24025_Crayton Printing Brownfields Assessment Report 20211222

Via Email

December 22, 2020

NCDEQ – Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attn: Mr. Bill Schmithorst

Re: Additional Brownfields Assessment Report
Crayton Printing
Distribution Street and Dunavant Street
Charlotte, North Carolina
Brownfields Project No. 24025-20-060
H&H Project No. AKR-005

Dear Mr. Schmithorst:

On behalf of KA D&D Holdings LLC, enclosed please find a copy of the Additional
Brownfields Assessment Report prepared for the Crayton Printing Brownfields property located
in Charlotte, Mecklenburg County.

Should you have questions or need additional information, please do not hesitate to contact us at
[phone].

Sincerely,
Hart & Hickman, PC
Matt Bramblett, PE Haley Martin, PG
Principal Assistant Project Geologist

Enclosure:

cc: Mr. Dan Coith and Mr. Dan Outen, Akridge (Via Email)
Ms. Mary Katherine Stukes, Moore & Van Allen (Via Email)
Ms. Pamela Tyrrell, Kettler (Via Email)
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Additional Brownfields Assessment Report
Crayton Printing
Distribution Street and Dunavant Street
Charlotte, North Carolina
Brownfields Project No. 24025-20-060
H&H Job No. AKR-005

Table of Contents

1.0 Introduction .............................................................................................................................2 
2.0 Monitoring Well Installation .................................................................................................4 
3.0 Groundwater Sampling Activities .........................................................................................6 
3.1 Well Development and Purging ............................................................................................6 
3.2 Groundwater Gauging Events ...............................................................................................7 
3.3 Groundwater Sample Analytical Results ...............................................................................7 
4.0 Quality Assurance – Quality Control ....................................................................................9 
4.1 Trip Blank ..............................................................................................................................9 
4.2 Laboratory Duplicates ...........................................................................................................9 
5.0 Summary and Conclusions ..................................................................................................11 

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List of Tables

Table 1 Summary of Well Construction and Groundwater Elevation Data
Table 2 Summary of VOC Groundwater Analytical Data for Temporary Wells –
September 2020
Table 3 Summary of Groundwater Analytical Data – October and November 2020

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Monitoring Well Location Map
Figure 4 Shallow Groundwater Potentiometric Map (November 2020)
Figure 5 Groundwater Plume Areas

List of Appendices

Appendix A Boring Logs & Well Construction Records
Appendix B Laboratory Analytical Reports
Appendix C Groundwater Sampling Forms

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Additional Brownfields Assessment Report
Crayton Printing
Distribution Street and Dunavant Street
Charlotte, North Carolina
Brownfields Project No. 24025-20-060
H&H Job No. AKR-005

1.0 Introduction

On behalf of KA D&D Holdings LLC (Prospective Developer or PD), Hart & Hickman, PC
(H&H) has prepared this report to document additional assessment activities recently completed
at the Crayton Printing Brownfields property (Brownfields Project No. [BPN] 24025-20-060)
located at 2301, 2321, 2327 Distribution Street and 2300, 2302, 2304, 2306 Dunavant Street in
Charlotte, Mecklenburg County, North Carolina (subject Site or Site). The Site consists of four
contiguous parcels (Mecklenburg County Parcel Identification Nos. 12104201, 12104402,
12104203, and 12104218) totaling approximately 2.83 acres of land located in a mixed
commercial and residential area of South End Charlotte. A Site location map is provided as
Figure 1, and the Site and surrounding area are shown in Figure 2.

On October 6, 2020, H&H completed a Brownfields Assessment Report for this Site. The report
included a review of site history; evaluation of the potential for sources of subsurface impacts;
and soil, groundwater, sub-slab vapor, and soil gas sampling activities. The report also included
a receptor survey. A key finding in the report was that groundwater impacts were present behind
the former Crayton Printing unit and the depth to the water table was shallow in that areas.

The groundwater assessment activities indicated the chlorinated VOCs PCE, TCE and vinyl
chloride were detected at concentrations above the 15A NCAC 2L Standard and/or North
Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM)
Residential Vapor Intrusion Groundwater Screening Levels (GWSLs) in the northern and
upgradient portion of the Site and in the vicinity of the former Crayton Printing facility. PCE
was detected above the 15A NCAC 2B Standard in temporary monitoring well TMW-3 which
was located in the area with a shallow water table. Locations of temporary monitoring wells
installed in the September 2020 assessment are shown in Figure 3 and analytical results are
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summarized in Table 2.

After review of proposed redevelopment plans for the proposed apartment building and parking
deck, shallow groundwater may be encountered during redevelopment activities. Therefore,
H&H provided Additional Brownfields Assessment Work Plan in an email for DEQ review and
approval. At the same time, H&H prepared an Environmental Management Plan (EMP). The
Additional Brownfields Assessment Work Plan email and EMP received DEQ approval in an
email dated October 12, 2020 and November 3, 2020, respectively.

Additional Brownfields assessment activities described herein were completed to further
evaluate the extent of VOCs in Site groundwater and to further evaluate the area of shallow
groundwater that may need to be managed during redevelopment activities. Details regarding
additional monitoring well installations, water level gauging, and groundwater sampling are
provided below.

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2.0 Monitoring Well Installation

In October 2020, H&H completed additional Brownfields assessment activities including
permanent groundwater monitoring well installation and groundwater sampling activities. Prior
to conducting field activities, H&H contacted North Carolina 811, the public utility locator, to
mark subsurface utilities at the Site. H&H also contracted with a private utility locator to mark
utilities which were not identified by the public locator. The private utility locator also utilized
ground penetrating radar (GPR) survey techniques to identify and mark utilities.

H&H directed the drilling contractor to hand clear each boring to a depth of approximately 5 feet
below ground surface (ft bgs) to further screen the boring locations for the presence of
subsurface utilities. In accordance with Mecklenburg County rules, H&H obtained a Subsurface
Investigation Permit (SIP) from Mecklenburg County (SIP No. 70002783) prior to monitoring
well installation and sampling.

The assessment activities were performed in general accordance with the DEQ approved Work
Plan, the DEQ Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup
of Contaminated Sites (Guidelines) dated January 2020, and the most recent versions of the U.S.
Environmental Protection Agency (EPA) Region IV Science and Ecosystem Support Division
(SESD) Field Branches Quality System and Technical Procedures guidance.

H&H provided oversight during installation of five (5) permanent groundwater monitoring wells
(MW-1 through MW-5) at the Site. The monitoring well locations are depicted on Figure 4, and
were installed in the following locations:
 near the western Site boundary along Distribution Street and in the topographic low area
of the subject Site (MW-1 and MW-2);
 in the south-central portion of the Site at the perimeter of the Crayton Printing unit (MW-
3 and MW-5); and
 within the former Crayton Printing unit (MW-4).
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The permanent monitoring wells were installed using a track-mounted hollow-stem auger drill
rig to advance soil borings until sufficient groundwater was encountered. Continuous soil
samples were collected from the monitoring well borings and logged for lithologic description,
observed for obvious evidence of staining and unusual odors, and field screened for the presence
of volatile organic vapors using a calibrated PID. Field screening results did not indicate the
likely presence of impacts in soil collected from the temporary monitoring well borings. As
such, soil samples were not collected for laboratory analysis.

Permanent monitoring wells were constructed of 2-inch diameter PVC with 10 ft or 15 ft of well
screen set to bracket the water table and 2-inch diameter PVC well casing to the ground surface.
Permanent monitoring wells were installed to depths ranging from approximately 12 to 18 ft bgs.
Auger refusal was encountered in four of the five monitoring well borings. Due to the
particularly shallow auger refusal in MW-2, this well was advanced deeper using air hammer
drilling.

The five monitoring wells were completed with a flush mounted well vault and an approximate 2
ft by 2 ft concrete pad. A summary of well construction and groundwater elevation information
is provided in Table 1. Monitoring well boring logs with well construction details and driller
provided well records are provided in Appendix A. The wells will be abandoned by a certified
well driller prior to site re-development.

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3.0 Groundwater Sampling Activities

3.1 Well Development and Purging

Upon completion of monitoring well installation activities, the wells were allowed to equilibrate
to static conditions and a decontaminated electronic water level indicator was used to measure
the depth to the water table relative to the ground surface and the tops of the well casings.
Groundwater was measured at depths ranging from approximately 1 ft bgs in the east-central
portion of the Site to approximately 5 ft bgs in the western portion of the Site. Once
groundwater measurements had been collected, each temporary well was developed by removing
a minimum of 3 to 5 well volumes until field parameters stabilized (pH ± 0.1 Standard Units
[SU] and specific conductivity varied no more than 5%).

After development, a groundwater sample was collected for laboratory analysis from each
monitoring wells utilizing low flow/low stress purging techniques using a peristaltic pump and
dedicated polyethylene tubing. The intake point of the pump tubing was placed in the
approximate mid-portion of the screened interval of the well and groundwater was removed at a
rate no greater than 200 milliliters per minute. H&H utilized water quality meters to collect
measurements of pH, temperature, dissolved oxygen, oxidation reduction potential, turbidity, and
specific conductivity during the purging process. Purging was considered complete when field
parameters stabilized (pH ± 0.1 SU, conductivity varied no more than 5% and turbidity was near
or less than 10 Nephelometric Turbidity Units [NTUs]). Groundwater sampling forms
completed by H&H sampling personnel are provided in Appendix C.

Once groundwater parameters stabilized or the well was purged dry, groundwater samples for
VOC analysis were collected directly into laboratory supplied sample containers using the “soda
straw” method to eliminate the potential for volatile loss through the peristaltic pump head.
Groundwater samples submitted for remaining analyses were collected directly into laboratory
supplied glassware from the sample tubing discharge. The sample containers were labeled with
the sample identification, date, time, and requested analysis, and placed in a laboratory supplied
cooler with ice. The samples were delivered to Pace under standard chain of custody protocols
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for analysis of VOCs by EPA Method 8260.

3.2 Groundwater Gauging Events

The wells were allowed to equilibrate to static conditions after installation and prior to
groundwater sampling activities. After reaching static conditions, groundwater was measured at
depths ranging from approximately 1 ft bgs in the east-central portion of the Site to
approximately 5 ft bgs in the western portion of the Site.

Following a heavy rain event on November 12, 2020, H&H mobilized to the Site to collect
additional water level measurements on November 13, 2020 in order to document potential
fluctuations of the water table. The depth to groundwater collected after the heavy rain event
raged from approximately 0.5 ft in the east-central portion of the Site to approximately 4.5 ft in
the western portion of the Site. These levels were slightly higher compared with the initial water
levels collected November 2, 2020.

In October 2020, H&H worked with a North Carolina professional surveyor to obtain the top of
casing and ground surface elevation at each monitoring well. The surveyed TOC elevations and
the measured depths to groundwater were used to calculate groundwater elevations for each
monitoring well. Based on the calculated groundwater elevations, groundwater flow direction
was estimated to be toward the west. A potentiometric surface map is provided as Figure 4.

3.3 Groundwater Sample Analytical Results

Laboratory analytical results indicate that select VOCs were detected at concentrations above the
laboratory method detection limits in the groundwater samples collected at the Site. Vinyl
chloride was detected in the duplicate groundwater sample collected from MW-4 (3.0
micrograms per liter [µg/L]) at a concentration above the 2L Standard of 0.03 µg/L, the DEQ
DWM Residential Vapor Intrusion GWSL of 1.5 µg/L, and the 2B Standard of 2.4 µg/L.
However, vinyl chloride was not detected above the laboratory method detection limits in the
parent sample collected from MW-4, which is located within the former Crayton Printing
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building. H&H contacted Pace about the discrepancy in the two vinyl chloride concentrations.
After further review, Pace indicated that they could not identify a reason for the vinyl chloride
discrepancy. Therefore, H&H re-sampled monitoring well MW-4 and collected an additional
duplicate sample in November 2020. Laboratory analytical results for the November 2020
sampling event confirmed detections of vinyl chloride (up to 3.1 µg/L) at concentrations that
exceed the 2L Standard, DEQ DWM Vapor Intrusion GWSL, and 2B Standard.

The VOC TCE was detected in groundwater samples collected from wells MW-3 (1.8 µg/L) and
MW-5 (2.5 µg/L) at concentrations that exceed the DEQ DWM Residential Vapor Intrusion
GWSL of 1 µg/L. The VOCs acetone (up to 47.0 µg/L), 2-butanone (up to 6.3 µg/L), cis-1,2-
dichloroethene (up to 14.0 µg/L), p-isopropyltoluene (up to 0.48 J µg/L), and toluene (up to 0.62
J µg/L) were detected in groundwater samples collected at the Site but at concentrations well
below the 2L Standards, DEQ DWM Residential Vapor Intrusion GWSLs, and 2B Standards.
VOCs were not detected above the laboratory method detection limits in the groundwater sample
collected from well MW-1.

During initial Brownfields Assessment activities, PCE was detected in TMW-3 located behind
the former Crayton Printing unit (see Figure 2). Relatively higher levels of PCE were also
detected in the soil gas sample collected beneath the Crayton Printing unit. Other constituents
detected in groundwater near the former Crayton Printing unit include TCE, cis-1,2-DCE, and
vinyl chloride. These compounds are potential reductive dechlorination biodegradation products
of PCE. Based on these results, it appears that the PCE plume and biodegradation products are
sourced at the former Crayton Printing unit. The groundwater TCE detected in temporary
monitoring well TMW-1 in the northwestern portion of the site is attributed to an off-Site source.
The estimated groundwater plume areas are shown on Figure 5.
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4.0 Quality Assurance – Quality Control

For quality assurance and quality control purposes (QA/QC), non-dedicated equipment and tools
were decontaminated prior to use at each boring or sampling location or following exposure to
soil or groundwater. Field QA/QC samples were analyzed along with the investigative samples
to determine potential variability introduced in sampling, handling, shipping, and analysis. One
trip blank was submitted for analysis of VOCs by EPA Method 8260. In addition, H&H
collected duplicate groundwater samples to evaluate the ability of the laboratory to reproduce
sample results. Duplicate samples were submitted to the laboratory for the same analysis as the
corresponding parent sample.

4.1 Trip Blank

The trip blank was prepared by the laboratory and consisted of certified-clean sample containers
filled with analyte-free water. The trip blank accompanied the empty laboratory sample
containers to the Site, remained within the sample cooler during sampling, and traveled back to
the laboratory with field samples. The purpose of a trip blank is to evaluate sample handling
conditions and the potential for external contaminants to compromise investigative samples
during transit. A trip blank accompanied the field groundwater samples. Laboratory analytical
results of the trip blank did not indicate the presence of VOCs at concentrations above the
laboratory method detection limits (Appendix B).

4.2 Laboratory Duplicates

Duplicate samples were collected to evaluate the precision of the field sampling procedures,
sample matrix variability, and analytical reproducibility. Duplicate groundwater samples were
collected directly into individual laboratory supplied sample containers using sampling
methodologies described in previous sections. The samples were analyzed for the same
parameters as the parent samples, and the analytical results were compared with those of the
parent sample. The analytical results of the parent sample and the duplicate sample were used to
evaluate the cumulative precision of the analytical method, sample matrix, and sample collection
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techniques.

The groundwater duplicate samples were collected from monitoring well MW-4, located within
the Crayton Printing facility. As discussed in Section 3.2, the data did not indicate good
correlation for vinyl chloride between the parent and duplicate samples collected on November
2, 2020. As such, H&H collected an additional parent and duplicate sample from monitoring
well MW-4 on November 13, 2020. The second sampling event data indicated good correlation
between the parent and duplicate samples and confirmed that vinyl chloride is present in the area
beneath the former Crayton Printing unit.
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5.0 Summary and Conclusions

H&H completed additional Brownfields assessment activities at the Crayton Printing
Brownfields property located in Charlotte, North Carolina. The assessment activities were
conducted in accordance with the DEQ Brownfields approved Work Plan email dated October
12, 2020. Brownfields assessment activities included installation of five permanent monitoring
wells, groundwater gauging events, and collection of groundwater samples for laboratory
analysis. A brief summary of the Brownfields assessment activities is provided below.

 Results of groundwater assessment activities indicate that the chlorinated VOCs TCE and
vinyl chloride were detected at concentrations above the 2L Standard and/or DEQ DWM
Residential Vapor Intrusion GWSLs in the vicinity of the former Crayton Printing facility
and in the southern portion of the Site. The vinyl chloride detected beneath the former
Crayton Printing unit also exceeds the 2B surface water standard.

 Results of groundwater gauging events indicate that depth to groundwater ranges from
approximately 0.5 ft bgs in the east-central portion of the Site to approximately 5 ft bgs in
the western portion of the Site. Based on depth to groundwater measurements, shallow
groundwater will likely be encountered during redevelopment activities (i.e. utility and
foundation installations) unless the site elevation is built up prior to development.

The depth to groundwater ranges from 0.5 to 5 ft below grade in the east-central and western
portion of the Site. In the event that groundwater is encountered near the former Crayton
Printing unit during construction, it will require special management. Impacted groundwater
management is discussed in the DEQ-approved EMP in the case that concentrations are below
surface water standards. Because groundwater concentrations for PCE and vinyl chloride exceed
surface water standards, water from construction dewatering will need to be containerized (such
as using frac tanks) and re-tested to check if levels meet surface water standards, containerized
and hauled to a permitted water treatment facility, or treated and discharged in accordance with a
NPDES permit. The process to obtain a NPDES permit is time consuming and extensive
monitoring is often required by such permits.
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The development team will consider proposed development plans, groundwater levels and the
plume area where surface water standards are exceeded to confirm that an NPDES permit is not
required post-construction.

Table 1Summary of Well Construction and Groundwater Elevation DataCrayton PrintingCharlotte, North CarolinaH&H Job No. AKR-005Well IDGround Surface Elecation (ft AMSL)TOC Elevation (ft AMSL)Well Diameter (in)Total Well Depth (ft bTOC)Screen Length (ft) Date Static Depth to Groundwater Measured Static Depth to Groundwater (ft bTOC)Groundwater Elevation (ft)11/02/2020 2.62 710.4511/13/2020 2.33 710.7411/02/2020 4.71 707.6111/13/2020 4.51 707.8111/02/2020 0.95 714.9711/13/2020 0.67 715.2511/02/2020 10.59 710.0411/13/2020 10.42 710.2111/02/2020 7.24 710.5911/13/2020 7.21 710.62Notes:Elevations were surveyed by R.B. Pharr relative to a known datum on October 30, 2020. bTOC = below top of casing; ft = feet; AMSL = above mean sea level12.7317.0711.5913.4910151010713.07712.32715.92720.632222MW-1MW-2MW-3MW-4713.59712.66716.66720.86MW-5 718.19 717.83 2 18.82 15S:\AAA‐Master Projects\Akridge\AKR.005 Dunavant Brownfileds Assessment\Additional Assessment\Tables\Data Tables.xlsx11/19/2020Table 1 (Page 1 of 1) Hart & Hickman, PC
Table 2 Summary of Groundwater VOC Analytical Data from Temporary Wells - September 2020Crayton PrintingCharlotte, North CarolinaH&H Job No. AKR-005Evaluation AreaDowngradient of Dunavant Street Brownfields PropertyVicinity of Crayton Printing FacilityDowngradient of Cherokee Southline Brownfields PropertySample IDTMW-1 TMW-3 TMW-4Date9/14/2020 9/14/2020 9/14/2020VOCs (8260D)cis-1,2-Dichloroethene5.6<0.29 <0.2921.8<0.2970 NE720 (4) Tetrachloroethene<0.16 <0.16 <0.1611.6<0.160.7 12 3Trichloroethene25<0.22 <0.226.8<0.223130Vinyl Chloride<0.24 <0.24 <0.241.7<0.240.03 1.5 2.4o-Xylene<0.220.29 J 0.25 J<0.22 <0.22500 98420 (4) Notes:1) NC Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) dated April 20132) NC DEQ Division of Waste Management (DWM) Vapor Intrusion Groundwater Screening Levels (GWSLs) dated July 20203) NC 15A NCAC 2B Surface Water Quality Standards (2B Standards) for Class C Waters dated June 2019 4) North Carolina In-Stream Target Values for Class C Surface Waters dated June 2019Concentrations are reported in micrograms per liter (µg/L).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown.Bold values exceed the 2L Standard.Underlined values exceed the GWSL. Shaded values exceed the 2B Standard.VOCs = volatile organic compoundsNE = not established;9/14/2020Upgradient - Northeastern Portion of Site Screening Criteria TMW-2 / TMW-DUP2L Standards(1) 2B Standards (3) Residential GWSLs(2)S:\AAA‐Master Projects\Akridge\AKR.005 Dunavant Brownfileds Assessment\Additional Assessment\Tables\Data Tables12/8/2020Table 2 (Page 1 of 1) Hart & Hickman, PC
Table 3 Summary of Groundwater Analytical Data - October and November 2020Crayton PrintingCharlotte, North CarolinaH&H Job No. AKR-005Evaluation AreaSouthern Portion of the Site Sample IDMW-1 MW-2 MW-3 MW-5Date10/30/2020 11/2/2020 10/30/2020 10/30/2020VOCs (8260D)Acetone<6.215.6 J<6.228.2 47.0 10.3 J 11.1 J<6.26,000 4,500,0002,000 (4)2-Butanone (MEK)<3.3 <3.3 <3.3 <3.36.3<3.3 <3.3 <3.34,000 450,00026,000 (4)cis-1,2-Dichloroethene<0.29 <0.29 <0.298.1 14.0 13.9 12.6<0.2970 NE720 (4) p-Isopropyltoluene<0.21 <0.21 <0.21 <0.210.48 J<0.21 <0.21 <0.2125* NE320 (4)Toluene<0.240.54 J 0.50 J 0.45 J 0.62 J 0.37 J 0.34 J<0.24600 3,800 11Trichloroethene<0.22 <0.221.8<0.22 <0.22 <0.22 <0.222.53130Vinyl Chloride<0.24 <0.24 <0.24 <0.243.03.12.7<0.240.03 1.5 2.4Notes:1) NC Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) dated April 20132) NC DEQ Division of Waste Management (DWM) Vapor Intrusion Groundwater Screening Levels (GWSLs) dated July 20203) NC 15A NCAC 2B Surface Water Quality Standards (2B Standards) for Class C Waters dated June 2019 4) North Carolina In-Stream Target Values for Class C Surface Waters dated June 2019* NC DEQ 15A NCAC 02L.0202 Interim Maximum Allowable Concentaration (IMAC) dated April 2013 updated April 2018Concentrations are reported in micrograms per liter (µg/L).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses.Only constituents detected in at least one sample are shown in the table above.Bold values exceed the 2L Standard.Underlined values exceed the Residential GWSL. Shaded values exceed the 2B Standard. VOCs = volatile organic compounds; NE = not establishedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. Western Site Boundary Residential GWSLs (2)11/2/2020Screening Criteria 2L Standards (1) 2B Standards (3)MW-4 / Duplicate11/13/2020Former Crayton Printing Facility S:\AAA‐Master Projects\Akridge\AKR.005 Dunavant Brownfileds Assessment\Additional Assessment\Tables\Data Tables12/8/2020Table 3 (Page 1 of 1) Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset,and National Transportation Dataset; USGS Global Ecosystems; U.S.Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;U.S. Department of State Humanitarian Information Unit; and NOAANational Centers for Environmental Information, U.S. Coastal ReliefModel. Data refreshed February, 2020.
SITE LOCATION MAP
CRAYTON PRINTINGDISTRIBUTION STREET AND DUNAVANT STREET CHARLOTTE, NORTH CAROLINA
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
0 2,000 4,000
SCALE IN FEET
SITE
N
U.S.G.S. QUADRANGLE MAP
CHARLOTTE EAST, NORTH CAROLINA 2013
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)DATE: 9-28-20
JOB NO. AKR-005
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SITE MAP
CRAYTON PRINTINGDISTRIBUTION STREET AND DUNAVANT STREETCHARLOTTE, NORTH CAROLINA
REVISION NO: 0
FIGURE NO: 2
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
0 75 150
SCALE IN FEET
N
DATE: 9-29-20
JOB NO. AKR-005
WORLD STONE FABRICATOR(2300 DISTRIBUTION STREET)
GRASS
DUNAVANT STREET
DISTRIBUTION STREETLEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY LINE
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1. BASE DATA OBTAINED FROM MECKLENBURG COUNTY GIS, 2019.
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CHARLOTTE GRILL(2322 DISTRIBUTION STREET)
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GRIER INTERIORS(2326 DISTRIBUTION STREET)
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FORMER CRAYTON PRINTING(2321B&C DISTRIBUTION STREET)
VACANT(2300 DUNAVANT STREET)
VACANT(2302 DUNAVANT STREET)
VACANT(2304 DUNAVANT STREET)
VACANT(2306 DUNAVANT STREET)
TIMELY FILTER SUPPLY(2327 DISTRIBUTION STREET)
THE DUNAVANT(2322 DUNAVANT STREET)
VACANT COMMERCIAL(2322 DUNAVANT STREET)
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#´Ñ
TMW-2
TMW-1
TMW-3
TMW-4
MW-1
MW-2
MW-4
MW-5
MW-3
MeckCoGIS
MONITORING WELL LOCATION MAP
CRAYTON PRINTINGDISTRIBUTION STREET AND DUNAVANT STREETCHARLOTTE, NORTH CAROLINA
REVISION NO: 0
FIGURE NO: 3
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
0 75 150
SCALE IN FEET
N
DATE: 12-1-20
JOB NO. AKR-005
WORLD STONE FABRICATOR(2300 DISTRIBUTION STREET)
GRASS
DUNAVANT STREET
DISTRIBUTION STREETLEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY LINE
#´Ñ PERMANENT MONITORING WELL
Ñ!!TEMPORARY MONITORING WELL
1. BASE DATA OBTAINED FROM MECKLENBURG COUNTY GIS, 2020.
2. AERIAL IMAGERY OBTAINED FROM MECKLENBURG COUNTY GIS, 2020.
3. MONITORING WELLS MW-1 THROUGH MW-5 WERE INSTALLED BY H&H ON 10/28/2020 AND 10/29/2020.
4. TEMPORARY MONITORING WELLS TMW-1 THROUGH TMW-04 WERE INSTALLED BY H&H ON 9/10/2020 AND WERE PERMANENTLY ABANDONED ON 9/15/2020.
DUNAVANT STREET BROWNFIELDS SITE(2250 HAWKINS STREET)(NCBP NO. 19038-15-060)Path: \\HHFS01\Redirectedfolders\sperry\My Documents\ArcGIS\PROJECTS\AKR-005\FIGURE 3 MW MAP.mxdHAWKINS STREETMULTI-TENANT RESIDENTIAL(1606-1632 MAINLINE BOULEVARD)(NCBP NO. 10036-06-060)
CHARLOTTE GRILL(2322 DISTRIBUTION STREET)
PET WANTS(2322 DISTRIBUTION STREET)
GRIER INTERIORS(2326 DISTRIBUTION STREET)
ELECTRICIAN(2301 DISTRIBUTION STREET)
VACANT(2321A DISTRIBUTION STREET)
FORMER CRAYTON PRINTING(2321B&C DISTRIBUTION STREET)
VACANT(2300-2306 DUNAVANT STREET)
TIMELY FILTER SUPPLY(2327 DISTRIBUTION STREET)
THE DUNAVANT(2322 DUNAVANT STREET)
VACANT COMMERCIAL(2322 DUNAVANT STREET)
CONCRETECUTOUT
THE PARKER BUILDING(2401 DISTRIBUTION STREET)
NOTES:
Ñ!!
Ñ!!
Ñ!!
Ñ!!#´Ñ
#´Ñ
#´Ñ
#´Ñ
#´Ñ
TMW-2
TMW-1
TMW-3
TMW-4
MW-1
MW-2
MW-4
MW-5
MW-3
726
710726
730
72 4
7 2 2
728
712
7 2 6
724
7 22
714
718716
720
MeckCoGIS
SHALLOW GROUNDWATERPOTENTIOMETRIC MAP (NOVEMBER 2020)
CRAYTON PRINTINGDISTRIBUTION STREET AND DUNAVANT STREETCHARLOTTE, NORTH CAROLINA
REVISION NO: 0
FIGURE NO: 4
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
0 50 100
SCALE IN FEET
N
DATE: 12-1-20
JOB NO. AKR-005
DUNAVANT STREET
DISTRIBUTION STREET1. BASE DATA OBTAINED FROM MECKLENBURG COUNTY GIS, 2020.
2. AERIAL IMAGERY OBTAINED FROM MECKLENBURG COUNTY GIS, 2020.
3. ELEVATION DATA OBTAINED FROM MECKLENBURG COUNTY LIDAR, 2013.
4. MONITORING WELLS MW-1 THROUGH MW-5 WERE INSTALLED BY H&H ON 10/28/2020 AND 10/29/2020.
5. TEMPORARY MONITORING WELLS TMW-1 THROUGH TMW-04 WERE INSTALLED BY H&H ON 9/10/2020 AND WERE PERMANENTLY ABANDONED ON 9/15/2020.
6. DEPTH TO GROUNDWATER MEASUREMENTS COLLECTED BY H&H ON 11/13/2020.Path: \\HHFS01\Redirectedfolders\sperry\My Documents\ArcGIS\PROJECTS\AKR-005\FIGURE 4 - GW Pot Map Nov 2020.mxdHAWKINS STREET708
(710.21)(715.25)
(710.74)
(710.74)
(707.81)
(710.62)
710
712
714
708710712714NOTES:
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY LINE
ELEVATION CONTOUR (FT)
PROPOSED BUILDING FOOTPRINT
PROPOSED PARKING DECK
#´Ñ PERMANENT MONITORING WELL
Ñ!!TEMPORARY MONITORING WELL
GROUNDWATER ELEVATION (FT.)
INFERRED GROUNDWATER CONTOUR (FT.)
INFERRED DIRECTION OF GROUNDWATERFLOW
712
PROPOSEDCOURTYARD
PROPOSEDPARKING DECK
Ñ!!
Ñ!!
Ñ!!
Ñ!!#´Ñ
#´Ñ
#´Ñ
#´Ñ
#´Ñ
TMW-2
TMW-1
TMW-3
TMW-4
MW-1
MW-2
MW-4
MW-5
MW-3
MeckCoGIS
GROUNDWATER PLUME AREAS
CRAYTON PRINTINGDISTRIBUTION STREET AND DUNAVANT STREETCHARLOTTE, NORTH CAROLINA
REVISION NO: 0
FIGURE NO: 5
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
0 50 100
SCALE IN FEET
N
DATE: 12-8-20
JOB NO. AKR-005
DUNAVANT STREET
DISTRIBUTION STREET1. BASE DATA OBTAINED FROM MECKLENBURG COUNTY GIS, 2020.
2. AERIAL IMAGERY OBTAINED FROM MECKLENBURG COUNTY GIS, 2020.
3. MONITORING WELLS MW-1 THROUGH MW-5 WERE INSTALLED BY H&H ON 10/28/2020 AND 10/29/2020.
4. TEMPORARY MONITORING WELLS TMW-1 THROUGH TMW-04 WERE INSTALLED BY H&H ON 9/10/2020 AND WERE PERMANENTLY ABANDONED ON 9/15/2020.Path: \\HHFS01\Redirectedfolders\sperry\My Documents\ArcGIS\PROJECTS\AKR-005\FIGURE 5 - GW Plume Areas.mxdHAWKINS STREETNOTES:
PROPOSEDCOURTYARD
PROPOSEDPARKING DECK
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY LINE
PROPOSED BUILDING FOOTPRINT
PROPOSED PARKING DECK
#´Ñ PERMANENT MONITORING WELL
Ñ!!TEMPORARY MONITORING WELL
CHLORINATED VOC PLUME IN AREA WITHSHALLOW GROUNDWATER
CHLORINATED VOC PLUME FROM OFF-SITESOURCE?
?

Appendix A

Boring Logs & Well Construction Records
NOTES: Hole precleared to 5' on 10/28/2020 by IET using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-005
Distribution & Dunavant Street,Mecklenburg, Charlotte, NC
WELL LOG
Well No.
Page:
MW-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
IET
Hollow Stem Auger
AMS Power Probe 9520
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
13
8
DP, GR
2.6
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
12.73
2
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
GR
GR
DP
DP
2.00
3.00
5.00
3.00
(0') SILT (ML); some fine-medium sand, some clay, soft, moist, brown
(9') SILT (ML); some fine-medium sand, soft, saturated, dark grey
5.5
6.2
5.9
5.6
6.5
7.7
5.1
0
5
10
15
20
25
1310/28/2020
10/29/2020
Not Measured
(2') SILT (ML); some fine-medium sand, some clay, soft, dry, brown
(4') SILT (ML); some fine-medium sand, some clay, medium stiff, dry, brown
(5') SILT (ML); some fine-medium sand, medium stiff, saturated, brown
NOTES: Hole precleared to 5' on 10/28/2020 by IET using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-005
Distribution & Dunavant Street,Mecklenburg, Charlotte, NC
WELL LOG
Well No.
Page:
MW-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
8
DP, GR
4.71
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
17.07
2
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
GR
GR
DP
2.00
3.00
3.00
7.8
8.4
7.8
9.6
0
5
10
15
20
25
113810/28/2020
10/29/2020
IET
Hollow Stem Auger/Air
AMS Power Probe 9520
KAM
Not Measured
(0') SILT (ML); trace clay, medium stiff, moist, dark yellowish brown
(5') SILT (ML); trace clay, soft, dry, yellowish brown
(8') Hollow Stem Auger Refusal - Weathered Bedrock
NOTES: Hole precleared to 5' on 10/28/2020 by IET using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-005
Distribution & Dunavant Street,Mecklenburg, Charlotte, NC
WELL LOG
Well No.
Page:
MW-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
IET
Hollow Stem Auger
AMS Power Probe 9520
KAM
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
8
DP, GR
0.95
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
11.59
2
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
GR
GR
DP
DP
2.00
3.00
5.00
2.00
2.3
1.6
2.4
3.0
5.2
5.4
0
5
10
15
20
25
11210/28/2020
10/29/2020
Not Measured
(0') SILT (ML); some sand, some clay, medium stiff, dry, brown
(4') SILT (ML); some sand, trace clay, medium stiff, dry, dark reddish grey
(5') SILT (ML); some fine-medium sand, trace clay, soft, saturated, red
(6') SILT (ML); some fine-medium sand, trace clay, stiff, moist, red
(9') SILT (ML); some fine-medium sand, stiff, moist, light reddish brown
(12') Hollow stem auger refusal
NOTES: Hole precleared to 5' on 10/28/2020 by IET using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-005
Distribution & Dunavant Street,Mecklenburg, Charlotte, NC
WELL LOG
Well No.
Page:
MW-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
8
DP, GR
0.95
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
11.59
2
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
GR
GR
DP
DP
2.00
3.00
5.00
3.00
1.7
3.1
4.6
5.2
4.8
5.1
0
5
10
15
20
25
11210/29/2020
10/29/2020
IET
Hollow Stem Auger
AMS Power Probe 9520
KAM
Not Measured
(0') SILT (ML); some sand, trace clay, medium stiff, dry, yellowish red
(5') SILT (ML); some sand, trace clay, soft, moist, dark yellowish brown
(13') Hollow stem auger refusal
2.3
(9') SILT (ML); some clay, soft, moist, very dark grey
(10') SILT (ML); some sand, trace clay, soft, saturated, yellowish brown
NOTES: Hole precleared to 5' on 10/28/2020 by IET using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-005
Distribution & Dunavant Street,Mecklenburg, Charlotte, NC
WELL LOG
Well No.
Page:
MW-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
8
DP, GR
7.24
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
18.82
2
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
GR
GR
DP
2.00
3.00
5.00
NM
0.5
1.0
4.2
0
5
10
15
20
25
10/28/2020
10/29/2020
IET
Hollow Stem Auger
AMS Power Probe 9520
KAM
Not Measured
(0') SILT (ML); some sand, trace clay, medium stiff, moist, dark yellowish brown
(5') SILT (ML); some sand, trace clay, soft, moist, dark yellowish brown
(10') SILT (ML); some sand, trace clay, medium stiff, dry, yellowish brown
20
DP
4.6
4.7
4.4
5.0
6.5
3.9
(15') SILT (ML); some sand, trace clay, medium stiff, dry, very pale brown
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
one
10/29/2020 MW-1
Crayton Printing
2301 Distribution St. Charlotte 28203
Mecklenburg
35 12 24 80 51 56
13
3
8
Auger
10/30/2020
3 13
0 3 2 sch40 pvc
3 13 2 0.010 sch40 pvc
0
2
2
13
Bentonite
#2 Sand poured
poured/50LB
See Consultant Log
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
one
10/29/2020 MW-2
Crayton Printing
2301 Distribution St. Charlotte 28203
Mecklenburg
35 12 24 80 51 56
17
Dry
8
Air Drilled
10/30/2020
0 7 2 sch40 pvc
7 17 2 0.010 sch40 pvc
3
0
5
5
3
17
Bentonite
neat cement
#2 Sand poured
poured/50LB
See Consultant Log
Supervised By Mike Tynan Driller # 2725-A
poured/55LB
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
one
10/29/2020 MW-3
Crayton Printing
2301 Distribution St. Charlotte 28203
Mecklenburg
35 12 24 80 51 56
12
3.2
8
Auger
10/30/2020
3.2 12
0 2 2 sch40 pvc
2 12 2 0.010 sch40 pvc
0
1
1
12
Bentonite
#2 Sand poured
poured/25LB
See Consultant Log
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
one
10/29/2020 MW-4
Crayton Printing
2301 Distribution St. Charlotte 28203
Mecklenburg
35 12 24 80 51 56
13.5
dry
8
Auger
10/30/2020
0 3.5 2 sch40 pvc
3.5 13.5 2 0.010 sch40 pvc
0
1.5
1.5
13.5
Bentonite
#2 Sand poured
poured/40LB
See Consultant Log
WELL CONSTRUCTION RECORD (GW-1)For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Terry White
3287-B
IET
one
10/29/2020 MW-5
Crayton Printing
2301 Distribution St. Charlotte 28203
Mecklenburg
35 12 24 80 51 56
19
7.12
8
Auger
10/30/2020
7.12 19
0 4 2 sch40 pvc
4 19 2 0.010 sch40 pvc
2
0
3
3
2
19
Bentonite
neat cement
#2 Sand poured
poured/25LB
See Consultant Log
poured/26LB

Appendix B

Laboratory Analytical Reports
#=CL#
November 06, 2020
LIMS USE: FR - MATT BRAMBLETT
LIMS OBJECT ID: 92503310
92503310
Project:
Pace Project No.:
RE:
Matt Bramblett
Hart & Hickman
2923 S.Tyron St.
Charlotte, NC 28203
Crayton Printing (AKR-005)
Dear Matt Bramblett:
Enclosed are the analytical results for sample(s) received by the laboratory on November 02, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
cc:Haley Martin, Hart & Hickman
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 33
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Lab ID Sample ID Matrix Date Collected Date Received
92503310001 MW-1 Water 10/30/20 12:10 11/02/20 14:00
92503310002 MW-2 Water 11/02/20 10:50 11/02/20 14:00
92503310003 MW-3 Water 10/30/20 10:20 11/02/20 14:00
92503310004 MW-4 Water 11/02/20 11:30 11/02/20 14:00
92503310005 MW-5 Water 10/30/20 13:40 11/02/20 14:00
92503310006 Duplicate Water 10/30/20 00:00 11/02/20 14:00
92503310007 Trip Blank Water 10/30/20 00:00 11/02/20 14:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 33
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92503310001 MW-1 EPA 8260D 63 PASI-CSAS
92503310002 MW-2 EPA 8260D 63 PASI-CSAS
92503310003 MW-3 EPA 8260D 63 PASI-CSAS
92503310004 MW-4 EPA 8260D 63 PASI-CSAS
92503310005 MW-5 EPA 8260D 63 PASI-CSAS
92503310006 Duplicate EPA 8260D 63 PASI-CPM1
92503310007 Trip Blank EPA 8260D 63 PASI-CPM1
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:MW-1 Lab ID:92503310001 Collected:10/30/20 12:10 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 11/03/20 18:58 67-64-125.0 6.2 1
Benzene ND ug/L 11/03/20 18:58 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/03/20 18:58 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 11/03/20 18:58 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/03/20 18:58 75-27-41.0 0.26 1
Bromoform ND ug/L 11/03/20 18:58 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/03/20 18:58 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 11/03/20 18:58 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/03/20 18:58 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/03/20 18:58 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/03/20 18:58 75-00-31.0 0.49 1
Chloroform ND ug/L 11/03/20 18:58 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/03/20 18:58 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/03/20 18:58 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/03/20 18:58 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/20 18:58 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/03/20 18:58 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/03/20 18:58 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/03/20 18:58 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/03/20 18:58 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/03/20 18:58 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/03/20 18:58 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/03/20 18:58 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/03/20 18:58 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/03/20 18:58 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/03/20 18:58 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 11/03/20 18:58 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/03/20 18:58 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/03/20 18:58 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/03/20 18:58 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/03/20 18:58 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/03/20 18:58 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/03/20 18:58 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/03/20 18:58 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/03/20 18:58 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/03/20 18:58 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/03/20 18:58 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/03/20 18:58 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/03/20 18:58 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/03/20 18:58 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/03/20 18:58 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/03/20 18:58 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/03/20 18:58 91-20-31.0 0.35 1
Styrene ND ug/L 11/03/20 18:58 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/20 18:58 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:MW-1 Lab ID:92503310001 Collected:10/30/20 12:10 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 11/03/20 18:58 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/03/20 18:58 127-18-41.0 0.16 1
Toluene ND ug/L 11/03/20 18:58 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/03/20 18:58 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/03/20 18:58 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/03/20 18:58 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/03/20 18:58 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/03/20 18:58 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/03/20 18:58 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/03/20 18:58 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/03/20 18:58 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 11/03/20 18:58 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/03/20 18:58 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/03/20 18:58 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/03/20 18:58 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)105 %11/03/20 18:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/03/20 18:58 17060-07-070-130 1
Toluene-d8 (S)99 %11/03/20 18:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:MW-2 Lab ID:92503310002 Collected:11/02/20 10:50 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 15.6J ug/L 11/03/20 19:16 67-64-125.0 6.2 1
Benzene ND ug/L 11/03/20 19:16 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/03/20 19:16 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 11/03/20 19:16 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/03/20 19:16 75-27-41.0 0.26 1
Bromoform ND ug/L 11/03/20 19:16 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/03/20 19:16 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 11/03/20 19:16 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/03/20 19:16 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/03/20 19:16 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/03/20 19:16 75-00-31.0 0.49 1
Chloroform ND ug/L 11/03/20 19:16 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/03/20 19:16 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/03/20 19:16 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/03/20 19:16 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/20 19:16 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/03/20 19:16 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/03/20 19:16 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/03/20 19:16 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/03/20 19:16 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/03/20 19:16 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/03/20 19:16 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/03/20 19:16 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/03/20 19:16 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/03/20 19:16 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/03/20 19:16 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 11/03/20 19:16 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/03/20 19:16 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/03/20 19:16 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/03/20 19:16 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/03/20 19:16 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/03/20 19:16 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/03/20 19:16 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/03/20 19:16 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/03/20 19:16 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/03/20 19:16 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/03/20 19:16 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/03/20 19:16 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/03/20 19:16 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/03/20 19:16 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/03/20 19:16 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/03/20 19:16 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/03/20 19:16 91-20-31.0 0.35 1
Styrene ND ug/L 11/03/20 19:16 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/20 19:16 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:MW-2 Lab ID:92503310002 Collected:11/02/20 10:50 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 11/03/20 19:16 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/03/20 19:16 127-18-41.0 0.16 1
Toluene 0.54J ug/L 11/03/20 19:16 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/03/20 19:16 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/03/20 19:16 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/03/20 19:16 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/03/20 19:16 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/03/20 19:16 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/03/20 19:16 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/03/20 19:16 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/03/20 19:16 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 11/03/20 19:16 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/03/20 19:16 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/03/20 19:16 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/03/20 19:16 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)99 %11/03/20 19:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %11/03/20 19:16 17060-07-070-130 1
Toluene-d8 (S)99 %11/03/20 19:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:MW-3 Lab ID:92503310003 Collected:10/30/20 10:20 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 11/03/20 19:34 67-64-125.0 6.2 1
Benzene ND ug/L 11/03/20 19:34 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/03/20 19:34 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 11/03/20 19:34 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/03/20 19:34 75-27-41.0 0.26 1
Bromoform ND ug/L 11/03/20 19:34 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/03/20 19:34 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 11/03/20 19:34 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/03/20 19:34 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/03/20 19:34 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/03/20 19:34 75-00-31.0 0.49 1
Chloroform ND ug/L 11/03/20 19:34 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/03/20 19:34 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/03/20 19:34 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/03/20 19:34 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/20 19:34 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/03/20 19:34 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/03/20 19:34 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/03/20 19:34 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/03/20 19:34 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/03/20 19:34 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/03/20 19:34 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/03/20 19:34 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/03/20 19:34 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/03/20 19:34 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/03/20 19:34 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 11/03/20 19:34 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/03/20 19:34 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/03/20 19:34 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/03/20 19:34 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/03/20 19:34 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/03/20 19:34 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/03/20 19:34 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/03/20 19:34 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/03/20 19:34 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/03/20 19:34 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/03/20 19:34 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/03/20 19:34 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/03/20 19:34 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/03/20 19:34 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/03/20 19:34 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/03/20 19:34 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/03/20 19:34 91-20-31.0 0.35 1
Styrene ND ug/L 11/03/20 19:34 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/20 19:34 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:MW-3 Lab ID:92503310003 Collected:10/30/20 10:20 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 11/03/20 19:34 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/03/20 19:34 127-18-41.0 0.16 1
Toluene 0.50J ug/L 11/03/20 19:34 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/03/20 19:34 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/03/20 19:34 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/03/20 19:34 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/03/20 19:34 79-00-51.0 0.24 1
Trichloroethene 1.8 ug/L 11/03/20 19:34 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/03/20 19:34 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/03/20 19:34 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/03/20 19:34 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 11/03/20 19:34 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/03/20 19:34 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/03/20 19:34 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/03/20 19:34 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)98 %11/03/20 19:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %11/03/20 19:34 17060-07-070-130 1
Toluene-d8 (S)100 %11/03/20 19:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:MW-4 Lab ID:92503310004 Collected:11/02/20 11:30 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 28.2 ug/L 11/03/20 19:52 67-64-125.0 6.2 1
Benzene ND ug/L 11/03/20 19:52 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/03/20 19:52 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 11/03/20 19:52 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/03/20 19:52 75-27-41.0 0.26 1
Bromoform ND ug/L 11/03/20 19:52 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/03/20 19:52 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 11/03/20 19:52 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/03/20 19:52 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/03/20 19:52 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/03/20 19:52 75-00-31.0 0.49 1
Chloroform ND ug/L 11/03/20 19:52 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/03/20 19:52 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/03/20 19:52 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/03/20 19:52 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/20 19:52 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/03/20 19:52 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/03/20 19:52 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/03/20 19:52 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/03/20 19:52 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/03/20 19:52 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/03/20 19:52 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/03/20 19:52 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/03/20 19:52 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/03/20 19:52 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/03/20 19:52 75-35-41.0 0.24 1
cis-1,2-Dichloroethene 8.1 ug/L 11/03/20 19:52 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/03/20 19:52 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/03/20 19:52 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/03/20 19:52 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/03/20 19:52 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/03/20 19:52 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/03/20 19:52 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/03/20 19:52 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/03/20 19:52 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/03/20 19:52 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/03/20 19:52 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/03/20 19:52 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/03/20 19:52 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/03/20 19:52 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/03/20 19:52 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/03/20 19:52 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/03/20 19:52 91-20-31.0 0.35 1
Styrene ND ug/L 11/03/20 19:52 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/20 19:52 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:MW-4 Lab ID:92503310004 Collected:11/02/20 11:30 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 11/03/20 19:52 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/03/20 19:52 127-18-41.0 0.16 1
Toluene 0.45J ug/L 11/03/20 19:52 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/03/20 19:52 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/03/20 19:52 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/03/20 19:52 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/03/20 19:52 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/03/20 19:52 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/03/20 19:52 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/03/20 19:52 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/03/20 19:52 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 11/03/20 19:52 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/03/20 19:52 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/03/20 19:52 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/03/20 19:52 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)99 %11/03/20 19:52 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/03/20 19:52 17060-07-070-130 1
Toluene-d8 (S)99 %11/03/20 19:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:MW-5 Lab ID:92503310005 Collected:10/30/20 13:40 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 11/03/20 20:10 67-64-125.0 6.2 1
Benzene ND ug/L 11/03/20 20:10 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/03/20 20:10 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 11/03/20 20:10 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/03/20 20:10 75-27-41.0 0.26 1
Bromoform ND ug/L 11/03/20 20:10 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/03/20 20:10 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 11/03/20 20:10 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/03/20 20:10 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/03/20 20:10 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/03/20 20:10 75-00-31.0 0.49 1
Chloroform ND ug/L 11/03/20 20:10 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/03/20 20:10 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/03/20 20:10 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/03/20 20:10 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/20 20:10 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/03/20 20:10 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/03/20 20:10 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/03/20 20:10 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/03/20 20:10 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/03/20 20:10 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/03/20 20:10 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/03/20 20:10 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/03/20 20:10 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/03/20 20:10 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/03/20 20:10 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 11/03/20 20:10 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/03/20 20:10 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/03/20 20:10 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/03/20 20:10 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/03/20 20:10 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/03/20 20:10 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/03/20 20:10 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/03/20 20:10 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/03/20 20:10 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/03/20 20:10 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/03/20 20:10 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/03/20 20:10 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/03/20 20:10 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/03/20 20:10 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/03/20 20:10 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/03/20 20:10 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/03/20 20:10 91-20-31.0 0.35 1
Styrene ND ug/L 11/03/20 20:10 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/20 20:10 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:MW-5 Lab ID:92503310005 Collected:10/30/20 13:40 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 11/03/20 20:10 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/03/20 20:10 127-18-41.0 0.16 1
Toluene ND ug/L 11/03/20 20:10 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/03/20 20:10 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/03/20 20:10 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/03/20 20:10 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/03/20 20:10 79-00-51.0 0.24 1
Trichloroethene 2.5 ug/L 11/03/20 20:10 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/03/20 20:10 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/03/20 20:10 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/03/20 20:10 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 11/03/20 20:10 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/03/20 20:10 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/03/20 20:10 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/03/20 20:10 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %11/03/20 20:10 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/03/20 20:10 17060-07-070-130 1
Toluene-d8 (S)98 %11/03/20 20:10 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:Duplicate Lab ID:92503310006 Collected:10/30/20 00:00 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 47.0 ug/L 11/04/20 04:50 67-64-125.0 6.2 1
Benzene ND ug/L 11/04/20 04:50 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/04/20 04:50 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 11/04/20 04:50 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/04/20 04:50 75-27-41.0 0.26 1
Bromoform ND ug/L 11/04/20 04:50 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/04/20 04:50 74-83-92.0 0.62 1
2-Butanone (MEK)6.3 ug/L 11/04/20 04:50 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/04/20 04:50 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/04/20 04:50 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/04/20 04:50 75-00-31.0 0.49 1
Chloroform ND ug/L 11/04/20 04:50 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/04/20 04:50 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/04/20 04:50 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/04/20 04:50 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/04/20 04:50 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/04/20 04:50 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/04/20 04:50 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/04/20 04:50 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/04/20 04:50 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/04/20 04:50 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/04/20 04:50 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/04/20 04:50 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/04/20 04:50 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/04/20 04:50 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/04/20 04:50 75-35-41.0 0.24 1
cis-1,2-Dichloroethene 14.0 ug/L 11/04/20 04:50 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/04/20 04:50 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/04/20 04:50 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/04/20 04:50 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/04/20 04:50 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/04/20 04:50 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/04/20 04:50 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/04/20 04:50 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/04/20 04:50 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/04/20 04:50 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/04/20 04:50 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/04/20 04:50 591-78-65.0 0.57 1
p-Isopropyltoluene 0.48J ug/L 11/04/20 04:50 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/04/20 04:50 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/04/20 04:50 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/04/20 04:50 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/04/20 04:50 91-20-31.0 0.35 1
Styrene ND ug/L 11/04/20 04:50 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/04/20 04:50 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:Duplicate Lab ID:92503310006 Collected:10/30/20 00:00 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 11/04/20 04:50 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/04/20 04:50 127-18-41.0 0.16 1
Toluene 0.62J ug/L 11/04/20 04:50 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/04/20 04:50 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/04/20 04:50 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/04/20 04:50 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/04/20 04:50 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/04/20 04:50 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/04/20 04:50 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/04/20 04:50 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/04/20 04:50 108-05-42.0 1.4 1
Vinyl chloride 3.0 ug/L 11/04/20 04:50 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/04/20 04:50 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/04/20 04:50 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/04/20 04:50 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)97 %11/04/20 04:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %11/04/20 04:50 17060-07-070-130 1
Toluene-d8 (S)100 %11/04/20 04:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:Trip Blank Lab ID:92503310007 Collected:10/30/20 00:00 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 11/04/20 03:38 67-64-125.0 6.2 1
Benzene ND ug/L 11/04/20 03:38 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/04/20 03:38 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 11/04/20 03:38 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/04/20 03:38 75-27-41.0 0.26 1
Bromoform ND ug/L 11/04/20 03:38 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/04/20 03:38 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 11/04/20 03:38 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/04/20 03:38 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/04/20 03:38 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/04/20 03:38 75-00-31.0 0.49 1
Chloroform ND ug/L 11/04/20 03:38 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/04/20 03:38 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/04/20 03:38 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/04/20 03:38 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/04/20 03:38 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/04/20 03:38 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/04/20 03:38 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/04/20 03:38 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/04/20 03:38 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/04/20 03:38 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/04/20 03:38 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/04/20 03:38 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/04/20 03:38 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/04/20 03:38 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/04/20 03:38 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 11/04/20 03:38 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/04/20 03:38 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/04/20 03:38 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/04/20 03:38 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/04/20 03:38 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/04/20 03:38 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/04/20 03:38 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/04/20 03:38 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/04/20 03:38 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/04/20 03:38 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/04/20 03:38 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/04/20 03:38 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/04/20 03:38 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/04/20 03:38 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/04/20 03:38 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/04/20 03:38 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/04/20 03:38 91-20-31.0 0.35 1
Styrene ND ug/L 11/04/20 03:38 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/04/20 03:38 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Sample:Trip Blank Lab ID:92503310007 Collected:10/30/20 00:00 Received:11/02/20 14:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 11/04/20 03:38 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/04/20 03:38 127-18-41.0 0.16 1
Toluene ND ug/L 11/04/20 03:38 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/04/20 03:38 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/04/20 03:38 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/04/20 03:38 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/04/20 03:38 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/04/20 03:38 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/04/20 03:38 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/04/20 03:38 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/04/20 03:38 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 11/04/20 03:38 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/04/20 03:38 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/04/20 03:38 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/04/20 03:38 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)98 %11/04/20 03:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %11/04/20 03:38 17060-07-070-130 1
Toluene-d8 (S)100 %11/04/20 03:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
577666
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92503310001, 92503310002, 92503310003, 92503310004, 92503310005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3056358
Associated Lab Samples:92503310001, 92503310002, 92503310003, 92503310004, 92503310005
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/03/20 10:380.34
1,1,1-Trichloroethane ug/L ND 1.0 11/03/20 10:380.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/03/20 10:380.22
1,1,2-Trichloroethane ug/L ND 1.0 11/03/20 10:380.24
1,1-Dichloroethane ug/L ND 1.0 11/03/20 10:380.27
1,1-Dichloroethene ug/L ND 1.0 11/03/20 10:380.24
1,1-Dichloropropene ug/L ND 1.0 11/03/20 10:380.21
1,2,3-Trichlorobenzene ug/L 0.60J 1.0 11/03/20 10:380.34
1,2,3-Trichloropropane ug/L ND 1.0 11/03/20 10:380.35
1,2,4-Trichlorobenzene ug/L 0.53J 1.0 11/03/20 10:380.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 11/03/20 10:380.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/03/20 10:380.26
1,2-Dichlorobenzene ug/L ND 1.0 11/03/20 10:380.29
1,2-Dichloroethane ug/L ND 1.0 11/03/20 10:380.34
1,2-Dichloropropane ug/L ND 1.0 11/03/20 10:380.19
1,3-Dichlorobenzene ug/L ND 1.0 11/03/20 10:380.22
1,3-Dichloropropane ug/L ND 1.0 11/03/20 10:380.16
1,4-Dichlorobenzene ug/L ND 1.0 11/03/20 10:380.26
2,2-Dichloropropane ug/L ND 1.0 11/03/20 10:380.27
2-Butanone (MEK)ug/L ND 5.0 11/03/20 10:383.3
2-Chlorotoluene ug/L ND 1.0 11/03/20 10:380.20
2-Hexanone ug/L ND 5.0 11/03/20 10:380.57
4-Chlorotoluene ug/L ND 1.0 11/03/20 10:380.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/03/20 10:384.5
Acetone ug/L ND 25.0 11/03/20 10:386.2
Benzene ug/L ND 1.0 11/03/20 10:380.15
Bromobenzene ug/L ND 1.0 11/03/20 10:380.22
Bromochloromethane ug/L ND 1.0 11/03/20 10:380.34
Bromodichloromethane ug/L ND 1.0 11/03/20 10:380.26
Bromoform ug/L ND 1.0 11/03/20 10:380.62
Bromomethane ug/L ND 2.0 11/03/20 10:380.62
Carbon tetrachloride ug/L ND 1.0 11/03/20 10:380.22
Chlorobenzene ug/L ND 1.0 11/03/20 10:380.23
Chloroethane ug/L ND 1.0 11/03/20 10:380.49
Chloroform ug/L ND 5.0 11/03/20 10:382.3
Chloromethane ug/L ND 1.0 11/03/20 10:380.39
cis-1,2-Dichloroethene ug/L ND 1.0 11/03/20 10:380.29
cis-1,3-Dichloropropene ug/L ND 1.0 11/03/20 10:380.30
Dibromochloromethane ug/L ND 1.0 11/03/20 10:380.41
Dibromomethane ug/L ND 1.0 11/03/20 10:380.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3056358
Associated Lab Samples:92503310001, 92503310002, 92503310003, 92503310004, 92503310005
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 11/03/20 10:380.23
Diisopropyl ether ug/L ND 1.0 11/03/20 10:380.22
Ethylbenzene ug/L ND 1.0 11/03/20 10:380.26
Hexachloro-1,3-butadiene ug/L ND 1.0 11/03/20 10:380.44
m&p-Xylene ug/L ND 2.0 11/03/20 10:380.41
Methyl-tert-butyl ether ug/L ND 1.0 11/03/20 10:380.28
Methylene Chloride ug/L ND 5.0 11/03/20 10:383.7
Naphthalene ug/L 0.62J 1.0 11/03/20 10:380.35
o-Xylene ug/L ND 1.0 11/03/20 10:380.22
p-Isopropyltoluene ug/L ND 1.0 11/03/20 10:380.21
Styrene ug/L ND 1.0 11/03/20 10:380.27
Tetrachloroethene ug/L ND 1.0 11/03/20 10:380.16
Toluene ug/L ND 1.0 11/03/20 10:380.24
trans-1,2-Dichloroethene ug/L ND 1.0 11/03/20 10:380.25
trans-1,3-Dichloropropene ug/L ND 1.0 11/03/20 10:380.31
Trichloroethene ug/L ND 1.0 11/03/20 10:380.22
Trichlorofluoromethane ug/L ND 1.0 11/03/20 10:380.31
Vinyl acetate ug/L ND 2.0 11/03/20 10:381.4
Vinyl chloride ug/L ND 1.0 11/03/20 10:380.24
Xylene (Total)ug/L ND 1.0 11/03/20 10:380.63
1,2-Dichloroethane-d4 (S)%101 70-130 11/03/20 10:38
4-Bromofluorobenzene (S)%96 70-130 11/03/20 10:38
Toluene-d8 (S)%100 70-130 11/03/20 10:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3056359LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.250 100 70-130
1,1,1-Trichloroethane ug/L 48.150 96 70-130
1,1,2,2-Tetrachloroethane ug/L 48.350 97 70-130
1,1,2-Trichloroethane ug/L 48.550 97 70-130
1,1-Dichloroethane ug/L 47.750 95 70-130
1,1-Dichloroethene ug/L 51.450 103 70-132
1,1-Dichloropropene ug/L 48.850 98 70-131
1,2,3-Trichlorobenzene ug/L 51.750 103 70-134
1,2,3-Trichloropropane ug/L 48.150 96 70-130
1,2,4-Trichlorobenzene ug/L 54.950 110 70-130
1,2-Dibromo-3-chloropropane ug/L 52.650 105 70-132
1,2-Dibromoethane (EDB)ug/L 50.450 101 70-130
1,2-Dichlorobenzene ug/L 51.950 104 70-130
1,2-Dichloroethane ug/L 45.350 91 70-130
1,2-Dichloropropane ug/L 48.350 97 70-130
1,3-Dichlorobenzene ug/L 52.450 105 70-130
1,3-Dichloropropane ug/L 50.850 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3056359LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 53.450 107 70-130
2,2-Dichloropropane ug/L 49.350 99 70-130
2-Butanone (MEK)ug/L 94.0100 94 70-133
2-Chlorotoluene ug/L 52.150 104 70-130
2-Hexanone ug/L 99.7100 100 70-130
4-Chlorotoluene ug/L 51.950 104 70-130
4-Methyl-2-pentanone (MIBK)ug/L 96.2100 96 70-130
Acetone ug/L 97.7100 98 70-144
Benzene ug/L 47.850 96 70-130
Bromobenzene ug/L 50.450 101 70-130
Bromochloromethane ug/L 46.350 93 70-130
Bromodichloromethane ug/L 47.150 94 70-130
Bromoform ug/L 46.750 93 70-131
Bromomethane ug/L 56.850 114 30-177
Carbon tetrachloride ug/L 48.950 98 70-130
Chlorobenzene ug/L 49.950 100 70-130
Chloroethane ug/L 37.450 75 46-131
Chloroform ug/L 48.550 97 70-130
Chloromethane ug/L 42.750 85 49-130
cis-1,2-Dichloroethene ug/L 46.650 93 70-130
cis-1,3-Dichloropropene ug/L 50.050 100 70-130
Dibromochloromethane ug/L 50.850 102 70-130
Dibromomethane ug/L 48.850 98 70-130
Dichlorodifluoromethane ug/L 43.750 87 52-134
Diisopropyl ether ug/L 46.050 92 70-131
Ethylbenzene ug/L 48.950 98 70-130
Hexachloro-1,3-butadiene ug/L 50.250 100 70-131
m&p-Xylene ug/L 98.8100 99 70-130
Methyl-tert-butyl ether ug/L 46.450 93 70-130
Methylene Chloride ug/L 44.250 88 68-130
Naphthalene ug/L 53.450 107 70-133
o-Xylene ug/L 50.450 101 70-130
p-Isopropyltoluene ug/L 52.850 106 70-130
Styrene ug/L 49.750 99 70-130
Tetrachloroethene ug/L 49.150 98 70-130
Toluene ug/L 48.150 96 70-130
trans-1,2-Dichloroethene ug/L 47.650 95 70-130
trans-1,3-Dichloropropene ug/L 49.150 98 70-130
Trichloroethene ug/L 48.650 97 70-130
Trichlorofluoromethane ug/L 40.850 82 61-130
Vinyl acetate ug/L 109100 109 70-140
Vinyl chloride ug/L 43.550 87 59-142
Xylene (Total)ug/L 149150 100 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3057010MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503310005
3057011
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 101 70-13599 2 3020ND20.2 19.8
1,1,1-Trichloroethane ug/L 20 100 70-14898 2 3020ND20.0 19.6
1,1,2,2-Tetrachloroethane ug/L 20 100 70-13197 3 3020ND19.9 19.4
1,1,2-Trichloroethane ug/L 20 96 70-13694 3 3020ND19.3 18.7
1,1-Dichloroethane ug/L 20 101 70-14799 2 3020ND20.2 19.7
1,1-Dichloroethene ug/L 20 115 70-158108 6 3020ND22.9 21.6
1,1-Dichloropropene ug/L 20 102 70-149100 2 3020ND20.4 20.0
1,2,3-Trichlorobenzene ug/L 20 103 68-140105 2 3020ND20.5 20.9
1,2,3-Trichloropropane ug/L 20 98 67-13797 2 3020ND19.7 19.3
1,2,4-Trichlorobenzene ug/L 20 108 70-139105 2 3020ND21.6 21.0
1,2-Dibromo-3-
chloropropane ug/L 20 106 69-136102 4 3020ND21.3 20.4
1,2-Dibromoethane (EDB)ug/L 20 102 70-13799 3 3020ND20.5 19.8
1,2-Dichlorobenzene ug/L 20 103 70-133102 0 3020ND20.5 20.5
1,2-Dichloroethane ug/L 20 95 67-13893 2 3020ND19.0 18.6
1,2-Dichloropropane ug/L 20 99 70-13897 2 3020ND19.8 19.4
1,3-Dichlorobenzene ug/L 20 104 70-133105 1 3020ND20.8 20.9
1,3-Dichloropropane ug/L 20 104 70-136102 2 3020ND20.7 20.3
1,4-Dichlorobenzene ug/L 20 107 70-133104 2 3020ND21.4 20.9
2,2-Dichloropropane ug/L 20 105 52-155100 5 3020ND21.0 20.1
2-Butanone (MEK)ug/L 40 96 61-14795 0 3040ND38.2 38.1
2-Chlorotoluene ug/L 20 105 70-141105 1 3020ND20.9 21.0
2-Hexanone ug/L 40 103 67-139102 1 3040ND41.1 40.7
4-Chlorotoluene ug/L 20 104 70-135104 0 3020ND20.8 20.7
4-Methyl-2-pentanone
(MIBK)ug/L 40 98 67-13697 1 3040ND39.2 39.0
Acetone ug/L 40 96 55-159106 9 3040ND38.4 42.2
Benzene ug/L 20 102 67-15098 4 3020ND20.4 19.6
Bromobenzene ug/L 20 105 70-134105 0 3020ND20.9 21.0
Bromochloromethane ug/L 20 95 70-14691 4 3020ND18.9 18.1
Bromodichloromethane ug/L 20 96 70-13892 4 3020ND19.3 18.5
Bromoform ug/L 20 92 57-13891 1 3020ND18.3 18.1
Bromomethane ug/L 20 111 10-200103 8 3020ND22.1 20.5
Carbon tetrachloride ug/L 20 104 70-147103 1 3020ND20.8 20.6
Chlorobenzene ug/L 20 103 70-137100 3 3020ND20.7 20.0
Chloroethane ug/L 20 92 51-16687 5 3020ND18.3 17.4
Chloroform ug/L 20 101 70-14497 4 3020ND20.3 19.4
Chloromethane ug/L 20 90 24-16187 3 3020ND18.0 17.5
cis-1,2-Dichloroethene ug/L 20 99 67-14894 5 3020ND20.0 19.1
cis-1,3-Dichloropropene ug/L 20 102 70-14299 3 3020ND20.4 19.7
Dibromochloromethane ug/L 20 102 68-13899 3 3020ND20.4 19.7
Dibromomethane ug/L 20 100 70-13496 4 3020ND20.0 19.3
Dichlorodifluoromethane ug/L 20 86 43-15581 5 3020ND17.1 16.3
Diisopropyl ether ug/L 20 96 65-14691 5 3020ND19.2 18.3
Ethylbenzene ug/L 20 105 68-143101 4 3020ND21.0 20.1
Hexachloro-1,3-butadiene ug/L 20 108 62-151102 6 3020ND21.6 20.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3057010MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503310005
3057011
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 107 53-157102 5 3040ND42.6 40.7
Methyl-tert-butyl ether ug/L 20 96 59-15692 5 3020ND19.3 18.4
Methylene Chloride ug/L 20 95 64-14891 5 3020ND19.0 18.2
Naphthalene ug/L 20 130 57-150110 17 3020ND26.0 22.0
o-Xylene ug/L 20 106 68-143101 5 3020ND21.2 20.1
p-Isopropyltoluene ug/L 20 111 70-141109 1 3020ND22.1 21.9
Styrene ug/L 20 100 70-13697 3 3020ND20.0 19.5
Tetrachloroethene ug/L 20 106 70-139103 3 3020ND21.3 20.7
Toluene ug/L 20 104 47-15799 5 3020ND20.7 19.8
trans-1,2-Dichloroethene ug/L 20 103 70-149100 4 3020ND20.7 19.9
trans-1,3-Dichloropropene ug/L 20 100 70-13898 2 3020ND19.9 19.5
Trichloroethene ug/L 20 104 70-149100 3 30202.5 23.3 22.5
Trichlorofluoromethane ug/L 20 93 61-15491 3 3020ND18.7 18.1
Vinyl acetate ug/L 40 112 48-156106 5 3040ND44.6 42.4
Vinyl chloride ug/L 20 90 55-17287 3 3020ND17.9 17.4
Xylene (Total)ug/L 60 106 66-145101 5 3060ND63.8 60.8
1,2-Dichloroethane-d4 (S)%107 70-130102
4-Bromofluorobenzene (S)%98 70-13099
Toluene-d8 (S)%98 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
577668
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92503310006, 92503310007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3056393
Associated Lab Samples:92503310006, 92503310007
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/04/20 02:260.34
1,1,1-Trichloroethane ug/L ND 1.0 11/04/20 02:260.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/04/20 02:260.22
1,1,2-Trichloroethane ug/L ND 1.0 11/04/20 02:260.24
1,1-Dichloroethane ug/L ND 1.0 11/04/20 02:260.27
1,1-Dichloroethene ug/L ND 1.0 11/04/20 02:260.24
1,1-Dichloropropene ug/L ND 1.0 11/04/20 02:260.21
1,2,3-Trichlorobenzene ug/L ND 1.0 11/04/20 02:260.34
1,2,3-Trichloropropane ug/L ND 1.0 11/04/20 02:260.35
1,2,4-Trichlorobenzene ug/L ND 1.0 11/04/20 02:260.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 11/04/20 02:260.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/04/20 02:260.26
1,2-Dichlorobenzene ug/L ND 1.0 11/04/20 02:260.29
1,2-Dichloroethane ug/L ND 1.0 11/04/20 02:260.34
1,2-Dichloropropane ug/L ND 1.0 11/04/20 02:260.19
1,3-Dichlorobenzene ug/L ND 1.0 11/04/20 02:260.22
1,3-Dichloropropane ug/L ND 1.0 11/04/20 02:260.16
1,4-Dichlorobenzene ug/L ND 1.0 11/04/20 02:260.26
2,2-Dichloropropane ug/L ND 1.0 11/04/20 02:260.27
2-Butanone (MEK)ug/L ND 5.0 11/04/20 02:263.3
2-Chlorotoluene ug/L ND 1.0 11/04/20 02:260.20
2-Hexanone ug/L ND 5.0 11/04/20 02:260.57
4-Chlorotoluene ug/L ND 1.0 11/04/20 02:260.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/04/20 02:264.5
Acetone ug/L ND 25.0 11/04/20 02:266.2
Benzene ug/L ND 1.0 11/04/20 02:260.15
Bromobenzene ug/L ND 1.0 11/04/20 02:260.22
Bromochloromethane ug/L ND 1.0 11/04/20 02:260.34
Bromodichloromethane ug/L ND 1.0 11/04/20 02:260.26
Bromoform ug/L ND 1.0 11/04/20 02:260.62
Bromomethane ug/L ND 2.0 11/04/20 02:260.62
Carbon tetrachloride ug/L ND 1.0 11/04/20 02:260.22
Chlorobenzene ug/L ND 1.0 11/04/20 02:260.23
Chloroethane ug/L ND 1.0 11/04/20 02:260.49
Chloroform ug/L ND 5.0 11/04/20 02:262.3
Chloromethane ug/L ND 1.0 11/04/20 02:260.39
cis-1,2-Dichloroethene ug/L ND 1.0 11/04/20 02:260.29
cis-1,3-Dichloropropene ug/L ND 1.0 11/04/20 02:260.30
Dibromochloromethane ug/L ND 1.0 11/04/20 02:260.41
Dibromomethane ug/L ND 1.0 11/04/20 02:260.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3056393
Associated Lab Samples:92503310006, 92503310007
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 11/04/20 02:260.23
Diisopropyl ether ug/L ND 1.0 11/04/20 02:260.22
Ethylbenzene ug/L ND 1.0 11/04/20 02:260.26
Hexachloro-1,3-butadiene ug/L ND 1.0 11/04/20 02:260.44
m&p-Xylene ug/L ND 2.0 11/04/20 02:260.41
Methyl-tert-butyl ether ug/L ND 1.0 11/04/20 02:260.28
Methylene Chloride ug/L ND 5.0 11/04/20 02:263.7
Naphthalene ug/L ND 1.0 11/04/20 02:260.35
o-Xylene ug/L ND 1.0 11/04/20 02:260.22
p-Isopropyltoluene ug/L ND 1.0 11/04/20 02:260.21
Styrene ug/L ND 1.0 11/04/20 02:260.27
Tetrachloroethene ug/L ND 1.0 11/04/20 02:260.16
Toluene ug/L ND 1.0 11/04/20 02:260.24
trans-1,2-Dichloroethene ug/L ND 1.0 11/04/20 02:260.25
trans-1,3-Dichloropropene ug/L ND 1.0 11/04/20 02:260.31
Trichloroethene ug/L ND 1.0 11/04/20 02:260.22
Trichlorofluoromethane ug/L ND 1.0 11/04/20 02:260.31
Vinyl acetate ug/L ND 2.0 11/04/20 02:261.4
Vinyl chloride ug/L ND 1.0 11/04/20 02:260.24
Xylene (Total)ug/L ND 1.0 11/04/20 02:260.63
1,2-Dichloroethane-d4 (S)%102 70-130 11/04/20 02:26
4-Bromofluorobenzene (S)%100 70-130 11/04/20 02:26
Toluene-d8 (S)%98 70-130 11/04/20 02:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3056394LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.350 113 70-130
1,1,1-Trichloroethane ug/L 54.750 109 70-130
1,1,2,2-Tetrachloroethane ug/L 51.650 103 70-130
1,1,2-Trichloroethane ug/L 50.650 101 70-130
1,1-Dichloroethane ug/L 53.650 107 70-130
1,1-Dichloroethene ug/L 53.950 108 70-132
1,1-Dichloropropene ug/L 52.150 104 70-131
1,2,3-Trichlorobenzene ug/L 46.750 93 70-134
1,2,3-Trichloropropane ug/L 50.650 101 70-130
1,2,4-Trichlorobenzene ug/L 51.150 102 70-130
1,2-Dibromo-3-chloropropane ug/L 56.650 113 70-132
1,2-Dibromoethane (EDB)ug/L 54.450 109 70-130
1,2-Dichlorobenzene ug/L 54.550 109 70-130
1,2-Dichloroethane ug/L 54.150 108 70-130
1,2-Dichloropropane ug/L 52.850 106 70-130
1,3-Dichlorobenzene ug/L 53.550 107 70-130
1,3-Dichloropropane ug/L 53.850 108 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3056394LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 55.450 111 70-130
2,2-Dichloropropane ug/L 50.350 101 70-130
2-Butanone (MEK)ug/L 114100 114 70-133
2-Chlorotoluene ug/L 55.250 110 70-130
2-Hexanone ug/L 118100 118 70-130
4-Chlorotoluene ug/L 54.150 108 70-130
4-Methyl-2-pentanone (MIBK)ug/L 111100 111 70-130
Acetone ug/L 125100 125 70-144
Benzene ug/L 51.050 102 70-130
Bromobenzene ug/L 54.850 110 70-130
Bromochloromethane ug/L 53.050 106 70-130
Bromodichloromethane ug/L 51.550 103 70-130
Bromoform ug/L 46.550 93 70-131
Bromomethane ug/L 46.450 93 30-177
Carbon tetrachloride ug/L 53.450 107 70-130
Chlorobenzene ug/L 52.750 105 70-130
Chloroethane ug/L 41.450 83 46-131
Chloroform ug/L 54.250 108 70-130
Chloromethane ug/L 53.550 107 49-130
cis-1,2-Dichloroethene ug/L 52.250 104 70-130
cis-1,3-Dichloropropene ug/L 53.850 108 70-130
Dibromochloromethane ug/L 58.450 117 70-130
Dibromomethane ug/L 52.450 105 70-130
Dichlorodifluoromethane ug/L 42.750 85 52-134
Diisopropyl ether ug/L 54.150 108 70-131
Ethylbenzene ug/L 51.150 102 70-130
Hexachloro-1,3-butadiene ug/L 47.150 94 70-131
m&p-Xylene ug/L 106100 106 70-130
Methyl-tert-butyl ether ug/L 49.850 100 70-130
Methylene Chloride ug/L 44.650 89 68-130
Naphthalene ug/L 51.650 103 70-133
o-Xylene ug/L 53.550 107 70-130
p-Isopropyltoluene ug/L 51.950 104 70-130
Styrene ug/L 52.950 106 70-130
Tetrachloroethene ug/L 50.850 102 70-130
Toluene ug/L 51.050 102 70-130
trans-1,2-Dichloroethene ug/L 53.850 108 70-130
trans-1,3-Dichloropropene ug/L 54.650 109 70-130
Trichloroethene ug/L 52.150 104 70-130
Trichlorofluoromethane ug/L 46.850 94 61-130
Vinyl acetate ug/L 118100 118 70-140
Vinyl chloride ug/L 47.050 94 59-142
Xylene (Total)ug/L 159150 106 70-130
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3056395MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503312003
3056396
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 107 70-135111 4 3020ND21.3 22.3
1,1,1-Trichloroethane ug/L 20 113 70-148110 2 3020ND22.5 22.1
1,1,2,2-Tetrachloroethane ug/L 20 99 70-131105 5 3020ND19.8 20.9
1,1,2-Trichloroethane ug/L 20 102 70-136104 2 3020ND20.4 20.9
1,1-Dichloroethane ug/L 20 106 70-147107 1 3020ND21.2 21.5
1,1-Dichloroethene ug/L 20 114 70-158113 1 3020ND22.7 22.6
1,1-Dichloropropene ug/L 20 108 70-149109 1 3020ND21.5 21.8
1,2,3-Trichlorobenzene ug/L 20 76 68-14079 3 3020ND15.2 15.8
1,2,3-Trichloropropane ug/L 20 99 67-137103 4 3020ND19.8 20.5
1,2,4-Trichlorobenzene ug/L 20 86 70-13988 3 3020ND17.1 17.6
1,2-Dibromo-3-
chloropropane ug/L 20 106 69-136109 3 3020ND21.1 21.8
1,2-Dibromoethane (EDB)ug/L 20 105 70-137109 4 3020ND20.9 21.8
1,2-Dichlorobenzene ug/L 20 101 70-133104 3 3020ND20.3 20.8
1,2-Dichloroethane ug/L 20 104 67-138105 1 3020ND20.7 21.0
1,2-Dichloropropane ug/L 20 108 70-138110 2 3020ND21.5 22.0
1,3-Dichlorobenzene ug/L 20 99 70-133101 2 3020ND19.9 20.2
1,3-Dichloropropane ug/L 20 104 70-136108 3 3020ND20.8 21.5
1,4-Dichlorobenzene ug/L 20 104 70-133104 0 3020ND20.8 20.8
2,2-Dichloropropane ug/L 20 102 52-155101 1 3020ND20.4 20.3
2-Butanone (MEK)ug/L 40 106 61-147114 8 3040ND42.3 45.7
2-Chlorotoluene ug/L 20 107 70-141108 1 3020ND21.4 21.6
2-Hexanone ug/L 40 103 67-139108 6 3040ND41.0 43.4
4-Chlorotoluene ug/L 20 106 70-135107 1 3020ND21.1 21.4
4-Methyl-2-pentanone
(MIBK)ug/L 40 102 67-136106 5 3040ND40.6 42.6
Acetone ug/L 40 105 55-159112 6 3040ND42.2 44.8
Benzene ug/L 20 105 67-150106 1 3020ND21.0 21.3
Bromobenzene ug/L 20 111 70-134114 2 3020ND22.3 22.8
Bromochloromethane ug/L 20 108 70-146107 1 3020ND21.6 21.4
Bromodichloromethane ug/L 20 99 70-138103 4 3020ND19.9 20.6
Bromoform ug/L 20 85 57-13888 4 3020ND17.0 17.6
Bromomethane ug/L 20 104 10-200105 1 3020ND20.8 21.1
Carbon tetrachloride ug/L 20 112 70-147112 1 3020ND22.3 22.5
Chlorobenzene ug/L 20 105 70-137108 3 3020ND21.0 21.6
Chloroethane ug/L 20 103 51-166101 2 3020ND20.7 20.2
Chloroform ug/L 20 102 70-144109 7 3020ND20.4 21.9
Chloromethane ug/L 20 102 24-161105 3 3020ND20.3 20.9
cis-1,2-Dichloroethene ug/L 20 104 67-148105 2 3020ND20.7 21.1
cis-1,3-Dichloropropene ug/L 20 103 70-142106 3 3020ND20.5 21.3
Dibromochloromethane ug/L 20 105 68-138108 3 3020ND21.1 21.7
Dibromomethane ug/L 20 106 70-134106 0 3020ND21.1 21.2
Dichlorodifluoromethane ug/L 20 95 43-15595 0 3020ND19.1 19.0
Diisopropyl ether ug/L 20 100 65-146102 1 3020ND20.0 20.3
Ethylbenzene ug/L 20 102 68-143104 2 3020ND20.4 20.8
Hexachloro-1,3-butadiene ug/L 20 80 62-15177 4 3020ND16.0 15.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
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Page 27 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3056395MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503312003
3056396
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 106 53-157107 2 3040ND42.2 42.9
Methyl-tert-butyl ether ug/L 20 96 59-15698 1 3020ND19.2 19.5
Methylene Chloride ug/L M1204564-14846 1 3020ND9.1 9.1
Naphthalene ug/L 20 95 57-15098 3 3020ND19.1 19.7
o-Xylene ug/L 20 104 68-143105 1 3020ND20.9 21.1
p-Isopropyltoluene ug/L 20 96 70-14198 2 3020ND19.2 19.6
Styrene ug/L 20 98 70-136100 2 3020ND19.6 20.1
Tetrachloroethene ug/L 20 100 70-139104 4 3020ND20.0 20.8
Toluene ug/L 20 104 47-157106 2 3020ND20.7 21.1
trans-1,2-Dichloroethene ug/L 20 107 70-149108 1 3020ND21.5 21.7
trans-1,3-Dichloropropene ug/L 20 104 70-138107 3 3020ND20.7 21.4
Trichloroethene ug/L 20 107 70-149110 2 3020ND21.5 22.0
Trichlorofluoromethane ug/L 20 104 61-154106 2 3020ND20.8 21.1
Vinyl acetate ug/L 40 101 48-156102 1 3040ND40.5 41.0
Vinyl chloride ug/L 20 100 55-172100 0 3020ND19.9 19.9
Xylene (Total)ug/L 60 105 66-145107 1 3060ND63.1 64.0
1,2-Dichloroethane-d4 (S)%105 70-130104
4-Bromofluorobenzene (S)%97 70-13099
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
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Page 28 of 33
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
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Page 29 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92503310
Crayton Printing (AKR-005)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92503310001 577666MW-1 EPA 8260D
92503310002 577666MW-2 EPA 8260D
92503310003 577666MW-3 EPA 8260D
92503310004 577666MW-4 EPA 8260D
92503310005 577666MW-5 EPA 8260D
92503310006 577668DuplicateEPA 8260D
92503310007 577668Trip Blank EPA 8260D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/06/2020 02:45 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 33
Page 31 of 33
Page 32 of 33
Page 33 of 33
#=CL#
November 20, 2020
LIMS USE: FR - MATT BRAMBLETT
LIMS OBJECT ID: 92506249
92506249
Project:
Pace Project No.:
RE:
Matt Bramblett
Hart & Hickman
2923 S.Tyron St.
Charlotte, NC 28203
Crayton Printing (AKR-005)
Dear Matt Bramblett:
Enclosed are the analytical results for sample(s) received by the laboratory on November 16, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 2 of 23
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Lab ID Sample ID Matrix Date Collected Date Received
92506249001 MW-4 Water 11/13/20 16:00 11/16/20 10:09
92506249002 DUP Water 11/13/20 00:00 11/16/20 10:09
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 3 of 23
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92506249001 MW-4 EPA 8260D 63 PASI-CSAS
92506249002 DUP EPA 8260D 63 PASI-CCL
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Sample:MW-4 Lab ID:92506249001 Collected:11/13/20 16:00 Received:11/16/20 10:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 10.3J ug/L 11/18/20 15:47 67-64-125.0 6.2 1
Benzene ND ug/L 11/18/20 15:47 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/18/20 15:47 108-86-1 M11.0 0.22 1
Bromochloromethane ND ug/L 11/18/20 15:47 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/18/20 15:47 75-27-41.0 0.26 1
Bromoform ND ug/L 11/18/20 15:47 75-25-2 IK1.0 0.62 1
Bromomethane ND ug/L 11/18/20 15:47 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 11/18/20 15:47 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/18/20 15:47 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/18/20 15:47 108-90-7 M11.0 0.23 1
Chloroethane ND ug/L 11/18/20 15:47 75-00-31.0 0.49 1
Chloroform ND ug/L 11/18/20 15:47 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/18/20 15:47 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/18/20 15:47 95-49-8 M11.0 0.20 1
4-Chlorotoluene ND ug/L 11/18/20 15:47 106-43-4 M11.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/18/20 15:47 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/18/20 15:47 124-48-1 IK1.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/18/20 15:47 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/18/20 15:47 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/18/20 15:47 95-50-1 M11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/18/20 15:47 541-73-1 M11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/18/20 15:47 106-46-7 M11.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/18/20 15:47 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/18/20 15:47 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/18/20 15:47 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/18/20 15:47 75-35-41.0 0.24 1
cis-1,2-Dichloroethene 13.9 ug/L 11/18/20 15:47 156-59-2 M11.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/18/20 15:47 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/18/20 15:47 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/18/20 15:47 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/18/20 15:47 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/18/20 15:47 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/18/20 15:47 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/18/20 15:47 10061-02-6 IK1.0 0.31 1
Diisopropyl ether ND ug/L 11/18/20 15:47 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/18/20 15:47 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/18/20 15:47 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/18/20 15:47 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/18/20 15:47 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/18/20 15:47 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/20 15:47 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/18/20 15:47 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/18/20 15:47 91-20-3 IK1.0 0.35 1
Styrene ND ug/L 11/18/20 15:47 100-42-5 M11.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/18/20 15:47 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
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Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Sample:MW-4 Lab ID:92506249001 Collected:11/13/20 16:00 Received:11/16/20 10:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 11/18/20 15:47 79-34-5 M11.0 0.22 1
Tetrachloroethene ND ug/L 11/18/20 15:47 127-18-41.0 0.16 1
Toluene 0.37J ug/L 11/18/20 15:47 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/18/20 15:47 87-61-6 IK,M11.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/18/20 15:47 120-82-1 IK,M11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/18/20 15:47 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/18/20 15:47 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/18/20 15:47 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/18/20 15:47 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/18/20 15:47 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/18/20 15:47 108-05-42.0 1.4 1
Vinyl chloride 3.1 ug/L 11/18/20 15:47 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/18/20 15:47 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/18/20 15:47 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/18/20 15:47 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)101 %11/18/20 15:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %11/18/20 15:47 17060-07-070-130 1
Toluene-d8 (S)104 %11/18/20 15:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Sample:DUP Lab ID:92506249002 Collected:11/13/20 00:00 Received:11/16/20 10:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 11.1J ug/L 11/18/20 18:30 67-64-1 v125.0 6.2 1
Benzene ND ug/L 11/18/20 18:30 71-43-21.0 0.15 1
Bromobenzene ND ug/L 11/18/20 18:30 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 11/18/20 18:30 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 11/18/20 18:30 75-27-41.0 0.26 1
Bromoform ND ug/L 11/18/20 18:30 75-25-21.0 0.62 1
Bromomethane ND ug/L 11/18/20 18:30 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 11/18/20 18:30 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 11/18/20 18:30 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 11/18/20 18:30 108-90-71.0 0.23 1
Chloroethane ND ug/L 11/18/20 18:30 75-00-31.0 0.49 1
Chloroform ND ug/L 11/18/20 18:30 67-66-35.0 2.3 1
Chloromethane ND ug/L 11/18/20 18:30 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 11/18/20 18:30 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 11/18/20 18:30 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 11/18/20 18:30 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 11/18/20 18:30 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 11/18/20 18:30 106-93-41.0 0.26 1
Dibromomethane ND ug/L 11/18/20 18:30 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 11/18/20 18:30 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 11/18/20 18:30 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 11/18/20 18:30 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 11/18/20 18:30 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 11/18/20 18:30 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 11/18/20 18:30 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 11/18/20 18:30 75-35-41.0 0.24 1
cis-1,2-Dichloroethene 12.6 ug/L 11/18/20 18:30 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 11/18/20 18:30 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 11/18/20 18:30 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 11/18/20 18:30 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 11/18/20 18:30 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 11/18/20 18:30 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 11/18/20 18:30 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 11/18/20 18:30 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 11/18/20 18:30 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 11/18/20 18:30 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 11/18/20 18:30 87-68-31.0 0.44 1
2-Hexanone ND ug/L 11/18/20 18:30 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 11/18/20 18:30 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 11/18/20 18:30 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 11/18/20 18:30 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 11/18/20 18:30 1634-04-41.0 0.28 1
Naphthalene ND ug/L 11/18/20 18:30 91-20-31.0 0.35 1
Styrene ND ug/L 11/18/20 18:30 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 11/18/20 18:30 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
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Page 7 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Sample:DUP Lab ID:92506249002 Collected:11/13/20 00:00 Received:11/16/20 10:09 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 11/18/20 18:30 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 11/18/20 18:30 127-18-41.0 0.16 1
Toluene 0.34J ug/L 11/18/20 18:30 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 11/18/20 18:30 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 11/18/20 18:30 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 11/18/20 18:30 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 11/18/20 18:30 79-00-51.0 0.24 1
Trichloroethene ND ug/L 11/18/20 18:30 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 11/18/20 18:30 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 11/18/20 18:30 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 11/18/20 18:30 108-05-4 v12.0 1.4 1
Vinyl chloride 2.7 ug/L 11/18/20 18:30 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 11/18/20 18:30 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 11/18/20 18:30 179601-23-12.0 0.41 1
o-Xylene ND ug/L 11/18/20 18:30 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)100 %11/18/20 18:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)110 %11/18/20 18:30 17060-07-070-130 1
Toluene-d8 (S)99 %11/18/20 18:30 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
581017
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92506249002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3073239
Associated Lab Samples:92506249002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/18/20 17:170.34
1,1,1-Trichloroethane ug/L ND 1.0 11/18/20 17:170.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/18/20 17:170.22
1,1,2-Trichloroethane ug/L ND 1.0 11/18/20 17:170.24
1,1-Dichloroethane ug/L ND 1.0 11/18/20 17:170.27
1,1-Dichloroethene ug/L ND 1.0 11/18/20 17:170.24
1,1-Dichloropropene ug/L ND 1.0 11/18/20 17:170.21
1,2,3-Trichlorobenzene ug/L ND 1.0 11/18/20 17:170.34
1,2,3-Trichloropropane ug/L ND 1.0 11/18/20 17:170.35
1,2,4-Trichlorobenzene ug/L ND 1.0 11/18/20 17:170.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 11/18/20 17:170.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/18/20 17:170.26
1,2-Dichlorobenzene ug/L ND 1.0 11/18/20 17:170.29
1,2-Dichloroethane ug/L ND 1.0 11/18/20 17:170.34
1,2-Dichloropropane ug/L ND 1.0 11/18/20 17:170.19
1,3-Dichlorobenzene ug/L ND 1.0 11/18/20 17:170.22
1,3-Dichloropropane ug/L ND 1.0 11/18/20 17:170.16
1,4-Dichlorobenzene ug/L ND 1.0 11/18/20 17:170.26
2,2-Dichloropropane ug/L ND 1.0 11/18/20 17:170.27
2-Butanone (MEK)ug/L ND 5.0 11/18/20 17:173.3
2-Chlorotoluene ug/L ND 1.0 11/18/20 17:170.20
2-Hexanone ug/L ND 5.0 11/18/20 17:170.57
4-Chlorotoluene ug/L ND 1.0 11/18/20 17:170.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/18/20 17:174.5
Acetone ug/L ND 25.0 v111/18/20 17:176.2
Benzene ug/L ND 1.0 11/18/20 17:170.15
Bromobenzene ug/L ND 1.0 11/18/20 17:170.22
Bromochloromethane ug/L ND 1.0 11/18/20 17:170.34
Bromodichloromethane ug/L ND 1.0 11/18/20 17:170.26
Bromoform ug/L ND 1.0 11/18/20 17:170.62
Bromomethane ug/L ND 2.0 11/18/20 17:170.62
Carbon tetrachloride ug/L ND 1.0 11/18/20 17:170.22
Chlorobenzene ug/L ND 1.0 11/18/20 17:170.23
Chloroethane ug/L ND 1.0 11/18/20 17:170.49
Chloroform ug/L ND 5.0 11/18/20 17:172.3
Chloromethane ug/L ND 1.0 11/18/20 17:170.39
cis-1,2-Dichloroethene ug/L ND 1.0 11/18/20 17:170.29
cis-1,3-Dichloropropene ug/L ND 1.0 11/18/20 17:170.30
Dibromochloromethane ug/L ND 1.0 11/18/20 17:170.41
Dibromomethane ug/L ND 1.0 11/18/20 17:170.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3073239
Associated Lab Samples:92506249002
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 11/18/20 17:170.23
Diisopropyl ether ug/L ND 1.0 11/18/20 17:170.22
Ethylbenzene ug/L ND 1.0 11/18/20 17:170.26
Hexachloro-1,3-butadiene ug/L ND 1.0 11/18/20 17:170.44
m&p-Xylene ug/L ND 2.0 11/18/20 17:170.41
Methyl-tert-butyl ether ug/L ND 1.0 11/18/20 17:170.28
Methylene Chloride ug/L ND 5.0 11/18/20 17:173.7
Naphthalene ug/L ND 1.0 11/18/20 17:170.35
o-Xylene ug/L ND 1.0 11/18/20 17:170.22
p-Isopropyltoluene ug/L ND 1.0 11/18/20 17:170.21
Styrene ug/L ND 1.0 11/18/20 17:170.27
Tetrachloroethene ug/L ND 1.0 11/18/20 17:170.16
Toluene ug/L ND 1.0 11/18/20 17:170.24
trans-1,2-Dichloroethene ug/L ND 1.0 11/18/20 17:170.25
trans-1,3-Dichloropropene ug/L ND 1.0 11/18/20 17:170.31
Trichloroethene ug/L ND 1.0 11/18/20 17:170.22
Trichlorofluoromethane ug/L ND 1.0 11/18/20 17:170.31
Vinyl acetate ug/L ND 2.0 v111/18/20 17:171.4
Vinyl chloride ug/L ND 1.0 11/18/20 17:170.24
Xylene (Total)ug/L ND 1.0 11/18/20 17:170.63
1,2-Dichloroethane-d4 (S)%110 70-130 11/18/20 17:17
4-Bromofluorobenzene (S)%100 70-130 11/18/20 17:17
Toluene-d8 (S)%100 70-130 11/18/20 17:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3073240LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.450 101 70-130
1,1,1-Trichloroethane ug/L 52.150 104 70-130
1,1,2,2-Tetrachloroethane ug/L 51.250 102 70-130
1,1,2-Trichloroethane ug/L 50.350 101 70-130
1,1-Dichloroethane ug/L 51.450 103 70-130
1,1-Dichloroethene ug/L 58.250 116 70-132
1,1-Dichloropropene ug/L 52.450 105 70-131
1,2,3-Trichlorobenzene ug/L 53.750 107 70-134
1,2,3-Trichloropropane ug/L 52.850 106 70-130
1,2,4-Trichlorobenzene ug/L 52.950 106 70-130
1,2-Dibromo-3-chloropropane ug/L 53.550 107 70-132
1,2-Dibromoethane (EDB)ug/L 51.950 104 70-130
1,2-Dichlorobenzene ug/L 48.750 97 70-130
1,2-Dichloroethane ug/L 53.550 107 70-130
1,2-Dichloropropane ug/L 49.750 99 70-130
1,3-Dichlorobenzene ug/L 48.350 97 70-130
1,3-Dichloropropane ug/L 50.850 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3073240LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 47.550 95 70-130
2,2-Dichloropropane ug/L 54.950 110 70-130
2-Butanone (MEK)ug/L 114100 114 70-133
2-Chlorotoluene ug/L 47.650 95 70-130
2-Hexanone ug/L 114100 114 70-130
4-Chlorotoluene ug/L 46.250 92 70-130
4-Methyl-2-pentanone (MIBK)ug/L 107100 107 70-130
Acetone ug/L 128 v110012870-144
Benzene ug/L 48.050 96 70-130
Bromobenzene ug/L 48.550 97 70-130
Bromochloromethane ug/L 51.150 102 70-130
Bromodichloromethane ug/L 46.450 93 70-130
Bromoform ug/L 50.350 101 70-131
Bromomethane ug/L 41.650 83 30-177
Carbon tetrachloride ug/L 54.550 109 70-130
Chlorobenzene ug/L 48.650 97 70-130
Chloroethane ug/L 46.550 93 46-131
Chloroform ug/L 50.550 101 70-130
Chloromethane ug/L 44.750 89 49-130
cis-1,2-Dichloroethene ug/L 51.350 103 70-130
cis-1,3-Dichloropropene ug/L 53.350 107 70-130
Dibromochloromethane ug/L 52.550 105 70-130
Dibromomethane ug/L 50.450 101 70-130
Dichlorodifluoromethane ug/L 47.050 94 52-134
Diisopropyl ether ug/L 49.550 99 70-131
Ethylbenzene ug/L 48.750 97 70-130
Hexachloro-1,3-butadiene ug/L 54.950 110 70-131
m&p-Xylene ug/L 98.5100 98 70-130
Methyl-tert-butyl ether ug/L 51.250 102 70-130
Methylene Chloride ug/L 50.150 100 68-130
Naphthalene ug/L 53.350 107 70-133
o-Xylene ug/L 47.450 95 70-130
p-Isopropyltoluene ug/L 48.350 97 70-130
Styrene ug/L 49.450 99 70-130
Tetrachloroethene ug/L 49.550 99 70-130
Toluene ug/L 48.450 97 70-130
trans-1,2-Dichloroethene ug/L 54.750 109 70-130
trans-1,3-Dichloropropene ug/L 52.650 105 70-130
Trichloroethene ug/L 52.350 105 70-130
Trichlorofluoromethane ug/L 50.050 100 61-130
Vinyl acetate ug/L 121 v110012170-140
Vinyl chloride ug/L 46.850 94 59-142
Xylene (Total)ug/L 146150 97 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3073241MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92506317003
3073242
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 108 70-135107 1 3020ND21.6 21.4
1,1,1-Trichloroethane ug/L 20 114 70-148116 1 3020ND22.8 23.2
1,1,2,2-Tetrachloroethane ug/L 20 103 70-131104 1 3020ND20.6 20.8
1,1,2-Trichloroethane ug/L 20 105 70-136107 2 3020ND21.0 21.4
1,1-Dichloroethane ug/L 20 110 70-147114 3 3020ND22.8 23.5
1,1-Dichloroethene ug/L 20 126 70-158128 1 3020ND25.2 25.5
1,1-Dichloropropene ug/L M1,R1206470-149111 53 3020ND12.9 22.1
1,2,3-Trichlorobenzene ug/L 20 98 68-140109 11 3020ND19.5 21.8
1,2,3-Trichloropropane ug/L 20 101 67-137104 4 3020ND20.2 20.9
1,2,4-Trichlorobenzene ug/L 20 102 70-139106 4 3020ND20.5 21.2
1,2-Dibromo-3-
chloropropane ug/L 20 103 69-136109 6 3020ND20.6 21.9
1,2-Dibromoethane (EDB)ug/L 20 106 70-137106 0 3020ND21.3 21.2
1,2-Dichlorobenzene ug/L 20 104 70-133104 0 3020ND20.8 20.8
1,2-Dichloroethane ug/L 20 110 67-138116 5 3020ND22.0 23.1
1,2-Dichloropropane ug/L 20 105 70-138107 1 3020ND21.0 21.3
1,3-Dichlorobenzene ug/L 20 105 70-133102 2 3020ND20.9 20.4
1,3-Dichloropropane ug/L 20 103 70-136107 3 3020ND20.7 21.4
1,4-Dichlorobenzene ug/L 20 104 70-133102 2 3020ND20.7 20.4
2,2-Dichloropropane ug/L 20 118 52-155122 3 3020ND23.7 24.4
2-Butanone (MEK)ug/L v14010461-147111 6 3040ND41.7 44.4
2-Chlorotoluene ug/L 20 105 70-141104 1 3020ND21.0 20.8
2-Hexanone ug/L v14010067-139109 9 3040ND39.9 43.8
4-Chlorotoluene ug/L 20 102 70-135103 1 3020ND20.4 20.5
4-Methyl-2-pentanone
(MIBK)ug/L 40 97 67-136102 5 3040ND38.8 40.9
Acetone ug/L v14011055-159122 10 3040ND44.0 48.7
Benzene ug/L 20 103 67-150105 2 3020ND20.6 21.0
Bromobenzene ug/L 20 104 70-134105 0 3020ND20.9 20.9
Bromochloromethane ug/L 20 110 70-146114 4 3020ND21.9 22.8
Bromodichloromethane ug/L 20 99 70-13897 1 3020ND19.7 19.4
Bromoform ug/L 20 100 57-138100 0 3020ND20.0 19.9
Bromomethane ug/L 20 83 10-20087 5 3020ND16.6 17.5
Carbon tetrachloride ug/L 20 124 70-147118 5 3020ND24.7 23.5
Chlorobenzene ug/L 20 103 70-137105 2 3020ND20.5 21.0
Chloroethane ug/L 20 105 51-166108 3 3020ND21.1 21.7
Chloroform ug/L 20 110 70-144114 4 3020ND22.3 23.1
Chloromethane ug/L 20 94 24-16196 2 3020ND18.8 19.2
cis-1,2-Dichloroethene ug/L 20 104 67-148112 7 3020ND20.9 22.4
cis-1,3-Dichloropropene ug/L 20 106 70-142109 3 3020ND21.3 21.8
Dibromochloromethane ug/L 20 104 68-138104 0 3020ND20.8 20.8
Dibromomethane ug/L 20 106 70-134107 1 3020ND21.2 21.4
Dichlorodifluoromethane ug/L 20 107 43-155115 8 3020ND21.3 23.0
Diisopropyl ether ug/L 20 97 65-14699 3 3020ND19.4 19.9
Ethylbenzene ug/L 20 102 68-143102 0 3020ND20.4 20.4
Hexachloro-1,3-butadiene ug/L 20 109 62-151117 7 3020ND21.8 23.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3073241MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92506317003
3073242
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 104 53-157104 0 3040ND41.4 41.6
Methyl-tert-butyl ether ug/L 20 100 59-156104 5 3020ND19.9 20.9
Methylene Chloride ug/L 20 108 64-148109 0 3020ND21.7 21.8
Naphthalene ug/L 20 97 57-150107 10 3020ND19.4 21.4
o-Xylene ug/L 20 99 68-14399 0 3020ND19.8 19.8
p-Isopropyltoluene ug/L 20 101 70-141101 1 3020ND20.1 20.2
Styrene ug/L 20 98 70-13696 2 3020ND19.5 19.1
Tetrachloroethene ug/L 20 102 70-139103 1 3020ND20.4 20.7
Toluene ug/L 20 101 47-157104 3 3020ND20.2 20.8
trans-1,2-Dichloroethene ug/L 20 114 70-149120 5 3020ND22.8 24.0
trans-1,3-Dichloropropene ug/L 20 106 70-138108 1 3020ND21.2 21.5
Trichloroethene ug/L 20 114 70-149116 2 3020ND22.8 23.3
Trichlorofluoromethane ug/L 20 113 61-154116 3 3020ND22.6 23.3
Vinyl acetate ug/L v14011348-156118 5 3040ND45.1 47.4
Vinyl chloride ug/L 20 105 55-172109 4 3020ND21.1 21.9
Xylene (Total)ug/L 60 102 66-145102 0 3060ND61.2 61.4
1,2-Dichloroethane-d4 (S)%107 70-130111
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%98 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
581079
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92506249001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3073451
Associated Lab Samples:92506249001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/18/20 12:510.34
1,1,1-Trichloroethane ug/L ND 1.0 11/18/20 12:510.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/18/20 12:510.22
1,1,2-Trichloroethane ug/L ND 1.0 11/18/20 12:510.24
1,1-Dichloroethane ug/L ND 1.0 11/18/20 12:510.27
1,1-Dichloroethene ug/L ND 1.0 11/18/20 12:510.24
1,1-Dichloropropene ug/L ND 1.0 11/18/20 12:510.21
1,2,3-Trichlorobenzene ug/L ND 1.0 IK11/18/20 12:510.34
1,2,3-Trichloropropane ug/L ND 1.0 11/18/20 12:510.35
1,2,4-Trichlorobenzene ug/L ND 1.0 IK11/18/20 12:510.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 11/18/20 12:510.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 11/18/20 12:510.26
1,2-Dichlorobenzene ug/L ND 1.0 11/18/20 12:510.29
1,2-Dichloroethane ug/L ND 1.0 11/18/20 12:510.34
1,2-Dichloropropane ug/L ND 1.0 11/18/20 12:510.19
1,3-Dichlorobenzene ug/L ND 1.0 11/18/20 12:510.22
1,3-Dichloropropane ug/L ND 1.0 11/18/20 12:510.16
1,4-Dichlorobenzene ug/L ND 1.0 11/18/20 12:510.26
2,2-Dichloropropane ug/L ND 1.0 11/18/20 12:510.27
2-Butanone (MEK)ug/L ND 5.0 11/18/20 12:513.3
2-Chlorotoluene ug/L ND 1.0 11/18/20 12:510.20
2-Hexanone ug/L ND 5.0 11/18/20 12:510.57
4-Chlorotoluene ug/L ND 1.0 11/18/20 12:510.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 11/18/20 12:514.5
Acetone ug/L ND 25.0 11/18/20 12:516.2
Benzene ug/L ND 1.0 11/18/20 12:510.15
Bromobenzene ug/L ND 1.0 11/18/20 12:510.22
Bromochloromethane ug/L ND 1.0 11/18/20 12:510.34
Bromodichloromethane ug/L ND 1.0 11/18/20 12:510.26
Bromoform ug/L ND 1.0 IK11/18/20 12:510.62
Bromomethane ug/L ND 2.0 11/18/20 12:510.62
Carbon tetrachloride ug/L ND 1.0 11/18/20 12:510.22
Chlorobenzene ug/L ND 1.0 11/18/20 12:510.23
Chloroethane ug/L ND 1.0 11/18/20 12:510.49
Chloroform ug/L ND 5.0 11/18/20 12:512.3
Chloromethane ug/L ND 1.0 11/18/20 12:510.39
cis-1,2-Dichloroethene ug/L ND 1.0 11/18/20 12:510.29
cis-1,3-Dichloropropene ug/L ND 1.0 11/18/20 12:510.30
Dibromochloromethane ug/L ND 1.0 IK11/18/20 12:510.41
Dibromomethane ug/L ND 1.0 11/18/20 12:510.46
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
Pace Analytical Services, LLC
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Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3073451
Associated Lab Samples:92506249001
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 11/18/20 12:510.23
Diisopropyl ether ug/L ND 1.0 11/18/20 12:510.22
Ethylbenzene ug/L ND 1.0 11/18/20 12:510.26
Hexachloro-1,3-butadiene ug/L ND 1.0 11/18/20 12:510.44
m&p-Xylene ug/L ND 2.0 11/18/20 12:510.41
Methyl-tert-butyl ether ug/L ND 1.0 11/18/20 12:510.28
Methylene Chloride ug/L ND 5.0 11/18/20 12:513.7
Naphthalene ug/L ND 1.0 IK11/18/20 12:510.35
o-Xylene ug/L ND 1.0 11/18/20 12:510.22
p-Isopropyltoluene ug/L ND 1.0 11/18/20 12:510.21
Styrene ug/L ND 1.0 11/18/20 12:510.27
Tetrachloroethene ug/L ND 1.0 11/18/20 12:510.16
Toluene ug/L ND 1.0 11/18/20 12:510.24
trans-1,2-Dichloroethene ug/L ND 1.0 11/18/20 12:510.25
trans-1,3-Dichloropropene ug/L ND 1.0 IK11/18/20 12:510.31
Trichloroethene ug/L ND 1.0 11/18/20 12:510.22
Trichlorofluoromethane ug/L ND 1.0 11/18/20 12:510.31
Vinyl acetate ug/L ND 2.0 11/18/20 12:511.4
Vinyl chloride ug/L ND 1.0 11/18/20 12:510.24
Xylene (Total)ug/L ND 1.0 11/18/20 12:510.63
1,2-Dichloroethane-d4 (S)%99 70-130 11/18/20 12:51
4-Bromofluorobenzene (S)%101 70-130 11/18/20 12:51
Toluene-d8 (S)%103 70-130 11/18/20 12:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3073452LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 41.250 82 70-130
1,1,1-Trichloroethane ug/L 48.850 98 70-130
1,1,2,2-Tetrachloroethane ug/L 48.650 97 70-130
1,1,2-Trichloroethane ug/L 48.950 98 70-130
1,1-Dichloroethane ug/L 49.350 99 70-130
1,1-Dichloroethene ug/L 52.450 105 70-132
1,1-Dichloropropene ug/L 51.450 103 70-131
1,2,3-Trichlorobenzene ug/L 38.2 IK507670-134
1,2,3-Trichloropropane ug/L 47.750 95 70-130
1,2,4-Trichlorobenzene ug/L 38.5 IK507770-130
1,2-Dibromo-3-chloropropane ug/L 50.550 101 70-132
1,2-Dibromoethane (EDB)ug/L 48.750 97 70-130
1,2-Dichlorobenzene ug/L 42.450 85 70-130
1,2-Dichloroethane ug/L 46.650 93 70-130
1,2-Dichloropropane ug/L 49.350 99 70-130
1,3-Dichlorobenzene ug/L 43.450 87 70-130
1,3-Dichloropropane ug/L 48.250 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3073452LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 43.250 86 70-130
2,2-Dichloropropane ug/L 50.950 102 70-130
2-Butanone (MEK)ug/L 107100 107 70-133
2-Chlorotoluene ug/L 43.950 88 70-130
2-Hexanone ug/L 100100 100 70-130
4-Chlorotoluene ug/L 43.950 88 70-130
4-Methyl-2-pentanone (MIBK)ug/L 99.1100 99 70-130
Acetone ug/L 103100 103 70-144
Benzene ug/L 47.350 95 70-130
Bromobenzene ug/L 43.650 87 70-130
Bromochloromethane ug/L 50.550 101 70-130
Bromodichloromethane ug/L 45.950 92 70-130
Bromoform ug/L 47.5 IK509570-131
Bromomethane ug/L 46.650 93 30-177
Carbon tetrachloride ug/L 46.050 92 70-130
Chlorobenzene ug/L 45.750 91 70-130
Chloroethane ug/L 41.750 83 46-131
Chloroform ug/L 47.850 96 70-130
Chloromethane ug/L 42.350 85 49-130
cis-1,2-Dichloroethene ug/L 47.650 95 70-130
cis-1,3-Dichloropropene ug/L 50.850 102 70-130
Dibromochloromethane ug/L 41.8 IK508470-130
Dibromomethane ug/L 47.950 96 70-130
Dichlorodifluoromethane ug/L 42.250 84 52-134
Diisopropyl ether ug/L 48.350 97 70-131
Ethylbenzene ug/L 45.550 91 70-130
Hexachloro-1,3-butadiene ug/L 38.150 76 70-131
m&p-Xylene ug/L 90.1100 90 70-130
Methyl-tert-butyl ether ug/L 48.850 98 70-130
Methylene Chloride ug/L 46.750 93 68-130
Naphthalene ug/L 42.3 IK508570-133
o-Xylene ug/L 45.950 92 70-130
p-Isopropyltoluene ug/L 45.150 90 70-130
Styrene ug/L 45.550 91 70-130
Tetrachloroethene ug/L 46.150 92 70-130
Toluene ug/L 46.650 93 70-130
trans-1,2-Dichloroethene ug/L 49.750 99 70-130
trans-1,3-Dichloropropene ug/L 43.1 IK508670-130
Trichloroethene ug/L 49.050 98 70-130
Trichlorofluoromethane ug/L 41.950 84 61-130
Vinyl acetate ug/L 117100 117 70-140
Vinyl chloride ug/L 43.350 87 59-142
Xylene (Total)ug/L 136150 91 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3075469MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92506249001
3075470
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 73 70-13579 7 3020ND14.7 15.7
1,1,1-Trichloroethane ug/L 20 83 70-14885 3 3020ND16.6 17.1
1,1,2,2-Tetrachloroethane ug/L M1206770-13177 14 3020ND13.4 15.4
1,1,2-Trichloroethane ug/L 20 74 70-13679 7 3020ND14.8 15.8
1,1-Dichloroethane ug/L 20 82 70-14786 5 3020ND16.3 17.2
1,1-Dichloroethene ug/L 20 86 70-15895 9 3020ND17.3 19.0
1,1-Dichloropropene ug/L 20 84 70-14989 6 3020ND16.8 17.9
1,2,3-Trichlorobenzene ug/L IK,M1206468-14060 6 3020ND12.8 12.0
1,2,3-Trichloropropane ug/L 20 71 67-13775 5 3020ND14.2 15.0
1,2,4-Trichlorobenzene ug/L IK,M1206770-13965 4 3020ND13.4 12.9
1,2-Dibromo-3-
chloropropane ug/L 20 75 69-13692 20 3020ND15.0 18.3
1,2-Dibromoethane (EDB)ug/L 20 70 70-13777 10 3020ND13.9 15.4
1,2-Dichlorobenzene ug/L M1206070-13366 10 3020ND12.0 13.2
1,2-Dichloroethane ug/L 20 76 67-13880 6 3020ND15.1 16.0
1,2-Dichloropropane ug/L 20 79 70-13885 8 3020ND15.8 17.1
1,3-Dichlorobenzene ug/L M1206470-13369 8 3020ND12.7 13.8
1,3-Dichloropropane ug/L 20 71 70-13678 9 3020ND14.2 15.6
1,4-Dichlorobenzene ug/L M1206270-13367 8 3020ND12.4 13.5
2,2-Dichloropropane ug/L 20 86 52-15591 6 3020ND17.2 18.3
2-Butanone (MEK)ug/L 40 83 61-14794 13 3040ND33.2 37.8
2-Chlorotoluene ug/L M1206570-14182 24 3020ND12.9 16.4
2-Hexanone ug/L 40 74 67-13985 14 3040ND29.5 33.9
4-Chlorotoluene ug/L M1206570-13573 12 3020ND12.9 14.6
4-Methyl-2-pentanone
(MIBK)ug/L 40 72 67-13682 12 3040ND28.8 32.6
Acetone ug/L 40 80 55-15992 11 304010.3J 42.1 47.0
Benzene ug/L 20 77 67-15083 8 3020ND15.3 16.6
Bromobenzene ug/L M1206570-13472 11 3020ND12.9 14.4
Bromochloromethane ug/L 20 81 70-14683 2 3020ND16.2 16.5
Bromodichloromethane ug/L 20 73 70-13878 7 3020ND14.6 15.7
Bromoform ug/L IK206157-13868 11 3020ND12.2 13.6
Bromomethane ug/L 20 97 10-20092 5 3020ND19.4 18.4
Carbon tetrachloride ug/L 20 80 70-14787 8 3020ND16.1 17.3
Chlorobenzene ug/L M1206970-13776 9 3020ND13.9 15.2
Chloroethane ug/L 20 86 51-16688 3 3020ND17.1 17.7
Chloroform ug/L 20 78 70-14480 2 3020ND15.6 15.9
Chloromethane ug/L 20 80 24-16183 4 3020ND16.0 16.7
cis-1,2-Dichloroethene ug/L M1206667-14869 2 302013.9 27.1 27.6
cis-1,3-Dichloropropene ug/L 20 73 70-14281 10 3020ND14.7 16.2
Dibromochloromethane ug/L IK207668-13881 7 3020ND15.1 16.2
Dibromomethane ug/L 20 77 70-13483 8 3020ND15.4 16.6
Dichlorodifluoromethane ug/L 20 80 43-15583 4 3020ND16.0 16.6
Diisopropyl ether ug/L 20 67 65-14675 11 3020ND13.4 14.9
Ethylbenzene ug/L 20 71 68-14378 11 3020ND14.1 15.7
Hexachloro-1,3-butadiene ug/L 20 64 62-15167 4 3020ND12.8 13.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3075469MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92506249001
3075470
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 70 53-15776 8 3040ND28.0 30.3
Methyl-tert-butyl ether ug/L 20 69 59-15676 10 3020ND13.8 15.2
Methylene Chloride ug/L 20 79 64-14882 5 3020ND15.7 16.5
Naphthalene ug/L IK206957-15071 3 3020ND13.8 14.2
o-Xylene ug/L 20 68 68-14374 9 3020ND13.7 14.9
p-Isopropyltoluene ug/L 20 71 70-14176 6 3020ND14.2 15.2
Styrene ug/L M1206570-13670 7 3020ND13.1 14.0
Tetrachloroethene ug/L 20 75 70-13981 8 3020ND15.0 16.1
Toluene ug/L 20 74 47-15782 10 30200.37J 15.3 16.8
trans-1,2-Dichloroethene ug/L 20 86 70-14987 2 3020ND17.1 17.5
trans-1,3-Dichloropropene ug/L IK207770-13882 6 3020ND15.3 16.4
Trichloroethene ug/L 20 80 70-14989 11 3020ND16.0 17.8
Trichlorofluoromethane ug/L 20 78 61-15484 8 3020ND15.6 16.8
Vinyl acetate ug/L 40 83 48-15690 8 3040ND33.3 36.2
Vinyl chloride ug/L 20 75 55-17278 2 30203.1 18.2 18.6
Xylene (Total)ug/L 60 69 66-14575 8 3060ND41.6 45.2
1,2-Dichloroethane-d4 (S)%104 70-130102
4-Bromofluorobenzene (S)%101 70-13097
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
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Huntersville, NC 28078
[phone]
Page 19 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92506249
Crayton Printing (AKR-005)
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92506249001 581079MW-4 EPA 8260D
92506249002 581017DUPEPA 8260D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/20/2020 12:12 PM
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Huntersville, NC 28078
[phone]
Page 20 of 23
Page 21 of 23
Page 22 of 23
Page 23 of 23

Appendix C

Groundwater Sampling Forms
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/AKR-005Crayton PrintingCharlotte, NC10/30/20713.0712.732.42KAM12.0Clear, 70s11:4111:4711:5011:5512:0012:052.422.713.303.353.463.580.0 L0.6 L0.9 L1.4 L1.9 L2.4 L100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min1.109.608.700.690.610.5023.223.423.423.523.723.8324.5333.9337.8341.9343.6346.57.187.107.117.117.127.12-108.0-105.1-106.0-108.5-110.7-110.419.6022.2024.9025.5026.1026.40YSI Pro Plus & HACH TurbidityMeterKAM 11/02/20VOCs:(x3)40 mL VOAs w/ HClPeristaltic PVC2-inch12:10Pace AnalyticalMW-1NA2.7312.73PolyethyleneTOC
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/AKR-005Crayton PrintingCharlotte, NC11/2/20712.3217.074.71KAM16.5Clear, 50s10:3010:3510:3810:4510:485.015.355.435.515.590.0 L.5 L1.0 L1.5 L2.0 L100 mL/min100 mL/min100 mL/min100 mL/min100 mL/min8.398.048.618.138.4114.315.214.715.717.13.63.43.63.43.38.929.089.169.279.29149.1174.3176.1174.0174.159.5027.1036.1019.1023.40YSI Pro Plus & HACH TurbidityMeterKAM 11/02/20VOCs:(x3)40 mL VOAs w/ HClPeristaltic PVC2-inch10:50Pace AnalyticalMW-2NA2.0717.07PolyethyleneTOC
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/AKR-005Crayton PrintingCharlotte, NC10/30/20715.9211.591.13KAM11.0Clear, 60s09:2509:3009:3509:4009:5009:5510:0010:1010:1510:201.131.131.171.171.191.191.221.231.231.230.0 L0.75 L1.5 L2.25 L3.75 L4.5 L5.25 L6.75 L7.5 L8.25 L150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min5.214.974.654.644.624.624.534.484.354.3119.219.319.219.119.119.119.119.119.219.2220.2222.6228.1228.6228.9226.0224.3220.2219.46.967.007.017.037.037.027.006.956.926.90-73.3-76.4-79.1-82.6-85.9-86.6-87.8-94.2-96.9-98.989.7088.8071.6067.7043.2044.5038.2030.2024.7023.90YSI Pro Plus & HACH TurbidityMeterKAM 11/02/20VOCs:(x3)40 mL VOAs w/ HClPeristaltic PVC2-inch10:20Pace AnalyticalMW-3NA1.5911.59PolyethyleneTOC218.6
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/AKR-005Crayton PrintingCharlotte, NC11/2/20720.6313.4910.59KAM13.0Clear, 50sDuplicate collected11:1011:1311:1611:2011:2310.7010.7210.7610.8010.830.0 L0.15 L0.3 L0.5 L0.65 L50 mL/min50 mL/min50 mL/min50 mL/min50 mL/min0.850.550.440.380.3520.620.620.820.921.1488.4473.5464.1455.6467.57.447.267.147.077.08-277.2-302.1-299.0-301.0-309.115.2011.008.838.098.28YSI Pro Plus & HACH TurbidityMeterKAM 11/02/20VOCs:(x3)40 mL VOAs w/ HClPeristaltic PVC2-inch11:30Pace AnalyticalMW-4NA3.4913.49PolyethyleneTOC
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater SamplingRecordDate://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/AKR-005Crayton PrintingCharlotte, NC10/30/20717.8318.827.24KAM18.0Clear, 60s13:0013:0513:1513:2013:2513:307.247.688.528.608.818.860.0 L.75 L1.5 L2.25 L3.0 L3.75 L150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min150 mL/min6.246.075.7864.4064.4063.4020.720.820.920.920.920.9339.1345.2350.1351.0353.6353.27.267.046.896.876.856.8051.858.563.264.165.768.383.1085.3083.6067.3065.2041.60YSI Pro Plus & HACH TurbidityMeterKAM 11/02/20VOCs:(x3)40 mL VOAs w/ HClPeristaltic PVC2-inch13:40Pace AnalyticalMW-5NA3.8218.82PolyethyleneTOC