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HomeMy WebLinkAbout09042_Scott Aviation Senior Center Vapor Report&Approval 20210916 September 16, 2021 Sent Via E-Mail Mr. Larry Faison City of Monroe P.O. Box 69 Monroe, North Carolina 28111 lfaison@monroenc.org Subject: Senior Center-Former EJ Building-Vapor LUR Approval Former Scott Aviation Brownfields Property 500 West Jefferson Street Monroe, Union County Brownfields Project Number 09042-05-090 Dear Mr. Faison, The Department of Environmental Quality (DEQ) Brownfields Program received the Soil Vapor Sampling Report dated September 6, 2021, prepared by Resolve Environmental Services, PLLC for the above referenced Brownfields Property. The report documents additional soil vapor assessment for building expansion of the Senior Center at 500 West Jefferson Street (a portion of the former Scott Aviation Brownfields Property). The additional assessment work was done at the request of DEQ Brownfields Program in reference to Land Use Restriction (“LUR”) Number 7 in the Notice of Brownfields Property. Assessment activities included soil gas vapor sample collection and analysis by EPA Method TO-15 for volatile organic compounds (VOCs). Based on the analytical results of the soil gas samples and DEQ Risk Calculator hazard risk index, DEQ Brownfields supports the conclusion that no additional measures, mitigation, or monitoring are required for the proposed redevelopment plan at 500 W Jefferson St as present in the assessment report. Please continue to submit the annual LUR Update certifications to remain compliant with the recorded Notice. Should you have additional concerns or questions regarding the information in this approval letter, please contact me at 704/661-0330 or carolyn.minnich@ncdenr.gov. Sincerely, Carolyn Mininch Brownfields Project Manager ec: Fern Paterson fernpaterson@parkerpoe.com Brian Borne bborne@monroenc.org Laura Minor resolveenviro@gmail.com Terry Kennedy tdk@geologicalresourcesinc.com Brownfields Property Management Unit September 6, 2021 Ms. Carolyn Minnich NCDEQ-Brownfields Program 1646 Mail Service Center Raleigh NC 27699-1646 RE: Soil-Vapor Sampling Report Senior Center Addition Former Scott Aviation Project ID: 09042-05-090 Dear Ms. Minnich: Please find attached, the Soil-Vapor Sampling Report for the above referenced site. Please do not hesitate to contact me regarding any questions or comments. Sincerely, Terry D. Kennedy, P.G. attachment cc: Ms. Fern Paterson, Parker Poe Brian Borne, City of Monroe SOIL-VAPOR SAMPLING REPORT FORMER SCOTT AVIATION (SENIOR CENTER ADDITION) 500 WEST JEFFERSON STREET (FORMER ENQUIRER JOURNAL) MONROE, UNION COUNTY, NORTH CAROLINA BROWNFIELDS PROJECT ID 09042-05-090 Prepared for: Ms. Carolyn Minnich North Carolina of Department of Environmental Quality Division of Waste Management Brownfields Program 217 West Jones Street Raleigh, North Carolina 27603 Prepared by: Resolve Environmental Services, PLLC 500 Devonport Drive Matthews, North Carolina 28104 September 6, 2021 __________________________ _________________________ Laura Minor Terry D. Kennedy, P.G. Project Manager Principal TABLE OF CONTENTS A. SITE INFORMATION ........................................................................................................................... 1 B. INTRODUCTION ................................................................................................................................. 2 C. ENVIRONMENTAL ASSESSMENT ACTIVITIES ..................................................................................... 2 D. DISCUSSION OF RESULTS .................................................................................................................. 4 E. LIMITATIONS ..................................................................................................................................... 4 FIGURES Figure 1: Site Location Map Figure 2: Soil-Vapor Sampling Location and Quality Map (8/6/2021) TABLES Table 1: Summary of QA/QC Data Table 2: Sub-Slab Soil Vapor Gas Sampling Results APPENDIX Appendix A: Laboratory Analytical Report 1 A. SITE INFORMATION  Site Name: Former Scott Aviation (Senior Center Addition)  Location: 500 West Jefferson Street Monroe, Union County, NC  Land Use: Non-Residential  Property Owner: City of Monroe P.O. Box 69 Monroe, NC 28111  Prospective Developer: City of Monroe P.O. Box 69 Monroe, NC 28111 704-282-4501  Consultant: Resolve Environmental Services, PLLC (Resolve) 500 Devonport Drive Matthews, North Carolina 28104 (704) 845-4010  Latitude: 36.983639° North Longitude: 80.554631° West 2 B. INTRODUCTION 1. Project Background The subject site is located at 500 West Jefferson Street in Monroe, North Carolina. The site is a portion of Brownfields Project 09042-05-090. The site is a currently proposed to be renovated into a Senior Center for the City of Monroe. Part of the proposed renovation is the addition of an approximate 3900 ft2 addition on the northwest corner of the existing building. Previous ground water assessment activities and soil vapor studies at the site indicated the presence of volatile organic compounds (VOCs) in the soil vapor and groundwater at and/or adjacent to the site. The proposed usage at the site has been characterized as “non-residential” by the NCDEQ’s Brownfields Program. A Site Location Map is included as Figure 1. At the request of the Brownfields Program Project Manager, a soil-gas survey vapor point was proposed to be installed within the footprint of the proposed addition. The collected soil-gas sample would be analyzed for VOCs by Method TO-15. The purpose of the sampling was to determine if soil vapor quality within the footprint of the proposed addition exceeds the NCDEQ’s non-residential vapor intrusion screening levels (VISLs). The purpose of this report is to present the methods and results from soil-gas sampling conducted at the site on August 6, 2021. The air samples were submitted to a nationally certified laboratory (National Voluntary Laboratory Accreditation Program, aka NVLAP) for a full-list of volatile organic compounds by EPA Method TO-15. C. ENVIRONMENTAL ASSESSMENT ACTIVITIES 1. Sample Point Installation, QA/QC and Sample Collection On August 2, 2021 Resolve supervised the installation of a vapor sampling point at the site. The soil-gas vapor sample point consisted of Geoprobe® Post-Run Tubing (PRT). A 1.5-inch diameter rod with a disposable end point was driven to a total depth of approximately 6 feet at the soil-gas vapor sample point. The rod was then retracted approximately 0.5-feet. A bentonite seal was placed around the perimeter of the 1.5-inch rod at ground surface to ensure no ambient air could enter the sampling point. The PRT sampling point and associated tubing was then attached to the end of the PRT sampling rod. 3 On August 6, 2021, a soil-gas vapor sample (SV-1) and duplicate sample were collected from the newly installed vapor sampling point. The samples were collected using laboratory supplied and certified 1-liter Summa canisters and calibrated flow controllers. Each Summa canister flow controller was pre- calibrated for a 30-minute sample collection at a target vacuum of 7-10 inches of mercury and a target flow rate of 23.4 cubic centimeters per minute (regulator 3197) and 51.3 cubic centimeters per minute (regulator 3198). Each canister passed a laboratory leak test prior to sampling. Additional leak testing was not conducted on the canisters in the field. The Summa canisters were placed on the ground adjacent to the vapor sampling point. Prior to sampling, pressure readings on the canister gauges ranged from 29 to 29.5 in Hg. The sample tubing at the sampling point was purged using an air pump. The volume of air removed from the vapor point was a minimum of three times the pore space and tubing. Prior to sample collection, a leak test was conducted at the sampling location. The leak test was conducted by placing a cover over the sampling point, tubing and connectors, and helium placed within the cover. The percentage of helium in the air beneath the cover was as close to saturation as possible, actual percentages were measured and recorded in field notes. The air was continuously monitored for helium using a helium detector during the purging of the sample locations. If a helium concentration was detected below 10 percent of the concentration under the cover, it was assumed that the sample point and connected tubing were properly sealed. Following the leak testing, the flow valves on the canisters were opened and samples were collected over a 30-minute period. Canister pressures at the completion of sampling activities ranged from 1 to 5 in Hg. Samples were collected by Resolve personnel wearing clean, disposable nitrile gloves. Following sample collection, the canisters were shipped directly to the laboratory for analyses following proper chain-of-custody protocol. The sample location is shown on Figure 2. Sample collection QA/QC data is provided in Table 1. 2. Vapor Intrusion Sampling Results Detectable and/or estimated concentrations of target VOCs were reported in each of the soil gas samples (SV-1 and in the duplicate sample). Based upon the laboratory analytical report, none of the detectable concentrations exceeded the NCDEQ’s non-residential VISLs. A summary of soil vapor quality sampling results is included in Table 2. A copy of the laboratory analytical report is attached as Appendix A. 4 D. DISCUSSION OF RESULTS  One soil-gas sample (SV-1) and a duplicate sample were collected from within the footprint of the proposed 3,900 ft2 building addition.  Concentrations of contaminants of concern were detected in both samples collected. However, none of the concentrations exceeded the non-residential VISLs in the samples.  Based upon the laboratory analytical results information, a passive vapor barrier and/or venting system are not required for the proposed building addition. E. LIMITATIONS This report has been prepared for the exclusive use of City of Monroe and the NCDEQ for specific application to the referenced site in Union County, North Carolina. The assessment was conducted based on the scope of work and level of effort specified by the NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of geology and hydrogeology practices in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied. The data that are presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional information can logically be inferred from these data. FIGURES Figure 1: Site Location Map Former Scott Aviation (Senior Center Addition) 500 West Jefferson Street Monroe, Union County, NC BF Project ID: 09042-05-090 1000 ft N➤➤N Untitled Map Write a description for your map. Legend 100 ft N➤➤N TABLES Sample ID Date Collected Air Type Summa Canister (6 L or 1 L) Serial Number Flow Controller Serial Number Leak Test Method Helium Reading2 (%) inside cover Helium Reading (%) on meter Volume Purged1 (cubic feet) Time Canister Pressure ("Hg) Temp (F)Time Canister Pressure ("Hg) Temp (F) SV-1 8/6/2021 Soil-Vapor BC2254 (1 L)3197 Purge 6.4 0.0 0.90 1015 29.0 77 1045 5 78 DUPLICATE 8/6/2021 Soil-Vapor BC2540 (1 L)3198 Purge NA NA NA 1015 29.5 77 1045 1 78 Note: 1. NA: Not applicable. Sampling Data Leak Testing/Purging Start Sampling Information Stop Sampling Information TABLE 1 FORMER SCOTT AVIATION - SENIOR CENTER ADDITION MONROE, NC QA/QC SUMMARY PROJECT ID 09042-05-090 Compound Date SV-1 DUPLICATE NCDEQ VISL SubSlab and Exterior Soil Gas Screening Level (Non-Residential) Unit Acetone 8/6/2021 2.50E+02 3.10E+02 2.72E+06 ug/m3 Benzene 8/6/2021 6.30E+00 6.20E+00 1.57E+02 ug/m3 2-Butanone (MEK)8/6/2021 4.00E+01 4.50E+01 4.38E+05 ug/m3 Carbon Disulfide 8/6/2021 4.70E+00 5.70E+00 6.13E+04 ug/m3 Carbon Tetrachloride 8/6/2021 4.8E-01J 4.8E-01J 2.04E+02 ug/m3 1,3-Dichlorobenzene 8/6/2021 4.10E+00 3.50E+00 NE ug/m3 cis-1,2-Dichloroethylene 8/6/2021 <0.13 6.10E-01 NE ug/m3 Ethanol 8/6/2021 1.80E+02 1.30E+02 NE ug/m3 Ethylbenzene 8/6/2021 1.70E+00 1.80E+00 4.91E+02 ug/m3 4-Ethyltoluene 8/6/2021 5.90E-01 6.30E-01 NE ug/m3 Heptane 8/6/2021 9.60E+00 1.20E+01 3.50E+04 ug/m3 Hexane 8/6/2021 5.10E+01 5.80E+01 6.13E+04 ug/m3 Isopropanol 8/6/2021 2.90E+01 2.40E+01 1.75E+04 ug/m3 Methylene Chloride 8/6/2021 2.3E+00J <8.0E-01 5.26E+04 ug/m3 Propene 8/6/2021 4.40E+02 4.00E+02 2.63E+05 ug/m3 Styrene 8/6/2021 7.80E-01 6.80E-01 8.76E+04 ug/m3 Tetrachloroethylene 8/6/2021 9.60E-01 1.10E+00 3.50E+03 ug/m3 Tetrahydrofuran 8/6/2021 3.50E+00 3.30E+00 NE ug/m3 Toluene 8/6/2021 6.50E+00 6.90E+00 4.38E+05 ug/m3 Trichloroethylene 8/6/2021 <2.0E-01 8.40E+00 1.75E+02 ug/m3 Trichlorofluoromethane (Freon 11)8/6/2021 1.5E+00J 1.5E+00J NE ug/m3 1,3,5-Trimethylbenzene 8/6/2021 6.00E-01 6.50E-01 5.26E+03 ug/m3 m&p-Xylene 8/6/2021 3.20E+00 3.50E+00 8.76E+03 ug/m3 o-Xylene 8/6/2021 1.20E+00 1.40E+00 8.76E+03 ug/m3 GC/MS Volatiles (TO-15) Notes: J:Estiamted value NE:Not established TABLE 2 FORMER SCOTT AVIATION - SENIOR CENTER ADDITION MONROE, NC SUB-SLAB SOIL VAPOR GAS SAMPLING RESULTS BROWNFIELDS PROJECT ID 09042-05-090 APPENDIX APPENDIX A Laboratory Analytical Report #=CL# August 16, 2021 LIMS USE: FR - LAURA MINOR LIMS OBJECT ID: 92554692 92554692 Project: Pace Project No.: RE: Ms. Laura Minor Resolve Environmental Services 500 Devonport Drive Matthews, NC 28104 Enquirer-Journal (EJ) Dear Ms. Minor: Enclosed are the analytical results for sample(s) received by the laboratory on August 06, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: If you have any questions concerning this report, please feel free to contact me. Sincerely, Angela Baioni angela.baioni@pacelabs.com Project Manager (704)875-9092 Enclosures cc:Ms. Laura Minor, Resolve Environmental Services REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 25 #=NA# PROJECT NARRATIVE Pace Project No.: Project: Method: Client: Date: Description: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 25 Page 3 of 25 Page 4 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 August 16, 2021 Angela Baioni Pace Analytical Services - NC 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Project Location: Enquirer-Journal (EJ) Client Job Number: Project Number: 92554692 Laboratory Work Order Number: 21H0536 Enclosed are results of analyses for samples received by the laboratory on August 6, 2021. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 21 Page 5 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL SUMMARY 8/16/2021Pace Analytical Services - NC 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 ATTN: Angela Baioni 92554692 21H0536 The results of analyses performed on the following samples submitted to Con-Test, a Pace Analytical Laboratory, are found in this report. PROJECT LOCATION: PURCHASE ORDER NUMBER: PROJECT NUMBER: REPORT DATE: WORK ORDER NUMBER: FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB Enquirer-Journal (EJ) SV-1 21H0536-01 Air EPA TO-15 Duplicate 21H0536-02 Air EPA TO-15 Page 2 of 21 Page 6 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. EPA TO-15 Qualifications: Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. Analyte & Samples(s) Qualified: 1,2,4-Trichlorobenzene B288293-BS1 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: 1,2,4-Trichlorobenzene B288293-BS1 The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Technical Representative Page 3 of 21 Page 7 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Enquirer-Journal (EJ) Date Received: 8/6/2021 Work Order: 21H0536Sample Description/Location: Field Sample #: SV-1 Sample ID: 21H0536-01 Sample Matrix: Air Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -7 Sampled: 8/6/2021 10:45 Canister ID: 2254 Flow Controller ID: 3197 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 30 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 MDL MDL Acetone 110 40 8/13/21 2:52 BRF250 20952457 Benzene 2.0 0.10 8/13/21 15:58 BRF6.3 20.320.029 0.093 Benzyl chloride ND 0.10 8/13/21 15:58 BRFND20.520.045 0.23 Bromodichloromethane ND 0.10 8/13/21 15:58 BRFND20.670.028 0.19 Bromoform ND 0.10 8/13/21 15:58 BRFND21.00.034 0.36 Bromomethane ND 0.10 8/13/21 15:58 BRFND20.390.053 0.21 1,3-Butadiene ND 0.10 8/13/21 15:58 BRFND20.220.073 0.16 2-Butanone (MEK)14 4.0 8/13/21 15:58 BRF40 2120.33 0.98 Carbon Disulfide 1.5 1.0 8/13/21 15:58 BRF4.7 23.10.25 0.79 Carbon Tetrachloride 0.076 0.10 8/13/21 15:58 BRFJ0.48 20.630.027 0.17 Chlorobenzene ND 0.10 8/13/21 15:58 BRFND20.460.024 0.11 Chloroethane ND 0.10 8/13/21 15:58 BRFND20.260.098 0.26 Chloroform ND 0.10 8/13/21 15:58 BRFND20.490.024 0.12 Chloromethane ND 0.20 8/13/21 15:58 BRFND20.410.076 0.16 Cyclohexane ND 0.10 8/13/21 15:58 BRFND20.340.049 0.17 Dibromochloromethane ND 0.10 8/13/21 15:58 BRFND20.850.034 0.29 1,2-Dibromoethane (EDB)ND 0.10 8/13/21 15:58 BRFND20.770.026 0.20 1,2-Dichlorobenzene ND 0.10 8/13/21 15:58 BRFND20.600.037 0.22 1,3-Dichlorobenzene 0.68 0.10 8/13/21 15:58 BRF4.1 20.600.036 0.22 1,4-Dichlorobenzene ND 0.10 8/13/21 15:58 BRFND20.600.022 0.13 Dichlorodifluoromethane (Freon 12)ND 0.10 8/13/21 15:58 BRFND20.490.031 0.16 1,1-Dichloroethane ND 0.10 8/13/21 15:58 BRFND20.400.031 0.13 1,2-Dichloroethane ND 0.10 8/13/21 15:58 BRFND20.400.037 0.15 1,1-Dichloroethylene ND 0.10 8/13/21 15:58 BRFND20.400.054 0.22 cis-1,2-Dichloroethylene ND 0.10 8/13/21 15:58 BRFND20.400.034 0.13 trans-1,2-Dichloroethylene ND 0.10 8/13/21 15:58 BRFND20.400.030 0.12 1,2-Dichloropropane ND 0.10 8/13/21 15:58 BRFND20.460.036 0.17 cis-1,3-Dichloropropene ND 0.10 8/13/21 15:58 BRFND20.450.046 0.21 trans-1,3-Dichloropropene ND 0.10 8/13/21 15:58 BRFND20.450.034 0.15 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.10 8/13/21 15:58 BRFND20.700.056 0.39 1,4-Dioxane ND 1.0 8/13/21 15:58 BRFND23.60.28 1.0 Ethanol 98 4.0 8/13/21 15:58 BRF180 27.51.2 2.3 Ethyl Acetate ND 1.0 8/13/21 15:58 BRFND23.60.59 2.1 Ethylbenzene 0.39 0.10 8/13/21 15:58 BRF1.7 20.430.021 0.090 4-Ethyltoluene 0.12 0.10 8/13/21 15:58 BRF0.59 20.490.031 0.15 Heptane 2.3 0.10 8/13/21 15:58 BRF9.6 20.410.043 0.18 Hexachlorobutadiene ND 0.10 8/13/21 15:58 BRFND21.10.044 0.47 Hexane 14 4.0 8/13/21 15:58 BRF51 2140.18 0.64 2-Hexanone (MBK)ND 0.10 8/13/21 15:58 BRFND20.410.056 0.23 Isopropanol 12 4.0 8/13/21 15:58 BRF29 29.80.92 2.3 Methyl tert-Butyl Ether (MTBE)ND 0.10 8/13/21 15:58 BRFND20.360.040 0.14 Methylene Chloride 0.66 1.0 8/13/21 15:58 BRFJ2.3 23.50.23 0.80 4-Methyl-2-pentanone (MIBK)ND 0.10 8/13/21 15:58 BRFND20.410.052 0.21 Naphthalene ND 0.10 8/13/21 15:58 BRFND20.520.056 0.29 Propene 250 40 8/13/21 2:52 BRF440 20693.4 5.8 Styrene 0.18 0.10 8/13/21 15:58 BRF0.78 20.430.029 0.12 1,1,2,2-Tetrachloroethane ND 0.10 8/13/21 15:58 BRFND20.690.027 0.18 Page 4 of 21 Page 8 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Enquirer-Journal (EJ) Date Received: 8/6/2021 Work Order: 21H0536Sample Description/Location: Field Sample #: SV-1 Sample ID: 21H0536-01 Sample Matrix: Air Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -7 Sampled: 8/6/2021 10:45 Canister ID: 2254 Flow Controller ID: 3197 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 30 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 MDL MDL Tetrachloroethylene 0.14 0.10 8/13/21 15:58 BRF0.96 20.680.033 0.22 Tetrahydrofuran 1.2 1.0 8/13/21 15:58 BRF3.5 22.90.25 0.73 Toluene 1.7 0.10 8/13/21 15:58 BRF6.5 20.380.029 0.11 1,2,4-Trichlorobenzene ND 0.10 8/13/21 15:58 BRFND20.740.061 0.45 1,1,1-Trichloroethane ND 0.10 8/13/21 15:58 BRFND20.550.033 0.18 1,1,2-Trichloroethane ND 0.10 8/13/21 15:58 BRFND20.550.037 0.20 Trichloroethylene ND 0.10 8/13/21 15:58 BRFND20.540.037 0.20 Trichlorofluoromethane (Freon 11)0.26 0.40 8/13/21 15:58 BRFJ1.5 22.20.076 0.43 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.40 8/13/21 15:58 BRFND23.10.075 0.58 1,2,4-Trimethylbenzene ND 0.10 8/13/21 15:58 BRFND20.490.023 0.11 1,3,5-Trimethylbenzene 0.12 0.10 8/13/21 15:58 BRF0.60 20.490.026 0.13 Vinyl Acetate ND 2.0 8/13/21 15:58 BRFND27.00.28 0.99 Vinyl Chloride ND 0.10 8/13/21 15:58 BRFND20.260.056 0.14 m&p-Xylene 0.75 0.20 8/13/21 15:58 BRF3.2 20.870.035 0.15 o-Xylene 0.29 0.10 8/13/21 15:58 BRF1.2 20.430.027 0.12 Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1)99.4 8/13/21 2:5270-130 4-Bromofluorobenzene (1)102 8/13/21 15:5870-130 Page 5 of 21 Page 9 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Enquirer-Journal (EJ) Date Received: 8/6/2021 Work Order: 21H0536Sample Description/Location: Field Sample #: Duplicate Sample ID: 21H0536-02 Sample Matrix: Air Initial Vacuum(in Hg): -29.5 Final Vacuum(in Hg): -1 Receipt Vacuum(in Hg): -1.4 Sampled: 8/6/2021 10:45 Canister ID: 2540 Flow Controller ID: 3198 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 30 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 MDL MDL Acetone 130 40 8/13/21 3:31 BRF310 20952457 Benzene 1.9 0.10 8/13/21 16:39 BRF6.2 20.320.029 0.093 Benzyl chloride ND 0.10 8/13/21 16:39 BRFND20.520.045 0.23 Bromodichloromethane ND 0.10 8/13/21 16:39 BRFND20.670.028 0.19 Bromoform ND 0.10 8/13/21 16:39 BRFND21.00.034 0.36 Bromomethane ND 0.10 8/13/21 16:39 BRFND20.390.053 0.21 1,3-Butadiene ND 0.10 8/13/21 16:39 BRFND20.220.073 0.16 2-Butanone (MEK)15 4.0 8/13/21 16:39 BRF45 2120.33 0.98 Carbon Disulfide 1.8 1.0 8/13/21 16:39 BRF5.7 23.10.25 0.79 Carbon Tetrachloride 0.076 0.10 8/13/21 16:39 BRFJ0.48 20.630.027 0.17 Chlorobenzene ND 0.10 8/13/21 16:39 BRFND20.460.024 0.11 Chloroethane ND 0.10 8/13/21 16:39 BRFND20.260.098 0.26 Chloroform ND 0.10 8/13/21 16:39 BRFND20.490.024 0.12 Chloromethane ND 0.20 8/13/21 16:39 BRFND20.410.076 0.16 Cyclohexane ND 0.10 8/13/21 16:39 BRFND20.340.049 0.17 Dibromochloromethane ND 0.10 8/13/21 16:39 BRFND20.850.034 0.29 1,2-Dibromoethane (EDB)ND 0.10 8/13/21 16:39 BRFND20.770.026 0.20 1,2-Dichlorobenzene ND 0.10 8/13/21 16:39 BRFND20.600.037 0.22 1,3-Dichlorobenzene 0.58 0.10 8/13/21 16:39 BRF3.5 20.600.036 0.22 1,4-Dichlorobenzene ND 0.10 8/13/21 16:39 BRFND20.600.022 0.13 Dichlorodifluoromethane (Freon 12)ND 0.10 8/13/21 16:39 BRFND20.490.031 0.16 1,1-Dichloroethane ND 0.10 8/13/21 16:39 BRFND20.400.031 0.13 1,2-Dichloroethane ND 0.10 8/13/21 16:39 BRFND20.400.037 0.15 1,1-Dichloroethylene ND 0.10 8/13/21 16:39 BRFND20.400.054 0.22 cis-1,2-Dichloroethylene 0.15 0.10 8/13/21 16:39 BRF0.61 20.400.034 0.13 trans-1,2-Dichloroethylene ND 0.10 8/13/21 16:39 BRFND20.400.030 0.12 1,2-Dichloropropane ND 0.10 8/13/21 16:39 BRFND20.460.036 0.17 cis-1,3-Dichloropropene ND 0.10 8/13/21 16:39 BRFND20.450.046 0.21 trans-1,3-Dichloropropene ND 0.10 8/13/21 16:39 BRFND20.450.034 0.15 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.10 8/13/21 16:39 BRFND20.700.056 0.39 1,4-Dioxane ND 1.0 8/13/21 16:39 BRFND23.60.28 1.0 Ethanol 72 4.0 8/13/21 16:39 BRF130 27.51.2 2.3 Ethyl Acetate ND 1.0 8/13/21 16:39 BRFND23.60.59 2.1 Ethylbenzene 0.42 0.10 8/13/21 16:39 BRF1.8 20.430.021 0.090 4-Ethyltoluene 0.13 0.10 8/13/21 16:39 BRF0.63 20.490.031 0.15 Heptane 3.0 0.10 8/13/21 16:39 BRF12 20.410.043 0.18 Hexachlorobutadiene ND 0.10 8/13/21 16:39 BRFND21.10.044 0.47 Hexane 16 4.0 8/13/21 16:39 BRF58 2140.18 0.64 2-Hexanone (MBK)ND 0.10 8/13/21 16:39 BRFND20.410.056 0.23 Isopropanol 9.9 4.0 8/13/21 16:39 BRF24 29.80.92 2.3 Methyl tert-Butyl Ether (MTBE)ND 0.10 8/13/21 16:39 BRFND20.360.040 0.14 Methylene Chloride ND 1.0 8/13/21 16:39 BRFND23.50.23 0.80 4-Methyl-2-pentanone (MIBK)ND 0.10 8/13/21 16:39 BRFND20.410.052 0.21 Naphthalene ND 0.10 8/13/21 16:39 BRFND20.520.056 0.29 Propene 230 40 8/13/21 3:31 BRF400 20693.4 5.8 Styrene 0.16 0.10 8/13/21 16:39 BRF0.68 20.430.029 0.12 1,1,2,2-Tetrachloroethane ND 0.10 8/13/21 16:39 BRFND20.690.027 0.18 Page 6 of 21 Page 10 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Enquirer-Journal (EJ) Date Received: 8/6/2021 Work Order: 21H0536Sample Description/Location: Field Sample #: Duplicate Sample ID: 21H0536-02 Sample Matrix: Air Initial Vacuum(in Hg): -29.5 Final Vacuum(in Hg): -1 Receipt Vacuum(in Hg): -1.4 Sampled: 8/6/2021 10:45 Canister ID: 2540 Flow Controller ID: 3198 Sub Description/Location: Canister Size: 1 liter Flow Controller Type: Fixed-Orifice Flow Controller Calibration RPD Pre and Post-Sampling: Sample Type: 30 min RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte Date/Time EPA TO-15 ppbv ug/m3 MDL MDL Tetrachloroethylene 0.16 0.10 8/13/21 16:39 BRF1.1 20.680.033 0.22 Tetrahydrofuran 1.1 1.0 8/13/21 16:39 BRF3.3 22.90.25 0.73 Toluene 1.8 0.10 8/13/21 16:39 BRF6.9 20.380.029 0.11 1,2,4-Trichlorobenzene ND 0.10 8/13/21 16:39 BRFND20.740.061 0.45 1,1,1-Trichloroethane ND 0.10 8/13/21 16:39 BRFND20.550.033 0.18 1,1,2-Trichloroethane ND 0.10 8/13/21 16:39 BRFND20.550.037 0.20 Trichloroethylene 1.6 0.10 8/13/21 16:39 BRF8.4 20.540.037 0.20 Trichlorofluoromethane (Freon 11)0.26 0.40 8/13/21 16:39 BRFJ1.5 22.20.076 0.43 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.40 8/13/21 16:39 BRFND23.10.075 0.58 1,2,4-Trimethylbenzene ND 0.10 8/13/21 16:39 BRFND20.490.023 0.11 1,3,5-Trimethylbenzene 0.13 0.10 8/13/21 16:39 BRF0.65 20.490.026 0.13 Vinyl Acetate ND 2.0 8/13/21 16:39 BRFND27.00.28 0.99 Vinyl Chloride ND 0.10 8/13/21 16:39 BRFND20.260.056 0.14 m&p-Xylene 0.80 0.20 8/13/21 16:39 BRF3.5 20.870.035 0.15 o-Xylene 0.32 0.10 8/13/21 16:39 BRF1.4 20.430.027 0.12 Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1)99.1 8/13/21 3:3170-130 4-Bromofluorobenzene (1)101 8/13/21 16:3970-130 Page 7 of 21 Page 11 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep-EPA TO-15 Lab Number [Field ID]Batch Date Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL 21H0536-01RE1 [SV-1]B288285 1.5 1 N/A 1000 400 30 08/12/21 21H0536-02RE1 [Duplicate]B288285 1.5 1 N/A 1000 400 30 08/12/21 Prep Method: TO-15 Prep-EPA TO-15 Lab Number [Field ID]Batch Date Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL 21H0536-01 [SV-1]B288293 1.5 1 N/A 1000 400 300 08/13/21 21H0536-02 [Duplicate]B288293 1.5 1 N/A 1000 400 300 08/13/21 Page 8 of 21 Page 12 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ug/m3 Spike Level Result Source %REC %REC Limits RPD RPD Limit Flag/Qual Analyte Air Toxics by EPA Compendium Methods - Quality Control QUALITY CONTROL RL ppbv Results RL Results ppbv Batch B288285 - TO-15 Prep Blank (B288285-BLK1)Prepared & Analyzed: 08/12/21 0.80NDAcetone 0.80NDPropene 8.00 70-130Surrogate: 4-Bromofluorobenzene (1)97.47.79 LCS (B288285-BS1)Prepared & Analyzed: 08/12/21 5.00 70-13086.64.33Acetone 5.00 70-13088.24.41Propene 8.00 70-130Surrogate: 4-Bromofluorobenzene (1)99.47.95 Batch B288293 - TO-15 Prep Blank (B288293-BLK1)Prepared & Analyzed: 08/13/21 0.80NDAcetone 0.020NDBenzene 0.020NDBenzyl chloride 0.020NDBromodichloromethane 0.020NDBromoform 0.020NDBromomethane 0.020ND1,3-Butadiene 0.80ND2-Butanone (MEK) 0.20NDCarbon Disulfide 0.020NDCarbon Tetrachloride 0.020NDChlorobenzene 0.020NDChloroethane 0.020NDChloroform 0.040NDChloromethane 0.020NDCyclohexane 0.020NDDibromochloromethane 0.020ND1,2-Dibromoethane (EDB) 0.020ND1,2-Dichlorobenzene 0.020ND1,3-Dichlorobenzene 0.020ND1,4-Dichlorobenzene 0.020NDDichlorodifluoromethane (Freon 12) 0.020ND1,1-Dichloroethane 0.020ND1,2-Dichloroethane 0.020ND1,1-Dichloroethylene 0.020NDcis-1,2-Dichloroethylene 0.020NDtrans-1,2-Dichloroethylene 0.020ND1,2-Dichloropropane 0.020NDcis-1,3-Dichloropropene 0.020NDtrans-1,3-Dichloropropene 0.020ND1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 0.20ND1,4-Dioxane 0.80NDEthanol 0.20NDEthyl Acetate 0.020NDEthylbenzene Page 9 of 21 Page 13 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ug/m3 Spike Level Result Source %REC %REC Limits RPD RPD Limit Flag/Qual Analyte Air Toxics by EPA Compendium Methods - Quality Control QUALITY CONTROL RL ppbv Results RL Results ppbv Batch B288293 - TO-15 Prep Blank (B288293-BLK1)Prepared & Analyzed: 08/13/21 0.020ND4-Ethyltoluene 0.020NDHeptane 0.020NDHexachlorobutadiene 0.80NDHexane 0.020ND2-Hexanone (MBK) 0.80NDIsopropanol 0.020NDMethyl tert-Butyl Ether (MTBE) 0.20NDMethylene Chloride 0.020ND4-Methyl-2-pentanone (MIBK) 0.020NDNaphthalene 0.80NDPropene 0.020NDStyrene 0.020ND1,1,2,2-Tetrachloroethane 0.020NDTetrachloroethylene 0.20NDTetrahydrofuran 0.020NDToluene 0.020ND1,2,4-Trichlorobenzene 0.020ND1,1,1-Trichloroethane 0.020ND1,1,2-Trichloroethane 0.020NDTrichloroethylene 0.080NDTrichlorofluoromethane (Freon 11) 0.080ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.020ND1,2,4-Trimethylbenzene 0.020ND1,3,5-Trimethylbenzene 0.40NDVinyl Acetate 0.020NDVinyl Chloride 0.040NDm&p-Xylene 0.020NDo-Xylene 8.00 70-130Surrogate: 4-Bromofluorobenzene (1)99.67.97 Page 10 of 21 Page 14 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ug/m3 Spike Level Result Source %REC %REC Limits RPD RPD Limit Flag/Qual Analyte Air Toxics by EPA Compendium Methods - Quality Control QUALITY CONTROL RL ppbv Results RL Results ppbv Batch B288293 - TO-15 Prep LCS (B288293-BS1)Prepared & Analyzed: 08/13/21 5.00 70-13090.14.51Acetone 5.00 70-13097.04.85Benzene 5.00 70-1301266.31Benzyl chloride 5.00 70-1301035.13Bromodichloromethane 5.00 70-1301246.21Bromoform 5.00 70-1301065.28Bromomethane 5.00 70-13092.04.601,3-Butadiene 5.00 70-13099.34.962-Butanone (MEK) 5.00 70-1301075.33Carbon Disulfide 5.00 70-1301085.42Carbon Tetrachloride 5.00 70-1301075.35Chlorobenzene 5.00 70-13098.14.90Chloroethane 5.00 70-1301125.58Chloroform 5.00 70-13095.74.78Chloromethane 5.00 70-13092.04.60Cyclohexane 5.00 70-1301125.60Dibromochloromethane 5.00 70-1301085.411,2-Dibromoethane (EDB) 5.00 70-1301226.111,2-Dichlorobenzene 5.00 70-1301216.031,3-Dichlorobenzene 5.00 70-1301185.891,4-Dichlorobenzene 5.00 70-1301216.07Dichlorodifluoromethane (Freon 12) 5.00 70-1301095.471,1-Dichloroethane 5.00 70-1301115.531,2-Dichloroethane 5.00 70-1301115.541,1-Dichloroethylene 5.00 70-1301095.45cis-1,2-Dichloroethylene 5.00 70-1301075.36trans-1,2-Dichloroethylene 5.00 70-13098.14.901,2-Dichloropropane 5.00 70-1301045.21cis-1,3-Dichloropropene 5.00 70-1301105.49trans-1,3-Dichloropropene 5.00 70-1301105.481,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 5.00 70-1301025.121,4-Dioxane 5.00 70-1301045.21Ethanol 5.00 70-13086.64.33Ethyl Acetate 5.00 70-1301025.11Ethylbenzene 5.00 70-1301185.914-Ethyltoluene 5.00 70-13092.44.62Heptane 5.00 70-1301135.66Hexachlorobutadiene 5.00 70-1301115.55Hexane 5.00 70-1301045.182-Hexanone (MBK) 5.00 70-13081.84.09Isopropanol 5.00 70-1301045.20Methyl tert-Butyl Ether (MTBE) 5.00 70-13094.94.75Methylene Chloride 5.00 70-13096.14.804-Methyl-2-pentanone (MIBK) 5.00 70-1301246.22Naphthalene 5.00 70-13090.24.51Propene 5.00 70-1301125.58Styrene Page 11 of 21 Page 15 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ug/m3 Spike Level Result Source %REC %REC Limits RPD RPD Limit Flag/Qual Analyte Air Toxics by EPA Compendium Methods - Quality Control QUALITY CONTROL RL ppbv Results RL Results ppbv Batch B288293 - TO-15 Prep LCS (B288293-BS1)Prepared & Analyzed: 08/13/21 5.00 70-1301105.481,1,2,2-Tetrachloroethane 5.00 70-13088.24.41Tetrachloroethylene 5.00 70-1301035.15Tetrahydrofuran 5.00 70-1301015.04Toluene 5.00 L-01, V-3670-1301457.251,2,4-Trichlorobenzene * 5.00 70-13099.04.951,1,1-Trichloroethane 5.00 70-1301065.321,1,2-Trichloroethane 5.00 70-1301015.05Trichloroethylene 5.00 70-1301155.74Trichlorofluoromethane (Freon 11) 5.00 70-1301165.801,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 5.00 70-1301145.721,2,4-Trimethylbenzene 5.00 70-1301095.471,3,5-Trimethylbenzene 5.00 70-1301246.20Vinyl Acetate 5.00 70-1301075.33Vinyl Chloride 10.0 70-13010710.7m&p-Xylene 5.00 70-1301035.16o-Xylene 8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1018.10 Page 12 of 21 Page 16 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Note: Blank Subtraction is not performed unless otherwise noted *QC result is outside of established limits. Wide recovery limits established for difficult compound. Wide RPD limits established for difficult compound. #Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency Percent Recovery% REC ND Not Detected Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. Not ApplicableN/A DL Detection Limit Not CalculatedNC LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation-Reduction Potential Not dry weight correctedwet Percent weight% wt KilogramKg Gramg Milligrammg Microgramg Nanogramng LiterL MillilitermL Microliter L Cubic Meterm3 Extractable Petroleum HydrocarbonsEPH Volatile Petroleum HydrocarbonsVPH Air Petroleum HydrocarbonsAPH Flame Ionization DetectorFID Photo Ionization DetectorPID FLAG/QUALIFIER SUMMARY Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). J Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. L-01 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. V-36 ANALYST Rebecca FaustRLF Kerry K. McGeeKKM Brittany R. FiskBRF Page 13 of 21 Page 17 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 RTResponseInternal Standard Area %RT DiffResponse Reference RT Reference Area % Limits RT Diff Limit Q SV-1 (21H0536-01RE1 )Lab File ID: G21A224025.D Analyzed: 08/13/21 02:52 Bromochloromethane (1)1492035 8.509 60 - 140 8.5090 +/-0.50 1,4-Difluorobenzene (1)4725196 10.283 60 - 140 10.2830 +/-0.50 Chlorobenzene-d5 (1)4553694 14.654 60 - 140 14.6540 +/-0.50 Duplicate (21H0536-02RE1 )Lab File ID: G21A224026.D Analyzed: 08/13/21 03:31 Bromochloromethane (1)1497222 8.503 60 - 140 8.5030 +/-0.50 1,4-Difluorobenzene (1)4666759 10.277 60 - 140 10.2770 +/-0.50 Chlorobenzene-d5 (1)4578700 14.648 60 - 140 14.6480 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 RTResponseInternal Standard Area %RT DiffResponse Reference RT Reference Area % Limits RT Diff Limit Q SV-1 (21H0536-01 )Lab File ID: G21A225009.D Analyzed: 08/13/21 15:58 Bromochloromethane (1)1393070 8.503 60 - 140 8.5030 +/-0.50 1,4-Difluorobenzene (1)4551276 10.283 60 - 140 10.2830 +/-0.50 Chlorobenzene-d5 (1)4436789 14.654 60 - 140 14.6540 +/-0.50 Duplicate (21H0536-02 )Lab File ID: G21A225010.D Analyzed: 08/13/21 16:39 Bromochloromethane (1)1383626 8.503 60 - 140 8.5030 +/-0.50 1,4-Difluorobenzene (1)4530978 10.283 60 - 140 10.2830 +/-0.50 Chlorobenzene-d5 (1)4452356 14.654 60 - 140 14.6540 +/-0.50 Page 14 of 21 Page 18 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CONTINUING CALIBRATION CHECK COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL % DIFF / DRIFTRESPONSE FACTOR STD * Values outside of QC limits # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk Page 15 of 21 Page 19 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA TO-15 in Air AIHA,NY,ME,NHAcetone AIHA,FL,NJ,NY,ME,NH,VABenzene AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride AIHA,NJ,NY,ME,NH,VABromodichloromethane AIHA,NJ,NY,ME,NH,VABromoform AIHA,FL,NJ,NY,ME,NHBromomethane AIHA,NJ,NY,ME,NH,VA1,3-Butadiene AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK) AIHA,NJ,NY,ME,NH,VACarbon Disulfide AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene AIHA,FL,NJ,NY,ME,NH,VAChloroethane AIHA,FL,NJ,NY,ME,NH,VAChloroform AIHA,FL,NJ,NY,ME,NH,VAChloromethane AIHA,NJ,NY,ME,NH,VACyclohexane AIHA,NY,ME,NHDibromochloromethane AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB) AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12) AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene AIHA,NY,ME,NHtrans-1,3-Dichloropropene AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) AIHA,NJ,NY,ME,NH,VA1,4-Dioxane AIHAEthanol AIHAEthyl Acetate AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene AIHA,NJ4-Ethyltoluene AIHA,NJ,NY,ME,NH,VAHeptane AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene AIHA,FL,NJ,NY,ME,NH,VAHexane AIHA2-Hexanone (MBK) AIHA,NY,ME,NHIsopropanol AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE) AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK) NY,ME,NHNaphthalene AIHAPropene AIHA,FL,NJ,NY,ME,NH,VAStyrene AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane Page 16 of 21 Page 20 of 25 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CertificationsAnalyte CERTIFICATIONS Certified Analyses included in this Report EPA TO-15 in Air AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene AIHATetrahydrofuran AIHA,FL,NJ,NY,ME,NH,VAToluene AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11) AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene AIHA,FL,NJ,NY,ME,NH,VAo-Xylene Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations: Code Description Number Expires 100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022 M-MA100Massachusetts DEPMA 06/30/2022 PH-0165Connecticut Department of Publilc HealthCT 12/31/2022 10899 NELAPNew York State Department of HealthNY 04/1/2022 2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2022 LAO00112Rhode Island Department of HealthRI 12/30/2021 652North Carolina Div. of Water QualityNC 12/31/2021 MA007 NELAPNew Jersey DEPNJ 06/30/2022 E871027 NELAPFlorida Department of HealthFL 06/30/2022 LL720741Vermont Department of Health Lead LaboratoryVT 07/30/2022 MA00100State of MaineME 06/9/2023 460217Commonwealth of VirginiaVA 12/14/2021 2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2021 VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2022 25703North Carolina Department of HealthNC-DW 07/31/2022 68-05812Commonwealth of Pennsylvania DEPPA 06/30/2022 9100Dept. of Env, Great Lakes, and EnergyMI 09/6/2021 Page 17 of 21 Page 21 of 25 Page 18 of 21 Page 22 of 25 Page 19 of 21 Page 23 of 25 Page 20 of 21 Page 24 of 25 Page 21 of 21 Page 25 of 25