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HomeMy WebLinkAbout020918 Terracon Limited Site InvestigationLIMITED SITE INVESTIGATION WWAY Building 615 North Front Street Wilmington, New Hanover County, North Carolina February 9, 2018 Terracon Project No. ES187011 Prepared for: Morris Multimedia, Inc. Savannah, Georgia Prepared by: Terracon Consultants, Inc. Savannah, Georgia Irerracon February 9, 2018 Morris Multimedia, Inc. 27 Abercorn Street Savannah, Georgia 31401 Attn: Mr. Jeffrey R. Samuels E: jsamuels@morrismultimedia.com Re: Limited Site Investigation WWAY Building 618 North Front Street Wilmington, New Hanover County, North Carolina Terracon Project No. ES187011 Dear Mr. Samuels: Terracon Consultants, Inc. (Terracon) has completed a Limited Site Investigation (LSI) for the above -referenced property. The purpose of our investigation was to assess soil and shallow groundwater conditions in areas of the subject property potentially impacted by historical on -site operations and historical operations on adjoining properties. We appreciate the opportunity to be of service to you on this project. If you have any questions regarding this report, please do not hesitate to contact us at your earliest convenience. Sincerely, Terracon Consultants, Inc. i Justi J. Johnson, PG Senior Geologist Stewart A. Dixon, PG Environmental Department Manager Terracon Consultants, Inc. 2201 Rowland Avenue Savannah, Georgia 31404 P (912) 629 4000 F (912) 629 4001 terracon comisavannah TABLE OF CONTENTS Section Page No. EXECUTIVE SUMMARY............................................................................................................................... i 1.0 INTRODUCTION..............................................................................................................................1 1.1 Site Description................................................................................................................... 1 1.2 Site Background.................................................................................................................. 1 1.3 Recognized Environmental Conditions............................................................................... 1 1.4 Scope of Work..................................................................................................................... 2 2.0 FIELD ACTIVITIES..........................................................................................................................3 2.1 Underground Utility Clearance............................................................................................ 3 2.2 Limited Geophysical Survey............................................................................................... 3 2.3 Soil Boring Advancement.................................................................................................... 3 2.4 Soil Sampling...................................................................................................................... 4 2.5 Hydrogeology......................................................................................................................5 2.6 Groundwater Sampling....................................................................................................... 5 2.7 Bore Hole Abandonment..................................................................................................... 6 3.0 DATA EVALUATION.......................................................................................................................6 3.1 Soil Analytical Results......................................................................................................... 6 3.1.1 VOCs...................................................................................................................... 7 3.1.2 SVOCs................................................................................................................... 7 3.1.3 RCRA Metals......................................................................................................... 8 3.1.4 PCBs...................................................................................................................... 8 3.2 Groundwater Analytical Results.......................................................................................... 8 3.2.1 VOCs...................................................................................................................... 8 3.2.2 SVOCs................................................................................................................... 9 3.2.3 PAHs...................................................................................................................... 9 3.2.4 RCRA Metals......................................................................................................... 9 4.0 CONCLUSIONS AND RECOMMENDATIONS.............................................................................10 4.1 Conclusions.......................................................................................................................10 4.2 Recommendations............................................................................................................ 11 5.0 LIMITATIONS................................................................................................................................ 12 5.1 Standard of Care............................................................................................................... 12 5.2 Additional Scope Limitations............................................................................................. 12 5.3 Reliance............................................................................................................................ 12 APPENDICES APPENDIX A FIGURES Figure 1 Figure 2 Figure 3 Figure 4 Figure 5 Figure 6 APPENDIX B TABLES Site Location Map Site Diagram Potentiometric Surface Map Shallow Soil Quality Map Deep Soil Quality Map Groundwater Quality Map Table 1: Groundwater Elevations Table 2: Summary of Soil Analytical Results Table 3: Summary of Groundwater Analytical Results APPENDIX C SOIL BORING LOGS / WELL CONSTRUCTION DETAILS APPENDIX D LABORATORY ANALYTICAL DATA Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 EXECUTIVE SUMMARY This Limited Site Investigation (LSI) Report was completed to document recent investigation activities completed at the WWAY Building property located at 615 North Front Street in the City of Wilmington, New Hanover County, North Carolina. The subject property consists of a 1.60-acre parcel (Parcel ID No. R04716-006-001) developed with a single -story commercial building, an emergency generator building, an asphalt paved parking lot, a television broadcast tower, and numerous satellite dishes. It should be recognized that details are not included or fully developed in this section, and the report must be read in its entirety for a comprehensive understanding of the items contained herein. Historical Use of the Property Based on a review of the historical information, the subject property was developed with a railcar maintenance and repair facility consisting of a foundry, blacksmith room, wood working room, machine shop, and offices from at least the 1880s until the 1950s. The existing WWAY television building was constructed on the subject property by 1973. Recognized Environmental Conditions Terracon Consultants, Inc. (Terracon) was provided with a copy of an Opinion of Cost for Brownfield Consulting and Requirements letter (dated January 8, 2018) prepared for the subject property by Atlantic Shores Environmental Services, Ltd. (ASE). According to the letter, ASE conducted a Phase I Environmental Site Assessment (ESA) for the subject property in December 2017 and identified the following recognized environmental conditions (RECs): A 3,000-gallon gasoline underground storage tank (UST) installed on the subject property on February 4, 1975, and closed in place by filling with concrete on April 30, 1994. A 250-gallon diesel fuel UST installed on the subject property on January 4, 1983, and removed from the ground on April 30, 1994. Closure sampling identified the presence of contamination in the subsurface soil. The UST release was granted closure with a deed restriction limiting the subject property to commercial use. The subject property was previously used as a railcar maintenance and repair facility, including a foundry and machine shop. Historical industrial operations on the northern and eastern adjacent properties have resulted in soil and groundwater contamination. The purpose of this LSI was to assess soil and shallow groundwater conditions in areas of the subject property potentially impacted by these RECs. A brief summary of our activities and findings is provided below. Responsive ■ Resourceful ■ Reliable Limited Site Investigation Irerracon 5 Carolan Street Savannah, Chatham County, Georgia June 26, 2017 Terracon Project No. ES177142 Field Activities Terracon advanced five direct push borings (SB-1 through SB-4 and TW-5) in areas of concern and collected shallow and deep soil samples for laboratory analysis. Soil samples were submitted to an independent, North Carolina certified laboratory for analysis of volatile organic compounds (VOCs), semi -volatile organic compounds (SVOCs), and Resource Conservation and Recovery Act (RCRA) metals. Soil samples collected from SB-1 through SB-3 were also analyzed for polychlorinated biphenyls (PCBs). Terracon installed five temporary wells (TW-1 through TW-5) in areas of concern to facilitate the collection of groundwater samples for laboratory analysis. Groundwater samples were submitted to an independent, North Carolina certified laboratory for analysis of VOCs, SVOCs, polycyclic aromatic hydrocarbons (PAHs), and RCRA metals. Shallow Soil Conditions Shallow soil (< 2 feet bgs) in the vicinity of the closed 3,000-gallon UST is impacted with arsenic, lead, and mercury at concentrations exceeding applicable North Carolina Department of Environmental Quality (NCDEQ) soil screening levels. Shallow soil in the vicinity of the former foundry and blacksmith room in the northeast corner of the subject property is impacted with arsenic, lead, mercury, naphthalene, and 1- methyl naphthalene at concentrations exceeding applicable NCDEQ soil screening levels. Shallow soil in the vicinity of the former machine shop and railcar repair shop in the southeast corner of the subject property is impacted with arsenic, lead, mercury, benz(a)anth race ne, benzo(a)pyrene, and benzo(b)fluoranthene at concentrations exceeding applicable NCDEQ soil screening levels. Deep Soil Conditions Deep soil (21 — 26 feet bgs) in the vicinity of the closed 3,000-gallon UST is impacted with benzo(a)pyrene, arsenic, and mercury at concentrations exceeding applicable NCDEQ soil screening levels. Deep soil (17 - 18 feet bgs) in the vicinity of the former foundry and blacksmith room in the northeast corner of the subject property is impacted with arsenic at concentrations exceeding the NCDEQ residential soil screening level. Groundwater Results Shallow groundwater downgradient of the closed 3,000-gallon UST is impacted with benz(a)anthracene, benzo(a)pyrene, and benzo(g,h,i)fluoranthene at concentrations exceeding applicable NCDEQ Groundwater Quality Standards. Responsive ■ Resourceful ■ Reliable ii Limited Site Investigation Irerracon 5 Carolan Street Savannah, Chatham County, Georgia June 26, 2017 Terracon Project No. ES177142 Shallow groundwater in the northern portion of the subject property and downgradient from the former on -site foundry and former off -site roundhouse is impacted with benz(a)anthracene at a concentration exceeding the applicable NCDEQ Groundwater Quality Standard. Conclusions and Recommendations The results of the LSI indicate that soil and groundwater on the subject property have been impacted by historical railroad operations and historical petroleum product release(s) from on -site UST(s). Based on these results, it is Terracon's opinion that the subject property is a suitable candidate for remediation and redevelopment as a residential property under North Carolina's Brownfield Program. The absence of significant VOC contamination in soil and groundwater suggests that soil vapor intrusion will not be an issue for the subject property. Therefore, a vapor barrier would not be necessary for future site structures. Prior to development, limited areas of shallow soil contamination on the subject property should be remediated through excavation and proper disposal at a subtitle D landfill. Deep soil contamination may remain in -place if it can be demonstrated that the contamination poses no unacceptable risk to people or the environment. The subject property may be redeveloped with existing groundwater contamination if all completed exposure pathways are eliminated for potential receptors. Completed exposure pathways for potential receptors can be identified and evaluated by conducting a thorough receptor survey. Potential receptors for contaminated groundwater include water supply wells, basements, underground utilities, and surface water bodies. It is recommended that the prospective purchaser discuss the possibility of removing the residential land use restriction from the subject property with both the NCDEQ UST Section and Brownfield Program. Under certain circumstances, the Brownfield Program land use restrictions may supersede those that have already been placed on the property. Responsive ■ Resourceful ■ Reliable iii LIMITED SITE INVESTIGATION WWAY Building 615 North Front Street Wilmington, New Hanover County, North Carolina Terracon Project No. ES187011 February 9, 2018 1.0 INTRODUCTION 1.1 Site Description A Limited Site Investigation (LSI) has been completed for the WWAY Building property located at 615 North Front Street in the City of Wilmington, New Hanover County, North Carolina (subject property). The site location is shown on reproduced portions of the 2016 Wilmington and Castle Hayne, North Carolina U.S. Geologic Survey (USGS) 7.5-minute series topographic maps presented on Figure 1 in Appendix A. The subject property consists of a 1.60-acre parcel (Parcel ID No. R04716-006-001) developed with a single -story commercial building, an emergency generator building, an asphalt paved parking lot, a television broadcast tower, and numerous satellite dishes. The commercial building is currently being used to house the WWAY television studio as well as general administration offices. A diagram of the subject property is shown on Figure 2 in Appendix A. 1.2 Site Background Based on a review of the historical information, the subject property was developed with a railcar maintenance and repair facility consisting of a foundry, blacksmith room, wood working room, machine shop, and offices from at least the 1880s until the 1950s. The existing WWAY television building was constructed on the subject property by 1973. 1.3 Recognized Environmental Conditions Terracon Consultants, Inc. (Terracon) was provided with a copy of an Opinion of Cost for Brownfield Consulting and Requirements letter (dated January 8, 2018) prepared for the subject property by Atlantic Shores Environmental Services, Ltd. (ASE). According to the letter, ASE conducted a Phase I Environmental Site Assessment (ESA) for the subject property in December 2017 and identified the following recognized environmental conditions (RECs): A 3,000-gallon gasoline underground storage tank (UST) was installed on the subject property on February 4, 1975. This UST was closed in place by filling with concrete on Responsive ■ Resourceful ■ Reliable Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 April 30, 1994. As part of closure activities, three soil samples were collected around the perimeter of the UST. Soil analytical results did not indicate that a release had occurred from the UST. ASE recommended additional sampling to further evaluate soil and groundwater conditions in the vicinity of the UST. A 250-gallon diesel fuel UST was installed on the subject property on January 4, 1983. This UST was closed by removing from the ground on April 30, 1994. Closure sampling identified the presence of soil contamination exceeding residential and commercial/industrial maximum soil contaminant concentrations (MSCCs) at depths of 10 to 12 feet and 15 to 17 feet below the ground surface (bgs). Petroleum hydrocarbon compounds were not detected in the groundwater at levels exceeding the NCAC 2L Groundwater Standards. The UST release was granted closure with a Notice of Residual Petroleum deed restriction limiting the subject property to commercial use. The subject property was previously used as a railcar maintenance and repair facility, including a foundry and machine shop. Historical rail car repair activities may have impacted soil and groundwater with petroleum compounds, metals, chlorinated solvents, and polychlorinated biphenyls (PCBs). Historical industrial operations on the northern and eastern adjacent properties have resulted in soil and groundwater contamination. The northern adjacent property was previously occupied by Standard Oil Company and the eastern adjacent property was previously operated as an engine repair shop. It is unknown if the groundwater on the subject property has been impacted by contamination from the adjoining properties. The purpose of this LSI was to evaluate soil and shallow groundwater conditions in the vicinity of these RECs at the subject property. 1.4 Scope of Work Pursuant to the completion of the LSI, Terracon performed the following investigation activities to evaluate soil and shallow groundwater conditions on the subject property: Limited geophysical survey to clear underground utilities for proposed boring locations and attempt to identify the location of the closed 3,000-gallon UST; Advanced two soil borings (SB-4 and TW-5) and collected surface and subsurface soil samples in the vicinity of the closed 3,000-gallon UST; Installed and sampled one temporary monitoring well (TW-5) downgradient of the closed 3,000-gallon UST; Installed and sampled four temporary monitoring wells (TW-1 through TW-4) to evaluate shallow groundwater conditions along the eastern, northern, and northwestern boundaries of the subject property; and Responsive ■ Resourceful ■ Reliable 2 Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 Advanced three soil borings (SB-1 through S13-3) and collected surface and subsurface soil samples in the vicinity of the former railcar repair facility. The property configuration, soil boring locations, and temporary groundwater monitoring well locations associated with the LSI are shown on Figure 2 in Appendix A. 2.0 FIELD ACTIVITIES 2.1 Underground Utility Clearance Prior to conducting subsurface investigation activities, Terracon requested a public utility locate for the subject property through North Carolina 811. On January 19, 2018, North Carolina 811 issued utility ticket # A180162880 to cover the LSI boring locations. Terracon verified that all affected members had responded to the locate request before initiating any subsurface activities. 2.2 Limited Geophysical Survey Terracon contracted East Coast Underground, LLC (ECU) to locate and mark privately owned underground utilities in the vicinity of the proposed boring locations. On January 22, 2018, ECU used ground penetrating radar (GPR) and electromagnetic (EM) equipment to clear proposed boring locations of underground utilities. ECU also conducted a limited GPR survey to determine the location of the closed 3,000-gallon UST. The GPR survey identified a subsurface anomaly in the reported UST location to the south of the generator building. This subsurface anomaly is suspected to be the closed UST. The suspected UST area is depicted on Figure 2 in Appendix A. 2.3 Soil Boring Advancement Terracon personnel mobilized to the subject property on January 23, 2018, and advanced five soil borings (denoted as SB-1 through SB-4 and TW-5) throughout the subject property in order to evaluate potential impacts to the surface and subsurface soil. The boring locations were selected based on the subject property and surrounding area's topography, proximity to areas of concern, and site conditions encountered during the field work. Each boring location was initially advanced with a stainless steel hand auger to a depth of 5 feet below the ground surface (bgs) in order to verify underground utility clearance. Once cleared, each boring was advanced to a depths ranging from 20 to 30 feet bgs using a track -mounted GeoProbe° 6620DT direct push rig. Responsive ■ Resourceful ■ Reliable 3 Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 Downhole equipment and sampling utensils were decontaminated in general accordance to ASTM D 5088 - 15 "Decontamination of Field Equipment Used at Waste Sites". The downhole sampling equipment was cleaned using Alconox soap and water before arrival at the site, before introduction into the subsurface, between each sampling, between each borehole location, and before leaving the site. New disposable gloves were also utilized between each sample to minimize the possibility of cross contamination. 2.4 Soil Sampling While hand auguring to verify utility clearance, soil samples from ground surface to a depth of 5 feet bgs were collected at 1-foot intervals. From 5 feet to the total boring depth at each location, soils were retrieved by advancing a stainless steel sampling sleeve equipped with an inner 5-foot long, disposable sampling tube. Soil samples were collected at 2-foot intervals for screening purposes and further classification based on lithologic and/or saturated zone changes. Soil samples were placed in a sealed container upon removal from the boring. The soils were visually classified in general accordance with ASTM D-2488 - 09a "Standard Practice for Description and Identification of Soils (Visual -Manual Procedure)" and field -screened for volatile organic vapors with a MiniRaeTm 3000 Photo -Ionization Detector (PID) with a 10.6 eV lamp source. Soil boring logs including PID readings are attached in Appendix C. The soil samples exhibiting the highest PID readings from between 0 to 2 feet bgs and from 2 feet to observed saturated zones were submitted for laboratory analysis from each boring. If no elevated PID reading were observed within the boring, the samples were collected from the interval of most likely environmental impact above the saturated zone as determined in the field by the geologist. The soil samples selected for analysis were placed in laboratory prepared containers, labeled, and stored on ice in insulated coolers secured with custody seals. The sealed coolers were shipped overnight to the ALS Environmental laboratory (NELAC No. 527) in Jacksonville, Florida (ALS) for analysis. The ten soil samples were analyzed for the following parameters: Volatile Organic Compounds (VOCs) by USEPA Method 8260B Semi -volatile Organic Compounds (SVOCs) by USEPA Method 8270C Resource Conservation and Recovery Act (RCRA) Metals by USEPA Methods 6010D and 7471 B In addition, soil samples collected from borings SB-1, SB-2, and SB-3 were analyzed for PCBs by USEPA Method 8082. Responsive ■ Resourceful ■ Reliable 4 Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 2.5 Hydrogeology The lithology of the subsurface soils encountered at the subject property generally consisted of sands and silty sands. Saturated soil conditions were generally noted at depths ranging from approximately 13 to 29 feet bgs. Soil boring logs are provided in Appendix C. Water levels were collected from temporary wells on January 24, 2018, using a Solinst° water level meter accurate to within 0.01 foot. The water level indicator was field decontaminated with Alconox° detergent and distilled water between wells. Depth to groundwater measurements for the shallow surficial aquifer at the subject property ranged from 9.74 to 23.85 feet bgs. Depth to groundwater measurements and corresponding top of well casing elevations were used to calculate groundwater elevations. A summary of depth to groundwater measurements and groundwater elevation data is presented in Table 1 in Appendix B. A groundwater potentiometric surface map was prepared using the available elevation data to estimate groundwater flow direction for the surficial aquifer. The approximate direction of groundwater flow was drawn perpendicular to equipotential contours established from measured groundwater elevations. The general groundwater flow direction within the shallow surficial aquifer at the subject property is west towards the Cape Fear River. The groundwater potentiometric surface is depicted on Figure 3 of Appendix A. 2.6 Groundwater Sampling Five temporary monitoring wells (denoted as TW-1 through TW-5) were installed on the subject property in general accordance with procedures described in the US EPA Region 4, Science and Ecosystem Support Division guidance document titled Design and Installation of Monitoring Wells (SESDGUID-101-R1, effective date January 29, 2013). The wells were constructed using 1-inch diameter, Schedule 40 PVC riser and screen. Well construction details are presented on soil boring logs provided in Appendix C. The temporary monitoring wells were developed with a GeoTeche peristaltic pump and new disposable Teflon tubing to restore the natural hydraulic conductivity of the surficial aquifer. Following the completion of development activities, the temporary monitoring wells were purged and sampled in general accordance with the low -flow sampling protocol EPA Region 4, SESD Groundwater Sampling Operating Procedure (SESDPROC-301-R4), April 2017. The pump intake (Teflon tubing) was maintained within the mid -point of the submerged screened interval during the purging and sampling of the wells. Field water quality parameters, including pH, specific conductance, temperature, oxidation reduction potential (ORP), dissolved oxygen, and turbidity were monitored throughout the purging of the wells. Since the groundwater samples were to be submitted for analysis of RCRA metal concentrations, groundwater from each well was purged until a turbidity of less than 10 Nephelometric Turbidity Responsive ■ Resourceful ■ Reliable 5 Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 Units (NTUs) was achieved. This ensures that detected metal concentrations are representative of dissolved concentrations in the groundwater and not total concentrations associated with particulates in the water. However, a turbidity level less than 10 NTU could not be achieved for groundwater sample TW-5 despite extensive purging efforts. In order to evaluate for dissolved concentrations of RCRA metals, an additional sample container was collected from TW-5 for filtration prior to analysis. Following the stabilization of field parameters, laboratory -supplied containers were filled with groundwater. The groundwater samples were logged on the chain of custody and placed in an insulated cooler with ice. The sealed coolers were shipped overnight to ALS. The four groundwater samples were analyzed for the following parameters: VOCs by USEPA Method 8260B SVOCs by USEPA Method 8270C Polycyclic Aromatic Hydrocarbons (PAHs) by USEPA Method 8270D Selected Ion Monitoring (SIM) RCRA Metals by USEPA Methods 6010D and 7470A 2.7 Bore Hole Abandonment Following the completion of groundwater sampling activities, each temporary monitoring well was abandoned in general accordance with the procedures described in the US EPA Region 4, Science and Ecosystem Support Division guidance document titled Design and Installation of Monitoring Wells (SESDGUID-101-RI, dated January 29, 2013). The 1-inch diameter PVC casings and screens were removed and the bore holes filled from total depth to surface with hydrated bentonite. Bore holes located in paved areas of the subject property were also patched at the surface with asphalt. 3.0 DATA EVALUATION 3.1 Soil Analytical Results Soil analytical results were compared to the North Carolina Department of Environmental Quality (NCDEQ) Preliminary Soil Remediation Goals (PSRGs) for residential use and protection of groundwater. Shallow and deep soil quality maps showing the detected constituents are presented as Figures 4 and 5 in Appendix A, respectively. A summary of soil analytical results and the applicable regulatory standards is provided in Table 2 of Appendix B. Copies of the laboratory data sheets are included in Appendix D. Responsive ■ Resourceful ■ Reliable 6 Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 3.1.1 VOCs No VOCs were detected above NCDEQ PSRGs for residential soil or protection of groundwater. The following VOCs were detected at above laboratory reporting limits (RLs) in the soil samples submitted for analysis: Total xylenes were detected in soil samples S13-2-1, S13-2-12, and SB-3-1 at concentrations of 0.0154 micrograms per kilogram (mg/kg), 0.404 mg/kg, and 0.323 mg/kg, respectively. Acetone was detected above the laboratory RLs in all ten soil samples submitted for analysis. Acetone is known to be a common laboratory contaminant. No other VOCs were detected above laboratory RLs in the soil samples submitted for analysis. 3.1.2 SVOCs The following SVOCs were detected at concentrations exceeding applicable NCDEQ PSRGs: Benz(a)anth race ne was detected at a concentration of 1.48 mg/kg in shallow sample SB- 3-1, which exceeds both the residential PSRG (1.1 mg/kg) and protection of groundwater PSRG (0.35 mg/kg); Benzo(a)pyrene was detected in soil samples SB-3-1 and TW-5-25 at concentrations of 1.15 mg/kg and 0.809 mg/kg, respectively. These benzo(a)pyrene detections exceed both the residential PSRG (0.11 mg/kg) and protection of groundwater PSRG (0.12 mg/kg); Benzo(b)fluoranthene was detected at a concentration of 1.19 mg/kg in shallow sample SB-3-1, which exceeds the residential PSRG (1.1 mg/kg), but is below the protection of groundwater PSRG (1.2 mg/kg); Naphthalene was detected at a concentration of 0.428 mg/kg in shallow sample SB-1-1, which exceeds the protection of groundwater PSRG (0.39 mg/kg), but is below the residential PSRG (4.1 mg/kg); and 1-Methyl naphthalene was detected at a concentration of 0.365 mg/kg in shallow sample SB-1-1, which exceeds the protection of groundwater PSRG (0.11 mg/kg), but is below the residential PSRG (18 mg/kg). Various other SVOCs were detected at concentrations below applicable NCDEQ PSRGs in soil samples SB-1-1, SB-3-1, and TW-5-25. No SVOCs were detected above laboratory RLs in soil samples collected from borings S13-2 and SB-4. Responsive ■ Resourceful ■ Reliable 7 Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 3.1.3 RCRA Metals The following RCRA metals were detected at concentrations exceeding applicable NCDEQ PSRGs: Arsenic was detected at concentrations exceeding both the residential PSRG (0.68 mg/kg) and protection of groundwater PSRG (5.8 mg/kg) in samples SB-3-1 (6.87 mg/kg), SB-4- 21 (7.03 mg/kg), and TW-5-1 (12.1 mg/kg). In addition, arsenic was detected at concentrations exceeding the residential PSRG but below protection of groundwater PSRG in samples SB-1-1 (5.18 mg/kg), SB-1-17 (0.88 mg/kg), SB-4-1 (2.84 mg/kg), and TW-5-25 (2.08 mg/kg); Lead was detected at concentrations exceeding both the residential PSRG (400 mg/kg) and protection of groundwater PSRG (270 mg/kg) in shallow samples SB-3-1 (479 mg/kg) and TW-5-1 (1,350 mg/kg). In addition, lead was detected at a concentration exceeding the protection of groundwater PSRG but below residential PSRG in sample SB-1-1 (296 mg/kg); and Mercury was detected at a concentration exceeding both the residential PSRG (2.3 mg/kg) and protection of groundwater PSRG (1.0 mg/kg) in sample SB-3-1 (4.62 mg/kg). In addition, mercury was detected at concentrations exceeding the protection of groundwater PSRG but below the residential PSRG in samples SB-1-1 (1.17 mg/kg), SB-4-1 (1.04 mg/kg), and SB-4-21 (173 mg/kg). Various other RCRA metals were detected at concentrations below applicable NCDEQ PSRGs in the ten soil samples submitted for laboratory analysis. 3.1.4 PCBs No PCBs were detected above laboratory RLs in the six soil samples submitted for analysis. 3.2 Groundwater Analytical Results Groundwater analytical results were compared to NCDEQ Groundwater Quality Standards (NCAC 2L). A groundwater quality map showing the detected constituents is presented as Figure 6 in Appendix A. A summary of groundwater analytical results and the applicable regulatory standards is provided in Table 3 of Appendix B. Copies of the laboratory data sheets are included in Appendix D. 3.2.1 VOCs Acetone was detected in groundwater sample TW-3 at concentration of 14 micrograms per liter (pg/L), which is below the NCDEQ Groundwater Quality Standard of 6,000 pg/L. Responsive ■ Resourceful ■ Reliable 8 Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 No other VOCs were detected above laboratory RLs in the five groundwater samples submitted for analysis. 3.2.2 SVOCs 2,4-Dinitrophenol was detected in groundwater sample TW-3 at concentration of 4.24 pg/L. There is no NCDEQ Groundwater Quality Standard currently established for 2,4-dinitrophenol. No other SVOCs were detected above laboratory RLs in the five groundwater samples submitted for analysis. 3.2.3 PAHs The following PAHs were at concentrations exceeding NCDEQ Groundwater Quality Standards: Benz(a)anthracene was detected at concentrations of 0.0555 pg/L and 0.0695 pg/L in groundwater samples TW-1 and TW-5, respectively. These benz(a)anthracene detections exceed the NCDEQ Groundwater Quality Standard of 0.05 pg/L; Benzo(a)pyrene was detected at a concentration of 0.0682 pg/L in groundwater sample TW-5, which exceeds the NCDEQ Groundwater Quality Standard of 0.005 pg/L; and Benzo(b)fluoranthene was detected at a concentration of 0.0787 mg/kg in groundwater sample TW-5, which exceeds the NCDEQ Groundwater Quality Standard of 0.05 pg/L. Various other PAHs were detected at concentrations below applicable NCDEQ Groundwater Quality Standards in samples TW-1, TW-3, and TW-5. No PAHs were detected above laboratory RLs in groundwater samples TW-2 and TW-4. 3.2.4 RCRA Metals The following RCRA metals were detected at concentrations exceeding NCDEQ Groundwater Quality Standards in groundwater sample TW-3: Total arsenic was detected at a concentration of 19 pg/L, exceeding the NCDEQ Groundwater Quality Standard of 10 pg/L. However, dissolved arsenic was detected at a concentration of 4 pg/L, which is below the NCDEQ Groundwater Quality Standard; Total chromium was detected at a concentration of 56 pg/L, exceeding the NCDEQ Groundwater Quality Standard of 10 pg/L. However, dissolved chromium was not detected above the laboratory RL; and Responsive ■ Resourceful ■ Reliable 9 Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 Total lead was detected at a concentration of 39 pg/L, exceeding the NCDEQ Groundwater Quality Standard of 15 pg/L. However, dissolved lead was not detected above the laboratory RL. Various other total RCRA metals were detected at concentrations below applicable NCDEQ Groundwater Quality Standards in the five groundwater samples submitted for laboratory analysis. 4.0 CONCLUSIONS AND RECOMMENDATIONS 4.1 Conclusions Terracon completed an LSI to evaluate potential impacts to the soils and shallow groundwater from the on -site and off -site RECs identified by ASE's 2017 Phase I ESA. The LSI results indicate that soil and groundwater on the subject property have been impacted by historical railroad operations and historical petroleum product release(s) from on -site UST(s). The following conclusions are based on the results of the LSI: Shallow soil (< 2 feet bgs) in the vicinity of the closed 3,000-gallon UST is impacted with arsenic, lead, and mercury at concentrations exceeding applicable NCDEQ soil screening levels. Shallow soil (< 2 feet bgs) in the vicinity of the former foundry and blacksmith room in the northeast corner of the subject property is impacted with arsenic, lead, mercury, naphthalene, and 1-methyl naphthalene at concentrations exceeding applicable NCDEQ soil screening levels. Shallow soil (< 2 feet bgs) in the vicinity of the former machine shop and railcar repair shop in the southeast corner of the subject property is impacted with arsenic, lead, mercury, benz(a)anthracene, benzo(a)pyrene, and benzo(b)fluoranthene at concentrations exceeding applicable NCDEQ soil screening levels. Deep soil (21 — 26 feet bgs) in the vicinity of the closed 3,000-gallon UST is impacted with benzo(a)pyrene, arsenic, and mercury at concentrations exceeding applicable NCDEQ soil screening levels. Deep soil (17 — 18 feet bgs) in the vicinity of the former foundry and blacksmith room in the northeast corner of the subject property is impacted with arsenic at concentrations exceeding the NCDEQ residential soil screening level. Shallow groundwater downgradient of the closed 3,000-gallon UST is impacted with benz(a)anthracene, benzo(a)pyrene, and benzo(g,h,i)fluoranthene at concentrations exceeding applicable NCDEQ Groundwater Quality Standards. Responsive ■ Resourceful ■ Reliable 10 Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 Shallow groundwater in the northern portion of the subject property and downgradient from the former on -site foundry and former off -site roundhouse is impacted with benz(a)anth race ne at a concentration exceeding the applicable NCDEQ Groundwater Quality Standard. Total arsenic, chromium, and lead were detected at concentrations exceeding applicable NCDEQ Groundwater Quality Standards in the groundwater sample collected from the northwest corner of the subject property (TW-3). However, this groundwater sample exhibited high turbidity (748 NTU), which can result in elevated total metals concentrations. Analytical results for this sample following filtration indicated that dissolved arsenic, chromium, and lead were either not detected or below the applicable NCDEQ Groundwater Quality Standards. Based on these results, the metals exceedances detected in the unfiltered sample are attributed to the elevated turbidity of the sample and not representative of the actual dissolved metals concentrations in the groundwater in the vicinity of TW-3. 4.2 Recommendations Based on the findings of the LSI, it is Terracon's opinion that the subject property is a suitable candidate for remediation and redevelopment as a residential property under North Carolina's Brownfield Program. The absence of significant VOC contamination in soil and groundwater suggests that soil vapor intrusion will not be an issue for the subject property. Therefore, a vapor barrier would not be necessary for future site structures. Prior to development, limited areas of shallow soil contamination on the subject property should be remediated through excavation and proper disposal at a subtitle D landfill. Deep soil contamination may remain in -place if it can be demonstrated that the contamination poses no unacceptable risk to people or the environment. The subject property may be redeveloped with existing groundwater contamination if all completed exposure pathways are eliminated for potential receptors. Completed exposure pathways for potential receptors can be identified and evaluated by conducting a thorough receptor survey. Potential receptors for contaminated groundwater include water supply wells, basements, underground utilities, and surface water bodies. It is recommended that the prospective purchaser discuss the possibility of removing the residential land use restriction from the subject property with both the NCDEQ UST Section and Brownfield Program. Under certain circumstances, the Brownfield Program land use restrictions may supersede those that have already been placed on the property. Responsive ■ Resourceful ■ Reliable 11 Limited Site Investigation Irerracon WWAY Building ■ Wilmington, New Hanover County, North Carolina February 9, 2018 ■ Terracon Project No. ES187011 5.0 LIMITATIONS 5.1 Standard of Care Terracon's services were performed in a manner consistent with generally accepted practices of the profession undertaken in similar studies in the same geographical area during the same time period. Terracon makes no warranties, either express or implied, regarding the findings, conclusions or recommendations. Please note that Terracon does not warrant the work of laboratories, regulatory agencies or other third parties supplying information used in the preparation of the report. These environmental services were performed in accordance with the scope of work agreed with you, our client, and were not bound by ASTM E1903-97. 5.2 Additional Scope Limitations Findings, conclusions, and recommendations resulting from these services are based upon information derived from the on -site activities and other services performed under this scope of work; such information may be subject to change over time. Certain indicators of the presence of hazardous substances, petroleum products, or other constituents may have been latent, inaccessible, unobservable, non -detectable or not present during these services, and we cannot represent that the subject property contains no hazardous substances, toxic materials, petroleum products, or other latent conditions beyond those identified during this investigation. Subsurface conditions may vary from those encountered at specific borings or wells or during other surveys, tests, assessments, investigations or exploratory services. Sample locations and analytical test methods were limited. The data, interpretations, findings, and our recommendations are based solely upon data obtained at the time and within the agreed upon scope of services. Neither a vapor encroachment assessment nor a methane gas assessment was proposed or conducted as part of this limited subsurface investigation. 5.3 Reliance This report has been prepared for the exclusive use of Morris Multimedia, Inc. (the Client). Any authorization for use or reliance by any other party (except a governmental entity having jurisdiction over the subject property) is prohibited without the express written authorization of the Client and Terracon Consultants, Inc. Any unauthorized distribution or reuse is at the client's sole risk. Notwithstanding the foregoing, reliance by authorized parties will be subject to the terms, conditions and limitations stated in the proposal, this report, and the Agreement for Services between Terracon and the Client. Responsive ■ Resourceful ■ Reliable 12 APPENDIX A FIGURES EXPLANATION Q Subject Site Note: Base map was taken from portions of the 2016 Wilmington and Castle Hayne, North Carolina U.S. Geologic Survey 7.5-minute series topographic quadrangle maps. Contour interval is ten feet. � Q O O' .�/ _ °Q 421 o D - 17 U 4`� Muddy "` -� - 74 Poi +� Peter -\oint z 133 44- 0 1,000' 2,000' 1" = 2,000' SCALE IN FEET BRUNSWICK ST�1, a � � -i ti 2 N a Bus tv ,�Ii etl/I S�r��'��� A �f r ..�►� PAWA r :1 ON EXPLANATION SUBJECT PARCEL BOUNDARY ---- ADJACENT PARCEL BOUNDARY SUSPECTED UST AREA SOIL SAMPLE LOCATION ® GROUNDWATER SAMPLE LOCATION SOIL AND GROUNDWATER SAMPLE LOCATION Note: Map elements were graphically estimated from Gi Hanover County tax maps, and on -site obser approximate. Not intended for construction purposes. iq �I 1 I C ADJACENT PARCEL Owner: City of Wilmington I PIN: R04716-001-011-000 1 t4.3 acres I V m I I r I I P 1 ESTELLE LEE DRIVE I `\ I \� I I 0 40' 80' 1"=80' SCALE IN FEET 1 �r 1 1 I N I I I I I 1 1 x ADJACENT PARCEL I I y , I 4tc tW Owner: NRMH Hotel Holdings LLC PIN: R04716-005-001-000 ,1 I t1.27 acres _ -- T-1 SB-1 1 I I 1 1 ® TW-2 1 �y I TW_3 l�i11 1 1 1 1 I I 1 1 1 1 I � 1 Z 1 o I I. SUBJECT PARCEL I 1 Owner: WWAY TV LLC = IN R04716-006-001-000 ; -n 1 ±1.60 acres 7J 1 I O 1 fn 1 t II rn se s m m 1 1 1 TW-4 I I ® 1 1 1 1 TVV 5 1 1 SB-4 11 I 1 1 I I — 1 ADJACENTPARCEL Owner: Cape Fear Community College 1 PIN: R04716-006-004-000 t1.2 acres Project Mngr. Project No. JJJ ES187011 SITE DIAGRAM Figure Drawn By: Scale: Irerracon VMG 1" = 80' WWAY Building Checked By: JJJ File Name: ES187011.dwg Consulting Engineers & Scientists 615 North Front Street /'� Approved By: SAD Date: February 8, 2018 z201 Rowland Avenue Savannah, Georgia 30 Phone Fax. 4001 Wilmington, New Hanover County, North Carolina L lslzjszsa000 lslz>szs EXPLANATION SUBJECT PARCEL BOUNDARY ---- ADJACENT PARCEL BOUNDARY SUSPECTED UST AREA u (10.83) SOIL SAMPLE LOCATION GROUNDWATER SAMPLE LOCATION SOIL AND GROUNDWATER SAMPLE LOCATION GROUNDWATER ELEVATION CONTOUR GROUNDWATER FLOW DIRECTION RELATIVE GROUNDWATER ELEVATION (FEET) Note: Static groundwater level measurements collected on January 24, 2018. Relative groundwater elevations calculated based on benchmark of 30 feet. Map elements were graphically estimated from Google Earth aerial imagery, Hanover County tax maps, and on -site observations. Parcel boundaries approximate. Not intended for construction purposes. � � r I I I 1 I 1 1 I T\ I (8 t. 1 I 1 I C I � 1 � I m II I I r. I ESTELLE LEE DRIVE I l 0 40' 80' 1"=80' SCALE IN FEET / SB-1 � 1 T�WWjy-2 A(117.16) t I'] Project Mngr. Project No. JJJ ES187011 9 POTENTIOM ETRIC SURFACE MAP Figure Drawn By: Scale: rerraco� VMG I..= 80' 1 WWAY Building Checked By: JJJ File Name: ES187011.dwg Consulting Engineers & Scientists 615 North Front Street3( /'� Approved By: SAD Date: February 8, 2018 Rowland Avenue Savannah, 301 Wilmington, New Hanover County, North Carolina Phone 912)62940Georgia Pnona szs a000 Fax. a001 ist2j (912)629 FXPI ANIATIC)NI i ---- SUBJECT PARCEL BOUNDARY ---- ADJACENT PARCEL BOUNDARY SUSPECTED UST AREA SOIL SAMPLE LOCATION SOIL AND GROUNDWATER SAMPLE LOCATION rv-t BORING ID '-9'flbgs SAMPLE DEPTH Benzene 143 Emyibe�:ene 60 so SAMPLE RESULTS iotai Xylenes 13. Note: Map elements were graphically estimated from Google Earth aerial imagery. New Hanover County tax maps and on -site observations. Site boundary is approximate. Not intended for construction purposes. Soil concentrations are presented in milligrams per kilogram (mg/kg) BGS = Below Ground Surface BRL = Below Reporting Limits SVOCs = Semi -volatile organic compounds PCBs = Polychlorinated biphenyls NCDEQ = North Carolina Department of Environmental Quality PSRG = Preliminary Soil Remediation Goals based on the June 2017 USEPA Regional Screening Levels PURPLE = Analytical detection exceeds NCDEQ PSRG for residential soil BLUE = Analytical detection exceeds NCDEQ PSRG for protection of groundwater RED = Analytical detection exceeds NCDEQ PSRGs for residential soil and protection of groundwater I . 1 1 I I 1 TW51 I I 1.0'-2.0'ft11s SVOCs BRL 1 Acetone 0.0365 1 1 Arsenic 12.1 I I - - Barium 273 I C Cadmium 0.54 1 Chromium 11.2 r 1 Lead 1,350 1 IN I Mercury 0.370 I A Selenium 2.4 k I 1 _ 1 1 I I 1 I 1 SB-4-1 1.0'- 2.0'ft bgs I SVOCs BRL Acetone 0.127 1 Arsenic 2.84 1 Barium 30.8 I ■ - Cadmium 0.13 Chromium 4.57 Lead 128 I Mercury 1.04 PP I Selenium 0.35 I Silver 0.09 , 1 ESTELLE LEE DRIVE 1 � \ I N 1 0 40' 80' 1"=80' SCALE IN FEET ■I HANOVER STREET 'l SB-1 1 1 I 1 it 1 �5 I A I L19 J :11 SB-1-1 1.0'- 2.0'ft bgs PCBs BRL Acetone 0.0661 1-Methylnaphthalene 0.365 2-Methylnaphthalene 0.493 Acetophenone 0.0529 Anthracene 0.418 Benz(a)anthracene 0.123 Benzo(a)pyrene 0.0934 Benzo(b)fluoranthene 0.113 Benzo(g,h,i)perylene 0.0835 Benzo(k)fluoranthene 0.0722 Chrysene 0.232 Dibenzofuran 0.114 Fluoranthene 0.151 Indeno(1,2,3-cd)pyrene 0.0558 Naphthalene 0.428 Phenanthrene 0.425 Pyrene 0.181 Arsenic 5.18 Barium 72.2 Cadmium 0.16 Chromium 6.81 Lead 296 Mercury 1.17 Selenium 0.51 Silver 0.23 SB-2 � r L I A SB-2-1 . F = 1 1.0'- 2.0'ft bgs SVOCs BRL 0 PCBs BRL I 1 Acetone 0.0584 Total Xylenes 0.0154 1 Barium 1.04 _ 1 Chromium 0.60 Y SB-3 m Lead 1.43 I Mercury 0.0072 1 I Selenium 0.15 I ti . 1 \ 1 SB-3-1 \\\ 1 1.0'- 2.0'ft bgs PCBs BRL Acetone 0.106 ® 5 Total Xylenes .323 1 Benz(a)anthracene .48 1 Benzo(a)pyrene 1.15 1 SB-4 11 Benzo(b)fluoranthene 1.19 (1 Benzo(g,h,i)perylene 0.684 Benzo(k)fluoranthene 1.15 I I Chrysene 1.67 Fluoranthene 2.73 � 1 1 1 1 Indeno(1,2,3-cd)pyrene 0.652 Phenanthrene 1.37 Pyrene 2.44 I Arsenic 6.87 1 Barium 79.6 1 Cadmium 0.34 1 Chromium 8.17 Lead 479 , Mercury 4.62 Selenium 0.49 1� � 1 F I Silver 0.12 L r I Project Mngr. Project No. JJJ ES187011 9 SHALLOW SOIL QUALITY MAP Figure Drawn By: Scale: rerrac0� VMG 1" = 80' 1 WWAY Building Checked By: JJJ File Name: ES187011.dwg Consulting Engineers & Scientists 615 North Front Street A Approved By: SAD Date: February 8, 2018 zho1 Rowland Avenue Savannah, Georgia 0 Phone Fax. 4001 Wilmington, New Hanover County, North Carolina 4 (s1z)szsa000 (siz)szs EXPLANATION SUBJECT PARCEL BOUNDARY ---- ADJACENT PARCEL BOUNDARY SUSPECTED UST AREA SOIL SAMPLE LOCATION SOIL AND GROUNDWATER SAMPLE LOCATION Tw-t BORING ID B'-9'flbgs SAMPLE DEPTH Benzene 1.A3 Emyibenzene so SAMPLE RESULTS Total Xyienes 13.0 Note: Map elements were graphically estimated from Google Earth aerial imagery. New Hanover County tax maps and on -site observations. Site boundary is approximate. Not intended for construction purposes. Soil concentrations are presented in milligrams per kilogram (mg/kg) BGS = Below Ground Surface BRL = Below Reporting Limits SVOCs = Semi -volatile organic compounds PCBs = Polychlorinated biphenyls NCDEQ = North Carolina Department of Environmental Quality PSRG = Preliminary Soil Remediation Goals based on the June 2017 USEPA Regional Screening Levels PURPLE = Analytical detection exceeds NCDEQ PSRG for residential soil BLUE = Analytical detection exceeds NCDEQ PSRG for protection of groundwater RED = Analytical detection exceeds NCDEQ PSRGs for residential soil and protection of groundwater I HANOVER STREET I I I I I I SB-1 1 I 1 } y I II 1 1 r I TW-5-25 1 = SB-2 25.07-26.0'ftbgs Acetone 0.0851 { _ Acenaphthylene 1.03 k Benzo(a)pyrene 0.809 1 Benzo(b)fluoranthene 0.498 1 Benzo(g,h,i)perylene 0.652 I`9 i ' Indeno(1,2,3-cd)pyrene Arsenic 0.611 2.08 hl m , 1 if - - Barium 7.79 * 1 I I 1 1 I 1 1 I Cadmium 0.04 1 • I SB-3 Chromium 3.35 � I Lead 6.16 Mercury 0.0276 Silver 0.40 1 1 S I I k--, SB-4-21 21.0'-22.0'ftb9 5s SVOCS BRL Acetone 0.0663 Arsenic 7.03 Barium 40.2 Cadmium 0.12 Chromium 6.28 Lead 235 Mercury 1.73 Silver 0.31 ESTELLE LEE DRIVE 0 40' 80' 1"=80' SCALE IN FEET WWI SB-1-17 17.0'-18.0'ft bgs SVOCS BRL PCBs BRL Acetone 0.0109 Arsenic 0.88 Barium 12.6 Chromium 1.95 Lead 64.1 Mercury 0.160 f SB-2-12 12.0'-13.0'ftbgs SVOCs BRL PCBs BRL Acetone 0.0466 Total Xylenes 0.404 Arsenic 0.27 Barium 7.92 Chromium 3.31 Lead 2.31 Mercury 0.0061 SB-3-14 14.0'-15.0'ftbgs SVOCs BRL PCBs BRL Acetone 0.0368 Arsenic 0.27 Barium 2.40 '•,"--� Chromium 5.18 r� Lead 1.32 Mercury 0.0090 Project Mngr. Project No. JJJ ES187011 9 DEEP SOIL QUALITY MAP Figure Drawn By: Scale: rerra�o VMG 1" = 80' 1 WWAY Building Checked By: JJJ File Name: ES187011.dwg Consulting Engineers & Scientists 615 North Front Street Approved By: SAD Date: February 8, 2018 Rowland Avenue Savannah, Georgia 0 Phone 4001 hone(s1z)szsa000 Fax. Wilmington, New Hanover County, North Carolina (siz)szs FXPI ANIATIC)NI -- SUBJECT PARCEL BOUNDARY ---- ADJACENT PARCEL BOUNDARY [= SUSPECTED UST AREA ® GROUNDWATER SAMPLE LOCATION KI WELL ID SAMPLE RESULTS Note: Map elements were graphically estimated from Google Earth aerial imagery. New Hanover County tax maps and on -site observations. Site boundary is approximate. Not intended for construction purposes. Groundwater concentrations are presented in micrograms per liter (pg/L) BRL = Below Reporting Limits VOCs = Volatile organic compounds SVOCs = Semi -volatile organic compounds PAHs = Polycyclic aromatic hydrocarbons NCDEQ = North Carolina Department of Environmental Quality RED = Analytical detection exceeds the NCDEQ Groundwater Quality Standard (15A NCAC 02L .0202) I II I II I _ d• HANOVER STREET TW-1 1 I I1 I I 1 ` TWW 2 I TW-3 TW-3 1 I 1/24/2018 Acetone 14 I 2,4-Dinitrophenol 4.24 1-Methylnaphthalene 0.0488� 1 Total Arsenic 19 _ 1 Dissolved Arsenic 4 1 _ r . Total Barium 57 Total Chromium 56 I k 11 1 Dissolved Chromium <0.4 Total Lead 39 1 I Dissolved Lead <3 I ` r Total Mercury 0.11 Z qq yy � 1 �• I I I m .. 1 w TW-5 1 1/24/2018 1 1 TW-4 I 1 lid I� I I II II 1I Z O A S -n 70 O Z U) VOCs BRL 7 - SVOCS BRL �. Acenaphthylene 0.0652 . - Anthracene 0.0401 - Benz(a)anthracene 0.0695 1 TW_5 Benzo(a)pyrene 0.0682 I r, Benzo(b)fluoranthene 0.0787 Benzo(g,h,i)perylene 0.0536 ;+y Chrysene 0.0277 - Indeno(1,2,3-cd)pyrene 0,0453 11 ato Phenanthrene 0.0715yrene 00922tal Barium 54otalChromium 3otal Lead 6otal Mercury 0.12 1otal Selenium 4 I ESTELLE LEE DRIVE 1 II 1 1 1 1 0 40' 80' 1"=80' SCALE IN FEET `N� TW-1 1/24/2018 VOCs BRL SVOCS BRL - - Benz(a)anthracene 0.0555 Chrysene 0.0241�. Phenanthrene 0.0363 Pyrene 0.0373 Total Barium 39 Total Chromium 2 Total Lead 8 I' Total Selenium 4 Total Silver 1 I I 1 TW-2 � 1/24/2018 VOCs BRL 1 SVOCS BRL PAHs BRL Total Barium 19 Total Chromium I 1 , TW-4 1/24/2018 j VOCs BRL SVOCS BRL PAHs BRL Total Barium 52 Total Selenium 8 I t I 1 Project Mngr. Project No. JJJ ES187011 9 GROUNDWATER QUALITY MAP Figure Drawn By: Scale: rerra�o VMG 1" = 80' 1 WWAY Building Checked By: JJJ File Name: ES187011.dwg Consulting Engineers & Scientists 615 North Front Street Approved By: SAD Date: February 8, 2018 2201 Rowland Avenue Savannah, Georgia 0 Phone Fax(siz)szs4001 Wilmington, New Hanover County, North Carolina (s1z)szsa000 APPENDIX B TABLES WWAY Building 615 North Front Street Wilmington, New Hanover County, North Carolina Terracon Project No. ES187011 TABLE 1: GROUNDWATER ELEVATIONS Top of Casing Depth of Screened Groundwater Well Date Depth to Water Elevation Interval Elevation Number Measured (ft btoc) (ft) (range in ft btoc) (ft) TW-1 1/24/2018 28.85 17 - 22 18.02 10.83 TW-2 1/24/2018 30.00 12 - 17 12.84 17.16 TW-3 1/24/2018 27.25 19 - 24 18.45 8.80 TW-4 1/24/2018 32.79 17 - 22 18.31 14.48 TW-5 1/24/2018 29.19 25 - 30 24.05 5.14 NOTES: All monitoring well top of casings surveyed on January 23, 2018 Relative top of casing and groundwater elevations calculated based on benchmark of 30.00 feet WWAY Building 615 North Front Street Wilmington, New Hanover County, North Carolina Terracon Project No. ES187011 TABLE 2: SUMMARY OF SOIL ANALYTICAL RESULTS Compound P NCDEQ Residential (mg/kg) NCDEQ Protection of Groundwater PSRG (mg/kg) SB-1-1 1.0-2.0ftb s g (mg/kg) SB-1-17 17.0-18.0ftb s g (mg/kg) SB-2-1 1.0-2.0ftb s g (mg/kg) SB-2-12 12.0-13.0ftb s g (mg/kg) SB-3-1 1.0-2.0ftb s g (mg/kg) SB-3-14 14.0-15.0ftb s g (mg/kg) SB-4-1 1.0-2.0ftb s g (mg/kg) SB-4-21 21.0-22.0ftb s g (mg/kg) TW-5-1 1.0-2.0ftb s g (mg/kg) TW-5-25 25.0-26.0ftbs g (mg/kg) Volatile Organic Compounds (VOCs) - USEPA Method 8260E Acetone 12,000 25 0.0661 0.0109 0.0584 0.0466 0.106 0.0368 0.127 0.0663 0.0365 0.0851 Total Xylenes 120 9.9 <0.370 <0.423 0.0154 0.404 0.323 <0.420 <0.485 <0.418 <0.870 <0.339 Semi -Volatile Organic Compounds (SVOCs) - USEPA Method 8270C 1-Methyl naphthalene 18 0.11 0.365 <0.687 <0.066 <0.698 <0.77 <0.0677 <0.0872 <0.712 <11.6 <0.802 2-Methyl naphthalene 48 3.1 0.493 <0.614 <0.059 <0.624 <0.688 <0.0605 <0.0780 <0.637 <10.4 <0.717 Acenaphthylene ns 41 <0.0515 <0.490 <0.047 <0.497 <0.548 <0.0482 <0.0621 <0.507 <8.26 1.03 Acetophenone 1,600 4.3 0.0529 <0.479 <0.046 <0.486 <0.536 <0.0472 <0.0608 <0.497 <8.09 <0.559 Anthracene 3,600 1,300 0.418 <0.448 <0.043 <0.455 <0.502 <0.0441 <0.0568 <0.464 <7.56 <0.523 Benz(a)anthracene 1.1 0.35 0.123 <0.490 <0.047 <0.497 1.48 <0.0482 <0.0621 <0.507 <8.26 <0.571 Benzo(a)pyrene 0.11 0.12 0.0934 <0.386 <0.037 <0.391 1.15 <0.0380 <0.0489 <0.400 <6.5 0.809 Benzo(b)fluoranthene 1.1 1.2 0.113 <0.271 <0.026 <0.275 1.19 <0.0267 <0.0344 <0.281 <4.57 0.498 Benzo(g,h,i)perylene ns 15,600 0.0835 <0.542 <0.052 <0.550 0.684 <0.0534 <0.0687 <0.561 <9.14 0.652 Benzo(k)fluoranthene 11 12 0.0722 <0.614 <0.059 <0.624 1.15 <0.0605 <0.0780 <0.637 <10.4 <0.717 Chrysene 110 36 0.232 <0.469 <0.045 <0.476 1.67 <0.0462 <0.0595 <0.486 <7.91 <0.547 Dibenzofuran 15 10 0.114 <0.479 <0.046 <0.486 <0.536 <0.0472 <0.0608 <0.497 <8.09 <0.559 Fluoranthene 480 670 0.151 <0.500 <0.048 <0.508 2.73 <0.0493 <0.0634 <0.518 <8.44 <0.583 Indeno(1,2,3-cd)pyrene 1.1 3.9 0.0558 <0.427 <0.041 <0.434 0.652 <0.0421 <0.0542 <0.443 <7.21 0.611 Naphthalene 4.1 0.39 0.428 <0.510 <0.049 <0.518 <0.571 <0.0503 <0.0647 <0.529 <8.61 <0.595 Phenanthrene ns 15,600 0.425 <0.438 <0.042 <0.444 1.37 <0.0431 <0.0555 <0.454 <7.38 <0.510 Pyrene 1 360 1 440 0.181 <0.479 <0.046 <0.486 2.44 <0.0472 <0.0608 <0.497 <8.09 <0.559 Total RCRA 8 Metals - USEPA Methods 6010C & 7471B Arsenic 0.68 5.8 5.18 0.88 <0.07 0.27 6.87 0.27 2.84 7.03 12.1 2.08 Barium 3,100 580 72.2 12.6 1.04 7.92 79.6 2.40 30.8 40.2 273 7.79 Cadmium 7.5 3 0.16 <0.02 <0.02 <0.02 0.34 <0.02 0.13 0.12 0.54 0.04 Chromium 47' 360,000 6.81 1.95 0.60 3.20 8.17 5.18 4.57 6.28 11.2 3.35 Lead 400' 270 296 64.1 1.43 2.31 479 1.32 128 235 1,350 6.16 Mercury 2.3 1.0 1.17 0.160 10.0072 1 0.0061 4.62 10.0090 11.04 11.73 10.370 0.0276 Selenium 78 2 0.51 <0.14 0.15 <0.14 0.49 <0.14 0.35 <0.27 2.4 0.40 Silver 1 78 1 3 1 0.23 <0.04 <0.04 <0.04 0.12 <0.04 0.09 0.31 <0.2 <0.04 Notes: ft bgs = feet below ground surface < = laboratory analytical result is below laboratory reporting limit BLACK = analytical detection above the laboratory reporting limit NCDEQ = North Carolina Department of Environmental Quality PSRG = Preliminary Soil Remediation Goals based on the June 2017 USEPA Regional Screening Levels PURPLE = analytical detection exceeds NCDEQ PSRG for residential soil BLUE = analytical detection exceeds NCDEQ PSRG for protection of groundwater RED = analytical detection exceeds NCDEQ PSRGs for residential soil and protection of groundwater ns = residential PSRG has not been established for this analyte WWAY Building 615 North Front Street Wilmington, New Hanover County, North Carolina Terracon Project No. ES187011 rr_1-]4=&M--111�,IJi/_1:&ONKr]:Z411111ZI1]viV_1%0:4:7_1ZFTITWAI[O_1IIIIIIN*PJA&I Compound NCDEQ Groundwater Quality Standards (ug/L) TW-1 1/24/2018 (ug/L) TW-2 1/24/2018 (ug/L) TW-3 1/24/2018 (ug/L) TW-4 1/24/2018 (ug/L) TW-5 1/24/2018 (ug/L) Volatile Organic Compounds (VOCs) - USEPA Method 8260E Acetone 1 6,000 1 <5.6 <5.6 14 <5.6 <5.6 Semi -Volatile Organic Compounds (SVOCs) - USEPA Method 8270C 2,4-Dinitrophenol ns 1 <0.760 1 <0.760 4.24 <0.760 <0.760 Polycyclic Aromatic Hydrocarbons (PAHs) - USEPA Method 8270D SIM 1 -M ethyl naphthalene ns <0.0440 <0.0440 0.0488 <0.0440 <0.0440 Acenaphthylene 200 <0.0250 <0.0250 <0.0250 <0.0250 0.0652 Anthracene ns <0.0380 <0.0380 <0.0380 <0.0380 0.0401 Benz(a)anthracene 0.05 0.0555 <0.0350 <0.0350 <0.0350 0.0695 Benzo(a)pyrene 0.005 <0.0310 <0.0310 <0.0310 <0.0310 0.0682 Benzo(b)fluoranthene 0.05 <0.0250 <0.0250 <0.0250 <0.0250 0.0787 Benzo(g,h,i)perylene 200 <0.0390 <0.0390 <0.0390 <0.0390 0.0536 Chrysene 5 0.0241 <0.0240 <0.0240 <0.0240 0.0277 Indeno(1,2,3-cd)pyrene 0.05 <0.0400 <0.0400 <0.0400 <0.0400 0.0453 Phenanthrene 200 0.0363 <0.0350 <0.0350 <0.0350 0.0715 Pyrene 200 0.0373 <0.0310 <0.0310 <0.0310 0.0922 Total RCRA 8 Metals - USEPA Methods 6010D & 7470A Arsenic 10 <2 <2 19 <2 <2 Barium 700 39 19 57 52 54 Chromium 10 2 1 56 <0.4 3 Lead 15 8 <2 39 <2 6 Mercury 1 <0.05 <0.05 0.11 <0.05 0.12 Selenium 20 4 <3 <3 8 4 Silver 20 1 <0.6 <0.6 <0.6 <0.6 Dissolved RCRA 8 Metals - USEPA Method 6010D Arsenic 10 na na 4 na na Chromium 10 na na <0.4 na na Lead 15 na na <3 na na NOTES: pg/L = micrograms per liter < = laboratory analytical result is below laboratory reporting limit BLACK = analytical detection above the laboratory reporting limit RED = analytical detection exceeds the NCDEQ Groundwater Quality Standard (15A NCAC 02L .0202) ns = groundwater quality standard has not been established for this analyte na = not analyzed NCDEQ = North Carolina Department of Environmental Quality APPENDIX C SOIL BORING LOGS / WELL CONSTRUCTION DETAILS 0 U) 0 0 J 0 Fr 0 m 0 0 w Irerracon Soil Boring and Well Construction Log Page 1 of 1 Project: Project Number: Boring/Well: ES187011 SBA WWAY Building LSI Well Construction Data Date Started: Latitude: 1 /23/18 341434.54 Logged By: Longitude: EMS 775659.45 Drilling Co.: Driller: William Walker William Walker Method: Equipment: Direct Push Geoprobe 6620DT Boring Depth (ft.): Saturated Zone: Date: 22.0 -V 18.00 1 /23/2018 Boring Diameter (in : Static Water Level: Date: .25 0 E E a o Description U) U J 1 1.7 ASPHALT SILTY SAND (SM), Moist, medium dense, 85% fine to medium sand, 15% fines, trace *2* *1.7* gravel to 0.25", trace brick and asphalt debris, no odor, no staining, 10YR 3/1 Very Dark 2 Gray 2 3 1.7 4 0.0 4 4 5 0.0 SILTY SAND (SM), Moist, medium dense, 75%fine to medium sand, 15% fines, 10% 6 angular gravel to 0.5", brick and asphalt debris, no odor, no staining, 10YR 3/1 Very Dark 6 Gary 6 0.0 POORLY GRADED SAND(SP), Moist, medium dense, 95% fine to medium sand, 5% g fines, no odor, no staining, 10YR 5/3 Brown g 10 10 WELL GRADED SAND (SW), Moist, medium dense, 95% fine to coarse sand, 5% > gravel to 0.5", brick and asphalt debris, no odor, no staining, 10YR 4/3 Brown 12 12 7 0.0 POORLY GRADED SAND(SP), Moist, medium dense, 95% fine to medium sand, 5% 14 : fines, no odor, no staining, 10YR 4/3 Brown 14 > WELL GRADED SAND (SW), Moist, medium dense, 95% fine to coarse sand, 5% 16 gravel to 0.5", brick and asphalt debris, no odor, no staining, 10YR 3/1 Very Dark Gray 16 *9* *0.0* 8 0.0 18 18 SILTY SAND (SM),Wet, medium dense,80% fine to medium sand, 20% fines, no odor, no staining, 10YR 4/4 Dark Yellowish Brown 20 20 10 0.0 11 0.0 22 Borehole terminated at 22 feet 22 Terracon 2201 Rowland Avenue, Savannah, Georgia 31404 Phone: 912-629-4000, Fax: 912-629-4001 0 U) 0 0 0 z Fr 0 m 0 LU w a z w z 0 z w 0 a 0 a U) Irerracon Soil Boring and Well Construction Log Page 1 of 1 Project: WWAY Building LSI Project Number: ES187011 Boring/Well: SB-2 Well Construction Data Date Started: Latitude: 1 /23/18 311433.35 Logged By: EMS Longitude: 775659.28 Drilling Co.: Driller: William Walker William Walker Method: Equipment: Direct Push Geoprobe 6620DT Boring Depth (ft.): 20.0 -V Saturated Zone: 13.00 Date: 1 /23/2018 Boring Diameter (in : .25 Static Water Level: Date: 0 E U) E U a o J Description 1 0.0 ASPHALT POORLY GRADED SAND(SP), Moist, medium dense, 100% fine to medium sand, no *2* *0.0* odor, no staining, 10YR 5/2 Grayish Brown 2 2 3 0.0 4 0.0 4 4 5 0.0 6 6 6 0.0 8 8 10 10 12 *8* *0.0* 12 7 0.0 POORLY GRADED SAND(SP), Wet, medium dense, 100%fine to medium sand, 14 trace gravel to 0.25", no odor, no staining. 10YR 4/3 Brown 14 16 16 9 0.0 18 18 20 10 0.0 ADto medium sand, 5% POORLY GRADED SAND(SP), Wet, medium dense, 95% fine gravel to 0.25", no odor, no staining 10YR 4/3 Brown 20 Borehole terminated at 20 feet Terracon 2201 Rowland Avenue, Savannah, Georgia 31404 Phone: 912-629-4000, Fax: 912-629-4001 0 U) 0 0 0 Fr 0 m 0 LU w a z w Z 0 z w 0 a 0 a U) Irerracon Soil Boring and Well Construction Log Page 1 of 1 Project: Project Number: Boring/Well: ES187011 SB-3 WWAY Building LSI Well Construction Data Date Started: Latitude: 1 /23/18 341432.39 Logged By: Longitude: EMS 775659.17 Drilling Co.: Driller: William Walker William Walker Method: Equipment: Direct Push Geoprobe 6620DT Boring Depth (ft.): Saturated Zone: Date: 20.0 -V 15.00 1 /23/2018 Boring Diameter (in : Static Water Level: Date: .25 0 E E a o Description U) U J 1 0.0 ASPHALT SILTY SAND (SM), Moist, medium dense, 85% fine to medium sand, 15% fines, brick *2* *0.7* and asphalt debris, no odor, no staining, 10YR 5/2 Grayish Brown 2 2 3 0.7 4 0.0 4 4 5 0.0 POORLY GRADED SAND(SP), Moist, medium dense, 95% fine to medium sand, 5% g fines, no odor, no staining, 10YR 5/2 Grayish Brown g 6 0.0 8 8 10 POORLY GRADED SAND(SP), Moist, medium dense, 95%fine to medium sand, 5% 10 fines, brick and asphalt debris, no odor, no staining, 10YR 4/3 Brown 12 7 0.0 AD POORLY GRADED SAND(SP), Moist, medium dense, 100% fine to medium sand, 12 :: laminated, no odor, no staining, 10YR 4/3 Brown 14 *8* *0.0* 14 POORLY GRADED SAND(SP), Wet, medium dense, 100% fine to medium sand, no 16 odor, no staining, 10YR 4/4 Dark Yellowish Brown 16 9 0.0 18 18 10 0.0 20 Borehole terminated at 20 feet 20 Terracon 2201 Rowland Avenue, Savannah, Georgia 31404 Phone: 912-629-4000, Fax: 912-629-4001 a Z w Z 0 Z w 0 a 0 a U) Irerracon Soil Boring and Well Construction Log Page 1 of 1 Project: Project Number: Boring/Well: ES187011 SB-4 WWAY Building LSI Well Construction Data Date Started: Latitude: 1 /23/18 341431.5 Logged By: Longitude: EMS 77570.18 Drilling Co.: Driller: William Walker William Walker Method: Equipment: Direct Push Geoprobe 6620DT Boring Depth (ft.): Saturated Zone: Date: 25.0 _V 22.00 1 /23/2018 Boring Diameter (in : Static Water Level: Date: .25 - S a E E 0E a ° o Description a U) U J 1 0.0 ASPHALT *2* *0.0* SILTY SAND (SM), Moist, medium dense, 85% fine to medium sand, 15% fines, trace 2 gravel to 0.5", brick and asphalt debris, no odor, no staining, 10YR 3/1 Very Dark Gray 2 3 0.0 4 0.0 4 4 5 0.0 6 6 6 0.0 8 8 10 10 WELL GRADED SAND (SW), Moist, medium dense, 7 5 % fine to coarse sand, 2 0 % angular gravel to 1 ", 5% fines, brick and asphalt debris, no odor, no staining, 10YR 4/2 12 Dark Grayish Brown *Note: Wood Debris at 1'* 7 12 7 0.0 14 14 16 16 8 0.9 0o 18 18 POORLY GRADED SAND(SP), Moist, medium dense, 95% fines to medium sand, 5% fines, brick debris, no odor, no staining, 10YR 4/3 Brown 20 20 9 0.9 22 POORLY GRADED SAND(SP), Wet, medium dense, 95% fines to medium sand, 5% 22 X *10* *0.9* fines, trace wood debris, no odor, no staining, 10YR 4/3 Brown 24 POORLY GRADED SAND(SP), Wet, medium dense, 95%fines to medium sand, 5% 24 11 0.5 fines, no odor, no staining, 10YR 4/3 Brown Borehole terminated at 25 feet Terracon 2201 Rowland Avenue, Savannah, Georgia 31404 Phone: 912-629-4000, Fax: 912-629-4001 0 0 0 z W 0 m 0 w z w 2 z 0 z w 0 0 z Irerracon Soil Boring and Well Construction Log Page 1 of 1 Project: Project Number: Boring/Well: ES 187011 TW-1 WWAY Building LSI Well Construction Data Date Started: Latitude: Screen: 1/23/18 341434.8 0.010" slotted PVC ® From: 17 To: 22 Logged y: ongltu e: Pack: 0 EMS 775659.88 Clean 20/30 Filter Sand From: 25 To: 10 Drilling Co.: Driller: Seal: William Walker William Walker Hydrated Bentonite Chips From: 10 To: 9 Method: Equipment: Grout: Direct Push Geoprobe 6620DT N/A From: To: Boring Depth (ft.): Saturated Zone: Date: Inner Casing: 25.0 �-z 18.50 1/23/2018 1„ Threaded Schedule 40 PVC Boring Diameter (in : Static Water Level: Date: Notes: .25 18.02 1/24/2018 Stick-up height: 2.51 EE ao Description Well a) p M n a Detail p J 1 0.1 ASPHALT ? POORLY GRADED SAND(SP), Moist, medium dense, 95% fine to medium 2 2 0.0 sand, 5% fines, trace gravel to 0.25", trace brick and asphalt debris, no odor, no 2 3 0.0 staining, 10YR 4/3 Brown 4 0.1 4 4 5 0.1 6 POORLY GRADED SAND(SP), Moist, medium dense, 95—%—fine to medium 6 sand, 5% fines, trace gravel to 0.25", trace brick and asphalt debris, no odor, no $ 6 0.0 ': staining, 10YR 4/3 Brown $ 10 10 12 12 7 0.0 14 14 16 16 8 0.0 18 POORLY GRADED SAND(SP), Wet, medium dense, 100% fine to medium - 18 sand, no odor, no staining,10YR 5/2 Grayish Brown .•: ••• 20 ? ------y----------------- POORLY GRADED SAND(SP), Wet, medium dense, 95%fine to medium ,• 20 sand, 5% fines, no odor, no staining, 10YR 4/4 Dark Yellowish Brown 22 22 9 0.0 24 24 10 0.0 Borehole terminated at 25 feet Terracon 2201 Rowland Avenue, Savannah, Georgia 31404 Phone: 912-6294000, Fax 912-629-4001 a z w Z 0 z w 0 a 0 a U) Irerracon Soil Boring and Well Construction Log Page 1 of 1 Project: Project Number: Boring/Well: ES187011 TW-2 WWAY Building LSI Well Construction Data Date Started: Latitude: Screen: 1/23/18 341434.02 0.010" slotted PVC ® From: 12 To: 17 Logged By: Longitude: Pack: EMS 775659.15 Clean 20/30 Filter Sand From: 20 To: 5 Drilling Co.: Driller: Seal: William Walker William Walker Hydrated Bentonite Chips From: 5 To: 4 Method: Equipment: Grout: Direct Push Geoprobe 6620DT N/A From: To: Boring Depth (ft.): Saturated Zone: Date: Inner Casing: 20.0 -7 13.12 1/23/2018 1„ Threaded Schedule 40 PVC Boring Diameter (in : Static Water Level: Date: Notes: .25 T 12.84 1/24/2018 Stick-up height: 3.10' a oo of a Description Well a o Detail p U) U) J 1 0.0 :: POORLY GRADED SAND(SP), Moist, medium dense, 100% fine to medium sand, trace asphalt debris, no odor, no staining, 10YR 5/2 Grayish Brown 2 0.0 2 2 3 0.0 4 0.0 4 4 5 0.0 6 6 6 0.0 POORLY GRADED SAND(SP), Moist, medium dense, 100% fine to medium g sand, no odor, no staining, 10YR 5/2 Grayish Brown .• g 10 RLYAD POOGRED SAND(SP), Moist, m00% edium dense, 1fine to medium '. 10 sand, trace asphalt debris, no odor, no staining, 10YR 5/4 Yellowish Brown 12 12 7 0.0 POORLY GRADED SAND(SP), Wet, medium dense, 100% fine to medium - 14 : sand, no odor, no staining, 10YR 5/4 Yellowish Brown 14 POORLY GRADED SAND(SP), Wet, medium dense, 100% fine to medium 16 sand, no odor, no staining, 10YR 4/4 Dark Yellowish Brown • 16 8 0.0 18 18 9 0.0 20 Borehole terminated at 20 feet 20 Terracon 2201 Rowland Avenue, Savannah, Georgia 31404 Phone: 912-629-4000, Fax: 912-629-4001 0 0 0 z a 0 m 0 w z w 2 z 0 z w 0 0 z Irerracon Soil Boring and Well Construction Log Page 1 of 1 Project: Project Number: Boring/Well: ES 187011 TW-3 WWAY Building LSI Well Construction Data Date Started: Latitude: Screen: 1/23/18 341434.16 0.010" slotted PVC ® From: 18 To: 23 Logged y: ongltu e: Pack: 0 EMS 77570.7 Clean 20/30 Filter Sand From: 25 To: 8.5 Drilling Co.: Driller: Seal: William Walker William Walker Hydrated Bentonite Chips From: 8.5 To: 7.5 Method: Equipment: Grout: Direct Push Geoprobe 6620DT N/A From: To: Boring Depth (ft.): Saturated Zone: Date: Inner Casing: 25.0 �-z 18.98 1/23/2018 1„ Threaded Schedule 40 PVC Boring Diameter (in : Static Water Level: Date: Notes: .25 18.45 1/24/2018 Stick-up height: 1.02' 0 E E� 0fl- a o Description Well Q) 0 � fl � Detail 0 J 1 0.2 Asphalt SILT (MIL), Moist, medium dense, 75% fine to medium sand, 15% fines, 10% 2 2 0.0 angular gravel to 0.5", brick and asphalt debris, no odor, no staining, 10YR 4/3 2 3 0.0 Brown 4 0.2 4 4 5 0.0 6 6 6 0.8 $ $ 10 10 12 12 7 1.8 14—X14 16 16 8 0.0 18 1s POORLY GRADED SAND(SP), Moist, medium dense, 95% fine to medium sand, 5% fines, no odor, no staining, 10YR 5/3 Brown 20 CLAYEY SAND (SC), Moist, medium dense, 80% fine to medium sand, 20% ' '. 20 fines, trace gravel to 0.25", no odor, no staining, 10YR 4/4 Dark Yellowish Brown POORLY GRADED SAND(SP), Wet, medium dense, 95% fine to medium 22 sand, 5% fines, no odor, no staining, 10YR 4/4 Dark Yellowish Brown '. 22 9 0.0 24 24 10 0.0 Borehole terminated at 25 feet Terracon 2201 Rowland Avenue, Savannah, Georgia 31404 Phone: 912-6294000, Fax 912-629-4001 0 U) 0 0 0 0 0 m 0 LU w Irerracon Soil Boring and Well Construction Log Page 1 of 1 Project: WWAY Building LSI Project Number: ES187011 Boring/Well: TW-4 Well Construction Data Date Started: Latitude: Screen: 1/23/18 341431.97 0.0 10" slotted PVC ® From: 17 To: 22 Logged By: EMS Longitude: 775658.91 Pack: Clean 20/30 Filter Sand From: 22 To: 9 Drilling Co.: Driller: Seal: William Walker William Walker Hydrated Bentonite Chips From: 9 To: 8 Method: Equipment: Grout: Direct Push Geoprobe 6620DT N/A From: To: Boring Depth (ft.): 22.0 -7 Saturated Zone: 18.76 Date: 1/23/2018 Inner Casing: 1„ Threaded Schedule 40 PVC Boring Diameter (in : .25 Static Water Level: T 18.31 Date: 1/24/2018 Notes: Stick-up height: 1.44' a o U) oo U) of FL a 0 J Description Well Detail a p 1 0.3 GRASS/ROOTS SILTY SAND (SM), Moist, medium dense, 85% fine to medium sand, 15% 2 0.0 fines, brick and asphalt debris, no odor, no staining, 10YR 5/2 Grayish Brown 2 2 3 0.0 4 0.0 4 4 5 0.0 6 6 POORLY GRADED SAND(SP), Moist, medium dense, 100% fine to medium sand, no odor, no staining, 10YR 5/2 Grayish Brown 6 0.0 8 8 10 10 POORLY GRADED SAND WITH SILT(SP-SM), Moist, medium dense, 90% 12 fine to medium sand,10% fines, no odor, no staining, 10YR 4/3 Brown 12 POORLY GRADED SAND(SP), Moist, medium dense, 100% fine to medium 7 0.0 sand, no odor, no staining, 10YR 4/3 Brown 14 14 16 16 8 0.0 18 18 POORLY GRADED SAND(SP), Wet, medium dense, 100% fine to medium - sand, no odor, no staining, 10YR 4/3 Brown 20 As above except color change to 10YR 4/4 Dark Yellowish Brown ,, ,, 20 9 0.0 22 Borehole terminated at 22 feet 22 Terracon 2201 Rowland Avenue, Savannah, Georgia 31404 Phone: 912-629-4000, Fax: 912-629-4001 a z w Z 0 z w 0 a 0 a Irerracon Soil Boring and Well Construction Log Page 1 of 1 Project: Project Number: Boring/Well: ES187011 TW-5 WWAY Building LSI Well Construction Data Date Started: Latitude: Screen: 1/23/18 341431.54 0.010" slotted PVC ® From: 30 To: 25 Logged By: Longitude: Pack: EMS 77570.33 Clean 20/30 Filter Sand From: 30 To: 15 Drilling Co.: Driller: Seal: William Walker William Walker Hydrated Bentonite Chips From: 15 To: 14 Method: Equipment: Grout: Direct Push Geoprobe 6620DT N/A From: To: Boring Depth (ft.): Saturated Zone: Date: Inner Casing: 30.0 -7 29.22 1/23/2018 1„ Threaded Schedule 40 PVC Boring Diameter (in : Static Water Level: Date: Notes: .25 T 24.05 1/24/2018 Stick-up height: 0.17' a oo of FL a 0 Description Well a a) o U) U) Detail J 1 0.0 ° " ° CONCRETE *2* *0.0* SILTY SAND (SM), Moist, medium dense, 85% fine to medium sand, 15% 2 3 0.0 fines, brick and asphlat debris, no odor, no staining, 10YR 4/3 Brown 2 4 0.0 4 5 0.0 4 o WELL GRADED SAND (SW), Moist, medium dense, 75% fine to coarse 6 sand, 20% angular gravel to 0.5", 5% fines, brick and asphlat debris, no odor, 6 o> no staining, 10YR 3/2 Very Dark Grayish Brown, 50% RECOVERY 8 6 0.0 8 10 10 POORLY GRADED SAND(SP), Moist, medium dense, 100% fine to medium 12 7 0 0 sand, trace gravel to 0.25", brick and asphlat debris, no odor, no staining, 10YR 12 3/2 Very Dark Grayish Brown 14 14 > WELL GRADED SAND (SW), Moist, medium dense, 75% fine to coarse 16 sand, 20% angular gravel, 5% fines, brick and asphlat debris, no odor, no 16 staining, 10YR 4/3 Brown :: 18 8 0.0 •, 18 POORLY GRADED SAND(SP), Moist, medium dense, 100% fine to coarse sand, trace gravel to 1 ", no odor, no staining, 10YR 4/3 Brown 20 POORLY GRADED SAND(SP), Moist, medium dense, 100% fine to coarse '• 20 sand, trace gravel to 1 ", brick and wood debris, no odor, no staining, 10YR 4/3 22 Brown 22 9 0.0 _______________________ POORLY GRADED SAND(SP),Very moist, medium dense, 100% fine to ..,1 .•.• 24 medium sand, trace gravel to 0.25", brick and asphlat debris, no odor, no - 24 staining, 10YR 5/3 Brown 26 26 *10* *0.0* SILTY SAND (SM),Wet, medium dense, 80%fine to medium sand, 20% 28 fines, no odor, no staining, 10YR 4/4 Dark Yellowish Brown •• 28 30 Borehole terminated at 30 feet 30 Terracon 2201 Rowland Avenue, Savannah, Georgia 31404 Phone: 912-629-4000, Fax: 912-629-4001 APPENDIX D LABORATORY ANALYTICAL DATA A February 05, 2018 Justin Johnson Terracon Environmental 2201 Rowland Avenue Savannah, GA 31404 Laboratory Results for: WWAY Building Dear Justin, Service Request No:J1800711 Enclosed are the results of the sample(s) submitted to our laboratory January 27, 2018 For your reference, these analyses have been assigned our service request numberJ1800711. All analyses were performed according to our laboratory's quality assurance program. The test results meet requirements of the NELAP standards except as noted in the case narrative report. All results are intended to be considered in their entirety, and ALS Environmental is not responsible for use of less than the complete report. Results apply only to the items submitted to the laboratory for analysis and individual items (samples) analyzed, as listed in the report. In accordance to the NELAC 2003 Standard, a statement on the estimated uncertainty of measurement of any quantitative analysis will be supplied upon request. Please contact me if you have any questions. My extension is 4410. You may also contact me via email at Jerry.Allen@alsglobal.com. Respectfully submitted, ALS Group USA, Corp. dba ALS Environmental Jerry Allen Project Manager ADDRESS 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 PHONE +1 904 739 2277 I FAX +1 904 739 2011 ALS Group USA, Corp. dba ALS Environmental Page 1 of 184 ALS Environmental ALS Group USA, Corp 9143 Philips Highway, Suite 200 Jacksonville, FL 32256 A L 5 T : +1 904 739 2277 F : +1 904 739 2011 www.aisgiobal.com Table of Contents CoverLetter 1 Table of Contents 2 Narrative Documents 7 Narrative Documents 8 Hit Summary List 10 Sample Receipt Information 15 Sample Cross -Reference 16 Chain Of Custody 17 Miscellaneous Forms 20 Qualifiers 21 Acronyms 23 Analyst Summary 24 Sample Results 29 Volatile Organic Compounds by GCMS 30 8260B - Volatile Organic Compounds by GC/MS SB-1-1 - VolatileOrganic 31 SIB-1-17 - VolatileOrganic 33 SB-2-1 - VolatileOrganic 35 SB-2-12 - VolatileOrganic 37 SB-3-1 - VolatileOrganic 39 SB-3-14 - VolatileOrganic 41 SB-4-1 - VolatileOrganic 43 RIGHT SOLUTIONS I RIGHT PARTNER Page 2 of 184 Table of Contents (continued) SB-4-21 - VolatileOrganic 45 TW-5-1 - VolatileOrganic 47 TW-5-25 - VolatileOrganic 49 TW-1 - VolatileOrganic 51 TW-3 - VolatileOrganic 53 TW-2 - VolatileOrganic 55 TW-4 - VolatileOrganic 57 TW-5 - VolatileOrganic 59 Semivolatile Organic Compounds by GCMS 61 8270C - Semivolatile Organic Compounds by GC/MS SB-1-1 - Semivoa GCMS 62 SB-1-17 - Semivoa GCMS 64 SB-2-1 - Semivoa GCMS 66 SB-2-12 - Semivoa GCMS 68 SB-3-1 - Semivoa GCMS 70 SB-3-14 - Semivoa GCMS 72 SB-4-1 - Semivoa GCMS 74 SB-4-21 - Semivoa GCMS 76 TW-5-1 - Semivoa GCMS 78 TW-5-25 - Semivoa GCMS 80 TW-1 - Semivoa GCMS 82 TW-3 - Semivoa GCMS 84 TW-2 - Semivoa GCMS 86 TW-4 - Semivoa GCMS 88 TW-5 - Semivoa GCMS 90 8270D SIM - Base Neutral Semivolatile Organic Compounds by GC/MS SIM TW-1 - Semivoa GCMS 92 TW-3 - Semivoa GCMS 93 TW-2 - Semivoa GCMS 94 TW-4 - Semivoa GCMS 95 TW-5 - Semivoa GCMS 96 Semivolatile Organic Compounds by GC 97 Page 3 of 184 Table of Contents (continued) 8082 - Polychlorinated Biphenyls (PCBs) by GC SIB-1-1 - Semivoa GC 98 SB-1-17 - Semivoa GC 99 SB-2-1 - Semivoa GC 100 SB-2-12 - Semivoa GC 101 SB-3-1 - Semivoa GC 102 SB-3-14 - Semivoa GC 103 Metals 104 SB-1-1 - Metals 105 SB-1-17 - Metals 106 SB-2-1 - Metals 107 SB-2-12 - Metals 108 SB-3-1 - Metals 109 SB-3-14 - Metals 110 SB-4-1 - Metals 111 SB-4-21 - Metals 112 TW-5-1 - Metals 113 TW-5-25 - Metals 114 TW-1 - Metals 115 TW-3 - Metals 116 TW-2 - Metals 117 TW-4 - Metals 118 TW-5 - Metals 119 General Chemistry 120 SB-1-1 - GenChem 121 SIB-1-17 - GenChem 122 SB-2-1 - GenChem 123 SB-2-12 - GenChem 124 SB-3-1 - GenChem 125 SB-3-14 - GenChem 126 SB-4-1 - GenChem 127 SB-4-21 - GenChem 128 Page 4 of 184 Table of Contents (continued) TW-5-1 - GenChem 129 TW-5-25 - GenChem 130 QC Summary Forms 131 Volatile Organic Compounds by GCMS 132 8260B - Volatile Organic Compounds by GC/MS VolatileOrganic Surrogate Summary 133 Method Blank - VolatileOrganic 137 Method Blank - VolatileOrganic 139 JQ1800803-01 - LCS VolatileOrganic 141 JQ1800782-04 - DLCS VolatileOrganic 143 Semivolatile Organic Compounds by GCMS 145 8270C - Semivolatile Organic Compounds by GC/MS Semivoa GCMS Surrogate Summary 146 JQ1800698-04 TW-1 - DMS Semivoa GCMS 150 JQ1800727-04 SB-1-17 - DMS Semivoa GCMS 152 Method Blank - Semivoa GCMS 154 Method Blank - Semivoa GCMS 156 Method Blank - Semivoa GCMS 158 JQ1800698-02 - LCS Semivoa GCMS 160 JQ1800727-02 - LCS Semivoa GCMS 162 JQ1800741-03 - DLCS Semivoa GCMS 164 8270D SIM - Base Neutral Semivolatile Organic Compounds by GC/MS SIM Semivoa GCMS Surrogate Summary 166 Method Blank - Semivoa GCMS 167 Semivolatile Organic Compounds by GC 168 8082 - Polychlorinated Biphenyls (PCBs) by GC Semivoa GC Surrogate Summary 169 JQ1800725-04 SB-1-1 - DMS Semivoa GC 170 Method Blank - Semivoa GC 171 JQ1800725-02 - LCS Semivoa GC 172 Dual Column Confirmation 173 Metals 176 Page 5 of 184 Table of Contents (continued) Method Blank - Metals 177 Method Blank - Metals 178 J1800711-002DMS SB-1-17 - DMS Metals 179 J1800711-006DMS SB-3-14 - DMS Metals 180 J 1800711-LCS 1 - LCS Metals 181 J 1800711-LCS2 - LCS Metals 182 General Chemistry 183 J1800711-005DUP SB-3-1 - DUP GenChem 184 Page 6 of 184 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904) 739-2277 Fax (904) 739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 7 of 184 AEnuironmentall 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 1904-739-2277 I www.alsglobal.com Client: Terracon Environmental Service Request:J1800711 Project: WWAY Building/ES187011 Sample Matrix: Soil CASE NARRATIVE Date Received:1/27/18 All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains analytical results for samples designated for Tier II data deliverables, including results of QC samples analyzed from this delivery group. When appropriate to the procedure, method blank results have been reported with each analytical test. Analytical procedures performed by the lab are validated in accordance with NELAC standards. Parameters that are included in the NELAC Fields of Testing but are not included in the lab's NELAC accreditation are identified in the discussion of each analytical procedure. Sample Receipt 10 soil & 5 water samples were received for analysis at ALS Environmental on 1/27/18. The samples were received in good condition and consistent with the accompanying chain of custody form. Samples are refrigerated at <6°C upon receipt at the lab except for aqueous samples designated for metals analyses, which are stored at room temperature. Volatile Organic Analyses: Method 8260B: The control criteria were exceeded for one or more surrogates in samples J1800711-005, J1800711-006, J1800711-008, and J1800711-010 due to suspected matrix interferences. No further corrective action was appropriate. Method 8260B: The upper control criterion was exceeded for the following analytes in Laboratory Control Sample (LCS) JQ1800803-01: 0-Dichloroethene, Bromomethane, Chloroethane, and Trichlorofluoromethane. The analytes in question were not detected in the associated field samples. The error associated with elevated recovery equates to a high bias. The sample data is not significantly affected. No further corrective action was appropriate. Semi -Volatile Organic Analyses: Method 8270: The spike recovery of analyte for Laboratory Control Sample (LCS) JQ1800698-002 was outside the lower control criterion. The analyte(s) in question were not detected in the associated field samples. The error associated with reduced recovery equates to a potential low bias. Additional analysis of the associated field samples J1800711-11, -12, and -15 could not be performed because insufficient sample remained for testing. The data is flagged to indicate the problem. Method 8270: The lower control criterion was exceeded for the following analytes in the Continuing Calibration Verification (CCV): multiple analytes. The analytes in question were not detected in the associated field samples. Since the analytes were detected in the MRL check standard, instrument sensitivity was documented. The data quality was not significantly affected and no further corrective action was taken. Method 8270: The control criteria were exceeded for the following surrogate(s) in JQ1800698-02: one or more surrogates. The associated matrix spike recoveries of target compounds were in control, indicating the analysis was in control. The surrogate outlier is flagged accordingly. No further corrective action was appropriate. Method 8270D SIM: The control criteria were exceeded for the following surrogate(s) in JQ1800740-001: one or more surrogates. The associated matrix spike recoveries of target compounds were in control, indicating the analysis was in control. The surrogate outlier is flagged accordingly. No further corrective action was appropriate. Method 8270D SIM: The control criterion was exceeded for the following surrogates in the Continuing Calibration Verification Approved by c%��` — -- ---_-- Date 2/5/2018 Page 8 of 184 AEnuironmentall 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 1904-739-2277 I www.alsglobal.com (CCV): one or more analytes. The surrogate in question was within acceptance criteria for the associated field samples. The data quality was not significantly affected and no further corrective action was taken. Metals Analyses: The reporting limit is elevated for analyte(s) analyzed by ICP/AES in sample(s) J1800711- (008, 009). These sample(s) contained high concentrations of Iron and Copper cause spectral interference that could not be corrected for without diluting the samples. General Chemistry Analyses: No significant data anomalies were noted with this analysis. Approved by Date 2/5/2018 Page 9 of 184 AALSEnuironmental SAMPLE DETECTION SUMMARY LIENT ID: SB-1-1 Lab ID: J1800711-001 Analyte --------------------------------------------------------------------------------------------------------------------------------------------------- Results Flag MDL ------------------- PQL --------------------- Units ------------------------ Method ----------------------- Solids, Total 90.9 Percent 160.3 Arsenic, Total 5.18 0.07 0.39 mg/Kg 6010D Barium, Total 72.2 0.02 0.39 mg/Kg 6010D Cadmium, Total 0.16 1 0.02 0.19 mg/Kg 6010D Chromium, Total 6.81 0.04 0.39 mg/Kg 6010D Lead, Total 296 0.04 0.39 mg/Kg 6010D Mercury, Total 1.17 0.005 0.073 mg/Kg 7471 B Selenium, Total 0.51 0.14 0.39 mg/Kg 6010D Silver, Total 0.23 IV 0.04 0.39 mg/Kg 6010D 1-Methyl naphthalene 365 72.3 186 ug/Kg 8270C 2-Methyl naphthalene 493 64.6 186 ug/Kg 8270C Acetophenone 52.9 1 50.4 372 ug/Kg 8270C Anthracene 418 47.1 186 ug/Kg 8270C Benz(a)anthracene 123 1 51.5 186 ug/Kg 8270C Benzo(a)pyrene 93.4 1 40.5 186 ug/Kg 8270C Benzo(b)fluoranthene 113 1 28.5 186 ug/Kg 8270C Benzo(g,h,i)perylene 83.5 1 57.0 186 ug/Kg 8270C Benzo(k)fluoranthene 72.2 1 64.6 186 ug/Kg 8270C Chrysene 232 49.3 186 ug/Kg 8270C Dibenzofuran 114 1 50.4 186 ug/Kg 8270C Fluoranthene 151 1 52.6 186 ug/Kg 8270C Indeno(1,2,3-cd)pyrene 55.8 1 44.9 186 ug/Kg 8270C Naphthalene 428 53.7 186 ug/Kg 8270C Phenanthrene 425 46.0 186 ug/Kg 8270C Pyrene 181 1 50.4 186 ug/Kg 8270C Acetone 66.1 2.30 18.2 ug/Kg 8260B LIENT ID: SB-1-17 Lab ID: J1800711-002 Analyte Results Flag MDL PQL Units Method Solids, Total 95.4 Percent 160.3 Arsenic, Total 0.88 0.07 0.35 mg/Kg 6010D Barium, Total 12.6 0.02 0.35 mg/Kg 6010D Chromium, Total 1.95 0.04 0.35 mg/Kg 6010D Lead, Total 64.1 0.04 0.35 mg/Kg 6010D Mercury, Total 0.160 0.0005 0.0069 mg/Kg 7471 B Acetone 10.9 1 2.62 22.8 ug/Kg 8260B LIENT ID: SB-2-1 Lab ID: J1800711-003 Analyte Results Flag MDL PQL Units Method Solids, Total 97.9 Percent 160.3 Barium, Total 1.04 0.02 0.30 mg/Kg 6010D Chromium, Total 0.60 0.04 0.30 mg/Kg 6010D Page 10 of 184 AALSEnuironmental SAMPLE DETECTION SUMMARY LIENT ID: SB-2-1 Lab ID: J1800711-003 Analyte Results Flag M D L P Q L Units Method Lead, Total 1.43 0.04 0.30 mg/Kgmg/Kg 6010D Mercury, Total 0.0072 0.0005 0.0068 mg/Kg 7471 B Selenium, Total 0.15 1 0.14 0.30 mg/Kg 6010D Acetone 58.4 2.30 19.2 ug/Kg 8260B m,p-Xylenes 10.6 0.210 9.59 ug/Kg 8260B o-Xylene 4.84 0.160 4.79 ug/Kg 8260B LIENT ID: SB-2-12 Lab ID: J1800711-004 Analyte Results Flag M D L P Q L Units Method ------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------ Solids, Total 92.8 Percent 160.3 Arsenic, Total 0.27 1 0.07 0.44 mg/Kg 6010D Barium, Total 7.92 0.02 0.44 mg/Kg 6010D Chromium, Total 3.20 0.04 0.44 mg/Kg 6010D Lead, Total 2.31 0.04 0.44 mg/Kg 6010D Mercury, Total 0.0061 1 0.0005 0.0071 mg/Kg 7471 B Acetone 46.6 2.51 21.8 ug/Kg 8260B m,p-Xylenes 0.404 1 0.230 10.9 ug/Kg 8260B LIENT ID: SB-3-1 Lab ID: J1800711-005 Analyte Results Flag MDL PQL Units Method --------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- Solids, Total 85.2 Percent 160.3 Arsenic, Total 6.87 0.07 0.31 mg/Kg 6010D Barium, Total 79.6 0.02 0.31 mg/Kg 6010D Cadmium, Total 0.34 0.02 0.15 mg/Kg 6010D Chromium, Total 8.17 0.04 0.31 mg/Kg 6010D Lead, Total 479 0.2 1.5 mg/Kg 6010D Mercury, Total 4.62 0.005 0.078 mg/Kg 7471 B Selenium, Total 0.49 0.14 0.31 mg/Kg 6010D Silver, Total 0.12 IV 0.04 0.31 mg/Kg 6010D Benz(a)anthracene 1480 1 548 1980 ug/Kg 8270C Benzo(a)pyrene 1150 1 432 1980 ug/Kg 8270C Benzo(b)fluoranthene 1190 1 303 1980 ug/Kg 8270C Benzo(g,h,i)perylene 684 I 606 1980 ug/Kg 8270C Benzo(k)fluoranthene 1150 1 688 1980 ug/Kg 8270C Chrysene 1670 1 525 1980 ug/Kg 8270C Fluoranthene 2730 560 1980 ug/Kg 8270C Indeno(1,2,3-cd)pyrene 652 1 478 1980 ug/Kg 8270C Phenanthrene 1370 1 490 1980 ug/Kg 8270C Pyrene 2440 536 1980 ug/Kg 8270C Acetone 106 2.75 23.9 ug/Kg 8260B m,p-Xylenes 0.323 1 0.252 12.0 ug/Kg 8260B Page 11 of 184 AALSEnuironmental SAMPLE DETECTION SUMMARY LIENT ID: SB-3-14 Lab ID: J1800711-006 Analyte ----------------------------------------------------------------- Results Flag MDL Flag MDL PQL Units Method ---------- Solids, Total 94.1 Percent 160.3 Arsenic, Total 0.27 1 0.07 0.39 mg/Kg 6010D Barium, Total 2.40 0.02 0.39 mg/Kg 6010D Chromium, Total 5.18 0.04 0.39 mg/Kg 6010D Lead, Total 1.32 0.04 0.39 mg/Kg 6010D Mercury, Total 0.0090 0.0005 0.0071 mg/Kg 7471 B Acetone 36.8 2.30 19.8 ug/Kg 8260B LIENT ID: SB-4-1 Lab ID: J1800711-007 Analyte Results Flag MDL PQL Units Method Solids, Total 76.4 Percent 160.3 Arsenic, Total 2.84 0.07 0.44 mg/Kg 6010D Barium, Total 30.8 0.02 0.44 mg/Kg 6010D Cadmium, Total 0.13 1 0.02 0.22 mg/Kg 6010D Chromium, Total 4.57 0.04 0.44 mg/Kg 6010D Lead, Total 128 0.04 0.44 mg/Kg 6010D Mercury, Total 1.04 0.006 0.084 mg/Kg 7471 B Selenium, Total 0.35 1 0.14 0.44 mg/Kg 6010D Silver, Total 0.09 IV 0.04 0.44 mg/Kg 6010D Acetone 127 3.02 26.2 ug/Kg 8260B LIENT ID: SB-4-21 Lab ID: J1800711-008 Analyte Results Flag MDL PQL Units Method Solids, Total 92.1 Percent 160.3 Arsenic, Total 7.03 0.13 0.62 mg/Kg 6010D Barium, Total 40.2 0.03 0.62 mg/Kg 6010D Cadmium, Total 0.12 1 0.03 0.31 mg/Kg 6010D Chromium, Total 6.28 0.07 0.62 mg/Kg 6010D Lead, Total 235 0.08 0.62 mg/Kg 6010D Mercury, Total 1.73 0.005 0.073 mg/Kg 7471 B Silver, Total 0.31 IV 0.08 0.62 mg/Kg 6010D Acetone 66.3 2.60 22.6 ug/Kg 8260B LIENT ID: TW-5-1 Lab ID: J1800711-009 Analyte Results Flag MDL PQL Units Method Solids, Total 83.8 Percent 160.3 Arsenic, Total 12.1 0.4 1.8 mg/Kg 6010D Barium, Total 273 0.06 1.8 mg/Kg 6010D Cadmium, Total 0.54 1 0.06 0.91 mg/Kg 6010D Chromium, Total 11.2 0.2 1.8 mg/Kg 6010D Lead, Total 1350 0.2 1.8 mg/Kg 6010D Mercury, Total 0.370 0.0005 0.0080 mg/Kg 7471 B Selenium, Total 2.4 0.7 1.8 mg/Kg 6010D Page 12 of 184 AALSEnuironmental SAMPLE DETECTION SUMMARY LIENT ID: TW-5-1 Lab ID: J1800711-009 Analyte Results Flag MDL PQL Units Method Acetone 36.5 1 5.41 47.0 ug/Kg 8260B LIENT ID: TW-5-25 Lab ID: J1800711-010 Analyte Results Flag MDL PQL Units Method ------------------------------------------------------------ Solids, Total --------------------------------------------- 80.8 ------------------------------------------------------------- Percent 160.3 Arsenic, Total 2.08 0.07 0.36 mg/Kg 6010D Barium, Total 7.79 0.02 0.36 mg/Kg 6010D Cadmium, Total 0.04 1 0.02 0.18 mg/Kg 6010D Chromium, Total 3.35 0.04 0.36 mg/Kg 6010D Lead, Total 6.16 0.04 0.36 mg/Kg 6010D Mercury, Total 0.0276 0.0005 0.0080 mg/Kg 7471 B Selenium, Total 0.40 0.14 0.36 mg/Kg 6010D Acenaphthylene 1030 1 571 2060 ug/Kg 8270C Benzo(a)pyrene 809 1 450 2060 ug/Kg 8270C Benzo(b)fluoranthene 498 1 316 2060 ug/Kg 8270C Benzo(g,h,i)perylene 652 1 632 2060 ug/Kg 8270C Indeno(1,2,3-cd)pyrene 611 1 498 2060 ug/Kg 8270C Acetone 85.1 2.48 21.5 ug/Kg 8260B LIENT ID: TW-1 Lab ID: J1800711-011 Analyte Results Flag MDL PQL Units Method Barium, Total 39 0.3 10 ug/L 6010D Chromium, Total 2 1 0.4 10 ug/L 6010D Lead, Total 8 1 2 10 ug/L 6010D Selenium, Total 4 1 3 10 ug/L 6010D Silver, Total 1 1 0.6 10 ug/L 6010D Benz(a)anthracene 0.0555 1 0.0350 0.0957 ug/L 8270D SIM Chrysene 0.0241 1 0.0240 0.0957 ug/L 8270D SIM Phenanthrene 0.0363 1 0.0350 0.0957 ug/L 8270D SIM Pyrene 0.0373 1 0.0310 0.0957 ug/L 8270D SIM LIENT ID: TW-3 Lab ID: J1800711-012 Analyte Results Flag M D L P Q L Units Method Arsenic, Total 19 2 10 ug/L 6010D Barium, Total 57 0.3 10 ug/L 6010D Chromium, Total 56 0.4 10 ug/L 6010D Lead, Total 39 2 10 ug/L 6010D Mercury, Total 0.11 0.05 0.10 ug/L 7470A 1-Methyl naphthalene 0.0488 1 0.0440 0.0957 ug/L 8270D SIM 2,4-Dinitrophenol 4.24 1 0.760 19.1 ug/L 8270C Acetone 14 1 5.6 20 ug/L 8260B Page 13 of 184 AALSEnuironmental SAMPLE DETECTION SUMMARY LIENT ID: TW-2 Lab ID: J1800711-013 Analyte Results Flag MDL PQL Units Method -------------- ----------- --------------------- ------------------------ ----------------------- Barium, Total 19 0.3 10 ug/L 6010D Chromium, Total 1 1 0.4 10 ug/L 6010D LIENT ID: TW-4 Lab ID: J1800711-014 Analyte Results Flag MDL PQL Units Method ------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------ Barium, Total 52 0.3 10 ug/L 6010D Selenium, Total 8 1 3 10 ug/L 6010D LIENT ID: TW-5 Lab ID: J1800711-015 Analyte Results Flag M D L P Q L Units Method Barium, Total 54 0.3 10 ug/L 6010D Chromium, Total 3 1 0.4 10 ug/L 6010D Lead, Total 6 1 2 10 ug/L 6010D Mercury, Total 0.12 0.05 0.10 ug/L 7470A Selenium, Total 4 1 3 10 ug/L 6010D Acenaphthylene 0.0652 1 0.0250 0.0957 ug/L 8270D SIM Anthracene 0.0401 1 0.0380 0.0957 ug/L 8270D SIM Benz(a)anthracene 0.0695 1 0.0350 0.0957 ug/L 8270D SIM Benzo(a)pyrene 0.0682 1 0.0310 0.0957 ug/L 8270D SIM Benzo(b)fluoranthene 0.0787 1 0.0250 0.0957 ug/L 8270D SIM Benzo(g,h,i)perylene 0.0536 1 0.0390 0.0957 ug/L 8270D SIM Chrysene 0.0277 1 0.0240 0.0957 ug/L 8270D SIM Indeno(1,2,3-cd)pyrene 0.0453 1 0.0400 0.0957 ug/L 8270D SIM Phenanthrene 0.0715 1 0.0350 0.0957 ug/L 8270D SIM Pyrene 0.0922 1 0.0310 0.0957 ug/L 8270D SIM Page 14 of 184 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904) 739-2277 Fax (904) 739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 15 of 184 Client: Terracon Environmental Service Request:J1800711 Project: WWAY Building/ES187011 SAMPLE CROSS-REFERENCE SAMPLE # CLIENT SAMPLE ID DATE TIME J 1800711-001 SB-1-1 1 /23/2018 0850 J 1800711-002 SB-1-17 1 /23/2018 0930 J 1800711-003 SB-2-1 1 /23/2018 1200 J 1800711-004 SB-2-12 1 /23/2018 1210 J 1800711-005 SB-3-1 1 /23/2018 1225 J 1800711-006 SB-3-14 1 /23/2018 1300 J 1800711-007 SB-4-1 1 /23/2018 1430 J 1800711-008 SB-4-21 1 /23/2018 1510 J 1800711-009 TW-5-1 1 /23/2018 1340 J 1800711-010 TW-5-25 1 /23/2018 1415 J 1800711-011 TW-1 1 /24/2018 1120 J 1800711-012 TW-3 1 /24/2018 1310 J 1800711-013 TW-2 1 /24/2018 1525 J 1800711-014 TW-4 1 /24/2018 1650 J 1800711-015 TW-5 1 /24/2018 1720 Printed 2/5/2018 3:02:06 PM Page 16 of 184 Sample Summary �« E....•.....�.�..r�.. Cooler Receipt Form Client: �� i-rct C'c 6� Service Request #: 0() Project: ✓ i ri/j Shipping paid by ALS? Cooler received on / i �l and opened on Z 7/ )�- by G>­-j Yes N? NIA COURIER: ALS UPg_FEDEX HL Client Other Airbill1i ^� 1 Were custody seals on outside of cooler? Yes ' No If yes, how many and where? 4: � on lid r- kother 2 Were seals intact and signature and date correct? Yes' ' No NIA 3 Were custody papers properly filled out? Yes No NIA 4 Temperature of cooler(s) upon receipt (Should be o°C and < 6°C) G C _ 5 Thermometer ID 6 Temperature Blank Present? Yes No 7 Were lee or Ice Packs present lce Ice Packs No 8 Did all bottles arrive in good condition (unbroken, etc....)? Yes No NIA - yp p g p Type of packing material resent�Wrp Netting Vial Holde Bubble Paper Styrofoam Other N/A 10 Were all bottle labels complete (sample ID, preservation, etc....)? Yes ` , No NIA I l Did all bottle labels and tags agree with custody papers? Yes No NIA 12 Were the correct bottles used for the tests indicated? No . NIA 13 Were a1 - f tlie,preserved bottles received with the appropriate preservative? �1.. Yes + No _ NIA H2SO4 pH<2 ZnAc2/NaOH pH>9 NaOH pH>12 (/ H�rvative HCI pH<2 s noted below 14 Were all samples received within analysis holding times? Ye %' No NIA 15 Were VOA vials free of air bubbles greater than 6mm? If present, note below __YN No NIA 16 Where -did the bottles originate? ALS Client Sample ID Reagent Lot # MI added Initials Date/Time Additional comments and/or explanation of all discrepancies noted above: ,pL4 ® Soil f wtrc ✓Gtety4,1 par} ytf A61grj . ient approval to run if discrepancies noted: Date: SMF-1 Cooler Receipt Form pa ea 1 0 14 12/6/2016 g 0 ny to C? O C] L j� U,) N O � Si} -. � QC � IA G7 ' fla d N 't m ❑ = ❑� 1 El El El 1:1 El Cd Q S.- E C c N �y ©_ vi uj N N u uj N N ♦'�. i11 Q un N Z Q C cn C V Y ❑ 03 Ln tL V) V) y a IL S �� a a U a Q > ro w z z m U z z O O r 80d X sielaW'dNDN S Y - IDt-OLZS Xxxx.x SJaUfL'7U0310'ON li! U` (j u� v ❑ U U r «� v U L) Y Q1 ` V V N d V V V L) L. C m m 0° 1. m m UJ = •Ln `m �s ad oo E z z z m a E N ¢¢ Q Q d O ay 0 0 O , ' er of pi Z m V z z z¢¢ J C [9 7 CD V- � W LLJ x LJ.9 C a Q � O 0 U o o Q e o m o /i Cn m - LJ ro as .. 4.1 Z 'w.. L) U .. I N ✓ Y cu N v °a v fE N ' } ° a ° ° o b m \% ' Ci (n ! o+ 0- is Q V U2 a a a vi — af V I — _ A v, O O f� Vl N. � — 01 6J eej 4 �; C E ¢LnC L Srta N 0 i ... ro � c 4 a N c N c V lJJ N N tA J � � Q N. 0 N N a LU N �n ro Z w - VI - LI) T y1 c vi ro CL LO 0 Q E Z Z m V ro z b z O D o SPI'M eaDa s XXX4 E --9 0 dal 4GZ8 t3; N U- U- s.aauiejuo, Jo 'ON I� u uk Qi \ w � U U G 0 i V U V J U m U U U d rJ rt rt m m 0 R) cci ai Q Q Q o z z z y. a 1 7��. 1 T; a¢ o 0 o a �- 61 a; N Z Z Z ¢ Q 9 O cn toLLJ � .•+r+ CL) rd Q a L o (D o °� o c a o C Q ?j 00 N Q 0 ro .. to :V) ..,. ro Qy Z c :� a ih eG Z Zrd j U i eL u a�i vs �_ 'i{i n+ w y? a 'v a: w o .1 2' V O Vi a etl a v Q U w a ci ca n Faj w U n 1 f 184 F�- ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904) 739-2277 Fax (904) 739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 20 of 184 Alffi-PlAronmerpt-al FLORIDA DEP DATA QUALIFIERS B Results based upon colony counts outside the acceptable range. D Measurement was made in the field. H Value based on field kit determination; results may not be accurate. I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. J Estimated value (one of the following reasons is discussed in the project case narrative). 1. The result may be inaccurate because the surrogate recovery limits have been exceeded. 2. No known quality control criteria exists for the component. 3. The reported value failed to meet the established quality control criteria for either precision or accuracy. 4. The sample matrix interfered with the ability to make any accurate determination (e.g., primary and confirmation results show greater than 40% RPD). 5. The data is questionable because of improper laboratory or field protocols (e.g., GUMS Tune did not meet method criteria). K Off scale low. The value is less than the lowest calibration standard but greater than the method reporting limit (MRL). L Off scale high. The analyte is above the upper limit of the linear calibration range. M The MDL/MRL has been elevated because the analyte could not be accurately quantified due to matrix interference. N Presumptive evidence of the analyte. Confirmation was not performed. Q Sample held beyond the accepted holding time. T Value reported is less than the laboratory method detection limit. The value is reported for informational purposes only. U Indicates that the compound was analyzed for but not detected. V Indicates that the analyte was detected in both the sample and the associated method blank. Y The laboratory analysis was from an improperly preserved sample. Z Too many colonies were present (TNTC). The numeric value represents the filtration volume. Page 21 of 184 Alffi-pailronment-al Jacksonville Lab ID # for State Certifications' Agency Number Expiration Date Department of Defense 66206 7/31/2018 Florida Department of Health E82502 6/30/2018 Georgia Department of Natural 958 6/30/2018 Resources Kentucky Division of Waste 123042 6/30/2018 Management Louisiana Department of 02086 6/30/2018 Environmental Quality Maine Department of Health and 2015002 2/3/2019 Human Services North Carolina Department of 527 12/31/2018 Environment and Natural Resources Pennsylvania Department of 68-04835 8/31/2018 Environmental Protection South Carolina Department of Health 96021001 6/30/2018 and Environmental Control Texas Commission on Environmental T104704197-16-8 5/31/2018 Quality Virginia Environmental Accreditation 460191 12/14/2018 Program Analyses were performed according to our laboratory's NELAP-approved quality assurance program and any applicable state or agency requirements. The test results meet requirements of the current NELAP/'INI standards or state or agency requirements, where applicable, except as noted in the laboratory case narrative provided. For a specific list of accredited analytes, refer to htt 2://www.aisglobal.com/en/Our-Services/Life-Sciences/Environmental/Downloads/North-America- Downloads Page 22 of 184 Aunvoironment-al ASTM American Society for Testing and Materials A2LA American Association for Laboratory Accreditation CARB California Air Resources Board CAS Number Chemical Abstract Service registry Number CFC Chlorofluorocarbon CFU Colony -Forming Unit DEC Department of Environmental Conservation DEQ Department of Environmental Quality DHS Department of Health Services DOE Department of Ecology DOH Department of Health EPA U. S. Environmental Protection Agency ELAP Environmental Laboratory Accreditation Program GC Gas Chromatography GC/MS Gas Chromatography/Mass Spectrometry LUFT Leaking Underground Fuel Tank M Modified MCL Maximum Contaminant Level is the highest permissible concentration of a substance allowed in drinking water as established by the USEPA. MDL Method Detection Limit MPN Most Probable Number MRL Method Reporting Limit NA Not Applicable NC Not Calculated NCASI National Council of the Paper Industry for Air and Stream Improvement ND Not Detected NIOSH National Institute for Occupational Safety and Health PQL Practical Quantitation Limit RCRA Resource Conservation and Recovery Act SIM Selected Ion Monitoring TPH Total Petroleum Hydrocarbons tr Trace level is the concentration of an analyte that is less than the PQL but greater than or equal to the MDL. Page 23 of 184 ALS Group USA, Corp. dba ALS Environmental Analyst Summary report Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Name: SB-1-1 Lab Code: J1800711-001 Sample Matrix: Soil Analysis Method 160.3 Modified 601 OD 7471B 8082 8260B 8270C Sample Name: SB-1-17 Lab Code: J1800711-002 Sample Matrix: Soil Analysis Method 160.3 Modified 6010D 7471B 8082 8260B 8270C Sample Name: SB-2-1 Lab Code: J1800711-003 Sample Matrix: Soil Analysis Method 160.3 Modified 6010D 7471B 8082 8260B 8270C Service Request: J1800711 Date Collected: 01/23/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By ALANE KW EGARDNER EGARDNER EGARDNER JSHEARD NHOWARD SALLEN SALLEN JSHEARD TYEREMYANTS Date Collected: 01/23/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By ALANE KW EGARDNER EGARDNER EGARDNER JSHEARD NHOWARD SALLEN SALLEN JSHEARD TYEREMYANTS Date Collected: 01/23/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By ALANE KW EGARDNER EGARDNER EGARDNER JSHEARD NHOWARD SALLEN SALLEN JSHEARD TYEREMYANTS Printed 2/5/2018 3:02:08 PM Page 24 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analyst Summary report Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Name: SB-2-12 Lab Code: J1800711-004 Sample Matrix: Soil Analysis Method 160.3 Modified 601 OD 7471B 8082 8260B 8270C Sample Name: SB-3-1 Lab Code: J1800711-005 Sample Matrix: Soil Analysis Method 160.3 Modified 6010D 7471B 8082 8260B 8270C Sample Name: SB-3-14 Lab Code: J1800711-006 Sample Matrix: Soil Analysis Method 160.3 Modified 6010D 7471B 8082 8260B 8270C Service Request: J1800711 Date Collected: 01/23/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By ALANE KW EGARDNER EGARDNER EGARDNER JSHEARD NHOWARD SALLEN SALLEN JSHEARD TYEREMYANTS Date Collected: 01/23/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By ALANE KW EGARDNER EGARDNER EGARDNER JSHEARD NHOWARD SALLEN SALLEN JSHEARD TYEREMYANTS Date Collected: 01/23/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By ALANE KW EGARDNER EGARDNER EGARDNER JSHEARD NHOWARD SALLEN SALLEN JSHEARD TYEREMYANTS Printed 2/5/2018 3:02:08 PM Page 25 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analyst Summary report Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Name: SB-4-1 Lab Code: J1800711-007 Sample Matrix: Soil Analysis Method 160.3 Modified 601 OD 7471B 8260B 8270C Sample Name: SB-4-21 Lab Code: J1800711-008 Sample Matrix: Soil Analysis Method 160.3 Modified 6010D 7471B 8260B 8270C Sample Name: TW-5-1 Lab Code: J1800711-009 Sample Matrix: Soil Analysis Method 160.3 Modified 6010D 7471B 8260B 8270C Service Request: J1800711 Date Collected: 01/23/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By ALANE KW EGARDNER EGARDNER EGARDNER SALLEN SALLEN JSHEARD TYEREMYANTS Date Collected: 01/23/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By ALANE KW EGARDNER EGARDNER EGARDNER SALLEN SALLEN JSHEARD TYEREMYANTS Extracted/Digested By KW EGARDNER SALLEN JSHEARD Date Collected: 01/23/18 Date Received: 01/27/18 Analyzed By ALANE EGARDNER EGARDNER SALLEN TYEREMYANTS Printed 2/5/2018 3:02:08 PM Page 26 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analyst Summary report Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Name: TW-5-25 Lab Code: J1800711-010 Sample Matrix: Soil Analysis Method 160.3 Modified 601 OD 7471B 8260B 8270C Sample Name: TW-1 Lab Code: J1800711-011 Sample Matrix: Water Analysis Method 6010D 7470A 8260B 8270C 8270D SIM Sample Name: TW-3 Lab Code: J1800711-012 Sample Matrix: Water Analysis Method 6010D 7470A 8260B 8270C 8270D SIM Service Request: J1800711 Date Collected: 01/23/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By ALANE KW EGARDNER EGARDNER EGARDNER SALLEN SALLEN JSHEARD TYEREMYANTS Date Collected: 01/24/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By EGARDNER EGARDNER EGARDNER EGARDNER SALLEN ACATRON JSHEARD ACATRON JSHEARD Extracted/Digested By EGARDNER EGARDNER ACATRON ACATRON Date Collected: 01/24/18 Date Received: 01/27/18 Analyzed By EGARDNER EGARDNER SALLEN JSHEARD JSHEARD Printed 2/5/2018 3:02:08 PM Page 27 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analyst Summary report Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Name: TW-2 Lab Code: J1800711-013 Sample Matrix: Water Analysis Method 6010D 7470A 8260B 8270C 8270D SIM Sample Name: TW-4 Lab Code: J1800711-014 Sample Matrix: Water Analysis Method 6010D 7470A 8260B 8270C 8270D SIM Sample Name: TW-5 Lab Code: J1800711-015 Sample Matrix: Water Analysis Method 6010D 7470A 8260B 8270C 8270D SIM Service Request: J1800711 Date Collected: 01/24/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By EGARDNER EGARDNER EGARDNER EGARDNER SALLEN ACATRON TYEREMYANTS ACATRON JSHEARD Date Collected: 01/24/18 Date Received: 01/27/18 Extracted/Digested By Analyzed By EGARDNER EGARDNER EGARDNER EGARDNER SALLEN ACATRON TYEREMYANTS ACATRON JSHEARD Extracted/Digested By EGARDNER EGARDNER ACATRON ACATRON Date Collected: 01/24/18 Date Received: 01/27/18 Analyzed By EGARDNER EGARDNER SALLEN JSHEARD JSHEARD Printed 2/5/2018 3:02:08 PM Page 28 of 184 Superset Reference:18-0000453045 rev 00 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904) 739-2277 Fax (904) 739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 29 of 184 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 30 of 184 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 08:50 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-1-1 Units: ug/Kg Lab Code: J1800711-001 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.410 U 4.56 0.410 1 01/31/18 17:23 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.230 U 4.56 0.230 1 01/31/18 17:23 1/31/18 1,1,2,2-Tetrachloroethane 0.230 U 4.56 0.230 1 01/31/18 17:23 1/31/18 1,1,2-Trichloroethane 0.390 U 4.56 0.390 1 01/31/18 17:23 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.310 U 4.56 0.310 1 01/31/18 17:23 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 0.690 U 4.56 0.690 1 01/31/18 17:23 1/31/18 1,2,3-Trichloropropane 0.760 U 4.56 0.760 1 01/31/18 17:23 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 0.530 U 9.11 0.530 1 01/31/18 17:23 1/31/18 1,2-Dibromoethane (EDB) 0.580 U 4.56 0.580 1 01/31/18 17:23 1/31/18 1,2-Dichlorobenzene 0.320 U 4.56 0.320 1 01/31/18 17:23 1/31/18 1,2-Dichloroethane 0.300 U 4.56 0.300 1 01/31/18 17:23 1/31/18 1,2-Dichloropropane 0.410 U 4.56 0.410 1 01/31/18 17:23 1/31/18 1,3-Dichlorobenzene 0.300 U 4.56 0.300 1 01/31/18 17:23 1/31/18 1,4-Dichlorobenzene 0.100 U 4.56 0.100 1 01/31/18 17:23 1/31/18 2-Butanone (MEK) 1.60 U 22.8 1.60 1 01/31/18 17:23 1/31/18 2-Hexanone 2.20 U 9.11 2.20 1 01/31/18 17:23 1/31/18 4-Methyl-2-pentanone (MIBK) 1.50 U 9.11 1.50 1 01/31/18 17:23 1/31/18 Acetone 66.1 18.2 2.30 1 01/31/18 17:23 1/31/18 Benzene 0.170 U 4.56 0.170 1 01/31/18 17:23 1/31/18 Bromochloromethane 0.600 U 4.56 0.600 1 01/31/18 17:23 1/31/18 Bromodichloromethane 0.370 U 4.56 0.370 1 01/31/18 17:23 1/31/18 Bromoform 0.340 U 4.56 0.340 1 01/31/18 17:23 1/31/18 Bromomethane 0.270 U 4.56 0.270 1 01/31/18 17:23 1/31/18 Carbon Disulfide 0.800 U 9.11 0.800 1 01/31/18 17:23 1/31/18 Carbon Tetrachloride 0.190 U 4.56 0.190 1 01/31/18 17:23 1/31/18 Chlorobenzene 0.140 U 4.56 0.140 1 01/31/18 17:23 1/31/18 Chloroethane 0.330 U 4.56 0.330 1 01/31/18 17:23 1/31/18 Chloroform 0.180 U 4.56 0.180 1 01/31/18 17:23 1/31/18 Chloromethane 0.210 U 4.56 0.210 1 01/31/18 17:23 1/31/18 cis-1,2-Dichloroethene 0.330 U 4.56 0.330 1 01/31/18 17:23 1/31/18 cis-1,3-Dichloropropene 0.140 U 4.56 0.140 1 01/31/18 17:23 1/31/18 Dibromochloromethane 0.220 U 4.56 0.220 1 01/31/18 17:23 1/31/18 Dibromomethane 0.390 U 4.56 0.390 1 01/31/18 17:23 1/31/18 Dichlorodifluoromethane 0.180 U 18.2 0.180 1 01/31/18 17:23 1/31/18 Ethylbenzene 0.120 U 4.56 0.120 1 01/31/18 17:23 1/31/18 Iodomethane 1.10 U 9.11 1.10 1 01/31/18 17:23 1/31/18 m,p-Xylenes 0.210 U 9.11 0.210 1 01/31/18 17:23 1/31/18 Methyl tert-Butyl Ether 0.260 U 4.56 0.260 1 01/31/18 17:23 1/31/18 Methylene Chloride 0.310 U 9.11 0.310 1 01/31/18 17:23 1/31/18 o-Xylene 0.160 U 4.56 0.160 1 01/31/18 17:23 1/31/18 Styrene 0.270 U 4.56 0.270 1 01/31/18 17:23 1/31/18 Tetrachloroethene (PCE) 0.250 U 4.56 0.250 1 01/31/18 17:23 1/31/18 Toluene 0.270 U 4.56 0.270 1 01/31/18 17:23 1/31/18 Printed 2/5/2018 3:02:09 PM Page 31 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 08:50 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-1-1 Units: ug/Kg Lab Code: J1800711-001 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.390 U 4.56 0.390 1 01/31/18 17:23 1/31/18 trans- l,3-Dichloropropene 0.220 U 4.56 0.220 1 01/31/18 17:23 1/31/18 trans-1,4-Dichloro-2-butene 0.540 U 18.2 0.540 1 01/31/18 17:23 1/31/18 Trichloroethene (TCE) 0.250 U 4.56 0.250 1 01/31/18 17:23 1/31/18 Trichlorofluoromethane 0.210 U 18.2 0.210 1 01/31/18 17:23 1/31/18 Vinyl Acetate 1.20 U 9.11 1.20 1 01/31/18 17:23 1/31/18 Vinyl Chloride 0.260 U 4.56 0.260 1 01/31/18 17:23 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 98 74 - 120 01/31/18 17:23 4-Bromofluorobenzene 102 77 - 130 01/31/18 17:23 Dibromofluoromethane 112 85 - 117 01/31/18 17:23 Toluene-d8 96 81 - 126 01/31/18 17:23 Printed 2/5/2018 3:02:09 PM Page 32 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 09:30 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-1-17 Units: ug/Kg Lab Code: J1800711-002 Basis: Dry Volatile Organic Compounds by GCIMS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.467 U 5.69 0.467 1 01/31/18 17:46 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.262 U 5.69 0.262 1 01/31/18 17:46 1/31/18 1,1,2,2-Tetrachloroethane 0.262 U 5.69 0.262 1 01/31/18 17:46 1/31/18 1,1,2-Trichloroethane 0.445 U 5.69 0.445 1 01/31/18 17:46 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.353 U 5.69 0.353 1 01/31/18 17:46 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 0.786 U 5.69 0.786 1 01/31/18 17:46 1/31/18 1,2,3-Trichloropropane 0.866 U 5.69 0.866 1 01/31/18 17:46 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 0.604 U 11.4 0.604 1 01/31/18 17:46 1/31/18 1,2-Dibromoethane (EDB) 0.661 U 5.69 0.661 1 01/31/18 17:46 1/31/18 1,2-Dichlorobenzene 0.365 U 5.69 0.365 1 01/31/18 17:46 1/31/18 1,2-Dichloroethane 0.342 U 5.69 0.342 1 01/31/18 17:46 1/31/18 1,2-Dichloropropane 0.467 U 5.69 0.467 1 01/31/18 17:46 1/31/18 1,3-Dichlorobenzene 0.342 U 5.69 0.342 1 01/31/18 17:46 1/31/18 1,4-Dichlorobenzene 0.114 U 5.69 0.114 1 01/31/18 17:46 1/31/18 2-Butanone (MEK) 1.83 U 28.5 1.83 1 01/31/18 17:46 1/31/18 2-Hexanone 2.51 U 11.4 2.51 1 01/31/18 17:46 1/31/18 4-Methyl-2-pentanone (MIBK) 1.71 U 11.4 1.71 1 01/31/18 17:46 1/31/18 Acetone 10.91 22.8 2.62 1 01/31/18 17:46 1/31/18 Benzene 0.194 U 5.69 0.194 1 01/31/18 17:46 1/31/18 Bromochloromethane 0.684 U 5.69 0.684 1 01/31/18 17:46 1/31/18 Bromodichloromethane 0.422 U 5.69 0.422 1 01/31/18 17:46 1/31/18 Bromoform 0.388 U 5.69 0.388 1 01/31/18 17:46 1/31/18 Bromomethane 0.308 U 5.69 0.308 1 01/31/18 17:46 1/31/18 Carbon Disulfide 0.911 U 11.4 0.911 1 01/31/18 17:46 1/31/18 Carbon Tetrachloride 0.217 U 5.69 0.217 1 01/31/18 17:46 1/31/18 Chlorobenzene 0.160 U 5.69 0.160 1 01/31/18 17:46 1/31/18 Chloroethane 0.376 U 5.69 0.376 1 01/31/18 17:46 1/31/18 Chloroform 0.205 U 5.69 0.205 1 01/31/18 17:46 1/31/18 Chloromethane 0.240 U 5.69 0.240 1 01/31/18 17:46 1/31/18 cis-1,2-Dichloroethene 0.376 U 5.69 0.376 1 01/31/18 17:46 1/31/18 cis-1,3-Dichloropropene 0.160 U 5.69 0.160 1 01/31/18 17:46 1/31/18 Dibromochloromethane 0.251 U 5.69 0.251 1 01/31/18 17:46 1/31/18 Dibromomethane 0.445 U 5.69 0.445 1 01/31/18 17:46 1/31/18 Dichlorodifluoromethane 0.205 U 22.8 0.205 1 01/31/18 17:46 1/31/18 Ethylbenzene 0.137 U 5.69 0.137 1 01/31/18 17:46 1/31/18 Iodomethane 1.26 U 11.4 1.26 1 01/31/18 17:46 1/31/18 m,p-Xylenes 0.240 U 11.4 0.240 1 01/31/18 17:46 1/31/18 Methyl tert-Butyl Ether 0.297 U 5.69 0.297 1 01/31/18 17:46 1/31/18 Methylene Chloride 0.353 U 11.4 0.353 1 01/31/18 17:46 1/31/18 o-Xylene 0.183 U 5.69 0.183 1 01/31/18 17:46 1/31/18 Styrene 0.308 U 5.69 0.308 1 01/31/18 17:46 1/31/18 Tetrachloroethene (PCE) 0.285 U 5.69 0.285 1 01/31/18 17:46 1/31/18 Toluene 0.308 U 5.69 0.308 1 01/31/18 17:46 1/31/18 Printed 2/5/2018 3:02:09 PM Page 33 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 09:30 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-1-17 Units: ug/Kg Lab Code: J1800711-002 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.445 U 5.69 0.445 1 01/31/18 17:46 1/31/18 trans- l,3-Dichloropropene 0.251 U 5.69 0.251 1 01/31/18 17:46 1/31/18 trans-1,4-Dichloro-2-butene 0.615 U 22.8 0.615 1 01/31/18 17:46 1/31/18 Trichloroethene (TCE) 0.285 U 5.69 0.285 1 01/31/18 17:46 1/31/18 Trichlorofluoromethane 0.240 U 22.8 0.240 1 01/31/18 17:46 1/31/18 Vinyl Acetate 1.37 U 11.4 1.37 1 01/31/18 17:46 1/31/18 Vinyl Chloride 0.297 U 5.69 0.297 1 01/31/18 17:46 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 108 74 - 120 01/31/18 17:46 4-Bromofluorobenzene 96 77 - 130 01/31/18 17:46 Dibromofluoromethane 98 85 - 117 01/31/18 17:46 Toluene-d8 94 81 - 126 01/31/18 17:46 Printed 2/5/2018 3:02:09 PM Page 34 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:00 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-2-1 Units: ug/Kg Lab Code: J1800711-003 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.410 U 4.79 0.410 1 01/31/18 18:10 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.230 U 4.79 0.230 1 01/31/18 18:10 1/31/18 1,1,2,2-Tetrachloroethane 0.230 U 4.79 0.230 1 01/31/18 18:10 1/31/18 1,1,2-Trichloroethane 0.390 U 4.79 0.390 1 01/31/18 18:10 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.310 U 4.79 0.310 1 01/31/18 18:10 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 0.690 U 4.79 0.690 1 01/31/18 18:10 1/31/18 1,2,3-Trichloropropane 0.760 U 4.79 0.760 1 01/31/18 18:10 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 0.530 U 9.59 0.530 1 01/31/18 18:10 1/31/18 1,2-Dibromoethane (EDB) 0.580 U 4.79 0.580 1 01/31/18 18:10 1/31/18 1,2-Dichlorobenzene 0.320 U 4.79 0.320 1 01/31/18 18:10 1/31/18 1,2-Dichloroethane 0.300 U 4.79 0.300 1 01/31/18 18:10 1/31/18 1,2-Dichloropropane 0.410 U 4.79 0.410 1 01/31/18 18:10 1/31/18 1,3-Dichlorobenzene 0.300 U 4.79 0.300 1 01/31/18 18:10 1/31/18 1,4-Dichlorobenzene 0.100 U 4.79 0.100 1 01/31/18 18:10 1/31/18 2-Butanone (MEK) 1.60 U 24.0 1.60 1 01/31/18 18:10 1/31/18 2-Hexanone 2.20 U 9.59 2.20 1 01/31/18 18:10 1/31/18 4-Methyl-2-pentanone (MIBK) 1.50 U 9.59 1.50 1 01/31/18 18:10 1/31/18 Acetone 58.4 19.2 2.30 1 01/31/18 18:10 1/31/18 Benzene 0.170 U 4.79 0.170 1 01/31/18 18:10 1/31/18 Bromochloromethane 0.600 U 4.79 0.600 1 01/31/18 18:10 1/31/18 Bromodichloromethane 0.370 U 4.79 0.370 1 01/31/18 18:10 1/31/18 Bromoform 0.340 U 4.79 0.340 1 01/31/18 18:10 1/31/18 Bromomethane 0.270 U 4.79 0.270 1 01/31/18 18:10 1/31/18 Carbon Disulfide 0.800 U 9.59 0.800 1 01/31/18 18:10 1/31/18 Carbon Tetrachloride 0.190 U 4.79 0.190 1 01/31/18 18:10 1/31/18 Chlorobenzene 0.140 U 4.79 0.140 1 01/31/18 18:10 1/31/18 Chloroethane 0.330 U 4.79 0.330 1 01/31/18 18:10 1/31/18 Chloroform 0.180 U 4.79 0.180 1 01/31/18 18:10 1/31/18 Chloromethane 0.210 U 4.79 0.210 1 01/31/18 18:10 1/31/18 cis-1,2-Dichloroethene 0.330 U 4.79 0.330 1 01/31/18 18:10 1/31/18 cis-1,3-Dichloropropene 0.140 U 4.79 0.140 1 01/31/18 18:10 1/31/18 Dibromochloromethane 0.220 U 4.79 0.220 1 01/31/18 18:10 1/31/18 Dibromomethane 0.390 U 4.79 0.390 1 01/31/18 18:10 1/31/18 Dichlorodifluoromethane 0.180 U 19.2 0.180 1 01/31/18 18:10 1/31/18 Ethylbenzene 0.120 U 4.79 0.120 1 01/31/18 18:10 1/31/18 Iodomethane 1.10 U 9.59 1.10 1 01/31/18 18:10 1/31/18 m,p-Xylenes 10.6 9.59 0.210 1 01/31/18 18:10 1/31/18 Methyl tert-Butyl Ether 0.260 U 4.79 0.260 1 01/31/18 18:10 1/31/18 Methylene Chloride 0.310 U 9.59 0.310 1 01/31/18 18:10 1/31/18 o-Xylene 4.84 4.79 0.160 1 01/31/18 18:10 1/31/18 Styrene 0.270 U 4.79 0.270 1 01/31/18 18:10 1/31/18 Tetrachloroethene (PCE) 0.250 U 4.79 0.250 1 01/31/18 18:10 1/31/18 Toluene 0.270 U 4.79 0.270 1 01/31/18 18:10 1/31/18 Printed 2/5/2018 3:02:10 PM Page 35 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:00 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-2-1 Units: ug/Kg Lab Code: J1800711-003 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.390 U 4.79 0.390 1 01/31/18 18:10 1/31/18 trans- l,3-Dichloropropene 0.220 U 4.79 0.220 1 01/31/18 18:10 1/31/18 trans-1,4-Dichloro-2-butene 0.540 U 19.2 0.540 1 01/31/18 18:10 1/31/18 Trichloroethene (TCE) 0.250 U 4.79 0.250 1 01/31/18 18:10 1/31/18 Trichlorofluoromethane 0.210 U 19.2 0.210 1 01/31/18 18:10 1/31/18 Vinyl Acetate 1.20 U 9.59 1.20 1 01/31/18 18:10 1/31/18 Vinyl Chloride 0.260 U 4.79 0.260 1 01/31/18 18:10 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 98 74 - 120 01/31/18 18:10 4-Bromofluorobenzene 105 77 - 130 01/31/18 18:10 Dibromofluoromethane 115 85 - 117 01/31/18 18:10 Toluene-d8 99 81 - 126 01/31/18 18:10 Printed 2/5/2018 3:02:10 PM Page 36 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:10 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-2-12 Units: ug/Kg Lab Code: J1800711-004 Basis: Dry Volatile Organic Compounds by GCIMS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.448 U 5.45 0.448 1 01/31/18 18:33 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.251 U 5.45 0.251 1 01/31/18 18:33 1/31/18 1,1,2,2-Tetrachloroethane 0.251 U 5.45 0.251 1 01/31/18 18:33 1/31/18 1,1,2-Trichloroethane 0.426 U 5.45 0.426 1 01/31/18 18:33 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.339 U 5.45 0.339 1 01/31/18 18:33 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 0.753 U 5.45 0.753 1 01/31/18 18:33 1/31/18 1,2,3-Trichloropropane 0.829 U 5.45 0.829 1 01/31/18 18:33 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 0.579 U 10.9 0.579 1 01/31/18 18:33 1/31/18 1,2-Dibromoethane (EDB) 0.633 U 5.45 0.633 1 01/31/18 18:33 1/31/18 1,2-Dichlorobenzene 0.350 U 5.45 0.350 1 01/31/18 18:33 1/31/18 1,2-Dichloroethane 0.328 U 5.45 0.328 1 01/31/18 18:33 1/31/18 1,2-Dichloropropane 0.448 U 5.45 0.448 1 01/31/18 18:33 1/31/18 1,3-Dichlorobenzene 0.328 U 5.45 0.328 1 01/31/18 18:33 1/31/18 1,4-Dichlorobenzene 0.110 U 5.45 0.110 1 01/31/18 18:33 1/31/18 2-Butanone (MEK) 1.75 U 27.3 1.75 1 01/31/18 18:33 1/31/18 2-Hexanone 2.40 U 10.9 2.40 1 01/31/18 18:33 1/31/18 4-Methyl-2-pentanone (MIBK) 1.64 U 10.9 1.64 1 01/31/18 18:33 1/31/18 Acetone 46.6 21.8 2.51 1 01/31/18 18:33 1/31/18 Benzene 0.186 U 5.45 0.186 1 01/31/18 18:33 1/31/18 Bromochloromethane 0.655 U 5.45 0.655 1 01/31/18 18:33 1/31/18 Bromodichloromethane 0.404 U 5.45 0.404 1 01/31/18 18:33 1/31/18 Bromoform 0.371 U 5.45 0.371 1 01/31/18 18:33 1/31/18 Bromomethane 0.295 U 5.45 0.295 1 01/31/18 18:33 1/31/18 Carbon Disulfide 0.873 U 10.9 0.873 1 01/31/18 18:33 1/31/18 Carbon Tetrachloride 0.208 U 5.45 0.208 1 01/31/18 18:33 1/31/18 Chlorobenzene 0.153 U 5.45 0.153 1 01/31/18 18:33 1/31/18 Chloroethane 0.360 U 5.45 0.360 1 01/31/18 18:33 1/31/18 Chloroform 0.197 U 5.45 0.197 1 01/31/18 18:33 1/31/18 Chloromethane 0.230 U 5.45 0.230 1 01/31/18 18:33 1/31/18 cis-1,2-Dichloroethene 0.360 U 5.45 0.360 1 01/31/18 18:33 1/31/18 cis-1,3-Dichloropropene 0.153 U 5.45 0.153 1 01/31/18 18:33 1/31/18 Dibromochloromethane 0.240 U 5.45 0.240 1 01/31/18 18:33 1/31/18 Dibromomethane 0.426 U 5.45 0.426 1 01/31/18 18:33 1/31/18 Dichlorodifluoromethane 0.197 U 21.8 0.197 1 01/31/18 18:33 1/31/18 Ethylbenzene 0.131 U 5.45 0.131 1 01/31/18 18:33 1/31/18 Iodomethane 1.20 U 10.9 1.20 1 01/31/18 18:33 1/31/18 m,p-Xylenes 0.4041 10.9 0.230 1 01/31/18 18:33 1/31/18 Methyl tert-Butyl Ether 0.284 U 5.45 0.284 1 01/31/18 18:33 1/31/18 Methylene Chloride 0.339 U 10.9 0.339 1 01/31/18 18:33 1/31/18 o-Xylene 0.175 U 5.45 0.175 1 01/31/18 18:33 1/31/18 Styrene 0.295 U 5.45 0.295 1 01/31/18 18:33 1/31/18 Tetrachloroethene (PCE) 0.273 U 5.45 0.273 1 01/31/18 18:33 1/31/18 Toluene 0.295 U 5.45 0.295 1 01/31/18 18:33 1/31/18 Printed 2/5/2018 3:02:10 PM Page 37 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:10 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-2-12 Units: ug/Kg Lab Code: J1800711-004 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.426 U 5.45 0.426 1 01/31/18 18:33 1/31/18 trans- l,3-Dichloropropene 0.240 U 5.45 0.240 1 01/31/18 18:33 1/31/18 trans-1,4-Dichloro-2-butene 0.589 U 21.8 0.589 1 01/31/18 18:33 1/31/18 Trichloroethene (TCE) 0.273 U 5.45 0.273 1 01/31/18 18:33 1/31/18 Trichlorofluoromethane 0.230 U 21.8 0.230 1 01/31/18 18:33 1/31/18 Vinyl Acetate 1.31 U 10.9 1.31 1 01/31/18 18:33 1/31/18 Vinyl Chloride 0.284 U 5.45 0.284 1 01/31/18 18:33 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 103 74 - 120 01/31/18 18:33 4-Bromofluorobenzene 86 77 - 130 01/31/18 18:33 Dibromofluoromethane ill 85 - 117 01/31/18 18:33 Toluene-d8 99 81 - 126 01/31/18 18:33 Printed 2/5/2018 3:02:10 PM Page 38 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:25 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-3-1 Units: ug/Kg Lab Code: J1800711-005 Basis: Dry Volatile Organic Compounds by GCIMS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.491 U 5.98 0.491 1 01/31/18 18:56 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.275 U 5.98 0.275 1 01/31/18 18:56 1/31/18 1,1,2,2-Tetrachloroethane 0.275 U 5.98 0.275 1 01/31/18 18:56 1/31/18 1,1,2-Trichloroethane 0.467 U 5.98 0.467 1 01/31/18 18:56 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.371 U 5.98 0.371 1 01/31/18 18:56 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 0.825 U 5.98 0.825 1 01/31/18 18:56 1/31/18 1,2,3-Trichloropropane 0.909 U 5.98 0.909 1 01/31/18 18:56 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 0.634 U 12.0 0.634 1 01/31/18 18:56 1/31/18 1,2-Dibromoethane (EDB) 0.694 U 5.98 0.694 1 01/31/18 18:56 1/31/18 1,2-Dichlorobenzene 0.383 U 5.98 0.383 1 01/31/18 18:56 1/31/18 1,2-Dichloroethane 0.359 U 5.98 0.359 1 01/31/18 18:56 1/31/18 1,2-Dichloropropane 0.491 U 5.98 0.491 1 01/31/18 18:56 1/31/18 1,3-Dichlorobenzene 0.359 U 5.98 0.359 1 01/31/18 18:56 1/31/18 1,4-Dichlorobenzene 0.120 U 5.98 0.120 1 01/31/18 18:56 1/31/18 2-Butanone (MEK) 1.92 U 29.9 1.92 1 01/31/18 18:56 1/31/18 2-Hexanone 2.63 U 12.0 2.63 1 01/31/18 18:56 1/31/18 4-Methyl-2-pentanone (MIBK) 1.80 U 12.0 1.80 1 01/31/18 18:56 1/31/18 Acetone 106 23.9 2.75 1 01/31/18 18:56 1/31/18 Benzene 0.204 U 5.98 0.204 1 01/31/18 18:56 1/31/18 Bromochloromethane 0.718 U 5.98 0.718 1 01/31/18 18:56 1/31/18 Bromodichloromethane 0.443 U 5.98 0.443 1 01/31/18 18:56 1/31/18 Bromoform 0.407 U 5.98 0.407 1 01/31/18 18:56 1/31/18 Bromomethane 0.323 U 5.98 0.323 1 01/31/18 18:56 1/31/18 Carbon Disulfide 0.957 U 12.0 0.957 1 01/31/18 18:56 1/31/18 Carbon Tetrachloride 0.228 U 5.98 0.228 1 01/31/18 18:56 1/31/18 Chlorobenzene 0.168 U 5.98 0.168 1 01/31/18 18:56 1/31/18 Chloroethane 0.395 U 5.98 0.395 1 01/31/18 18:56 1/31/18 Chloroform 0.216 U 5.98 0.216 1 01/31/18 18:56 1/31/18 Chloromethane 0.252 U 5.98 0.252 1 01/31/18 18:56 1/31/18 cis-1,2-Dichloroethene 0.395 U 5.98 0.395 1 01/31/18 18:56 1/31/18 cis-1,3-Dichloropropene 0.168 U 5.98 0.168 1 01/31/18 18:56 1/31/18 Dibromochloromethane 0.263 U 5.98 0.263 1 01/31/18 18:56 1/31/18 Dibromomethane 0.467 U 5.98 0.467 1 01/31/18 18:56 1/31/18 Dichlorodifluoromethane 0.216 U 23.9 0.216 1 01/31/18 18:56 1/31/18 Ethylbenzene 0.144 U 5.98 0.144 1 01/31/18 18:56 1/31/18 Iodomethane 1.32 U 12.0 1.32 1 01/31/18 18:56 1/31/18 m,p-Xylenes 0.323 I 12.0 0.252 1 01/31/18 18:56 1/31/18 Methyl tert-Butyl Ether 0.311 U 5.98 0.311 1 01/31/18 18:56 1/31/18 Methylene Chloride 0.371 U 12.0 0.371 1 01/31/18 18:56 1/31/18 o-Xylene 0.192 U 5.98 0.192 1 01/31/18 18:56 1/31/18 Styrene 0.323 U 5.98 0.323 1 01/31/18 18:56 1/31/18 Tetrachloroethene (PCE) 0.299 U 5.98 0.299 1 01/31/18 18:56 1/31/18 Toluene 0.323 U 5.98 0.323 1 01/31/18 18:56 1/31/18 Printed 2/5/2018 3:02:10 PM Page 39 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:25 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-3-1 Units: ug/Kg Lab Code: J1800711-005 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.467 U 5.98 0.467 1 01/31/18 18:56 1/31/18 trans- l,3-Dichloropropene 0.263 U 5.98 0.263 1 01/31/18 18:56 1/31/18 trans-1,4-Dichloro-2-butene 0.646 U 23.9 0.646 1 01/31/18 18:56 1/31/18 Trichloroethene (TCE) 0.299 U 5.98 0.299 1 01/31/18 18:56 1/31/18 Trichlorofluoromethane 0.252 U 23.9 0.252 1 01/31/18 18:56 1/31/18 Vinyl Acetate 1.44 U 12.0 1.44 1 01/31/18 18:56 1/31/18 Vinyl Chloride 0.311 U 5.98 0.311 1 01/31/18 18:56 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 117 74 - 120 01/31/18 18:56 4-Bromofluorobenzene 75 * 77 - 130 01/31/18 18:56 Dibromofluoromethane 117 85 - 117 01/31/18 18:56 Toluene-d8 111 81 - 126 01/31/18 18:56 Printed 2/5/2018 3:02:10 PM Page 40 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 13:00 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-3-14 Units: ug/Kg Lab Code: J1800711-006 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.410 U 4.94 0.410 1 01/31/18 19:20 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.230 U 4.94 0.230 1 01/31/18 19:20 1/31/18 1,1,2,2-Tetrachloroethane 0.230 U 4.94 0.230 1 01/31/18 19:20 1/31/18 1,1,2-Trichloroethane 0.390 U 4.94 0.390 1 01/31/18 19:20 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.310 U 4.94 0.310 1 01/31/18 19:20 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 0.690 U 4.94 0.690 1 01/31/18 19:20 1/31/18 1,2,3-Trichloropropane 0.760 U 4.94 0.760 1 01/31/18 19:20 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 0.530 U 9.88 0.530 1 01/31/18 19:20 1/31/18 1,2-Dibromoethane (EDB) 0.580 U 4.94 0.580 1 01/31/18 19:20 1/31/18 1,2-Dichlorobenzene 0.320 U 4.94 0.320 1 01/31/18 19:20 1/31/18 1,2-Dichloroethane 0.300 U 4.94 0.300 1 01/31/18 19:20 1/31/18 1,2-Dichloropropane 0.410 U 4.94 0.410 1 01/31/18 19:20 1/31/18 1,3-Dichlorobenzene 0.300 U 4.94 0.300 1 01/31/18 19:20 1/31/18 1,4-Dichlorobenzene 0.100 U 4.94 0.100 1 01/31/18 19:20 1/31/18 2-Butanone (MEK) 1.60 U 24.7 1.60 1 01/31/18 19:20 1/31/18 2-Hexanone 2.20 U 9.88 2.20 1 01/31/18 19:20 1/31/18 4-Methyl-2-pentanone (MIBK) 1.50 U 9.88 1.50 1 01/31/18 19:20 1/31/18 Acetone 36.8 19.8 2.30 1 01/31/18 19:20 1/31/18 Benzene 0.170 U 4.94 0.170 1 01/31/18 19:20 1/31/18 Bromochloromethane 0.600 U 4.94 0.600 1 01/31/18 19:20 1/31/18 Bromodichloromethane 0.370 U 4.94 0.370 1 01/31/18 19:20 1/31/18 Bromoform 0.340 U 4.94 0.340 1 01/31/18 19:20 1/31/18 Bromomethane 0.270 U 4.94 0.270 1 01/31/18 19:20 1/31/18 Carbon Disulfide 0.800 U 9.88 0.800 1 01/31/18 19:20 1/31/18 Carbon Tetrachloride 0.190 U 4.94 0.190 1 01/31/18 19:20 1/31/18 Chlorobenzene 0.140 U 4.94 0.140 1 01/31/18 19:20 1/31/18 Chloroethane 0.330 U 4.94 0.330 1 01/31/18 19:20 1/31/18 Chloroform 0.180 U 4.94 0.180 1 01/31/18 19:20 1/31/18 Chloromethane 0.210 U 4.94 0.210 1 01/31/18 19:20 1/31/18 cis-1,2-Dichloroethene 0.330 U 4.94 0.330 1 01/31/18 19:20 1/31/18 cis-1,3-Dichloropropene 0.140 U 4.94 0.140 1 01/31/18 19:20 1/31/18 Dibromochloromethane 0.220 U 4.94 0.220 1 01/31/18 19:20 1/31/18 Dibromomethane 0.390 U 4.94 0.390 1 01/31/18 19:20 1/31/18 Dichlorodifluoromethane 0.180 U 19.8 0.180 1 01/31/18 19:20 1/31/18 Ethylbenzene 0.120 U 4.94 0.120 1 01/31/18 19:20 1/31/18 Iodomethane 1.10 U 9.88 1.10 1 01/31/18 19:20 1/31/18 m,p-Xylenes 0.210 U 9.88 0.210 1 01/31/18 19:20 1/31/18 Methyl tert-Butyl Ether 0.260 U 4.94 0.260 1 01/31/18 19:20 1/31/18 Methylene Chloride 0.310 U 9.88 0.310 1 01/31/18 19:20 1/31/18 o-Xylene 0.160 U 4.94 0.160 1 01/31/18 19:20 1/31/18 Styrene 0.270 U 4.94 0.270 1 01/31/18 19:20 1/31/18 Tetrachloroethene (PCE) 0.250 U 4.94 0.250 1 01/31/18 19:20 1/31/18 Toluene 0.270 U 4.94 0.270 1 01/31/18 19:20 1/31/18 Printed 2/5/2018 3:02:11 PM Page 41 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 13:00 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-3-14 Units: ug/Kg Lab Code: J1800711-006 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.390 U 4.94 0.390 1 01/31/18 19:20 1/31/18 trans- l,3-Dichloropropene 0.220 U 4.94 0.220 1 01/31/18 19:20 1/31/18 trans-1,4-Dichloro-2-butene 0.540 U 19.8 0.540 1 01/31/18 19:20 1/31/18 Trichloroethene (TCE) 0.250 U 4.94 0.250 1 01/31/18 19:20 1/31/18 Trichlorofluoromethane 0.210 U 19.8 0.210 1 01/31/18 19:20 1/31/18 Vinyl Acetate 1.20 U 9.88 1.20 1 01/31/18 19:20 1/31/18 Vinyl Chloride 0.260 U 4.94 0.260 1 01/31/18 19:20 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 106 74 - 120 01/31/18 19:20 4-Bromofluorobenzene 114 77 - 130 01/31/18 19:20 Dibromofluoromethane 112 85 - 117 01/31/18 19:20 Toluene-d8 80 * 81 - 126 01/31/18 19:20 Printed 2/5/2018 3:02:11 PM Page 42 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 14:30 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-4-1 Units: ug/Kg Lab Code: J1800711-007 Basis: Dry Volatile Organic Compounds by GCIMS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.537 U 6.55 0.537 1 01/31/18 19:43 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.302 U 6.55 0.302 1 01/31/18 19:43 1/31/18 1,1,2,2-Tetrachloroethane 0.302 U 6.55 0.302 1 01/31/18 19:43 1/31/18 1,1,2-Trichloroethane 0.511 U 6.55 0.511 1 01/31/18 19:43 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.406 U 6.55 0.406 1 01/31/18 19:43 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 0.904 U 6.55 0.904 1 01/31/18 19:43 1/31/18 1,2,3-Trichloropropane 0.995 U 6.55 0.995 1 01/31/18 19:43 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 0.694 U 13.1 0.694 1 01/31/18 19:43 1/31/18 1,2-Dibromoethane (EDB) 0.760 U 6.55 0.760 1 01/31/18 19:43 1/31/18 1,2-Dichlorobenzene 0.419 U 6.55 0.419 1 01/31/18 19:43 1/31/18 1,2-Dichloroethane 0.393 U 6.55 0.393 1 01/31/18 19:43 1/31/18 1,2-Dichloropropane 0.537 U 6.55 0.537 1 01/31/18 19:43 1/31/18 1,3-Dichlorobenzene 0.393 U 6.55 0.393 1 01/31/18 19:43 1/31/18 1,4-Dichlorobenzene 0.131 U 6.55 0.131 1 01/31/18 19:43 1/31/18 2-Butanone (MEK) 2.10 U 32.7 2.10 1 01/31/18 19:43 1/31/18 2-Hexanone 2.88 U 13.1 2.88 1 01/31/18 19:43 1/31/18 4-Methyl-2-pentanone (MIBK) 1.97 U 13.1 1.97 1 01/31/18 19:43 1/31/18 Acetone 127 26.2 3.02 1 01/31/18 19:43 1/31/18 Benzene 0.223 U 6.55 0.223 1 01/31/18 19:43 1/31/18 Bromochloromethane 0.786 U 6.55 0.786 1 01/31/18 19:43 1/31/18 Bromodichloromethane 0.485 U 6.55 0.485 1 01/31/18 19:43 1/31/18 Bromoform 0.446 U 6.55 0.446 1 01/31/18 19:43 1/31/18 Bromomethane 0.354 U 6.55 0.354 1 01/31/18 19:43 1/31/18 Carbon Disulfide 1.05 U 13.1 1.05 1 01/31/18 19:43 1/31/18 Carbon Tetrachloride 0.249 U 6.55 0.249 1 01/31/18 19:43 1/31/18 Chlorobenzene 0.184 U 6.55 0.184 1 01/31/18 19:43 1/31/18 Chloroethane 0.432 U 6.55 0.432 1 01/31/18 19:43 1/31/18 Chloroform 0.236 U 6.55 0.236 1 01/31/18 19:43 1/31/18 Chloromethane 0.275 U 6.55 0.275 1 01/31/18 19:43 1/31/18 cis-1,2-Dichloroethene 0.432 U 6.55 0.432 1 01/31/18 19:43 1/31/18 cis-1,3-Dichloropropene 0.184 U 6.55 0.184 1 01/31/18 19:43 1/31/18 Dibromochloromethane 0.288 U 6.55 0.288 1 01/31/18 19:43 1/31/18 Dibromomethane 0.511 U 6.55 0.511 1 01/31/18 19:43 1/31/18 Dichlorodifluoromethane 0.236 U 26.2 0.236 1 01/31/18 19:43 1/31/18 Ethylbenzene 0.158 U 6.55 0.158 1 01/31/18 19:43 1/31/18 Iodomethane 1.44 U 13.1 1.44 1 01/31/18 19:43 1/31/18 m,p-Xylenes 0.275 U 13.1 0.275 1 01/31/18 19:43 1/31/18 Methyl tert-Butyl Ether 0.341 U 6.55 0.341 1 01/31/18 19:43 1/31/18 Methylene Chloride 0.406 U 13.1 0.406 1 01/31/18 19:43 1/31/18 o-Xylene 0.210 U 6.55 0.210 1 01/31/18 19:43 1/31/18 Styrene 0.354 U 6.55 0.354 1 01/31/18 19:43 1/31/18 Tetrachloroethene (PCE) 0.328 U 6.55 0.328 1 01/31/18 19:43 1/31/18 Toluene 0.354 U 6.55 0.354 1 01/31/18 19:43 1/31/18 Printed 2/5/2018 3:02:11 PM Page 43 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 14:30 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-4-1 Units: ug/Kg Lab Code: J1800711-007 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.511 U 6.55 0.511 1 01/31/18 19:43 1/31/18 trans- l,3-Dichloropropene 0.288 U 6.55 0.288 1 01/31/18 19:43 1/31/18 trans-1,4-Dichloro-2-butene 0.707 U 26.2 0.707 1 01/31/18 19:43 1/31/18 Trichloroethene (TCE) 0.328 U 6.55 0.328 1 01/31/18 19:43 1/31/18 Trichlorofluoromethane 0.275 U 26.2 0.275 1 01/31/18 19:43 1/31/18 Vinyl Acetate 1.58 U 13.1 1.58 1 01/31/18 19:43 1/31/18 Vinyl Chloride 0.341 U 6.55 0.341 1 01/31/18 19:43 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 99 74 - 120 01/31/18 19:43 4-Bromofluorobenzene 126 77 - 130 01/31/18 19:43 Dibromofluoromethane 113 85 - 117 01/31/18 19:43 Toluene-d8 106 81 - 126 01/31/18 19:43 Printed 2/5/2018 3:02:11 PM Page 44 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 15:10 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-4-21 Units: ug/Kg Lab Code: J1800711-008 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.463 U 5.64 0.463 1 01/31/18 20:07 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.260 U 5.64 0.260 1 01/31/18 20:07 1/31/18 1,1,2,2-Tetrachloroethane 0.260 U 5.64 0.260 1 01/31/18 20:07 1/31/18 1,1,2-Trichloroethane 0.441 U 5.64 0.441 1 01/31/18 20:07 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.350 U 5.64 0.350 1 01/31/18 20:07 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 0.779 U 5.64 0.779 1 01/31/18 20:07 1/31/18 1,2,3-Trichloropropane 0.858 U 5.64 0.858 1 01/31/18 20:07 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 0.599 U 11.3 0.599 1 01/31/18 20:07 1/31/18 1,2-Dibromoethane (EDB) 0.655 U 5.64 0.655 1 01/31/18 20:07 1/31/18 1,2-Dichlorobenzene 0.362 U 5.64 0.362 1 01/31/18 20:07 1/31/18 1,2-Dichloroethane 0.339 U 5.64 0.339 1 01/31/18 20:07 1/31/18 1,2-Dichloropropane 0.463 U 5.64 0.463 1 01/31/18 20:07 1/31/18 1,3-Dichlorobenzene 0.339 U 5.64 0.339 1 01/31/18 20:07 1/31/18 1,4-Dichlorobenzene 0.113 U 5.64 0.113 1 01/31/18 20:07 1/31/18 2-Butanone (MEK) 1.81 U 28.2 1.81 1 01/31/18 20:07 1/31/18 2-Hexanone 2.49 U 11.3 2.49 1 01/31/18 20:07 1/31/18 4-Methyl-2-pentanone (MIBK) 1.70 U 11.3 1.70 1 01/31/18 20:07 1/31/18 Acetone 66.3 22.6 2.60 1 01/31/18 20:07 1/31/18 Benzene 0.192 U 5.64 0.192 1 01/31/18 20:07 1/31/18 Bromochloromethane 0.678 U 5.64 0.678 1 01/31/18 20:07 1/31/18 Bromodichloromethane 0.418 U 5.64 0.418 1 01/31/18 20:07 1/31/18 Bromoform 0.384 U 5.64 0.384 1 01/31/18 20:07 1/31/18 Bromomethane 0.305 U 5.64 0.305 1 01/31/18 20:07 1/31/18 Carbon Disulfide 0.903 U 11.3 0.903 1 01/31/18 20:07 1/31/18 Carbon Tetrachloride 0.215 U 5.64 0.215 1 01/31/18 20:07 1/31/18 Chlorobenzene 0.158 U 5.64 0.158 1 01/31/18 20:07 1/31/18 Chloroethane 0.373 U 5.64 0.373 1 01/31/18 20:07 1/31/18 Chloroform 0.204 U 5.64 0.204 1 01/31/18 20:07 1/31/18 Chloromethane 0.237 U 5.64 0.237 1 01/31/18 20:07 1/31/18 cis-1,2-Dichloroethene 0.373 U 5.64 0.373 1 01/31/18 20:07 1/31/18 cis-1,3-Dichloropropene 0.158 U 5.64 0.158 1 01/31/18 20:07 1/31/18 Dibromochloromethane 0.249 U 5.64 0.249 1 01/31/18 20:07 1/31/18 Dibromomethane 0.441 U 5.64 0.441 1 01/31/18 20:07 1/31/18 Dichlorodifluoromethane 0.204 U 22.6 0.204 1 01/31/18 20:07 1/31/18 Ethylbenzene 0.136 U 5.64 0.136 1 01/31/18 20:07 1/31/18 Iodomethane 1.25 U 11.3 1.25 1 01/31/18 20:07 1/31/18 m,p-Xylenes 0.237 U 11.3 0.237 1 01/31/18 20:07 1/31/18 Methyl tert-Butyl Ether 0.294 U 5.64 0.294 1 01/31/18 20:07 1/31/18 Methylene Chloride 0.350 U 11.3 0.350 1 01/31/18 20:07 1/31/18 o-Xylene 0.181 U 5.64 0.181 1 01/31/18 20:07 1/31/18 Styrene 0.305 U 5.64 0.305 1 01/31/18 20:07 1/31/18 Tetrachloroethene (PCE) 0.283 U 5.64 0.283 1 01/31/18 20:07 1/31/18 Toluene 0.305 U 5.64 0.305 1 01/31/18 20:07 1/31/18 Printed 2/5/2018 3:02:11 PM Page 45 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 15:10 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-4-21 Units: ug/Kg Lab Code: J1800711-008 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.441 U 5.64 0.441 1 01/31/18 20:07 1/31/18 trans- l,3-Dichloropropene 0.249 U 5.64 0.249 1 01/31/18 20:07 1/31/18 trans-1,4-Dichloro-2-butene 0.610 U 22.6 0.610 1 01/31/18 20:07 1/31/18 Trichloroethene (TCE) 0.283 U 5.64 0.283 1 01/31/18 20:07 1/31/18 Trichlorofluoromethane 0.237 U 22.6 0.237 1 01/31/18 20:07 1/31/18 Vinyl Acetate 1.36 U 11.3 1.36 1 01/31/18 20:07 1/31/18 Vinyl Chloride 0.294 U 5.64 0.294 1 01/31/18 20:07 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 110 74 - 120 01/31/18 20:07 4-Bromofluorobenzene 80 77 - 130 01/31/18 20:07 Dibromofluoromethane 114 85 - 117 01/31/18 20:07 Toluene-d8 145 * 81 - 126 01/31/18 20:07 Printed 2/5/2018 3:02:11 PM Page 46 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 13:40 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: TW-5-1 Units: ug/Kg Lab Code: J1800711-009 Basis: Dry Volatile Organic Compounds by GCIMS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.964 U 11.7 0.964 1 01/31/18 20:30 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.541 U 11.7 0.541 1 01/31/18 20:30 1/31/18 1,1,2,2-Tetrachloroethane 0.541 U 11.7 0.541 1 01/31/18 20:30 1/31/18 1,1,2-Trichloroethane 0.917 U 11.7 0.917 1 01/31/18 20:30 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.729 U 11.7 0.729 1 01/31/18 20:30 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 1.63 U 11.7 1.63 1 01/31/18 20:30 1/31/18 1,2,3-Trichloropropane 1.79 U 11.7 1.79 1 01/31/18 20:30 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 1.25 U 23.5 1.25 1 01/31/18 20:30 1/31/18 1,2-Dibromoethane (EDB) 1.37 U 11.7 1.37 1 01/31/18 20:30 1/31/18 1,2-Dichlorobenzene 0.752 U 11.7 0.752 1 01/31/18 20:30 1/31/18 1,2-Dichloroethane 0.705 U 11.7 0.705 1 01/31/18 20:30 1/31/18 1,2-Dichloropropane 0.964 U 11.7 0.964 1 01/31/18 20:30 1/31/18 1,3-Dichlorobenzene 0.705 U 11.7 0.705 1 01/31/18 20:30 1/31/18 1,4-Dichlorobenzene 0.235 U 11.7 0.235 1 01/31/18 20:30 1/31/18 2-Butanone (MEK) 3.76 U 58.7 3.76 1 01/31/18 20:30 1/31/18 2-Hexanone 5.17 U 23.5 5.17 1 01/31/18 20:30 1/31/18 4-Methyl-2-pentanone (MIBK) 3.53 U 23.5 3.53 1 01/31/18 20:30 1/31/18 Acetone 36.5 I 47.0 5.41 1 01/31/18 20:30 1/31/18 Benzene 0.400 U 11.7 0.400 1 01/31/18 20:30 1/31/18 Bromochloromethane 1.41 U 11.7 1.41 1 01/31/18 20:30 1/31/18 Bromodichloromethane 0.870 U 11.7 0.870 1 01/31/18 20:30 1/31/18 Bromoform 0.799 U 11.7 0.799 1 01/31/18 20:30 1/31/18 Bromomethane 0.635 U 11.7 0.635 1 01/31/18 20:30 1/31/18 Carbon Disulfide 1.88 U 23.5 1.88 1 01/31/18 20:30 1/31/18 Carbon Tetrachloride 0.447 U 11.7 0.447 1 01/31/18 20:30 1/31/18 Chlorobenzene 0.329 U 11.7 0.329 1 01/31/18 20:30 1/31/18 Chloroethane 0.776 U 11.7 0.776 1 01/31/18 20:30 1/31/18 Chloroform 0.423 U 11.7 0.423 1 01/31/18 20:30 1/31/18 Chloromethane 0.494 U 11.7 0.494 1 01/31/18 20:30 1/31/18 cis-1,2-Dichloroethene 0.776 U 11.7 0.776 1 01/31/18 20:30 1/31/18 cis-1,3-Dichloropropene 0.329 U 11.7 0.329 1 01/31/18 20:30 1/31/18 Dibromochloromethane 0.517 U 11.7 0.517 1 01/31/18 20:30 1/31/18 Dibromomethane 0.917 U 11.7 0.917 1 01/31/18 20:30 1/31/18 Dichlorodifluoromethane 0.423 U 47.0 0.423 1 01/31/18 20:30 1/31/18 Ethylbenzene 0.282 U 11.7 0.282 1 01/31/18 20:30 1/31/18 Iodomethane 2.59 U 23.5 2.59 1 01/31/18 20:30 1/31/18 m,p-Xylenes 0.494 U 23.5 0.494 1 01/31/18 20:30 1/31/18 Methyl tert-Butyl Ether 0.611 U 11.7 0.611 1 01/31/18 20:30 1/31/18 Methylene Chloride 0.729 U 23.5 0.729 1 01/31/18 20:30 1/31/18 o-Xylene 0.376 U 11.7 0.376 1 01/31/18 20:30 1/31/18 Styrene 0.635 U 11.7 0.635 1 01/31/18 20:30 1/31/18 Tetrachloroethene (PCE) 0.588 U 11.7 0.588 1 01/31/18 20:30 1/31/18 Toluene 0.635 U 11.7 0.635 1 01/31/18 20:30 1/31/18 Printed 2/5/2018 3:02:12 PM Page 47 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 13:40 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: TW-5-1 Units: ug/Kg Lab Code: J1800711-009 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.917 U 11.7 0.917 1 01/31/18 20:30 1/31/18 trans- l,3-Dichloropropene 0.517 U 11.7 0.517 1 01/31/18 20:30 1/31/18 trans-1,4-Dichloro-2-butene 1.27 U 47.0 1.27 1 01/31/18 20:30 1/31/18 Trichloroethene (TCE) 0.588 U 11.7 0.588 1 01/31/18 20:30 1/31/18 Trichlorofluoromethane 0.494 U 47.0 0.494 1 01/31/18 20:30 1/31/18 Vinyl Acetate 2.82 U 23.5 2.82 1 01/31/18 20:30 1/31/18 Vinyl Chloride 0.611 U 11.7 0.611 1 01/31/18 20:30 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 96 74 - 120 01/31/18 20:30 4-Bromofluorobenzene 90 77 - 130 01/31/18 20:30 Dibromofluoromethane 116 85 - 117 01/31/18 20:30 Toluene-d8 97 81 - 126 01/31/18 20:30 Printed 2/5/2018 3:02:12 PM Page 48 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 14:15 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: TW-5-25 Units: ug/Kg Lab Code: J1800711-010 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.442 U 5.38 0.442 1 01/31/18 20:53 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.248 U 5.38 0.248 1 01/31/18 20:53 1/31/18 1,1,2,2-Tetrachloroethane 0.248 U 5.38 0.248 1 01/31/18 20:53 1/31/18 1,1,2-Trichloroethane 0.420 U 5.38 0.420 1 01/31/18 20:53 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.334 U 5.38 0.334 1 01/31/18 20:53 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 0.743 U 5.38 0.743 1 01/31/18 20:53 1/31/18 1,2,3-Trichloropropane 0.818 U 5.38 0.818 1 01/31/18 20:53 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 0.571 U 10.8 0.571 1 01/31/18 20:53 1/31/18 1,2-Dibromoethane (EDB) 0.625 U 5.38 0.625 1 01/31/18 20:53 1/31/18 1,2-Dichlorobenzene 0.345 U 5.38 0.345 1 01/31/18 20:53 1/31/18 1,2-Dichloroethane 0.323 U 5.38 0.323 1 01/31/18 20:53 1/31/18 1,2-Dichloropropane 0.442 U 5.38 0.442 1 01/31/18 20:53 1/31/18 1,3-Dichlorobenzene 0.323 U 5.38 0.323 1 01/31/18 20:53 1/31/18 1,4-Dichlorobenzene 0.108 U 5.38 0.108 1 01/31/18 20:53 1/31/18 2-Butanone (MEK) 1.73 U 26.9 1.73 1 01/31/18 20:53 1/31/18 2-Hexanone 2.37 U 10.8 2.37 1 01/31/18 20:53 1/31/18 4-Methyl-2-pentanone (MIBK) 1.62 U 10.8 1.62 1 01/31/18 20:53 1/31/18 Acetone 85.1 21.5 2.48 1 01/31/18 20:53 1/31/18 Benzene 0.183 U 5.38 0.183 1 01/31/18 20:53 1/31/18 Bromochloromethane 0.646 U 5.38 0.646 1 01/31/18 20:53 1/31/18 Bromodichloromethane 0.399 U 5.38 0.399 1 01/31/18 20:53 1/31/18 Bromoform 0.366 U 5.38 0.366 1 01/31/18 20:53 1/31/18 Bromomethane 0.291 U 5.38 0.291 1 01/31/18 20:53 1/31/18 Carbon Disulfide 0.861 U 10.8 0.861 1 01/31/18 20:53 1/31/18 Carbon Tetrachloride 0.205 U 5.38 0.205 1 01/31/18 20:53 1/31/18 Chlorobenzene 0.151 U 5.38 0.151 1 01/31/18 20:53 1/31/18 Chloroethane 0.356 U 5.38 0.356 1 01/31/18 20:53 1/31/18 Chloroform 0.194 U 5.38 0.194 1 01/31/18 20:53 1/31/18 Chloromethane 0.226 U 5.38 0.226 1 01/31/18 20:53 1/31/18 cis-1,2-Dichloroethene 0.356 U 5.38 0.356 1 01/31/18 20:53 1/31/18 cis-1,3-Dichloropropene 0.151 U 5.38 0.151 1 01/31/18 20:53 1/31/18 Dibromochloromethane 0.237 U 5.38 0.237 1 01/31/18 20:53 1/31/18 Dibromomethane 0.420 U 5.38 0.420 1 01/31/18 20:53 1/31/18 Dichlorodifluoromethane 0.194 U 21.5 0.194 1 01/31/18 20:53 1/31/18 Ethylbenzene 0.130 U 5.38 0.130 1 01/31/18 20:53 1/31/18 Iodomethane 1.19 U 10.8 1.19 1 01/31/18 20:53 1/31/18 m,p-Xylenes 0.226 U 10.8 0.226 1 01/31/18 20:53 1/31/18 Methyl tert-Butyl Ether 0.280 U 5.38 0.280 1 01/31/18 20:53 1/31/18 Methylene Chloride 0.334 U 10.8 0.334 1 01/31/18 20:53 1/31/18 o-Xylene 0.173 U 5.38 0.173 1 01/31/18 20:53 1/31/18 Styrene 0.291 U 5.38 0.291 1 01/31/18 20:53 1/31/18 Tetrachloroethene (PCE) 0.270 U 5.38 0.270 1 01/31/18 20:53 1/31/18 Toluene 0.291 U 5.38 0.291 1 01/31/18 20:53 1/31/18 Printed 2/5/2018 3:02:12 PM Page 49 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 14:15 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: TW-5-25 Units: ug/Kg Lab Code: J1800711-010 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.420 U 5.38 0.420 1 01/31/18 20:53 1/31/18 trans- l,3-Dichloropropene 0.237 U 5.38 0.237 1 01/31/18 20:53 1/31/18 trans-1,4-Dichloro-2-butene 0.582 U 21.5 0.582 1 01/31/18 20:53 1/31/18 Trichloroethene (TCE) 0.270 U 5.38 0.270 1 01/31/18 20:53 1/31/18 Trichlorofluoromethane 0.226 U 21.5 0.226 1 01/31/18 20:53 1/31/18 Vinyl Acetate 1.30 U 10.8 1.30 1 01/31/18 20:53 1/31/18 Vinyl Chloride 0.280 U 5.38 0.280 1 01/31/18 20:53 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 108 74 - 120 01/31/18 20:53 4-Bromofluorobenzene 76 * 77 - 130 01/31/18 20:53 Dibromofluoromethane 105 85 - 117 01/31/18 20:53 Toluene-d8 96 81 - 126 01/31/18 20:53 Printed 2/5/2018 3:02:12 PM Page 50 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 11:20 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-1 Units: ug/L Lab Code: J1800711-011 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q 1, 1, 1,2-Tetrachloroethane 0.19 U 1.0 0.19 1 01/31/18 14:27 1, 1, 1 -Trichloroethane (TCA) 0.17 U 1.0 0.17 1 01/31/18 14:27 1,1,2,2-Tetrachloroethane 0.29 U 1.0 0.29 1 01/31/18 14:27 1,1,2-Trichloroethane 0.40 U 1.0 0.40 1 01/31/18 14:27 1, 1 -Dichloroethane (1,1-DCA) 0.30 U 1.0 0.30 1 01/31/18 14:27 1, 1 -Dichloroethene (1,1-DCE) 0.16 U 1.0 0.16 1 01/31/18 14:27 1,2,3-Trichloropropane 0.42 U 2.0 0.42 1 01/31/18 14:27 1,2-Dibromo-3-chloropropane (DBCP) 2.3 U 5.0 2.3 1 01/31/18 14:27 1,2-Dibromoethane (EDB) 0.46 U 1.0 0.46 1 01/31/18 14:27 1,2-Dichlorobenzene 0.48 U 1.0 0.48 1 01/31/18 14:27 1,2-Dichloroethane 0.22 U 1.0 0.22 1 01/31/18 14:27 1,2-Dichloropropane 0.19 U 1.0 0.19 1 01/31/18 14:27 1,3-Dichlorobenzene 0.22 U 1.0 0.22 1 01/31/18 14:27 1,4-Dichlorobenzene 0.16 U 1.0 0.16 1 01/31/18 14:27 2-Butanone (MEK) 3.8 U 10 3.8 1 01/31/18 14:27 2-Hexanone 2.2 U 25 2.2 1 01/31/18 14:27 4-Methyl-2-pentanone (MIBK) 1.1 U 25 1.1 1 01/31/18 14:27 Acetone 5.6 U 20 5.6 1 01/31/18 14:27 Benzene 0.21 U 1.0 0.21 1 01/31/18 14:27 Bromochloromethane 0.27 U 5.0 0.27 1 01/31/18 14:27 Bromodichloromethane 0.22 U 1.0 0.22 1 01/31/18 14:27 Bromoform 0.42 U 2.0 0.42 1 01/31/18 14:27 Bromomethane 0.23 U 5.0 0.23 1 01/31/18 14:27 Carbon Disulfide 2.4 U 10 2.4 1 01/31/18 14:27 Carbon Tetrachloride 0.34 U 1.0 0.34 1 01/31/18 14:27 Chlorobenzene 0.16 U 1.0 0.16 1 01/31/18 14:27 Chloroethane 0.52 U 5.0 0.52 1 01/31/18 14:27 Chloroform 0.35 U 1.0 0.35 1 01/31/18 14:27 Chloromethane 0.36 U 1.0 0.36 1 01/31/18 14:27 cis-1,2-Dichloroethene 0.36 U 1.0 0.36 1 01/31/18 14:27 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 1 01/31/18 14:27 Dibromochloromethane 0.21 U 1.0 0.21 1 01/31/18 14:27 Dibromomethane 0.36 U 5.0 0.36 1 01/31/18 14:27 Dichlorodifluoromethane 0.23 U 20 0.23 1 01/31/18 14:27 Ethylbenzene 0.21 U 1.0 0.21 1 01/31/18 14:27 Iodomethane 2.7 U 5.0 2.7 1 01/31/18 14:27 m,p-Xylenes 0.31 U 2.0 0.31 1 01/31/18 14:27 Methyl tert-Butyl Ether 0.24 U 2.0 0.24 1 01/31/18 14:27 Methylene Chloride 0.21 U 5.0 0.21 1 01/31/18 14:27 o-Xylene 0.14 U 1.0 0.14 1 01/31/18 14:27 Styrene 0.29 U 1.0 0.29 1 01/31/18 14:27 Tetrachloroethene (PCE) 0.22 U 1.0 0.22 1 01/31/18 14:27 Toluene 0.19 U 1.0 0.19 1 01/31/18 14:27 Printed 2/5/2018 3:02:12 PM Page 51 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 11:20 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-1 Units: ug/L Lab Code: J1800711-011 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q trans-1,2-Dichloroethene 0.19 U 1.0 0.19 1 01/31/18 14:27 trans- l,3-Dichloropropene 0.23 U 1.0 0.23 1 01/31/18 14:27 trans-1,4-Dichloro-2-butene 2.2 U 20 2.2 1 01/31/18 14:27 Trichloroethene (TCE) 0.36 U 1.0 0.36 1 01/31/18 14:27 Trichlorofluoromethane 0.24 U 20 0.24 1 01/31/18 14:27 Vinyl Acetate 1.9 U 10 1.9 1 01/31/18 14:27 Vinyl Chloride 0.36 U 1.0 0.36 1 01/31/18 14:27 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 100 72 - 127 01/31/18 14:27 4-Bromofluorobenzene 93 88 - 120 01/31/18 14:27 Dibromofluoromethane 102 85 - 115 01/31/18 14:27 Toluene-d8 98 83 - 123 01/31/18 14:27 Printed 2/5/2018 3:02:12 PM Page 52 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 13:10 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-3 Units: ug/L Lab Code: J1800711-012 Basis: NA Volatile Organic Compounds by GCIMS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q 1, 1, 1,2-Tetrachloroethane 0.19 U 1.0 0.19 1 01/31/18 14:49 1, 1, 1 -Trichloroethane (TCA) 0.17 U 1.0 0.17 1 01/31/18 14:49 1,1,2,2-Tetrachloroethane 0.29 U 1.0 0.29 1 01/31/18 14:49 1,1,2-Trichloroethane 0.40 U 1.0 0.40 1 01/31/18 14:49 1, 1 -Dichloroethane (1,1-DCA) 0.30 U 1.0 0.30 1 01/31/18 14:49 1, 1 -Dichloroethene (1,1-DCE) 0.16 U 1.0 0.16 1 01/31/18 14:49 1,2,3-Trichloropropane 0.42 U 2.0 0.42 1 01/31/18 14:49 1,2-Dibromo-3-chloropropane (DBCP) 2.3 U 5.0 2.3 1 01/31/18 14:49 1,2-Dibromoethane (EDB) 0.46 U 1.0 0.46 1 01/31/18 14:49 1,2-Dichlorobenzene 0.48 U 1.0 0.48 1 01/31/18 14:49 1,2-Dichloroethane 0.22 U 1.0 0.22 1 01/31/18 14:49 1,2-Dichloropropane 0.19 U 1.0 0.19 1 01/31/18 14:49 1,3-Dichlorobenzene 0.22 U 1.0 0.22 1 01/31/18 14:49 1,4-Dichlorobenzene 0.16 U 1.0 0.16 1 01/31/18 14:49 2-Butanone (MEK) 3.8 U 10 3.8 1 01/31/18 14:49 2-Hexanone 2.2 U 25 2.2 1 01/31/18 14:49 4-Methyl-2-pentanone (MIBK) 1.1 U 25 1.1 1 01/31/18 14:49 Acetone 141 20 5.6 1 01/31/18 14:49 Benzene 0.21 U 1.0 0.21 1 01/31/18 14:49 Bromochloromethane 0.27 U 5.0 0.27 1 01/31/18 14:49 Bromodichloromethane 0.22 U 1.0 0.22 1 01/31/18 14:49 Bromoform 0.42 U 2.0 0.42 1 01/31/18 14:49 Bromomethane 0.23 U 5.0 0.23 1 01/31/18 14:49 Carbon Disulfide 2.4 U 10 2.4 1 01/31/18 14:49 Carbon Tetrachloride 0.34 U 1.0 0.34 1 01/31/18 14:49 Chlorobenzene 0.16 U 1.0 0.16 1 01/31/18 14:49 Chloroethane 0.52 U 5.0 0.52 1 01/31/18 14:49 Chloroform 0.35 U 1.0 0.35 1 01/31/18 14:49 Chloromethane 0.36 U 1.0 0.36 1 01/31/18 14:49 cis-1,2-Dichloroethene 0.36 U 1.0 0.36 1 01/31/18 14:49 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 1 01/31/18 14:49 Dibromochloromethane 0.21 U 1.0 0.21 1 01/31/18 14:49 Dibromomethane 0.36 U 5.0 0.36 1 01/31/18 14:49 Dichlorodifluoromethane 0.23 U 20 0.23 1 01/31/18 14:49 Ethylbenzene 0.21 U 1.0 0.21 1 01/31/18 14:49 Iodomethane 2.7 U 5.0 2.7 1 01/31/18 14:49 m,p-Xylenes 0.31 U 2.0 0.31 1 01/31/18 14:49 Methyl tert-Butyl Ether 0.24 U 2.0 0.24 1 01/31/18 14:49 Methylene Chloride 0.21 U 5.0 0.21 1 01/31/18 14:49 o-Xylene 0.14 U 1.0 0.14 1 01/31/18 14:49 Styrene 0.29 U 1.0 0.29 1 01/31/18 14:49 Tetrachloroethene (PCE) 0.22 U 1.0 0.22 1 01/31/18 14:49 Toluene 0.19 U 1.0 0.19 1 01/31/18 14:49 Printed 2/5/2018 3:02:13 PM Page 53 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 13:10 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-3 Units: ug/L Lab Code: J1800711-012 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q trans-1,2-Dichloroethene 0.19 U 1.0 0.19 1 01/31/18 14:49 trans- l,3-Dichloropropene 0.23 U 1.0 0.23 1 01/31/18 14:49 trans-1,4-Dichloro-2-butene 2.2 U 20 2.2 1 01/31/18 14:49 Trichloroethene (TCE) 0.36 U 1.0 0.36 1 01/31/18 14:49 Trichlorofluoromethane 0.24 U 20 0.24 1 01/31/18 14:49 Vinyl Acetate 1.9 U 10 1.9 1 01/31/18 14:49 Vinyl Chloride 0.36 U 1.0 0.36 1 01/31/18 14:49 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 103 72 - 127 01/31/18 14:49 4-Bromofluorobenzene 97 88 - 120 01/31/18 14:49 Dibromofluoromethane 103 85 - 115 01/31/18 14:49 Toluene-d8 96 83 - 123 01/31/18 14:49 Printed 2/5/2018 3:02:13 PM Page 54 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 15:25 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-2 Units: ug/L Lab Code: J1800711-013 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q 1, 1, 1,2-Tetrachloroethane 0.19 U 1.0 0.19 1 01/31/18 15:10 1, 1, 1 -Trichloroethane (TCA) 0.17 U 1.0 0.17 1 01/31/18 15:10 1,1,2,2-Tetrachloroethane 0.29 U 1.0 0.29 1 01/31/18 15:10 1,1,2-Trichloroethane 0.40 U 1.0 0.40 1 01/31/18 15:10 1, 1 -Dichloroethane (1,1-DCA) 0.30 U 1.0 0.30 1 01/31/18 15:10 1, 1 -Dichloroethene (1,1-DCE) 0.16 U 1.0 0.16 1 01/31/18 15:10 1,2,3-Trichloropropane 0.42 U 2.0 0.42 1 01/31/18 15:10 1,2-Dibromo-3-chloropropane (DBCP) 2.3 U 5.0 2.3 1 01/31/18 15:10 1,2-Dibromoethane (EDB) 0.46 U 1.0 0.46 1 01/31/18 15:10 1,2-Dichlorobenzene 0.48 U 1.0 0.48 1 01/31/18 15:10 1,2-Dichloroethane 0.22 U 1.0 0.22 1 01/31/18 15:10 1,2-Dichloropropane 0.19 U 1.0 0.19 1 01/31/18 15:10 1,3-Dichlorobenzene 0.22 U 1.0 0.22 1 01/31/18 15:10 1,4-Dichlorobenzene 0.16 U 1.0 0.16 1 01/31/18 15:10 2-Butanone (MEK) 3.8 U 10 3.8 1 01/31/18 15:10 2-Hexanone 2.2 U 25 2.2 1 01/31/18 15:10 4-Methyl-2-pentanone (MIBK) 1.1 U 25 1.1 1 01/31/18 15:10 Acetone 5.6 U 20 5.6 1 01/31/18 15:10 Benzene 0.21 U 1.0 0.21 1 01/31/18 15:10 Bromochloromethane 0.27 U 5.0 0.27 1 01/31/18 15:10 Bromodichloromethane 0.22 U 1.0 0.22 1 01/31/18 15:10 Bromoform 0.42 U 2.0 0.42 1 01/31/18 15:10 Bromomethane 0.23 U 5.0 0.23 1 01/31/18 15:10 Carbon Disulfide 2.4 U 10 2.4 1 01/31/18 15:10 Carbon Tetrachloride 0.34 U 1.0 0.34 1 01/31/18 15:10 Chlorobenzene 0.16 U 1.0 0.16 1 01/31/18 15:10 Chloroethane 0.52 U 5.0 0.52 1 01/31/18 15:10 Chloroform 0.35 U 1.0 0.35 1 01/31/18 15:10 Chloromethane 0.36 U 1.0 0.36 1 01/31/18 15:10 cis-1,2-Dichloroethene 0.36 U 1.0 0.36 1 01/31/18 15:10 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 1 01/31/18 15:10 Dibromochloromethane 0.21 U 1.0 0.21 1 01/31/18 15:10 Dibromomethane 0.36 U 5.0 0.36 1 01/31/18 15:10 Dichlorodifluoromethane 0.23 U 20 0.23 1 01/31/18 15:10 Ethylbenzene 0.21 U 1.0 0.21 1 01/31/18 15:10 Iodomethane 2.7 U 5.0 2.7 1 01/31/18 15:10 m,p-Xylenes 0.31 U 2.0 0.31 1 01/31/18 15:10 Methyl tert-Butyl Ether 0.24 U 2.0 0.24 1 01/31/18 15:10 Methylene Chloride 0.21 U 5.0 0.21 1 01/31/18 15:10 o-Xylene 0.14 U 1.0 0.14 1 01/31/18 15:10 Styrene 0.29 U 1.0 0.29 1 01/31/18 15:10 Tetrachloroethene (PCE) 0.22 U 1.0 0.22 1 01/31/18 15:10 Toluene 0.19 U 1.0 0.19 1 01/31/18 15:10 Printed 2/5/2018 3:02:13 PM Page 55 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 15:25 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-2 Units: ug/L Lab Code: J1800711-013 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q trans-1,2-Dichloroethene 0.19 U 1.0 0.19 1 01/31/18 15:10 trans- l,3-Dichloropropene 0.23 U 1.0 0.23 1 01/31/18 15:10 trans-1,4-Dichloro-2-butene 2.2 U 20 2.2 1 01/31/18 15:10 Trichloroethene (TCE) 0.36 U 1.0 0.36 1 01/31/18 15:10 Trichlorofluoromethane 0.24 U 20 0.24 1 01/31/18 15:10 Vinyl Acetate 1.9 U 10 1.9 1 01/31/18 15:10 Vinyl Chloride 0.36 U 1.0 0.36 1 01/31/18 15:10 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 103 72 - 127 01/31/18 15:10 4-Bromofluorobenzene 99 88 - 120 01/31/18 15:10 Dibromofluoromethane 104 85 - 115 01/31/18 15:10 Toluene-d8 96 83 - 123 01/31/18 15:10 Printed 2/5/2018 3:02:13 PM Page 56 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 16:50 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-4 Units: ug/L Lab Code: J1800711-014 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q 1, 1, 1,2-Tetrachloroethane 0.19 U 1.0 0.19 1 01/31/18 15:32 1, 1, 1 -Trichloroethane (TCA) 0.17 U 1.0 0.17 1 01/31/18 15:32 1,1,2,2-Tetrachloroethane 0.29 U 1.0 0.29 1 01/31/18 15:32 1,1,2-Trichloroethane 0.40 U 1.0 0.40 1 01/31/18 15:32 1, 1 -Dichloroethane (1,1-DCA) 0.30 U 1.0 0.30 1 01/31/18 15:32 1, 1 -Dichloroethene (1,1-DCE) 0.16 U 1.0 0.16 1 01/31/18 15:32 1,2,3-Trichloropropane 0.42 U 2.0 0.42 1 01/31/18 15:32 1,2-Dibromo-3-chloropropane (DBCP) 2.3 U 5.0 2.3 1 01/31/18 15:32 1,2-Dibromoethane (EDB) 0.46 U 1.0 0.46 1 01/31/18 15:32 1,2-Dichlorobenzene 0.48 U 1.0 0.48 1 01/31/18 15:32 1,2-Dichloroethane 0.22 U 1.0 0.22 1 01/31/18 15:32 1,2-Dichloropropane 0.19 U 1.0 0.19 1 01/31/18 15:32 1,3-Dichlorobenzene 0.22 U 1.0 0.22 1 01/31/18 15:32 1,4-Dichlorobenzene 0.16 U 1.0 0.16 1 01/31/18 15:32 2-Butanone (MEK) 3.8 U 10 3.8 1 01/31/18 15:32 2-Hexanone 2.2 U 25 2.2 1 01/31/18 15:32 4-Methyl-2-pentanone (MIBK) 1.1 U 25 1.1 1 01/31/18 15:32 Acetone 5.6 U 20 5.6 1 01/31/18 15:32 Benzene 0.21 U 1.0 0.21 1 01/31/18 15:32 Bromochloromethane 0.27 U 5.0 0.27 1 01/31/18 15:32 Bromodichloromethane 0.22 U 1.0 0.22 1 01/31/18 15:32 Bromoform 0.42 U 2.0 0.42 1 01/31/18 15:32 Bromomethane 0.23 U 5.0 0.23 1 01/31/18 15:32 Carbon Disulfide 2.4 U 10 2.4 1 01/31/18 15:32 Carbon Tetrachloride 0.34 U 1.0 0.34 1 01/31/18 15:32 Chlorobenzene 0.16 U 1.0 0.16 1 01/31/18 15:32 Chloroethane 0.52 U 5.0 0.52 1 01/31/18 15:32 Chloroform 0.35 U 1.0 0.35 1 01/31/18 15:32 Chloromethane 0.36 U 1.0 0.36 1 01/31/18 15:32 cis-1,2-Dichloroethene 0.36 U 1.0 0.36 1 01/31/18 15:32 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 1 01/31/18 15:32 Dibromochloromethane 0.21 U 1.0 0.21 1 01/31/18 15:32 Dibromomethane 0.36 U 5.0 0.36 1 01/31/18 15:32 Dichlorodifluoromethane 0.23 U 20 0.23 1 01/31/18 15:32 Ethylbenzene 0.21 U 1.0 0.21 1 01/31/18 15:32 Iodomethane 2.7 U 5.0 2.7 1 01/31/18 15:32 m,p-Xylenes 0.31 U 2.0 0.31 1 01/31/18 15:32 Methyl tert-Butyl Ether 0.24 U 2.0 0.24 1 01/31/18 15:32 Methylene Chloride 0.21 U 5.0 0.21 1 01/31/18 15:32 o-Xylene 0.14 U 1.0 0.14 1 01/31/18 15:32 Styrene 0.29 U 1.0 0.29 1 01/31/18 15:32 Tetrachloroethene (PCE) 0.22 U 1.0 0.22 1 01/31/18 15:32 Toluene 0.19 U 1.0 0.19 1 01/31/18 15:32 Printed 2/5/2018 3:02:13 PM Page 57 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 16:50 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-4 Units: ug/L Lab Code: J1800711-014 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q trans-1,2-Dichloroethene 0.19 U 1.0 0.19 1 01/31/18 15:32 trans- l,3-Dichloropropene 0.23 U 1.0 0.23 1 01/31/18 15:32 trans-1,4-Dichloro-2-butene 2.2 U 20 2.2 1 01/31/18 15:32 Trichloroethene (TCE) 0.36 U 1.0 0.36 1 01/31/18 15:32 Trichlorofluoromethane 0.24 U 20 0.24 1 01/31/18 15:32 Vinyl Acetate 1.9 U 10 1.9 1 01/31/18 15:32 Vinyl Chloride 0.36 U 1.0 0.36 1 01/31/18 15:32 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 107 72 - 127 01/31/18 15:32 4-Bromofluorobenzene 99 88 - 120 01/31/18 15:32 Dibromofluoromethane 107 85 - 115 01/31/18 15:32 Toluene-d8 95 83 - 123 01/31/18 15:32 Printed 2/5/2018 3:02:13 PM Page 58 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 17:20 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-5 Units: ug/L Lab Code: J1800711-015 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q 1, 1, 1,2-Tetrachloroethane 0.19 U 1.0 0.19 1 01/31/18 15:54 1, 1, 1 -Trichloroethane (TCA) 0.17 U 1.0 0.17 1 01/31/18 15:54 1,1,2,2-Tetrachloroethane 0.29 U 1.0 0.29 1 01/31/18 15:54 1,1,2-Trichloroethane 0.40 U 1.0 0.40 1 01/31/18 15:54 1, 1 -Dichloroethane (1,1-DCA) 0.30 U 1.0 0.30 1 01/31/18 15:54 1, 1 -Dichloroethene (1,1-DCE) 0.16 U 1.0 0.16 1 01/31/18 15:54 1,2,3-Trichloropropane 0.42 U 2.0 0.42 1 01/31/18 15:54 1,2-Dibromo-3-chloropropane (DBCP) 2.3 U 5.0 2.3 1 01/31/18 15:54 1,2-Dibromoethane (EDB) 0.46 U 1.0 0.46 1 01/31/18 15:54 1,2-Dichlorobenzene 0.48 U 1.0 0.48 1 01/31/18 15:54 1,2-Dichloroethane 0.22 U 1.0 0.22 1 01/31/18 15:54 1,2-Dichloropropane 0.19 U 1.0 0.19 1 01/31/18 15:54 1,3-Dichlorobenzene 0.22 U 1.0 0.22 1 01/31/18 15:54 1,4-Dichlorobenzene 0.16 U 1.0 0.16 1 01/31/18 15:54 2-Butanone (MEK) 3.8 U 10 3.8 1 01/31/18 15:54 2-Hexanone 2.2 U 25 2.2 1 01/31/18 15:54 4-Methyl-2-pentanone (MIBK) 1.1 U 25 1.1 1 01/31/18 15:54 Acetone 5.6 U 20 5.6 1 01/31/18 15:54 Benzene 0.21 U 1.0 0.21 1 01/31/18 15:54 Bromochloromethane 0.27 U 5.0 0.27 1 01/31/18 15:54 Bromodichloromethane 0.22 U 1.0 0.22 1 01/31/18 15:54 Bromoform 0.42 U 2.0 0.42 1 01/31/18 15:54 Bromomethane 0.23 U 5.0 0.23 1 01/31/18 15:54 Carbon Disulfide 2.4 U 10 2.4 1 01/31/18 15:54 Carbon Tetrachloride 0.34 U 1.0 0.34 1 01/31/18 15:54 Chlorobenzene 0.16 U 1.0 0.16 1 01/31/18 15:54 Chloroethane 0.52 U 5.0 0.52 1 01/31/18 15:54 Chloroform 0.35 U 1.0 0.35 1 01/31/18 15:54 Chloromethane 0.36 U 1.0 0.36 1 01/31/18 15:54 cis-1,2-Dichloroethene 0.36 U 1.0 0.36 1 01/31/18 15:54 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 1 01/31/18 15:54 Dibromochloromethane 0.21 U 1.0 0.21 1 01/31/18 15:54 Dibromomethane 0.36 U 5.0 0.36 1 01/31/18 15:54 Dichlorodifluoromethane 0.23 U 20 0.23 1 01/31/18 15:54 Ethylbenzene 0.21 U 1.0 0.21 1 01/31/18 15:54 Iodomethane 2.7 U 5.0 2.7 1 01/31/18 15:54 m,p-Xylenes 0.31 U 2.0 0.31 1 01/31/18 15:54 Methyl tert-Butyl Ether 0.24 U 2.0 0.24 1 01/31/18 15:54 Methylene Chloride 0.21 U 5.0 0.21 1 01/31/18 15:54 o-Xylene 0.14 U 1.0 0.14 1 01/31/18 15:54 Styrene 0.29 U 1.0 0.29 1 01/31/18 15:54 Tetrachloroethene (PCE) 0.22 U 1.0 0.22 1 01/31/18 15:54 Toluene 0.19 U 1.0 0.19 1 01/31/18 15:54 Printed 2/5/2018 3:02:14 PM Page 59 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 17:20 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-5 Units: ug/L Lab Code: J1800711-015 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q trans-1,2-Dichloroethene 0.19 U 1.0 0.19 1 01/31/18 15:54 trans- l,3-Dichloropropene 0.23 U 1.0 0.23 1 01/31/18 15:54 trans-1,4-Dichloro-2-butene 2.2 U 20 2.2 1 01/31/18 15:54 Trichloroethene (TCE) 0.36 U 1.0 0.36 1 01/31/18 15:54 Trichlorofluoromethane 0.24 U 20 0.24 1 01/31/18 15:54 Vinyl Acetate 1.9 U 10 1.9 1 01/31/18 15:54 Vinyl Chloride 0.36 U 1.0 0.36 1 01/31/18 15:54 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 110 72 - 127 01/31/18 15:54 4-Bromofluorobenzene 96 88 - 120 01/31/18 15:54 Dibromofluoromethane 108 85 - 115 01/31/18 15:54 Toluene-d8 94 83 - 123 01/31/18 15:54 Printed 2/5/2018 3:02:14 PM Page 60 of 184 Superset Reference:18-0000453045 rev 00 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 61 of 184 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 08:50 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-1-1 Units: ug/Kg Lab Code: J1800711-001 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 69.0 U 186 69.0 1 01/30/18 22:40 1/30/18 1,2-Dichlorobenzene 35.1 U 186 35.1 1 01/30/18 22:40 1/30/18 1,3-Dichlorobenzene 41.6 U 186 41.6 1 01/30/18 22:40 1/30/18 1,4-Dichlorobenzene 44.9 U 186 44.9 1 01/30/18 22:40 1/30/18 1-Methylnaphthalene 365 186 72.3 1 01/30/18 22:40 1/30/18 2,4,5-Trichlorophenol 62.4 U 186 62.4 1 01/30/18 22:40 1/30/18 2,4,6-Trichlorophenol 54.8 U 186 54.8 1 01/30/18 22:40 1/30/18 2,4-Dichlorophenol 69.0 U 186 69.0 1 01/30/18 22:40 1/30/18 2,4-Dimethylphenol 90.9 U 186 90.9 1 01/30/18 22:40 1/30/18 2,4-Dinitrophenol 25.2 U 733 25.2 1 01/30/18 22:40 1/30/18 2,4-Dinitrotoluene 44.9 U 186 44.9 1 01/30/18 22:40 1/30/18 2,6-Dinitrotoluene 52.6 U 186 52.6 1 01/30/18 22:40 1/30/18 2-Chloronaphthalene 47.1 U 186 47.1 1 01/30/18 22:40 1/30/18 2-Chlorophenol 38.3 U 186 38.3 1 01/30/18 22:40 1/30/18 2-Methylnaphthalene 493 186 64.6 1 01/30/18 22:40 1/30/18 2-Methylphenol 52.6 U 186 52.6 1 01/30/18 22:40 1/30/18 2-Nitroaniline 55.9 U 186 55.9 1 01/30/18 22:40 1/30/18 2-Nitrophenol 57.0 U 733 57.0 1 01/30/18 22:40 1/30/18 3- and 4-Methylphenol Coelution 47.1 U 186 47.1 1 01/30/18 22:40 1/30/18 3,3'-Dichlorobenzidine 93.1 U 733 93.1 1 01/30/18 22:40 1/30/18 3-Nitroaniline 55.9 U 186 55.9 1 01/30/18 22:40 1/30/18 4,6-Dinitro-2-methylphenol 52.6 U 733 52.6 1 01/30/18 22:40 1/30/18 4-Bromophenyl Phenyl Ether 57.0 U 186 57.0 1 01/30/18 22:40 1/30/18 4-Chloro-3-methylphenol 58.0 U 186 58.0 1 01/30/18 22:40 1/30/18 4-Chloroaniline 75.6 U 186 75.6 1 01/30/18 22:40 1/30/18 4-Chlorophenyl Phenyl Ether 57.0 U 186 57.0 1 01/30/18 22:40 1/30/18 4-Nitroaniline 60.2 U 186 60.2 1 01/30/18 22:40 1/30/18 4-Nitrophenol 61.3 U 733 61.3 1 01/30/18 22:40 1/30/18 Acenaphthene 58.0 U 186 58.0 1 01/30/18 22:40 1/30/18 Acenaphthylene 51.5 U 186 51.5 1 01/30/18 22:40 1/30/18 Acetophenone 52.9 I 372 50.4 1 01/30/18 22:40 1/30/18 Anthracene 418 186 47.1 1 01/30/18 22:40 1/30/18 Benz(a)anthracene 123 I 186 51.5 1 01/30/18 22:40 1/30/18 Benzo(a)pyrene 93.4 I 186 40.5 1 01/30/18 22:40 1/30/18 Benzo(b)fluoranthene 113 I 186 28.5 1 01/30/18 22:40 1/30/18 Benzo(g,h,i)perylene 83.5 I 186 57.0 1 01/30/18 22:40 1/30/18 Benzo(k)fluoranthene 72.2 I 186 64.6 1 01/30/18 22:40 1/30/18 Benzyl Alcohol 41.6 U 372 41.6 1 01/30/18 22:40 1/30/18 Bis(2-chloroethoxy)methane 58.0 U 186 58.0 1 01/30/18 22:40 1/30/18 Bis(2-chloroethyl) Ether 46.0 U 186 46.0 1 01/30/18 22:40 1/30/18 Bis(2-chloroisopropyl) Ether 38.3 U 186 38.3 1 01/30/18 22:40 1/30/18 Bis(2-ethylhexyl) Phthalate 48.2 U 186 48.2 1 01/30/18 22:40 1/30/18 Butyl Benzyl Phthalate 51.5 U 372 51.5 1 01/30/18 22:40 1/30/18 Printed 2/5/2018 3:02:42 PM Page 62 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 08:50 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-1-1 Units: ug/Kg Lab Code: J1800711-001 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 62.4 U 186 62.4 1 01/30/18 22:40 1/30/18 Chrysene 232 186 49.3 1 01/30/18 22:40 1/30/18 Dibenz(a,h)anthracene 50.4 U 186 50.4 1 01/30/18 22:40 1/30/18 Dibenzofuran 114 I 186 50.4 1 01/30/18 22:40 1/30/18 Diethyl Phthalate 55.9 U 186 55.9 1 01/30/18 22:40 1/30/18 Dimethyl Phthalate 58.0 U 186 58.0 1 01/30/18 22:40 1/30/18 Di-n-butyl Phthalate 37.3 U 186 37.3 1 01/30/18 22:40 1/30/18 Di-n-octyl Phthalate 57.0 U 372 57.0 1 01/30/18 22:40 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 40.5 U 186 40.5 1 01/30/18 22:40 1/30/18 Fluoranthene 151 I 186 52.6 1 01/30/18 22:40 1/30/18 Fluorene 51.5 U 186 51.5 1 01/30/18 22:40 1/30/18 Hexachlorobenzene 52.6 U 186 52.6 1 01/30/18 22:40 1/30/18 Hexachlorobutadiene 60.2 U 186 60.2 1 01/30/18 22:40 1/30/18 Hexachlorocyclopentadiene 37.3 U 186 37.3 1 01/30/18 22:40 1/30/18 Hexachloroethane 34.0 U 186 34.0 1 01/30/18 22:40 1/30/18 Indeno(1,2,3-cd)pyrene 55.8 I 186 44.9 1 01/30/18 22:40 1/30/18 Isophorone 63.5 U 186 63.5 1 01/30/18 22:40 1/30/18 Naphthalene 428 186 53.7 1 01/30/18 22:40 1/30/18 Nitrobenzene 42.7 U 186 42.7 1 01/30/18 22:40 1/30/18 N-Nitrosodi-n-propylamine 54.8 U 186 54.8 1 01/30/18 22:40 1/30/18 Pentachlorophenol (PCP) 38.3 U 733 38.3 1 01/30/18 22:40 1/30/18 Phenanthrene 425 186 46.0 1 01/30/18 22:40 1/30/18 Phenol 50.4 U 186 50.4 1 01/30/18 22:40 1/30/18 Pyrene 181 I 186 50.4 1 01/30/18 22:40 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 45 30 - 136 01/30/18 22:40 2-Fluorobiphenyl 57 20 - 115 01/30/18 22:40 2-Fluorophenol 39 10 - 110 01/30/18 22:40 Nitrobenzene-d5 56 20 - 110 01/30/18 22:40 Phenol-d6 45 14 - 100 01/30/18 22:40 p-Terphenyl-dl4 69 32 - 119 01/30/18 22:40 Printed 2/5/2018 3:02:42 PM Page 63 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 09:30 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-1-17 Units: ug/Kg Lab Code: J1800711-002 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 656 U 1770 656 10 01/30/18 23:05 1/30/18 1,2-Dichlorobenzene 333 U 1770 333 10 01/30/18 23:05 1/30/18 1,3-Dichlorobenzene 396 U 1770 396 10 01/30/18 23:05 1/30/18 1,4-Dichlorobenzene 427 U 1770 427 10 01/30/18 23:05 1/30/18 1-Methylnaphthalene 687 U 1770 687 10 01/30/18 23:05 1/30/18 2,4,5-Trichlorophenol 594 U 1770 594 10 01/30/18 23:05 1/30/18 2,4,6-Trichlorophenol 521 U 1770 521 10 01/30/18 23:05 1/30/18 2,4-Dichlorophenol 656 U 1770 656 10 01/30/18 23:05 1/30/18 2,4-Dimethylphenol 864 U 1770 864 10 01/30/18 23:05 1/30/18 2,4-Dinitrophenol 240 U 6970 240 10 01/30/18 23:05 1/30/18 2,4-Dinitrotoluene 427 U 1770 427 10 01/30/18 23:05 1/30/18 2,6-Dinitrotoluene 500 U 1770 500 10 01/30/18 23:05 1/30/18 2-Chloronaphthalene 448 U 1770 448 10 01/30/18 23:05 1/30/18 2-Chlorophenol 365 U 1770 365 10 01/30/18 23:05 1/30/18 2-Methylnaphthalene 614 U 1770 614 10 01/30/18 23:05 1/30/18 2-Methylphenol 500 U 1770 500 10 01/30/18 23:05 1/30/18 2-Nitroaniline 531 U 1770 531 10 01/30/18 23:05 1/30/18 2-Nitrophenol 542 U 6970 542 10 01/30/18 23:05 1/30/18 3- and 4-Methylphenol Coelution 448 U 1770 448 10 01/30/18 23:05 1/30/18 3,3'-Dichlorobenzidine 885 U 6970 885 10 01/30/18 23:05 1/30/18 3-Nitroaniline 531 U 1770 531 10 01/30/18 23:05 1/30/18 4,6-Dinitro-2-methylphenol 500 U 6970 500 10 01/30/18 23:05 1/30/18 4-Bromophenyl Phenyl Ether 542 U 1770 542 10 01/30/18 23:05 1/30/18 4-Chloro-3-methylphenol 552 U 1770 552 10 01/30/18 23:05 1/30/18 4-Chloroaniline 719 U 1770 719 10 01/30/18 23:05 1/30/18 4-Chlorophenyl Phenyl Ether 542 U 1770 542 10 01/30/18 23:05 1/30/18 4-Nitroaniline 573 U 1770 573 10 01/30/18 23:05 1/30/18 4-Nitrophenol 583 U 6970 583 10 01/30/18 23:05 1/30/18 Acenaphthene 552 U 1770 552 10 01/30/18 23:05 1/30/18 Acenaphthylene 490 U 1770 490 10 01/30/18 23:05 1/30/18 Acetophenone 479 U 3540 479 10 01/30/18 23:05 1/30/18 Anthracene 448 U 1770 448 10 01/30/18 23:05 1/30/18 Benz(a)anthracene 490 U 1770 490 10 01/30/18 23:05 1/30/18 Benzo(a)pyrene 386 U 1770 386 10 01/30/18 23:05 1/30/18 Benzo(k)fluoranthene 271 U 1770 271 10 01/30/18 23:05 1/30/18 Benzo(g,h,i)perylene 542 U 1770 542 10 01/30/18 23:05 1/30/18 Benzo(k)fluoranthene 614 U 1770 614 10 01/30/18 23:05 1/30/18 Benzyl Alcohol 396 U 3540 396 10 01/30/18 23:05 1/30/18 Bis(2-chloroethoxy)methane 552 U 1770 552 10 01/30/18 23:05 1/30/18 Bis(2-chloroethyl) Ether 438 U 1770 438 10 01/30/18 23:05 1/30/18 Bis(2-chloroisopropyl) Ether 365 U 1770 365 10 01/30/18 23:05 1/30/18 Bis(2-ethylhexyl) Phthalate 458 U 1770 458 10 01/30/18 23:05 1/30/18 Butyl Benzyl Phthalate 490 U 3540 490 10 01/30/18 23:05 1/30/18 Printed 2/5/2018 3:02:43 PM Page 64 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 09:30 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-1-17 Units: ug/Kg Lab Code: J1800711-002 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 594 U 1770 594 10 01/30/18 23:05 1/30/18 Chrysene 469 U 1770 469 10 01/30/18 23:05 1/30/18 Dibenz(a,h)anthracene 479 U 1770 479 10 01/30/18 23:05 1/30/18 Dibenzofuran 479 U 1770 479 10 01/30/18 23:05 1/30/18 Diethyl Phthalate 531 U 1770 531 10 01/30/18 23:05 1/30/18 Dimethyl Phthalate 552 U 1770 552 10 01/30/18 23:05 1/30/18 Di-n-butyl Phthalate 354 U 1770 354 10 01/30/18 23:05 1/30/18 Di-n-octyl Phthalate 542 U 3540 542 10 01/30/18 23:05 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 386 U 1770 386 10 01/30/18 23:05 1/30/18 Fluoranthene 500 U 1770 500 10 01/30/18 23:05 1/30/18 Fluorene 490 U 1770 490 10 01/30/18 23:05 1/30/18 Hexachlorobenzene 500 U 1770 500 10 01/30/18 23:05 1/30/18 Hexachlorobutadiene 573 U 1770 573 10 01/30/18 23:05 1/30/18 Hexachlorocyclopentadiene 354 U 1770 354 10 01/30/18 23:05 1/30/18 Hexachloroethane 323 U 1770 323 10 01/30/18 23:05 1/30/18 Indeno(1,2,3-cd)pyrene 427 U 1770 427 10 01/30/18 23:05 1/30/18 Isophorone 604 U 1770 604 10 01/30/18 23:05 1/30/18 Naphthalene 510 U 1770 510 10 01/30/18 23:05 1/30/18 Nitrobenzene 406 U 1770 406 10 01/30/18 23:05 1/30/18 N-Nitrosodi-n-propylamine 521 U 1770 521 10 01/30/18 23:05 1/30/18 Pentachlorophenol (PCP) 365 U 6970 365 10 01/30/18 23:05 1/30/18 Phenanthrene 438 U 1770 438 10 01/30/18 23:05 1/30/18 Phenol 479 U 1770 479 10 01/30/18 23:05 1/30/18 Pyrene 479 U 1770 479 10 01/30/18 23:05 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 39 30 - 136 01/30/18 23:05 2-Fluorobiphenyl 65 20 - 115 01/30/18 23:05 2-Fluorophenol 50 10 - 110 01/30/18 23:05 Nitrobenzene-d5 58 20 - 110 01/30/18 23:05 Phenol-d6 51 14 - 100 01/30/18 23:05 p-Terphenyl-dl4 79 32 - 119 01/30/18 23:05 Printed 2/5/2018 3:02:43 PM Page 65 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:00 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-2-1 Units: ug/Kg Lab Code: J1800711-003 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 63.0 U 170 63.0 1 01/31/18 00:19 1/30/18 1,2-Dichlorobenzene 32.0 U 170 32.0 1 01/31/18 00:19 1/30/18 1,3-Dichlorobenzene 38.0 U 170 38.0 1 01/31/18 00:19 1/30/18 1,4-Dichlorobenzene 41.0 U 170 41.0 1 01/31/18 00:19 1/30/18 1-Methylnaphthalene 66.0 U 170 66.0 1 01/31/18 00:19 1/30/18 2,4,5-Trichlorophenol 57.0 U 170 57.0 1 01/31/18 00:19 1/30/18 2,4,6-Trichlorophenol 50.0 U 170 50.0 1 01/31/18 00:19 1/30/18 2,4-Dichlorophenol 63.0 U 170 63.0 1 01/31/18 00:19 1/30/18 2,4-Dimethylphenol 83.0 U 170 83.0 1 01/31/18 00:19 1/30/18 2,4-Dinitrophenol 23.0 U 670 23.0 1 01/31/18 00:19 1/30/18 2,4-Dinitrotoluene 41.0 U 170 41.0 1 01/31/18 00:19 1/30/18 2,6-Dinitrotoluene 48.0 U 170 48.0 1 01/31/18 00:19 1/30/18 2-Chloronaphthalene 43.0 U 170 43.0 1 01/31/18 00:19 1/30/18 2-Chlorophenol 35.0 U 170 35.0 1 01/31/18 00:19 1/30/18 2-Methylnaphthalene 59.0 U 170 59.0 1 01/31/18 00:19 1/30/18 2-Methylphenol 48.0 U 170 48.0 1 01/31/18 00:19 1/30/18 2-Nitroaniline 51.0 U 170 51.0 1 01/31/18 00:19 1/30/18 2-Nitrophenol 52.0 U 670 52.0 1 01/31/18 00:19 1/30/18 3- and 4-Methylphenol Coelution 43.0 U 170 43.0 1 01/31/18 00:19 1/30/18 3,3'-Dichlorobenzidine 85.0 U 670 85.0 1 01/31/18 00:19 1/30/18 3-Nitroaniline 51.0 U 170 51.0 1 01/31/18 00:19 1/30/18 4,6-Dinitro-2-methylphenol 48.0 U 670 48.0 1 01/31/18 00:19 1/30/18 4-Bromophenyl Phenyl Ether 52.0 U 170 52.0 1 01/31/18 00:19 1/30/18 4-Chloro-3-methylphenol 53.0 U 170 53.0 1 01/31/18 00:19 1/30/18 4-Chloroaniline 69.0 U 170 69.0 1 01/31/18 00:19 1/30/18 4-Chlorophenyl Phenyl Ether 52.0 U 170 52.0 1 01/31/18 00:19 1/30/18 4-Nitroaniline 55.0 U 170 55.0 1 01/31/18 00:19 1/30/18 4-Nitrophenol 56.0 U 670 56.0 1 01/31/18 00:19 1/30/18 Acenaphthene 53.0 U 170 53.0 1 01/31/18 00:19 1/30/18 Acenaphthylene 47.0 U 170 47.0 1 01/31/18 00:19 1/30/18 Acetophenone 46.0 U 340 46.0 1 01/31/18 00:19 1/30/18 Anthracene 43.0 U 170 43.0 1 01/31/18 00:19 1/30/18 Benz(a)anthracene 47.0 U 170 47.0 1 01/31/18 00:19 1/30/18 Benzo(a)pyrene 37.0 U 170 37.0 1 01/31/18 00:19 1/30/18 Benzo(b)fluoranthene 26.0 U 170 26.0 1 01/31/18 00:19 1/30/18 Benzo(g,h,i)perylene 52.0 U 170 52.0 1 01/31/18 00:19 1/30/18 Benzo(k)fluoranthene 59.0 U 170 59.0 1 01/31/18 00:19 1/30/18 Benzyl Alcohol 38.0 U 340 38.0 1 01/31/18 00:19 1/30/18 Bis(2-chloroethoxy)methane 53.0 U 170 53.0 1 01/31/18 00:19 1/30/18 Bis(2-chloroethyl) Ether 42.0 U 170 42.0 1 01/31/18 00:19 1/30/18 Bis(2-chloroisopropyl) Ether 35.0 U 170 35.0 1 01/31/18 00:19 1/30/18 Bis(2-ethylhexyl) Phthalate 44.0 U 170 44.0 1 01/31/18 00:19 1/30/18 Butyl Benzyl Phthalate 47.0 U 340 47.0 1 01/31/18 00:19 1/30/18 Printed 2/5/2018 3:02:43 PM Page 66 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:00 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-2-1 Units: ug/Kg Lab Code: J1800711-003 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 57.0 U 170 57.0 1 01/31/18 00:19 1/30/18 Chrysene 45.0 U 170 45.0 1 01/31/18 00:19 1/30/18 Dibenz(a,h)anthracene 46.0 U 170 46.0 1 01/31/18 00:19 1/30/18 Dibenzofuran 46.0 U 170 46.0 1 01/31/18 00:19 1/30/18 Diethyl Phthalate 51.0 U 170 51.0 1 01/31/18 00:19 1/30/18 Dimethyl Phthalate 53.0 U 170 53.0 1 01/31/18 00:19 1/30/18 Di-n-butyl Phthalate 34.0 U 170 34.0 1 01/31/18 00:19 1/30/18 Di-n-octyl Phthalate 52.0 U 340 52.0 1 01/31/18 00:19 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 37.0 U 170 37.0 1 01/31/18 00:19 1/30/18 Fluoranthene 48.0 U 170 48.0 1 01/31/18 00:19 1/30/18 Fluorene 47.0 U 170 47.0 1 01/31/18 00:19 1/30/18 Hexachlorobenzene 48.0 U 170 48.0 1 01/31/18 00:19 1/30/18 Hexachlorobutadiene 55.0 U 170 55.0 1 01/31/18 00:19 1/30/18 Hexachlorocyclopentadiene 34.0 U 170 34.0 1 01/31/18 00:19 1/30/18 Hexachloroethane 31.0 U 170 31.0 1 01/31/18 00:19 1/30/18 Indeno(1,2,3-cd)pyrene 41.0 U 170 41.0 1 01/31/18 00:19 1/30/18 Isophorone 58.0 U 170 58.0 1 01/31/18 00:19 1/30/18 Naphthalene 49.0 U 170 49.0 1 01/31/18 00:19 1/30/18 Nitrobenzene 39.0 U 170 39.0 1 01/31/18 00:19 1/30/18 N-Nitrosodi-n-propylamine 50.0 U 170 50.0 1 01/31/18 00:19 1/30/18 Pentachlorophenol (PCP) 35.0 U 670 35.0 1 01/31/18 00:19 1/30/18 Phenanthrene 42.0 U 170 42.0 1 01/31/18 00:19 1/30/18 Phenol 46.0 U 170 46.0 1 01/31/18 00:19 1/30/18 Pyrene 46.0 U 170 46.0 1 01/31/18 00:19 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 51 30 - 136 01/31/18 00:19 2-Fluorobiphenyl 58 20 - 115 01/31/18 00:19 2-Fluorophenol 55 10 - 110 01/31/18 00:19 Nitrobenzene-d5 60 20 - 110 01/31/18 00:19 Phenol-d6 61 14 - 100 01/31/18 00:19 p-Terphenyl-dl4 83 32 - 119 01/31/18 00:19 Printed 2/5/2018 3:02:43 PM Page 67 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:10 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-2-12 Units: ug/Kg Lab Code: J1800711-004 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 666 U 1800 666 10 01/31/18 00:44 1/30/18 1,2-Dichlorobenzene 339 U 1800 339 10 01/31/18 00:44 1/30/18 1,3-Dichlorobenzene 402 U 1800 402 10 01/31/18 00:44 1/30/18 1,4-Dichlorobenzene 434 U 1800 434 10 01/31/18 00:44 1/30/18 1-Methylnaphthalene 698 U 1800 698 10 01/31/18 00:44 1/30/18 2,4,5-Trichlorophenol 603 U 1800 603 10 01/31/18 00:44 1/30/18 2,4,6-Trichlorophenol 529 U 1800 529 10 01/31/18 00:44 1/30/18 2,4-Dichlorophenol 666 U 1800 666 10 01/31/18 00:44 1/30/18 2,4-Dimethylphenol 877 U 1800 877 10 01/31/18 00:44 1/30/18 2,4-Dinitrophenol 243 U 7080 243 10 01/31/18 00:44 1/30/18 2,4-Dinitrotoluene 434 U 1800 434 10 01/31/18 00:44 1/30/18 2,6-Dinitrotoluene 508 U 1800 508 10 01/31/18 00:44 1/30/18 2-Chloronaphthalene 455 U 1800 455 10 01/31/18 00:44 1/30/18 2-Chlorophenol 370 U 1800 370 10 01/31/18 00:44 1/30/18 2-Methylnaphthalene 624 U 1800 624 10 01/31/18 00:44 1/30/18 2-Methylphenol 508 U 1800 508 10 01/31/18 00:44 1/30/18 2-Nitroaniline 539 U 1800 539 10 01/31/18 00:44 1/30/18 2-Nitrophenol 550 U 7080 550 10 01/31/18 00:44 1/30/18 3- and 4-Methylphenol Coelution 455 U 1800 455 10 01/31/18 00:44 1/30/18 3,3'-Dichlorobenzidine 898 U 7080 898 10 01/31/18 00:44 1/30/18 3-Nitroaniline 539 U 1800 539 10 01/31/18 00:44 1/30/18 4,6-Dinitro-2-methylphenol 508 U 7080 508 10 01/31/18 00:44 1/30/18 4-Bromophenyl Phenyl Ether 550 U 1800 550 10 01/31/18 00:44 1/30/18 4-Chloro-3-methylphenol 560 U 1800 560 10 01/31/18 00:44 1/30/18 4-Chloroaniline 729 U 1800 729 10 01/31/18 00:44 1/30/18 4-Chlorophenyl Phenyl Ether 550 U 1800 550 10 01/31/18 00:44 1/30/18 4-Nitroaniline 582 U 1800 582 10 01/31/18 00:44 1/30/18 4-Nitrophenol 592 U 7080 592 10 01/31/18 00:44 1/30/18 Acenaphthene 560 U 1800 560 10 01/31/18 00:44 1/30/18 Acenaphthylene 497 U 1800 497 10 01/31/18 00:44 1/30/18 Acetophenone 486 U 3590 486 10 01/31/18 00:44 1/30/18 Anthracene 455 U 1800 455 10 01/31/18 00:44 1/30/18 Benz(a)anthracene 497 U 1800 497 10 01/31/18 00:44 1/30/18 Benzo(a)pyrene 391 U 1800 391 10 01/31/18 00:44 1/30/18 Benzo(k)fluoranthene 275 U 1800 275 10 01/31/18 00:44 1/30/18 Benzo(g,h,i)perylene 550 U 1800 550 10 01/31/18 00:44 1/30/18 Benzo(k)fluoranthene 624 U 1800 624 10 01/31/18 00:44 1/30/18 Benzyl Alcohol 402 U 3590 402 10 01/31/18 00:44 1/30/18 Bis(2-chloroethoxy)methane 560 U 1800 560 10 01/31/18 00:44 1/30/18 Bis(2-chloroethyl) Ether 444 U 1800 444 10 01/31/18 00:44 1/30/18 Bis(2-chloroisopropyl) Ether 370 U 1800 370 10 01/31/18 00:44 1/30/18 Bis(2-ethylhexyl) Phthalate 465 U 1800 465 10 01/31/18 00:44 1/30/18 Butyl Benzyl Phthalate 497 U 3590 497 10 01/31/18 00:44 1/30/18 Printed 2/5/2018 3:02:43 PM Page 68 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:10 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-2-12 Units: ug/Kg Lab Code: J1800711-004 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 603 U 1800 603 10 01/31/18 00:44 1/30/18 Chrysene 476 U 1800 476 10 01/31/18 00:44 1/30/18 Dibenz(a,h)anthracene 486 U 1800 486 10 01/31/18 00:44 1/30/18 Dibenzofuran 486 U 1800 486 10 01/31/18 00:44 1/30/18 Diethyl Phthalate 539 U 1800 539 10 01/31/18 00:44 1/30/18 Dimethyl Phthalate 560 U 1800 560 10 01/31/18 00:44 1/30/18 Di-n-butyl Phthalate 360 U 1800 360 10 01/31/18 00:44 1/30/18 Di-n-octyl Phthalate 550 U 3590 550 10 01/31/18 00:44 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 391 U 1800 391 10 01/31/18 00:44 1/30/18 Fluoranthene 508 U 1800 508 10 01/31/18 00:44 1/30/18 Fluorene 497 U 1800 497 10 01/31/18 00:44 1/30/18 Hexachlorobenzene 508 U 1800 508 10 01/31/18 00:44 1/30/18 Hexachlorobutadiene 582 U 1800 582 10 01/31/18 00:44 1/30/18 Hexachlorocyclopentadiene 360 U 1800 360 10 01/31/18 00:44 1/30/18 Hexachloroethane 328 U 1800 328 10 01/31/18 00:44 1/30/18 Indeno(1,2,3-cd)pyrene 434 U 1800 434 10 01/31/18 00:44 1/30/18 Isophorone 613 U 1800 613 10 01/31/18 00:44 1/30/18 Naphthalene 518 U 1800 518 10 01/31/18 00:44 1/30/18 Nitrobenzene 413 U 1800 413 10 01/31/18 00:44 1/30/18 N-Nitrosodi-n-propylamine 529 U 1800 529 10 01/31/18 00:44 1/30/18 Pentachlorophenol (PCP) 370 U 7080 370 10 01/31/18 00:44 1/30/18 Phenanthrene 444 U 1800 444 10 01/31/18 00:44 1/30/18 Phenol 486 U 1800 486 10 01/31/18 00:44 1/30/18 Pyrene 486 U 1800 486 10 01/31/18 00:44 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 40 30 - 136 01/31/18 00:44 2-Fluorobiphenyl 70 20 - 115 01/31/18 00:44 2-Fluorophenol 63 10 - 110 01/31/18 00:44 Nitrobenzene-d5 64 20 - 110 01/31/18 00:44 Phenol-d6 65 14 - 100 01/31/18 00:44 p-Terphenyl-dl4 83 32 - 119 01/31/18 00:44 Printed 2/5/2018 3:02:43 PM Page 69 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:25 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-3-1 Units: ug/Kg Lab Code: J1800711-005 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 735 U 1980 735 10 01/31/18 01:09 1/30/18 1,2-Dichlorobenzene 373 U 1980 373 10 01/31/18 01:09 1/30/18 1,3-Dichlorobenzene 443 U 1980 443 10 01/31/18 01:09 1/30/18 1,4-Dichlorobenzene 478 U 1980 478 10 01/31/18 01:09 1/30/18 1-Methylnaphthalene 770 U 1980 770 10 01/31/18 01:09 1/30/18 2,4,5-Trichlorophenol 665 U 1980 665 10 01/31/18 01:09 1/30/18 2,4,6-Trichlorophenol 583 U 1980 583 10 01/31/18 01:09 1/30/18 2,4-Dichlorophenol 735 U 1980 735 10 01/31/18 01:09 1/30/18 2,4-Dimethylphenol 968 U 1980 968 10 01/31/18 01:09 1/30/18 2,4-Dinitrophenol 268 U 7810 268 10 01/31/18 01:09 1/30/18 2,4-Dinitrotoluene 478 U 1980 478 10 01/31/18 01:09 1/30/18 2,6-Dinitrotoluene 560 U 1980 560 10 01/31/18 01:09 1/30/18 2-Chloronaphthalene 502 U 1980 502 10 01/31/18 01:09 1/30/18 2-Chlorophenol 408 U 1980 408 10 01/31/18 01:09 1/30/18 2-Methylnaphthalene 688 U 1980 688 10 01/31/18 01:09 1/30/18 2-Methylphenol 560 U 1980 560 10 01/31/18 01:09 1/30/18 2-Nitroaniline 595 U 1980 595 10 01/31/18 01:09 1/30/18 2-Nitrophenol 606 U 7810 606 10 01/31/18 01:09 1/30/18 3- and 4-Methylphenol Coelution 502 U 1980 502 10 01/31/18 01:09 1/30/18 3,3'-Dichlorobenzidine 991 U 7810 991 10 01/31/18 01:09 1/30/18 3-Nitroaniline 595 U 1980 595 10 01/31/18 01:09 1/30/18 4,6-Dinitro-2-methylphenol 560 U 7810 560 10 01/31/18 01:09 1/30/18 4-Bromophenyl Phenyl Ether 606 U 1980 606 10 01/31/18 01:09 1/30/18 4-Chloro-3-methylphenol 618 U 1980 618 10 01/31/18 01:09 1/30/18 4-Chloroaniline 804 U 1980 804 10 01/31/18 01:09 1/30/18 4-Chlorophenyl Phenyl Ether 606 U 1980 606 10 01/31/18 01:09 1/30/18 4-Nitroaniline 641 U 1980 641 10 01/31/18 01:09 1/30/18 4-Nitrophenol 653 U 7810 653 10 01/31/18 01:09 1/30/18 Acenaphthene 618 U 1980 618 10 01/31/18 01:09 1/30/18 Acenaphthylene 548 U 1980 548 10 01/31/18 01:09 1/30/18 Acetophenone 536 U 3960 536 10 01/31/18 01:09 1/30/18 Anthracene 502 U 1980 502 10 01/31/18 01:09 1/30/18 Benz(a)anthracene 1480 I 1980 548 10 01/31/18 01:09 1/30/18 Benzo(a)pyrene 1150 I 1980 432 10 01/31/18 01:09 1/30/18 Benzo(b)fluoranthene 1190 I 1980 303 10 01/31/18 01:09 1/30/18 Benzo(g,h,i)perylene 684 I 1980 606 10 01/31/18 01:09 1/30/18 Benzo(k)fluoranthene 1150 I 1980 688 10 01/31/18 01:09 1/30/18 Benzyl Alcohol 443 U 3960 443 10 01/31/18 01:09 1/30/18 Bis(2-chloroethoxy)methane 618 U 1980 618 10 01/31/18 01:09 1/30/18 Bis(2-chloroethyl) Ether 490 U 1980 490 10 01/31/18 01:09 1/30/18 Bis(2-chloroisopropyl) Ether 408 U 1980 408 10 01/31/18 01:09 1/30/18 Bis(2-ethylhexyl) Phthalate 513 U 1980 513 10 01/31/18 01:09 1/30/18 Butyl Benzyl Phthalate 548 U 3960 548 10 01/31/18 01:09 1/30/18 Printed 2/5/2018 3:02:44 PM Page 70 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:25 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-3-1 Units: ug/Kg Lab Code: J1800711-005 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 665 U 1980 665 10 01/31/18 01:09 1/30/18 Chrysene 1670 I 1980 525 10 01/31/18 01:09 1/30/18 Dibenz(a,h)anthracene 536 U 1980 536 10 01/31/18 01:09 1/30/18 Dibenzofuran 536 U 1980 536 10 01/31/18 01:09 1/30/18 Diethyl Phthalate 595 U 1980 595 10 01/31/18 01:09 1/30/18 Dimethyl Phthalate 618 U 1980 618 10 01/31/18 01:09 1/30/18 Di-n-butyl Phthalate 397 U 1980 397 10 01/31/18 01:09 1/30/18 Di-n-octyl Phthalate 606 U 3960 606 10 01/31/18 01:09 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 432 U 1980 432 10 01/31/18 01:09 1/30/18 Fluoranthene 2730 1980 560 10 01/31/18 01:09 1/30/18 Fluorene 548 U 1980 548 10 01/31/18 01:09 1/30/18 Hexachlorobenzene 560 U 1980 560 10 01/31/18 01:09 1/30/18 Hexachlorobutadiene 641 U 1980 641 10 01/31/18 01:09 1/30/18 Hexachlorocyclopentadiene 397 U 1980 397 10 01/31/18 01:09 1/30/18 Hexachloroethane 362 U 1980 362 10 01/31/18 01:09 1/30/18 Indeno(1,2,3-cd)pyrene 652 I 1980 478 10 01/31/18 01:09 1/30/18 Isophorone 676 U 1980 676 10 01/31/18 01:09 1/30/18 Naphthalene 571 U 1980 571 10 01/31/18 01:09 1/30/18 Nitrobenzene 455 U 1980 455 10 01/31/18 01:09 1/30/18 N-Nitrosodi-n-propylamine 583 U 1980 583 10 01/31/18 01:09 1/30/18 Pentachlorophenol (PCP) 408 U 7810 408 10 01/31/18 01:09 1/30/18 Phenanthrene 1370 I 1980 490 10 01/31/18 01:09 1/30/18 Phenol 536 U 1980 536 10 01/31/18 01:09 1/30/18 Pyrene 2440 1980 536 10 01/31/18 01:09 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 34 30 - 136 01/31/18 01:09 2-Fluorobiphenyl 61 20 - 115 01/31/18 01:09 2-Fluorophenol 43 10 - 110 01/31/18 01:09 Nitrobenzene-d5 55 20 - 110 01/31/18 01:09 Phenol-d6 45 14 - 100 01/31/18 01:09 p-Terphenyl-dl4 68 32 - 119 01/31/18 01:09 Printed 2/5/2018 3:02:44 PM Page 71 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 13:00 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-3-14 Units: ug/Kg Lab Code: J1800711-006 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 64.6 U 174 64.6 1 01/31/18 01:34 1/30/18 1,2-Dichlorobenzene 32.9 U 174 32.9 1 01/31/18 01:34 1/30/18 1,3-Dichlorobenzene 39.0 U 174 39.0 1 01/31/18 01:34 1/30/18 1,4-Dichlorobenzene 42.1 U 174 42.1 1 01/31/18 01:34 1/30/18 1-Methylnaphthalene 67.7 U 174 67.7 1 01/31/18 01:34 1/30/18 2,4,5-Trichlorophenol 58.5 U 174 58.5 1 01/31/18 01:34 1/30/18 2,4,6-Trichlorophenol 51.3 U 174 51.3 1 01/31/18 01:34 1/30/18 2,4-Dichlorophenol 64.6 U 174 64.6 1 01/31/18 01:34 1/30/18 2,4-Dimethylphenol 85.1 U 174 85.1 1 01/31/18 01:34 1/30/18 2,4-Dinitrophenol 23.6 U 687 23.6 1 01/31/18 01:34 1/30/18 2,4-Dinitrotoluene 42.1 U 174 42.1 1 01/31/18 01:34 1/30/18 2,6-Dinitrotoluene 49.3 U 174 49.3 1 01/31/18 01:34 1/30/18 2-Chloronaphthalene 44.1 U 174 44.1 1 01/31/18 01:34 1/30/18 2-Chlorophenol 35.9 U 174 35.9 1 01/31/18 01:34 1/30/18 2-Methylnaphthalene 60.5 U 174 60.5 1 01/31/18 01:34 1/30/18 2-Methylphenol 49.3 U 174 49.3 1 01/31/18 01:34 1/30/18 2-Nitroaniline 52.3 U 174 52.3 1 01/31/18 01:34 1/30/18 2-Nitrophenol 53.4 U 687 53.4 1 01/31/18 01:34 1/30/18 3- and 4-Methylphenol Coelution 44.1 U 174 44.1 1 01/31/18 01:34 1/30/18 3,3'-Dichlorobenzidine 87.2 U 687 87.2 1 01/31/18 01:34 1/30/18 3-Nitroaniline 52.3 U 174 52.3 1 01/31/18 01:34 1/30/18 4,6-Dinitro-2-methylphenol 49.3 U 687 49.3 1 01/31/18 01:34 1/30/18 4-Bromophenyl Phenyl Ether 53.4 U 174 53.4 1 01/31/18 01:34 1/30/18 4-Chloro-3-methylphenol 54.4 U 174 54.4 1 01/31/18 01:34 1/30/18 4-Chloroaniline 70.8 U 174 70.8 1 01/31/18 01:34 1/30/18 4-Chlorophenyl Phenyl Ether 53.4 U 174 53.4 1 01/31/18 01:34 1/30/18 4-Nitroaniline 56.4 U 174 56.4 1 01/31/18 01:34 1/30/18 4-Nitrophenol 57.5 U 687 57.5 1 01/31/18 01:34 1/30/18 Acenaphthene 54.4 U 174 54.4 1 01/31/18 01:34 1/30/18 Acenaphthylene 48.2 U 174 48.2 1 01/31/18 01:34 1/30/18 Acetophenone 47.2 U 349 47.2 1 01/31/18 01:34 1/30/18 Anthracene 44.1 U 174 44.1 1 01/31/18 01:34 1/30/18 Benz(a)anthracene 48.2 U 174 48.2 1 01/31/18 01:34 1/30/18 Benzo(a)pyrene 38.0 U 174 38.0 1 01/31/18 01:34 1/30/18 Benzo(k)fluoranthene 26.7 U 174 26.7 1 01/31/18 01:34 1/30/18 Benzo(g,h,i)perylene 53.4 U 174 53.4 1 01/31/18 01:34 1/30/18 Benzo(k)fluoranthene 60.5 U 174 60.5 1 01/31/18 01:34 1/30/18 Benzyl Alcohol 39.0 U 349 39.0 1 01/31/18 01:34 1/30/18 Bis(2-chloroethoxy)methane 54.4 U 174 54.4 1 01/31/18 01:34 1/30/18 Bis(2-chloroethyl) Ether 43.1 U 174 43.1 1 01/31/18 01:34 1/30/18 Bis(2-chloroisopropyl) Ether 35.9 U 174 35.9 1 01/31/18 01:34 1/30/18 Bis(2-ethylhexyl) Phthalate 45.2 U 174 45.2 1 01/31/18 01:34 1/30/18 Butyl Benzyl Phthalate 48.2 U 349 48.2 1 01/31/18 01:34 1/30/18 Printed 2/5/2018 3:02:44 PM Page 72 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 13:00 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-3-14 Units: ug/Kg Lab Code: J1800711-006 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 58.5 U 174 58.5 1 01/31/18 01:34 1/30/18 Chrysene 46.2 U 174 46.2 1 01/31/18 01:34 1/30/18 Dibenz(a,h)anthracene 47.2 U 174 47.2 1 01/31/18 01:34 1/30/18 Dibenzofuran 47.2 U 174 47.2 1 01/31/18 01:34 1/30/18 Diethyl Phthalate 52.3 U 174 52.3 1 01/31/18 01:34 1/30/18 Dimethyl Phthalate 54.4 U 174 54.4 1 01/31/18 01:34 1/30/18 Di-n-butyl Phthalate 34.9 U 174 34.9 1 01/31/18 01:34 1/30/18 Di-n-octyl Phthalate 53.4 U 349 53.4 1 01/31/18 01:34 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 38.0 U 174 38.0 1 01/31/18 01:34 1/30/18 Fluoranthene 49.3 U 174 49.3 1 01/31/18 01:34 1/30/18 Fluorene 48.2 U 174 48.2 1 01/31/18 01:34 1/30/18 Hexachlorobenzene 49.3 U 174 49.3 1 01/31/18 01:34 1/30/18 Hexachlorobutadiene 56.4 U 174 56.4 1 01/31/18 01:34 1/30/18 Hexachlorocyclopentadiene 34.9 U 174 34.9 1 01/31/18 01:34 1/30/18 Hexachloroethane 31.8 U 174 31.8 1 01/31/18 01:34 1/30/18 Indeno(1,2,3-cd)pyrene 42.1 U 174 42.1 1 01/31/18 01:34 1/30/18 Isophorone 59.5 U 174 59.5 1 01/31/18 01:34 1/30/18 Naphthalene 50.3 U 174 50.3 1 01/31/18 01:34 1/30/18 Nitrobenzene 40.0 U 174 40.0 1 01/31/18 01:34 1/30/18 N-Nitrosodi-n-propylamine 51.3 U 174 51.3 1 01/31/18 01:34 1/30/18 Pentachlorophenol (PCP) 35.9 U 687 35.9 1 01/31/18 01:34 1/30/18 Phenanthrene 43.1 U 174 43.1 1 01/31/18 01:34 1/30/18 Phenol 47.2 U 174 47.2 1 01/31/18 01:34 1/30/18 Pyrene 47.2 U 174 47.2 1 01/31/18 01:34 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 43 30 - 136 01/31/18 01:34 2-Fluorobiphenyl 60 20 - 115 01/31/18 01:34 2-Fluorophenol 55 10 - 110 01/31/18 01:34 Nitrobenzene-d5 64 20 - 110 01/31/18 01:34 Phenol-d6 57 14 - 100 01/31/18 01:34 p-Terphenyl-dl4 63 32 - 119 01/31/18 01:34 Printed 2/5/2018 3:02:44 PM Page 73 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 14:30 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-4-1 Units: ug/Kg Lab Code: J1800711-007 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 83.2 U 224 83.2 1 01/31/18 01:59 1/30/18 1,2-Dichlorobenzene 42.3 U 224 42.3 1 01/31/18 01:59 1/30/18 1,3-Dichlorobenzene 50.2 U 224 50.2 1 01/31/18 01:59 1/30/18 1,4-Dichlorobenzene 54.2 U 224 54.2 1 01/31/18 01:59 1/30/18 1-Methylnaphthalene 87.2 U 224 87.2 1 01/31/18 01:59 1/30/18 2,4,5-Trichlorophenol 75.3 U 224 75.3 1 01/31/18 01:59 1/30/18 2,4,6-Trichlorophenol 66.1 U 224 66.1 1 01/31/18 01:59 1/30/18 2,4-Dichlorophenol 83.2 U 224 83.2 1 01/31/18 01:59 1/30/18 2,4-Dimethylphenol 110 U 224 110 1 01/31/18 01:59 1/30/18 2,4-Dinitrophenol 30.4 U 885 30.4 1 01/31/18 01:59 1/30/18 2,4-Dinitrotoluene 54.2 U 224 54.2 1 01/31/18 01:59 1/30/18 2,6-Dinitrotoluene 63.4 U 224 63.4 1 01/31/18 01:59 1/30/18 2-Chloronaphthalene 56.8 U 224 56.8 1 01/31/18 01:59 1/30/18 2-Chlorophenol 46.3 U 224 46.3 1 01/31/18 01:59 1/30/18 2-Methylnaphthalene 78.0 U 224 78.0 1 01/31/18 01:59 1/30/18 2-Methylphenol 63.4 U 224 63.4 1 01/31/18 01:59 1/30/18 2-Nitroaniline 67.4 U 224 67.4 1 01/31/18 01:59 1/30/18 2-Nitrophenol 68.7 U 885 68.7 1 01/31/18 01:59 1/30/18 3- and 4-Methylphenol Coelution 56.8 U 224 56.8 1 01/31/18 01:59 1/30/18 3,3'-Dichlorobenzidine 113 U 885 113 1 01/31/18 01:59 1/30/18 3-Nitroaniline 67.4 U 224 67.4 1 01/31/18 01:59 1/30/18 4,6-Dinitro-2-methylphenol 63.4 U 885 63.4 1 01/31/18 01:59 1/30/18 4-Bromophenyl Phenyl Ether 68.7 U 224 68.7 1 01/31/18 01:59 1/30/18 4-Chloro-3-methylphenol 70.0 U 224 70.0 1 01/31/18 01:59 1/30/18 4-Chloroaniline 91.2 U 224 91.2 1 01/31/18 01:59 1/30/18 4-Chlorophenyl Phenyl Ether 68.7 U 224 68.7 1 01/31/18 01:59 1/30/18 4-Nitroaniline 72.7 U 224 72.7 1 01/31/18 01:59 1/30/18 4-Nitrophenol 74.0 U 885 74.0 1 01/31/18 01:59 1/30/18 Acenaphthene 70.0 U 224 70.0 1 01/31/18 01:59 1/30/18 Acenaphthylene 62.1 U 224 62.1 1 01/31/18 01:59 1/30/18 Acetophenone 60.8 U 449 60.8 1 01/31/18 01:59 1/30/18 Anthracene 56.8 U 224 56.8 1 01/31/18 01:59 1/30/18 Benz(a)anthracene 62.1 U 224 62.1 1 01/31/18 01:59 1/30/18 Benzo(a)pyrene 48.9 U 224 48.9 1 01/31/18 01:59 1/30/18 Benzo(b)fluoranthene 34.4 U 224 34.4 1 01/31/18 01:59 1/30/18 Benzo(g,h,i)perylene 68.7 U 224 68.7 1 01/31/18 01:59 1/30/18 Benzo(k)fluoranthene 78.0 U 224 78.0 1 01/31/18 01:59 1/30/18 Benzyl Alcohol 50.2 U 449 50.2 1 01/31/18 01:59 1/30/18 Bis(2-chloroethoxy)methane 70.0 U 224 70.0 1 01/31/18 01:59 1/30/18 Bis(2-chloroethyl) Ether 55.5 U 224 55.5 1 01/31/18 01:59 1/30/18 Bis(2-chloroisopropyl) Ether 46.3 U 224 46.3 1 01/31/18 01:59 1/30/18 Bis(2-ethylhexyl) Phthalate 58.1 U 224 58.1 1 01/31/18 01:59 1/30/18 Butyl Benzyl Phthalate 62.1 U 449 62.1 1 01/31/18 01:59 1/30/18 Printed 2/5/2018 3:02:45 PM Page 74 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 14:30 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-4-1 Units: ug/Kg Lab Code: J1800711-007 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 75.3 U 224 75.3 1 01/31/18 01:59 1/30/18 Chrysene 59.5 U 224 59.5 1 01/31/18 01:59 1/30/18 Dibenz(a,h)anthracene 60.8 U 224 60.8 1 01/31/18 01:59 1/30/18 Dibenzofuran 60.8 U 224 60.8 1 01/31/18 01:59 1/30/18 Diethyl Phthalate 67.4 U 224 67.4 1 01/31/18 01:59 1/30/18 Dimethyl Phthalate 70.0 U 224 70.0 1 01/31/18 01:59 1/30/18 Di-n-butyl Phthalate 44.9 U 224 44.9 1 01/31/18 01:59 1/30/18 Di-n-octyl Phthalate 68.7 U 449 68.7 1 01/31/18 01:59 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 48.9 U 224 48.9 1 01/31/18 01:59 1/30/18 Fluoranthene 63.4 U 224 63.4 1 01/31/18 01:59 1/30/18 Fluorene 62.1 U 224 62.1 1 01/31/18 01:59 1/30/18 Hexachlorobenzene 63.4 U 224 63.4 1 01/31/18 01:59 1/30/18 Hexachlorobutadiene 72.7 U 224 72.7 1 01/31/18 01:59 1/30/18 Hexachlorocyclopentadiene 44.9 U 224 44.9 1 01/31/18 01:59 1/30/18 Hexachloroethane 41.0 U 224 41.0 1 01/31/18 01:59 1/30/18 Indeno(1,2,3-cd)pyrene 54.2 U 224 54.2 1 01/31/18 01:59 1/30/18 Isophorone 76.6 U 224 76.6 1 01/31/18 01:59 1/30/18 Naphthalene 64.7 U 224 64.7 1 01/31/18 01:59 1/30/18 Nitrobenzene 51.5 U 224 51.5 1 01/31/18 01:59 1/30/18 N-Nitrosodi-n-propylamine 66.1 U 224 66.1 1 01/31/18 01:59 1/30/18 Pentachlorophenol (PCP) 46.3 U 885 46.3 1 01/31/18 01:59 1/30/18 Phenanthrene 55.5 U 224 55.5 1 01/31/18 01:59 1/30/18 Phenol 60.8 U 224 60.8 1 01/31/18 01:59 1/30/18 Pyrene 60.8 U 224 60.8 1 01/31/18 01:59 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 52 30 - 136 01/31/18 01:59 2-Fluorobiphenyl 61 20 - 115 01/31/18 01:59 2-Fluorophenol 61 10 - 110 01/31/18 01:59 Nitrobenzene-d5 68 20 - 110 01/31/18 01:59 Phenol-d6 62 14 - 100 01/31/18 01:59 p-Terphenyl-dl4 45 32 - 119 01/31/18 01:59 Printed 2/5/2018 3:02:45 PM Page 75 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 15:10 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-4-21 Units: ug/Kg Lab Code: J1800711-008 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 680 U 1830 680 10 01/31/18 02:24 1/30/18 1,2-Dichlorobenzene 346 U 1830 346 10 01/31/18 02:24 1/30/18 1,3-Dichlorobenzene 410 U 1830 410 10 01/31/18 02:24 1/30/18 1,4-Dichlorobenzene 443 U 1830 443 10 01/31/18 02:24 1/30/18 1-Methylnaphthalene 712 U 1830 712 10 01/31/18 02:24 1/30/18 2,4,5-Trichlorophenol 615 U 1830 615 10 01/31/18 02:24 1/30/18 2,4,6-Trichlorophenol 540 U 1830 540 10 01/31/18 02:24 1/30/18 2,4-Dichlorophenol 680 U 1830 680 10 01/31/18 02:24 1/30/18 2,4-Dimethylphenol 896 U 1830 896 10 01/31/18 02:24 1/30/18 2,4-Dinitrophenol 249 U 7230 249 10 01/31/18 02:24 1/30/18 2,4-Dinitrotoluene 443 U 1830 443 10 01/31/18 02:24 1/30/18 2,6-Dinitrotoluene 518 U 1830 518 10 01/31/18 02:24 1/30/18 2-Chloronaphthalene 464 U 1830 464 10 01/31/18 02:24 1/30/18 2-Chlorophenol 378 U 1830 378 10 01/31/18 02:24 1/30/18 2-Methylnaphthalene 637 U 1830 637 10 01/31/18 02:24 1/30/18 2-Methylphenol 518 U 1830 518 10 01/31/18 02:24 1/30/18 2-Nitroaniline 551 U 1830 551 10 01/31/18 02:24 1/30/18 2-Nitrophenol 561 U 7230 561 10 01/31/18 02:24 1/30/18 3- and 4-Methylphenol Coelution 464 U 1830 464 10 01/31/18 02:24 1/30/18 3,3'-Dichlorobenzidine 917 U 7230 917 10 01/31/18 02:24 1/30/18 3-Nitroaniline 551 U 1830 551 10 01/31/18 02:24 1/30/18 4,6-Dinitro-2-methylphenol 518 U 7230 518 10 01/31/18 02:24 1/30/18 4-Bromophenyl Phenyl Ether 561 U 1830 561 10 01/31/18 02:24 1/30/18 4-Chloro-3-methylphenol 572 U 1830 572 10 01/31/18 02:24 1/30/18 4-Chloroaniline 745 U 1830 745 10 01/31/18 02:24 1/30/18 4-Chlorophenyl Phenyl Ether 561 U 1830 561 10 01/31/18 02:24 1/30/18 4-Nitroaniline 594 U 1830 594 10 01/31/18 02:24 1/30/18 4-Nitrophenol 605 U 7230 605 10 01/31/18 02:24 1/30/18 Acenaphthene 572 U 1830 572 10 01/31/18 02:24 1/30/18 Acenaphthylene 507 U 1830 507 10 01/31/18 02:24 1/30/18 Acetophenone 497 U 3670 497 10 01/31/18 02:24 1/30/18 Anthracene 464 U 1830 464 10 01/31/18 02:24 1/30/18 Benz(a)anthracene 507 U 1830 507 10 01/31/18 02:24 1/30/18 Benzo(a)pyrene 400 U 1830 400 10 01/31/18 02:24 1/30/18 Benzo(k)fluoranthene 281 U 1830 281 10 01/31/18 02:24 1/30/18 Benzo(g,h,i)perylene 561 U 1830 561 10 01/31/18 02:24 1/30/18 Benzo(k)fluoranthene 637 U 1830 637 10 01/31/18 02:24 1/30/18 Benzyl Alcohol 410 U 3670 410 10 01/31/18 02:24 1/30/18 Bis(2-chloroethoxy)methane 572 U 1830 572 10 01/31/18 02:24 1/30/18 Bis(2-chloroethyl) Ether 454 U 1830 454 10 01/31/18 02:24 1/30/18 Bis(2-chloroisopropyl) Ether 378 U 1830 378 10 01/31/18 02:24 1/30/18 Bis(2-ethylhexyl) Phthalate 475 U 1830 475 10 01/31/18 02:24 1/30/18 Butyl Benzyl Phthalate 507 U 3670 507 10 01/31/18 02:24 1/30/18 Printed 2/5/2018 3:02:45 PM Page 76 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 15:10 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-4-21 Units: ug/Kg Lab Code: J1800711-008 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 615 U 1830 615 10 01/31/18 02:24 1/30/18 Chrysene 486 U 1830 486 10 01/31/18 02:24 1/30/18 Dibenz(a,h)anthracene 497 U 1830 497 10 01/31/18 02:24 1/30/18 Dibenzofuran 497 U 1830 497 10 01/31/18 02:24 1/30/18 Diethyl Phthalate 551 U 1830 551 10 01/31/18 02:24 1/30/18 Dimethyl Phthalate 572 U 1830 572 10 01/31/18 02:24 1/30/18 Di-n-butyl Phthalate 367 U 1830 367 10 01/31/18 02:24 1/30/18 Di-n-octyl Phthalate 561 U 3670 561 10 01/31/18 02:24 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 400 U 1830 400 10 01/31/18 02:24 1/30/18 Fluoranthene 518 U 1830 518 10 01/31/18 02:24 1/30/18 Fluorene 507 U 1830 507 10 01/31/18 02:24 1/30/18 Hexachlorobenzene 518 U 1830 518 10 01/31/18 02:24 1/30/18 Hexachlorobutadiene 594 U 1830 594 10 01/31/18 02:24 1/30/18 Hexachlorocyclopentadiene 367 U 1830 367 10 01/31/18 02:24 1/30/18 Hexachloroethane 335 U 1830 335 10 01/31/18 02:24 1/30/18 Indeno(1,2,3-cd)pyrene 443 U 1830 443 10 01/31/18 02:24 1/30/18 Isophorone 626 U 1830 626 10 01/31/18 02:24 1/30/18 Naphthalene 529 U 1830 529 10 01/31/18 02:24 1/30/18 Nitrobenzene 421 U 1830 421 10 01/31/18 02:24 1/30/18 N-Nitrosodi-n-propylamine 540 U 1830 540 10 01/31/18 02:24 1/30/18 Pentachlorophenol (PCP) 378 U 7230 378 10 01/31/18 02:24 1/30/18 Phenanthrene 454 U 1830 454 10 01/31/18 02:24 1/30/18 Phenol 497 U 1830 497 10 01/31/18 02:24 1/30/18 Pyrene 497 U 1830 497 10 01/31/18 02:24 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 41 30 - 136 01/31/18 02:24 2-Fluorobiphenyl 67 20 - 115 01/31/18 02:24 2-Fluorophenol 56 10 - 110 01/31/18 02:24 Nitrobenzene-d5 59 20 - 110 01/31/18 02:24 Phenol-d6 58 14 - 100 01/31/18 02:24 p-Terphenyl-dl4 75 32 - 119 01/31/18 02:24 Printed 2/5/2018 3:02:45 PM Page 77 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 13:40 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: TW-5-1 Units: ug/Kg Lab Code: J1800711-009 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 11100 U 29900 11100 5 02/02/18 19:17 1/30/18 1,2-Dichlorobenzene 5630 U 29900 5630 5 02/02/18 19:17 1/30/18 1,3-Dichlorobenzene 6680 U 29900 6680 5 02/02/18 19:17 1/30/18 1,4-Dichlorobenzene 7210 U 29900 7210 5 02/02/18 19:17 1/30/18 1-Methylnaphthalene 11600 U 29900 11600 5 02/02/18 19:17 1/30/18 2,4,5-Trichlorophenol 10100 U 29900 10100 5 02/02/18 19:17 1/30/18 2,4,6-Trichlorophenol 8790 U 29900 8790 5 02/02/18 19:17 1/30/18 2,4-Dichlorophenol 11100 U 29900 11100 5 02/02/18 19:17 1/30/18 2,4-Dimethylphenol 14600 U 29900 14600 5 02/02/18 19:17 1/30/18 2,4-Dinitrophenol 4050 U 118000 4050 5 02/02/18 19:17 1/30/18 2,4-Dinitrotoluene 7210 U 29900 7210 5 02/02/18 19:17 1/30/18 2,6-Dinitrotoluene 8440 U 29900 8440 5 02/02/18 19:17 1/30/18 2-Chloronaphthalene 7560 U 29900 7560 5 02/02/18 19:17 1/30/18 2-Chlorophenol 6150 U 29900 6150 5 02/02/18 19:17 1/30/18 2-Methylnaphthalene 10400 U 29900 10400 5 02/02/18 19:17 1/30/18 2-Methylphenol 8440 U 29900 8440 5 02/02/18 19:17 1/30/18 2-Nitroaniline 8960 U 29900 8960 5 02/02/18 19:17 1/30/18 2-Nitrophenol 9140 U 118000 9140 5 02/02/18 19:17 1/30/18 3- and 4-Methylphenol Coelution 7560 U 29900 7560 5 02/02/18 19:17 1/30/18 3,3'-Dichlorobenzidine 15000 U 118000 15000 5 02/02/18 19:17 1/30/18 3-Nitroaniline 8960 U 29900 8960 5 02/02/18 19:17 1/30/18 4,6-Dinitro-2-methylphenol 8440 U 118000 8440 5 02/02/18 19:17 1/30/18 4-Bromophenyl Phenyl Ether 9140 U 29900 9140 5 02/02/18 19:17 1/30/18 4-Chloro-3-methylphenol 9310 U 29900 9310 5 02/02/18 19:17 1/30/18 4-Chloroaniline 12200 U 29900 12200 5 02/02/18 19:17 1/30/18 4-Chlorophenyl Phenyl Ether 9140 U 29900 9140 5 02/02/18 19:17 1/30/18 4-Nitroaniline 9670 U 29900 9670 5 02/02/18 19:17 1/30/18 4-Nitrophenol 9840 U 118000 9840 5 02/02/18 19:17 1/30/18 Acenaphthene 9310 U 29900 9310 5 02/02/18 19:17 1/30/18 Acenaphthylene 8260 U 29900 8260 5 02/02/18 19:17 1/30/18 Acetophenone 8090 U 59700 8090 5 02/02/18 19:17 1/30/18 Anthracene 7560 U 29900 7560 5 02/02/18 19:17 1/30/18 Benz(a)anthracene 8260 U 29900 8260 5 02/02/18 19:17 1/30/18 Benzo(a)pyrene 6500 U 29900 6500 5 02/02/18 19:17 1/30/18 Benzo(b)fluoranthene 4570 U 29900 4570 5 02/02/18 19:17 1/30/18 Benzo(g,h,i)perylene 9140 U 29900 9140 5 02/02/18 19:17 1/30/18 Benzo(k)fluoranthene 10400 U 29900 10400 5 02/02/18 19:17 1/30/18 Benzyl Alcohol 6680 U 59700 6680 5 02/02/18 19:17 1/30/18 Bis(2-chloroethoxy)methane 9310 U 29900 9310 5 02/02/18 19:17 1/30/18 Bis(2-chloroethyl) Ether 7380 U 29900 7380 5 02/02/18 19:17 1/30/18 Bis(2-chloroisopropyl) Ether 6150 U 29900 6150 5 02/02/18 19:17 1/30/18 Bis(2-ethylhexyl) Phthalate 7730 U 29900 7730 5 02/02/18 19:17 1/30/18 Butyl Benzyl Phthalate 8260 U 59700 8260 5 02/02/18 19:17 1/30/18 Printed 2/5/2018 3:02:45 PM Page 78 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 13:40 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: TW-5-1 Units: ug/Kg Lab Code: J1800711-009 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 10100 U 29900 10100 5 02/02/18 19:17 1/30/18 Chrysene 7910 U 29900 7910 5 02/02/18 19:17 1/30/18 Dibenz(a,h)anthracene 8090 U 29900 8090 5 02/02/18 19:17 1/30/18 Dibenzofuran 8090 U 29900 8090 5 02/02/18 19:17 1/30/18 Diethyl Phthalate 8960 U 29900 8960 5 02/02/18 19:17 1/30/18 Dimethyl Phthalate 9310 U 29900 9310 5 02/02/18 19:17 1/30/18 Di-n-butyl Phthalate 5980 U 29900 5980 5 02/02/18 19:17 1/30/18 Di-n-octyl Phthalate 9140 U 59700 9140 5 02/02/18 19:17 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 6500 U 29900 6500 5 02/02/18 19:17 1/30/18 Fluoranthene 8440 U 29900 8440 5 02/02/18 19:17 1/30/18 Fluorene 8260 U 29900 8260 5 02/02/18 19:17 1/30/18 Hexachlorobenzene 8440 U 29900 8440 5 02/02/18 19:17 1/30/18 Hexachlorobutadiene 9670 U 29900 9670 5 02/02/18 19:17 1/30/18 Hexachlorocyclopentadiene 5980 U 29900 5980 5 02/02/18 19:17 1/30/18 Hexachloroethane 5450 U 29900 5450 5 02/02/18 19:17 1/30/18 Indeno(1,2,3-cd)pyrene 7210 U 29900 7210 5 02/02/18 19:17 1/30/18 Isophorone 10200 U 29900 10200 5 02/02/18 19:17 1/30/18 Naphthalene 8610 U 29900 8610 5 02/02/18 19:17 1/30/18 Nitrobenzene 6860 U 29900 6860 5 02/02/18 19:17 1/30/18 N-Nitrosodi-n-propylamine 8790 U 29900 8790 5 02/02/18 19:17 1/30/18 Pentachlorophenol (PCP) 6150 U 118000 6150 5 02/02/18 19:17 1/30/18 Phenanthrene 7380 U 29900 7380 5 02/02/18 19:17 1/30/18 Phenol 8090 U 29900 8090 5 02/02/18 19:17 1/30/18 Pyrene 8090 U 29900 8090 5 02/02/18 19:17 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 54 30 - 136 02/02/18 19:17 2-Fluorobiphenyl 69 20 - 115 02/02/18 19:17 2-Fluorophenol 57 10-110 02/02/18 19:17 Nitrobenzene-d5 60 20 - 110 02/02/18 19:17 Phenol-d6 60 14 - 100 02/02/18 19:17 p-Terphenyl-dl4 92 32 - 119 02/02/18 19:17 Printed 2/5/2018 3:02:46 PM Page 79 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 14:15 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: TW-5-25 Units: ug/Kg Lab Code: J1800711-010 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 765 U 2060 765 10 01/31/18 02:48 1/30/18 1,2-Dichlorobenzene 389 U 2060 389 10 01/31/18 02:48 1/30/18 1,3-Dichlorobenzene 462 U 2060 462 10 01/31/18 02:48 1/30/18 1,4-Dichlorobenzene 498 U 2060 498 10 01/31/18 02:48 1/30/18 1-Methylnaphthalene 802 U 2060 802 10 01/31/18 02:48 1/30/18 2,4,5-Trichlorophenol 693 U 2060 693 10 01/31/18 02:48 1/30/18 2,4,6-Trichlorophenol 608 U 2060 608 10 01/31/18 02:48 1/30/18 2,4-Dichlorophenol 765 U 2060 765 10 01/31/18 02:48 1/30/18 2,4-Dimethylphenol 1010 U 2060 1010 10 01/31/18 02:48 1/30/18 2,4-Dinitrophenol 280 U 8130 280 10 01/31/18 02:48 1/30/18 2,4-Dinitrotoluene 498 U 2060 498 10 01/31/18 02:48 1/30/18 2,6-Dinitrotoluene 583 U 2060 583 10 01/31/18 02:48 1/30/18 2-Chloronaphthalene 523 U 2060 523 10 01/31/18 02:48 1/30/18 2-Chlorophenol 425 U 2060 425 10 01/31/18 02:48 1/30/18 2-Methylnaphthalene 717 U 2060 717 10 01/31/18 02:48 1/30/18 2-Methylphenol 583 U 2060 583 10 01/31/18 02:48 1/30/18 2-Nitroaniline 620 U 2060 620 10 01/31/18 02:48 1/30/18 2-Nitrophenol 632 U 8130 632 10 01/31/18 02:48 1/30/18 3- and 4-Methylphenol Coelution 523 U 2060 523 10 01/31/18 02:48 1/30/18 3,3'-Dichlorobenzidine 1040 U 8130 1040 10 01/31/18 02:48 1/30/18 3-Nitroaniline 620 U 2060 620 10 01/31/18 02:48 1/30/18 4,6-Dinitro-2-methylphenol 583 U 8130 583 10 01/31/18 02:48 1/30/18 4-Bromophenyl Phenyl Ether 632 U 2060 632 10 01/31/18 02:48 1/30/18 4-Chloro-3-methylphenol 644 U 2060 644 10 01/31/18 02:48 1/30/18 4-Chloroaniline 838 U 2060 838 10 01/31/18 02:48 1/30/18 4-Chlorophenyl Phenyl Ether 632 U 2060 632 10 01/31/18 02:48 1/30/18 4-Nitroaniline 668 U 2060 668 10 01/31/18 02:48 1/30/18 4-Nitrophenol 680 U 8130 680 10 01/31/18 02:48 1/30/18 Acenaphthene 644 U 2060 644 10 01/31/18 02:48 1/30/18 Acenaphthylene 1030 I 2060 571 10 01/31/18 02:48 1/30/18 Acetophenone 559 U 4130 559 10 01/31/18 02:48 1/30/18 Anthracene 523 U 2060 523 10 01/31/18 02:48 1/30/18 Benz(a)anthracene 571 U 2060 571 10 01/31/18 02:48 1/30/18 Benzo(a)pyrene 809 I 2060 450 10 01/31/18 02:48 1/30/18 Benzo(b)fluoranthene 498 I 2060 316 10 01/31/18 02:48 1/30/18 Benzo(g,h,i)perylene 652 I 2060 632 10 01/31/18 02:48 1/30/18 Benzo(k)fluoranthene 717 U 2060 717 10 01/31/18 02:48 1/30/18 Benzyl Alcohol 462 U 4130 462 10 01/31/18 02:48 1/30/18 Bis(2-chloroethoxy)methane 644 U 2060 644 10 01/31/18 02:48 1/30/18 Bis(2-chloroethyl) Ether 510 U 2060 510 10 01/31/18 02:48 1/30/18 Bis(2-chloroisopropyl) Ether 425 U 2060 425 10 01/31/18 02:48 1/30/18 Bis(2-ethylhexyl) Phthalate 535 U 2060 535 10 01/31/18 02:48 1/30/18 Butyl Benzyl Phthalate 571 U 4130 571 10 01/31/18 02:48 1/30/18 Printed 2/5/2018 3:02:46 PM Page 80 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 14:15 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: TW-5-25 Units: ug/Kg Lab Code: J1800711-010 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 693 U 2060 693 10 01/31/18 02:48 1/30/18 Chrysene 547 U 2060 547 10 01/31/18 02:48 1/30/18 Dibenz(a,h)anthracene 559 U 2060 559 10 01/31/18 02:48 1/30/18 Dibenzofuran 559 U 2060 559 10 01/31/18 02:48 1/30/18 Diethyl Phthalate 620 U 2060 620 10 01/31/18 02:48 1/30/18 Dimethyl Phthalate 644 U 2060 644 10 01/31/18 02:48 1/30/18 Di-n-butyl Phthalate 413 U 2060 413 10 01/31/18 02:48 1/30/18 Di-n-octyl Phthalate 632 U 4130 632 10 01/31/18 02:48 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 450 U 2060 450 10 01/31/18 02:48 1/30/18 Fluoranthene 583 U 2060 583 10 01/31/18 02:48 1/30/18 Fluorene 571 U 2060 571 10 01/31/18 02:48 1/30/18 Hexachlorobenzene 583 U 2060 583 10 01/31/18 02:48 1/30/18 Hexachlorobutadiene 668 U 2060 668 10 01/31/18 02:48 1/30/18 Hexachlorocyclopentadiene 413 U 2060 413 10 01/31/18 02:48 1/30/18 Hexachloroethane 377 U 2060 377 10 01/31/18 02:48 1/30/18 Indeno(1,2,3-cd)pyrene 611 I 2060 498 10 01/31/18 02:48 1/30/18 Isophorone 705 U 2060 705 10 01/31/18 02:48 1/30/18 Naphthalene 595 U 2060 595 10 01/31/18 02:48 1/30/18 Nitrobenzene 474 U 2060 474 10 01/31/18 02:48 1/30/18 N-Nitrosodi-n-propylamine 608 U 2060 608 10 01/31/18 02:48 1/30/18 Pentachlorophenol (PCP) 425 U 8130 425 10 01/31/18 02:48 1/30/18 Phenanthrene 510 U 2060 510 10 01/31/18 02:48 1/30/18 Phenol 559 U 2060 559 10 01/31/18 02:48 1/30/18 Pyrene 559 U 2060 559 10 01/31/18 02:48 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 36 30 - 136 01/31/18 02:48 2-Fluorobiphenyl 45 20 - 115 01/31/18 02:48 2-Fluorophenol 44 10 - 110 01/31/18 02:48 Nitrobenzene-d5 42 20 - 110 01/31/18 02:48 Phenol-d6 41 14 - 100 01/31/18 02:48 p-Terphenyl-dl4 44 32 - 119 01/31/18 02:48 Printed 2/5/2018 3:02:46 PM Page 81 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 11:20 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-1 Units: ug/L Lab Code: J1800711-011 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 0.600 U 4.78 0.600 1 01/29/18 21:54 1/29/18 1,2-Dichlorobenzene 0.640 U 4.78 0.640 1 01/29/18 21:54 1/29/18 1,3-Dichlorobenzene 0.920 U 4.78 0.920 1 01/29/18 21:54 1/29/18 1,4-Dichlorobenzene 0.910 U 4.78 0.910 1 01/29/18 21:54 1/29/18 1-Methylnaphthalene 0.730 U 4.78 0.730 1 01/29/18 21:54 1/29/18 2,4,5-Trichlorophenol 1.30 U 4.78 1.30 1 01/29/18 21:54 1/29/18 2,4,6-Trichlorophenol 0.890 U 4.78 0.890 1 01/29/18 21:54 1/29/18 2,4-Dichlorophenol 1.20 U 4.78 1.20 1 01/29/18 21:54 1/29/18 2,4-Dimethylphenol 1.50 U 4.78 1.50 1 01/29/18 21:54 1/29/18 2,4-Dinitrophenol 0.760 U 19.1 0.760 1 01/29/18 21:54 1/29/18 2,4-Dinitrotoluene 1.30 U 4.78 1.30 1 01/29/18 21:54 1/29/18 2,6-Dinitrotoluene 1.10 U 4.78 1.10 1 01/29/18 21:54 1/29/18 2-Chloronaphthalene 4.60 U 4.78 4.60 1 01/29/18 21:54 1/29/18 2-Chlorophenol 1.20 U 4.78 1.20 1 01/29/18 21:54 1/29/18 2-Methylnaphthalene 0.630 U 4.78 0.630 1 01/29/18 21:54 1/29/18 2-Methylphenol 1.30 U 4.78 1.30 1 01/29/18 21:54 1/29/18 2-Nitroaniline 1.50 U 4.78 1.50 1 01/29/18 21:54 1/29/18 2-Nitrophenol 1.40 U 19.1 1.40 1 01/29/18 21:54 1/29/18 3- and 4-Methylphenol Coelution 1.00 U 4.78 1.00 1 01/29/18 21:54 1/29/18 3,3'-Dichlorobenzidine 1.40 U 19.1 1.40 1 01/29/18 21:54 1/29/18 3-Nitroaniline 1.10 U 4.78 1.10 1 01/29/18 21:54 1/29/18 4,6-Dinitro-2-methylphenol 1.00 U 19.1 1.00 1 01/29/18 21:54 1/29/18 4-Bromophenyl Phenyl Ether 1.30 U 4.78 1.30 1 01/29/18 21:54 1/29/18 4-Chloro-3-methylphenol 1.80 U 4.78 1.80 1 01/29/18 21:54 1/29/18 4-Chloroaniline 1.40 U 4.78 1.40 1 01/29/18 21:54 1/29/18 4-Chlorophenyl Phenyl Ether 0.960 U 4.78 0.960 1 01/29/18 21:54 1/29/18 4-Nitroaniline 1.00 U 4.78 1.00 1 01/29/18 21:54 1/29/18 4-Nitrophenol 1.80 U 19.1 1.80 1 01/29/18 21:54 1/29/18 Acenaphthene 4.20 U 4.78 4.20 1 01/29/18 21:54 1/29/18 Acenaphthylene 0.990 U 4.78 0.990 1 01/29/18 21:54 1/29/18 Acetophenone 1.60 U 9.57 1.60 1 01/29/18 21:54 1/29/18 Anthracene 1.60 U 4.78 1.60 1 01/29/18 21:54 1/29/18 Benz(a)anthracene 1.00 U 4.78 1.00 1 01/29/18 21:54 1/29/18 Benzo(a)pyrene 1.20 U 4.78 1.20 1 01/29/18 21:54 1/29/18 Benzo(b)fluoranthene 1.00 U 4.78 1.00 1 01/29/18 21:54 1/29/18 Benzo(g,h,i)perylene 1.40 U 4.78 1.40 1 01/29/18 21:54 1/29/18 Benzo(k)fluoranthene 1.80 U 4.78 1.80 1 01/29/18 21:54 1/29/18 Benzyl Alcohol 1.40 U 4.78 1.40 1 01/29/18 21:54 1/29/18 Bis(2-chloroethoxy)methane 1.20 U 4.78 1.20 1 01/29/18 21:54 1/29/18 Bis(2-chloroethyl) Ether 1.90 U 4.78 1.90 1 01/29/18 21:54 1/29/18 Bis(2-chloroisopropyl) Ether 1.50 U 4.78 1.50 1 01/29/18 21:54 1/29/18 Bis(2-ethylhexyl) Phthalate 1.50 U 4.78 1.50 1 01/29/18 21:54 1/29/18 Butyl Benzyl Phthalate 0.860 U 9.57 0.860 1 01/29/18 21:54 1/29/18 Printed 2/5/2018 3:02:46 PM Page 82 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 11:20 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-1 Units: ug/L Lab Code: J1800711-011 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 1.80 U 4.78 1.80 1 01/29/18 21:54 1/29/18 Chrysene 1.20 U 4.78 1.20 1 01/29/18 21:54 1/29/18 Dibenz(a,h)anthracene L50 U 4.78 1.50 1 01/29/18 21:54 1/29/18 Dibenzofuran 1.30 U 4.78 1.30 1 01/29/18 21:54 1/29/18 Diethyl Phthalate 1.70 U 4.78 1.70 1 01/29/18 21:54 1/29/18 Dimethyl Phthalate 1.30 U 4.78 1.30 1 01/29/18 21:54 1/29/18 Di-n-butyl Phthalate 2.20 U 4.78 2.20 1 01/29/18 21:54 1/29/18 Di-n-octyl Phthalate 2.80 U 9.57 2.80 1 01/29/18 21:54 1/29/18 Diphenylamine + n-Nitrosodiphenylamine 1.10 U 4.78 1.10 1 01/29/18 21:54 1/29/18 Fluoranthene 1.40 U 4.78 1.40 1 01/29/18 21:54 1/29/18 Fluorene 0.840 U 4.78 0.840 1 01/29/18 21:54 1/29/18 Hexachlorobenzene 1.70 U 4.78 1.70 1 01/29/18 21:54 1/29/18 Hexachlorobutadiene 1.20 U 4.78 1.20 1 01/29/18 21:54 1/29/18 Hexachlorocyclopentadiene 0.500 U 4.78 0.500 1 01/29/18 21:54 1/29/18 Hexachloroethane 0.810 U 4.78 0.810 1 01/29/18 21:54 1/29/18 Indeno(1,2,3-cd)pyrene 1.70 U 4.78 1.70 1 01/29/18 21:54 1/29/18 Isophorone 1.80 U 4.78 1.80 1 01/29/18 21:54 1/29/18 Naphthalene 0.530 U 4.78 0.530 1 01/29/18 21:54 1/29/18 Nitrobenzene 2.10 U 4.78 2.10 1 01/29/18 21:54 1/29/18 N-Nitrosodi-n-propylamine 2.20 U 4.78 2.20 1 01/29/18 21:54 1/29/18 Pentachlorophenol (PCP) 1.10 U 19.1 1.10 1 01/29/18 21:54 1/29/18 Phenanthrene 1.40 U 4.78 1.40 1 01/29/18 21:54 1/29/18 Phenol 0.590 U 4.78 0.590 1 01/29/18 21:54 1/29/18 Pyrene 0.740 U 4.78 0.740 1 01/29/18 21:54 1/29/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 61 23 - 122 01/29/18 21:54 2-Fluorobiphenyl 55 15 - 117 01/29/18 21:54 2-Fluorophenol 50 10 - 85 01/29/18 21:54 Nitrobenzene-d5 57 10 - 110 01/29/18 21:54 Phenol-d6 42 7 - 60 01/29/18 21:54 p-Terphenyl-dl4 89 40 - 125 01/29/18 21:54 Printed 2/5/2018 3:02:46 PM Page 83 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 13:10 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-3 Units: ug/L Lab Code: J1800711-012 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 0.600 U 4.78 0.600 1 01/29/18 23:09 1/29/18 1,2-Dichlorobenzene 0.640 U 4.78 0.640 1 01/29/18 23:09 1/29/18 1,3-Dichlorobenzene 0.920 U 4.78 0.920 1 01/29/18 23:09 1/29/18 1,4-Dichlorobenzene 0.910 U 4.78 0.910 1 01/29/18 23:09 1/29/18 1-Methylnaphthalene 0.730 U 4.78 0.730 1 01/29/18 23:09 1/29/18 2,4,5-Trichlorophenol 1.30 U 4.78 1.30 1 01/29/18 23:09 1/29/18 2,4,6-Trichlorophenol 0.890 U 4.78 0.890 1 01/29/18 23:09 1/29/18 2,4-Dichlorophenol 1.20 U 4.78 1.20 1 01/29/18 23:09 1/29/18 2,4-Dimethylphenol 1.50 U 4.78 1.50 1 01/29/18 23:09 1/29/18 2,4-Dinitrophenol 4.24 I 19.1 0.760 1 01/29/18 23:09 1/29/18 2,4-Dinitrotoluene 1.30 U 4.78 1.30 1 01/29/18 23:09 1/29/18 2,6-Dinitrotoluene 1.10 U 4.78 1.10 1 01/29/18 23:09 1/29/18 2-Chloronaphthalene 4.60 U 4.78 4.60 1 01/29/18 23:09 1/29/18 2-Chlorophenol 1.20 U 4.78 1.20 1 01/29/18 23:09 1/29/18 2-Methylnaphthalene 0.630 U 4.78 0.630 1 01/29/18 23:09 1/29/18 2-Methylphenol 1.30 U 4.78 1.30 1 01/29/18 23:09 1/29/18 2-Nitroaniline 1.50 U 4.78 1.50 1 01/29/18 23:09 1/29/18 2-Nitrophenol 1.40 U 19.1 1.40 1 01/29/18 23:09 1/29/18 3- and 4-Methylphenol Coelution 1.00 U 4.78 1.00 1 01/29/18 23:09 1/29/18 3,3'-Dichlorobenzidine 1.40 U 19.1 1.40 1 01/29/18 23:09 1/29/18 3-Nitroaniline 1.10 U 4.78 1.10 1 01/29/18 23:09 1/29/18 4,6-Dinitro-2-methylphenol 1.00 U 19.1 1.00 1 01/29/18 23:09 1/29/18 4-Bromophenyl Phenyl Ether 1.30 U 4.78 1.30 1 01/29/18 23:09 1/29/18 4-Chloro-3-methylphenol 1.80 U 4.78 1.80 1 01/29/18 23:09 1/29/18 4-Chloroaniline 1.40 U 4.78 1.40 1 01/29/18 23:09 1/29/18 4-Chlorophenyl Phenyl Ether 0.960 U 4.78 0.960 1 01/29/18 23:09 1/29/18 4-Nitroaniline 1.00 U 4.78 1.00 1 01/29/18 23:09 1/29/18 4-Nitrophenol 1.80 U 19.1 1.80 1 01/29/18 23:09 1/29/18 Acenaphthene 4.20 U 4.78 4.20 1 01/29/18 23:09 1/29/18 Acenaphthylene 0.990 U 4.78 0.990 1 01/29/18 23:09 1/29/18 Acetophenone 1.60 U 9.57 1.60 1 01/29/18 23:09 1/29/18 Anthracene 1.60 U 4.78 1.60 1 01/29/18 23:09 1/29/18 Benz(a)anthracene 1.00 U 4.78 1.00 1 01/29/18 23:09 1/29/18 Benzo(a)pyrene 1.20 U 4.78 1.20 1 01/29/18 23:09 1/29/18 Benzo(b)fluoranthene 1.00 U 4.78 1.00 1 01/29/18 23:09 1/29/18 Benzo(g,h,i)perylene 1.40 U 4.78 1.40 1 01/29/18 23:09 1/29/18 Benzo(k)fluoranthene 1.80 U 4.78 1.80 1 01/29/18 23:09 1/29/18 Benzyl Alcohol 1.40 U 4.78 1.40 1 01/29/18 23:09 1/29/18 Bis(2-chloroethoxy)methane 1.20 U 4.78 1.20 1 01/29/18 23:09 1/29/18 Bis(2-chloroethyl) Ether 1.90 U 4.78 1.90 1 01/29/18 23:09 1/29/18 Bis(2-chloroisopropyl) Ether 1.50 U 4.78 1.50 1 01/29/18 23:09 1/29/18 Bis(2-ethylhexyl) Phthalate 1.50 U 4.78 1.50 1 01/29/18 23:09 1/29/18 Butyl Benzyl Phthalate 0.860 U 9.57 0.860 1 01/29/18 23:09 1/29/18 Printed 2/5/2018 3:02:47 PM Page 84 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 13:10 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-3 Units: ug/L Lab Code: J1800711-012 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 1.80 U 4.78 1.80 1 01/29/18 23:09 1/29/18 Chrysene 1.20 U 4.78 1.20 1 01/29/18 23:09 1/29/18 Dibenz(a,h)anthracene L50 U 4.78 1.50 1 01/29/18 23:09 1/29/18 Dibenzofuran 1.30 U 4.78 1.30 1 01/29/18 23:09 1/29/18 Diethyl Phthalate 1.70 U 4.78 1.70 1 01/29/18 23:09 1/29/18 Dimethyl Phthalate 1.30 U 4.78 1.30 1 01/29/18 23:09 1/29/18 Di-n-butyl Phthalate 2.20 U 4.78 2.20 1 01/29/18 23:09 1/29/18 Di-n-octyl Phthalate 2.80 U 9.57 2.80 1 01/29/18 23:09 1/29/18 Diphenylamine + n-Nitrosodiphenylamine 1.10 U 4.78 1.10 1 01/29/18 23:09 1/29/18 Fluoranthene 1.40 U 4.78 1.40 1 01/29/18 23:09 1/29/18 Fluorene 0.840 U 4.78 0.840 1 01/29/18 23:09 1/29/18 Hexachlorobenzene 1.70 U 4.78 1.70 1 01/29/18 23:09 1/29/18 Hexachlorobutadiene 1.20 U 4.78 1.20 1 01/29/18 23:09 1/29/18 Hexachlorocyclopentadiene 0.500 U 4.78 0.500 1 01/29/18 23:09 1/29/18 Hexachloroethane 0.810 U 4.78 0.810 1 01/29/18 23:09 1/29/18 Indeno(1,2,3-cd)pyrene 1.70 U 4.78 1.70 1 01/29/18 23:09 1/29/18 Isophorone 1.80 U 4.78 1.80 1 01/29/18 23:09 1/29/18 Naphthalene 0.530 U 4.78 0.530 1 01/29/18 23:09 1/29/18 Nitrobenzene 2.10 U 4.78 2.10 1 01/29/18 23:09 1/29/18 N-Nitrosodi-n-propylamine 2.20 U 4.78 2.20 1 01/29/18 23:09 1/29/18 Pentachlorophenol (PCP) 1.10 U 19.1 1.10 1 01/29/18 23:09 1/29/18 Phenanthrene 1.40 U 4.78 1.40 1 01/29/18 23:09 1/29/18 Phenol 0.590 U 4.78 0.590 1 01/29/18 23:09 1/29/18 Pyrene 0.740 U 4.78 0.740 1 01/29/18 23:09 1/29/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 72 23 - 122 01/29/18 23:09 2-Fluorobiphenyl 53 15 - 117 01/29/18 23:09 2-Fluorophenol 37 10 - 85 01/29/18 23:09 Nitrobenzene-d5 48 10 - 110 01/29/18 23:09 Phenol-d6 29 7 - 60 01/29/18 23:09 p-Terphenyl-dl4 73 40 - 125 01/29/18 23:09 Printed 2/5/2018 3:02:47 PM Page 85 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 15:25 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-2 Units: ug/L Lab Code: J1800711-013 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 0.600 U 4.81 0.600 1 01/30/18 19:45 1/30/18 1,2-Dichlorobenzene 0.640 U 4.81 0.640 1 01/30/18 19:45 1/30/18 1,3-Dichlorobenzene 0.920 U 4.81 0.920 1 01/30/18 19:45 1/30/18 1,4-Dichlorobenzene 0.910 U 4.81 0.910 1 01/30/18 19:45 1/30/18 1-Methylnaphthalene 0.730 U 4.81 0.730 1 01/30/18 19:45 1/30/18 2,4,5-Trichlorophenol 1.30 U 4.81 1.30 1 01/30/18 19:45 1/30/18 2,4,6-Trichlorophenol 0.890 U 4.81 0.890 1 01/30/18 19:45 1/30/18 2,4-Dichlorophenol 1.20 U 4.81 1.20 1 01/30/18 19:45 1/30/18 2,4-Dimethylphenol 1.50 U 4.81 1.50 1 01/30/18 19:45 1/30/18 2,4-Dinitrophenol 0.760 U 19.2 0.760 1 01/30/18 19:45 1/30/18 2,4-Dinitrotoluene 1.30 U 4.81 1.30 1 01/30/18 19:45 1/30/18 2,6-Dinitrotoluene 1.10 U 4.81 1.10 1 01/30/18 19:45 1/30/18 2-Chloronaphthalene 4.60 U 4.81 4.60 1 01/30/18 19:45 1/30/18 2-Chlorophenol 1.20 U 4.81 1.20 1 01/30/18 19:45 1/30/18 2-Methylnaphthalene 0.630 U 4.81 0.630 1 01/30/18 19:45 1/30/18 2-Methylphenol 1.30 U 4.81 1.30 1 01/30/18 19:45 1/30/18 2-Nitroaniline 1.50 U 4.81 1.50 1 01/30/18 19:45 1/30/18 2-Nitrophenol 1.40 U 19.2 1.40 1 01/30/18 19:45 1/30/18 3- and 4-Methylphenol Coelution 1.00 U 4.81 1.00 1 01/30/18 19:45 1/30/18 3,3'-Dichlorobenzidine 1.40 U 19.2 1.40 1 01/30/18 19:45 1/30/18 3-Nitroaniline 1.10 U 4.81 1.10 1 01/30/18 19:45 1/30/18 4,6-Dinitro-2-methylphenol 1.00 U 19.2 1.00 1 01/30/18 19:45 1/30/18 4-Bromophenyl Phenyl Ether 1.30 U 4.81 1.30 1 01/30/18 19:45 1/30/18 4-Chloro-3-methylphenol 1.80 U 4.81 1.80 1 01/30/18 19:45 1/30/18 4-Chloroaniline 1.40 U 4.81 1.40 1 01/30/18 19:45 1/30/18 4-Chlorophenyl Phenyl Ether 0.960 U 4.81 0.960 1 01/30/18 19:45 1/30/18 4-Nitroaniline 1.00 U 4.81 1.00 1 01/30/18 19:45 1/30/18 4-Nitrophenol 1.80 U 19.2 1.80 1 01/30/18 19:45 1/30/18 Acenaphthene 4.20 U 4.81 4.20 1 01/30/18 19:45 1/30/18 Acenaphthylene 0.990 U 4.81 0.990 1 01/30/18 19:45 1/30/18 Acetophenone 1.60 U 9.62 1.60 1 01/30/18 19:45 1/30/18 Anthracene 1.60 U 4.81 1.60 1 01/30/18 19:45 1/30/18 Benz(a)anthracene 1.00 U 4.81 1.00 1 01/30/18 19:45 1/30/18 Benzo(a)pyrene 1.20 U 4.81 1.20 1 01/30/18 19:45 1/30/18 Benzo(b)fluoranthene 1.00 U 4.81 1.00 1 01/30/18 19:45 1/30/18 Benzo(g,h,i)perylene 1.40 U 4.81 1.40 1 01/30/18 19:45 1/30/18 Benzo(k)fluoranthene 1.80 U 4.81 1.80 1 01/30/18 19:45 1/30/18 Benzyl Alcohol 1.40 U 4.81 1.40 1 01/30/18 19:45 1/30/18 Bis(2-chloroethoxy)methane 1.20 U 4.81 1.20 1 01/30/18 19:45 1/30/18 Bis(2-chloroethyl) Ether 1.90 U 4.81 1.90 1 01/30/18 19:45 1/30/18 Bis(2-chloroisopropyl) Ether 1.50 U 4.81 1.50 1 01/30/18 19:45 1/30/18 Bis(2-ethylhexyl) Phthalate 1.50 U 4.81 1.50 1 01/30/18 19:45 1/30/18 Butyl Benzyl Phthalate 0.860 U 9.62 0.860 1 01/30/18 19:45 1/30/18 Printed 2/5/2018 3:02:47 PM Page 86 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 15:25 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-2 Units: ug/L Lab Code: J1800711-013 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 1.80 U 4.81 1.80 1 01/30/18 19:45 1/30/18 Chrysene 1.20 U 4.81 1.20 1 01/30/18 19:45 1/30/18 Dibenz(a,h)anthracene L50 U 4.81 1.50 1 01/30/18 19:45 1/30/18 Dibenzofuran 1.30 U 4.81 1.30 1 01/30/18 19:45 1/30/18 Diethyl Phthalate 1.70 U 4.81 1.70 1 01/30/18 19:45 1/30/18 Dimethyl Phthalate 1.30 U 4.81 1.30 1 01/30/18 19:45 1/30/18 Di-n-butyl Phthalate 2.20 U 4.81 2.20 1 01/30/18 19:45 1/30/18 Di-n-octyl Phthalate 2.80 U 9.62 2.80 1 01/30/18 19:45 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 1.10 U 4.81 1.10 1 01/30/18 19:45 1/30/18 Fluoranthene 1.40 U 4.81 1.40 1 01/30/18 19:45 1/30/18 Fluorene 0.840 U 4.81 0.840 1 01/30/18 19:45 1/30/18 Hexachlorobenzene 1.70 U 4.81 1.70 1 01/30/18 19:45 1/30/18 Hexachlorobutadiene 1.20 U 4.81 1.20 1 01/30/18 19:45 1/30/18 Hexachlorocyclopentadiene 0.500 U 4.81 0.500 1 01/30/18 19:45 1/30/18 Hexachloroethane 0.810 U 4.81 0.810 1 01/30/18 19:45 1/30/18 Indeno(1,2,3-cd)pyrene 1.70 U 4.81 1.70 1 01/30/18 19:45 1/30/18 Isophorone 1.80 U 4.81 1.80 1 01/30/18 19:45 1/30/18 Naphthalene 0.530 U 4.81 0.530 1 01/30/18 19:45 1/30/18 Nitrobenzene 2.10 U 4.81 2.10 1 01/30/18 19:45 1/30/18 N-Nitrosodi-n-propylamine 2.20 U 4.81 2.20 1 01/30/18 19:45 1/30/18 Pentachlorophenol (PCP) 1.10 U 19.2 1.10 1 01/30/18 19:45 1/30/18 Phenanthrene 1.40 U 4.81 1.40 1 01/30/18 19:45 1/30/18 Phenol 0.590 U 4.81 0.590 1 01/30/18 19:45 1/30/18 Pyrene 0.740 U 4.81 0.740 1 01/30/18 19:45 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 63 23 - 122 01/30/18 19:45 2-Fluorobiphenyl 68 15 - 117 01/30/18 19:45 2-Fluorophenol 51 10 - 85 01/30/18 19:45 Nitrobenzene-d5 70 10 - 110 01/30/18 19:45 Phenol-d6 40 7 - 60 01/30/18 19:45 p-Terphenyl-dl4 86 40 - 125 01/30/18 19:45 Printed 2/5/2018 3:02:47 PM Page 87 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 16:50 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-4 Units: ug/L Lab Code: J1800711-014 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 0.600 U 4.81 0.600 1 01/30/18 20:10 1/30/18 1,2-Dichlorobenzene 0.640 U 4.81 0.640 1 01/30/18 20:10 1/30/18 1,3-Dichlorobenzene 0.920 U 4.81 0.920 1 01/30/18 20:10 1/30/18 1,4-Dichlorobenzene 0.910 U 4.81 0.910 1 01/30/18 20:10 1/30/18 1-Methylnaphthalene 0.730 U 4.81 0.730 1 01/30/18 20:10 1/30/18 2,4,5-Trichlorophenol 1.30 U 4.81 1.30 1 01/30/18 20:10 1/30/18 2,4,6-Trichlorophenol 0.890 U 4.81 0.890 1 01/30/18 20:10 1/30/18 2,4-Dichlorophenol 1.20 U 4.81 1.20 1 01/30/18 20:10 1/30/18 2,4-Dimethylphenol 1.50 U 4.81 1.50 1 01/30/18 20:10 1/30/18 2,4-Dinitrophenol 0.760 U 19.2 0.760 1 01/30/18 20:10 1/30/18 2,4-Dinitrotoluene 1.30 U 4.81 1.30 1 01/30/18 20:10 1/30/18 2,6-Dinitrotoluene 1.10 U 4.81 1.10 1 01/30/18 20:10 1/30/18 2-Chloronaphthalene 4.60 U 4.81 4.60 1 01/30/18 20:10 1/30/18 2-Chlorophenol 1.20 U 4.81 1.20 1 01/30/18 20:10 1/30/18 2-Methylnaphthalene 0.630 U 4.81 0.630 1 01/30/18 20:10 1/30/18 2-Methylphenol 1.30 U 4.81 1.30 1 01/30/18 20:10 1/30/18 2-Nitroaniline 1.50 U 4.81 1.50 1 01/30/18 20:10 1/30/18 2-Nitrophenol 1.40 U 19.2 1.40 1 01/30/18 20:10 1/30/18 3- and 4-Methylphenol Coelution 1.00 U 4.81 1.00 1 01/30/18 20:10 1/30/18 3,3'-Dichlorobenzidine 1.40 U 19.2 1.40 1 01/30/18 20:10 1/30/18 3-Nitroaniline 1.10 U 4.81 1.10 1 01/30/18 20:10 1/30/18 4,6-Dinitro-2-methylphenol 1.00 U 19.2 1.00 1 01/30/18 20:10 1/30/18 4-Bromophenyl Phenyl Ether 1.30 U 4.81 1.30 1 01/30/18 20:10 1/30/18 4-Chloro-3-methylphenol 1.80 U 4.81 1.80 1 01/30/18 20:10 1/30/18 4-Chloroaniline 1.40 U 4.81 1.40 1 01/30/18 20:10 1/30/18 4-Chlorophenyl Phenyl Ether 0.960 U 4.81 0.960 1 01/30/18 20:10 1/30/18 4-Nitroaniline 1.00 U 4.81 1.00 1 01/30/18 20:10 1/30/18 4-Nitrophenol 1.80 U 19.2 1.80 1 01/30/18 20:10 1/30/18 Acenaphthene 4.20 U 4.81 4.20 1 01/30/18 20:10 1/30/18 Acenaphthylene 0.990 U 4.81 0.990 1 01/30/18 20:10 1/30/18 Acetophenone 1.60 U 9.62 1.60 1 01/30/18 20:10 1/30/18 Anthracene 1.60 U 4.81 1.60 1 01/30/18 20:10 1/30/18 Benz(a)anthracene 1.00 U 4.81 1.00 1 01/30/18 20:10 1/30/18 Benzo(a)pyrene 1.20 U 4.81 1.20 1 01/30/18 20:10 1/30/18 Benzo(b)fluoranthene 1.00 U 4.81 1.00 1 01/30/18 20:10 1/30/18 Benzo(g,h,i)perylene 1.40 U 4.81 1.40 1 01/30/18 20:10 1/30/18 Benzo(k)fluoranthene 1.80 U 4.81 1.80 1 01/30/18 20:10 1/30/18 Benzyl Alcohol 1.40 U 4.81 1.40 1 01/30/18 20:10 1/30/18 Bis(2-chloroethoxy)methane 1.20 U 4.81 1.20 1 01/30/18 20:10 1/30/18 Bis(2-chloroethyl) Ether 1.90 U 4.81 1.90 1 01/30/18 20:10 1/30/18 Bis(2-chloroisopropyl) Ether 1.50 U 4.81 1.50 1 01/30/18 20:10 1/30/18 Bis(2-ethylhexyl) Phthalate 1.50 U 4.81 1.50 1 01/30/18 20:10 1/30/18 Butyl Benzyl Phthalate 0.860 U 9.62 0.860 1 01/30/18 20:10 1/30/18 Printed 2/5/2018 3:02:48 PM Page 88 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 16:50 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-4 Units: ug/L Lab Code: J1800711-014 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 1.80 U 4.81 1.80 1 01/30/18 20:10 1/30/18 Chrysene 1.20 U 4.81 1.20 1 01/30/18 20:10 1/30/18 Dibenz(a,h)anthracene L50 U 4.81 1.50 1 01/30/18 20:10 1/30/18 Dibenzofuran 1.30 U 4.81 1.30 1 01/30/18 20:10 1/30/18 Diethyl Phthalate 1.70 U 4.81 1.70 1 01/30/18 20:10 1/30/18 Dimethyl Phthalate 1.30 U 4.81 1.30 1 01/30/18 20:10 1/30/18 Di-n-butyl Phthalate 2.20 U 4.81 2.20 1 01/30/18 20:10 1/30/18 Di-n-octyl Phthalate 2.80 U 9.62 2.80 1 01/30/18 20:10 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 1.10 U 4.81 1.10 1 01/30/18 20:10 1/30/18 Fluoranthene 1.40 U 4.81 1.40 1 01/30/18 20:10 1/30/18 Fluorene 0.840 U 4.81 0.840 1 01/30/18 20:10 1/30/18 Hexachlorobenzene 1.70 U 4.81 1.70 1 01/30/18 20:10 1/30/18 Hexachlorobutadiene 1.20 U 4.81 1.20 1 01/30/18 20:10 1/30/18 Hexachlorocyclopentadiene 0.500 U 4.81 0.500 1 01/30/18 20:10 1/30/18 Hexachloroethane 0.810 U 4.81 0.810 1 01/30/18 20:10 1/30/18 Indeno(1,2,3-cd)pyrene 1.70 U 4.81 1.70 1 01/30/18 20:10 1/30/18 Isophorone 1.80 U 4.81 1.80 1 01/30/18 20:10 1/30/18 Naphthalene 0.530 U 4.81 0.530 1 01/30/18 20:10 1/30/18 Nitrobenzene 2.10 U 4.81 2.10 1 01/30/18 20:10 1/30/18 N-Nitrosodi-n-propylamine 2.20 U 4.81 2.20 1 01/30/18 20:10 1/30/18 Pentachlorophenol (PCP) 1.10 U 19.2 1.10 1 01/30/18 20:10 1/30/18 Phenanthrene 1.40 U 4.81 1.40 1 01/30/18 20:10 1/30/18 Phenol 0.590 U 4.81 0.590 1 01/30/18 20:10 1/30/18 Pyrene 0.740 U 4.81 0.740 1 01/30/18 20:10 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 56 23 - 122 01/30/18 20:10 2-Fluorobiphenyl 59 15 - 117 01/30/18 20:10 2-Fluorophenol 46 10 - 85 01/30/18 20:10 Nitrobenzene-d5 62 10 - 110 01/30/18 20:10 Phenol-d6 35 7 - 60 01/30/18 20:10 p-Terphenyl-dl4 79 40 - 125 01/30/18 20:10 Printed 2/5/2018 3:02:48 PM Page 89 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 17:20 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-5 Units: ug/L Lab Code: J1800711-015 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 0.600 U 4.78 0.600 1 01/30/18 00:24 1/29/18 1,2-Dichlorobenzene 0.640 U 4.78 0.640 1 01/30/18 00:24 1/29/18 1,3-Dichlorobenzene 0.920 U 4.78 0.920 1 01/30/18 00:24 1/29/18 1,4-Dichlorobenzene 0.910 U 4.78 0.910 1 01/30/18 00:24 1/29/18 1-Methylnaphthalene 0.730 U 4.78 0.730 1 01/30/18 00:24 1/29/18 2,4,5-Trichlorophenol 1.30 U 4.78 1.30 1 01/30/18 00:24 1/29/18 2,4,6-Trichlorophenol 0.890 U 4.78 0.890 1 01/30/18 00:24 1/29/18 2,4-Dichlorophenol 1.20 U 4.78 1.20 1 01/30/18 00:24 1/29/18 2,4-Dimethylphenol 1.50 U 4.78 1.50 1 01/30/18 00:24 1/29/18 2,4-Dinitrophenol 0.760 U 19.1 0.760 1 01/30/18 00:24 1/29/18 2,4-Dinitrotoluene 1.30 U 4.78 1.30 1 01/30/18 00:24 1/29/18 2,6-Dinitrotoluene 1.10 U 4.78 1.10 1 01/30/18 00:24 1/29/18 2-Chloronaphthalene 4.60 U 4.78 4.60 1 01/30/18 00:24 1/29/18 2-Chlorophenol 1.20 U 4.78 1.20 1 01/30/18 00:24 1/29/18 2-Methylnaphthalene 0.630 U 4.78 0.630 1 01/30/18 00:24 1/29/18 2-Methylphenol 1.30 U 4.78 1.30 1 01/30/18 00:24 1/29/18 2-Nitroaniline 1.50 U 4.78 1.50 1 01/30/18 00:24 1/29/18 2-Nitrophenol 1.40 U 19.1 1.40 1 01/30/18 00:24 1/29/18 3- and 4-Methylphenol Coelution 1.00 U 4.78 1.00 1 01/30/18 00:24 1/29/18 3,3'-Dichlorobenzidine 1.40 U 19.1 1.40 1 01/30/18 00:24 1/29/18 3-Nitroaniline 1.10 U 4.78 1.10 1 01/30/18 00:24 1/29/18 4,6-Dinitro-2-methylphenol 1.00 U 19.1 1.00 1 01/30/18 00:24 1/29/18 4-Bromophenyl Phenyl Ether 1.30 U 4.78 1.30 1 01/30/18 00:24 1/29/18 4-Chloro-3-methylphenol 1.80 U 4.78 1.80 1 01/30/18 00:24 1/29/18 4-Chloroaniline 1.40 U 4.78 1.40 1 01/30/18 00:24 1/29/18 4-Chlorophenyl Phenyl Ether 0.960 U 4.78 0.960 1 01/30/18 00:24 1/29/18 4-Nitroaniline 1.00 U 4.78 1.00 1 01/30/18 00:24 1/29/18 4-Nitrophenol 1.80 U 19.1 1.80 1 01/30/18 00:24 1/29/18 Acenaphthene 4.20 U 4.78 4.20 1 01/30/18 00:24 1/29/18 Acenaphthylene 0.990 U 4.78 0.990 1 01/30/18 00:24 1/29/18 Acetophenone 1.60 U 9.57 1.60 1 01/30/18 00:24 1/29/18 Anthracene 1.60 U 4.78 1.60 1 01/30/18 00:24 1/29/18 Benz(a)anthracene 1.00 U 4.78 1.00 1 01/30/18 00:24 1/29/18 Benzo(a)pyrene 1.20 U 4.78 1.20 1 01/30/18 00:24 1/29/18 Benzo(b)fluoranthene 1.00 U 4.78 1.00 1 01/30/18 00:24 1/29/18 Benzo(g,h,i)perylene 1.40 U 4.78 1.40 1 01/30/18 00:24 1/29/18 Benzo(k)fluoranthene 1.80 U 4.78 1.80 1 01/30/18 00:24 1/29/18 Benzyl Alcohol 1.40 U 4.78 1.40 1 01/30/18 00:24 1/29/18 Bis(2-chloroethoxy)methane 1.20 U 4.78 1.20 1 01/30/18 00:24 1/29/18 Bis(2-chloroethyl) Ether 1.90 U 4.78 1.90 1 01/30/18 00:24 1/29/18 Bis(2-chloroisopropyl) Ether 1.50 U 4.78 1.50 1 01/30/18 00:24 1/29/18 Bis(2-ethylhexyl) Phthalate 1.50 U 4.78 1.50 1 01/30/18 00:24 1/29/18 Butyl Benzyl Phthalate 0.860 U 9.57 0.860 1 01/30/18 00:24 1/29/18 Printed 2/5/2018 3:02:48 PM Page 90 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/24/18 17:20 Sample Matrix: Water Date Received: 01/27/18 08:50 Sample Name: TW-5 Units: ug/L Lab Code: J1800711-015 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 1.80 U 4.78 1.80 1 01/30/18 00:24 1/29/18 Chrysene 1.20 U 4.78 1.20 1 01/30/18 00:24 1/29/18 Dibenz(a,h)anthracene L50 U 4.78 1.50 1 01/30/18 00:24 1/29/18 Dibenzofuran 1.30 U 4.78 1.30 1 01/30/18 00:24 1/29/18 Diethyl Phthalate 1.70 U 4.78 1.70 1 01/30/18 00:24 1/29/18 Dimethyl Phthalate 1.30 U 4.78 1.30 1 01/30/18 00:24 1/29/18 Di-n-butyl Phthalate 2.20 U 4.78 2.20 1 01/30/18 00:24 1/29/18 Di-n-octyl Phthalate 2.80 U 9.57 2.80 1 01/30/18 00:24 1/29/18 Diphenylamine + n-Nitrosodiphenylamine 1.10 U 4.78 1.10 1 01/30/18 00:24 1/29/18 Fluoranthene 1.40 U 4.78 1.40 1 01/30/18 00:24 1/29/18 Fluorene 0.840 U 4.78 0.840 1 01/30/18 00:24 1/29/18 Hexachlorobenzene 1.70 U 4.78 1.70 1 01/30/18 00:24 1/29/18 Hexachlorobutadiene 1.20 U 4.78 1.20 1 01/30/18 00:24 1/29/18 Hexachlorocyclopentadiene 0.500 U 4.78 0.500 1 01/30/18 00:24 1/29/18 Hexachloroethane 0.810 U 4.78 0.810 1 01/30/18 00:24 1/29/18 Indeno(1,2,3-cd)pyrene 1.70 U 4.78 1.70 1 01/30/18 00:24 1/29/18 Isophorone 1.80 U 4.78 1.80 1 01/30/18 00:24 1/29/18 Naphthalene 0.530 U 4.78 0.530 1 01/30/18 00:24 1/29/18 Nitrobenzene 2.10 U 4.78 2.10 1 01/30/18 00:24 1/29/18 N-Nitrosodi-n-propylamine 2.20 U 4.78 2.20 1 01/30/18 00:24 1/29/18 Pentachlorophenol (PCP) 1.10 U 19.1 1.10 1 01/30/18 00:24 1/29/18 Phenanthrene 1.40 U 4.78 1.40 1 01/30/18 00:24 1/29/18 Phenol 0.590 U 4.78 0.590 1 01/30/18 00:24 1/29/18 Pyrene 0.740 U 4.78 0.740 1 01/30/18 00:24 1/29/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 56 23 - 122 01/30/18 00:24 2-Fluorobiphenyl 49 15 - 117 01/30/18 00:24 2-Fluorophenol 42 10 - 85 01/30/18 00:24 Nitrobenzene-d5 49 10 - 110 01/30/18 00:24 Phenol-d6 39 7 - 60 01/30/18 00:24 p-Terphenyl-dl4 74 40 - 125 01/30/18 00:24 Printed 2/5/2018 3:02:48 PM Page 91 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Analysis Method: Prep Method: Terracon Environmental WWAY Building/ES187011 Water TW-1 J1800711-011 8270D SIM EPA 3510C Service Request: J1800711 Date Collected: 01/24/18 11:20 Date Received: 01/27/18 08:50 Base Neutral Semivolatile Organic Compounds by GC/MS SIM Units: ug/L Basis: NA Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1-Methylnaphthalene 0.0440 U 0.0957 0.0440 1 01/29/18 21:54 1/29/18 2-Methylnaphthalene 0.0440 U 0.0957 0.0440 1 01/29/18 21:54 1/29/18 Acenaphthene 0.0410 U 0.0957 0.0410 1 01/29/18 21:54 1/29/18 Acenaphthylene 0.0250 U 0.0957 0.0250 1 01/29/18 21:54 1/29/18 Anthracene 0.0380 U 0.0957 0.0380 1 01/29/18 21:54 1/29/18 Benz(a)anthracene 0.0555 I 0.0957 0.0350 1 01/29/18 21:54 1/29/18 Benzo(a)pyrene 0.0310 U 0.0957 0.0310 1 01/29/18 21:54 1/29/18 Benzo(b)fluoranthene 0.0250 U 0.0957 0.0250 1 01/29/18 21:54 1/29/18 Benzo(g,h,i)perylene 0.0390 U 0.0957 0.0390 1 01/29/18 21:54 1/29/18 Benzo(k)fluoranthene 0.0350 U 0.0957 0.0350 1 01/29/18 21:54 1/29/18 Chrysene 0.0241 I 0.0957 0.0240 1 01/29/18 21:54 1/29/18 Dibenz(a,h)anthracene 0.0360 U 0.0957 0.0360 1 01/29/18 21:54 1/29/18 Fluoranthene 0.0390 U 0.0957 0.0390 1 01/29/18 21:54 1/29/18 Fluorene 0.0470 U 0.0957 0.0470 1 01/29/18 21:54 1/29/18 Indeno(1,2,3-cd)pyrene 0.0400 U 0.0957 0.0400 1 01/29/18 21:54 1/29/18 Phenanthrene 0.0363 I 0.0957 0.0350 1 01/29/18 21:54 1/29/18 Pyrene 0.0373 I 0.0957 0.0310 1 01/29/18 21:54 1/29/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2-Fluorobiphenyl 60 22 - 105 01/29/18 21:54 p-Terphenyl-dl4 116 25 - 127 01/29/18 21:54 Printed 2/5/2018 3:02:58 PM Page 92 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Analysis Method: Prep Method: Terracon Environmental WWAY Building/ES187011 Water TW-3 J1800711-012 8270D SIM EPA 3510C Service Request: J1800711 Date Collected: 01/24/18 13:10 Date Received: 01/27/18 08:50 Base Neutral Semivolatile Organic Compounds by GC/MS SIM Units: ug/L Basis: NA Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1-Methylnaphthalene 0.0488 I 0.0957 0.0440 1 01/29/18 22:21 1/29/18 2-Methylnaphthalene 0.0440 U 0.0957 0.0440 1 01/29/18 22:21 1/29/18 Acenaphthene 0.0410 U 0.0957 0.0410 1 01/29/18 22:21 1/29/18 Acenaphthylene 0.0250 U 0.0957 0.0250 1 01/29/18 22:21 1/29/18 Anthracene 0.0380 U 0.0957 0.0380 1 01/29/18 22:21 1/29/18 Benz(a)anthracene 0.0350 U 0.0957 0.0350 1 01/29/18 22:21 1/29/18 Benzo(a)pyrene 0.0310 U 0.0957 0.0310 1 01/29/18 22:21 1/29/18 Benzo(b)fluoranthene 0.0250 U 0.0957 0.0250 1 01/29/18 22:21 1/29/18 Benzo(g,h,i)perylene 0.0390 U 0.0957 0.0390 1 01/29/18 22:21 1/29/18 Benzo(k)fluoranthene 0.0350 U 0.0957 0.0350 1 01/29/18 22:21 1/29/18 Chrysene 0.0240 U 0.0957 0.0240 1 01/29/18 22:21 1/29/18 Dibenz(a,h)anthracene 0.0360 U 0.0957 0.0360 1 01/29/18 22:21 1/29/18 Fluoranthene 0.0390 U 0.0957 0.0390 1 01/29/18 22:21 1/29/18 Fluorene 0.0470 U 0.0957 0.0470 1 01/29/18 22:21 1/29/18 Indeno(1,2,3-cd)pyrene 0.0400 U 0.0957 0.0400 1 01/29/18 22:21 1/29/18 Phenanthrene 0.0350 U 0.0957 0.0350 1 01/29/18 22:21 1/29/18 Pyrene 0.0310 U 0.0957 0.0310 1 01/29/18 22:21 1/29/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2-Fluorobiphenyl 52 22 - 105 01/29/18 22:21 p-Terphenyl-dl4 118 25 - 127 01/29/18 22:21 Printed 2/5/2018 3:02:58 PM Page 93 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Analysis Method: Prep Method: Terracon Environmental WWAY Building/ES187011 Water TW-2 J1800711-013 8270D SIM EPA 3510C Service Request: J1800711 Date Collected: 01/24/18 15:25 Date Received: 01/27/18 08:50 Base Neutral Semivolatile Organic Compounds by GC/MS SIM Units: ug/L Basis: NA Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1-Methylnaphthalene 0.0440 U 0.0943 0.0440 1 01/29/18 22:48 1/29/18 2-Methylnaphthalene 0.0440 U 0.0943 0.0440 1 01/29/18 22:48 1/29/18 Acenaphthene 0.0410 U 0.0943 0.0410 1 01/29/18 22:48 1/29/18 Acenaphthylene 0.0250 U 0.0943 0.0250 1 01/29/18 22:48 1/29/18 Anthracene 0.0380 U 0.0943 0.0380 1 01/29/18 22:48 1/29/18 Benz(a)anthracene 0.0350 U 0.0943 0.0350 1 01/29/18 22:48 1/29/18 Benzo(a)pyrene 0.0310 U 0.0943 0.0310 1 01/29/18 22:48 1/29/18 Benzo(b)fluoranthene 0.0250 U 0.0943 0.0250 1 01/29/18 22:48 1/29/18 Benzo(g,h,i)perylene 0.0390 U 0.0943 0.0390 1 01/29/18 22:48 1/29/18 Benzo(k)fluoranthene 0.0350 U 0.0943 0.0350 1 01/29/18 22:48 1/29/18 Chrysene 0.0240 U 0.0943 0.0240 1 01/29/18 22:48 1/29/18 Dibenz(a,h)anthracene 0.0360 U 0.0943 0.0360 1 01/29/18 22:48 1/29/18 Fluoranthene 0.0390 U 0.0943 0.0390 1 01/29/18 22:48 1/29/18 Fluorene 0.0470 U 0.0943 0.0470 1 01/29/18 22:48 1/29/18 Indeno(1,2,3-cd)pyrene 0.0400 U 0.0943 0.0400 1 01/29/18 22:48 1/29/18 Phenanthrene 0.0350 U 0.0943 0.0350 1 01/29/18 22:48 1/29/18 Pyrene 0.0310 U 0.0943 0.0310 1 01/29/18 22:48 1/29/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2-Fluorobiphenyl 33 22 - 105 01/29/18 22:48 p-Terphenyl-dl4 88 25 - 127 01/29/18 22:48 Printed 2/5/2018 3:02:58 PM Page 94 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Analysis Method: Prep Method: Terracon Environmental WWAY Building/ES187011 Water TW-4 J1800711-014 8270D SIM EPA 3510C Service Request: J1800711 Date Collected: 01/24/18 16:50 Date Received: 01/27/18 08:50 Base Neutral Semivolatile Organic Compounds by GC/MS SIM Units: ug/L Basis: NA Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1-Methylnaphthalene 0.0440 U 0.0943 0.0440 1 01/29/18 23:15 1/29/18 2-Methylnaphthalene 0.0440 U 0.0943 0.0440 1 01/29/18 23:15 1/29/18 Acenaphthene 0.0410 U 0.0943 0.0410 1 01/29/18 23:15 1/29/18 Acenaphthylene 0.0250 U 0.0943 0.0250 1 01/29/18 23:15 1/29/18 Anthracene 0.0380 U 0.0943 0.0380 1 01/29/18 23:15 1/29/18 Benz(a)anthracene 0.0350 U 0.0943 0.0350 1 01/29/18 23:15 1/29/18 Benzo(a)pyrene 0.0310 U 0.0943 0.0310 1 01/29/18 23:15 1/29/18 Benzo(b)fluoranthene 0.0250 U 0.0943 0.0250 1 01/29/18 23:15 1/29/18 Benzo(g,h,i)perylene 0.0390 U 0.0943 0.0390 1 01/29/18 23:15 1/29/18 Benzo(k)fluoranthene 0.0350 U 0.0943 0.0350 1 01/29/18 23:15 1/29/18 Chrysene 0.0240 U 0.0943 0.0240 1 01/29/18 23:15 1/29/18 Dibenz(a,h)anthracene 0.0360 U 0.0943 0.0360 1 01/29/18 23:15 1/29/18 Fluoranthene 0.0390 U 0.0943 0.0390 1 01/29/18 23:15 1/29/18 Fluorene 0.0470 U 0.0943 0.0470 1 01/29/18 23:15 1/29/18 Indeno(1,2,3-cd)pyrene 0.0400 U 0.0943 0.0400 1 01/29/18 23:15 1/29/18 Phenanthrene 0.0350 U 0.0943 0.0350 1 01/29/18 23:15 1/29/18 Pyrene 0.0310 U 0.0943 0.0310 1 01/29/18 23:15 1/29/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2-Fluorobiphenyl 59 22 - 105 01/29/18 23:15 p-Terphenyl-dl4 104 25 - 127 01/29/18 23:15 Printed 2/5/2018 3:02:58 PM Page 95 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Analysis Method: Prep Method: Terracon Environmental WWAY Building/ES187011 Water TW-5 J1800711-015 8270D SIM EPA 3510C Service Request: J1800711 Date Collected: 01/24/18 17:20 Date Received: 01/27/18 08:50 Base Neutral Semivolatile Organic Compounds by GC/MS SIM Units: ug/L Basis: NA Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1-Methylnaphthalene 0.0440 U 0.0957 0.0440 1 01/29/18 23:43 1/29/18 2-Methylnaphthalene 0.0440 U 0.0957 0.0440 1 01/29/18 23:43 1/29/18 Acenaphthene 0.0410 U 0.0957 0.0410 1 01/29/18 23:43 1/29/18 Acenaphthylene 0.0652 I 0.0957 0.0250 1 01/29/18 23:43 1/29/18 Anthracene 0.0401 I 0.0957 0.0380 1 01/29/18 23:43 1/29/18 Benz(a)anthracene 0.0695 I 0.0957 0.0350 1 01/29/18 23:43 1/29/18 Benzo(a)pyrene 0.0682 I 0.0957 0.0310 1 01/29/18 23:43 1/29/18 Benzo(b)fluoranthene 0.0787 I 0.0957 0.0250 1 01/29/18 23:43 1/29/18 Benzo(g,h,i)perylene 0.0536 I 0.0957 0.0390 1 01/29/18 23:43 1/29/18 Benzo(k)fluoranthene 0.0350 U 0.0957 0.0350 1 01/29/18 23:43 1/29/18 Chrysene 0.0277 I 0.0957 0.0240 1 01/29/18 23:43 1/29/18 Dibenz(a,h)anthracene 0.0360 U 0.0957 0.0360 1 01/29/18 23:43 1/29/18 Fluoranthene 0.0390 U 0.0957 0.0390 1 01/29/18 23:43 1/29/18 Fluorene 0.0470 U 0.0957 0.0470 1 01/29/18 23:43 1/29/18 Indeno(1,2,3-cd)pyrene 0.0453 I 0.0957 0.0400 1 01/29/18 23:43 1/29/18 Phenanthrene 0.0715 I 0.0957 0.0350 1 01/29/18 23:43 1/29/18 Pyrene 0.0922 I 0.0957 0.0310 1 01/29/18 23:43 1/29/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2-Fluorobiphenyl 49 22 - 105 01/29/18 23:43 p-Terphenyl-dl4 93 25 - 127 01/29/18 23:43 Printed 2/5/2018 3:02:58 PM Page 96 of 184 Superset Reference:18-0000453045 rev 00 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 97 of 184 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 08:50 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-1-1 Units: ug/Kg Lab Code: J1800711-001 Basis: Dry Polychlorinated Biphenyls (PCBs) by GC Analysis Method: 8082 Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Aroclor 1016 9.93 U 36.1 9.93 1 01/30/18 17:09 1/30/18 Aroclor 1221 7.32 U 36.1 7.32 1 01/30/18 17:09 1/30/18 Aroclor 1232 23.7 U 36.1 23.7 1 01/30/18 17:09 1/30/18 Aroclor 1242 9.74 U 36.1 9.74 1 01/30/18 17:09 1/30/18 Aroclor 1248 17.6 U 36.1 17.6 1 01/30/18 17:09 1/30/18 Aroclor 1254 13.4 U 36.1 13.4 1 01/30/18 17:09 1/30/18 Aroclor 1260 10.2 U 36.1 10.2 1 01/30/18 17:09 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q Decachlorobiphenyl 70 10 - 155 01/30/18 17:09 Printed 2/5/2018 3:03:05 PM Page 98 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 09:30 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-1-17 Units: ug/Kg Lab Code: J1800711-002 Basis: Dry Polychlorinated Biphenyls (PCBs) by GC Analysis Method: 8082 Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Aroclor 1016 9.45 U 34.4 9.45 1 01/30/18 17:46 1/30/18 Aroclor 1221 6.97 U 34.4 6.97 1 01/30/18 17:46 1/30/18 Aroclor 1232 22.6 U 34.4 22.6 1 01/30/18 17:46 1/30/18 Aroclor 1242 9.27 U 34.4 9.27 1 01/30/18 17:46 1/30/18 Aroclor 1248 16.8 U 34.4 16.8 1 01/30/18 17:46 1/30/18 Aroclor 1254 12.7 U 34.4 12.7 1 01/30/18 17:46 1/30/18 Aroclor 1260 9.70 U 34.4 9.70 1 01/30/18 17:46 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q Decachlorobiphenyl 70 10 - 155 01/30/18 17:46 Printed 2/5/2018 3:03:05 PM Page 99 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:00 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-2-1 Units: ug/Kg Lab Code: J1800711-003 Basis: Dry Polychlorinated Biphenyls (PCBs) by GC Analysis Method: 8082 Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Aroclor 1016 9.22 U 33.6 9.22 1 01/30/18 17:58 1/30/18 Aroclor 1221 6.80 U 33.6 6.80 1 01/30/18 17:58 1/30/18 Aroclor 1232 22.0 U 33.6 22.0 1 01/30/18 17:58 1/30/18 Aroclor 1242 9.04 U 33.6 9.04 1 01/30/18 17:58 1/30/18 Aroclor 1248 16.4 U 33.6 16.4 1 01/30/18 17:58 1/30/18 Aroclor 1254 12.4 U 33.6 12.4 1 01/30/18 17:58 1/30/18 Aroclor 1260 9.46 U 33.6 9.46 1 01/30/18 17:58 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q Decachlorobiphenyl 80 10 - 155 01/30/18 00:00 Printed 2/5/2018 3:03:05 PM Page 100 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:10 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-2-12 Units: ug/Kg Lab Code: J1800711-004 Basis: Dry Polychlorinated Biphenyls (PCBs) by GC Analysis Method: 8082 Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Aroclor 1016 9.63 U 35.1 9.63 1 01/30/18 18:10 1/30/18 Aroclor 1221 7.10 U 35.1 7.10 1 01/30/18 18:10 1/30/18 Aroclor 1232 23.0 U 35.1 23.0 1 01/30/18 18:10 1/30/18 Aroclor 1242 9.45 U 35.1 9.45 1 01/30/18 18:10 1/30/18 Aroclor 1248 17.1 U 35.1 17.1 1 01/30/18 18:10 1/30/18 Aroclor 1254 13.0 U 35.1 13.0 1 01/30/18 18:10 1/30/18 Aroclor 1260 9.89 U 35.1 9.89 1 01/30/18 18:10 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q Decachlorobiphenyl 80 10 - 155 01/30/18 00:00 Printed 2/5/2018 3:03:05 PM Page 101 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 12:25 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-3-1 Units: ug/Kg Lab Code: J1800711-005 Basis: Dry Polychlorinated Biphenyls (PCBs) by GC Analysis Method: 8082 Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Aroclor 1016 10.7 U 38.7 10.7 1 01/30/18 18:22 1/30/18 Aroclor 1221 7.84 U 38.7 7.84 1 01/30/18 18:22 1/30/18 Aroclor 1232 25.4 U 38.7 25.4 1 01/30/18 18:22 1/30/18 Aroclor 1242 10.5 U 38.7 10.5 1 01/30/18 18:22 1/30/18 Aroclor 1248 18.9 U 38.7 18.9 1 01/30/18 18:22 1/30/18 Aroclor 1254 14.3 U 38.7 14.3 1 01/30/18 18:22 1/30/18 Aroclor 1260 11.0 U 38.7 11.0 1 01/30/18 18:22 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q Decachlorobiphenyl 70 10 - 155 01/30/18 00:00 Printed 2/5/2018 3:03:05 PM Page 102 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 13:00 Sample Matrix: Soil Date Received: 01/27/18 08:50 Sample Name: SB-3-14 Units: ug/Kg Lab Code: J1800711-006 Basis: Dry Polychlorinated Biphenyls (PCBs) by GC Analysis Method: 8082 Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Aroclor 1016 9.38 U 34.1 9.38 1 01/30/18 18:34 1/30/18 Aroclor 1221 6.91 U 34.1 6.91 1 01/30/18 18:34 1/30/18 Aroclor 1232 22.4 U 34.1 22.4 1 01/30/18 18:34 1/30/18 Aroclor 1242 9.20 U 34.1 9.20 1 01/30/18 18:34 1/30/18 Aroclor 1248 16.7 U 34.1 16.7 1 01/30/18 18:34 1/30/18 Aroclor 1254 12.6 U 34.1 12.6 1 01/30/18 18:34 1/30/18 Aroclor 1260 9.63 U 34.1 9.63 1 01/30/18 18:34 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q Decachlorobiphenyl 80 10 - 155 01/30/18 18:34 Printed 2/5/2018 3:03:05 PM Page 103 of 184 Superset Reference:18-0000453045 rev 00 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 104 of 184 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-1-1 J1800711-001 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 08:50 Date Received: 01/27/18 08:50 Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dfl. Date Analyzed Date Extracted Q Arsenic, Total 6010D 5.18 mg/Kg 0.39 0.07 1 02/01/18 21:17 02/01/18 Barium, Total 6010D 72.2 mg/Kg 0.39 0.02 1 02/01/18 21:17 02/01/18 Cadmium, Total 6010D 0.16 1 mg/Kg 0.19 0.02 1 02/01/18 21:17 02/01/18 Chromium, Total 6010D 6.81 mg/Kg 0.39 0.04 1 02/01/18 21:17 02/01/18 Lead, Total 6010D 296 mg/Kg 0.39 0.04 1 02/01/18 21:17 02/01/18 Mercury, Total 7471B 1.17 mg/Kg 0.073 0.005 10 01/30/18 14:48 01/29/18 Selenium, Total 6010D 0.51 mg/Kg 0.39 0.14 1 02/01/18 21:17 02/01/18 Silver, Total 6010D 0.23 IV mg/Kg 0.39 0.04 1 02/01/18 21:17 02/01/18 Printed 2/5/2018 3:03:08 PM Page 105 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-1-17 J1800711-002 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 09:30 Date Received: 01/27/18 08:50 Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dfl. Date Analyzed Date Extracted Q Arsenic, Total 6010D 0.88 mg/Kg 0.35 0.07 1 02/01/18 21:22 02/01/18 Barium, Total 6010D 12.6 mg/Kg 0.35 0.02 1 02/01/18 21:22 02/01/18 Cadmium, Total 6010D 0.02 U mg/Kg 0.18 0.02 1 02/01/18 21:22 02/01/18 Chromium, Total 6010D 1.95 mg/Kg 0.35 0.04 1 02/01/18 21:22 02/01/18 Lead, Total 6010D 64.1 mg/Kg 0.35 0.04 1 02/01/18 21:22 02/01/18 Mercury, Total 7471B 0.160 mg/Kg 0.0069 0.0005 1 01/30/18 14:19 01/29/18 Selenium, Total 6010D 0.14 U mg/Kg 0.35 0.14 1 02/01/18 21:22 02/01/18 Silver, Total 6010D 0.04 U mg/Kg 0.35 0.04 1 02/01/18 21:22 02/01/18 Printed 2/5/2018 3:03:08 PM Page 106 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-2-1 J1800711-003 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 12:00 Date Received: 01/27/18 08:50 Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dfl. Date Analyzed Date Extracted Q Arsenic, Total 6010D 0.07 U mg/Kg 0.30 0.07 1 02/01/18 22:21 02/01/18 Barium, Total 6010D 1.04 mg/Kg 0.30 0.02 1 02/01/18 22:21 02/01/18 Cadmium, Total 6010D 0.02 U mg/Kg 0.15 0.02 1 02/01/18 22:21 02/01/18 Chromium, Total 6010D 0.60 mg/Kg 0.30 0.04 1 02/01/18 22:21 02/01/18 Lead, Total 6010D 1.43 mg/Kg 0.30 0.04 1 02/01/18 22:21 02/01/18 Mercury, Total 7471B 0.0072 mg/Kg 0.0068 0.0005 1 01/30/18 14:21 01/29/18 Selenium, Total 6010D 0.15 I mg/Kg 0.30 0.14 1 02/01/18 22:21 02/01/18 Silver, Total 6010D 0.04 U mg/Kg 0.30 0.04 1 02/01/18 22:21 02/01/18 Printed 2/5/2018 3:03:09 PM Page 107 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-2-12 J1800711-004 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 12:10 Date Received: 01/27/18 08:50 Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dfl. Date Analyzed Date Extracted Q Arsenic, Total 6010D 0.27 I mg/Kg 0.44 0.07 1 02/01/18 22:26 02/01/18 Barium, Total 6010D 7.92 mg/Kg 0.44 0.02 1 02/01/18 22:26 02/01/18 Cadmium, Total 6010D 0.02 U mg/Kg 0.22 0.02 1 02/01/18 22:26 02/01/18 Chromium, Total 6010D 3.20 mg/Kg 0.44 0.04 1 02/01/18 22:26 02/01/18 Lead, Total 6010D 2.31 mg/Kg 0.44 0.04 1 02/01/18 22:26 02/01/18 Mercury, Total 7471B 0.0061 I mg/Kg 0.0071 0.0005 1 01/30/18 14:22 01/29/18 Selenium, Total 6010D 0.14 U mg/Kg 0.44 0.14 1 02/01/18 22:26 02/01/18 Silver, Total 6010D 0.04 U mg/Kg 0.44 0.04 1 02/01/18 22:26 02/01/18 Printed 2/5/2018 3:03:09 PM Page 108 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-3-1 J1800711-005 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 12:25 Date Received: 01/27/18 08:50 Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Date Extracted Q Arsenic, Total 6010D 6.87 mg/Kg 0.31 0.07 1 02/01/18 22:30 02/01/18 Barium, Total 6010D 79.6 mg/Kg 0.31 0.02 1 02/01/18 22:30 02/01/18 Cadmium, Total 6010D 0.34 mg/Kg 0.15 0.02 1 02/01/18 22:30 02/01/18 Chromium, Total 6010D 8.17 mg/Kg 0.31 0.04 1 02/01/18 22:30 02/01/18 Lead, Total 6010D 479 mg/Kg 1.5 0.2 5 02/02/18 16:50 02/01/18 Mercury, Total 7471B 4.62 mg/Kg 0.078 0.005 10 01/30/18 14:52 01/29/18 Selenium, Total 6010D 0.49 mg/Kg 0.31 0.14 1 02/01/18 22:30 02/01/18 Silver, Total 6010D 0.12 IV mg/Kg 0.31 0.04 1 02/01/18 22:30 02/01/18 Printed 2/5/2018 3:03:09 PM Page 109 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-3-14 J1800711-006 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 13:00 Date Received: 01/27/18 08:50 Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dfl. Date Analyzed Date Extracted Q Arsenic, Total 6010D 0.27 I mg/Kg 0.39 0.07 1 02/01/18 22:41 02/01/18 Barium, Total 6010D 2.40 mg/Kg 0.39 0.02 1 02/01/18 22:41 02/01/18 Cadmium, Total 6010D 0.02 U mg/Kg 0.19 0.02 1 02/01/18 22:41 02/01/18 Chromium, Total 6010D 5.18 mg/Kg 0.39 0.04 1 02/01/18 22:41 02/01/18 Lead, Total 6010D 1.32 mg/Kg 0.39 0.04 1 02/01/18 22:41 02/01/18 Mercury, Total 7471B 0.0090 mg/Kg 0.0071 0.0005 1 01/30/18 14:27 01/29/18 Selenium, Total 6010D 0.14 U mg/Kg 0.39 0.14 1 02/01/18 22:41 02/01/18 Silver, Total 6010D 0.04 U mg/Kg 0.39 0.04 1 02/01/18 22:40 02/01/18 Printed 2/5/2018 3:03:09 PM Page 110 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-4-1 J1800711-007 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 14:30 Date Received: 01/27/18 08:50 Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dfl. Date Analyzed Date Extracted Q Arsenic, Total 6010D 2.84 mg/Kg 0.44 0.07 1 02/01/18 22:46 02/01/18 Barium, Total 6010D 30.8 mg/Kg 0.44 0.02 1 02/01/18 22:45 02/01/18 Cadmium, Total 6010D 0.13 I mg/Kg 0.22 0.02 1 02/01/18 22:46 02/01/18 Chromium, Total 6010D 4.57 mg/Kg 0.44 0.04 1 02/01/18 22:46 02/01/18 Lead, Total 6010D 128 mg/Kg 0.44 0.04 1 02/01/18 22:46 02/01/18 Mercury, Total 7471B 1.04 mg/Kg 0.084 0.006 10 01/30/18 14:53 01/29/18 Selenium, Total 6010D 0.35 I mg/Kg 0.44 0.14 1 02/01/18 22:46 02/01/18 Silver, Total 6010D 0.09 IV mg/Kg 0.44 0.04 1 02/01/18 22:45 02/01/18 Printed 2/5/2018 3:03:09 PM Page 111 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-4-21 J1800711-008 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 15:10 Date Received: 01/27/18 08:50 Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Date Extracted Q Arsenic, Total 6010D 7.03 mg/Kg 0.62 0.13 2 02/02/18 16:55 02/01/18 Barium, Total 6010D 40.2 mg/Kg 0.62 0.03 2 02/02/18 16:54 02/01/18 Cadmium, Total 6010D 0.12 1 mg/Kg 0.31 0.03 2 02/02/18 16:55 02/01/18 Chromium, Total 6010D 6.28 mg/Kg 0.62 0.07 2 02/02/18 16:55 02/01/18 Lead, Total 6010D 235 mg/Kg 0.62 0.08 2 02/02/18 16:54 02/01/18 Mercury, Total 7471B 1.73 mg/Kg 0.073 0.005 10 01/30/18 14:55 01/29/18 Selenium, Total 6010D 0.27 U mg/Kg 0.62 0.27 2 02/02/18 16:55 02/01/18 Silver, Total 6010D 0.31 IV mg/Kg 0.62 0.08 2 02/02/18 16:54 02/01/18 Printed 2/5/2018 3:03:09 PM Page 112 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil TW-5-1 J1800711-009 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 13:40 Date Received: 01/27/18 08:50 Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Date Extracted Q Arsenic, Total 6010D 12.1 mg/Kg 1.8 0.4 5 02/02/18 17:00 02/01/18 Barium, Total 6010D 273 mg/Kg 1.8 0.06 5 02/02/18 16:59 02/01/18 Cadmium, Total 6010D 0.54 I mg/Kg 0.91 0.06 5 02/02/18 17:00 02/01/18 Chromium, Total 6010D 11.2 mg/Kg 1.8 0.2 5 02/02/18 17:00 02/01/18 Lead, Total 6010D 1350 mg/Kg 1.8 0.2 5 02/02/18 16:59 02/01/18 Mercury, Total 7471B 0.370 mg/Kg 0.0080 0.0005 1 01/30/18 14:42 01/29/18 Selenium, Total 6010D 2.4 mg/Kg 1.8 0.7 5 02/02/18 17:00 02/01/18 Silver, Total 6010D 0.2 U mg/Kg 1.8 0.2 5 02/02/18 16:59 02/01/18 Printed 2/5/2018 3:03:09 PM Page 113 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil TW-5-25 J1800711-010 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 14:15 Date Received: 01/27/18 08:50 Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dfl. Date Analyzed Date Extracted Q Arsenic, Total 6010D 2.08 mg/Kg 0.36 0.07 1 02/01/18 23:28 02/01/18 Barium, Total 6010D 7.79 mg/Kg 0.36 0.02 1 02/01/18 23:28 02/01/18 Cadmium, Total 6010D 0.04 I mg/Kg 0.18 0.02 1 02/01/18 23:28 02/01/18 Chromium, Total 6010D 3.35 mg/Kg 0.36 0.04 1 02/01/18 23:28 02/01/18 Lead, Total 6010D 6.16 mg/Kg 0.36 0.04 1 02/01/18 23:28 02/01/18 Mercury, Total 7471B 0.0276 mg/Kg 0.0080 0.0005 1 01/30/18 14:44 01/29/18 Selenium, Total 6010D 0.40 mg/Kg 0.36 0.14 1 02/01/18 23:28 02/01/18 Silver, Total 6010D 0.04 U mg/Kg 0.36 0.04 1 02/01/18 23:28 02/01/18 Printed 2/5/2018 3:03:09 PM Page 114 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Water TW-1 J1800711-011 Inorganic Parameters Service Request: J1800711 Date Collected: 01/24/18 11:20 Date Received: 01/27/18 08:50 Basis: NA Analysis Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Date Extracted Q Arsenic, Total 6010D 2 U ug/L 10 2 1 01/30/18 01:37 01/29/18 Barium, Total 6010D 39 ug/L 10 0.3 1 01/30/18 01:37 01/29/18 Cadmium, Total 6010D 0.2 U ug/L 5.0 0.2 1 01/30/18 01:37 01/29/18 Chromium, Total 6010D 2 I ug/L 10 0.4 1 01/30/18 01:37 01/29/18 Lead, Total 6010D 8 I ug/L 10 2 1 01/30/18 01:37 01/29/18 Mercury, Total 7470A 0.05 U ug/L 0.10 0.05 1 01/30/18 14:03 01/29/18 Selenium, Total 6010D 4 I ug/L 10 3 1 01/30/18 01:37 01/29/18 Silver, Total 6010D 1 I ug/L 10 0.6 1 01/30/18 01:36 01/29/18 Printed 2/5/2018 3:03:09 PM Page 115 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Water TW-3 J1800711-012 Inorganic Parameters Service Request: J1800711 Date Collected: 01/24/18 13:10 Date Received: 01/27/18 08:50 Basis: NA Analysis Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Date Extracted Q Arsenic, Total 6010D 19 ug/L 10 2 1 01/30/18 01:42 01/29/18 Barium, Total 6010D 57 ug/L 10 0.3 1 01/30/18 01:42 01/29/18 Cadmium, Total 6010D 0.2 U ug/L 5.0 0.2 1 01/30/18 01:42 01/29/18 Chromium, Total 6010D 56 ug/L 10 0.4 1 01/30/18 01:42 01/29/18 Lead, Total 6010D 39 ug/L 10 2 1 01/30/18 01:42 01/29/18 Mercury, Total 7470A 0.11 ug/L 0.10 0.05 1 01/30/18 14:04 01/29/18 Selenium, Total 6010D 3 U ug/L 10 3 1 01/30/18 01:42 01/29/18 Silver, Total 6010D 0.6 U ug/L 10 0.6 1 01/30/18 01:41 01/29/18 Printed 2/5/2018 3:03:10 PM Page 116 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Water TW-2 J1800711-013 Inorganic Parameters Service Request: J1800711 Date Collected: 01/24/18 15:25 Date Received: 01/27/18 08:50 Basis: NA Analysis Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Date Extracted Q Arsenic, Total 6010D 2 U ug/L 10 2 1 01/30/18 01:46 01/29/18 Barium, Total 6010D 19 ug/L 10 0.3 1 01/30/18 01:46 01/29/18 Cadmium, Total 6010D 0.2 U ug/L 5.0 0.2 1 01/30/18 01:46 01/29/18 Chromium, Total 6010D 1 I ug/L 10 0.4 1 01/30/18 01:46 01/29/18 Lead, Total 6010D 2 U ug/L 10 2 1 01/30/18 01:46 01/29/18 Mercury, Total 7470A 0.05 U ug/L 0.10 0.05 1 01/30/18 14:06 01/29/18 Selenium, Total 6010D 3 U ug/L 10 3 1 01/30/18 01:46 01/29/18 Silver, Total 6010D 0.6 U ug/L 10 0.6 1 01/30/18 01:46 01/29/18 Printed 2/5/2018 3:03:10 PM Page 117 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Water TW-4 J1800711-014 Inorganic Parameters Service Request: J1800711 Date Collected: 01/24/18 16:50 Date Received: 01/27/18 08:50 Basis: NA Analysis Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Date Extracted Q Arsenic, Total 6010D 2 U ug/L 10 2 1 01/30/18 01:51 01/29/18 Barium, Total 6010D 52 ug/L 10 0.3 1 01/30/18 01:51 01/29/18 Cadmium, Total 6010D 0.2 U ug/L 5.0 0.2 1 01/30/18 01:51 01/29/18 Chromium, Total 6010D 0.4 U ug/L 10 0.4 1 01/30/18 01:51 01/29/18 Lead, Total 6010D 2 U ug/L 10 2 1 01/30/18 01:51 01/29/18 Mercury, Total 7470A 0.05 U ug/L 0.10 0.05 1 01/30/18 14:07 01/29/18 Selenium, Total 6010D 8 I ug/L 10 3 1 01/30/18 01:51 01/29/18 Silver, Total 6010D 0.6 U ug/L 10 0.6 1 01/30/18 01:51 01/29/18 Printed 2/5/2018 3:03:10 PM Page 118 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Water TW-5 J1800711-015 Inorganic Parameters Service Request: J1800711 Date Collected: 01/24/18 17:20 Date Received: 01/27/18 08:50 Basis: NA Analysis Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Date Extracted Q Arsenic, Total 6010D 2 U ug/L 10 2 1 01/30/18 01:56 01/29/18 Barium, Total 6010D 54 ug/L 10 0.3 1 01/30/18 01:56 01/29/18 Cadmium, Total 6010D 0.2 U ug/L 5.0 0.2 1 01/30/18 01:56 01/29/18 Chromium, Total 6010D 3 I ug/L 10 0.4 1 01/30/18 01:56 01/29/18 Lead, Total 6010D 6 I ug/L 10 2 1 01/30/18 01:56 01/29/18 Mercury, Total 7470A 0.12 ug/L 0.10 0.05 1 01/30/18 14:09 01/29/18 Selenium, Total 6010D 4 1 ug/L 10 3 1 01/30/18 01:56 01/29/18 Silver, Total 6010D 0.6 U ug/L 10 0.6 1 01/30/18 01:56 01/29/18 Printed 2/5/2018 3:03:10 PM Page 119 of 184 Superset Reference:18-0000453045 rev 00 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 120 of 184 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-1-1 J1800711-001 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 08:50 Date Received: 01/27/18 08:50 Basis: As Received Analyte Name Analysis Method Result Units PQL MDL Dil. Date Analyzed Q Solids, Total 160.3 Modified 90.9 Percent - - 1 01/29/18 12:26 Printed 2/5/2018 3:03:12 PM Page 121 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-1-17 J1800711-002 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 09:30 Date Received: 01/27/18 08:50 Basis: As Received Analyte Name Analysis Method Result Units PQL MDL Dil. Date Analyzed Q Solids, Total 160.3 Modified 95.4 Percent - - 1 01/29/18 12:26 Printed 2/5/2018 3:03:12 PM Page 122 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-2-1 J1800711-003 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 12:00 Date Received: 01/27/18 08:50 Basis: As Received Analyte Name Analysis Method Result Units PQL MDL Dil. Date Analyzed Q Solids, Total 160.3 Modified 97.9 Percent - - 1 01/29/18 12:26 Printed 2/5/2018 3:03:12 PM Page 123 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-2-12 J1800711-004 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 12:10 Date Received: 01/27/18 08:50 Basis: As Received Analyte Name Analysis Method Result Units PQL MDL Dil. Date Analyzed Q Solids, Total 160.3 Modified 92.8 Percent - - 1 01/29/18 12:26 Printed 2/5/2018 3:03:12 PM Page 124 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-3-1 J1800711-005 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 12:25 Date Received: 01/27/18 08:50 Basis: As Received Analyte Name Analysis Method Result Units PQL MDL Dil. Date Analyzed Q Solids, Total 160.3 Modified 85.2 Percent - - 1 01/29/18 12:26 Printed 2/5/2018 3:03:12 PM Page 125 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-3-14 J1800711-006 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 13:00 Date Received: 01/27/18 08:50 Basis: As Received Analyte Name Analysis Method Result Units PQL MDL Dil. Date Analyzed Q Solids, Total 160.3 Modified 94.1 Percent - - 1 01/29/18 12:26 Printed 2/5/2018 3:03:12 PM Page 126 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-4-1 J1800711-007 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 14:30 Date Received: 01/27/18 08:50 Basis: As Received Analyte Name Analysis Method Result Units PQL MDL Dil. Date Analyzed Q Solids, Total 160.3 Modified 76.4 Percent - - 1 01/29/18 12:26 Printed 2/5/2018 3:03:12 PM Page 127 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil SB-4-21 J1800711-008 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 15:10 Date Received: 01/27/18 08:50 Basis: As Received Analyte Name Analysis Method Result Units PQL MDL Dil. Date Analyzed Q Solids, Total 160.3 Modified 92.1 Percent - - 1 01/29/18 12:26 Printed 2/5/2018 3:03:13 PM Page 128 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil TW-5-1 J1800711-009 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 13:40 Date Received: 01/27/18 08:50 Basis: As Received Analyte Name Analysis Method Result Units PQL MDL Dil. Date Analyzed Q Solids, Total 160.3 Modified 83.8 Percent - - 1 01/29/18 12:26 Printed 2/5/2018 3:03:13 PM Page 129 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil TW-5-25 J1800711-010 Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 14:15 Date Received: 01/27/18 08:50 Basis: As Received Analyte Name Analysis Method Result Units PQL MDL Dil. Date Analyzed Q Solids, Total 160.3 Modified 80.8 Percent - - 1 01/29/18 12:26 Printed 2/5/2018 3:03:13 PM Page 130 of 184 Superset Reference:18-0000453045 rev 00 ALS Environmental ALS Environmental -Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904) 739-2277 Fax (904) 739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 131 of 184 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 132 of 184 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Matrix: Soil SURROGATE RECOVERY SUMMARY Volatile Organic Compounds by GC/MS Analysis Method: 8260B Extraction Method: EPA 5035 Sample Name SB-1-1 SB-1-17 SB-2-1 SB-2-12 SB-3-1 SB-3-14 SB-4-1 SB-4-21 TW-5-1 TW-5-25 Lab Control Sample Method Blank Lab Code J1800711-001 J1800711-002 J1800711-003 J1800711-004 J1800711-005 J1800711-006 J1800711-007 J1800711-008 J1800711-009 J1800711-010 JQ1800803-01 JQ1800803-02 1,2-Dichloroethane-d4 74 -120 98 108 98 103 117 106 99 110 96 108 105 107 Service Request: J1800711 4-Bromofluorobenzene 77 -130 102 96 105 86 75 * 114 126 80 90 76 95 104 Dibromotluoromethane 85 -117 112 98 115 111 117 112 113 114 116 105 106 99 Printed 2/5/2018 3:02:17 PM Page 133 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Matrix: Soil SURROGATE RECOVERY SUMMARY Volatile Organic Compounds by GC/MS Analysis Method: 8260B Extraction Method: EPA 5035 Service Request: J1800711 Toluene-d8 Sample Name Lab Code 81-126 SB-1-1 J1800711-001 96 SB-1-17 J1800711-002 94 SB-2-1 J1800711-003 99 SB-2-12 J1800711-004 99 SB-3-1 J1800711-005 111 SB-3-14 J1800711-006 80 * SB-4-1 J1800711-007 106 SB-4-21 J1800711-008 145 TW-5-1 J1800711-009 97 TW-5-25 J1800711-010 96 Lab Control Sample JQ1800803-01 91 Method Blank JQ1800803-02 84 Printed 2/5/2018 3:02:17 PM Page 134 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Sample Matrix: Water SURROGATE RECOVERY SUMMARY Volatile Organic Compounds by GC/MS Analysis Method: 8260B Sample Name TW-1 TW-3 TW-2 TW-4 TW-5 Lab Control Sample Duplicate Lab Control Sample Method Blank Lab Code J1800711-011 J1800711-012 J1800711-013 J1800711-014 J1800711-015 JQ1800782-03 JQ1800782-04 JQ1800782-05 1,2-Dichloroethane-d4 74 -120 100 103 103 107 110 88 91 99 4-Bromofluorobenzene 77 -130 93 97 99 99 96 97 97 100 Dibromotluoromethane 85 -117 102 103 104 107 108 94 98 102 Printed 2/5/2018 3:02:17 PM Page 135 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Matrix: Water SURROGATE RECOVERY SUMMARY Volatile Organic Compounds by GC/MS Service Request: J1800711 Analysis Method: 8260B Toluene-d8 Sample Name Lab Code 81-126 TW-1 J1800711-011 98 TW-3 J1800711-012 96 TW-2 J1800711-013 96 TW-4 J1800711-014 95 TW-5 J1800711-015 94 Lab Control Sample JQ1800782-03 101 Duplicate Lab Control Sample JQ1800782-04 104 Method Blank JQ1800782-05 98 Printed 2/5/2018 3:02:17 PM Page 136 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Water Date Received: NA Sample Name: Method Blank Units: ug/L Lab Code: JQ1800782-05 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q 1, 1, 1,2-Tetrachloroethane 0.19 U 1.0 0.19 1 01/31/18 13:21 1, 1, 1 -Trichloroethane (TCA) 0.17 U 1.0 0.17 1 01/31/18 13:21 1,1,2,2-Tetrachloroethane 0.29 U 1.0 0.29 1 01/31/18 13:21 1,1,2-Trichloroethane 0.40 U 1.0 0.40 1 01/31/18 13:21 1, 1 -Dichloroethane (1,1-DCA) 0.30 U 1.0 0.30 1 01/31/18 13:21 1, 1 -Dichloroethene (1,1-DCE) 0.16 U 1.0 0.16 1 01/31/18 13:21 1,2,3-Trichloropropane 0.42 U 2.0 0.42 1 01/31/18 13:21 1,2-Dibromo-3-chloropropane (DBCP) 2.3 U 5.0 2.3 1 01/31/18 13:21 1,2-Dibromoethane (EDB) 0.46 U 1.0 0.46 1 01/31/18 13:21 1,2-Dichlorobenzene 0.48 U 1.0 0.48 1 01/31/18 13:21 1,2-Dichloroethane 0.22 U 1.0 0.22 1 01/31/18 13:21 1,2-Dichloropropane 0.19 U 1.0 0.19 1 01/31/18 13:21 1,3-Dichlorobenzene 0.22 U 1.0 0.22 1 01/31/18 13:21 1,4-Dichlorobenzene 0.16 U 1.0 0.16 1 01/31/18 13:21 2-Butanone (MEK) 3.8 U 10 3.8 1 01/31/18 13:21 2-Hexanone 2.2 U 25 2.2 1 01/31/18 13:21 4-Methyl-2-pentanone (MIBK) 1.1 U 25 1.1 1 01/31/18 13:21 Acetone 5.6 U 20 5.6 1 01/31/18 13:21 Benzene 0.21 U 1.0 0.21 1 01/31/18 13:21 Bromochloromethane 0.27 U 5.0 0.27 1 01/31/18 13:21 Bromodichloromethane 0.22 U 1.0 0.22 1 01/31/18 13:21 Bromoform 0.42 U 2.0 0.42 1 01/31/18 13:21 Bromomethane 0.23 U 5.0 0.23 1 01/31/18 13:21 Carbon Disulfide 2.4 U 10 2.4 1 01/31/18 13:21 Carbon Tetrachloride 0.34 U 1.0 0.34 1 01/31/18 13:21 Chlorobenzene 0.16 U 1.0 0.16 1 01/31/18 13:21 Chloroethane 0.52 U 5.0 0.52 1 01/31/18 13:21 Chloroform 0.35 U 1.0 0.35 1 01/31/18 13:21 Chloromethane 0.36 U 1.0 0.36 1 01/31/18 13:21 cis-1,2-Dichloroethene 0.36 U 1.0 0.36 1 01/31/18 13:21 cis-1,3-Dichloropropene 0.20 U 1.0 0.20 1 01/31/18 13:21 Dibromochloromethane 0.21 U 1.0 0.21 1 01/31/18 13:21 Dibromomethane 0.36 U 5.0 0.36 1 01/31/18 13:21 Dichlorodifluoromethane 0.23 U 20 0.23 1 01/31/18 13:21 Ethylbenzene 0.21 U 1.0 0.21 1 01/31/18 13:21 Iodomethane 2.7 U 5.0 2.7 1 01/31/18 13:21 m,p-Xylenes 0.31 U 2.0 0.31 1 01/31/18 13:21 Methyl tert-Butyl Ether 0.24 U 2.0 0.24 1 01/31/18 13:21 Methylene Chloride 0.21 U 5.0 0.21 1 01/31/18 13:21 o-Xylene 0.14 U 1.0 0.14 1 01/31/18 13:21 Styrene 0.29 U 1.0 0.29 1 01/31/18 13:21 Tetrachloroethene (PCE) 0.22 U 1.0 0.22 1 01/31/18 13:21 Toluene 0.19 U 1.0 0.19 1 01/31/18 13:21 Printed 2/5/2018 3:02:15 PM Page 137 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Water Date Received: NA Sample Name: Method Blank Units: ug/L Lab Code: JQ1800782-05 Basis: NA Volatile Organic Compounds by GC/MS Analysis Method: 8260B Analyte Name Result PQL MDL Dil. Date Analyzed Q trans-1,2-Dichloroethene 0.19 U 1.0 0.19 1 01/31/18 13:21 trans- l,3-Dichloropropene 0.23 U 1.0 0.23 1 01/31/18 13:21 trans-1,4-Dichloro-2-butene 2.2 U 20 2.2 1 01/31/18 13:21 Trichloroethene (TCE) 0.36 U 1.0 0.36 1 01/31/18 13:21 Trichlorofluoromethane 0.24 U 20 0.24 1 01/31/18 13:21 Vinyl Acetate 1.9 U 10 1.9 1 01/31/18 13:21 Vinyl Chloride 0.36 U 1.0 0.36 1 01/31/18 13:21 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 99 72 - 127 01/31/18 13:21 4-Bromofluorobenzene 100 88 - 120 01/31/18 13:21 Dibromofluoromethane 102 85 - 115 01/31/18 13:21 Toluene-d8 98 83 - 123 01/31/18 13:21 Printed 2/5/2018 3:02:15 PM Page 138 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Soil Date Received: NA Sample Name: Method Blank Units: ug/Kg Lab Code: JQ1800803-02 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1, 1, 1,2-Tetrachloroethane 0.410 U 5.00 0.410 1 01/31/18 14:16 1/31/18 1, 1, 1 -Trichloroethane (TCA) 0.230 U 5.00 0.230 1 01/31/18 14:16 1/31/18 1,1,2,2-Tetrachloroethane 0.230 U 5.00 0.230 1 01/31/18 14:16 1/31/18 1,1,2-Trichloroethane 0.390 U 5.00 0.390 1 01/31/18 14:16 1/31/18 1, 1 -Dichloroethane (1,1-DCA) 0.310 U 5.00 0.310 1 01/31/18 14:16 1/31/18 1, 1 -Dichloroethene (1,1-DCE) 0.690 U 5.00 0.690 1 01/31/18 14:16 1/31/18 1,2,3-Trichloropropane 0.760 U 5.00 0.760 1 01/31/18 14:16 1/31/18 1,2-Dibromo-3-chloropropane (DBCP) 0.530 U 10.0 0.530 1 01/31/18 14:16 1/31/18 1,2-Dibromoethane (EDB) 0.580 U 5.00 0.580 1 01/31/18 14:16 1/31/18 1,2-Dichlorobenzene 0.320 U 5.00 0.320 1 01/31/18 14:16 1/31/18 1,2-Dichloroethane 0.300 U 5.00 0.300 1 01/31/18 14:16 1/31/18 1,2-Dichloropropane 0.410 U 5.00 0.410 1 01/31/18 14:16 1/31/18 1,3-Dichlorobenzene 0.300 U 5.00 0.300 1 01/31/18 14:16 1/31/18 1,4-Dichlorobenzene 0.100 U 5.00 0.100 1 01/31/18 14:16 1/31/18 2-Butanone (MEK) 1.60 U 25.0 1.60 1 01/31/18 14:16 1/31/18 2-Hexanone 2.20 U 10.0 2.20 1 01/31/18 14:16 1/31/18 4-Methyl-2-pentanone (MIBK) 1.50 U 10.0 1.50 1 01/31/18 14:16 1/31/18 Acetone 2.30 U 20.0 2.30 1 01/31/18 14:16 1/31/18 Benzene 0.170 U 5.00 0.170 1 01/31/18 14:16 1/31/18 Bromochloromethane 0.600 U 5.00 0.600 1 01/31/18 14:16 1/31/18 Bromodichloromethane 0.370 U 5.00 0.370 1 01/31/18 14:16 1/31/18 Bromoform 0.340 U 5.00 0.340 1 01/31/18 14:16 1/31/18 Bromomethane 0.270 U 5.00 0.270 1 01/31/18 14:16 1/31/18 Carbon Disulfide 0.800 U 10.0 0.800 1 01/31/18 14:16 1/31/18 Carbon Tetrachloride 0.190 U 5.00 0.190 1 01/31/18 14:16 1/31/18 Chlorobenzene 0.140 U 5.00 0.140 1 01/31/18 14:16 1/31/18 Chloroethane 0.330 U 5.00 0.330 1 01/31/18 14:16 1/31/18 Chloroform 0.180 U 5.00 0.180 1 01/31/18 14:16 1/31/18 Chloromethane 0.210 U 5.00 0.210 1 01/31/18 14:16 1/31/18 cis-1,2-Dichloroethene 0.330 U 5.00 0.330 1 01/31/18 14:16 1/31/18 cis-1,3-Dichloropropene 0.140 U 5.00 0.140 1 01/31/18 14:16 1/31/18 Dibromochloromethane 0.220 U 5.00 0.220 1 01/31/18 14:16 1/31/18 Dibromomethane 0.390 U 5.00 0.390 1 01/31/18 14:16 1/31/18 Dichlorodifluoromethane 0.180 U 20.0 0.180 1 01/31/18 14:16 1/31/18 Ethylbenzene 0.120 U 5.00 0.120 1 01/31/18 14:16 1/31/18 Iodomethane 1.10 U 10.0 1.10 1 01/31/18 14:16 1/31/18 m,p-Xylenes 0.210 U 10.0 0.210 1 01/31/18 14:16 1/31/18 Methyl tert-Butyl Ether 0.260 U 5.00 0.260 1 01/31/18 14:16 1/31/18 Methylene Chloride 0.310 U 10.0 0.310 1 01/31/18 14:16 1/31/18 o-Xylene 0.160 U 5.00 0.160 1 01/31/18 14:16 1/31/18 Styrene 0.270 U 5.00 0.270 1 01/31/18 14:16 1/31/18 Tetrachloroethene (PCE) 0.250 U 5.00 0.250 1 01/31/18 14:16 1/31/18 Toluene 0.270 U 5.00 0.270 1 01/31/18 14:16 1/31/18 Printed 2/5/2018 3:02:16 PM Page 139 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Soil Date Received: NA Sample Name: Method Blank Units: ug/Kg Lab Code: JQ1800803-02 Basis: Dry Volatile Organic Compounds by GC/MS Analysis Method: 8260B Prep Method: EPA 5035 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q trans-1,2-Dichloroethene 0.390 U 5.00 0.390 1 01/31/18 14:16 1/31/18 trans- l,3-Dichloropropene 0.220 U 5.00 0.220 1 01/31/18 14:16 1/31/18 trans-1,4-Dichloro-2-butene 0.540 U 20.0 0.540 1 01/31/18 14:16 1/31/18 Trichloroethene (TCE) 0.250 U 5.00 0.250 1 01/31/18 14:16 1/31/18 Trichlorofluoromethane 0.210 U 20.0 0.210 1 01/31/18 14:16 1/31/18 Vinyl Acetate 1.20 U 10.0 1.20 1 01/31/18 14:16 1/31/18 Vinyl Chloride 0.260 U 5.00 0.260 1 01/31/18 14:16 1/31/18 Surrogate Name % Rec Control Limits Date Analyzed Q 1,2-Dichloroethane-d4 107 74 - 120 01/31/18 14:16 4-Bromofluorobenzene 104 77 - 130 01/31/18 14:16 Dibromofluoromethane 99 85 - 117 01/31/18 14:16 Toluene-d8 84 81 - 126 01/31/18 14:16 Printed 2/5/2018 3:02:16 PM Page 140 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Project: Sample Matrix: Analysis Method: Prep Method: Terracon Environmental WWAY Building/ES187011 Soil 8260B EPA 5035 Lab Control Sample Summary Volatile Organic Compounds by GC/MS Service Request: Date Analyzed: Date Extracted: Units: Basis: Analysis Lot: Lab Control Sample JQ1800803-01 J1800711 01/31/18 01/31/18 ug/Kg Dry 578990 Analyte Name Result Spike Amount % Rec % Rec Limits 1, 1, 1,2-Tetrachloroethane 52.9 52.0 102 76-124 1,1,1-Trichloroethane (TCA) 56.1 52.0 108 65-140 1,1,2,2-Tetrachloroethane 58.8 52.0 113 79-120 1,1,2-Trichloroethane 54.3 52.0 104 78-120 1, 1 -Dichloroethane (1,1-DCA) 62.4 52.0 120 71-126 1, 1 -Dichloroethene (1,1-DCE) 71.8 52.0 138 65-140 1,2,3-Trichloropropane 58.8 52.0 113 80-120 1,2-Dibromo-3-chloropropane (DBCP) 50.9 52.0 98 80-130 1,2-Dibromoethane (EDB) 43.5 52.0 84 80-120 1,2-Dichlorobenzene 55.3 52.0 106 80-120 1,2-Dichloroethane 49.4 52.0 95 73-133 1,2-Dichloropropane 50.0 52.0 96 73-121 1,3-Dichlorobenzene 59.0 52.0 113 77-121 1,4-Dichlorobenzene 57.3 52.0 110 75-120 2-Butanone (MEK) 61.2 52.0 118 60-138 2-Hexanone 51.4 52.0 99 72-126 4-Methyl-2-pentanone (MIBK) 53.5 52.0 103 78-127 Acetone 69.0 52.0 133 49-150 Benzene 56.6 52.0 109 71-125 Bromochloromethane 56.4 52.0 108 76-120 Bromodichloromethane 49.1 52.0 94 76-131 Bromoform 58.8 52.0 113 76-129 Bromomethane 93.9 52.0 181 * 35-150 Carbon Disulfide 61.5 52.0 118 56-129 Carbon Tetrachloride 55.8 52.0 107 67-143 Chlorobenzene 57.8 52.0 111 73-123 Chloroethane 80.4 52.0 155 * 52-150 Chloroform 55.0 52.0 106 73-129 Chloromethane 55.2 52.0 106 50-136 cis-1,2-Dichloroethene 56.7 52.0 109 74-131 cis-1,3-Dichloropropene 47.8 52.0 92 76-120 Dibromochloromethane 46.8 52.0 90 80-120 Dibromomethane 55.6 52.0 107 77-122 Dichlorodifluoromethane 51.9 52.0 100 45-150 Ethylbenzene 56.8 52.0 109 70-128 Iodomethane 50.0 52.0 96 30-150 m,p-Xylenes 117 104 112 72-124 Methyl tert-Butyl Ether 54.0 52.0 104 60-125 Methylene Chloride 61.6 52.0 118 61-135 o-Xylene 55.8 52.0 107 73-125 Styrene 60.3 52.0 116 76-124 Printed 2/5/2018 3:02:15 PM Superset Reference:18-0000453045 rev 00 Page 141 of 184 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Analyzed: 01/31/18 Sample Matrix: Soil Date Extracted: 01/31/18 Lab Control Sample Summary Volatile Organic Compounds by GC/MS Analysis Method: 8260B Units: ug/Kg Prep Method: EPA 5035 Basis: Dry Analysis Lot: 578990 Lab Control Sample JQ1800803-01 Analyte Name Result Spike Amount % Rec % Rec Limits Tetrachloroethene (PCE) 52.8 52.0 102 67-130 Toluene 55.0 52.0 106 70-126 trans-1,2-Dichloroethene 63.8 52.0 123 70-135 trans-1,3-Dichloropropene 46.1 52.0 89 80-125 trans-1,4-Dichloro-2-butene 61.3 52.0 118 56-147 Trichloroethene (TCE) 59.2 52.0 114 70-132 Trichlorofluoromethane 85.5 52.0 164 * 62-150 Vinyl Acetate 49.0 52.0 94 64-136 Vinyl Chloride 62.4 52.0 120 60-144 Printed 2/5/2018 3:02:15 PM Page 142 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Analyzed: 01/31/18 Sample Matrix: Water Duplicate Lab Control Sample Summary Volatile Organic Compounds by GC/MS Analysis Method: 8260B Units: ug/L Basis: NA Analysis Lot: 578809 Lab Control Sample Duplicate Lab Control Sample JQ1800782-03 JQ1800782-04 Spike Spike % Rec RPD Analyte Name Result Amount % Rec Result Amount % Rec Limits RPD Limit 1, 1, 1,2-Tetrachloroethane 55.8 52.0 107 55.4 52.0 106 80-125 <1 30 1,1,1-Trichloroethane (TCA) 49.0 52.0 94 47.9 52.0 92 73-128 2 30 1,1,2,2-Tetrachloroethane 51.8 52.0 100 54.2 52.0 104 70-129 5 30 1,1,2-Trichloroethane 54.3 52.0 104 56.9 52.0 109 79-120 5 30 1, 1 -Dichloroethane (1,1-DCA) 50.4 52.0 97 51.0 52.0 98 80-122 1 30 1, 1 -Dichloroethene (1,1-DCE) 52.6 52.0 101 50.8 52.0 98 71-131 3 30 1,2,3-Trichloropropane 49.7 52.0 96 53.3 52.0 103 72-130 7 30 1,2-Dibromo-3-chloropropane (DBCP) 48.7 52.0 94 51.8 52.0 100 72-130 6 30 1,2-Dibromoethane (EDB) 51.9 52.0 100 54.4 52.0 105 79-122 5 30 1,2-Dichlorobenzene 54.5 52.0 105 53.4 52.0 103 80-120 2 30 1,2-Dichloroethane 45.5 52.0 88 44.4 52.0 85 75-123 2 30 1,2-Dichloropropane 53.4 52.0 103 51.9 52.0 100 76-120 3 30 1,3-Dichlorobenzene 53.4 52.0 103 51.0 52.0 98 80-120 4 30 1,4-Dichlorobenzene 54.8 52.0 105 53.3 52.0 103 80-120 3 30 2-Butanone (MEK) 47.1 52.0 91 52.0 52.0 100 56-147 10 30 2-Hexanone 48.4 52.0 93 52.3 52.0 101 60-146 8 30 4-Methyl-2-pentanone (MIBK) 50.1 52.0 96 54.0 52.0 104 67-140 7 30 Acetone 43.9 52.0 84 46.8 52.0 90 60-145 6 30 Benzene 54.7 52.0 105 54.3 52.0 104 77-124 <1 30 Bromochloromethane 52.2 52.0 100 50.9 52.0 98 74-124 3 30 Bromodichloromethane 51.3 52.0 99 49.5 52.0 95 80-127 4 30 Bromoform 53.1 52.0 102 55.8 52.0 107 70-128 5 30 Bromomethane 46.5 52.0 89 49.2 52.0 95 31-150 6 30 Carbon Disulfide 53.8 52.0 104 51.9 52.0 100 55-140 4 30 Carbon Tetrachloride 49.5 52.0 95 49.3 52.0 95 70-126 <1 30 Chlorobenzene 56.1 52.0 108 54.1 52.0 104 75-123 4 30 Chloroethane 61.4 52.0 118 57.1 52.0 110 60-150 7 30 Chloroform 48.4 52.0 93 49.2 52.0 95 80-121 2 30 Chloromethane 45.1 52.0 87 43.0 52.0 83 47-134 5 30 cis-1,2-Dichloroethene 53.4 52.0 103 52.4 52.0 101 79-120 2 30 cis-1,3-Dichloropropene 56.1 52.0 108 53.5 52.0 103 78-120 5 30 Dibromochloromethane 52.9 52.0 102 52.7 52.0 101 80-122 <1 30 Dibromomethane 49.9 52.0 96 48.6 52.0 93 80-120 3 30 Dichlorodifluoromethane 39.4 52.0 76 38.0 52.0 73 50-145 4 30 Ethylbenzene 56.5 52.0 109 55.0 52.0 106 70-130 3 30 Iodomethane 54.6 52.0 105 51.5 52.0 99 30-130 6 30 m,p-Xylenes 116 104 ill 112 104 107 73-126 4 30 Methyl tert-Butyl Ether 49.1 52.0 94 50.5 52.0 97 79-124 3 30 Methylene Chloride 52.9 52.0 102 52.9 52.0 102 73-120 <1 30 o-Xylene 56.8 52.0 109 55.6 52.0 107 77-120 2 30 Styrene 58.1 52.0 112 56.9 52.0 109 80-120 2 30 Printed 2/5/2018 3:02:15 PM Superset Reference:18-0000453045 rev 00 Page 143 of 184 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Analyzed: 01/31/18 Sample Matrix: Water Duplicate Lab Control Sample Summary Volatile Organic Compounds by GC/MS Analysis Method: 8260B Units: ug/L Basis: NA Analysis Lot: 578809 Lab Control Sample Duplicate Lab Control Sample JQ1800782-03 JQ1800782-04 Spike Spike % Rec RPD Analyte Name Result Amount % Rec Result Amount % Rec Limits RPD Limit Tetrachloroethene (PCE) 57.0 52.0 110 55.9 52.0 107 69-128 2 30 Toluene 57.2 52.0 110 55.0 52.0 106 74-124 4 30 trans-1,2-Dichloroethene 53.0 52.0 102 50.8 52.0 98 79-120 4 30 trans- l,3-Dichloropropene 55.5 52.0 107 54.7 52.0 105 80-121 1 30 trans-1,4-Dichloro-2-butene 52.8 52.0 102 57.4 52.0 110 61-132 8 30 Trichloroethene (TCE) 52.6 52.0 101 52.5 52.0 101 76-120 <1 30 Trichlorofluoromethane 47.8 52.0 92 46.4 52.0 89 60-145 3 30 Vinyl Acetate 40.9 52.0 79 43.2 52.0 83 59-133 6 30 Vinyl Chloride 52.3 52.0 101 50.8 52.0 98 60-138 3 30 Printed 2/5/2018 3:02:15 PM Page 144 of 184 Superset Reference:18-0000453045 rev 00 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 145 of 184 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Sample Matrix: Soil SURROGATE RECOVERY SUMMARY Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Extraction Method: EPA 3546 2,4,6-Tribromophenol 2-Fluorobiphenyl 2-Fluorophenol Sample Name Lab Code 30 -136 20 -115 10 -110 SB-1-1 J1800711-001 45 57 39 SB-1-17 J1800711-002 39 65 50 SB-2-1 J1800711-003 51 58 55 SB-2-12 J1800711-004 40 70 63 SB-3-1 J1800711-005 34 61 43 SB-3-14 J1800711-006 43 60 55 SB-4-1 J1800711-007 52 61 61 SB-4-21 J1800711-008 41 67 56 TW-5-1 J1800711-009 54 69 57 TW-5-25 J1800711-010 36 45 44 Method Blank JQ1800727-01 47 55 53 Lab Control Sample JQ1800727-02 71 73 71 SB-1-17 JQ1800727-03 44 69 54 SB-1-17 JQ1800727-04 50 70 64 Printed 2/5/2018 3:02:54 PM Page 146 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Sample Matrix: Soil SURROGATE RECOVERY SUMMARY Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Extraction Method: EPA 3546 Nitrobenzene-d5 Phenol-d6 p-Terphenyl-04 Sample Name Lab Code 20 -110 14 -100 32 -119 SB-1-1 J1800711-001 56 45 69 SB-1-17 J1800711-002 58 51 79 SB-2-1 J1800711-003 60 61 83 SB-2-12 J1800711-004 64 65 83 SB-3-1 J1800711-005 55 45 68 SB-3-14 J1800711-006 64 57 63 SB-4-1 J1800711-007 68 62 45 SB-4-21 J1800711-008 59 58 75 TW-5-1 J1800711-009 60 60 92 TW-5-25 J1800711-010 42 41 44 Method Blank JQ1800727-01 55 57 73 Lab Control Sample JQ1800727-02 79 78 84 SB-1-17 JQ1800727-03 70 63 74 SB-1-17 JQ1800727-04 73 67 71 Printed 2/5/2018 3:02:54 PM Page 147 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Sample Matrix: Water SURROGATE RECOVERY SUMMARY Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Extraction Method: EPA 3510C 2,4,6-Tribromophenol 2-Fluorobiphenyl 2-Fluorophenol Sample Name Lab Code 30 -136 20 -115 10 -110 TW-1 J1800711-011 61 55 50 TW-3 J1800711-012 72 53 37 TW-2 J1800711-013 63 68 51 TW-4 J1800711-014 56 59 46 TW-5 J1800711-015 56 49 42 Method Blank JQ1800698-01 71 73 67 Lab Control Sample JQ1800698-02 64 43 3 * TW-1 JQ 1800698-03 66 54 49 TW-1 JQ 1800698-04 65 51 48 Method Blank JQ1800741-01 60 64 53 Lab Control Sample JQ1800741-02 67 61 48 Duplicate Lab Control Sample JQ1800741-03 72 70 55 Printed 2/5/2018 3:02:54 PM Page 148 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Sample Matrix: Water SURROGATE RECOVERY SUMMARY Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Extraction Method: EPA 3510C Nitrobenzene-d5 Phenol-d6 p-Terphenyl-04 Sample Name Lab Code 20 -110 14 -100 32 -119 TW-1 J1800711-011 57 42 89 TW-3 J1800711-012 48 29 73 TW-2 J1800711-013 70 40 86 TW-4 J1800711-014 62 35 79 TW-5 J1800711-015 49 39 74 Method Blank JQ1800698-01 77 60 91 Lab Control Sample JQ1800698-02 17 17 87 TW-1 JQ 1800698-03 55 52 81 TW-1 JQ1800698-04 54 53 78 Method Blank JQ1800741-01 69 43 87 Lab Control Sample JQ1800741-02 64 40 82 Duplicate Lab Control Sample JQ1800741-03 73 45 87 Printed 2/5/2018 3:02:54 PM Page 149 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba AILS Environmental Client: Project: Sample Matrix: Sample Name: Lab Code: Analysis Method: Prep Method: QA/QC Report Terracon Environmental WWAY Building/ES187011 Water Service Request: J1800711 Date Collected: 01/24/18 Date Received: 01/27/18 Date Analyzed: 01/29/18 Date Extracted: 01/29/18 Duplicate Matrix Spike Summary Semivolatile Organic Compounds by GC/MS TW-1 Units: ug/L J1800711-011 Basis: NA 8270C EPA 3510C Matrix Spike Duplicate Matrix Spike JQ1800698-03 JQ1800698-04 Sample Spike Spike % Rec RPD Analyte Name Result Result Amount % Rec Result Amount % Rec Limits RPD Limit 1,2,4-Trichlorobenzene 1.16 U 41.5 76.9 54 41.5 76.9 54 30-110 <1 30 1,2-Dichlorobenzene 1.24 U 40.7 76.9 53 41.0 76.9 53 30-110 <1 30 1,3-Dichlorobenzene 1.77 U 39.4 76.9 51 40.0 76.9 52 25-110 1 30 1,4-Dichlorobenzene 1.75 U 40.7 76.9 53 40.9 76.9 53 21-110 <1 30 1-Methylnaphthalene 1.41 U 44.8 76.9 58 44.4 76.9 58 34-113 <1 30 2,4,5-Trichlorophenol 2.50 U 49.0 76.9 64 48.2 76.9 63 43-116 2 30 2,4,6-Trichlorophenol 1.72 U 46.1 76.9 60 44.6 76.9 58 34-119 3 30 2,4-Dichlorophenol 2.31 U 44.6 76.9 58 42.7 76.9 55 32-115 4 30 2,4-Dimethylphenol 2.89 U 43.8 76.9 57 43.8 76.9 57 31-111 <1 30 2,4-Dinitrophenol 1.47 U 50.5 76.9 66 51.5 76.9 67 22-113 2 30 2,4-Dinitrotoluene 2.50 U 55.1 76.9 72 55.7 76.9 72 49-117 1 30 2,6-Dinitrotoluene 2.12 U 52.1 76.9 68 51.7 76.9 67 47-120 <1 30 2-Chloronaphthalene 8.85 U 42.4 76.9 55 41.7 76.9 54 30-115 2 30 2-Chlorophenol 2.31 U 40.8 76.9 53 41.1 76.9 53 25-110 <1 30 2-Methylnaphthalene 1.22 U 44.8 76.9 58 44.2 76.9 57 29-110 1 30 2-Methylphenol 2.50 U 42.9 76.9 56 41.9 76.9 54 29-112 2 30 2-Nitroaniline 2.89 U 54.2 76.9 70 54.8 76.9 71 38-145 1 30 2-Nitrophenol 2.70 U 44.1 76.9 57 44.1 76.9 57 24-119 <1 30 3- and 4-Methylphenol Coelution 1.93 U 43.5 76.9 57 42.6 76.9 55 29-110 2 30 3,3'-Dichlorobenzidine 2.70 U 69.3 76.9 90 67.5 76.9 88 43-150 3 30 3-Nitroaniline 2.12 U 56.8 76.9 74 56.1 76.9 73 55-128 1 30 4,6-Dinitro-2-methylphenol 1.93 U 57.3 76.9 74 58.3 76.9 76 26-115 2 30 4-Bromophenyl Phenyl Ether 2.50 U 50.8 76.9 66 49.5 76.9 64 49-115 3 30 4-Chloro-3-methylphenol 3.47 U 49.9 76.9 65 50.2 76.9 65 45-113 <1 30 4-Chloroaniline 2.70 U 48.4 76.9 63 47.5 76.9 62 33-122 2 30 4-Chlorophenyl Phenyl Ether 1.85 U 46.0 76.9 60 45.3 76.9 59 42-115 2 30 4-Nitroaniline 1.93 U 60.2 76.9 78 59.5 76.9 77 52-128 1 30 4-Nitrophenol 3.47 U 51.3 76.9 67 52.9 76.9 69 15-85 3 30 Acenaphthene 8.08 U 46.3 76.9 60 45.0 76.9 58 32-112 3 30 Acenaphthylene 1.91 U 46.3 76.9 60 44.8 76.9 58 33-115 3 30 Acetophenone 3.08 U 44.3 76.9 58 43.8 76.9 57 30-115 1 30 Anthracene 3.08 U 57.9 76.9 75 57.3 76.9 74 54-114 1 30 Benz(a)anthracene 1.93 U 63.4 76.9 82 62.2 76.9 81 54-120 2 30 Benzo(a)pyrene 2.31 U 60.5 76.9 79 60.1 76.9 78 48-125 <1 30 Benzo(b)fluoranthene 1.93 U 59.6 76.9 78 58.4 76.9 76 50-125 2 30 Results flagged with an asterisk (*) indicate values outside control criteria. Results flagged with a pound (#) indicate the control criteria is not applicable. Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded. Printed 2/5/2018 3:02:50 PM Superset Reference:18-0000453045 rev 00 Page 150 of 184 ALS Group USA, Corp. dba AILS Environmental Client: Project: Sample Matrix: Sample Name: Lab Code: Analysis Method: Prep Method: QA/QC Report Terracon Environmental WWAY Building/ES187011 Water Service Request: J1800711 Date Collected: 01/24/18 Date Received: 01/27/18 Date Analyzed: 01/29/18 Date Extracted: 01/29/18 Duplicate Matrix Spike Summary Semivolatile Organic Compounds by GC/MS TW-1 Units: ug/L J1800711-011 Basis: NA 8270C EPA 3510C Matrix Spike Duplicate Matrix Spike JQ1800698-03 JQ1800698-04 Sample Spike Spike % Rec RPD Analyte Name Result Result Amount % Rec Result Amount % Rec Limits RPD Limit Benzo(g,h,i)perylene 2.70 U 58.2 76.9 76 57.2 76.9 74 50-125 2 30 Benzo(k)fluoranthene 3.47 U 60.1 76.9 78 59.2 76.9 77 45-120 1 30 Benzyl Alcohol 2.70 U 42.4 76.9 55 42.3 76.9 55 25-111 <1 30 Bis(2-chloroethoxy)methane 2.31 U 44.3 76.9 58 42.9 76.9 56 28-116 3 30 Bis(2-chloroethyl) Ether 3.66 U 41.0 76.9 53 40.6 76.9 53 26-114 1 30 Bis(2-chloroisopropyl) Ether 2.89 U 58.3 76.9 76 57.3 76.9 74 26-130 2 30 Bis(2-ethylhexyl) Phthalate 2.89 U 70.8 76.9 92 69.3 76.9 90 48-125 2 30 Butyl Benzyl Phthalate 1.66 U 71.0 76.9 92 68.8 76.9 89 50-128 3 30 Carbazole 3.47 U 61.3 76.9 80 60.2 76.9 78 53-117 2 30 Chrysene 2.31 U 62.8 76.9 82 61.5 76.9 80 51-120 2 30 Dibenz(a,h)anthracene 2.89 U 58.2 76.9 76 56.8 76.9 74 50-125 2 30 Dibenzofuran 2.50 U 46.1 76.9 60 45.3 76.9 59 38-115 2 30 Diethyl Phthalate 3.27 U 53.6 76.9 70 53.8 76.9 70 52-120 <1 30 Dimethyl Phthalate 2.50 U 50.0 76.9 65 50.7 76.9 66 47-120 1 30 Di-n-butyl Phthalate 4.24 U 63.8 76.9 83 62.5 76.9 81 54-121 2 30 Di-n-octyl Phthalate 5.39 U 64.0 76.9 83 62.8 76.9 82 46-117 2 30 Diphenylamine + n- 2.12 U 52.6 76.9 68 52.5 76.9 68 51-120 <1 30 Nitrosodiphenylamine Fluoranthene 2.70 U 59.7 76.9 78 58.5 76.9 76 56-120 2 30 Fluorene 1.62 U 48.5 76.9 63 48.1 76.9 63 42-115 <1 30 Hexachlorobenzene 3.27 U 48.8 76.9 63 49.2 76.9 64 50-117 <1 30 Hexachlorobutadiene 2.31 U 40.1 76.9 52 40.6 76.9 53 25-110 1 30 Hexachlorocyclopentadiene 0.962 U 81.7 76.9 106 83.5 76.9 109 22-126 2 30 Hexachloroethane 1.56 U 40.8 76.9 53 41.9 76.9 55 21-115 3 30 Indeno(1,2,3-cd)pyrene 3.27 U 58.2 76.9 76 57.5 76.9 75 49-125 1 30 Isophorone 3.47 U 46.4 76.9 60 44.8 76.9 58 31-120 3 30 Naphthalene 1.02 U 46.1 76.9 60 46.0 76.9 60 33-115 <1 30 Nitrobenzene 4.04 U 42.7 76.9 56 42.5 76.9 55 25-118 <1 30 N-Nitrosodi-n-propylamine 4.24 U 44.7 76.9 58 43.5 76.9 57 30-123 3 30 Pentachlorophenol (PCP) 2.12 U 46.2 76.9 60 45.9 76.9 60 36-110 <1 30 Phenanthrene 2.70 U 57.3 76.9 75 57.3 76.9 74 52-117 <1 30 Phenol 1.14 U 35.3 76.9 46 35.6 76.9 46 13-90 <1 30 Pyrene 1.43 U 62.4 76.9 81 60.8 76.9 79 50-121 3 30 Results flagged with an asterisk (*) indicate values outside control criteria. Results flagged with a pound (#) indicate the control criteria is not applicable. Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded. Printed 2/5/2018 3:02:50 PM Superset Reference:18-0000453045 rev 00 Page 151 of 184 ALS Group USA, Corp. dba AILS Environmental Client: Project: Sample Matrix: Sample Name: Lab Code: Analysis Method: Prep Method: QA/QC Report Terracon Environmental WWAY Building/ES187011 Soil Service Request: J1800711 Date Collected: 01/23/18 Date Received: 01/27/18 Date Analyzed: 01/30/18 Date Extracted: 01/30/18 Duplicate Matrix Spike Summary Semivolatile Organic Compounds by GC/MS SB-1-17 Units: ug/Kg J1800711-002 Basis: Dry 8270C EPA 3546 Matrix Spike Duplicate Matrix Spike JQ1800727-03 JQ1800727-04 Sample Spike Spike % Rec RPD Analyte Name Result Result Amount % Rec Result Amount % Rec Limits RPD Limit 1,2,4-Trichlorobenzene 658 U 10701 1390 77 10601 1390 77 31-110 1 30 1,2-Dichlorobenzene 335 U 10101 1390 72 1040I 1390 75 30-110 3 30 1,3-Dichlorobenzene 397 U 9851 1390 71 10101 1390 73 30-110 3 30 1,4-Dichlorobenzene 429 U 10501 1390 75 10201 1390 74 29-110 2 30 1-Methylnaphthalene 690 U 12001 1390 86 11701 1390 85 39-112 2 30 2,4,5-Trichlorophenol 596 U 9221 1390 66 9781 1390 70 59-115 6 30 2,4,6-Trichlorophenol 523 U 8741 1390 63 8531 1390 61 49-115 2 30 2,4-Dichlorophenol 658 U 9221 1390 66 9431 1390 68 44-110 2 30 2,4-Dimethylphenol 867 U 8741 1390 63 9261 1390 67 40-112 6 30 2,4-Dinitrophenol 241 U 241 U 1390 0 * 240 U 1390 0 * 21-117 NC 30 2,4-Dinitrotoluene 429 U 8631 1390 62 8391 1390 61 49-119 3 30 2,6-Dinitrotoluene 502 U 9401 1390 67 9391 1390 68 56-116 <1 30 2-Chloronaphthalene 449 U 9641 1390 69 9781 1390 70 42-111 1 30 2-Chlorophenol 366 U 9331 1390 67 9811 1390 71 26-110 5 30 2-Methylnaphthalene 616 U 11801 1390 84 11401 1390 82 38-110 3 30 2-Methylphenol 502 U 8321 1390 60 9531 1390 69 32-113 14 30 2-Nitroaniline 533 U 957I 1390 69 1010I 1390 73 49-131 6 30 2-Nitrophenol 543 U 877I 1390 63 874I 1390 63 33-111 <1 30 3- and 4-Methylphenol Coelution 449 U 8601 1390 62 9261 1390 67 34-110 7 30 3,3'-Dichlorobenzidine 888 U 20901 1390 150 21201 1390 153 * 37-150 2 30 3-Nitroaniline 533 U 9151 1390 66 9431 1390 68 59-124 3 30 4,6-Dinitro-2-methylphenol 502 U 502 U 1390 0 * 500 U 1390 0 * 44-112 NC 30 4-Bromophenyl Phenyl Ether 543 U 9781 1390 70 9121 1390 66 56-114 7 30 4-Chloro-3-methylphenol 554 U 10301 1390 74 10301 1390 74 53-116 <1 30 4-Chloroaniline 721 U 12001 1390 86 1330I 1390 96 42-118 10 30 4-Chlorophenyl Phenyl Ether 543 U 9781 1390 70 9321 1390 67 52-113 5 30 4-Nitroaniline 575 U 8251 1390 59 9121 1390 66 56-134 10 30 4-Nitrophenol 585 U 585 U 1390 0 * 583 U 1390 0 * 42-133 NC 30 Acenaphthene 554 U 1060I 1390 76 1030I 1390 74 47-111 3 30 Acenaphthylene 491 U 10101 1390 72 1020I 1390 74 49-112 1 30 Acetophenone 481 U 10801 1390 77 1080I 1390 78 30-113 <1 30 Anthracene 449 U 10501 1390 76 10001 1390 72 54-116 5 30 Benz(a)anthracene 491 U 10701 1390 77 9671 1390 70 54-117 10 30 Benzo(a)pyrene 387 U 957I 1390 69 853I 1390 61 54-120 12 30 Benzo(b)fluoranthene 272 U 9221 1390 66 8981 1390 65 53-118 3 30 Results flagged with an asterisk (*) indicate values outside control criteria. Results flagged with a pound (#) indicate the control criteria is not applicable. Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded. Printed 2/5/2018 3:02:51 PM Superset Reference:18-0000453045 rev 00 Page 152 of 184 ALS Group USA, Corp. dba AILS Environmental Client: Project: Sample Matrix: Sample Name: Lab Code: Analysis Method: Prep Method: QA/QC Report Terracon Environmental WWAY Building/ES187011 Soil Service Request: J1800711 Date Collected: 01/23/18 Date Received: 01/27/18 Date Analyzed: 01/30/18 Date Extracted: 01/30/18 Duplicate Matrix Spike Summary Semivolatile Organic Compounds by GC/MS SB-1-17 Units: ug/Kg J1800711-002 Basis: Dry 8270C EPA 3546 Matrix Spike Duplicate Matrix Spike JQ1800727-03 JQ1800727-04 Sample Spike Spike % Rec RPD Analyte Name Result Result Amount % Rec Result Amount % Rec Limits RPD Limit Benzo(g,h,i)perylene 543 U 8561 1390 62 8321 1390 60 54-123 3 30 Benzo(k)fluoranthene 616 U 10201 1390 73 8801 1390 64 47-122 14 30 Benzyl Alcohol 397 U 8701 1390 63 9671 1390 70 27-111 11 30 Bis(2-chloroethoxy)methane 554 U 10701 1390 77 10901 1390 79 30-112 2 30 Bis(2-chloroethyl) Ether 439 U 10401 1390 75 10601 1390 77 21-110 2 30 Bis(2-chloroisopropyl) Ether 366 U 14701 1390 105 14801 1390 107 25-120 <1 30 Bis(2-ethylhexyl) Phthalate 460 U 10801 1390 77 9261 1390 67 45-122 15 30 Butyl Benzyl Phthalate 491 U 11001 1390 79 9781 1390 70 47-119 12 30 Carbazole 596 U 10301 1390 74 10101 1390 72 51-120 2 30 Chrysene 470 U 1120I 1390 80 10101 1390 73 53-118 10 30 Dibenz(a,h)anthracene 481 U 926I 1390 67 8011 1390 58 54-119 14 30 Dibenzofuran 481 U 1000I 1390 72 981I 1390 71 46-113 2 30 Diethyl Phthalate 533 U 10401 1390 75 10301 1390 74 54-118 2 30 Dimethyl Phthalate 554 U 10201 1390 73 9981 1390 72 53-115 2 30 Di-n-butyl Phthalate 355 U 10301 1390 74 9151 1390 66 46-120 11 30 Di-n-octyl Phthalate 543 U 9641 1390 69 8041 1390 58 42-115 18 30 Diphenylamine + n- 387 U 9881 1390 71 9841 1390 71 56-119 <1 30 Nitrosodiphenylamine Fluoranthene 502 U 1020I 1390 73 950I 1390 69 53-120 7 30 Fluorene 491 U 1020I 1390 73 988I 1390 71 51-115 3 30 Hexachlorobenzene 502 U 967I 1390 69 860I 1390 62 58-116 12 30 Hexachlorobutadiene 575 U 10501 1390 76 10301 1390 74 21-122 2 30 Hexachlorocyclopentadiene 355 U 355 U 1390 0 * 4401 1390 32 27-110 NC 30 Hexachloroethane 324 U 1030I 1390 74 1020I 1390 74 20-110 1 30 Indeno(1,2,3-cd)pyrene 429 U 8741 1390 63 8221 1390 59 54-120 6 30 Isophorone 606 U 1160I 1390 83 1120I 1390 80 36-116 3 30 Naphthalene 512 U 12001 1390 86 11801 1390 85 30-111 2 30 Nitrobenzene 408 U 1050I 1390 75 1100I 1390 79 30-114 4 30 N-Nitrosodi-n-propylamine 523 U 10801 1390 78 1080I 1390 78 25-117 <1 30 Pentachlorophenol (PCP) 366 U 16301 1390 117 16501 1390 119 20-126 2 30 Phenanthrene 439 U 1120I 1390 80 1060I 1390 76 54-115 6 30 Phenol 481 U 752I 1390 54 822I 1390 59 34-115 9 30 Pyrene 481 U 1110I 1390 80 1030I 1390 74 50-117 8 30 Results flagged with an asterisk (*) indicate values outside control criteria. Results flagged with a pound (#) indicate the control criteria is not applicable. Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded. Printed 2/5/2018 3:02:51 PM Superset Reference:18-0000453045 rev 00 Page 153 of 184 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Water Date Received: NA Sample Name: Method Blank Units: ug/L Lab Code: JQ1800698-01 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 0.600 U 5.00 0.600 1 01/30/18 00:49 1/29/18 1,2-Dichlorobenzene 0.640 U 5.00 0.640 1 01/30/18 00:49 1/29/18 1,3-Dichlorobenzene 0.920 U 5.00 0.920 1 01/30/18 00:49 1/29/18 1,4-Dichlorobenzene 0.910 U 5.00 0.910 1 01/30/18 00:49 1/29/18 1-Methylnaphthalene 0.730 U 5.00 0.730 1 01/30/18 00:49 1/29/18 2,4,5-Trichlorophenol 1.30 U 5.00 1.30 1 01/30/18 00:49 1/29/18 2,4,6-Trichlorophenol 0.890 U 5.00 0.890 1 01/30/18 00:49 1/29/18 2,4-Dichlorophenol 1.20 U 5.00 1.20 1 01/30/18 00:49 1/29/18 2,4-Dimethylphenol 1.50 U 5.00 1.50 1 01/30/18 00:49 1/29/18 2,4-Dinitrophenol 0.760 U 20.0 0.760 1 01/30/18 00:49 1/29/18 2,4-Dinitrotoluene 1.30 U 5.00 1.30 1 01/30/18 00:49 1/29/18 2,6-Dinitrotoluene 1.10 U 5.00 1.10 1 01/30/18 00:49 1/29/18 2-Chloronaphthalene 4.60 U 5.00 4.60 1 01/30/18 00:49 1/29/18 2-Chlorophenol 1.20 U 5.00 1.20 1 01/30/18 00:49 1/29/18 2-Methylnaphthalene 0.630 U 5.00 0.630 1 01/30/18 00:49 1/29/18 2-Methylphenol 1.30 U 5.00 1.30 1 01/30/18 00:49 1/29/18 2-Nitroaniline 1.50 U 5.00 1.50 1 01/30/18 00:49 1/29/18 2-Nitrophenol 1.40 U 20.0 1.40 1 01/30/18 00:49 1/29/18 3- and 4-Methylphenol Coelution 1.00 U 5.00 1.00 1 01/30/18 00:49 1/29/18 3,3'-Dichlorobenzidine 1.40 U 20.0 1.40 1 01/30/18 00:49 1/29/18 3-Nitroaniline 1.10 U 5.00 1.10 1 01/30/18 00:49 1/29/18 4,6-Dinitro-2-methylphenol 1.00 U 20.0 1.00 1 01/30/18 00:49 1/29/18 4-Bromophenyl Phenyl Ether 1.30 U 5.00 1.30 1 01/30/18 00:49 1/29/18 4-Chloro-3-methylphenol 1.80 U 5.00 1.80 1 01/30/18 00:49 1/29/18 4-Chloroaniline 1.40 U 5.00 1.40 1 01/30/18 00:49 1/29/18 4-Chlorophenyl Phenyl Ether 0.960 U 5.00 0.960 1 01/30/18 00:49 1/29/18 4-Nitroaniline 1.00 U 5.00 1.00 1 01/30/18 00:49 1/29/18 4-Nitrophenol 1.80 U 20.0 1.80 1 01/30/18 00:49 1/29/18 Acenaphthene 4.20 U 5.00 4.20 1 01/30/18 00:49 1/29/18 Acenaphthylene 0.990 U 5.00 0.990 1 01/30/18 00:49 1/29/18 Acetophenone 1.60 U 10.0 1.60 1 01/30/18 00:49 1/29/18 Anthracene 1.60 U 5.00 1.60 1 01/30/18 00:49 1/29/18 Benz(a)anthracene 1.00 U 5.00 1.00 1 01/30/18 00:49 1/29/18 Benzo(a)pyrene 1.20 U 5.00 1.20 1 01/30/18 00:49 1/29/18 Benzo(b)fluoranthene 1.00 U 5.00 1.00 1 01/30/18 00:49 1/29/18 Benzo(g,h,i)perylene 1.40 U 5.00 1.40 1 01/30/18 00:49 1/29/18 Benzo(k)fluoranthene 1.80 U 5.00 1.80 1 01/30/18 00:49 1/29/18 Benzyl Alcohol 1.40 U 5.00 1.40 1 01/30/18 00:49 1/29/18 Bis(2-chloroethoxy)methane 1.20 U 5.00 1.20 1 01/30/18 00:49 1/29/18 Bis(2-chloroethyl) Ether 1.90 U 5.00 1.90 1 01/30/18 00:49 1/29/18 Bis(2-chloroisopropyl) Ether 1.50 U 5.00 1.50 1 01/30/18 00:49 1/29/18 Bis(2-ethylhexyl) Phthalate 1.50 U 5.00 1.50 1 01/30/18 00:49 1/29/18 Butyl Benzyl Phthalate 0.860 U 10.0 0.860 1 01/30/18 00:49 1/29/18 Printed 2/5/2018 3:02:49 PM Page 154 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Water Date Received: NA Sample Name: Method Blank Units: ug/L Lab Code: JQ1800698-01 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 1.80 U 5.00 1.80 1 01/30/18 00:49 1/29/18 Chrysene 1.20 U 5.00 1.20 1 01/30/18 00:49 1/29/18 Dibenz(a,h)anthracene L50 U 5.00 1.50 1 01/30/18 00:49 1/29/18 Dibenzofuran 1.30 U 5.00 1.30 1 01/30/18 00:49 1/29/18 Diethyl Phthalate 1.70 U 5.00 1.70 1 01/30/18 00:49 1/29/18 Dimethyl Phthalate 1.30 U 5.00 1.30 1 01/30/18 00:49 1/29/18 Di-n-butyl Phthalate 2.20 U 5.00 2.20 1 01/30/18 00:49 1/29/18 Di-n-octyl Phthalate 2.80 U 10.0 2.80 1 01/30/18 00:49 1/29/18 Diphenylamine + n-Nitrosodiphenylamine 1.10 U 5.00 1.10 1 01/30/18 00:49 1/29/18 Fluoranthene 1.40 U 5.00 1.40 1 01/30/18 00:49 1/29/18 Fluorene 0.840 U 5.00 0.840 1 01/30/18 00:49 1/29/18 Hexachlorobenzene 1.70 U 5.00 1.70 1 01/30/18 00:49 1/29/18 Hexachlorobutadiene 1.20 U TOO 1.20 1 01/30/18 00:49 1/29/18 Hexachlorocyclopentadiene 0.500 U 5.00 0.500 1 01/30/18 00:49 1/29/18 Hexachloroethane 0.810 U 5.00 0.810 1 01/30/18 00:49 1/29/18 Indeno(1,2,3-cd)pyrene 1.70 U 5.00 1.70 1 01/30/18 00:49 1/29/18 Isophorone 1.80 U 5.00 1.80 1 01/30/18 00:49 1/29/18 Naphthalene 0.530 U 5.00 0.530 1 01/30/18 00:49 1/29/18 Nitrobenzene 2.10 U 5.00 2.10 1 01/30/18 00:49 1/29/18 N-Nitrosodi-n-propylamine 2.20 U 5.00 2.20 1 01/30/18 00:49 1/29/18 Pentachlorophenol (PCP) 1.10 U 20.0 1.10 1 01/30/18 00:49 1/29/18 Phenanthrene 1.40 U 5.00 1.40 1 01/30/18 00:49 1/29/18 Phenol 0.590 U 5.00 0.590 1 01/30/18 00:49 1/29/18 Pyrene 0.740 U 5.00 0.740 1 01/30/18 00:49 1/29/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 71 23 - 122 01/30/18 00:49 2-Fluorobiphenyl 73 15 - 117 01/30/18 00:49 2-Fluorophenol 67 10 - 85 01/30/18 00:49 Nitrobenzene-d5 77 10 - 110 01/30/18 00:49 Phenol-d6 60 7 - 60 01/30/18 00:49 p-Terphenyl-dl4 91 40 - 125 01/30/18 00:49 Printed 2/5/2018 3:02:49 PM Page 155 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Soil Date Received: NA Sample Name: Method Blank Units: ug/Kg Lab Code: JQ1800727-01 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 63.0 U 170 63.0 1 01/30/18 17:40 1/30/18 1,2-Dichlorobenzene 32.0 U 170 32.0 1 01/30/18 17:40 1/30/18 1,3-Dichlorobenzene 38.0 U 170 38.0 1 01/30/18 17:40 1/30/18 1,4-Dichlorobenzene 41.0 U 170 41.0 1 01/30/18 17:40 1/30/18 1-Methylnaphthalene 66.0 U 170 66.0 1 01/30/18 17:40 1/30/18 2,4,5-Trichlorophenol 57.0 U 170 57.0 1 01/30/18 17:40 1/30/18 2,4,6-Trichlorophenol 50.0 U 170 50.0 1 01/30/18 17:40 1/30/18 2,4-Dichlorophenol 63.0 U 170 63.0 1 01/30/18 17:40 1/30/18 2,4-Dimethylphenol 83.0 U 170 83.0 1 01/30/18 17:40 1/30/18 2,4-Dinitrophenol 23.0 U 670 23.0 1 01/30/18 17:40 1/30/18 2,4-Dinitrotoluene 41.0 U 170 41.0 1 01/30/18 17:40 1/30/18 2,6-Dinitrotoluene 48.0 U 170 48.0 1 01/30/18 17:40 1/30/18 2-Chloronaphthalene 43.0 U 170 43.0 1 01/30/18 17:40 1/30/18 2-Chlorophenol 35.0 U 170 35.0 1 01/30/18 17:40 1/30/18 2-Methylnaphthalene 59.0 U 170 59.0 1 01/30/18 17:40 1/30/18 2-Methylphenol 48.0 U 170 48.0 1 01/30/18 17:40 1/30/18 2-Nitroaniline 51.0 U 170 51.0 1 01/30/18 17:40 1/30/18 2-Nitrophenol 52.0 U 670 52.0 1 01/30/18 17:40 1/30/18 3- and 4-Methylphenol Coelution 43.0 U 170 43.0 1 01/30/18 17:40 1/30/18 3,3'-Dichlorobenzidine 85.0 U 670 85.0 1 01/30/18 17:40 1/30/18 3-Nitroaniline 51.0 U 170 51.0 1 01/30/18 17:40 1/30/18 4,6-Dinitro-2-methylphenol 48.0 U 670 48.0 1 01/30/18 17:40 1/30/18 4-Bromophenyl Phenyl Ether 52.0 U 170 52.0 1 01/30/18 17:40 1/30/18 4-Chloro-3-methylphenol 53.0 U 170 53.0 1 01/30/18 17:40 1/30/18 4-Chloroaniline 69.0 U 170 69.0 1 01/30/18 17:40 1/30/18 4-Chlorophenyl Phenyl Ether 52.0 U 170 52.0 1 01/30/18 17:40 1/30/18 4-Nitroaniline 55.0 U 170 55.0 1 01/30/18 17:40 1/30/18 4-Nitrophenol 56.0 U 670 56.0 1 01/30/18 17:40 1/30/18 Acenaphthene 53.0 U 170 53.0 1 01/30/18 17:40 1/30/18 Acenaphthylene 47.0 U 170 47.0 1 01/30/18 17:40 1/30/18 Acetophenone 46.0 U 340 46.0 1 01/30/18 17:40 1/30/18 Anthracene 43.0 U 170 43.0 1 01/30/18 17:40 1/30/18 Benz(a)anthracene 47.0 U 170 47.0 1 01/30/18 17:40 1/30/18 Benzo(a)pyrene 37.0 U 170 37.0 1 01/30/18 17:40 1/30/18 Benzo(b)fluoranthene 26.0 U 170 26.0 1 01/30/18 17:40 1/30/18 Benzo(g,h,i)perylene 52.0 U 170 52.0 1 01/30/18 17:40 1/30/18 Benzo(k)fluoranthene 59.0 U 170 59.0 1 01/30/18 17:40 1/30/18 Benzyl Alcohol 38.0 U 340 38.0 1 01/30/18 17:40 1/30/18 Bis(2-chloroethoxy)methane 53.0 U 170 53.0 1 01/30/18 17:40 1/30/18 Bis(2-chloroethyl) Ether 42.0 U 170 42.0 1 01/30/18 17:40 1/30/18 Bis(2-chloroisopropyl) Ether 35.0 U 170 35.0 1 01/30/18 17:40 1/30/18 Bis(2-ethylhexyl) Phthalate 44.0 U 170 44.0 1 01/30/18 17:40 1/30/18 Butyl Benzyl Phthalate 47.0 U 340 47.0 1 01/30/18 17:40 1/30/18 Printed 2/5/2018 3:02:50 PM Page 156 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Soil Date Received: NA Sample Name: Method Blank Units: ug/Kg Lab Code: JQ1800727-01 Basis: Dry Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 57.0 U 170 57.0 1 01/30/18 17:40 1/30/18 Chrysene 45.0 U 170 45.0 1 01/30/18 17:40 1/30/18 Dibenz(a,h)anthracene 46.0 U 170 46.0 1 01/30/18 17:40 1/30/18 Dibenzofuran 46.0 U 170 46.0 1 01/30/18 17:40 1/30/18 Diethyl Phthalate 51.0 U 170 51.0 1 01/30/18 17:40 1/30/18 Dimethyl Phthalate 53.0 U 170 53.0 1 01/30/18 17:40 1/30/18 Di-n-butyl Phthalate 34.0 U 170 34.0 1 01/30/18 17:40 1/30/18 Di-n-octyl Phthalate 52.0 U 340 52.0 1 01/30/18 17:40 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 37.0 U 170 37.0 1 01/30/18 17:40 1/30/18 Fluoranthene 48.0 U 170 48.0 1 01/30/18 17:40 1/30/18 Fluorene 47.0 U 170 47.0 1 01/30/18 17:40 1/30/18 Hexachlorobenzene 48.0 U 170 48.0 1 01/30/18 17:40 1/30/18 Hexachlorobutadiene 55.0 U 170 55.0 1 01/30/18 17:40 1/30/18 Hexachlorocyclopentadiene 34.0 U 170 34.0 1 01/30/18 17:40 1/30/18 Hexachloroethane 31.0 U 170 31.0 1 01/30/18 17:40 1/30/18 Indeno(1,2,3-cd)pyrene 41.0 U 170 41.0 1 01/30/18 17:40 1/30/18 Isophorone 58.0 U 170 58.0 1 01/30/18 17:40 1/30/18 Naphthalene 49.0 U 170 49.0 1 01/30/18 17:40 1/30/18 Nitrobenzene 39.0 U 170 39.0 1 01/30/18 17:40 1/30/18 N-Nitrosodi-n-propylamine 50.0 U 170 50.0 1 01/30/18 17:40 1/30/18 Pentachlorophenol (PCP) 35.0 U 670 35.0 1 01/30/18 17:40 1/30/18 Phenanthrene 42.0 U 170 42.0 1 01/30/18 17:40 1/30/18 Phenol 46.0 U 170 46.0 1 01/30/18 17:40 1/30/18 Pyrene 46.0 U 170 46.0 1 01/30/18 17:40 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 47 30 - 136 01/30/18 17:40 2-Fluorobiphenyl 55 20 - 115 01/30/18 17:40 2-Fluorophenol 53 10 - 110 01/30/18 17:40 Nitrobenzene-d5 55 20 - 110 01/30/18 17:40 Phenol-d6 57 14 - 100 01/30/18 17:40 p-Terphenyl-dl4 73 32 - 119 01/30/18 17:40 Printed 2/5/2018 3:02:50 PM Page 157 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Water Date Received: NA Sample Name: Method Blank Units: ug/L Lab Code: JQ1800741-01 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1,2,4-Trichlorobenzene 0.600 U 5.00 0.600 1 01/30/18 18:30 1/30/18 1,2-Dichlorobenzene 0.640 U 5.00 0.640 1 01/30/18 18:30 1/30/18 1,3-Dichlorobenzene 0.920 U 5.00 0.920 1 01/30/18 18:30 1/30/18 1,4-Dichlorobenzene 0.910 U 5.00 0.910 1 01/30/18 18:30 1/30/18 1-Methylnaphthalene 0.730 U 5.00 0.730 1 01/30/18 18:30 1/30/18 2,4,5-Trichlorophenol 1.30 U 5.00 1.30 1 01/30/18 18:30 1/30/18 2,4,6-Trichlorophenol 0.890 U 5.00 0.890 1 01/30/18 18:30 1/30/18 2,4-Dichlorophenol 1.20 U 5.00 1.20 1 01/30/18 18:30 1/30/18 2,4-Dimethylphenol 1.50 U 5.00 1.50 1 01/30/18 18:30 1/30/18 2,4-Dinitrophenol 0.760 U 20.0 0.760 1 01/30/18 18:30 1/30/18 2,4-Dinitrotoluene 1.30 U 5.00 1.30 1 01/30/18 18:30 1/30/18 2,6-Dinitrotoluene 1.10 U 5.00 1.10 1 01/30/18 18:30 1/30/18 2-Chloronaphthalene 4.60 U 5.00 4.60 1 01/30/18 18:30 1/30/18 2-Chlorophenol 1.20 U 5.00 1.20 1 01/30/18 18:30 1/30/18 2-Methylnaphthalene 0.630 U 5.00 0.630 1 01/30/18 18:30 1/30/18 2-Methylphenol 1.30 U 5.00 1.30 1 01/30/18 18:30 1/30/18 2-Nitroaniline 1.50 U 5.00 1.50 1 01/30/18 18:30 1/30/18 2-Nitrophenol 1.40 U 20.0 1.40 1 01/30/18 18:30 1/30/18 3- and 4-Methylphenol Coelution 1.00 U 5.00 1.00 1 01/30/18 18:30 1/30/18 3,3'-Dichlorobenzidine 1.40 U 20.0 1.40 1 01/30/18 18:30 1/30/18 3-Nitroaniline 1.10 U 5.00 1.10 1 01/30/18 18:30 1/30/18 4,6-Dinitro-2-methylphenol 1.00 U 20.0 1.00 1 01/30/18 18:30 1/30/18 4-Bromophenyl Phenyl Ether 1.30 U 5.00 1.30 1 01/30/18 18:30 1/30/18 4-Chloro-3-methylphenol 1.80 U 5.00 1.80 1 01/30/18 18:30 1/30/18 4-Chloroaniline 1.40 U 5.00 1.40 1 01/30/18 18:30 1/30/18 4-Chlorophenyl Phenyl Ether 0.960 U 5.00 0.960 1 01/30/18 18:30 1/30/18 4-Nitroaniline 1.00 U 5.00 1.00 1 01/30/18 18:30 1/30/18 4-Nitrophenol 1.80 U 20.0 1.80 1 01/30/18 18:30 1/30/18 Acenaphthene 4.20 U 5.00 4.20 1 01/30/18 18:30 1/30/18 Acenaphthylene 0.990 U 5.00 0.990 1 01/30/18 18:30 1/30/18 Acetophenone 1.60 U 10.0 1.60 1 01/30/18 18:30 1/30/18 Anthracene 1.60 U 5.00 1.60 1 01/30/18 18:30 1/30/18 Benz(a)anthracene 1.00 U 5.00 1.00 1 01/30/18 18:30 1/30/18 Benzo(a)pyrene 1.20 U 5.00 1.20 1 01/30/18 18:30 1/30/18 Benzo(k)fluoranthene 1.00 U 5.00 1.00 1 01/30/18 18:30 1/30/18 Benzo(g,h,i)perylene 1.40 U 5.00 1.40 1 01/30/18 18:30 1/30/18 Benzo(k)fluoranthene 1.80 U 5.00 1.80 1 01/30/18 18:30 1/30/18 Benzyl Alcohol 1.40 U 5.00 1.40 1 01/30/18 18:30 1/30/18 Bis(2-chloroethoxy)methane 1.20 U 5.00 1.20 1 01/30/18 18:30 1/30/18 Bis(2-chloroethyl) Ether 1.90 U 5.00 1.90 1 01/30/18 18:30 1/30/18 Bis(2-chloroisopropyl) Ether 1.50 U 5.00 1.50 1 01/30/18 18:30 1/30/18 Bis(2-ethylhexyl) Phthalate 1.50 U 5.00 1.50 1 01/30/18 18:30 1/30/18 Butyl Benzyl Phthalate 0.860 U 10.0 0.860 1 01/30/18 18:30 1/30/18 Printed 2/5/2018 3:02:52 PM Page 158 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Water Date Received: NA Sample Name: Method Blank Units: ug/L Lab Code: JQ1800741-01 Basis: NA Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Prep Method: EPA 3510C Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Carbazole 1.80 U 5.00 1.80 1 01/30/18 18:30 1/30/18 Chrysene 1.20 U 5.00 1.20 1 01/30/18 18:30 1/30/18 Dibenz(a,h)anthracene L50 U 5.00 1.50 1 01/30/18 18:30 1/30/18 Dibenzofuran 1.30 U 5.00 1.30 1 01/30/18 18:30 1/30/18 Diethyl Phthalate 1.70 U 5.00 1.70 1 01/30/18 18:30 1/30/18 Dimethyl Phthalate 1.30 U 5.00 1.30 1 01/30/18 18:30 1/30/18 Di-n-butyl Phthalate 2.20 U 5.00 2.20 1 01/30/18 18:30 1/30/18 Di-n-octyl Phthalate 2.80 U 10.0 2.80 1 01/30/18 18:30 1/30/18 Diphenylamine + n-Nitrosodiphenylamine 1.10 U 5.00 1.10 1 01/30/18 18:30 1/30/18 Fluoranthene 1.40 U 5.00 1.40 1 01/30/18 18:30 1/30/18 Fluorene 0.840 U 5.00 0.840 1 01/30/18 18:30 1/30/18 Hexachlorobenzene 1.70 U 5.00 1.70 1 01/30/18 18:30 1/30/18 Hexachlorobutadiene 1.20 U TOO 1.20 1 01/30/18 18:30 1/30/18 Hexachlorocyclopentadiene 0.500 U 5.00 0.500 1 01/30/18 18:30 1/30/18 Hexachloroethane 0.810 U 5.00 0.810 1 01/30/18 18:30 1/30/18 Indeno(1,2,3-cd)pyrene 1.70 U 5.00 1.70 1 01/30/18 18:30 1/30/18 Isophorone 1.80 U 5.00 1.80 1 01/30/18 18:30 1/30/18 Naphthalene 0.530 U 5.00 0.530 1 01/30/18 18:30 1/30/18 Nitrobenzene 2.10 U 5.00 2.10 1 01/30/18 18:30 1/30/18 N-Nitrosodi-n-propylamine 2.20 U 5.00 2.20 1 01/30/18 18:30 1/30/18 Pentachlorophenol (PCP) 1.10 U 20.0 1.10 1 01/30/18 18:30 1/30/18 Phenanthrene 1.40 U 5.00 1.40 1 01/30/18 18:30 1/30/18 Phenol 0.590 U 5.00 0.590 1 01/30/18 18:30 1/30/18 Pyrene 0.740 U 5.00 0.740 1 01/30/18 18:30 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2,4,6-Tribromophenol 60 23 - 122 01/30/18 18:30 2-Fluorobiphenyl 64 15 - 117 01/30/18 18:30 2-Fluorophenol 53 10 - 85 01/30/18 18:30 Nitrobenzene-d5 69 10 - 110 01/30/18 18:30 Phenol-d6 43 7 - 60 01/30/18 18:30 p-Terphenyl-dl4 87 40 - 125 01/30/18 18:30 Printed 2/5/2018 3:02:52 PM Page 159 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Analyzed: 01/29/18 Sample Matrix: Water Date Extracted: 01/29/18 Lab Control Sample Summary Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Units: ug/L Prep Method: EPA 3510C Basis: NA Analysis Lot: 578562 Lab Control Sample JQ1800698-02 Analyte Name Result Spike Amount % Rec % Rec Limits 1,2,4-Trichlorobenzene 5.82 40.0 15 * 30-110 1,2-Dichlorobenzene 0.640 U 40.0 0 * 30-110 1,3-Dichlorobenzene 0.920 U 40.0 0 * 25-110 1,4-Dichlorobenzene 0.910 U 40.0 0 * 21-110 1-Methylnaphthalene 15.5 40.0 39 34-113 2,4,5-Trichlorophenol 23.8 40.0 59 43-116 2,4,6-Trichlorophenol 22.1 40.0 55 34-119 2,4-Dichlorophenol 16.7 40.0 42 32-115 2,4-Dimethylphenol 17.0 40.0 42 31-111 2,4-Dinitrophenol 23.9 40.0 60 22-113 2,4-Dinitrotoluene 27.5 40.0 69 49-117 2,6-Dinitrotoluene 25.6 40.0 64 47-120 2-Chloronaphthalene 17.0 40.0 42 30-115 2-Chlorophenol 4.24I 40.0 11 * 25-110 2-Methylnaphthalene 14.4 40.0 36 29-110 2-Methylphenol 11.4 40.0 29 29-112 2-Nitroaniline 26.7 40.0 67 38-145 2-Nitrophenol 9.181 40.0 23 * 24-119 3- and 4-Methylphenol Coelution 14.5 40.0 36 29-110 3,3'-Dichlorobenzidine 37.8 40.0 94 43-150 3-Nitroaniline 27.5 40.0 69 55-128 4,6-Dinitro-2-methylphenol 28.9 40.0 72 26-115 4-Bromophenyl Phenyl Ether 24.2 40.0 61 49-115 4-Chloro-3-methylphenol 25.4 40.0 64 45-113 4-Chloroaniline 18.3 40.0 46 33-122 4-Chlorophenyl Phenyl Ether 22.6 40.0 57 42-115 4-Nitroaniline 30.4 40.0 76 52-128 4-Nitrophenol 21.4 40.0 53 15-85 Acenaphthene 21.0 40.0 53 32-112 Acenaphthylene 20.8 40.0 52 33-115 Acetophenone 8.44I 40.0 21 * 30-115 Anthracene 27.9 40.0 70 54-114 Benz(a)anthracene 33.4 40.0 84 54-120 Benzo(a)pyrene 32.1 40.0 80 48-125 Benzo(b)fluoranthene 31.2 40.0 78 50-125 Benzo(g,h,i)perylene 30.8 40.0 77 50-125 Benzo(k)fluoranthene 31.5 40.0 79 45-120 Benzyl Alcohol 10.4 40.0 26 25-111 Bis(2-chloroethoxy)methane 12.5 40.0 31 28-116 Bis(2-chloroethyl) Ether 1.90 U 40.0 0 * 26-114 Bis(2-chloroisopropyl) Ether 3.811 40.0 10 * 26-130 Printed 2/5/2018 3:02:49 PM Superset Reference:18-0000453045 rev 00 Page 160 of 184 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Project: Sample Matrix: Analysis Method: Prep Method: Terracon Environmental WWAY Building/ES187011 Water 8270C EPA 3510C Lab Control Sample Summary Semivolatile Organic Compounds by GC/MS Service Request: Date Analyzed: Date Extracted: Units: Basis: Analysis Lot: Lab Control Sample JQ1800698-02 J1800711 01/29/18 01/29/18 ug/L NA 578562 Analyte Name Result Spike Amount % Rec % Rec Limits Bis(2-ethylhexyl) Phthalate 37.1 40.0 93 48-125 Butyl Benzyl Phthalate 38.0 40.0 95 50-128 Carbazole 30.7 40.0 77 53-117 Chrysene 33.0 40.0 82 51-120 Dibenz(a,h)anthracene 30.9 40.0 77 50-125 Dibenzofuran 21.6 40.0 54 38-115 Diethyl Phthalate 26.7 40.0 67 52-120 Dimethyl Phthalate 25.3 40.0 63 47-120 Di-n-butyl Phthalate 32.4 40.0 81 54-121 Di-n-octyl Phthalate 32.6 40.0 82 46-117 Diphenylamine + n-Nitrosodiphenylamine 25.4 40.0 64 51-120 Fluoranthene 29.9 40.0 75 56-120 Fluorene 23.2 40.0 58 42-115 Hexachlorobenzene 23.7 40.0 59 50-117 Hexachlorobutadiene 3.341 40.0 8 * 25-110 Hexachlorocyclopentadiene 13.8 40.0 35 22-126 Hexachloroethane 0.810 U 40.0 0 * 21-115 Indeno(1,2,3-cd)pyrene 31.0 40.0 78 49-125 Isophorone 16.6 40.0 42 31-120 Naphthalene 8.44 40.0 21 * 33-115 Nitrobenzene 7.00 40.0 18 * 25-118 N-Nitrosodi-n-propylamine 11.9 40.0 30 30-123 Pentachlorophenol (PCP) 22.3 40.0 56 36-110 Phenanthrene 27.6 40.0 69 52-117 Phenol 6.11 40.0 15 13-90 Pyrene 31.8 40.0 79 50-121 Printed 2/5/2018 3:02:49 PM Page 161 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Analyzed: 01/30/18 Sample Matrix: Soil Date Extracted: 01/30/18 Lab Control Sample Summary Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Units: ug/Kg Prep Method: EPA 3546 Basis: Dry Analysis Lot: 578811 Lab Control Sample JQ1800727-02 Analyte Name Result Spike Amount % Rec % Rec Limits 1,2,4-Trichlorobenzene 975 1330 73 31-110 1,2-Dichlorobenzene 1020 1330 77 30-110 1,3-Dichlorobenzene 975 1330 73 30-110 1,4-Dichlorobenzene 996 1330 75 29-110 1-Methylnaphthalene 1060 1330 80 39-112 2,4,5-Trichlorophenol 995 1330 75 59-115 2,4,6-Trichlorophenol 1010 1330 76 49-115 2,4-Dichlorophenol 1020 1330 76 44-110 2,4-Dimethylphenol 1030 1330 77 40-112 2,4-Dinitrophenol 934 1330 70 21-117 2,4-Dinitrotoluene 1090 1330 82 49-119 2,6-Dinitrotoluene 1060 1330 80 56-116 2-Chloronaphthalene 984 1330 74 42-111 2-Chlorophenol 1020 1330 77 26-110 2-Methylnaphthalene 1040 1330 78 38-110 2-Methylphenol 1040 1330 78 32-113 2-Nitroaniline 1160 1330 87 49-131 2-Nitrophenol 1040 1330 78 33-111 3- and 4-Methylphenol Coelution 1080 1330 81 34-110 3,3'-Dichlorobenzidine 1170 1330 88 37-150 3-Nitroaniline 1080 1330 81 59-124 4,6-Dinitro-2-methylphenol 1090 1330 82 44-112 4-Bromophenyl Phenyl Ether 1010 1330 76 56-114 4-Chloro-3-methylphenol 1060 1330 80 53-116 4-Chloroaniline 1130 1330 85 42-118 4-Chlorophenyl Phenyl Ether 994 1330 75 52-113 4-Nitroaniline 1080 1330 81 56-134 4-Nitrophenol 961 1330 72 42-133 Acenaphthene 1030 1330 77 47-111 Acenaphthylene 1040 1330 78 49-112 Acetophenone 1090 1330 81 30-113 Anthracene 1100 1330 82 54-116 Benz(a)anthracene 1140 1330 85 54-117 Benzo(a)pyrene 1090 1330 82 54-120 Benzo(b)fluoranthene 1090 1330 82 53-118 Benzo(g,h,i)perylene 1080 1330 81 54-123 Benzo(k)fluoranthene 1080 1330 81 47-122 Benzyl Alcohol 1050 1330 78 27-111 Bis(2-chloroethoxy)methane 1010 1330 76 30-112 Bis(2-chloroethyl) Ether 992 1330 74 21-110 Bis(2-chloroisopropyl) Ether 1440 1330 108 25-120 Printed 2/5/2018 3:02:50 PM Superset Reference:18-0000453045 rev 00 Page 162 of 184 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Project: Sample Matrix: Analysis Method: Prep Method: Terracon Environmental WWAY Building/ES187011 Soil 8270C EPA 3546 Lab Control Sample Summary Semivolatile Organic Compounds by GC/MS Service Request: Date Analyzed: Date Extracted: Units: Basis: Analysis Lot: Lab Control Sample JQ1800727-02 J1800711 01/30/18 01/30/18 ug/Kg Dry 578811 Analyte Name Result Spike Amount % Rec % Rec Limits Bis(2-ethylhexyl) Phthalate 1260 1330 94 45-122 Butyl Benzyl Phthalate 1220 1330 91 47-119 Carbazole 1110 1330 83 51-120 Chrysene 1130 1330 85 53-118 Dibenz(a,h)anthracene 1070 1330 80 54-119 Dibenzofuran 996 1330 75 46-113 Diethyl Phthalate 1050 1330 78 54-118 Dimethyl Phthalate 1030 1330 77 53-115 Di-n-butyl Phthalate 1140 1330 86 46-120 Di-n-octyl Phthalate 1110 1330 84 42-115 Diphenylamine + n-Nitrosodiphenylamine 1020 1330 77 56-119 Fluoranthene 1080 1330 81 53-120 Fluorene 1020 1330 77 51-115 Hexachlorobenzene 962 1330 72 58-116 Hexachlorobutadiene 954 1330 72 21-122 Hexachlorocyclopentadiene 1920 1330 144 * 27-110 Hexachloroethane 1050 1330 79 20-110 Indeno(1,2,3-cd)pyrene 1070 1330 80 54-120 Isophorone 1060 1330 80 36-116 Naphthalene 1040 1330 78 30-111 Nitrobenzene 1050 1330 79 30-114 N-Nitrosodi-n-propylamine 1080 1330 81 25-117 Pentachlorophenol(PCP) 836 1330 63 20-126 Phenanthrene 1100 1330 82 54-115 Phenol 912 1330 68 34-115 Pyrene 1120 1330 84 50-117 Printed 2/5/2018 3:02:50 PM Page 163 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Analyzed: 01/30/18 Sample Matrix: Water Date Extracted: 01/30/18 Duplicate Lab Control Sample Summary Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Units: ug/L Prep Method: EPA 3510C Basis: NA Analysis Lot: 578811 Lab Control Sample Duplicate Lab Control Sample JQ1800741-02 JQ1800741-03 Spike Spike % Rec RPD Analyte Name Result Amount % Rec Result Amount % Rec Limits RPD Limit 1,2,4-Trichlorobenzene 24.0 40.0 60 27.7 40.0 69 30-110 15 30 1,2-Dichlorobenzene 24.1 40.0 60 28.3 40.0 71 30-110 16 30 1,3-Dichlorobenzene 23.2 40.0 58 27.4 40.0 68 25-110 16 30 1,4-Dichlorobenzene 24.1 40.0 60 27.9 40.0 70 21-110 14 30 1-Methylnaphthalene 26.5 40.0 66 30.0 40.0 75 34-113 12 30 2,4,5-Trichlorophenol 27.8 40.0 69 31.0 40.0 78 43-116 11 30 2,4,6-Trichlorophenol 26.9 40.0 67 29.1 40.0 73 34-119 8 30 2,4-Dichlorophenol 26.0 40.0 65 28.9 40.0 72 32-115 11 30 2,4-Dimethylphenol 25.8 40.0 65 29.2 40.0 73 31-111 12 30 2,4-Dinitrophenol 27.0 40.0 67 29.0 40.0 72 22-113 7 30 2,4-Dinitrotoluene 30.4 40.0 76 33.4 40.0 83 49-117 9 30 2,6-Dinitrotoluene 30.1 40.0 75 32.9 40.0 82 47-120 9 30 2-Chloronaphthalene 24.8 40.0 62 28.3 40.0 71 30-115 13 30 2-Chlorophenol 24.4 40.0 61 28.1 40.0 70 25-110 14 30 2-Methylnaphthalene 26.3 40.0 66 29.9 40.0 75 29-110 13 30 2-Methylphenol 25.9 40.0 65 28.8 40.0 72 29-112 10 30 2-Nitroaniline 31.3 40.0 78 34.6 40.0 86 38-145 10 30 2-Nitrophenol 26.0 40.0 65 30.0 40.0 75 24-119 14 30 3- and 4-Methylphenol Coelution 26.0 40.0 65 28.8 40.0 72 29-110 10 30 3,3'-Dichlorobenzidine 36.0 40.0 90 39.0 40.0 98 43-150 8 30 3-Nitroaniline 31.5 40.0 79 34.5 40.0 86 55-128 9 30 4,6-Dinitro-2-methylphenol 31.2 40.0 78 34.0 40.0 85 26-115 8 30 4-Bromophenyl Phenyl Ether 26.8 40.0 67 30.4 40.0 76 49-115 13 30 4-Chloro-3-methylphenol 29.4 40.0 74 31.9 40.0 80 45-113 8 30 4-Chloroaniline 29.9 40.0 75 34.7 40.0 87 33-122 15 30 4-Chlorophenyl Phenyl Ether 27.2 40.0 68 29.7 40.0 74 42-115 9 30 4-Nitroaniline 31.3 40.0 78 34.7 40.0 87 52-128 11 30 4-Nitrophenol 16.01 40.0 40 17.61 40.0 44 15-85 9 30 Acenaphthene 27.0 40.0 67 30.4 40.0 76 32-112 12 30 Acenaphthylene 27.3 40.0 68 30.5 40.0 76 33-115 11 30 Acetophenone 27.0 40.0 68 31.0 40.0 77 30-115 14 30 Anthracene 31.3 40.0 78 34.1 40.0 85 54-114 9 30 Benz(a)anthracene 32.9 40.0 82 35.5 40.0 89 54-120 8 30 Benzo(a)pyrene 31.0 40.0 78 34.7 40.0 87 48-125 11 30 Benzo(b)fluoranthene 29.6 40.0 74 32.5 40.0 81 50-125 9 30 Benzo(g,h,i)perylene 30.3 40.0 76 33.9 40.0 85 50-125 11 30 Benzo(k)fluoranthene 31.7 40.0 79 34.9 40.0 87 45-120 10 30 Benzyl Alcohol 24.9 40.0 62 28.3 40.0 71 25-111 13 30 Bis(2-chloroethoxy)methane 25.7 40.0 64 29.1 40.0 73 28-116 13 30 Bis(2-chloroethyl) Ether 24.7 40.0 62 28.3 40.0 71 26-114 14 30 Bis(2-chloroisopropyl) Ether 35.2 40.0 88 40.1 40.0 100 26-130 13 30 Printed 2/5/2018 3:02:52 PM Superset Reference:18-0000453045 rev 00 Page 164 of 184 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Analyzed: 01/30/18 Sample Matrix: Water Date Extracted: 01/30/18 Duplicate Lab Control Sample Summary Semivolatile Organic Compounds by GC/MS Analysis Method: 8270C Units: ug/L Prep Method: EPA 3510C Basis: NA Analysis Lot: 578811 Lab Control Sample Duplicate Lab Control Sample JQ1800741-02 JQ1800741-03 Spike Spike % Rec RPD Analyte Name Result Amount % Rec Result Amount % Rec Limits RPD Limit Bis(2-ethylhexyl) Phthalate 35.8 40.0 89 39.2 40.0 98 48-125 9 30 Butyl Benzyl Phthalate 36.5 40.0 91 39.4 40.0 98 50-128 8 30 Carbazole 31.9 40.0 80 34.4 40.0 86 53-117 8 30 Chrysene 32.6 40.0 81 35.1 40.0 88 51-120 7 30 Dibenz(a,h)anthracene 30.3 40.0 76 33.6 40.0 84 50-125 10 30 Dibenzofuran 26.8 40.0 67 30.0 40.0 75 38-115 11 30 Diethyl Phthalate 29.8 40.0 75 32.3 40.0 81 52-120 8 30 Dimethyl Phthalate 28.9 40.0 72 31.4 40.0 79 47-120 8 30 Di-n-butyl Phthalate 33.0 40.0 83 35.7 40.0 89 54-121 8 30 Di-n-octyl Phthalate 32.0 40.0 80 35.1 40.0 88 46-117 9 30 Diphenylamine + n- 29.0 40.0 72 31.6 40.0 79 51-120 9 30 Nitrosodiphenylamine Fluoranthene 31.1 40.0 78 33.6 40.0 84 56-120 8 30 Fluorene 28.2 40.0 71 31.0 40.0 78 42-115 10 30 Hexachlorobenzene 26.6 40.0 66 29.6 40.0 74 50-117 11 30 Hexachlorobutadiene 23.6 40.0 59 26.8 40.0 67 25-110 13 30 Hexachlorocyclopentadiene 46.3 40.0 116 53.2 40.0 133 * 22-126 14 30 Hexachloroethane 24.6 40.0 62 29.0 40.0 72 21-115 16 30 Indeno(1,2,3-cd)pyrene 30.3 40.0 76 33.5 40.0 84 49-125 10 30 Isophorone 27.7 40.0 69 30.9 40.0 77 31-120 11 30 Naphthalene 26.1 40.0 65 30.0 40.0 75 33-115 14 30 Nitrobenzene 25.7 40.0 64 29.8 40.0 75 25-118 15 30 N-Nitrosodi-n-propylamine 27.5 40.0 69 30.9 40.0 77 30-123 12 30 Pentachlorophenol (PCP) 21.9 40.0 55 23.4 40.0 59 36-110 7 30 Phenanthrene 30.7 40.0 77 33.2 40.0 83 52-117 8 30 Phenol 2.781 40.0 7 * 3.34I 40.0 8 * 13-90 18 30 Pyrene 32.3 40.0 81 35.1 40.0 88 50-121 8 30 Printed 2/5/2018 3:02:52 PM Superset Reference:18-0000453045 rev 00 Page 165 of 184 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Sample Matrix: Water SURROGATE RECOVERY SUMMARY Base Neutral Semivolatile Organic Compounds by GC/MS SIM Analysis Method: 8270D SIM Extraction Method: EPA 3510C Sample Name Lab Code 2-Fluorobiphenyl 22 -105 p-Terphenyl-04 25 -127 TW-1 J1800711-011 60 116 TW-3 J1800711-012 52 118 TW-2 J1800711-013 33 88 TW-4 J1800711-014 59 104 TW-5 J1800711-015 49 93 Method Blank JQ1800740-01 5 * 105 Printed 2/5/2018 3:02:59 PM Page 166 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Analysis Method: Prep Method: Terracon Environmental WWAY Building/ES187011 Water Method Blank JQ1800740-01 8270D SIM EPA 3510C Service Request: J1800711 Date Collected: NA Date Received: NA Base Neutral Semivolatile Organic Compounds by GC/MS SIM Units: ug/L Basis: NA Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q 1-Methylnaphthalene 0.0440 U 0.100 0.0440 1 01/29/18 19:10 1/29/18 2-Methylnaphthalene 0.0440 U 0.100 0.0440 1 01/29/18 19:10 1/29/18 Acenaphthene 0.0410 U 0.100 0.0410 1 01/29/18 19:10 1/29/18 Acenaphthylene 0.0250 U 0.100 0.0250 1 01/29/18 19:10 1/29/18 Anthracene 0.0380 U 0.100 0.0380 1 01/29/18 19:10 1/29/18 Benz(a)anthracene 0.0350 U 0.100 0.0350 1 01/29/18 19:10 1/29/18 Benzo(a)pyrene 0.0310 U 0.100 0.0310 1 01/29/18 19:10 1/29/18 Benzo(b)fluoranthene 0.0250 U 0.100 0.0250 1 01/29/18 19:10 1/29/18 Benzo(g,h,i)perylene 0.0390 U 0.100 0.0390 1 01/29/18 19:10 1/29/18 Benzo(k)fluoranthene 0.0350 U 0.100 0.0350 1 01/29/18 19:10 1/29/18 Chrysene 0.0240 U 0.100 0.0240 1 01/29/18 19:10 1/29/18 Dibenz(a,h)anthracene 0.0360 U 0.100 0.0360 1 01/29/18 19:10 1/29/18 Fluoranthene 0.0390 U 0.100 0.0390 1 01/29/18 19:10 1/29/18 Fluorene 0.0470 U 0.100 0.0470 1 01/29/18 19:10 1/29/18 Indeno(1,2,3-cd)pyrene 0.0400 U 0.100 0.0400 1 01/29/18 19:10 1/29/18 Phenanthrene 0.0350 U 0.100 0.0350 1 01/29/18 19:10 1/29/18 Pyrene 0.0310 U 0.100 0.0310 1 01/29/18 19:10 1/29/18 Surrogate Name % Rec Control Limits Date Analyzed Q 2-Fluorobiphenyl 5 * 22 - 105 01/29/18 19:10 p-Terphenyl-dl4 105 25 - 127 01/29/18 19:10 Printed 2/5/2018 3:02:58 PM Page 167 of 184 Superset Reference:18-0000453045 rev 00 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 168 of 184 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Matrix: Soil SURROGATE RECOVERY SUMMARY Polychlorinated Biphenyls (PCBs) by GC Analysis Method: 8082 Extraction Method: EPA 3546 Service Request: J1800711 Sample Name Lab Code Decachlorobiphenyl 10 -155 SB-1-1 J1800711-001 70 SB-1-17 J1800711-002 70 SB-2-1 J1800711-003 80 SB-2-12 J1800711-004 80 SB-3-1 J1800711-005 70 SB-3-14 J1800711-006 80 Method Blank JQ1800725-01 100 Lab Control Sample JQ1800725-02 100 SB-1-1 JQ1800725-03 80 SB-1-1 JQ1800725-04 80 Printed 2/5/2018 3:03:06 PM Page 169 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba AILS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: 01/23/18 Sample Matrix: Soil Date Received: 01/27/18 Date Analyzed: 01/30/18 Date Extracted: 01/30/18 Duplicate Matrix Spike Summary Polychlorinated Biphenyls (PCBs) by GC Sample Name: SB-1-1 Units: ug/Kg Lab Code: J1800711-001 Basis: Dry Analysis Method: 8082 Prep Method: EPA 3546 Matrix Spike Duplicate Matrix Spike JQ1800725-03 JQ1800725-04 Sample Spike Spike % Rec RPD Analyte Name Result Result Amount % Rec Result Amount % Rec Limits RPD Limit Aroclor 1016 9.83 U 363 361 101 330 365 91 38-150 10 30 Aroclor 1260 10.1 U 334 361 93 312 365 85 29-150 7 30 Results flagged with an asterisk (*) indicate values outside control criteria. Results flagged with a pound (#) indicate the control criteria is not applicable. Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded. Printed 2/5/2018 3:03:06 PM Page 170 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Collected: NA Sample Matrix: Soil Date Received: NA Sample Name: Method Blank Units: ug/Kg Lab Code: JQ1800725-01 Basis: Dry Polychlorinated Biphenyls (PCBs) by GC Analysis Method: 8082 Prep Method: EPA 3546 Analyte Name Result PQL MDL Dil. Date Analyzed Date Extracted Q Aroclor 1016 9.06 U 33.0 9.06 1 01/30/18 16:45 1/30/18 Aroclor 1221 6.68 U 33.0 6.68 1 01/30/18 16:45 1/30/18 Aroclor 1232 21.6 U 33.0 21.6 1 01/30/18 16:45 1/30/18 Aroclor 1242 8.89 U 33.0 8.89 1 01/30/18 16:45 1/30/18 Aroclor 1248 16.1 U 33.0 16.1 1 01/30/18 16:45 1/30/18 Aroclor 1254 12.2 U 33.0 12.2 1 01/30/18 16:45 1/30/18 Aroclor 1260 9.30 U 33.0 9.30 1 01/30/18 16:45 1/30/18 Surrogate Name % Rec Control Limits Date Analyzed Q Decachlorobiphenyl 100 10 - 155 01/30/18 16:45 Printed 2/5/2018 3:03:05 PM Page 171 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800711 Project: WWAY Building/ES187011 Date Analyzed: 01/30/18 Sample Matrix: Soil Date Extracted: 01/30/18 Lab Control Sample Summary Polychlorinated Biphenyls (PCBs) by GC Analysis Method: 8082 Prep Method: EPA 3546 Lab Control Sample JQ1800725-02 Units: ug/Kg Basis: Dry Analysis Lot: 578693 Analyte Name Result Spike Amount % Rec % Rec Limits Aroclor 1016 359 333 108 38-150 Aroclor 1260 330 333 99 29-150 Printed 2/5/2018 3:03:06 PM Page 172 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Confirmation Results Client: Terracon Environmental Project: WWAY Building/ES187011 SRM Matrix: Soil Sample Name: Lab Control Sample Lab Code: JQ1800725-02 Polychlorinated Biphenyls (PCBs) by GC Analytical Method: 8082 Prep Method: EPA 3546 Service Request: J1800711 Date Collected: NA Date Received: Units: ug/Kg Basis: Dry Primary Confirmation Dilution MDL Result Result RPD Q Factor Date Analyzed Aroclor 1016 9.06 359 366 2 1 01/30/18 16:57 Aroclor 1260 9.30 330 332 <1 1 01/30/18 16:57 Printed 2/5/2018 3:03:07 PM Superset Reference:18-0000453045 rev 00 Page 173 of 184 ALS Group USA, Corp. dba ALS Environmental Confirmation Results Client: Terracon Environmental Project: WWAY Building/ES187011 SRM Matrix: Soil Sample Name: S13-1-1 Lab Code: JQ1800725-03 Polychlorinated Biphenyls (PCBs) by GC Analytical Method: 8082 Prep Method: EPA 3546 Service Request: J1800711 Date Collected: 01/23/18 08:50 Date Received: 1/27/18 Units: ug/Kg Basis: Dry Percent Solids: 90.9 Primary Confirmation Dilution MDL Result Result RPD Q Factor Date Analyzed Aroclor 1016 9.83 363 370 2 1 01/30/18 17:21 Aroclor 1260 10.1 334 303 10 1 01/30/18 17:21 Printed 2/5/2018 3:03:07 PM Superset Reference:18-0000453045 rev 00 Page 174 of 184 ALS Group USA, Corp. dba ALS Environmental Confirmation Results Client: Terracon Environmental Project: WWAY Building/ES187011 SRM Matrix: Soil Sample Name: S13-1-1 Lab Code: JQ1800725-04 Polychlorinated Biphenyls (PCBs) by GC Analytical Method: 8082 Prep Method: EPA 3546 Service Request: J1800711 Date Collected: 01/23/18 08:50 Date Received: 1/27/18 Units: ug/Kg Basis: Dry Percent Solids: 90.9 Primary Confirmation Dilution MDL Result Result RPD Q Factor Date Analyzed Aroclor 1016 9.91 330 348 5 1 01/30/18 17:34 Aroclor 1260 10.2 312 299 4 1 01/30/18 17:34 Printed 2/5/2018 3:03:07 PM Superset Reference:18-0000453045 rev 00 Page 175 of 184 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 176 of 184 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Soil Method Blank J 1800711-MB 1 Inorganic Parameters Service Request: J1800711 Date Collected: NA Date Received: NA Basis: Dry Analysis Analyte Name Method Result Units PQL MDL Dfl. Date Analyzed Date Extracted Q Arsenic, Total 6010D 0.07 U mg/Kg 0.50 0.07 1 02/01/18 20:52 02/01/18 Barium, Total 6010D 0.02 U mg/Kg 0.50 0.02 1 02/01/18 20:52 02/01/18 Cadmium, Total 6010D 0.02 U mg/Kg 0.25 0.02 1 02/01/18 20:52 02/01/18 Chromium, Total 6010D 0.04 U mg/Kg 0.50 0.04 1 02/01/18 20:52 02/01/18 Lead, Total 6010D 0.04 U mg/Kg 0.50 0.04 1 02/01/18 20:52 02/01/18 Mercury, Total 7471B 0.0025 I mg/Kg 0.0067 0.0005 1 01/30/18 14:11 01/29/18 Selenium, Total 6010D 0.14 U mg/Kg 0.50 0.14 1 02/01/18 20:52 02/01/18 Silver, Total 6010D 0.05 I mg/Kg 0.50 0.04 1 02/01/18 20:52 02/01/18 Printed 2/5/2018 3:03:10 PM Page 177 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Project: Sample Matrix: Sample Name: Lab Code: Terracon Environmental WWAY Building/ES187011 Water Method Blank J 1800711-MB2 Inorganic Parameters Service Request: J1800711 Date Collected: NA Date Received: NA Basis: NA Analysis Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Date Extracted Q Arsenic, Total 6010D 2 U ug/L 10 2 1 01/29/18 20:16 01/29/18 Barium, Total 6010D 0.3 U ug/L 10 0.3 1 01/29/18 20:16 01/29/18 Cadmium, Total 6010D 0.2 U ug/L 5.0 0.2 1 01/29/18 20:16 01/29/18 Chromium, Total 6010D 0.4 U ug/L 10 0.4 1 01/29/18 20:16 01/29/18 Lead, Total 6010D 2 U ug/L 10 2 1 01/29/18 20:16 01/29/18 Mercury, Total 7470A 0.05 U ug/L 0.10 0.05 1 01/30/18 13:41 01/29/18 Selenium, Total 6010D 3 U ug/L 10 3 1 01/29/18 20:16 01/29/18 Silver, Total 6010D 0.6 U ug/L 10 0.6 1 01/29/18 20:16 01/29/18 Printed 2/5/2018 3:03:10 PM Page 178 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba AILS Environmental Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Matrix: Soil QA/QC Report Duplicate Matrix Spike Summary Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 Date Received: 01/27/18 Date Analyzed: 02/1/18 Date Extracted: 02/1/18 Sample Name: SB-1-17 Units: mg/Kg Lab Code: J1800711-002 Basis: Dry Analysis Method: 6010D Prep Method: EPA 3050B Matrix Spike Duplicate Matrix Spike J 1800711-002MS J 1800711-002DMS Sample Spike Spike % Rec RPD Analyte Name Result Result Amount % Rec Result Amount % Rec Limits RPD Limit Arsenic, Total 0.88 19.1 17.7 103 20.7 19.7 101 75-125 8 20 Barium, Total 12.6 33.0 17.7 116 34.3 19.7 110 75-125 4 20 Cadmium, Total 0.02 U 9.22 8.83 104 10.3 9.86 104 75-125 11 20 Chromium, Total 1.95 21.5 17.7 ill 23.6 19.7 110 75-125 9 20 Lead, Total 64.1 81.3 17.7 97 75.5 19.7 58 * 75-125 7 20 Selenium, Total 0.14 U 18.8 17.7 106 20.8 19.7 106 75-125 10 20 Silver, Total 0.04 U 18.2 17.7 103 20.2 19.7 102 75-125 10 20 Results flagged with an asterisk (*) indicate values outside control criteria. Results flagged with a pound (#) indicate the control criteria is not applicable. Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded. Printed 2/5/2018 3:03:08 PM Page 179 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba AILS Environmental Client: Terracon Environmental Project: WWAY Building/ES187011 Sample Matrix: Soil QA/QC Report Duplicate Matrix Spike Summary Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 Date Received: 01/27/18 Date Analyzed: 01/30/18 Date Extracted: 01/29/18 Sample Name: SB-3-14 Units: mg/Kg Lab Code: J1800711-006 Basis: Dry Analysis Method: 7471B Prep Method: Method Matrix Spike Duplicate Matrix Spike J 1800711-006MS J 1800711-006DMS Sample Spike Spike % Rec RPD Analyte Name Result Result Amount % Rec Result Amount % Rec Limits RPD Limit Mercury, Total 0.0090 0.101 0.0856 107 0.0978 0.0849 105 75-125 3 20 Results flagged with an asterisk (*) indicate values outside control criteria. Results flagged with a pound (#) indicate the control criteria is not applicable. Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded. Printed 2/5/2018 3:03:10 PM Page 180 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Project: Sample Matrix: Terracon Environmental WWAY Building/ES187011 Soil Lab Control Sample Summary Inorganic Parameters Lab Control Sample J 1800711-LCS 1 Service Request: J1800711 Date Analyzed: 01/30/18 - 02/01/18 Units:mg/Kg Basis:Dry Analyte Name Analytical Method Result Spike Amount % Rec % Rec Limits Arsenic, Total 6010D 24.9 25.0 100 80-120 Barium, Total 6010D 25.7 25.0 103 80-120 Cadmium, Total 6010D 12.6 12.5 100 80-120 Chromium, Total 6010D 26.1 25.0 104 80-120 Lead, Total 6010D 25.7 25.0 103 80-120 Mercury, Total 7471B 0.0900 0.0833 108 80-120 Selenium, Total 6010D 25.4 25.0 101 80-120 Silver, Total 6010D 25.0 25.0 100 80-120 Printed 2/5/2018 3:03:10 PM Page 181 of 184 Superset Reference:18-0000453045 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Project: Sample Matrix: Terracon Environmental WWAY Building/ES187011 Water Lab Control Sample Summary Inorganic Parameters Lab Control Sample J 1800711-LCS2 Service Request: J1800711 Date Analyzed: 01/29/18 - 01/30/18 Units:ug/L Basis:NA Analyte Name Analytical Method Result Spike Amount % Rec % Rec Limits Arsenic, Total 6010D 505 500 101 80-120 Barium, Total 6010D 504 500 101 80-120 Cadmium, Total 6010D 257 250 103 80-120 Chromium, Total 6010D 513 500 103 80-120 Lead, Total 6010D 516 500 103 80-120 Mercury, Total 7470A 1.23 1.25 98 80-120 Selenium, Total 6010D 534 500 107 80-120 Silver, Total 6010D 513 500 103 80-120 Printed 2/5/2018 3:03:10 PM Page 182 of 184 Superset Reference:18-0000453045 rev 00 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 183 of 184 ALS Group USA, Corp. dba ALS Environmental Client: Terracon Environmental Project WWAY Building/ES187011 Sample Matrix: Soil QA/QC Report Replicate Sample Summary Inorganic Parameters Service Request: J1800711 Date Collected: 01/23/18 Date Received: 01/27/18 Date Analyzed: 01/29/18 Sample Name: SB-3-1 Units: Percent Lab Code: J1800711-005 Basis: As Received Duplicate Sample J1800711- Sample 005DUP Analyte Name Analysis Method PQL MDL Result Result Average RPD RPD Limit Solids, Total 160.3 Modified - - 85.2 84.9 85.1 <1 10 Results flagged with an asterisk (*) indicate values outside control criteria. Results flagged with a pound (#) indicate the control criteria is not applicable. Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded. Printed 2/5/2018 3:03:12 PM Page 184 of 184 Superset Reference:18-0000453045 rev 00 A February 09, 2018 Justin Johnson Terracon Environmental 2201 Rowland Avenue Savannah, GA 31404 Laboratory Results for: WWAY Building Dear Justin, Service Request No:J1800891 Enclosed are the results of the sample(s) submitted to our laboratory January 27, 2018 For your reference, these analyses have been assigned our service request numberJ1800891. All analyses were performed according to our laboratory's quality assurance program. The test results meet requirements of the NELAP standards except as noted in the case narrative report. All results are intended to be considered in their entirety, and ALS Environmental is not responsible for use of less than the complete report. Results apply only to the items submitted to the laboratory for analysis and individual items (samples) analyzed, as listed in the report. In accordance to the NELAC 2003 Standard, a statement on the estimated uncertainty of measurement of any quantitative analysis will be supplied upon request. Please contact me if you have any questions. My extension is 4410. You may also contact me via email at Jerry.Allen@alsglobal.com. Respectfully submitted, ALS Group USA, Corp. dba ALS Environmental Jerry Allen Project Manager ADDRESS 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 PHONE +1 904 739 2277 FAX +1 904 739 2011 ALS Group USA, Corp. dba ALS Environmental Page 1 of 22 ALS CoverLetter Table of Contents Narrative Documents Narrative Documents Hit Summary List Sample Receipt Information Sample Cross -Reference Chain Of Custody Miscellaneous Forms Qualifiers Acronyms Analyst Summary Sample Results Metals TW-3 - Metals QC Summary Forms Metals ALS Environmental ALS Group USA, Corp 9143 Philips Highway, Suite 200 Jacksonville, FL 32256 T : +1 904 739 2277 F : +1 904 739 2011 www.aisgiobal.com Table of Contents Method Blank - Metals J1800891-001DMS TW-3 - DMS Metals J 1800891-LCS - LCS Metals 1 2 3 4 5 6 7 8 10 11 13 14 15 16 17 18 19 20 21 22 RIGHT SOLUTIONS I RIGHT PARTNER Page 2 of 22 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904) 739-2277 Fax (904) 739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 3 of 22 AllEnuironmentall 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 1904-739-2277 I www.alsglobal.com Client: Terracon Environmental Service Request:J1800891 Project: WWAY Building Sample Matrix: Water CASE NARRATIVE Date Received:1/27/18 All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains analytical results for samples designated for Tier II data deliverables, including results of QC samples analyzed from this delivery group. When appropriate to the procedure, method blank results have been reported with each analytical test. Analytical procedures performed by the lab are validated in accordance with NELAC standards. Parameters that are included in the NELAC Fields of Testing but are not included in the lab's NELAC accreditation are identified in the discussion of each analytical procedure. Sample Receipt Samples were received for analysis at ALS Environmental and were received in good condition and consistent with the accompanying chain of custody form. Samples are refrigerated at <6°C upon receipt at the lab except for aqueous samples designated for metals analyses, which are stored at room temperature. Analyses Notes: No significant data anomalies were noted with this analysis. Approved by Date 2/9/2018 Page 4 of 22 AALSEnuironmental SAMPLE DETECTION SUMMARY LIENT ID: TW-3 Lab ID: J1800891-001 Analyte Arsenic, Dissolved Results Flag MDL PQL Units Method ---- ------------------ 4 IV 1.0 10 ug/L 6010D Page 5 of 22 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904) 739-2277 Fax (904) 739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 6 of 22 Client: Terracon Environmental Project: WWAY Building SAMPLE CROSS-REFERENCE SAMPLE # CLIENT SAMPLE ID J 1800891-001 TW-3 Service Request:J1800891 DATE TIME 1 /24/2018 1310 Printed 2/9/2018 8:09:40 AM Page 7 of 22 Sample Summary C J � � � X N 0 t 3 0 b � j 7 ', >j o j r 0. Q co O O w` Cm Go _ aA =DOA /009 c OAS WS (IOLZR OAS IDOLZ8 ¢ oo It n r.. E ,, o 41 /91LbL v ry oo cd .1 0 p f�. C4 ❑ ❑ � W � 4 �i. '"'� i-+ I :-: �w�. ; rn : i-r �I � I � I � � �r � i-�s : I--i �I i--� : w I .+r ; �s t Q, Ofj i rw .w : - �--� sn • I.r : nr rK r+ r..r rr : �--i o Q a a a I. SIBIO i /Q0109 T219TON F091 a� L........_..,_ E 'o la In :c LLo :.n Jo yo n ;Mo �N a •M �� ,N :N .,n •N Uj .... O •O _V W 'W 'W •oa �W �OO �00 �00 'GO '00 '00 'W '00 'oC APO V N �N ��N •N ��N •N 'N ��N ;�I �N ��N �N ��N �N �N I�o ,V) �IJo (o :Vo n ,�o : o :Ll o j coo V I I O ❑ E' E" j c �d�a-71 �� E CC E Xt W O �:CD:lo Ic Slo lo Llon w O M ;T N M � �n 0o;FF�r m 7, 7- o o cp L 2*�_ U _ UG] ��-+ e6 i [� : M1 : [� : n : n [� C p;ola :C� � O O O y � � � � � co •oc �co Ica •oo �oo :oc goo �� Boa •w Boa goo �co Boa �� ^-� � � Page 4of� = •— .� H V P. Z L 0 0 3 o �L�� v, q o .n N w S] Sri A y '.. O O N .� Q7 +A :0 I Ir Q v m M J o. 4! i N 4 N V LU N N ffi N v Ln LU � u � N c° ��_ JE m U Q U w z z p O fled o sl eL 3l7b 8xxx !� b IDI OZZR IDl- o9Z8 w u LL u + siauieauoD jo'ON y y u-77 u 4 V� U U U u a+ c ` w Q U � w Q o U U} � to C m � m a ¢ <a2 _.' tD no L a v z z z o CL a a� a F- v. 1 N j� < Q Z z :. W z Q ¢ J C CD } r R q p C -. Ln L U § xf C xu "7 D O C O O C (Z c Q �0 CG d N .' U., w w w m d a v u y . ro y .. M m a a+ kA 4 n �: v ai a�i N a y ?° i N o - p ro Otn � v C) O cL u¢ V w n. a s ci Ln t- aavr a V n a e 1901 164 Q �- IIQ Page 9 of 22 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904) 739-2277 Fax (904) 739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 10 of 22 Alffi-PlAronmerpt-al FLORIDA DEP DATA QUALIFIERS B Results based upon colony counts outside the acceptable range. D Measurement was made in the field. H Value based on field kit determination; results may not be accurate. I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. J Estimated value (one of the following reasons is discussed in the project case narrative). 1. The result may be inaccurate because the surrogate recovery limits have been exceeded. 2. No known quality control criteria exists for the component. 3. The reported value failed to meet the established quality control criteria for either precision or accuracy. 4. The sample matrix interfered with the ability to make any accurate determination (e.g., primary and confirmation results show greater than 40% RPD). 5. The data is questionable because of improper laboratory or field protocols (e.g., GUMS Tune did not meet method criteria). K Off scale low. The value is less than the lowest calibration standard but greater than the method reporting limit (MRL). L Off scale high. The analyte is above the upper limit of the linear calibration range. M The MDL/MRL has been elevated because the analyte could not be accurately quantified due to matrix interference. N Presumptive evidence of the analyte. Confirmation was not performed. Q Sample held beyond the accepted holding time. T Value reported is less than the laboratory method detection limit. The value is reported for informational purposes only. U Indicates that the compound was analyzed for but not detected. V Indicates that the analyte was detected in both the sample and the associated method blank. Y The laboratory analysis was from an improperly preserved sample. Z Too many colonies were present (TNTC). The numeric value represents the filtration volume. Page 11 of 22 Alffi-pailronment-al Jacksonville Lab ID # for State Certifications' Agency Number Expiration Date Department of Defense 66206 7/31/2018 Florida Department of Health E82502 6/30/2018 Georgia Department of Natural 958 6/30/2018 Resources Kentucky Division of Waste 123042 6/30/2018 Management Louisiana Department of 02086 6/30/2018 Environmental Quality Maine Department of Health and 2015002 2/3/2019 Human Services North Carolina Department of 527 12/31/2018 Environment and Natural Resources Pennsylvania Department of 68-04835 8/31/2018 Environmental Protection South Carolina Department of Health 96021001 6/30/2018 and Environmental Control Texas Commission on Environmental T104704197-16-8 5/31/2018 Quality Virginia Environmental Accreditation 460191 12/14/2018 Program Analyses were performed according to our laboratory's NELAP-approved quality assurance program and any applicable state or agency requirements. The test results meet requirements of the current NELAP/'INI standards or state or agency requirements, where applicable, except as noted in the laboratory case narrative provided. For a specific list of accredited analytes, refer to htt 2://www.aisglobal.com/en/Our-Services/Life-Sciences/Environmental/Downloads/North-America- Downloads Page 12 of 22 Aunvoironment-al ASTM American Society for Testing and Materials A2LA American Association for Laboratory Accreditation CARB California Air Resources Board CAS Number Chemical Abstract Service registry Number CFC Chlorofluorocarbon CFU Colony -Forming Unit DEC Department of Environmental Conservation DEQ Department of Environmental Quality DHS Department of Health Services DOE Department of Ecology DOH Department of Health EPA U. S. Environmental Protection Agency ELAP Environmental Laboratory Accreditation Program GC Gas Chromatography GC/MS Gas Chromatography/Mass Spectrometry LUFT Leaking Underground Fuel Tank M Modified MCL Maximum Contaminant Level is the highest permissible concentration of a substance allowed in drinking water as established by the USEPA. MDL Method Detection Limit MPN Most Probable Number MRL Method Reporting Limit NA Not Applicable NC Not Calculated NCASI National Council of the Paper Industry for Air and Stream Improvement ND Not Detected NIOSH National Institute for Occupational Safety and Health PQL Practical Quantitation Limit RCRA Resource Conservation and Recovery Act SIM Selected Ion Monitoring TPH Total Petroleum Hydrocarbons tr Trace level is the concentration of an analyte that is less than the PQL but greater than or equal to the MDL. Page 13 of 22 ALS Group USA, Corp. dba ALS Environmental Analyst Summary report Client: Terracon Environmental Service Request: J1800891 Project: WWAY Building Sample Name: TW-3 Date Collected: 01/24/18 Lab Code: J1800891-001 Date Received: 01/27/18 Sample Matrix: Water Analysis Method Extracted/Digested By Analyzed By 6010D EGARDNER EGARDNER Printed 2/9/2018 8:09:41 AM Superset Reference: 18-0000453991 rev 00 Page 14 of 22 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904) 739-2277 Fax (904) 739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 15 of 22 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 16 of 22 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Project: WWAY Building Sample Matrix: Water Sample Name: TW-3 Lab Code: J1800891-001 Inorganic Parameters Service Request: J1800891 Date Collected: 01/24/18 13:10 Date Received: 01/27/18 08:50 Basis: NA Analysis Date Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Extracted Q Arsenic, Dissolved 6010D 4 IV ug/L 10 1.0 1 02/07/18 17:52 02/07/18 Chromium, Dissolved 6010D 0.4 U ug/L 10 0.4 1 02/07/18 17:52 02/07/18 Lead, Dissolved 6010D 3 U ug/L 10 3 1 02/07/18 17:52 02/07/18 Printed 2/9/2018 8:09:42 AM Page 17 of 22 Superset Reference:18-0000453991 rev 00 ALS Environmental ALS Environmental -Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904) 739-2277 Fax (904) 739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 18 of 22 ALS Environmental ALS Environmental —Jacksonville Laboratory 9143 Philips Highway, Suite 200, Jacksonville, FL 32256 Phone (904)739-2277 Fax (904)739-201 1 www.alsglobal.com RIGHT SOLUTIONS I RIGHT PARTNER Page 19 of 22 ALS Group USA, Corp. dba ALS Environmental Analytical Report Client: Terracon Environmental Project: WWAY Building Sample Matrix: Water Sample Name: Method Blank Lab Code: J1800891-MB Inorganic Parameters Service Request: J1800891 Date Collected: NA Date Received: NA Basis: NA Analysis Date Analyte Name Method Result Units PQL MDL Dil. Date Analyzed Extracted Q Arsenic, Dissolved 6010D 2 I ug/L 10 1.0 1 02/07/18 17:37 02/07/18 Chromium, Dissolved 6010D 0.4 U ug/L 10 0.4 1 02/07/18 17:37 02/07/18 Lead, Dissolved 6010D 3 U ug/L 10 3 1 02/07/18 17:37 02/07/18 Printed 2/9/2018 8:09:42 AM Page 20 of 22 Superset Reference:18-0000453991 rev 00 ALS Group USA, Corp. dba AILS Environmental Client: Terracon Environmental Project: WWAY Building Sample Matrix: Water QA/QC Report Duplicate Matrix Spike Summary Inorganic Parameters Service Request: J1800891 Date Collected: 01/24/18 Date Received: 01/27/18 Date Analyzed: 02/7/18 Date Extracted: 02/7/18 Sample Name: TW-3 Units: ug/L Lab Code: J1800891-001 Basis: NA Analysis Method: 6010D Prep Method: EPA 3005A Matrix Spike Duplicate Matrix Spike J 1800891-001 MS J 1800891-001 DMS Sample Spike Spike % Rec RPD Analyte Name Result Result Amount % Rec Result Amount % Rec Limits RPD Limit Arsenic, Dissolved 4 IV 493 500 98 505 500 100 75-125 2 20 Chromium, Dissolved 0.4 U 495 500 99 502 500 100 75-125 1 20 Lead, Dissolved 3 U 475 500 95 489 500 98 75-125 3 20 Results flagged with an asterisk (*) indicate values outside control criteria. Results flagged with a pound (#) indicate the control criteria is not applicable. Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded. Printed 2/9/2018 8:09:42 AM Page 21 of 22 Superset Reference:18-0000453991 rev 00 ALS Group USA, Corp. dba ALS Environmental QA/QC Report Client: Terracon Environmental Service Request: J1800891 Project: WWAY Building Date Analyzed: 02/07/18 Sample Matrix: Water Date Extracted: 02/07/18 Lab Control Sample Summary Inorganic Parameters Analysis Method: 601 OD Prep Method: EPA 3005A Lab Control Sample J1800891-LCS Units: ug/L Basis: NA Analysis Lot: 579478 Analyte Name Result Spike Amount % Rec % Rec Limits Arsenic, Dissolved 492 500 98 80-120 Chromium, Dissolved 507 500 101 80-120 Lead, Dissolved 500 500 100 80-120 Printed 2/9/2018 8:09:42 AM Page 22 of 22 Superset Reference: 18-000045 3991 rev 00