24004-20-060 - Seventh Street Properties - Tank Removal Letter Report - September 8, 2021

UNDERGROUND STORAGE TANK REMOVAL LETTER REPORT_REV1 SEVENTH STREET PROPERTIES BROWNFIELDS PROJECT NO. 24004-20-060 EAST 7TH STREET & NORTH CASWELL ROAD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA ECS PROJECT NO. 49-8832-C

SEPTEMBER 8, 2021

Underground Storage Tank Removal Letter Report_Rev1 Seventh Street Properties Brownfields Project No. 24004-20-060
East 7th Street & North Caswell Road Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:8832-C September 8, 2021
1
TABLE OF CONTENTS 1.0 PROJECT INFORMATION ................................................................................................. 1
2.0 UST REMOVAL SERVICES ................................................................................................ 1
3.0 LABORATORY ANALYTICAL RESULTS ............................................................................. 2
4.0 CLOSING ............................................................................................................................. 3
FIGURES Figure 1 Site Topographic Map Figure 2 Approximate UST & Sample Location Map TABLES Table 1 Summary of Soil Analytical Results APPENDICES Appendix A Photographic Log Appendix B Disposal Manifests Appendix C Laboratory Data Sheets and Chain-of-Custody Records
Underground Storage Tank Removal Letter Report Seventh Street Properties Brownfields Project No. 24004-20-060
East 7th Street & North Caswell Road Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:8832-C September 8, 2021

1

1.0 PROJECT INFORMATION
The subject property is located at the intersection of East 7th Street and North Caswell Road in Charlotte, Mecklenburg County, North Carolina (Figures 1 and 2). The subject property is identified by the Mecklenburg County GIS website as Parcel identification Number (PIN) 12703509 and owned by CC Elizabeth on Seventh LLC. The subject property is a North Carolina Department of Environmental Quality (NCDEQ), Division of Waste Management (DWM), Brownfields Program site. The Brownfields assigned project name is Seventh Street Properties and has the Brownfields Project No. of 24004-20-060. Currently the site is undergoing redevelopment.
Throughout the site grading/redevelopment activities, a total of 8 previously unknown underground storage tanks (USTs) were encountered. In accordance with the approved Environmental Management Plan (EMP) which was approved on April 23, 2020 for the site, the USTs were
documented, removed, and samples were collected from the UST excavations. This letter report documents the UST removal activities and presents the laboratory data and disposal documentation. 2.0 UST REMOVAL SERVICES On September 88, 2020 ECS observed and documented the removal of one 550-gallon UST by Choate Construction (Choate), the on-site general contractor. ECS subcontracted Contaminant Control Inc. Environmental Services (CCI) to remove the contents of the UST prior to removal, and to transport the UST and contents for off-site disposal. Following the removal of the UST and based on the length of the UST (i.e., less than 10 feet), ECS collected one soil sample (TS-1) beneath the location of the former UST. The approximate location of the UST is indicated on Figure 2. On January 25, 2021 ECS observed and documented the removal of four additional USTs. One
of the USTs was approximately 300-gallons and was paired with an approximately 50-gallon UST that was believed to be part of a hydraulic lift reservoir (located above the 300-gallon UST). The other two USTs were approximately 550-gallons in size. Each of the USTs were located in the
eastern corner of the site near the intersection of East 7th St and North Caswell Rd and were removed by Choate. ECS subcontracted CCI to remove the contents of the USTs prior to removal, and to transport the USTs and contents for off-site disposal. Following removal of the USTs, based
on size and locations, ECS collected three soil samples. One beneath the former location of each of the 550-gallon USTs (T-1 and T-3, and one beneath the 300-gallon UST (T-2). The approximate location of the USTs is indicated on Figure 2. On January 29, 2021 ECS observed and documented the removal of two more USTs thought to be associated with another hydraulic lift reservoir. The larger UST was approximately 300-gallons in size, and the smaller UST was approximately 50-gallons. The USTs, including remaining liquids inside were removed by Choate and staged onsite (placed on and covered with plastic). Following removal, ECS collected one soil sample (T-4) from the area beneath the USTs. ECS subcontracted CCI to remove the remaining product in the USTs and transport the USTs and contents for off-site disposal on February 8, 2021. The approximate location of the USTs are indicated on Figure 2.
Underground Storage Tank Removal Letter Report Seventh Street Properties Brownfields Project No. 24004-20-060
East 7th Street & North Caswell Road Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:8832-C September 8, 2021

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On February 1, 2021 ECS observed and documented the removal of one approximately 700-gallon UST by Choate, which was staged with the previously mentioned 300-gallon UST and 50-gallon UST. Following the removal of the tank and based on the size, ECS collected one soil sample (T-5) from the area below the UST. The 700-gallon UST was removed by CCI for off-site disposal on February 8, 2021. The approximate location of the UST is indicated on Figure 2. Photographs taken during the various UST removal activities are included in Appendix A and disposal manifests for the removed contents and the USTs are included in Appendix B. Each soil sample was collected from a depth of approximately 8 feet below the ground surface.
Approximately one to two feet of soil was removed from the base of each UST prior to the collection of the soil samples. Groundwater was not encountered during the removal of the USTs.
Each of the soil samples collected from the base of the UST excavations were submitted to either Pace Analytical Services, LLC or Waypoint Analytical, both of which are North Carolina certified laboratories. In accordance with the approved EMP, the soil samples were submitted for laboratory analysis of volatile organic compounds (VOCs) using EPA Method 8260, semi-volatile organic compounds (SVOCs) using EPA Method 8270, Resource Conservation and Recovery Act (RCRA) Metals using EPA Methods 6010/6020 and 7471, and hexavalent chromium (Cr6) using EPA Method 7199. In accordance with the EMP, the NCDEQ, Brownfields was notified within approximately 48 hours of the discovery of each of the USTs. 3.0 LABORATORY ANALYTICAL RESULTS
Review of the laboratory analytical results for sample TS-1 indicated concentrations of various
VOCs, SVOCs, and RCRA Metals at concentrations below their respective NCDEQ Preliminary Soil Remediation Goals (PSRGs). Laboratory analytical results indicated concentrations of arsenic at 1.5 milligrams per kilogram (mg/kg), which is above the Residential Health Based
PSRG; as well as cadmium at 4.5 mg/kg and selenium at 3.5 mg/kg, which are above their respective Protection of Groundwater PSRGs.
Review of the laboratory analytical results for sample T-1 indicated concentrations of barium at 31.6 mg/kg, cadmium at 0.10 mg/kg, total chromium at 20.8 mg/kg, lead at 11 mg/kg, and mercury at 0.060 mg/kg. Each of these detections were below respective PSRGs. Laboratory analytical results also indicated concentrations of selenium at 5.2 mg/kg, which is above the Protection of Groundwater PSRG. VOCs and SVOCs were not detected at concentrations above the laboratory detection limits in the T-1 sample. Review of the laboratory analytical results of sample T-2 indicated concentrations of multiple VOCs, SVOCs, RCRA Metals, and Cr6 above the laboratory detection limits. Cr6 was indicated at a concentration above the Residential Health Based PSRG. Multiple VOCs and SVOCs were detected at concentrations above the Protection of Groundwater PSRGs. Naphthalene and lead
were detected at concentrations above their respective Protection of Groundwater PSRGs, Residential, and Industrial/Commercial Health Based PSRGs.
Underground Storage Tank Removal Letter Report Seventh Street Properties Brownfields Project No. 24004-20-060
East 7th Street & North Caswell Road Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:8832-C September 8, 2021

3

Review of the laboratory analytical results for sample T-3 indicated concentrations of multiple VOCs, SVOCs, RCRA Metals, and Cr6 above the laboratory detection limits. Cr6 and ethylbenzene were indicated at concentrations above the Residential Health Based PSRG. Multiple VOCs and SVOCs were detected at concentrations above the Protection of Groundwater PSRGs. Lead was detected at a concentration above the Protection of Groundwater and Residential Health Based PSRG. Naphthalene was detected at a concentration above the Protection of Groundwater PSRGs, and the Residential and Industrial/Commercial Health Based PSRGs. Review of the laboratory analytical results for sample T-4 indicated concentrations of multiple
VOCs, SVOCs, and RCRA metals above the laboratory detection limits. Arsenic was detected at a concentration above the Protection to Groundwater and Industrial/Commercial Health Based PSRG. 1-Methylnaphthalene was detected at a concentration above the Protection of
Groundwater PSRG. Review of the laboratory analytical results for sample T-5 indicated concentrations of multiple metals above the laboratory detection limits. Arsenic was detected at a concentration above the Residential Health Based PSRG. VOCs, SVOCs, and Cr6 were not detected at concentrations above the laboratory detection limits. The results are summarized in Table 1. Laboratory analytical data sheets are included in Appendix A. 4.0 CLOSING The USTs discovered during the site redevelopment activities for the Seventh Street Properties Brownfields site were removed in accordance with the approved EMP for the site. The areas of
remaining impacted soil are covered by either two feet of clean fill or covered by hardscape. This report has been prepared for documentation purposes and ECS recommends it be submitted to the Brownfields Program for their review.
According to the Environmental Protection Agency Technical Guide For Addressing Petroleum Vapor Intrusion At Leaking Underground Storage Tank Sites (dated June 2015):
• For each building within the lateral inclusion zone, collection additional soil gas, soil, and groundwater samples as necessary to determine the vertical separation distance. Additional
investigation is generally unnecessary if the distance to contamination is greater than: o 6 feet for dissolved contamination beneath buildings of any size, or o 15 feet for LNAPL if the overlying building has at least one side shorter than 66 feet in length. Based on the results of the historical sampling activities at the site (notably the previous soil gas sampling results as documented in the Report of Environmental Assessment prepared by ECS dated March 30, 2020), the impacts remaining in the vicinity of T-2 and T-3 are petroleum based, the depths (greater than 6 feet deep) of the samples collected, and the non-residential re-use of the area with slab on-grade construction, the impacts remaining in place do not appear to represent a vapor intrusion concern for the proposed development.

FIGURES

FIGURE 1SITE TOPOGRAPHIC MAP
EAST 7TH STREET SITE –TANK REMOVAL
EAST 7TH STREET & NORTH CASWELL ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH
CAROLINA
ECS PROJECT NO. 49:8832-C
SOURCE:
ECS PHASE I DATED MARCH 1, 2019
SCALE:
AS SHOWN
SITE LOCATION
FIGURE 2APPROXIMATE UST & SAMPLE LOCATION MAP
EAST 7TH STREET SITE –TANK REMOVALEAST 7TH STREET & NORTH CASWELL ROADCHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49:8832-C
SOURCE:
GOOGLE EARTH DATED AUGUST 29, 2019
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE LOCATION OF TANK REMOVAL
APPROXIMATE LOCATION OF SOIL SAMPLE
TS-1
T-5
T-1
T-4
T-2
T-3

TABLES

Parameter
Sample ID TS-1 T-1 T-2 T-3 T-4 T-5
Collection Date 9/28/20 1/25/21 1/25/21 1/25/21 1/29/21 2/1/21
Acetone 0.17 <0.053 <0.55 <0.54 <0.043 <0.052 25 12,000 140,000Benzene<0.00089 <0.0033 0.51 0.22 <0.0027 <0.0032 0.01 1.2 5.4cis-1,2-Dichloroethene <0.00090 <0.0028 0.20 <0.029 <0.0023 <0.0028 0.41 31 470
Ethylbenzene 0.0042J <0.0038 5.6 7.0 0.0047J <0.0038 13 6.1 272-Hexanone <0.0079 <0.0079 <0.0079 <0.0079 0.051J <0.0079 0.18 42.0 280Isopropylbenzene0.0093 <0.0028 1.3 1.9 <0.0023 <0.0028 2.3 410 2,100
p-Isopropyltoluene <0.0041 <0.0041 2.9 3.8 0.034 <0.0040 NS NS NS4-Methyl-2-pentanone (MIBK)<0.00046 <0.0079 <0.082 0.52J <0.0065 <0.0079 0.45 7,000 30,000Napthalene0.16 <0.0043 21.7 28.6 0.23 <0.0043 0.39 2.1 8.8
Tetrachloroethene <0.0010 <0.0026 0.30 <0.027 <0.0021 <0.0026 0.0063 17.0 82.0Toluene<0.00091 <0.0023 0.75 0.26 0.016 <0.0023 8.3 990 9,700
1,2,4-Trimethylbenzene <0.0023 <0.0023 46.3 50.7 0.37 <0.0022 12 63 370
1,3,5-Trimethylbenzene <0.0028 <0.0028 12.7 14.6 0.11 <0.0027 11 56 320Xylene (Total)0.028 <0.0047 39.6 25.6 0.056 <0.0047 9.9 120 530
m&p-Xylene 0.016 <0.0056 27.2 19.4 0.016 <0.0056 9.8 120 520o-Xylene 0.012 <0.0036 12.4 6.2 0.039 <0.0082 9.8 140 590
bis(2-Ethylhexyl)phthalate <0.21 <0.15 2.5J 1.7J <0.14 <0.15 14 39 160
1-Methylnaphthalene <0.12 <0.12 7.2 28.1 0.33J <0.12 0.11 18 73
2-Methylnaphthalene 0.44J <0.12 15.2 46.5 0.64 <0.11 3.1 48 600Fluorene0.079J <0.12 <1.2 3.1J <0.11 <0.12 110 480 6000
Naphthalene 0.050J <0.11 9.3 11.1 0.19J <0.11 0.39 2.1 8.8Phenanthrene0.26J <0.12 1.2J 5.8 <0.11 <0.11 NS NS NS
Arsenic 1.5 <0.50 <26.7 <0.57 4.0 1.9J 5.8 0.68 3.0Barium3031.6 200 52.1 112 12.4 580 3,100 47,000
Cadmium 4.5 0.10 <2.7 0.064J <0.051 0.16 3.0 14 200
Chromium 16 20.8 346 37.2 133 17.5 NS NS NSLead131193956320.1 9.1 250 400 800
Selenium 3.5 5.2 <26.7 4.4 1.9 <0.51 2.1 78 1,200Mercury<0.021 0.060 0.015 0.018 0.035 0.024 1.0 2.3 9.7
Hexavalent Chromium <0.355 <0.355 1.94 1.80 <0.301 <0.341 3.8 0.31 6.5
Notes:Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)
Only those constituents detected in at least one sample are listed above. For complete results, refer to laboratory report.Sample ID: First sample is composite / second sample listed is the grab collected for VOCs only
Soil sample results are compared to the NCDEQ PSRGs dated July 2020
NCDEQ = North Carolina Department of Environmental QualityPSRG = Preliminary Soil Remediation Goal
J= Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.Bold denotes concentration equal to or an exceedance of the Protection of Groundwater PSRGItalics denotes concentration equal to or an exceedance of the Residential Health Based PSRG
Underline denotes concentration equal to or an exceedance of the Industrial/Commercial Health Based PSRG
Semi-Volatile Organic Compounds (SVOCs) by EPA Method 8270
Resource Conservation and Recovery Act (RCRA) Metals & Hex Chrome by EPA Methods 6010, 7471, and 7199
COMPARISON CRITERIA
Protection of Groundwater PSRG Residential Health Based PSRG
Industrial/ Commercial Health Based PSRGVolatile Organic Compounds (VOCs) by EPA Method 8260
ANALYTICAL RESULTS
TABLE 1: SUMMARY OF SOIL ANALYTICAL RESULTSSEVENTH STREET PROPERTIESEAST 7TH STREET & NORTH CASWELL ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-8832-CNCDEQ, BROWNFIELDS PROJECT NO. 24004-20-060

APPENDIX A

PHOTOGRAPHIC LOG
EAST 7TH STREET SITE
EAST 7TH STREET & NORTH CASWELL ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NUMBER: 49-8832-A
Photograph 1: CCI contractor vacuuming product out of UST.
Photograph 2: View inside UST after being vacuumed out from small hole on top caused by excavator during discovery.
PHOTOGRAPHIC LOG
EAST 7TH STREET SITE
EAST 7TH STREET & NORTH CASWELL ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NUMBER: 49-8832-A
Photograph 3: View of UST in place prior to removal.
Photograph 4: View of removal of the UST.
PHOTOGRAPHIC LOG
EAST 7TH STREET SITE
EAST 7TH STREET & NORTH CASWELL ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NUMBER: 49-8832-A
Photograph 5: View of the bottom side of the UST with no visible holes.
Photograph 6: View of the in-situ soil beneath the UST.

APPENDIX B

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NON-HAZARDOUS WASTE MANIFEST
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WASTE MANIFEST
1. Generator's US EPA ID No.
3. Generator's Name and Mailing Address F-(. S:, _ C.. \-\. 0.. ( { ()
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4. Generator's Phone ( 70 o-3 ·3
5. Transporter 1 Company Name
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7. Transporter 2 Company Name 8.
9. Designated Facility Name and Site Address /
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10.
a.
b.
US EPA ID Number
US EPA ID Number
US EPA ID Number
Manifest
Document No.
A. State Transporter's ID
B. Transporter 1 Phone
C. State Transporter's ID
D. Transporter 2 Phone
E. State Facility's ID
F. Facility's Phone
Containers
No. Type
13.
Total
Quantity
2. Page 1
of f
14.
Unit
Wt.Nol.
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G. Additional Descriptions for Materials Listed Above H. Handling Codes for Wastes Listed Above
15. Special Handling Instructions and Additional Information
16. GENERATOR'S CERTIFICATION: I hereby certify that the contents of this shipment are fully and accurately described and are in all respects
in proper condition for transport. The materials described on this manifest are not subject to federal hazardous waste regulations.
Signature ~ Month i>v
Date
Day !Jr
Date T 17. Transporter 1 Acknowledgement of Receipt of Materials Rl--------------------------.-------....,,.------------------------1 A PrlntedfTyped Name ~ 1---.....:....~_-....;;A./;:.__...i.:::::,;..:.:.,o........,_-'-=...__ _______ ..._---'-__ ::;...._ ____________ .a......;;:::'---'-;;;...._--I
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19. Discrepancy Indication Space
Signature Month Day Year
1t---------------------------------------------------l L 20. Facility Owner or Operator: Certification of receipt of the waste materials covered by this manifest, except as noted in item 19.
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Date

APPENDIX C

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this
case narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
10/8/20 16:10
ECS Carolinas, LLP (Charlotte)
Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: 7th & Caswell
Lab Submittal Date: 09/28/2020
Work Order: 0090375
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Project Manager
Terri W. Cole
Data Qualifiers Key Reference:
CCVL CCV result is below control limits but within method parameters. A standard at or below the RL was analyzed and
found acceptable. Result is reported but considered estimated.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
M Matrix spike outside of the control limits.
SR Surrogate recovery outside of the QC limits.
Method Detection LimitMDL
Not Detected at the MDLU
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 21
Sample Receipt Summary
10/08/2020
Work Order: 0090375
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
0090375-01 09/28/20 11:00TS-1 09/28/20 14:43Solid
Samples were received in good condition at 3.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 21
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 0090375
10/08/2020
Summary of Detections
0.44 J mg/kg dry0090375-01 TS-1 2-Methylnaphthalene 8270E
0.079 J mg/kg dry0090375-01 TS-1 Fluorene 8270E
0.050 J mg/kg dry0090375-01 TS-1 Naphthalene 8270E
0.26 J mg/kg dry0090375-01 TS-1 Phenanthrene 8270E
1.5 mg/kg dry0090375-01 TS-1 Arsenic *6020B
30 mg/kg dry0090375-01 TS-1 Barium *6020B
4.5 mg/kg dry0090375-01 TS-1 Cadmium *6020B
16 mg/kg dry0090375-01 TS-1 Chromium *6020B
13 mg/kg dry0090375-01 TS-1 Lead *6020B
3.5 mg/kg dry0090375-01 TS-1 Selenium *6020B
0.17 CCVL mg/kg dry0090375-01 TS-1 Acetone 8260D
0.0042 J mg/kg dry0090375-01 TS-1 Ethylbenzene 8260D
0.0093 mg/kg dry0090375-01 TS-1 Isopropylbenzene (Cumene)8260D
0.016 mg/kg dry0090375-01 TS-1 m,p-Xylenes 8260D
0.16 mg/kg dry0090375-01 TS-1 Naphthalene 8260D
0.012 mg/kg dry0090375-01 TS-1 o-Xylene 8260D
0.028 mg/kg dry0090375-01 TS-1 Xylenes, total 8260D
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 21
Laboratory Report
10/08/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Sample Matrix: Solid
Client Sample ID:
Sample ID: 0090375-01
Work Order: 0090375
Time Collected: 09/28/20 11:00
Time Submitted: 09/28/20 14:43
TS-1
General Chemistry Parameters
*SM2540 G P0J000610.100 10/2/20 0:46 EDV% by
Weight
0.100% Solids 71.5
Semivolatile Organic Compounds by GC/MS
8270E P0J000210.46 10/2/20 15:42 JMVmg/kg dry 0.121,1’-Biphenyl 0.12 U
8270E P0J000210.46 10/2/20 15:42 JMVmg/kg dry 0.272,3,4,6-Tetrachlorophenol 0.27 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.192,4,5-Trichlorophenol 0.19 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.222,4,6-Trichlorophenol 0.22 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.182,4-Dichlorophenol 0.18 U
8270E P0J000210.46 10/2/20 15:42 JMVmg/kg dry 0.192,4-Dimethylphenol 0.19 U
8270E P0J000212.1 10/2/20 15:42 JMVmg/kg dry 0.542,4-Dinitrophenol 0.54 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.242,4-Dinitrotoluene 0.24 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.242,6-Dinitrotoluene 0.24 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.222-Chloronaphthalene 0.22 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.172-Chlorophenol 0.17 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.0182-Methylnaphthalene 0.44 J
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.172-Methylphenol 0.17 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.202-Nitroaniline 0.20 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.152-Nitrophenol 0.15 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.183,3’-Dichlorobenzidine 0.18 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.203/4-Methylphenol 0.20 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.173-Nitroaniline 0.17 U
8270E P0J000212.1 10/2/20 15:42 JMVmg/kg dry 0.504,6-Dinitro-2-methylphenol 0.50 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.214-Bromophenyl phenyl ether 0.21 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.174-Chloro-3-methylphenol 0.17 U
8270E P0J000210.46 10/2/20 15:42 JMVmg/kg dry 0.114-Chloroaniline 0.11 U
8270E P0J000211.4 10/2/20 15:42 JMVmg/kg dry 0.284-Chlorophenyl phenyl ether 0.28 U
8270E P0J000210.46 10/2/20 15:42 JMVmg/kg dry 0.144-Nitroaniline 0.14 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.234-Nitrophenol 0.23 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.021Acenaphthene0.021 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.018Acenaphthylene0.018 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.22Acetophenone0.22 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.010Anthracene0.010 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.11Atrazine0.11 U
8270E P0J000210.46 10/2/20 15:42 JMVmg/kg dry 0.079Benzaldehyde0.079 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.011Benzo(a)anthracene 0.011 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.0082Benzo(a)pyrene 0.0082 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.0084Benzo(b)fluoranthene 0.0084 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.0090Benzo(g,h,i)perylene 0.0090 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.0097Benzo(k)fluoranthene 0.0097 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.17bis(2-Chloroethoxy)methane 0.17 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.15Bis(2-Chloroethyl)ether 0.15 U
8270E P0J000210.46 10/2/20 15:42 JMVmg/kg dry 0.16Bis(2-chloroisopropyl)ether 0.16 U
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 21
Laboratory Report
10/08/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Sample Matrix: Solid
Client Sample ID:
Sample ID: 0090375-01
Work Order: 0090375
Time Collected: 09/28/20 11:00
Time Submitted: 09/28/20 14:43
TS-1
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.21Bis(2-Ethylhexyl)phthalate 0.21 U
8270E P0J000210.46 10/2/20 15:42 JMVmg/kg dry 0.16Butyl benzyl phthalate 0.16 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.17Caprolactam0.17 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.21Carbazole0.21 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.011Chrysene0.011 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.026Dibenzo(a,h)anthracene 0.026 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.25Dibenzofuran0.25 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.24Diethyl phthalate 0.24 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.22Dimethyl phthalate 0.22 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.23Di-n-butyl phthalate 0.23 U
8270E P0J000210.46 10/2/20 15:42 JMVmg/kg dry 0.24Di-n-octyl phthalate 0.24 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.010Fluoranthene0.010 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.016Fluorene0.079 J
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.20Hexachlorobenzene0.20 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.21Hexachlorobutadiene0.21 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.31Hexachlorocyclopentadiene0.31 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.14Hexachloroethane0.14 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.026Indeno(1,2,3-cd)pyrene 0.026 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.20Isophorone0.20 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.019Naphthalene0.050 J
8270E P0J000210.46 10/2/20 15:42 JMVmg/kg dry 0.19Nitrobenzene0.19 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.21N-Nitroso-di-n-propylamine 0.21 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.25N-Nitrosodiphenylamine 0.25 U
8270E P0J000211.4 10/2/20 15:42 JMVmg/kg dry 0.58Pentachlorophenol0.58 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.010Phenanthrene0.26 J
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.15Phenol0.15 U
8270E P0J000210.91 10/2/20 15:42 JMVmg/kg dry 0.013Pyrene0.013 U
Surrogate Recovery Control Limits
37-131103 %2,4,6-Tribromophenol
47-13095 %2-Fluorobiphenyl
44-11795 %2-Fluorophenol
45-12185 %Nitrobenzene-d5
37-12793 %Phenol-d5
38-13590 %Terphenyl-d14
Total Metals
*7471B P0I098610.070 9/29/20 13:53 EDVmg/kg dry 0.021Mercury0.021 U
*6020B P0I0983101.4 10/6/20 19:24 JABmg/kg dry 0.12Arsenic1.5
*6020B P0I0983101410/6/20 19:24 JABmg/kg dry 0.50Barium30
*6020B P0I0983100.70 10/6/20 19:24 JABmg/kg dry 0.052Cadmium4.5
*6020B P0I0983101410/6/20 19:24 JABmg/kg dry 3.4Chromium16
*6020B P0J0108101.4 10/8/20 14:11 JABmg/kg dry 0.11Lead13
*6020B P0I0983101.4 10/6/20 19:24 JABmg/kg dry 0.32Selenium3.5
*6020B P0I0983100.70 10/6/20 19:24 JABmg/kg dry 0.071Silver0.071 U
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 21
Laboratory Report
10/08/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Sample Matrix: Solid
Client Sample ID:
Sample ID: 0090375-01
Work Order: 0090375
Time Collected: 09/28/20 11:00
Time Submitted: 09/28/20 14:43
TS-1
Volatile Organic Compounds by GC/MS
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.000841,1,1-Trichloroethane 0.00084 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.000411,1,2,2-Tetrachloroethane 0.00041 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.000991,1,2-Trichloro-1,2,2-trifluoroethane 0.00099 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.000621,1,2-Trichloroethane 0.00062 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00101,1-Dichloroethane 0.0010 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00101,1-Dichloroethylene 0.0010 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.000821,2,3-Trichlorobenzene 0.00082 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.000541,2,4-Trichlorobenzene 0.00054 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.000721,2-Dibromo-3-chloropropane 0.00072 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.000511,2-Dibromoethane 0.00051 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.000641,2-Dichlorobenzene 0.00064 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.000681,2-Dichloroethane 0.00068 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.000861,2-Dichloropropane 0.00086 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.000711,3-Dichlorobenzene 0.00071 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.000721,4-Dichlorobenzene 0.00072 U
8260D P0I100010.11 9/29/20 16:00 TBLmg/kg dry 0.0161,4-Dioxane 0.016 U
8260D P0I100010.023 9/29/20 16:00 TBLmg/kg dry 0.0015Acetone0.17 CCVL
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00089Benzene0.00089 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00094Bromochloromethane0.00094 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00054Bromodichloromethane0.00054 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00044Bromoform0.00044 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.0028Bromomethane0.0028 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00098Carbon disulfide 0.00098 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.0011Carbon Tetrachloride 0.0011 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00089Chlorobenzene0.00089 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.0011Chloroethane0.0011 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00070Chloroform0.00070 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.0017Chloromethane0.0017 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00090cis-1,2-Dichloroethylene 0.00090 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00056cis-1,3-Dichloropropylene 0.00056 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00069Cyclohexane0.00069 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00038Dibromochloromethane0.00038 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.0016Dichlorodifluoromethane0.0016 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00086Ethylbenzene0.0042 J
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00066Isopropylbenzene (Cumene)0.0093
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.0015m,p-Xylenes 0.016
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00053Methyl Acetate 0.00053 U
8260D P0I100010.023 9/29/20 16:00 TBLmg/kg dry 0.00039Methyl Butyl Ketone (2-Hexanone)0.00039 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00034Methylcyclohexane0.00034 U
8260D P0I100010.023 9/29/20 16:00 TBLmg/kg dry 0.0013Methyl Ethyl Ketone (2-Butanone)0.0013 U
8260D P0I100010.023 9/29/20 16:00 TBLmg/kg dry 0.00046Methyl Isobutyl Ketone 0.00046 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00092Methylene Chloride 0.00092 U
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 21
Laboratory Report
10/08/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Sample Matrix: Solid
Client Sample ID:
Sample ID: 0090375-01
Work Order: 0090375
Time Collected: 09/28/20 11:00
Time Submitted: 09/28/20 14:43
TS-1
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00080Methyl-tert-Butyl Ether 0.00080 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.00058Naphthalene0.16
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00061o-Xylene 0.012
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00055Styrene0.00055 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.0010Tetrachloroethylene0.0010 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00091Toluene0.00091 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.0011trans-1,2-Dichloroethylene 0.0011 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.00049trans-1,3-Dichloropropylene 0.00049 U
8260D P0I100010.0057 9/29/20 16:00 TBLmg/kg dry 0.0011Trichloroethylene0.0011 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.0015Trichlorofluoromethane0.0015 U
8260D P0I100010.011 9/29/20 16:00 TBLmg/kg dry 0.0011Vinyl chloride 0.0011 U
8260D P0I100010.017 9/29/20 16:00 TBLmg/kg dry 0.0021Xylenes, total 0.028
Surrogate Recovery Control Limits
70-13096 %4-Bromofluorobenzene
84-123104 %Dibromofluoromethane
76-12993 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0I1000 - 5035
Blank (P0I1000-BLK1)Prepared & Analyzed: 09/29/20
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wetBRL0.010
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.010
1,2,4-Trichlorobenzene mg/kg wetBRL0.010
1,2-Dibromo-3-chloropropane mg/kg wetBRL0.010
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
1,4-Dioxane mg/kg wetBRL0.10
Acetone mg/kg wetBRL0.020
Benzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon disulfide mg/kg wetBRL0.0050
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.010
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Cyclohexane mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.010
Ethylbenzene mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Acetate mg/kg wetBRL0.0050
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.020
Methylcyclohexane mg/kg wetBRL0.0050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.020
Methyl Isobutyl Ketone mg/kg wetBRL0.020
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.0050
Naphthalene mg/kg wetBRL0.010
o-Xylene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0I1000 - 5035
Blank (P0I1000-BLK1)Prepared & Analyzed: 09/29/20
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.010
Vinyl chloride mg/kg wetBRL0.010
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.4
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10050.0
ug/L 50.00 76-129Surrogate: Toluene-d8 9848.8
LCS (P0I1000-BS1)Prepared & Analyzed: 09/29/20
1,1,1-Trichloroethane mg/kg wet0.0534 0.0050 0.05000 67-131107
1,1,2,2-Tetrachloroethane mg/kg wet0.0465 0.0050 0.05000 56-12693
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wet0.0519 0.010 0.05000 70-130104
1,1,2-Trichloroethane mg/kg wet0.0470 0.0050 0.05000 70-13394
1,1-Dichloroethane mg/kg wet0.0509 0.0050 0.05000 74-127102
1,1-Dichloroethylene mg/kg wet0.0515 0.0050 0.05000 67-149103
1,2,3-Trichlorobenzene mg/kg wet0.0514 0.010 0.05000 68-130103
1,2,4-Trichlorobenzene mg/kg wet0.0531 0.010 0.05000 66-125106
1,2-Dibromo-3-chloropropane mg/kg wet0.0491 0.010 0.05000 55-15798
1,2-Dibromoethane mg/kg wet0.0473 0.0050 0.05000 70-13295
1,2-Dichlorobenzene mg/kg wet0.0489 0.0050 0.05000 72-12398
1,2-Dichloroethane mg/kg wet0.0467 0.0050 0.05000 68-12893
1,2-Dichloropropane mg/kg wet0.0516 0.0050 0.05000 73-130103
1,3-Dichlorobenzene mg/kg wet0.0500 0.0050 0.05000 71-120100
1,4-Dichlorobenzene mg/kg wet0.0492 0.0050 0.05000 71-12398
1,4-Dioxane mg/kg wet0.466 0.10 0.5000 70-13093
Acetone mg/kg wet0.0800 0.020 0.1000 29-19880
Benzene mg/kg wet0.0514 0.0050 0.05000 74-127103
Bromochloromethane mg/kg wet0.0514 0.0050 0.05000 72-134103
Bromodichloromethane mg/kg wet0.0518 0.0050 0.05000 75-122104
Bromoform mg/kg wet0.0524 0.0050 0.05000 66-135105
Bromomethane mg/kg wet0.0567 0.010 0.05000 20-180113
Carbon disulfide mg/kg wet0.0502 0.0050 0.05000 61-129100
Carbon Tetrachloride mg/kg wet0.0549 0.0050 0.05000 64-143110
Chlorobenzene mg/kg wet0.0489 0.0050 0.05000 74-11898
Chloroethane mg/kg wet0.0423 0.010 0.05000 33-14985
Chloroform mg/kg wet0.0516 0.0050 0.05000 73-127103
Chloromethane mg/kg wet0.0464 0.010 0.05000 45-14393
cis-1,2-Dichloroethylene mg/kg wet0.0503 0.0050 0.05000 76-134101
cis-1,3-Dichloropropylene mg/kg wet0.0528 0.0050 0.05000 71-125106
Cyclohexane mg/kg wet0.0541 0.0050 0.05000 70-130108
Dibromochloromethane mg/kg wet0.0506 0.0050 0.05000 73-122101
Dichlorodifluoromethane mg/kg wet0.0396 0.010 0.05000 26-14679
Ethylbenzene mg/kg wet0.0513 0.0050 0.05000 74-128103
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0I1000 - 5035
LCS (P0I1000-BS1)Prepared & Analyzed: 09/29/20
Isopropylbenzene (Cumene)mg/kg wet0.0529 0.0050 0.05000 68-126106
m,p-Xylenes mg/kg wet0.105 0.010 0.1000 75-124105
Methyl Acetate mg/kg wet0.0399 0.0050 0.05000 70-13080
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0476 0.020 0.05000 61-15795
Methylcyclohexane mg/kg wet0.0510 0.0050 0.05000 70-130102
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0463 0.020 0.05000 63-14993
Methyl Isobutyl Ketone mg/kg wet0.0475 0.020 0.05000 57-16295
Methylene Chloride mg/kg wet0.0465 0.0050 0.05000 74-12993
Methyl-tert-Butyl Ether mg/kg wet0.0472 0.0050 0.05000 70-13094
o-Xylene mg/kg wet0.0522 0.0050 0.05000 74-126104
Styrene mg/kg wet0.0510 0.0050 0.05000 77-121102
Tetrachloroethylene mg/kg wet0.0543 0.0050 0.05000 68-130109
Toluene mg/kg wet0.0514 0.0050 0.05000 71-129103
trans-1,2-Dichloroethylene mg/kg wet0.0515 0.0050 0.05000 73-132103
trans-1,3-Dichloropropylene mg/kg wet0.0529 0.0050 0.05000 68-123106
Trichloroethylene mg/kg wet0.0531 0.0050 0.05000 75-133106
Trichlorofluoromethane mg/kg wet0.0476 0.010 0.05000 44-14695
Vinyl chloride mg/kg wet0.0478 0.010 0.05000 48-14796
Xylenes, total mg/kg wet0.157 0.015 0.1500 74-126105
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.6
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9949.4
ug/L 50.00 76-129Surrogate: Toluene-d8 9647.8
Matrix Spike (P0I1000-MS1)Prepared & Analyzed: 09/29/20 Source: 0090375-01
1,1,1-Trichloroethane mg/kg dry0.0577 0.0070 0.06994 BRL 52-13982
1,1,2,2-Tetrachloroethane mg/kg dry0.0510 0.0070 0.06994 BRL 39-13573
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg dry0.0560 0.014 0.06994 BRL 70-13080
1,1,2-Trichloroethane mg/kg dry0.0516 0.0070 0.06994 BRL 44-14074
1,1-Dichloroethane mg/kg dry0.0563 0.0070 0.06994 BRL 59-13781
1,1-Dichloroethylene mg/kg dry0.0576 0.0070 0.06994 BRL 54-16282
1,2,3-Trichlorobenzene mg/kg dry0.0484 0.014 0.06994 BRL 34-12069
1,2,4-Trichlorobenzene mg/kg dry0.0477 0.014 0.06994 BRL 35-11668
1,2-Dibromo-3-chloropropane mg/kg dry0.0525 0.014 0.06994 BRL 27-13275
1,2-Dibromoethane mg/kg dry0.0525 0.0070 0.06994 BRL 49-13275
1,2-Dichlorobenzene mg/kg dry0.0499 0.0070 0.06994 BRL 42-13071
1,2-Dichloroethane mg/kg dry0.0524 0.0070 0.06994 BRL 51-13175
1,2-Dichloropropane mg/kg dry0.0575 0.0070 0.06994 BRL 55-13882
1,3-Dichlorobenzene mg/kg dry0.0491 0.0070 0.06994 BRL 41-12970
1,4-Dichlorobenzene mg/kg dry0.0489 0.0070 0.06994 BRL 44-13470
1,4-Dioxane mg/kg dry0.558 0.14 0.6994 BRL 70-13080
Acetone mg/kg dry0.0837 0.028 0.1399 0.167 M34-143NR
Benzene mg/kg dry0.0573 0.0070 0.06994 BRL 60-13582
Bromochloromethane mg/kg dry0.0577 0.0070 0.06994 BRL 55-13682
Bromodichloromethane mg/kg dry0.0557 0.0070 0.06994 BRL 55-12780
Bromoform mg/kg dry0.0533 0.0070 0.06994 BRL 40-13676
Bromomethane mg/kg dry0.0621 0.014 0.06994 BRL 30-13789
Carbon disulfide mg/kg dry0.0561 0.0070 0.06994 BRL 49-13980
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0I1000 - 5035
Matrix Spike (P0I1000-MS1)Prepared & Analyzed: 09/29/20 Source: 0090375-01
Carbon Tetrachloride mg/kg dry0.0560 0.0070 0.06994 BRL 48-15380
Chlorobenzene mg/kg dry0.0536 0.0070 0.06994 BRL 57-12577
Chloroethane mg/kg dry0.0506 0.014 0.06994 BRL 16-17772
Chloroform mg/kg dry0.0573 0.0070 0.06994 BRL 56-13782
Chloromethane mg/kg dry0.0499 0.014 0.06994 BRL 40-14571
cis-1,2-Dichloroethylene mg/kg dry0.0566 0.0070 0.06994 BRL 58-14081
cis-1,3-Dichloropropylene mg/kg dry0.0565 0.0070 0.06994 BRL 42-13581
Cyclohexane mg/kg dry0.0533 0.0070 0.06994 BRL 70-13076
Dibromochloromethane mg/kg dry0.0542 0.0070 0.06994 BRL 49-12778
Dichlorodifluoromethane mg/kg dry0.0428 0.014 0.06994 BRL 25-15161
Ethylbenzene mg/kg dry0.0541 0.0070 0.06994 0.00424 44-14471
Isopropylbenzene (Cumene)mg/kg dry0.0525 0.0070 0.06994 0.00933 41-14062
m,p-Xylenes mg/kg dry0.110 0.014 0.1399 0.0159 36-14868
Methyl Acetate mg/kg dry0.0486 0.0070 0.06994 BRL M70-13069
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0419 0.028 0.06994 BRL 30-14760
Methylcyclohexane mg/kg dry0.0448 0.0070 0.06994 BRL M70-13064
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0358 0.028 0.06994 BRL 24-16051
Methyl Isobutyl Ketone mg/kg dry0.0501 0.028 0.06994 BRL 25-16372
Methylene Chloride mg/kg dry0.0502 0.0070 0.06994 BRL 53-14472
Methyl-tert-Butyl Ether mg/kg dry0.0520 0.0070 0.06994 BRL 49-13574
o-Xylene mg/kg dry0.0566 0.0070 0.06994 0.0120 43-14364
Styrene mg/kg dry0.0536 0.0070 0.06994 BRL 42-13277
Tetrachloroethylene mg/kg dry0.0541 0.0070 0.06994 BRL 47-14277
Toluene mg/kg dry0.0561 0.0070 0.06994 BRL 57-13580
trans-1,2-Dichloroethylene mg/kg dry0.0574 0.0070 0.06994 BRL 58-14182
trans-1,3-Dichloropropylene mg/kg dry0.0545 0.0070 0.06994 BRL 41-12478
Trichloroethylene mg/kg dry0.0571 0.0070 0.06994 BRL 38-16482
Trichlorofluoromethane mg/kg dry0.0496 0.014 0.06994 BRL 30-15771
Vinyl chloride mg/kg dry0.0527 0.014 0.06994 BRL 40-15675
Xylenes, total mg/kg dry0.167 0.021 0.2098 0.0279 36-14866
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.7
ug/L 50.00 76-129Surrogate: Toluene-d8 9748.7
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0I1000 - 5035
Matrix Spike Dup (P0I1000-MSD1)Prepared & Analyzed: 09/29/20 Source: 0090375-01
1,1,1-Trichloroethane mg/kg dry0.0544 0.0070 0.06994 BRL 2152-13978 6
1,1,2,2-Tetrachloroethane mg/kg dry0.0485 0.0070 0.06994 BRL 2239-13569 5
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg dry0.0527 0.014 0.06994 BRL 2070-13075 6
1,1,2-Trichloroethane mg/kg dry0.0488 0.0070 0.06994 BRL 2144-14070 6
1,1-Dichloroethane mg/kg dry0.0540 0.0070 0.06994 BRL 2159-13777 4
1,1-Dichloroethylene mg/kg dry0.0540 0.0070 0.06994 BRL 2254-16277 6
1,2,3-Trichlorobenzene mg/kg dry0.0474 0.014 0.06994 BRL 4134-12068 2
1,2,4-Trichlorobenzene mg/kg dry0.0460 0.014 0.06994 BRL 6235-11666 4
1,2-Dibromo-3-chloropropane mg/kg dry0.0510 0.014 0.06994 BRL 2527-13273 3
1,2-Dibromoethane mg/kg dry0.0490 0.0070 0.06994 BRL 1549-13270 7
1,2-Dichlorobenzene mg/kg dry0.0472 0.0070 0.06994 BRL 2142-13067 5
1,2-Dichloroethane mg/kg dry0.0497 0.0070 0.06994 BRL 1351-13171 5
1,2-Dichloropropane mg/kg dry0.0542 0.0070 0.06994 BRL 1655-13878 6
1,3-Dichlorobenzene mg/kg dry0.0465 0.0070 0.06994 BRL 2441-12966 6
1,4-Dichlorobenzene mg/kg dry0.0460 0.0070 0.06994 BRL 2144-13466 6
1,4-Dioxane mg/kg dry0.523 0.14 0.6994 BRL 2070-13075 7
Acetone mg/kg dry0.0806 0.028 0.1399 0.167 49 M34-143NR 4
Benzene mg/kg dry0.0541 0.0070 0.06994 BRL 2060-13577 6
Bromochloromethane mg/kg dry0.0562 0.0070 0.06994 BRL 1855-13680 2
Bromodichloromethane mg/kg dry0.0534 0.0070 0.06994 BRL 1755-12776 4
Bromoform mg/kg dry0.0501 0.0070 0.06994 BRL 3540-13672 6
Bromomethane mg/kg dry0.0597 0.014 0.06994 BRL 3030-13785 4
Carbon disulfide mg/kg dry0.0532 0.0070 0.06994 BRL 2649-13976 5
Carbon Tetrachloride mg/kg dry0.0546 0.0070 0.06994 BRL 2348-15378 2
Chlorobenzene mg/kg dry0.0497 0.0070 0.06994 BRL 1457-12571 8
Chloroethane mg/kg dry0.0463 0.014 0.06994 BRL 4716-17766 9
Chloroform mg/kg dry0.0535 0.0070 0.06994 BRL 1856-13777 7
Chloromethane mg/kg dry0.0493 0.014 0.06994 BRL 2640-14570 1
cis-1,2-Dichloroethylene mg/kg dry0.0535 0.0070 0.06994 BRL 2858-14076 6
cis-1,3-Dichloropropylene mg/kg dry0.0546 0.0070 0.06994 BRL 3242-13578 3
Cyclohexane mg/kg dry0.0511 0.0070 0.06994 BRL 2070-13073 4
Dibromochloromethane mg/kg dry0.0505 0.0070 0.06994 BRL 2449-12772 7
Dichlorodifluoromethane mg/kg dry0.0406 0.014 0.06994 BRL 3725-15158 5
Ethylbenzene mg/kg dry0.0500 0.0070 0.06994 0.00424 1944-14465 8
Isopropylbenzene (Cumene)mg/kg dry0.0495 0.0070 0.06994 0.00933 2741-14058 6
m,p-Xylenes mg/kg dry0.102 0.014 0.1399 0.0159 2036-14862 8
Methyl Acetate mg/kg dry0.0418 0.0070 0.06994 BRL 20 M70-13060 15
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0391 0.028 0.06994 BRL 4230-14756 7
Methylcyclohexane mg/kg dry0.0438 0.0070 0.06994 BRL 20 M70-13063 2
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0350 0.028 0.06994 BRL 4224-16050 2
Methyl Isobutyl Ketone mg/kg dry0.0485 0.028 0.06994 BRL 4425-16369 3
Methylene Chloride mg/kg dry0.0473 0.0070 0.06994 BRL 1453-14468 6
Methyl-tert-Butyl Ether mg/kg dry0.0505 0.0070 0.06994 BRL 2249-13572 3
o-Xylene mg/kg dry0.0522 0.0070 0.06994 0.0120 1743-14357 8
Styrene mg/kg dry0.0495 0.0070 0.06994 BRL 2842-13271 8
Tetrachloroethylene mg/kg dry0.0516 0.0070 0.06994 BRL 2647-14274 5
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0I1000 - 5035
Matrix Spike Dup (P0I1000-MSD1)Prepared & Analyzed: 09/29/20 Source: 0090375-01
Toluene mg/kg dry0.0529 0.0070 0.06994 BRL 2257-13576 6
trans-1,2-Dichloroethylene mg/kg dry0.0549 0.0070 0.06994 BRL 1858-14179 4
trans-1,3-Dichloropropylene mg/kg dry0.0531 0.0070 0.06994 BRL 2041-12476 3
Trichloroethylene mg/kg dry0.0543 0.0070 0.06994 BRL 1838-16478 5
Trichlorofluoromethane mg/kg dry0.0456 0.014 0.06994 BRL 2730-15765 8
Vinyl chloride mg/kg dry0.0496 0.014 0.06994 BRL 3540-15671 6
Xylenes, total mg/kg dry0.155 0.021 0.2098 0.0279 2036-14860 8
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.2
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9949.6
ug/L 50.00 76-129Surrogate: Toluene-d8 9547.6
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0J0002 - 3546
Blank (P0J0002-BLK1)Prepared: 10/01/20 Analyzed: 10/02/20
1,1’-Biphenyl mg/kg wetBRL0.33
2,3,4,6-Tetrachlorophenol mg/kg wetBRL0.33
2,4,5-Trichlorophenol mg/kg wetBRL0.66
2,4,6-Trichlorophenol mg/kg wetBRL0.66
2,4-Dichlorophenol mg/kg wetBRL0.66
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL1.5
2,4-Dinitrotoluene mg/kg wetBRL0.66
2,6-Dinitrotoluene mg/kg wetBRL0.66
2-Chloronaphthalene mg/kg wetBRL0.66
2-Chlorophenol mg/kg wetBRL0.66
2-Methylnaphthalene mg/kg wetBRL0.66
2-Methylphenol mg/kg wetBRL0.66
2-Nitroaniline mg/kg wetBRL0.66
2-Nitrophenol mg/kg wetBRL0.66
3,3’-Dichlorobenzidine mg/kg wetBRL0.66
3/4-Methylphenol mg/kg wetBRL0.66
3-Nitroaniline mg/kg wetBRL0.66
4,6-Dinitro-2-methylphenol mg/kg wetBRL1.5
4-Bromophenyl phenyl ether mg/kg wetBRL0.66
4-Chloro-3-methylphenol mg/kg wetBRL0.66
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL1.0
4-Nitroaniline mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.66
Acenaphthene mg/kg wetBRL0.66
Acenaphthylene mg/kg wetBRL0.66
Acetophenone mg/kg wetBRL0.66
Anthracene mg/kg wetBRL0.66
Atrazine mg/kg wetBRL0.66
Benzaldehyde mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.66
Benzo(a)pyrene mg/kg wetBRL0.66
Benzo(b)fluoranthene mg/kg wetBRL0.66
Benzo(g,h,i)perylene mg/kg wetBRL0.66
Benzo(k)fluoranthene mg/kg wetBRL0.66
bis(2-Chloroethoxy)methane mg/kg wetBRL0.66
Bis(2-Chloroethyl)ether mg/kg wetBRL0.66
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.66
Butyl benzyl phthalate mg/kg wetBRL0.33
Caprolactam mg/kg wetBRL0.66
Carbazole mg/kg wetBRL0.66
Chrysene mg/kg wetBRL0.66
Dibenzo(a,h)anthracene mg/kg wetBRL0.66
Dibenzofuran mg/kg wetBRL0.66
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0J0002 - 3546
Blank (P0J0002-BLK1)Prepared: 10/01/20 Analyzed: 10/02/20
Diethyl phthalate mg/kg wetBRL0.66
Dimethyl phthalate mg/kg wetBRL0.66
Di-n-butyl phthalate mg/kg wetBRL0.66
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.66
Fluorene mg/kg wetBRL0.66
Hexachlorobenzene mg/kg wetBRL0.66
Hexachlorobutadiene mg/kg wetBRL0.66
Hexachlorocyclopentadiene mg/kg wetBRL0.66
Hexachloroethane mg/kg wetBRL0.66
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.66
Isophorone mg/kg wetBRL0.66
Naphthalene mg/kg wetBRL0.66
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.66
N-Nitrosodiphenylamine mg/kg wetBRL0.66
Pentachlorophenol mg/kg wetBRL1.0
Phenanthrene mg/kg wetBRL0.66
Phenol mg/kg wetBRL0.66
Pyrene mg/kg wetBRL0.66
mg/kg wet 3.330 37-131Surrogate: 2,4,6-Tribromophenol 1103.65
mg/kg wet 1.665 47-130Surrogate: 2-Fluorobiphenyl 1191.99
mg/kg wet 3.330 SR44-117Surrogate: 2-Fluorophenol 1173.89
mg/kg wet 1.665 45-121Surrogate: Nitrobenzene-d5 1061.77
mg/kg wet 3.330 37-127Surrogate: Phenol-d5 1204.00
mg/kg wet 1.665 38-135Surrogate: Terphenyl-d14 1161.92
LCS (P0J0002-BS1)Prepared: 10/01/20 Analyzed: 10/02/20
2,4,5-Trichlorophenol mg/kg wet1.93 0.66 1.666 41-124116
2,4,6-Trichlorophenol mg/kg wet1.91 0.66 1.666 39-126115
2,4-Dichlorophenol mg/kg wet1.87 0.66 1.666 40-122113
2,4-Dimethylphenol mg/kg wet1.98 0.33 1.666 30-127119
2,4-Dinitrophenol mg/kg wet1.59 1.5 1.666 27-12996
2,4-Dinitrotoluene mg/kg wet2.07 0.66 1.666 48-126124
2,6-Dinitrotoluene mg/kg wet2.03 0.66 1.666 46-124122
2-Chloronaphthalene mg/kg wet1.84 0.66 1.666 41-114111
2-Chlorophenol mg/kg wet1.87 0.66 1.666 34-121112
2-Methylnaphthalene mg/kg wet1.77 0.66 1.666 38-122106
2-Methylphenol mg/kg wet1.90 0.66 1.666 32-122114
2-Nitroaniline mg/kg wet2.08 0.66 1.666 44-127125
2-Nitrophenol mg/kg wet1.81 0.66 1.666 36-123109
3,3’-Dichlorobenzidine mg/kg wet1.87 0.66 1.666 22-121112
3/4-Methylphenol mg/kg wet1.73 0.66 1.666 34-119104
3-Nitroaniline mg/kg wet1.86 0.66 1.666 33-119112
4,6-Dinitro-2-methylphenol mg/kg wet1.73 1.5 1.666 29-132104
4-Bromophenyl phenyl ether mg/kg wet1.91 0.66 1.666 46-124115
4-Chloro-3-methylphenol mg/kg wet1.96 0.66 1.666 45-122118
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0J0002 - 3546
LCS (P0J0002-BS1)Prepared: 10/01/20 Analyzed: 10/02/20
4-Chloroaniline mg/kg wet1.77 0.33 1.666 LH17-106106
4-Chlorophenyl phenyl ether mg/kg wet1.84 1.0 1.666 45-121111
4-Nitroaniline mg/kg wet2.09 0.33 1.666 63-147125
4-Nitrophenol mg/kg wet1.94 0.66 1.666 30-132116
Acenaphthene mg/kg wet1.91 0.66 1.666 40-123115
Acenaphthylene mg/kg wet1.99 0.66 1.666 32-132119
Acetophenone mg/kg wet1.37 0.66 1.666 33-11582
Anthracene mg/kg wet2.03 0.66 1.666 47-123122
Benzo(a)anthracene mg/kg wet1.89 0.66 1.666 49-126114
Benzo(a)pyrene mg/kg wet2.13 0.66 1.666 45-129128
Benzo(b)fluoranthene mg/kg wet1.98 0.66 1.666 45-132119
Benzo(g,h,i)perylene mg/kg wet2.05 0.66 1.666 43-134123
Benzo(k)fluoranthene mg/kg wet2.06 0.66 1.666 47-132123
bis(2-Chloroethoxy)methane mg/kg wet1.93 0.66 1.666 36-121116
Bis(2-Chloroethyl)ether mg/kg wet1.60 0.66 1.666 31-12096
Bis(2-chloroisopropyl)ether mg/kg wet1.65 0.33 1.666 33-13199
Bis(2-Ethylhexyl)phthalate mg/kg wet2.13 0.66 1.666 51-133128
Butyl benzyl phthalate mg/kg wet2.07 0.33 1.666 48-132124
Carbazole mg/kg wet2.00 0.66 1.666 50-123120
Chrysene mg/kg wet1.77 0.66 1.666 50-124106
Dibenzo(a,h)anthracene mg/kg wet0.949 0.66 1.666 45-13457
Dibenzofuran mg/kg wet1.75 0.66 1.666 44-120105
Diethyl phthalate mg/kg wet1.93 0.66 1.666 50-124116
Dimethyl phthalate mg/kg wet1.95 0.66 1.666 48-124117
Di-n-butyl phthalate mg/kg wet2.11 0.66 1.666 51-128127
Di-n-octyl phthalate mg/kg wet2.12 0.33 1.666 45-140127
Fluoranthene mg/kg wet1.98 0.66 1.666 50-127119
Fluorene mg/kg wet1.95 0.66 1.666 43-125117
Hexachlorobenzene mg/kg wet1.89 0.66 1.666 45-122114
Hexachlorobutadiene mg/kg wet1.79 0.66 1.666 32-123108
Hexachlorocyclopentadiene mg/kg wet1.86 0.66 1.666 32-117112
Hexachloroethane mg/kg wet1.56 0.66 1.666 28-11794
Indeno(1,2,3-cd)pyrene mg/kg wet1.99 0.66 1.666 45-133120
Isophorone mg/kg wet1.37 0.66 1.666 30-12283
Naphthalene mg/kg wet1.79 0.66 1.666 35-123107
Nitrobenzene mg/kg wet1.61 0.33 1.666 34-12297
N-Nitroso-di-n-propylamine mg/kg wet1.74 0.66 1.666 36-120105
N-Nitrosodiphenylamine mg/kg wet2.31 0.66 1.666 LH38-127139
Pentachlorophenol mg/kg wet2.06 1.0 1.666 25-133123
Phenanthrene mg/kg wet1.98 0.66 1.666 50-121119
Phenol mg/kg wet1.83 0.66 1.666 34-121110
Pyrene mg/kg wet1.98 0.66 1.666 47-127119
mg/kg wet 3.331 37-131Surrogate: 2,4,6-Tribromophenol 1163.86
mg/kg wet 1.666 47-130Surrogate: 2-Fluorobiphenyl 1011.68
mg/kg wet 3.331 44-117Surrogate: 2-Fluorophenol 1043.45
mg/kg wet 1.666 45-121Surrogate: Nitrobenzene-d5 901.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P0J0002 - 3546
LCS (P0J0002-BS1)Prepared: 10/01/20 Analyzed: 10/02/20
mg/kg wet 3.331 37-127Surrogate: Phenol-d5 993.30
mg/kg wet 1.666 38-135Surrogate: Terphenyl-d14 1001.66
LCS (P0J0002-BS2)Prepared: 10/01/20 Analyzed: 10/02/20
1,1’-Biphenyl mg/kg wet1.73 0.33 1.661 40-117104
2,3,4,6-Tetrachlorophenol mg/kg wet2.17 0.33 1.661 L144-125131
Atrazine mg/kg wet1.88 0.66 1.661 47-127113
Benzaldehyde mg/kg wet1.61 0.33 1.661 35-11597
Caprolactam mg/kg wet1.80 0.66 1.661 46-117108
mg/kg wet 3.321 37-131Surrogate: 2,4,6-Tribromophenol 1023.40
mg/kg wet 1.661 47-130Surrogate: 2-Fluorobiphenyl 941.56
mg/kg wet 3.321 44-117Surrogate: 2-Fluorophenol 1013.36
mg/kg wet 1.661 45-121Surrogate: Nitrobenzene-d5 861.43
mg/kg wet 3.321 37-127Surrogate: Phenol-d5 1003.33
mg/kg wet 1.661 38-135Surrogate: Terphenyl-d14 901.50
LCS Dup (P0J0002-BSD2)Prepared: 10/01/20 Analyzed: 10/02/20
1,1’-Biphenyl mg/kg wet1.66 0.33 1.667 2040-117100 4
2,3,4,6-Tetrachlorophenol mg/kg wet2.08 0.33 1.667 2044-125125 4
Atrazine mg/kg wet1.87 0.66 1.667 2047-127112 0.6
Benzaldehyde mg/kg wet1.54 0.33 1.667 2035-11592 4
Caprolactam mg/kg wet1.75 0.66 1.667 2046-117105 3
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 993.31
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 921.54
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 983.25
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 851.41
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 963.19
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 891.49
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P0I0983 - 3050B
Blank (P0I0983-BLK1)Prepared: 09/29/20 Analyzed: 10/06/20
Arsenic mg/kg wetBRL1.0
Barium mg/kg wetBRL10
Cadmium mg/kg wetBRL0.50
Chromium mg/kg wetBRL10
Selenium mg/kg wetBRL1.0
Silver mg/kg wetBRL0.50
LCS (P0I0983-BS1)Prepared: 09/29/20 Analyzed: 10/06/20
Arsenic mg/kg wet12.0 1.0 12.50 80-12096
Barium mg/kg wet11.4 10 12.50 80-12091
Cadmium mg/kg wet12.9 0.50 12.50 80-120103
Chromium mg/kg wet13.2 10 12.50 80-120106
Selenium mg/kg wet11.3 1.0 12.50 80-12091
Silver mg/kg wet5.20 0.50 5.000 80-120104
Matrix Spike (P0I0983-MS1)Prepared: 09/29/20 Analyzed: 10/06/20 Source: 0090375-01
Arsenic mg/kg dry14.1 1.4 17.49 1.53 M75-12572
Barium mg/kg dry54.8 14 17.48 30.3 M75-125140
Cadmium mg/kg dry20.2 0.70 17.48 4.49 75-12590
Chromium mg/kg dry33.5 14 17.49 16.2 75-12599
Selenium mg/kg dry18.2 1.4 17.48 3.53 75-12584
Silver mg/kg dry7.23 0.70 6.994 BRL 75-125103
Matrix Spike Dup (P0I0983-MSD1)Prepared: 09/29/20 Analyzed: 10/06/20 Source: 0090375-01
Arsenic mg/kg dry14.6 1.4 17.49 1.53 20 M75-12574 3
Barium mg/kg dry51.9 14 17.48 30.3 2075-125124 5
Cadmium mg/kg dry23.4 0.70 17.48 4.49 2075-125108 15
Chromium mg/kg dry33.6 14 17.49 16.2 2075-12599 0.09
Selenium mg/kg dry16.5 1.4 17.48 3.53 20 M75-12574 10
Silver mg/kg dry7.19 0.70 6.994 BRL 2075-125103 0.5
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P0I0983 - 3050B
Post Spike (P0I0983-PS1)Prepared: 09/29/20 Analyzed: 10/06/20 Source: 0090375-01
Arsenic ug/L95.7 100.0 4.37 80-12091
Barium ug/L170 100.0 86.6 80-12084
Cadmium ug/L112 100.0 12.8 80-12099
Chromium ug/L142 100.0 46.3 80-12095
Selenium ug/L102 100.0 10.1 80-12092
Silver ug/L99.5 100.0 0.0250 80-12099
Batch P0I0986 - 7471B
Blank (P0I0986-BLK1)Prepared & Analyzed: 09/29/20
Mercury mg/kg wetBRL0.050
LCS (P0I0986-BS1)Prepared & Analyzed: 09/29/20
Mercury mg/kg wet0.417 0.050 0.4167 80-120100
Batch P0J0108 - 3050B
Blank (P0J0108-BLK1)Prepared & Analyzed: 10/08/20
Lead mg/kg wetBRL1.0
LCS (P0J0108-BS1)Prepared & Analyzed: 10/08/20
Lead mg/kg wet12.7 1.0 12.50 80-120101
Matrix Spike (P0J0108-MS1)Prepared & Analyzed: 10/08/20 Source: 0090375-01
Lead mg/kg dry34.6 1.4 17.49 13.2 75-125122
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 21
10/8/20
Level II QC Report
1812 Center Park Drive, Suite D
Project: 7th & CaswellECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Chris Orrell
Work Order: 0090375
Time Submitted: 9/28/2020 2:43:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P0J0108 - 3050B
Matrix Spike Dup (P0J0108-MSD1)Prepared & Analyzed: 10/08/20 Source: 0090375-01
Lead mg/kg dry32.0 1.4 17.49 13.2 2075-125107 8
Post Spike (P0J0108-PS1)Prepared & Analyzed: 10/08/20 Source: 0090375-01
Lead ug/L136 100.0 37.7 80-12098
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P0J00060090375-01 10/01/20 8:3830 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P0J00020090375-01 10/01/20 7:3030.34 1g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P0J01080090375-01 10/08/20 7:522 50g mL
P0I09830090375-01 09/29/20 10:002 50g mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P0I09860090375-01 09/29/20 11:350.6 50g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P0I10000090375-01 09/29/20 9:416.14 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 21
Page 21 of 21
#=CL#
February 04, 2021
LIMS USE: FR - CHRIS ORRELL
LIMS OBJECT ID: 92518589
92518589
Project:
Pace Project No.:
RE:
Chris Orrell
ECS Southeast, LLP
1900 Center Park Dr Suite D
9809 Aviary Hill Way, Charlott
Charlotte, NC 28217
7th & Caswell Tank Pull
Dear Chris Orrell:
Enclosed are the analytical results for sample(s) received by the laboratory on January 26, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
A revised report is being submitted on 2/4/21 to include MDLs and J values, per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Jenna Dew, ECS Southeast
ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 45
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 45
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Lab ID Sample ID Matrix Date Collected Date Received
92518589001 T-1 Solid 01/25/21 09:00 01/26/21 11:45
92518589002 T-2 Solid 01/25/21 09:30 01/26/21 11:45
92518589003 T-3 Solid 01/25/21 10:00 01/26/21 11:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 45
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92518589001 T-1 EPA 6010D 7 PASI-AKQ, SH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92518589002 T-2 EPA 6010D 7 PASI-AKQ
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92518589003 T-3 EPA 6010D 7 PASI-AKQ, SH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-1 Lab ID:92518589001 Collected:01/25/21 09:00 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND mg/kg 01/31/21 17:01 7440-38-201/27/21 15:542.5 0.50 1
Barium 31.6 mg/kg 01/29/21 04:00 7440-39-301/27/21 15:541.0 0.25 1
Cadmium 0.10 mg/kg 01/29/21 04:00 7440-43-901/27/21 15:540.10 0.050 1
Chromium 20.8 mg/kg 01/29/21 04:00 7440-47-301/27/21 15:540.50 0.25 1
Lead 11.0 mg/kg 01/29/21 04:00 7439-92-101/27/21 15:541.0 0.25 1
Selenium 5.2 mg/kg 01/29/21 04:00 7782-49-201/27/21 15:541.0 0.50 1
Silver ND mg/kg 01/29/21 04:00 7440-22-401/27/21 15:540.50 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.060 mg/kg 01/27/21 16:42 7439-97-601/27/21 15:200.0042 0.0032 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 01/29/21 14:13 83-32-901/28/21 10:510.46 0.12 1
Acenaphthylene ND mg/kg 01/29/21 14:13 208-96-801/28/21 10:510.46 0.11 1
Aniline ND mg/kg 01/29/21 14:13 62-53-301/28/21 10:510.46 0.10 1
Anthracene ND mg/kg 01/29/21 14:13 120-12-701/28/21 10:510.46 0.12 1
Benzo(a)anthracene ND mg/kg 01/29/21 14:13 56-55-301/28/21 10:510.46 0.15 1
Benzo(a)pyrene ND mg/kg 01/29/21 14:13 50-32-801/28/21 10:510.46 0.20 1
Benzo(b)fluoranthene ND mg/kg 01/29/21 14:13 205-99-201/28/21 10:510.46 0.18 1
Benzo(g,h,i)perylene ND mg/kg 01/29/21 14:13 191-24-201/28/21 10:510.46 0.18 1
Benzo(k)fluoranthene ND mg/kg 01/29/21 14:13 207-08-901/28/21 10:510.46 0.19 1
Benzoic Acid ND mg/kg 01/29/21 14:13 65-85-001/28/21 10:512.3 0.49 1
Benzyl alcohol ND mg/kg 01/29/21 14:13 100-51-601/28/21 10:510.92 0.24 1
4-Bromophenylphenyl ether ND mg/kg 01/29/21 14:13 101-55-301/28/21 10:510.46 0.12 1
Butylbenzylphthalate ND mg/kg 01/29/21 14:13 85-68-701/28/21 10:510.46 0.12 1
4-Chloro-3-methylphenol ND mg/kg 01/29/21 14:13 59-50-701/28/21 10:510.92 0.28 1
4-Chloroaniline ND mg/kg 01/29/21 14:13 106-47-801/28/21 10:510.92 0.28 1
bis(2-Chloroethoxy)methane ND mg/kg 01/29/21 14:13 111-91-101/28/21 10:510.46 0.12 1
bis(2-Chloroethyl) ether ND mg/kg 01/29/21 14:13 111-44-401/28/21 10:510.46 0.097 1
2-Chloronaphthalene ND mg/kg 01/29/21 14:13 91-58-701/28/21 10:510.46 0.10 1
2-Chlorophenol ND mg/kg 01/29/21 14:13 95-57-801/28/21 10:510.46 0.11 1
4-Chlorophenylphenyl ether ND mg/kg 01/29/21 14:13 7005-72-301/28/21 10:510.46 0.12 1
Chrysene ND mg/kg 01/29/21 14:13 218-01-901/28/21 10:510.46 0.13 1
Dibenz(a,h)anthracene ND mg/kg 01/29/21 14:13 53-70-301/28/21 10:510.46 0.18 1
Dibenzofuran ND mg/kg 01/29/21 14:13 132-64-901/28/21 10:510.46 0.11 1
1,2-Dichlorobenzene ND mg/kg 01/29/21 14:13 95-50-101/28/21 10:510.46 0.099 1
1,3-Dichlorobenzene ND mg/kg 01/29/21 14:13 541-73-101/28/21 10:510.46 0.10 1
1,4-Dichlorobenzene ND mg/kg 01/29/21 14:13 106-46-701/28/21 10:510.46 0.10 1
3,3'-Dichlorobenzidine ND mg/kg 01/29/21 14:13 91-94-1 IL01/28/21 10:510.92 0.32 1
2,4-Dichlorophenol ND mg/kg 01/29/21 14:13 120-83-201/28/21 10:510.46 0.15 1
Diethylphthalate ND mg/kg 01/29/21 14:13 84-66-201/28/21 10:510.46 0.099 1
2,4-Dimethylphenol ND mg/kg 01/29/21 14:13 105-67-901/28/21 10:510.46 0.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-1 Lab ID:92518589001 Collected:01/25/21 09:00 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 01/29/21 14:13 131-11-301/28/21 10:510.46 0.10 1
Di-n-butylphthalate ND mg/kg 01/29/21 14:13 84-74-201/28/21 10:510.46 0.11 1
4,6-Dinitro-2-methylphenol ND mg/kg 01/29/21 14:13 534-52-101/28/21 10:510.92 0.74 1
2,4-Dinitrophenol ND mg/kg 01/29/21 14:13 51-28-501/28/21 10:512.3 1.5 1
2,4-Dinitrotoluene ND mg/kg 01/29/21 14:13 121-14-201/28/21 10:510.46 0.12 1
2,6-Dinitrotoluene ND mg/kg 01/29/21 14:13 606-20-201/28/21 10:510.46 0.12 1
Di-n-octylphthalate ND mg/kg 01/29/21 14:13 117-84-001/28/21 10:510.46 0.26 1
bis(2-Ethylhexyl)phthalate ND mg/kg 01/29/21 14:13 117-81-701/28/21 10:510.46 0.15 1
Fluoranthene ND mg/kg 01/29/21 14:13 206-44-001/28/21 10:510.46 0.14 1
Fluorene ND mg/kg 01/29/21 14:13 86-73-701/28/21 10:510.46 0.12 1
Hexachloro-1,3-butadiene ND mg/kg 01/29/21 14:13 87-68-301/28/21 10:510.46 0.11 1
Hexachlorobenzene ND mg/kg 01/29/21 14:13 118-74-101/28/21 10:510.46 0.12 1
Hexachlorocyclopentadiene ND mg/kg 01/29/21 14:13 77-47-4 v201/28/21 10:510.46 0.18 1
Hexachloroethane ND mg/kg 01/29/21 14:13 67-72-101/28/21 10:510.46 0.10 1
Indeno(1,2,3-cd)pyrene ND mg/kg 01/29/21 14:13 193-39-501/28/21 10:510.46 0.21 1
Isophorone ND mg/kg 01/29/21 14:13 78-59-101/28/21 10:510.46 0.099 1
1-Methylnaphthalene ND mg/kg 01/29/21 14:13 90-12-001/28/21 10:510.46 0.12 1
2-Methylnaphthalene ND mg/kg 01/29/21 14:13 91-57-601/28/21 10:510.46 0.12 1
2-Methylphenol(o-Cresol)ND mg/kg 01/29/21 14:13 95-48-701/28/21 10:510.46 0.10 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 01/29/21 14:13 15831-10-401/28/21 10:510.46 0.12 1
Naphthalene ND mg/kg 01/29/21 14:13 91-20-301/28/21 10:510.46 0.11 1
2-Nitroaniline ND mg/kg 01/29/21 14:13 88-74-401/28/21 10:512.3 0.23 1
3-Nitroaniline ND mg/kg 01/29/21 14:13 99-09-201/28/21 10:512.3 0.24 1
4-Nitroaniline ND mg/kg 01/29/21 14:13 100-01-601/28/21 10:510.92 0.23 1
Nitrobenzene ND mg/kg 01/29/21 14:13 98-95-301/28/21 10:510.46 0.11 1
2-Nitrophenol ND mg/kg 01/29/21 14:13 88-75-501/28/21 10:510.46 0.14 1
4-Nitrophenol ND mg/kg 01/29/21 14:13 100-02-701/28/21 10:512.3 0.73 1
N-Nitrosodimethylamine ND mg/kg 01/29/21 14:13 62-75-901/28/21 10:510.46 0.13 1
N-Nitroso-di-n-propylamine ND mg/kg 01/29/21 14:13 621-64-701/28/21 10:510.46 0.13 1
N-Nitrosodiphenylamine ND mg/kg 01/29/21 14:13 86-30-601/28/21 10:510.46 0.12 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 01/29/21 14:13 108-60-101/28/21 10:510.46 0.13 1
Pentachlorophenol ND mg/kg 01/29/21 14:13 87-86-501/28/21 10:510.92 0.21 1
Phenanthrene ND mg/kg 01/29/21 14:13 85-01-801/28/21 10:510.46 0.12 1
Phenol ND mg/kg 01/29/21 14:13 108-95-201/28/21 10:510.46 0.11 1
Pyrene ND mg/kg 01/29/21 14:13 129-00-001/28/21 10:510.46 0.13 1
Pyridine ND mg/kg 01/29/21 14:13 110-86-101/28/21 10:510.46 0.12 1
1,2,4-Trichlorobenzene ND mg/kg 01/29/21 14:13 120-82-101/28/21 10:510.46 0.10 1
2,4,5-Trichlorophenol ND mg/kg 01/29/21 14:13 95-95-401/28/21 10:510.46 0.12 1
2,4,6-Trichlorophenol ND mg/kg 01/29/21 14:13 88-06-201/28/21 10:510.46 0.12 1
Surrogates
Nitrobenzene-d5 (S)83 %01/29/21 14:13 4165-60-001/28/21 10:5121-130 1
2-Fluorobiphenyl (S)84 %01/29/21 14:13 321-60-801/28/21 10:5119-130 1
Terphenyl-d14 (S)110 %01/29/21 14:13 1718-51-001/28/21 10:5115-130 1
Phenol-d6 (S)80 %01/29/21 14:13 13127-88-301/28/21 10:5118-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-1 Lab ID:92518589001 Collected:01/25/21 09:00 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)73 %01/29/21 14:13 367-12-401/28/21 10:5118-130 1
2,4,6-Tribromophenol (S)91 %01/29/21 14:13 118-79-601/28/21 10:5118-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 01/27/21 19:01 67-64-101/27/21 12:550.16 0.053 1
Benzene ND mg/kg 01/27/21 19:01 71-43-201/27/21 12:550.0082 0.0033 1
Bromobenzene ND mg/kg 01/27/21 19:01 108-86-101/27/21 12:550.0082 0.0027 1
Bromochloromethane ND mg/kg 01/27/21 19:01 74-97-501/27/21 12:550.0082 0.0024 1
Bromodichloromethane ND mg/kg 01/27/21 19:01 75-27-401/27/21 12:550.0082 0.0032 1
Bromoform ND mg/kg 01/27/21 19:01 75-25-201/27/21 12:550.0082 0.0029 1
Bromomethane ND mg/kg 01/27/21 19:01 74-83-9 IK01/27/21 12:550.016 0.013 1
2-Butanone (MEK)ND mg/kg 01/27/21 19:01 78-93-301/27/21 12:550.16 0.040 1
n-Butylbenzene ND mg/kg 01/27/21 19:01 104-51-801/27/21 12:550.0082 0.0039 1
sec-Butylbenzene ND mg/kg 01/27/21 19:01 135-98-801/27/21 12:550.0082 0.0036 1
tert-Butylbenzene ND mg/kg 01/27/21 19:01 98-06-601/27/21 12:550.0082 0.0029 1
Carbon tetrachloride ND mg/kg 01/27/21 19:01 56-23-501/27/21 12:550.0082 0.0031 1
Chlorobenzene ND mg/kg 01/27/21 19:01 108-90-701/27/21 12:550.0082 0.0016 1
Chloroethane ND mg/kg 01/27/21 19:01 75-00-301/27/21 12:550.016 0.0064 1
Chloroform ND mg/kg 01/27/21 19:01 67-66-301/27/21 12:550.0082 0.0050 1
Chloromethane ND mg/kg 01/27/21 19:01 74-87-301/27/21 12:550.016 0.0069 1
2-Chlorotoluene ND mg/kg 01/27/21 19:01 95-49-801/27/21 12:550.0082 0.0029 1
4-Chlorotoluene ND mg/kg 01/27/21 19:01 106-43-401/27/21 12:550.0082 0.0015 1
1,2-Dibromo-3-chloropropane ND mg/kg 01/27/21 19:01 96-12-801/27/21 12:550.0082 0.0032 1
Dibromochloromethane ND mg/kg 01/27/21 19:01 124-48-101/27/21 12:550.0082 0.0046 1
1,2-Dibromoethane (EDB)ND mg/kg 01/27/21 19:01 106-93-401/27/21 12:550.0082 0.0036 1
Dibromomethane ND mg/kg 01/27/21 19:01 74-95-301/27/21 12:550.0082 0.0018 1
1,2-Dichlorobenzene ND mg/kg 01/27/21 19:01 95-50-101/27/21 12:550.0082 0.0030 1
1,3-Dichlorobenzene ND mg/kg 01/27/21 19:01 541-73-101/27/21 12:550.0082 0.0026 1
1,4-Dichlorobenzene ND mg/kg 01/27/21 19:01 106-46-701/27/21 12:550.0082 0.0021 1
Dichlorodifluoromethane ND mg/kg 01/27/21 19:01 75-71-801/27/21 12:550.016 0.0036 1
1,1-Dichloroethane ND mg/kg 01/27/21 19:01 75-34-301/27/21 12:550.0082 0.0034 1
1,2-Dichloroethane ND mg/kg 01/27/21 19:01 107-06-201/27/21 12:550.0082 0.0055 1
1,1-Dichloroethene ND mg/kg 01/27/21 19:01 75-35-401/27/21 12:550.0082 0.0034 1
cis-1,2-Dichloroethene ND mg/kg 01/27/21 19:01 156-59-201/27/21 12:550.0082 0.0028 1
trans-1,2-Dichloroethene ND mg/kg 01/27/21 19:01 156-60-501/27/21 12:550.0082 0.0029 1
1,2-Dichloropropane ND mg/kg 01/27/21 19:01 78-87-501/27/21 12:550.0082 0.0025 1
1,3-Dichloropropane ND mg/kg 01/27/21 19:01 142-28-901/27/21 12:550.0082 0.0026 1
2,2-Dichloropropane ND mg/kg 01/27/21 19:01 594-20-701/27/21 12:550.0082 0.0027 1
1,1-Dichloropropene ND mg/kg 01/27/21 19:01 563-58-601/27/21 12:550.0082 0.0040 1
cis-1,3-Dichloropropene ND mg/kg 01/27/21 19:01 10061-01-501/27/21 12:550.0082 0.0022 1
trans-1,3-Dichloropropene ND mg/kg 01/27/21 19:01 10061-02-601/27/21 12:550.0082 0.0028 1
Diisopropyl ether ND mg/kg 01/27/21 19:01 108-20-301/27/21 12:550.0082 0.0022 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-1 Lab ID:92518589001 Collected:01/25/21 09:00 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 01/27/21 19:01 100-41-401/27/21 12:550.0082 0.0038 1
Hexachloro-1,3-butadiene ND mg/kg 01/27/21 19:01 87-68-301/27/21 12:550.016 0.013 1
2-Hexanone ND mg/kg 01/27/21 19:01 591-78-601/27/21 12:550.082 0.0079 1
Isopropylbenzene (Cumene)ND mg/kg 01/27/21 19:01 98-82-801/27/21 12:550.0082 0.0028 1
p-Isopropyltoluene ND mg/kg 01/27/21 19:01 99-87-601/27/21 12:550.0082 0.0041 1
Methylene Chloride ND mg/kg 01/27/21 19:01 75-09-201/27/21 12:550.033 0.023 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 01/27/21 19:01 108-10-101/27/21 12:550.082 0.0079 1
Methyl-tert-butyl ether ND mg/kg 01/27/21 19:01 1634-04-401/27/21 12:550.0082 0.0031 1
Naphthalene ND mg/kg 01/27/21 19:01 91-20-301/27/21 12:550.0082 0.0043 1
n-Propylbenzene ND mg/kg 01/27/21 19:01 103-65-101/27/21 12:550.0082 0.0029 1
Styrene ND mg/kg 01/27/21 19:01 100-42-501/27/21 12:550.0082 0.0022 1
1,1,1,2-Tetrachloroethane ND mg/kg 01/27/21 19:01 630-20-601/27/21 12:550.0082 0.0032 1
1,1,2,2-Tetrachloroethane ND mg/kg 01/27/21 19:01 79-34-501/27/21 12:550.0082 0.0022 1
Tetrachloroethene ND mg/kg 01/27/21 19:01 127-18-401/27/21 12:550.0082 0.0026 1
Toluene ND mg/kg 01/27/21 19:01 108-88-301/27/21 12:550.0082 0.0023 1
1,2,3-Trichlorobenzene ND mg/kg 01/27/21 19:01 87-61-601/27/21 12:550.0082 0.0067 1
1,2,4-Trichlorobenzene ND mg/kg 01/27/21 19:01 120-82-101/27/21 12:550.0082 0.0069 1
1,1,1-Trichloroethane ND mg/kg 01/27/21 19:01 71-55-601/27/21 12:550.0082 0.0043 1
1,1,2-Trichloroethane ND mg/kg 01/27/21 19:01 79-00-501/27/21 12:550.0082 0.0027 1
Trichloroethene ND mg/kg 01/27/21 19:01 79-01-601/27/21 12:550.0082 0.0021 1
Trichlorofluoromethane ND mg/kg 01/27/21 19:01 75-69-401/27/21 12:550.0082 0.0045 1
1,2,3-Trichloropropane ND mg/kg 01/27/21 19:01 96-18-401/27/21 12:550.0082 0.0042 1
1,2,4-Trimethylbenzene ND mg/kg 01/27/21 19:01 95-63-601/27/21 12:550.0082 0.0023 1
1,3,5-Trimethylbenzene ND mg/kg 01/27/21 19:01 108-67-801/27/21 12:550.0082 0.0028 1
Vinyl acetate ND mg/kg 01/27/21 19:01 108-05-401/27/21 12:550.082 0.0060 1
Vinyl chloride ND mg/kg 01/27/21 19:01 75-01-401/27/21 12:550.016 0.0042 1
Xylene (Total)ND mg/kg 01/27/21 19:01 1330-20-701/27/21 12:550.016 0.0047 1
m&p-Xylene ND mg/kg 01/27/21 19:01 179601-23-101/27/21 12:550.016 0.0056 1
o-Xylene ND mg/kg 01/27/21 19:01 95-47-601/27/21 12:550.0082 0.0036 1
Surrogates
Toluene-d8 (S)99 %01/27/21 19:01 2037-26-501/27/21 12:5570-130 1
4-Bromofluorobenzene (S)96 %01/27/21 19:01 460-00-401/27/21 12:5569-134 1
1,2-Dichloroethane-d4 (S)109 %01/27/21 19:01 17060-07-001/27/21 12:5570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.2 %01/26/21 17:03 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.8 %02/03/21 08:5202/03/21 08:411
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-1 Lab ID:92518589001 Collected:01/25/21 09:00 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 02/01/21 21:23 18540-29-902/01/21 16:101.39 0.355 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-2 Lab ID:92518589002 Collected:01/25/21 09:30 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND mg/kg 01/31/21 17:04 7440-38-2 D301/27/21 15:5413326.7 50
Barium 200 mg/kg 01/31/21 17:04 7440-39-301/27/21 15:5453.3 13.3 50
Cadmium ND mg/kg 01/31/21 17:04 7440-43-9 D301/27/21 15:545.3 2.7 50
Chromium 346 mg/kg 01/31/21 17:04 7440-47-301/27/21 15:5426.7 13.3 50
Lead 939 mg/kg 01/31/21 17:04 7439-92-101/27/21 15:5453.3 13.3 50
Selenium ND mg/kg 01/31/21 17:04 7782-49-2 D301/27/21 15:5453.3 26.7 50
Silver ND mg/kg 01/31/21 17:04 7440-22-4 D301/27/21 15:5426.7 13.3 50
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.015 mg/kg 01/27/21 16:44 7439-97-601/27/21 15:200.0066 0.0051 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 01/29/21 12:51 83-32-901/28/21 10:514.6 1.2 10
Acenaphthylene ND mg/kg 01/29/21 12:51 208-96-801/28/21 10:514.6 1.1 10
Aniline ND mg/kg 01/29/21 12:51 62-53-301/28/21 10:514.6 1.0 10
Anthracene ND mg/kg 01/29/21 12:51 120-12-701/28/21 10:514.6 1.2 10
Benzo(a)anthracene ND mg/kg 01/29/21 12:51 56-55-301/28/21 10:514.6 1.4 10
Benzo(a)pyrene ND mg/kg 01/29/21 12:51 50-32-801/28/21 10:514.6 2.0 10
Benzo(b)fluoranthene ND mg/kg 01/29/21 12:51 205-99-201/28/21 10:514.6 1.8 10
Benzo(g,h,i)perylene ND mg/kg 01/29/21 12:51 191-24-201/28/21 10:514.6 1.8 10
Benzo(k)fluoranthene ND mg/kg 01/29/21 12:51 207-08-901/28/21 10:514.6 1.9 10
Benzoic Acid ND mg/kg 01/29/21 12:51 65-85-001/28/21 10:5122.8 4.9 10
Benzyl alcohol ND mg/kg 01/29/21 12:51 100-51-601/28/21 10:519.1 2.4 10
4-Bromophenylphenyl ether ND mg/kg 01/29/21 12:51 101-55-301/28/21 10:514.6 1.2 10
Butylbenzylphthalate ND mg/kg 01/29/21 12:51 85-68-701/28/21 10:514.6 1.2 10
4-Chloro-3-methylphenol ND mg/kg 01/29/21 12:51 59-50-701/28/21 10:519.1 2.8 10
4-Chloroaniline ND mg/kg 01/29/21 12:51 106-47-801/28/21 10:519.1 2.8 10
bis(2-Chloroethoxy)methane ND mg/kg 01/29/21 12:51 111-91-101/28/21 10:514.6 1.2 10
bis(2-Chloroethyl) ether ND mg/kg 01/29/21 12:51 111-44-401/28/21 10:514.6 0.97 10
2-Chloronaphthalene ND mg/kg 01/29/21 12:51 91-58-701/28/21 10:514.6 1.0 10
2-Chlorophenol ND mg/kg 01/29/21 12:51 95-57-801/28/21 10:514.6 1.1 10
4-Chlorophenylphenyl ether ND mg/kg 01/29/21 12:51 7005-72-301/28/21 10:514.6 1.2 10
Chrysene ND mg/kg 01/29/21 12:51 218-01-901/28/21 10:514.6 1.3 10
Dibenz(a,h)anthracene ND mg/kg 01/29/21 12:51 53-70-301/28/21 10:514.6 1.8 10
Dibenzofuran ND mg/kg 01/29/21 12:51 132-64-901/28/21 10:514.6 1.1 10
1,2-Dichlorobenzene ND mg/kg 01/29/21 12:51 95-50-101/28/21 10:514.6 0.98 10
1,3-Dichlorobenzene ND mg/kg 01/29/21 12:51 541-73-101/28/21 10:514.6 1.0 10
1,4-Dichlorobenzene ND mg/kg 01/29/21 12:51 106-46-701/28/21 10:514.6 1.0 10
3,3'-Dichlorobenzidine ND mg/kg 01/29/21 12:51 91-94-1 IL01/28/21 10:519.1 3.2 10
2,4-Dichlorophenol ND mg/kg 01/29/21 12:51 120-83-201/28/21 10:514.6 1.5 10
Diethylphthalate ND mg/kg 01/29/21 12:51 84-66-201/28/21 10:514.6 0.99 10
2,4-Dimethylphenol ND mg/kg 01/29/21 12:51 105-67-901/28/21 10:514.6 1.1 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-2 Lab ID:92518589002 Collected:01/25/21 09:30 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 01/29/21 12:51 131-11-301/28/21 10:514.6 1.0 10
Di-n-butylphthalate ND mg/kg 01/29/21 12:51 84-74-201/28/21 10:514.6 1.1 10
4,6-Dinitro-2-methylphenol ND mg/kg 01/29/21 12:51 534-52-101/28/21 10:519.1 7.3 10
2,4-Dinitrophenol ND mg/kg 01/29/21 12:51 51-28-501/28/21 10:5122.8 14.5 10
2,4-Dinitrotoluene ND mg/kg 01/29/21 12:51 121-14-201/28/21 10:514.6 1.2 10
2,6-Dinitrotoluene ND mg/kg 01/29/21 12:51 606-20-201/28/21 10:514.6 1.2 10
Di-n-octylphthalate ND mg/kg 01/29/21 12:51 117-84-001/28/21 10:514.6 2.6 10
bis(2-Ethylhexyl)phthalate 2.5J mg/kg 01/29/21 12:51 117-81-701/28/21 10:514.6 1.5 10
Fluoranthene ND mg/kg 01/29/21 12:51 206-44-001/28/21 10:514.6 1.4 10
Fluorene ND mg/kg 01/29/21 12:51 86-73-701/28/21 10:514.6 1.2 10
Hexachloro-1,3-butadiene ND mg/kg 01/29/21 12:51 87-68-301/28/21 10:514.6 1.1 10
Hexachlorobenzene ND mg/kg 01/29/21 12:51 118-74-101/28/21 10:514.6 1.2 10
Hexachlorocyclopentadiene ND mg/kg 01/29/21 12:51 77-47-4 v201/28/21 10:514.6 1.8 10
Hexachloroethane ND mg/kg 01/29/21 12:51 67-72-101/28/21 10:514.6 1.0 10
Indeno(1,2,3-cd)pyrene ND mg/kg 01/29/21 12:51 193-39-501/28/21 10:514.6 2.1 10
Isophorone ND mg/kg 01/29/21 12:51 78-59-101/28/21 10:514.6 0.99 10
1-Methylnaphthalene 7.2 mg/kg 01/29/21 12:51 90-12-001/28/21 10:514.6 1.2 10
2-Methylnaphthalene 15.2 mg/kg 01/29/21 12:51 91-57-601/28/21 10:514.6 1.2 10
2-Methylphenol(o-Cresol)ND mg/kg 01/29/21 12:51 95-48-701/28/21 10:514.6 1.0 10
3&4-Methylphenol(m&p Cresol)ND mg/kg 01/29/21 12:51 15831-10-401/28/21 10:514.6 1.1 10
Naphthalene 9.3 mg/kg 01/29/21 12:51 91-20-301/28/21 10:514.6 1.1 10
2-Nitroaniline ND mg/kg 01/29/21 12:51 88-74-401/28/21 10:5122.8 2.3 10
3-Nitroaniline ND mg/kg 01/29/21 12:51 99-09-201/28/21 10:5122.8 2.4 10
4-Nitroaniline ND mg/kg 01/29/21 12:51 100-01-601/28/21 10:519.1 2.2 10
Nitrobenzene ND mg/kg 01/29/21 12:51 98-95-301/28/21 10:514.6 1.1 10
2-Nitrophenol ND mg/kg 01/29/21 12:51 88-75-501/28/21 10:514.6 1.4 10
4-Nitrophenol ND mg/kg 01/29/21 12:51 100-02-701/28/21 10:5122.8 7.3 10
N-Nitrosodimethylamine ND mg/kg 01/29/21 12:51 62-75-901/28/21 10:514.6 1.3 10
N-Nitroso-di-n-propylamine ND mg/kg 01/29/21 12:51 621-64-701/28/21 10:514.6 1.3 10
N-Nitrosodiphenylamine ND mg/kg 01/29/21 12:51 86-30-601/28/21 10:514.6 1.2 10
2,2'-Oxybis(1-chloropropane)ND mg/kg 01/29/21 12:51 108-60-101/28/21 10:514.6 1.3 10
Pentachlorophenol ND mg/kg 01/29/21 12:51 87-86-501/28/21 10:519.1 2.1 10
Phenanthrene 1.2J mg/kg 01/29/21 12:51 85-01-801/28/21 10:514.6 1.1 10
Phenol ND mg/kg 01/29/21 12:51 108-95-201/28/21 10:514.6 1.1 10
Pyrene ND mg/kg 01/29/21 12:51 129-00-001/28/21 10:514.6 1.3 10
Pyridine ND mg/kg 01/29/21 12:51 110-86-101/28/21 10:514.6 1.2 10
1,2,4-Trichlorobenzene ND mg/kg 01/29/21 12:51 120-82-101/28/21 10:514.6 1.0 10
2,4,5-Trichlorophenol ND mg/kg 01/29/21 12:51 95-95-401/28/21 10:514.6 1.2 10
2,4,6-Trichlorophenol ND mg/kg 01/29/21 12:51 88-06-201/28/21 10:514.6 1.1 10
Surrogates
Nitrobenzene-d5 (S)0 %01/29/21 12:51 4165-60-0 D3,S401/28/21 10:5121-130 10
2-Fluorobiphenyl (S)0 %01/29/21 12:51 321-60-8 S401/28/21 10:5119-130 10
Terphenyl-d14 (S)0 %01/29/21 12:51 1718-51-0 S401/28/21 10:5115-130 10
Phenol-d6 (S)0 %01/29/21 12:51 13127-88-3 S401/28/21 10:5118-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-2 Lab ID:92518589002 Collected:01/25/21 09:30 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)0 %01/29/21 12:51 367-12-4 S401/28/21 10:5118-130 10
2,4,6-Tribromophenol (S)0 %01/29/21 12:51 118-79-6 S401/28/21 10:5118-130 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 01/28/21 15:19 67-64-101/28/21 12:061.7 0.55 10
Benzene 0.51 mg/kg 01/28/21 15:19 71-43-201/28/21 12:060.085 0.034 10
Bromobenzene ND mg/kg 01/28/21 15:19 108-86-101/28/21 12:060.085 0.028 10
Bromochloromethane ND mg/kg 01/28/21 15:19 74-97-501/28/21 12:060.085 0.025 10
Bromodichloromethane ND mg/kg 01/28/21 15:19 75-27-401/28/21 12:060.085 0.033 10
Bromoform ND mg/kg 01/28/21 15:19 75-25-201/28/21 12:060.085 0.030 10
Bromomethane ND mg/kg 01/28/21 15:19 74-83-9 IK01/28/21 12:060.17 0.13 10
2-Butanone (MEK)ND mg/kg 01/28/21 15:19 78-93-301/28/21 12:061.7 0.41 10
n-Butylbenzene ND mg/kg 01/28/21 15:19 104-51-801/28/21 12:060.085 0.040 10
sec-Butylbenzene ND mg/kg 01/28/21 15:19 135-98-801/28/21 12:060.085 0.037 10
tert-Butylbenzene ND mg/kg 01/28/21 15:19 98-06-601/28/21 12:060.085 0.030 10
Carbon tetrachloride ND mg/kg 01/28/21 15:19 56-23-501/28/21 12:060.085 0.032 10
Chlorobenzene ND mg/kg 01/28/21 15:19 108-90-701/28/21 12:060.085 0.016 10
Chloroethane ND mg/kg 01/28/21 15:19 75-00-301/28/21 12:060.17 0.066 10
Chloroform ND mg/kg 01/28/21 15:19 67-66-301/28/21 12:060.085 0.052 10
Chloromethane ND mg/kg 01/28/21 15:19 74-87-301/28/21 12:060.17 0.071 10
2-Chlorotoluene ND mg/kg 01/28/21 15:19 95-49-801/28/21 12:060.085 0.030 10
4-Chlorotoluene ND mg/kg 01/28/21 15:19 106-43-401/28/21 12:060.085 0.015 10
1,2-Dibromo-3-chloropropane ND mg/kg 01/28/21 15:19 96-12-801/28/21 12:060.085 0.033 10
Dibromochloromethane ND mg/kg 01/28/21 15:19 124-48-101/28/21 12:060.085 0.048 10
1,2-Dibromoethane (EDB)ND mg/kg 01/28/21 15:19 106-93-401/28/21 12:060.085 0.037 10
Dibromomethane ND mg/kg 01/28/21 15:19 74-95-301/28/21 12:060.085 0.018 10
1,2-Dichlorobenzene ND mg/kg 01/28/21 15:19 95-50-101/28/21 12:060.085 0.031 10
1,3-Dichlorobenzene ND mg/kg 01/28/21 15:19 541-73-101/28/21 12:060.085 0.026 10
1,4-Dichlorobenzene ND mg/kg 01/28/21 15:19 106-46-701/28/21 12:060.085 0.022 10
Dichlorodifluoromethane ND mg/kg 01/28/21 15:19 75-71-801/28/21 12:060.17 0.037 10
1,1-Dichloroethane ND mg/kg 01/28/21 15:19 75-34-301/28/21 12:060.085 0.035 10
1,2-Dichloroethane ND mg/kg 01/28/21 15:19 107-06-201/28/21 12:060.085 0.056 10
1,1-Dichloroethene ND mg/kg 01/28/21 15:19 75-35-401/28/21 12:060.085 0.035 10
cis-1,2-Dichloroethene 0.20 mg/kg 01/28/21 15:19 156-59-201/28/21 12:060.085 0.029 10
trans-1,2-Dichloroethene ND mg/kg 01/28/21 15:19 156-60-501/28/21 12:060.085 0.030 10
1,2-Dichloropropane ND mg/kg 01/28/21 15:19 78-87-501/28/21 12:060.085 0.026 10
1,3-Dichloropropane ND mg/kg 01/28/21 15:19 142-28-901/28/21 12:060.085 0.027 10
2,2-Dichloropropane ND mg/kg 01/28/21 15:19 594-20-701/28/21 12:060.085 0.028 10
1,1-Dichloropropene ND mg/kg 01/28/21 15:19 563-58-601/28/21 12:060.085 0.041 10
cis-1,3-Dichloropropene ND mg/kg 01/28/21 15:19 10061-01-501/28/21 12:060.085 0.023 10
trans-1,3-Dichloropropene ND mg/kg 01/28/21 15:19 10061-02-601/28/21 12:060.085 0.029 10
Diisopropyl ether ND mg/kg 01/28/21 15:19 108-20-301/28/21 12:060.085 0.023 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-2 Lab ID:92518589002 Collected:01/25/21 09:30 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene 5.6 mg/kg 01/28/21 15:19 100-41-401/28/21 12:060.085 0.040 10
Hexachloro-1,3-butadiene ND mg/kg 01/28/21 15:19 87-68-301/28/21 12:060.17 0.14 10
2-Hexanone ND mg/kg 01/28/21 15:19 591-78-601/28/21 12:060.85 0.082 10
Isopropylbenzene (Cumene)1.3 mg/kg 01/28/21 15:19 98-82-801/28/21 12:060.085 0.029 10
p-Isopropyltoluene 2.9 mg/kg 01/28/21 15:19 99-87-601/28/21 12:060.085 0.042 10
Methylene Chloride ND mg/kg 01/28/21 15:19 75-09-201/28/21 12:060.34 0.23 10
4-Methyl-2-pentanone (MIBK)ND mg/kg 01/28/21 15:19 108-10-101/28/21 12:060.85 0.082 10
Methyl-tert-butyl ether ND mg/kg 01/28/21 15:19 1634-04-401/28/21 12:060.085 0.032 10
Naphthalene 21.7 mg/kg 01/28/21 15:19 91-20-301/28/21 12:060.085 0.045 10
n-Propylbenzene ND mg/kg 01/28/21 15:19 103-65-101/28/21 12:060.085 0.030 10
Styrene ND mg/kg 01/28/21 15:19 100-42-501/28/21 12:060.085 0.022 10
1,1,1,2-Tetrachloroethane ND mg/kg 01/28/21 15:19 630-20-601/28/21 12:060.085 0.033 10
1,1,2,2-Tetrachloroethane ND mg/kg 01/28/21 15:19 79-34-501/28/21 12:060.085 0.022 10
Tetrachloroethene 0.30 mg/kg 01/28/21 15:19 127-18-401/28/21 12:060.085 0.027 10
Toluene 0.75 mg/kg 01/28/21 15:19 108-88-301/28/21 12:060.085 0.024 10
1,2,3-Trichlorobenzene ND mg/kg 01/28/21 15:19 87-61-601/28/21 12:060.085 0.069 10
1,2,4-Trichlorobenzene ND mg/kg 01/28/21 15:19 120-82-101/28/21 12:060.085 0.071 10
1,1,1-Trichloroethane ND mg/kg 01/28/21 15:19 71-55-601/28/21 12:060.085 0.044 10
1,1,2-Trichloroethane ND mg/kg 01/28/21 15:19 79-00-501/28/21 12:060.085 0.028 10
Trichloroethene ND mg/kg 01/28/21 15:19 79-01-601/28/21 12:060.085 0.022 10
Trichlorofluoromethane ND mg/kg 01/28/21 15:19 75-69-401/28/21 12:060.085 0.047 10
1,2,3-Trichloropropane ND mg/kg 01/28/21 15:19 96-18-401/28/21 12:060.085 0.043 10
1,2,4-Trimethylbenzene 46.3 mg/kg 01/28/21 15:19 95-63-601/28/21 12:060.085 0.023 10
1,3,5-Trimethylbenzene 12.7 mg/kg 01/28/21 15:19 108-67-801/28/21 12:060.085 0.029 10
Vinyl acetate ND mg/kg 01/28/21 15:19 108-05-401/28/21 12:060.85 0.062 10
Vinyl chloride ND mg/kg 01/28/21 15:19 75-01-401/28/21 12:060.17 0.043 10
Xylene (Total)39.6 mg/kg 01/28/21 15:19 1330-20-701/28/21 12:060.17 0.048 10
m&p-Xylene 27.2 mg/kg 01/28/21 15:19 179601-23-101/28/21 12:060.17 0.058 10
o-Xylene 12.4 mg/kg 01/28/21 15:19 95-47-601/28/21 12:060.085 0.038 10
Surrogates
Toluene-d8 (S)101 %01/28/21 15:19 2037-26-501/28/21 12:0670-130 10
4-Bromofluorobenzene (S)101 %01/28/21 15:19 460-00-401/28/21 12:0669-134 10
1,2-Dichloroethane-d4 (S)109 %01/28/21 15:19 17060-07-001/28/21 12:0670-130 10
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.8 %01/26/21 17:03 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 74.2 %02/03/21 08:5202/03/21 08:411
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-2 Lab ID:92518589002 Collected:01/25/21 09:30 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.94 mg/kg 02/01/21 21:28 18540-29-902/01/21 16:101.35 0.344 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-3 Lab ID:92518589003 Collected:01/25/21 10:00 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic ND mg/kg 01/31/21 16:31 7440-38-2 M101/27/21 15:542.8 0.57 1
Barium 52.1 mg/kg 01/29/21 03:38 7440-39-301/27/21 15:541.1 0.28 1
Cadmium 0.064J mg/kg 01/29/21 03:38 7440-43-901/27/21 15:540.11 0.057 1
Chromium 37.2 mg/kg 01/29/21 03:38 7440-47-301/27/21 15:540.57 0.28 1
Lead 563 mg/kg 01/29/21 03:38 7439-92-1 M101/27/21 15:541.1 0.28 1
Selenium 4.4 mg/kg 01/29/21 03:38 7782-49-2 M101/27/21 15:541.1 0.57 1
Silver ND mg/kg 01/29/21 03:38 7440-22-401/27/21 15:540.57 0.28 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.018 mg/kg 01/27/21 17:03 7439-97-601/27/21 15:200.0030 0.0023 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 01/29/21 13:46 83-32-901/28/21 10:514.5 1.1 10
Acenaphthylene ND mg/kg 01/29/21 13:46 208-96-801/28/21 10:514.5 1.1 10
Aniline ND mg/kg 01/29/21 13:46 62-53-301/28/21 10:514.5 1.0 10
Anthracene ND mg/kg 01/29/21 13:46 120-12-701/28/21 10:514.5 1.2 10
Benzo(a)anthracene ND mg/kg 01/29/21 13:46 56-55-301/28/21 10:514.5 1.4 10
Benzo(a)pyrene ND mg/kg 01/29/21 13:46 50-32-801/28/21 10:514.5 1.9 10
Benzo(b)fluoranthene ND mg/kg 01/29/21 13:46 205-99-201/28/21 10:514.5 1.8 10
Benzo(g,h,i)perylene ND mg/kg 01/29/21 13:46 191-24-201/28/21 10:514.5 1.7 10
Benzo(k)fluoranthene ND mg/kg 01/29/21 13:46 207-08-901/28/21 10:514.5 1.9 10
Benzoic Acid ND mg/kg 01/29/21 13:46 65-85-001/28/21 10:5122.3 4.8 10
Benzyl alcohol ND mg/kg 01/29/21 13:46 100-51-601/28/21 10:518.9 2.4 10
4-Bromophenylphenyl ether ND mg/kg 01/29/21 13:46 101-55-301/28/21 10:514.5 1.2 10
Butylbenzylphthalate ND mg/kg 01/29/21 13:46 85-68-701/28/21 10:514.5 1.2 10
4-Chloro-3-methylphenol ND mg/kg 01/29/21 13:46 59-50-701/28/21 10:518.9 2.7 10
4-Chloroaniline ND mg/kg 01/29/21 13:46 106-47-801/28/21 10:518.9 2.7 10
bis(2-Chloroethoxy)methane ND mg/kg 01/29/21 13:46 111-91-101/28/21 10:514.5 1.2 10
bis(2-Chloroethyl) ether ND mg/kg 01/29/21 13:46 111-44-401/28/21 10:514.5 0.95 10
2-Chloronaphthalene ND mg/kg 01/29/21 13:46 91-58-701/28/21 10:514.5 0.99 10
2-Chlorophenol ND mg/kg 01/29/21 13:46 95-57-801/28/21 10:514.5 1.0 10
4-Chlorophenylphenyl ether ND mg/kg 01/29/21 13:46 7005-72-301/28/21 10:514.5 1.2 10
Chrysene ND mg/kg 01/29/21 13:46 218-01-901/28/21 10:514.5 1.3 10
Dibenz(a,h)anthracene ND mg/kg 01/29/21 13:46 53-70-301/28/21 10:514.5 1.8 10
Dibenzofuran ND mg/kg 01/29/21 13:46 132-64-901/28/21 10:514.5 1.1 10
1,2-Dichlorobenzene ND mg/kg 01/29/21 13:46 95-50-101/28/21 10:514.5 0.97 10
1,3-Dichlorobenzene ND mg/kg 01/29/21 13:46 541-73-101/28/21 10:514.5 1.0 10
1,4-Dichlorobenzene ND mg/kg 01/29/21 13:46 106-46-701/28/21 10:514.5 0.98 10
3,3'-Dichlorobenzidine ND mg/kg 01/29/21 13:46 91-94-1 IL01/28/21 10:518.9 3.1 10
2,4-Dichlorophenol ND mg/kg 01/29/21 13:46 120-83-201/28/21 10:514.5 1.5 10
Diethylphthalate ND mg/kg 01/29/21 13:46 84-66-201/28/21 10:514.5 0.97 10
2,4-Dimethylphenol ND mg/kg 01/29/21 13:46 105-67-901/28/21 10:514.5 1.1 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-3 Lab ID:92518589003 Collected:01/25/21 10:00 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 01/29/21 13:46 131-11-301/28/21 10:514.5 1.0 10
Di-n-butylphthalate ND mg/kg 01/29/21 13:46 84-74-201/28/21 10:514.5 1.1 10
4,6-Dinitro-2-methylphenol ND mg/kg 01/29/21 13:46 534-52-101/28/21 10:518.9 7.2 10
2,4-Dinitrophenol ND mg/kg 01/29/21 13:46 51-28-501/28/21 10:5122.3 14.3 10
2,4-Dinitrotoluene ND mg/kg 01/29/21 13:46 121-14-201/28/21 10:514.5 1.2 10
2,6-Dinitrotoluene ND mg/kg 01/29/21 13:46 606-20-201/28/21 10:514.5 1.2 10
Di-n-octylphthalate ND mg/kg 01/29/21 13:46 117-84-001/28/21 10:514.5 2.5 10
bis(2-Ethylhexyl)phthalate 1.7J mg/kg 01/29/21 13:46 117-81-701/28/21 10:514.5 1.5 10
Fluoranthene ND mg/kg 01/29/21 13:46 206-44-001/28/21 10:514.5 1.3 10
Fluorene 3.1J mg/kg 01/29/21 13:46 86-73-701/28/21 10:514.5 1.2 10
Hexachloro-1,3-butadiene ND mg/kg 01/29/21 13:46 87-68-301/28/21 10:514.5 1.1 10
Hexachlorobenzene ND mg/kg 01/29/21 13:46 118-74-101/28/21 10:514.5 1.1 10
Hexachlorocyclopentadiene ND mg/kg 01/29/21 13:46 77-47-4 v201/28/21 10:514.5 1.8 10
Hexachloroethane ND mg/kg 01/29/21 13:46 67-72-101/28/21 10:514.5 1.0 10
Indeno(1,2,3-cd)pyrene ND mg/kg 01/29/21 13:46 193-39-501/28/21 10:514.5 2.0 10
Isophorone ND mg/kg 01/29/21 13:46 78-59-101/28/21 10:514.5 0.97 10
1-Methylnaphthalene 28.1 mg/kg 01/29/21 13:46 90-12-001/28/21 10:514.5 1.2 10
2-Methylnaphthalene 46.5 mg/kg 02/01/21 11:19 91-57-601/28/21 10:518.9 2.3 20
2-Methylphenol(o-Cresol)ND mg/kg 01/29/21 13:46 95-48-701/28/21 10:514.5 0.99 10
3&4-Methylphenol(m&p Cresol)ND mg/kg 01/29/21 13:46 15831-10-401/28/21 10:514.5 1.1 10
Naphthalene 11.1 mg/kg 01/29/21 13:46 91-20-301/28/21 10:514.5 1.1 10
2-Nitroaniline ND mg/kg 01/29/21 13:46 88-74-401/28/21 10:5122.3 2.2 10
3-Nitroaniline ND mg/kg 01/29/21 13:46 99-09-201/28/21 10:5122.3 2.4 10
4-Nitroaniline ND mg/kg 01/29/21 13:46 100-01-601/28/21 10:518.9 2.2 10
Nitrobenzene ND mg/kg 01/29/21 13:46 98-95-301/28/21 10:514.5 1.1 10
2-Nitrophenol ND mg/kg 01/29/21 13:46 88-75-501/28/21 10:514.5 1.4 10
4-Nitrophenol ND mg/kg 01/29/21 13:46 100-02-701/28/21 10:5122.3 7.1 10
N-Nitrosodimethylamine ND mg/kg 01/29/21 13:46 62-75-901/28/21 10:514.5 1.3 10
N-Nitroso-di-n-propylamine ND mg/kg 01/29/21 13:46 621-64-701/28/21 10:514.5 1.2 10
N-Nitrosodiphenylamine ND mg/kg 01/29/21 13:46 86-30-601/28/21 10:514.5 1.1 10
2,2'-Oxybis(1-chloropropane)ND mg/kg 01/29/21 13:46 108-60-101/28/21 10:514.5 1.2 10
Pentachlorophenol ND mg/kg 01/29/21 13:46 87-86-501/28/21 10:518.9 2.0 10
Phenanthrene 5.8 mg/kg 01/29/21 13:46 85-01-801/28/21 10:514.5 1.1 10
Phenol ND mg/kg 01/29/21 13:46 108-95-201/28/21 10:514.5 1.1 10
Pyrene ND mg/kg 01/29/21 13:46 129-00-001/28/21 10:514.5 1.2 10
Pyridine ND mg/kg 01/29/21 13:46 110-86-101/28/21 10:514.5 1.1 10
1,2,4-Trichlorobenzene ND mg/kg 01/29/21 13:46 120-82-101/28/21 10:514.5 1.0 10
2,4,5-Trichlorophenol ND mg/kg 01/29/21 13:46 95-95-401/28/21 10:514.5 1.2 10
2,4,6-Trichlorophenol ND mg/kg 01/29/21 13:46 88-06-201/28/21 10:514.5 1.1 10
Surrogates
Nitrobenzene-d5 (S)0 %01/29/21 13:46 4165-60-0 D3,S401/28/21 10:5121-130 10
2-Fluorobiphenyl (S)0 %01/29/21 13:46 321-60-8 S401/28/21 10:5119-130 10
Terphenyl-d14 (S)0 %01/29/21 13:46 1718-51-0 S401/28/21 10:5115-130 10
Phenol-d6 (S)0 %01/29/21 13:46 13127-88-3 S401/28/21 10:5118-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-3 Lab ID:92518589003 Collected:01/25/21 10:00 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)0 %01/29/21 13:46 367-12-4 S401/28/21 10:5118-130 10
2,4,6-Tribromophenol (S)0 %01/29/21 13:46 118-79-6 S401/28/21 10:5118-130 10
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 01/28/21 15:39 67-64-101/28/21 12:061.7 0.54 10
Benzene 0.22 mg/kg 01/28/21 15:39 71-43-201/28/21 12:060.085 0.034 10
Bromobenzene ND mg/kg 01/28/21 15:39 108-86-101/28/21 12:060.085 0.028 10
Bromochloromethane ND mg/kg 01/28/21 15:39 74-97-501/28/21 12:060.085 0.025 10
Bromodichloromethane ND mg/kg 01/28/21 15:39 75-27-401/28/21 12:060.085 0.033 10
Bromoform ND mg/kg 01/28/21 15:39 75-25-201/28/21 12:060.085 0.030 10
Bromomethane ND mg/kg 01/28/21 15:39 74-83-9 IK01/28/21 12:060.17 0.13 10
2-Butanone (MEK)ND mg/kg 01/28/21 15:39 78-93-301/28/21 12:061.7 0.41 10
n-Butylbenzene ND mg/kg 01/28/21 15:39 104-51-801/28/21 12:060.085 0.040 10
sec-Butylbenzene ND mg/kg 01/28/21 15:39 135-98-801/28/21 12:060.085 0.037 10
tert-Butylbenzene ND mg/kg 01/28/21 15:39 98-06-601/28/21 12:060.085 0.030 10
Carbon tetrachloride ND mg/kg 01/28/21 15:39 56-23-501/28/21 12:060.085 0.032 10
Chlorobenzene ND mg/kg 01/28/21 15:39 108-90-701/28/21 12:060.085 0.016 10
Chloroethane ND mg/kg 01/28/21 15:39 75-00-301/28/21 12:060.17 0.065 10
Chloroform ND mg/kg 01/28/21 15:39 67-66-301/28/21 12:060.085 0.051 10
Chloromethane ND mg/kg 01/28/21 15:39 74-87-301/28/21 12:060.17 0.071 10
2-Chlorotoluene ND mg/kg 01/28/21 15:39 95-49-801/28/21 12:060.085 0.030 10
4-Chlorotoluene ND mg/kg 01/28/21 15:39 106-43-401/28/21 12:060.085 0.015 10
1,2-Dibromo-3-chloropropane ND mg/kg 01/28/21 15:39 96-12-801/28/21 12:060.085 0.033 10
Dibromochloromethane ND mg/kg 01/28/21 15:39 124-48-101/28/21 12:060.085 0.048 10
1,2-Dibromoethane (EDB)ND mg/kg 01/28/21 15:39 106-93-401/28/21 12:060.085 0.037 10
Dibromomethane ND mg/kg 01/28/21 15:39 74-95-301/28/21 12:060.085 0.018 10
1,2-Dichlorobenzene ND mg/kg 01/28/21 15:39 95-50-101/28/21 12:060.085 0.030 10
1,3-Dichlorobenzene ND mg/kg 01/28/21 15:39 541-73-101/28/21 12:060.085 0.026 10
1,4-Dichlorobenzene ND mg/kg 01/28/21 15:39 106-46-701/28/21 12:060.085 0.022 10
Dichlorodifluoromethane ND mg/kg 01/28/21 15:39 75-71-801/28/21 12:060.17 0.037 10
1,1-Dichloroethane ND mg/kg 01/28/21 15:39 75-34-301/28/21 12:060.085 0.035 10
1,2-Dichloroethane ND mg/kg 01/28/21 15:39 107-06-201/28/21 12:060.085 0.056 10
1,1-Dichloroethene ND mg/kg 01/28/21 15:39 75-35-401/28/21 12:060.085 0.035 10
cis-1,2-Dichloroethene ND mg/kg 01/28/21 15:39 156-59-201/28/21 12:060.085 0.029 10
trans-1,2-Dichloroethene ND mg/kg 01/28/21 15:39 156-60-501/28/21 12:060.085 0.030 10
1,2-Dichloropropane ND mg/kg 01/28/21 15:39 78-87-501/28/21 12:060.085 0.025 10
1,3-Dichloropropane ND mg/kg 01/28/21 15:39 142-28-901/28/21 12:060.085 0.026 10
2,2-Dichloropropane ND mg/kg 01/28/21 15:39 594-20-701/28/21 12:060.085 0.028 10
1,1-Dichloropropene ND mg/kg 01/28/21 15:39 563-58-601/28/21 12:060.085 0.041 10
cis-1,3-Dichloropropene ND mg/kg 01/28/21 15:39 10061-01-501/28/21 12:060.085 0.023 10
trans-1,3-Dichloropropene ND mg/kg 01/28/21 15:39 10061-02-601/28/21 12:060.085 0.029 10
Diisopropyl ether ND mg/kg 01/28/21 15:39 108-20-301/28/21 12:060.085 0.023 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-3 Lab ID:92518589003 Collected:01/25/21 10:00 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene 7.0 mg/kg 01/28/21 15:39 100-41-401/28/21 12:060.085 0.039 10
Hexachloro-1,3-butadiene ND mg/kg 01/28/21 15:39 87-68-301/28/21 12:060.17 0.14 10
2-Hexanone ND mg/kg 01/28/21 15:39 591-78-601/28/21 12:060.85 0.082 10
Isopropylbenzene (Cumene)1.9 mg/kg 01/28/21 15:39 98-82-801/28/21 12:060.085 0.029 10
p-Isopropyltoluene 3.8 mg/kg 01/28/21 15:39 99-87-601/28/21 12:060.085 0.042 10
Methylene Chloride ND mg/kg 01/28/21 15:39 75-09-201/28/21 12:060.34 0.23 10
4-Methyl-2-pentanone (MIBK)0.52J mg/kg 01/28/21 15:39 108-10-101/28/21 12:060.85 0.082 10
Methyl-tert-butyl ether ND mg/kg 01/28/21 15:39 1634-04-401/28/21 12:060.085 0.032 10
Naphthalene 28.6 mg/kg 01/28/21 15:39 91-20-301/28/21 12:060.085 0.044 10
n-Propylbenzene ND mg/kg 01/28/21 15:39 103-65-101/28/21 12:060.085 0.030 10
Styrene ND mg/kg 01/28/21 15:39 100-42-501/28/21 12:060.085 0.022 10
1,1,1,2-Tetrachloroethane ND mg/kg 01/28/21 15:39 630-20-601/28/21 12:060.085 0.032 10
1,1,2,2-Tetrachloroethane ND mg/kg 01/28/21 15:39 79-34-501/28/21 12:060.085 0.022 10
Tetrachloroethene ND mg/kg 01/28/21 15:39 127-18-401/28/21 12:060.085 0.027 10
Toluene 0.26 mg/kg 01/28/21 15:39 108-88-301/28/21 12:060.085 0.024 10
1,2,3-Trichlorobenzene ND mg/kg 01/28/21 15:39 87-61-601/28/21 12:060.085 0.068 10
1,2,4-Trichlorobenzene ND mg/kg 01/28/21 15:39 120-82-101/28/21 12:060.085 0.071 10
1,1,1-Trichloroethane ND mg/kg 01/28/21 15:39 71-55-601/28/21 12:060.085 0.044 10
1,1,2-Trichloroethane ND mg/kg 01/28/21 15:39 79-00-501/28/21 12:060.085 0.028 10
Trichloroethene ND mg/kg 01/28/21 15:39 79-01-601/28/21 12:060.085 0.022 10
Trichlorofluoromethane ND mg/kg 01/28/21 15:39 75-69-401/28/21 12:060.085 0.047 10
1,2,3-Trichloropropane ND mg/kg 01/28/21 15:39 96-18-401/28/21 12:060.085 0.043 10
1,2,4-Trimethylbenzene 50.7 mg/kg 01/28/21 15:39 95-63-601/28/21 12:060.085 0.023 10
1,3,5-Trimethylbenzene 14.6 mg/kg 01/28/21 15:39 108-67-801/28/21 12:060.085 0.028 10
Vinyl acetate ND mg/kg 01/28/21 15:39 108-05-401/28/21 12:060.85 0.062 10
Vinyl chloride ND mg/kg 01/28/21 15:39 75-01-401/28/21 12:060.17 0.043 10
Xylene (Total)25.6 mg/kg 01/28/21 15:39 1330-20-701/28/21 12:060.17 0.048 10
m&p-Xylene 19.4 mg/kg 01/28/21 15:39 179601-23-101/28/21 12:060.17 0.058 10
o-Xylene 6.2 mg/kg 01/28/21 15:39 95-47-601/28/21 12:060.085 0.037 10
Surrogates
Toluene-d8 (S)99 %01/28/21 15:39 2037-26-501/28/21 12:0670-130 10
4-Bromofluorobenzene (S)103 %01/28/21 15:39 460-00-401/28/21 12:0669-134 10
1,2-Dichloroethane-d4 (S)110 %01/28/21 15:39 17060-07-001/28/21 12:0670-130 10
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.6 %01/26/21 17:03 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.3 %02/03/21 08:5202/03/21 08:411
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Sample:T-3 Lab ID:92518589003 Collected:01/25/21 10:00 Received:01/26/21 11:45 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.80 mg/kg 02/01/21 21:43 18540-29-902/01/21 16:101.40 0.358 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
595763
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92518589001, 92518589002, 92518589003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3142203
Associated Lab Samples:92518589001, 92518589002, 92518589003
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 01/27/21 16:270.0046
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3142204LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0730.083 88 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3142205MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92518618001
3142206
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg M10.045 148 75-125157 3 200.0440.031 0.097 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
595682
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92518589001, 92518589002, 92518589003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3141744
Associated Lab Samples:92518589001, 92518589002, 92518589003
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 2.5 01/31/21 16:250.50
Barium mg/kg ND 1.0 01/29/21 03:320.25
Cadmium mg/kg ND 0.10 01/29/21 03:320.050
Chromium mg/kg ND 0.50 01/29/21 03:320.25
Lead mg/kg ND 1.0 01/29/21 03:320.25
Selenium mg/kg ND 1.0 01/29/21 03:320.50
Silver mg/kg ND 0.50 01/29/21 03:320.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3141745LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 46.850 94 80-120
Barium mg/kg 51.650 103 80-120
Cadmium mg/kg 47.050 94 80-120
Chromium mg/kg 45.450 91 80-120
Lead mg/kg 49.350 99 80-120
Selenium mg/kg 45.650 91 80-120
Silver mg/kg 22.625 90 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3141746MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92518589003
3141747
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg M158.7 75 75-12571 9 2056.8ND 44.2 40.5
Barium mg/kg 58.7 91 75-125101 4 2056.852.1 106 110
Cadmium mg/kg 58.7 89 75-12587 6 2056.80.064J 52.1 49.3
Chromium mg/kg 58.7 94 75-12599 1 2056.837.2 92.1 93.1
Lead mg/kg M158.7 61 75-12567 0 2056.8563 599 601
Selenium mg/kg M158.7 78 75-12574 8 2056.84.4 50.0 46.2
Silver mg/kg 29.4 86 75-12586 4 2028.3ND 25.4 24.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
595702
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92518589001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3141853
Associated Lab Samples:92518589001
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 01/27/21 13:460.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 01/27/21 13:460.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 01/27/21 13:460.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 01/27/21 13:460.0017
1,1-Dichloroethane mg/kg ND 0.0050 01/27/21 13:460.0021
1,1-Dichloroethene mg/kg ND 0.0050 01/27/21 13:460.0021
1,1-Dichloropropene mg/kg ND 0.0050 01/27/21 13:460.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 01/27/21 13:460.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 01/27/21 13:460.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 01/27/21 13:460.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 01/27/21 13:460.0014
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 01/27/21 13:460.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 01/27/21 13:460.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 01/27/21 13:460.0018
1,2-Dichloroethane mg/kg ND 0.0050 01/27/21 13:460.0033
1,2-Dichloropropane mg/kg ND 0.0050 01/27/21 13:460.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 01/27/21 13:460.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 01/27/21 13:460.0016
1,3-Dichloropropane mg/kg ND 0.0050 01/27/21 13:460.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 01/27/21 13:460.0013
2,2-Dichloropropane mg/kg ND 0.0050 01/27/21 13:460.0016
2-Butanone (MEK)mg/kg ND 0.10 01/27/21 13:460.024
2-Chlorotoluene mg/kg ND 0.0050 01/27/21 13:460.0018
2-Hexanone mg/kg ND 0.050 01/27/21 13:460.0048
4-Chlorotoluene mg/kg ND 0.0050 01/27/21 13:460.00088
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 01/27/21 13:460.0048
Acetone mg/kg ND 0.10 01/27/21 13:460.032
Benzene mg/kg ND 0.0050 01/27/21 13:460.0020
Bromobenzene mg/kg ND 0.0050 01/27/21 13:460.0016
Bromochloromethane mg/kg ND 0.0050 01/27/21 13:460.0015
Bromodichloromethane mg/kg ND 0.0050 01/27/21 13:460.0019
Bromoform mg/kg ND 0.0050 01/27/21 13:460.0018
Bromomethane mg/kg ND 0.010 IK01/27/21 13:460.0079
Carbon tetrachloride mg/kg ND 0.0050 01/27/21 13:460.0019
Chlorobenzene mg/kg ND 0.0050 01/27/21 13:460.00096
Chloroethane mg/kg ND 0.010 01/27/21 13:460.0039
Chloroform mg/kg ND 0.0050 01/27/21 13:460.0030
Chloromethane mg/kg ND 0.010 01/27/21 13:460.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 01/27/21 13:460.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 01/27/21 13:460.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3141853
Associated Lab Samples:92518589001
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 01/27/21 13:460.0028
Dibromomethane mg/kg ND 0.0050 01/27/21 13:460.0011
Dichlorodifluoromethane mg/kg ND 0.010 01/27/21 13:460.0022
Diisopropyl ether mg/kg ND 0.0050 01/27/21 13:460.0014
Ethylbenzene mg/kg ND 0.0050 01/27/21 13:460.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 01/27/21 13:460.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 01/27/21 13:460.0017
m&p-Xylene mg/kg ND 0.010 01/27/21 13:460.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 01/27/21 13:460.0019
Methylene Chloride mg/kg ND 0.020 01/27/21 13:460.014
n-Butylbenzene mg/kg ND 0.0050 01/27/21 13:460.0024
n-Propylbenzene mg/kg ND 0.0050 01/27/21 13:460.0018
Naphthalene mg/kg ND 0.0050 01/27/21 13:460.0026
o-Xylene mg/kg ND 0.0050 01/27/21 13:460.0022
p-Isopropyltoluene mg/kg ND 0.0050 01/27/21 13:460.0025
sec-Butylbenzene mg/kg ND 0.0050 01/27/21 13:460.0022
Styrene mg/kg ND 0.0050 01/27/21 13:460.0013
tert-Butylbenzene mg/kg ND 0.0050 01/27/21 13:460.0018
Tetrachloroethene mg/kg ND 0.0050 01/27/21 13:460.0016
Toluene mg/kg ND 0.0050 01/27/21 13:460.0014
trans-1,2-Dichloroethene mg/kg ND 0.0050 01/27/21 13:460.0018
trans-1,3-Dichloropropene mg/kg ND 0.0050 01/27/21 13:460.0017
Trichloroethene mg/kg ND 0.0050 01/27/21 13:460.0013
Trichlorofluoromethane mg/kg ND 0.0050 01/27/21 13:460.0028
Vinyl acetate mg/kg ND 0.050 01/27/21 13:460.0036
Vinyl chloride mg/kg ND 0.010 01/27/21 13:460.0025
Xylene (Total)mg/kg ND 0.010 01/27/21 13:460.0028
1,2-Dichloroethane-d4 (S)%105 70-130 01/27/21 13:46
4-Bromofluorobenzene (S)%96 69-134 01/27/21 13:46
Toluene-d8 (S)%99 70-130 01/27/21 13:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3141854LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.981.2 79 70-130
1,1,1-Trichloroethane mg/kg 1.21.2 95 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.921.2 74 70-130
1,1,2-Trichloroethane mg/kg 1.21.2 92 70-130
1,1-Dichloroethane mg/kg 1.11.2 91 70-130
1,1-Dichloroethene mg/kg 1.21.2 97 70-130
1,1-Dichloropropene mg/kg 1.21.2 94 70-130
1,2,3-Trichlorobenzene mg/kg 1.11.2 84 65-130
1,2,3-Trichloropropane mg/kg 0.971.2 78 70-130
1,2,4-Trichlorobenzene mg/kg 1.01.2 84 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3141854LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.11.2 88 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.11.2 89 70-130
1,2-Dibromoethane (EDB)mg/kg 0.971.2 78 70-130
1,2-Dichlorobenzene mg/kg 1.11.2 85 70-130
1,2-Dichloroethane mg/kg 1.11.2 92 63-130
1,2-Dichloropropane mg/kg 1.21.2 94 70-130
1,3,5-Trimethylbenzene mg/kg 1.11.2 88 70-130
1,3-Dichlorobenzene mg/kg 1.01.2 83 70-130
1,3-Dichloropropane mg/kg 0.971.2 78 70-130
1,4-Dichlorobenzene mg/kg 1.01.2 81 70-130
2,2-Dichloropropane mg/kg 1.21.2 96 66-130
2-Butanone (MEK)mg/kg 2.22.5 87 70-130
2-Chlorotoluene mg/kg 1.11.2 87 70-130
2-Hexanone mg/kg 1.92.5 77 70-130
4-Chlorotoluene mg/kg 1.11.2 84 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.32.5 92 70-130
Acetone mg/kg 2.22.5 87 69-130
Benzene mg/kg 1.11.2 91 70-130
Bromobenzene mg/kg 1.01.2 83 70-130
Bromochloromethane mg/kg 1.21.2 96 70-130
Bromodichloromethane mg/kg 1.11.2 91 69-130
Bromoform mg/kg 0.981.2 79 70-130
Bromomethane mg/kg 1.4 IK1.2 109 52-130
Carbon tetrachloride mg/kg 1.31.2 101 70-130
Chlorobenzene mg/kg 0.941.2 75 70-130
Chloroethane mg/kg 1.11.2 92 65-130
Chloroform mg/kg 1.11.2 87 70-130
Chloromethane mg/kg 0.961.2 77 55-130
cis-1,2-Dichloroethene mg/kg 1.11.2 86 70-130
cis-1,3-Dichloropropene mg/kg 1.21.2 95 70-130
Dibromochloromethane mg/kg 0.991.2 79 70-130
Dibromomethane mg/kg 1.11.2 88 70-130
Dichlorodifluoromethane mg/kg 1.21.2 95 45-156
Diisopropyl ether mg/kg 1.11.2 88 70-130
Ethylbenzene mg/kg 0.921.2 74 70-130
Hexachloro-1,3-butadiene mg/kg 1.01.2 80 66-130
Isopropylbenzene (Cumene)mg/kg 1.01.2 80 70-130
m&p-Xylene mg/kg 1.92.5 77 70-130
Methyl-tert-butyl ether mg/kg 1.11.2 88 70-130
Methylene Chloride mg/kg 1.11.2 90 65-130
n-Butylbenzene mg/kg 1.11.2 87 67-130
n-Propylbenzene mg/kg 1.11.2 86 70-130
Naphthalene mg/kg 1.01.2 82 70-130
o-Xylene mg/kg 0.971.2 78 70-130
p-Isopropyltoluene mg/kg 1.11.2 89 67-130
sec-Butylbenzene mg/kg 1.11.2 90 69-130
Styrene mg/kg 1.01.2 81 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3141854LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 0.891.2 72 67-130
Tetrachloroethene mg/kg 0.951.2 76 70-130
Toluene mg/kg 1.11.2 91 70-130
trans-1,2-Dichloroethene mg/kg 1.01.2 84 70-130
trans-1,3-Dichloropropene mg/kg 1.21.2 93 68-130
Trichloroethene mg/kg 1.21.2 93 70-130
Trichlorofluoromethane mg/kg 1.21.2 96 70-130
Vinyl acetate mg/kg 2.62.5 104 70-130
Vinyl chloride mg/kg 1.11.2 87 61-130
Xylene (Total)mg/kg 2.93.8 77 70-130
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%95 69-134
Toluene-d8 (S)%126 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3141855MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
30402521015
3141856
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane mg/kg 1.1 92 70-13198 6 301.1ND 0.99 1.0
1,1,1-Trichloroethane mg/kg 1.1 98 65-133101 3 301.1ND 1.1 1.1
1,1,2,2-Tetrachloroethane mg/kg 1.1 88 66-13093 6 301.1ND 0.94 1.0
1,1,2-Trichloroethane mg/kg 1.1 91 66-13394 3 301.1ND 0.98 1.0
1,1-Dichloroethane mg/kg 1.1 93 65-13095 3 301.1ND 0.99 1.0
1,1-Dichloroethene mg/kg 1.1 93 10-15898 5 301.1ND 1.0 1.0
1,1-Dichloropropene mg/kg 1.1 101 68-133100 0 301.1ND 1.1 1.1
1,2,3-Trichlorobenzene mg/kg 1.1 97 27-138103 6 301.1ND 1.0 1.1
1,2,3-Trichloropropane mg/kg 1.1 90 67-13096 6 301.1ND 0.97 1.0
1,2,4-Trichlorobenzene mg/kg 1.1 100 51-134104 4 301.1ND 1.1 1.1
1,2,4-Trimethylbenzene mg/kg 1.1 107 63-136105 2 301.1ND 1.1 1.1
1,2-Dibromo-3-
chloropropane mg/kg 1.1 96 32-130100 4 301.1ND 1.0 1.1
1,2-Dibromoethane (EDB)mg/kg 1.1 92 70-13096 4 301.1ND 0.99 1.0
1,2-Dichlorobenzene mg/kg 1.1 101 69-130100 1 301.1ND 1.1 1.1
1,2-Dichloroethane mg/kg 1.1 89 59-13094 5 301.1ND 0.96 1.0
1,2-Dichloropropane mg/kg 1.1 92 70-13096 4 301.1ND 0.99 1.0
1,3,5-Trimethylbenzene mg/kg 1.1 105 65-137106 0 301.1ND 1.1 1.1
1,3-Dichlorobenzene mg/kg 1.1 97 70-13098 1 301.1ND 1.0 1.0
1,3-Dichloropropane mg/kg 1.1 92 70-13097 5 301.1ND 0.99 1.0
1,4-Dichlorobenzene mg/kg 1.1 96 68-13096 1 301.1ND 1.0 1.0
2,2-Dichloropropane mg/kg 1.1 88 32-13089 1 301.1ND 0.94 0.95
2-Butanone (MEK)mg/kg 2.1 79 10-13686 8 302.1ND 1.7 1.8
2-Chlorotoluene mg/kg 1.1 102 69-141104 2 301.1ND 1.1 1.1
2-Hexanone mg/kg 2.1 83 10-14491 9 302.1ND 1.8 2.0
4-Chlorotoluene mg/kg 1.1 99 70-132100 1 301.1ND 1.1 1.1
4-Methyl-2-pentanone
(MIBK)mg/kg 2.1 83 25-14388 6 302.1ND 1.8 1.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3141855MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
30402521015
3141856
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acetone mg/kg 2.1 72 10-13077 6 302.1ND 1.5 1.6
Benzene mg/kg 1.1 91 67-13095 4 301.1ND 0.98 1.0
Bromobenzene mg/kg 1.1 109 70-130122 11 301.1ND 1.2 1.3
Bromochloromethane mg/kg 1.1 96 69-13497 1 301.1ND 1.0 1.0
Bromodichloromethane mg/kg 1.1 85 64-13089 4 301.1ND 0.91 0.95
Bromoform mg/kg 1.1 84 62-13090 7 301.1ND 0.90 0.97
Bromomethane mg/kg IK1.1 78 20-17670 11 301.1ND 0.84 0.75
Carbon tetrachloride mg/kg 1.1 100 65-140105 4 301.1ND 1.1 1.1
Chlorobenzene mg/kg 1.1 92 70-13097 6 301.1ND 0.99 1.0
Chloroethane mg/kg 1.1 32 10-13033 2 301.1ND 0.35 0.35
Chloroform mg/kg 1.1 89 63-13093 5 301.1ND 0.95 1.0
Chloromethane mg/kg 1.1 83 58-13089 8 301.1ND 0.89 0.96
cis-1,2-Dichloroethene mg/kg 1.1 86 66-13091 5 301.1ND 0.92 0.97
cis-1,3-Dichloropropene mg/kg 1.1 91 67-13094 4 301.1ND 0.97 1.0
Dibromochloromethane mg/kg 1.1 91 67-13095 5 301.1ND 0.98 1.0
Dibromomethane mg/kg 1.1 84 63-13188 4 301.1ND 0.90 0.94
Dichlorodifluoromethane mg/kg 1.1 98 44-180105 7 301.1ND 1.1 1.1
Diisopropyl ether mg/kg 1.1 84 63-13089 6 301.1ND 0.90 0.96
Ethylbenzene mg/kg 1.1 91 66-13096 6 301.1ND 0.97 1.0
Hexachloro-1,3-butadiene mg/kg 1.1 102 64-150105 3 301.1ND 1.1 1.1
Isopropylbenzene
(Cumene)mg/kg 1.1 99 69-135106 7 301.1ND 1.1 1.1
m&p-Xylene mg/kg 2.1 95 60-133102 8 302.1ND 2.0 2.2
Methyl-tert-butyl ether mg/kg 1.1 86 65-13090 4 301.1ND 0.92 0.96
Methylene Chloride mg/kg 1.1 91 61-13094 3 301.1ND 0.98 1.0
n-Butylbenzene mg/kg 1.1 105 65-140106 1 301.1ND 1.1 1.1
n-Propylbenzene mg/kg 1.1 102 67-140105 3 301.1ND 1.1 1.1
Naphthalene mg/kg 1.1 112 15-145101 11 301.1ND 1.2 1.1
o-Xylene mg/kg 1.1 96 66-13399 3 301.1ND 1.0 1.1
p-Isopropyltoluene mg/kg 1.1 108 56-147110 1 301.1ND 1.2 1.2
sec-Butylbenzene mg/kg 1.1 109 65-139110 2 301.1ND 1.2 1.2
Styrene mg/kg 1.1 96 70-13299 3 301.1ND 1.0 1.1
tert-Butylbenzene mg/kg 1.1 74 62-13577 4 301.1ND 0.79 0.83
Tetrachloroethene mg/kg 1.1 94 70-135100 6 301.1ND 1.0 1.1
Toluene mg/kg 1.1 92 67-13095 3 301.1ND 0.99 1.0
trans-1,2-Dichloroethene mg/kg 1.1 87 69-13090 4 301.1ND 0.93 0.97
trans-1,3-Dichloropropene mg/kg 1.1 88 62-13090 2 301.1ND 0.95 0.96
Trichloroethene mg/kg 1.1 94 70-13599 6 301.1ND 1.0 1.1
Trichlorofluoromethane mg/kg 1.1 44 10-13046 4 301.1ND 0.47 0.49
Vinyl acetate mg/kg 2.1 92 53-13098 5 302.1ND 2.0 2.1
Vinyl chloride mg/kg 1.1 89 61-14896 8 301.1ND 0.95 1.0
Xylene (Total)mg/kg 3.2 95 63-132102 6 303.2ND 3.1 3.3
1,2-Dichloroethane-d4 (S)%105 70-130106
4-Bromofluorobenzene (S)%99 69-13499
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
596037
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92518589002, 92518589003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3143611
Associated Lab Samples:92518589002, 92518589003
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 01/28/21 11:290.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 01/28/21 11:290.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 01/28/21 11:290.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 01/28/21 11:290.0017
1,1-Dichloroethane mg/kg ND 0.0050 01/28/21 11:290.0021
1,1-Dichloroethene mg/kg ND 0.0050 01/28/21 11:290.0021
1,1-Dichloropropene mg/kg ND 0.0050 01/28/21 11:290.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 01/28/21 11:290.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 01/28/21 11:290.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 01/28/21 11:290.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 01/28/21 11:290.0014
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 01/28/21 11:290.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 01/28/21 11:290.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 01/28/21 11:290.0018
1,2-Dichloroethane mg/kg ND 0.0050 01/28/21 11:290.0033
1,2-Dichloropropane mg/kg ND 0.0050 01/28/21 11:290.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 01/28/21 11:290.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 01/28/21 11:290.0016
1,3-Dichloropropane mg/kg ND 0.0050 01/28/21 11:290.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 01/28/21 11:290.0013
2,2-Dichloropropane mg/kg ND 0.0050 01/28/21 11:290.0016
2-Butanone (MEK)mg/kg ND 0.10 01/28/21 11:290.024
2-Chlorotoluene mg/kg ND 0.0050 01/28/21 11:290.0018
2-Hexanone mg/kg ND 0.050 01/28/21 11:290.0048
4-Chlorotoluene mg/kg ND 0.0050 01/28/21 11:290.00088
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 01/28/21 11:290.0048
Acetone mg/kg ND 0.10 01/28/21 11:290.032
Benzene mg/kg ND 0.0050 01/28/21 11:290.0020
Bromobenzene mg/kg ND 0.0050 01/28/21 11:290.0016
Bromochloromethane mg/kg ND 0.0050 01/28/21 11:290.0015
Bromodichloromethane mg/kg ND 0.0050 01/28/21 11:290.0019
Bromoform mg/kg ND 0.0050 01/28/21 11:290.0018
Bromomethane mg/kg ND 0.010 IK01/28/21 11:290.0079
Carbon tetrachloride mg/kg ND 0.0050 01/28/21 11:290.0019
Chlorobenzene mg/kg ND 0.0050 01/28/21 11:290.00096
Chloroethane mg/kg ND 0.010 01/28/21 11:290.0039
Chloroform mg/kg ND 0.0050 01/28/21 11:290.0030
Chloromethane mg/kg ND 0.010 01/28/21 11:290.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 01/28/21 11:290.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 01/28/21 11:290.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3143611
Associated Lab Samples:92518589002, 92518589003
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 01/28/21 11:290.0028
Dibromomethane mg/kg ND 0.0050 01/28/21 11:290.0011
Dichlorodifluoromethane mg/kg ND 0.010 01/28/21 11:290.0022
Diisopropyl ether mg/kg ND 0.0050 01/28/21 11:290.0014
Ethylbenzene mg/kg ND 0.0050 01/28/21 11:290.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 01/28/21 11:290.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 01/28/21 11:290.0017
m&p-Xylene mg/kg ND 0.010 01/28/21 11:290.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 01/28/21 11:290.0019
Methylene Chloride mg/kg ND 0.020 01/28/21 11:290.014
n-Butylbenzene mg/kg ND 0.0050 01/28/21 11:290.0024
n-Propylbenzene mg/kg ND 0.0050 01/28/21 11:290.0018
Naphthalene mg/kg ND 0.0050 01/28/21 11:290.0026
o-Xylene mg/kg ND 0.0050 01/28/21 11:290.0022
p-Isopropyltoluene mg/kg ND 0.0050 01/28/21 11:290.0025
sec-Butylbenzene mg/kg ND 0.0050 01/28/21 11:290.0022
Styrene mg/kg ND 0.0050 01/28/21 11:290.0013
tert-Butylbenzene mg/kg ND 0.0050 01/28/21 11:290.0018
Tetrachloroethene mg/kg ND 0.0050 01/28/21 11:290.0016
Toluene mg/kg ND 0.0050 01/28/21 11:290.0014
trans-1,2-Dichloroethene mg/kg ND 0.0050 01/28/21 11:290.0018
trans-1,3-Dichloropropene mg/kg ND 0.0050 01/28/21 11:290.0017
Trichloroethene mg/kg ND 0.0050 01/28/21 11:290.0013
Trichlorofluoromethane mg/kg ND 0.0050 01/28/21 11:290.0028
Vinyl acetate mg/kg ND 0.050 01/28/21 11:290.0036
Vinyl chloride mg/kg ND 0.010 01/28/21 11:290.0025
Xylene (Total)mg/kg ND 0.010 01/28/21 11:290.0028
1,2-Dichloroethane-d4 (S)%113 70-130 01/28/21 11:29
4-Bromofluorobenzene (S)%95 69-134 01/28/21 11:29
Toluene-d8 (S)%99 70-130 01/28/21 11:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3143612LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.31.2 104 70-130
1,1,1-Trichloroethane mg/kg 1.21.2 97 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.21.2 100 70-130
1,1,2-Trichloroethane mg/kg 1.21.2 97 70-130
1,1-Dichloroethane mg/kg 1.21.2 94 70-130
1,1-Dichloroethene mg/kg 1.21.2 99 70-130
1,1-Dichloropropene mg/kg 1.21.2 95 70-130
1,2,3-Trichlorobenzene mg/kg 1.31.2 107 65-130
1,2,3-Trichloropropane mg/kg 1.31.2 105 70-130
1,2,4-Trichlorobenzene mg/kg 1.31.2 108 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3143612LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.41.2 109 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.51.2 120 70-130
1,2-Dibromoethane (EDB)mg/kg 1.31.2 104 70-130
1,2-Dichlorobenzene mg/kg 1.31.2 107 70-130
1,2-Dichloroethane mg/kg 1.21.2 96 63-130
1,2-Dichloropropane mg/kg 1.21.2 98 70-130
1,3,5-Trimethylbenzene mg/kg 1.41.2 108 70-130
1,3-Dichlorobenzene mg/kg 1.31.2 106 70-130
1,3-Dichloropropane mg/kg 1.31.2 102 70-130
1,4-Dichlorobenzene mg/kg 1.31.2 101 70-130
2,2-Dichloropropane mg/kg 1.21.2 98 66-130
2-Butanone (MEK)mg/kg 2.52.5 101 70-130
2-Chlorotoluene mg/kg 1.31.2 103 70-130
2-Hexanone mg/kg 2.72.5 109 70-130
4-Chlorotoluene mg/kg 1.31.2 103 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.52.5 100 70-130
Acetone mg/kg 2.52.5 102 69-130
Benzene mg/kg 1.21.2 94 70-130
Bromobenzene mg/kg 1.31.2 106 70-130
Bromochloromethane mg/kg 1.31.2 102 70-130
Bromodichloromethane mg/kg 1.21.2 96 69-130
Bromoform mg/kg 1.31.2 107 70-130
Bromomethane mg/kg 1.4 IK1.2 115 52-130
Carbon tetrachloride mg/kg 1.31.2 101 70-130
Chlorobenzene mg/kg 1.21.2 97 70-130
Chloroethane mg/kg 1.21.2 95 65-130
Chloroform mg/kg 1.21.2 94 70-130
Chloromethane mg/kg 1.01.2 80 55-130
cis-1,2-Dichloroethene mg/kg 1.11.2 90 70-130
cis-1,3-Dichloropropene mg/kg 1.31.2 100 70-130
Dibromochloromethane mg/kg 1.31.2 105 70-130
Dibromomethane mg/kg 1.21.2 93 70-130
Dichlorodifluoromethane mg/kg 1.11.2 90 45-156
Diisopropyl ether mg/kg 1.21.2 92 70-130
Ethylbenzene mg/kg 1.21.2 95 70-130
Hexachloro-1,3-butadiene mg/kg 1.21.2 98 66-130
Isopropylbenzene (Cumene)mg/kg 1.31.2 103 70-130
m&p-Xylene mg/kg 2.52.5 99 70-130
Methyl-tert-butyl ether mg/kg 1.21.2 93 70-130
Methylene Chloride mg/kg 1.21.2 94 65-130
n-Butylbenzene mg/kg 1.31.2 107 67-130
n-Propylbenzene mg/kg 1.41.2 110 70-130
Naphthalene mg/kg 1.31.2 106 70-130
o-Xylene mg/kg 1.31.2 102 70-130
p-Isopropyltoluene mg/kg 1.31.2 107 67-130
sec-Butylbenzene mg/kg 1.41.2 108 69-130
Styrene mg/kg 1.31.2 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3143612LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.11.2 88 67-130
Tetrachloroethene mg/kg 1.21.2 98 70-130
Toluene mg/kg 1.21.2 93 70-130
trans-1,2-Dichloroethene mg/kg 1.11.2 88 70-130
trans-1,3-Dichloropropene mg/kg 1.21.2 98 68-130
Trichloroethene mg/kg 1.21.2 96 70-130
Trichlorofluoromethane mg/kg 1.21.2 93 70-130
Vinyl acetate mg/kg 2.72.5 110 70-130
Vinyl chloride mg/kg 1.11.2 87 61-130
Xylene (Total)mg/kg 3.83.8 100 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%102 69-134
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3143613MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92518292001
3143614
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane mg/kg 11.7 108 70-131111 2 3011.7ND 12.7 13.0
1,1,1-Trichloroethane mg/kg 11.7 112 65-133111 1 3011.7ND 13.2 13.0
1,1,2,2-Tetrachloroethane mg/kg 11.7 101 66-130107 6 3011.7ND 11.9 12.6
1,1,2-Trichloroethane mg/kg 11.7 103 66-133105 2 3011.7ND 12.0 12.3
1,1-Dichloroethane mg/kg 11.7 107 65-130107 1 3011.7ND 12.5 12.6
1,1-Dichloroethene mg/kg 11.7 118 10-158117 1 3011.7ND 13.9 13.8
1,1-Dichloropropene mg/kg 11.7 113 68-133111 2 3011.7ND 13.3 13.0
1,2,3-Trichlorobenzene mg/kg 11.7 116 27-138110 6 3011.7ND 13.6 12.9
1,2,3-Trichloropropane mg/kg 11.7 104 67-130106 2 3011.7ND 12.2 12.4
1,2,4-Trichlorobenzene mg/kg 11.7 119 51-134113 5 3011.7ND 14.0 13.2
1,2,4-Trimethylbenzene mg/kg M111.7 -55 63-136-1 8 3011.787.3 80.8 87.1
1,2-Dibromo-3-
chloropropane mg/kg 11.7 117 32-130118 1 3011.7ND 13.8 13.9
1,2-Dibromoethane (EDB)mg/kg 11.7 107 70-130107 0 3011.7ND 12.5 12.5
1,2-Dichlorobenzene mg/kg 11.7 113 69-130116 2 3011.7ND 13.3 13.6
1,2-Dichloroethane mg/kg 11.7 104 59-130105 1 3011.7ND 12.2 12.3
1,2-Dichloropropane mg/kg 11.7 106 70-130106 1 3011.7ND 12.5 12.4
1,3,5-Trimethylbenzene mg/kg M111.7 37 65-13761 7 3011.737.5 41.8 44.7
1,3-Dichlorobenzene mg/kg 11.7 115 70-130107 7 3011.7ND 13.5 12.6
1,3-Dichloropropane mg/kg 11.7 107 70-130107 0 3011.7ND 12.5 12.5
1,4-Dichlorobenzene mg/kg 11.7 111 68-130110 0 3011.7ND 13.0 12.9
2,2-Dichloropropane mg/kg 11.7 116 32-130116 0 3011.7ND 13.6 13.6
2-Butanone (MEK)mg/kg 23.5 97 10-13699 3 3023.5ND 22.7 23.4
2-Chlorotoluene mg/kg 11.7 135 69-141136 0 3011.7ND 15.9 15.9
2-Hexanone mg/kg 23.5 100 10-144102 3 3023.5ND 23.4 24.0
4-Chlorotoluene mg/kg 11.7 111 70-132113 2 3011.7ND 13.1 13.3
4-Methyl-2-pentanone
(MIBK)mg/kg 23.5 103 25-143104 1 3023.5ND 24.1 24.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3143613MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92518292001
3143614
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acetone mg/kg 23.5 96 10-13099 2 3023.5ND 22.6 23.1
Benzene mg/kg 11.7 102 67-130103 1 3011.70.21 12.2 12.3
Bromobenzene mg/kg 11.7 113 70-130115 2 3011.7ND 13.3 13.5
Bromochloromethane mg/kg 11.7 108 69-134108 0 3011.7ND 12.6 12.7
Bromodichloromethane mg/kg 11.7 101 64-130101 0 3011.7ND 11.9 11.9
Bromoform mg/kg 11.7 104 62-130106 2 3011.7ND 12.2 12.4
Bromomethane mg/kg IK11.7 109 20-176104 5 3011.7ND 12.8 12.2
Carbon tetrachloride mg/kg 11.7 119 65-140120 1 3011.7ND 14.0 14.1
Chlorobenzene mg/kg 11.7 106 70-130106 1 3011.7ND 12.4 12.5
Chloroethane mg/kg 11.7 103 10-130102 1 3011.7ND 12.1 12.0
Chloroform mg/kg 11.7 103 63-130105 1 3011.7ND 12.1 12.3
Chloromethane mg/kg 11.7 97 58-13093 4 3011.7ND 11.4 10.9
cis-1,2-Dichloroethene mg/kg 11.7 101 66-13099 2 3011.7ND 11.9 11.6
cis-1,3-Dichloropropene mg/kg 11.7 106 67-130108 2 3011.7ND 12.4 12.7
Dibromochloromethane mg/kg 11.7 107 67-130107 0 3011.7ND 12.5 12.6
Dibromomethane mg/kg 11.7 101 63-131100 1 3011.7ND 11.8 11.7
Dichlorodifluoromethane mg/kg 11.7 117 44-180118 1 3011.7ND 13.8 13.9
Diisopropyl ether mg/kg 11.7 98 63-13098 0 3011.7ND 11.5 11.5
Ethylbenzene mg/kg 11.7 105 66-130109 4 3011.7ND 12.3 12.7
Hexachloro-1,3-butadiene mg/kg 11.7 138 64-150142 3 3011.7ND 16.2 16.7
Isopropylbenzene
(Cumene)mg/kg 11.7 119 69-135120 2 3011.7ND 13.9 14.1
m&p-Xylene mg/kg 23.5 102 60-133105 3 3023.55.5 29.4 30.2
Methyl-tert-butyl ether mg/kg 11.7 99 65-13099 1 3011.7ND 11.6 11.6
Methylene Chloride mg/kg 11.7 104 61-130102 1 3011.7ND 12.2 12.0
n-Butylbenzene mg/kg M111.7 180 65-140175 3 3011.7ND 21.1 20.5
n-Propylbenzene mg/kg 11.7 134 67-140140 4 3011.7ND 15.8 16.4
Naphthalene mg/kg 11.7 96 15-145108 5 3011.717.2 28.5 29.9
o-Xylene mg/kg 11.7 108 66-133112 4 3011.7ND 12.7 13.2
p-Isopropyltoluene mg/kg 11.7 96 56-147100 2 3011.710.0 21.3 21.7
sec-Butylbenzene mg/kg 11.7 132 65-139138 4 3011.7ND 15.5 16.1
Styrene mg/kg 11.7 111 70-132112 1 3011.7ND 13.0 13.1
tert-Butylbenzene mg/kg 11.7 87 62-13588 1 3011.7ND 10.3 10.4
Tetrachloroethene mg/kg 11.7 111 70-135111 0 3011.7ND 13.0 13.0
Toluene mg/kg 11.7 97 67-130100 3 3011.70.69 12.1 12.4
trans-1,2-Dichloroethene mg/kg 11.7 102 69-13099 2 3011.7ND 11.9 11.7
trans-1,3-Dichloropropene mg/kg 11.7 104 62-130103 0 3011.7ND 12.2 12.1
Trichloroethene mg/kg 11.7 108 70-135110 1 3011.7ND 12.7 12.9
Trichlorofluoromethane mg/kg 11.7 118 10-130116 1 3011.7ND 13.8 13.7
Vinyl acetate mg/kg 23.5 112 53-130112 0 3023.5ND 26.4 26.3
Vinyl chloride mg/kg 11.7 108 61-148106 2 3011.7ND 12.7 12.4
Xylene (Total)mg/kg 35.2 104 63-132108 3 3035.25.5 42.1 43.4
1,2-Dichloroethane-d4 (S)%107 70-130105
4-Bromofluorobenzene (S)%102 69-134102
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
595929
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92518589001, 92518589002, 92518589003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3142918
Associated Lab Samples:92518589001, 92518589002, 92518589003
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 01/29/21 11:280.075
1,2-Dichlorobenzene mg/kg ND 0.33 01/29/21 11:280.070
1,3-Dichlorobenzene mg/kg ND 0.33 01/29/21 11:280.073
1,4-Dichlorobenzene mg/kg ND 0.33 01/29/21 11:280.072
1-Methylnaphthalene mg/kg ND 0.33 01/29/21 11:280.087
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 01/29/21 11:280.090
2,4,5-Trichlorophenol mg/kg ND 0.33 01/29/21 11:280.085
2,4,6-Trichlorophenol mg/kg ND 0.33 01/29/21 11:280.082
2,4-Dichlorophenol mg/kg ND 0.33 01/29/21 11:280.11
2,4-Dimethylphenol mg/kg ND 0.33 01/29/21 11:280.081
2,4-Dinitrophenol mg/kg ND 1.6 01/29/21 11:281.0
2,4-Dinitrotoluene mg/kg ND 0.33 01/29/21 11:280.086
2,6-Dinitrotoluene mg/kg ND 0.33 01/29/21 11:280.085
2-Chloronaphthalene mg/kg ND 0.33 01/29/21 11:280.073
2-Chlorophenol mg/kg ND 0.33 01/29/21 11:280.076
2-Methylnaphthalene mg/kg ND 0.33 01/29/21 11:280.083
2-Methylphenol(o-Cresol)mg/kg ND 0.33 01/29/21 11:280.072
2-Nitroaniline mg/kg ND 1.6 01/29/21 11:280.16
2-Nitrophenol mg/kg ND 0.33 01/29/21 11:280.10
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 01/29/21 11:280.082
3,3'-Dichlorobenzidine mg/kg ND 0.65 IL01/29/21 11:280.23
3-Nitroaniline mg/kg ND 1.6 01/29/21 11:280.17
4,6-Dinitro-2-methylphenol mg/kg ND 0.65 01/29/21 11:280.52
4-Bromophenylphenyl ether mg/kg ND 0.33 01/29/21 11:280.085
4-Chloro-3-methylphenol mg/kg ND 0.65 01/29/21 11:280.20
4-Chloroaniline mg/kg ND 0.65 01/29/21 11:280.20
4-Chlorophenylphenyl ether mg/kg ND 0.33 01/29/21 11:280.085
4-Nitroaniline mg/kg ND 0.65 01/29/21 11:280.16
4-Nitrophenol mg/kg ND 1.6 01/29/21 11:280.52
Acenaphthene mg/kg ND 0.33 01/29/21 11:280.084
Acenaphthylene mg/kg ND 0.33 01/29/21 11:280.077
Aniline mg/kg ND 0.33 01/29/21 11:280.073
Anthracene mg/kg ND 0.33 01/29/21 11:280.084
Benzo(a)anthracene mg/kg ND 0.33 01/29/21 11:280.10
Benzo(a)pyrene mg/kg ND 0.33 01/29/21 11:280.14
Benzo(b)fluoranthene mg/kg ND 0.33 01/29/21 11:280.13
Benzo(g,h,i)perylene mg/kg ND 0.33 01/29/21 11:280.13
Benzo(k)fluoranthene mg/kg ND 0.33 01/29/21 11:280.14
Benzoic Acid mg/kg ND 1.6 01/29/21 11:280.35
Benzyl alcohol mg/kg ND 0.65 01/29/21 11:280.17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3142918
Associated Lab Samples:92518589001, 92518589002, 92518589003
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane mg/kg ND 0.33 01/29/21 11:280.087
bis(2-Chloroethyl) ether mg/kg ND 0.33 01/29/21 11:280.069
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 01/29/21 11:280.11
Butylbenzylphthalate mg/kg ND 0.33 01/29/21 11:280.087
Chrysene mg/kg ND 0.33 01/29/21 11:280.095
Di-n-butylphthalate mg/kg ND 0.33 01/29/21 11:280.080
Di-n-octylphthalate mg/kg ND 0.33 01/29/21 11:280.19
Dibenz(a,h)anthracene mg/kg ND 0.33 01/29/21 11:280.13
Dibenzofuran mg/kg ND 0.33 01/29/21 11:280.081
Diethylphthalate mg/kg ND 0.33 01/29/21 11:280.071
Dimethylphthalate mg/kg ND 0.33 01/29/21 11:280.074
Fluoranthene mg/kg ND 0.33 01/29/21 11:280.098
Fluorene mg/kg ND 0.33 01/29/21 11:280.087
Hexachloro-1,3-butadiene mg/kg ND 0.33 01/29/21 11:280.079
Hexachlorobenzene mg/kg ND 0.33 01/29/21 11:280.083
Hexachlorocyclopentadiene mg/kg ND 0.33 v201/29/21 11:280.13
Hexachloroethane mg/kg ND 0.33 01/29/21 11:280.074
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 01/29/21 11:280.15
Isophorone mg/kg ND 0.33 01/29/21 11:280.071
N-Nitroso-di-n-propylamine mg/kg ND 0.33 01/29/21 11:280.091
N-Nitrosodimethylamine mg/kg ND 0.33 01/29/21 11:280.092
N-Nitrosodiphenylamine mg/kg ND 0.33 01/29/21 11:280.083
Naphthalene mg/kg ND 0.33 01/29/21 11:280.078
Nitrobenzene mg/kg ND 0.33 01/29/21 11:280.078
Pentachlorophenol mg/kg ND 0.65 01/29/21 11:280.15
Phenanthrene mg/kg ND 0.33 01/29/21 11:280.082
Phenol mg/kg ND 0.33 01/29/21 11:280.078
Pyrene mg/kg ND 0.33 01/29/21 11:280.090
Pyridine mg/kg ND 0.33 01/29/21 11:280.082
2,4,6-Tribromophenol (S)%79 18-130 01/29/21 11:28
2-Fluorobiphenyl (S)%81 19-130 01/29/21 11:28
2-Fluorophenol (S)%79 18-130 01/29/21 11:28
Nitrobenzene-d5 (S)%83 21-130 01/29/21 11:28
Phenol-d6 (S)%83 18-130 01/29/21 11:28
Terphenyl-d14 (S)%121 15-130 01/29/21 11:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3142919LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.41.6 83 47-130
1,2-Dichlorobenzene mg/kg 1.51.6 90 49-130
1,3-Dichlorobenzene mg/kg 1.41.6 86 48-130
1,4-Dichlorobenzene mg/kg 1.51.6 89 49-130
1-Methylnaphthalene mg/kg 1.51.6 92 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3142919LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.41.6 88 38-130
2,4,5-Trichlorophenol mg/kg 1.51.6 90 49-130
2,4,6-Trichlorophenol mg/kg 1.41.6 86 50-130
2,4-Dichlorophenol mg/kg 1.61.6 96 51-130
2,4-Dimethylphenol mg/kg 1.61.6 99 53-130
2,4-Dinitrophenol mg/kg 6.58.2 79 39-130
2,4-Dinitrotoluene mg/kg 1.61.6 97 53-130
2,6-Dinitrotoluene mg/kg 1.61.6 96 55-130
2-Chloronaphthalene mg/kg 1.41.6 86 48-130
2-Chlorophenol mg/kg 1.61.6 100 54-130
2-Methylnaphthalene mg/kg 1.51.6 94 57-130
2-Methylphenol(o-Cresol)mg/kg 1.81.6 108 50-130
2-Nitroaniline mg/kg 2.93.3 88 49-130
2-Nitrophenol mg/kg 1.51.6 94 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.81.6 110 50-130
3,3'-Dichlorobenzidine mg/kg 2.5 IL3.3 75 47-130
3-Nitroaniline mg/kg 3.13.3 94 45-130
4,6-Dinitro-2-methylphenol mg/kg 2.73.3 83 50-142
4-Bromophenylphenyl ether mg/kg 1.41.6 86 55-130
4-Chloro-3-methylphenol mg/kg 3.43.3 103 52-130
4-Chloroaniline mg/kg 2.63.3 80 49-130
4-Chlorophenylphenyl ether mg/kg 1.51.6 89 53-130
4-Nitroaniline mg/kg 3.03.3 92 51-130
4-Nitrophenol mg/kg 7.68.2 93 40-130
Acenaphthene mg/kg 1.41.6 86 56-130
Acenaphthylene mg/kg 1.51.6 89 58-130
Aniline mg/kg 1.31.6 79 44-130
Anthracene mg/kg 1.31.6 79 60-130
Benzo(a)anthracene mg/kg 1.51.6 91 59-130
Benzo(a)pyrene mg/kg 1.51.6 90 57-130
Benzo(b)fluoranthene mg/kg 1.51.6 92 54-130
Benzo(g,h,i)perylene mg/kg 1.31.6 80 59-130
Benzo(k)fluoranthene mg/kg 1.61.6 96 54-130
Benzoic Acid mg/kg 5.08.2 61 19-130
Benzyl alcohol mg/kg 3.43.3 103 50-130
bis(2-Chloroethoxy)methane mg/kg 1.41.6 88 55-130
bis(2-Chloroethyl) ether mg/kg 1.61.6 96 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.61.6 98 58-130
Butylbenzylphthalate mg/kg 1.61.6 95 46-138
Chrysene mg/kg 1.61.6 96 57-130
Di-n-butylphthalate mg/kg 1.51.6 92 57-130
Di-n-octylphthalate mg/kg 1.71.6 106 57-130
Dibenz(a,h)anthracene mg/kg 1.41.6 84 60-130
Dibenzofuran mg/kg 1.51.6 90 54-130
Diethylphthalate mg/kg 1.61.6 96 55-130
Dimethylphthalate mg/kg 1.51.6 94 57-130
Fluoranthene mg/kg 1.51.6 89 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3142919LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.51.6 90 56-130
Hexachloro-1,3-butadiene mg/kg 1.31.6 79 41-130
Hexachlorobenzene mg/kg 1.41.6 84 53-130
Hexachlorocyclopentadiene mg/kg 0.75 v31.6 46 23-130
Hexachloroethane mg/kg 1.41.6 88 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.31.6 82 61-130
Isophorone mg/kg 1.51.6 91 49-130
N-Nitroso-di-n-propylamine mg/kg 1.71.6 102 52-130
N-Nitrosodimethylamine mg/kg 1.41.6 84 45-130
N-Nitrosodiphenylamine mg/kg 1.41.6 85 56-130
Naphthalene mg/kg 1.41.6 86 56-130
Nitrobenzene mg/kg 1.51.6 89 50-130
Pentachlorophenol mg/kg 2.73.3 81 33-130
Phenanthrene mg/kg 1.41.6 87 60-130
Phenol mg/kg 1.81.6 111 54-130
Pyrene mg/kg 1.51.6 90 61-130
Pyridine mg/kg 1.11.6 65 35-130
2,4,6-Tribromophenol (S)%87 18-130
2-Fluorobiphenyl (S)%84 19-130
2-Fluorophenol (S)%96 18-130
Nitrobenzene-d5 (S)%86 21-130
Phenol-d6 (S)%102 18-130
Terphenyl-d14 (S)%111 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92518589003
3142921SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
1-Methylnaphthalene mg/kg 22.7 21 3028.1
2,2'-Oxybis(1-chloropropane)mg/kg ND 30ND
2,4,5-Trichlorophenol mg/kg ND 30ND
2,4,6-Trichlorophenol mg/kg ND 30ND
2,4-Dichlorophenol mg/kg ND 30ND
2,4-Dimethylphenol mg/kg ND 30ND
2,4-Dinitrophenol mg/kg ND 30ND
2,4-Dinitrotoluene mg/kg ND 30ND
2,6-Dinitrotoluene mg/kg ND 30ND
2-Chloronaphthalene mg/kg ND 30ND
2-Chlorophenol mg/kg ND 30ND
2-Methylnaphthalene mg/kg 38.2 20 3046.5
2-Methylphenol(o-Cresol)mg/kg ND 30ND
2-Nitroaniline mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92518589003
3142921SAMPLE DUPLICATE:
2-Nitrophenol mg/kg ND 30ND
3&4-Methylphenol(m&p Cresol)mg/kg ND 30ND
3,3'-Dichlorobenzidine mg/kg ND IL30ND
3-Nitroaniline mg/kg ND 30ND
4,6-Dinitro-2-methylphenol mg/kg ND 30ND
4-Bromophenylphenyl ether mg/kg ND 30ND
4-Chloro-3-methylphenol mg/kg ND 30ND
4-Chloroaniline mg/kg ND 30ND
4-Chlorophenylphenyl ether mg/kg ND 30ND
4-Nitroaniline mg/kg ND 30ND
4-Nitrophenol mg/kg ND 30ND
Acenaphthene mg/kg ND 30ND
Acenaphthylene mg/kg ND 30ND
Aniline mg/kg ND 30ND
Anthracene mg/kg ND 30ND
Benzo(a)anthracene mg/kg ND 30ND
Benzo(a)pyrene mg/kg ND 30ND
Benzo(b)fluoranthene mg/kg ND 30ND
Benzo(g,h,i)perylene mg/kg ND 30ND
Benzo(k)fluoranthene mg/kg ND 30ND
Benzoic Acid mg/kg ND 30ND
Benzyl alcohol mg/kg ND 30ND
bis(2-Chloroethoxy)methane mg/kg ND 30ND
bis(2-Chloroethyl) ether mg/kg ND 30ND
bis(2-Ethylhexyl)phthalate mg/kg 1.7J 301.7J
Butylbenzylphthalate mg/kg ND 30ND
Chrysene mg/kg ND 30ND
Di-n-butylphthalate mg/kg ND 30ND
Di-n-octylphthalate mg/kg ND 30ND
Dibenz(a,h)anthracene mg/kg ND 30ND
Dibenzofuran mg/kg 1.3J 30ND
Diethylphthalate mg/kg ND 30ND
Dimethylphthalate mg/kg ND 30ND
Fluoranthene mg/kg ND 30ND
Fluorene mg/kg 2.4J 303.1J
Hexachloro-1,3-butadiene mg/kg ND 30ND
Hexachlorobenzene mg/kg ND 30ND
Hexachlorocyclopentadiene mg/kg ND v230ND
Hexachloroethane mg/kg ND 30ND
Indeno(1,2,3-cd)pyrene mg/kg ND 30ND
Isophorone mg/kg ND 30ND
N-Nitroso-di-n-propylamine mg/kg ND 30ND
N-Nitrosodimethylamine mg/kg ND 30ND
N-Nitrosodiphenylamine mg/kg ND 30ND
Naphthalene mg/kg 9.6 15 3011.1
Nitrobenzene mg/kg ND 30ND
Pentachlorophenol mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 36 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92518589003
3142921SAMPLE DUPLICATE:
Phenanthrene mg/kg 4.8 19 305.8
Phenol mg/kg ND 30ND
Pyrene mg/kg ND 30ND
Pyridine mg/kg ND 30ND
2,4,6-Tribromophenol (S)%0 S40
2-Fluorobiphenyl (S)%0 S40
2-Fluorophenol (S)%0 S40
Nitrobenzene-d5 (S)%0 D3,S40
Phenol-d6 (S)%0 S40
Terphenyl-d14 (S)%0 S40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 37 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
595458
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92518589001, 92518589002, 92518589003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92518308001
3140898SAMPLE DUPLICATE:
Percent Moisture %11.9 N2172514.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92518589003
3140974SAMPLE DUPLICATE:
Percent Moisture %25.5 N242526.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
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[phone]
Page 38 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1614567
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92518589001, 92518589002, 92518589003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3619251-1
Associated Lab Samples:92518589001, 92518589002, 92518589003
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 02/03/21 08:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3619251-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92518589001
R3619251-3SAMPLE DUPLICATE:
Total Solids %71.9 0.224 1071.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
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[phone]
Page 39 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1613765
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92518589001, 92518589002, 92518589003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3618475-1
Associated Lab Samples:92518589001, 92518589002, 92518589003
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 02/01/21 19:040.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3618475-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.7910.0 97.9 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3618475-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1310181-01
R3618475-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg E,P623.0 0.00 75.0-1250.00 0.821 2023.0489 415 411
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3618475-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1310181-01
Chromium, Hexavalent mg/kg 758 ML76435.2 75.0-125489
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1310169-01
R3618475-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 23.3 3.17 2022.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1311256-04
R3618475-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
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9800 Kincey Ave. Suite 100
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Page 40 of 45
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte concentration exceeded the calibration range. The reported result is estimated.E
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the
spike level.P6
Surrogate recovery not evaluated against control limits due to sample dilution.S4
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
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[phone]
Page 41 of 45
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92518589
7th & Caswell Tank Pull
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92518589001 595682 595847T-1 EPA 3050B EPA 6010D
92518589002 595682 595847T-2 EPA 3050B EPA 6010D
92518589003 595682 595847T-3 EPA 3050B EPA 6010D
92518589001 595763 595766T-1 EPA 7471B EPA 7471B
92518589002 595763 595766T-2 EPA 7471B EPA 7471B
92518589003 595763 595766T-3 EPA 7471B EPA 7471B
92518589001 595929 596357T-1 EPA 3546 EPA 8270E
92518589002 595929 596357T-2 EPA 3546 EPA 8270E
92518589003 595929 596357T-3 EPA 3546 EPA 8270E
92518589001 595702 595704T-1 EPA 5035A/5030B EPA 8260D
92518589002 596037 596041T-2 EPA 5035A/5030B EPA 8260D
92518589003 596037 596041T-3 EPA 5035A/5030B EPA 8260D
92518589001 595458T-1 SW-846
92518589002 595458T-2 SW-846
92518589003 595458T-3 SW-846
92518589001 1614567 1614567T-1 SM 2540 G SM 2540G
92518589002 1614567 1614567T-2 SM 2540 G SM 2540G
92518589003 1614567 1614567T-3 SM 2540 G SM 2540G
92518589001 1613765 1613765T-1 3060A EPA 7199
92518589002 1613765 1613765T-2 3060A EPA 7199
92518589003 1613765 1613765T-3 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/04/2021 04:45 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 42 of 45
Page 43 of 45
Page 44 of 45
Page 45 of 45
#=CL#
February 09, 2021
LIMS USE: FR - CHRIS ORRELL
LIMS OBJECT ID: 92519538
92519538
Project:
Pace Project No.:
RE:
Chris Orrell
ECS Southeast, LLP
1900 Center Park Dr Suite D
9809 Aviary Hill Way, Charlott
Charlotte, NC 28217
7th & Caswell Tank Pull
Dear Chris Orrell:
Enclosed are the analytical results for sample(s) received by the laboratory on February 01, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Jenna Dew, ECS Southeast
ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 32
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
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New Mexico DW Certification
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North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
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Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 32
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Lab ID Sample ID Matrix Date Collected Date Received
92519538001 T-4 Solid 01/29/21 16:00 02/01/21 07:15
REPORT OF LABORATORY ANALYSIS
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Page 3 of 32
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92519538001 T-4 EPA 6010D 7 PASI-ADS
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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Page 4 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Sample:T-4 Lab ID:92519538001 Collected:01/29/21 16:00 Received:02/01/21 07:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 4.0 mg/kg 02/03/21 19:19 7440-38-202/02/21 14:502.6 0.51 1
Barium 112 mg/kg 02/03/21 19:19 7440-39-302/02/21 14:501.0 0.26 1
Cadmium ND mg/kg 02/03/21 19:19 7440-43-902/02/21 14:500.10 0.051 1
Chromium 133 mg/kg 02/03/21 19:19 7440-47-302/02/21 14:500.51 0.26 1
Lead 20.1 mg/kg 02/03/21 19:19 7439-92-102/02/21 14:501.0 0.26 1
Selenium 1.9 mg/kg 02/03/21 19:19 7782-49-202/02/21 14:501.0 0.51 1
Silver ND mg/kg 02/03/21 19:19 7440-22-402/02/21 14:500.51 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.035 mg/kg 02/04/21 13:10 7439-97-602/03/21 12:450.0031 0.0023 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 02/02/21 20:25 83-32-902/02/21 12:220.43 0.11 1
Acenaphthylene ND mg/kg 02/02/21 20:25 208-96-802/02/21 12:220.43 0.10 1
Aniline ND mg/kg 02/02/21 20:25 62-53-302/02/21 12:220.43 0.096 1
Anthracene ND mg/kg 02/02/21 20:25 120-12-702/02/21 12:220.43 0.11 1
Benzo(a)anthracene ND mg/kg 02/02/21 20:25 56-55-302/02/21 12:220.43 0.14 1
Benzo(a)pyrene ND mg/kg 02/02/21 20:25 50-32-802/02/21 12:220.43 0.18 1
Benzo(b)fluoranthene ND mg/kg 02/02/21 20:25 205-99-202/02/21 12:220.43 0.17 1
Benzo(g,h,i)perylene ND mg/kg 02/02/21 20:25 191-24-202/02/21 12:220.43 0.17 1
Benzo(k)fluoranthene ND mg/kg 02/02/21 20:25 207-08-902/02/21 12:220.43 0.18 1
Benzoic Acid ND mg/kg 02/02/21 20:25 65-85-002/02/21 12:222.1 0.46 1
Benzyl alcohol ND mg/kg 02/02/21 20:25 100-51-602/02/21 12:220.85 0.23 1
4-Bromophenylphenyl ether ND mg/kg 02/02/21 20:25 101-55-302/02/21 12:220.43 0.11 1
Butylbenzylphthalate ND mg/kg 02/02/21 20:25 85-68-702/02/21 12:220.43 0.11 1
4-Chloro-3-methylphenol ND mg/kg 02/02/21 20:25 59-50-702/02/21 12:220.85 0.26 1
4-Chloroaniline ND mg/kg 02/02/21 20:25 106-47-802/02/21 12:220.85 0.26 1
bis(2-Chloroethoxy)methane ND mg/kg 02/02/21 20:25 111-91-102/02/21 12:220.43 0.11 1
bis(2-Chloroethyl) ether ND mg/kg 02/02/21 20:25 111-44-402/02/21 12:220.43 0.090 1
2-Chloronaphthalene ND mg/kg 02/02/21 20:25 91-58-702/02/21 12:220.43 0.095 1
2-Chlorophenol ND mg/kg 02/02/21 20:25 95-57-802/02/21 12:220.43 0.099 1
4-Chlorophenylphenyl ether ND mg/kg 02/02/21 20:25 7005-72-302/02/21 12:220.43 0.11 1
Chrysene ND mg/kg 02/02/21 20:25 218-01-902/02/21 12:220.43 0.12 1
Dibenz(a,h)anthracene ND mg/kg 02/02/21 20:25 53-70-302/02/21 12:220.43 0.17 1
Dibenzofuran ND mg/kg 02/02/21 20:25 132-64-902/02/21 12:220.43 0.11 1
1,2-Dichlorobenzene ND mg/kg 02/02/21 20:25 95-50-102/02/21 12:220.43 0.092 1
1,3-Dichlorobenzene ND mg/kg 02/02/21 20:25 541-73-102/02/21 12:220.43 0.096 1
1,4-Dichlorobenzene ND mg/kg 02/02/21 20:25 106-46-702/02/21 12:220.43 0.094 1
3,3'-Dichlorobenzidine ND mg/kg 02/02/21 20:25 91-94-102/02/21 12:220.85 0.30 1
2,4-Dichlorophenol ND mg/kg 02/02/21 20:25 120-83-202/02/21 12:220.43 0.14 1
Diethylphthalate ND mg/kg 02/02/21 20:25 84-66-202/02/21 12:220.43 0.092 1
2,4-Dimethylphenol ND mg/kg 02/02/21 20:25 105-67-902/02/21 12:220.43 0.11 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
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[phone]
Page 5 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Sample:T-4 Lab ID:92519538001 Collected:01/29/21 16:00 Received:02/01/21 07:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 02/02/21 20:25 131-11-302/02/21 12:220.43 0.096 1
Di-n-butylphthalate ND mg/kg 02/02/21 20:25 84-74-202/02/21 12:220.43 0.10 1
4,6-Dinitro-2-methylphenol ND mg/kg 02/02/21 20:25 534-52-102/02/21 12:220.85 0.69 1
2,4-Dinitrophenol ND mg/kg 02/02/21 20:25 51-28-502/02/21 12:222.1 1.4 1
2,4-Dinitrotoluene ND mg/kg 02/02/21 20:25 121-14-202/02/21 12:220.43 0.11 1
2,6-Dinitrotoluene ND mg/kg 02/02/21 20:25 606-20-202/02/21 12:220.43 0.11 1
Di-n-octylphthalate ND mg/kg 02/02/21 20:25 117-84-002/02/21 12:220.43 0.24 1
bis(2-Ethylhexyl)phthalate ND mg/kg 02/02/21 20:25 117-81-702/02/21 12:220.43 0.14 1
Fluoranthene ND mg/kg 02/02/21 20:25 206-44-002/02/21 12:220.43 0.13 1
Fluorene ND mg/kg 02/02/21 20:25 86-73-702/02/21 12:220.43 0.11 1
Hexachloro-1,3-butadiene ND mg/kg 02/02/21 20:25 87-68-302/02/21 12:220.43 0.10 1
Hexachlorobenzene ND mg/kg 02/02/21 20:25 118-74-102/02/21 12:220.43 0.11 1
Hexachlorocyclopentadiene ND mg/kg 02/02/21 20:25 77-47-402/02/21 12:220.43 0.17 1
Hexachloroethane ND mg/kg 02/02/21 20:25 67-72-102/02/21 12:220.43 0.097 1
Indeno(1,2,3-cd)pyrene ND mg/kg 02/02/21 20:25 193-39-502/02/21 12:220.43 0.19 1
Isophorone ND mg/kg 02/02/21 20:25 78-59-102/02/21 12:220.43 0.092 1
1-Methylnaphthalene 0.33J mg/kg 02/02/21 20:25 90-12-002/02/21 12:220.43 0.11 1
2-Methylnaphthalene 0.64 mg/kg 02/02/21 20:25 91-57-602/02/21 12:220.43 0.11 1
2-Methylphenol(o-Cresol)ND mg/kg 02/02/21 20:25 95-48-702/02/21 12:220.43 0.094 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 02/02/21 20:25 15831-10-402/02/21 12:220.43 0.11 1
Naphthalene 0.19J mg/kg 02/02/21 20:25 91-20-302/02/21 12:220.43 0.10 1
2-Nitroaniline ND mg/kg 02/02/21 20:25 88-74-402/02/21 12:222.1 0.21 1
3-Nitroaniline ND mg/kg 02/02/21 20:25 99-09-2 IL02/02/21 12:222.1 0.23 1
4-Nitroaniline ND mg/kg 02/02/21 20:25 100-01-602/02/21 12:220.85 0.21 1
Nitrobenzene ND mg/kg 02/02/21 20:25 98-95-302/02/21 12:220.43 0.10 1
2-Nitrophenol ND mg/kg 02/02/21 20:25 88-75-502/02/21 12:220.43 0.13 1
4-Nitrophenol ND mg/kg 02/02/21 20:25 100-02-702/02/21 12:222.1 0.68 1
N-Nitrosodimethylamine ND mg/kg 02/02/21 20:25 62-75-902/02/21 12:220.43 0.12 1
N-Nitroso-di-n-propylamine ND mg/kg 02/02/21 20:25 621-64-702/02/21 12:220.43 0.12 1
N-Nitrosodiphenylamine ND mg/kg 02/02/21 20:25 86-30-602/02/21 12:220.43 0.11 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 02/02/21 20:25 108-60-102/02/21 12:220.43 0.12 1
Pentachlorophenol ND mg/kg 02/02/21 20:25 87-86-502/02/21 12:220.85 0.19 1
Phenanthrene ND mg/kg 02/02/21 20:25 85-01-802/02/21 12:220.43 0.11 1
Phenol ND mg/kg 02/02/21 20:25 108-95-202/02/21 12:220.43 0.10 1
Pyrene ND mg/kg 02/02/21 20:25 129-00-002/02/21 12:220.43 0.12 1
Pyridine ND mg/kg 02/02/21 20:25 110-86-102/02/21 12:220.43 0.11 1
1,2,4-Trichlorobenzene ND mg/kg 02/02/21 20:25 120-82-102/02/21 12:220.43 0.097 1
2,4,5-Trichlorophenol ND mg/kg 02/02/21 20:25 95-95-402/02/21 12:220.43 0.11 1
2,4,6-Trichlorophenol ND mg/kg 02/02/21 20:25 88-06-202/02/21 12:220.43 0.11 1
Surrogates
Nitrobenzene-d5 (S)86 %02/02/21 20:25 4165-60-002/02/21 12:2221-130 1
2-Fluorobiphenyl (S)82 %02/02/21 20:25 321-60-802/02/21 12:2219-130 1
Terphenyl-d14 (S)110 %02/02/21 20:25 1718-51-002/02/21 12:2215-130 1
Phenol-d6 (S)79 %02/02/21 20:25 13127-88-302/02/21 12:2218-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Sample:T-4 Lab ID:92519538001 Collected:01/29/21 16:00 Received:02/01/21 07:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)72 %02/02/21 20:25 367-12-402/02/21 12:2218-130 1
2,4,6-Tribromophenol (S)113 %02/02/21 20:25 118-79-602/02/21 12:2218-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 02/04/21 15:58 67-64-102/04/21 10:170.14 0.043 1
Benzene ND mg/kg 02/04/21 15:58 71-43-202/04/21 10:170.0068 0.0027 1
Bromobenzene ND mg/kg 02/04/21 15:58 108-86-102/04/21 10:170.0068 0.0022 1
Bromochloromethane ND mg/kg 02/04/21 15:58 74-97-502/04/21 10:170.0068 0.0020 1
Bromodichloromethane ND mg/kg 02/04/21 15:58 75-27-402/04/21 10:170.0068 0.0026 1
Bromoform ND mg/kg 02/04/21 15:58 75-25-202/04/21 10:170.0068 0.0024 1
Bromomethane ND mg/kg 02/04/21 15:58 74-83-902/04/21 10:170.014 0.011 1
2-Butanone (MEK)ND mg/kg 02/04/21 15:58 78-93-302/04/21 10:170.14 0.032 1
n-Butylbenzene ND mg/kg 02/04/21 15:58 104-51-802/04/21 10:170.0068 0.0032 1
sec-Butylbenzene ND mg/kg 02/04/21 15:58 135-98-802/04/21 10:170.0068 0.0030 1
tert-Butylbenzene ND mg/kg 02/04/21 15:58 98-06-602/04/21 10:170.0068 0.0024 1
Carbon tetrachloride ND mg/kg 02/04/21 15:58 56-23-502/04/21 10:170.0068 0.0025 1
Chlorobenzene ND mg/kg 02/04/21 15:58 108-90-702/04/21 10:170.0068 0.0013 1
Chloroethane ND mg/kg 02/04/21 15:58 75-00-302/04/21 10:170.014 0.0052 1
Chloroform ND mg/kg 02/04/21 15:58 67-66-302/04/21 10:170.0068 0.0041 1
Chloromethane ND mg/kg 02/04/21 15:58 74-87-302/04/21 10:170.014 0.0057 1
2-Chlorotoluene ND mg/kg 02/04/21 15:58 95-49-802/04/21 10:170.0068 0.0024 1
4-Chlorotoluene ND mg/kg 02/04/21 15:58 106-43-402/04/21 10:170.0068 0.0012 1
1,2-Dibromo-3-chloropropane ND mg/kg 02/04/21 15:58 96-12-802/04/21 10:170.0068 0.0026 1
Dibromochloromethane ND mg/kg 02/04/21 15:58 124-48-102/04/21 10:170.0068 0.0038 1
1,2-Dibromoethane (EDB)ND mg/kg 02/04/21 15:58 106-93-402/04/21 10:170.0068 0.0030 1
Dibromomethane ND mg/kg 02/04/21 15:58 74-95-302/04/21 10:170.0068 0.0014 1
1,2-Dichlorobenzene ND mg/kg 02/04/21 15:58 95-50-102/04/21 10:170.0068 0.0024 1
1,3-Dichlorobenzene ND mg/kg 02/04/21 15:58 541-73-102/04/21 10:170.0068 0.0021 1
1,4-Dichlorobenzene ND mg/kg 02/04/21 15:58 106-46-702/04/21 10:170.0068 0.0018 1
Dichlorodifluoromethane ND mg/kg 02/04/21 15:58 75-71-802/04/21 10:170.014 0.0029 1
1,1-Dichloroethane ND mg/kg 02/04/21 15:58 75-34-302/04/21 10:170.0068 0.0028 1
1,2-Dichloroethane ND mg/kg 02/04/21 15:58 107-06-202/04/21 10:170.0068 0.0045 1
1,1-Dichloroethene ND mg/kg 02/04/21 15:58 75-35-402/04/21 10:170.0068 0.0028 1
cis-1,2-Dichloroethene ND mg/kg 02/04/21 15:58 156-59-202/04/21 10:170.0068 0.0023 1
trans-1,2-Dichloroethene ND mg/kg 02/04/21 15:58 156-60-502/04/21 10:170.0068 0.0024 1
1,2-Dichloropropane ND mg/kg 02/04/21 15:58 78-87-502/04/21 10:170.0068 0.0020 1
1,3-Dichloropropane ND mg/kg 02/04/21 15:58 142-28-902/04/21 10:170.0068 0.0021 1
2,2-Dichloropropane ND mg/kg 02/04/21 15:58 594-20-702/04/21 10:170.0068 0.0022 1
1,1-Dichloropropene ND mg/kg 02/04/21 15:58 563-58-602/04/21 10:170.0068 0.0032 1
cis-1,3-Dichloropropene ND mg/kg 02/04/21 15:58 10061-01-502/04/21 10:170.0068 0.0018 1
trans-1,3-Dichloropropene ND mg/kg 02/04/21 15:58 10061-02-602/04/21 10:170.0068 0.0023 1
Diisopropyl ether ND mg/kg 02/04/21 15:58 108-20-302/04/21 10:170.0068 0.0018 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Sample:T-4 Lab ID:92519538001 Collected:01/29/21 16:00 Received:02/01/21 07:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene 0.0047J mg/kg 02/04/21 15:58 100-41-402/04/21 10:170.0068 0.0032 1
Hexachloro-1,3-butadiene ND mg/kg 02/04/21 15:58 87-68-302/04/21 10:170.014 0.011 1
2-Hexanone 0.051J mg/kg 02/04/21 15:58 591-78-602/04/21 10:170.068 0.0065 1
Isopropylbenzene (Cumene)ND mg/kg 02/04/21 15:58 98-82-802/04/21 10:170.0068 0.0023 1
p-Isopropyltoluene 0.034 mg/kg 02/04/21 15:58 99-87-602/04/21 10:170.0068 0.0033 1
Methylene Chloride ND mg/kg 02/04/21 15:58 75-09-202/04/21 10:170.027 0.019 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 02/04/21 15:58 108-10-102/04/21 10:170.068 0.0065 1
Methyl-tert-butyl ether ND mg/kg 02/04/21 15:58 1634-04-402/04/21 10:170.0068 0.0025 1
Naphthalene 0.23 mg/kg 02/04/21 15:58 91-20-302/04/21 10:170.0068 0.0036 1
n-Propylbenzene ND mg/kg 02/04/21 15:58 103-65-102/04/21 10:170.0068 0.0024 1
Styrene ND mg/kg 02/04/21 15:58 100-42-502/04/21 10:170.0068 0.0018 1
1,1,1,2-Tetrachloroethane ND mg/kg 02/04/21 15:58 630-20-602/04/21 10:170.0068 0.0026 1
1,1,2,2-Tetrachloroethane ND mg/kg 02/04/21 15:58 79-34-502/04/21 10:170.0068 0.0018 1
Tetrachloroethene ND mg/kg 02/04/21 15:58 127-18-402/04/21 10:170.0068 0.0021 1
Toluene 0.016 mg/kg 02/04/21 15:58 108-88-302/04/21 10:170.0068 0.0019 1
1,2,3-Trichlorobenzene ND mg/kg 02/04/21 15:58 87-61-602/04/21 10:170.0068 0.0055 1
1,2,4-Trichlorobenzene ND mg/kg 02/04/21 15:58 120-82-102/04/21 10:170.0068 0.0057 1
1,1,1-Trichloroethane ND mg/kg 02/04/21 15:58 71-55-602/04/21 10:170.0068 0.0035 1
1,1,2-Trichloroethane ND mg/kg 02/04/21 15:58 79-00-502/04/21 10:170.0068 0.0022 1
Trichloroethene ND mg/kg 02/04/21 15:58 79-01-602/04/21 10:170.0068 0.0017 1
Trichlorofluoromethane ND mg/kg 02/04/21 15:58 75-69-402/04/21 10:170.0068 0.0037 1
1,2,3-Trichloropropane ND mg/kg 02/04/21 15:58 96-18-402/04/21 10:170.0068 0.0034 1
1,2,4-Trimethylbenzene 0.37 mg/kg 02/04/21 15:58 95-63-602/04/21 10:170.0068 0.0019 1
1,3,5-Trimethylbenzene 0.11 mg/kg 02/04/21 15:58 108-67-802/04/21 10:170.0068 0.0023 1
Vinyl acetate ND mg/kg 02/04/21 15:58 108-05-402/04/21 10:170.068 0.0049 1
Vinyl chloride ND mg/kg 02/04/21 15:58 75-01-402/04/21 10:170.014 0.0034 1
Xylene (Total)0.056 mg/kg 02/04/21 15:58 1330-20-702/04/21 10:170.014 0.0039 1
m&p-Xylene 0.016 mg/kg 02/04/21 15:58 179601-23-102/04/21 10:170.014 0.0046 1
o-Xylene 0.039 mg/kg 02/04/21 15:58 95-47-602/04/21 10:170.0068 0.0030 1
Surrogates
Toluene-d8 (S)102 %02/04/21 15:58 2037-26-502/04/21 10:1770-130 1
4-Bromofluorobenzene (S)102 %02/04/21 15:58 460-00-402/04/21 10:1769-134 1
1,2-Dichloroethane-d4 (S)106 %02/04/21 15:58 17060-07-002/04/21 10:1770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.7 %02/01/21 15:01 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 84.6 %02/05/21 10:2102/05/21 10:101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Sample:T-4 Lab ID:92519538001 Collected:01/29/21 16:00 Received:02/01/21 07:15 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 02/09/21 01:27 18540-29-902/08/21 16:141.18 0.301 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597289
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92519538001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3149590
Associated Lab Samples:92519538001
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 02/04/21 12:060.0046
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3149591LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0830.083 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3149592MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92519090001
3149593
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg M10.025 71 75-12575 4 200.0250.0022 0.020 0.021
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597002
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92519538001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3148161
Associated Lab Samples:92519538001
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 2.5 02/03/21 18:400.50
Barium mg/kg ND 1.0 02/03/21 18:400.25
Cadmium mg/kg ND 0.10 02/03/21 18:400.050
Chromium mg/kg ND 0.50 02/03/21 18:400.25
Lead mg/kg ND 1.0 02/03/21 18:400.25
Selenium mg/kg ND 1.0 02/03/21 18:400.50
Silver mg/kg ND 0.50 02/03/21 18:400.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3148162LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 47.650 95 80-120
Barium mg/kg 48.850 98 80-120
Cadmium mg/kg 46.850 94 80-120
Chromium mg/kg 47.850 96 80-120
Lead mg/kg 47.650 95 80-120
Selenium mg/kg 41.950 84 80-120
Silver mg/kg 23.725 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3148163MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92516781001
3148164
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 1940 97 75-12598 1 201920ND18901880
Barium mg/kg 1940 101 75-125100 2 20192015821202080
Cadmium mg/kg 1940 97 75-12596 2 201920ND18701840
Chromium mg/kg 1940 99 75-12598 2 20192024.1 1940 1910
Lead mg/kg 1940 100 75-12598 3 20192015721002040
Selenium mg/kg 1940 84 75-12583 2 201920ND16301590
Silver mg/kg 969 97 75-12597 1 20955ND945931
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597618
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519538001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3151170
Associated Lab Samples:92519538001
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 02/04/21 12:030.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 02/04/21 12:030.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 02/04/21 12:030.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 02/04/21 12:030.0017
1,1-Dichloroethane mg/kg ND 0.0050 02/04/21 12:030.0021
1,1-Dichloroethene mg/kg ND 0.0050 02/04/21 12:030.0021
1,1-Dichloropropene mg/kg ND 0.0050 02/04/21 12:030.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 02/04/21 12:030.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 02/04/21 12:030.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 02/04/21 12:030.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 02/04/21 12:030.0014
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 02/04/21 12:030.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 02/04/21 12:030.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 02/04/21 12:030.0018
1,2-Dichloroethane mg/kg ND 0.0050 02/04/21 12:030.0033
1,2-Dichloropropane mg/kg ND 0.0050 02/04/21 12:030.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 02/04/21 12:030.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 02/04/21 12:030.0016
1,3-Dichloropropane mg/kg ND 0.0050 02/04/21 12:030.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 02/04/21 12:030.0013
2,2-Dichloropropane mg/kg ND 0.0050 02/04/21 12:030.0016
2-Butanone (MEK)mg/kg ND 0.10 02/04/21 12:030.024
2-Chlorotoluene mg/kg ND 0.0050 02/04/21 12:030.0018
2-Hexanone mg/kg ND 0.050 02/04/21 12:030.0048
4-Chlorotoluene mg/kg ND 0.0050 02/04/21 12:030.00088
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 02/04/21 12:030.0048
Acetone mg/kg ND 0.10 02/04/21 12:030.032
Benzene mg/kg ND 0.0050 02/04/21 12:030.0020
Bromobenzene mg/kg ND 0.0050 02/04/21 12:030.0016
Bromochloromethane mg/kg ND 0.0050 02/04/21 12:030.0015
Bromodichloromethane mg/kg ND 0.0050 02/04/21 12:030.0019
Bromoform mg/kg ND 0.0050 02/04/21 12:030.0018
Bromomethane mg/kg ND 0.010 02/04/21 12:030.0079
Carbon tetrachloride mg/kg ND 0.0050 02/04/21 12:030.0019
Chlorobenzene mg/kg ND 0.0050 02/04/21 12:030.00096
Chloroethane mg/kg ND 0.010 02/04/21 12:030.0039
Chloroform mg/kg ND 0.0050 02/04/21 12:030.0030
Chloromethane mg/kg ND 0.010 02/04/21 12:030.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 02/04/21 12:030.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 02/04/21 12:030.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3151170
Associated Lab Samples:92519538001
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 02/04/21 12:030.0028
Dibromomethane mg/kg ND 0.0050 02/04/21 12:030.0011
Dichlorodifluoromethane mg/kg ND 0.010 02/04/21 12:030.0022
Diisopropyl ether mg/kg ND 0.0050 02/04/21 12:030.0014
Ethylbenzene mg/kg ND 0.0050 02/04/21 12:030.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 02/04/21 12:030.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 02/04/21 12:030.0017
m&p-Xylene mg/kg ND 0.010 02/04/21 12:030.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 02/04/21 12:030.0019
Methylene Chloride mg/kg ND 0.020 02/04/21 12:030.014
n-Butylbenzene mg/kg ND 0.0050 02/04/21 12:030.0024
n-Propylbenzene mg/kg ND 0.0050 02/04/21 12:030.0018
Naphthalene mg/kg ND 0.0050 02/04/21 12:030.0026
o-Xylene mg/kg ND 0.0050 02/04/21 12:030.0022
p-Isopropyltoluene mg/kg ND 0.0050 02/04/21 12:030.0025
sec-Butylbenzene mg/kg ND 0.0050 02/04/21 12:030.0022
Styrene mg/kg ND 0.0050 02/04/21 12:030.0013
tert-Butylbenzene mg/kg ND 0.0050 02/04/21 12:030.0018
Tetrachloroethene mg/kg ND 0.0050 02/04/21 12:030.0016
Toluene mg/kg ND 0.0050 02/04/21 12:030.0014
trans-1,2-Dichloroethene mg/kg ND 0.0050 02/04/21 12:030.0018
trans-1,3-Dichloropropene mg/kg ND 0.0050 02/04/21 12:030.0017
Trichloroethene mg/kg ND 0.0050 02/04/21 12:030.0013
Trichlorofluoromethane mg/kg ND 0.0050 02/04/21 12:030.0028
Vinyl acetate mg/kg ND 0.050 02/04/21 12:030.0036
Vinyl chloride mg/kg ND 0.010 02/04/21 12:030.0025
Xylene (Total)mg/kg ND 0.010 02/04/21 12:030.0028
1,2-Dichloroethane-d4 (S)%102 70-130 02/04/21 12:03
4-Bromofluorobenzene (S)%103 69-134 02/04/21 12:03
Toluene-d8 (S)%99 70-130 02/04/21 12:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151171LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.31.2 101 70-130
1,1,1-Trichloroethane mg/kg 1.21.2 99 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.31.2 101 70-130
1,1,2-Trichloroethane mg/kg 1.31.2 100 70-130
1,1-Dichloroethane mg/kg 1.21.2 99 70-130
1,1-Dichloroethene mg/kg 1.41.2 108 70-130
1,1-Dichloropropene mg/kg 1.31.2 102 70-130
1,2,3-Trichlorobenzene mg/kg 1.21.2 96 65-130
1,2,3-Trichloropropane mg/kg 1.31.2 100 70-130
1,2,4-Trichlorobenzene mg/kg 1.31.2 102 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151171LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.21.2 97 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.31.2 104 70-130
1,2-Dibromoethane (EDB)mg/kg 1.31.2 103 70-130
1,2-Dichlorobenzene mg/kg 1.31.2 100 70-130
1,2-Dichloroethane mg/kg 1.21.2 96 63-130
1,2-Dichloropropane mg/kg 1.31.2 101 70-130
1,3,5-Trimethylbenzene mg/kg 1.31.2 100 70-130
1,3-Dichlorobenzene mg/kg 1.21.2 100 70-130
1,3-Dichloropropane mg/kg 1.21.2 100 70-130
1,4-Dichlorobenzene mg/kg 1.21.2 97 70-130
2,2-Dichloropropane mg/kg 1.21.2 99 66-130
2-Butanone (MEK)mg/kg 2.52.5 102 70-130
2-Chlorotoluene mg/kg 1.31.2 104 70-130
2-Hexanone mg/kg 2.52.5 101 70-130
4-Chlorotoluene mg/kg 1.31.2 100 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.52.5 100 70-130
Acetone mg/kg 2.52.5 100 69-130
Benzene mg/kg 1.21.2 97 70-130
Bromobenzene mg/kg 1.31.2 102 70-130
Bromochloromethane mg/kg 1.21.2 98 70-130
Bromodichloromethane mg/kg 1.31.2 101 69-130
Bromoform mg/kg 1.41.2 109 70-130
Bromomethane mg/kg 1.21.2 95 52-130
Carbon tetrachloride mg/kg 1.41.2 109 70-130
Chlorobenzene mg/kg 1.21.2 99 70-130
Chloroethane mg/kg 1.31.2 101 65-130
Chloroform mg/kg 1.21.2 95 70-130
Chloromethane mg/kg 1.11.2 87 55-130
cis-1,2-Dichloroethene mg/kg 1.21.2 99 70-130
cis-1,3-Dichloropropene mg/kg 1.31.2 103 70-130
Dibromochloromethane mg/kg 1.31.2 108 70-130
Dibromomethane mg/kg 1.31.2 105 70-130
Dichlorodifluoromethane mg/kg 1.31.2 102 45-156
Diisopropyl ether mg/kg 1.21.2 95 70-130
Ethylbenzene mg/kg 1.21.2 93 70-130
Hexachloro-1,3-butadiene mg/kg 1.41.2 111 66-130
Isopropylbenzene (Cumene)mg/kg 1.31.2 102 70-130
m&p-Xylene mg/kg 2.52.5 99 70-130
Methyl-tert-butyl ether mg/kg 1.21.2 97 70-130
Methylene Chloride mg/kg 1.11.2 90 65-130
n-Butylbenzene mg/kg 1.31.2 106 67-130
n-Propylbenzene mg/kg 1.31.2 101 70-130
Naphthalene mg/kg 1.31.2 101 70-130
o-Xylene mg/kg 1.21.2 100 70-130
p-Isopropyltoluene mg/kg 1.31.2 102 67-130
sec-Butylbenzene mg/kg 1.31.2 100 69-130
Styrene mg/kg 1.31.2 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151171LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.21.2 95 67-130
Tetrachloroethene mg/kg 1.21.2 95 70-130
Toluene mg/kg 1.21.2 97 70-130
trans-1,2-Dichloroethene mg/kg 1.21.2 98 70-130
trans-1,3-Dichloropropene mg/kg 1.21.2 99 68-130
Trichloroethene mg/kg 1.31.2 101 70-130
Trichlorofluoromethane mg/kg 1.31.2 101 70-130
Vinyl acetate mg/kg 2.82.5 111 70-130
Vinyl chloride mg/kg 1.21.2 93 61-130
Xylene (Total)mg/kg 3.73.8 99 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3151173MATRIX SPIKE SAMPLE:
MSSpike
Result
92519952002
1,1,1,2-Tetrachloroethane mg/kg 0.730.7 104 70-131ND
1,1,1-Trichloroethane mg/kg 0.770.7 110 65-133ND
1,1,2,2-Tetrachloroethane mg/kg 0.720.7 102 66-130ND
1,1,2-Trichloroethane mg/kg 0.750.7 107 66-133ND
1,1-Dichloroethane mg/kg 0.710.7 101 65-130ND
1,1-Dichloroethene mg/kg 0.790.7 112 10-158ND
1,1-Dichloropropene mg/kg 0.790.7 113 68-133ND
1,2,3-Trichlorobenzene mg/kg 0.700.7 99 27-138ND
1,2,3-Trichloropropane mg/kg 0.690.7 99 67-130ND
1,2,4-Trichlorobenzene mg/kg 0.750.7 108 51-134ND
1,2,4-Trimethylbenzene mg/kg 0.750.7 107 63-136ND
1,2-Dibromo-3-chloropropane mg/kg 0.650.7 93 32-130ND
1,2-Dibromoethane (EDB)mg/kg 0.740.7 106 70-130ND
1,2-Dichlorobenzene mg/kg 0.750.7 107 69-130ND
1,2-Dichloroethane mg/kg 0.720.7 103 59-130ND
1,2-Dichloropropane mg/kg 0.760.7 108 70-130ND
1,3,5-Trimethylbenzene mg/kg 0.760.7 108 65-137ND
1,3-Dichlorobenzene mg/kg 0.760.7 109 70-130ND
1,3-Dichloropropane mg/kg 0.710.7 102 70-130ND
1,4-Dichlorobenzene mg/kg 0.730.7 104 68-130ND
2,2-Dichloropropane mg/kg 0.720.7 102 32-130ND
2-Butanone (MEK)mg/kg 1.21.4 88 10-136ND
2-Chlorotoluene mg/kg 0.770.7 110 69-141ND
2-Hexanone mg/kg 1.31.4 92 10-144ND
4-Chlorotoluene mg/kg 0.750.7 107 70-132ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.41.4 98 25-143ND
Acetone mg/kg 1.21.4 83 10-130ND
Benzene mg/kg 0.750.7 106 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3151173MATRIX SPIKE SAMPLE:
MSSpike
Result
92519952002
Bromobenzene mg/kg 0.730.7 105 70-130ND
Bromochloromethane mg/kg 0.700.7 100 69-134ND
Bromodichloromethane mg/kg 0.730.7 105 64-130ND
Bromoform mg/kg 0.680.7 96 62-130ND
Bromomethane mg/kg 0.590.7 84 20-176ND
Carbon tetrachloride mg/kg 0.800.7 115 65-140ND
Chlorobenzene mg/kg 0.740.7 106 70-130ND
Chloroethane mg/kg 0.190.7 28 10-130ND
Chloroform mg/kg 0.700.7 100 63-130ND
Chloromethane mg/kg 0.690.7 98 58-130ND
cis-1,2-Dichloroethene mg/kg 0.730.7 104 66-130ND
cis-1,3-Dichloropropene mg/kg 0.730.7 104 67-130ND
Dibromochloromethane mg/kg 0.740.7 106 67-130ND
Dibromomethane mg/kg 0.750.7 107 63-131ND
Dichlorodifluoromethane mg/kg 0.760.7 108 44-180ND
Diisopropyl ether mg/kg 0.680.7 96 63-130ND
Ethylbenzene mg/kg 0.720.7 103 66-130ND
Hexachloro-1,3-butadiene mg/kg 0.860.7 123 64-150ND
Isopropylbenzene (Cumene)mg/kg 0.790.7 112 69-135ND
m&p-Xylene mg/kg 1.51.4 107 60-133ND
Methyl-tert-butyl ether mg/kg 0.690.7 99 65-130ND
Methylene Chloride mg/kg 0.660.7 94 61-130ND
n-Butylbenzene mg/kg 0.810.7 116 65-140ND
n-Propylbenzene mg/kg 0.770.7 109 67-140ND
Naphthalene mg/kg 0.750.7 106 15-145ND
o-Xylene mg/kg 0.760.7 109 66-133ND
p-Isopropyltoluene mg/kg 0.810.7 115 56-147ND
sec-Butylbenzene mg/kg 0.800.7 114 65-139ND
Styrene mg/kg 0.780.7 111 70-132ND
tert-Butylbenzene mg/kg 0.730.7 104 62-135ND
Tetrachloroethene mg/kg 0.730.7 104 70-135ND
Toluene mg/kg 0.760.7 109 67-130ND
trans-1,2-Dichloroethene mg/kg 0.720.7 103 69-130ND
trans-1,3-Dichloropropene mg/kg 0.890.7 126 62-130ND
Trichloroethene mg/kg 0.790.7 113 70-135ND
Trichlorofluoromethane mg/kg 0.260.7 38 10-130ND
Vinyl acetate mg/kg 1.51.4 109 53-130ND
Vinyl chloride mg/kg 0.790.7 112 61-148ND
Xylene (Total)mg/kg 2.32.1 108 63-132ND
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519952001
3151172SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND 30ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519952001
3151172SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%101102
4-Bromofluorobenzene (S)%99100
Toluene-d8 (S)%9999
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
596955
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519538001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3147934
Associated Lab Samples:92519538001
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 02/02/21 15:290.076
1,2-Dichlorobenzene mg/kg ND 0.33 02/02/21 15:290.071
1,3-Dichlorobenzene mg/kg ND 0.33 02/02/21 15:290.074
1,4-Dichlorobenzene mg/kg ND 0.33 02/02/21 15:290.073
1-Methylnaphthalene mg/kg ND 0.33 02/02/21 15:290.088
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 02/02/21 15:290.092
2,4,5-Trichlorophenol mg/kg ND 0.33 02/02/21 15:290.086
2,4,6-Trichlorophenol mg/kg ND 0.33 02/02/21 15:290.083
2,4-Dichlorophenol mg/kg ND 0.33 02/02/21 15:290.11
2,4-Dimethylphenol mg/kg ND 0.33 02/02/21 15:290.082
2,4-Dinitrophenol mg/kg ND 1.6 02/02/21 15:291.1
2,4-Dinitrotoluene mg/kg ND 0.33 02/02/21 15:290.087
2,6-Dinitrotoluene mg/kg ND 0.33 02/02/21 15:290.086
2-Chloronaphthalene mg/kg ND 0.33 02/02/21 15:290.074
2-Chlorophenol mg/kg ND 0.33 02/02/21 15:290.077
2-Methylnaphthalene mg/kg ND 0.33 02/02/21 15:290.084
2-Methylphenol(o-Cresol)mg/kg ND 0.33 02/02/21 15:290.073
2-Nitroaniline mg/kg ND 1.6 02/02/21 15:290.17
2-Nitrophenol mg/kg ND 0.33 02/02/21 15:290.10
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 02/02/21 15:290.083
3,3'-Dichlorobenzidine mg/kg ND 0.66 02/02/21 15:290.23
3-Nitroaniline mg/kg ND 1.6 IL02/02/21 15:290.18
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 02/02/21 15:290.53
4-Bromophenylphenyl ether mg/kg ND 0.33 02/02/21 15:290.087
4-Chloro-3-methylphenol mg/kg ND 0.66 02/02/21 15:290.20
4-Chloroaniline mg/kg ND 0.66 02/02/21 15:290.20
4-Chlorophenylphenyl ether mg/kg ND 0.33 02/02/21 15:290.086
4-Nitroaniline mg/kg ND 0.66 02/02/21 15:290.16
4-Nitrophenol mg/kg ND 1.6 02/02/21 15:290.53
Acenaphthene mg/kg ND 0.33 02/02/21 15:290.085
Acenaphthylene mg/kg ND 0.33 02/02/21 15:290.078
Aniline mg/kg ND 0.33 02/02/21 15:290.074
Anthracene mg/kg ND 0.33 02/02/21 15:290.086
Benzo(a)anthracene mg/kg ND 0.33 02/02/21 15:290.10
Benzo(a)pyrene mg/kg ND 0.33 02/02/21 15:290.14
Benzo(b)fluoranthene mg/kg ND 0.33 02/02/21 15:290.13
Benzo(g,h,i)perylene mg/kg ND 0.33 02/02/21 15:290.13
Benzo(k)fluoranthene mg/kg ND 0.33 02/02/21 15:290.14
Benzoic Acid mg/kg ND 1.6 02/02/21 15:290.36
Benzyl alcohol mg/kg ND 0.66 02/02/21 15:290.18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3147934
Associated Lab Samples:92519538001
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane mg/kg ND 0.33 02/02/21 15:290.088
bis(2-Chloroethyl) ether mg/kg ND 0.33 02/02/21 15:290.070
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 02/02/21 15:290.11
Butylbenzylphthalate mg/kg ND 0.33 02/02/21 15:290.088
Chrysene mg/kg ND 0.33 02/02/21 15:290.096
Di-n-butylphthalate mg/kg ND 0.33 02/02/21 15:290.081
Di-n-octylphthalate mg/kg ND 0.33 02/02/21 15:290.19
Dibenz(a,h)anthracene mg/kg ND 0.33 02/02/21 15:290.13
Dibenzofuran mg/kg ND 0.33 02/02/21 15:290.082
Diethylphthalate mg/kg ND 0.33 02/02/21 15:290.072
Dimethylphthalate mg/kg ND 0.33 02/02/21 15:290.075
Fluoranthene mg/kg ND 0.33 02/02/21 15:290.10
Fluorene mg/kg ND 0.33 02/02/21 15:290.088
Hexachloro-1,3-butadiene mg/kg ND 0.33 02/02/21 15:290.080
Hexachlorobenzene mg/kg ND 0.33 02/02/21 15:290.084
Hexachlorocyclopentadiene mg/kg ND 0.33 02/02/21 15:290.13
Hexachloroethane mg/kg ND 0.33 02/02/21 15:290.075
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 02/02/21 15:290.15
Isophorone mg/kg ND 0.33 02/02/21 15:290.072
N-Nitroso-di-n-propylamine mg/kg ND 0.33 02/02/21 15:290.092
N-Nitrosodimethylamine mg/kg ND 0.33 02/02/21 15:290.093
N-Nitrosodiphenylamine mg/kg ND 0.33 02/02/21 15:290.084
Naphthalene mg/kg ND 0.33 02/02/21 15:290.079
Nitrobenzene mg/kg ND 0.33 02/02/21 15:290.079
Pentachlorophenol mg/kg ND 0.66 02/02/21 15:290.15
Phenanthrene mg/kg ND 0.33 02/02/21 15:290.083
Phenol mg/kg ND 0.33 02/02/21 15:290.079
Pyrene mg/kg ND 0.33 02/02/21 15:290.091
Pyridine mg/kg ND 0.33 02/02/21 15:290.084
2,4,6-Tribromophenol (S)%74 18-130 02/02/21 15:29
2-Fluorobiphenyl (S)%59 19-130 02/02/21 15:29
2-Fluorophenol (S)%65 18-130 02/02/21 15:29
Nitrobenzene-d5 (S)%67 21-130 02/02/21 15:29
Phenol-d6 (S)%66 18-130 02/02/21 15:29
Terphenyl-d14 (S)%93 15-130 02/02/21 15:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3147935LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.31.7 79 47-130
1,2-Dichlorobenzene mg/kg 1.31.7 76 49-130
1,3-Dichlorobenzene mg/kg 1.21.7 73 48-130
1,4-Dichlorobenzene mg/kg 1.31.7 76 49-130
1-Methylnaphthalene mg/kg 1.21.7 74 54-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3147935LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.31.7 78 38-130
2,4,5-Trichlorophenol mg/kg 1.41.7 84 49-130
2,4,6-Trichlorophenol mg/kg 1.41.7 82 50-130
2,4-Dichlorophenol mg/kg 1.41.7 83 51-130
2,4-Dimethylphenol mg/kg 1.41.7 86 53-130
2,4-Dinitrophenol mg/kg 6.48.3 77 39-130
2,4-Dinitrotoluene mg/kg 1.31.7 78 53-130
2,6-Dinitrotoluene mg/kg 1.31.7 79 55-130
2-Chloronaphthalene mg/kg 1.21.7 75 48-130
2-Chlorophenol mg/kg 1.31.7 78 54-130
2-Methylnaphthalene mg/kg 1.31.7 76 57-130
2-Methylphenol(o-Cresol)mg/kg 1.31.7 78 50-130
2-Nitroaniline mg/kg 2.53.3 74 49-130
2-Nitrophenol mg/kg 1.31.7 78 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.41.7 86 50-130
3,3'-Dichlorobenzidine mg/kg 2.03.3 62 47-130
3-Nitroaniline mg/kg 1.7 IL3.3 50 45-130
4,6-Dinitro-2-methylphenol mg/kg 2.83.3 83 50-142
4-Bromophenylphenyl ether mg/kg 1.41.7 87 55-130
4-Chloro-3-methylphenol mg/kg 2.93.3 87 52-130
4-Chloroaniline mg/kg 2.23.3 65 49-130
4-Chlorophenylphenyl ether mg/kg 1.41.7 82 53-130
4-Nitroaniline mg/kg 2.03.3 61 51-130
4-Nitrophenol mg/kg 7.38.3 88 40-130
Acenaphthene mg/kg 1.21.7 73 56-130
Acenaphthylene mg/kg 1.21.7 73 58-130
Aniline mg/kg 1.01.7 63 44-130
Anthracene mg/kg 1.11.7 68 60-130
Benzo(a)anthracene mg/kg 1.31.7 79 59-130
Benzo(a)pyrene mg/kg 1.31.7 79 57-130
Benzo(b)fluoranthene mg/kg 1.31.7 81 54-130
Benzo(g,h,i)perylene mg/kg 1.31.7 75 59-130
Benzo(k)fluoranthene mg/kg 1.31.7 80 54-130
Benzoic Acid mg/kg 4.68.3 55 19-130
Benzyl alcohol mg/kg 2.63.3 80 50-130
bis(2-Chloroethoxy)methane mg/kg 1.21.7 74 55-130
bis(2-Chloroethyl) ether mg/kg 1.31.7 77 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.31.7 78 58-130
Butylbenzylphthalate mg/kg 1.41.7 85 46-138
Chrysene mg/kg 1.31.7 76 57-130
Di-n-butylphthalate mg/kg 1.31.7 77 57-130
Di-n-octylphthalate mg/kg 1.31.7 76 57-130
Dibenz(a,h)anthracene mg/kg 1.31.7 76 60-130
Dibenzofuran mg/kg 1.31.7 76 54-130
Diethylphthalate mg/kg 1.31.7 78 55-130
Dimethylphthalate mg/kg 1.31.7 79 57-130
Fluoranthene mg/kg 1.21.7 72 57-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3147935LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.31.7 76 56-130
Hexachloro-1,3-butadiene mg/kg 1.41.7 86 41-130
Hexachlorobenzene mg/kg 1.41.7 86 53-130
Hexachlorocyclopentadiene mg/kg 1.21.7 72 23-130
Hexachloroethane mg/kg 1.31.7 78 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.31.7 78 61-130
Isophorone mg/kg 1.31.7 81 49-130
N-Nitroso-di-n-propylamine mg/kg 1.41.7 86 52-130
N-Nitrosodimethylamine mg/kg 1.21.7 73 45-130
N-Nitrosodiphenylamine mg/kg 1.31.7 80 56-130
Naphthalene mg/kg 1.21.7 72 56-130
Nitrobenzene mg/kg 1.31.7 80 50-130
Pentachlorophenol mg/kg 2.83.3 85 33-130
Phenanthrene mg/kg 1.31.7 76 60-130
Phenol mg/kg 1.41.7 84 54-130
Pyrene mg/kg 1.51.7 89 61-130
Pyridine mg/kg 0.921.7 56 35-130
2,4,6-Tribromophenol (S)%93 18-130
2-Fluorobiphenyl (S)%76 19-130
2-Fluorophenol (S)%76 18-130
Nitrobenzene-d5 (S)%79 21-130
Phenol-d6 (S)%78 18-130
Terphenyl-d14 (S)%111 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519391001
3147937SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg ND 30<89.3 ug/kg
1,2-Dichlorobenzene mg/kg ND 30<84.3 ug/kg
1,3-Dichlorobenzene mg/kg ND 30<87.7 ug/kg
1,4-Dichlorobenzene mg/kg ND 30<85.7 ug/kg
1-Methylnaphthalene mg/kg ND 30<104 ug/kg
2,2'-Oxybis(1-chloropropane)mg/kg ND 30<108 ug/kg
2,4,5-Trichlorophenol mg/kg ND 30<101 ug/kg
2,4,6-Trichlorophenol mg/kg ND 30<97.9 ug/kg
2,4-Dichlorophenol mg/kg ND 30<129 ug/kg
2,4-Dimethylphenol mg/kg ND 30<97.1 ug/kg
2,4-Dinitrophenol mg/kg ND 30<1240 ug/kg
2,4-Dinitrotoluene mg/kg ND 30<103 ug/kg
2,6-Dinitrotoluene mg/kg ND 30<102 ug/kg
2-Chloronaphthalene mg/kg ND 30<86.8 ug/kg
2-Chlorophenol mg/kg ND 30<90.7 ug/kg
2-Methylnaphthalene mg/kg ND 30<99.2 ug/kg
2-Methylphenol(o-Cresol)mg/kg ND 30<86.3 ug/kg
2-Nitroaniline mg/kg ND 30<196 ug/kg
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519391001
3147937SAMPLE DUPLICATE:
2-Nitrophenol mg/kg ND 30<120 ug/kg
3&4-Methylphenol(m&p Cresol)mg/kg ND 30<98.0 ug/kg
3,3'-Dichlorobenzidine mg/kg ND 30<272 ug/kg
3-Nitroaniline mg/kg ND IL30<207 ug/kg
4,6-Dinitro-2-methylphenol mg/kg ND 30<628 ug/kg
4-Bromophenylphenyl ether mg/kg ND 30<102 ug/kg
4-Chloro-3-methylphenol mg/kg ND 30<237 ug/kg
4-Chloroaniline mg/kg ND 30<238 ug/kg
4-Chlorophenylphenyl ether mg/kg ND 30<101 ug/kg
4-Nitroaniline mg/kg ND 30<192 ug/kg
4-Nitrophenol mg/kg ND 30<621 ug/kg
Acenaphthene mg/kg ND 30<100 ug/kg
Acenaphthylene mg/kg ND 30<92.2 ug/kg
Aniline mg/kg ND 30<87.5 ug/kg
Anthracene mg/kg ND 30<101 ug/kg
Benzo(a)anthracene mg/kg ND 30<124 ug/kg
Benzo(a)pyrene mg/kg ND 30<169 ug/kg
Benzo(b)fluoranthene mg/kg ND 30<157 ug/kg
Benzo(g,h,i)perylene mg/kg ND 30<152 ug/kg
Benzo(k)fluoranthene mg/kg ND 30<164 ug/kg
Benzoic Acid mg/kg ND 30<420 ug/kg
Benzyl alcohol mg/kg ND 30<207 ug/kg
bis(2-Chloroethoxy)methane mg/kg ND 30<104 ug/kg
bis(2-Chloroethyl) ether mg/kg ND 30<82.8 ug/kg
bis(2-Ethylhexyl)phthalate mg/kg ND 30<128 ug/kg
Butylbenzylphthalate mg/kg ND 30<104 ug/kg
Chrysene mg/kg ND 30<113 ug/kg
Di-n-butylphthalate mg/kg ND 30<96.1 ug/kg
Di-n-octylphthalate mg/kg ND 30<222 ug/kg
Dibenz(a,h)anthracene mg/kg ND 30<156 ug/kg
Dibenzofuran mg/kg ND 30<97.4 ug/kg
Diethylphthalate mg/kg ND 30<84.5 ug/kg
Dimethylphthalate mg/kg ND 30<88.1 ug/kg
Fluoranthene mg/kg ND 30<118 ug/kg
Fluorene mg/kg ND 30<104 ug/kg
Hexachloro-1,3-butadiene mg/kg ND 30<94.7 ug/kg
Hexachlorobenzene mg/kg ND 30<98.9 ug/kg
Hexachlorocyclopentadiene mg/kg ND 30<156 ug/kg
Hexachloroethane mg/kg ND 30<88.8 ug/kg
Indeno(1,2,3-cd)pyrene mg/kg ND 30<178 ug/kg
Isophorone mg/kg ND 30<84.7 ug/kg
N-Nitroso-di-n-propylamine mg/kg ND 30<109 ug/kg
N-Nitrosodimethylamine mg/kg ND 30<110 ug/kg
N-Nitrosodiphenylamine mg/kg ND 30<99.4 ug/kg
Naphthalene mg/kg ND 30<93.3 ug/kg
Nitrobenzene mg/kg ND 30<93.0 ug/kg
Pentachlorophenol mg/kg ND 30<178 ug/kg
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519391001
3147937SAMPLE DUPLICATE:
Phenanthrene mg/kg ND 30<98.1 ug/kg
Phenol mg/kg ND 30<93.0 ug/kg
Pyrene mg/kg ND 30<107 ug/kg
Pyridine mg/kg ND 30<98.6 ug/kg
2,4,6-Tribromophenol (S)%7175
2-Fluorobiphenyl (S)%5760
2-Fluorophenol (S)%6058
Nitrobenzene-d5 (S)%6464
Phenol-d6 (S)%6059
Terphenyl-d14 (S)%7872
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
596720
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519538001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519451002
3147008SAMPLE DUPLICATE:
Percent Moisture %19.1 N2152516.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519381005
3147277SAMPLE DUPLICATE:
Percent Moisture %10.4 N222510.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1616612
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92519538001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3619999-1
Associated Lab Samples:92519538001
Matrix:Solid
AnalyzedMDL
Total Solids %0.00300 02/05/21 10:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3619999-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1313697-01
R3619999-3SAMPLE DUPLICATE:
Total Solids %78.2 0.347 1078.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1618092
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92519538001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3620707-1
Associated Lab Samples:92519538001
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 02/08/21 20:420.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3620707-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.6310.0 96.3 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3620707-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1312546-01
R3620707-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg ML23.4 52.0 75.0-12546.9 10.1 2023.4ND 12.2 11.0
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3620707-7MATRIX SPIKE SAMPLE:
MSSpike
Result
L1312546-01
Chromium, Hexavalent mg/kg 806906 88.9 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1312354-01
R3620707-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 11.5 13.3 2013.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1313701-03
R3620707-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 32
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 32
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92519538
7th & Caswell Tank Pull
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92519538001 597002 597100T-4 EPA 3050B EPA 6010D
92519538001 597289 597323T-4 EPA 7471B EPA 7471B
92519538001 596955 597166T-4 EPA 3546 EPA 8270E
92519538001 597618 597634T-4 EPA 5035A/5030B EPA 8260D
92519538001 596720T-4 SW-846
92519538001 1616612 1616612T-4 SM 2540 G SM 2540G
92519538001 1618092 1618092T-4 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/09/2021 02:14 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 32
Page 30 of 32
Page 31 of 32
Page 32 of 32
#=CL#
February 08, 2021
LIMS USE: FR - CHRIS ORRELL
LIMS OBJECT ID: 92519759
92519759
Project:
Pace Project No.:
RE:
Chris Orrell
ECS Southeast, LLP
1900 Center Park Dr Suite D
9809 Aviary Hill Way, Charlott
Charlotte, NC 28217
7th & Caswell Tank Pull
Dear Chris Orrell:
Enclosed are the analytical results for sample(s) received by the laboratory on February 02, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
A revised report is being submitted on 2/8/21 to report MDLs and J values, per client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:Jenna Dew, ECS Southeast
ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 33
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Lab ID Sample ID Matrix Date Collected Date Received
92519759001 T-5 Solid 02/01/21 11:30 02/02/21 14:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 33
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92519759001 T-5 EPA 6010D 7 PASI-ASH1
EPA 7471B 1 PASI-ASOO
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Sample:T-5 Lab ID:92519759001 Collected:02/01/21 11:30 Received:02/02/21 14:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 1.9J mg/kg 02/05/21 03:38 7440-38-202/03/21 15:302.5 0.51 1
Barium 12.4 mg/kg 02/05/21 03:38 7440-39-302/03/21 15:301.0 0.25 1
Cadmium 0.16 mg/kg 02/05/21 03:38 7440-43-902/03/21 15:300.10 0.051 1
Chromium 17.5 mg/kg 02/05/21 03:38 7440-47-302/03/21 15:300.51 0.25 1
Lead 9.1 mg/kg 02/05/21 03:38 7439-92-102/03/21 15:301.0 0.25 1
Selenium ND mg/kg 02/05/21 03:38 7782-49-202/03/21 15:301.0 0.51 1
Silver ND mg/kg 02/05/21 03:38 7440-22-402/03/21 15:300.51 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.024 mg/kg 02/04/21 13:15 7439-97-602/03/21 12:450.0032 0.0024 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 02/04/21 14:24 83-32-902/03/21 21:460.45 0.11 1
Acenaphthylene ND mg/kg 02/04/21 14:24 208-96-802/03/21 21:460.45 0.11 1
Aniline ND mg/kg 02/04/21 14:24 62-53-302/03/21 21:460.45 0.10 1
Anthracene ND mg/kg 02/04/21 14:24 120-12-702/03/21 21:460.45 0.12 1
Benzo(a)anthracene ND mg/kg 02/04/21 14:24 56-55-302/03/21 21:460.45 0.14 1
Benzo(a)pyrene ND mg/kg 02/04/21 14:24 50-32-802/03/21 21:460.45 0.19 1
Benzo(b)fluoranthene ND mg/kg 02/04/21 14:24 205-99-202/03/21 21:460.45 0.18 1
Benzo(g,h,i)perylene ND mg/kg 02/04/21 14:24 191-24-202/03/21 21:460.45 0.17 1
Benzo(k)fluoranthene ND mg/kg 02/04/21 14:24 207-08-902/03/21 21:460.45 0.19 1
Benzoic Acid ND mg/kg 02/04/21 14:24 65-85-002/03/21 21:462.2 0.48 1
Benzyl alcohol ND mg/kg 02/04/21 14:24 100-51-602/03/21 21:460.89 0.24 1
4-Bromophenylphenyl ether ND mg/kg 02/04/21 14:24 101-55-302/03/21 21:460.45 0.12 1
Butylbenzylphthalate ND mg/kg 02/04/21 14:24 85-68-702/03/21 21:460.45 0.12 1
4-Chloro-3-methylphenol ND mg/kg 02/04/21 14:24 59-50-702/03/21 21:460.89 0.27 1
4-Chloroaniline ND mg/kg 02/04/21 14:24 106-47-802/03/21 21:460.89 0.27 1
bis(2-Chloroethoxy)methane ND mg/kg 02/04/21 14:24 111-91-102/03/21 21:460.45 0.12 1
bis(2-Chloroethyl) ether ND mg/kg 02/04/21 14:24 111-44-402/03/21 21:460.45 0.095 1
2-Chloronaphthalene ND mg/kg 02/04/21 14:24 91-58-702/03/21 21:460.45 0.099 1
2-Chlorophenol ND mg/kg 02/04/21 14:24 95-57-802/03/21 21:460.45 0.10 1
4-Chlorophenylphenyl ether ND mg/kg 02/04/21 14:24 7005-72-302/03/21 21:460.45 0.12 1
Chrysene ND mg/kg 02/04/21 14:24 218-01-902/03/21 21:460.45 0.13 1
Dibenz(a,h)anthracene ND mg/kg 02/04/21 14:24 53-70-302/03/21 21:460.45 0.18 1
Dibenzofuran ND mg/kg 02/04/21 14:24 132-64-902/03/21 21:460.45 0.11 1
1,2-Dichlorobenzene ND mg/kg 02/04/21 14:24 95-50-102/03/21 21:460.45 0.097 1
1,3-Dichlorobenzene ND mg/kg 02/04/21 14:24 541-73-102/03/21 21:460.45 0.10 1
1,4-Dichlorobenzene ND mg/kg 02/04/21 14:24 106-46-702/03/21 21:460.45 0.098 1
3,3'-Dichlorobenzidine ND mg/kg 02/04/21 14:24 91-94-102/03/21 21:460.89 0.31 1
2,4-Dichlorophenol ND mg/kg 02/04/21 14:24 120-83-202/03/21 21:460.45 0.15 1
Diethylphthalate ND mg/kg 02/04/21 14:24 84-66-202/03/21 21:460.45 0.097 1
2,4-Dimethylphenol ND mg/kg 02/04/21 14:24 105-67-902/03/21 21:460.45 0.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Sample:T-5 Lab ID:92519759001 Collected:02/01/21 11:30 Received:02/02/21 14:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND mg/kg 02/04/21 14:24 131-11-302/03/21 21:460.45 0.10 1
Di-n-butylphthalate ND mg/kg 02/04/21 14:24 84-74-202/03/21 21:460.45 0.11 1
4,6-Dinitro-2-methylphenol ND mg/kg 02/04/21 14:24 534-52-102/03/21 21:460.89 0.72 1
2,4-Dinitrophenol ND mg/kg 02/04/21 14:24 51-28-502/03/21 21:462.2 1.4 1
2,4-Dinitrotoluene ND mg/kg 02/04/21 14:24 121-14-202/03/21 21:460.45 0.12 1
2,6-Dinitrotoluene ND mg/kg 02/04/21 14:24 606-20-202/03/21 21:460.45 0.12 1
Di-n-octylphthalate ND mg/kg 02/04/21 14:24 117-84-002/03/21 21:460.45 0.25 1
bis(2-Ethylhexyl)phthalate ND mg/kg 02/04/21 14:24 117-81-702/03/21 21:460.45 0.15 1
Fluoranthene ND mg/kg 02/04/21 14:24 206-44-002/03/21 21:460.45 0.13 1
Fluorene ND mg/kg 02/04/21 14:24 86-73-702/03/21 21:460.45 0.12 1
Hexachloro-1,3-butadiene ND mg/kg 02/04/21 14:24 87-68-302/03/21 21:460.45 0.11 1
Hexachlorobenzene ND mg/kg 02/04/21 14:24 118-74-102/03/21 21:460.45 0.11 1
Hexachlorocyclopentadiene ND mg/kg 02/04/21 14:24 77-47-402/03/21 21:460.45 0.18 1
Hexachloroethane ND mg/kg 02/04/21 14:24 67-72-102/03/21 21:460.45 0.10 1
Indeno(1,2,3-cd)pyrene ND mg/kg 02/04/21 14:24 193-39-502/03/21 21:460.45 0.20 1
Isophorone ND mg/kg 02/04/21 14:24 78-59-102/03/21 21:460.45 0.097 1
1-Methylnaphthalene ND mg/kg 02/04/21 14:24 90-12-002/03/21 21:460.45 0.12 1
2-Methylnaphthalene ND mg/kg 02/04/21 14:24 91-57-602/03/21 21:460.45 0.11 1
2-Methylphenol(o-Cresol)ND mg/kg 02/04/21 14:24 95-48-702/03/21 21:460.45 0.099 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 02/04/21 14:24 15831-10-402/03/21 21:460.45 0.11 1
Naphthalene ND mg/kg 02/04/21 14:24 91-20-302/03/21 21:460.45 0.11 1
2-Nitroaniline ND mg/kg 02/04/21 14:24 88-74-402/03/21 21:462.2 0.22 1
3-Nitroaniline ND mg/kg 02/04/21 14:24 99-09-2 IL02/03/21 21:462.2 0.24 1
4-Nitroaniline ND mg/kg 02/04/21 14:24 100-01-602/03/21 21:460.89 0.22 1
Nitrobenzene ND mg/kg 02/04/21 14:24 98-95-302/03/21 21:460.45 0.11 1
2-Nitrophenol ND mg/kg 02/04/21 14:24 88-75-502/03/21 21:460.45 0.14 1
4-Nitrophenol ND mg/kg 02/04/21 14:24 100-02-702/03/21 21:462.2 0.71 1
N-Nitrosodimethylamine ND mg/kg 02/04/21 14:24 62-75-902/03/21 21:460.45 0.13 1
N-Nitroso-di-n-propylamine ND mg/kg 02/04/21 14:24 621-64-702/03/21 21:460.45 0.13 1
N-Nitrosodiphenylamine ND mg/kg 02/04/21 14:24 86-30-602/03/21 21:460.45 0.11 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 02/04/21 14:24 108-60-102/03/21 21:460.45 0.12 1
Pentachlorophenol ND mg/kg 02/04/21 14:24 87-86-502/03/21 21:460.89 0.20 1
Phenanthrene ND mg/kg 02/04/21 14:24 85-01-802/03/21 21:460.45 0.11 1
Phenol ND mg/kg 02/04/21 14:24 108-95-202/03/21 21:460.45 0.11 1
Pyrene ND mg/kg 02/04/21 14:24 129-00-002/03/21 21:460.45 0.12 1
Pyridine ND mg/kg 02/04/21 14:24 110-86-102/03/21 21:460.45 0.11 1
1,2,4-Trichlorobenzene ND mg/kg 02/04/21 14:24 120-82-102/03/21 21:460.45 0.10 1
2,4,5-Trichlorophenol ND mg/kg 02/04/21 14:24 95-95-402/03/21 21:460.45 0.12 1
2,4,6-Trichlorophenol ND mg/kg 02/04/21 14:24 88-06-202/03/21 21:460.45 0.11 1
Surrogates
Nitrobenzene-d5 (S)76 %02/04/21 14:24 4165-60-002/03/21 21:4621-130 1
2-Fluorobiphenyl (S)68 %02/04/21 14:24 321-60-802/03/21 21:4619-130 1
Terphenyl-d14 (S)99 %02/04/21 14:24 1718-51-002/03/21 21:4615-130 1
Phenol-d6 (S)63 %02/04/21 14:24 13127-88-302/03/21 21:4618-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Sample:T-5 Lab ID:92519759001 Collected:02/01/21 11:30 Received:02/02/21 14:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)61 %02/04/21 14:24 367-12-402/03/21 21:4618-130 1
2,4,6-Tribromophenol (S)90 %02/04/21 14:24 118-79-602/03/21 21:4618-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 02/04/21 18:23 67-64-102/04/21 10:170.16 0.052 1
Benzene ND mg/kg 02/04/21 18:23 71-43-202/04/21 10:170.0082 0.0032 1
Bromobenzene ND mg/kg 02/04/21 18:23 108-86-102/04/21 10:170.0082 0.0027 1
Bromochloromethane ND mg/kg 02/04/21 18:23 74-97-502/04/21 10:170.0082 0.0024 1
Bromodichloromethane ND mg/kg 02/04/21 18:23 75-27-402/04/21 10:170.0082 0.0032 1
Bromoform ND mg/kg 02/04/21 18:23 75-25-202/04/21 10:170.0082 0.0029 1
Bromomethane ND mg/kg 02/04/21 18:23 74-83-902/04/21 10:170.016 0.013 1
2-Butanone (MEK)ND mg/kg 02/04/21 18:23 78-93-302/04/21 10:170.16 0.039 1
n-Butylbenzene ND mg/kg 02/04/21 18:23 104-51-802/04/21 10:170.0082 0.0039 1
sec-Butylbenzene ND mg/kg 02/04/21 18:23 135-98-802/04/21 10:170.0082 0.0036 1
tert-Butylbenzene ND mg/kg 02/04/21 18:23 98-06-602/04/21 10:170.0082 0.0029 1
Carbon tetrachloride ND mg/kg 02/04/21 18:23 56-23-502/04/21 10:170.0082 0.0031 1
Chlorobenzene ND mg/kg 02/04/21 18:23 108-90-702/04/21 10:170.0082 0.0016 1
Chloroethane ND mg/kg 02/04/21 18:23 75-00-302/04/21 10:170.016 0.0063 1
Chloroform ND mg/kg 02/04/21 18:23 67-66-302/04/21 10:170.0082 0.0050 1
Chloromethane ND mg/kg 02/04/21 18:23 74-87-302/04/21 10:170.016 0.0069 1
2-Chlorotoluene ND mg/kg 02/04/21 18:23 95-49-802/04/21 10:170.0082 0.0029 1
4-Chlorotoluene ND mg/kg 02/04/21 18:23 106-43-402/04/21 10:170.0082 0.0014 1
1,2-Dibromo-3-chloropropane ND mg/kg 02/04/21 18:23 96-12-802/04/21 10:170.0082 0.0032 1
Dibromochloromethane ND mg/kg 02/04/21 18:23 124-48-102/04/21 10:170.0082 0.0046 1
1,2-Dibromoethane (EDB)ND mg/kg 02/04/21 18:23 106-93-402/04/21 10:170.0082 0.0036 1
Dibromomethane ND mg/kg 02/04/21 18:23 74-95-302/04/21 10:170.0082 0.0017 1
1,2-Dichlorobenzene ND mg/kg 02/04/21 18:23 95-50-102/04/21 10:170.0082 0.0029 1
1,3-Dichlorobenzene ND mg/kg 02/04/21 18:23 541-73-102/04/21 10:170.0082 0.0025 1
1,4-Dichlorobenzene ND mg/kg 02/04/21 18:23 106-46-702/04/21 10:170.0082 0.0021 1
Dichlorodifluoromethane ND mg/kg 02/04/21 18:23 75-71-802/04/21 10:170.016 0.0035 1
1,1-Dichloroethane ND mg/kg 02/04/21 18:23 75-34-302/04/21 10:170.0082 0.0034 1
1,2-Dichloroethane ND mg/kg 02/04/21 18:23 107-06-202/04/21 10:170.0082 0.0054 1
1,1-Dichloroethene ND mg/kg 02/04/21 18:23 75-35-402/04/21 10:170.0082 0.0034 1
cis-1,2-Dichloroethene ND mg/kg 02/04/21 18:23 156-59-202/04/21 10:170.0082 0.0028 1
trans-1,2-Dichloroethene ND mg/kg 02/04/21 18:23 156-60-502/04/21 10:170.0082 0.0029 1
1,2-Dichloropropane ND mg/kg 02/04/21 18:23 78-87-502/04/21 10:170.0082 0.0024 1
1,3-Dichloropropane ND mg/kg 02/04/21 18:23 142-28-902/04/21 10:170.0082 0.0025 1
2,2-Dichloropropane ND mg/kg 02/04/21 18:23 594-20-702/04/21 10:170.0082 0.0027 1
1,1-Dichloropropene ND mg/kg 02/04/21 18:23 563-58-602/04/21 10:170.0082 0.0039 1
cis-1,3-Dichloropropene ND mg/kg 02/04/21 18:23 10061-01-502/04/21 10:170.0082 0.0022 1
trans-1,3-Dichloropropene ND mg/kg 02/04/21 18:23 10061-02-602/04/21 10:170.0082 0.0028 1
Diisopropyl ether ND mg/kg 02/04/21 18:23 108-20-302/04/21 10:170.0082 0.0022 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Sample:T-5 Lab ID:92519759001 Collected:02/01/21 11:30 Received:02/02/21 14:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND mg/kg 02/04/21 18:23 100-41-402/04/21 10:170.0082 0.0038 1
Hexachloro-1,3-butadiene ND mg/kg 02/04/21 18:23 87-68-302/04/21 10:170.016 0.013 1
2-Hexanone ND mg/kg 02/04/21 18:23 591-78-602/04/21 10:170.082 0.0079 1
Isopropylbenzene (Cumene)ND mg/kg 02/04/21 18:23 98-82-802/04/21 10:170.0082 0.0028 1
p-Isopropyltoluene ND mg/kg 02/04/21 18:23 99-87-602/04/21 10:170.0082 0.0040 1
Methylene Chloride ND mg/kg 02/04/21 18:23 75-09-202/04/21 10:170.033 0.022 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 02/04/21 18:23 108-10-102/04/21 10:170.082 0.0079 1
Methyl-tert-butyl ether ND mg/kg 02/04/21 18:23 1634-04-402/04/21 10:170.0082 0.0031 1
Naphthalene ND mg/kg 02/04/21 18:23 91-20-302/04/21 10:170.0082 0.0043 1
n-Propylbenzene ND mg/kg 02/04/21 18:23 103-65-102/04/21 10:170.0082 0.0029 1
Styrene ND mg/kg 02/04/21 18:23 100-42-502/04/21 10:170.0082 0.0022 1
1,1,1,2-Tetrachloroethane ND mg/kg 02/04/21 18:23 630-20-602/04/21 10:170.0082 0.0031 1
1,1,2,2-Tetrachloroethane ND mg/kg 02/04/21 18:23 79-34-502/04/21 10:170.0082 0.0022 1
Tetrachloroethene ND mg/kg 02/04/21 18:23 127-18-402/04/21 10:170.0082 0.0026 1
Toluene ND mg/kg 02/04/21 18:23 108-88-302/04/21 10:170.0082 0.0023 1
1,2,3-Trichlorobenzene ND mg/kg 02/04/21 18:23 87-61-602/04/21 10:170.0082 0.0066 1
1,2,4-Trichlorobenzene ND mg/kg 02/04/21 18:23 120-82-102/04/21 10:170.0082 0.0069 1
1,1,1-Trichloroethane ND mg/kg 02/04/21 18:23 71-55-602/04/21 10:170.0082 0.0042 1
1,1,2-Trichloroethane ND mg/kg 02/04/21 18:23 79-00-502/04/21 10:170.0082 0.0027 1
Trichloroethene ND mg/kg 02/04/21 18:23 79-01-602/04/21 10:170.0082 0.0021 1
Trichlorofluoromethane ND mg/kg 02/04/21 18:23 75-69-402/04/21 10:170.0082 0.0045 1
1,2,3-Trichloropropane ND mg/kg 02/04/21 18:23 96-18-402/04/21 10:170.0082 0.0041 1
1,2,4-Trimethylbenzene ND mg/kg 02/04/21 18:23 95-63-602/04/21 10:170.0082 0.0022 1
1,3,5-Trimethylbenzene ND mg/kg 02/04/21 18:23 108-67-802/04/21 10:170.0082 0.0027 1
Vinyl acetate ND mg/kg 02/04/21 18:23 108-05-402/04/21 10:170.082 0.0059 1
Vinyl chloride ND mg/kg 02/04/21 18:23 75-01-402/04/21 10:170.016 0.0041 1
Xylene (Total)ND mg/kg 02/04/21 18:23 1330-20-702/04/21 10:170.016 0.0047 1
m&p-Xylene ND mg/kg 02/04/21 18:23 179601-23-102/04/21 10:170.016 0.0056 1
o-Xylene ND mg/kg 02/04/21 18:23 95-47-602/04/21 10:170.0082 0.0036 1
Surrogates
Toluene-d8 (S)101 %02/04/21 18:23 2037-26-502/04/21 10:1770-130 1
4-Bromofluorobenzene (S)108 %02/04/21 18:23 460-00-402/04/21 10:1769-134 1
1,2-Dichloroethane-d4 (S)103 %02/04/21 18:23 17060-07-002/04/21 10:1770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.1 %02/02/21 16:34 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 74.7 %02/05/21 10:2102/05/21 10:101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Sample:T-5 Lab ID:92519759001 Collected:02/01/21 11:30 Received:02/02/21 14:00 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 02/04/21 21:58 18540-29-902/04/21 01:191.34 0.341 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597289
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92519759001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3149590
Associated Lab Samples:92519759001
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 02/04/21 12:060.0046
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3149591LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0830.083 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3149592MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92519090001
3149593
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg M10.025 71 75-12575 4 200.0250.0022 0.020 0.021
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597338
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92519759001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3149816
Associated Lab Samples:92519759001
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 2.5 02/05/21 03:120.50
Barium mg/kg ND 1.0 02/05/21 03:120.25
Cadmium mg/kg ND 0.10 02/05/21 03:120.050
Chromium mg/kg ND 0.50 02/06/21 00:140.25
Lead mg/kg ND 1.0 02/05/21 03:120.25
Selenium mg/kg ND 1.0 02/06/21 00:140.50
Silver mg/kg ND 0.50 02/05/21 03:120.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3149817LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 46.950 94 80-120
Barium mg/kg 45.850 92 80-120
Cadmium mg/kg 44.750 89 80-120
Chromium mg/kg 49.550 99 80-120
Lead mg/kg 44.150 88 80-120
Selenium mg/kg 44.250 88 80-120
Silver mg/kg 22.725 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3149818MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92519689001
3149819
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 37.9 102 75-12599 2 2037.9ND 38.9 37.9
Barium mg/kg 37.9 94 75-12593 1 2037.9ND 35.6 35.3
Cadmium mg/kg 37.9 98 75-12596 1 2037.9ND 37.0 36.4
Chromium mg/kg 37.9 93 75-12591 2 2037.9ND 35.2 34.5
Lead mg/kg 37.9 93 75-12592 1 2037.9ND 35.1 34.8
Selenium mg/kg 37.9 110 75-125108 2 2037.9ND 42.0 41.3
Silver mg/kg 18.9 97 75-12597 1 2018.9ND 18.5 18.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597618
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519759001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3151170
Associated Lab Samples:92519759001
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 02/04/21 12:030.0019
1,1,1-Trichloroethane mg/kg ND 0.0050 02/04/21 12:030.0026
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 02/04/21 12:030.0013
1,1,2-Trichloroethane mg/kg ND 0.0050 02/04/21 12:030.0017
1,1-Dichloroethane mg/kg ND 0.0050 02/04/21 12:030.0021
1,1-Dichloroethene mg/kg ND 0.0050 02/04/21 12:030.0021
1,1-Dichloropropene mg/kg ND 0.0050 02/04/21 12:030.0024
1,2,3-Trichlorobenzene mg/kg ND 0.0050 02/04/21 12:030.0040
1,2,3-Trichloropropane mg/kg ND 0.0050 02/04/21 12:030.0025
1,2,4-Trichlorobenzene mg/kg ND 0.0050 02/04/21 12:030.0042
1,2,4-Trimethylbenzene mg/kg ND 0.0050 02/04/21 12:030.0014
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 02/04/21 12:030.0019
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 02/04/21 12:030.0022
1,2-Dichlorobenzene mg/kg ND 0.0050 02/04/21 12:030.0018
1,2-Dichloroethane mg/kg ND 0.0050 02/04/21 12:030.0033
1,2-Dichloropropane mg/kg ND 0.0050 02/04/21 12:030.0015
1,3,5-Trimethylbenzene mg/kg ND 0.0050 02/04/21 12:030.0017
1,3-Dichlorobenzene mg/kg ND 0.0050 02/04/21 12:030.0016
1,3-Dichloropropane mg/kg ND 0.0050 02/04/21 12:030.0016
1,4-Dichlorobenzene mg/kg ND 0.0050 02/04/21 12:030.0013
2,2-Dichloropropane mg/kg ND 0.0050 02/04/21 12:030.0016
2-Butanone (MEK)mg/kg ND 0.10 02/04/21 12:030.024
2-Chlorotoluene mg/kg ND 0.0050 02/04/21 12:030.0018
2-Hexanone mg/kg ND 0.050 02/04/21 12:030.0048
4-Chlorotoluene mg/kg ND 0.0050 02/04/21 12:030.00088
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 02/04/21 12:030.0048
Acetone mg/kg ND 0.10 02/04/21 12:030.032
Benzene mg/kg ND 0.0050 02/04/21 12:030.0020
Bromobenzene mg/kg ND 0.0050 02/04/21 12:030.0016
Bromochloromethane mg/kg ND 0.0050 02/04/21 12:030.0015
Bromodichloromethane mg/kg ND 0.0050 02/04/21 12:030.0019
Bromoform mg/kg ND 0.0050 02/04/21 12:030.0018
Bromomethane mg/kg ND 0.010 02/04/21 12:030.0079
Carbon tetrachloride mg/kg ND 0.0050 02/04/21 12:030.0019
Chlorobenzene mg/kg ND 0.0050 02/04/21 12:030.00096
Chloroethane mg/kg ND 0.010 02/04/21 12:030.0039
Chloroform mg/kg ND 0.0050 02/04/21 12:030.0030
Chloromethane mg/kg ND 0.010 02/04/21 12:030.0042
cis-1,2-Dichloroethene mg/kg ND 0.0050 02/04/21 12:030.0017
cis-1,3-Dichloropropene mg/kg ND 0.0050 02/04/21 12:030.0014
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3151170
Associated Lab Samples:92519759001
Matrix:Solid
AnalyzedMDL
Dibromochloromethane mg/kg ND 0.0050 02/04/21 12:030.0028
Dibromomethane mg/kg ND 0.0050 02/04/21 12:030.0011
Dichlorodifluoromethane mg/kg ND 0.010 02/04/21 12:030.0022
Diisopropyl ether mg/kg ND 0.0050 02/04/21 12:030.0014
Ethylbenzene mg/kg ND 0.0050 02/04/21 12:030.0023
Hexachloro-1,3-butadiene mg/kg ND 0.010 02/04/21 12:030.0082
Isopropylbenzene (Cumene)mg/kg ND 0.0050 02/04/21 12:030.0017
m&p-Xylene mg/kg ND 0.010 02/04/21 12:030.0034
Methyl-tert-butyl ether mg/kg ND 0.0050 02/04/21 12:030.0019
Methylene Chloride mg/kg ND 0.020 02/04/21 12:030.014
n-Butylbenzene mg/kg ND 0.0050 02/04/21 12:030.0024
n-Propylbenzene mg/kg ND 0.0050 02/04/21 12:030.0018
Naphthalene mg/kg ND 0.0050 02/04/21 12:030.0026
o-Xylene mg/kg ND 0.0050 02/04/21 12:030.0022
p-Isopropyltoluene mg/kg ND 0.0050 02/04/21 12:030.0025
sec-Butylbenzene mg/kg ND 0.0050 02/04/21 12:030.0022
Styrene mg/kg ND 0.0050 02/04/21 12:030.0013
tert-Butylbenzene mg/kg ND 0.0050 02/04/21 12:030.0018
Tetrachloroethene mg/kg ND 0.0050 02/04/21 12:030.0016
Toluene mg/kg ND 0.0050 02/04/21 12:030.0014
trans-1,2-Dichloroethene mg/kg ND 0.0050 02/04/21 12:030.0018
trans-1,3-Dichloropropene mg/kg ND 0.0050 02/04/21 12:030.0017
Trichloroethene mg/kg ND 0.0050 02/04/21 12:030.0013
Trichlorofluoromethane mg/kg ND 0.0050 02/04/21 12:030.0028
Vinyl acetate mg/kg ND 0.050 02/04/21 12:030.0036
Vinyl chloride mg/kg ND 0.010 02/04/21 12:030.0025
Xylene (Total)mg/kg ND 0.010 02/04/21 12:030.0028
1,2-Dichloroethane-d4 (S)%102 70-130 02/04/21 12:03
4-Bromofluorobenzene (S)%103 69-134 02/04/21 12:03
Toluene-d8 (S)%99 70-130 02/04/21 12:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151171LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.31.2 101 70-130
1,1,1-Trichloroethane mg/kg 1.21.2 99 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.31.2 101 70-130
1,1,2-Trichloroethane mg/kg 1.31.2 100 70-130
1,1-Dichloroethane mg/kg 1.21.2 99 70-130
1,1-Dichloroethene mg/kg 1.41.2 108 70-130
1,1-Dichloropropene mg/kg 1.31.2 102 70-130
1,2,3-Trichlorobenzene mg/kg 1.21.2 96 65-130
1,2,3-Trichloropropane mg/kg 1.31.2 100 70-130
1,2,4-Trichlorobenzene mg/kg 1.31.2 102 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151171LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.21.2 97 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.31.2 104 70-130
1,2-Dibromoethane (EDB)mg/kg 1.31.2 103 70-130
1,2-Dichlorobenzene mg/kg 1.31.2 100 70-130
1,2-Dichloroethane mg/kg 1.21.2 96 63-130
1,2-Dichloropropane mg/kg 1.31.2 101 70-130
1,3,5-Trimethylbenzene mg/kg 1.31.2 100 70-130
1,3-Dichlorobenzene mg/kg 1.21.2 100 70-130
1,3-Dichloropropane mg/kg 1.21.2 100 70-130
1,4-Dichlorobenzene mg/kg 1.21.2 97 70-130
2,2-Dichloropropane mg/kg 1.21.2 99 66-130
2-Butanone (MEK)mg/kg 2.52.5 102 70-130
2-Chlorotoluene mg/kg 1.31.2 104 70-130
2-Hexanone mg/kg 2.52.5 101 70-130
4-Chlorotoluene mg/kg 1.31.2 100 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.52.5 100 70-130
Acetone mg/kg 2.52.5 100 69-130
Benzene mg/kg 1.21.2 97 70-130
Bromobenzene mg/kg 1.31.2 102 70-130
Bromochloromethane mg/kg 1.21.2 98 70-130
Bromodichloromethane mg/kg 1.31.2 101 69-130
Bromoform mg/kg 1.41.2 109 70-130
Bromomethane mg/kg 1.21.2 95 52-130
Carbon tetrachloride mg/kg 1.41.2 109 70-130
Chlorobenzene mg/kg 1.21.2 99 70-130
Chloroethane mg/kg 1.31.2 101 65-130
Chloroform mg/kg 1.21.2 95 70-130
Chloromethane mg/kg 1.11.2 87 55-130
cis-1,2-Dichloroethene mg/kg 1.21.2 99 70-130
cis-1,3-Dichloropropene mg/kg 1.31.2 103 70-130
Dibromochloromethane mg/kg 1.31.2 108 70-130
Dibromomethane mg/kg 1.31.2 105 70-130
Dichlorodifluoromethane mg/kg 1.31.2 102 45-156
Diisopropyl ether mg/kg 1.21.2 95 70-130
Ethylbenzene mg/kg 1.21.2 93 70-130
Hexachloro-1,3-butadiene mg/kg 1.41.2 111 66-130
Isopropylbenzene (Cumene)mg/kg 1.31.2 102 70-130
m&p-Xylene mg/kg 2.52.5 99 70-130
Methyl-tert-butyl ether mg/kg 1.21.2 97 70-130
Methylene Chloride mg/kg 1.11.2 90 65-130
n-Butylbenzene mg/kg 1.31.2 106 67-130
n-Propylbenzene mg/kg 1.31.2 101 70-130
Naphthalene mg/kg 1.31.2 101 70-130
o-Xylene mg/kg 1.21.2 100 70-130
p-Isopropyltoluene mg/kg 1.31.2 102 67-130
sec-Butylbenzene mg/kg 1.31.2 100 69-130
Styrene mg/kg 1.31.2 105 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3151171LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.21.2 95 67-130
Tetrachloroethene mg/kg 1.21.2 95 70-130
Toluene mg/kg 1.21.2 97 70-130
trans-1,2-Dichloroethene mg/kg 1.21.2 98 70-130
trans-1,3-Dichloropropene mg/kg 1.21.2 99 68-130
Trichloroethene mg/kg 1.31.2 101 70-130
Trichlorofluoromethane mg/kg 1.31.2 101 70-130
Vinyl acetate mg/kg 2.82.5 111 70-130
Vinyl chloride mg/kg 1.21.2 93 61-130
Xylene (Total)mg/kg 3.73.8 99 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3151173MATRIX SPIKE SAMPLE:
MSSpike
Result
92519952002
1,1,1,2-Tetrachloroethane mg/kg 0.730.7 104 70-131ND
1,1,1-Trichloroethane mg/kg 0.770.7 110 65-133ND
1,1,2,2-Tetrachloroethane mg/kg 0.720.7 102 66-130ND
1,1,2-Trichloroethane mg/kg 0.750.7 107 66-133ND
1,1-Dichloroethane mg/kg 0.710.7 101 65-130ND
1,1-Dichloroethene mg/kg 0.790.7 112 10-158ND
1,1-Dichloropropene mg/kg 0.790.7 113 68-133ND
1,2,3-Trichlorobenzene mg/kg 0.700.7 99 27-138ND
1,2,3-Trichloropropane mg/kg 0.690.7 99 67-130ND
1,2,4-Trichlorobenzene mg/kg 0.750.7 108 51-134ND
1,2,4-Trimethylbenzene mg/kg 0.750.7 107 63-136ND
1,2-Dibromo-3-chloropropane mg/kg 0.650.7 93 32-130ND
1,2-Dibromoethane (EDB)mg/kg 0.740.7 106 70-130ND
1,2-Dichlorobenzene mg/kg 0.750.7 107 69-130ND
1,2-Dichloroethane mg/kg 0.720.7 103 59-130ND
1,2-Dichloropropane mg/kg 0.760.7 108 70-130ND
1,3,5-Trimethylbenzene mg/kg 0.760.7 108 65-137ND
1,3-Dichlorobenzene mg/kg 0.760.7 109 70-130ND
1,3-Dichloropropane mg/kg 0.710.7 102 70-130ND
1,4-Dichlorobenzene mg/kg 0.730.7 104 68-130ND
2,2-Dichloropropane mg/kg 0.720.7 102 32-130ND
2-Butanone (MEK)mg/kg 1.21.4 88 10-136ND
2-Chlorotoluene mg/kg 0.770.7 110 69-141ND
2-Hexanone mg/kg 1.31.4 92 10-144ND
4-Chlorotoluene mg/kg 0.750.7 107 70-132ND
4-Methyl-2-pentanone (MIBK)mg/kg 1.41.4 98 25-143ND
Acetone mg/kg 1.21.4 83 10-130ND
Benzene mg/kg 0.750.7 106 67-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
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[phone]
Page 15 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3151173MATRIX SPIKE SAMPLE:
MSSpike
Result
92519952002
Bromobenzene mg/kg 0.730.7 105 70-130ND
Bromochloromethane mg/kg 0.700.7 100 69-134ND
Bromodichloromethane mg/kg 0.730.7 105 64-130ND
Bromoform mg/kg 0.680.7 96 62-130ND
Bromomethane mg/kg 0.590.7 84 20-176ND
Carbon tetrachloride mg/kg 0.800.7 115 65-140ND
Chlorobenzene mg/kg 0.740.7 106 70-130ND
Chloroethane mg/kg 0.190.7 28 10-130ND
Chloroform mg/kg 0.700.7 100 63-130ND
Chloromethane mg/kg 0.690.7 98 58-130ND
cis-1,2-Dichloroethene mg/kg 0.730.7 104 66-130ND
cis-1,3-Dichloropropene mg/kg 0.730.7 104 67-130ND
Dibromochloromethane mg/kg 0.740.7 106 67-130ND
Dibromomethane mg/kg 0.750.7 107 63-131ND
Dichlorodifluoromethane mg/kg 0.760.7 108 44-180ND
Diisopropyl ether mg/kg 0.680.7 96 63-130ND
Ethylbenzene mg/kg 0.720.7 103 66-130ND
Hexachloro-1,3-butadiene mg/kg 0.860.7 123 64-150ND
Isopropylbenzene (Cumene)mg/kg 0.790.7 112 69-135ND
m&p-Xylene mg/kg 1.51.4 107 60-133ND
Methyl-tert-butyl ether mg/kg 0.690.7 99 65-130ND
Methylene Chloride mg/kg 0.660.7 94 61-130ND
n-Butylbenzene mg/kg 0.810.7 116 65-140ND
n-Propylbenzene mg/kg 0.770.7 109 67-140ND
Naphthalene mg/kg 0.750.7 106 15-145ND
o-Xylene mg/kg 0.760.7 109 66-133ND
p-Isopropyltoluene mg/kg 0.810.7 115 56-147ND
sec-Butylbenzene mg/kg 0.800.7 114 65-139ND
Styrene mg/kg 0.780.7 111 70-132ND
tert-Butylbenzene mg/kg 0.730.7 104 62-135ND
Tetrachloroethene mg/kg 0.730.7 104 70-135ND
Toluene mg/kg 0.760.7 109 67-130ND
trans-1,2-Dichloroethene mg/kg 0.720.7 103 69-130ND
trans-1,3-Dichloropropene mg/kg 0.890.7 126 62-130ND
Trichloroethene mg/kg 0.790.7 113 70-135ND
Trichlorofluoromethane mg/kg 0.260.7 38 10-130ND
Vinyl acetate mg/kg 1.51.4 109 53-130ND
Vinyl chloride mg/kg 0.790.7 112 61-148ND
Xylene (Total)mg/kg 2.32.1 108 63-132ND
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519952001
3151172SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND 30ND
1,1,1-Trichloroethane mg/kg ND 30ND
1,1,2,2-Tetrachloroethane mg/kg ND 30ND
1,1,2-Trichloroethane mg/kg ND 30ND
1,1-Dichloroethane mg/kg ND 30ND
1,1-Dichloroethene mg/kg ND 30ND
1,1-Dichloropropene mg/kg ND 30ND
1,2,3-Trichlorobenzene mg/kg ND 30ND
1,2,3-Trichloropropane mg/kg ND 30ND
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2,4-Trimethylbenzene mg/kg ND 30ND
1,2-Dibromo-3-chloropropane mg/kg ND 30ND
1,2-Dibromoethane (EDB)mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,2-Dichloroethane mg/kg ND 30ND
1,2-Dichloropropane mg/kg ND 30ND
1,3,5-Trimethylbenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,3-Dichloropropane mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
2,2-Dichloropropane mg/kg ND 30ND
2-Butanone (MEK)mg/kg ND 30ND
2-Chlorotoluene mg/kg ND 30ND
2-Hexanone mg/kg ND 30ND
4-Chlorotoluene mg/kg ND 30ND
4-Methyl-2-pentanone (MIBK)mg/kg ND 30ND
Acetone mg/kg ND 30ND
Benzene mg/kg ND 30ND
Bromobenzene mg/kg ND 30ND
Bromochloromethane mg/kg ND 30ND
Bromodichloromethane mg/kg ND 30ND
Bromoform mg/kg ND 30ND
Bromomethane mg/kg ND 30ND
Carbon tetrachloride mg/kg ND 30ND
Chlorobenzene mg/kg ND 30ND
Chloroethane mg/kg ND 30ND
Chloroform mg/kg ND 30ND
Chloromethane mg/kg ND 30ND
cis-1,2-Dichloroethene mg/kg ND 30ND
cis-1,3-Dichloropropene mg/kg ND 30ND
Dibromochloromethane mg/kg ND 30ND
Dibromomethane mg/kg ND 30ND
Dichlorodifluoromethane mg/kg ND 30ND
Diisopropyl ether mg/kg ND 30ND
Ethylbenzene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Isopropylbenzene (Cumene)mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519952001
3151172SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND 30ND
Methyl-tert-butyl ether mg/kg ND 30ND
Methylene Chloride mg/kg ND 30ND
n-Butylbenzene mg/kg ND 30ND
n-Propylbenzene mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
o-Xylene mg/kg ND 30ND
p-Isopropyltoluene mg/kg ND 30ND
sec-Butylbenzene mg/kg ND 30ND
Styrene mg/kg ND 30ND
tert-Butylbenzene mg/kg ND 30ND
Tetrachloroethene mg/kg ND 30ND
Toluene mg/kg ND 30ND
trans-1,2-Dichloroethene mg/kg ND 30ND
trans-1,3-Dichloropropene mg/kg ND 30ND
Trichloroethene mg/kg ND 30ND
Trichlorofluoromethane mg/kg ND 30ND
Vinyl acetate mg/kg ND 30ND
Vinyl chloride mg/kg ND 30ND
Xylene (Total)mg/kg ND 30ND
1,2-Dichloroethane-d4 (S)%101102
4-Bromofluorobenzene (S)%99100
Toluene-d8 (S)%9999
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597473
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519759001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3150723
Associated Lab Samples:92519759001
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene mg/kg ND 0.33 02/04/21 08:080.076
1,2-Dichlorobenzene mg/kg ND 0.33 02/04/21 08:080.072
1,3-Dichlorobenzene mg/kg ND 0.33 02/04/21 08:080.075
1,4-Dichlorobenzene mg/kg ND 0.33 02/04/21 08:080.073
1-Methylnaphthalene mg/kg ND 0.33 02/04/21 08:080.088
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 02/04/21 08:080.092
2,4,5-Trichlorophenol mg/kg ND 0.33 02/04/21 08:080.086
2,4,6-Trichlorophenol mg/kg ND 0.33 02/04/21 08:080.083
2,4-Dichlorophenol mg/kg ND 0.33 02/04/21 08:080.11
2,4-Dimethylphenol mg/kg ND 0.33 02/04/21 08:080.082
2,4-Dinitrophenol mg/kg ND 1.7 02/04/21 08:081.1
2,4-Dinitrotoluene mg/kg ND 0.33 02/04/21 08:080.088
2,6-Dinitrotoluene mg/kg ND 0.33 02/04/21 08:080.087
2-Chloronaphthalene mg/kg ND 0.33 02/04/21 08:080.074
2-Chlorophenol mg/kg ND 0.33 02/04/21 08:080.077
2-Methylnaphthalene mg/kg ND 0.33 02/04/21 08:080.084
2-Methylphenol(o-Cresol)mg/kg ND 0.33 02/04/21 08:080.073
2-Nitroaniline mg/kg ND 1.7 02/04/21 08:080.17
2-Nitrophenol mg/kg ND 0.33 02/04/21 08:080.10
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 02/04/21 08:080.083
3,3'-Dichlorobenzidine mg/kg ND 0.66 02/04/21 08:080.23
3-Nitroaniline mg/kg ND 1.7 IL02/04/21 08:080.18
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 02/04/21 08:080.53
4-Bromophenylphenyl ether mg/kg ND 0.33 02/04/21 08:080.087
4-Chloro-3-methylphenol mg/kg ND 0.66 02/04/21 08:080.20
4-Chloroaniline mg/kg ND 0.66 02/04/21 08:080.20
4-Chlorophenylphenyl ether mg/kg ND 0.33 02/04/21 08:080.086
4-Nitroaniline mg/kg ND 0.66 02/04/21 08:080.16
4-Nitrophenol mg/kg ND 1.7 02/04/21 08:080.53
Acenaphthene mg/kg ND 0.33 02/04/21 08:080.085
Acenaphthylene mg/kg ND 0.33 02/04/21 08:080.078
Aniline mg/kg ND 0.33 02/04/21 08:080.074
Anthracene mg/kg ND 0.33 02/04/21 08:080.086
Benzo(a)anthracene mg/kg ND 0.33 02/04/21 08:080.11
Benzo(a)pyrene mg/kg ND 0.33 02/04/21 08:080.14
Benzo(b)fluoranthene mg/kg ND 0.33 02/04/21 08:080.13
Benzo(g,h,i)perylene mg/kg ND 0.33 02/04/21 08:080.13
Benzo(k)fluoranthene mg/kg ND 0.33 02/04/21 08:080.14
Benzoic Acid mg/kg ND 1.7 02/04/21 08:080.36
Benzyl alcohol mg/kg ND 0.66 02/04/21 08:080.18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3150723
Associated Lab Samples:92519759001
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane mg/kg ND 0.33 02/04/21 08:080.088
bis(2-Chloroethyl) ether mg/kg ND 0.33 02/04/21 08:080.070
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 02/04/21 08:080.11
Butylbenzylphthalate mg/kg ND 0.33 02/04/21 08:080.088
Chrysene mg/kg ND 0.33 02/04/21 08:080.096
Di-n-butylphthalate mg/kg ND 0.33 02/04/21 08:080.082
Di-n-octylphthalate mg/kg ND 0.33 02/04/21 08:080.19
Dibenz(a,h)anthracene mg/kg ND 0.33 02/04/21 08:080.13
Dibenzofuran mg/kg ND 0.33 02/04/21 08:080.083
Diethylphthalate mg/kg ND 0.33 02/04/21 08:080.072
Dimethylphthalate mg/kg ND 0.33 02/04/21 08:080.075
Fluoranthene mg/kg ND 0.33 02/04/21 08:080.10
Fluorene mg/kg ND 0.33 02/04/21 08:080.089
Hexachloro-1,3-butadiene mg/kg ND 0.33 02/04/21 08:080.080
Hexachlorobenzene mg/kg ND 0.33 02/04/21 08:080.084
Hexachlorocyclopentadiene mg/kg ND 0.33 02/04/21 08:080.13
Hexachloroethane mg/kg ND 0.33 02/04/21 08:080.075
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 02/04/21 08:080.15
Isophorone mg/kg ND 0.33 02/04/21 08:080.072
N-Nitroso-di-n-propylamine mg/kg ND 0.33 02/04/21 08:080.093
N-Nitrosodimethylamine mg/kg ND 0.33 02/04/21 08:080.093
N-Nitrosodiphenylamine mg/kg ND 0.33 02/04/21 08:080.084
Naphthalene mg/kg ND 0.33 02/04/21 08:080.079
Nitrobenzene mg/kg ND 0.33 02/04/21 08:080.079
Pentachlorophenol mg/kg ND 0.66 02/04/21 08:080.15
Phenanthrene mg/kg ND 0.33 02/04/21 08:080.083
Phenol mg/kg ND 0.33 02/04/21 08:080.079
Pyrene mg/kg ND 0.33 02/04/21 08:080.091
Pyridine mg/kg ND 0.33 02/04/21 08:080.084
2,4,6-Tribromophenol (S)%86 18-130 02/04/21 08:08
2-Fluorobiphenyl (S)%71 19-130 02/04/21 08:08
2-Fluorophenol (S)%63 18-130 02/04/21 08:08
Nitrobenzene-d5 (S)%75 21-130 02/04/21 08:08
Phenol-d6 (S)%66 18-130 02/04/21 08:08
Terphenyl-d14 (S)%106 15-130 02/04/21 08:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3150724LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.61.7 97 47-130
1,2-Dichlorobenzene mg/kg 1.51.7 90 49-130
1,3-Dichlorobenzene mg/kg 1.51.7 87 48-130
1,4-Dichlorobenzene mg/kg 1.51.7 89 49-130
1-Methylnaphthalene mg/kg 1.61.7 95 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3150724LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.51.7 89 38-130
2,4,5-Trichlorophenol mg/kg 1.81.7 104 49-130
2,4,6-Trichlorophenol mg/kg 1.81.7 104 50-130
2,4-Dichlorophenol mg/kg 1.81.7 106 51-130
2,4-Dimethylphenol mg/kg 1.81.7 109 53-130
2,4-Dinitrophenol mg/kg 8.98.4 106 39-130
2,4-Dinitrotoluene mg/kg 1.81.7 109 53-130
2,6-Dinitrotoluene mg/kg 1.81.7 107 55-130
2-Chloronaphthalene mg/kg 1.61.7 95 48-130
2-Chlorophenol mg/kg 1.61.7 93 54-130
2-Methylnaphthalene mg/kg 1.61.7 96 57-130
2-Methylphenol(o-Cresol)mg/kg 1.61.7 92 50-130
2-Nitroaniline mg/kg 3.33.4 98 49-130
2-Nitrophenol mg/kg 1.71.7 100 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.71.7 103 50-130
3,3'-Dichlorobenzidine mg/kg 3.03.4 90 47-130
3-Nitroaniline mg/kg 2.7 IL3.4 81 45-130
4,6-Dinitro-2-methylphenol mg/kg 3.73.4 109 50-142
4-Bromophenylphenyl ether mg/kg 1.81.7 105 55-130
4-Chloro-3-methylphenol mg/kg 3.73.4 111 52-130
4-Chloroaniline mg/kg 3.03.4 89 49-130
4-Chlorophenylphenyl ether mg/kg 1.81.7 107 53-130
4-Nitroaniline mg/kg 3.23.4 96 51-130
4-Nitrophenol mg/kg 10.68.4 125 40-130
Acenaphthene mg/kg 1.61.7 94 56-130
Acenaphthylene mg/kg 1.61.7 94 58-130
Aniline mg/kg 1.31.7 77 44-130
Anthracene mg/kg 1.51.7 88 60-130
Benzo(a)anthracene mg/kg 1.71.7 100 59-130
Benzo(a)pyrene mg/kg 1.71.7 102 57-130
Benzo(b)fluoranthene mg/kg 1.71.7 103 54-130
Benzo(g,h,i)perylene mg/kg 1.61.7 96 59-130
Benzo(k)fluoranthene mg/kg 1.71.7 99 54-130
Benzoic Acid mg/kg 5.88.4 69 19-130
Benzyl alcohol mg/kg 3.23.4 95 50-130
bis(2-Chloroethoxy)methane mg/kg 1.61.7 93 55-130
bis(2-Chloroethyl) ether mg/kg 1.51.7 92 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.71.7 103 58-130
Butylbenzylphthalate mg/kg 1.81.7 104 46-138
Chrysene mg/kg 1.61.7 97 57-130
Di-n-butylphthalate mg/kg 1.81.7 106 57-130
Di-n-octylphthalate mg/kg 1.91.7 110 57-130
Dibenz(a,h)anthracene mg/kg 1.71.7 99 60-130
Dibenzofuran mg/kg 1.71.7 100 54-130
Diethylphthalate mg/kg 1.81.7 107 55-130
Dimethylphthalate mg/kg 1.81.7 104 57-130
Fluoranthene mg/kg 1.81.7 105 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3150724LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.71.7 100 56-130
Hexachloro-1,3-butadiene mg/kg 1.81.7 106 41-130
Hexachlorobenzene mg/kg 1.81.7 107 53-130
Hexachlorocyclopentadiene mg/kg 1.51.7 88 23-130
Hexachloroethane mg/kg 1.51.7 91 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.71.7 101 61-130
Isophorone mg/kg 1.71.7 102 49-130
N-Nitroso-di-n-propylamine mg/kg 1.71.7 101 52-130
N-Nitrosodimethylamine mg/kg 1.51.7 87 45-130
N-Nitrosodiphenylamine mg/kg 1.61.7 97 56-130
Naphthalene mg/kg 1.51.7 91 56-130
Nitrobenzene mg/kg 1.71.7 100 50-130
Pentachlorophenol mg/kg 3.73.4 109 33-130
Phenanthrene mg/kg 1.61.7 98 60-130
Phenol mg/kg 1.71.7 100 54-130
Pyrene mg/kg 1.61.7 94 61-130
Pyridine mg/kg 1.11.7 67 35-130
2,4,6-Tribromophenol (S)%110 18-130
2-Fluorobiphenyl (S)%91 19-130
2-Fluorophenol (S)%89 18-130
Nitrobenzene-d5 (S)%96 21-130
Phenol-d6 (S)%91 18-130
Terphenyl-d14 (S)%113 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3150725MATRIX SPIKE SAMPLE:
MSSpike
Result
92519820003
1,2,4-Trichlorobenzene mg/kg 1.41.9 75 22-130ND
1,2-Dichlorobenzene mg/kg 1.31.9 70 23-130ND
1,3-Dichlorobenzene mg/kg 1.21.9 68 26-130ND
1,4-Dichlorobenzene mg/kg 1.31.9 70 27-130ND
1-Methylnaphthalene mg/kg 1.31.9 73 30-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.31.9 69 30-130ND
2,4,5-Trichlorophenol mg/kg 1.51.9 81 26-130ND
2,4,6-Trichlorophenol mg/kg 1.51.9 80 23-130ND
2,4-Dichlorophenol mg/kg 1.51.9 80 29-130ND
2,4-Dimethylphenol mg/kg 1.41.9 77 13-130ND
2,4-Dinitrophenol mg/kg 7.99.2 86 10-131ND
2,4-Dinitrotoluene mg/kg 1.51.9 81 28-130ND
2,6-Dinitrotoluene mg/kg 1.51.9 82 36-130ND
2-Chloronaphthalene mg/kg 1.31.9 73 27-130ND
2-Chlorophenol mg/kg 1.31.9 72 29-130ND
2-Methylnaphthalene mg/kg 1.41.9 74 29-130ND
2-Methylphenol(o-Cresol)mg/kg 1.21.9 68 20-130ND
2-Nitroaniline mg/kg 2.73.7 75 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3150725MATRIX SPIKE SAMPLE:
MSSpike
Result
92519820003
2-Nitrophenol mg/kg 1.41.9 75 26-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.41.9 76 10-176ND
3,3'-Dichlorobenzidine mg/kg 2.53.7 68 15-130ND
3-Nitroaniline mg/kg 2.3 IL3.7 63 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 3.23.7 87 15-132ND
4-Bromophenylphenyl ether mg/kg 1.51.9 84 35-130ND
4-Chloro-3-methylphenol mg/kg 3.13.7 84 30-130ND
4-Chloroaniline mg/kg 2.53.7 68 28-130ND
4-Chlorophenylphenyl ether mg/kg 1.51.9 82 32-130ND
4-Nitroaniline mg/kg 2.53.7 69 30-130ND
4-Nitrophenol mg/kg 8.49.2 91 17-130ND
Acenaphthene mg/kg 1.31.9 71 29-130ND
Acenaphthylene mg/kg 1.31.9 73 31-130ND
Aniline mg/kg 0.941.9 51 10-130ND
Anthracene mg/kg 1.21.9 67 33-130ND
Benzo(a)anthracene mg/kg 1.41.9 75 32-130ND
Benzo(a)pyrene mg/kg 1.41.9 77 32-130ND
Benzo(b)fluoranthene mg/kg 1.51.9 80 33-130ND
Benzo(g,h,i)perylene mg/kg 1.3 v31.9 70 28-130ND
Benzo(k)fluoranthene mg/kg 1.51.9 80 31-130ND
Benzoic Acid mg/kg 3.99.2 42 10-130ND
Benzyl alcohol mg/kg 2.73.7 74 31-130ND
bis(2-Chloroethoxy)methane mg/kg 1.31.9 71 30-130ND
bis(2-Chloroethyl) ether mg/kg 1.31.9 71 68-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.51.9 81 40-130ND
Butylbenzylphthalate mg/kg 1.51.9 84 40-130ND
Chrysene mg/kg 1.41.9 74 30-130ND
Di-n-butylphthalate mg/kg 1.51.9 79 41-130ND
Di-n-octylphthalate mg/kg 1.41.9 77 42-130ND
Dibenz(a,h)anthracene mg/kg 1.31.9 69 27-130ND
Dibenzofuran mg/kg 1.41.9 76 32-130ND
Diethylphthalate mg/kg 1.51.9 82 40-130ND
Dimethylphthalate mg/kg 1.51.9 80 37-130ND
Fluoranthene mg/kg 1.41.9 75 26-130ND
Fluorene mg/kg 1.41.9 76 31-130ND
Hexachloro-1,3-butadiene mg/kg 1.51.9 83 20-130ND
Hexachlorobenzene mg/kg 1.51.9 84 29-130ND
Hexachlorocyclopentadiene mg/kg 1.21.9 67 10-130ND
Hexachloroethane mg/kg 1.31.9 71 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.31.9 71 28-130ND
Isophorone mg/kg 1.41.9 79 32-130ND
N-Nitroso-di-n-propylamine mg/kg 1.51.9 80 31-130ND
N-Nitrosodimethylamine mg/kg 1.21.9 63 20-130ND
N-Nitrosodiphenylamine mg/kg 1.41.9 75 32-130ND
Naphthalene mg/kg 1.31.9 70 30-130ND
Nitrobenzene mg/kg 1.41.9 75 25-130ND
Pentachlorophenol mg/kg 3.03.7 83 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3150725MATRIX SPIKE SAMPLE:
MSSpike
Result
92519820003
Phenanthrene mg/kg 1.41.9 74 34-130ND
Phenol mg/kg 1.41.9 75 14-130ND
Pyrene mg/kg 1.51.9 82 31-130ND
Pyridine mg/kg 0.661.9 36 10-130ND
2,4,6-Tribromophenol (S)%88 18-130
2-Fluorobiphenyl (S)%72 19-130
2-Fluorophenol (S)%68 18-130
Nitrobenzene-d5 (S)%74 21-130
Phenol-d6 (S)%70 18-130
Terphenyl-d14 (S)%103 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519820005
3150726SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg ND 30ND
1,2-Dichlorobenzene mg/kg ND 30ND
1,3-Dichlorobenzene mg/kg ND 30ND
1,4-Dichlorobenzene mg/kg ND 30ND
1-Methylnaphthalene mg/kg ND 30ND
2,2'-Oxybis(1-chloropropane)mg/kg ND 30ND
2,4,5-Trichlorophenol mg/kg ND 30ND
2,4,6-Trichlorophenol mg/kg ND 30ND
2,4-Dichlorophenol mg/kg ND 30ND
2,4-Dimethylphenol mg/kg ND 30ND
2,4-Dinitrophenol mg/kg ND 30ND
2,4-Dinitrotoluene mg/kg ND 30ND
2,6-Dinitrotoluene mg/kg ND 30ND
2-Chloronaphthalene mg/kg ND 30ND
2-Chlorophenol mg/kg ND 30ND
2-Methylnaphthalene mg/kg ND 30ND
2-Methylphenol(o-Cresol)mg/kg ND 30ND
2-Nitroaniline mg/kg ND 30ND
2-Nitrophenol mg/kg ND 30ND
3&4-Methylphenol(m&p Cresol)mg/kg ND 30ND
3,3'-Dichlorobenzidine mg/kg ND 30ND
3-Nitroaniline mg/kg ND IL30ND
4,6-Dinitro-2-methylphenol mg/kg ND 30ND
4-Bromophenylphenyl ether mg/kg ND 30ND
4-Chloro-3-methylphenol mg/kg ND 30ND
4-Chloroaniline mg/kg ND 30ND
4-Chlorophenylphenyl ether mg/kg ND 30ND
4-Nitroaniline mg/kg ND 30ND
4-Nitrophenol mg/kg ND 30ND
Acenaphthene mg/kg ND 30ND
Acenaphthylene mg/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519820005
3150726SAMPLE DUPLICATE:
Aniline mg/kg ND 30ND
Anthracene mg/kg ND 30ND
Benzo(a)anthracene mg/kg ND 30ND
Benzo(a)pyrene mg/kg ND 30ND
Benzo(b)fluoranthene mg/kg ND 30ND
Benzo(g,h,i)perylene mg/kg ND 30ND
Benzo(k)fluoranthene mg/kg ND 30ND
Benzoic Acid mg/kg ND 30ND
Benzyl alcohol mg/kg ND 30ND
bis(2-Chloroethoxy)methane mg/kg ND 30ND
bis(2-Chloroethyl) ether mg/kg ND 30ND
bis(2-Ethylhexyl)phthalate mg/kg ND 30ND
Butylbenzylphthalate mg/kg ND 30ND
Chrysene mg/kg ND 30ND
Di-n-butylphthalate mg/kg ND 30ND
Di-n-octylphthalate mg/kg ND 30ND
Dibenz(a,h)anthracene mg/kg ND 30ND
Dibenzofuran mg/kg ND 30ND
Diethylphthalate mg/kg ND 30ND
Dimethylphthalate mg/kg ND 30ND
Fluoranthene mg/kg ND 30ND
Fluorene mg/kg ND 30ND
Hexachloro-1,3-butadiene mg/kg ND 30ND
Hexachlorobenzene mg/kg ND 30ND
Hexachlorocyclopentadiene mg/kg ND 30ND
Hexachloroethane mg/kg ND 30ND
Indeno(1,2,3-cd)pyrene mg/kg ND 30ND
Isophorone mg/kg ND 30ND
N-Nitroso-di-n-propylamine mg/kg ND 30ND
N-Nitrosodimethylamine mg/kg ND 30ND
N-Nitrosodiphenylamine mg/kg ND 30ND
Naphthalene mg/kg ND 30ND
Nitrobenzene mg/kg ND 30ND
Pentachlorophenol mg/kg ND 30ND
Phenanthrene mg/kg ND 30ND
Phenol mg/kg ND 30ND
Pyrene mg/kg ND 30ND
Pyridine mg/kg ND 30ND
2,4,6-Tribromophenol (S)%9879
2-Fluorobiphenyl (S)%8065
2-Fluorophenol (S)%7161
Nitrobenzene-d5 (S)%8270
Phenol-d6 (S)%7363
Terphenyl-d14 (S)%13495
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
597006
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92519759001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519317001
3148195SAMPLE DUPLICATE:
Percent Moisture %95.5 N202595.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519508002
3148452SAMPLE DUPLICATE:
Percent Moisture %72.4 N202572.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1616612
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92519759001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3619999-1
Associated Lab Samples:92519759001
Matrix:Solid
AnalyzedMDL
Total Solids %0.00300 02/05/21 10:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3619999-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1313697-01
R3619999-3SAMPLE DUPLICATE:
Total Solids %78.2 0.347 1078.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1613768
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92519759001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3619698-1
Associated Lab Samples:92519759001
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 02/04/21 18:180.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3619698-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.5010.0 95.0 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3619698-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1311761-16
R3619698-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 22.0 92.4 75.0-12591.9 0.539 2022.0ND 20.3 20.2
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3619698-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1311761-16
Chromium, Hexavalent mg/kg 11801200 98.2 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1311761-01
R3619698-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 1.52 200.643
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92519759001
R3619698-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 33
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92519759
7th & Caswell Tank Pull
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92519759001 597338 597465T-5 EPA 3050B EPA 6010D
92519759001 597289 597323T-5 EPA 7471B EPA 7471B
92519759001 597473 597558T-5 EPA 3546 EPA 8270E
92519759001 597618 597634T-5 EPA 5035A/5030B EPA 8260D
92519759001 597006T-5 SW-846
92519759001 1616612 1616612T-5 SM 2540 G SM 2540G
92519759001 1613768 1613768T-5 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/08/2021 04:43 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 33
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