-2086
May 19, 2014
Edmund Woloszyn, J .,
Project Manager

Soil Vapor and Water Supply Well Sampling Report
AMI, Inc. Burlington, Alamance County, North Carolina
May 19, 2014
S&ME Project No. 1054-14-2086
1.0 INTRODUCTION................................................................................. I
2.0
PROJECT BACKGROUND AND PURPOSE........................................1
3.0
METHODS..........................................................................................2
3.1
HEALTH AND SAFETY PLAN............................................................................................ 2
3.2
SOIL VAPOR SAMPLING................................................................................................... 2
3.3
WATER SUPPLY WELL SAMPLING.................................................................................. 2
3.4
QUALITY ASSURANCE/QUALITY CONTROL.................................................................... 3
4.0
RESULTS...........................................................................................3
4.1
SOIL VAPOR SAMPLING RESULTS................................................................................... 3
4.2
WATER SUPPLY WELL SAMPLING RESULTS.................................................................. 3
4.3
QUALITY ASSURANCE/QUALITY CONTROL RESULTS .................................................... 3
5.0
CONCLUSIONS..................................................................................4
5.1
SOIL VAPOR..................................................................................................................... 4
5.2
WATER SUPPLY WELL.................................................................................................... 4
Tables
Table I Soil Vapor Sampling Analytical Results
Table 2 Water Supply Well Sampling Analytical Results
Fi ures
Figure 1 Vicinity Map
Figure 2 Site Map
Figure 3 Sample Results Map
Appendices
Appendix I Photographic Log
Appendix II Field Sampling Summary Sheet
Appendix III Laboratory Analytical Report

Soil Vapor and Water Supply Well Sampling Report May 19, 2014
AMI, Inc. Burlington, Alamance County, North Carolina S&ME Project No. 1054-14-2086
1.0 INTRODUCTION
S&ME, Inc.'s scope of services were performed in general accordance with proposal number 43-
14000148 Revision 1.2, dated February 26, 2014, and as authorized by the North Carolina
Department of Environment and Natural Resources (NCDENR) Task Authorization dated
February 26, 2014 under Contract #N10005S.
S&ME completed the following scope of services approved for this task authorization:
• Prepared a site specific health and safety plan;
• Installed nine soil gas probes;
• Collected soil gas samples from each of the soil gas probes;
• Collected a water supply well sample from water supply well WSW-1; and,
• Prepared this report.
2.0 PROJECT BACKGROUND AND PURPOSE
The AMI, Inc. site is located at 2609 Tucker Street, Burlington, Alamance County, North
Carolina. A groundwater plume containing chlorinated hydrocarbons has been documented in
the shallow and bedrock groundwater aquifers. The primary chemicals of concern (COCs) in
groundwater are tetrachloroethylene (PCE), trichloroethylene (TCE), and the degradation
daughter products of PCE and TCE (Additional Investigation; Kleinfelder; April 12, 2011). A
vicinity map is provided as Figure 1 and the site and the surrounding area shown in Figure 2.
On March 25, 2014, Mr. Adam Ulishney of NCDENR Inactive Hazardous Sites Branch (IHSB)
contacted Mr. Edmund Woloszyn of S&ME requesting a proposal to assess properties proximal
to the AMI, Inc. site for COCs in soil vapor. S&ME proposed to use a Geoprobe drill rig to
install post -run tubing (PRT) system to approximately 10 feet below ground surface (ft. bgs.) to
collect soil vapor samples. Mr. Ulishney also requested that if groundwater was encountered at
10 ft. bgs. or above, that a temporary monitor well be installed and a groundwater sample
collected. In addition, IHSB requested the sampling and analyses of a water supply well located
at 2523 Tucker Street, which is located north of the AMI, Inc. site.
This report presents the field methods of the assessment conducted at the AMI, Inc. site, the
laboratory analytical results of soil gas and water samples collected, and conclusions.

Soil Vapor and Water Supply Well Sampling Report
AMI, Inc. Burlington, Alamance County, North Carolina
3.0 METHODS
3.1 Health and Safety Plan
May 19, 2014
S&ME Project No. 1054-14-2086
S&ME prepared a site -specific Health and Safety Plan (HASP) in general accordance with 29
CFR 1910.120, which addressed the contaminants known or suspected to be present on -site,
personal protective equipment, monitoring performed during the field activities, and response
actions to be taken in the event monitoring thresholds are exceeded. To mitigate the potential for
damage to underground utilities, S&ME contacted One Call and retained the services of a private
utility locating service to clear the locations for the PRT borings.
3.2 Soil Vapor Sampling
Between April 8 and April 10, 2014, S&ME installed and sampled nine soil vapor points using
the PRT system. The PRT system was advanced by a track -mounted Geoprobe 7730DT using
1.5-inch direct push rods. The PRT system was installed to target depths of between nine and 10
ft. bgs. Groundwater was not encountered in any of the borings; therefore, no temporary
monitoring wells were installed, and no shallow groundwater samples were collected.
Following installation of the PRT system, S&ME performed a leak test. The sampling array was
tested for leaks by placing a plastic shroud over the soil vapor monitoring point and injecting
helium (tracer) gas into the plastic shroud. The sampling array was monitored for leaks by
monitoring the tracer gas using a helium detection meter that was connected to the sampling
array. No tracer gas was detected in any of the nine sampling arrays, indicating that the
sampling array did not have leaks.
After successfully passing the leak test, a six -liter SUMMA canister equipped with a three hour
regulator was connected to each sampling array. A total of nine record samples were collected,
along with one QA/QC split sample. The SUMMA canisters were shipped to ESC Lab Sciences
(ESC) of Mt Juliet, Tennessee for analysis. The samples were analyzed for volatile organic
compounds (VOCs) by Method TO-15 SIM standard parameter list.
After the soil vapor samples were collected, S&ME removed the stainless steel casing materials
and filled the boreholes with a mixture of soil and bentonite clay. The locations of the soil vapor
probes were recorded with a mapping grade sub -meter GPS unit. A photographic log of the
activities performed is provided in Appendix I.
3.3 Water Supply Well Sampling
On April 9, 2014, S&ME personnel sampled one water supply well, WSW-1, located at 2523
Tucker Street. A spigot at the wellhead was opened, and the water allowed to flow for
approximately 15 minutes. Field parameters of pH, temperature, and conductivity were
measured and recorded. The field parameter measurements sheet is provided in Appendix II.
After purging, two samples were collected, one record sample and one replicate sample, placed
directly into laboratory supplied containers, and shipped under standard chain -of -custody
procedure to ESC for analysis. The samples were analyzed for VOCs by EPA Method 8260B.

Soil Vapor and Water Supply Well Sampling Report May 19, 2014
AMI, Inc. Burlington, Alamance County, North Carolina S&ME Project No. 1054-14-2086
3.4 Quality Assurance/Quality Control
S&ME collected QA/QC samples for soil vapor and water supply well samples. A "split"
sample was collected at vapor point VP-6 by installing a split sample train, to which a summa
canister was attached at both ends. Each of the split samples were allowed to draw until the
regulators had collected sufficient volume for analysis. The split sample was submitted to ESC
for laboratory analysis by EPA Method TO-15.
One duplicate sample was collected from water supply well WSW-1. The sample was collected
in series after the record sample and submitted for laboratory analysis for VOCs by EPA Method
8260B. In addition, one trip blank was included in the cooler and analyzed for VOCs.
4.0 RESULTS
4.1 Soil Vapor Sampling Results
The laboratory analytical results of the soil vapor samples collected on April 9 and 10, 2014,
indicated that PCE and TCE were reported at concentrations above the sub -slab and exterior
vapor intrusion screening levels (VISLs) in sample VP-4. Sample VP-4 was collected at the
property located at 1006 Hahn Road. During the field activities, it was noted that this property
has a basement.
Additional constituents were reported in samples VP-1 through VP-9 at concentrations above the
reporting limits, but below the VISLs. The laboratory analytical results for the soil vapor
samples is presented in Table 2, and shown on Figure 3. A copy of the laboratory analytical
report is provided in Appendix III.
4.2 Water Supply Well Sampling Results
The laboratory analytical results of the record and duplicate samples collected from water supply
well WSW-1 indicated that two constituents, PCE and TCE, were reported at concentrations
above the 2L Standards. A summary of the water supply well analytical results is provided in
Table 2, and shown in Figure 3. A copy of the laboratory analytical report is provided in
Appendix III.
4.3 Quality Assurance/Quality Control Results
According to the laboratory analytical results, the QA/QC split sample for the soil vapor sample
of VP-6 were similar in comparison. Benzene, chloromethane, and ethylbenzene were reported
in both VP-6 and the split sample (DUP-1) and comparable concentrations. However, the record
sample VP6 had reported concentrations of carbon tetrachloride and PCE near the method's
detection limit. Whereas carbon tetrachloride and PCE were below the method's detection limit
of the split sample DUP-1.
The results of the duplicate water supply well sample DUP-2 were well within ten percent of the
results of the record sample WSW-1. No VOCs were reported in the trip blank. The analytical
results of the QA/QC soil vapor and water samples are provided in Tables 1 and 2, respectively.

Soil Vapor and Water Supply Well Sampling Report
AMI, Inc. Burlington, Alamance County, North Carolina
5.0 CONCLUSIONS
5.1 Soil Vapor
May 19, 2014
S&ME Project No. 1054-14-2086
Soil vapor sample analytical results indicate that COCs reported at the AMI, Inc. site are present
in sub -surface soils near the residences along Hahn Road. One soil vapor sample, VP-6, which
is located at 1006 Hahn Road, had reported concentrations of PCE and TCE above the sub -slab
and exterior VISLs. The residence located at this address has a basement, and may be a possible
receptor of PCE and TCE through vapor intrusion from the soil into the basement.
5.2 Water Supply Well
The laboratory analytical results of the water supply well sample, WSW-1, collected at 2523
Tucker Street, indicated that PCE and TCE were detected at concentrations above the 2L
Standards. S&ME was told by Mr. Gary Oakley, the property owner, that this well is not used as
a source of potable water; however, the future use of the well from this well may need to be
evaluated for possible exposure to the COCs.

TABLES

TABLE 1
Soil Vapor Sampling Analytical Results
IHSB AMI, Inc. NONCD0001259
Burlington, Alamance County, North Carolina
S&ME Project No. 1054-14-2086
Client Sample ID
VP -I
2523 S TUCKER
VP-2
I010 HAHN RD.
VP-3
1003 HAHN RD
VP-4
1006 HAHN RD
VP-5
963 HAHN RD
VP-6
960 RAHN RD
DUP-1
(Duplica6t) of VP-
VP-7
952 HAHN ROAD
VP-8
939 HAHN ROAD
VP-9
930 HAHN ROAD
Sub -Slab and
Collect Date
4/9/2014
4/9/2014
4/9/2014
4/9/2014
4/9/2014
4/9/2014
4/9/2014
4/9/2014
4/9/2014
4/10/2014
Exterior VISE,
Method
Parameter
Units
Value
Value
Value
Value
Value
Value
Value
Value
Value
Value
TO-15
Benzene
µg/m3
7.3
0.48
7.7
9.6
9.6
10
11
4.5
5.7
3.8
104
TO-15
Carbon tetrachloride
µg/m3
0.43
0.45
0.33
<0.13
0.4
0.37
<0.13
0.2
0.35
<0.13
135
TO-15
Chloroform
µg/m3
1.7
0.1
<0.097
4.2
<0.097
<0.097
<0.097
<0.097
<0.097
<0.097
35.3
TO-15
Chloromethane
µg/m3
3.3
1.1
<0.062
3.3
5
3.7
2.9
2
5.4
11
626
TO-15
1,4-Dichlorobenzene
µg/m3
<0.12
<0.12
<0.12
<0.12
<0.12
<0.12
0.14
<0.12
<0.12
<0.12
73.7
TO-15
cis-1,2-Dichloroethene
µg/m3
<0.079
<0.079
<0.079
0.71
<0.079
<0.079
<0.079
<0.079
<0.079
<0.079
NE
TO-15
Ethylbenzene
µg/m3
3.3
0.16
2.5
1.5
3.2
2.9
2.6
1.2
1.9
1.4
324
TO-15
Tetrachlomethylene
µg/m3
0.33
<0.14
0.81
2,400
0.81
0.31
<0.14
0.14
0.18
0.17
278
TO-15
Trichloroethylene
µg/m3
<0.11
<0.11
<0.I1
390
<0.11
<0.11
<0.11
<0.11
<0.11
<0.11
13.9
Notes
µg/m3: microgam per cubic meter
VISL: Vapor Intrusion Screening Level (North Carolina Department of Environment and Natural Resources, January 2014)

TABLE 2
Water Supply Well Sampling Analytical Results
IHSB AMI, Inc. Site NONCD0001259
Burlington, Alamance County, North Carolina
S&ME Proposal No.1054-14-2086
Client Sample ID
WSW-1
DUP-2
TRIP BLANK
2L Standard
Collect Date
4/9/2014
4/9/2014
4/9/2014
Method
Parameter
Units
Value
Value
Value
8260B
cis- 1,2-Dichloroethene
µg/1
3.2
3.1
<1.0
70
8260B
Tetrachloroethene
µg/1
ENEF-
32
31
<1.0
0.7
8260B
Trichloroethene
µg/1
30
29
<1.0
3
Notes
µg/l: micrograms per liter
2L Standard: 15A NCAC 2L Groundwater Standards
Samples in BOLD were reported at concentrations above the laboratory method detection limits.
Samples in BOLD and shaded were reported at concentrations above the 2L standards.

FIGURES

N
GRAPHIC SCALE
1000 0 500 1000 2000
DATA SOURCE: USGS DRG (IN FEET)
BURLINGTON, DATED 2013
CONTOUR INTERVAL 10 FEET A-4304
SCALE: 1„ _ 2000, FIGURE NO.
DATE: APRIL 2014 *S&ME VICINITY MAP
DRAWN BY: BTR 1
WWW.SMEINC.COM IHSB AMI, INC - 2609 TUCKER ST
PROJECT NO: NC ENGINEER LICENSE#F-0176 BURLINGTON, NORTH CAROLINA
1054-14-2086 3201 SPRING FOREST RD, RALEIGH, NC 27616

IMAGE SOURCE: NC ONEMAP, DATED 2010
SCALE: 1" = 300,
DATE: APRIL 2014 > S&ME
DRAWN BY: BTR '
WWW.SMEINC.COM
PROJECT NO: NC ENGINEER LICENSE #F-0176
1054-14-2086 3201 SPRING FOREST RD, RALEIGH, NC 27616
GRAPHIC SCALE
150 0 75 150 300
( IN FEET)
SITE MAP
IHSB AMI, INC - 2609 TUCKER ST
BURLINGTON, NORTH CAROLINA
A-4305
FIGURE NO.
2

LEGEND
VAPOR RESULTS IN ug/m3 - MICROGRAMS PER CUBIC METER GRAPHIC SCALE
GROUNDWATER RESULTS IN ug/L - MICROGRAMS PER LITER 150 0 75 150 300
* ONLY EXCEEDENCES OF VISL OR 2L ARE SHOWN
VISL -VAPOR INTRUSION SCREENING LEVEL ( IN FEET)
< VISL - RESULTS BELOW VAPOR INTRUSION SCREENING LEVEL
IMAGE SOURCE: NC ONEMAP, DATED 2010 A-4306
SCALE: 1" = 300,
FIGURE NO.
DATE: APRIL2014 *S&ME
SAMPLE RESULTS MAP
DRAWN BY: BTR 3
WWW.SMEINC.COM IHSB AMI, INC - 2609 TUCKER ST
PROJECT NO: NC ENGINEER LICENSE #F-0176 BURLINGTON, NORTH CAROLINA
1054-14-2086 3201 SPRING FOREST RD, RALEIGH, NC 27616

APPENDIX I
Photographic Log

010 Hahn Road (VP-2)
OR
003 Hahn Road (VP-3)
S&ME Soil Vapor Assessment and Water Supply Well Sampling Report S&ME Project No. 1054-14-2086
Tucker St, and Hahn Rd. Burlington, North Carolina Taken by: BW/CE/BB I Date Taken: April 8-10, 2014

ti
f J
r'
IN
6 Installing vapor point VP-4. This home has a basement.
+cr '
_ r
8 Installing vapor point VP-6.
S&ME Soil Vapor Assessment and Water Supply Well Sampling Report S&ME Project No. 1054-14-2086
Tucker St, and Hahn Rd. Burlington, North Carolina Taken by: BW/CE/BB I Date Taken: April 8-10, 2014
2

Hahn Road (VP-7).
11 Vapor point VP-7; duplication sample was collected here.
S&ME Soil Vapor Assessment and Water Supply Well Sampling Report S&ME Project No. 1054-14-2086
Tucker St, and Hahn Rd. Burlington, North Carolina Taken by: BW/CE/BB I Date Taken: April 8-10, 2014
3

939 i
13 I939 Hahn Road (VP-8).
15 Collecting sample at VP-4.
&ME I Soil Vapor Assessment and Water Supply Well Sampling Report I S&ME Project No. 1054-14-2086
Tucker St, and Hahn Rd. Burlington, North Carolina I Taken by: BW/CE/BB I Date Taken: April 8-10, 2014
4

APPENDIX II
Field Sampling Parameters

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APPENDIX III
Laboratory Analytical Report

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Ed Woloszyn / Candy Elliott
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
Report Summary
Wednesday April 16, 2014
Report Number: L693156
Samples Received: 04/11/14
Client Project: 1054-14-2086
Description: AMI, Inc. Site
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
II I
Entire Report Reviewed By: IIII
Tom Mellette , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 15

REPORT OF ANALYSIS
Ed Woloszyn / Candy Elliott
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
Date Received April 11, 2014
Description AMI, Inc. Site
Sample ID WSW-1
Collected By CE/BB
Collection Date 04/09/14 12:05
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 16,2014
ESC Sample # : L693156-01
Site ID :
Project # 1054-14-2086
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
3.2
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
04/14/14
50.
ug/l
8260B
04/14/14
10.
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
5.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
5.0
ug/1
8260B
04/14/14
50.
ug/l
8260B
04/14/14
5.0
ug/1
8260B
04/14/14
2.5
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
5.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
5.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
Page 2 of 15

Ed Woloszyn / Candy Elliott
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
Date Received
Description
Sample ID
Collected By
Collection Date
Parameter
April 11, 2014
AMI, Inc. Site
WSW-1
CE/BB
04/09/14 12:05
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 16,2014
ESC Sample # : L693156-01
Site ID :
Project # 1054-14-2086
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
04/14/14
Methylene Chloride
BDL
5.0
ug/1
8260B
04/14/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
04/14/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
04/14/14
Naphthalene
BDL
5.0
ug/1
8260B
04/14/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
04/14/14
Styrene
BDL
1.0
ug/1
8260B
04/14/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
04/14/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
04/14/14
Tetrachloroethene
32.
1.0
ug/l
8260B
04/14/14
Toluene
BDL
5.0
ug/1
8260B
04/14/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
04/14/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
04/14/14
1,1,1-Trichloroethane
BDL
1.0
ug/1
8260B
04/14/14
1,1,2-Trichloroethane
BDL
1.0
ug/l
8260B
04/14/14
Trichloroethene
30.
1.0
ug/1
8260B
04/14/14
Trichlorofluoromethane
BDL
5.0
ug/l
8260B
04/14/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
04/14/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/l
8260B
04/14/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
04/14/14
Vinyl chloride
BDL
1.0
ug/l
8260B
04/14/14
Xylenes, Total
BDL
3.0
ug/1
8260B
04/14/14
Surrogate Recovery
Toluene-d8
97.9
% Rec.
8260B
04/14/14
Dibromofluoromethane
115.
% Rec.
8260B
04/14/14
4-Bromofluorobenzene
98.5
% Rec.
8260B
04/14/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/16/14 08:26 Printed: 04/16/14 08:27
Page 3 of 15

REPORT OF ANALYSIS
Ed Woloszyn / Candy Elliott
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
Date Received April 11, 2014
Description AMI, Inc. Site
Sample ID DUP-2
Collected By CE/BB
Collection Date 04/09/14 00:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 16,2014
ESC Sample # : L693156-02
Site ID :
Project # 1054-14-2086
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
3.1
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
04/14/14
50.
ug/l
8260B
04/14/14
10.
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
5.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
5.0
ug/1
8260B
04/14/14
50.
ug/l
8260B
04/14/14
5.0
ug/1
8260B
04/14/14
2.5
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
5.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
5.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
1.0
ug/l
8260B
04/14/14
1.0
ug/1
8260B
04/14/14
Page 4 of 15

Ed Woloszyn / Candy Elliott
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
Date Received
Description
Sample ID
Collected By
Collection Date
Parameter
April 11, 2014
AMI, Inc. Site
DUP-2
CE/BB
04/09/14 00:00
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 16,2014
ESC Sample # : L693156-02
Site ID :
Project # 1054-14-2086
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
04/14/14
Methylene Chloride
BDL
5.0
ug/1
8260B
04/14/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
04/14/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
04/14/14
Naphthalene
BDL
5.0
ug/1
8260B
04/14/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
04/14/14
Styrene
BDL
1.0
ug/1
8260B
04/14/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
04/14/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
04/14/14
Tetrachloroethene
31.
1.0
ug/l
8260B
04/14/14
Toluene
BDL
5.0
ug/1
8260B
04/14/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
04/14/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
04/14/14
1,1,1-Trichloroethane
BDL
1.0
ug/1
8260B
04/14/14
1,1,2-Trichloroethane
BDL
1.0
ug/l
8260B
04/14/14
Trichloroethene
29.
1.0
ug/1
8260B
04/14/14
Trichlorofluoromethane
BDL
5.0
ug/l
8260B
04/14/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
04/14/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/l
8260B
04/14/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
04/14/14
Vinyl chloride
BDL
1.0
ug/l
8260B
04/14/14
Xylenes, Total
BDL
3.0
ug/1
8260B
04/14/14
Surrogate Recovery
Toluene-d8
96.8
% Rec.
8260B
04/14/14
Dibromofluoromethane
115.
% Rec.
8260B
04/14/14
4-Bromofluorobenzene
96.7
% Rec.
8260B
04/14/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/16/14 08:26 Printed: 04/16/14 08:27
Page 5 of 15

REPORT OF ANALYSIS
Ed Woloszyn / Candy Elliott
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
Date Received April 11, 2014
Description AMI, Inc. Site
Sample ID TRIP BLANK
Collected By CE/BB
Collection Date 04/09/14 00:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 16,2014
ESC Sample # : L693156-03
Site ID :
Project # 1054-14-2086
Parameter Result Det. Limit Units Method Date Dil.
Volatile Organics
Acetone
BDL
Acrolein
BDL
Acrylonitrile
BDL
Benzene
BDL
Bromobenzene
BDL
Bromodichloromethane
BDL
Bromoform
BDL
Bromomethane
BDL
n-Butylbenzene
BDL
sec-Butylbenzene
BDL
tert-Butylbenzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chlorodibromomethane
BDL
Chloroethane
BDL
2-Chloroethyl vinyl ether
BDL
Chloroform
BDL
Chloromethane
BDL
2-Chlorotoluene
BDL
4-Chlorotoluene
BDL
1,2-Dibromo-3-Chloropropane
BDL
1,2-Dibromoethane
BDL
Dibromomethane
BDL
1,2-Dichlorobenzene
BDL
1,3-Dichlorobenzene
BDL
1,4-Dichlorobenzene
BDL
Dichlorodifluoromethane
BDL
1,1-Dichloroethane
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
cis-1,2-Dichloroethene
BDL
trans-1,2-Dichloroethene
BDL
1,2-Dichloropropane
BDL
1,1-Dichloropropene
BDL
1,3-Dichloropropane
BDL
cis-1,3-Dichloropropene
BDL
trans-1,3-Dichloropropene
BDL
2,2-Dichloropropane
BDL
Di -isopropyl ether
BDL
Ethylbenzene
BDL
Hexachloro-1,3-butadiene
BDL
Isopropylbenzene
BDL
p-Isopropyltoluene
BDL
BDL - Below Detection Limit
Det. Limit - Practical Quantitation
Limit(PQL)
50.
ug/1
8260B
04/13/14
50.
ug/l
8260B
04/13/14
10.
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
5.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
5.0
ug/1
8260B
04/13/14
50.
ug/l
8260B
04/13/14
5.0
ug/1
8260B
04/13/14
2.5
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
5.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
5.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
1.0
ug/l
8260B
04/13/14
1.0
ug/1
8260B
04/13/14
Page 6 of 15

Ed Woloszyn / Candy Elliott
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
Date Received
Description
Sample ID
Collected By
Collection Date
Parameter
April 11, 2014
AMI, Inc. Site
TRIP BLANK
CE/BB
04/09/14 00:00
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 16,2014
ESC Sample # : L693156-03
Site ID :
Project # 1054-14-2086
Result Det. Limit Units Method Date Dil.
2-Butanone (MEK)
BDL
10.
ug/l
8260B
04/13/14
Methylene Chloride
BDL
5.0
ug/1
8260B
04/13/14
4-Methyl-2-pentanone (MIBK)
BDL
10.
ug/l
8260B
04/13/14
Methyl tert-butyl ether
BDL
1.0
ug/l
8260B
04/13/14
Naphthalene
BDL
5.0
ug/1
8260B
04/13/14
n-Propylbenzene
BDL
1.0
ug/l
8260B
04/13/14
Styrene
BDL
1.0
ug/1
8260B
04/13/14
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/l
8260B
04/13/14
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
8260B
04/13/14
Tetrachloroethene
BDL
1.0
ug/l
8260B
04/13/14
Toluene
BDL
5.0
ug/1
8260B
04/13/14
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
8260B
04/13/14
1,2,4-Trichlorobenzene
BDL
1.0
ug/1
8260B
04/13/14
1,1,1-Trichloroethane
BDL
1.0
ug/1
8260B
04/13/14
1,1,2-Trichloroethane
BDL
1.0
ug/l
8260B
04/13/14
Trichloroethene
BDL
1.0
ug/1
8260B
04/13/14
Trichlorofluoromethane
BDL
5.0
ug/l
8260B
04/13/14
1,2,3-Trichloropropane
BDL
2.5
ug/1
8260B
04/13/14
1,2,4-Trimethylbenzene
BDL
1.0
ug/l
8260B
04/13/14
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
8260B
04/13/14
Vinyl chloride
BDL
1.0
ug/l
8260B
04/13/14
Xylenes, Total
BDL
3.0
ug/1
8260B
04/13/14
Surrogate Recovery
Toluene-d8
99.0
% Rec.
8260B
04/13/14
Dibromofluoromethane
114.
% Rec.
8260B
04/13/14
4-Bromofluorobenzene
98.4
% Rec.
8260B
04/13/14
BDL - Below Detection Limit
Det. Limit - Practical Quantitation Limit(PQL)
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/16/14 08:26 Printed: 04/16/14 08:27
Page 7 of 15

Summary of Remarks For Samples Printed
04/16/14 at 08:27:06
TSR Signing Reports: 690
R5 - Desired TAT
Sample: L693156-01 Account: SMERLNC Received: 04/11/14 07:00 Due Date: 04/18/14 00:00 RPT Date: 04/16/14 08:26
Sample: L693156-02 Account: SMERLNC Received: 04/11/14 07:00 Due Date: 04/18/14 00:00 RPT Date: 04/16/14 08:26
Sample: L693156-03 Account: SMERLNC Received: 04/11/14 07:00 Due Date: 04/18/14 00:00 RPT Date: 04/16/14 08:26

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
S&ME Inc. - Raleigh NC
Ed Woloszyn / Candy Elliott
3201 Spring Forest Road
Quality Assurance Report
Level II
Raleigh, NC 27616
April 16, 2014
L693156
Laboratory Blank
Analyte
Result
Units % Rec Limit
Batch
Date Analyzed
1,1,1,2-Tetrachloroethane
<
.001
mg/l
WG715755
04/13/14
21:03
1,1,1-Trichloroethane
<
.001
mg/l
WG715755
04/13/14
21:03
1,1,2,2-Tetrachloroethane
<
.001
mg/l
WG715755
04/13/14
21:03
1,1,2-Trichloroethane
<
.001
mg/l
WG715755
04/13/14
21:03
1,1-Dichloroethane
<
.001
mg/l
WG715755
04/13/14
21:03
1,1-Dichloroethene
<
.001
mg/l
WG715755
04/13/14
21:03
1,1-Dichloropropene
<
.001
mg/l
WG715755
04/13/14
21:03
1,2,3-Trichlorobenzene
<
.001
mg/l
WG715755
04/13/14
21:03
1,2,3-Trichloropropane
<
.001
mg/1
WG715755
04/13/14
21:03
1,2,4-Trichlorobenzene
<
.001
mg/l
WG715755
04/13/14
21:03
1,2,4-Trimethylbenzene
<
.001
mg/l
WG715755
04/13/14
21:03
1,2-Dibromo-3-Chloropropane
<
.005
mg/l
WG715755
04/13/14
21:03
1,2-Dibromoethane
<
.001
mg/l
WG715755
04/13/14
21:03
1,2-Dichlorobenzene
<
.001
mg/l
WG715755
04/13/14
21:03
1,2-Dichloroethane
<
.001
mg/l
WG715755
04/13/14
21:03
1,2-Dichloropropane
<
.001
mg/l
WG715755
04/13/14
21:03
1,3,5-Trimethylbenzene
<
.001
mg/l
WG715755
04/13/14
21:03
1,3-Dichlorobenzene
<
.001
mg/l
WG715755
04/13/14
21:03
1,3-Dichloropropane
<
.001
mg/l
WG715755
04/13/14
21:03
1,4-Dichlorobenzene
<
.001
mg/1
WG715755
04/13/14
21:03
2,2-Dichloropropane
<
.001
mg/l
WG715755
04/13/14
21:03
2-Butanone (MEK)
<
.01
mg/l
WG715755
04/13/14
21:03
2-Chloroethyl vinyl ether
<
.05
mg/l
WG715755
04/13/14
21:03
2-Chlorotoluene
<
.001
mg/l
WG715755
04/13/14
21:03
4-Chlorotoluene
<
.001
mg/l
WG715755
04/13/14
21:03
4-Methyl-2-pentanone (MIBK)
<
.01
mg/l
WG715755
04/13/14
21:03
Acetone
<
.05
mg/l
WG715755
04/13/14
21:03
Acrolein
<
.025
mg/l
WG715755
04/13/14
21:03
Acrylonitrile
<
.01
mg/l
WG715755
04/13/14
21:03
Benzene
<
.001
mg/l
WG715755
04/13/14
21:03
Bromobenzene
<
.001
mg/l
WG715755
04/13/14
21:03
Bromodichloromethane
<
.001
mg/l
WG715755
04/13/14
21:03
Bromoform
<
.001
mg/l
WG715755
04/13/14
21:03
Bromomethane
<
.005
mg/l
WG715755
04/13/14
21:03
Carbon tetrachloride
<
.001
mg/l
WG715755
04/13/14
21:03
Chlorobenzene
<
.001
mg/l
WG715755
04/13/14
21:03
Chlorodibromomethane
<
.001
mg/l
WG715755
04/13/14
21:03
Chloroethane
<
.005
mg/l
WG715755
04/13/14
21:03
Chloroform
<
.005
mg/l
WG715755
04/13/14
21:03
Chloromethane
<
.0025
mg/l
WG715755
04/13/14
21:03
cis-1,2-Dichloroethene
<
.001
mg/l
WG713755
04/13/14
21:03
cis-1,3-Dichloropropene
<
.001
mg/l
WG715755
04/13/14
21:03
Di -isopropyl ether
<
.001
mg/l
WG715755
04/13/14
21:03
Dibromomethane
<
.001
mg/l
WG715755
04/13/14
21:03
Dichlorodifluoromethane
<
.005
mg/l
WG715755
04/13/14
21:03
Ethylbenzene
<
.001
mg/l
WG715755
04/13/14
21:03
Hexachloro-1,3-butadiene
<
.001
mg/l
WG715755
04/13/14
21:03
Isopropylbenzene
<
.001
mg/l
WG715755
04/13/14
21:03
Methyl tert-butyl ether
<
.001
mg/l
WG715755
04/13/14
21:03
Methylene Chloride
<
.005
mg/l
WG715755
04/13/14
21:03
n-Butylbenzene
<
.001
mg/l
WG715755
04/13/14
21:03
n-Propylbenzene
<
.001
mg/l
WG715755
04/13/14
21:03
Naphthalene
<
.005
mg/l
WG715755
04/13/14
21:03
p-Isopropyltoluene
<
.001
mg/l
WG715755
04/13/14
21:03
sec-Butylbenzene
<
.001
mg/l
WG715755
04/13/14
21:03
Styrene
<
.001
mg/l
WG715755
04/13/14
21:03
tert-Butylbenzene
<
.001
mg/l
WG715755
04/13/14
21:03
Tetrachloroethene
<
.001
mg/l
WG715755
04/13/14
21:03
Toluene
<
.005
mg/l
WG715755
04/13/14
21:03
* Performance of this Analyte
is outside of
established criteria.
For additional information,
please
see Attachment A 'List of Analytes with QC Qualifiers.'
Page 8 of 15

S&ME Inc. - Raleigh NC
Ed Woloszyn / Candy Elliott
3201 Spring Forest Road
Raleigh, NC 27616
Quality Assurance Report
Level II
L693156
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 16, 2014
Laboratory Blank
Analyte Result Units % Rec Limit Batch Date Analyzed
trans-1,2-Dichloroethene
<
.001
mg/1
WG715755
04/13/14
21:03
trans-1,3-Dichloropropene
<
.001
mg/1
WG715755
04/13/14
21:03
Trichloroethene
<
.001
mg/1
WG715755
04/13/14
21:03
Trichlorofluoromethane
<
.005
mg/1
WG715755
04/13/14
21:03
Vinyl chloride
<
.001
mg/1
WG715755
04/13/14
21:03
Xylenes, Total
<
.003
mg/1
WG715755
04/13/14
21:03
4-Bromofluorobenzene
% Rec. 102.0
71-126 WG715755
04/13/14
21:03
Dibromofluoromethane
% Rec. 114.0
78.3-121 WG715755
04/13/14
21:03
Toluene-d8
% Rec. 99.80
88.5-111 WG715755
04/13/14
21:03
Analyte
Units
Laboratory
Known Val
Control Sample
Result
% Rec
Limit
Batch
1,1,1,2-Tetrachloroethane
mg/1
.025
0.0233
93.4
74.2-124
WG715755
1,1,1-Trichloroethane
mg/1
.025
0.0225
90.2
73.2-123
WG715755
1,1,2,2-Tetrachloroethane
mg/1
.025
0.0239
95.6
70.7-122
WG715755
1,1,2-Trichloroethane
mg/1
.025
0.0235
94.2
77.7-118
WG715755
1,1-Dichloroethane
mg/1
.025
0.0239
95.4
70.7-126
WG715755
1,1-Dichloroethene
mg/1
.025
0.0239
95.5
67.8-129
WG715755
1,1-Dichloropropene
mg/1
.025
0.0215
86.1
73.1-125
WG715755
1,2,3-Trichlorobenzene
mg/1
.025
0.0258
103.
64.9-135
WG715755
1,2,3-Trichloropropane
mg/1
.025
0.0243
97.4
71.8-121
WG715755
1,2,4-Trichlorobenzene
mg/1
.025
0.0260
104.
69.7-136
WG715755
1,2,4-Trimethylbenzene
mg/1
.025
0.0220
87.9
75-123
WG715755
1,2-Dibromo-3-Chloropropane
mg/1
.025
0.0253
101.
65.4-128
WG715755
1,2-Dibromoethane
mg/1
.025
0.0236
94.2
76.6-121
WG715755
1,2-Dichlorobenzene
mg/1
.025
0.0247
98.8
78.4-117
WG715755
1,2-Dichloroethane
mg/1
.025
0.0250
100.
68.8-124
WG715755
1,2-Dichloropropane
mg/1
.025
0.0230
92.1
76.5-119
WG715755
1,3,5-Trimethylbenzene
mg/1
.025
0.0225
90.0
75.6-124
WG715755
1,3-Dichlorobenzene
mg/1
.025
0.0233
93.3
70.8-128
WG715755
1,3-Dichloropropane
mg/1
.025
0.0229
91.7
77.4-117
WG715755
1,4-Dichlorobenzene
mg/1
.025
0.0232
93.0
78.8-115
WG715755
2,2-Dichloropropane
mg/1
.025
0.0219
87.6
62.4-133
WG715755
2-Butanone (MEK)
mg/1
.125
0.114
91.3
55-149
WG715755
2-Chloroethyl vinyl ether
mg/1
.125
0.101
80.6
43.8-150
WG715755
2-Chlorotoluene
mg/1
.025
0.0218
87.3
74.7-122
WG715755
4-Chlorotoluene
mg/1
.025
0.0220
87.9
77.5-120
WG715755
4-Methyl-2-pentanone (MIBK)
mg/1
.125
0.119
95.1
70.5-133
WG715755
Acetone
mg/1
.125
0.128
103.
35.6-163
WG715755
Acrolein
mg/1
.125
0.103
82.7
10-190
WG715755
Acrylonitrile
mg/1
.125
0.135
108.
55.2-130
WG715755
Benzene
mg/1
.025
0.0223
89.3
74.8-121
WG715755
Bromobenzene
mg/1
.025
0.0226
90.4
77.5-116
WG715755
Bromodichloromethane
mg/1
.025
0.0235
94.0
75.1-116
WG715755
Bromoform
mg/1
.025
0.0235
94.1
67.5-130
WG715755
Bromomethane
mg/1
.025
0.0239
95.5
49.9-162
WG715755
Carbon tetrachloride
mg/1
.025
0.0210
84.1
70.2-123
WG715755
Chlorobenzene
mg/1
.025
0.0220
88.1
78.1-119
WG715755
Chlorodibromomethane
mg/1
.025
0.0232
92.9
74-121
WG715755
Chloroethane
mg/l
.025
0.0234
93.5
61.7-135
WG715755
Chloroform
mg/1
.025
0.0242
96.6
76-121
WG715755
Chloromethane
mg/1
.025
0.0197
78.8
61.5-129
WG715755
cis-1,2-Dichloroethene
mg/1
.025
0.0225
89.9
76-119
WG715755
cis-1,3-Dichloropropene
mg/1
.025
0.0228
91.2
78.2-120
WG715755
Di -isopropyl ether
mg/1
.025
0.0217
87.0
65.6-132
WG715755
Dibromomethane
mg/1
.025
0.0251
101.
79.5-118
WG715755
Dichlorodifluoromethane
mg/1
.025
0.0197
78.8
54.8-135
WG715755
Ethylbenzene
mg/1
.025
0.0208
83.3
78.8-122
WG715755
* Performance of this Analyte
is outside
of established
criteria.
For additional information,
please see
Attachment A 'List
of Analytes with
QC Qualifiers.'
Page 9 of 15

12065 Lebanon Rd.
Mt.
Juliet, TN 37122
(615)
758-5858
1-800-767-5859
Fax
[phone]
Tax
I.D. 62-0814289
Est.
1970
S&ME Inc. - Raleigh NC
Ed Woloszyn / Candy Elliott
3201 Spring Forest Road
Quality
Assurance
Report
Level
II
Raleigh, NC 27616
April 16,
2014
L693156
Laboratory Control Sample
Analyte
Units
Known
Val
Result
% Rec
Limit
Batch
Hexachloro-1,3-butadiene
mg/1
.025
0.0221
88.4
64.7-129
WG715755
Isopropylbenzene
mg/1
.025
0.0229
91.7
78.6-132
WG715755
Methyl tert-butyl ether
mg/l
.025
0.0271
108.
71.2-126
WG715755
Methylene Chloride
mg/1
.025
0.0243
97.1
70.3-120
WG715755
n-Butylbenzene
mg/1
.025
0.0229
91.7
76.2-126
WG715755
n-Propylbenzene
mg/1
.025
0.0213
85.1
78.2-122
WG715755
Naphthalene
mg/1
.025
0.0246
98.5
68.4-128
WG715755
p-Isopropyltoluene
mg/1
.025
0.0227
90.6
74-131
WG715755
sec-Butylbenzene
mg/1
.025
0.0217
86.9
74.4-127
WG715755
Styrene
mg/1
.025
0.0216
86.5
80.4-126
WG715755
tert-Butylbenzene
mg/1
.025
0.0219
87.7
75.3-126
WG715755
Tetrachloroethene
mg/1
.025
0.0213
85.2
72.6-126
WG715755
Toluene
mg/1
.025
0.0207
82.8
79.7-116
WG715755
trans-1,2-Dichloroethene
mg/1
.025
0.0209
83.7
72.6-121
WG715755
trans-1,3-Dichloropropene
mg/1
.025
0.0207
82.8
74.3-123
WG715755
Trichloroethene
mg/1
.025
0.0226
90.6
77.7-118
WG715755
Trichlorofluoromethane
mg/1
.025
0.0195
78.0
63.5-135
WG715755
Vinyl chloride
mg/1
.025
0.0217
86.7
65.9-128
WG715755
Xylenes, Total
mg/1
.075
0.0646
86.1
78.7-121
WG715755
4-Bromofluorobenzene
95.30
71-126
WG715755
Dibromofluoromethane
109.0
78.3-121
WG715755
Toluene-d8
97.70
88.5-111
WG715755
Laboratory
Control Sample
Duplicate
Analyte
Units
Result
Ref
%Rec
Limit
RPD
Limit
Batch
1,1,1,2-Tetrachloroethane
mg/1
0.0222
0.0233
89.0
74.2-124
4.99
20
WG715755
1,1,1-Trichloroethane
mg/1
0.0222
0.0225
89.0
73.2-123
1.31
20
WG715755
1,1,2,2-Tetrachloroethane
mg/1
0.0233
0.0239
93.0
70.7-122
2.74
20
WG715755
1,1,2-Trichloroethane
mg/1
0.0226
0.0235
90.0
77.7-118
4.29
20
WG715755
1,1-Dichloroethane
mg/1
0.0234
0.0239
94.0
70.7-126
1.94
20
WG715755
1,1-Dichloroethene
mg/1
0.0234
0.0239
94.0
67.8-129
1.96
20
WG715755
1,1-Dichloropropene
mg/1
0.0214
0.0215
86.0
73.1-125
0.490
20
WG715755
1,2,3-Trichlorobenzene
mg/1
0.0249
0.0258
100.
64.9-135
3.42
20
WG715755
1,2,3-Trichloropropane
mg/1
0.0230
0.0243
92.0
71.8-121
5.60
20
WG715755
1,2,4-Trichlorobenzene
mg/1
0.0251
0.0260
100.
69.7-136
3.74
20
WG715755
1,2,4-Trimethylbenzene
mg/1
0.0214
0.0220
86.0
75-123
2.63
20
WG715755
1,2-Dibromo-3-Chloropropane
mg/1
0.0248
0.0253
99.0
65.4-128
1.64
20
WG715755
1,2-Dibromoethane
mg/1
0.0229
0.0236
92.0
76.6-121
2.69
20
WG715755
1,2-Dichlorobenzene
mg/1
0.0243
0.0247
97.0
78.4-117
1.66
20
WG715755
1,2-Dichloroethane
mg/1
0.0248
0.0250
99.0
68.8-124
0.990
20
WG715755
1,2-Dichloropropane
mg/1
0.0223
0.0230
89.0
76.5-119
3.06
20
WG715755
1,3,5-Trimethylbenzene
mg/1
0.0218
0.0225
87.0
75.6-124
3.05
20
WG715755
1,3-Dichlorobenzene
mg/1
0.0225
0.0233
90.0
70.8-128
3.51
20
WG715755
1,3-Dichloropropane
mg/1
0.0221
0.0229
88.0
77.4-117
3.52
20
WG715755
1,4-Dichlorobenzene
mg/1
0.0229
0.0232
92.0
78.8-115
1.38
20
WG715755
2,2-Dichloropropane
mg/1
0.0227
0.0219
91.0
62.4-133
3.43
20
WG715755
2-Butanone (MEK)
mg/1
0.106
0.114
85.0
55-149
7.51
20
WG715755
2-Chloroethyl vinyl ether
mg/1
0.0989
0.101
79.0
43.8-150
1.81
20
WG715755
2-Chlorotoluene
mg/1
0.0209
0.0218
84.0
74.7-122
4.13
20
WG715755
4-Chlorotoluene
mg/l
0.0213
0.0220
85.0
77.5-120
3.08
20
WG715755
4-Methyl-2-pentanone (MIBK)
mg/1
0.116
0.119
92.0
70.5-133
2.74
20
WG715755
Acetone
mg/1
0.111
0.128
89.0
35.6-163
14.6
23.9
WG715755
Acrolein
mg/1
0.0934
0.103
75.0
10-190
10.2
28.1
WG715755
Acrylonitrile
mg/1
0.130
0.135
104.
55.2-130
4.01
20
WG715755
Benzene
mg/1
0.0215
0.0223
86.0
74.8-121
3.54
20
WG715755
Bromobenzene
mg/1
0.0221
0.0226
88.0
77.5-116
2.15
20
WG715755
Bromodichloromethane
mg/1
0.0226
0.0235
90.0
75.1-116
4.08
20
WG715755
Bromoform
mg/1
0.0230
0.0235
92.0
67.5-130
2.16
20
WG715755
* Performance of this Analyte
is outside
of established
criteria.
For additional information,
please see
Attachment
A 'List of
Analytes with
QC Qualifiers.'
Page 10 of 15

12065 Lebanon Rd.
Mt.
Juliet, TN 37122
(615)
758-5858
1-800-767-5859
Fax
[phone]
Tax
I.D. 62-0814289
Est.
1970
S&ME Inc. - Raleigh NC
Ed Woloszyn / Candy Elliott
3201 Spring Forest Road
Quality Assurance
Report
Level
II
Raleigh, NC 27616
April 16,
2014
L693156
Laboratory
Control Sample Duplicate
Analyte
Units
Result
Ref
oRec
Limit
RPD
Limit
Batch
Bromomethane
mg/1
0.0241
0.0239
96.0
49.9-162
1.06
20
WG715755
Carbon tetrachloride
mg/1
0.0209
0.0210
83.0
70.2-123
0.720
20
WG715755
Chlorobenzene
mg/l
0.0210
0.0220
84.0
78.1-119
4.97
20
WG715755
Chlorodibromomethane
mg/1
0.0223
0.0232
89.0
74-121
4.06
20
WG715755
Chloroethane
mg/1
0.0233
0.0234
93.0
61.7-135
0.240
20
WG715755
Chloroform
mg/1
0.0240
0.0242
96.0
76-121
0.690
20
WG715755
Chloromethane
mg/1
0.0193
0.0197
77.0
61.5-129
2.34
20
WG715755
cis-1,2-Dichloroethene
mg/1
0.0225
0.0225
90.0
76-119
0.120
20
WG715755
cis-1,3-Dichloropropene
mg/1
0.0221
0.0228
88.0
78.2-120
3.31
20
WG715755
Di -isopropyl ether
mg/1
0.0211
0.0217
84.0
65.6-132
3.03
20
WG715755
Dibromomethane
mg/1
0.0242
0.0251
97.0
79.5-118
3.56
20
WG715755
Dichlorodifluoromethane
mg/1
0.0193
0.0197
77.0
54.8-135
2.13
20
WG715755
Ethylbenzene
mg/1
0.0200
0.0208
80.0
78.8-122
4.17
20
WG715755
Hexachloro-1,3-butadiene
mg/1
0.0219
0.0221
87.0
64.7-129
1.04
20
WG715755
Isopropylbenzene
mg/1
0.0224
0.0229
89.0
78.6-132
2.42
20
WG715755
Methyl tert-butyl ether
mg/1
0.0265
0.0271
106.
71.2-126
2.18
20
WG715755
Methylene Chloride
mg/1
0.0242
0.0243
97.0
70.3-120
0.140
20
WG715755
n-Butylbenzene
mg/1
0.0221
0.0229
88.0
76.2-126
3.56
20
WG715755
n-Propylbenzene
mg/1
0.0209
0.0213
83.0
78.2-122
1.97
20
WG715755
Naphthalene
mg/1
0.0236
0.0246
94.0
68.4-128
4.45
20
WG715755
p-Isopropyltoluene
mg/1
0.0227
0.0227
91.0
74-131
0.190
20
WG715755
sec-Butylbenzene
mg/1
0.0213
0.0217
85.0
74.4-127
1.94
20
WG715755
Styrene
mg/1
0.0211
0.0216
84.0
80.4-126
2.39
20
WG715755
tert-Butylbenzene
mg/1
0.0216
0.0219
86.0
75.3-126
1.30
20
WG715755
Tetrachloroethene
mg/1
0.0205
0.0213
82.0
72.6-126
3.98
20
WG715755
Toluene
mg/1
0.0206
0.0207
82.0
79.7-116
0.700
20
WG715755
trans-1,2-Dichloroethene
mg/1
0.0209
0.0209
83.0
72.6-121
0.350
20
WG715755
trans-1,3-Dichloropropene
mg/1
0.0208
0.0207
83.0
74.3-123
0.590
20
WG715755
Trichloroethene
mg/1
0.0216
0.0226
86.0
77.7-118
4.70
20
WG715755
Trichlorofluoromethane
mg/1
0.0196
0.0195
78.0
63.5-135
0.490
20
WG715755
Vinyl chloride
mg/1
0.0209
0.0217
84.0
65.9-128
3.75
20
WG715755
Xylenes, Total
mg/1
0.0619
0.0646
82.0
78.7-121
4.31
20
WG715755
4-Bromofluorobenzene
95.20
71-126
WG715755
Dibromofluoromethane
112.0
78.3-121
WG715755
Toluene-d8
99.90
88.5-111
WG715755
Matrix Spike
Analyte
Units
MS Res
Ref Res
TV
% Rec
Limit
Ref Samp
Batch
1,1,1,2-Tetrachloroethane
mg/1
0.0240
0.0
.025
96.0
64-128
L693149-01
WG715755
1,1,1-Trichloroethane
mg/1
0.0230
0.0
.025
92.0
58.7-134
L693149-01
WG715755
1,1,2,2-Tetrachloroethane
mg/1
0.0237
0.0
.025
95.0
56-132
L693149-01
WG715755
1,1,2-Trichloroethane
mg/1
0.0236
0.0
.025
94.0
66.3-125
L693149-01
WG715755
1,1-Dichloroethane
mg/1
0.0240
0.0
.025
96.0
58.5-132
L693149-01
WG715755
1,1-Dichloroethene
mg/1
0.0246
0.0
.025
98.0
51.1-140
L693149-01
WG715755
1,1-Dichloropropene
mg/1
0.0224
0.0
.025
90.0
57.3-136
L693149-01
WG715755
1,2,3-Trichlorobenzene
mg/1
0.0267
0.0
.025
110.
59.1-138
L693149-01
WG715755
1,2,3-Trichloropropane
mg/1
0.0245
0.0
.025
98.0
61.4-128
L693149-01
WG715755
1,2,4-Trichlorobenzene
mg/1
0.0274
0.0
.025
110.
63.6-143
L693149-01
WG715755
1,2,4-Trimethylbenzene
mg/1
0.0231
0.0
.025
92.0
57.4-137
L693149-01
WG715755
1,2-Dibromo-3-Chloropropane
mg/1
0.0260
0.0
.025
100.
57.3-136
L693149-01
WG715755
1,2-Dibromoethane
mg/1
0.0237
0.0
.025
95.0
67.1-125
L693149-01
WG715755
1,2-Dichlorobenzene
mg/1
0.0251
0.0
.025
100.
68.2-123
L693149-01
WG715755
1,2-Dichloroethane
mg/1
0.0250
0.0
.025
100.
60-126
L693149-01
WG715755
1,2-Dichloropropane
mg/1
0.0229
0.0
.025
92.0
64.2-123
L693149-01
WG715755
1,3,5-Trimethylbenzene
mg/1
0.0242
0.0
.025
97.0
63.6-132
L693149-01
WG715755
1,3-Dichlorobenzene
mg/1
0.0246
0.0
.025
98.0
63.1-131
L693149-01
WG715755
1,3-Dichloropropane
mg/1
0.0231
0.0
.025
92.0
67.9-121
L693149-01
WG715755
1,4-Dichlorobenzene
mg/1
0.0238
0.0
.025
95.0
68.6-123
L693149-01
WG715755
* Performance of this Analyte
is outside
of established criteria.
For additional information,
please see
Attachment
A 'List of
Analytes
with QC
Qualifiers.'
Page 11 of 15

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
S&ME Inc. - Raleigh NC
Ed Woloszyn / Candy Elliott
3201 Spring Forest Road Quality Assurance Report
Level II
Raleigh, NC 27616 April 16, 2014
L693156
Analyte
Units
MS Res
Matrix Spike
Ref Res
TV
% Rec
Limit
Ref Samp
Batch
2,2-Dichloropropane
mg/l
0.0238
0.0
.025
95.0
50.5-144
L693149-01
WG715755
2-Butanone (MEK)
mg/l
0.109
0.0
.125
87.0
22.4-138
L693149-01
WG715755
2-Chloroethyl vinyl ether
mg/l
0.00160
0.0
.125
1.30*
10-155
L693149-01
WG715755
2-Chlorotoluene
mg/l
0.0226
0.0
.025
90.0
63.6-128
L693149-01
WG715755
4-Chlorotoluene
mg/l
0.0230
0.0
.025
92.0
65.7-127
L693149-01
WG715755
4-Methyl-2-pentanone (MIBK)
mg/l
0.118
0.0
.125
94.0
60.8-140
L693149-01
WG715755
Acetone
mg/l
0.119
0.00254
.125
93.0
10-130
L693149-01
WG715755
Acrolein
mg/l
0.136
0.0
.125
110.
10-200
L693149-01
WG715755
Acrylonitrile
mg/1
0.131
0.0
.125
100.
49.4-133
L693149-01
WG715755
Benzene
mg/l
0.0223
0.0
.025
89.0
54.3-133
L693149-01
WG715755
Bromobenzene
mg/l
0.0228
0.0
.025
91.0
63.9-124
L693149-01
WG715755
Bromodichloromethane
mg/l
0.0232
0.0
.025
93.0
63.9-121
L693149-01
WG715755
Bromoform
mg/l
0.0230
0.0
.025
92.0
59.5-134
L693149-01
WG715755
Bromomethane
mg/l
0.0232
0.0
.025
93.0
41.7-155
L693149-01
WG715755
Carbon tetrachloride
mg/l
0.0217
0.0
.025
87.0
55.7-134
L693149-01
WG715755
Chlorobenzene
mg/l
0.0224
0.0
.025
90.0
67-125
L693149-01
WG715755
Chlorodibromomethane
mg/l
0.0232
0.0
.025
93.0
64.3-125
L693149-01
WG715755
Chloroethane
mg/l
0.0241
0.0
.025
96.0
51.5-136
L693149-01
WG715755
Chloroform
mg/l
0.0244
0.0
.025
98.0
63-129
L693149-01
WG715755
Chloromethane
mg/1
0.0199
0.0
.025
80.0
42.4-135
L693149-01
WG715755
cis-1,2-Dichloroethene
mg/l
0.0228
0.0
.025
91.0
59.2-129
L693149-01
WG715755
cis-1,3-Dichloropropene
mg/l
0.0222
0.0
.025
89.0
66.4-125
L693149-01
WG715755
Di -isopropyl ether
mg/l
0.0216
0.0
.025
86.0
56.9-136
L693149-01
WG715755
Dibromomethane
mg/l
0.0246
0.0
.025
99.0
68.2-124
L693149-01
WG715755
Dichlorodifluoromethane
mg/l
0.0210
0.0
.025
84.0
40.6-144
L693149-01
WG715755
Ethylbenzene
mg/l
0.0220
0.0
.025
88.0
61.4-133
L693149-01
WG715755
Hexachloro-1,3-butadiene
mg/l
0.0239
0.0
.025
96.0
55.1-136
L693149-01
WG715755
Isopropylbenzene
mg/l
0.0249
0.0
.025
100.
66.8-141
L693149-01
WG715755
Methyl tert-butyl ether
mg/l
0.0269
0.0
.025
110.
57.7-134
L693149-01
WG715755
Methylene Chloride
mg/l
0.0243
0.0
.025
97.0
58.1-122
L693149-01
WG715755
n-Butylbenzene
mg/l
0.0242
0.0
.025
97.0
62.7-140
L693149-01
WG715755
n-Propylbenzene
mg/l
0.0226
0.0
.025
91.0
65.9-131
L693149-01
WG715755
Naphthalene
mg/l
0.0255
0.0
.025
100.
58-135
L693149-01
WG715755
p-Isopropyltoluene
mg/l
0.0248
0.0
.025
99.0
63.2-139
L693149-01
WG715755
sec-Butylbenzene
mg/l
0.0238
0.0
.025
95.0
62.2-136
L693149-01
WG715755
Styrene
mg/l
0.0220
0.0
.025
88.0
66.8-133
L693149-01
WG715755
tert-Butylbenzene
mg/l
0.0238
0.0
.025
95.0
63.3-134
L693149-01
WG715755
Tetrachloroethene
mg/l
0.0220
0.0
.025
88.0
53-139
L693149-01
WG715755
Toluene
mg/l
0.0215
0.0
.025
86.0
61.4-130
L693149-01
WG715755
trans-1,2-Dichloroethene
mg/l
0.0214
0.0
.025
85.0
56.5-129
L693149-01
WG715755
trans-1,3-Dichloropropene
mg/l
0.0208
0.0
.025
83.0
64.1-128
L693149-01
WG715755
Trichloroethene
mg/l
0.0228
0.0
.025
91.0
44.1-149
L693149-01
WG715755
Trichlorofluoromethane
mg/l
0.0214
0.0
.025
86.0
49.6-145
L693149-01
WG715755
Vinyl chloride
mg/l
0.0223
0.0
.025
89.0
47.8-137
L693149-01
WG715755
Xylenes, Total
mg/l
0.0668
0.0
.075
89.0
63.3-131
L693149-01
WG715755
4-Bromofluorobenzene
97.70
71-126
WG715755
Dibromofluoromethane
111.0
78.3-121
WG715755
Toluene-d8
99.00
88.5-111
WG715755
Matrix
Spike Duplicate
Analyte
Units
MSD
Ref %Rec
Limit
RPD Limit
Ref Samp
Batch
1,1,1,2-Tetrachloroethane
mg/l
0.0222
0.0240
88.9
64-128
7.85
20
L693149-01
WG715755
1,1,1-Trichloroethane
mg/l
0.0223
0.0230
89.3
58.7-134
3.01
20
L693149-01
WG715755
1,1,2,2-Tetrachloroethane
mg/l
0.0234
0.0237
93.7
56-132
1.12
22.2
L693149-01
WG715755
1,1,2-Trichloroethane
mg/l
0.0233
0.0236
93.1
66.3-125
1.47
20
L693149-01
WG715755
1,1-Dichloroethane
mg/l
0.0236
0.0240
94.4
58.5-132
1.49
20
L693149-01
WG715755
1,1-Dichloroethene
mg/l
0.0231
0.0246
92.4
51.1-140
6.26
20.2
L693149-01
WG715755
1,1-Dichloropropene
mg/l
0.0217
0.0224
86.7
57.3-136
3.18
20
L693149-01
WG715755
* Performance of this Analyte
is outside
of established
criteria.
For additional information,
please see
Attachment
A 'List
of Analytes
with QC
Qualifiers.'
Page 12 of 15

S&ME Inc. - Raleigh NC
Ed Woloszyn / Candy Elliott
3201 Spring Forest Road
Raleigh, NC 27616
Quality Assurance Report
Level II
L693156
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
April 16, 2014
Matrix Spike Duplicate
Analyte Units MSD Ref oRec Limit RPD Limit Ref Samp Batch
1,2,3-Trichlorobenzene
mg/1
0.0260
0.0267
104.
59.1-138
2.40
23.7
L693149-01
WG715755
1,2,3-Trichloropropane
mg/1
0.0233
0.0245
93.3
61.4-128
4.93
22.4
L693149-01
WG715755
1,2,4-Trichlorobenzene
mg/1
0.0265
0.0274
106.
63.6-143
3.49
21.9
L693149-01
WG715755
1,2,4-Trimethylbenzene
mg/1
0.0218
0.0231
87.3
57.4-137
5.53
20
L693149-01
WG715755
1,2-Dibromo-3-Chloropropane
mg/1
0.0253
0.0260
101.
57.3-136
3.03
27
L693149-01
WG715755
1,2-Dibromoethane
mg/1
0.0231
0.0237
92.4
67.1-125
2.72
20
L693149-01
WG715755
1,2-Dichlorobenzene
mg/1
0.0243
0.0251
97.4
68.2-123
2.92
20
L693149-01
WG715755
1,2-Dichloroethane
mg/1
0.0248
0.0250
99.2
60-126
0.980
20
L693149-01
WG715755
1,2-Dichloropropane
mg/1
0.0219
0.0229
87.8
64.2-123
4.17
20
L693149-01
WG715755
1,3,5-Trimethylbenzene
mg/1
0.0223
0.0242
89.4
63.6-132
7.81
20.5
L693149-01
WG715755
1,3-Dichlorobenzene
mg/1
0.0231
0.0246
92.4
63.1-131
6.38
20
L693149-01
WG715755
1,3-Dichloropropane
mg/1
0.0223
0.0231
89.3
67.9-121
3.39
20
L693149-01
WG715755
1,4-Dichlorobenzene
mg/1
0.0236
0.0238
94.3
68.6-123
1.05
20
L693149-01
WG715755
2,2-Dichloropropane
mg/1
0.0231
0.0238
92.4
50.5-144
2.85
21.9
L693149-01
WG715755
2-Butanone (MEK)
mg/1
0.111
0.109
89.0
22.4-138
1.74
27
L693149-01
WG715755
2-Chloroethyl vinyl ether
mg/1
0.0
0.00160
0*
10-155
200.*
20
L693149-01
WG715755
2-Chlorotoluene
mg/1
0.0218
0.0226
87.1
63.6-128
3.70
20
L693149-01
WG715755
4-Chlorotoluene
mg/1
0.0221
0.0230
88.5
65.7-127
4.04
20
L693149-01
WG715755
4-Methyl-2-pentanone (MIBK)
mg/1
0.118
0.118
94.5
60.8-140
0.0
25.1
L693149-01
WG715755
Acetone
mg/1
0.122
0.119
95.5
10-130
2.49
27.9
L693149-01
WG715755
Acrolein
mg/1
0.137
0.136
110.
10-200
0.960
27.7
L693149-01
WG715755
Acrylonitrile
mg/1
0.133
0.131
106.
49.4-133
0.990
25.3
L693149-01
WG715755
Benzene
mg/1
0.0215
0.0223
86.1
54.3-133
3.51
20
L693149-01
WG715755
Bromobenzene
mg/1
0.0218
0.0228
87.0
63.9-124
4.81
20
L693149-01
WG715755
Bromodichloromethane
mg/1
0.0225
0.0232
90.1
63.9-121
3.05
20
L693149-01
WG715755
Bromoform
mg/1
0.0231
0.0230
92.3
59.5-134
0.190
20.5
L693149-01
WG715755
Bromomethane
mg/1
0.0234
0.0232
93.5
41.7-155
0.600
21.9
L693149-01
WG715755
Carbon tetrachloride
mg/1
0.0208
0.0217
83.2
55.7-134
4.40
20
L693149-01
WG715755
Chlorobenzene
mg/1
0.0215
0.0224
86.0
67-125
4.21
20
L693149-01
WG715755
Chlorodibromomethane
mg/1
0.0225
0.0232
90.0
64.3-125
2.87
20.8
L693149-01
WG715755
Chloroethane
mg/1
0.0232
0.0241
92.6
51.5-136
4.04
40
L693149-01
WG715755
Chloroform
mg/1
0.0238
0.0244
95.1
63-129
2.80
20
L693149-01
WG715755
Chloromethane
mg/1
0.0191
0.0199
76.6
42.4-135
3.86
20
L693149-01
WG715755
cis-1,2-Dichloroethene
mg/1
0.0216
0.0228
86.6
59.2-129
5.38
20
L693149-01
WG715755
cis-1,3-Dichloropropene
mg/1
0.0216
0.0222
86.4
66.4-125
2.62
20
L693149-01
WG715755
Di -isopropyl ether
mg/1
0.0216
0.0216
86.5
56.9-136
0.290
20
L693149-01
WG715755
Dibromomethane
mg/1
0.0242
0.0246
97.0
68.2-124
1.63
20
L693149-01
WG715755
Dichlorodifluoromethane
mg/1
0.0191
0.0210
76.5
40.6-144
9.28
20.2
L693149-01
WG715755
Ethylbenzene
mg/1
0.0205
0.0220
82.2
61.4-133
6.87
20
L693149-01
WG715755
Hexachloro-1,3-butadiene
mg/1
0.0225
0.0239
90.1
55.1-136
5.98
23.6
L693149-01
WG715755
Isopropylbenzene
mg/1
0.0232
0.0249
92.9
66.8-141
7.08
20
L693149-01
WG715755
Methyl tert-butyl ether
mg/1
0.0271
0.0269
108.
57.7-134
0.730
20
L693149-01
WG715755
Methylene Chloride
mg/1
0.0242
0.0243
96.8
58.1-122
0.310
20
L693149-01
WG715755
n-Butylbenzene
mg/1
0.0228
0.0242
91.3
62.7-140
5.86
20.3
L693149-01
WG715755
n-Propylbenzene
mg/1
0.0209
0.0226
83.6
65.9-131
8.04
20
L693149-01
WG715755
Naphthalene
mg/1
0.0247
0.0255
98.9
58-135
3.27
25.5
L693149-01
WG715755
p-Isopropyltoluene
mg/1
0.0234
0.0248
93.6
63.2-139
5.78
20.4
L693149-01
WG715755
sec-Butylbenzene
mg/1
0.0223
0.0238
89.1
62.2-136
6.67
20.3
L693149-01
WG715755
Styrene
mg/1
0.0218
0.0220
87.3
66.8-133
0.670
20
L693149-01
WG715755
tert-Butylbenzene
mg/1
0.0222
0.0238
88.8
63.3-134
6.87
21
L693149-01
WG715755
Tetrachloroethene
mg/1
0.0205
0.0220
82.2
53-139
7.05
20
L693149-01
WG715755
Toluene
mg/1
0.0207
0.0215
83.0
61.4-130
3.82
20
L693149-01
WG715755
trans-1,2-Dichloroethene
mg/1
0.0210
0.0214
84.1
56.5-129
1.56
20
L693149-01
WG715755
trans-1,3-Dichloropropene
mg/1
0.0206
0.0208
82.3
64.1-128
1.29
20
L693149-01
WG715755
Trichloroethene
mg/1
0.0217
0.0228
87.0
44.1-149
4.51
20
L693149-01
WG715755
Trichlorofluoromethane
mg/1
0.0206
0.0214
82.4
49.6-145
3.99
21.2
L693149-01
WG715755
Vinyl chloride
mg/1
0.0206
0.0223
82.2
47.8-137
8.26
20
L693149-01
WG715755
Xylenes, Total
mg/1
0.0635
0.0668
84.7
63.3-131
4.95
20
L693149-01
WG715755
4-Bromofluorobenzene
96.80
71-126
WG715755
* Performance of this Analyte
is outside
of established
criteria.
For additional information,
please see
Attachment
A 'List
of Analytes
with QC
Qualifiers.'
Page 13 of 15

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
S&ME Inc. -
Raleigh NC
Ed Woloszyn
/ Candy Elliott
3201 Spring
Forest Road
Quality Assurance Report
Level II
Raleigh, NC
27616
April 16, 2014
L693156
Matrix Spike Duplicate
Analyte
Units MSD Ref oRec Limit RPD
Limit Ref Samp Batch
Dibromofluoromethane
111.0 78.3-121
Toluene-d8
100.0 88.5-111
Batch number /Run number / Sample number cross reference
WG715755: R2904911: L693156-01 02 03
* * Calculations are performed prior to rounding of reported values.
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 14 of 15

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
S&ME Inc. - Raleigh NC
Ed Woloszyn / Candy Elliott
3201 Spring Forest Road Quality Assurance Report
Level II
Raleigh, NC 27616
L693156
The data package includes a summary of the analytic results of the quality
control samples required by the SW-846 or CWA methods. The quality control
samples include a method blank, a laboratory control sample, and the matrix
spike/matrix spike duplicate analysis. If a target parameter is outside
the method limits, every sample that is effected is flagged with the
appropriate qualifier in Appendix B of the analytic report.
Method Blank - an aliquot of reagent water carried through the
entire analytic process. The method blank results indicate if
any possible contamination exposure during the sample handling,
digestion or extraction process, and analysis. Concentrations of
target analytes above the reporting limit in the method blank are
qualified with the "B" qualifier.
Laboratory Control Sample - is a sample of known concentration
that is carried through the digestion/extraction and analysis
process. The percent recovery, expressed as a percentage of the
theoretical concentration, has statistical control limits
indicating that the analytic process is "in control". If a
target analyte is outside the control limits for the laboratory
control sample or any other control sample, the parameter is
flagged with a "J4" qualifier for all effected samples.
Matrix Spike and Matrix Spike Duplicate - is two aliquots of an
environmental sample that is spiked with known concentrations of
target analytes. The percent recovery of the target analytes
also has statistical control limits. If any recoveries that are
outside the method control limits, the sample that was selected
for matrix spike/matrix spike duplicate analysis is flagged with
either a "J5" or a "J6". The relative percent difference (%RPD)
between the matrix spike and the matrix spike duplicate
recoveries is all calculated. If the RPD is above the method
limit, the effected samples are flagged with a "J3" qualifier.
Page 15 of 15
April 16, 2014

Company Namei,rWdreSc.
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12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
Ed Eoloszyn/Candy Elliott
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
Report Summary
Friday April 18, 2014
Report Number: L693331
Samples Received: 04/11/14
Client Project: 1054-14-2086
Description: AMI, Inc Site
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
II I
Entire Report Reviewed By: IIII
Tom Mellette , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 14

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
1-800-767-5859
Fax (615)
758-5859
Tax I.D. 62-0814289
Est. 1970
REPORT
OF
ANALYSIS
Ed Eoloszyn/Candy Elliott
April
18, 2014
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample
#
L693331-01
Date Received April
11, 2014
Description AMI, Inc
Site
Site
ID
Sample ID VP-1 2523
TUCKER ST.
Project
#
1054-14-2086
Collected By Candy E.
Elliott
Collection Date 04/09/14
08:43
Parameter
Cas#
Mol Wght
RDL1
RDL2
ppbv
ug/m3
Method
Date
Dil.
Volatile Organics - TO-15 SIM
Benzene
71-43-2
78.1
0.080
0.26
2.3
7.3
TO-15
04/16/14
4
Carbon tetrachloride
56-23-5
154
0.020
0.13
0.068
0.43
TO-15
04/16/14
1
Chloroethane
75-00-3
64.5
0.040
0.11
<
0.040
< 0.11
TO-15
04/16/14
1
Chloroform
67-66-3
119
0.020
0.097
0.35
1.7
TO-15
04/16/14
1
Chloromethane
74-87-3
50.5
0.030
0.062
1.6
3.3
TO-15
04/16/14
1
1,2-Dibromoethane
106-93-4
188
0.020
0.15
<
0.020
< 0.15
TO-15
04/16/14
1
1,4-Dichlorobenzene
106-46-7
147
0.020
0.12
<
0.020
< 0.12
TO-15
04/16/14
1
1,1-Dichloroethane
75-34-3
98
0.020
0.080
<
0.020
< 0.080
TO-15
04/16/14
1
1,1-Dichloroethene
75-35-4
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
cis-1,2-Dichloroethene
156-59-2
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
trans-1,2-Dichloroethene
156-60-5
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
1,2-Dichloropropane
78-87-5
113
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
cis-1,3-Dichloropropene
10061-01-5
111
0.020
0.091
<
0.020
< 0.091
TO-15
04/16/14
1
trans-1,3-Dichloropropene
10061-02-6
111
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
Ethylbenzene
100-41-4
106
0.030
0.13
0.75
3.3
TO-15
04/16/14
1
1,1,2,2-Tetrachloroethane
79-34-5
168
0.020
0.14
<
0.020
< 0.14
TO-15
04/16/14
1
Tetrachloroethylene
127-18-4
166
0.020
0.14
0.049
0.33
TO-15
04/16/14
1
1,1,1-Trichloroethane
71-55-6
133
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
1,1,2-Trichloroethane
79-00-5
133
0.030
0.16
<
0.030
< 0.16
TO-15
04/16/14
1
Trichloroethylene
79-01-6
131
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
Vinyl chloride
75-01-4
62.5
0.020
0.051
<
0.020
< 0.051
TO-15
04/16/14
1
Vinyl acetate
108-05-4
86.1
0.020
0.070
<
0.020
< 0.070
TO-15
04/16/14
1
1,4-Bromofluorobenzene
460-00-4
93.2
o Rec.
TO-15
04/16/14
1
RDL1 = ppbv , RDL2 = ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/18/14 11:17 Printed: 04/18/14 11:18
Page 2 of 14

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Ed Eoloszyn/Candy Elliott April 18, 2014
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample # L693331-02
Date Received April 11, 2014
Description AMI, Inc Site
Site ID
Sample ID VP-2 1010 HAHN RD.
Project # 1054-14-2086
Collected By Candy E. Elliott
Collection Date 04/09/14 09:20
Parameter Cas# Mol Wght RDL1 RDL2 ppbv ug/m3 Method Date Dil.
Volatile Organics - TO-15 SIM
Benzene
71-43-2
78.1
0.020
0.064
0.15
0.48
TO-15
04/16/14
1
Carbon tetrachloride
56-23-5
154
0.020
0.13
0.072
0.45
TO-15
04/16/14
1
Chloroethane
75-00-3
64.5
0.040
0.11
<
0.040
< 0.11
TO-15
04/16/14
1
Chloroform
67-66-3
119
0.020
0.097
0.021
0.10
TO-15
04/16/14
1
Chloromethane
74-87-3
50.5
0.030
0.062
0.52
1.1
TO-15
04/16/14
1
1,2-Dibromoethane
106-93-4
188
0.020
0.15
<
0.020
< 0.15
TO-15
04/16/14
1
1,4-Dichlorobenzene
106-46-7
147
0.020
0.12
<
0.020
< 0.12
TO-15
04/16/14
1
1,1-Dichloroethane
75-34-3
98
0.020
0.080
<
0.020
< 0.080
TO-15
04/16/14
1
1,1-Dichloroethene
75-35-4
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
cis-1,2-Dichloroethene
156-59-2
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
trans-1,2-Dichloroethene
156-60-5
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
1,2-Dichloropropane
78-87-5
113
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
cis-1,3-Dichloropropene
10061-01-5
111
0.020
0.091
<
0.020
< 0.091
TO-15
04/16/14
1
trans-1,3-Dichloropropene
10061-02-6
111
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
Ethylbenzene
100-41-4
106
0.030
0.13
0.038
0.16
TO-15
04/16/14
1
1,1,2,2-Tetrachloroethane
79-34-5
168
0.020
0.14
<
0.020
< 0.14
TO-15
04/16/14
1
Tetrachloroethylene
127-18-4
166
0.020
0.14
<
0.020
< 0.14
TO-15
04/16/14
1
1,1,1-Trichloroethane
71-55-6
133
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
1,1,2-Trichloroethane
79-00-5
133
0.030
0.16
<
0.030
< 0.16
TO-15
04/16/14
1
Trichloroethylene
79-01-6
131
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
Vinyl chloride
75-01-4
62.5
0.020
0.051
<
0.020
< 0.051
TO-15
04/16/14
1
Vinyl acetate
108-05-4
86.1
0.020
0.070
<
0.020
< 0.070
TO-15
04/16/14
1
1,4-Bromofluorobenzene
460-00-4
92.7
o Rec.
TO-15
04/16/14
1
RDL1 = ppbv , RDL2 = ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/18/14 11:17 Printed: 04/18/14 11:18
Page 3 of 14

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
1-800-767-5859
Fax (615)
758-5859
Tax I.D. 62-0814289
Est. 1970
REPORT
OF
ANALYSIS
Ed Eoloszyn/Candy Elliott
April
18, 2014
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample
#
L693331-03
Date Received April 11,
2014
Description AMI, Inc Site
Site
ID
Sample ID VP-3 1003 HAHN
RD
Project
#
1054-14-2086
Collected By Candy E. Elliott
Collection Date 04/09/14 09:44
Parameter
Cas#
Mol Wght
RDL1
RDL2
ppbv
ug/m3
Method
Date
Dil.
Volatile Organics - TO-15 SIM
Benzene
71-43-2
78.1
0.080
0.26
2.4
7.7
TO-15
04/16/14
4
Carbon tetrachloride
56-23-5
154
0.020
0.13
0.053
0.33
TO-15
04/16/14
1
Chloroethane
75-00-3
64.5
0.040
0.11
<
0.040
< 0.11
TO-15
04/16/14
1
Chloroform
67-66-3
119
0.020
0.097
<
0.020
< 0.097
TO-15
04/16/14
1
Chloromethane
74-87-3
50.5
0.030
0.062
<
0.030
< 0.062
TO-15
04/16/14
1
1,2-Dibromoethane
106-93-4
188
0.020
0.15
<
0.020
< 0.15
TO-15
04/16/14
1
1,4-Dichlorobenzene
106-46-7
147
0.020
0.12
<
0.020
< 0.12
TO-15
04/16/14
1
1,1-Dichloroethane
75-34-3
98
0.020
0.080
<
0.020
< 0.080
TO-15
04/16/14
1
1,1-Dichloroethene
75-35-4
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
cis-1,2-Dichloroethene
156-59-2
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
trans-1,2-Dichloroethene
156-60-5
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
1,2-Dichloropropane
78-87-5
113
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
cis-1,3-Dichloropropene
10061-01-5
111
0.020
0.091
<
0.020
< 0.091
TO-15
04/16/14
1
trans-1,3-Dichloropropene
10061-02-6
111
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
Ethylbenzene
100-41-4
106
0.030
0.13
0.58
2.5
TO-15
04/16/14
1
1,1,2,2-Tetrachloroethane
79-34-5
168
0.020
0.14
<
0.020
< 0.14
TO-15
04/16/14
1
Tetrachloroethylene
127-18-4
166
0.020
0.14
0.12
0.81
TO-15
04/16/14
1
1,1,1-Trichloroethane
71-55-6
133
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
1,1,2-Trichloroethane
79-00-5
133
0.030
0.16
<
0.030
< 0.16
TO-15
04/16/14
1
Trichloroethylene
79-01-6
131
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
Vinyl chloride
75-01-4
62.5
0.020
0.051
<
0.020
< 0.051
TO-15
04/16/14
1
Vinyl acetate
108-05-4
86.1
0.020
0.070
<
0.020
< 0.070
TO-15
04/16/14
1
1,4-Bromofluorobenzene
460-00-4
92.3
o Rec.
TO-15
04/16/14
1
RDL1 = ppbv , RDL2 = ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/18/14 11:17 Printed: 04/18/14 11:18
Page 4 of 14

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Ed Eoloszyn/Candy Elliott April 18, 2014
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample # L693331-04
Date Received April 11, 2014
Description AMI, Inc Site
Site ID
Sample ID VP-4 1006 HAHN RD
Project # 1054-14-2086
Collected By Candy E. Elliott
Collection Date 04/09/14 09:34
Parameter Cas# Mol Wght RDL1 RDL2 ppbv ug/m3 Method Date Dil.
Volatile Organics - TO-15 SIM
Benzene
71-43-2
78.1
0.080
0.26
3.0
9.6
TO-15
04/16/14
4
Carbon tetrachloride
56-23-5
154
0.020
0.13
<
0.020
< 0.13
TO-15
04/16/14
1
Chloroethane
75-00-3
64.5
0.040
0.11
<
0.040
< 0.11
TO-15
04/16/14
1
Chloroform
67-66-3
119
0.020
0.097
0.86
4.2
TO-15
04/16/14
1
Chloromethane
74-87-3
50.5
0.030
0.062
1.6
3.3
TO-15
04/16/14
1
1,2-Dibromoethane
106-93-4
188
0.020
0.15
<
0.020
< 0.15
TO-15
04/16/14
1
1,4-Dichlorobenzene
106-46-7
147
0.020
0.12
<
0.020
< 0.12
TO-15
04/16/14
1
1,1-Dichloroethane
75-34-3
98
0.020
0.080
<
0.020
< 0.080
TO-15
04/16/14
1
1,1-Dichloroethene
75-35-4
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
cis-1,2-Dichloroethene
156-59-2
96.9
0.020
0.079
0.18
0.71
TO-15
04/16/14
1
trans-1,2-Dichloroethene
156-60-5
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
1,2-Dichloropropane
78-87-5
113
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
cis-1,3-Dichloropropene
10061-01-5
111
0.020
0.091
<
0.020
< 0.091
TO-15
04/16/14
1
trans-1,3-Dichloropropene
10061-02-6
111
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
Ethylbenzene
100-41-4
106
0.030
0.13
0.34
1.5
TO-15
04/16/14
1
1,1,2,2-Tetrachloroethane
79-34-5
168
0.020
0.14
<
0.020
< 0.14
TO-15
04/16/14
1
Tetrachloroethylene
127-18-4
166
4.0
27.
360
2400
TO-15
04/17/14
200
1,1,1-Trichloroethane
71-55-6
133
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
1,1,2-Trichloroethane
79-00-5
133
0.030
0.16
<
0.030
< 0.16
TO-15
04/16/14
1
Trichloroethylene
79-01-6
131
4.0
21.
72.
390
TO-15
04/17/14
200
Vinyl chloride
75-01-4
62.5
0.020
0.051
<
0.020
< 0.051
TO-15
04/16/14
1
Vinyl acetate
108-05-4
86.1
0.020
0.070
<
0.020
< 0.070
TO-15
04/16/14
1
1,4-Bromofluorobenzene
460-00-4
107
o Rec.
TO-15
04/16/14
1
RDL1 = ppbv , RDL2 = ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/18/14 11:17 Printed: 04/18/14 11:18
Page 5 of 14

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
1-800-767-5859
Fax (615)
758-5859
Tax I.D. 62-0814289
Est. 1970
REPORT
OF
ANALYSIS
Ed Eoloszyn/Candy Elliott
April
18, 2014
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample
#
L693331-05
Date Received April
11,
2014
Description AMI, Inc
Site
Site
ID
Sample ID VP-5 963
HAHN
RD
Project
#
1054-14-2086
Collected By Candy E.
Elliott
Collection Date 04/09/14
10:00
Parameter
Cas#
Mol Wght
RDL1
RDL2
ppbv
ug/m3
Method
Date
Dil.
Volatile Organics - TO-15 SIM
Benzene
71-43-2
78.1
0.080
0.26
3.0
9.6
TO-15
04/17/14
4
Carbon tetrachloride
56-23-5
154
0.020
0.13
0.063
0.40
TO-15
04/17/14
1
Chloroethane
75-00-3
64.5
0.040
0.11
<
0.040
< 0.11
TO-15
04/17/14
1
Chloroform
67-66-3
119
0.020
0.097
<
0.020
< 0.097
TO-15
04/17/14
1
Chloromethane
74-87-3
50.5
0.12
0.25
2.4
5.0
TO-15
04/17/14
4
1,2-Dibromoethane
106-93-4
188
0.020
0.15
<
0.020
< 0.15
TO-15
04/17/14
1
1,4-Dichlorobenzene
106-46-7
147
0.020
0.12
<
0.020
< 0.12
TO-15
04/17/14
1
1,1-Dichloroethane
75-34-3
98
0.020
0.080
<
0.020
< 0.080
TO-15
04/17/14
1
1,1-Dichloroethene
75-35-4
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
cis-1,2-Dichloroethene
156-59-2
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
trans-1,2-Dichloroethene
156-60-5
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
1,2-Dichloropropane
78-87-5
113
0.030
0.14
<
0.030
< 0.14
TO-15
04/17/14
1
cis-1,3-Dichloropropene
10061-01-5
111
0.020
0.091
<
0.020
< 0.091
TO-15
04/17/14
1
trans-1,3-Dichloropropene
10061-02-6
111
0.030
0.14
<
0.030
< 0.14
TO-15
04/17/14
1
Ethylbenzene
100-41-4
106
0.030
0.13
0.74
3.2
TO-15
04/17/14
1
1,1,2,2-Tetrachloroethane
79-34-5
168
0.020
0.14
<
0.020
< 0.14
TO-15
04/17/14
1
Tetrachloroethylene
127-18-4
166
0.020
0.14
0.12
0.81
TO-15
04/17/14
1
1,1,1-Trichloroethane
71-55-6
133
0.020
0.11
<
0.020
< 0.11
TO-15
04/17/14
1
1,1,2-Trichloroethane
79-00-5
133
0.030
0.16
<
0.030
< 0.16
TO-15
04/17/14
1
Trichloroethylene
79-01-6
131
0.020
0.11
<
0.020
< 0.11
TO-15
04/17/14
1
Vinyl chloride
75-01-4
62.5
0.020
0.051
<
0.020
< 0.051
TO-15
04/17/14
1
Vinyl acetate
108-05-4
86.1
0.020
0.070
<
0.020
< 0.070
TO-15
04/17/14
1
1,4-Bromofluorobenzene
460-00-4
88.3
o Rec.
TO-15
04/17/14
1
RDL1 = ppbv , RDL2 = ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/18/14 11:17 Printed: 04/18/14 11:18
Page 6 of 14

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
1-800-767-5859
Fax (615)
758-5859
Tax I.D. 62-0814289
Est. 1970
REPORT
OF
ANALYSIS
Ed Eoloszyn/Candy Elliott
April
18, 2014
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample
#
L693331-06
Date Received April
11,
2014
Description AMI, Inc
Site
Site
ID
Sample ID VP-6 960
HAHN
RD
Project
#
1054-14-2086
Collected By Candy E.
Elliott
Collection Date 04/09/14
10:11
Parameter
Cas#
Mol Wght
RDL1
RDL2
ppbv
ug/m3
Method
Date
Dil.
Volatile Organics - TO-15 SIM
Benzene
71-43-2
78.1
0.10
0.32
3.2
10.
TO-15
04/17/14
5
Carbon tetrachloride
56-23-5
154
0.020
0.13
0.059
0.37
TO-15
04/17/14
1
Chloroethane
75-00-3
64.5
0.040
0.11
<
0.040
< 0.11
TO-15
04/17/14
1
Chloroform
67-66-3
119
0.020
0.097
<
0.020
< 0.097
TO-15
04/17/14
1
Chloromethane
74-87-3
50.5
0.030
0.062
1.8
3.7
TO-15
04/17/14
1
1,2-Dibromoethane
106-93-4
188
0.020
0.15
<
0.020
< 0.15
TO-15
04/17/14
1
1,4-Dichlorobenzene
106-46-7
147
0.020
0.12
<
0.020
< 0.12
TO-15
04/17/14
1
1,1-Dichloroethane
75-34-3
98
0.020
0.080
<
0.020
< 0.080
TO-15
04/17/14
1
1,1-Dichloroethene
75-35-4
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
cis-1,2-Dichloroethene
156-59-2
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
trans-1,2-Dichloroethene
156-60-5
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
1,2-Dichloropropane
78-87-5
113
0.030
0.14
<
0.030
< 0.14
TO-15
04/17/14
1
cis-1,3-Dichloropropene
10061-01-5
111
0.020
0.091
<
0.020
< 0.091
TO-15
04/17/14
1
trans-1,3-Dichloropropene
10061-02-6
111
0.030
0.14
<
0.030
< 0.14
TO-15
04/17/14
1
Ethylbenzene
100-41-4
106
0.030
0.13
0.67
2.9
TO-15
04/17/14
1
1,1,2,2-Tetrachloroethane
79-34-5
168
0.020
0.14
<
0.020
< 0.14
TO-15
04/17/14
1
Tetrachloroethylene
127-18-4
166
0.020
0.14
0.045
0.31
TO-15
04/17/14
1
1,1,1-Trichloroethane
71-55-6
133
0.020
0.11
<
0.020
< 0.11
TO-15
04/17/14
1
1,1,2-Trichloroethane
79-00-5
133
0.030
0.16
<
0.030
< 0.16
TO-15
04/17/14
1
Trichloroethylene
79-01-6
131
0.020
0.11
<
0.020
< 0.11
TO-15
04/17/14
1
Vinyl chloride
75-01-4
62.5
0.020
0.051
<
0.020
< 0.051
TO-15
04/17/14
1
Vinyl acetate
108-05-4
86.1
0.020
0.070
<
0.020
< 0.070
TO-15
04/17/14
1
1,4-Bromofluorobenzene
460-00-4
92.4
o Rec.
TO-15
04/17/14
1
RDL1 = ppbv , RDL2 = ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/18/14 11:17 Printed: 04/18/14 11:18
Page 7 of 14

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Ed Eoloszyn/Candy Elliott April 18, 2014
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample # L693331-07
Date Received April 11, 2014
Description AMI, Inc Site
Site ID
Sample ID VP-7 952 HAHN ROAD
Project # 1054-14-2086
Collected By Candy E. Elliott
Collection Date 04/09/14 10:20
Parameter Cas# Mol Wght RDL1 RDL2 ppbv ug/m3 Method Date Dil.
Volatile Organics - TO-15 SIM
Benzene
71-43-2
78.1
0.020
0.064
1.4
4.5
TO-15
04/17/14
1
Carbon tetrachloride
56-23-5
154
0.020
0.13
0.032
0.20
TO-15
04/17/14
1
Chloroethane
75-00-3
64.5
0.040
0.11
<
0.040
< 0.11
TO-15
04/17/14
1
Chloroform
67-66-3
119
0.020
0.097
<
0.020
< 0.097
TO-15
04/17/14
1
Chloromethane
74-87-3
50.5
0.030
0.062
0.97
2.0
TO-15
04/17/14
1
1,2-Dibromoethane
106-93-4
188
0.020
0.15
<
0.020
< 0.15
TO-15
04/17/14
1
1,4-Dichlorobenzene
106-46-7
147
0.020
0.12
<
0.020
< 0.12
TO-15
04/17/14
1
1,1-Dichloroethane
75-34-3
98
0.020
0.080
<
0.020
< 0.080
TO-15
04/17/14
1
1,1-Dichloroethene
75-35-4
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
cis-1,2-Dichloroethene
156-59-2
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
trans-1,2-Dichloroethene
156-60-5
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
1,2-Dichloropropane
78-87-5
113
0.030
0.14
<
0.030
< 0.14
TO-15
04/17/14
1
cis-1,3-Dichloropropene
10061-01-5
111
0.020
0.091
<
0.020
< 0.091
TO-15
04/17/14
1
trans-1,3-Dichloropropene
10061-02-6
111
0.030
0.14
<
0.030
< 0.14
TO-15
04/17/14
1
Ethylbenzene
100-41-4
106
0.030
0.13
0.27
1.2
TO-15
04/17/14
1
1,1,2,2-Tetrachloroethane
79-34-5
168
0.020
0.14
<
0.020
< 0.14
TO-15
04/17/14
1
Tetrachloroethylene
127-18-4
166
0.020
0.14
0.020
0.14
TO-15
04/17/14
1
1,1,1-Trichloroethane
71-55-6
133
0.020
0.11
<
0.020
< 0.11
TO-15
04/17/14
1
1,1,2-Trichloroethane
79-00-5
133
0.030
0.16
<
0.030
< 0.16
TO-15
04/17/14
1
Trichloroethylene
79-01-6
131
0.020
0.11
<
0.020
< 0.11
TO-15
04/17/14
1
Vinyl chloride
75-01-4
62.5
0.020
0.051
<
0.020
< 0.051
TO-15
04/17/14
1
Vinyl acetate
108-05-4
86.1
0.020
0.070
<
0.020
< 0.070
TO-15
04/17/14
1
1,4-Bromofluorobenzene
460-00-4
90
o Rec.
TO-15
04/17/14
1
RDL1 = ppbv , RDL2 = ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/18/14 11:17 Printed: 04/18/14 11:18
Page 8 of 14

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
1-800-767-5859
Fax (615)
758-5859
Tax I.D. 62-0814289
Est. 1970
REPORT
OF
ANALYSIS
Ed Eoloszyn/Candy Elliott
April
18, 2014
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample
#
L693331-08
Date Received April
11,
2014
Description AMI, Inc
Site
Site
ID
Sample ID VP-8 939
HAHN
ROAD
Project
#
1054-14-2086
Collected By Candy E.
Elliott
Collection Date 04/09/14
10:54
Parameter
Cas#
Mol Wght
RDL1
RDL2
ppbv
ug/m3
Method
Date
Dil.
Volatile Organics - TO-15 SIM
Benzene
71-43-2
78.1
0.020
0.064
1.8
5.7
TO-15
04/17/14
1
Carbon tetrachloride
56-23-5
154
0.020
0.13
0.055
0.35
TO-15
04/17/14
1
Chloroethane
75-00-3
64.5
0.040
0.11
<
0.040
< 0.11
TO-15
04/17/14
1
Chloroform
67-66-3
119
0.020
0.097
<
0.020
< 0.097
TO-15
04/17/14
1
Chloromethane
74-87-3
50.5
0.12
0.25
2.6
5.4
TO-15
04/17/14
4
1,2-Dibromoethane
106-93-4
188
0.020
0.15
<
0.020
< 0.15
TO-15
04/17/14
1
1,4-Dichlorobenzene
106-46-7
147
0.020
0.12
<
0.020
< 0.12
TO-15
04/17/14
1
1,1-Dichloroethane
75-34-3
98
0.020
0.080
<
0.020
< 0.080
TO-15
04/17/14
1
1,1-Dichloroethene
75-35-4
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
cis-1,2-Dichloroethene
156-59-2
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
trans-1,2-Dichloroethene
156-60-5
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/17/14
1
1,2-Dichloropropane
78-87-5
113
0.030
0.14
<
0.030
< 0.14
TO-15
04/17/14
1
cis-1,3-Dichloropropene
10061-01-5
111
0.020
0.091
<
0.020
< 0.091
TO-15
04/17/14
1
trans-1,3-Dichloropropene
10061-02-6
111
0.030
0.14
<
0.030
< 0.14
TO-15
04/17/14
1
Ethylbenzene
100-41-4
106
0.030
0.13
0.44
1.9
TO-15
04/17/14
1
1,1,2,2-Tetrachloroethane
79-34-5
168
0.020
0.14
<
0.020
< 0.14
TO-15
04/17/14
1
Tetrachloroethylene
127-18-4
166
0.020
0.14
0.027
0.18
TO-15
04/17/14
1
1,1,1-Trichloroethane
71-55-6
133
0.020
0.11
<
0.020
< 0.11
TO-15
04/17/14
1
1,1,2-Trichloroethane
79-00-5
133
0.030
0.16
<
0.030
< 0.16
TO-15
04/17/14
1
Trichloroethylene
79-01-6
131
0.020
0.11
<
0.020
< 0.11
TO-15
04/17/14
1
Vinyl chloride
75-01-4
62.5
0.020
0.051
<
0.020
< 0.051
TO-15
04/17/14
1
Vinyl acetate
108-05-4
86.1
0.020
0.070
<
0.020
< 0.070
TO-15
04/17/14
1
1,4-Bromofluorobenzene
460-00-4
96.9
o Rec.
TO-15
04/17/14
1
RDL1 = ppbv , RDL2 = ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/18/14 11:17 Printed: 04/18/14 11:18
Page 9 of 14

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
1-800-767-5859
Fax (615)
758-5859
Tax I.D. 62-0814289
Est. 1970
REPORT
OF
ANALYSIS
Ed Eoloszyn/Candy Elliott
April
18, 2014
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample
#
L693331-09
Date Received April
11, 2014
Description AMI, Inc
Site
Site
ID
Sample ID DUP-1
Project
#
1054-14-2086
Collected By Candy E.
Elliott
Collection Date 04/09/14
00:00
Parameter
Cas#
Mol Wght
RDL1
RDL2
ppbv
ug/m3
Method
Date
Dil.
Volatile Organics - TO-15 SIM
Benzene
71-43-2
78.1
0.10
0.32
3.3
11.
TO-15
04/17/14
5
Carbon tetrachloride
56-23-5
154
0.020
0.13
<
0.020
< 0.13
TO-15
04/16/14
1
Chloroethane
75-00-3
64.5
0.040
0.11
<
0.040
< 0.11
TO-15
04/16/14
1
Chloroform
67-66-3
119
0.020
0.097
<
0.020
< 0.097
TO-15
04/16/14
1
Chloromethane
74-87-3
50.5
0.030
0.062
1.4
2.9
TO-15
04/16/14
1
1,2-Dibromoethane
106-93-4
188
0.020
0.15
<
0.020
< 0.15
TO-15
04/16/14
1
1,4-Dichlorobenzene
106-46-7
147
0.020
0.12
0.023
0.14
TO-15
04/16/14
1
1,1-Dichloroethane
75-34-3
98
0.020
0.080
<
0.020
< 0.080
TO-15
04/16/14
1
1,1-Dichloroethene
75-35-4
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
cis-1,2-Dichloroethene
156-59-2
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
trans-1,2-Dichloroethene
156-60-5
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
1,2-Dichloropropane
78-87-5
113
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
cis-1,3-Dichloropropene
10061-01-5
111
0.020
0.091
<
0.020
< 0.091
TO-15
04/16/14
1
trans-1,3-Dichloropropene
10061-02-6
111
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
Ethylbenzene
100-41-4
106
0.030
0.13
0.59
2.6
TO-15
04/16/14
1
1,1,2,2-Tetrachloroethane
79-34-5
168
0.020
0.14
<
0.020
< 0.14
TO-15
04/16/14
1
Tetrachloroethylene
127-18-4
166
0.020
0.14
<
0.020
< 0.14
TO-15
04/16/14
1
1,1,1-Trichloroethane
71-55-6
133
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
1,1,2-Trichloroethane
79-00-5
133
0.030
0.16
<
0.030
< 0.16
TO-15
04/16/14
1
Trichloroethylene
79-01-6
131
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
Vinyl chloride
75-01-4
62.5
0.020
0.051
<
0.020
< 0.051
TO-15
04/16/14
1
Vinyl acetate
108-05-4
86.1
0.020
0.070
<
0.020
< 0.070
TO-15
04/16/14
1
1,4-Bromofluorobenzene
460-00-4
92.8
o Rec.
TO-15
04/16/14
1
RDL1 = ppbv , RDL2 = ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/18/14 11:17 Printed: 04/18/14 11:18
Page 10 of 14

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
1-800-767-5859
Fax (615)
758-5859
Tax I.D. 62-0814289
Est. 1970
REPORT
OF
ANALYSIS
Ed Eoloszyn/Candy Elliott
April
18, 2014
S&ME Inc. - Raleigh NC
3201 Spring Forest Road
Raleigh, NC 27616
ESC Sample
#
L693331-10
Date Received April
11,
2014
Description AMI, Inc
Site
Site
ID
Sample ID VP-9 930
HAHN
ROAD
Project
#
1054-14-2086
Collected By Candy E.
Elliott
Collection Date 04/10/14
12:20
Parameter
Cas#
Mol Wght
RDL1
RDL2
ppbv
ug/m3
Method
Date
Dil.
Volatile Organics - TO-15 SIM
Benzene
71-43-2
78.1
0.020
0.064
1.2
3.8
TO-15
04/16/14
1
Carbon tetrachloride
56-23-5
154
0.020
0.13
<
0.020
< 0.13
TO-15
04/16/14
1
Chloroethane
75-00-3
64.5
0.040
0.11
<
0.040
< 0.11
TO-15
04/16/14
1
Chloroform
67-66-3
119
0.020
0.097
<
0.020
< 0.097
TO-15
04/16/14
1
Chloromethane
74-87-3
50.5
0.12
0.25
5.3
11.
TO-15
04/17/14
4
1,2-Dibromoethane
106-93-4
188
0.020
0.15
<
0.020
< 0.15
TO-15
04/16/14
1
1,4-Dichlorobenzene
106-46-7
147
0.020
0.12
<
0.020
< 0.12
TO-15
04/16/14
1
1,1-Dichloroethane
75-34-3
98
0.020
0.080
<
0.020
< 0.080
TO-15
04/16/14
1
1,1-Dichloroethene
75-35-4
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
cis-1,2-Dichloroethene
156-59-2
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
trans-1,2-Dichloroethene
156-60-5
96.9
0.020
0.079
<
0.020
< 0.079
TO-15
04/16/14
1
1,2-Dichloropropane
78-87-5
113
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
cis-1,3-Dichloropropene
10061-01-5
111
0.020
0.091
<
0.020
< 0.091
TO-15
04/16/14
1
trans-1,3-Dichloropropene
10061-02-6
111
0.030
0.14
<
0.030
< 0.14
TO-15
04/16/14
1
Ethylbenzene
100-41-4
106
0.030
0.13
0.33
1.4
TO-15
04/16/14
1
1,1,2,2-Tetrachloroethane
79-34-5
168
0.020
0.14
<
0.020
< 0.14
TO-15
04/16/14
1
Tetrachloroethylene
127-18-4
166
0.020
0.14
0.025
0.17
TO-15
04/16/14
1
1,1,1-Trichloroethane
71-55-6
133
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
1,1,2-Trichloroethane
79-00-5
133
0.030
0.16
<
0.030
< 0.16
TO-15
04/16/14
1
Trichloroethylene
79-01-6
131
0.020
0.11
<
0.020
< 0.11
TO-15
04/16/14
1
Vinyl chloride
75-01-4
62.5
0.020
0.051
<
0.020
< 0.051
TO-15
04/16/14
1
Vinyl acetate
108-05-4
86.1
0.020
0.070
<
0.020
< 0.070
TO-15
04/16/14
1
1,4-Bromofluorobenzene
460-00-4
100
o Rec.
TO-15
04/16/14
1
RDL1 = ppbv , RDL2 = ug/m3
Note:
Units are based on (STP) - Standard Temperature and Pressure
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 04/18/14 11:17 Printed: 04/18/14 11:18
Page 11 of 14

Summary of Remarks For Samples Printed
04/18/14 at 11:18:22
TSR Signing Reports: 690
R5 - Desired TAT
Sample: L693331-01 Account: SMERLNC Received: 04/11/14 10:15 Due Date: 04/18/14 00:00 RPT Date: 04/18/14 11:17
Sample: L693331-02 Account: SMERLNC Received: 04/11/14 10:15 Due Date: 04/18/14 00:00 RPT Date: 04/18/14 11:17
Sample: L693331-03 Account: SMERLNC Received: 04/11/14 10:15 Due Date: 04/18/14 00:00 RPT Date: 04/18/14 11:17
Sample: L693331-04 Account: SMERLNC Received: 04/11/14 10:15 Due Date: 04/18/14 00:00 RPT Date: 04/18/14 11:17
Sample: L693331-05 Account: SMERLNC Received: 04/11/14 10:15 Due Date: 04/18/14 00:00 RPT Date: 04/18/14 11:17
Sample: L693331-06 Account: SMERLNC Received: 04/11/14 10:15 Due Date: 04/18/14 00:00 RPT Date: 04/18/14 11:17
Sample: L693331-07 Account: SMERLNC Received: 04/11/14 10:15 Due Date: 04/18/14 00:00 RPT Date: 04/18/14 11:17
Sample: L693331-08 Account: SMERLNC Received: 04/11/14 10:15 Due Date: 04/18/14 00:00 RPT Date: 04/18/14 11:17
Sample: L693331-09 Account: SMERLNC Received: 04/11/14 10:15 Due Date: 04/18/14 00:00 RPT Date: 04/18/14 11:17
Sample: L693331-10 Account: SMERLNC Received: 04/11/14 10:15 Due Date: 04/18/14 00:00 RPT Date: 04/18/14 11:17

12065 Lebanon Rd.
Mt. Juliet,
TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
S&ME Inc. - Raleigh NC
Ed Eoloszyn/Candy Elliott
3201 Spring Forest Road
Quality
Assurance
Report
Level
II
Raleigh, NC 27616
April 18, 2014
L693331
Laboratory Blank
Analyte
Result
Units
% Rec
Limit
Batch
Date Analyzed
1,1,1-Trichloroethane
< .02
ppb
WG716408
04/16/14 14:18
1,1,2,2-Tetrachloroethane
< .02
ppb
WG716408
04/16/14 14:18
1,1,2-Trichloroethane
< .03
ppb
WG716408
04/16/14 14:18
1,1-Dichloroethane
< .02
ppb
WG716408
04/16/14 14:18
1,1-Dichloroethene
< .02
ppb
WG716408
04/16/14 14:18
1,2-Dibromoethane
< .02
ppb
WG716408
04/16/14 14:18
1,2-Dichloropropane
< .03
ppb
WG716408
04/16/14 14:18
1,4-Dichlorobenzene
< .02
ppb
WG716408
04/16/14 14:18
Benzene
< .02
ppb
WG716408
04/16/14 14:18
Carbon tetrachloride
< .02
ppb
WG716408
04/16/14 14:18
Chloroethane
< .04
ppb
WG716408
04/16/14 14:18
Chloroform
< .02
ppb
WG716408
04/16/14 14:18
Chloromethane
< .03
ppb
WG716408
04/16/14 14:18
cis-1,2-Dichloroethene
< .02
ppb
WG716408
04/16/14 14:18
cis-1,3-Dichloropropene
< .02
ppb
WG716408
04/16/14 14:18
Ethylbenzene
< .03
ppb
WG716408
04/16/14 14:18
Tetrachloroethylene
< .02
ppb
WG716408
04/16/14 14:18
trans-1,2-Dichloroethene
< .02
ppb
WG716408
04/16/14 14:18
trans-1,3-Dichloropropene
< .03
ppb
WG716408
04/16/14 14:18
Trichloroethylene
< .02
ppb
WG716408
04/16/14 14:18
Vinyl acetate
< .02
ppb
WG716408
04/16/14 14:18
Vinyl chloride
< .02
ppb
WG716408
04/16/14 14:18
1,4-Bromofluorobenzene
% Rec.
96.70
60-140
WG716408
04/16/14 14:18
Benzene
< .02
ppb
WG716576
04/17/14 12:28
Chloromethane
< .03
ppb
WG716576
04/17/14 12:28
1,4-Bromofluorobenzene
% Rec.
93.40
60-140
WG716576
04/17/14 12:28
Laboratory Control
Sample
Analyte
Units
Known Val
Result
% Rec
Limit
Batch
1,1,1-Trichloroethane
ppb
.5
0.468
93.6
70-130
WG716408
1,1,2,2-Tetrachloroethane
ppb
.5
0.425
85.1
70-130
WG716408
1,1,2-Trichloroethane
ppb
.5
0.475
95.0
70-130
WG716408
1,1-Dichloroethane
ppb
.5
0.482
96.5
70-130
WG716408
1,1-Dichloroethene
ppb
.5
0.426
85.1
70-130
WG716408
1,2-Dibromoethane
ppb
.5
0.449
89.8
70-130
WG716408
1,2-Dichloropropane
ppb
.5
0.499
99.7
70-130
WG716408
1,4-Dichlorobenzene
ppb
.5
0.368
73.5
70-130
WG716408
Benzene
ppb
.5
0.457
91.5
70-130
WG716408
Carbon tetrachloride
ppb
.5
0.442
88.4
70-130
WG716408
Chloroethane
ppb
.5
0.440
88.1
70-130
WG716408
Chloroform
ppb
.5
0.481
96.2
70-130
WG716408
Chloromethane
ppb
.5
0.463
92.6
70-130
WG716408
cis-1,2-Dichloroethene
ppb
.5
0.496
99.2
70-130
WG716408
cis-1,3-Dichloropropene
ppb
.5
0.483
96.6
70-130
WG716408
Ethylbenzene
ppb
.5
0.472
94.3
70-130
WG716408
Tetrachloroethylene
ppb
.5
0.452
90.4
70-130
WG716408
trans-1,2-Dichloroethene
ppb
.5
0.465
93.0
70-130
WG716408
trans-1,3-Dichloropropene
ppb
.5
0.488
97.6
70-130
WG716408
Trichloroethylene
ppb
.5
0.459
91.8
70-130
WG716408
Vinyl acetate
ppb
.5
0.616
123.
70-130
WG716408
Vinyl chloride
ppb
.5
0.439
87.9
70-130
WG716408
1,4-Bromofluorobenzene
96.30
60-140
WG716408
Benzene
ppb
.5
0.456
91.2
70-130
WG716576
Chloromethane
ppb
.5
0.457
91.4
70-130
WG716576
* Performance of this Analyte
is outside
of established
criteria.
For additional information,
please see
Attachment
A 'List of
Analytes with
QC Qualifiers.'
Page 12 of 14

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
S&ME Inc. - Raleigh NC
Ed Eoloszyn/Candy Elliott
3201 Spring Forest Road Quality Assurance Report
Level II
Raleigh, NC 27616 April 18, 2014
L693331
Laboratory Control Sample Duplicate
Analyte Units Result Ref %Rec Limit RPD Limit Batch
1,4-Bromofluorobenzene 90.80 60-140
Laboratory
Control
Sample Duplicate
Analyte
Units
Result
Ref
%Rec
Limit
RPD
Limit
Batch
1,1,1-Trichloroethane
ppb
0.452
0.468
90.0
70-130
3.35
25
WG716408
1,1,2,2-Tetrachloroethane
ppb
0.402
0.425
80.0
70-130
5.67
25
WG716408
1,1,2-Trichloroethane
ppb
0.457
0.475
91.0
70-130
3.84
25
WG716408
1,1-Dichloroethane
ppb
0.462
0.482
92.0
70-130
4.38
25
WG716408
1,1-Dichloroethene
ppb
0.416
0.426
83.0
70-130
2.19
25
WG716408
1,2-Dibromoethane
ppb
0.430
0.449
86.0
70-130
4.28
25
WG716408
1,2-Dichloropropane
ppb
0.481
0.499
96.0
70-130
3.58
25
WG716408
1,4-Dichlorobenzene
ppb
0.355
0.368
71.0
70-130
3.51
25
WG716408
Benzene
ppb
0.447
0.457
89.0
70-130
2.34
25
WG716408
Carbon tetrachloride
ppb
0.448
0.442
90.0
70-130
1.40
25
WG716408
Chloroethane
ppb
0.442
0.440
88.0
70-130
0.300
25
WG716408
Chloroform
ppb
0.468
0.481
94.0
70-130
2.69
25
WG716408
Chloromethane
ppb
0.453
0.463
90.0
70-130
2.28
25
WG716408
cis-1,2-Dichloroethene
ppb
0.455
0.496
91.0
70-130
8.63
25
WG716408
cis-1,3-Dichloropropene
ppb
0.459
0.483
92.0
70-130
5.10
25
WG716408
Ethylbenzene
ppb
0.450
0.472
90.0
70-130
4.79
25
WG716408
Tetrachloroethylene
ppb
0.438
0.452
88.0
70-130
3.19
25
WG716408
trans-1,2-Dichloroethene
ppb
0.453
0.465
90.0
70-130
2.61
25
WG716408
trans-1,3-Dichloropropene
ppb
0.460
0.488
92.0
70-130
5.88
25
WG716408
Trichloroethylene
ppb
0.445
0.459
89.0
70-130
3.10
25
WG716408
Vinyl acetate
ppb
0.544
0.616
109.
70-130
12.5
25
WG716408
Vinyl chloride
ppb
0.421
0.439
84.0
70-130
4.16
25
WG716408
1,4-Bromofluorobenzene
96.00
60-140
WG716408
Benzene
ppb
0.461
0.456
92.0
70-130
1.04
25
WG716576
Chloromethane
ppb
0.470
0.457
94.0
70-130
2.77
25
WG716576
1,4-Bromofluorobenzene
87.80
60-140
WG716576
Batch number /Run number / Sample number cross reference
WG716408: R2905415: L693331-01 02 03 04 05 06 07 08 09 10
WG716576: R2905820: L693331-05 06 08
* * Calculations are performed prior to rounding of reported values.
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 13 of 14

12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
S&ME Inc. - Raleigh NC
Ed Eoloszyn/Candy Elliott
3201 Spring Forest Road Quality Assurance Report
Level II
Raleigh, NC 27616
L693331
The data package includes a summary of the analytic results of the quality
control samples required by the SW-846 or CWA methods. The quality control
samples include a method blank, a laboratory control sample, and the matrix
spike/matrix spike duplicate analysis. If a target parameter is outside
the method limits, every sample that is effected is flagged with the
appropriate qualifier in Appendix B of the analytic report.
Method Blank - an aliquot of reagent water carried through the
entire analytic process. The method blank results indicate if
any possible contamination exposure during the sample handling,
digestion or extraction process, and analysis. Concentrations of
target analytes above the reporting limit in the method blank are
qualified with the "B" qualifier.
Laboratory Control Sample - is a sample of known concentration
that is carried through the digestion/extraction and analysis
process. The percent recovery, expressed as a percentage of the
theoretical concentration, has statistical control limits
indicating that the analytic process is "in control". If a
target analyte is outside the control limits for the laboratory
control sample or any other control sample, the parameter is
flagged with a "J4" qualifier for all effected samples.
Matrix Spike and Matrix Spike Duplicate - is two aliquots of an
environmental sample that is spiked with known concentrations of
target analytes. The percent recovery of the target analytes
also has statistical control limits. If any recoveries that are
outside the method control limits, the sample that was selected
for matrix spike/matrix spike duplicate analysis is flagged with
either a "J5" or a "J6". The relative percent difference (%RPD)
between the matrix spike and the matrix spike duplicate
recoveries is all calculated. If the RPD is above the method
limit, the effected samples are flagged with a "J3" qualifier.
Page 14 of 14
April 18, 2014

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