24054_AJACC Auto_Verbena Soil Excavation Letter Report_20210512

Assess. Manage. Consult.
A Minority-Owned Business

May 10, 2021

NCDEQ – Brownfields Program
610 E. Center Avenue
Suite 301
Mooresville, NC 28115

Attn: Mr. Peter Dorn

Re: Brownfield Assessment Report
Verbena Street Assemblage (AJACC Auto Brownfields Project)
Brownfields Project Number: 24054-20-060
301 Verbena Street
Charlotte, Mecklenburg County, North Carolina 28203
F&R Project No. 59Z-0029

Dear Mr. Dorn:

As previously discussed, Froehling & Robertson, Inc., (F&R) has completed soil excavation on behalf of the
current property owner/tenant with confirmatory soil sampling at the above referenced Property in order
to address an apparent oil spill. The spill was identified during the recent Brownfields Assessment at the
Property on April 14, 2021, at which time you were notified. This letter report briefly summarizes the soil
excavation and confirmatory soil sampling.

PROPERTY DESCRIPTION AND BACKGROUND

According to the Mecklenburg County GIS, the Property consists of thirteen contiguous, irregular-shaped
parcels totaling 4.985 acres and the land underlying the current Macie Street public right-of-way consisting
of approximately 0.3 acres, which collectively total approximately 5.29 acres. The Property is located
between Yeoman Road and Verbena Street, in Charlotte, Mecklenburg County, North Carolina, herein
referred to as the Property. The Property location is shown on Figure 1: Topographic Site Location Map.
For the purposes of this report, the Property has been separated into the Macie Street Parcel, Verbena
Street Tract, and the Yeoman Street Tract.

The Macie Street Parcel consists of one parcel (Parcel Identification Number (PIN) 149-033-05) and is
improved with an approximate 10,200 square-foot (SF) one-story commercial warehouse building built in
1991 and the building operates as Carolina Moldings.

The Verbena Street tract (301 Verbena Street) includes five parcels (PINs 1490-33-09, 149-033-10, 149-033-
11, 149-033-12, and 149-033-13). The tract is improved with an approximate 5,250 SF two-story
commercial warehouse building that was built in 1981 which currently operates as Blankenship Lighting, an

300 Yeoman Street AJACC Auto Soil Excavation
F&R Project No. 59Z-0029 2 May 10, 2021

approximate 3,267 SF two-story building addition that was built in 1985 which is currently used as a storage
building by Sun Stone Marble & Granite; and, an approximate 12,648 SF one-story industrial warehouse
building that was built in 1985 which operates as Sun Stone Marble & Granite.

The Yeoman Street Tract (300, 301, 304, 308, 310, and 321 Yeoman Road) includes seven parcels (PINs 149-
033-01, 149-033-31, 149-033-33, 149-043-34, 149-043-35, 149-043-36, and 149-043-38) and is improved
with various residential and commercial structures. The location of the Property is depicted in the attached
Topographic Property Location Map (Figure 1) and Property Observation Map with Spill Location (Figure 2).

F&R previously conducted a Phase I Environmental Site Assessment (ESA), and Limited Soil, Groundwater
and Soil Gas Assessment which identified potential environmental concerns associated with the Property.
Based on these findings, the Property was submitted to the NCDEQ Brownfields Program. During
implementation of the Brownfields Assessment in accordance with the March 19, 2021 Brownfields Work
Plan, evidence of an oil spill was observed on April 14, 2021 at the AJACC Auto facility that was not present
during the prior assessments. It appeared that it was potentially used oil that was spilled during the
tenant’s recent vacating of the building. F&R collected a soil sample from the impacted soils for
characterization. The results of this sample are (designated ‘Spill’) included on Table 1. The lab report
including this sample is attached, the sample designation is ‘still’ in the laboratory analytical report.

SCOPE OF WORK

Prior to soil excavation and sampling activities, F&R contacted NC One Call to mark public utility locations in
the vicinity of the planned excavation. Following receipt of utility clearance, F&R mobilized to the Property
on April 23, 2021 to oversee excavation of impacted soil. F&R contracted CCI Environmental Services (CCI)
to conduct the soil excavation and disposal activities. F&R notes that no disturbances to subsurface utilities
were apparent during the subsequent excavation activities.

A photo-ionization detector (PID) was utilized to screen soils for excavation. Soils were placed into re-
sealable plastic bags, and field-screened using a photo-ionization detector (PID) for evidence of Volatile
Organic Compounds (VOCs). Soils were excavated until PID readings were consistent with background
levels (0-0.1 parts per million (ppm)). Approximately 22 tons of soil were excavated for disposal. The
excavation measured approximately 35 feet long, by 4 feet wide at the northeast end and 8 feet wide at
the southwest end. The excavation ranged from 5 to 10 inches below ground surface (bgs). F&R notes that
evidence of historic fill material was encountered on the eastern half of the excavation at approximately 8
to 10 inches bgs.

A total of six confirmatory soil samples were collected after soil excavation, two from the base of the
excavation, and one along each sidewall at the base of the sidewall and designated Base-1, Base-2 (listed as
Busy-1 and Busy-2 in the laboratory analytical report), and S-1 through S-4 as shown on Figure 3:
Excavation Limits and Soil Sample Location Map. Photographs are included in Appendix 1. The soils
excavated by CCI were transported by CCI to Alternative Energy Solutions of NC, LLC (AES) in Sanford, North
Carolina, and the disposal manifests are included in Appendix 2.

300 Yeoman Street AJACC Auto Soil Excavation
F&R Project No. 59Z-0029 3 May 10, 2021

LABORATORY RESULTS

The soil samples were analyzed for volatile organic compounds (VOCs), semi-volatile organic compounds
(SVOCs), and RCRA Metals plus hexavalent chromium.

The sample collected from the impacted soil on April 14, 2021, prior to soil excavation, detected multiple
VOCs, SVOCs, and metals above laboratory reporting limits. The compounds detected did not exceed the
North Carolina Residential Maximum Soil Contaminant Concentrations (MSCCs). Arsenic exceeded the
North Carolina Preliminary Soil Remediation Goal (PSRG), but the concentration was consistent with
background levels elsewhere on the Property. Hexavalent Chromium was not detected. The results of this
analysis were not received until after the soil excavation activities were completed. Soil analytical results
have been tabulated, and are presented compared to the MSCCs in the attached Table 1, Summary of Soil
Analytical Results- Pre-Excavation.

The post-excavation soil samples collected on April 23, 2021, detected multiple VOCs, SVOCs, and metals
above laboratory reporting limits. Hexavalent Chromium was not detected. Lead was detected in samples
S-1, S-2, and Base-1 above the MSCC and PSRG of 400 mg/kg. As these levels are higher than the Spill
sample collected directly from the impacted material, they may be indicative of the fill material
encountered in the excavation. Benzo(a)pyrene was detected in sample Base-1 at an estimated
concentration above the PSRG, but did not exceed the MSCC. Hexavalent Chromium was detected in the
post-excavation soil samples at an estimated concentration above the PSRG, but did not exceed the MSCC
Arsenic also exceeded the PSRG, but the concentration was consistent with background levels elsewhere
on the Property. These compounds could also be indicative of the fill material observed rather than the
apparent oil spill. F&R notes that overall, the post excavation concentrations are lower than the sample
collected from the impacted material on April 14, 2021 with the exception of the elevated lead levels. Soil
analytical results have been tabulated, and are presented in the attached Table 2, Summary of Soil
Analytical Results- Post-Excavation. The Sample locations are presented in Figure 3, Excavation Limits and
Soil Sample Location Map.

The complete laboratory results and chain-of-custody are attached to this Report in Appendix 3.

FINDINGS & RECOMMENDATIONS

F&R has performed soil excavation on behalf of the current property owner/tenant with confirmatory soil
sampling at the Property due to an apparent surface oil spill discovered on April 14, 2021, during
Brownfields Assessment activities. Target compounds were not detected above regulatory screening levels.
F&R identified the following conclusions:

 Lead exceeded the Residential MSCC in several samples. The elevated concentrations may also be
indicative of fill material that was observed rather that the apparent oil spill based on the
concentrations of the other target compounds.
 Soil samples collected at the Property and submitted for analysis did not detect other target
compounds above the Residential MSCCs in the pre- or post- excavation sample.
 Arsenic exceeded the PSRG in the samples; however, the concentrations were consistent with
background levels elsewhere on the Property.
 Benzo(a)pyrene and Hexavalent Chromium were detected at estimated concentrations above the

300 Yeoman Street AJACC Auto Soil Excavation
F&R Project No. 59Z-0029 4 May 10, 2021

PSRGs, but did not exceed the MSCCs.
 Overall, the target compounds concentrations in the post-excavation soil samples were generally
lower than the characterization sample collected from the impacted soils with the exception of
lead.

Based on these findings, F&R recommends the following:

 Based on the compounds detected, which may also be indicative of potential fill material observed,
the low concentrations detected, and the consistency of concentrations across the Property,
additional excavation is not recommend, and these residual levels should be managed in conjunction
with the Brownfields activities.
 Based on the excavation of soils associated with the petroleum spill and the analytical results, the
petroleum impacts resulting from this spill appear to have been properly excavated and disposed of.

REPORT LIMITATIONS

These services have been performed under authorization of Greystar Development East, LLC on behalf of
the current property owner/tenant, and for the NCDEQ for specific application on this project. These
services have been performed in accordance with generally accepted environmental practices. No other
warranty, expressed or implied is made. As with any subsurface investigation, actual conditions exist only
at the precise locations from which samples were taken. Certain inferences are based on the results of
sampling and related testing to form a professional opinion of conditions in areas beyond those from which
samples were taken. Our conclusions and recommendations are based upon information provided to us by
others, our sampling and testing results and our Property observations. We have not verified the
completeness or accuracy of the information provided by others, unless otherwise noted. Our
observations are based upon conditions readily visible at the Property at the time of our field visits.

Froehling & Robertson, Inc. by virtue of providing the services described in this report, does not assume the
responsibility of the person(s) in charge of the Property, or otherwise undertake responsibility for reporting
to any local, state or federal public agencies any conditions at the Property that may present a potential
danger to public health, safety or the environment. In areas that require notification of local, state, or
federal public agencies as required by law, it is the Client's responsibility to so notify.

300 Yeoman Street AJACC Auto Soil Excavation
F&R Project No. 59Z-0029 5 May 10, 2021

If you have any questions/comments or require further information, please do not hesitate to contact the
undersigned at [phone].

Sincerely,
FROEHLING & ROBERTSON, INC.

Brian T. Olin, P.G. Alyssa S. Budlong
Lead Environmental Scientist Senior Environmental Professional

Attachments: Figure 1: Topographic Property Location Map
Figure 2: Property Observation Map with Spill Location
Figure 3: Excavation Limits and Soil Sample Location Map

Table 1: Summary of Analytical Results- Pre-Excavation
Table 2: Summary of Analytical Results- Post-Excavation

Appendix 1: Photographic Log
Appendix 2: Soil Disposal Manifests
Appendix 3: Laboratory Results and Chain of Custody

Client:
Project:
Locaon:
Project Number:
Data Source:
Date:
Froehling & Robertson, Inc.
Scale:
FIGURE
No.:
Topographic Site Locaon Map
Greystar Development East, LLC
Verbena Street Assemblage
Verbena and Macie Street, Charlo+e, Mecklenburg County, North Carolina
59Z-0029
USGS 2013
February 23, 2021 NTS
1
3300 Internaonal Airport Drive,
Suite 600
Charloe, North Carolina 28208
Client:
Project:
Locaon:
Project Number:
Data Source:
Date:
Froehling & Robertson, Inc.
Scale:
FIGURE
No.:
Property Observaon Map with Spill Locaon
Greystar Development East, LLC
Verbena Street Assemblage
Verbena and Macie Street, Charlo+e, Mecklenburg County, North Carolina
59Z-0029
Google Earth 2020
May 4, 2021 As Shown
2
3300 Internaonal Airport Drive,
Suite 600
Charloe, North Carolina 28208
Blankenship
Lighng
Sun and Stone
Marble & Granite
Williams
Electric
Carolina Molding
Piedmont
Natural Gas
Piedmont
Natural Gas
S.T. Towing
A.J.A.C.C
Auto
Williams
Electric
&
Landscaper
Abandoned AST
Containers & Compressor
Drums
Tote and
Compressors (2)
Former Underground
Hydraulic Li>
Approximate Locaon of
Monitoring Well MW-7
Approximate Locaon of
Monitoring Well MW-5
Spill
Client:
Project:
Locaon:
Project Number:
Data Source:
Date:
Froehling & Robertson, Inc.
Scale:
FIGURE
No.:
Excavaon Limits and Soil Sample Locaon Map
Greystar Development East, LLC
Verbena Street Assemblage
Verbena and Macie Street, Charlo+e, Mecklenburg County, North Carolina
59Z-0029
Google Earth 2020
May 4, 2021 As Shown
2
3300 Internaonal Airport Drive,
Suite 600
Charloe, North Carolina 28208
Soil Sample
Base-1
Base-2 S-1
S-2
S-3
S-4
Table 1 - Summary of Soil Analytical Results (Pre-Excavation)Verbena Street Assemblage301 Verbena StreetCharlotte, North Carolina 28203 Project No.: 59Z-0029EPA 7471BArsenic Barium Cadmium ChromiumHexavalent ChromiumLead Selenium SilverMercury (Total)Acetonen- Butylbenzenesec- ButylbenzeneEthylbenzene Isopropylbenzene 4-IsopropyltolueneMethyl Ethyl Ketone (MEK)Spill (0.0'-0.2')4/23/20211.05276 0.126 J 18.3 18.3 18.4 2.5 ND ND 0.048 0.011 0.003 J 0.02 0.005 0.002 J 0.018 JNSE 3,100 NSE 23,400 32 400 NSE 78.2 NSE 14,000 782 782 60.3 1,560 1,560 9,3800.68 3,100 NSE 23,000 0.31 400 78 78 2.3 12,000 1,600 1,600 6.1 410 23,300 5,500Concentrations reported in mg/kgBolded results exceed their respective Residential MSCCs or PSRGsCompounds not listed were not detected above the laboratory method detection limits.Chromium was analyzed for total chromium and hexavalent chromium. The standard for trivalent chromium is used for total chromium based on speciated analysis for hexavalent chromium.A complete list of target compounds is provided in the laboratory reportND = Not detected (below method detection limits)J = Estimated resultNSE = No Standard ExistsSample ID (Depth)Date CollectedEPA 6020BEPA 8260DNorth Carolina Residential Soil Cleanup Levels (MSCCs)North Carolina Preliminary Soil Remediation Goals (PSRGs)
Table 1 - Summary of Soil Analytical Results (Pre-Excavation)Verbena Street Assemblage301 Verbena StreetCharlotte, North Carolina 28203 Project No.: 59Z-00294-Methyl-2-PentanoneNapthalenen-PropylbenzeneToluene1,3,5-Trimethylbenzeneo-Xylene m,p-Xylene Total Xylene AnthraceneBenzo(a) pyreneBenzo(g,h,i) peryleneSpill 4/23/2021 0.141 0.113 0.019 0.027 0.005 0.049 0.087 0.137 0.287 J 0.291 J 0.247 J1,250 5.5 1,560 1,250 156 3,120 3,120 3,120 4,600 0.66 4697,000 2 1,250 990 56 140 120 120 3,600 0.11 NSEConcentrations reported in mg/kgBolded results exceed their respective Residential MSCCs or PSRGsCompounds not listed were not detected above the laboratory method detection limits.Chromium was analyzed for total chromium and hexavalent chromium. The standard for trivalent chromium is used for total chromium based on speciated analysis for hexavalent chromium.A complete list of target compounds is provided in the laboratory reportND = Not detected (below method detection limits)J = Estimated resultNSE = No Standard ExistsSample ID (Depth)Date CollectedEPA 8260DEPA Method 8270ENorth Carolina Residential Soil Cleanup Levels (MSCCs)North Carolina Preliminary Soil Remediation Goals (PSRGs)
Table 1 - Summary of Soil Analytical Results (Pre-Excavation)Verbena Street Assemblage301 Verbena StreetCharlotte, North Carolina 28203 Project No.: 59Z-0029Fluoranthane Fluorene 1-Methylnapthalene 2-Methylnaphthalene Naphthalene Phenanthrene PyreneSpill 4/23/2021 0.385 0.211 1.13 J 1.82 J 0.540 J 0.710 J 0.533 J625 625 22.8 62.5 5.5 469 469480 480 18 48 2 NSE 360Concentrations reported in mg/kgBolded results exceed their respective Residential MSCCs or PSRGsCompounds not listed were not detected above the laboratory method detection limits.Chromium was analyzed for total chromium and hexavalent chromium. The standard for trivalent chromium is used for total chromium based on speciated analysis for hexavalent chromium.A complete list of target compounds is provided in the laboratory reportND = Not detected (below method detection limits)J = Estimated resultNSE = No Standard ExistsEPA Method 8270ESample ID (Depth)Date CollectedNorth Carolina Residential Soil Cleanup Levels (MSCCs)North Carolina Preliminary Soil Remediation Goals (PSRGs)
Table 2 - Summary of Soil Analytical Results (Post-Excavation)Verbena Street Assemblage301 Verbena StreetCharlotte, North Carolina 28203 Project No.: 59Z-0029EPA 7471BArsenic Barium Cadmium ChromiumHexavalent ChromiumLead Selenium Silver Mercury (Total) AcetoneMethyl Ethyl Ketone (MEK)S-1 (0.3')4.82214 3.13 62.60.36 J 7313.83 0.168 0.11 0.08 0.009 JS-2 (0.3')4.381,020 1.67 43.10.53 J 7362.24 J 0.724 0.498 0.018 J 0.041 JS-3 (0.4')1.32197 0.266 J 31.10.31 J22 2.93 0.0443 J ND 0.034 0.004 JS-4 (0.6')1.58167 0.356 J 49.7 ND 49.6 2.32 0.0453 J ND 0.028 0.002 JBase-1 (0.4')7.953,110 3.69 59.61.0 BJ 2,0101.95 J 3.86 0.226 0.041 NDBase-2 (0.7')3.12463 0.654 27.30.70 BJ305 1.49 J 1.72 J 0.0624 0.037 0.006NSE 3,100 NSE 23,400 32 400 NSE 78.2 NSE 14,000 9,3800.68 3,100 NSE 23,000 0.31 400 78 78 2.3 12,000 5,500Concentrations reported in mg/kgBolded results exceed their respective Residential MSCC or PSRGCompounds not listed were not detected above the laboratory method detection limits.Chromium was analyzed for total chromium and hexavalent chromium. The standard for trivalent chromium is used for total chromium based on speciated analysis for hexavalent chromium.A complete list of target compounds is provided in the laboratory reportND = Not detected (below method detection limits)J = Detected below the laboratory reporting limitB = Detected in the laboratory method blankNSE = No Standard ExistsEPA 6020BEPA 8260DNorth Carolina Residential Soil Cleanup Levels (MSCCs)North Carolina Preliminary Soil Remediation Goals (PSRGs)Sample ID (Depth)Date Collected4/23/2021
Table 2 - Summary of Soil Analytical Results (Post-Excavation)Verbena Street Assemblage301 Verbena StreetCharlotte, North Carolina 28203 Project No.: 59Z-0029Acenaphthylene AnthraceneBenzo(a) anthraceneBenzo(a) pyreneBenzo(b) fluorantheneBenzo(g,h,i) peryleneBenzo(k) fluorantheneBis(2-ethylhexyl) phthalateS-1 ND 0.021 J 0.062 J 0.085 J 0.152 J 0.107 J ND 7.74S-2 ND ND ND 0.045 J 0.069 J ND 0.02 J NDS-3 ND ND 0.025 J 0.029 J 0.050 J ND 0.022 J NDS-4 ND ND ND ND 0.018 J ND ND NDBase-1 0.033 J 0.073 J 0.345 J0.313 J0.389 J ND 0.113 J NDBase-2 ND ND 0.039 J 0.033 J 0.043 J ND 0.022 J ND930 4,600 6.6 0.66 6.6 469 66 47720 3,600 1.1 0.11 1.1 NSE 11 39Concentrations reported in mg/kgBolded results exceed their respective Residential or Commercial Regulatory StandardCompounds not listed were not detected above the laboratory method detection limits.Chromium was analyzed for total chromium and hexavalent chromium. The standard for trivalent chromium is used for total chromium based on speciated analysis for hexavalent chromium.A complete list of target compounds is provided in the laboratory reportND = Not detected (below method detection limits)J = Detected below the laboratory reporting limitB = Detected in the laboratory method blankNSE = No Standard ExistsNorth Carolina Preliminary Soil Remediation Goals (PSRGs)Sample ID (Depth)Date CollectedNorth Carolina Residential Soil Cleanup Levels (MSCCs)EPA Method 8270EEPA Method 8270E4/23/2021
Table 2 - Summary of Soil Analytical Results (Post-Excavation)Verbena Street Assemblage301 Verbena StreetCharlotte, North Carolina 28203 Project No.: 59Z-0029Chrysene Fluoranthane DibenzofuranIndeno(1,2,3-cd) pyrene1-Methylnapthalene 2-Methylnaphthalene Naphthalene Phenanthrene PyreneS-1 0.076 J 0.084 J ND 0.069 J 0.037 J 0.073 J 0.051 J 0.068 J 0.088 JS-2 0.05 J 0.066 J ND ND 0.026 J 0.036 J 0.029 J ND 0.061 JS-3 0.025 J 0.031 J ND ND ND ND ND ND NDS-4 ND ND ND ND ND ND ND ND NDBusy-1 0.327 J ND 0.033 J 0.171 J 0.047 J 0.065 J 0.088 J 0.275 J 0.491 JBusy-2 0.041 J 0.046 J ND ND 0.019 J 0.022 J 0.020 J 0.035 J ND88 625 62 0.88 22.8 62.5 5.5 469 46911 480 NSE 1.1 18 48 2.1 NSE 360Concentrations reported in mg/kgBolded results exceed their respective Residential or Commercial Regulatory StandardCompounds not listed were not detected above the laboratory method detection limits.Chromium was analyzed for total chromium and hexavalent chromium. The standard for trivalent chromium is used for total chromium based on speciated analysis for hexavalent chromium.A complete list of target compounds is provided in the laboratory reportND = Not detected (below method detection limits)J = Detected below the laboratory reporting limitB = Detected in the laboratory method blankNSE = No Standard ExistsEPA Method 8270ESample ID (Depth)Date CollectedNorth Carolina Residential Soil Cleanup Levels (MSCCs)North Carolina Preliminary Soil Remediation Goals (PSRGs)4/23/2021

AJACC Auto Brownfields Project (No. 24054-20-060) Soil Excava$on
2. A view of the northwest end of the excavaon bei ng excavated.
1. A view of the stained area prior to excavaon.

AJACC Auto Brownfields Project (No. 24054-20-060) Soil Excava$on
4. A view of the northwest poron of the excavaon being backfilled.
3. A view of the soils being excavated.

AJACC Auto Brownfields Project (No. 24054-20-060) Soil Excava$on
6. A view of the excavaon area aer removal of im pacted soils and backfilling.
5. A view of the southeast poron of the excavaon.

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/3/2021
F&R, Inc. - Charlotte Brian Olin
3300 International Airport Dr., Suite 600 Charlotte, NC, 28208
Ref: Analytical Testing
Lab Report Number: 21-113-0038 Client Project Description: Verbena
Dear Brian Olin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/23/2021 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 96
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202137735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202199012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-113-0038
Page 2 of 96
Report Number:
Sample Summary Table
Client Project Description:
21-113-0038
Verbena
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
04/23/2021 12:30Solids 97536 S-1 04/23/2021 15:55 7199
04/23/2021 12:30Solids 97536 S-1 04/23/2021 15:55
04/23/2021 12:30Solids 97537 S-2 04/23/2021 15:55 7199
04/23/2021 12:30Solids 97537 S-2 04/23/2021 15:55
04/23/2021 13:40Solids 97538 S-3 04/23/2021 15:55 7199
04/23/2021 13:40Solids 97538 S-3 04/23/2021 15:55
04/23/2021 12:50Solids 97539 S-4 04/23/2021 15:55 7199
04/23/2021 12:50Solids 97539 S-4 04/23/2021 15:55
04/23/2021 12:35Solids 97540 Busy-1 04/23/2021 15:55 7199
04/23/2021 12:35Solids 97540 Busy-1 04/23/2021 15:55
04/23/2021 13:50Solids 97541 Busy-2 04/23/2021 15:55 7199
04/23/2021 13:50Solids 97541 Busy-2 04/23/2021 15:55
: Pace Analytical - Columbia, SC (Shealy), West Columbia, SC
Page 3 of 96
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-113-0038
Report Limit
Project:Verbena
V 97536S-1
4.82 04/27/2021 01:146020BArsenicmg/Kg - dry 0.111
214 04/27/2021 01:146020BBariummg/Kg - dry 1.65
3.13 04/27/2021 01:146020BCadmiummg/Kg - dry 0.0649
62.6 04/27/2021 01:146020BChromiummg/Kg - dry 0.342
731 04/27/2021 01:146020BLeadmg/Kg - dry 0.165
3.83 04/27/2021 01:146020BSeleniummg/Kg - dry 1.06
J0.168 04/27/2021 01:146020BSilvermg/Kg - dry 0.0484
0.110 04/27/2021 16:087471BMercury (Total)mg/Kg - dry 0.0177
0.080 04/26/2021 12:408260DAcetonemg/Kg - dry 0.002
J0.009 04/26/2021 12:408260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.021 04/28/2021 17:548270EAnthracenemg/Kg - dry 0.008
J0.062 04/28/2021 17:548270EBenzo(a)anthracene mg/Kg - dry 0.009
J0.085 04/28/2021 17:548270EBenzo(a)pyrene mg/Kg - dry 0.006
J0.152 04/28/2021 17:548270EBenzo(b)fluoranthene mg/Kg - dry 0.007
J0.107 04/28/2021 17:548270EBenzo(g,h,i)perylene mg/Kg - dry 0.007
7.74 04/28/2021 17:548270EBis(2-ethylhexyl)phthalate mg/Kg - dry 0.175
J0.076 04/28/2021 17:548270EChrysenemg/Kg - dry 0.009
J0.084 04/28/2021 17:548270EFluoranthenemg/Kg - dry 0.008
J0.069 04/28/2021 17:548270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.021
J0.037 04/28/2021 17:548270E1-Methylnaphthalene mg/Kg - dry 0.011
J0.073 04/28/2021 17:548270E2-Methylnaphthalene mg/Kg - dry 0.015
J0.051 04/28/2021 17:548270ENaphthalenemg/Kg - dry 0.016
J0.068 04/28/2021 17:548270EPhenanthrenemg/Kg - dry 0.008
J0.088 04/28/2021 17:548270EPyrenemg/Kg - dry 0.011
15.3 04/28/2021 16:11SW-DRYWT Moisture %
V 97537S-2
4.38 04/27/2021 01:206020BArsenicmg/Kg - dry 0.113
1020 04/27/2021 01:206020BBariummg/Kg - dry 1.68
1.67 04/27/2021 01:206020BCadmiummg/Kg - dry 0.0660
43.1 04/27/2021 01:206020BChromiummg/Kg - dry 0.348
736 04/27/2021 01:206020BLeadmg/Kg - dry 0.168
J2.24 04/27/2021 01:206020BSeleniummg/Kg - dry 1.08
0.724 04/27/2021 01:206020BSilvermg/Kg - dry 0.0492
0.498 04/27/2021 16:137471BMercury (Total)mg/Kg - dry 0.0180
J0.018 04/26/2021 13:108260DAcetonemg/Kg - dry 0.002
J0.041 04/28/2021 17:328270EBenzo(a)anthracene mg/Kg - dry 0.009
Page 4 of 96
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-113-0038
Report Limit
Project:Verbena
V 97537S-2
J0.045 04/28/2021 17:328270EBenzo(a)pyrene mg/Kg - dry 0.007
J0.069 04/28/2021 17:328270EBenzo(b)fluoranthene mg/Kg - dry 0.007
J0.020 04/28/2021 17:328270EBenzo(k)fluoranthene mg/Kg - dry 0.008
J0.050 04/28/2021 17:328270EChrysenemg/Kg - dry 0.009
J0.066 04/28/2021 17:328270EFluoranthenemg/Kg - dry 0.009
J0.026 04/28/2021 17:328270E1-Methylnaphthalene mg/Kg - dry 0.012
J0.036 04/28/2021 17:328270E2-Methylnaphthalene mg/Kg - dry 0.015
J0.029 04/28/2021 17:328270ENaphthalenemg/Kg - dry 0.016
J0.061 04/28/2021 17:328270EPyrenemg/Kg - dry 0.011
16.7 04/28/2021 16:11SW-DRYWT Moisture %
V 97538S-3
1.32 04/27/2021 01:406020BArsenicmg/Kg - dry 0.0972
197 04/27/2021 01:406020BBariummg/Kg - dry 1.45
J0.266 04/27/2021 01:406020BCadmiummg/Kg - dry 0.0569
31.1 04/27/2021 01:406020BChromiummg/Kg - dry 0.300
22.0 04/27/2021 01:406020BLeadmg/Kg - dry 0.145
2.93 04/27/2021 01:406020BSeleniummg/Kg - dry 0.931
J0.0443 04/27/2021 01:406020BSilvermg/Kg - dry 0.0424
0.034 04/26/2021 13:408260DAcetonemg/Kg - dry 0.002
J0.004 04/26/2021 13:408260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.025 04/28/2021 15:408270EBenzo(a)anthracene mg/Kg - dry 0.008
J0.029 04/28/2021 15:408270EBenzo(a)pyrene mg/Kg - dry 0.006
J0.050 04/28/2021 15:408270EBenzo(b)fluoranthene mg/Kg - dry 0.006
J0.022 04/28/2021 15:408270EBenzo(k)fluoranthene mg/Kg - dry 0.007
J0.025 04/28/2021 15:408270EChrysenemg/Kg - dry 0.008
J0.031 04/28/2021 15:408270EFluoranthenemg/Kg - dry 0.007
3.39 04/28/2021 16:11SW-DRYWT Moisture %
V 97539S-4
1.58 04/27/2021 01:466020BArsenicmg/Kg - dry 0.0972
167 04/27/2021 01:466020BBariummg/Kg - dry 1.45
J0.356 04/27/2021 01:466020BCadmiummg/Kg - dry 0.0569
49.7 04/27/2021 01:466020BChromiummg/Kg - dry 0.300
49.6 04/27/2021 01:466020BLeadmg/Kg - dry 0.145
2.32 04/27/2021 01:466020BSeleniummg/Kg - dry 0.931
J0.0453 04/27/2021 01:466020BSilvermg/Kg - dry 0.0424
0.028 04/26/2021 15:108260DAcetonemg/Kg - dry 0.002
Page 5 of 96
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-113-0038
Report Limit
Project:Verbena
V 97539S-4
J0.002 04/26/2021 15:108260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.018 04/28/2021 14:328270EBenzo(b)fluoranthene mg/Kg - dry 0.006
3.34 04/28/2021 16:11SW-DRYWT Moisture %
V 97540Busy-1
7.95 04/27/2021 01:526020BArsenicmg/Kg - dry 0.127
3110 04/27/2021 15:026020BBariummg/Kg - dry 4.73
3.69 04/27/2021 01:526020BCadmiummg/Kg - dry 0.0743
59.6 04/27/2021 01:526020BChromiummg/Kg - dry 0.391
2010 04/27/2021 15:026020BLeadmg/Kg - dry 0.473
J1.95 04/27/2021 01:526020BSeleniummg/Kg - dry 1.22
3.86 04/27/2021 01:526020BSilvermg/Kg - dry 0.0554
0.226 04/27/2021 16:407471BMercury (Total)mg/Kg - dry 0.0203
0.041 04/26/2021 14:108260DAcetonemg/Kg - dry 0.003
J0.033 04/28/2021 16:478270EAcenaphthylenemg/Kg - dry 0.017
J0.073 04/28/2021 16:478270EAnthracenemg/Kg - dry 0.009
J0.345 04/28/2021 16:478270EBenzo(a)anthracene mg/Kg - dry 0.010
J0.313 04/28/2021 16:478270EBenzo(a)pyrene mg/Kg - dry 0.007
J0.389 04/28/2021 16:478270EBenzo(b)fluoranthene mg/Kg - dry 0.008
J0.113 04/28/2021 16:478270EBenzo(k)fluoranthene mg/Kg - dry 0.009
J0.327 04/28/2021 16:478270EChrysenemg/Kg - dry 0.010
J0.033 04/28/2021 16:478270EDibenzofuranmg/Kg - dry 0.024
J0.171 04/28/2021 16:478270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.025
J0.047 04/28/2021 16:478270E1-Methylnaphthalene mg/Kg - dry 0.013
J0.065 04/28/2021 16:478270E2-Methylnaphthalene mg/Kg - dry 0.017
J0.088 04/28/2021 16:478270ENaphthalenemg/Kg - dry 0.018
J0.275 04/28/2021 16:478270EPhenanthrenemg/Kg - dry 0.009
J0.491 04/28/2021 16:478270EPyrenemg/Kg - dry 0.012
26.0 04/28/2021 16:11SW-DRYWT Moisture %
V 97541Busy-2
3.12 04/27/2021 01:596020BArsenicmg/Kg - dry 0.104
463 04/27/2021 01:596020BBariummg/Kg - dry 1.55
0.654 04/27/2021 01:596020BCadmiummg/Kg - dry 0.0610
27.3 04/27/2021 01:596020BChromiummg/Kg - dry 0.321
305 04/27/2021 01:596020BLeadmg/Kg - dry 0.155
J1.49 04/27/2021 01:596020BSeleniummg/Kg - dry 0.998
1.72 04/27/2021 01:596020BSilvermg/Kg - dry 0.0454
Page 6 of 96
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-113-0038
Report Limit
Project:Verbena
V 97541Busy-2
0.0624 04/27/2021 16:517471BMercury (Total)mg/Kg - dry 0.0166
0.037 04/26/2021 14:408260DAcetonemg/Kg - dry 0.002
J0.006 04/26/2021 14:408260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
J0.039 04/28/2021 17:098270EBenzo(a)anthracene mg/Kg - dry 0.008
J0.033 04/28/2021 17:098270EBenzo(a)pyrene mg/Kg - dry 0.006
J0.043 04/28/2021 17:098270EBenzo(b)fluoranthene mg/Kg - dry 0.006
J0.022 04/28/2021 17:098270EBenzo(k)fluoranthene mg/Kg - dry 0.007
J0.041 04/28/2021 17:098270EChrysenemg/Kg - dry 0.008
J0.046 04/28/2021 17:098270EFluoranthenemg/Kg - dry 0.008
J0.019 04/28/2021 17:098270E1-Methylnaphthalene mg/Kg - dry 0.011
J0.022 04/28/2021 17:098270E2-Methylnaphthalene mg/Kg - dry 0.014
J0.020 04/28/2021 17:098270ENaphthalenemg/Kg - dry 0.015
J0.035 04/28/2021 17:098270EPhenanthrenemg/Kg - dry 0.007
9.87 04/28/2021 16:11SW-DRYWT Moisture %
Page 7 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-1
97536 Matrix:
4/23/2021 12:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
15.3 %Moisture 1 04/28/21 16:11 SW-DRYWTEDV
4.82 mg/Kg - dry 0.111 0.118Arsenic 10 04/27/21 01:14 6020BMMR
214 mg/Kg - dry 1.65 11.8Barium 10 04/27/21 01:14 6020BMMR
3.13 mg/Kg - dry 0.0649 0.590Cadmium 10 04/27/21 01:14 6020BMMR
62.6 mg/Kg - dry 0.342 1.18Chromium 10 04/27/21 01:14 6020BMMR
731 mg/Kg - dry 0.165 1.18
Lead 10 04/27/21 01:14 6020BMMR
0.110 mg/Kg - dry 0.0177 0.0590Mercury (Total)1 04/27/21 16:08 7471BEDV
3.83 mg/Kg - dry 1.06 2.36Selenium 10 04/27/21 01:14 6020BMMR
0.168 J mg/Kg - dry 0.0484 0.590Silver 10 04/27/21 01:14 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 8 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-1
97536 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
0.080 mg/Kg - dry 0.002 0.023Acetone 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 04/26/21 12:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 04/26/21 12:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 04/26/21 12:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 04/26/21 12:40 V3553TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 04/26/21 12:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 04/26/21 12:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 04/26/21 12:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 04/26/21 12:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 04/26/21 12:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 04/26/21 12:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 04/26/21 12:40 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-1
97536 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 04/26/21 12:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 04/26/21 12:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 04/26/21 12:40 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 04/26/21 12:40 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 04/26/21 12:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 04/26/21 12:40 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 04/26/21 12:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 04/26/21 12:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 04/26/21 12:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 04/26/21 12:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 04/26/21 12:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 04/26/21 12:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 04/26/21 12:40 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.059Ethyl Tertiary Butyl Ether (ETBE)1 04/26/21 12:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 04/26/21 12:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 04/26/21 12:40 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-1
97536 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 04/26/21 12:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 04/26/21 12:40 V3553TBL
0.009 J mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 04/26/21 12:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 04/26/21 12:40 V3553TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005
n-Propylbenzene 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 04/26/21 12:40 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 04/26/21 12:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 04/26/21 12:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.011
1,2,4-Trichlorobenzene 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 04/26/21 12:40 V3553TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 04/26/21 12:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,2,3-Trichloropropane 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 04/26/21 12:40 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-1
97536 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 04/26/21 12:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 04/26/21 12:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 04/26/21 12:40 V3553
Surrogate: 4-Bromofluorobenzene 109 Limits: 70-130%04/26/21 12:401 TBL V3553
Surrogate: Dibromofluoromethane 107 Limits: 84-123%04/26/21 12:401 TBL V3553
Surrogate: Toluene-d8 101 Limits: 76-129%04/26/21 12:401 TBL V3553
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.017 mg/Kg - dry 0.017 0.779Acenaphthene 1 04/28/21 17:54 V3638JMV
<0.015 mg/Kg - dry 0.015 0.779Acenaphthylene 1 04/28/21 17:54 V3638JMV
<0.192 mg/Kg - dry 0.192 0.779Aniline 1 04/28/21 17:54 V3638JMV
0.021 J mg/Kg - dry 0.008 0.779Anthracene 1 04/28/21 17:54 V3638JMV
0.062 J mg/Kg - dry 0.009 0.779Benzo(a)anthracene 1 04/28/21 17:54 V3638JMV
0.085 J mg/Kg - dry 0.006 0.779Benzo(a)pyrene 1 04/28/21 17:54 V3638JMV
0.152 J
mg/Kg - dry 0.007 0.779
Benzo(b)fluoranthene 1 04/28/21 17:54 V3638JMV
0.107 J mg/Kg - dry 0.007 0.779Benzo(g,h,i)perylene 1 04/28/21 17:54 V3638JMV
<0.008 mg/Kg - dry 0.008 0.779Benzo(k)fluoranthene 1 04/28/21 17:54 V3638JMV
<0.646 mg/Kg - dry 0.646 2.36Benzoic Acid 1 04/28/21 17:54 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-1
97536 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.146 mg/Kg - dry 0.146 0.779Benzyl alcohol 1 04/28/21 17:54 V3638JMV
<0.148 mg/Kg - dry 0.148 0.779Bis(2-Chloroethoxy)methane 1 04/28/21 17:54 V3638JMV
<0.125 mg/Kg - dry 0.125 0.779Bis(2-Chloroethyl)ether 1 04/28/21 17:54 V3638JMV
<0.139 mg/Kg - dry 0.139 0.389Bis(2-Chloroisopropyl)ether 1 04/28/21 17:54 V3638JMV
7.74 mg/Kg - dry 0.175 0.779Bis(2-ethylhexyl)phthalate 1 04/28/21 17:54 V3638JMV
<0.182 mg/Kg - dry 0.182 0.7794-Bromophenyl phenyl ether 1 04/28/21 17:54 V3638JMV
<0.134 mg/Kg - dry 0.134 0.389Butyl benzyl phthalate 1 04/28/21 17:54 V3638JMV
<0.148 mg/Kg - dry 0.148 0.7794-Chloro-3-methylphenol 1 04/28/21 17:54 V3638JMV
<0.094 mg/Kg - dry 0.094 0.389
4-Chloroaniline 1 04/28/21 17:54 V3638JMV
<0.190 mg/Kg - dry 0.190 0.7792-Chloronaphthalene 1 04/28/21 17:54 V3638JMV
<0.148 mg/Kg - dry 0.148 0.7792-Chlorophenol 1 04/28/21 17:54 V3638JMV
<0.238 mg/Kg - dry 0.238 1.184-Chlorophenyl phenyl ether 1 04/28/21 17:54 V3638JMV
0.076 J mg/Kg - dry 0.009 0.779Chrysene 1 04/28/21 17:54 V3638JMV
<0.022 mg/Kg - dry 0.022 0.779Dibenz(a,h)anthracene 1 04/28/21 17:54 V3638JMV
<0.021 mg/Kg - dry 0.021 0.779Dibenzofuran 1 04/28/21 17:54 V3638JMV
<0.126 mg/Kg - dry 0.126 0.779
1,2-Dichlorobenzene 1 04/28/21 17:54 V3638JMV
<0.114 mg/Kg - dry 0.114 0.7791,3-Dichlorobenzene 1 04/28/21 17:54 V3638JMV
<0.122 mg/Kg - dry 0.122 0.3891,4-Dichlorobenzene 1 04/28/21 17:54 V3638JMV
<0.154 mg/Kg - dry 0.154 0.7793,3'-Dichlorobenzidine 1 04/28/21 17:54 V3638JMV
<0.152 mg/Kg - dry 0.152 0.7792,4-Dichlorophenol 1 04/28/21 17:54 V3638JMV
<0.200 mg/Kg - dry 0.200 0.779Diethyl phthalate 1 04/28/21 17:54 V3638JMV
<0.186 mg/Kg - dry 0.186 0.779Dimethyl phthalate 1 04/28/21 17:54 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-1
97536 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.161 mg/Kg - dry 0.161 0.3892,4-Dimethylphenol 1 04/28/21 17:54 V3638JMV
<0.193 mg/Kg - dry 0.193 0.779Di-n-butyl phthalate 1 04/28/21 17:54 V3638JMV
<0.429 mg/Kg - dry 0.429 1.774,6-Dinitro-2-methylphenol 1 04/28/21 17:54 V3638JMV
<0.456 mg/Kg - dry 0.456 1.772,4-Dinitrophenol 1 04/28/21 17:54 V3638JMV
<0.206 mg/Kg - dry 0.206 0.7792,4-Dinitrotoluene 1 04/28/21 17:54 V3638JMV
<0.201 mg/Kg - dry 0.201 0.7792,6-Dinitrotoluene 1 04/28/21 17:54 V3638JMV
<0.201 mg/Kg - dry 0.201 0.389Di-n-Octyl Phthalate 1 04/28/21 17:54 V3638JMV
0.084 J mg/Kg - dry 0.008 0.779Fluoranthene 1 04/28/21 17:54 V3638JMV
<0.017 mg/Kg - dry 0.017 0.779
Fluorene 1 04/28/21 17:54 V3638JMV
<0.171 mg/Kg - dry 0.171 0.779Hexachlorobenzene 1 04/28/21 17:54 V3638JMV
<0.175 mg/Kg - dry 0.175 0.779Hexachlorobutadiene 1 04/28/21 17:54 V3638JMV
<0.268 mg/Kg - dry 0.268 0.779Hexachlorocyclopentadiene 1 04/28/21 17:54 V3638JMV
<0.122 mg/Kg - dry 0.122 0.779Hexachloroethane 1 04/28/21 17:54 V3638JMV
0.069 J mg/Kg - dry 0.021 0.779Indeno(1,2,3-cd)pyrene 1 04/28/21 17:54 V3638JMV
<0.167 mg/Kg - dry 0.167 0.779Isophorone 1 04/28/21 17:54 V3638JMV
0.037 J
mg/Kg - dry 0.011 0.779
1-Methylnaphthalene 1 04/28/21 17:54 V3638JMV
0.073 J mg/Kg - dry 0.015 0.7792-Methylnaphthalene 1 04/28/21 17:54 V3638JMV
<0.148 mg/Kg - dry 0.148 0.7792-Methylphenol 1 04/28/21 17:54 V3638JMV
<0.168 mg/Kg - dry 0.168 0.7793&4 Methylphenol 1 04/28/21 17:54 V3638JMV
0.051 J mg/Kg - dry 0.016 0.779Naphthalene 1 04/28/21 17:54 V3638JMV
<0.167 mg/Kg - dry 0.167 0.7792-Nitroaniline 1 04/28/21 17:54 V3638JMV
<0.141 mg/Kg - dry 0.141 0.7793-Nitroaniline 1 04/28/21 17:54 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-1
97536 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.121 mg/Kg - dry 0.121 0.3894-Nitroaniline 1 04/28/21 17:54 V3638JMV
<0.165 mg/Kg - dry 0.165 0.389Nitrobenzene 1 04/28/21 17:54 V3638JMV
<0.129 mg/Kg - dry 0.129 0.7792-Nitrophenol 1 04/28/21 17:54 V3638JMV
<0.192 mg/Kg - dry 0.192 0.7794-Nitrophenol 1 04/28/21 17:54 V3638JMV
<0.006 mg/Kg - dry 0.006 0.200N-Nitrosodimethylamine 1 04/28/21 17:54 V3638JMV
<0.213 mg/Kg - dry 0.213 0.779N-Nitrosodiphenylamine 1 04/28/21 17:54 V3638JMV
<0.179 mg/Kg - dry 0.179 0.779N-Nitroso-di-n-propylamine 1 04/28/21 17:54 V3638JMV
<0.497 mg/Kg - dry 0.497 1.18Pentachlorophenol 1 04/28/21 17:54 V3638JMV
0.068 J
mg/Kg - dry 0.008 0.779
Phenanthrene 1 04/28/21 17:54 V3638JMV
<0.127 mg/Kg - dry 0.127 0.779Phenol 1 04/28/21 17:54 V3638JMV
0.088 J mg/Kg - dry 0.011 0.779Pyrene 1 04/28/21 17:54 V3638JMV
<0.074 mg/Kg - dry 0.074 0.389Pyridine 1 04/28/21 17:54 V3638JMV
<0.138 mg/Kg - dry 0.138 0.7791,2,4-Trichlorobenzene 1 04/28/21 17:54 V3638JMV
<0.165 mg/Kg - dry 0.165 0.7792,4,5-Trichlorophenol 1 04/28/21 17:54 V3638JMV
<0.188 mg/Kg - dry 0.188 0.7792,4,6-Trichlorophenol 1 04/28/21 17:54 V3638JMV
Surrogate: Phenol-d5 39.1 Limits: 34-121%04/28/21 17:541 JMV V3638
Surrogate: 2-Fluorobiphenyl 54.0 Limits: 44-115%04/28/21 17:541 JMV V3638
Surrogate: 2-Fluorophenol 38.5 Limits: 35-115%04/28/21 17:541 JMV V3638
Surrogate: Nitrobenzene-d5 47.3 Limits: 37-122%04/28/21 17:541 JMV V3638
Surrogate: 4-Terphenyl-d14 52.8 *Limits: 54-127%04/28/21 17:541 JMV V3638
Surrogate: 2,4,6-Tribromophenol 52.1 Limits: 39-132%04/28/21 17:541 JMV V3638
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-2
97537 Matrix:
4/23/2021 12:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
16.7 %Moisture 1 04/28/21 16:11 SW-DRYWTEDV
4.38 mg/Kg - dry 0.113 0.120Arsenic 10 04/27/21 01:20 6020BMMR
1020 mg/Kg - dry 1.68 12.0Barium 10 04/27/21 01:20 6020BMMR
1.67 mg/Kg - dry 0.0660 0.600Cadmium 10 04/27/21 01:20 6020BMMR
43.1 mg/Kg - dry 0.348 1.20Chromium 10 04/27/21 01:20 6020BMMR
736 mg/Kg - dry 0.168 1.20
Lead 10 04/27/21 01:20 6020BMMR
0.498 mg/Kg - dry 0.0180 0.0600Mercury (Total)1 04/27/21 16:13 7471BEDV
2.24 J mg/Kg - dry 1.08 2.40Selenium 10 04/27/21 01:20 6020BMMR
0.724 mg/Kg - dry 0.0492 0.600Silver 10 04/27/21 01:20 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 16 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-2
97537 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
0.018 J mg/Kg - dry 0.002 0.024Acetone 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 04/26/21 13:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 04/26/21 13:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 04/26/21 13:10 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/26/21 13:10 V3553TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 04/26/21 13:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 04/26/21 13:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 04/26/21 13:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/26/21 13:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 04/26/21 13:10 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/26/21 13:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 04/26/21 13:10 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-2
97537 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 04/26/21 13:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 04/26/21 13:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 04/26/21 13:10 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/26/21 13:10 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/26/21 13:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 04/26/21 13:10 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 04/26/21 13:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 04/26/21 13:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.006cis-1,2-Dichloroethene 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/26/21 13:10 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 04/26/21 13:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/26/21 13:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.006cis-1,3-Dichloropropene 1 04/26/21 13:10 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 04/26/21 13:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 04/26/21 13:10 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.060Ethyl Tertiary Butyl Ether (ETBE)1 04/26/21 13:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.012Hexachlorobutadiene 1 04/26/21 13:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 04/26/21 13:10 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-2
97537 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0242-Hexanone 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/26/21 13:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 04/26/21 13:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006Methyl tert-butyl ether (MTBE)1 04/26/21 13:10 V3553TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.006
n-Propylbenzene 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/26/21 13:10 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/26/21 13:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2,3-Trichlorobenzene 1 04/26/21 13:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.012
1,2,4-Trichlorobenzene 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/26/21 13:10 V3553TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 04/26/21 13:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,3,5-Trimethylbenzene 1 04/26/21 13:10 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-2
97537 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 04/26/21 13:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 04/26/21 13:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 04/26/21 13:10 V3553
Surrogate: 4-Bromofluorobenzene 109 Limits: 70-130%04/26/21 13:101 TBL V3553
Surrogate: Dibromofluoromethane 105 Limits: 84-123%04/26/21 13:101 TBL V3553
Surrogate: Toluene-d8 103 Limits: 76-129%04/26/21 13:101 TBL V3553
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.018 mg/Kg - dry 0.018 0.792Acenaphthene 1 04/28/21 17:32 V3638JMV
<0.015 mg/Kg - dry 0.015 0.792Acenaphthylene 1 04/28/21 17:32 V3638JMV
<0.195 mg/Kg - dry 0.195 0.792Aniline 1 04/28/21 17:32 V3638JMV
<0.008 mg/Kg - dry 0.008 0.792Anthracene 1 04/28/21 17:32 V3638JMV
0.041 J mg/Kg - dry 0.009 0.792Benzo(a)anthracene 1 04/28/21 17:32 V3638JMV
0.045 J mg/Kg - dry 0.007 0.792Benzo(a)pyrene 1 04/28/21 17:32 V3638JMV
0.069 J
mg/Kg - dry 0.007 0.792
Benzo(b)fluoranthene 1 04/28/21 17:32 V3638JMV
<0.007 mg/Kg - dry 0.007 0.792Benzo(g,h,i)perylene 1 04/28/21 17:32 V3638JMV
0.020 J mg/Kg - dry 0.008 0.792Benzo(k)fluoranthene 1 04/28/21 17:32 V3638JMV
<0.657 mg/Kg - dry 0.657 2.40Benzoic Acid 1 04/28/21 17:32 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-2
97537 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.148 mg/Kg - dry 0.148 0.792Benzyl alcohol 1 04/28/21 17:32 V3638JMV
<0.151 mg/Kg - dry 0.151 0.792Bis(2-Chloroethoxy)methane 1 04/28/21 17:32 V3638JMV
<0.127 mg/Kg - dry 0.127 0.792Bis(2-Chloroethyl)ether 1 04/28/21 17:32 V3638JMV
<0.141 mg/Kg - dry 0.141 0.396Bis(2-Chloroisopropyl)ether 1 04/28/21 17:32 V3638JMV
<0.178 mg/Kg - dry 0.178 0.792Bis(2-ethylhexyl)phthalate 1 04/28/21 17:32 V3638JMV
<0.186 mg/Kg - dry 0.186 0.7924-Bromophenyl phenyl ether 1 04/28/21 17:32 V3638JMV
<0.136 mg/Kg - dry 0.136 0.396Butyl benzyl phthalate 1 04/28/21 17:32 V3638JMV
<0.151 mg/Kg - dry 0.151 0.7924-Chloro-3-methylphenol 1 04/28/21 17:32 V3638JMV
<0.096 mg/Kg - dry 0.096 0.396
4-Chloroaniline 1 04/28/21 17:32 V3638JMV
<0.193 mg/Kg - dry 0.193 0.7922-Chloronaphthalene 1 04/28/21 17:32 V3638JMV
<0.151 mg/Kg - dry 0.151 0.7922-Chlorophenol 1 04/28/21 17:32 V3638JMV
<0.242 mg/Kg - dry 0.242 1.204-Chlorophenyl phenyl ether 1 04/28/21 17:32 V3638JMV
0.050 J mg/Kg - dry 0.009 0.792Chrysene 1 04/28/21 17:32 V3638JMV
<0.022 mg/Kg - dry 0.022 0.792Dibenz(a,h)anthracene 1 04/28/21 17:32 V3638JMV
<0.021 mg/Kg - dry 0.021 0.792Dibenzofuran 1 04/28/21 17:32 V3638JMV
<0.128 mg/Kg - dry 0.128 0.792
1,2-Dichlorobenzene 1 04/28/21 17:32 V3638JMV
<0.116 mg/Kg - dry 0.116 0.7921,3-Dichlorobenzene 1 04/28/21 17:32 V3638JMV
<0.124 mg/Kg - dry 0.124 0.3961,4-Dichlorobenzene 1 04/28/21 17:32 V3638JMV
<0.157 mg/Kg - dry 0.157 0.7923,3'-Dichlorobenzidine 1 04/28/21 17:32 V3638JMV
<0.154 mg/Kg - dry 0.154 0.7922,4-Dichlorophenol 1 04/28/21 17:32 V3638JMV
<0.204 mg/Kg - dry 0.204 0.792Diethyl phthalate 1 04/28/21 17:32 V3638JMV
<0.189 mg/Kg - dry 0.189 0.792Dimethyl phthalate 1 04/28/21 17:32 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-2
97537 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.164 mg/Kg - dry 0.164 0.3962,4-Dimethylphenol 1 04/28/21 17:32 V3638JMV
<0.196 mg/Kg - dry 0.196 0.792Di-n-butyl phthalate 1 04/28/21 17:32 V3638JMV
<0.436 mg/Kg - dry 0.436 1.804,6-Dinitro-2-methylphenol 1 04/28/21 17:32 V3638JMV
<0.464 mg/Kg - dry 0.464 1.802,4-Dinitrophenol 1 04/28/21 17:32 V3638JMV
<0.210 mg/Kg - dry 0.210 0.7922,4-Dinitrotoluene 1 04/28/21 17:32 V3638JMV
<0.205 mg/Kg - dry 0.205 0.7922,6-Dinitrotoluene 1 04/28/21 17:32 V3638JMV
<0.205 mg/Kg - dry 0.205 0.396Di-n-Octyl Phthalate 1 04/28/21 17:32 V3638JMV
0.066 J mg/Kg - dry 0.009 0.792Fluoranthene 1 04/28/21 17:32 V3638JMV
<0.017 mg/Kg - dry 0.017 0.792
Fluorene 1 04/28/21 17:32 V3638JMV
<0.174 mg/Kg - dry 0.174 0.792Hexachlorobenzene 1 04/28/21 17:32 V3638JMV
<0.178 mg/Kg - dry 0.178 0.792Hexachlorobutadiene 1 04/28/21 17:32 V3638JMV
<0.272 mg/Kg - dry 0.272 0.792Hexachlorocyclopentadiene 1 04/28/21 17:32 V3638JMV
<0.124 mg/Kg - dry 0.124 0.792Hexachloroethane 1 04/28/21 17:32 V3638JMV
<0.022 mg/Kg - dry 0.022 0.792Indeno(1,2,3-cd)pyrene 1 04/28/21 17:32 V3638JMV
<0.170 mg/Kg - dry 0.170 0.792Isophorone 1 04/28/21 17:32 V3638JMV
0.026 J
mg/Kg - dry 0.012 0.792
1-Methylnaphthalene 1 04/28/21 17:32 V3638JMV
0.036 J mg/Kg - dry 0.015 0.7922-Methylnaphthalene 1 04/28/21 17:32 V3638JMV
<0.151 mg/Kg - dry 0.151 0.7922-Methylphenol 1 04/28/21 17:32 V3638JMV
<0.171 mg/Kg - dry 0.171 0.7923&4 Methylphenol 1 04/28/21 17:32 V3638JMV
0.029 J mg/Kg - dry 0.016 0.792Naphthalene 1 04/28/21 17:32 V3638JMV
<0.170 mg/Kg - dry 0.170 0.7922-Nitroaniline 1 04/28/21 17:32 V3638JMV
<0.144 mg/Kg - dry 0.144 0.7923-Nitroaniline 1 04/28/21 17:32 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-2
97537 Matrix:
4/23/2021 12:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.123 mg/Kg - dry 0.123 0.3964-Nitroaniline 1 04/28/21 17:32 V3638JMV
<0.168 mg/Kg - dry 0.168 0.396Nitrobenzene 1 04/28/21 17:32 V3638JMV
<0.132 mg/Kg - dry 0.132 0.7922-Nitrophenol 1 04/28/21 17:32 V3638JMV
<0.195 mg/Kg - dry 0.195 0.7924-Nitrophenol 1 04/28/21 17:32 V3638JMV
<0.006 mg/Kg - dry 0.006 0.204N-Nitrosodimethylamine 1 04/28/21 17:32 V3638JMV
<0.217 mg/Kg - dry 0.217 0.792N-Nitrosodiphenylamine 1 04/28/21 17:32 V3638JMV
<0.182 mg/Kg - dry 0.182 0.792N-Nitroso-di-n-propylamine 1 04/28/21 17:32 V3638JMV
<0.505 mg/Kg - dry 0.505 1.20Pentachlorophenol 1 04/28/21 17:32 V3638JMV
<0.008 mg/Kg - dry 0.008 0.792
Phenanthrene 1 04/28/21 17:32 V3638JMV
<0.129 mg/Kg - dry 0.129 0.792Phenol 1 04/28/21 17:32 V3638JMV
0.061 J mg/Kg - dry 0.011 0.792Pyrene 1 04/28/21 17:32 V3638JMV
<0.075 mg/Kg - dry 0.075 0.396Pyridine 1 04/28/21 17:32 V3638JMV
<0.140 mg/Kg - dry 0.140 0.7921,2,4-Trichlorobenzene 1 04/28/21 17:32 V3638JMV
<0.168 mg/Kg - dry 0.168 0.7922,4,5-Trichlorophenol 1 04/28/21 17:32 V3638JMV
<0.192 mg/Kg - dry 0.192 0.7922,4,6-Trichlorophenol 1 04/28/21 17:32 V3638JMV
Surrogate: Phenol-d5 52.6 Limits: 34-121%04/28/21 17:321 JMV V3638
Surrogate: 2-Fluorobiphenyl 70.9 Limits: 44-115%04/28/21 17:321 JMV V3638
Surrogate: 2-Fluorophenol 52.3 Limits: 35-115%04/28/21 17:321 JMV V3638
Surrogate: Nitrobenzene-d5 61.2 Limits: 37-122%04/28/21 17:321 JMV V3638
Surrogate: 4-Terphenyl-d14 69.1 Limits: 54-127%04/28/21 17:321 JMV V3638
Surrogate: 2,4,6-Tribromophenol 67.5 Limits: 39-132%04/28/21 17:321 JMV V3638
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-3
97538 Matrix:
4/23/2021 13:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
3.39 %Moisture 1 04/28/21 16:11 SW-DRYWTEDV
1.32 mg/Kg - dry 0.0972 0.104Arsenic 10 04/27/21 01:40 6020BMMR
197 mg/Kg - dry 1.45 10.4Barium 10 04/27/21 01:40 6020BMMR
0.266 J mg/Kg - dry 0.0569 0.518Cadmium 10 04/27/21 01:40 6020BMMR
31.1 mg/Kg - dry 0.300 1.04Chromium 10 04/27/21 01:40 6020BMMR
22.0 mg/Kg - dry 0.145 1.04
Lead 10 04/27/21 01:40 6020BMMR
<0.0155 mg/Kg - dry 0.0155 0.0518Mercury (Total)1 04/27/21 16:17 7471BEDV
2.93 mg/Kg - dry 0.931 2.07Selenium 10 04/27/21 01:40 6020BMMR
0.0443 J mg/Kg - dry 0.0424 0.518Silver 10 04/27/21 01:40 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 24 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-3
97538 Matrix:
4/23/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
0.034 mg/Kg - dry 0.002 0.020Acetone 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.020Acrolein 1 04/26/21 13:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.020Acrylonitrile 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 04/26/21 13:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 04/26/21 13:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005Bromochloromethane 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.010
Bromomethane 1 04/26/21 13:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 04/26/21 13:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 04/26/21 13:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 04/26/21 13:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 04/26/21 13:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005
Chlorodibromomethane 1 04/26/21 13:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.010Chloroethane 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 04/26/21 13:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 04/26/21 13:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0052-Chlorotoluene 1 04/26/21 13:40 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 04/26/21 13:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 04/26/21 13:40 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-3
97538 Matrix:
4/23/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 04/26/21 13:40 V3553TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 04/26/21 13:40 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,4-Dichlorobenzene 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 04/26/21 13:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethane 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 04/26/21 13:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 04/26/21 13:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005cis-1,2-Dichloroethene 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 04/26/21 13:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 04/26/21 13:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloropropene 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 04/26/21 13:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005trans-1,3-Dichloropropene 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 04/26/21 13:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.051Ethyl Tertiary Butyl Ether (ETBE)1 04/26/21 13:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.010Hexachlorobutadiene 1 04/26/21 13:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 04/26/21 13:40 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-3
97538 Matrix:
4/23/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0202-Hexanone 1 04/26/21 13:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 04/26/21 13:40 V3553TBL
0.004 J mg/Kg - dry 0.0007 0.020Methyl Ethyl Ketone (MEK)1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Methyl tert-butyl ether (MTBE)1 04/26/21 13:40 V3553TBL
<0.015 mg/Kg - dry 0.015 0.0204-Methyl-2-Pentanone 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005
n-Propylbenzene 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 04/26/21 13:40 V3553TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,1,2,2-Tetrachloroethane 1 04/26/21 13:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005Tetrachloroethene 1 04/26/21 13:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 04/26/21 13:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.010
1,2,4-Trichlorobenzene 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 04/26/21 13:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 04/26/21 13:40 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.005Trichloroethene 1 04/26/21 13:40 V3553TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 04/26/21 13:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2,3-Trichloropropane 1 04/26/21 13:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 04/26/21 13:40 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 27 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-3
97538 Matrix:
4/23/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 04/26/21 13:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 04/26/21 13:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005o-Xylene 1 04/26/21 13:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.010m,p-Xylene 1 04/26/21 13:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005Xylene (Total)1 04/26/21 13:40 V3553
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%04/26/21 13:401 TBL V3553
Surrogate: Dibromofluoromethane 104 Limits: 84-123%04/26/21 13:401 TBL V3553
Surrogate: Toluene-d8 97.3 Limits: 76-129%04/26/21 13:401 TBL V3553
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.015 mg/Kg - dry 0.015 0.683Acenaphthene 1 04/28/21 15:40 V3638JMV
<0.013 mg/Kg - dry 0.013 0.683Acenaphthylene 1 04/28/21 15:40 V3638JMV
<0.168 mg/Kg - dry 0.168 0.683Aniline 1 04/28/21 15:40 V3638JMV
<0.007 mg/Kg - dry 0.007 0.683Anthracene 1 04/28/21 15:40 V3638JMV
0.025 J mg/Kg - dry 0.008 0.683Benzo(a)anthracene 1 04/28/21 15:40 V3638JMV
0.029 J mg/Kg - dry 0.006 0.683Benzo(a)pyrene 1 04/28/21 15:40 V3638JMV
0.050 J
mg/Kg - dry 0.006 0.683
Benzo(b)fluoranthene 1 04/28/21 15:40 V3638JMV
<0.006 mg/Kg - dry 0.006 0.683Benzo(g,h,i)perylene 1 04/28/21 15:40 V3638JMV
0.022 J mg/Kg - dry 0.007 0.683Benzo(k)fluoranthene 1 04/28/21 15:40 V3638JMV
<0.567 mg/Kg - dry 0.567 2.07Benzoic Acid 1 04/28/21 15:40 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 28 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-3
97538 Matrix:
4/23/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.128 mg/Kg - dry 0.128 0.683Benzyl alcohol 1 04/28/21 15:40 V3638JMV
<0.130 mg/Kg - dry 0.130 0.683Bis(2-Chloroethoxy)methane 1 04/28/21 15:40 V3638JMV
<0.109 mg/Kg - dry 0.109 0.683Bis(2-Chloroethyl)ether 1 04/28/21 15:40 V3638JMV
<0.122 mg/Kg - dry 0.122 0.341Bis(2-Chloroisopropyl)ether 1 04/28/21 15:40 V3638JMV
<0.154 mg/Kg - dry 0.154 0.683Bis(2-ethylhexyl)phthalate 1 04/28/21 15:40 V3638JMV
<0.160 mg/Kg - dry 0.160 0.6834-Bromophenyl phenyl ether 1 04/28/21 15:40 V3638JMV
<0.118 mg/Kg - dry 0.118 0.341Butyl benzyl phthalate 1 04/28/21 15:40 V3638JMV
<0.130 mg/Kg - dry 0.130 0.6834-Chloro-3-methylphenol 1 04/28/21 15:40 V3638JMV
<0.082 mg/Kg - dry 0.082 0.341
4-Chloroaniline 1 04/28/21 15:40 V3638JMV
<0.166 mg/Kg - dry 0.166 0.6832-Chloronaphthalene 1 04/28/21 15:40 V3638JMV
<0.130 mg/Kg - dry 0.130 0.6832-Chlorophenol 1 04/28/21 15:40 V3638JMV
<0.209 mg/Kg - dry 0.209 1.044-Chlorophenyl phenyl ether 1 04/28/21 15:40 V3638JMV
0.025 J mg/Kg - dry 0.008 0.683Chrysene 1 04/28/21 15:40 V3638JMV
<0.019 mg/Kg - dry 0.019 0.683Dibenz(a,h)anthracene 1 04/28/21 15:40 V3638JMV
<0.018 mg/Kg - dry 0.018 0.683Dibenzofuran 1 04/28/21 15:40 V3638JMV
<0.110 mg/Kg - dry 0.110 0.683
1,2-Dichlorobenzene 1 04/28/21 15:40 V3638JMV
<0.100 mg/Kg - dry 0.100 0.6831,3-Dichlorobenzene 1 04/28/21 15:40 V3638JMV
<0.107 mg/Kg - dry 0.107 0.3411,4-Dichlorobenzene 1 04/28/21 15:40 V3638JMV
<0.135 mg/Kg - dry 0.135 0.6833,3'-Dichlorobenzidine 1 04/28/21 15:40 V3638JMV
<0.133 mg/Kg - dry 0.133 0.6832,4-Dichlorophenol 1 04/28/21 15:40 V3638JMV
<0.175 mg/Kg - dry 0.175 0.683Diethyl phthalate 1 04/28/21 15:40 V3638JMV
<0.163 mg/Kg - dry 0.163 0.683Dimethyl phthalate 1 04/28/21 15:40 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 29 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-3
97538 Matrix:
4/23/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.141 mg/Kg - dry 0.141 0.3412,4-Dimethylphenol 1 04/28/21 15:40 V3638JMV
<0.169 mg/Kg - dry 0.169 0.683Di-n-butyl phthalate 1 04/28/21 15:40 V3638JMV
<0.376 mg/Kg - dry 0.376 1.554,6-Dinitro-2-methylphenol 1 04/28/21 15:40 V3638JMV
<0.400 mg/Kg - dry 0.400 1.552,4-Dinitrophenol 1 04/28/21 15:40 V3638JMV
<0.181 mg/Kg - dry 0.181 0.6832,4-Dinitrotoluene 1 04/28/21 15:40 V3638JMV
<0.177 mg/Kg - dry 0.177 0.6832,6-Dinitrotoluene 1 04/28/21 15:40 V3638JMV
<0.177 mg/Kg - dry 0.177 0.341Di-n-Octyl Phthalate 1 04/28/21 15:40 V3638JMV
0.031 J mg/Kg - dry 0.007 0.683Fluoranthene 1 04/28/21 15:40 V3638JMV
<0.014 mg/Kg - dry 0.014 0.683
Fluorene 1 04/28/21 15:40 V3638JMV
<0.150 mg/Kg - dry 0.150 0.683Hexachlorobenzene 1 04/28/21 15:40 V3638JMV
<0.154 mg/Kg - dry 0.154 0.683Hexachlorobutadiene 1 04/28/21 15:40 V3638JMV
<0.234 mg/Kg - dry 0.234 0.683Hexachlorocyclopentadiene 1 04/28/21 15:40 V3638JMV
<0.107 mg/Kg - dry 0.107 0.683Hexachloroethane 1 04/28/21 15:40 V3638JMV
<0.019 mg/Kg - dry 0.019 0.683Indeno(1,2,3-cd)pyrene 1 04/28/21 15:40 V3638JMV
<0.146 mg/Kg - dry 0.146 0.683Isophorone 1 04/28/21 15:40 V3638JMV
<0.010 mg/Kg - dry 0.010 0.683
1-Methylnaphthalene 1 04/28/21 15:40 V3638JMV
<0.013 mg/Kg - dry 0.013 0.6832-Methylnaphthalene 1 04/28/21 15:40 V3638JMV
<0.130 mg/Kg - dry 0.130 0.6832-Methylphenol 1 04/28/21 15:40 V3638JMV
<0.148 mg/Kg - dry 0.148 0.6833&4 Methylphenol 1 04/28/21 15:40 V3638JMV
<0.014 mg/Kg - dry 0.014 0.683Naphthalene 1 04/28/21 15:40 V3638JMV
<0.146 mg/Kg - dry 0.146 0.6832-Nitroaniline 1 04/28/21 15:40 V3638JMV
<0.124 mg/Kg - dry 0.124 0.6833-Nitroaniline 1 04/28/21 15:40 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 30 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-3
97538 Matrix:
4/23/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.106 mg/Kg - dry 0.106 0.3414-Nitroaniline 1 04/28/21 15:40 V3638JMV
<0.144 mg/Kg - dry 0.144 0.341Nitrobenzene 1 04/28/21 15:40 V3638JMV
<0.113 mg/Kg - dry 0.113 0.6832-Nitrophenol 1 04/28/21 15:40 V3638JMV
<0.168 mg/Kg - dry 0.168 0.6834-Nitrophenol 1 04/28/21 15:40 V3638JMV
<0.005 mg/Kg - dry 0.005 0.175N-Nitrosodimethylamine 1 04/28/21 15:40 V3638JMV
<0.187 mg/Kg - dry 0.187 0.683N-Nitrosodiphenylamine 1 04/28/21 15:40 V3638JMV
<0.157 mg/Kg - dry 0.157 0.683N-Nitroso-di-n-propylamine 1 04/28/21 15:40 V3638JMV
<0.435 mg/Kg - dry 0.435 1.04Pentachlorophenol 1 04/28/21 15:40 V3638JMV
<0.007 mg/Kg - dry 0.007 0.683
Phenanthrene 1 04/28/21 15:40 V3638JMV
<0.111 mg/Kg - dry 0.111 0.683Phenol 1 04/28/21 15:40 V3638JMV
<0.009 mg/Kg - dry 0.009 0.683Pyrene 1 04/28/21 15:40 V3638JMV
<0.065 mg/Kg - dry 0.065 0.341Pyridine 1 04/28/21 15:40 V3638JMV
<0.121 mg/Kg - dry 0.121 0.6831,2,4-Trichlorobenzene 1 04/28/21 15:40 V3638JMV
<0.144 mg/Kg - dry 0.144 0.6832,4,5-Trichlorophenol 1 04/28/21 15:40 V3638JMV
<0.165 mg/Kg - dry 0.165 0.6832,4,6-Trichlorophenol 1 04/28/21 15:40 V3638JMV
Surrogate: Phenol-d5 60.3 Limits: 34-121%04/28/21 15:401 JMV V3638
Surrogate: 2-Fluorobiphenyl 80.6 Limits: 44-115%04/28/21 15:401 JMV V3638
Surrogate: 2-Fluorophenol 59.7 Limits: 35-115%04/28/21 15:401 JMV V3638
Surrogate: Nitrobenzene-d5 69.7 Limits: 37-122%04/28/21 15:401 JMV V3638
Surrogate: 4-Terphenyl-d14 83.6 Limits: 54-127%04/28/21 15:401 JMV V3638
Surrogate: 2,4,6-Tribromophenol 83.9 Limits: 39-132%04/28/21 15:401 JMV V3638
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 31 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-4
97539 Matrix:
4/23/2021 12:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
3.34 %Moisture 1 04/28/21 16:11 SW-DRYWTEDV
1.58 mg/Kg - dry 0.0972 0.103Arsenic 10 04/27/21 01:46 6020BMMR
167 mg/Kg - dry 1.45 10.3Barium 10 04/27/21 01:46 6020BMMR
0.356 J mg/Kg - dry 0.0569 0.517Cadmium 10 04/27/21 01:46 6020BMMR
49.7 mg/Kg - dry 0.300 1.03Chromium 10 04/27/21 01:46 6020BMMR
49.6 mg/Kg - dry 0.145 1.03
Lead 10 04/27/21 01:46 6020BMMR
<0.0155 mg/Kg - dry 0.0155 0.0517Mercury (Total)1 04/27/21 16:28 7471BEDV
2.32 mg/Kg - dry 0.931 2.07Selenium 10 04/27/21 01:46 6020BMMR
0.0453 J mg/Kg - dry 0.0424 0.517Silver 10 04/27/21 01:46 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 32 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-4
97539 Matrix:
4/23/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
0.028 mg/Kg - dry 0.002 0.022Acetone 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 04/26/21 15:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 04/26/21 15:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 04/26/21 15:10 V3553TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 04/26/21 15:10 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 04/26/21 15:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 04/26/21 15:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 04/26/21 15:10 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.005
Chlorodibromomethane 1 04/26/21 15:10 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 04/26/21 15:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 04/26/21 15:10 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 04/26/21 15:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 04/26/21 15:10 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 33 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-4
97539 Matrix:
4/23/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 04/26/21 15:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 04/26/21 15:10 V3553TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 04/26/21 15:10 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 04/26/21 15:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 04/26/21 15:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 04/26/21 15:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 04/26/21 15:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 04/26/21 15:10 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 04/26/21 15:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloropropene 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 04/26/21 15:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 04/26/21 15:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 04/26/21 15:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 04/26/21 15:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 04/26/21 15:10 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 34 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-4
97539 Matrix:
4/23/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 04/26/21 15:10 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 04/26/21 15:10 V3553TBL
0.002 J mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 04/26/21 15:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 04/26/21 15:10 V3553TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005
n-Propylbenzene 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 04/26/21 15:10 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 04/26/21 15:10 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 04/26/21 15:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 04/26/21 15:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.011
1,2,4-Trichlorobenzene 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 04/26/21 15:10 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 04/26/21 15:10 V3553TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 04/26/21 15:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 04/26/21 15:10 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 35 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-4
97539 Matrix:
4/23/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 04/26/21 15:10 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 04/26/21 15:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 04/26/21 15:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 04/26/21 15:10 V3553
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%04/26/21 15:101 TBL V3553
Surrogate: Dibromofluoromethane 105 Limits: 84-123%04/26/21 15:101 TBL V3553
Surrogate: Toluene-d8 99.1 Limits: 76-129%04/26/21 15:101 TBL V3553
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.015 mg/Kg - dry 0.015 0.684Acenaphthene 1 04/28/21 14:32 V3638JMV
<0.013 mg/Kg - dry 0.013 0.684Acenaphthylene 1 04/28/21 14:32 V3638JMV
<0.168 mg/Kg - dry 0.168 0.684Aniline 1 04/28/21 14:32 V3638JMV
<0.007 mg/Kg - dry 0.007 0.684Anthracene 1 04/28/21 14:32 V3638JMV
<0.008 mg/Kg - dry 0.008 0.684Benzo(a)anthracene 1 04/28/21 14:32 V3638JMV
<0.006 mg/Kg - dry 0.006 0.684Benzo(a)pyrene 1 04/28/21 14:32 V3638JMV
0.018 J
mg/Kg - dry 0.006 0.684
Benzo(b)fluoranthene 1 04/28/21 14:32 V3638JMV
<0.006 mg/Kg - dry 0.006 0.684Benzo(g,h,i)perylene 1 04/28/21 14:32 V3638JMV
<0.007 mg/Kg - dry 0.007 0.684Benzo(k)fluoranthene 1 04/28/21 14:32 V3638JMV
<0.570 mg/Kg - dry 0.570 2.08Benzoic Acid 1 04/28/21 14:32 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 36 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-4
97539 Matrix:
4/23/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.128 mg/Kg - dry 0.128 0.684Benzyl alcohol 1 04/28/21 14:32 V3638JMV
<0.130 mg/Kg - dry 0.130 0.684Bis(2-Chloroethoxy)methane 1 04/28/21 14:32 V3638JMV
<0.109 mg/Kg - dry 0.109 0.684Bis(2-Chloroethyl)ether 1 04/28/21 14:32 V3638JMV
<0.122 mg/Kg - dry 0.122 0.342Bis(2-Chloroisopropyl)ether 1 04/28/21 14:32 V3638JMV
<0.154 mg/Kg - dry 0.154 0.684Bis(2-ethylhexyl)phthalate 1 04/28/21 14:32 V3638JMV
<0.160 mg/Kg - dry 0.160 0.6844-Bromophenyl phenyl ether 1 04/28/21 14:32 V3638JMV
<0.117 mg/Kg - dry 0.117 0.342Butyl benzyl phthalate 1 04/28/21 14:32 V3638JMV
<0.130 mg/Kg - dry 0.130 0.6844-Chloro-3-methylphenol 1 04/28/21 14:32 V3638JMV
<0.082 mg/Kg - dry 0.082 0.342
4-Chloroaniline 1 04/28/21 14:32 V3638JMV
<0.166 mg/Kg - dry 0.166 0.6842-Chloronaphthalene 1 04/28/21 14:32 V3638JMV
<0.130 mg/Kg - dry 0.130 0.6842-Chlorophenol 1 04/28/21 14:32 V3638JMV
<0.208 mg/Kg - dry 0.208 1.034-Chlorophenyl phenyl ether 1 04/28/21 14:32 V3638JMV
<0.008 mg/Kg - dry 0.008 0.684Chrysene 1 04/28/21 14:32 V3638JMV
<0.019 mg/Kg - dry 0.019 0.684Dibenz(a,h)anthracene 1 04/28/21 14:32 V3638JMV
<0.018 mg/Kg - dry 0.018 0.684Dibenzofuran 1 04/28/21 14:32 V3638JMV
<0.110 mg/Kg - dry 0.110 0.684
1,2-Dichlorobenzene 1 04/28/21 14:32 V3638JMV
<0.100 mg/Kg - dry 0.100 0.6841,3-Dichlorobenzene 1 04/28/21 14:32 V3638JMV
<0.107 mg/Kg - dry 0.107 0.3421,4-Dichlorobenzene 1 04/28/21 14:32 V3638JMV
<0.135 mg/Kg - dry 0.135 0.6843,3'-Dichlorobenzidine 1 04/28/21 14:32 V3638JMV
<0.133 mg/Kg - dry 0.133 0.6842,4-Dichlorophenol 1 04/28/21 14:32 V3638JMV
<0.176 mg/Kg - dry 0.176 0.684Diethyl phthalate 1 04/28/21 14:32 V3638JMV
<0.163 mg/Kg - dry 0.163 0.684Dimethyl phthalate 1 04/28/21 14:32 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 37 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-4
97539 Matrix:
4/23/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.141 mg/Kg - dry 0.141 0.3422,4-Dimethylphenol 1 04/28/21 14:32 V3638JMV
<0.169 mg/Kg - dry 0.169 0.684Di-n-butyl phthalate 1 04/28/21 14:32 V3638JMV
<0.378 mg/Kg - dry 0.378 1.564,6-Dinitro-2-methylphenol 1 04/28/21 14:32 V3638JMV
<0.403 mg/Kg - dry 0.403 1.562,4-Dinitrophenol 1 04/28/21 14:32 V3638JMV
<0.182 mg/Kg - dry 0.182 0.6842,4-Dinitrotoluene 1 04/28/21 14:32 V3638JMV
<0.177 mg/Kg - dry 0.177 0.6842,6-Dinitrotoluene 1 04/28/21 14:32 V3638JMV
<0.177 mg/Kg - dry 0.177 0.342Di-n-Octyl Phthalate 1 04/28/21 14:32 V3638JMV
<0.007 mg/Kg - dry 0.007 0.684Fluoranthene 1 04/28/21 14:32 V3638JMV
<0.014 mg/Kg - dry 0.014 0.684
Fluorene 1 04/28/21 14:32 V3638JMV
<0.150 mg/Kg - dry 0.150 0.684Hexachlorobenzene 1 04/28/21 14:32 V3638JMV
<0.154 mg/Kg - dry 0.154 0.684Hexachlorobutadiene 1 04/28/21 14:32 V3638JMV
<0.235 mg/Kg - dry 0.235 0.684Hexachlorocyclopentadiene 1 04/28/21 14:32 V3638JMV
<0.107 mg/Kg - dry 0.107 0.684Hexachloroethane 1 04/28/21 14:32 V3638JMV
<0.019 mg/Kg - dry 0.019 0.684Indeno(1,2,3-cd)pyrene 1 04/28/21 14:32 V3638JMV
<0.146 mg/Kg - dry 0.146 0.684Isophorone 1 04/28/21 14:32 V3638JMV
<0.010 mg/Kg - dry 0.010 0.684
1-Methylnaphthalene 1 04/28/21 14:32 V3638JMV
<0.013 mg/Kg - dry 0.013 0.6842-Methylnaphthalene 1 04/28/21 14:32 V3638JMV
<0.130 mg/Kg - dry 0.130 0.6842-Methylphenol 1 04/28/21 14:32 V3638JMV
<0.147 mg/Kg - dry 0.147 0.6843&4 Methylphenol 1 04/28/21 14:32 V3638JMV
<0.014 mg/Kg - dry 0.014 0.684Naphthalene 1 04/28/21 14:32 V3638JMV
<0.146 mg/Kg - dry 0.146 0.6842-Nitroaniline 1 04/28/21 14:32 V3638JMV
<0.124 mg/Kg - dry 0.124 0.6843-Nitroaniline 1 04/28/21 14:32 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 38 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:S-4
97539 Matrix:
4/23/2021 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.106 mg/Kg - dry 0.106 0.3424-Nitroaniline 1 04/28/21 14:32 V3638JMV
<0.144 mg/Kg - dry 0.144 0.342Nitrobenzene 1 04/28/21 14:32 V3638JMV
<0.113 mg/Kg - dry 0.113 0.6842-Nitrophenol 1 04/28/21 14:32 V3638JMV
<0.168 mg/Kg - dry 0.168 0.6844-Nitrophenol 1 04/28/21 14:32 V3638JMV
<0.005 mg/Kg - dry 0.005 0.176N-Nitrosodimethylamine 1 04/28/21 14:32 V3638JMV
<0.188 mg/Kg - dry 0.188 0.684N-Nitrosodiphenylamine 1 04/28/21 14:32 V3638JMV
<0.157 mg/Kg - dry 0.157 0.684N-Nitroso-di-n-propylamine 1 04/28/21 14:32 V3638JMV
<0.435 mg/Kg - dry 0.435 1.03Pentachlorophenol 1 04/28/21 14:32 V3638JMV
<0.007 mg/Kg - dry 0.007 0.684
Phenanthrene 1 04/28/21 14:32 V3638JMV
<0.111 mg/Kg - dry 0.111 0.684Phenol 1 04/28/21 14:32 V3638JMV
<0.009 mg/Kg - dry 0.009 0.684Pyrene 1 04/28/21 14:32 V3638JMV
<0.065 mg/Kg - dry 0.065 0.342Pyridine 1 04/28/21 14:32 V3638JMV
<0.121 mg/Kg - dry 0.121 0.6841,2,4-Trichlorobenzene 1 04/28/21 14:32 V3638JMV
<0.144 mg/Kg - dry 0.144 0.6842,4,5-Trichlorophenol 1 04/28/21 14:32 V3638JMV
<0.165 mg/Kg - dry 0.165 0.6842,4,6-Trichlorophenol 1 04/28/21 14:32 V3638JMV
Surrogate: Phenol-d5 70.4 Limits: 34-121%04/28/21 14:321 JMV V3638
Surrogate: 2-Fluorobiphenyl 88.6 Limits: 44-115%04/28/21 14:321 JMV V3638
Surrogate: 2-Fluorophenol 69.5 Limits: 35-115%04/28/21 14:321 JMV V3638
Surrogate: Nitrobenzene-d5 80.8 Limits: 37-122%04/28/21 14:321 JMV V3638
Surrogate: 4-Terphenyl-d14 97.6 Limits: 54-127%04/28/21 14:321 JMV V3638
Surrogate: 2,4,6-Tribromophenol 95.8 Limits: 39-132%04/28/21 14:321 JMV V3638
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 39 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-1
97540 Matrix:
4/23/2021 12:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
26.0 %Moisture 1 04/28/21 16:11 SW-DRYWTEDV
7.95 mg/Kg - dry 0.127 0.135Arsenic 10 04/27/21 01:52 6020BMMR
3110 mg/Kg - dry 4.73 33.8Barium 25 04/27/21 15:02 6020BMMR
3.69 mg/Kg - dry 0.0743 0.676Cadmium 10 04/27/21 01:52 6020BMMR
59.6 mg/Kg - dry 0.391 1.35Chromium 10 04/27/21 01:52 6020BMMR
2010 mg/Kg - dry 0.473 3.38
Lead 25 04/27/21 15:02 6020BMMR
0.226 mg/Kg - dry 0.0203 0.0676Mercury (Total)1 04/27/21 16:40 7471BEDV
1.95 J mg/Kg - dry 1.22 2.70Selenium 10 04/27/21 01:52 6020BMMR
3.86 mg/Kg - dry 0.0554 0.676Silver 10 04/27/21 01:52 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 40 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-1
97540 Matrix:
4/23/2021 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
0.041 mg/Kg - dry 0.003 0.027Acetone 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 04/26/21 14:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 04/26/21 14:10 V3553TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 04/26/21 14:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 04/26/21 14:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 04/26/21 14:10 V3553TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 04/26/21 14:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 04/26/21 14:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 04/26/21 14:10 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 04/26/21 14:10 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 04/26/21 14:10 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 41 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-1
97540 Matrix:
4/23/2021 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 04/26/21 14:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 04/26/21 14:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 04/26/21 14:10 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 04/26/21 14:10 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 04/26/21 14:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 04/26/21 14:10 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 04/26/21 14:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 04/26/21 14:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.067Ethyl Tertiary Butyl Ether (ETBE)1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 04/26/21 14:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 04/26/21 14:10 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 42 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-1
97540 Matrix:
4/23/2021 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0008 mg/Kg - dry 0.0008 0.0272-Hexanone 1 04/26/21 14:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 04/26/21 14:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 04/26/21 14:10 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 04/26/21 14:10 V3553TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006
n-Propylbenzene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 04/26/21 14:10 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 04/26/21 14:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 04/26/21 14:10 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.013
1,2,4-Trichlorobenzene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 04/26/21 14:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 04/26/21 14:10 V3553TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 04/26/21 14:10 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 04/26/21 14:10 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 43 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-1
97540 Matrix:
4/23/2021 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 04/26/21 14:10 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 04/26/21 14:10 V3553TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 04/26/21 14:10 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 04/26/21 14:10 V3553
Surrogate: 4-Bromofluorobenzene 107 Limits: 70-130%04/26/21 14:101 TBL V3553
Surrogate: Dibromofluoromethane 104 Limits: 84-123%04/26/21 14:101 TBL V3553
Surrogate: Toluene-d8 105 Limits: 76-129%04/26/21 14:101 TBL V3553
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.020 mg/Kg - dry 0.020 0.891Acenaphthene 1 04/28/21 16:47 V3638JMV
0.033 J mg/Kg - dry 0.017 0.891Acenaphthylene 1 04/28/21 16:47 V3638JMV
<0.220 mg/Kg - dry 0.220 0.891Aniline 1 04/28/21 16:47 V3638JMV
0.073 J mg/Kg - dry 0.009 0.891Anthracene 1 04/28/21 16:47 V3638JMV
0.345 J mg/Kg - dry 0.010 0.891Benzo(a)anthracene 1 04/28/21 16:47 V3638JMV
0.313 J mg/Kg - dry 0.007 0.891Benzo(a)pyrene 1 04/28/21 16:47 V3638JMV
0.389 J
mg/Kg - dry 0.008 0.891
Benzo(b)fluoranthene 1 04/28/21 16:47 V3638JMV
<0.008 mg/Kg - dry 0.008 0.891Benzo(g,h,i)perylene 1 04/28/21 16:47 V3638JMV
0.113 J mg/Kg - dry 0.009 0.891Benzo(k)fluoranthene 1 04/28/21 16:47 V3638JMV
<0.740 mg/Kg - dry 0.740 2.70Benzoic Acid 1 04/28/21 16:47 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 44 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-1
97540 Matrix:
4/23/2021 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.167 mg/Kg - dry 0.167 0.891Benzyl alcohol 1 04/28/21 16:47 V3638JMV
<0.170 mg/Kg - dry 0.170 0.891Bis(2-Chloroethoxy)methane 1 04/28/21 16:47 V3638JMV
<0.143 mg/Kg - dry 0.143 0.891Bis(2-Chloroethyl)ether 1 04/28/21 16:47 V3638JMV
<0.159 mg/Kg - dry 0.159 0.445Bis(2-Chloroisopropyl)ether 1 04/28/21 16:47 V3638JMV
<0.201 mg/Kg - dry 0.201 0.891Bis(2-ethylhexyl)phthalate 1 04/28/21 16:47 V3638JMV
<0.209 mg/Kg - dry 0.209 0.8914-Bromophenyl phenyl ether 1 04/28/21 16:47 V3638JMV
<0.154 mg/Kg - dry 0.154 0.445Butyl benzyl phthalate 1 04/28/21 16:47 V3638JMV
<0.170 mg/Kg - dry 0.170 0.8914-Chloro-3-methylphenol 1 04/28/21 16:47 V3638JMV
<0.108 mg/Kg - dry 0.108 0.445
4-Chloroaniline 1 04/28/21 16:47 V3638JMV
<0.217 mg/Kg - dry 0.217 0.8912-Chloronaphthalene 1 04/28/21 16:47 V3638JMV
<0.170 mg/Kg - dry 0.170 0.8912-Chlorophenol 1 04/28/21 16:47 V3638JMV
<0.272 mg/Kg - dry 0.272 1.354-Chlorophenyl phenyl ether 1 04/28/21 16:47 V3638JMV
0.327 J mg/Kg - dry 0.010 0.891Chrysene 1 04/28/21 16:47 V3638JMV
<0.025 mg/Kg - dry 0.025 0.891Dibenz(a,h)anthracene 1 04/28/21 16:47 V3638JMV
0.033 J mg/Kg - dry 0.024 0.891Dibenzofuran 1 04/28/21 16:47 V3638JMV
<0.144 mg/Kg - dry 0.144 0.891
1,2-Dichlorobenzene 1 04/28/21 16:47 V3638JMV
<0.131 mg/Kg - dry 0.131 0.8911,3-Dichlorobenzene 1 04/28/21 16:47 V3638JMV
<0.140 mg/Kg - dry 0.140 0.4451,4-Dichlorobenzene 1 04/28/21 16:47 V3638JMV
<0.177 mg/Kg - dry 0.177 0.8913,3'-Dichlorobenzidine 1 04/28/21 16:47 V3638JMV
<0.174 mg/Kg - dry 0.174 0.8912,4-Dichlorophenol 1 04/28/21 16:47 V3638JMV
<0.229 mg/Kg - dry 0.229 0.891Diethyl phthalate 1 04/28/21 16:47 V3638JMV
<0.213 mg/Kg - dry 0.213 0.891Dimethyl phthalate 1 04/28/21 16:47 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 45 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-1
97540 Matrix:
4/23/2021 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.185 mg/Kg - dry 0.185 0.4452,4-Dimethylphenol 1 04/28/21 16:47 V3638JMV
<0.221 mg/Kg - dry 0.221 0.891Di-n-butyl phthalate 1 04/28/21 16:47 V3638JMV
<0.491 mg/Kg - dry 0.491 2.034,6-Dinitro-2-methylphenol 1 04/28/21 16:47 V3638JMV
<0.522 mg/Kg - dry 0.522 2.032,4-Dinitrophenol 1 04/28/21 16:47 V3638JMV
<0.236 mg/Kg - dry 0.236 0.8912,4-Dinitrotoluene 1 04/28/21 16:47 V3638JMV
<0.231 mg/Kg - dry 0.231 0.8912,6-Dinitrotoluene 1 04/28/21 16:47 V3638JMV
<0.231 mg/Kg - dry 0.231 0.445Di-n-Octyl Phthalate 1 04/28/21 16:47 V3638JMV
<0.010 mg/Kg - dry 0.010 0.891Fluoranthene 1 04/28/21 16:47 V3638JMV
<0.019 mg/Kg - dry 0.019 0.891
Fluorene 1 04/28/21 16:47 V3638JMV
<0.195 mg/Kg - dry 0.195 0.891Hexachlorobenzene 1 04/28/21 16:47 V3638JMV
<0.201 mg/Kg - dry 0.201 0.891Hexachlorobutadiene 1 04/28/21 16:47 V3638JMV
<0.306 mg/Kg - dry 0.306 0.891Hexachlorocyclopentadiene 1 04/28/21 16:47 V3638JMV
<0.140 mg/Kg - dry 0.140 0.891Hexachloroethane 1 04/28/21 16:47 V3638JMV
0.171 J mg/Kg - dry 0.025 0.891Indeno(1,2,3-cd)pyrene 1 04/28/21 16:47 V3638JMV
<0.191 mg/Kg - dry 0.191 0.891Isophorone 1 04/28/21 16:47 V3638JMV
0.047 J
mg/Kg - dry 0.013 0.891
1-Methylnaphthalene 1 04/28/21 16:47 V3638JMV
0.065 J mg/Kg - dry 0.017 0.8912-Methylnaphthalene 1 04/28/21 16:47 V3638JMV
<0.170 mg/Kg - dry 0.170 0.8912-Methylphenol 1 04/28/21 16:47 V3638JMV
<0.193 mg/Kg - dry 0.193 0.8913&4 Methylphenol 1 04/28/21 16:47 V3638JMV
0.088 J mg/Kg - dry 0.018 0.891Naphthalene 1 04/28/21 16:47 V3638JMV
<0.191 mg/Kg - dry 0.191 0.8912-Nitroaniline 1 04/28/21 16:47 V3638JMV
<0.162 mg/Kg - dry 0.162 0.8913-Nitroaniline 1 04/28/21 16:47 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 46 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-1
97540 Matrix:
4/23/2021 12:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.139 mg/Kg - dry 0.139 0.4454-Nitroaniline 1 04/28/21 16:47 V3638JMV
<0.189 mg/Kg - dry 0.189 0.445Nitrobenzene 1 04/28/21 16:47 V3638JMV
<0.148 mg/Kg - dry 0.148 0.8912-Nitrophenol 1 04/28/21 16:47 V3638JMV
<0.220 mg/Kg - dry 0.220 0.8914-Nitrophenol 1 04/28/21 16:47 V3638JMV
<0.007 mg/Kg - dry 0.007 0.229N-Nitrosodimethylamine 1 04/28/21 16:47 V3638JMV
<0.244 mg/Kg - dry 0.244 0.891N-Nitrosodiphenylamine 1 04/28/21 16:47 V3638JMV
<0.205 mg/Kg - dry 0.205 0.891N-Nitroso-di-n-propylamine 1 04/28/21 16:47 V3638JMV
<0.568 mg/Kg - dry 0.568 1.35Pentachlorophenol 1 04/28/21 16:47 V3638JMV
0.275 J
mg/Kg - dry 0.009 0.891
Phenanthrene 1 04/28/21 16:47 V3638JMV
<0.145 mg/Kg - dry 0.145 0.891Phenol 1 04/28/21 16:47 V3638JMV
0.491 J mg/Kg - dry 0.012 0.891Pyrene 1 04/28/21 16:47 V3638JMV
<0.085 mg/Kg - dry 0.085 0.445Pyridine 1 04/28/21 16:47 V3638JMV
<0.158 mg/Kg - dry 0.158 0.8911,2,4-Trichlorobenzene 1 04/28/21 16:47 V3638JMV
<0.189 mg/Kg - dry 0.189 0.8912,4,5-Trichlorophenol 1 04/28/21 16:47 V3638JMV
<0.216 mg/Kg - dry 0.216 0.8912,4,6-Trichlorophenol 1 04/28/21 16:47 V3638JMV
Surrogate: Phenol-d5 53.8 Limits: 34-121%04/28/21 16:471 JMV V3638
Surrogate: 2-Fluorobiphenyl 71.3 Limits: 44-115%04/28/21 16:471 JMV V3638
Surrogate: 2-Fluorophenol 52.3 Limits: 35-115%04/28/21 16:471 JMV V3638
Surrogate: Nitrobenzene-d5 62.2 Limits: 37-122%04/28/21 16:471 JMV V3638
Surrogate: 4-Terphenyl-d14 74.4 Limits: 54-127%04/28/21 16:471 JMV V3638
Surrogate: 2,4,6-Tribromophenol 68.7 Limits: 39-132%04/28/21 16:471 JMV V3638
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 47 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-2
97541 Matrix:
4/23/2021 13:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.87 %Moisture 1 04/28/21 16:11 SW-DRYWTEDV
3.12 mg/Kg - dry 0.104 0.111Arsenic 10 04/27/21 01:59 6020BMMR
463 mg/Kg - dry 1.55 11.1Barium 10 04/27/21 01:59 6020BMMR
0.654 mg/Kg - dry 0.0610 0.555Cadmium 10 04/27/21 01:59 6020BMMR
27.3 mg/Kg - dry 0.321 1.11Chromium 10 04/27/21 01:59 6020BMMR
305 mg/Kg - dry 0.155 1.11
Lead 10 04/27/21 01:59 6020BMMR
0.0624 mg/Kg - dry 0.0166 0.0555Mercury (Total)1 04/27/21 16:51 7471BEDV
1.49 J mg/Kg - dry 0.998 2.22Selenium 10 04/27/21 01:59 6020BMMR
1.72 mg/Kg - dry 0.0454 0.555Silver 10 04/27/21 01:59 6020BMMR
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Limit ExceededLEstimated valueJ
Method Quantitation LimitMQL
Page 48 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-2
97541 Matrix:
4/23/2021 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
0.037 mg/Kg - dry 0.002 0.022Acetone 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 04/26/21 14:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 04/26/21 14:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 04/26/21 14:40 V3553TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 04/26/21 14:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 04/26/21 14:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 04/26/21 14:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 04/26/21 14:40 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.005
Chlorodibromomethane 1 04/26/21 14:40 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 04/26/21 14:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 04/26/21 14:40 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 04/26/21 14:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 04/26/21 14:40 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 49 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-2
97541 Matrix:
4/23/2021 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 04/26/21 14:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 04/26/21 14:40 V3553TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 04/26/21 14:40 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 04/26/21 14:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 04/26/21 14:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 04/26/21 14:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 04/26/21 14:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 04/26/21 14:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 04/26/21 14:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.005
1,1-Dichloropropene 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 04/26/21 14:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 04/26/21 14:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 04/26/21 14:40 V3553TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 04/26/21 14:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 04/26/21 14:40 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 50 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-2
97541 Matrix:
4/23/2021 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 04/26/21 14:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 04/26/21 14:40 V3553TBL
0.006 J mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 04/26/21 14:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 04/26/21 14:40 V3553TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005
n-Propylbenzene 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 04/26/21 14:40 V3553TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 04/26/21 14:40 V3553TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 04/26/21 14:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.005Toluene 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 04/26/21 14:40 V3553TBL
<0.0007 mg/Kg - dry 0.0007 0.011
1,2,4-Trichlorobenzene 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 04/26/21 14:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 04/26/21 14:40 V3553TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 04/26/21 14:40 V3553TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 04/26/21 14:40 V3553TBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 51 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-2
97541 Matrix:
4/23/2021 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V3552 04/26/21 08:00
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 04/26/21 14:40 V3553TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 04/26/21 14:40 V3553TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 04/26/21 14:40 V3553TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 04/26/21 14:40 V3553
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%04/26/21 14:401 TBL V3553
Surrogate: Dibromofluoromethane 103 Limits: 84-123%04/26/21 14:401 TBL V3553
Surrogate: Toluene-d8 97.3 Limits: 76-129%04/26/21 14:401 TBL V3553
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.016 mg/Kg - dry 0.016 0.732Acenaphthene 1 04/28/21 17:09 V3638JMV
<0.014 mg/Kg - dry 0.014 0.732Acenaphthylene 1 04/28/21 17:09 V3638JMV
<0.180 mg/Kg - dry 0.180 0.732Aniline 1 04/28/21 17:09 V3638JMV
<0.008 mg/Kg - dry 0.008 0.732Anthracene 1 04/28/21 17:09 V3638JMV
0.039 J mg/Kg - dry 0.008 0.732Benzo(a)anthracene 1 04/28/21 17:09 V3638JMV
0.033 J mg/Kg - dry 0.006 0.732Benzo(a)pyrene 1 04/28/21 17:09 V3638JMV
0.043 J
mg/Kg - dry 0.006 0.732
Benzo(b)fluoranthene 1 04/28/21 17:09 V3638JMV
<0.007 mg/Kg - dry 0.007 0.732Benzo(g,h,i)perylene 1 04/28/21 17:09 V3638JMV
0.022 J mg/Kg - dry 0.007 0.732Benzo(k)fluoranthene 1 04/28/21 17:09 V3638JMV
<0.608 mg/Kg - dry 0.608 2.22Benzoic Acid 1 04/28/21 17:09 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 52 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-2
97541 Matrix:
4/23/2021 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.137 mg/Kg - dry 0.137 0.732Benzyl alcohol 1 04/28/21 17:09 V3638JMV
<0.139 mg/Kg - dry 0.139 0.732Bis(2-Chloroethoxy)methane 1 04/28/21 17:09 V3638JMV
<0.117 mg/Kg - dry 0.117 0.732Bis(2-Chloroethyl)ether 1 04/28/21 17:09 V3638JMV
<0.130 mg/Kg - dry 0.130 0.366Bis(2-Chloroisopropyl)ether 1 04/28/21 17:09 V3638JMV
<0.165 mg/Kg - dry 0.165 0.732Bis(2-ethylhexyl)phthalate 1 04/28/21 17:09 V3638JMV
<0.171 mg/Kg - dry 0.171 0.7324-Bromophenyl phenyl ether 1 04/28/21 17:09 V3638JMV
<0.126 mg/Kg - dry 0.126 0.366Butyl benzyl phthalate 1 04/28/21 17:09 V3638JMV
<0.139 mg/Kg - dry 0.139 0.7324-Chloro-3-methylphenol 1 04/28/21 17:09 V3638JMV
<0.088 mg/Kg - dry 0.088 0.366
4-Chloroaniline 1 04/28/21 17:09 V3638JMV
<0.178 mg/Kg - dry 0.178 0.7322-Chloronaphthalene 1 04/28/21 17:09 V3638JMV
<0.139 mg/Kg - dry 0.139 0.7322-Chlorophenol 1 04/28/21 17:09 V3638JMV
<0.224 mg/Kg - dry 0.224 1.114-Chlorophenyl phenyl ether 1 04/28/21 17:09 V3638JMV
0.041 J mg/Kg - dry 0.008 0.732Chrysene 1 04/28/21 17:09 V3638JMV
<0.021 mg/Kg - dry 0.021 0.732Dibenz(a,h)anthracene 1 04/28/21 17:09 V3638JMV
<0.019 mg/Kg - dry 0.019 0.732Dibenzofuran 1 04/28/21 17:09 V3638JMV
<0.118 mg/Kg - dry 0.118 0.732
1,2-Dichlorobenzene 1 04/28/21 17:09 V3638JMV
<0.107 mg/Kg - dry 0.107 0.7321,3-Dichlorobenzene 1 04/28/21 17:09 V3638JMV
<0.115 mg/Kg - dry 0.115 0.3661,4-Dichlorobenzene 1 04/28/21 17:09 V3638JMV
<0.145 mg/Kg - dry 0.145 0.7323,3'-Dichlorobenzidine 1 04/28/21 17:09 V3638JMV
<0.143 mg/Kg - dry 0.143 0.7322,4-Dichlorophenol 1 04/28/21 17:09 V3638JMV
<0.188 mg/Kg - dry 0.188 0.732Diethyl phthalate 1 04/28/21 17:09 V3638JMV
<0.175 mg/Kg - dry 0.175 0.732Dimethyl phthalate 1 04/28/21 17:09 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 53 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-2
97541 Matrix:
4/23/2021 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.152 mg/Kg - dry 0.152 0.3662,4-Dimethylphenol 1 04/28/21 17:09 V3638JMV
<0.181 mg/Kg - dry 0.181 0.732Di-n-butyl phthalate 1 04/28/21 17:09 V3638JMV
<0.403 mg/Kg - dry 0.403 1.664,6-Dinitro-2-methylphenol 1 04/28/21 17:09 V3638JMV
<0.429 mg/Kg - dry 0.429 1.662,4-Dinitrophenol 1 04/28/21 17:09 V3638JMV
<0.194 mg/Kg - dry 0.194 0.7322,4-Dinitrotoluene 1 04/28/21 17:09 V3638JMV
<0.189 mg/Kg - dry 0.189 0.7322,6-Dinitrotoluene 1 04/28/21 17:09 V3638JMV
<0.189 mg/Kg - dry 0.189 0.366Di-n-Octyl Phthalate 1 04/28/21 17:09 V3638JMV
0.046 J mg/Kg - dry 0.008 0.732Fluoranthene 1 04/28/21 17:09 V3638JMV
<0.015 mg/Kg - dry 0.015 0.732
Fluorene 1 04/28/21 17:09 V3638JMV
<0.160 mg/Kg - dry 0.160 0.732Hexachlorobenzene 1 04/28/21 17:09 V3638JMV
<0.165 mg/Kg - dry 0.165 0.732Hexachlorobutadiene 1 04/28/21 17:09 V3638JMV
<0.251 mg/Kg - dry 0.251 0.732Hexachlorocyclopentadiene 1 04/28/21 17:09 V3638JMV
<0.115 mg/Kg - dry 0.115 0.732Hexachloroethane 1 04/28/21 17:09 V3638JMV
<0.020 mg/Kg - dry 0.020 0.732Indeno(1,2,3-cd)pyrene 1 04/28/21 17:09 V3638JMV
<0.157 mg/Kg - dry 0.157 0.732Isophorone 1 04/28/21 17:09 V3638JMV
0.019 J
mg/Kg - dry 0.011 0.732
1-Methylnaphthalene 1 04/28/21 17:09 V3638JMV
0.022 J mg/Kg - dry 0.014 0.7322-Methylnaphthalene 1 04/28/21 17:09 V3638JMV
<0.139 mg/Kg - dry 0.139 0.7322-Methylphenol 1 04/28/21 17:09 V3638JMV
<0.158 mg/Kg - dry 0.158 0.7323&4 Methylphenol 1 04/28/21 17:09 V3638JMV
0.020 J mg/Kg - dry 0.015 0.732Naphthalene 1 04/28/21 17:09 V3638JMV
<0.157 mg/Kg - dry 0.157 0.7322-Nitroaniline 1 04/28/21 17:09 V3638JMV
<0.133 mg/Kg - dry 0.133 0.7323-Nitroaniline 1 04/28/21 17:09 V3638JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 54 of 96
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28208
21-113-0038
00019
F&R, Inc. - Charlotte
3300 International Airport Dr., Suite 600
Brian Olin
Charlotte
Received : 04/23/2021
Verbena
Report Date : 05/03/2021
Sample ID :
Lab No :
Sampled:Busy-2
97541 Matrix:
4/23/2021 13:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V3558 04/27/21 07:57
<0.114 mg/Kg - dry 0.114 0.3664-Nitroaniline 1 04/28/21 17:09 V3638JMV
<0.155 mg/Kg - dry 0.155 0.366Nitrobenzene 1 04/28/21 17:09 V3638JMV
<0.122 mg/Kg - dry 0.122 0.7322-Nitrophenol 1 04/28/21 17:09 V3638JMV
<0.180 mg/Kg - dry 0.180 0.7324-Nitrophenol 1 04/28/21 17:09 V3638JMV
<0.006 mg/Kg - dry 0.006 0.188N-Nitrosodimethylamine 1 04/28/21 17:09 V3638JMV
<0.200 mg/Kg - dry 0.200 0.732N-Nitrosodiphenylamine 1 04/28/21 17:09 V3638JMV
<0.168 mg/Kg - dry 0.168 0.732N-Nitroso-di-n-propylamine 1 04/28/21 17:09 V3638JMV
<0.467 mg/Kg - dry 0.467 1.11Pentachlorophenol 1 04/28/21 17:09 V3638JMV
0.035 J
mg/Kg - dry 0.007 0.732
Phenanthrene 1 04/28/21 17:09 V3638JMV
<0.119 mg/Kg - dry 0.119 0.732Phenol 1 04/28/21 17:09 V3638JMV
<0.010 mg/Kg - dry 0.010 0.732Pyrene 1 04/28/21 17:09 V3638JMV
<0.069 mg/Kg - dry 0.069 0.366Pyridine 1 04/28/21 17:09 V3638JMV
<0.129 mg/Kg - dry 0.129 0.7321,2,4-Trichlorobenzene 1 04/28/21 17:09 V3638JMV
<0.155 mg/Kg - dry 0.155 0.7322,4,5-Trichlorophenol 1 04/28/21 17:09 V3638JMV
<0.177 mg/Kg - dry 0.177 0.7322,4,6-Trichlorophenol 1 04/28/21 17:09 V3638JMV
Surrogate: Phenol-d5 51.2 Limits: 34-121%04/28/21 17:091 JMV V3638
Surrogate: 2-Fluorobiphenyl 67.3 Limits: 44-115%04/28/21 17:091 JMV V3638
Surrogate: 2-Fluorophenol 50.9 Limits: 35-115%04/28/21 17:091 JMV V3638
Surrogate: Nitrobenzene-d5 58.4 Limits: 37-122%04/28/21 17:091 JMV V3638
Surrogate: 4-Terphenyl-d14 67.3 Limits: 54-127%04/28/21 17:091 JMV V3638
Surrogate: 2,4,6-Tribromophenol 65.8 Limits: 39-132%04/28/21 17:091 JMV V3638
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 55 of 96
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172Tel: [phone] Fax: [phone] www.pacelabs.com
Report of Analysis
Waypoint Analytical
PO Box 240543Charlotte, NC 28224Attention: Angela Overcash
Project Name: 21-113-0038
Lot Number:WD26034
Date Completed:04/30/2021
04/30/2021 4:27 PMApproved and released by:
Project Manager II:Lucas Odom
Page 1 of 20
Page 56 of 96
PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Case Narrative
Waypoint Analytical
Lot Number: WD26034
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header informationassociated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page ordiscussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on thecover page.
Hexavalent Chromium
The method blank associated with batch 90350 yielded a '"J" value detection for the target compound. No
corrective action is required as this is an estimated value recovered below the LOQ. Associateddetections have been qualified with a "B".
Page 2 of 20
Page 57 of 96
PACE ANALYTICAL SERVICES, LLC
Sample Summary
Waypoint Analytical
Lot Number: WD26034

Sample Number Sample ID Matrix Date Sampled Date Received
001 04/23/2021 1230S-1 Solid 04/26/2021
002 04/23/2021 1230S-2 Solid 04/26/2021
003 04/23/2021 1340S-3 Solid 04/26/2021
004 04/23/2021 1250S-4 Solid 04/26/2021
005 04/23/2021 1235Busy-1 Solid 04/26/2021
006 04/23/2021 1350Busy-2 Solid 04/26/2021
(6 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 3 of 20
PACE ANALYTICAL SERVICES, LLC
Detection Summary
Waypoint Analytical
Lot Number: WD26034

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 S-1 Solid Hexavalent Chromium 7199 0.36 J mg/kg 5
002 S-2 Solid Hexavalent Chromium 7199 0.53 J mg/kg 6
003 S-3 Solid Hexavalent Chromium 7199 0.31 J mg/kg 7
005 Busy-1 Solid Hexavalent Chromium 7199 1.0 BJ mg/kg 9
006 Busy-2 Solid Hexavalent Chromium 7199 0.70 BJ mg/kg 10
(5 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 4 of 20
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S-1
WD26034-001
04/23/2021 1230
04/26/2021
Solid
% Solids:85.8 04/26/2021 2343
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 04/29/2021 0045 AMR 04/28/2021 1252 90349
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.36 J 1mg/kg0.231.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 5 of 20
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S-2
WD26034-002
04/23/2021 1230
04/26/2021
Solid
% Solids:81.2 04/26/2021 2343
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 04/29/2021 0058 AMR 04/28/2021 1252 90349
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.53 J 1mg/kg0.251.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 6 of 20
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S-3
WD26034-003
04/23/2021 1340
04/26/2021
Solid
% Solids:98.1 04/26/2021 2343
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 04/29/2021 0111 AMR 04/28/2021 1252 90349
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.31 J 1mg/kg0.201.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 7 of 20
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
S-4
WD26034-004
04/23/2021 1250
04/26/2021
Solid
% Solids:94.7 04/26/2021 2343
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 04/29/2021 0216 AMR 04/28/2021 1252 90349
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 ND 1mg/kg0.211.1
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 8 of 20
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
Busy-1
WD26034-005
04/23/2021 1235
04/26/2021
Solid
% Solids:64.6 04/26/2021 2343
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
3 3060A (Hexavalent C) 7199 1 04/30/2021 1242 AMR 04/29/2021 1139 90350
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 1.0 BJ 3mg/kg0.311.5
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 9 of 20
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Waypoint Analytical
Busy-2
WD26034-006
04/23/2021 1350
04/26/2021
Solid
% Solids:90.3 04/26/2021 2343
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3060A (Hexavalent C) 7199 1 04/29/2021 1905 AMR 04/29/2021 1139 90350
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Hexavalent Chromium 18540-29-9 7199 0.70 BJ 1mg/kg0.221.1
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 10 of 20
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 11 of 20
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ90349-001
90349 3060A
04/28/2021 1252Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium ND 04/28/2021 19341.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 12 of 20
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ90349-002
90349 3060A
04/28/2021 1252Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 11 04/28/2021 19471091080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 13 of 20
Inorganic non-metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:WD26034-003MS
90349 3060A
04/28/2021 1252Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
Limit
Sample
Amount
Dil(mg/kg) (mg/kg) (mg/kg)
Hexavalent Chromium 7.9 04/29/2021 0124751075-1250.31 1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 14 of 20
Inorganic non-metals - MSD
Batch:Prep Method:
Prep Date:
Sample ID:WD26034-003MD
90349 3060A
04/28/2021 1252Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
%Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/kg) (mg/kg) (mg/kg)
Hexavalent Chromium 9.1 04/29/2021 0203861075-12513 200.31 1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 15 of 20
Inorganic non-metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:WQ90350-001
90350 3060A
04/29/2021 1139Analytical Method:7199
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexavalent Chromium 0.22 04/29/2021 1839J 1.0 0.20 mg/kg1
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 16 of 20
Inorganic non-metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:WQ90350-002
90350 3060A
04/29/2021 1139Analytical Method:7199
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
%Rec
LimitDil(mg/kg) (mg/kg)
Hexavalent Chromium 9.4 04/29/2021 1852941080-1201
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
_DL = Detection Limit
* = RSD is out of criteria
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 17 of 20
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 18 of 20
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 19 of 20
PACE ANALYTICAL SERVICES, LLC

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)

Page 20 of 20
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Metals Analyses
6020B
V3584QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V3530
Associated Lab Samples: 97536, 97537, 97538, 97539, 97540, 97541
LRB-V3530 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/27/21 00:030.1000.0940<0.0940mg/KgArsenic
04/27/21 00:0310.01.40<1.40mg/KgBarium
04/27/21 00:030.5000.0550<0.0550mg/KgCadmium
04/27/21 00:031.000.290<0.290mg/KgChromium
04/27/21 00:031.000.140<0.140mg/KgLead
04/27/21 00:032.000.900<0.900mg/KgSelenium
04/27/21 00:030.5000.0410<0.0410mg/KgSilver
LCS-V3530Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
98.012.212.5mg/KgArsenic 80-120
10312.912.5mg/KgBarium 80-120
10312.912.5mg/KgCadmium 80-120
99.012.412.5mg/KgChromium 80-120
10312.912.5mg/KgLead 80-120
10212.812.5mg/KgSelenium 80-120
1015.055.00mg/KgSilver 80-120
V 97589-MS-V3530 V 97589-MSD-V3530Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
12.5 98.012.312.512.50.203mg/KgArsenic 97.0 75-125 1.6 20
18.1 145*18.412.512.56.32mg/KgBarium 147*75-125 1.6 20
28.5 92.028.612.512.517.0mg/KgCadmium 93.0 75-125 0.3 20
13.8 97.013.412.512.51.73mg/KgChromium 93.0 75-125 2.9 20
Page 1 of 19* QC Fail Date:05/03/2021 11:05 AM
Page 76 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Metals Analyses
6020B
V3584QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V3530
V 97589-MS-V3530 V 97589-MSD-V3530Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
82.9 66.0*78.512.512.574.6mg/KgLead 31.0*75-125 5.4 20
12.8 10213.012.512.5<0.900mg/KgSelenium 104 75-125 1.5 20
7.92 1037.655.005.002.75mg/KgSilver 98.0 75-125 3.4 20
V 97589-PDS-V3530Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/27/21 00:4897.012.3mg/KgArsenic
04/27/21 00:4812515.6mg/KgBarium
04/27/21 00:4810121.3mg/KgCadmium
04/27/21 00:4896.012.9mg/KgChromium
04/27/21 00:4899.049.5mg/KgLead
04/27/21 00:4810212.8mg/KgSelenium
04/27/21 00:4810214.2mg/KgSilver
Page 2 of 19* QC Fail Date:05/03/2021 11:05 AM
Page 77 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V3604QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V3560
Associated Lab Samples: 97536, 97537, 97538, 97539, 97540, 97541
LRB-V3560 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/27/21 15:100.05000.0150<0.0150mg/KgMercury (Total)
LCS-V3560Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1040.4320.417mg/KgMercury (Total)80-120
V 97360-MS-V3560 V 97360-MSD-V3560Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.450 1080.4470.4170.4170.0204mg/KgMercury (Total)107 80-120 0.6 20
V 97360-PDS-V3560Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/27/21 15:321120.232mg/KgMercury (Total)
Page 3 of 19Date:05/03/2021 11:05 AM
Page 78 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3552
Associated Lab Samples: 97536, 97537, 97538, 97539, 97540, 97541
LRB-V3552 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/26/21 12:100.0200.002<0.002mg/KgAcetone
04/26/21 12:100.0200.001<0.001mg/KgAcrolein
04/26/21 12:100.0200.0008<0.0008mg/KgAcrylonitrile
04/26/21 12:100.0050.0006<0.0006mg/KgBenzene
04/26/21 12:100.0050.0005<0.0005mg/KgBromobenzene
04/26/21 12:100.0050.0008<0.0008mg/KgBromochloromethane
04/26/21 12:100.0050.001<0.001mg/KgBromodichloromethane
04/26/21 12:100.0050.001<0.001mg/KgBromoform
04/26/21 12:100.0100.001<0.001mg/KgBromomethane
04/26/21 12:100.0050.0005<0.0005mg/Kgn-Butylbenzene
04/26/21 12:100.0050.0006<0.0006mg/Kgsec-Butyl benzene
04/26/21 12:100.0050.0005<0.0005mg/Kgtert-Butyl benzene
04/26/21 12:100.0050.0006<0.0006mg/KgCarbon Disulfide
04/26/21 12:100.0050.001<0.001mg/KgCarbon Tetrachloride
04/26/21 12:100.0050.0007<0.0007mg/KgChlorobenzene
04/26/21 12:100.0050.0009<0.0009mg/KgChlorodibromomethane
04/26/21 12:100.0100.0009<0.0009mg/KgChloroethane
04/26/21 12:100.0050.001<0.001mg/KgChloroform
04/26/21 12:100.0100.0006<0.0006mg/KgChloromethane
04/26/21 12:100.0050.0005<0.0005mg/Kg2-Chlorotoluene
04/26/21 12:100.0050.0004<0.0004mg/Kg4-Chlorotoluene
04/26/21 12:100.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
04/26/21 12:100.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
04/26/21 12:100.0050.0006<0.0006mg/Kg1,2-Dibromoethane
04/26/21 12:100.0050.0006<0.0006mg/KgDibromomethane
04/26/21 12:100.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
04/26/21 12:100.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 19Date:05/03/2021 11:05 AM
Page 79 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3552
Associated Lab Samples: 97536, 97537, 97538, 97539, 97540, 97541
LRB-V3552 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/26/21 12:100.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
04/26/21 12:100.0100.001<0.001mg/KgDichlorodifluoromethane
04/26/21 12:100.0050.0008<0.0008mg/Kg1,1-Dichloroethane
04/26/21 12:100.0050.001<0.001mg/Kg1,2-Dichloroethane
04/26/21 12:100.0050.0007<0.0007mg/Kg1,1-Dichloroethene
04/26/21 12:100.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
04/26/21 12:100.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
04/26/21 12:100.0050.0004<0.0004mg/Kg1,2-Dichloropropane
04/26/21 12:100.0050.0006<0.0006mg/Kg1,3-Dichloropropane
04/26/21 12:100.0050.001<0.001mg/Kg2,2-Dichloropropane
04/26/21 12:100.0050.0008<0.0008mg/Kg1,1-Dichloropropene
04/26/21 12:100.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
04/26/21 12:100.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
04/26/21 12:100.0050.0006<0.0006mg/KgEthylbenzene
04/26/21 12:100.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
04/26/21 12:100.0100.0008<0.0008mg/KgHexachlorobutadiene
04/26/21 12:100.0100.0007<0.0007mg/Kgn-Hexane
04/26/21 12:100.0200.0006<0.0006mg/Kg2-Hexanone
04/26/21 12:100.0050.0005<0.0005mg/KgIsopropylbenzene
04/26/21 12:100.0050.001<0.001mg/Kg4-Isopropyl toluene
04/26/21 12:100.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
04/26/21 12:100.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
04/26/21 12:100.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
04/26/21 12:100.0100.001<0.001mg/KgMethylene Chloride
04/26/21 12:100.0100.0010<0.0010mg/KgNaphthalene
04/26/21 12:100.0050.0005<0.0005mg/Kgn-Propylbenzene
04/26/21 12:100.0050.001<0.001mg/KgStyrene
Page 5 of 19Date:05/03/2021 11:05 AM
Page 80 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3552
Associated Lab Samples: 97536, 97537, 97538, 97539, 97540, 97541
LRB-V3552 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/26/21 12:100.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
04/26/21 12:100.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
04/26/21 12:100.0050.0009<0.0009mg/KgTetrachloroethene
04/26/21 12:100.0050.0007<0.0007mg/KgToluene
04/26/21 12:100.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
04/26/21 12:100.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
04/26/21 12:100.0050.001<0.001mg/Kg1,1,1-Trichloroethane
04/26/21 12:100.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
04/26/21 12:100.0050.0009<0.0009mg/KgTrichloroethene
04/26/21 12:100.0100.002<0.002mg/KgTrichlorofluoromethane
04/26/21 12:100.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
04/26/21 12:100.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
04/26/21 12:100.0100.0005<0.0005mg/KgVinyl Acetate
04/26/21 12:100.0100.0005<0.0005mg/KgVinyl Chloride
04/26/21 12:100.0050.0005<0.0005mg/Kgo-Xylene
04/26/21 12:100.0100.001<0.001mg/Kgm,p-Xylene
04/26/21 12:104-Bromofluorobenzene (S)97.4 70-130
04/26/21 12:10Dibromofluoromethane (S)101 84-123
04/26/21 12:10Toluene-d8 (S)98.6 76-129
LCS-V3552 LCSD-V3552Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.106 1061050.1050.100mg/KgAcetone 29-198 0.9 20
0.110 1101080.1080.100mg/KgAcrolein 70-130 1.8 20
0.104 1041020.1020.100mg/KgAcrylonitrile 65-134 1.9 20
Page 6 of 19Date:05/03/2021 11:05 AM
Page 81 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3552
LCS-V3552 LCSD-V3552Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 92.495.20.0470.050mg/KgBenzene 74-127 2.9 20
0.047 94.095.20.0470.050mg/KgBromobenzene 73-125 1.2 20
0.048 97.895.40.0470.050mg/KgBromochloromethane 72-134 2.4 20
0.048 97.497.80.0480.050mg/KgBromodichloromethane 75-122 0.4 20
0.051 10298.80.0490.050mg/KgBromoform 66-135 3.3 20
0.051 10393.60.0460.050mg/KgBromomethane 20-180 9.5 20
0.046 93.81000.0500.050mg/Kgn-Butylbenzene 65-135 6.5 20
0.045 91.498.00.0490.050mg/Kgsec-Butyl benzene 66-131 6.9 20
0.045 90.496.40.0480.050mg/Kgtert-Butyl benzene 67-132 6.4 20
0.044 88.894.80.0470.050mg/KgCarbon Disulfide 61-129 6.5 20
0.045 91.097.40.0480.050mg/KgCarbon Tetrachloride 64-143 6.7 20
0.047 95.494.00.0470.050mg/KgChlorobenzene 74-118 1.4 20
0.049 99.296.00.0480.050mg/KgChlorodibromomethane 73-122 3.2 20
0.045 91.091.20.0450.050mg/KgChloroethane 33-149 0.2 20
0.046 92.696.60.0480.050mg/KgChloroform 73-127 4.2 20
0.045 91.895.80.0470.050mg/KgChloromethane 45-143 4.2 20
0.046 93.899.80.0490.050mg/Kg2-Chlorotoluene 67-124 6.1 20
0.046 93.01050.0520.050mg/Kg4-Chlorotoluene 71-126 12.3 20
0.048 96.899.40.0490.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.6 20
0.052 1051030.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.9 20
0.049 99.897.20.0480.050mg/Kg1,2-Dibromoethane 70-132 2.6 20
0.049 98.298.60.0490.050mg/KgDibromomethane 74-133 0.4 20
0.046 93.297.20.0480.050mg/Kg1,2-Dichlorobenzene 72-123 4.2 20
0.046 93.696.60.0480.050mg/Kg1,3-Dichlorobenzene 71-120 3.1 20
0.047 95.097.80.0480.050mg/Kg1,4-Dichlorobenzene 71-123 2.9 20
0.042 84.692.80.0460.050mg/KgDichlorodifluoromethane 26-146 9.2 20
Page 7 of 19Date:05/03/2021 11:05 AM
Page 82 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3552
LCS-V3552 LCSD-V3552Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 93.297.20.0480.050mg/Kg1,1-Dichloroethane 74-127 4.2 20
0.048 96.298.00.0490.050mg/Kg1,2-Dichloroethane 68-128 1.8 20
0.044 89.299.00.0490.050mg/Kg1,1-Dichloroethene 67-149 10.4 20
0.046 92.296.20.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 4.2 20
0.045 90.694.20.0470.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.8 20
0.047 94.897.40.0480.050mg/Kg1,2-Dichloropropane 73-130 2.7 20
0.049 98.496.80.0480.050mg/Kg1,3-Dichloropropane 75-124 1.6 20
0.046 92.699.60.0490.050mg/Kg2,2-Dichloropropane 50-142 7.2 20
0.045 91.294.00.0470.050mg/Kg1,1-Dichloropropene 71-130 3.0 20
0.050 10199.20.0490.050mg/Kgcis-1,3-Dichloropropene 71-125 1.4 20
0.051 1041030.0510.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.1 20
0.046 92.694.00.0470.050mg/KgEthylbenzene 74-128 1.5 20
0.099 99.499.80.0990.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.4 20
0.046 93.699.80.0490.050mg/KgHexachlorobutadiene 64-125 6.4 20
0.045 91.699.20.0490.050mg/Kgn-Hexane 70-130 7.9 20
0.055 1111050.0520.050mg/Kg2-Hexanone 61-157 5.7 20
0.045 90.898.80.0490.050mg/KgIsopropylbenzene 68-126 8.4 20
0.046 93.099.20.0490.050mg/Kg4-Isopropyl toluene 68-129 6.4 20
0.052 1051050.0520.050mg/KgMethyl Ethyl Ketone (MEK)63-149 0.5 20
0.050 10098.40.0490.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.8 20
0.054 1081050.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 3.3 20
0.046 92.292.40.0460.050mg/KgMethylene Chloride 74-129 0.2 20
0.049 99.41000.0500.050mg/KgNaphthalene 57-157 0.8 20
0.046 92.299.20.0490.050mg/Kgn-Propylbenzene 67-130 7.3 20
0.047 95.492.20.0460.050mg/KgStyrene 77-121 3.4 20
0.048 96.894.60.0470.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 2.2 20
Page 8 of 19Date:05/03/2021 11:05 AM
Page 83 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V3553QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V3552
LCS-V3552 LCSD-V3552Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.048 97.296.20.0480.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.0 20
0.045 90.096.20.0480.050mg/KgTetrachloroethene 68-130 6.6 20
0.045 90.094.20.0470.050mg/KgToluene 71-129 4.5 20
0.048 96.699.80.0490.050mg/Kg1,2,3-Trichlorobenzene 68-130 3.2 20
0.049 98.698.80.0490.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.2 20
0.044 89.897.00.0480.050mg/Kg1,1,1-Trichloroethane 67-131 7.7 20
0.049 99.693.60.0460.050mg/Kg1,1,2-Trichloroethane 70-133 6.2 20
0.046 93.898.00.0490.050mg/KgTrichloroethene 75-133 4.3 20
0.045 90.61010.0500.050mg/KgTrichlorofluoromethane 44-146 11.0 20
0.050 10099.00.0490.050mg/Kg1,2,3-Trichloropropane 60-137 1.2 20
0.045 90.898.80.0490.050mg/Kg1,3,5-Trimethylbenzene 69-128 8.4 20
0.052 1061060.0520.050mg/KgVinyl Acetate 85-161 0.0 20
0.045 90.695.00.0470.050mg/KgVinyl Chloride 48-147 4.7 20
0.047 94.294.00.0470.050mg/Kgo-Xylene 74-126 0.2 20
0.094 94.695.70.0950.100mg/Kgm,p-Xylene 75-124 1.1 20
99.099.24-Bromofluorobenzene (S)70-130
10199.4Dibromofluoromethane (S)84-123
10299.4Toluene-d8 (S)76-129
Page 9 of 19Date:05/03/2021 11:05 AM
Page 84 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3638QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3558
Associated Lab Samples: 97536, 97537, 97538, 97539, 97540, 97541
LRB-V3558 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/28/21 10:250.6600.015<0.015mg/KgAcenaphthene
04/28/21 10:250.6600.013<0.013mg/KgAcenaphthylene
04/28/21 10:250.6600.163<0.163mg/KgAniline
04/28/21 10:250.6600.007<0.007mg/KgAnthracene
04/28/21 10:250.6600.007<0.007mg/KgBenzo(a)anthracene
04/28/21 10:250.6600.005<0.005mg/KgBenzo(a)pyrene
04/28/21 10:250.6600.006<0.006mg/KgBenzo(b)fluoranthene
04/28/21 10:250.6600.006<0.006mg/KgBenzo(g,h,i)perylene
04/28/21 10:250.6600.007<0.007mg/KgBenzo(k)fluoranthene
04/28/21 10:252.000.548<0.548mg/KgBenzoic Acid
04/28/21 10:250.6600.124<0.124mg/KgBenzyl alcohol
04/28/21 10:250.6600.126<0.126mg/KgBis(2-Chloroethoxy)methane
04/28/21 10:250.6600.106<0.106mg/KgBis(2-Chloroethyl)ether
04/28/21 10:250.3300.118<0.118mg/KgBis(2-Chloroisopropyl)ether
04/28/21 10:250.6600.149<0.149mg/KgBis(2-ethylhexyl)phthalate
04/28/21 10:250.6600.155<0.155mg/Kg4-Bromophenyl phenyl ether
04/28/21 10:250.3300.114<0.114mg/KgButyl benzyl phthalate
04/28/21 10:250.6600.126<0.126mg/Kg4-Chloro-3-methylphenol
04/28/21 10:250.3300.080<0.080mg/Kg4-Chloroaniline
04/28/21 10:250.6600.161<0.161mg/Kg2-Chloronaphthalene
04/28/21 10:250.6600.126<0.126mg/Kg2-Chlorophenol
04/28/21 10:251.000.202<0.202mg/Kg4-Chlorophenyl phenyl ether
04/28/21 10:250.6600.007<0.007mg/KgChrysene
04/28/21 10:250.6600.019<0.019mg/KgDibenz(a,h)anthracene
04/28/21 10:250.6600.017<0.017mg/KgDibenzofuran
04/28/21 10:250.6600.107<0.107mg/Kg1,2-Dichlorobenzene
04/28/21 10:250.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 10 of 19Date:05/03/2021 11:05 AM
Page 85 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3638QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3558
Associated Lab Samples: 97536, 97537, 97538, 97539, 97540, 97541
LRB-V3558 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/28/21 10:250.3300.104<0.104mg/Kg1,4-Dichlorobenzene
04/28/21 10:250.6600.131<0.131mg/Kg3,3'-Dichlorobenzidine
04/28/21 10:250.6600.129<0.129mg/Kg2,4-Dichlorophenol
04/28/21 10:250.6600.170<0.170mg/KgDiethyl phthalate
04/28/21 10:250.6600.158<0.158mg/KgDimethyl phthalate
04/28/21 10:250.3300.137<0.137mg/Kg2,4-Dimethylphenol
04/28/21 10:250.6600.164<0.164mg/KgDi-n-butyl phthalate
04/28/21 10:251.500.364<0.364mg/Kg4,6-Dinitro-2-methylphenol
04/28/21 10:251.500.387<0.387mg/Kg2,4-Dinitrophenol
04/28/21 10:250.6600.175<0.175mg/Kg2,4-Dinitrotoluene
04/28/21 10:250.6600.171<0.171mg/Kg2,6-Dinitrotoluene
04/28/21 10:250.3300.171<0.171mg/KgDi-n-Octyl Phthalate
04/28/21 10:250.6600.007<0.007mg/KgFluoranthene
04/28/21 10:250.6600.014<0.014mg/KgFluorene
04/28/21 10:250.6600.145<0.145mg/KgHexachlorobenzene
04/28/21 10:250.6600.149<0.149mg/KgHexachlorobutadiene
04/28/21 10:250.6600.227<0.227mg/KgHexachlorocyclopentadiene
04/28/21 10:250.6600.104<0.104mg/KgHexachloroethane
04/28/21 10:250.6600.018<0.018mg/KgIndeno(1,2,3-cd)pyrene
04/28/21 10:250.6600.142<0.142mg/KgIsophorone
04/28/21 10:250.6600.010<0.010mg/Kg1-Methylnaphthalene
04/28/21 10:250.6600.012<0.012mg/Kg2-Methylnaphthalene
04/28/21 10:250.6600.126<0.126mg/Kg2-Methylphenol
04/28/21 10:250.6600.143<0.143mg/Kg3&4 Methylphenol
04/28/21 10:250.6600.014<0.014mg/KgNaphthalene
04/28/21 10:250.6600.142<0.142mg/Kg2-Nitroaniline
04/28/21 10:250.6600.120<0.120mg/Kg3-Nitroaniline
Page 11 of 19Date:05/03/2021 11:05 AM
Page 86 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3638QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3558
Associated Lab Samples: 97536, 97537, 97538, 97539, 97540, 97541
LRB-V3558 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/28/21 10:250.3300.103<0.103mg/Kg4-Nitroaniline
04/28/21 10:250.3300.140<0.140mg/KgNitrobenzene
04/28/21 10:250.6600.110<0.110mg/Kg2-Nitrophenol
04/28/21 10:250.6600.163<0.163mg/Kg4-Nitrophenol
04/28/21 10:250.1700.005<0.005mg/KgN-Nitrosodimethylamine
04/28/21 10:250.6600.181<0.181mg/KgN-Nitrosodiphenylamine
04/28/21 10:250.6600.152<0.152mg/KgN-Nitroso-di-n-propylamine
04/28/21 10:251.000.421<0.421mg/KgPentachlorophenol
04/28/21 10:250.6600.007<0.007mg/KgPhenanthrene
04/28/21 10:250.6600.108<0.108mg/KgPhenol
04/28/21 10:250.6600.009<0.009mg/KgPyrene
04/28/21 10:250.3300.063<0.063mg/KgPyridine
04/28/21 10:250.6600.117<0.117mg/Kg1,2,4-Trichlorobenzene
04/28/21 10:250.6600.140<0.140mg/Kg2,4,5-Trichlorophenol
04/28/21 10:250.6600.160<0.160mg/Kg2,4,6-Trichlorophenol
04/28/21 10:252-Fluorobiphenyl (S)109 44-115
04/28/21 10:252-Fluorophenol (S)86.7 35-115
04/28/21 10:25Nitrobenzene-d5 (S)99.4 37-122
04/28/21 10:254-Terphenyl-d14 (S)115 54-127
04/28/21 10:252,4,6-Tribromophenol (S)112 39-132
04/28/21 10:25Phenol-d5 (S)90.3 34-121
LCS-V3558Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
83.81.401.67mg/KgAcenaphthene 40-123
92.21.541.67mg/KgAcenaphthylene 32-132
Page 12 of 19Date:05/03/2021 11:05 AM
Page 87 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3638QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3558
LCS-V3558Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1141.901.67mg/KgAniline 12-197
95.21.591.67mg/KgAnthracene 47-123
92.21.541.67mg/KgBenzo(a)anthracene 49-126
1091.821.67mg/KgBenzo(a)pyrene 45-129
93.41.561.67mg/KgBenzo(b)fluoranthene 45-132
92.21.541.67mg/KgBenzo(g,h,i)perylene 43-134
91.01.521.67mg/KgBenzo(k)fluoranthene 47-132
0.0*1.091.67mg/KgBenzoic Acid 10-83
89.81.501.67mg/KgBenzyl alcohol 29-122
89.21.491.67mg/KgBis(2-Chloroethoxy)methane 36-121
69.41.161.67mg/KgBis(2-Chloroethyl)ether 31-120
79.01.321.67mg/KgBis(2-Chloroisopropyl)ether 33-131
88.01.471.67mg/KgBis(2-ethylhexyl)phthalate 51-133
92.81.551.67mg/Kg4-Bromophenyl phenyl ether 46-124
85.61.431.67mg/KgButyl benzyl phthalate 48-132
67.01.121.67mg/Kg4-Chloro-3-methylphenol 45-122
74.21.241.67mg/Kg4-Chloroaniline 17-106
73.61.231.67mg/Kg2-Chloronaphthalene 41-114
69.41.161.67mg/Kg2-Chlorophenol 34-121
89.81.501.67mg/Kg4-Chlorophenyl phenyl ether 45-121
92.21.541.67mg/KgChrysene 50-124
85.61.431.67mg/KgDibenz(a,h)anthracene 45-134
82.61.381.67mg/KgDibenzofuran 44-120
64.61.081.67mg/Kg1,2-Dichlorobenzene 33-117
63.41.061.67mg/Kg1,3-Dichlorobenzene 30-115
64.01.071.67mg/Kg1,4-Dichlorobenzene 31-115
94.01.571.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 13 of 19* QC Fail Date:05/03/2021 11:05 AM
Page 88 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3638QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3558
LCS-V3558Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
65.81.101.67mg/Kg2,4-Dichlorophenol 40-122
85.61.431.67mg/KgDiethyl phthalate 50-124
80.81.351.67mg/KgDimethyl phthalate 48-124
71.21.191.67mg/Kg2,4-Dimethylphenol 30-127
93.41.561.67mg/KgDi-n-butyl phthalate 51-128
0.0*1.171.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
0.0*1.281.67mg/Kg2,4-Dinitrophenol 27-129
89.81.501.67mg/Kg2,4-Dinitrotoluene 48-126
89.21.491.67mg/Kg2,6-Dinitrotoluene 46-124
83.21.391.67mg/KgDi-n-Octyl Phthalate 45-140
95.21.591.67mg/KgFluoranthene 50-127
91.61.531.67mg/KgFluorene 43-125
88.01.471.67mg/KgHexachlorobenzene 45-122
65.21.091.67mg/KgHexachlorobutadiene 32-123
66.41.111.67mg/KgHexachlorocyclopentadiene 32-117
63.41.061.67mg/KgHexachloroethane 28-117
91.61.531.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
66.41.111.67mg/KgIsophorone 30-122
76.61.281.67mg/Kg1-Methylnaphthalene 40-119
73.01.221.67mg/Kg2-Methylnaphthalene 38-122
73.61.231.67mg/Kg2-Methylphenol 32-122
64.01.071.67mg/Kg3&4 Methylphenol 34-119
71.81.201.67mg/KgNaphthalene 35-123
88.61.481.67mg/Kg2-Nitroaniline 44-127
88.01.471.67mg/Kg3-Nitroaniline 33-119
92.21.541.67mg/Kg4-Nitroaniline 63-147
70.61.181.67mg/KgNitrobenzene 34-122
Page 14 of 19* QC Fail Date:05/03/2021 11:05 AM
Page 89 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3638QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3558
LCS-V3558Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
59.81.001.67mg/Kg2-Nitrophenol 36-123
80.81.351.67mg/Kg4-Nitrophenol 30-132
55.30.9251.67mg/KgN-Nitrosodimethylamine 10-146
1051.751.67mg/KgN-Nitrosodiphenylamine 38-127
79.01.321.67mg/KgN-Nitroso-di-n-propylamine 36-120
96.41.611.67mg/KgPentachlorophenol 25-133
92.81.551.67mg/KgPhenanthrene 50-121
68.81.151.67mg/KgPhenol 34-121
94.01.571.67mg/KgPyrene 47-127
42.70.7141.67mg/KgPyridine 10-80
61.61.031.67mg/Kg1,2,4-Trichlorobenzene 34-118
71.21.191.67mg/Kg2,4,5-Trichlorophenol 41-124
73.01.221.67mg/Kg2,4,6-Trichlorophenol 39-126
88.62-Fluorobiphenyl (S)44-115
72.02-Fluorophenol (S)35-115
72.4Nitrobenzene-d5 (S)37-122
90.44-Terphenyl-d14 (S)54-127
88.22,4,6-Tribromophenol (S)39-132
72.0Phenol-d5 (S)34-121
V 97540-MS-V3558 V 97540-MSD-V3558Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.16 68.61.161.641.69<0.015mg/KgAcenaphthene 70.7 40-123 0.0 20
1.30 76.91.301.641.690.024mg/KgAcenaphthylene 79.2 32-132 0.0 20
0.631 0.0*0.4111.641.69<0.165mg/KgAniline 0.0*12-197 0.0 20
Page 15 of 19* QC Fail Date:05/03/2021 11:05 AM
Page 90 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3638QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3558
V 97540-MS-V3558 V 97540-MSD-V3558Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.32 78.11.291.641.690.054mg/KgAnthracene 78.6 47-123 2.2 20
1.33 78.61.251.641.690.256mg/KgBenzo(a)anthracene 76.2 49-126 6.2 20
1.48 87.51.361.641.690.232mg/KgBenzo(a)pyrene 82.9 45-129 8.4 20
1.32 78.11.261.641.690.288mg/KgBenzo(b)fluoranthene 76.8 45-132 4.6 20
1.19 70.41.021.641.69<0.006mg/KgBenzo(g,h,i)perylene 62.1 43-134 15.3 20
1.28 75.71.181.641.690.084mg/KgBenzo(k)fluoranthene 71.9 47-132 8.1 20
<0.556 0.0*<0.5481.641.69<0.556mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.24 73.31.271.641.69<0.126mg/KgBenzyl alcohol 77.4 29-122 2.3 20
1.22 72.11.241.641.69<0.128mg/KgBis(2-Chloroethoxy)methane 75.6 36-121 1.6 20
1.03 60.91.181.641.69<0.108mg/KgBis(2-Chloroethyl)ether 71.9 31-120 13.5 20
0.993 58.70.9931.641.69<0.120mg/KgBis(2-Chloroisopropyl)ether 60.5 33-131 0.0 20
1.28 75.71.261.641.69<0.151mg/KgBis(2-ethylhexyl)phthalate 76.8 51-133 1.5 20
1.39 82.21.381.641.69<0.157mg/Kg4-Bromophenyl phenyl ether 84.1 46-124 0.7 20
1.15 68.01.171.641.69<0.116mg/KgButyl benzyl phthalate 71.3 48-132 1.7 20
0.930 55.00.9221.641.69<0.128mg/Kg4-Chloro-3-methylphenol 56.2 45-122 0.8 20
0.697 41.20.6441.641.69<0.081mg/Kg4-Chloroaniline 39.2 17-106 7.9 20
1.06 62.71.061.641.69<0.163mg/Kg2-Chloronaphthalene 64.6 41-114 0.0 20
0.910 53.80.9261.641.69<0.128mg/Kg2-Chlorophenol 56.4 34-121 1.7 20
1.33 78.61.311.641.69<0.206mg/Kg4-Chlorophenyl phenyl ether 79.8 45-121 1.5 20
1.33 78.61.241.641.690.242mg/KgChrysene 75.6 50-124 7.0 20
1.13 66.81.011.641.69<0.019mg/KgDibenz(a,h)anthracene 61.5 45-134 11.2 20
1.21 71.51.221.641.690.024mg/KgDibenzofuran 74.3 44-120 0.8 20
0.890 52.60.8921.641.69<0.109mg/Kg1,2-Dichlorobenzene 54.3 33-117 0.2 20
0.884 52.30.8651.641.69<0.098mg/Kg1,3-Dichlorobenzene 52.7 30-115 2.1 20
0.872 51.50.8751.641.69<0.106mg/Kg1,4-Dichlorobenzene 53.3 31-115 0.3 20
0.228 0.0*0.1681.641.69<0.133mg/Kg3,3'-Dichlorobenzidine 0.0*22-121 0.0 20
Page 16 of 19* QC Fail Date:05/03/2021 11:05 AM
Page 91 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3638QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3558
V 97540-MS-V3558 V 97540-MSD-V3558Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.928 54.90.9521.641.69<0.131mg/Kg2,4-Dichlorophenol 58.0 40-122 2.5 20
1.25 73.91.241.641.69<0.173mg/KgDiethyl phthalate 75.6 50-124 0.8 20
1.18 69.81.191.641.69<0.160mg/KgDimethyl phthalate 72.5 48-124 0.8 30
0.908 53.70.9191.641.69<0.139mg/Kg2,4-Dimethylphenol 56.0 30-127 1.2 20
1.32 78.11.311.641.69<0.166mg/KgDi-n-butyl phthalate 79.8 51-128 0.7 20
0.448 0.0*0.3921.641.69<0.369mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
<0.392 0.0*<0.3871.641.69<0.392mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.22 72.11.211.641.69<0.178mg/Kg2,4-Dinitrotoluene 73.7 48-126 0.8 20
1.26 74.51.261.641.69<0.174mg/Kg2,6-Dinitrotoluene 76.8 46-124 0.0 20
1.18 69.81.131.641.69<0.174mg/KgDi-n-Octyl Phthalate 68.9 45-140 4.3 20
1.41 83.41.311.641.69<0.007mg/KgFluoranthene 79.8 50-127 7.3 20
1.31 77.51.311.641.69<0.014mg/KgFluorene 79.8 43-125 0.0 20
1.34 79.21.281.641.69<0.147mg/KgHexachlorobenzene 78.0 45-122 4.5 20
0.983 58.10.9821.641.69<0.151mg/KgHexachlorobutadiene 59.8 32-123 0.1 20
<0.230 0.0*<0.2271.641.69<0.230mg/KgHexachlorocyclopentadiene 0.0*32-117 0.0 20
0.765 45.20.7601.641.69<0.106mg/KgHexachloroethane 46.3 28-117 0.6 20
1.21 71.51.041.641.690.127mg/KgIndeno(1,2,3-cd)pyrene 63.4 45-133 15.1 20
0.917 54.20.9131.641.69<0.144mg/KgIsophorone 55.6 30-122 0.4 20
1.12 66.21.111.641.690.035mg/Kg1-Methylnaphthalene 67.6 40-119 0.8 20
1.09 64.41.061.641.690.048mg/Kg2-Methylnaphthalene 64.6 38-122 2.7 20
0.931 55.00.8981.641.69<0.128mg/Kg2-Methylphenol 54.7 32-122 3.6 20
0.852 50.40.8601.641.69<0.145mg/Kg3&4 Methylphenol 52.4 34-119 0.9 20
1.09 64.41.051.641.690.065mg/KgNaphthalene 64.0 35-123 3.7 20
1.10 65.01.141.641.69<0.144mg/Kg2-Nitroaniline 69.5 44-127 3.5 20
0.885 52.30.8841.641.69<0.122mg/Kg3-Nitroaniline 53.9 33-119 0.1 20
0.720 42.6*0.7351.641.69<0.105mg/Kg4-Nitroaniline 44.8*63-147 2.0 20
Page 17 of 19* QC Fail Date:05/03/2021 11:05 AM
Page 92 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V3638QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V3558
V 97540-MS-V3558 V 97540-MSD-V3558Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.927 54.80.9501.641.69<0.142mg/KgNitrobenzene 57.9 34-122 2.4 20
0.774 45.70.8061.641.69<0.112mg/Kg2-Nitrophenol 49.1 32-123 4.0 20
0.808 47.80.8611.641.69<0.165mg/Kg4-Nitrophenol 52.5 30-132 6.3 20
0.666 39.40.6421.641.69<0.005mg/KgN-Nitrosodimethylamine 39.1 10-146 3.6 30
1.47 86.91.491.641.69<0.184mg/KgN-Nitrosodiphenylamine 90.8 38-127 1.3 20
1.06 62.71.051.641.69<0.154mg/KgN-Nitroso-di-n-propylamine 64.0 36-120 0.9 20
1.17 69.21.201.641.69<0.429mg/KgPentachlorophenol 73.1 25-133 2.5 20
1.47 86.91.351.641.690.204mg/KgPhenanthrene 82.3 50-121 8.5 20
0.888 52.50.9091.641.69<0.110mg/KgPhenol 55.4 34-121 2.3 20
1.44 85.21.281.641.690.364mg/KgPyrene 78.0 47-127 11.7 20
0.416 24.60.4071.641.69<0.064mg/KgPyridine 24.8 10-80 2.1 20
0.886 52.40.8961.641.69<0.119mg/Kg1,2,4-Trichlorobenzene 54.6 34-118 1.1 20
1.01 59.71.031.641.69<0.142mg/Kg2,4,5-Trichlorophenol 62.8 41-124 1.9 20
1.02 60.31.041.641.69<0.162mg/Kg2,4,6-Trichlorophenol 63.4 39-126 1.9 20
73.32-Fluorobiphenyl (S)77.4 44-115
52.92-Fluorophenol (S)54.5 35-115
55.2Nitrobenzene-d5 (S)59.2 37-122
75.74-Terphenyl-d14 (S)77.4 54-127
71.02,4,6-Tribromophenol (S)74.6 39-132
54.4Phenol-d5 (S)55.4 34-121
Page 18 of 19Date:05/03/2021 11:05 AM
Page 93 of 96
Quality Control Data
21-113-0038Report No:
Project Description:
Client ID:F&R, Inc. - Charlotte
Verbena
Dry Weight Determination
SW-DRYWT
V3663QC Analytical Batch:
Analysis Method:
Analysis Description:
V 97542-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/28/21 16:110.013.813.8%Moisture
V 97700-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/28/21 16:1112.917.319.7%Moisture
Page 19 of 19Date:05/03/2021 11:05 AM
Page 94 of 96
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-113-0038
F&R, Inc. - Charlotte
00019
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 15.2
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Stacy L Ortiz Date & Time:04/23/2021 16:25:32
Special precautions or instructions included?
Comments:
Page 95 of 96
Page 96 of 96