24050_Vernon Packaging_Soil Import Data and Approval_20211214

December 14, 2021 Sent Via E-mail Mr. Mark Miller Terracon
7327-G West Friendly Avenue Greensboro, North Carolina 27410 [e-mail] Subject: Brownfields Soil Import Approval
Vernon Packaging Winston-Salem, Forsyth County Brownfields Project No. 24050-20-034 Dear Mr. Miller:
The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received and reviewed the laboratory data attached to your email dated December 13, 2021, regarding the Brownfields Property referenced above. The request is for approval to import no more than 1,000 cubic yards of soil from the Vulcan Forsyth East Quarry (Quarry) at 2868 NC Highway 66 S. in Kernersville, NC.
Upon review of the data, no volatile organic compounds (VOCs) or semi-volatile organic compounds (SVOCs) were detected above the DEQ Preliminary Soil Remediation Goals (PSRGs) in the soil sampled at the Quarry. Except for arsenic, all metals detected are either below the PSRGs or consistent with concentrations at the Brownfields Property. Since the concentration of arsenic at the Quarry exceeds the
range of concentrations at the Brownfields Property, risk was evaluated using the DEQ Risk Calculator. The calculated risk indicates that import of the soil from the Quarry will not have a negative impact on the Brownfields Property. As such, import from the Vulcan Forsyth East Quarry is approved. Please note that import of additional soil will require additional sampling from the source area.

Please be advised that this approval does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local entities. If you have questions about this correspondence or require additional information, please feel free to contact Pete Doorn by phone at 984-275-5391 or by email at [e-mail].

Sincerely,
Peter L. Doorn, Project Manager Brownfields Program Ec: Porter Jones, DPJ Residential, LLC
Tracy Wahl, DEQ Brownfields
From:Miller, Mark I
To:Doorn, Peter L
Subject:[External] Vernon Packaging
Date:Monday, December 13, 2021 11:36:06 AM
Attachments:Import Soils Lab Report.pdf
CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
attachment to Report Spam.
Hi Pete:

We collected the soil import soil samples from the Vulcan East Forsyth quarry in accordance with our
workplan dated 10/15/2021. The lab results are attached. The samples were ND for VOCs and
SVOCs. The laboratory reported the presence of arsenic at 13.2 mg/kg, barium at 144 mg/kg, total
chromium at 68.8 mg/kg, lead at 23.1 mg/kg and mercury at 1.04 mg/kg. Hexavalent chrome,
cadmium, selenium and silver were not detected. It appears that the arsenic concentration exceeds
the Residential PSRG of 0.68 mg/kg, and the total chromium concentration exceeds the Residential
PSRG (for hexavalent chrome) of 0.31 mg/kg (comparison pursuant to the PSRG Table notes). The
metals concentrations in the quarry soils are almost certainly naturally occurring. Please let me
know if you have questions or comments.

Best wishes,

Mark I. Miller, L.G.
Licensed Geologist I Environmental Services

7327-G West Friendly Avenue, Greensboro, NC 27410
Direct: 336-854-8135 I Mobile: [phone] I Fax: [phone]
[e-mail] I www.terracon.com/greensboro
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ANALYTICAL REPORT
November 22, 2021
Terracon - Greensboro, NC
Sample Delivery Group:L1431305
Samples Received:11/13/2021
Project Number:75217006
Description:Vernon Packaging
Report To:Mark Miller
7327-G, West Friendly Ave
Greensboro, NC 27410
Entire Report Reviewed By:
November 22, 2021
[Preliminary Report]
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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November 23, 2021
Heather J Wagner
Project Manager
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
S-1 L1431305-01 5
S-1 L1431305-02 7
Qc: Quality Control Summary 9
Total Solids by Method 2540 G-2011 9
Wet Chemistry by Method 7199 10
Mercury by Method 7471B 11
Metals (ICP) by Method 6010D 12
Volatile Organic Compounds (GC/MS) by Method 8260D 13
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 17
Gl: Glossary of Terms 22
Al: Accreditations & Locations 23
Sc: Sample Chain of Custody 24
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
S-1 L1431305-01 Solid Mark Miller 11/10/21 10:00 11/13/21 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1775163 1 11/17/21 17:03 11/17/21 17:44 KDW Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1776437 2.67 11/10/21 10:00 11/18/21 17:44 DWR Mt. Juliet, TN
Collected by Collected date/time Received date/time
S-1 L1431305-02 Solid Mark Miller 11/10/21 10:00 11/13/21 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1775163 1 11/17/21 17:03 11/17/21 17:44 KDW Mt. Juliet, TN
Wet Chemistry by Method 7199 WG1775672 1 11/18/21 09:53 11/19/21 00:27 JER Mt. Juliet, TN
Mercury by Method 7471B WG1776009 1 11/21/21 13:16 11/22/21 09:31 ABL Mt. Juliet, TN
Metals (ICP) by Method 6010D WG1776335 1 11/18/21 08:48 11/19/21 21:09 KMG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1777168 1 11/19/21 16:49 11/20/21 21:20 JNJ Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Heather J Wagner
Project Manager
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Heather J Wagner
Project Manager
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SAMPLE RESULTS - 01
L1431305
S-1
Collected date/time: 11/10/21 10:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.6 1 11/17/2021 17:44 WG1775163
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acetone ND 0.181 2.67 11/18/2021 17:44 WG1776437
Acrylonitrile ND 0.0452 2.67 11/18/2021 17:44 WG1776437
Benzene ND 0.00361 2.67 11/18/2021 17:44 WG1776437
Bromobenzene ND 0.0452 2.67 11/18/2021 17:44 WG1776437
Bromodichloromethane ND 0.00903 2.67 11/18/2021 17:44 WG1776437
Bromoform ND 0.0903 2.67 11/18/2021 17:44 WG1776437
Bromomethane ND 0.0452 2.67 11/18/2021 17:44 WG1776437
n-Butylbenzene ND 0.0452 2.67 11/18/2021 17:44 WG1776437
sec-Butylbenzene ND 0.0452 2.67 11/18/2021 17:44 WG1776437
tert-Butylbenzene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
Carbon tetrachloride ND 0.0181 2.67 11/18/2021 17:44 WG1776437
Chlorobenzene ND 0.00903 2.67 11/18/2021 17:44 WG1776437
Chlorodibromomethane ND 0.00903 2.67 11/18/2021 17:44 WG1776437
Chloroethane ND 0.0181 2.67 11/18/2021 17:44 WG1776437
Chloroform ND 0.00903 2.67 11/18/2021 17:44 WG1776437
Chloromethane ND 0.0452 2.67 11/18/2021 17:44 WG1776437
2-Chlorotoluene ND 0.00903 2.67 11/18/2021 17:44 WG1776437
4-Chlorotoluene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
1,2-Dibromo-3-Chloropropane ND C3 0.0903 2.67 11/18/2021 17:44 WG1776437
1,2-Dibromoethane ND 0.00903 2.67 11/18/2021 17:44 WG1776437
Dibromomethane ND 0.0181 2.67 11/18/2021 17:44 WG1776437
1,2-Dichlorobenzene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
1,3-Dichlorobenzene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
1,4-Dichlorobenzene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
Dichlorodifluoromethane ND 0.00903 2.67 11/18/2021 17:44 WG1776437
1,1-Dichloroethane ND 0.00903 2.67 11/18/2021 17:44 WG1776437
1,2-Dichloroethane ND 0.00903 2.67 11/18/2021 17:44 WG1776437
1,1-Dichloroethene ND 0.00903 2.67 11/18/2021 17:44 WG1776437
cis-1,2-Dichloroethene ND 0.00903 2.67 11/18/2021 17:44 WG1776437
trans-1,2-Dichloroethene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
1,2-Dichloropropane ND 0.0181 2.67 11/18/2021 17:44 WG1776437
1,1-Dichloropropene ND 0.00903 2.67 11/18/2021 17:44 WG1776437
1,3-Dichloropropane ND 0.0181 2.67 11/18/2021 17:44 WG1776437
cis-1,3-Dichloropropene ND 0.00903 2.67 11/18/2021 17:44 WG1776437
trans-1,3-Dichloropropene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
2,2-Dichloropropane ND 0.00903 2.67 11/18/2021 17:44 WG1776437
Di-isopropyl ether ND 0.00361 2.67 11/18/2021 17:44 WG1776437
Ethylbenzene ND 0.00903 2.67 11/18/2021 17:44 WG1776437
Hexachloro-1,3-butadiene ND 0.0903 2.67 11/18/2021 17:44 WG1776437
Isopropylbenzene ND 0.00903 2.67 11/18/2021 17:44 WG1776437
p-Isopropyltoluene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
2-Butanone (MEK)ND C3 0.361 2.67 11/18/2021 17:44 WG1776437
Methylene Chloride ND 0.0903 2.67 11/18/2021 17:44 WG1776437
4-Methyl-2-pentanone (MIBK)ND C3 0.0903 2.67 11/18/2021 17:44 WG1776437
Methyl tert-butyl ether ND 0.00361 2.67 11/18/2021 17:44 WG1776437
Naphthalene ND C3 0.0452 2.67 11/18/2021 17:44 WG1776437
n-Propylbenzene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
Styrene ND 0.0452 2.67 11/18/2021 17:44 WG1776437
1,1,1,2-Tetrachloroethane ND J4 0.00903 2.67 11/18/2021 17:44 WG1776437
1,1,2,2-Tetrachloroethane ND C3 0.00903 2.67 11/18/2021 17:44 WG1776437
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 01
L1431305
S-1
Collected date/time: 11/10/21 10:00
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,1,2-Trichlorotrifluoroethane ND 0.00903 2.67 11/18/2021 17:44 WG1776437
Tetrachloroethene ND 0.00903 2.67 11/18/2021 17:44 WG1776437
Toluene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
1,2,3-Trichlorobenzene ND 0.0452 2.67 11/18/2021 17:44 WG1776437
1,2,4-Trichlorobenzene ND 0.0452 2.67 11/18/2021 17:44 WG1776437
1,1,1-Trichloroethane ND J4 0.00903 2.67 11/18/2021 17:44 WG1776437
1,1,2-Trichloroethane ND 0.00903 2.67 11/18/2021 17:44 WG1776437
Trichloroethene ND 0.00361 2.67 11/18/2021 17:44 WG1776437
Trichlorofluoromethane ND 0.00903 2.67 11/18/2021 17:44 WG1776437
1,2,3-Trichloropropane ND 0.0452 2.67 11/18/2021 17:44 WG1776437
1,2,4-Trimethylbenzene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
1,2,3-Trimethylbenzene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
Vinyl chloride ND 0.00903 2.67 11/18/2021 17:44 WG1776437
1,3,5-Trimethylbenzene ND 0.0181 2.67 11/18/2021 17:44 WG1776437
Xylenes, Total ND 0.0235 2.67 11/18/2021 17:44 WG1776437
(S) Toluene-d8 106 75.0-131 11/18/2021 17:44 WG1776437
(S) 4-Bromofluorobenzene 99.6 67.0-138 11/18/2021 17:44 WG1776437
(S) 1,2-Dichloroethane-d4 83.8 70.0-130 11/18/2021 17:44 WG1776437
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1431305
S-1
Collected date/time: 11/10/21 10:00
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 80.1 1 11/17/2021 17:44 WG1775163
Wet Chemistry by Method 7199
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Hexavalent Chromium ND 1.25 1 11/19/2021 00:27 WG1775672
Mercury by Method 7471B
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury 1.04 0.0500 1 11/22/2021 09:31 WG1776009
Metals (ICP) by Method 6010D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Arsenic 13.2 2.50 1 11/19/2021 21:09 WG1776335
Barium 144 0.624 1 11/19/2021 21:09 WG1776335
Cadmium ND 0.624 1 11/19/2021 21:09 WG1776335
Chromium 68.8 1.25 1 11/19/2021 21:09 WG1776335
Lead 23.1 0.624 1 11/19/2021 21:09 WG1776335
Selenium ND 2.50 1 11/19/2021 21:09 WG1776335
Silver ND 1.25 1 11/19/2021 21:09 WG1776335
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0416 1 11/20/2021 21:20 WG1777168
Acenaphthylene ND 0.0416 1 11/20/2021 21:20 WG1777168
Anthracene ND 0.0416 1 11/20/2021 21:20 WG1777168
Benzidine ND J6 2.09 1 11/20/2021 21:20 WG1777168
Benzo(a)anthracene ND 0.0416 1 11/20/2021 21:20 WG1777168
Benzo(b)fluoranthene ND 0.0416 1 11/20/2021 21:20 WG1777168
Benzo(k)fluoranthene ND 0.0416 1 11/20/2021 21:20 WG1777168
Benzo(g,h,i)perylene ND 0.0416 1 11/20/2021 21:20 WG1777168
Benzo(a)pyrene ND 0.0416 1 11/20/2021 21:20 WG1777168
Bis(2-chlorethoxy)methane ND 0.416 1 11/20/2021 21:20 WG1777168
Bis(2-chloroethyl)ether ND C3 0.416 1 11/20/2021 21:20 WG1777168
2,2-Oxybis(1-Chloropropane)ND 0.416 1 11/20/2021 21:20 WG1777168
4-Bromophenyl-phenylether ND 0.416 1 11/20/2021 21:20 WG1777168
2-Chloronaphthalene ND 0.0416 1 11/20/2021 21:20 WG1777168
4-Chlorophenyl-phenylether ND 0.416 1 11/20/2021 21:20 WG1777168
Chrysene ND 0.0416 1 11/20/2021 21:20 WG1777168
Dibenz(a,h)anthracene ND 0.0416 1 11/20/2021 21:20 WG1777168
3,3-Dichlorobenzidine ND 0.416 1 11/20/2021 21:20 WG1777168
2,4-Dinitrotoluene ND 0.416 1 11/20/2021 21:20 WG1777168
2,6-Dinitrotoluene ND 0.416 1 11/20/2021 21:20 WG1777168
Fluoranthene ND 0.0416 1 11/20/2021 21:20 WG1777168
Fluorene ND 0.0416 1 11/20/2021 21:20 WG1777168
Hexachlorobenzene ND 0.416 1 11/20/2021 21:20 WG1777168
Hexachloro-1,3-butadiene ND 0.416 1 11/20/2021 21:20 WG1777168
Hexachlorocyclopentadiene ND 0.416 1 11/20/2021 21:20 WG1777168
Hexachloroethane ND 0.416 1 11/20/2021 21:20 WG1777168
Indeno(1,2,3-cd)pyrene ND 0.0416 1 11/20/2021 21:20 WG1777168
Isophorone ND 0.416 1 11/20/2021 21:20 WG1777168
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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SAMPLE RESULTS - 02
L1431305
S-1
Collected date/time: 11/10/21 10:00
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Naphthalene ND 0.0416 1 11/20/2021 21:20 WG1777168
Nitrobenzene ND 0.416 1 11/20/2021 21:20 WG1777168
n-Nitrosodimethylamine ND 0.416 1 11/20/2021 21:20 WG1777168
n-Nitrosodiphenylamine ND 0.416 1 11/20/2021 21:20 WG1777168
n-Nitrosodi-n-propylamine ND 0.416 1 11/20/2021 21:20 WG1777168
Phenanthrene ND 0.0416 1 11/20/2021 21:20 WG1777168
Benzylbutyl phthalate ND 0.416 1 11/20/2021 21:20 WG1777168
Bis(2-ethylhexyl)phthalate 1.03 J6 0.416 1 11/20/2021 21:20 WG1777168
Di-n-butyl phthalate ND J6 0.416 1 11/20/2021 21:20 WG1777168
Diethyl phthalate ND 0.416 1 11/20/2021 21:20 WG1777168
Dimethyl phthalate ND 0.416 1 11/20/2021 21:20 WG1777168
Di-n-octyl phthalate ND 0.416 1 11/20/2021 21:20 WG1777168
Pyrene ND 0.0416 1 11/20/2021 21:20 WG1777168
1,2,4-Trichlorobenzene ND 0.416 1 11/20/2021 21:20 WG1777168
4-Chloro-3-methylphenol ND 0.416 1 11/20/2021 21:20 WG1777168
2-Chlorophenol ND 0.416 1 11/20/2021 21:20 WG1777168
2,4-Dichlorophenol ND 0.416 1 11/20/2021 21:20 WG1777168
2,4-Dimethylphenol ND 0.416 1 11/20/2021 21:20 WG1777168
4,6-Dinitro-2-methylphenol ND 0.416 1 11/20/2021 21:20 WG1777168
2,4-Dinitrophenol ND 0.416 1 11/20/2021 21:20 WG1777168
2-Nitrophenol ND 0.416 1 11/20/2021 21:20 WG1777168
4-Nitrophenol ND 0.416 1 11/20/2021 21:20 WG1777168
Pentachlorophenol ND 0.416 1 11/20/2021 21:20 WG1777168
Phenol ND 0.416 1 11/20/2021 21:20 WG1777168
2,4,6-Trichlorophenol ND 0.416 1 11/20/2021 21:20 WG1777168
(S) 2-Fluorophenol 32.4 12.0-120 11/20/2021 21:20 WG1777168
(S) Phenol-d5 28.1 10.0-120 11/20/2021 21:20 WG1777168
(S) Nitrobenzene-d5 32.1 10.0-122 11/20/2021 21:20 WG1777168
(S) 2-Fluorobiphenyl 32.4 15.0-120 11/20/2021 21:20 WG1777168
(S) 2,4,6-Tribromophenol 33.5 10.0-127 11/20/2021 21:20 WG1777168
(S) p-Terphenyl-d14 32.4 10.0-120 11/20/2021 21:20 WG1777168
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1775163
Total Solids by Method 2540 G-2011 L1431305-01,02
Method Blank (MB)
(MB) R3731089-1 11/17/21 17:44
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00300
L1431305-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1431305-01 11/17/21 17:44 • (DUP) R3731089-3 11/17/21 17:44
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 79.6 86.8 1 8.66 10
Laboratory Control Sample (LCS)
(LCS) R3731089-2 11/17/21 17:44
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 99.9 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1775672
Wet Chemistry by Method 7199 L1431305-02
Method Blank (MB)
(MB) R3731651-1 11/18/21 22:10
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Hexavalent Chromium U 0.255 1.00
L1430758-06 Original Sample (OS) • Duplicate (DUP)
(OS) L1430758-06 11/18/21 23:15 • (DUP) R3731651-7 11/18/21 23:20
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
L1430892-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1430892-01 11/19/21 00:17 • (DUP) R3731651-8 11/19/21 00:22
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %%
Hexavalent Chromium ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3731651-2 11/18/21 22:18
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Hexavalent Chromium 10.0 10.8 108 80.0-120
L1430758-05 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1430758-05 11/18/21 22:33 • (MS) R3731651-3 11/18/21 22:38 • (MSD) R3731651-4 11/18/21 22:43
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Hexavalent Chromium 20.0 ND 19.9 19.0 99.3 95.1 1 75.0-125 4.29 20
L1430758-05 Original Sample (OS) • Matrix Spike (MS)
(OS) L1430758-05 11/18/21 22:33 • (MS) R3731651-5 11/18/21 22:49
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte mg/kg mg/kg mg/kg %%
Hexavalent Chromium 641 ND 538 84.0 50 75.0-125
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1776009
Mercury by Method 7471B L1431305-02
Method Blank (MB)
(MB) R3732269-1 11/22/21 08:38
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.0180 0.0400
Laboratory Control Sample (LCS)
(LCS) R3732269-2 11/22/21 08:40
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Mercury 0.500 0.511 102 80.0-120
L1431200-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1431200-01 11/22/21 08:42 • (MS) R3732269-3 11/22/21 08:44 • (MSD) R3732269-4 11/22/21 08:46
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.500 ND 0.442 0.436 88.4 87.1 1 75.0-125 1.47 20
L1431197-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1431197-04 11/22/21 08:48 • (MS) R3732269-5 11/22/21 08:50 • (MSD) R3732269-6 11/22/21 08:52
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Mercury 0.500 ND 0.557 0.533 111 107 1 75.0-125 4.38 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1776335
Metals (ICP) by Method 6010D L1431305-02
Method Blank (MB)
(MB) R3731917-1 11/19/21 19:53
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Arsenic U 0.518 2.00
Barium U 0.0852 0.500
Cadmium U 0.0471 0.500
Chromium U 0.133 1.00
Lead U 0.208 0.500
Selenium U 0.764 2.00
Silver U 0.127 1.00
Laboratory Control Sample (LCS)
(LCS) R3731917-2 11/19/21 19:56
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Arsenic 100 101 101 80.0-120
Barium 100 107 107 80.0-120
Cadmium 100 100 100 80.0-120
Chromium 100 101 101 80.0-120
Lead 100 103 103 80.0-120
Selenium 100 102 102 80.0-120
Silver 20.0 18.0 89.9 80.0-120
L1431197-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1431197-04 11/19/21 19:58 • (MS) R3731917-5 11/19/21 20:06 • (MSD) R3731917-6 11/19/21 20:08
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Arsenic 100 2.44 105 96.9 102 94.5 1 75.0-125 7.68 20
Barium 100 115 221 202 107 87.3 1 75.0-125 9.09 20
Cadmium 100 ND 103 94.9 103 94.6 1 75.0-125 8.33 20
Chromium 100 20.6 122 113 102 92.1 1 75.0-125 8.10 20
Lead 100 7.66 120 111 112 103 1 75.0-125 7.46 20
Selenium 100 ND 103 94.3 103 94.3 1 75.0-125 8.53 20
Silver 20.0 ND 17.7 16.2 88.7 80.8 1 75.0-125 9.33 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1776437
Volatile Organic Compounds (GC/MS) by Method 8260D L1431305-01
Method Blank (MB)
(MB) R3732044-2 11/18/21 09:57
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0365 0.0500
Acrylonitrile U 0.00361 0.0125
Benzene U 0.000467 0.00100
Bromobenzene U 0.000900 0.0125
Bromodichloromethane U 0.000725 0.00250
Bromoform U 0.00117 0.0250
Bromomethane U 0.00197 0.0125
n-Butylbenzene U 0.00525 0.0125
sec-Butylbenzene U 0.00288 0.0125
tert-Butylbenzene U 0.00195 0.00500
Carbon tetrachloride U 0.000898 0.00500
Chlorobenzene U 0.000210 0.00250
Chlorodibromomethane U 0.000612 0.00250
Chloroethane U 0.00170 0.00500
Chloroform U 0.00103 0.00250
Chloromethane U 0.00435 0.0125
2-Chlorotoluene U 0.000865 0.00250
4-Chlorotoluene U 0.000450 0.00500
1,2-Dibromo-3-Chloropropane U 0.00390 0.0250
1,2-Dibromoethane U 0.000648 0.00250
Dibromomethane U 0.000750 0.00500
1,2-Dichlorobenzene U 0.000425 0.00500
1,3-Dichlorobenzene U 0.000600 0.00500
1,4-Dichlorobenzene U 0.000700 0.00500
Dichlorodifluoromethane U 0.00161 0.00250
1,1-Dichloroethane U 0.000491 0.00250
1,2-Dichloroethane U 0.000649 0.00250
1,1-Dichloroethene U 0.000606 0.00250
cis-1,2-Dichloroethene U 0.000734 0.00250
trans-1,2-Dichloroethene U 0.00104 0.00500
1,2-Dichloropropane U 0.00142 0.00500
1,1-Dichloropropene U 0.000809 0.00250
1,3-Dichloropropane U 0.000501 0.00500
cis-1,3-Dichloropropene U 0.000757 0.00250
trans-1,3-Dichloropropene U 0.00114 0.00500
2,2-Dichloropropane U 0.00138 0.00250
Di-isopropyl ether U 0.000410 0.00100
Ethylbenzene U 0.000737 0.00250
Hexachloro-1,3-butadiene U 0.00600 0.0250
Isopropylbenzene U 0.000425 0.00250
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1776437
Volatile Organic Compounds (GC/MS) by Method 8260D L1431305-01
Method Blank (MB)
(MB) R3732044-2 11/18/21 09:57
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
p-Isopropyltoluene U 0.00255 0.00500
2-Butanone (MEK)0.0785 J 0.0635 0.100
Methylene Chloride U 0.00664 0.0250
4-Methyl-2-pentanone (MIBK)U 0.00228 0.0250
Methyl tert-butyl ether U 0.000350 0.00100
Naphthalene U 0.00488 0.0125
n-Propylbenzene U 0.000950 0.00500
Styrene U 0.000229 0.0125
1,1,1,2-Tetrachloroethane U 0.000948 0.00250
1,1,2,2-Tetrachloroethane U 0.000695 0.00250
Tetrachloroethene U 0.000896 0.00250
Toluene U 0.00130 0.00500
1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250
1,2,3-Trichlorobenzene U 0.00733 0.0125
1,2,4-Trichlorobenzene U 0.00440 0.0125
1,1,1-Trichloroethane U 0.000923 0.00250
1,1,2-Trichloroethane U 0.000597 0.00250
Trichloroethene U 0.000584 0.00100
Trichlorofluoromethane U 0.000827 0.00250
1,2,3-Trichloropropane U 0.00162 0.0125
1,2,3-Trimethylbenzene U 0.00158 0.00500
1,2,4-Trimethylbenzene U 0.00158 0.00500
1,3,5-Trimethylbenzene U 0.00200 0.00500
Vinyl chloride U 0.00116 0.00250
Xylenes, Total U 0.000880 0.00650
(S) Toluene-d8 106 75.0-131
(S) 4-Bromofluorobenzene 101 67.0-138
(S) 1,2-Dichloroethane-d4 83.0 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3732044-1 11/18/21 08:59 • (LCSD) R3732044-3 11/18/21 12:53
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Acetone 0.625 0.578 0.604 92.5 96.6 10.0-160 4.40 31
Acrylonitrile 0.625 0.538 0.533 86.1 85.3 45.0-153 0.934 22
Benzene 0.125 0.143 0.139 114 111 70.0-123 2.84 20
Bromobenzene 0.125 0.111 0.104 88.8 83.2 73.0-121 6.51 20
Bromodichloromethane 0.125 0.130 0.124 104 99.2 73.0-121 4.72 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1776437
Volatile Organic Compounds (GC/MS) by Method 8260D L1431305-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3732044-1 11/18/21 08:59 • (LCSD) R3732044-3 11/18/21 12:53
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Bromoform 0.125 0.132 0.129 106 103 64.0-132 2.30 20
Bromomethane 0.125 0.163 0.166 130 133 56.0-147 1.82 20
n-Butylbenzene 0.125 0.105 0.103 84.0 82.4 68.0-135 1.92 20
sec-Butylbenzene 0.125 0.108 0.104 86.4 83.2 74.0-130 3.77 20
tert-Butylbenzene 0.125 0.104 0.0941 83.2 75.3 75.0-127 9.99 20
Carbon tetrachloride 0.125 0.144 0.146 115 117 66.0-128 1.38 20
Chlorobenzene 0.125 0.141 0.131 113 105 76.0-128 7.35 20
Chlorodibromomethane 0.125 0.130 0.124 104 99.2 74.0-127 4.72 20
Chloroethane 0.125 0.129 0.134 103 107 61.0-134 3.80 20
Chloroform 0.125 0.144 0.143 115 114 72.0-123 0.697 20
Chloromethane 0.125 0.102 0.105 81.6 84.0 51.0-138 2.90 20
2-Chlorotoluene 0.125 0.106 0.106 84.8 84.8 75.0-124 0.000 20
4-Chlorotoluene 0.125 0.103 0.0959 82.4 76.7 75.0-124 7.14 20
1,2-Dibromo-3-Chloropropane 0.125 0.0924 0.0928 73.9 74.2 59.0-130 0.432 20
1,2-Dibromoethane 0.125 0.121 0.114 96.8 91.2 74.0-128 5.96 20
Dibromomethane 0.125 0.136 0.136 109 109 75.0-122 0.000 20
1,2-Dichlorobenzene 0.125 0.127 0.126 102 101 76.0-124 0.791 20
1,3-Dichlorobenzene 0.125 0.121 0.117 96.8 93.6 76.0-125 3.36 20
1,4-Dichlorobenzene 0.125 0.122 0.116 97.6 92.8 77.0-121 5.04 20
Dichlorodifluoromethane 0.125 0.131 0.140 105 112 43.0-156 6.64 20
1,1-Dichloroethane 0.125 0.120 0.119 96.0 95.2 70.0-127 0.837 20
1,2-Dichloroethane 0.125 0.104 0.103 83.2 82.4 65.0-131 0.966 20
1,1-Dichloroethene 0.125 0.121 0.125 96.8 100 65.0-131 3.25 20
cis-1,2-Dichloroethene 0.125 0.146 0.145 117 116 73.0-125 0.687 20
trans-1,2-Dichloroethene 0.125 0.150 0.156 120 125 71.0-125 3.92 20
1,2-Dichloropropane 0.125 0.119 0.111 95.2 88.8 74.0-125 6.96 20
1,1-Dichloropropene 0.125 0.127 0.126 102 101 73.0-125 0.791 20
1,3-Dichloropropane 0.125 0.117 0.110 93.6 88.0 80.0-125 6.17 20
cis-1,3-Dichloropropene 0.125 0.121 0.110 96.8 88.0 76.0-127 9.52 20
trans-1,3-Dichloropropene 0.125 0.112 0.106 89.6 84.8 73.0-127 5.50 20
2,2-Dichloropropane 0.125 0.152 0.160 122 128 59.0-135 5.13 20
Di-isopropyl ether 0.125 0.105 0.107 84.0 85.6 60.0-136 1.89 20
Ethylbenzene 0.125 0.141 0.135 113 108 74.0-126 4.35 20
Hexachloro-1,3-butadiene 0.125 0.116 0.123 92.8 98.4 57.0-150 5.86 20
Isopropylbenzene 0.125 0.141 0.136 113 109 72.0-127 3.61 20
p-Isopropyltoluene 0.125 0.109 0.103 87.2 82.4 72.0-133 5.66 20
2-Butanone (MEK)0.625 0.450 0.432 72.0 69.1 30.0-160 4.08 24
Methylene Chloride 0.125 0.135 0.140 108 112 68.0-123 3.64 20
4-Methyl-2-pentanone (MIBK)0.625 0.450 0.442 72.0 70.7 56.0-143 1.79 20
Methyl tert-butyl ether 0.125 0.129 0.134 103 107 66.0-132 3.80 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1776437
Volatile Organic Compounds (GC/MS) by Method 8260D L1431305-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3732044-1 11/18/21 08:59 • (LCSD) R3732044-3 11/18/21 12:53
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.125 0.0939 0.100 75.1 80.0 59.0-130 6.29 20
n-Propylbenzene 0.125 0.101 0.0953 80.8 76.2 74.0-126 5.81 20
Styrene 0.125 0.129 0.121 103 96.8 72.0-127 6.40 20
1,1,1,2-Tetrachloroethane 0.125 0.163 0.164 130 131 74.0-129 J4 J4 0.612 20
1,1,2,2-Tetrachloroethane 0.125 0.0986 0.0962 78.9 77.0 68.0-128 2.46 20
Tetrachloroethene 0.125 0.156 0.148 125 118 70.0-136 5.26 20
Toluene 0.125 0.137 0.128 110 102 75.0-121 6.79 20
1,1,2-Trichlorotrifluoroethane 0.125 0.147 0.150 118 120 61.0-139 2.02 20
1,2,3-Trichlorobenzene 0.125 0.112 0.120 89.6 96.0 59.0-139 6.90 20
1,2,4-Trichlorobenzene 0.125 0.140 0.149 112 119 62.0-137 6.23 20
1,1,1-Trichloroethane 0.125 0.156 0.159 125 127 69.0-126 J4 1.90 20
1,1,2-Trichloroethane 0.125 0.141 0.131 113 105 78.0-123 7.35 20
Trichloroethene 0.125 0.157 0.146 126 117 76.0-126 7.26 20
Trichlorofluoromethane 0.125 0.146 0.148 117 118 61.0-142 1.36 20
1,2,3-Trichloropropane 0.125 0.100 0.0944 80.0 75.5 67.0-129 5.76 20
1,2,3-Trimethylbenzene 0.125 0.106 0.105 84.8 84.0 74.0-124 0.948 20
1,2,4-Trimethylbenzene 0.125 0.111 0.106 88.8 84.8 70.0-126 4.61 20
1,3,5-Trimethylbenzene 0.125 0.105 0.0984 84.0 78.7 73.0-127 6.49 20
Vinyl chloride 0.125 0.130 0.133 104 106 63.0-134 2.28 20
Xylenes, Total 0.375 0.423 0.401 113 107 72.0-127 5.34 20
(S) Toluene-d8 102 103 75.0-131
(S) 4-Bromofluorobenzene 103 103 67.0-138
(S) 1,2-Dichloroethane-d4 88.6 90.8 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1777168
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1431305-02
Method Blank (MB)
(MB) R3732458-2 11/20/21 14:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00539 0.0333
Acenaphthylene U 0.00469 0.0333
Anthracene U 0.00593 0.0333
Benzidine U 0.0626 1.67
Benzo(a)anthracene U 0.00587 0.0333
Benzo(b)fluoranthene U 0.00621 0.0333
Benzo(k)fluoranthene U 0.00592 0.0333
Benzo(g,h,i)perylene U 0.00609 0.0333
Benzo(a)pyrene U 0.00619 0.0333
Bis(2-chlorethoxy)methane U 0.0100 0.333
Bis(2-chloroethyl)ether U 0.0110 0.333
2,2-oxybis(1-chloropropane)U 0.0144 0.333
4-Bromophenyl-phenylether U 0.0117 0.333
2-Chloronaphthalene U 0.00585 0.0333
4-Chlorophenyl-phenylether U 0.0116 0.333
Chrysene U 0.00662 0.0333
Dibenz(a,h)anthracene U 0.00923 0.0333
3,3-Dichlorobenzidine U 0.0123 0.333
2,4-Dinitrotoluene U 0.00955 0.333
2,6-Dinitrotoluene U 0.0109 0.333
Fluoranthene U 0.00601 0.0333
Fluorene U 0.00542 0.0333
Hexachlorobenzene U 0.0118 0.333
Hexachloro-1,3-butadiene U 0.0112 0.333
Hexachlorocyclopentadiene U 0.0175 0.333
Hexachloroethane U 0.0131 0.333
Indeno(1,2,3-cd)pyrene U 0.00941 0.0333
Isophorone U 0.0102 0.333
Naphthalene U 0.00836 0.0333
Nitrobenzene U 0.0116 0.333
n-Nitrosodimethylamine U 0.0494 0.333
n-Nitrosodiphenylamine U 0.0252 0.333
n-Nitrosodi-n-propylamine U 0.0111 0.333
Phenanthrene U 0.00661 0.0333
Benzylbutyl phthalate U 0.0104 0.333
Bis(2-ethylhexyl)phthalate U 0.0422 0.333
Di-n-butyl phthalate U 0.0114 0.333
Diethyl phthalate U 0.0110 0.333
Dimethyl phthalate U 0.0706 0.333
Di-n-octyl phthalate U 0.0225 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1777168
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1431305-02
Method Blank (MB)
(MB) R3732458-2 11/20/21 14:59
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Pyrene U 0.00648 0.0333
1,2,4-Trichlorobenzene U 0.0104 0.333
4-Chloro-3-methylphenol U 0.0108 0.333
2-Chlorophenol U 0.0110 0.333
2,4-Dichlorophenol U 0.00970 0.333
2,4-Dimethylphenol U 0.00870 0.333
4,6-Dinitro-2-methylphenol U 0.0755 0.333
2,4-Dinitrophenol U 0.0779 0.333
2-Nitrophenol U 0.0119 0.333
4-Nitrophenol U 0.0104 0.333
Pentachlorophenol U 0.00896 0.333
Phenol U 0.0134 0.333
2,4,6-Trichlorophenol U 0.0107 0.333
(S) Nitrobenzene-d5 54.4 10.0-122
(S) 2-Fluorobiphenyl 58.0 15.0-120
(S) p-Terphenyl-d14 67.0 10.0-120
(S) Phenol-d5 51.4 10.0-120
(S) 2-Fluorophenol 58.3 12.0-120
(S) 2,4,6-Tribromophenol 47.6 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3732458-1 11/20/21 14:38
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.345 51.8 38.0-120
Acenaphthylene 0.666 0.355 53.3 40.0-120
Anthracene 0.666 0.354 53.2 42.0-120
Benzidine 1.33 0.328 24.7 10.0-120
Benzo(a)anthracene 0.666 0.407 61.1 44.0-120
Benzo(b)fluoranthene 0.666 0.364 54.7 43.0-120
Benzo(k)fluoranthene 0.666 0.365 54.8 44.0-120
Benzo(g,h,i)perylene 0.666 0.409 61.4 43.0-120
Benzo(a)pyrene 0.666 0.366 55.0 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.288 43.2 20.0-120
Bis(2-chloroethyl)ether 0.666 0.386 58.0 16.0-120
2,2-Oxybis(1-Chloropropane)0.666 0.333 50.0 23.0-120
4-Bromophenyl-phenylether 0.666 0.369 55.4 40.0-120
2-Chloronaphthalene 0.666 0.350 52.6 35.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1777168
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1431305-02
Laboratory Control Sample (LCS)
(LCS) R3732458-1 11/20/21 14:38
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4-Chlorophenyl-phenylether 0.666 0.358 53.8 40.0-120
Chrysene 0.666 0.383 57.5 43.0-120
Dibenz(a,h)anthracene 0.666 0.413 62.0 44.0-120
3,3-Dichlorobenzidine 1.33 0.721 54.2 28.0-120
2,4-Dinitrotoluene 0.666 0.400 60.1 45.0-120
2,6-Dinitrotoluene 0.666 0.376 56.5 42.0-120
Fluoranthene 0.666 0.357 53.6 44.0-120
Fluorene 0.666 0.359 53.9 41.0-120
Hexachlorobenzene 0.666 0.360 54.1 39.0-120
Hexachloro-1,3-butadiene 0.666 0.294 44.1 15.0-120
Hexachlorocyclopentadiene 0.666 0.335 50.3 15.0-120
Hexachloroethane 0.666 0.332 49.8 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.405 60.8 45.0-120
Isophorone 0.666 0.304 45.6 23.0-120
Naphthalene 0.666 0.288 43.2 18.0-120
Nitrobenzene 0.666 0.294 44.1 17.0-120
n-Nitrosodimethylamine 0.666 0.288 43.2 10.0-125
n-Nitrosodiphenylamine 0.666 0.352 52.9 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.337 50.6 26.0-120
Phenanthrene 0.666 0.362 54.4 42.0-120
Benzylbutyl phthalate 0.666 0.415 62.3 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.439 65.9 41.0-120
Di-n-butyl phthalate 0.666 0.393 59.0 43.0-120
Diethyl phthalate 0.666 0.407 61.1 43.0-120
Dimethyl phthalate 0.666 0.382 57.4 43.0-120
Di-n-octyl phthalate 0.666 0.429 64.4 40.0-120
Pyrene 0.666 0.385 57.8 41.0-120
1,2,4-Trichlorobenzene 0.666 0.305 45.8 17.0-120
4-Chloro-3-methylphenol 0.666 0.288 43.2 28.0-120
2-Chlorophenol 0.666 0.348 52.3 28.0-120
2,4-Dichlorophenol 0.666 0.292 43.8 25.0-120
2,4-Dimethylphenol 0.666 0.289 43.4 15.0-120
4,6-Dinitro-2-methylphenol 0.666 0.374 56.2 16.0-120
2,4-Dinitrophenol 0.666 0.251 37.7 10.0-120
2-Nitrophenol 0.666 0.320 48.0 20.0-120
4-Nitrophenol 0.666 0.397 59.6 27.0-120
Pentachlorophenol 0.666 0.322 48.3 29.0-120
Phenol 0.666 0.313 47.0 28.0-120
2,4,6-Trichlorophenol 0.666 0.335 50.3 37.0-120
(S) Nitrobenzene-d5 47.4 10.0-122
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1777168
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1431305-02
Laboratory Control Sample (LCS)
(LCS) R3732458-1 11/20/21 14:38
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
(S) 2-Fluorobiphenyl 56.2 15.0-120
(S) p-Terphenyl-d14 61.9 10.0-120
(S) Phenol-d5 50.0 10.0-120
(S) 2-Fluorophenol 57.7 12.0-120
(S) 2,4,6-Tribromophenol 54.1 10.0-127
L1431305-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1431305-02 11/20/21 21:20 • (MS) R3732458-3 11/20/21 21:40 • (MSD) R3732458-4 11/20/21 22:00
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.809 ND 0.221 0.235 27.3 29.2 1 18.0-120 6.03 32
Acenaphthylene 0.809 ND 0.215 0.221 26.5 27.5 1 25.0-120 2.87 32
Anthracene 0.809 ND 0.220 0.225 27.2 28.0 1 22.0-120 2.25 29
Benzidine 1.62 ND ND ND 0.000 0.000 1 10.0-120 J6 J6 0.000 40
Benzo(a)anthracene 0.809 ND 0.245 0.249 30.2 30.9 1 25.0-120 1.52 29
Benzo(b)fluoranthene 0.809 ND 0.231 0.229 28.5 28.4 1 19.0-122 1.09 31
Benzo(k)fluoranthene 0.809 ND 0.217 0.219 26.9 27.2 1 23.0-120 0.573 30
Benzo(g,h,i)perylene 0.809 ND 0.194 0.184 23.9 22.8 1 10.0-120 5.30 33
Benzo(a)pyrene 0.809 ND 0.215 0.219 26.5 27.2 1 24.0-120 1.73 30
Bis(2-chlorethoxy)methane 0.809 ND ND ND 25.2 26.1 1 10.0-120 3.02 34
Bis(2-chloroethyl)ether 0.809 ND ND ND 24.7 26.4 1 10.0-120 6.06 40
2,2-Oxybis(1-Chloropropane)0.809 ND ND ND 28.9 29.5 1 10.0-120 1.59 40
4-Bromophenyl-phenylether 0.809 ND ND ND 30.4 30.3 1 27.0-120 1.02 30
2-Chloronaphthalene 0.809 ND 0.226 0.235 27.9 29.2 1 20.0-120 3.79 32
4-Chlorophenyl-phenylether 0.809 ND ND ND 29.9 30.7 1 24.0-120 2.04 29
Chrysene 0.809 ND 0.232 0.235 28.7 29.2 1 21.0-120 1.07 29
Dibenz(a,h)anthracene 0.809 ND 0.200 0.191 24.7 23.8 1 10.0-120 4.47 32
3,3-Dichlorobenzidine 1.62 ND ND ND 16.2 13.6 1 10.0-120 18.2 34
2,4-Dinitrotoluene 0.809 ND ND ND 30.7 32.1 1 30.0-120 3.94 31
2,6-Dinitrotoluene 0.809 ND ND ND 29.2 31.8 1 25.0-120 8.12 31
Fluoranthene 0.809 ND 0.224 0.237 27.6 29.5 1 18.0-126 5.96 32
Fluorene 0.809 ND 0.231 0.239 28.5 29.7 1 25.0-120 3.19 30
Hexachlorobenzene 0.809 ND ND ND 28.2 30.0 1 27.0-120 5.32 28
Hexachloro-1,3-butadiene 0.809 ND ND ND 27.9 27.5 1 10.0-120 2.23 38
Hexachlorocyclopentadiene 0.809 ND ND ND 13.1 11.3 1 10.0-120 15.4 40
Hexachloroethane 0.809 ND ND ND 29.0 26.7 1 10.0-120 8.89 40
Indeno(1,2,3-cd)pyrene 0.809 ND 0.205 0.192 25.3 23.9 1 10.0-120 6.29 32
Isophorone 0.809 ND ND ND 26.2 27.0 1 13.0-120 2.33 34
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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QUALITY CONTROL SUMMARYWG1777168
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1431305-02
L1431305-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1431305-02 11/20/21 21:20 • (MS) R3732458-3 11/20/21 21:40 • (MSD) R3732458-4 11/20/21 22:00
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Naphthalene 0.809 ND 0.206 0.206 25.5 25.6 1 10.0-120 0.000 35
Nitrobenzene 0.809 ND ND ND 25.0 26.1 1 10.0-120 3.64 36
n-Nitrosodimethylamine 0.809 ND ND ND 22.1 22.5 1 10.0-127 1.39 40
n-Nitrosodiphenylamine 0.809 ND ND ND 26.7 27.5 1 17.0-120 2.29 29
n-Nitrosodi-n-propylamine 0.809 ND ND ND 28.5 29.8 1 10.0-120 3.71 37
Phenanthrene 0.809 ND 0.229 0.235 28.2 29.2 1 17.0-120 2.70 31
Benzylbutyl phthalate 0.809 ND 0.445 ND 42.1 36.0 1 23.0-120 12.2 30
Bis(2-ethylhexyl)phthalate 0.809 1.03 0.967 0.962 0.000 0.000 1 17.0-126 J6 J6 0.518 30
Di-n-butyl phthalate 0.809 ND ND ND 28.5 29.2 1 30.0-120 J6 J6 1.36 29
Diethyl phthalate 0.809 ND ND ND 32.9 34.9 1 26.0-120 5.48 28
Dimethyl phthalate 0.809 ND ND ND 29.8 31.4 1 25.0-120 4.56 29
Di-n-octyl phthalate 0.809 ND ND ND 38.6 40.4 1 21.0-123 3.92 29
Pyrene 0.809 ND 0.235 0.246 29.0 30.6 1 16.0-121 4.68 32
1,2,4-Trichlorobenzene 0.809 ND ND ND 27.6 27.5 1 12.0-120 1.12 37
4-Chloro-3-methylphenol 0.809 ND ND ND 24.2 24.5 1 15.0-120 0.635 30
2-Chlorophenol 0.809 ND ND ND 27.3 28.6 1 15.0-120 3.88 37
2,4-Dichlorophenol 0.809 ND ND ND 25.3 24.5 1 20.0-120 3.73 31
2,4-Dimethylphenol 0.809 ND ND ND 21.5 19.7 1 10.0-120 9.02 33
4,6-Dinitro-2-methylphenol 0.809 ND ND ND 34.0 33.9 1 10.0-120 0.913 39
2,4-Dinitrophenol 0.809 ND ND ND 28.2 30.1 1 10.0-121 5.84 40
2-Nitrophenol 0.809 ND ND ND 28.9 29.5 1 12.0-120 1.59 39
4-Nitrophenol 0.809 ND ND ND 34.0 35.9 1 10.0-137 4.88 32
Pentachlorophenol 0.809 ND ND ND 24.5 25.3 1 10.0-160 2.48 31
Phenol 0.809 ND ND ND 24.5 22.7 1 12.0-120 8.52 38
2,4,6-Trichlorophenol 0.809 ND ND ND 25.8 25.8 1 19.0-120 0.601 32
(S) Nitrobenzene-d5 27.8 29.6 10.0-122
(S) 2-Fluorobiphenyl 31.2 32.6 15.0-120
(S) p-Terphenyl-d14 33.6 32.0 10.0-120
(S) Phenol-d5 26.5 24.8 10.0-120
(S) 2-Fluorophenol 30.6 30.9 12.0-120
(S) 2,4,6-Tribromophenol 29.3 30.7 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
C3 The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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Idaho TN00003 Ohio–VAP CL0069
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Indiana C-TN-01 Oregon TN200002
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Kansas E-10277 Rhode Island LAO00356
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ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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