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HomeMy WebLinkAboutMO-28415_47669_CA_UST-61_20200403_24-Hour Release and UST Leak Reporting FormUST-61 24-Hour Release and UST Leak Reporting Form. For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or in NC suspected release (DWM USE ONLY) Suspected Contamination? (Y/N) Y Facility ID Number Incident # Risk (H,I,L,U) Confirmed GW Contamination? (Y/N) N Date Leak Discovered 11/25/19 Received On Received By Confirmed Soil Contamination ?(Y/N) N Comm/Non-Commercial? Non-Com Reported by (circle one): Phone, Fax or Report Samples Taken?(Y/N) N Reg/Non-regulated? Non -Reg Region Free Product? (Y/N) If Yes, State Greatest Thickness INCIDENT DESCRIPTION Incident Name: Evans Property Address: 9920 Mallard Glen Drive County: Mecklenbur Regional Office (circle one): Ashevill ,Mooresville, ayetteville, City/Town: Charlotte Zip Code: 28262 Raleigh, Washington, Wilmington, Wi Latitude (decimal degrees): 35.330495 Longitude (decimal degrees) : _80.732292 Obtained by: Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount ❑GPS of release, amount of free product resent and recoveryefforts, initial responses conducted, impacts to receptors) Limited assessment by soil borings identified soil staining at one end of heating oil UST. ❑Topographic map Lab analysis confirmed petro impacts. See report attached. ®GIs Address matching ❑Other ❑ Unknown Describe location: HOW RELEASE WAS DISCOVERED (Release code) (Check one) ❑Release Detection Equipment or Methods ❑X Visual/Odor ❑Groundwater Contamination ❑During UST Closure/Removal ❑Water in Tank ❑Surface Water Contamination ©Property Transfer ❑Water Supply Well Contamination ❑Other (specify) SOURCE OF CONTAMINATION Source of Release Cause of Release Type of Release Product Type Released (Check primary source) (Check primary cause) (Check one) (Check primary product type released) ® Tank ❑ Spill ® Petroleum ❑ Gasoline/ Diesel/ ❑ Diesel/Veg. Oil ❑ Piping ❑ Overfill ❑ Non -Petroleum Kerosene Blend Heating Oil ❑ Vegetable Oil 100% ®❑ Dispenser ®Corrosion Both ❑ ❑ Other Petroleum ❑ E10 - E20 ❑ Submersible Turbine Pump ❑Physical/Mechanical Location Products ❑ (Check one) Metals Delivery Problem Damage ❑ E21 - E84 ❑ ❑ Install Problem ❑ E85 - E99 ❑ Spill Bucket ❑ Other Inorganics ❑ Other [-]Facility ❑Ethanol 100% ❑ Other ❑ Other Organics ❑ Unknown Residence ❑ E01 - E09 ❑ Unknown ❑Other Definitions presented on reverse Definitions presented on reverse Ownership 1. Municipal 2. Military 3. Unknow 4. Private Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining UST Form 61 (02/19) Page 1 of 2 IMPACT ON DRINKING WATER SUPPLIES Water Supply Wells Affected? 1. Yes 2. No Unknow Number of Water Supply Wells Affected Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3. UST SYSTEM OWNER UST Owner/Company Kevin Evans Point of Contact Address 1150 Liberty Road City State Zip Code Telephone Number Gold Hill NC 28071 UST SYSTEM OPERATOR Same as above UST Operator/Company Address City State Zip Code Telephone Number LANDOWNER AT LOCATION OF UST INCIDENT Same as above Landowner Address City State Zip Code Telephone Number Draw Sketch of Area (showing two major road intersections) or Attach Map See Attached investigation report Person Reporting Incident Patrick Lowery, PG Company SUMMIT ELT, PC plowery@summit-companies.com Telephone Number 803-230-5087 Title Env Manager Address 3575 Centre Circle Drive, Ft. Mill, SC 29715 Date 4/3/20 UST Form 61 (02/19) Page 2 of 2 Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined MECKLENBURG COUNTY - PROPERTY RECORD CARD PROPERTY SEARCH PARCEL ID: 02903112 EVANS KEVIN, EVANS ANN 9920 MALLARD GLEN DR 1150 LIBERTY RD CHARLOTTE NC GOLD HILL NC 28071 KEY INFORMATION Land Use Code R120 Neighborhood Land Use Desc SINGLE FAMILY RESIDENTIAL - ACREAGE Land Exemption/Deferment Municipality Last Sale Date Fire District Last Sale Price Special District Legal Description NA ASSESSMENT DETAILS Land Value Building Value Features Total BUILDING (1) Finished Area Story Foundation Full Bath(s) Total (SgFt) LAND Use R120 Units 1.49 1,246 1 STORY CRAWL SPACE 1 1,285 Type ACRE FEATURES Year Built Type 1984 STORAGE 1956 PUMP HOUSE Notice of 2019 Real Estate Assessed Value Total Appraised Value $119,300 C901 1.49 ACRE CHARLOTTE CITY OF CHARLOTTE NA Year Built 1956 Built Use / Style Heat FORCED AIR - NOT Fuel DUCTED External Wall FACE BRICK Fireplace(s) Half Bath(s) Bedroom(s) $32,900 $85,600 $800 $119,300 SINGLE FAMILY RESIDENTIAL OIL, WOOD OR COAL 1 3 Neighborhood Assessment C901 $32,900 Quantity Units Value 1 1 $500 1 72 $300 VALUE CHANGES The value change history shows only changes in appraised value; it does not show exemptions, exclusions or deferrals that could reduce a property's taxable value. If any of these are in effect for a particular tax year, it will be shown on the property tax bill for that year. It is also possible that some previous value changes might be missing from this list or listed in the wrong order. If you have any questions, please call the County Assessor's Office at 704-336-7600. Date of Value Change 01 /14/2019 08/08/2014 02/04/2011 01/02/2003 Tiger Lar), 500 ft Effective for Tax Year Reason for Change New Value 2019 COUNTYWIDE REVALUATION $119,300 2011 REVALUATION REVIEW - PEARSON $116,200 2011 COUNTYWIDE REVALUATION $116,300 2003 COUNTYWIDE REVALUATION $94,800 �t 029 2 5y Hyde Pointe Cox){` Disclaimer Mecklenburg County makes every effort to produce the most accurate information possible. No warranties, expressed or implied, are provided for the data herein, its use or interpretation. m� CELEBRATING 15 YEARS 4 ■ SUMMIT" aNGINLMNG. W0RA7OR7.7iS"NO., RC. November 25, 2019 Stefan Gassner Aspen Heights Partners 8008 Corporate Center Drive Suite 201 Charlotte, NC 28226 SUMMIT Engineering, Laboratory & Testing, P.C. 3575 Centre Circle Fort Mill, South Carolina 29715 www.SUMNUT-coMpanies.com Phone: (704) 504-1717 Fax: (704) 504-1125 Subject: Letter of Limited UST Assessment and Sampling The Heritage at UNCC 9920 Mallard Glen Drive Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 5778.500 SUMMIT ENGINEERING, LABRATORY & TESTING, P.C. (SUMMIT) has completed a limited assessment of a Home Heating Oil (HHO) underground storage tank (UST) at 9920 Mallard Glenb Drive, Mecklenburg County, North Carolina. SUMMIT personnel conducted the site field work on November 8, 2019. The site is irregular in shape and was noted to be comprised of one (1) parcel totaling approximately 1.49 acres in area. The site is developed with one (1) single family home and associated outbuildings. The residential structure is approximately a 1,2464 SF home, constructed in 1956. SUMMIT personnel visited the site on November 8, 2019. The HHO UST was observed to be located near the southeast of the home near the driveway. Utilizing a soil probe, SUMMIT personnel determined the size of the UST to be approximately 8 feet in length and 4 feet in diameter. SUMMIT completed five (5) geo-probe borings around the UST. Boring SB-1 and SB-2 were located at the approximate end of the UST. SB-3 was located on the downgradient side of the UST. SB-4 and SB- 5 were offset away from the UST. Each soil boring was extended to 10 feet below ground surface (bgs). Typical brown -tan sandy Silts were encountered in the soil borings. SB-2 exhibited petroleum soil staining, odors and positive detections of field screening equipment from 3 to 6 ff bgs. Soil sample SS-1 was collected from 5 ft bgs and soil sample SS-2 collected from 7 ft bgs. The collection of SS-1 and SS-2 will help define the vertical extent of impacts. SB-4 and SB-5 were spaced out in 2 directions from SB-2 in order to help define the lateral extent of impacts. SB-4 did not display indicators of petroleum impact. SB-5 detected slight petroleum staining and odors at approximately 5 ft bgs. SS-3 was collected from SB-5 at 5 ft bgs. Typical brown -tan sandy Silts were encountered in the soil borings. Soil samples collected were bottled for submittal to a North Carolina certified The Heritage at UNCC SUMMIT Project No. 5778.500 Charlotte, North Carolina November 25, 2019 laboratory for analysis of BTEX, Naphthalene and Poly -cyclic Aromatic Hydrocarbons (PAHs). (It should be noted that groundwater was not encountered) Laboratory results were compared to North Carolina Department of Environmental Quality (NCDEQ) Maximum Soil Contaminant Concentrations (MSCCs). Table 1.0 attached to this document summarizes the detections. As indicated on the attached summary table, sample SS-1, collected at 5 ft bgs adjacent to the northern tank end, detected the presence of petroleum compound Naphthalene above the established Soil to Groundwater MSCC. No detections were reported for SS- 2 or SS-3. Based on the results of our inspection, SUMMIT concludes that the HHO USTs has released petroleum products into the surrounding soils. Per NCDEQ regulations, the UST owner is required to submit a 24-Hour Release notification (Form UST-6 1). A copy of this form is attached to this letter and a copy can be obtained at https://deq.nc.gov/about/divisions/waste-management/ust/forfns. A copy of this limited assessment should be submitted along with the UST 61 to the NCDEQ Mooresville Regional Office. SUMMIT recommends the removal and proper closure of the UST in accordance with NCDEQ UST guidelines. Based on the detections of concentrations above the established Residential MSCCs, the Notice of Residual Petroleum (NRP) would be required if soils are to remain in place following UST removal. Soil over -excavation would be required in order to avoid an NRP and receive a No Further Action status from NCDEQ. This letter includes a description of the methodology of our investigation and a summary of our findings and conclusions. If you have any questions regarding our assessment of the subject property, our conclusions or recommendations, please do not hesitate to call us at (704) 504-1717. Sincerely, SUMMIT ENGINEERING, LABORATORY & TESTING, P.C. Patrick W. Lowery, PG Senior Environmental Manager Attachments Table 1.0 — Summary of Soil Detections (3 pages) Site Figures Analytical Laboratory Report UST 61 Morgan W. Drakeford, SC Forester # 1805 Environmental Professional ENGINEERING IN • LABORATORY • TESTING 3575 Centre Circle Drive I Fort Mill, South Carolina 29715 1 (704) SW - 1717 1 (704) 504 - 1125 (Fox) WVI W. UMMIT- MPANIE . M The Heritage at UNCC Charlotte, North Carolina APPENDIX I TABLES SUMMIT Project No. 5778.500 November 25, 2019 DA\Project Forms\Projects\5778.500 The UNCC Heritage Phase I - Test Pits\Phase II\Appendix Lrtf Page 1 of 1 TABLE 1.0 - Summary of Soil Detections (Continued) Project: Heritage Project #: 5778.5 Analytical Method (e.g., VOC by EPA 8260) 8260B 8260B 8260B 8270D 8270D 8270D 4 Contaminant of Concern o Incident Sample Date Source Sample Phase Cd C Collected Depth (ft (Closure, ID (m/dd/yy) Area BGS), 20Day, W Z > d Z a LSA, etc... SS-1 11/8/2019 Tank End 5 Initial 0.011 5.8 0.0 .470 J 5.8 3.4 SS-2 11/8/2019 Tank End 7 Initial ND ND ND ND ND ND SS-3 11/8/2019 Offset 5 Initial ND ND ND ND ND ND Minimum Reporting Limit m /k 0.002 0.300 0.0041 0.290 0.3 0.250 Soil to groundwater MSCC m /k 4.9 0.160 4.60 940 0.160 56 Residential MSCC m /k' 1590 313 3129 4600 313 469 Industrial/Commercial MSCC m /k 400001 8176 81760 1220001 81761 12264 Bold -Reported concentration exceeds Soil to Groundwater MSCC Bold -Reported concentration exceeds Residential MSCC ND - Non Detection NA - Not Available The Heritage at UNCC Charlotte, North Carolina APPENDIX II FIGURES SUMMIT Project No. 5778.500 November 25, 2019 DA\Project Forms\Projects\5778.500 The UNCC Heritage Phase I - Test Pits\Phase II\Appendix II.rtf Image rroviaea try r-um uaua LA ►i• r go. "ah r I L _ I � �s r � •�fl y f �r e Boundaries are SUMMIT ENGINEERING • LABORATORY • TESTING rl 1� l TOPOGRAPHIC MAP The Heritage at UNCC 300 Heritage Lake Drive Charlotte, North Carolina 28262 10/31 /2019 Image rrovlaea Isy rarer oireei FGallaway Rd N t � R ell �gert ar���� Glen DT University city North SUMMIT ENGINEERING • LABORATORY. TESTING Sir.q,1f �5 o� a� �S t 0 Z `L0 r Boundaries are approximate SITE LOCATION MAP The Heritage at UNCC 300 Heritage Lake Drive Charlotte, North Carolina 28262 10/31 /2019 //Aa& SUMMIT Aspen Heights Partners Scale 8008 Corporate Center Drive, Suite 201 Charotte, NC 28226 t ivy T Checked By\Date: MZ/11/19 Aerial Map 9920 Mallard Glen Drive Charlotte, North Carolina NTS Figure 1 Well House Gravel Driveway —40' i i i i i i i i "35' S B-4 SS,1 (5' bgs) SS; 2 (7' bgs) ~® SB-5 SB 2 SS-3 (5' bgs) UST 4x8 ® SB-3 ------------------- Gravel Driveway The Heritage at UNCC Charlotte, North Carolina APPENDIX III SUMMIT Project No. 5778.500 November 25, 2019 ANALYTICAL LABORATORY REPORT DA\Project Forms\Projects\5778.500 The UNCC Heritage Phase I - Test Pits\Phase II\Appendix III.rtf SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis SUMMIT Engineering, Laboratory & Testing, P.C. 3575 Centre Circle Fort Mill, SC 28715 Attention: Patrick Lowery Project Name: Heritage Project Number: 5778.5 Lot Number:UK08120 Date Completed:11/15/2019 11 /15/2019 2:37 PM Approved and released by: Lab Director - Greenville: Lucas Odom pCCRF�4 AM AC CF ED I T E D qB 11900 ELAP The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 1 of 23 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative SUMMIT Engineering, Laboratory & Testing, P.C. Lot Number: UK08120 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. PAHs by GC/MS The following sample was diluted due to the nature of the sample matrix: UK08120-003. The LOQ has been elevated to reflect the dilution. VOCs by GC/MS The following sample was diluted due to the nature of the sample matrix: UK08120-003. The LOQ has been elevated to reflect the dilution. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 23 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary SUMMIT Engineering, Laboratory & Testing, P.C. Lot Number: UK08120 Sample Number Sample ID Matrix Date Sampled Date Received 001 SS-1 Solid 11/08/20191000 11/08/2019 002 SS-2 Solid 11/08/20191020 11/08/2019 003 SS-3 Solid 11/08/20191040 11/08/2019 (3 samples) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 23 SHEALY ENVIRONMENTAL SERVICES, INC. Detection Summary SUMMIT Engineering, Laboratory & Testing, P.C. Lot Number: UK08120 Sample Sample ID Matrix Parameter Method Result Q Units Page 001 SS-1 Solid Ethylbenzene 8260B 11 ug/kg 5 001 SS-1 Solid Naphthalene 8260B 5800 ug/kg 5 001 SS-1 Solid Xylenes (total) 8260B 33 ug/kg 5 001 SS-1 Solid Anthracene 8270D 470 J ug/kg 5 001 SS-1 Solid Naphthalene 8270D 5800 ug/kg 5 001 SS-1 Solid Phenanthrene 8270D 3400 ug/kg 5 (6 detections) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 23 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:UK08120-001 Description: SS-1 Matrix: Solid Date Sampled:11/08/2019 1000 % Solids: 86.7 11/09/2019 0343 )ate Received: 11 /08/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260B 1 11/13/2019 0222 ALR1 35469 5.65 2 5035 High 8260B 1 11/13/2019 2238 ALR1 35622 5.51 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 8260B ND 5.1 2.0 ug/kg 1 Ethylbenzene 100-41-4 8260B 11 5.1 2.0 ug/kg 1 Naphthalene 91-20-3 8260B 5800 300 120 ug/kg 2 Toluene 108-88-3 8260B ND 5.1 2.0 ug/kg 1 Xylenes (total) 1330-20-7 8260B 33 10 4.1 ug/kg 1 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits 1,2-Dichloroethane-d4 82 53-142 76 53-142 Bromofluorobenzene 92 47-138 85 47-138 Toluene-d8 106 68-124 84 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270D 100 11/12/2019 2022 SCD 11/11/2019 2045 35280 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 8270D ND 1500 560 ug/kg 1 Acenaphthylene 208-96-8 8270D ND 1500 350 ug/kg 1 Anthracene 120-12-7 8270D 470 J 1500 290 ug/kg 1 Benzo(a)anthracene 56-55-3 8270D ND 1500 220 ug/kg 1 Benzo(a)pyrene 50-32-8 8270D ND 1500 190 ug/kg 1 Benzo(b)fluoranthene 205-99-2 8270D ND 1500 220 ug/kg 1 Benzo(g,h,i)perylene 191-24-2 8270D ND 1500 420 ug/kg 1 Benzo(k)fluoranthene 207-08-9 8270D ND 1500 240 ug/kg 1 Chrysene 218-01-9 8270D ND 1500 340 ug/kg 1 Dibenzo(a,h)anthracene 53-70-3 8270D ND 1500 330 ug/kg 1 Fluoranthene 206-44-0 8270D ND 1500 240 ug/kg 1 Fluorene 86-73-7 8270D ND 1500 210 ug/kg 1 Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1500 300 ug/kg 1 Naphthalene 91-20-3 8270D 5800 1500 520 ug/kg 1 Phenanthrene 85-01-8 8270D 3400 1500 250 ug/kg 1 Pyrene 129-00-0 8270D ND 1500 310 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 125 24-137 Nitrobenzene-d5 90 12-144 Terphenyl-d14 100 20-127 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5 of 23 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:UK08120-002 Description: SS-2 Matrix: Solid Date Sampled:11/08/2019 1020 % Solids: 85.7 11/09/2019 0343 Date Received: 11 /08/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 1 5035 8260B 1 11/13/2019 0244 ALR1 35469 5.60 2 5035 8260B 1 11/14/2019 0009 ALR1 35621 5.57 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 8260B ND 5.2 2.1 ug/kg 1 Ethylbenzene 100-41-4 8260B ND 5.2 2.1 ug/kg 1 Naphthalene 91-20-3 8260B ND 5.2 2.1 ug/kg 2 Toluene 108-88-3 8260B ND 5.2 2.1 ug/kg 1 Xylenes (total) 1330-20-7 8260B ND 10 4.2 ug/kg 1 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits 1,2-Dichloroethane-d4 79 53-142 79 53-142 Bromofluorobenzene 100 47-138 100 47-138 Toluene-d8 96 68-124 95 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270D 1 11/12/2019 1957 SCD 11/11/2019 2045 35280 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 8270D ND 15 5.6 ug/kg 1 Acenaphthylene 208-96-8 8270D ND 15 3.6 ug/kg 1 Anthracene 120-12-7 8270D ND 15 2.9 ug/kg 1 Benzo(a)anthracene 56-55-3 8270D ND 15 2.2 ug/kg 1 Benzo(a)pyrene 50-32-8 8270D ND 15 1.9 ug/kg 1 Benzo(b)fluoranthene 205-99-2 8270D ND 15 2.2 ug/kg 1 Benzo(g,h,i)perylene 191-24-2 8270D ND 15 4.2 ug/kg 1 Benzo(k)fluoranthene 207-08-9 8270D ND 15 2.4 ug/kg 1 Chrysene 218-01-9 8270D ND 15 3.5 ug/kg 1 Dibenzo(a,h)anthracene 53-70-3 8270D ND 15 3.3 ug/kg 1 Fluoranthene 206-44-0 8270D ND 15 2.4 ug/kg 1 Fluorene 86-73-7 8270D ND 15 2.2 ug/kg 1 Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 15 3.0 ug/kg 1 Naphthalene 91-20-3 8270D ND 15 5.2 ug/kg 1 Phenanthrene 85-01-8 8270D ND 15 2.5 ug/kg 1 Pyrene 129-00-0 8270D ND 15 3.2 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 88 24-137 Nitrobenzene-d5 96 12-144 Terphenyl-d14 106 20-127 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 23 Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory ID:UK08120-003 Description: SS-3 Matrix: Solid Date Sampled:11/08/2019 1040 % Solids: 82.8 11/09/2019 0343 Date Received: 11 /08/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 2 5035 High 8260B 1 11/13/2019 2301 ALR1 35622 4.76 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 8260B ND 370 150 ug/kg 2 Ethylbenzene 100-41-4 8260B ND 370 150 ug/kg 2 Naphthalene 91-20-3 8260B ND 370 150 ug/kg 2 Toluene 108-88-3 8260B ND 370 150 ug/kg 2 Xylenes (total) 1330-20-7 8260B ND 740 300 ug/kg 2 Run 2 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 81 53-142 Bromofluorobenzene 85 47-138 Toluene-d8 86 68-124 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270D 50 11/12/2019 1817 SCD 11/11/2019 2045 35280 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 8270D ND 800 300 ug/kg 1 Acenaphthylene 208-96-8 8270D ND 800 190 ug/kg 1 Anthracene 120-12-7 8270D ND 800 150 ug/kg 1 Benzo(a)anthracene 56-55-3 8270D ND 800 120 ug/kg 1 Benzo(a)pyrene 50-32-8 8270D ND 800 100 ug/kg 1 Benzo(b)fluoranthene 205-99-2 8270D ND 800 120 ug/kg 1 Benzo(g,h,i)perylene 191-24-2 8270D ND 800 230 ug/kg 1 Benzo(k)fluoranthene 207-08-9 8270D ND 800 130 ug/kg 1 Chrysene 218-01-9 8270D ND 800 190 ug/kg 1 Dibenzo(a,h)anthracene 53-70-3 8270D ND 800 180 ug/kg 1 Fluoranthene 206-44-0 8270D ND 800 130 ug/kg 1 Fluorene 86-73-7 8270D ND 800 120 ug/kg 1 Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 800 160 ug/kg 1 Naphthalene 91-20-3 8270D ND 800 280 ug/kg 1 Phenanthrene 85-01-8 8270D ND 800 130 ug/kg 1 Pyrene 129-00-0 8270D ND 800 170 ug/kg 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 130 24-137 Nitrobenzene-d5 N 211 12-144 Terphenyl-d14 95 20-127 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 23 QC Summary Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 23 Volatile Organic Compounds by GC/MS - MB Sample ID: UQ35469-001 Matrix: Solid Batch: 35469 Prep Method: 5035 Analytical Method: 8260B Parameter Result Q Dil LOQ DL Units Analysis Date Benzene ND 1 5.0 2.0 ug/kg 11/12/2019 2111 Ethylbenzene ND 1 5.0 2.0 ug/kg 11/12/2019 2111 Toluene ND 1 5.0 2.0 ug/kg 11/12/2019 2111 Xylenes (total) ND 1 10 4.0 ug/kg 11/12/2019 2111 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 84 53-142 Bromofluorobenzene 100 47-138 Toluene-d8 98 68-124 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9 of 23 Volatile Organic Compounds by GC/MS - LCS Sample ID: UQ35469-002 Matrix: Solid Batch: 35469 Prep Method: 5035 Analytical Method: 8260B Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Benzene 50 48 1 96 70-130 11/12/2019 2008 Ethylbenzene 50 50 1 101 70-130 11/12/2019 2008 Toluene 50 49 1 98 70-130 11/12/2019 2008 Xylenes (total) 100 100 1 101 70-130 11/12/2019 2008 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 86 53-142 Bromofluorobenzene 103 47-138 Toluene-d8 101 68-124 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 23 Volatile Organic Compounds by GC/MS - LCSD Sample ID: UQ35469-003 Matrix: Solid Batch: 35469 Prep Method: 5035 Analytical Method: 8260B Spike Amount Result % Rec % RPD Parameter (ug/kg) (ug/kg) Q Dil % Rec % RPD Limit Limit Analysis Date Benzene 50 46 1 93 3.4 70-130 20 11/12/2019 2031 Ethylbenzene 50 49 1 98 3.1 70-130 20 11/12/2019 2031 Toluene 50 49 1 98 0.28 70-130 20 11/12/2019 2031 Xylenes (total) 100 98 1 98 2.4 70-130 20 11/12/2019 2031 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 83 53-142 Bromofluorobenzene 99 47-138 Toluene-d8 98 68-124 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 11 of 23 Volatile Organic Compounds by GC/MS - MB Sample ID: UQ35621-001 Matrix: Solid Batch:35621 Prep Method: 5035 Analytical Method: 8260B Parameter Result Q Dil LOQ DL Units Analysis Date Naphthalene ND 1 5.0 2.0 ug/kg 11/13/2019 2157 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 80 53-142 Bromofluorobenzene 99 47-138 Toluene-d8 96 68-124 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 23 Volatile Organic Compounds by GC/MS - LCS Sample ID: UQ35621-002 Matrix: Solid Batch:35621 Prep Method: 5035 Analytical Method: 8260B Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Naphthalene 50 50 1 101 70-130 11 /13/2019 1958 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 79 53-142 Bromofluorobenzene 98 47-138 Toluene-d8 96 68-124 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 13 of 23 Volatile Organic Compounds by GC/MS - LCSD Sample ID: UQ35621-003 Matrix: Solid Batch:35621 Prep Method: 5035 Analytical Method: 8260B Spike Amount Result % Rec % RPD Parameter (ug/kg) (ug/kg) Q Dil % Rec % RPD Limit Limit Analysis Date Naphthalene 50 51 1 101 0.53 70-130 20 11/13/2019 2020 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 77 53-142 Bromofluorobenzene 95 47-138 Toluene-d8 97 68-124 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 14 of 23 Volatile Organic Compounds by GC/MS - MB Sample ID: UQ35622-001 Matrix: Solid Batch: 35622 Prep Method: 5035 High Analytical Method: 8260B Parameter Result Q Dil LOQ DL Units Analysis Date Benzene ND 1 250 100 ug/kg 11/13/2019 2122 Ethylbenzene ND 1 250 100 ug/kg 11/13/2019 2122 Naphthalene ND 1 250 100 ug/kg 11/13/2019 2122 Toluene ND 1 250 100 ug/kg 11/13/2019 2122 Xylenes (total) ND 1 500 200 ug/kg 11/13/2019 2122 Surrogate Q % Rec Acceptance Limit 1,2-Dichloroethane-d4 83 53-142 Bromofluorobenzene 93 47-138 Toluene-d8 91 68-124 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 15 of 23 Volatile Organic Compounds by GC/MS - LCS Sample ID: UQ35622-002 Matrix: Solid Batch: 35622 Prep Method: 5035 High Analytical Method: 8260B Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Benzene 2500 2400 1 96 70-130 11/13/2019 2059 Ethylbenzene 2500 2700 1 106 70-130 11/13/2019 2059 Naphthalene 2500 2500 1 102 70-130 11/13/2019 2059 Toluene 2500 2600 1 104 70-130 11/13/2019 2059 Xylenes (total) 5000 5300 1 106 70-130 11/13/2019 2059 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 79 53-142 Bromofluorobenzene 93 47-138 Toluene-d8 91 68-124 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 16 of 23 Semivolatile Organic Compounds by GC/MS - MB Sample ID: UQ35280-001 Matrix: Solid Batch: 35280 Prep Method: 3546 Analytical Method: 8270D Prep Date: 11/11/2019 2045 Parameter Result Q Dil LOQ DL Units Analysis Date Acenaphthene ND 1 13 5.0 ug/kg 11/12/20191431 Acenaphthylene ND 1 13 3.2 ug/kg 11/12/20191431 Anthracene ND 1 13 2.6 ug/kg 11/12/20191431 Benzo(a)anthracene ND 1 13 2.0 ug/kg 11/12/20191431 Benzo(a)pyrene ND 1 13 1.7 ug/kg 11/12/20191431 Benzo(b)fluoranthene ND 1 13 1.9 ug/kg 11/12/20191431 Benzo(g,h,i)perylene ND 1 13 3.8 ug/kg 11/12/20191431 Benzo(k)fluoranthene ND 1 13 2.1 ug/kg 11/12/20191431 Chrysene ND 1 13 3.1 ug/kg 11/12/20191431 Dibenzo(a,h)anthracene ND 1 13 3.0 ug/kg 11/12/20191431 Fluoranthene ND 1 13 2.2 ug/kg 11/12/20191431 Fluorene ND 1 13 1.9 ug/kg 11/12/20191431 Indeno(1,2,3-c,d)pyrene ND 1 13 2.7 ug/kg 11/12/20191431 Naphthalene ND 1 13 4.7 ug/kg 11/12/20191431 Phenanthrene ND 1 13 2.3 ug/kg 11/12/20191431 Pyrene ND 1 13 2.8 ug/kg 11/12/20191431 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 89 24-137 Nitrobenzene-d5 100 12-144 Terphenyl-d14 116 20-127 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 17 of 23 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: UQ35280-002 Matrix: Solid Batch: 35280 Prep Method: 3546 Analytical Method: 8270D Prep Date: 11/11/2019 2045 Spike Amount Result % Rec Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Acenaphthene 670 550 1 83 46-114 11/12/20191456 Acenaphthylene 670 580 1 87 44-122 11/12/20191456 Anthracene 670 620 1 93 50-119 11/12/20191456 Benzo(a)anthracene 670 600 1 90 47-121 11/12/20191456 Benzo(a)pyrene 670 630 1 94 55-134 11/12/20191456 Benzo(b)fluoranthene 670 550 1 83 28-139 11/12/20191456 Benzo(g,h,i)perylene 670 700 1 105 36-125 11/12/20191456 Benzo(k)fluoranthene 670 550 1 82 47-130 11/12/20191456 Chrysene 670 630 1 95 45-126 11/12/20191456 Dibenzo(a,h)anthracene 670 660 1 100 45-122 11/12/20191456 Fluoranthene 670 610 1 92 50-123 11/12/20191456 Fluorene 670 590 1 89 48-117 11/12/20191456 Indeno(1,2,3-c,d)pyrene 670 650 1 97 45-123 11/12/20191456 Naphthalene 670 560 1 84 36-110 11/12/20191456 Phenanthrene 670 590 1 89 49-117 11/12/20191456 Pyrene 670 590 1 88 47-119 11/12/20191456 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 88 24-137 Nitrobenzene-d5 112 12-144 Terphenyl-d14 107 20-127 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 18 of 23 Semivolatile Organic Compounds by GC/MS - MS Sample ID: UK08120-001 MS Matrix: Solid Batch: 35280 Prep Method: 3546 Analytical Method: 8270D Prep Date: 11/11/2019 2045 Sample Spike Amount Amount Result % Rec Parameter (ug/kg) (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date Acenaphthene ND 750 1300 N 100 167 46-114 11/12/2019 2047 Acenaphthylene ND 750 1500 N 100 201 44-122 11/12/2019 2047 Anthracene 470 750 1400 100 119 50-119 11/12/2019 2047 Benzo(a)anthracene ND 750 1000 N 100 133 47-121 11/12/2019 2047 Benzo(a)pyrene ND 750 700 100 93 55-134 11/12/2019 2047 Benzo(b)fluoranthene ND 750 700 100 93 28-139 11/12/2019 2047 Benzo(g,h,i)perylene ND 750 460 100 61 36-125 11/12/2019 2047 Benzo(k)fluoranthene ND 750 680 100 90 47-130 11/12/2019 2047 Chrysene ND 750 770 100 102 45-126 11/12/2019 2047 Dibenzo(a,h)anthracene ND 750 ND N 100 0.00 45-122 11/12/2019 2047 Fluoranthene ND 750 1000 N 100 136 50-123 11/12/2019 2047 Fluorene ND 750 2700 N 100 365 48-117 11/12/2019 2047 Indeno(1,2,3-c,d)pyrene ND 750 ND N 100 0.00 45-123 11/12/2019 2047 Naphthalene 5800 750 6600 100 101 36-110 11/12/2019 2047 Phenanthrene 3400 750 4300 100 117 49-117 11/12/2019 2047 Pyrene ND 750 820 100 109 47-119 11/12/2019 2047 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 121 24-137 Nitrobenzene-d5 31 12-144 Terphenyl-d14 98 20-127 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 19 of 23 Semivolatile Organic Compounds by GC/MS - MSD Sample ID: UK08120-001 MD Matrix: Solid Batch: 35280 Prep Method: 3546 Analytical Method: 8270D Prep Date: 11/11/2019 2045 Sample Spike Amount Amount Result % Rec % RPD Parameter (ug/kg) (ug/kg) (ug/kg) Q Dil % Rec % RPD Limit Limit Analysis Date Acenaphthene ND 760 1100 N 100 139 17 46-114 30 11/12/2019 2112 Acenaphthylene ND 760 1300 N 100 173 14 44-122 30 11/12/2019 2112 Anthracene 470 760 1300 100 112 3.4 50-119 30 11/12/2019 2112 Benzo(a)anthracene ND 760 1000 N 100 130 0.76 47-121 30 11/12/2019 2112 Benzo(a)pyrene ND 760 680 100 89 3.7 55-134 30 11/12/2019 2112 Benzo(b)fluoranthene ND 760 710 100 94 2.0 28-139 30 11/12/2019 2112 Benzo(g,h,i)perylene ND 760 ND N,+ 100 0.00 200 36-125 30 11/12/2019 2112 Benzo(k)fluoranthene ND 760 720 100 94 5.2 47-130 30 11/12/2019 2112 Chrysene ND 760 810 100 106 5.2 45-126 30 11/12/2019 2112 Dibenzo(a,h)anthracene ND 760 ND N 100 0.00 0.00 45-122 30 11/12/2019 2112 Fluoranthene ND 760 1100 N 100 150 11 50-123 30 11/12/2019 2112 Fluorene ND 760 2700 N 100 359 0.11 48-117 30 11/12/2019 2112 Indeno(1,2,3-c,d)pyrene ND 760 ND N 100 0.00 0.00 45-123 30 11/12/2019 2112 Naphthalene 5800 760 6200 100 50 6.0 36-110 30 11/12/2019 2112 Phenanthrene 3400 760 4100 100 93 4.1 49-117 30 11/12/2019 2112 Pyrene ND 760 990 N 100 130 19 47-119 30 11/12/2019 2112 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 128 24-137 Nitrobenzene-d5 21 12-144 Terphenyl-d14 95 20-127 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 20 of 23 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 21 of 23 SHEALY ENVIRONMENTAL SERVICES. INC. g J "I 4S E E IZZ E i r R HT U. o G YO �L-j Ldj _ C u�y SHVd K j El I o FFrt� �J t IN IN139 } a � F 140rN q12 — Ot4 U-1 > LZ caa Y :QNFI — LU — Z ti P S7FI x enaan H- o ,J c a� ell�a J �R3 4 E eo 0 > �' a ,. o S J. VJ q � � O a- r T A I` '►M S 3 Z� lla +•1 e s o IL ` V E e v m 7 13 —_ Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 22 of 23 SHEALY ENVIRONMENTAL SERVICES, INC. Sheaf &vlronmcntal SrTvum, Im Pugs 1 nF1 Pxrurami Nnrnhs MFM I Rf r 14 Ef Edda-Wim. W2120111 Sample ReeALApt Clk"I list { RQ C',licrll.: 5111013it Cooler lnsuccted bvidate: WO 11N4119 1_a 4: UKOS120 ';,kEtnyof r4; ipt; &3 5U31 ❑ C<ILunt ❑ UP5 ❑ FedEx n Other: Yes I W1 No m m 11, Wcrc custody seals present on the cooler'' 1-1 Yes Nu-1 14NA 12. if cost ' seals were vent, a erg hkm intact and tutor oke,l? phi Strip FD: NA Chlurinc Strip lb: TEA T W by; NA rJrigiaal temperature upon receipt f 37eriv cl (CQrrcetcd) L-mperatuiv upon receipt %,gcFlid Snap -Cup lb: 19-1616 11 11.8 -' NA ,'Kk -,C NA ?VA_wC: NA .,,NA EC MQ:Lhudl. ®'I mp iratilrc Nail EjrL�,ainst Baal as TR Gun 111 � _ IR Chen Carreaiai rm=Lur 0 °C`- ahod of coolant Q1 U10 Ice ❑ 1L:v Pack; ❑ TIlry Xaa ❑ None D No I1 NA I' If temperature of any cooler exceeded 6.0°C. vh%9 Project Manager K ntifmd? PM -,vas N otifred bv" phatie ? email 1 rave-lu-fax (chic one)- ❑ N(1 I1NA - Is the cornm&eial anurieT'R packing slip a[#adjed [o Ulis Corm? El No 5. Wam prupe_� custody pmMduTex (Telinqu3shedfrefielv�(E) toila,4td? FU0001yyy Ntl 6. Were sample If]5 IiSRCtI on the COC' ❑ No 7- Weir sample fl]� IiAW un all sample ommjn='' n No �.Was coIlectinn dale & Ili= listed on the C.00? ❑1Ko Was Colleetiva data & time listed On a.11 5XIn le GOI!Aaint�? ❑ l+o 10. Did all c4ntalioet Lobel informs#ion (11), date, Lime) p with flee COCe- ❑ Nq 11. Were tests to bs performed listed.011 the CQC? 0 Yes ❑ No 12. Did 3l1.3alripks ard%-. in did prnper containers for pact test andlor in good SonCli[iwl (unhlnlcpn, lids an, etc-)'' Yes ❑ No 13. %Ym adequate sample volume avail W7 Ycs —Yes TO =4. �4�crc all sainplest+et6i1,etl witllin V2 the holding Emu ur48 hours. whichever rorlu's lill'Sto CT ®Vo h 5. Ware any sam ley eorttairmm miss in 'excess (cirele one) samples Not lis[erl on (,'O '? ❑ YC5 ❑ L Il} rJ 1r7711 1 A 1f1- Fur VOA and RSK-175 samples, were bubbles present zzF-viae'd (�."or 6mrn in diameter) in env of the VOA AaW.. ❑ Yes ❑ IVU NA 17-'None all DR4Xm,4al9rnutrient sam les receivext at N pH of<2F Yes No O NA 18. %Vera W1 cyanidg yam pies received at a VH > 12 and sul fide s¢utlpl es received at a114> 9? ❑ Y�-v ❑ No O NA 19. Were a]I applicahle ?wl s KNJcyanideefpberllrli62;5 (< 0.51nprL) sample[~ free of rest u l El Y` El ri!o 1 A {11- Wem+:limln eremarkwrequ sty (i& mque5tcd dIlutio , MF ISD d.esigna11411$, Q'lr C..,) Gun-x:tly trameribed ftm the Coe into the cammellt secnon in L[M$? Li YA yj 1'10 21. Was the tjwle riumbu 16tcd on the cowaiMrr EPba"' li es Qkjoue 4 NA Sampic PreservaticA (MLNt he couiplexed for !]Lk.Y npi�{:) incorreorTy preserved or with headspace.) tialnple(s) NA were 1+meiVerf-lwcrrm ly pl�erv�ed anriwcre adjusted a"ar-dingly Insamp[e recei*drigwith NA _ny1.ofciruic r1nC; H2Sb4, 111103, HCI.NR011 usirig RR 9 NA 13irre t)t'preservation NA TFrnom than one prese;ryalivr is netadod, pieagn-note iti 111W COITIMe11ts brio'Lv. ample(3) were received with bubbles >6 rllm in diametier err,p[cs(s) NA wcne received -,with TRC > 4.5 ing, !- (1f 419 is no) and wem 4LLetcd acoordin¢ly in 5drnp]e! receiving with sodium thiowlfate (NSzSz0a) with Shealy TD. NA SR barcede labels applied bl'; B[b G7SH lam- 11MV19 C4mmerlts.• . Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 23 of 23 The Heritage at UNCC Charlotte, North Carolina APPENDIX IV UST 61 SUMMIT Project No. 5778.500 November 25, 2019 DA\Project Forms\Projects\5778.500 The UNCC Heritage Phase I - Test Pits\Phase II\Appendix IV.rtf UST-61 24-Hour Release and UST Leak Reporting Form. For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or in NC suspected release (DWM USE ONLY) Suspected Contamination? (Y/N) Facility ID Number Incident # Risk (H,I,L,U) Confirmed GW Contamination? (Y/N) Date Leak Discovered Received On Received By Confirmed Soil Contamination ?(Y/N) Comm/Non-Commercial? Reported by (circle one): Phone, Fax or Report Samples Taken?(Y/N) Reg/Non-regulated? Region Free Product? (Y/N) If Yes, State Greatest Thickness INCIDENT DESCRIPTION Incident Name: Address: County: Regional Office (circle one): Asheville, Mooresville, Fayetteville, City/Town: Zip Code: Raleigh, Washington, Wilmington, Winston-Salem Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by: ❑GPS Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors) ❑Topographic map ❑GIS Address matching ❑Other ❑ Unknown Describe location: HOW RELEASE WAS DISCOVERED (Release code) (Check one) ❑Release Detection Equipment or Methods ❑Visual/Odor ❑Groundwater Contamination ❑During UST Closure/Removal ❑Water in Tank ❑Surface Water Contamination ❑Property Transfer ❑Water Supply Well Contamination ❑Other (specify) SOURCE OF CONTAMINATION Source of Release Cause of Release Type of Release Product Type Released (Check primary source) (Check primary cause) (Check one) (Check primary product type released) ❑ Tank ❑ Spill ❑ Petroleum ❑ Gasoline/ Diesel/ ❑ Diesel/Veg. Oil ❑ Piping ❑ Overfill ❑ Non -Petroleum Kerosene Blend ❑ Dispenser ❑Heating Oil ❑ Vegetable Oil 100% Corrosion Both ❑❑ ❑ Other Petroleum ❑ E10 - E20 ❑ Submersible Turbine Pump ❑Physical/Mechanical ❑ Delivery Problem Location Products Damage ❑ E21 - E84 (Check one) Metals ❑ ❑ Install Problem ❑ E85 - E99 ❑ Spill Bucket ❑ Other Inorganics ❑ Other [-]Facility ❑Ethanol 100% ❑ Other ❑ Other Organics ❑ Unknown ❑Residence ❑ E01 - E09 ❑ Unknown ❑Other Definitions presented on reverse Definitions presented on reverse Ownership 1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining UST Form 61 (02/19) Page 1 of 2 IMPACT ON DRINKING WATER SUPPLIES Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected Water Supply Wells Contaminated: 1. 2. 3. (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) UST Owner/Company UST SYSTEM OWNER Point of Contact Address City State Zip Code Telephone Number UST SYSTEM OPERATOR UST Operator/Company Address City State Zip Code Telephone Number LANDOWNER AT LOCATION OF UST INCIDENT Landowner Address City State Zip Code Telephone Number Draw Sketch of Area (showing two major road intersections) or Attach Map Person Reporting Incident Company Telephone Number Title Address Date UST Form 61 (02/19) Page 2 of 2 Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined Beverly, Trudy From: Patrick Lowery <plowery@summit-companies.com> Sent: Monday, April 19, 2021 1:08 PM To: Beverly, Trudy Subject: RE: [External] Release Notification - 9920 Mallard Glen Drive CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Hi Trudy, Thanks for sending over this information. Im working up the IAA report for this closure and ran into an issue. Just wanted to confirm with you before we jumped back in the field. We did the initial closure and had exceedances of the MSCC Soil to groundwater in a few sidewalls and base. The developer wants to go for clean closure so we went out and pulled more soil out. All sidewalls were excavated and base. We collected samples from the sidewalls and base that we determined to be over MSCC. I overlooked a sidewall that had previously shown 0.061 mg/kg benzo(a)pyrene above the Soil to Groundwater of 0.058 mg/k and Aromatics at 53 mg/kg above the 31 mg/kg MSCC. We did remove more from that sidewall, but I do not have a confirmation sample. If submitted as is, would you need that sidewall sample for NFA? If so, can we run only the analysis for the compound that was above MSCC (PAHs, EPH/VPH for this one) previously? Feel free to call my cell if that is easier. Thanks for your help. Patrick PATRICK W. LOWERY, P.G. Senior Environmental Manager plowery@summit-companies.com Columbia Office • 101 Rice Bent Way, Unit 9 • Columbia, SC 29229 803.708.7945 Office • 803.708.7946 Fax • 803.230.5087 Cell www.summit-companies.com Charlotte -HQ • Raleigh • Columbia • Greenville • Charleston From: Beverly, Trudy <trudy.beverly@ncdenr.gov> Sent: Monday, April 5, 2021 3:43 PM To: Patrick Lowery <plowery@summit-companies.com> Subject: RE: [External] Release Notification - 9920 Mallard Glen Drive Hey Patrick, Incident #47669 Updated guidance documents were put on the UST website 1/19/2021. Report templates can be found at the following link Comprehesive Guidelines Appendices or STIRA, Assessment Guidelines and Corrective Action Guidelines (appendices) https://deg.nc.gov/about/divisions/waste-management/ust/guidance-documents (starts on page 25 of 211) Appendix A 8. Initial Abatement Action (Site Check, UST Closure with UST-2 Form, Excavation, Post -Excavation Soil Contamination Assessment) Report Trudy Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality UST Section, Mooresville Regional Office r4rvnR mt qu.Yry�` 704.235.2182 (Office) Trudy.B everly(ancdenr. gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: hit2s://deq.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: hitps://deg.nc.gov/about/divisions/waste-management/ust/ast-proeram INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: https://dea.nc. eov/about/divisions/waste-manaaement/waste-management-rules-data/waste-management-eis-mans File Review Procedures: https://deq.nc. gov/about/divisions/waste-mana2ement/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): hitps://deq.nc.gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: htti)s:Hfiles.nc.¢ov/ncdea/Waste%2OManaizement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policv.adf https:Hfiles.nc. gov/ncdeq/Waste%2OManagement/D WMiUST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx From: Patrick Lowery [mailto:plowery@summit-companies.com] Sent: Monday, April 5, 2021 2:14 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: RE: [External] Release Notification - 9920 Mallard Glen Drive CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to Report Spam. Trudy, Good afternoon. We submitted the attached release notification last May for the heating oil tank at 9920 Mallard Glen Drive. I cant seem to locate a incident # for this release on laserfiche or DWM GIS. Not sure this one got logged in as I initially sent this over to Dan. Either way, our client finely moved forward with closure earlier this year and we need to submit the documentation for closure. Soil was excavated and we were able to get clean margins on all 4 sidewalls and base. Looking at the updated Corrective Action report formats, it looks like the Initial Abatement Action report is no longer presented. Would we be going the format for Soil Cleanup with Closure Request (#12)? Since this appears new I wanted to reach out and get your advise on how to proceed. Could you point me to a recent approved heating oil tank closure site that I can look up and review to ensure I cover all my bases. I will have a few more of these to produce so I want to be sure I get you exactly what you are needing. Feel free to call me on my cell at 803-230-5087 anytime. Thank you, Patrick From: Patrick Lowery Sent: Monday, May 4, 2020 11:48 AM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: RE: [External] Release Notification - 9920 Mallard Glen Drive Thank you Trudy. I will keep your information for future notifications. Thanks Patrick From: Beverly, Trudy <trudy.beverly@ncdenr.gov> Sent: Monday, May 4, 2020 6:35 AM To: Patrick Lowery <plowery@summit-companies.com> Subject: RE: [External] Release Notification - 9920 Mallard Glen Drive Good Morning Patrick, I handle non -regulated ust releases in Mecklenburg County. Please send future Mecklenburg County non -regulated ust related documents to my attention. Thank you and have a wonderful day, Trudy cc���DE W rH V44 _� dt aWny�� Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudy. B everlygncdenn gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: https:Hdeq.nc.gov/about/divisions/waste-management/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httDs://dea.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans File Review Procedures: https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): hqps://deg.nc.gov/about/divisions/waste-management/laserfiche Document Submittal & UST File Names for Laserfiche Policies: httys://files.nc.¢ov/ncdeci/Waste%2OManagement/DWM/UST[WhatsNew/Final-Electronic-Document-Submittal-Policv.adf https:Hfiles.nc. gov/ncdeq/Waste%2OManagement/D WM[UST/Corrective%2OAction/UST%2Ofile%20names%20for%2OLaserfiche.docx From: Bowser, Daniel P Sent: Friday, May 1, 2020 5:08 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: Fwd: [External] Release Notification - 9920 Mallard Glen Drive Dan Bowser, PG NCDEQ UST Section Corrective Action Branch From: Patrick Lowery <plowerv@summit-companies.com> Sent: Friday, May 1, 2020 4:44:08 PM To: Bowser, Daniel P <dan.bowser@ncdenr.gov> Subject: [External] Release Notification - 9920 Mallard Glen Drive External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to report.spam@nc.gov Dan, I hope you are well. I have attached a release notification for a heating oil UST we assessed in November last year. Our client requested the owner complete the attached, however it did not get completed. We are submitting on their behalf prior to real-estate transaction. If there is a person or admin I should be sending these too, please let me know. Thanks Patrick "k. MIA M SUMMIT PATRICK W. LOWERY, P.G. Senior Environmental Manager plowerv@summit-companies.com Columbia Office • 101 Rice Bent Way, Unit 9 • Columbia, SC 29229 803.708.7945 Office • 803.708.7946 Fax • 803.230.5087 Cell www.summit-companies.com [summit-companies.coml Charlotte -HQ • Raleigh • Columbia • Greenville • Charleston