22007_Final Grade Soil Assessment Report_South Tryon Commercial 20200518

Via Email

May 18, 2020

NCDEQ – Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646

Attn: Ms. Sue Murphy, PE

Re: Final Grade Soil Assessment Report
South Tryon Commercial
340 W. Tremont Avenue
Charlotte, North Carolina
Brownfields Project No. 22007-18-060
H&H Project No. RMR-006

Dear Ms. Murphy:

On behalf of RRPV South Tryon Charlotte, LP, enclosed please find a copy of the Final Grade
Soil Assessment Report prepared for the South Tryon Commercial Brownfields property
(Brownfields Project No. 22007-18-060) located in Charlotte, Mecklenburg County.

Should you have any questions or need additional information, please do not hesitate to contact
me at [phone].

Sincerely,

Hart & Hickman, PC
Ralph McGee, PG
Project Manager

Enclosure

cc: Mr. Ashley Saulpaugh, Ram Real Estate Advisors (Via Email)
Ms. Joselyn Harriger, PG, NCDEQ (Via Email)
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Final Grade Soil Assessment Report
South Tryon Commercial
Charlotte, North Carolina
Brownfields Project No. 22007-18-060
H&H Job No. RMR-006

Table of Contents

1.0 Introduction ............................................................................................................................ 1 
2.0 Background Information....................................................................................................... 2 
2.1 Site History ........................................................................................................................... 2 
2.2 Summary of Previous Environmental Assessment Activities .............................................. 2 
3.0 Final Grade Soil Assessment Activities ................................................................................ 6 
3.1 Final Grade Soil Sampling Methodologies .......................................................................... 6 
3.2 Soil Sample Results .............................................................................................................. 8 
3.3 Risk Evaluation..................................................................................................................... 8 
4.0 Summary and Conclusions ................................................................................................. 10 

List of Attachments

Table 1 Summary of Final Grade Soil Sample Analytical Results

Figure 1 Site Location Map
Figure 2 Final Grade Soil Sample Location Map

Appendix A Site Plan
Appendix B Laboratory Analytical Report
Appendix C DEQ Risk Calculator

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Final Grade Soil Assessment Report
South Tryon Commercial
Charlotte, North Carolina
Brownfields Project No. 22007-18-060
H&H Job No. RMR-006

1.0 Introduction

On behalf of RRPV South Tryon Charlotte, LP (Prospective Developer or PD), Hart & Hickman,
PC (H&H) has prepared this Final Grade Soil Assessment Report for the South Tryon Commercial
Brownfields property (Brownfields Project No. 22007-18-060) located northeast of the
intersection of S. Tryon Street and W. Tremont Avenue at 340 W. Tremont Avenue in Charlotte,
Mecklenburg County, North Carolina (Site). The Site consists of one approximately 2.4-acre
parcel of land located in a mixed commercial and residential area of South End Charlotte. The
Site has been redeveloped with two multi-tenant commercial buildings and associated access
roads, parking areas, and open spaces. A Site location map is included as Figure 1, and a Site Plan
prepared by Bohler Engineering NC, PLLC depicting the redevelopment is included as
Appendix A.

A Brownfields Agreement between the North Carolina Department of Environmental Quality
(DEQ) and the PD was recorded on April 26, 2019. Land Use Restriction (LUR) Paragraph 15.c.
generally states that physical redevelopment of the Site will be completed in accordance with a
DEQ-approved Environmental Management Plan (EMP). The EMP for the redevelopment dated
March 26, 2019 received DEQ-approval on March 27, 2019.

Requirements of the EMP include collection of final grade soil samples upon completion of soil
disturbance activities (i.e., following completion of utility installations and final grading). In
accordance with the DEQ-approved EMP, a Final Grade Soil Assessment Work Plan (Work Plan)
and revisions to the Work Plan based on DEQ comments was submitted to the DEQ Brownfields
Program and received approval in a letter dated April 24, 2020. Brief summaries of Site history
and previous assessment activities completed at the Site are provided in the following sections.

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2.0 Background Information
2.1 Site History
The Site remained undeveloped until the late 1930s when the central portion of the Site along S.
Tryon Street was developed with a farm machinery service company that was later used as an
electrical supply warehouse. An addition was constructed on the northern side of the electrical
supply warehouse building in the late 1970s. The electrical supply warehouse operated until the
1990s when the building was occupied by Grinnell Fire Sprinkler Systems. The facility was then
vacant until 2005 when it was leased to a dog daycare business.
A restaurant operated in the southern portion of the Site, south of the electrical supply warehouse
building between 1948 and the mid-1960s. The restaurant building was demolished in the early
1980s. A warehouse building constructed in the southern portion of the Site near W. Tremont
Avenue was occupied by a motor freight company beginning in the 1940s and later by a welding
supply company in the 1960s. By 1980, the original 1940s motor freight company warehouse
building in the southern portion of the Site was demolished and B&B Contracting Co., Inc.
constructed a warehouse building for use as a drywall contracting business until the late 2000s.
The northern portion of the Site remained undeveloped until the late 1960s when it was developed
with a Terminix pest control facility. Terminix operations continued in the northern and
northeastern portions of the Site until the late 2000s. The Site buildings were razed in 2011 and
the Site remained vacant until recent construction of the new commercial office campus.
2.2 Summary of Previous Environmental Assessment Activities
According to information provided in a Phase I Environmental Site Assessment (ESA) completed
by H&H on May 31, 2019, the following potential environmental concerns associated with
historical Site operations and nearby off-Site operations were identified in connection with the
Site:
The former Virginia Carolina Chemical Company facility was located on the adjacent property
to the south across W. Tremont Avenue and topographically cross-gradient to upgradient of
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the Site. The Virginia Chemical Company formerly operated as a phosphate fertilizer plant
from at least the 1890s until the 1960s. Results of assessment activities conducted on the
former Virginia Carolina Chemical Company property have identified the presence of lead,
arsenic, tetrachloroethene (PCE), and trichloroethene (TCE) in groundwater at concentrations
above the DEQ 2L Groundwater Standards (2L Standards).

The former Parks Cramer facility (a.k.a. Atherton Mill Property) is located approximately
1,100 ft east-southeast and topographically upgradient of the Site. Parks Cramer manufactured
textile-related equipment. Soil and groundwater impacts consisting of chlorinated solvent and
petroleum-related compounds associated with former Parks Cramer operations are well
documented. Groundwater impacts extend downgradient of the Parks Cramer property and
have been identified within approximately 400 ft of the Site. Plume migration modeling
prepared by the consultant for Parks Cramer indicated that the plume is expected to travel
toward the Site.

In July 2007, H&H conducted soil and groundwater sampling activities at the Site on behalf
of a previous prospective purchaser. Results of groundwater assessment activities identified
low levels of PCE and TCE at concentrations above 2L Standards in monitoring wells installed
in western and southwestern portions of the Site. Groundwater impacts identified at the Site
that are attributable to historical nearby off-Site operations were identified as an environmental
concern in connection with the Site.

 The northern portion of the Site and portions of the property located on the eastern adjacent
West Tremont Brownfields property were previously occupied by Terminix and B&B
Contracting Company. Results of previous assessment activities conducted at the Site and
West Tremont Brownfields property in the mid and late 2000s identified pesticide compounds
at concentrations exceeding DEQ screening criteria in soil and groundwater samples.
Excavation activities to remediate elevated levels of pesticides in soils were conducted on the
east adjacent property in the early 2010s. Approximately 8,500 tons of non-hazardous
pesticide-impacted soil and approximately 560 tons of hazardous pesticide-impacted soil were
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removed and transported for disposal at a permitted facility. Post-excavation confirmation soil
sample results indicate that no pesticide compounds were detected at concentrations exceeding
the DEQ Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals
(PSRGs). The potential for pesticide impacts to persist at the Site was identified as a potential
environmental concern.

To address environmental concerns, the PD elected to enter the Site into the DEQ Brownfields
Program and received a letter of eligibility on February 18, 2018. H&H subsequently completed
Brownfields soil and soil gas assessment activities at the Site in May 2018 to further evaluate the
potential for impact and to assist in management of Site media during the planned commercial
redevelopment. The May 2018 assessment activities are documented in a Brownfields Assessment
Report prepared by H&H dated July 9, 2018.

May 2018 Brownfields soil sample laboratory analytical results did not identify organic
compounds at concentrations above the DEQ IHSB Industrial/Commercial PSRGs. Metals
concentrations were detected in the soil samples at concentrations consistent with naturally
occurring levels. Based on soil assessment results, cumulative risk calculations using the DEQ
Risk Calculator indicated that compound concentrations detected in soil samples collected at the
Site would not pose unacceptable carcinogenic or noncarcinogenic risks to construction workers
or future non-residential workers.

Brownfields soil gas samples were collected within the footprints of the proposed commercial
buildings in May 2018 to evaluate the potential for structural vapor intrusion. Soil gas sample
laboratory analytical results did not identify compounds at concentrations above the DEQ Division
of Waste Management (DWM) Non-Residential Vapor Intrusion Sub-slab and Exterior Soil Gas
Screening Levels (SGSLs). Results of cumulative risk calculations indicated that there is not a
significant vapor intrusion risk at unacceptable levels into either commercial building.

Based on results of the 2007 groundwater assessment activities and May 2018 soil gas assessment
activities, DEQ Brownfields requested supplemental vapor intrusion assessment activities within
the footprints of the proposed commercial buildings to further evaluate the potential for structural
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vapor intrusion and confirm that there are no vadose zone soil impacts at the Site that would
contribute to potential vapor intrusion upon completion of proposed redevelopment activities.
H&H completed vertical soil gas profile assessment activities at the Site in April 2019. The
supplemental soil gas assessment activities are documented in a Vertical Soil Gas Profile
Assessment Report prepared by H&H dated May 15, 2019.

Results of the vertical soil gas profile assessment activities confirmed that no compounds were
detected at concentrations above the DEQ DWM Non-Residential Vapor Intrusion SGSLs in
shallow or deeper soil gas samples collected at the Site. In addition, compound concentrations in
shallow soil gas samples were lower than compound concentrations in deeper soil gas samples
indicating that there was no significant soil source that would contribute to potential vapor
intrusion. Consistent with previous soil gas assessment results, results of the vertical soil gas
profile assessment activities and hypothetical worst-case scenario risk calculations confirmed there
is no significant risk for structural vapor intrusion into the proposed commercial buildings.

Grading activities and construction of the new commercial buildings have been completed in
accordance with the DEQ-approved EMP. Contractors have installed asphalt-paved access drives
and parking areas, concrete sidewalks and handicap access ramps, and tightly spaced pavers in
select open areas. H&H completed final grade soil assessment activities at the Site to evaluate the
potential for impacts in shallow soil that is not covered impervious materials. A summary of the
final grade soil sampling activities is provided in the following sections.
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3.0 Final Grade Soil Assessment Activities

Final grade soil sampling activities were completed at the Site to evaluate the potential for impacts
in landscape area shallow soil that may pose unacceptable exposure risks to future non-residential
occupants. The soil sampling activities were performed in general accordance with the DEQ IHSB
Guidelines for Assessment and Cleanup of Contaminated Sites (Guidelines) dated January 2020,
the DEQ-approved Work Plan, and the most recent versions of the U.S. Environmental Protection
Agency (EPA) Region IV Science and Ecosystem Support Division (SESD) Field Branches
Quality System and Technical Procedures guidance.

3.1 Final Grade Soil Sampling Methodologies

Based on review of the Site Plan (Appendix A), conversations with the general contractor, and
observations at the Site, the Site is predominately covered with hardscape surfaces with the
exception of landscaped and/or grassed areas surrounding the Site buildings and islands within the
parking areas. Landscaped and/or grassy areas are shown as green shading in Figure 2.

To evaluate for the potential presence of impacts in unpaved areas at the Site, landscaped areas
were divided into four final grade evaluation areas (FG-1 through FG-4) and a representative final
grade soil sample was collected from each area. The four final grade evaluation areas are shown
on Figure 2 and are described below:
 Final grade evaluation area FG-1 includes landscaped areas located near the northern Site
boundary along Doggett Street;
 Final grade evaluation area FG-2 includes landscaped areas located in the eastern portion
of the Site south of Building C;
 Final grade evaluation area FG-3 includes landscaped areas located in the southwestern
portion of the Site and along S. Tryon Street; and
 Final grade evaluation area FG-4 includes landscaped areas located in the southeastern
portion of the Site near W. Tremont Avenue.

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To collect representative soil samples, five aliquot soil borings were advanced within each final
grade evaluation area (Figure 2). Each aliquot soil boring was advanced to approximately 2 feet
below the ground surface utilizing a decontaminated stainless-steel hand auger. Continuous soil
samples were collected from the center of the hand auger bucket at each boring and observed for
lithologic description, the presence of obvious staining or unusual odors, and field screened for
volatile organic vapors using a calibrated photo-ionization detector (PID). Field personnel did not
observe the presence of staining or odors in the aliquot soil samples and field screening did not
indicate obvious evidence of impact. Soil lithology at the aliquot locations generally consisted of
dry to moist clayey silt.

Following boring advancement, one representative grab soil sample was collected from an
undisturbed portion of an aliquot soil sample in each final grade evaluation area. The remaining
soil sample aliquots from each area were combined and homogenized to form one composite soil
sample representative of that evaluation area for a total of four (4) composite soil samples (FG-1
through FG-4). Soil samples selected for laboratory analysis from each evaluation area were
collected directly into dedicated laboratory supplied sample containers, labeled with the sample
identification, date, time, and requested analysis and placed in a laboratory supplied cooler with
ice. The samples were then delivered to Pace Analytical (Pace) under standard chain of custody
protocols for analysis. The composite soil samples were submitted to Pace for analysis of semi-
volatile organic compounds (SVOCs) by EPA Method 8270, Resource Conservation and Recovery
Act (RCRA) metals plus hexavalent chromium by EPA Methods 6020/7471/7196, and pesticides
by EPA Method 8081. The grab soil samples were submitted to Pace for analysis of VOCs by
EPA Method 8260.

For quality assurance and quality control purposes (QA/QC), H&H collected a duplicate composite
and grab sample (FG-DUP-1) from final grade evaluation area FG-2. The duplicate soil sample
was submitted for the same analyses as the parent samples as described above.

Following sampling activities, the soil borings were properly abandoned and the surfaces were
repaired similar to pre-drilling conditions. Additionally, the soil boring locations were estimated
using a hand-held global positioning system (GPS) unit.
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3.2 Soil Sample Results

A tabular summary of final grade soil sample laboratory analytical results is presented in Table 1,
and a copy of the laboratory analytical report and chain of custody record is provided in Appendix
B. The laboratory analytical results were compared to the DEQ IHSB Industrial/Commercial
PSRGs dated February 2018. In addition to the PSRGs, metals results were compared to Site-
specific and published concentrations for naturally occurring metals in soil.

Laboratory analytical results indicate that trace levels of acetone (up to 0.014 J milligrams per
kilogram [mg/kg]), ethylbenzene 0.0019 J mg/kg), xylenes (0.0049 J mg/kg), aldrin (0.0314 J
mg/kg), chlordane (up to 0.364 mg/kg), and dieldrin (up to 0.414 mg/kg) were detected in at least
one final grade soil sample at concentrations above the laboratory method detection limits. The
dieldrin concentration detected in the FG-1 soil sample (0.414 mg/kg) is slightly above the DEQ
IHSB Industrial/Commercial PSRG of 0.14 mg/kg. No other organic compounds were detected
at concentrations above the laboratory method detection limits in final grade soil samples collected
at the Site.

As expected, several metals were detected at concentrations above laboratory method detection
limits in the final grade samples collected at the Site. Metals concentrations detected in the soil
samples are consistent with naturally occurring levels for the Site area.

3.3 Risk Evaluation

The DEQ IHSB health-based PSRGs are very conservative and based on the lower of a Target
Carcinogenic Risk (TCR) of 1 x 10-6 for potential carcinogenic risks and a Target Hazard Quotient
(THQ) of 0.2 for potential noncarcinogenic risks. The DEQ and EPA acceptable risks for potential
carcinogenic risks is cumulative lifetime incremental carcinogenic risk (LICR) of 1 x 10-4 and a
cumulative hazard index (HI) of 1 for noncarcinogenic risks. Therefore, H&H utilized the DEQ
Risk Calculator (December 2019) to further evaluate cumulative risks to future non-residential
workers based the final grade soil sample analytical results.

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The highest concentration of each compound detected in any final grade soil sample was used to
model a hypothetical worst-case exposure risk under a non-residential use scenario. The risk
calculator results indicate that the cumulative LICR is 4.2 x 10-6 and the cumulative HI is 0.002. The
results of the risk calculations indicate that the calculated cumulative carcinogenic and
noncarcinogenic risks are orders of magnitude below the DEQ and EPA acceptable levels for non-
residential use. A copy of the completed DEQ Risk Calculator is provided as Appendix C.

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4.0 Summary and Conclusions

Redevelopment activities have been completed at the South Tryon Commercial Brownfields
property located northeast of the intersection of S. Tryon Street and W. Tremont Avenue at 340
W. Tremont Avenue in Charlotte, North Carolina. Redevelopment activities included mass
grading and construction of two multi-tenant commercial buildings with associated access drives,
parking areas, and common areas. H&H has completed final grade soil sampling activities at the
Site in accordance with the DEQ Brownfields approved Work Plan dated April 23, 2020. Final
grade soil sampling activities included the collection of soil samples to evaluate the potential for
impacts in areas at the Site that were not covered by building foundations, sidewalks, or asphaltic
or concrete parking areas and driveways following redevelopment.

Laboratory analytical results indicate that a trace level of dieldrin was detected in sample FG-1 at
a concentration slightly above the DEQ IHSB Industrial/Commercial PSRG. No other compounds
were detected at concentrations above the DEQ IHSB Industrial/Commercial PSRGs or naturally
occurring levels in the case of metals.

H&H utilized the DEQ Risk Calculator to further evaluate cumulative risks to future non-
residential workers based on the final grade soil sample analytical results. The results of
hypothetical worst-case risk calculations indicate that cumulative carcinogenic and
noncarcinogenic risks are orders of magnitude below the DEQ and EPA acceptable levels under a
non-residential use scenario.

The Site has been redeveloped for its intended use in accordance with the DEQ-approved EMP.

Table 1Summary of Final Grade Soil Sample Analytical ResultsSouth Tryon Commercial Charlotte, North CarolinaBrownfields Project No. 22007-18-060H&H Job No. RMR-006Evaluation Area North West SoutheastSample IDFG-1 FG-2 FG-DUP-1 FG-3 FG-4 BKG-01 BKG-02Date4/28/2020 4/28/2020 4/28/2020Depth (ft bgs)0-2 0-2 0-2 0.5-1.5 0.5-1.5 Range Mean Range MeanUnitsVOCs (8260D)Acetone<0.00950.0113 J<0.00960.0140 J<0.0093 -- --140,000-- -- -- --Ethylbenzene<0.0011 <0.0011 <0.00110.0019 J<0.0010 -- --27-- -- -- --Xylenes (Total)<0.0035 <0.0037 <0.00350.0049 J<0.0035 -- --530-- -- -- --SVOCs (8270E)All BDL All BDL All BDL All BDL All BDL -- -- -- -- -- -- --Pesticides (8081B)Aldrin0.0314 J<0.0020 <0.0024 <0.0089 <0.0019 -- --0.18-- -- -- --Chlordane0.364<0.019 <0.02280.132<0.0188 -- --7.7-- -- -- --Dieldrin0.414<0.0022 <0.00260.0205 J<0.0022 -- --0.14-- -- -- --Metals (6020B/7471B/7199)Arsenic2.78 2.29 1.71 3.14 1.87 0.28 2.60 3 0.28 - 2.6 1.43 1.0 - 18 4.8Barium40.7 66.9 47.8 73.1 74.9 63.0 100 47,000 63 - 100 81.5 50 - 1,000 356Cadmium<0.513 <0.562 <0.597 <0.567 <0.561 <0.0130.120 J 110 <0.013 - 0.12 0.07 1.0 - 10 4.3Chromium (total)26.3 41.4 74.9 38.3 30.3 3.1 J 34.0 NS 3.1 - 34 18.6 7.0 - 300 65Hexavalent Chromium0.340 J 0.447 J<0.3750.377 J<0.353 <0.24 DL-030.63 J, DL-03 6.5 <0.24- 0.63 0.44 NS NSTrivalent Chromium26.0 41.0 74.9 37.9 30.3 0.70 33.37 350,000 0.7-33 26.9 NS NSLead47.1 41.0 13.7 28.1 24.3 5.70 28.0 800 5.7 - 28 16.9 ND - 50 16Mercury0.0464 J 0.0391 J 0.0369 J 0.0278 J 0.0350 J 0.009 J 0.033 9.7 0.009 - 0.033 0.021 0.03 - 0.52 0.121Selenium<1.28 <1.40 <1.49 <1.41 <1.40 <0.056 <0.0511,200ALL BDL --<0.1 - 0.8 0.42Silver<0.269 <0.295 <0.313 <0.298 <0.2950.061 J 0.070 J 1,200 0.061 - 0.070 0.066 ND - 5.0 NSNotes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (February 2018). 2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conteminous US soils. Aside from metals, only those compounds detected in at least one sample are shown in the table above. Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses. Bold value indicates an exceedance of the Industrial/Commercial PSRG. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; FG = Final Gradeft bgs= feet below ground surface; NS = not specified; -- = not applicable; ND = not detected; BDL = below laboratory method detection limitsJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. DL-03 = Elevated reporting limit due to matrixmg/kg0-24/28/2020EastBackground5/17/2018Industrial/ Commercial PSRGs (1)Regional Background Metals in Soils (2)Screening CriteriaSite-Specific Background Metals in SoilS:\AAA‐Master Projects\Ram Realty ‐ RMR\RMR‐006 Tryon & Tremont Brownfields Assistance\Final Grade Soil Sampling\Assessment Report\Tables\Data Table_rev1.xlsx5/15/2020Table 1 Hart & Hickman, PC
TITLE
PROJECT
SITE LOCATION MAP
SOUTH TRYON COMMERICAL
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
3-20-20 0
1RMR-006
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NORTH CAROLINA, 1991
REVISION NO. 0
JOB NO. RMR-006
DATE: 5-15-20
FIGURE NO. 2
SOUTH TRYON COMMERCIAL
CHARLOTTE, NORTH CAROLINA
FINAL GRADE SOIL SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
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NOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG COUNTY
GIS (2017).
2.FINAL GRADE SOIL SAMPLES COLLECTED BY H&H ON
4/28/20.
BUILDING C
BUILDING A/B
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
FINAL GRADE EVALUATION AREA
FINAL GRADE AREA IDENTIFICATION
BUILDING FOOTPRINT
HARDSCAPED SURFACE
LANDSCAPED SURFACE
SOIL SAMPLE ALIQUOT LOCATION
APPROXIMATE LOCATION OF FORMER
ORPHAN UST
FG-1
FG-4
FG-2
FG-3
FG-1
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Appendix A
Site Plan
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PROP. 16' SETBACK FROM EX. B.O.C.LOADI
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T
B
A
C
K

F
R
O
M

F
U
T
U
R
E
B.
O
.
C
.
P
E
R

R
E
Z
O
N
I
N
G

P
L
A
N

2
0
0
7
-
1
2
4 16'PROP. 16' SETBACK FROM EX. B.
O
.
C
.
17
'24'17'24'9'
8'
9'
17
'9'17'8'8'
9'6.3'10'10
'25'9'9'
9'
1
6
'
8.
5
'8.5'8.5'8.5' PROP. PLANTING STRIP8.3'10'9'3.5'9'
7.
7
'
5'
5.
4
'9.8'18.5'18.5'24
'17'8'
8'8'8'5'
8'
WIDT
H V
ARI
ES 8' PROP. SW5.3'6'OHOHOHOHOHOHOHOHOHOHT
17'1.
5
'
BUILDING A/B
17,375 SF GROSS
(1 STORY)
FFE1= 731.63
BUILDING C
14,605 SF GROSS /FLOOR
(3 STORY)
FFE = 730.4
FFE2 = 734.30
PROP. PATIO
± 1,000 SF
PROP. PARKING
STRIPING
PROP. PARKING
STRIPING (TYP)
PROP. PARKING
STRIPING (TYP)PROP. 45°
PAVEMENT
MARKINGS (TYP.)
LIMITS OF NEW CURB
LIMITS OF NEW CURB
PROP. 30" C&G
CONTRACTOR TO SAWCUT
EDGE OF EX. PAVEMENT
FOR SMOOTH TRANSITION
LIMITS OF
NEW CURB
LIMITS OF NEW CURB
LIMITS OF NEW CURB
LIMITS OF NEW CURB
PROP. BOLLARD
MOUNTED ACCESSIBLE
PARKING SIGN (TYP.)
PROP. STOP SIGN &
STOP BAR (TYP.)
PROP. BOLLARD
MOUNTED ACCESSIBLE
PARKING SIGN (TYP.)
PROP. BOLLARD
MOUNTED ACCESSIBLE
PARKING SIGN (TYP.)
PROP. INVERTED
U BIKE RACK (2).
REFER TO DETAIL
PROP. CURB TO MATCH EX. AT
DRIVEWAY LOCATION (TYP.)
PROP. INVERTED
U BIKE RACK (2).
REFER TO DETAIL
LIMITS OF
NEW CURB
PROP. SAWCUT
LINE (TYP.)
PROP. SAWCUT LINE (TYP.)
PROP. SAWCUT
LINE (TYP.)
PROP. SAWCUT
LINE (TYP.)
PROP.
RETAINING WALL
W/ SAFETY RAIL
PROP. 9' CURB
TRANSITION TO FLUSH
PROP. 9' CURB
TRANSITION TO FLUSH
PROP. INVERTED
U BIKE RACK (2).
REFER TO DETAIL
PROP. STEPS
PROP. ADA
RAMP (TYP.)
PROP. FIRST FLOOR
COVERED PATIO.
REF. ARCH.
PROP. FUTURE BACK
OF CURB LINE PER
REZONING PLAN
PROP. 8' SW
EASEMENT
PROP. INVERTED
U BIKE RACK (2).
REFER TO DETAIL
REFER TO NCDOT
TRAFFIC CONTROL
PLANS FOR WORK
IN NCDOT ROW
PROP CURB RAMP
PER CLDSM 10.40A
(TYP.)
PROP. BUILDING MOUNTED
FDC TO CONNECT
INTERNALLY TO RISER ROOM
PROP. BUILDING
MOUNTED FDC TO
CONNECT INTERNALLY
TO RISER ROOM
REF. HARDSCAPE
SHEETS FOR
PLAZA DETAILS
PROP. ADA RAMP
REF. DETAIL
PROP. HANDRAIL AT
STAIRS (TYP.)
REF. ARCH. FOR DETAIL
PROP. ADA RAMP
REF. DETAIL
PROP.
RETAINING WALL
W/ SAFETY RAIL
PROP. 3'X2' RIVER
STONE PAD
ENCROACHMENT
AGREEMENT IS NEEDED
PRIOR TO INSTALLATION
OF HARDSCAPE FEATURES
8.8'10.1'6'50' X 50' SIGHT
DISTANCE TRIANGLE
50' X 50' SIGHT
DISTANCE TRIANGLE
10'X10' CITY OF
CHARLOTTE
PEDESTRIAN
SIGHT TRIANGLE
10'X10' CITY OF
CHARLOTTE
PEDESTRIAN
SIGHT TRIANGLE
OBJ
SSSSLODLODLODLODLODLODLODLODLODLODLODPROP. 3 CY
RECYCLE (X6)
PROP. MARATHON
RJ-250SC 34 CY
TRASH COMPACTOR
PROP. 8 CY
RECYCLE
3'
PROP.
MASONRY WALL
(BY OTHERS)
PROP. POWER
ASSSEMBLY2.5'1'PROP.
MASONRY WALL
(BY OTHERS)
TRANSITION TO
FLUSH CURB
TRANSITION TO
FLUSH CURB
PROP. HD CONC.
PROP. HD
CONC.3'
4" STEEL BOLLARDS
PAINTED YELLOW (X5)
4" STEEL BOLLARDS
PAINTED YELLOW (X3)
2'2'
2'
7
3
0
726
727
728729
G 731.05
TC 726.15
G 725.5+/-
MATCH EX.
G 727.09
G 730.53
G 726.5+/-
MATCH EX.
BW 727.07
BW 726.64
BW 726.85
BW 726.64
BW 725.95BW 725.91
BW 726.54
BW 726.58
G 727.02
G 727.02
726
G 730.44
G 730.07
G 729.98
G 725.75
G 725.67
G 726.25
TC 727.00
TC 725.57+/-
MATCH EX.
REVISIONS
REV DATE COMMENT BY
LOCATION OF SITE
FOR
PROJECT No.:
DRAWN BY:
CHECKED BY:
DATE:
SCALE:
CAD I.D.:
SHEET NUMBER:
SHEET TITLE:
PROJECT:
H:\2017\NCC172144\DRAWINGS\PLAN SETS\CONSTRUCTION DOCUMENTS\NCC172144SS0.DWG PRINTED BY: DRENCKENS 7.15.19 @ 2:09 PM LAST SAVED BY: DRENCKENS
NCC172144
DR/RB
DR
04/01/2019
CONSTRUCTION
DOCUMENTS
335 TREMONT
MIXED USE
BUILDING A/B: 340 W TREMONT AVE.
BUILDING C: 330 W TREMONT AVE.
PID: 121-033-02
1 06/21/2019 DRREVISION 2: CYCLE 2
2 07/15/2019 DRDUMPSTER
RECONFIGURATION
KNOW WHAT'S BELOW
ALWAYS CALL 811
BEFORE YOU DIG
It's fast. It's free. It's the law.
TM
1927 S. TRYON STREET, SUITE 310
CHARLOTTE, NC 28203
Phone:[phone]
Fax:[phone]
[e-mail]
NCBELS P-1132TM THE INFORMATION, DESIGN AND CONTENT OF THIS PLAN ARE PROPRIETARY AND SHALL NOT BE COPIED OR USED FOR ANY PURPOSE WITHOUT PRIOR WRITTEN AUTHORIZATIONFROM BOHLER ENGINEERING. ONLY APPROVED, SIGNED AND SEALED PLANS SHALL BE UTILIZED FOR CONSTRUCTION PURPOSES©NEW ENGLANDUPSTATE NEW YORKNEW YORK, NYPHILADELPHIA, PALEHIGH VALLEY, PABALTIMORE, MDREHOBOTH BEACH, DEWASHINGTON, DCNORTHERN VIRGINIARALEIGH, NCCENTRAL VIRGINIASOUTHERN MARYLANDNORTHERN NEW JERSEYSOUTHEASTERN, PACHARLOTTE, NCBOSTON, MASOUTHERN NEW JERSEYNEW YORK METROTAMPA, FLSOUTH FLORIDADALLAS, TXATLANTA, GAPITTSBURGH, PATMSUSTAINABLE DESIGNLANDSCAPE ARCHITECTURESITE CIVIL AND CONSULTING ENGINEERINGLAND SURVEYINGPROGRAM MANAGEMENTPERMITTING SERVICESTRANSPORTATION SERVICES2017 BOHLER ENGINEERINGSEAL
ENGI NE E RPROFESSIO
N
ALNO R T H CAROLI
NA048031
DANI
E
L J . R E N C K ENS07/15/2019
1"=20'
0 2051020
5.ZONING ORDINANCE PROVISIONS
REQUIRED PROPOSED
A.)SETBACKS/BUFFERS/STRIP:BUILDING BUFFER BUILDING BUFFER
FRONT (TRYON) -16 FT FROM BOC N/A 16 FT N/A
SIDE (W TREMONT) - 16 FT (SEE N/A 16 FT N/A
APPROVED
REZONING DOCUMENTS)
REQUIRED/ALLOWED PROPOSED
B.)MAXIMUM BUILDING HEIGHT:
40 FT W/ INCREASED 1' PER 10' SETBACK
C.)PARKING REQUIRED: 70 SPACES15,000 GROSS SF OF EATING, DRINKING, AND +30 SPACES SHARED BETWEEN
ENTERTAINMENT ESTABLISHMENT ADJACENT MULTIFAMILY (EXTRA SPACES AVAILABLE)
1 SPACE / 150 S.F. * 15,000 SF = 100 SPACES TOTAL: 100 SPACES
29,210 GROSS SF OF OFFICE SPACE 0 SPACES
MAX 1 SPACE / 300 SF, MINIMUM = 0
ADJACENT SITE PARKING INFORMATION:
164 UNITS 268 SPACES
MINIMUM = 0, MAXIMUM = 1.6/UNIT = 263 SURFACE PARK = 80 SPACES, GARAGE = 188 SPACES
D.)BIKE PARKING REQUIRED:
LONG TERM: 1/10,000 SF, MIN OF 2 4 SPACES (LOCATED IN THREE30FIVE PARKING DECK)
31250/10,000 = 4 SPACESSHORT TERM: 5% OF AUTO PARKING 12 SPACES (LOCATED IN THREE30FIVE PARKING DECK)
209 SPACES X 5% = 11 SPACES
HANDICAP PARKING REQUIRED: HANDICAP - 76-100 SPACES 4 TOTAL SPACES 5 SPACES
VAN ACCESSIBLE 1 SPACE 2 SPACES

STANDARD DIMENSION 8.5 FT x 18.5 FT 24 SPACESSTANDARD DIMENSION 9.0 FT x 17.0 FT 40 SPACES
ACCESSIBLE DIMENSION 8.0 FT x 17.0 FT 6 SPACES
SHARED PARKING VARIES 30 SPACES
E.)OPEN SPACE: :
PUBLIC OPEN SPACE= 1SF/100 GFA OR 104,238 GFA / 100 SF = 1043 SF
1SF/200 SF LOT AREA, WHICHEVER IS GREATER 3,076 SF PROVIDED
6.FLOOR AREA (F.A.R.) REQUIREMENT BUILDING A:8,168 S.F.0.50 MINIMUM BUILDING B: 8,514 S.F.
BUILDING C:43,698 S.F.
TOTAL SITE AREA:104,238 S.F
TOTAL F.A.R.:±0.58
GENERAL NOTES
1. DEVELOPER/APPLICANT:
RAM REALTY ADVISORS
CONTACT: ASHLEY SAULPAUGHEMAIL:[e-mail]
PHONE:[phone]
2. THIS PLAN IS BASED UPON THE FOLLOWING:
THE JOHN R. MCADAMS COMPANY, INC.
"2001 SOUTH TRYON"
PROJECT #: SURS-16203
DATED:04/15/2016
3. EX. SITE INFORMATION
OWNER:2001 SOUTH TRYON LLC
ADDRESS:2035 SOUTH TRYON STREET
CHARLOTTE, NC 28203
PARCEL NUMBER:121103302 AND 12103301
D.B. 27409 P.N. 714
GROSS AREA: ±2.39 ACRES
ZONING: TOD-M
4.EXISTING USE:
VACANT
PROPOSED USE:
MIXED USE
PERMITTED LAND USE:
YES
1" = 20'
SS0
C-302
SITE PLAN
1.NON-STANDARD ITEMS(IE: PAVERS,IRRIGATION
SYSTEMS,ETC.) IN THE RIGHT-OF-WAY REQUIRE A
RIGHT-OF-WAY ENCROACHMENT AGREEMENT WITH THE
CHARLOTTE DEPARTMENT OF TRANSPORTATION/ NORTH
CAROLINA DEPARTMENT OF TRANSPORTATION BEFORE
INSTALLATION. FOR CITY OF CHARLOTTE MAINTAINED
STREETS, CONTACT CDOT AT [phone].
2.ANY WORK WITHIN THE CITY'S R/W THAT REQUIRES
CLOSURE OF A SIDEWALK OR TRAVEL LANE MUST BE
APPROVED BY CDOT AND WILL REQUIRE A R/W USE PERMIT
OR R/W LEASE DEPENDING UPON THE PROPOSED
DURATION OF CLOSURE. THESE APPROVALS ARE IN
ADDITION TO SITE APPROVALS AND SHOULD BE
COORDINATED WITH CDOT PRIOR TO CONSTRUCTION.
CONTRACTOR SHALL CONTACT CDOT AT [phone] AT
LEAST 5 BUSINESS DAYS PRIOR TO BEGINNING WORK FOR
IMPACTS LESS THAT 30 DAYS. CONTRACTOR SHALL
CONTACT CDOT AT [phone] AS SOON AS POSSIBLE
FOR IMPACTS GREATER THEN 30 DAYS. EVERY EFFORT
SHALL BE MADE TO CONSTRUCT IMPROVEMENTS WITH
MINIMAL IMPACT TO DRIVERS AND PEDESTRIANS.
CITY OF CHARLOTTE NOTES:
SEE INSET A
INSET A1"=10'
0 105

Appendix B
Laboratory Analytical Report
#=CL#
May 07, 2020
LIMS USE: FR - RALPH MCGEE
LIMS OBJECT ID: 92475481
92475481
Project:
Pace Project No.:
RE:
Ralph McGee
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
RMR-006
Dear Ralph McGee:
Enclosed are the analytical results for sample(s) received by the laboratory on April 29, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 65
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92475481
RMR-006
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 65
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92475481
RMR-006
Lab ID Sample ID Matrix Date Collected Date Received
92475481001 FG-1 (0-2)Solid 04/28/20 12:05 04/29/20 13:13
92475481002 FG-2 (0-2)Solid 04/28/20 11:00 04/29/20 13:13
92475481003 FG-3 (0-2)Solid 04/28/20 10:00 04/29/20 13:13
92475481004 FG-4 (0-2)Solid 04/28/20 08:55 04/29/20 13:13
92475481005 FG-DUP-1 Solid 04/28/20 00:00 04/29/20 13:13
92475481006 FG-TRIP BLANK Water 04/28/20 00:00 04/29/20 13:13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 65
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92475481
RMR-006
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92475481001 FG-1 (0-2)EPA 8081B 24 PASI-CBAJ
EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92475481002 FG-2 (0-2)EPA 8081B 24 PASI-CBAJ
EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92475481003 FG-3 (0-2)EPA 8081B 24 PASI-CBAJ
EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92475481004 FG-4 (0-2)EPA 8081B 24 PASI-CBAJ
EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92475481005 FG-DUP-1 EPA 8081B 24 PASI-CBAJ
EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 65
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92475481
RMR-006
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANGB
92475481006 FG-TRIP BLANK EPA 8260D 70 PASI-CCL
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-1 (0-2)Lab ID:92475481001 Collected:04/28/20 12:05 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8081 GCS Pesticides
Aldrin 31.4J ug/kg 05/06/20 11:52 309-00-204/29/20 18:4963.0 22.8 25
alpha-BHC ND ug/kg 05/06/20 11:52 319-84-604/29/20 18:4963.0 21.9 25
beta-BHC ND ug/kg 05/06/20 11:52 319-85-704/29/20 18:4963.0 22.7 25
delta-BHC ND ug/kg 05/06/20 11:52 319-86-804/29/20 18:4963.0 22.4 25
gamma-BHC (Lindane)ND ug/kg 05/06/20 11:52 58-89-904/29/20 18:4963.0 25.9 25
Chlordane (Technical)364 ug/kg 05/06/20 11:52 57-74-904/29/20 18:4922022025
4,4'-DDD ND ug/kg 05/06/20 11:52 72-54-804/29/20 18:4963.0 26.2 25
4,4'-DDE ND ug/kg 05/06/20 11:52 72-55-904/29/20 18:4963.0 24.8 25
4,4'-DDT ND ug/kg 05/06/20 11:52 50-29-304/29/20 18:4963.0 22.8 25
Dieldrin 414 ug/kg 05/06/20 11:52 60-57-104/29/20 18:4963.0 25.6 25
Endosulfan I ND ug/kg 05/06/20 11:52 959-98-804/29/20 18:4963.0 25.3 25
Endosulfan II ND ug/kg 05/06/20 11:52 33213-65-904/29/20 18:4963.0 25.3 25
Endosulfan sulfate ND ug/kg 05/06/20 11:52 1031-07-804/29/20 18:4963.0 27.4 25
Endrin ND ug/kg 05/06/20 11:52 72-20-804/29/20 18:4963.0 26.4 25
Endrin aldehyde ND ug/kg 05/06/20 11:52 7421-93-404/29/20 18:4963.0 24.6 25
Endrin ketone ND ug/kg 05/06/20 11:52 53494-70-504/29/20 18:4963.0 33.1 25
Heptachlor ND ug/kg 05/06/20 11:52 76-44-804/29/20 18:4963.0 20.8 25
Heptachlor epoxide ND ug/kg 05/06/20 11:52 1024-57-304/29/20 18:4963.0 21.0 25
Hexachlorobenzene ND ug/kg 05/06/20 11:52 118-74-104/29/20 18:4963.0 20.7 25
Methoxychlor ND ug/kg 05/06/20 11:52 72-43-504/29/20 18:4915782.5 25
Mirex ND ug/kg 05/06/20 11:52 2385-85-504/29/20 18:4915776.5 25
Toxaphene ND ug/kg 05/06/20 11:52 8001-35-204/29/20 18:4922022025
Surrogates
Tetrachloro-m-xylene (S)0 %05/06/20 11:52 877-09-8 S404/29/20 18:4915-130 25
Decachlorobiphenyl (S)0 %05/06/20 11:52 2051-24-3 S404/29/20 18:4910-130 25
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.78 mg/kg 05/02/20 14:43 7440-38-205/02/20 06:481.26 0.533 5
Barium 40.7 mg/kg 05/02/20 14:43 7440-39-3 MH05/02/20 06:483.16 1.58 5
Cadmium ND mg/kg 05/02/20 14:43 7440-43-905/02/20 06:481.26 0.513 5
Chromium 26.3 mg/kg 05/02/20 14:43 7440-47-305/02/20 06:486.31 2.83 5
Lead 47.1 mg/kg 05/02/20 14:43 7439-92-105/02/20 06:482.53 1.26 5
Selenium ND mg/kg 05/02/20 14:43 7782-49-205/02/20 06:483.16 1.28 5
Silver ND mg/kg 05/02/20 14:43 7440-22-405/02/20 06:480.631 0.269 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0464J mg/kg 05/04/20 19:28 7439-97-6 J05/04/20 15:060.0505 0.0227 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/05/20 10:14 83-32-904/30/20 16:544161071
Acenaphthylene ND ug/kg 05/05/20 10:14 208-96-804/30/20 16:5441698.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-1 (0-2)Lab ID:92475481001 Collected:04/28/20 12:05 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Aniline ND ug/kg 05/05/20 10:14 62-53-3 v104/30/20 16:5441693.3 1
Anthracene ND ug/kg 05/05/20 10:14 120-12-704/30/20 16:544161081
Benzo(a)anthracene ND ug/kg 05/05/20 10:14 56-55-304/30/20 16:544161321
Benzo(a)pyrene ND ug/kg 05/05/20 10:14 50-32-804/30/20 16:544161801
Benzo(b)fluoranthene ND ug/kg 05/05/20 10:14 205-99-204/30/20 16:544161671
Benzo(g,h,i)perylene ND ug/kg 05/05/20 10:14 191-24-204/30/20 16:544161621
Benzo(k)fluoranthene ND ug/kg 05/05/20 10:14 207-08-904/30/20 16:544161751
Benzoic Acid ND ug/kg 05/05/20 10:14 65-85-004/30/20 16:5420804481
Benzyl alcohol ND ug/kg 05/05/20 10:14 100-51-604/30/20 16:548312201
4-Bromophenylphenyl ether ND ug/kg 05/05/20 10:14 101-55-304/30/20 16:544161091
Butylbenzylphthalate ND ug/kg 05/05/20 10:14 85-68-704/30/20 16:544161111
4-Chloro-3-methylphenol ND ug/kg 05/05/20 10:14 59-50-704/30/20 16:548312531
4-Chloroaniline ND ug/kg 05/05/20 10:14 106-47-804/30/20 16:548312541
bis(2-Chloroethoxy)methane ND ug/kg 05/05/20 10:14 111-91-104/30/20 16:544161111
bis(2-Chloroethyl) ether ND ug/kg 05/05/20 10:14 111-44-404/30/20 16:5441688.3 1
2-Chloronaphthalene ND ug/kg 05/05/20 10:14 91-58-704/30/20 16:5441692.6 1
2-Chlorophenol ND ug/kg 05/05/20 10:14 95-57-804/30/20 16:5441696.7 1
4-Chlorophenylphenyl ether ND ug/kg 05/05/20 10:14 7005-72-304/30/20 16:544161081
Chrysene ND ug/kg 05/05/20 10:14 218-01-904/30/20 16:544161211
Dibenz(a,h)anthracene ND ug/kg 05/05/20 10:14 53-70-304/30/20 16:544161661
Dibenzofuran ND ug/kg 05/05/20 10:14 132-64-904/30/20 16:544161041
1,2-Dichlorobenzene ND ug/kg 05/05/20 10:14 95-50-104/30/20 16:5441689.9 1
1,3-Dichlorobenzene ND ug/kg 05/05/20 10:14 541-73-104/30/20 16:5441693.6 1
1,4-Dichlorobenzene ND ug/kg 05/05/20 10:14 106-46-704/30/20 16:5441691.4 1
3,3'-Dichlorobenzidine ND ug/kg 05/05/20 10:14 91-94-104/30/20 16:548312901
2,4-Dichlorophenol ND ug/kg 05/05/20 10:14 120-83-204/30/20 16:544161371
Diethylphthalate ND ug/kg 05/05/20 10:14 84-66-204/30/20 16:5441690.2 1
2,4-Dimethylphenol ND ug/kg 05/05/20 10:14 105-67-904/30/20 16:544161041
Dimethylphthalate ND ug/kg 05/05/20 10:14 131-11-304/30/20 16:5441693.9 1
Di-n-butylphthalate ND ug/kg 05/05/20 10:14 84-74-204/30/20 16:544161031
4,6-Dinitro-2-methylphenol ND ug/kg 05/05/20 10:14 534-52-104/30/20 16:548316701
2,4-Dinitrophenol ND ug/kg 05/05/20 10:14 51-28-504/30/20 16:54208013301
2,4-Dinitrotoluene ND ug/kg 05/05/20 10:14 121-14-204/30/20 16:544161101
2,6-Dinitrotoluene ND ug/kg 05/05/20 10:14 606-20-204/30/20 16:544161091
Di-n-octylphthalate ND ug/kg 05/05/20 10:14 117-84-004/30/20 16:544162371
bis(2-Ethylhexyl)phthalate ND ug/kg 05/05/20 10:14 117-81-704/30/20 16:544161361
Fluoranthene ND ug/kg 05/05/20 10:14 206-44-004/30/20 16:544161261
Fluorene ND ug/kg 05/05/20 10:14 86-73-704/30/20 16:544161111
Hexachloro-1,3-butadiene ND ug/kg 05/05/20 10:14 87-68-304/30/20 16:544161011
Hexachlorobenzene ND ug/kg 05/05/20 10:14 118-74-104/30/20 16:544161061
Hexachlorocyclopentadiene ND ug/kg 05/05/20 10:14 77-47-4 v204/30/20 16:544161661
Hexachloroethane ND ug/kg 05/05/20 10:14 67-72-104/30/20 16:5441694.7 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/05/20 10:14 193-39-504/30/20 16:544161901
Isophorone ND ug/kg 05/05/20 10:14 78-59-104/30/20 16:5441690.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-1 (0-2)Lab ID:92475481001 Collected:04/28/20 12:05 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1-Methylnaphthalene ND ug/kg 05/05/20 10:14 90-12-004/30/20 16:544161111
2-Methylnaphthalene ND ug/kg 05/05/20 10:14 91-57-604/30/20 16:544161061
2-Methylphenol(o-Cresol)ND ug/kg 05/05/20 10:14 95-48-704/30/20 16:5441692.1 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/05/20 10:14 15831-10-404/30/20 16:544161051
Naphthalene ND ug/kg 05/05/20 10:14 91-20-304/30/20 16:5441699.5 1
2-Nitroaniline ND ug/kg 05/05/20 10:14 88-74-404/30/20 16:5420802091
3-Nitroaniline ND ug/kg 05/05/20 10:14 99-09-2 v104/30/20 16:5420802201
4-Nitroaniline ND ug/kg 05/05/20 10:14 100-01-6 v104/30/20 16:548312051
Nitrobenzene ND ug/kg 05/05/20 10:14 98-95-3 v104/30/20 16:5441699.2 1
2-Nitrophenol ND ug/kg 05/05/20 10:14 88-75-504/30/20 16:544161281
4-Nitrophenol ND ug/kg 05/05/20 10:14 100-02-704/30/20 16:5420806621
N-Nitrosodimethylamine ND ug/kg 05/05/20 10:14 62-75-9 v104/30/20 16:544161171
N-Nitroso-di-n-propylamine ND ug/kg 05/05/20 10:14 621-64-704/30/20 16:544161161
N-Nitrosodiphenylamine ND ug/kg 05/05/20 10:14 86-30-604/30/20 16:544161061
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/05/20 10:14 108-60-1 v204/30/20 16:544161151
Pentachlorophenol ND ug/kg 05/05/20 10:14 87-86-504/30/20 16:548311901
Phenanthrene ND ug/kg 05/05/20 10:14 85-01-804/30/20 16:544161051
Phenol ND ug/kg 05/05/20 10:14 108-95-204/30/20 16:5441699.2 1
Pyrene ND ug/kg 05/05/20 10:14 129-00-004/30/20 16:544161141
Pyridine ND ug/kg 05/05/20 10:14 110-86-1 v104/30/20 16:544161051
1,2,4-Trichlorobenzene ND ug/kg 05/05/20 10:14 120-82-104/30/20 16:5441695.2 1
2,4,5-Trichlorophenol ND ug/kg 05/05/20 10:14 95-95-404/30/20 16:544161081
2,4,6-Trichlorophenol ND ug/kg 05/05/20 10:14 88-06-204/30/20 16:544161041
Surrogates
Nitrobenzene-d5 (S)79 %05/05/20 10:14 4165-60-004/30/20 16:5423-110 1
2-Fluorobiphenyl (S)61 %05/05/20 10:14 321-60-804/30/20 16:5430-110 1
Terphenyl-d14 (S)79 %05/05/20 10:14 1718-51-004/30/20 16:5428-110 1
Phenol-d6 (S)81 %05/05/20 10:14 13127-88-304/30/20 16:5422-110 1
2-Fluorophenol (S)88 %05/05/20 10:14 367-12-404/30/20 16:5413-110 1
2,4,6-Tribromophenol (S)77 %05/05/20 10:14 118-79-604/30/20 16:5427-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone ND ug/kg 04/30/20 19:01 67-64-104/30/20 14:321019.5 1
Benzene ND ug/kg 04/30/20 19:01 71-43-204/30/20 14:325.0 0.90 1
Bromobenzene ND ug/kg 04/30/20 19:01 108-86-104/30/20 14:325.0 1.4 1
Bromochloromethane ND ug/kg 04/30/20 19:01 74-97-504/30/20 14:325.0 1.2 1
Bromodichloromethane ND ug/kg 04/30/20 19:01 75-27-404/30/20 14:325.0 0.99 1
Bromoform ND ug/kg 04/30/20 19:01 75-25-204/30/20 14:325.0 2.5 1
Bromomethane ND ug/kg 04/30/20 19:01 74-83-9 IH04/30/20 14:3210.1 2.4 1
2-Butanone (MEK)ND ug/kg 04/30/20 19:01 78-93-304/30/20 14:3210112.0 1
n-Butylbenzene ND ug/kg 04/30/20 19:01 104-51-804/30/20 14:325.0 2.8 1
sec-Butylbenzene ND ug/kg 04/30/20 19:01 135-98-804/30/20 14:325.0 2.1 1
tert-Butylbenzene ND ug/kg 04/30/20 19:01 98-06-604/30/20 14:325.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-1 (0-2)Lab ID:92475481001 Collected:04/28/20 12:05 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Carbon tetrachloride ND ug/kg 04/30/20 19:01 56-23-504/30/20 14:325.0 0.96 1
Chlorobenzene ND ug/kg 04/30/20 19:01 108-90-704/30/20 14:325.0 0.97 1
Chloroethane ND ug/kg 04/30/20 19:01 75-00-304/30/20 14:3210.1 2.1 1
Chloroform ND ug/kg 04/30/20 19:01 67-66-304/30/20 14:325.0 1.1 1
Chloromethane ND ug/kg 04/30/20 19:01 74-87-304/30/20 14:3210.1 3.3 1
2-Chlorotoluene ND ug/kg 04/30/20 19:01 95-49-804/30/20 14:325.0 1.5 1
4-Chlorotoluene ND ug/kg 04/30/20 19:01 106-43-404/30/20 14:325.0 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/30/20 19:01 96-12-804/30/20 14:325.0 2.6 1
Dibromochloromethane ND ug/kg 04/30/20 19:01 124-48-104/30/20 14:325.0 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 04/30/20 19:01 106-93-404/30/20 14:325.0 1.1 1
Dibromomethane ND ug/kg 04/30/20 19:01 74-95-304/30/20 14:325.0 1.5 1
1,2-Dichlorobenzene ND ug/kg 04/30/20 19:01 95-50-104/30/20 14:325.0 1.8 1
1,3-Dichlorobenzene ND ug/kg 04/30/20 19:01 541-73-104/30/20 14:325.0 1.8 1
1,4-Dichlorobenzene ND ug/kg 04/30/20 19:01 106-46-704/30/20 14:325.0 1.7 1
Dichlorodifluoromethane ND ug/kg 04/30/20 19:01 75-71-804/30/20 14:3210.1 4.1 1
1,1-Dichloroethane ND ug/kg 04/30/20 19:01 75-34-304/30/20 14:325.0 0.74 1
1,2-Dichloroethane ND ug/kg 04/30/20 19:01 107-06-204/30/20 14:325.0 1.0 1
1,1-Dichloroethene ND ug/kg 04/30/20 19:01 75-35-404/30/20 14:325.0 1.2 1
cis-1,2-Dichloroethene ND ug/kg 04/30/20 19:01 156-59-204/30/20 14:325.0 0.87 1
trans-1,2-Dichloroethene ND ug/kg 04/30/20 19:01 156-60-504/30/20 14:325.0 0.99 1
1,2-Dichloropropane ND ug/kg 04/30/20 19:01 78-87-504/30/20 14:325.0 1.9 1
1,3-Dichloropropane ND ug/kg 04/30/20 19:01 142-28-904/30/20 14:325.0 1.9 1
2,2-Dichloropropane ND ug/kg 04/30/20 19:01 594-20-704/30/20 14:325.0 0.50 1
1,1-Dichloropropene ND ug/kg 04/30/20 19:01 563-58-604/30/20 14:325.0 2.1 1
cis-1,3-Dichloropropene ND ug/kg 04/30/20 19:01 10061-01-504/30/20 14:325.0 2.3 1
trans-1,3-Dichloropropene ND ug/kg 04/30/20 19:01 10061-02-604/30/20 14:325.0 0.88 1
Diisopropyl ether ND ug/kg 04/30/20 19:01 108-20-304/30/20 14:325.0 2.9 1
Ethylbenzene ND ug/kg 04/30/20 19:01 100-41-404/30/20 14:325.0 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/30/20 19:01 87-68-304/30/20 14:325.0 2.5 1
2-Hexanone ND ug/kg 04/30/20 19:01 591-78-604/30/20 14:3250.4 5.2 1
Isopropylbenzene (Cumene)ND ug/kg 04/30/20 19:01 98-82-804/30/20 14:325.0 1.5 1
p-Isopropyltoluene ND ug/kg 04/30/20 19:01 99-87-604/30/20 14:325.0 2.4 1
Methylene Chloride ND ug/kg 04/30/20 19:01 75-09-204/30/20 14:3220.1 6.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/30/20 19:01 108-10-104/30/20 14:3250.4 3.8 1
Methyl-tert-butyl ether ND ug/kg 04/30/20 19:01 1634-04-404/30/20 14:325.0 2.9 1
Naphthalene ND ug/kg 04/30/20 19:01 91-20-304/30/20 14:325.0 4.3 1
n-Propylbenzene ND ug/kg 04/30/20 19:01 103-65-104/30/20 14:325.0 1.7 1
Styrene ND ug/kg 04/30/20 19:01 100-42-504/30/20 14:325.0 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/30/20 19:01 630-20-604/30/20 14:325.0 1.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/30/20 19:01 79-34-504/30/20 14:325.0 1.7 1
Tetrachloroethene ND ug/kg 04/30/20 19:01 127-18-404/30/20 14:325.0 1.6 1
Toluene ND ug/kg 04/30/20 19:01 108-88-304/30/20 14:325.0 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 04/30/20 19:01 87-61-604/30/20 14:325.0 3.6 1
1,2,4-Trichlorobenzene ND ug/kg 04/30/20 19:01 120-82-104/30/20 14:325.0 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-1 (0-2)Lab ID:92475481001 Collected:04/28/20 12:05 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
1,1,1-Trichloroethane ND ug/kg 04/30/20 19:01 71-55-604/30/20 14:325.0 0.88 1
1,1,2-Trichloroethane ND ug/kg 04/30/20 19:01 79-00-504/30/20 14:325.0 1.1 1
Trichloroethene ND ug/kg 04/30/20 19:01 79-01-604/30/20 14:325.0 1.3 1
Trichlorofluoromethane ND ug/kg 04/30/20 19:01 75-69-404/30/20 14:325.0 1.2 1
1,2,3-Trichloropropane ND ug/kg 04/30/20 19:01 96-18-404/30/20 14:325.0 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 04/30/20 19:01 95-63-604/30/20 14:325.0 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/30/20 19:01 108-67-804/30/20 14:325.0 1.7 1
Vinyl acetate ND ug/kg 04/30/20 19:01 108-05-404/30/20 14:3250.4 16.4 1
Vinyl chloride ND ug/kg 04/30/20 19:01 75-01-404/30/20 14:3210.1 1.9 1
Xylene (Total)ND ug/kg 04/30/20 19:01 1330-20-704/30/20 14:3210.1 3.5 1
m&p-Xylene ND ug/kg 04/30/20 19:01 179601-23-104/30/20 14:3210.1 2.4 1
o-Xylene ND ug/kg 04/30/20 19:01 95-47-604/30/20 14:325.0 1.2 1
Surrogates
Toluene-d8 (S)101 %04/30/20 19:01 2037-26-504/30/20 14:3270-130 1
4-Bromofluorobenzene (S)101 %04/30/20 19:01 460-00-404/30/20 14:3270-130 1
1,2-Dichloroethane-d4 (S)106 %04/30/20 19:01 17060-07-004/30/20 14:3270-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.1 %04/29/20 17:050.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 79.2 %05/05/20 10:5805/05/20 10:501
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.340J mg/kg 05/04/20 11:27 18540-29-9 J05/02/20 11:141.26 0.322 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-2 (0-2)Lab ID:92475481002 Collected:04/28/20 11:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8081 GCS Pesticides
Aldrin ND ug/kg 05/06/20 01:13 309-00-204/29/20 18:495.4 2.0 2
alpha-BHC ND ug/kg 05/06/20 01:13 319-84-604/29/20 18:495.4 1.9 2
beta-BHC ND ug/kg 05/06/20 01:13 319-85-704/29/20 18:495.4 2.0 2
delta-BHC ND ug/kg 05/06/20 01:13 319-86-804/29/20 18:495.4 1.9 2
gamma-BHC (Lindane)ND ug/kg 05/06/20 01:13 58-89-904/29/20 18:495.4 2.2 2
Chlordane (Technical)ND ug/kg 05/06/20 01:13 57-74-904/29/20 18:4919.0 19.0 2
4,4'-DDD ND ug/kg 05/06/20 01:13 72-54-804/29/20 18:495.4 2.3 2
4,4'-DDE ND ug/kg 05/06/20 01:13 72-55-904/29/20 18:495.4 2.1 2
4,4'-DDT ND ug/kg 05/06/20 01:13 50-29-304/29/20 18:495.4 2.0 2
Dieldrin ND ug/kg 05/06/20 01:13 60-57-104/29/20 18:495.4 2.2 2
Endosulfan I ND ug/kg 05/06/20 01:13 959-98-804/29/20 18:495.4 2.2 2
Endosulfan II ND ug/kg 05/06/20 01:13 33213-65-904/29/20 18:495.4 2.2 2
Endosulfan sulfate ND ug/kg 05/06/20 01:13 1031-07-804/29/20 18:495.4 2.4 2
Endrin ND ug/kg 05/06/20 01:13 72-20-804/29/20 18:495.4 2.3 2
Endrin aldehyde ND ug/kg 05/06/20 01:13 7421-93-404/29/20 18:495.4 2.1 2
Endrin ketone ND ug/kg 05/06/20 01:13 53494-70-504/29/20 18:495.4 2.9 2
Heptachlor ND ug/kg 05/06/20 01:13 76-44-804/29/20 18:495.4 1.8 2
Heptachlor epoxide ND ug/kg 05/06/20 01:13 1024-57-304/29/20 18:495.4 1.8 2
Hexachlorobenzene ND ug/kg 05/06/20 01:13 118-74-104/29/20 18:495.4 1.8 2
Methoxychlor ND ug/kg 05/06/20 01:13 72-43-504/29/20 18:4913.6 7.1 2
Mirex ND ug/kg 05/06/20 01:13 2385-85-504/29/20 18:4913.6 6.6 2
Toxaphene ND ug/kg 05/06/20 01:13 8001-35-204/29/20 18:4919.0 19.0 2
Surrogates
Tetrachloro-m-xylene (S)59 %05/06/20 01:13 877-09-8 D304/29/20 18:4915-130 2
Decachlorobiphenyl (S)62 %05/06/20 01:13 2051-24-304/29/20 18:4910-130 2
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.29 mg/kg 05/02/20 15:40 7440-38-205/02/20 06:481.38 0.584 5
Barium 66.9 mg/kg 05/02/20 15:40 7440-39-305/02/20 06:483.46 1.73 5
Cadmium ND mg/kg 05/02/20 15:40 7440-43-905/02/20 06:481.38 0.562 5
Chromium 41.4 mg/kg 05/02/20 15:40 7440-47-305/02/20 06:486.92 3.10 5
Lead 41.0 mg/kg 05/02/20 15:40 7439-92-105/02/20 06:482.77 1.38 5
Selenium ND mg/kg 05/02/20 15:40 7782-49-205/02/20 06:483.46 1.40 5
Silver ND mg/kg 05/02/20 15:40 7440-22-405/02/20 06:480.692 0.295 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0391J mg/kg 05/04/20 19:52 7439-97-6 J05/04/20 15:060.0553 0.0249 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/05/20 11:35 83-32-904/30/20 16:544521161
Acenaphthylene ND ug/kg 05/05/20 11:35 208-96-804/30/20 16:544521071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-2 (0-2)Lab ID:92475481002 Collected:04/28/20 11:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Aniline ND ug/kg 05/05/20 11:35 62-53-3 v104/30/20 16:544521011
Anthracene ND ug/kg 05/05/20 11:35 120-12-704/30/20 16:544521171
Benzo(a)anthracene ND ug/kg 05/05/20 11:35 56-55-304/30/20 16:544521441
Benzo(a)pyrene ND ug/kg 05/05/20 11:35 50-32-804/30/20 16:544521961
Benzo(b)fluoranthene ND ug/kg 05/05/20 11:35 205-99-204/30/20 16:544521821
Benzo(g,h,i)perylene ND ug/kg 05/05/20 11:35 191-24-204/30/20 16:544521771
Benzo(k)fluoranthene ND ug/kg 05/05/20 11:35 207-08-904/30/20 16:544521901
Benzoic Acid ND ug/kg 05/05/20 11:35 65-85-004/30/20 16:5422604871
Benzyl alcohol ND ug/kg 05/05/20 11:35 100-51-604/30/20 16:549042401
4-Bromophenylphenyl ether ND ug/kg 05/05/20 11:35 101-55-304/30/20 16:544521191
Butylbenzylphthalate ND ug/kg 05/05/20 11:35 85-68-704/30/20 16:544521201
4-Chloro-3-methylphenol ND ug/kg 05/05/20 11:35 59-50-704/30/20 16:549042751
4-Chloroaniline ND ug/kg 05/05/20 11:35 106-47-804/30/20 16:549042771
bis(2-Chloroethoxy)methane ND ug/kg 05/05/20 11:35 111-91-104/30/20 16:544521211
bis(2-Chloroethyl) ether ND ug/kg 05/05/20 11:35 111-44-404/30/20 16:5445296.0 1
2-Chloronaphthalene ND ug/kg 05/05/20 11:35 91-58-704/30/20 16:544521011
2-Chlorophenol ND ug/kg 05/05/20 11:35 95-57-804/30/20 16:544521051
4-Chlorophenylphenyl ether ND ug/kg 05/05/20 11:35 7005-72-304/30/20 16:544521171
Chrysene ND ug/kg 05/05/20 11:35 218-01-904/30/20 16:544521311
Dibenz(a,h)anthracene ND ug/kg 05/05/20 11:35 53-70-304/30/20 16:544521811
Dibenzofuran ND ug/kg 05/05/20 11:35 132-64-904/30/20 16:544521131
1,2-Dichlorobenzene ND ug/kg 05/05/20 11:35 95-50-104/30/20 16:5445297.8 1
1,3-Dichlorobenzene ND ug/kg 05/05/20 11:35 541-73-104/30/20 16:544521021
1,4-Dichlorobenzene ND ug/kg 05/05/20 11:35 106-46-704/30/20 16:5445299.4 1
3,3'-Dichlorobenzidine ND ug/kg 05/05/20 11:35 91-94-104/30/20 16:549043151
2,4-Dichlorophenol ND ug/kg 05/05/20 11:35 120-83-204/30/20 16:544521491
Diethylphthalate ND ug/kg 05/05/20 11:35 84-66-204/30/20 16:5445298.0 1
2,4-Dimethylphenol ND ug/kg 05/05/20 11:35 105-67-904/30/20 16:544521131
Dimethylphthalate ND ug/kg 05/05/20 11:35 131-11-304/30/20 16:544521021
Di-n-butylphthalate ND ug/kg 05/05/20 11:35 84-74-204/30/20 16:544521111
4,6-Dinitro-2-methylphenol ND ug/kg 05/05/20 11:35 534-52-104/30/20 16:549047281
2,4-Dinitrophenol ND ug/kg 05/05/20 11:35 51-28-504/30/20 16:54226014401
2,4-Dinitrotoluene ND ug/kg 05/05/20 11:35 121-14-204/30/20 16:544521201
2,6-Dinitrotoluene ND ug/kg 05/05/20 11:35 606-20-204/30/20 16:544521181
Di-n-octylphthalate ND ug/kg 05/05/20 11:35 117-84-004/30/20 16:544522571
bis(2-Ethylhexyl)phthalate ND ug/kg 05/05/20 11:35 117-81-704/30/20 16:544521481
Fluoranthene ND ug/kg 05/05/20 11:35 206-44-004/30/20 16:544521371
Fluorene ND ug/kg 05/05/20 11:35 86-73-704/30/20 16:544521211
Hexachloro-1,3-butadiene ND ug/kg 05/05/20 11:35 87-68-304/30/20 16:544521101
Hexachlorobenzene ND ug/kg 05/05/20 11:35 118-74-104/30/20 16:544521151
Hexachlorocyclopentadiene ND ug/kg 05/05/20 11:35 77-47-4 v204/30/20 16:544521811
Hexachloroethane ND ug/kg 05/05/20 11:35 67-72-104/30/20 16:544521031
Indeno(1,2,3-cd)pyrene ND ug/kg 05/05/20 11:35 193-39-504/30/20 16:544522071
Isophorone ND ug/kg 05/05/20 11:35 78-59-104/30/20 16:5445298.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-2 (0-2)Lab ID:92475481002 Collected:04/28/20 11:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1-Methylnaphthalene ND ug/kg 05/05/20 11:35 90-12-004/30/20 16:544521201
2-Methylnaphthalene ND ug/kg 05/05/20 11:35 91-57-604/30/20 16:544521151
2-Methylphenol(o-Cresol)ND ug/kg 05/05/20 11:35 95-48-704/30/20 16:544521001
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/05/20 11:35 15831-10-404/30/20 16:544521141
Naphthalene ND ug/kg 05/05/20 11:35 91-20-304/30/20 16:544521081
2-Nitroaniline ND ug/kg 05/05/20 11:35 88-74-404/30/20 16:5422602271
3-Nitroaniline ND ug/kg 05/05/20 11:35 99-09-2 v104/30/20 16:5422602401
4-Nitroaniline ND ug/kg 05/05/20 11:35 100-01-6 v104/30/20 16:549042231
Nitrobenzene ND ug/kg 05/05/20 11:35 98-95-3 v104/30/20 16:544521081
2-Nitrophenol ND ug/kg 05/05/20 11:35 88-75-504/30/20 16:544521401
4-Nitrophenol ND ug/kg 05/05/20 11:35 100-02-704/30/20 16:5422607201
N-Nitrosodimethylamine ND ug/kg 05/05/20 11:35 62-75-9 v104/30/20 16:544521271
N-Nitroso-di-n-propylamine ND ug/kg 05/05/20 11:35 621-64-704/30/20 16:544521271
N-Nitrosodiphenylamine ND ug/kg 05/05/20 11:35 86-30-604/30/20 16:544521151
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/05/20 11:35 108-60-1 v204/30/20 16:544521261
Pentachlorophenol ND ug/kg 05/05/20 11:35 87-86-504/30/20 16:549042071
Phenanthrene ND ug/kg 05/05/20 11:35 85-01-804/30/20 16:544521141
Phenol ND ug/kg 05/05/20 11:35 108-95-204/30/20 16:544521081
Pyrene ND ug/kg 05/05/20 11:35 129-00-004/30/20 16:544521241
Pyridine ND ug/kg 05/05/20 11:35 110-86-1 v104/30/20 16:544521141
1,2,4-Trichlorobenzene ND ug/kg 05/05/20 11:35 120-82-104/30/20 16:544521041
2,4,5-Trichlorophenol ND ug/kg 05/05/20 11:35 95-95-404/30/20 16:544521171
2,4,6-Trichlorophenol ND ug/kg 05/05/20 11:35 88-06-204/30/20 16:544521141
Surrogates
Nitrobenzene-d5 (S)72 %05/05/20 11:35 4165-60-004/30/20 16:5423-110 1
2-Fluorobiphenyl (S)43 %05/05/20 11:35 321-60-804/30/20 16:5430-110 1
Terphenyl-d14 (S)68 %05/05/20 11:35 1718-51-004/30/20 16:5428-110 1
Phenol-d6 (S)69 %05/05/20 11:35 13127-88-304/30/20 16:5422-110 1
2-Fluorophenol (S)77 %05/05/20 11:35 367-12-404/30/20 16:5413-110 1
2,4,6-Tribromophenol (S)64 %05/05/20 11:35 118-79-604/30/20 16:5427-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone 11.3J ug/kg 04/30/20 19:25 67-64-104/30/20 14:3210610.0 1
Benzene ND ug/kg 04/30/20 19:25 71-43-204/30/20 14:325.3 0.95 1
Bromobenzene ND ug/kg 04/30/20 19:25 108-86-104/30/20 14:325.3 1.4 1
Bromochloromethane ND ug/kg 04/30/20 19:25 74-97-504/30/20 14:325.3 1.3 1
Bromodichloromethane ND ug/kg 04/30/20 19:25 75-27-404/30/20 14:325.3 1.0 1
Bromoform ND ug/kg 04/30/20 19:25 75-25-204/30/20 14:325.3 2.6 1
Bromomethane ND ug/kg 04/30/20 19:25 74-83-9 IH04/30/20 14:3210.6 2.5 1
2-Butanone (MEK)ND ug/kg 04/30/20 19:25 78-93-304/30/20 14:3210612.7 1
n-Butylbenzene ND ug/kg 04/30/20 19:25 104-51-804/30/20 14:325.3 3.0 1
sec-Butylbenzene ND ug/kg 04/30/20 19:25 135-98-804/30/20 14:325.3 2.3 1
tert-Butylbenzene ND ug/kg 04/30/20 19:25 98-06-604/30/20 14:325.3 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-2 (0-2)Lab ID:92475481002 Collected:04/28/20 11:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Carbon tetrachloride ND ug/kg 04/30/20 19:25 56-23-504/30/20 14:325.3 1.0 1
Chlorobenzene ND ug/kg 04/30/20 19:25 108-90-704/30/20 14:325.3 1.0 1
Chloroethane ND ug/kg 04/30/20 19:25 75-00-304/30/20 14:3210.6 2.2 1
Chloroform ND ug/kg 04/30/20 19:25 67-66-304/30/20 14:325.3 1.1 1
Chloromethane ND ug/kg 04/30/20 19:25 74-87-304/30/20 14:3210.6 3.5 1
2-Chlorotoluene ND ug/kg 04/30/20 19:25 95-49-804/30/20 14:325.3 1.6 1
4-Chlorotoluene ND ug/kg 04/30/20 19:25 106-43-404/30/20 14:325.3 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/30/20 19:25 96-12-804/30/20 14:325.3 2.7 1
Dibromochloromethane ND ug/kg 04/30/20 19:25 124-48-104/30/20 14:325.3 2.7 1
1,2-Dibromoethane (EDB)ND ug/kg 04/30/20 19:25 106-93-404/30/20 14:325.3 1.2 1
Dibromomethane ND ug/kg 04/30/20 19:25 74-95-304/30/20 14:325.3 1.6 1
1,2-Dichlorobenzene ND ug/kg 04/30/20 19:25 95-50-104/30/20 14:325.3 1.9 1
1,3-Dichlorobenzene ND ug/kg 04/30/20 19:25 541-73-104/30/20 14:325.3 1.9 1
1,4-Dichlorobenzene ND ug/kg 04/30/20 19:25 106-46-704/30/20 14:325.3 1.8 1
Dichlorodifluoromethane ND ug/kg 04/30/20 19:25 75-71-804/30/20 14:3210.6 4.4 1
1,1-Dichloroethane ND ug/kg 04/30/20 19:25 75-34-304/30/20 14:325.3 0.78 1
1,2-Dichloroethane ND ug/kg 04/30/20 19:25 107-06-204/30/20 14:325.3 1.1 1
1,1-Dichloroethene ND ug/kg 04/30/20 19:25 75-35-404/30/20 14:325.3 1.2 1
cis-1,2-Dichloroethene ND ug/kg 04/30/20 19:25 156-59-204/30/20 14:325.3 0.92 1
trans-1,2-Dichloroethene ND ug/kg 04/30/20 19:25 156-60-504/30/20 14:325.3 1.0 1
1,2-Dichloropropane ND ug/kg 04/30/20 19:25 78-87-504/30/20 14:325.3 2.0 1
1,3-Dichloropropane ND ug/kg 04/30/20 19:25 142-28-904/30/20 14:325.3 2.0 1
2,2-Dichloropropane ND ug/kg 04/30/20 19:25 594-20-704/30/20 14:325.3 0.53 1
1,1-Dichloropropene ND ug/kg 04/30/20 19:25 563-58-604/30/20 14:325.3 2.3 1
cis-1,3-Dichloropropene ND ug/kg 04/30/20 19:25 10061-01-504/30/20 14:325.3 2.4 1
trans-1,3-Dichloropropene ND ug/kg 04/30/20 19:25 10061-02-604/30/20 14:325.3 0.93 1
Diisopropyl ether ND ug/kg 04/30/20 19:25 108-20-304/30/20 14:325.3 3.0 1
Ethylbenzene ND ug/kg 04/30/20 19:25 100-41-404/30/20 14:325.3 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/30/20 19:25 87-68-304/30/20 14:325.3 2.6 1
2-Hexanone ND ug/kg 04/30/20 19:25 591-78-604/30/20 14:3253.2 5.5 1
Isopropylbenzene (Cumene)ND ug/kg 04/30/20 19:25 98-82-804/30/20 14:325.3 1.5 1
p-Isopropyltoluene ND ug/kg 04/30/20 19:25 99-87-604/30/20 14:325.3 2.6 1
Methylene Chloride ND ug/kg 04/30/20 19:25 75-09-204/30/20 14:3221.3 6.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/30/20 19:25 108-10-104/30/20 14:3253.2 4.0 1
Methyl-tert-butyl ether ND ug/kg 04/30/20 19:25 1634-04-404/30/20 14:325.3 3.0 1
Naphthalene ND ug/kg 04/30/20 19:25 91-20-304/30/20 14:325.3 4.5 1
n-Propylbenzene ND ug/kg 04/30/20 19:25 103-65-104/30/20 14:325.3 1.8 1
Styrene ND ug/kg 04/30/20 19:25 100-42-504/30/20 14:325.3 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/30/20 19:25 630-20-604/30/20 14:325.3 1.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/30/20 19:25 79-34-504/30/20 14:325.3 1.8 1
Tetrachloroethene ND ug/kg 04/30/20 19:25 127-18-404/30/20 14:325.3 1.7 1
Toluene ND ug/kg 04/30/20 19:25 108-88-304/30/20 14:325.3 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 04/30/20 19:25 87-61-604/30/20 14:325.3 3.8 1
1,2,4-Trichlorobenzene ND ug/kg 04/30/20 19:25 120-82-104/30/20 14:325.3 2.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-2 (0-2)Lab ID:92475481002 Collected:04/28/20 11:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
1,1,1-Trichloroethane ND ug/kg 04/30/20 19:25 71-55-604/30/20 14:325.3 0.93 1
1,1,2-Trichloroethane ND ug/kg 04/30/20 19:25 79-00-504/30/20 14:325.3 1.2 1
Trichloroethene ND ug/kg 04/30/20 19:25 79-01-604/30/20 14:325.3 1.4 1
Trichlorofluoromethane ND ug/kg 04/30/20 19:25 75-69-404/30/20 14:325.3 1.3 1
1,2,3-Trichloropropane ND ug/kg 04/30/20 19:25 96-18-404/30/20 14:325.3 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 04/30/20 19:25 95-63-604/30/20 14:325.3 2.1 1
1,3,5-Trimethylbenzene ND ug/kg 04/30/20 19:25 108-67-804/30/20 14:325.3 1.8 1
Vinyl acetate ND ug/kg 04/30/20 19:25 108-05-404/30/20 14:3253.2 17.3 1
Vinyl chloride ND ug/kg 04/30/20 19:25 75-01-404/30/20 14:3210.6 2.0 1
Xylene (Total)ND ug/kg 04/30/20 19:25 1330-20-704/30/20 14:3210.6 3.7 1
m&p-Xylene ND ug/kg 04/30/20 19:25 179601-23-104/30/20 14:3210.6 2.5 1
o-Xylene ND ug/kg 04/30/20 19:25 95-47-604/30/20 14:325.3 1.2 1
Surrogates
Toluene-d8 (S)102 %04/30/20 19:25 2037-26-504/30/20 14:3270-130 1
4-Bromofluorobenzene (S)100 %04/30/20 19:25 460-00-404/30/20 14:3270-130 1
1,2-Dichloroethane-d4 (S)107 %04/30/20 19:25 17060-07-004/30/20 14:3270-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 27.5 %04/29/20 17:050.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 72.3 %05/05/20 10:5805/05/20 10:501
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.447J mg/kg 05/04/20 11:32 18540-29-9 J05/02/20 11:141.38 0.353 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-3 (0-2)Lab ID:92475481003 Collected:04/28/20 10:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8081 GCS Pesticides
Aldrin ND ug/kg 05/06/20 01:28 309-00-204/29/20 18:4924.6 8.9 10
alpha-BHC ND ug/kg 05/06/20 01:28 319-84-604/29/20 18:4924.6 8.5 10
beta-BHC ND ug/kg 05/06/20 01:28 319-85-704/29/20 18:4924.6 8.9 10
delta-BHC ND ug/kg 05/06/20 01:28 319-86-804/29/20 18:4924.6 8.7 10
gamma-BHC (Lindane)ND ug/kg 05/06/20 01:28 58-89-904/29/20 18:4924.6 10.1 10
Chlordane (Technical)132 ug/kg 05/06/20 01:28 57-74-904/29/20 18:4986.0 86.0 10
4,4'-DDD ND ug/kg 05/06/20 01:28 72-54-804/29/20 18:4924.6 10.2 10
4,4'-DDE ND ug/kg 05/06/20 01:28 72-55-904/29/20 18:4924.6 9.7 10
4,4'-DDT ND ug/kg 05/06/20 01:28 50-29-304/29/20 18:4924.6 8.9 10
Dieldrin 20.5J ug/kg 05/06/20 01:28 60-57-104/29/20 18:4924.6 10 10
Endosulfan I ND ug/kg 05/06/20 01:28 959-98-804/29/20 18:4924.6 9.9 10
Endosulfan II ND ug/kg 05/06/20 01:28 33213-65-904/29/20 18:4924.6 9.9 10
Endosulfan sulfate ND ug/kg 05/06/20 01:28 1031-07-804/29/20 18:4924.6 10.7 10
Endrin ND ug/kg 05/06/20 01:28 72-20-804/29/20 18:4924.6 10.3 10
Endrin aldehyde ND ug/kg 05/06/20 01:28 7421-93-404/29/20 18:4924.6 9.6 10
Endrin ketone ND ug/kg 05/06/20 01:28 53494-70-504/29/20 18:4924.6 12.9 10
Heptachlor ND ug/kg 05/06/20 01:28 76-44-804/29/20 18:4924.6 8.1 10
Heptachlor epoxide ND ug/kg 05/06/20 01:28 1024-57-304/29/20 18:4924.6 8.2 10
Hexachlorobenzene ND ug/kg 05/06/20 01:28 118-74-104/29/20 18:4924.6 8.1 10
Methoxychlor ND ug/kg 05/06/20 01:28 72-43-504/29/20 18:4961.4 32.2 10
Mirex ND ug/kg 05/06/20 01:28 2385-85-504/29/20 18:4961.4 29.8 10
Toxaphene ND ug/kg 05/06/20 01:28 8001-35-204/29/20 18:4986.0 86.0 10
Surrogates
Tetrachloro-m-xylene (S)0 %05/06/20 01:28 877-09-8 S404/29/20 18:4915-130 10
Decachlorobiphenyl (S)0 %05/06/20 01:28 2051-24-3 S404/29/20 18:4910-130 10
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 3.14 mg/kg 05/02/20 15:43 7440-38-205/02/20 06:481.40 0.590 5
Barium 73.1 mg/kg 05/02/20 15:43 7440-39-305/02/20 06:483.49 1.75 5
Cadmium ND mg/kg 05/02/20 15:43 7440-43-905/02/20 06:481.40 0.567 5
Chromium 38.3 mg/kg 05/02/20 15:43 7440-47-305/02/20 06:486.99 3.13 5
Lead 28.1 mg/kg 05/02/20 15:43 7439-92-105/02/20 06:482.80 1.40 5
Selenium ND mg/kg 05/02/20 15:43 7782-49-205/02/20 06:483.49 1.41 5
Silver ND mg/kg 05/02/20 15:43 7440-22-405/02/20 06:480.699 0.298 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0278J mg/kg 05/04/20 19:54 7439-97-6 J05/04/20 15:060.0559 0.0252 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/05/20 12:03 83-32-904/30/20 16:544161071
Acenaphthylene ND ug/kg 05/05/20 12:03 208-96-804/30/20 16:5441698.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-3 (0-2)Lab ID:92475481003 Collected:04/28/20 10:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Aniline ND ug/kg 05/05/20 12:03 62-53-3 v104/30/20 16:5441693.5 1
Anthracene ND ug/kg 05/05/20 12:03 120-12-704/30/20 16:544161081
Benzo(a)anthracene ND ug/kg 05/05/20 12:03 56-55-304/30/20 16:544161321
Benzo(a)pyrene ND ug/kg 05/05/20 12:03 50-32-804/30/20 16:544161801
Benzo(b)fluoranthene ND ug/kg 05/05/20 12:03 205-99-204/30/20 16:544161681
Benzo(g,h,i)perylene ND ug/kg 05/05/20 12:03 191-24-204/30/20 16:544161631
Benzo(k)fluoranthene ND ug/kg 05/05/20 12:03 207-08-904/30/20 16:544161751
Benzoic Acid ND ug/kg 05/05/20 12:03 65-85-004/30/20 16:5420804491
Benzyl alcohol ND ug/kg 05/05/20 12:03 100-51-604/30/20 16:548332211
4-Bromophenylphenyl ether ND ug/kg 05/05/20 12:03 101-55-304/30/20 16:544161091
Butylbenzylphthalate ND ug/kg 05/05/20 12:03 85-68-704/30/20 16:544161111
4-Chloro-3-methylphenol ND ug/kg 05/05/20 12:03 59-50-704/30/20 16:548332541
4-Chloroaniline ND ug/kg 05/05/20 12:03 106-47-804/30/20 16:548332551
bis(2-Chloroethoxy)methane ND ug/kg 05/05/20 12:03 111-91-104/30/20 16:544161111
bis(2-Chloroethyl) ether ND ug/kg 05/05/20 12:03 111-44-404/30/20 16:5441688.4 1
2-Chloronaphthalene ND ug/kg 05/05/20 12:03 91-58-704/30/20 16:5441692.7 1
2-Chlorophenol ND ug/kg 05/05/20 12:03 95-57-804/30/20 16:5441696.9 1
4-Chlorophenylphenyl ether ND ug/kg 05/05/20 12:03 7005-72-304/30/20 16:544161081
Chrysene ND ug/kg 05/05/20 12:03 218-01-904/30/20 16:544161211
Dibenz(a,h)anthracene ND ug/kg 05/05/20 12:03 53-70-304/30/20 16:544161671
Dibenzofuran ND ug/kg 05/05/20 12:03 132-64-904/30/20 16:544161041
1,2-Dichlorobenzene ND ug/kg 05/05/20 12:03 95-50-104/30/20 16:5441690.1 1
1,3-Dichlorobenzene ND ug/kg 05/05/20 12:03 541-73-104/30/20 16:5441693.7 1
1,4-Dichlorobenzene ND ug/kg 05/05/20 12:03 106-46-704/30/20 16:5441691.6 1
3,3'-Dichlorobenzidine ND ug/kg 05/05/20 12:03 91-94-104/30/20 16:548332901
2,4-Dichlorophenol ND ug/kg 05/05/20 12:03 120-83-204/30/20 16:544161381
Diethylphthalate ND ug/kg 05/05/20 12:03 84-66-204/30/20 16:5441690.3 1
2,4-Dimethylphenol ND ug/kg 05/05/20 12:03 105-67-904/30/20 16:544161041
Dimethylphthalate ND ug/kg 05/05/20 12:03 131-11-304/30/20 16:5441694.1 1
Di-n-butylphthalate ND ug/kg 05/05/20 12:03 84-74-204/30/20 16:544161031
4,6-Dinitro-2-methylphenol ND ug/kg 05/05/20 12:03 534-52-104/30/20 16:548336711
2,4-Dinitrophenol ND ug/kg 05/05/20 12:03 51-28-504/30/20 16:54208013301
2,4-Dinitrotoluene ND ug/kg 05/05/20 12:03 121-14-204/30/20 16:544161101
2,6-Dinitrotoluene ND ug/kg 05/05/20 12:03 606-20-204/30/20 16:544161091
Di-n-octylphthalate ND ug/kg 05/05/20 12:03 117-84-004/30/20 16:544162371
bis(2-Ethylhexyl)phthalate ND ug/kg 05/05/20 12:03 117-81-704/30/20 16:544161361
Fluoranthene ND ug/kg 05/05/20 12:03 206-44-004/30/20 16:544161261
Fluorene ND ug/kg 05/05/20 12:03 86-73-704/30/20 16:544161111
Hexachloro-1,3-butadiene ND ug/kg 05/05/20 12:03 87-68-304/30/20 16:544161011
Hexachlorobenzene ND ug/kg 05/05/20 12:03 118-74-104/30/20 16:544161061
Hexachlorocyclopentadiene ND ug/kg 05/05/20 12:03 77-47-4 v204/30/20 16:544161671
Hexachloroethane ND ug/kg 05/05/20 12:03 67-72-104/30/20 16:5441694.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/05/20 12:03 193-39-504/30/20 16:544161901
Isophorone ND ug/kg 05/05/20 12:03 78-59-104/30/20 16:5441690.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-3 (0-2)Lab ID:92475481003 Collected:04/28/20 10:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1-Methylnaphthalene ND ug/kg 05/05/20 12:03 90-12-004/30/20 16:544161111
2-Methylnaphthalene ND ug/kg 05/05/20 12:03 91-57-604/30/20 16:544161061
2-Methylphenol(o-Cresol)ND ug/kg 05/05/20 12:03 95-48-704/30/20 16:5441692.2 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/05/20 12:03 15831-10-404/30/20 16:544161051
Naphthalene ND ug/kg 05/05/20 12:03 91-20-304/30/20 16:5441699.7 1
2-Nitroaniline ND ug/kg 05/05/20 12:03 88-74-404/30/20 16:5420802091
3-Nitroaniline ND ug/kg 05/05/20 12:03 99-09-2 v104/30/20 16:5420802211
4-Nitroaniline ND ug/kg 05/05/20 12:03 100-01-6 v104/30/20 16:548332061
Nitrobenzene ND ug/kg 05/05/20 12:03 98-95-3 v104/30/20 16:5441699.4 1
2-Nitrophenol ND ug/kg 05/05/20 12:03 88-75-504/30/20 16:544161291
4-Nitrophenol ND ug/kg 05/05/20 12:03 100-02-704/30/20 16:5420806641
N-Nitrosodimethylamine ND ug/kg 05/05/20 12:03 62-75-9 v104/30/20 16:544161171
N-Nitroso-di-n-propylamine ND ug/kg 05/05/20 12:03 621-64-704/30/20 16:544161171
N-Nitrosodiphenylamine ND ug/kg 05/05/20 12:03 86-30-604/30/20 16:544161061
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/05/20 12:03 108-60-1 v204/30/20 16:544161161
Pentachlorophenol ND ug/kg 05/05/20 12:03 87-86-504/30/20 16:548331901
Phenanthrene ND ug/kg 05/05/20 12:03 85-01-804/30/20 16:544161051
Phenol ND ug/kg 05/05/20 12:03 108-95-204/30/20 16:5441699.4 1
Pyrene ND ug/kg 05/05/20 12:03 129-00-004/30/20 16:544161151
Pyridine ND ug/kg 05/05/20 12:03 110-86-1 v104/30/20 16:544161051
1,2,4-Trichlorobenzene ND ug/kg 05/05/20 12:03 120-82-104/30/20 16:5441695.4 1
2,4,5-Trichlorophenol ND ug/kg 05/05/20 12:03 95-95-404/30/20 16:544161081
2,4,6-Trichlorophenol ND ug/kg 05/05/20 12:03 88-06-204/30/20 16:544161051
Surrogates
Nitrobenzene-d5 (S)82 %05/05/20 12:03 4165-60-004/30/20 16:5423-110 1
2-Fluorobiphenyl (S)51 %05/05/20 12:03 321-60-804/30/20 16:5430-110 1
Terphenyl-d14 (S)93 %05/05/20 12:03 1718-51-004/30/20 16:5428-110 1
Phenol-d6 (S)83 %05/05/20 12:03 13127-88-304/30/20 16:5422-110 1
2-Fluorophenol (S)92 %05/05/20 12:03 367-12-404/30/20 16:5413-110 1
2,4,6-Tribromophenol (S)86 %05/05/20 12:03 118-79-604/30/20 16:5427-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone 14.0J ug/kg 04/30/20 19:49 67-64-104/30/20 14:3294.3 8.9 1
Benzene ND ug/kg 04/30/20 19:49 71-43-204/30/20 14:324.7 0.85 1
Bromobenzene ND ug/kg 04/30/20 19:49 108-86-104/30/20 14:324.7 1.3 1
Bromochloromethane ND ug/kg 04/30/20 19:49 74-97-504/30/20 14:324.7 1.2 1
Bromodichloromethane ND ug/kg 04/30/20 19:49 75-27-404/30/20 14:324.7 0.92 1
Bromoform ND ug/kg 04/30/20 19:49 75-25-204/30/20 14:324.7 2.3 1
Bromomethane ND ug/kg 04/30/20 19:49 74-83-9 IH04/30/20 14:329.4 2.2 1
2-Butanone (MEK)ND ug/kg 04/30/20 19:49 78-93-304/30/20 14:3294.3 11.2 1
n-Butylbenzene ND ug/kg 04/30/20 19:49 104-51-804/30/20 14:324.7 2.7 1
sec-Butylbenzene ND ug/kg 04/30/20 19:49 135-98-804/30/20 14:324.7 2.0 1
tert-Butylbenzene ND ug/kg 04/30/20 19:49 98-06-604/30/20 14:324.7 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-3 (0-2)Lab ID:92475481003 Collected:04/28/20 10:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Carbon tetrachloride ND ug/kg 04/30/20 19:49 56-23-504/30/20 14:324.7 0.90 1
Chlorobenzene ND ug/kg 04/30/20 19:49 108-90-704/30/20 14:324.7 0.91 1
Chloroethane ND ug/kg 04/30/20 19:49 75-00-304/30/20 14:329.4 2.0 1
Chloroform ND ug/kg 04/30/20 19:49 67-66-304/30/20 14:324.7 1.0 1
Chloromethane ND ug/kg 04/30/20 19:49 74-87-304/30/20 14:329.4 3.1 1
2-Chlorotoluene ND ug/kg 04/30/20 19:49 95-49-804/30/20 14:324.7 1.4 1
4-Chlorotoluene ND ug/kg 04/30/20 19:49 106-43-404/30/20 14:324.7 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/30/20 19:49 96-12-804/30/20 14:324.7 2.4 1
Dibromochloromethane ND ug/kg 04/30/20 19:49 124-48-104/30/20 14:324.7 2.4 1
1,2-Dibromoethane (EDB)ND ug/kg 04/30/20 19:49 106-93-404/30/20 14:324.7 1.1 1
Dibromomethane ND ug/kg 04/30/20 19:49 74-95-304/30/20 14:324.7 1.4 1
1,2-Dichlorobenzene ND ug/kg 04/30/20 19:49 95-50-104/30/20 14:324.7 1.7 1
1,3-Dichlorobenzene ND ug/kg 04/30/20 19:49 541-73-104/30/20 14:324.7 1.7 1
1,4-Dichlorobenzene ND ug/kg 04/30/20 19:49 106-46-704/30/20 14:324.7 1.6 1
Dichlorodifluoromethane ND ug/kg 04/30/20 19:49 75-71-804/30/20 14:329.4 3.9 1
1,1-Dichloroethane ND ug/kg 04/30/20 19:49 75-34-304/30/20 14:324.7 0.69 1
1,2-Dichloroethane ND ug/kg 04/30/20 19:49 107-06-204/30/20 14:324.7 0.94 1
1,1-Dichloroethene ND ug/kg 04/30/20 19:49 75-35-404/30/20 14:324.7 1.1 1
cis-1,2-Dichloroethene ND ug/kg 04/30/20 19:49 156-59-204/30/20 14:324.7 0.82 1
trans-1,2-Dichloroethene ND ug/kg 04/30/20 19:49 156-60-504/30/20 14:324.7 0.92 1
1,2-Dichloropropane ND ug/kg 04/30/20 19:49 78-87-504/30/20 14:324.7 1.8 1
1,3-Dichloropropane ND ug/kg 04/30/20 19:49 142-28-904/30/20 14:324.7 1.8 1
2,2-Dichloropropane ND ug/kg 04/30/20 19:49 594-20-704/30/20 14:324.7 0.47 1
1,1-Dichloropropene ND ug/kg 04/30/20 19:49 563-58-604/30/20 14:324.7 2.0 1
cis-1,3-Dichloropropene ND ug/kg 04/30/20 19:49 10061-01-504/30/20 14:324.7 2.1 1
trans-1,3-Dichloropropene ND ug/kg 04/30/20 19:49 10061-02-604/30/20 14:324.7 0.82 1
Diisopropyl ether ND ug/kg 04/30/20 19:49 108-20-304/30/20 14:324.7 2.7 1
Ethylbenzene 1.9J ug/kg 04/30/20 19:49 100-41-404/30/20 14:324.7 1.0 1
Hexachloro-1,3-butadiene ND ug/kg 04/30/20 19:49 87-68-304/30/20 14:324.7 2.3 1
2-Hexanone ND ug/kg 04/30/20 19:49 591-78-604/30/20 14:3247.1 4.9 1
Isopropylbenzene (Cumene)ND ug/kg 04/30/20 19:49 98-82-804/30/20 14:324.7 1.4 1
p-Isopropyltoluene ND ug/kg 04/30/20 19:49 99-87-604/30/20 14:324.7 2.3 1
Methylene Chloride ND ug/kg 04/30/20 19:49 75-09-204/30/20 14:3218.9 5.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/30/20 19:49 108-10-104/30/20 14:3247.1 3.5 1
Methyl-tert-butyl ether ND ug/kg 04/30/20 19:49 1634-04-404/30/20 14:324.7 2.7 1
Naphthalene ND ug/kg 04/30/20 19:49 91-20-304/30/20 14:324.7 4.0 1
n-Propylbenzene ND ug/kg 04/30/20 19:49 103-65-104/30/20 14:324.7 1.6 1
Styrene ND ug/kg 04/30/20 19:49 100-42-504/30/20 14:324.7 1.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/30/20 19:49 630-20-604/30/20 14:324.7 1.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/30/20 19:49 79-34-504/30/20 14:324.7 1.6 1
Tetrachloroethene ND ug/kg 04/30/20 19:49 127-18-404/30/20 14:324.7 1.5 1
Toluene ND ug/kg 04/30/20 19:49 108-88-304/30/20 14:324.7 1.5 1
1,2,3-Trichlorobenzene ND ug/kg 04/30/20 19:49 87-61-604/30/20 14:324.7 3.4 1
1,2,4-Trichlorobenzene ND ug/kg 04/30/20 19:49 120-82-104/30/20 14:324.7 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-3 (0-2)Lab ID:92475481003 Collected:04/28/20 10:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
1,1,1-Trichloroethane ND ug/kg 04/30/20 19:49 71-55-604/30/20 14:324.7 0.82 1
1,1,2-Trichloroethane ND ug/kg 04/30/20 19:49 79-00-504/30/20 14:324.7 1.1 1
Trichloroethene ND ug/kg 04/30/20 19:49 79-01-604/30/20 14:324.7 1.2 1
Trichlorofluoromethane ND ug/kg 04/30/20 19:49 75-69-404/30/20 14:324.7 1.1 1
1,2,3-Trichloropropane ND ug/kg 04/30/20 19:49 96-18-404/30/20 14:324.7 1.6 1
1,2,4-Trimethylbenzene ND ug/kg 04/30/20 19:49 95-63-604/30/20 14:324.7 1.8 1
1,3,5-Trimethylbenzene ND ug/kg 04/30/20 19:49 108-67-804/30/20 14:324.7 1.6 1
Vinyl acetate ND ug/kg 04/30/20 19:49 108-05-404/30/20 14:3247.1 15.4 1
Vinyl chloride ND ug/kg 04/30/20 19:49 75-01-404/30/20 14:329.4 1.8 1
Xylene (Total)4.9J ug/kg 04/30/20 19:49 1330-20-704/30/20 14:329.4 3.3 1
m&p-Xylene 7.2J ug/kg 04/30/20 19:49 179601-23-104/30/20 14:329.4 2.2 1
o-Xylene 4.9 ug/kg 04/30/20 19:49 95-47-604/30/20 14:324.7 1.1 1
Surrogates
Toluene-d8 (S)102 %04/30/20 19:49 2037-26-504/30/20 14:3270-130 1
4-Bromofluorobenzene (S)102 %04/30/20 19:49 460-00-404/30/20 14:3270-130 1
1,2-Dichloroethane-d4 (S)105 %04/30/20 19:49 17060-07-004/30/20 14:3270-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.4 %04/29/20 17:060.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 71.5 %05/05/20 10:5805/05/20 10:501
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.377J mg/kg 05/04/20 11:37 18540-29-9 J05/02/20 11:141.40 0.356 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-4 (0-2)Lab ID:92475481004 Collected:04/28/20 08:55 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8081 GCS Pesticides
Aldrin ND ug/kg 05/06/20 01:42 309-00-204/29/20 18:495.4 1.9 2
alpha-BHC ND ug/kg 05/06/20 01:42 319-84-604/29/20 18:495.4 1.9 2
beta-BHC ND ug/kg 05/06/20 01:42 319-85-704/29/20 18:495.4 1.9 2
delta-BHC ND ug/kg 05/06/20 01:42 319-86-804/29/20 18:495.4 1.9 2
gamma-BHC (Lindane)ND ug/kg 05/06/20 01:42 58-89-904/29/20 18:495.4 2.2 2
Chlordane (Technical)ND ug/kg 05/06/20 01:42 57-74-904/29/20 18:4918.8 18.8 2
4,4'-DDD ND ug/kg 05/06/20 01:42 72-54-804/29/20 18:495.4 2.2 2
4,4'-DDE ND ug/kg 05/06/20 01:42 72-55-904/29/20 18:495.4 2.1 2
4,4'-DDT ND ug/kg 05/06/20 01:42 50-29-304/29/20 18:495.4 1.9 2
Dieldrin ND ug/kg 05/06/20 01:42 60-57-104/29/20 18:495.4 2.2 2
Endosulfan I ND ug/kg 05/06/20 01:42 959-98-804/29/20 18:495.4 2.2 2
Endosulfan II ND ug/kg 05/06/20 01:42 33213-65-904/29/20 18:495.4 2.2 2
Endosulfan sulfate ND ug/kg 05/06/20 01:42 1031-07-804/29/20 18:495.4 2.3 2
Endrin ND ug/kg 05/06/20 01:42 72-20-804/29/20 18:495.4 2.2 2
Endrin aldehyde ND ug/kg 05/06/20 01:42 7421-93-404/29/20 18:495.4 2.1 2
Endrin ketone ND ug/kg 05/06/20 01:42 53494-70-504/29/20 18:495.4 2.8 2
Heptachlor ND ug/kg 05/06/20 01:42 76-44-804/29/20 18:495.4 1.8 2
Heptachlor epoxide ND ug/kg 05/06/20 01:42 1024-57-304/29/20 18:495.4 1.8 2
Hexachlorobenzene ND ug/kg 05/06/20 01:42 118-74-104/29/20 18:495.4 1.8 2
Methoxychlor ND ug/kg 05/06/20 01:42 72-43-504/29/20 18:4913.4 7.0 2
Mirex ND ug/kg 05/06/20 01:42 2385-85-504/29/20 18:4913.4 6.5 2
Toxaphene ND ug/kg 05/06/20 01:42 8001-35-204/29/20 18:4918.8 18.8 2
Surrogates
Tetrachloro-m-xylene (S)54 %05/06/20 01:42 877-09-8 D304/29/20 18:4915-130 2
Decachlorobiphenyl (S)33 %05/06/20 01:42 2051-24-304/29/20 18:4910-130 2
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 1.87 mg/kg 05/02/20 15:46 7440-38-205/02/20 06:481.38 0.584 5
Barium 74.9 mg/kg 05/02/20 15:46 7440-39-305/02/20 06:483.46 1.73 5
Cadmium ND mg/kg 05/02/20 15:46 7440-43-905/02/20 06:481.38 0.561 5
Chromium 30.3 mg/kg 05/02/20 15:46 7440-47-305/02/20 06:486.91 3.10 5
Lead 24.3 mg/kg 05/02/20 15:46 7439-92-105/02/20 06:482.77 1.38 5
Selenium ND mg/kg 05/02/20 15:46 7782-49-205/02/20 06:483.46 1.40 5
Silver ND mg/kg 05/02/20 15:46 7440-22-405/02/20 06:480.691 0.295 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0350J mg/kg 05/04/20 20:02 7439-97-6 J05/04/20 15:060.0553 0.0249 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/05/20 12:30 83-32-904/30/20 16:544581181
Acenaphthylene ND ug/kg 05/05/20 12:30 208-96-804/30/20 16:544581081
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-4 (0-2)Lab ID:92475481004 Collected:04/28/20 08:55 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Aniline ND ug/kg 05/05/20 12:30 62-53-3 v104/30/20 16:544581031
Anthracene ND ug/kg 05/05/20 12:30 120-12-704/30/20 16:544581191
Benzo(a)anthracene ND ug/kg 05/05/20 12:30 56-55-304/30/20 16:544581461
Benzo(a)pyrene ND ug/kg 05/05/20 12:30 50-32-804/30/20 16:544581981
Benzo(b)fluoranthene ND ug/kg 05/05/20 12:30 205-99-204/30/20 16:544581851
Benzo(g,h,i)perylene ND ug/kg 05/05/20 12:30 191-24-204/30/20 16:544581791
Benzo(k)fluoranthene ND ug/kg 05/05/20 12:30 207-08-904/30/20 16:544581931
Benzoic Acid ND ug/kg 05/05/20 12:30 65-85-004/30/20 16:5422904941
Benzyl alcohol ND ug/kg 05/05/20 12:30 100-51-604/30/20 16:549162431
4-Bromophenylphenyl ether ND ug/kg 05/05/20 12:30 101-55-304/30/20 16:544581201
Butylbenzylphthalate ND ug/kg 05/05/20 12:30 85-68-704/30/20 16:544581221
4-Chloro-3-methylphenol ND ug/kg 05/05/20 12:30 59-50-704/30/20 16:549162791
4-Chloroaniline ND ug/kg 05/05/20 12:30 106-47-804/30/20 16:549162801
bis(2-Chloroethoxy)methane ND ug/kg 05/05/20 12:30 111-91-104/30/20 16:544581221
bis(2-Chloroethyl) ether ND ug/kg 05/05/20 12:30 111-44-404/30/20 16:5445897.3 1
2-Chloronaphthalene ND ug/kg 05/05/20 12:30 91-58-704/30/20 16:544581021
2-Chlorophenol ND ug/kg 05/05/20 12:30 95-57-804/30/20 16:544581071
4-Chlorophenylphenyl ether ND ug/kg 05/05/20 12:30 7005-72-304/30/20 16:544581191
Chrysene ND ug/kg 05/05/20 12:30 218-01-904/30/20 16:544581331
Dibenz(a,h)anthracene ND ug/kg 05/05/20 12:30 53-70-304/30/20 16:544581831
Dibenzofuran ND ug/kg 05/05/20 12:30 132-64-904/30/20 16:544581141
1,2-Dichlorobenzene ND ug/kg 05/05/20 12:30 95-50-104/30/20 16:5445899.1 1
1,3-Dichlorobenzene ND ug/kg 05/05/20 12:30 541-73-104/30/20 16:544581031
1,4-Dichlorobenzene ND ug/kg 05/05/20 12:30 106-46-704/30/20 16:544581011
3,3'-Dichlorobenzidine ND ug/kg 05/05/20 12:30 91-94-104/30/20 16:549163191
2,4-Dichlorophenol ND ug/kg 05/05/20 12:30 120-83-204/30/20 16:544581511
Diethylphthalate ND ug/kg 05/05/20 12:30 84-66-204/30/20 16:5445899.4 1
2,4-Dimethylphenol ND ug/kg 05/05/20 12:30 105-67-904/30/20 16:544581141
Dimethylphthalate ND ug/kg 05/05/20 12:30 131-11-304/30/20 16:544581041
Di-n-butylphthalate ND ug/kg 05/05/20 12:30 84-74-204/30/20 16:544581131
4,6-Dinitro-2-methylphenol ND ug/kg 05/05/20 12:30 534-52-104/30/20 16:549167381
2,4-Dinitrophenol ND ug/kg 05/05/20 12:30 51-28-504/30/20 16:54229014601
2,4-Dinitrotoluene ND ug/kg 05/05/20 12:30 121-14-204/30/20 16:544581211
2,6-Dinitrotoluene ND ug/kg 05/05/20 12:30 606-20-204/30/20 16:544581201
Di-n-octylphthalate ND ug/kg 05/05/20 12:30 117-84-004/30/20 16:544582611
bis(2-Ethylhexyl)phthalate ND ug/kg 05/05/20 12:30 117-81-704/30/20 16:544581501
Fluoranthene ND ug/kg 05/05/20 12:30 206-44-004/30/20 16:544581381
Fluorene ND ug/kg 05/05/20 12:30 86-73-704/30/20 16:544581231
Hexachloro-1,3-butadiene ND ug/kg 05/05/20 12:30 87-68-304/30/20 16:544581111
Hexachlorobenzene ND ug/kg 05/05/20 12:30 118-74-104/30/20 16:544581161
Hexachlorocyclopentadiene ND ug/kg 05/05/20 12:30 77-47-4 v204/30/20 16:544581831
Hexachloroethane ND ug/kg 05/05/20 12:30 67-72-104/30/20 16:544581041
Indeno(1,2,3-cd)pyrene ND ug/kg 05/05/20 12:30 193-39-504/30/20 16:544582101
Isophorone ND ug/kg 05/05/20 12:30 78-59-104/30/20 16:5445899.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-4 (0-2)Lab ID:92475481004 Collected:04/28/20 08:55 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1-Methylnaphthalene ND ug/kg 05/05/20 12:30 90-12-004/30/20 16:544581221
2-Methylnaphthalene ND ug/kg 05/05/20 12:30 91-57-604/30/20 16:544581171
2-Methylphenol(o-Cresol)ND ug/kg 05/05/20 12:30 95-48-704/30/20 16:544581011
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/05/20 12:30 15831-10-404/30/20 16:544581151
Naphthalene ND ug/kg 05/05/20 12:30 91-20-304/30/20 16:544581101
2-Nitroaniline ND ug/kg 05/05/20 12:30 88-74-404/30/20 16:5422902301
3-Nitroaniline ND ug/kg 05/05/20 12:30 99-09-2 v104/30/20 16:5422902431
4-Nitroaniline ND ug/kg 05/05/20 12:30 100-01-6 v104/30/20 16:549162261
Nitrobenzene ND ug/kg 05/05/20 12:30 98-95-3 v104/30/20 16:544581091
2-Nitrophenol ND ug/kg 05/05/20 12:30 88-75-504/30/20 16:544581421
4-Nitrophenol ND ug/kg 05/05/20 12:30 100-02-704/30/20 16:5422907301
N-Nitrosodimethylamine ND ug/kg 05/05/20 12:30 62-75-9 v104/30/20 16:544581291
N-Nitroso-di-n-propylamine ND ug/kg 05/05/20 12:30 621-64-704/30/20 16:544581281
N-Nitrosodiphenylamine ND ug/kg 05/05/20 12:30 86-30-604/30/20 16:544581171
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/05/20 12:30 108-60-1 v204/30/20 16:544581271
Pentachlorophenol ND ug/kg 05/05/20 12:30 87-86-504/30/20 16:549162101
Phenanthrene ND ug/kg 05/05/20 12:30 85-01-804/30/20 16:544581151
Phenol ND ug/kg 05/05/20 12:30 108-95-204/30/20 16:544581091
Pyrene ND ug/kg 05/05/20 12:30 129-00-004/30/20 16:544581261
Pyridine ND ug/kg 05/05/20 12:30 110-86-1 v104/30/20 16:544581161
1,2,4-Trichlorobenzene ND ug/kg 05/05/20 12:30 120-82-104/30/20 16:544581051
2,4,5-Trichlorophenol ND ug/kg 05/05/20 12:30 95-95-404/30/20 16:544581191
2,4,6-Trichlorophenol ND ug/kg 05/05/20 12:30 88-06-204/30/20 16:544581151
Surrogates
Nitrobenzene-d5 (S)83 %05/05/20 12:30 4165-60-004/30/20 16:5423-110 1
2-Fluorobiphenyl (S)70 %05/05/20 12:30 321-60-804/30/20 16:5430-110 1
Terphenyl-d14 (S)91 %05/05/20 12:30 1718-51-004/30/20 16:5428-110 1
Phenol-d6 (S)89 %05/05/20 12:30 13127-88-304/30/20 16:5422-110 1
2-Fluorophenol (S)99 %05/05/20 12:30 367-12-404/30/20 16:5413-110 1
2,4,6-Tribromophenol (S)82 %05/05/20 12:30 118-79-604/30/20 16:5427-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone ND ug/kg 04/30/20 20:14 67-64-104/30/20 14:3298.9 9.3 1
Benzene ND ug/kg 04/30/20 20:14 71-43-204/30/20 14:324.9 0.89 1
Bromobenzene ND ug/kg 04/30/20 20:14 108-86-104/30/20 14:324.9 1.3 1
Bromochloromethane ND ug/kg 04/30/20 20:14 74-97-504/30/20 14:324.9 1.2 1
Bromodichloromethane ND ug/kg 04/30/20 20:14 75-27-404/30/20 14:324.9 0.97 1
Bromoform ND ug/kg 04/30/20 20:14 75-25-204/30/20 14:324.9 2.4 1
Bromomethane ND ug/kg 04/30/20 20:14 74-83-9 IH04/30/20 14:329.9 2.3 1
2-Butanone (MEK)ND ug/kg 04/30/20 20:14 78-93-304/30/20 14:3298.9 11.8 1
n-Butylbenzene ND ug/kg 04/30/20 20:14 104-51-804/30/20 14:324.9 2.8 1
sec-Butylbenzene ND ug/kg 04/30/20 20:14 135-98-804/30/20 14:324.9 2.1 1
tert-Butylbenzene ND ug/kg 04/30/20 20:14 98-06-604/30/20 14:324.9 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-4 (0-2)Lab ID:92475481004 Collected:04/28/20 08:55 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Carbon tetrachloride ND ug/kg 04/30/20 20:14 56-23-504/30/20 14:324.9 0.95 1
Chlorobenzene ND ug/kg 04/30/20 20:14 108-90-704/30/20 14:324.9 0.96 1
Chloroethane ND ug/kg 04/30/20 20:14 75-00-304/30/20 14:329.9 2.1 1
Chloroform ND ug/kg 04/30/20 20:14 67-66-304/30/20 14:324.9 1.0 1
Chloromethane ND ug/kg 04/30/20 20:14 74-87-304/30/20 14:329.9 3.2 1
2-Chlorotoluene ND ug/kg 04/30/20 20:14 95-49-804/30/20 14:324.9 1.5 1
4-Chlorotoluene ND ug/kg 04/30/20 20:14 106-43-404/30/20 14:324.9 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/30/20 20:14 96-12-804/30/20 14:324.9 2.5 1
Dibromochloromethane ND ug/kg 04/30/20 20:14 124-48-104/30/20 14:324.9 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 04/30/20 20:14 106-93-404/30/20 14:324.9 1.1 1
Dibromomethane ND ug/kg 04/30/20 20:14 74-95-304/30/20 14:324.9 1.5 1
1,2-Dichlorobenzene ND ug/kg 04/30/20 20:14 95-50-104/30/20 14:324.9 1.7 1
1,3-Dichlorobenzene ND ug/kg 04/30/20 20:14 541-73-104/30/20 14:324.9 1.8 1
1,4-Dichlorobenzene ND ug/kg 04/30/20 20:14 106-46-704/30/20 14:324.9 1.7 1
Dichlorodifluoromethane ND ug/kg 04/30/20 20:14 75-71-804/30/20 14:329.9 4.1 1
1,1-Dichloroethane ND ug/kg 04/30/20 20:14 75-34-304/30/20 14:324.9 0.73 1
1,2-Dichloroethane ND ug/kg 04/30/20 20:14 107-06-204/30/20 14:324.9 0.99 1
1,1-Dichloroethene ND ug/kg 04/30/20 20:14 75-35-404/30/20 14:324.9 1.1 1
cis-1,2-Dichloroethene ND ug/kg 04/30/20 20:14 156-59-204/30/20 14:324.9 0.86 1
trans-1,2-Dichloroethene ND ug/kg 04/30/20 20:14 156-60-504/30/20 14:324.9 0.97 1
1,2-Dichloropropane ND ug/kg 04/30/20 20:14 78-87-504/30/20 14:324.9 1.9 1
1,3-Dichloropropane ND ug/kg 04/30/20 20:14 142-28-904/30/20 14:324.9 1.9 1
2,2-Dichloropropane ND ug/kg 04/30/20 20:14 594-20-704/30/20 14:324.9 0.49 1
1,1-Dichloropropene ND ug/kg 04/30/20 20:14 563-58-604/30/20 14:324.9 2.1 1
cis-1,3-Dichloropropene ND ug/kg 04/30/20 20:14 10061-01-504/30/20 14:324.9 2.2 1
trans-1,3-Dichloropropene ND ug/kg 04/30/20 20:14 10061-02-604/30/20 14:324.9 0.87 1
Diisopropyl ether ND ug/kg 04/30/20 20:14 108-20-304/30/20 14:324.9 2.8 1
Ethylbenzene ND ug/kg 04/30/20 20:14 100-41-404/30/20 14:324.9 1.0 1
Hexachloro-1,3-butadiene ND ug/kg 04/30/20 20:14 87-68-304/30/20 14:324.9 2.4 1
2-Hexanone ND ug/kg 04/30/20 20:14 591-78-604/30/20 14:3249.4 5.1 1
Isopropylbenzene (Cumene)ND ug/kg 04/30/20 20:14 98-82-804/30/20 14:324.9 1.4 1
p-Isopropyltoluene ND ug/kg 04/30/20 20:14 99-87-604/30/20 14:324.9 2.4 1
Methylene Chloride ND ug/kg 04/30/20 20:14 75-09-204/30/20 14:3219.8 5.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/30/20 20:14 108-10-104/30/20 14:3249.4 3.7 1
Methyl-tert-butyl ether ND ug/kg 04/30/20 20:14 1634-04-404/30/20 14:324.9 2.8 1
Naphthalene ND ug/kg 04/30/20 20:14 91-20-304/30/20 14:324.9 4.2 1
n-Propylbenzene ND ug/kg 04/30/20 20:14 103-65-104/30/20 14:324.9 1.7 1
Styrene ND ug/kg 04/30/20 20:14 100-42-504/30/20 14:324.9 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/30/20 20:14 630-20-604/30/20 14:324.9 1.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/30/20 20:14 79-34-504/30/20 14:324.9 1.7 1
Tetrachloroethene ND ug/kg 04/30/20 20:14 127-18-404/30/20 14:324.9 1.6 1
Toluene ND ug/kg 04/30/20 20:14 108-88-304/30/20 14:324.9 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 04/30/20 20:14 87-61-604/30/20 14:324.9 3.5 1
1,2,4-Trichlorobenzene ND ug/kg 04/30/20 20:14 120-82-104/30/20 14:324.9 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-4 (0-2)Lab ID:92475481004 Collected:04/28/20 08:55 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
1,1,1-Trichloroethane ND ug/kg 04/30/20 20:14 71-55-604/30/20 14:324.9 0.86 1
1,1,2-Trichloroethane ND ug/kg 04/30/20 20:14 79-00-504/30/20 14:324.9 1.1 1
Trichloroethene ND ug/kg 04/30/20 20:14 79-01-604/30/20 14:324.9 1.3 1
Trichlorofluoromethane ND ug/kg 04/30/20 20:14 75-69-404/30/20 14:324.9 1.2 1
1,2,3-Trichloropropane ND ug/kg 04/30/20 20:14 96-18-404/30/20 14:324.9 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 04/30/20 20:14 95-63-604/30/20 14:324.9 1.9 1
1,3,5-Trimethylbenzene ND ug/kg 04/30/20 20:14 108-67-804/30/20 14:324.9 1.7 1
Vinyl acetate ND ug/kg 04/30/20 20:14 108-05-404/30/20 14:3249.4 16.1 1
Vinyl chloride ND ug/kg 04/30/20 20:14 75-01-404/30/20 14:329.9 1.9 1
Xylene (Total)ND ug/kg 04/30/20 20:14 1330-20-704/30/20 14:329.9 3.5 1
m&p-Xylene ND ug/kg 04/30/20 20:14 179601-23-104/30/20 14:329.9 2.3 1
o-Xylene ND ug/kg 04/30/20 20:14 95-47-604/30/20 14:324.9 1.2 1
Surrogates
Toluene-d8 (S)102 %04/30/20 20:14 2037-26-504/30/20 14:3270-130 1
4-Bromofluorobenzene (S)101 %04/30/20 20:14 460-00-404/30/20 14:3270-130 1
1,2-Dichloroethane-d4 (S)105 %04/30/20 20:14 17060-07-004/30/20 14:3270-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.7 %04/29/20 17:060.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 72.3 %05/05/20 10:5805/05/20 10:501
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 05/04/20 11:42 18540-29-905/02/20 11:141.38 0.353 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-DUP-1 Lab ID:92475481005 Collected:04/28/20 00:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8081B Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8081 GCS Pesticides
Aldrin ND ug/kg 05/06/20 01:57 309-00-204/29/20 18:496.5 2.4 2.5
alpha-BHC ND ug/kg 05/06/20 01:57 319-84-604/29/20 18:496.5 2.3 2.5
beta-BHC ND ug/kg 05/06/20 01:57 319-85-704/29/20 18:496.5 2.3 2.5
delta-BHC ND ug/kg 05/06/20 01:57 319-86-804/29/20 18:496.5 2.3 2.5
gamma-BHC (Lindane)ND ug/kg 05/06/20 01:57 58-89-904/29/20 18:496.5 2.7 2.5
Chlordane (Technical)ND ug/kg 05/06/20 01:57 57-74-904/29/20 18:4922.8 22.8 2.5
4,4'-DDD ND ug/kg 05/06/20 01:57 72-54-804/29/20 18:496.5 2.7 2.5
4,4'-DDE ND ug/kg 05/06/20 01:57 72-55-904/29/20 18:496.5 2.6 2.5
4,4'-DDT ND ug/kg 05/06/20 01:57 50-29-304/29/20 18:496.5 2.4 2.5
Dieldrin ND ug/kg 05/06/20 01:57 60-57-104/29/20 18:496.5 2.6 2.5
Endosulfan I ND ug/kg 05/06/20 01:57 959-98-804/29/20 18:496.5 2.6 2.5
Endosulfan II ND ug/kg 05/06/20 01:57 33213-65-904/29/20 18:496.5 2.6 2.5
Endosulfan sulfate ND ug/kg 05/06/20 01:57 1031-07-804/29/20 18:496.5 2.8 2.5
Endrin ND ug/kg 05/06/20 01:57 72-20-804/29/20 18:496.5 2.7 2.5
Endrin aldehyde ND ug/kg 05/06/20 01:57 7421-93-404/29/20 18:496.5 2.5 2.5
Endrin ketone ND ug/kg 05/06/20 01:57 53494-70-504/29/20 18:496.5 3.4 2.5
Heptachlor ND ug/kg 05/06/20 01:57 76-44-804/29/20 18:496.5 2.1 2.5
Heptachlor epoxide ND ug/kg 05/06/20 01:57 1024-57-304/29/20 18:496.5 2.2 2.5
Hexachlorobenzene ND ug/kg 05/06/20 01:57 118-74-104/29/20 18:496.5 2.1 2.5
Methoxychlor ND ug/kg 05/06/20 01:57 72-43-504/29/20 18:4916.3 8.5 2.5
Mirex ND ug/kg 05/06/20 01:57 2385-85-504/29/20 18:4916.3 7.9 2.5
Toxaphene ND ug/kg 05/06/20 01:57 8001-35-204/29/20 18:4922.8 22.8 2.5
Surrogates
Tetrachloro-m-xylene (S)64 %05/06/20 01:57 877-09-8 D304/29/20 18:4915-130 2.5
Decachlorobiphenyl (S)46 %05/06/20 01:57 2051-24-304/29/20 18:4910-130 2.5
Analytical Method: EPA 6020B Preparation Method: 3050B
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 1.71 mg/kg 05/02/20 15:50 7440-38-205/02/20 06:481.47 0.621 5
Barium 47.8 mg/kg 05/02/20 15:50 7440-39-305/02/20 06:483.68 1.84 5
Cadmium ND mg/kg 05/02/20 15:50 7440-43-905/02/20 06:481.47 0.597 5
Chromium 74.9 mg/kg 05/02/20 15:50 7440-47-305/02/20 06:487.35 3.29 5
Lead 13.7 mg/kg 05/02/20 15:50 7439-92-105/02/20 06:482.94 1.47 5
Selenium ND mg/kg 05/02/20 15:50 7782-49-205/02/20 06:483.68 1.49 5
Silver ND mg/kg 05/02/20 15:50 7440-22-405/02/20 06:480.735 0.313 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0369J mg/kg 05/04/20 20:04 7439-97-6 J05/04/20 15:060.0588 0.0265 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/05/20 12:57 83-32-904/30/20 16:544251091
Acenaphthylene ND ug/kg 05/05/20 12:57 208-96-804/30/20 16:544251011
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-DUP-1 Lab ID:92475481005 Collected:04/28/20 00:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Aniline ND ug/kg 05/05/20 12:57 62-53-304/30/20 16:5442595.5 1
Anthracene ND ug/kg 05/05/20 12:57 120-12-704/30/20 16:544251101
Benzo(a)anthracene ND ug/kg 05/05/20 12:57 56-55-304/30/20 16:544251351
Benzo(a)pyrene ND ug/kg 05/05/20 12:57 50-32-804/30/20 16:544251841
Benzo(b)fluoranthene ND ug/kg 05/05/20 12:57 205-99-204/30/20 16:544251711
Benzo(g,h,i)perylene ND ug/kg 05/05/20 12:57 191-24-204/30/20 16:544251661
Benzo(k)fluoranthene ND ug/kg 05/05/20 12:57 207-08-904/30/20 16:544251791
Benzoic Acid ND ug/kg 05/05/20 12:57 65-85-004/30/20 16:5421304591
Benzyl alcohol ND ug/kg 05/05/20 12:57 100-51-604/30/20 16:548502251
4-Bromophenylphenyl ether ND ug/kg 05/05/20 12:57 101-55-304/30/20 16:544251121
Butylbenzylphthalate ND ug/kg 05/05/20 12:57 85-68-704/30/20 16:544251131
4-Chloro-3-methylphenol ND ug/kg 05/05/20 12:57 59-50-704/30/20 16:548502591
4-Chloroaniline ND ug/kg 05/05/20 12:57 106-47-804/30/20 16:548502601
bis(2-Chloroethoxy)methane ND ug/kg 05/05/20 12:57 111-91-104/30/20 16:544251131
bis(2-Chloroethyl) ether ND ug/kg 05/05/20 12:57 111-44-404/30/20 16:5442590.3 1
2-Chloronaphthalene ND ug/kg 05/05/20 12:57 91-58-704/30/20 16:5442594.7 1
2-Chlorophenol ND ug/kg 05/05/20 12:57 95-57-804/30/20 16:5442598.9 1
4-Chlorophenylphenyl ether ND ug/kg 05/05/20 12:57 7005-72-304/30/20 16:544251101
Chrysene ND ug/kg 05/05/20 12:57 218-01-904/30/20 16:544251231
Dibenz(a,h)anthracene ND ug/kg 05/05/20 12:57 53-70-304/30/20 16:544251701
Dibenzofuran ND ug/kg 05/05/20 12:57 132-64-904/30/20 16:544251061
1,2-Dichlorobenzene ND ug/kg 05/05/20 12:57 95-50-104/30/20 16:5442592.0 1
1,3-Dichlorobenzene ND ug/kg 05/05/20 12:57 541-73-104/30/20 16:5442595.7 1
1,4-Dichlorobenzene ND ug/kg 05/05/20 12:57 106-46-704/30/20 16:5442593.5 1
3,3'-Dichlorobenzidine ND ug/kg 05/05/20 12:57 91-94-104/30/20 16:548502961
2,4-Dichlorophenol ND ug/kg 05/05/20 12:57 120-83-204/30/20 16:544251401
Diethylphthalate ND ug/kg 05/05/20 12:57 84-66-204/30/20 16:5442592.2 1
2,4-Dimethylphenol ND ug/kg 05/05/20 12:57 105-67-904/30/20 16:544251061
Dimethylphthalate ND ug/kg 05/05/20 12:57 131-11-304/30/20 16:5442596.1 1
Di-n-butylphthalate ND ug/kg 05/05/20 12:57 84-74-204/30/20 16:544251051
4,6-Dinitro-2-methylphenol ND ug/kg 05/05/20 12:57 534-52-104/30/20 16:548506851
2,4-Dinitrophenol ND ug/kg 05/05/20 12:57 51-28-504/30/20 16:54213013601
2,4-Dinitrotoluene ND ug/kg 05/05/20 12:57 121-14-204/30/20 16:544251131
2,6-Dinitrotoluene ND ug/kg 05/05/20 12:57 606-20-204/30/20 16:544251111
Di-n-octylphthalate ND ug/kg 05/05/20 12:57 117-84-004/30/20 16:544252421
bis(2-Ethylhexyl)phthalate ND ug/kg 05/05/20 12:57 117-81-704/30/20 16:544251391
Fluoranthene ND ug/kg 05/05/20 12:57 206-44-004/30/20 16:544251281
Fluorene ND ug/kg 05/05/20 12:57 86-73-704/30/20 16:544251141
Hexachloro-1,3-butadiene ND ug/kg 05/05/20 12:57 87-68-304/30/20 16:544251031
Hexachlorobenzene ND ug/kg 05/05/20 12:57 118-74-104/30/20 16:544251081
Hexachlorocyclopentadiene ND ug/kg 05/05/20 12:57 77-47-404/30/20 16:544251701
Hexachloroethane ND ug/kg 05/05/20 12:57 67-72-104/30/20 16:5442596.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 05/05/20 12:57 193-39-504/30/20 16:544251951
Isophorone ND ug/kg 05/05/20 12:57 78-59-104/30/20 16:5442592.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-DUP-1 Lab ID:92475481005 Collected:04/28/20 00:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1-Methylnaphthalene ND ug/kg 05/05/20 12:57 90-12-004/30/20 16:544251131
2-Methylnaphthalene ND ug/kg 05/05/20 12:57 91-57-604/30/20 16:544251081
2-Methylphenol(o-Cresol)ND ug/kg 05/05/20 12:57 95-48-704/30/20 16:5442594.2 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/05/20 12:57 15831-10-404/30/20 16:544251071
Naphthalene ND ug/kg 05/05/20 12:57 91-20-304/30/20 16:544251021
2-Nitroaniline ND ug/kg 05/05/20 12:57 88-74-404/30/20 16:5421302141
3-Nitroaniline ND ug/kg 05/05/20 12:57 99-09-204/30/20 16:5421302251
4-Nitroaniline ND ug/kg 05/05/20 12:57 100-01-604/30/20 16:548502101
Nitrobenzene ND ug/kg 05/05/20 12:57 98-95-304/30/20 16:544251021
2-Nitrophenol ND ug/kg 05/05/20 12:57 88-75-504/30/20 16:544251311
4-Nitrophenol ND ug/kg 05/05/20 12:57 100-02-704/30/20 16:5421306781
N-Nitrosodimethylamine ND ug/kg 05/05/20 12:57 62-75-904/30/20 16:544251201
N-Nitroso-di-n-propylamine ND ug/kg 05/05/20 12:57 621-64-704/30/20 16:544251191
N-Nitrosodiphenylamine ND ug/kg 05/05/20 12:57 86-30-604/30/20 16:544251081
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/05/20 12:57 108-60-104/30/20 16:544251181
Pentachlorophenol ND ug/kg 05/05/20 12:57 87-86-504/30/20 16:548501951
Phenanthrene ND ug/kg 05/05/20 12:57 85-01-804/30/20 16:544251071
Phenol ND ug/kg 05/05/20 12:57 108-95-204/30/20 16:544251021
Pyrene ND ug/kg 05/05/20 12:57 129-00-004/30/20 16:544251171
Pyridine ND ug/kg 05/05/20 12:57 110-86-104/30/20 16:544251081
1,2,4-Trichlorobenzene ND ug/kg 05/05/20 12:57 120-82-104/30/20 16:5442597.4 1
2,4,5-Trichlorophenol ND ug/kg 05/05/20 12:57 95-95-404/30/20 16:544251101
2,4,6-Trichlorophenol ND ug/kg 05/05/20 12:57 88-06-204/30/20 16:544251071
Surrogates
Nitrobenzene-d5 (S)81 %05/05/20 12:57 4165-60-004/30/20 16:5423-110 1
2-Fluorobiphenyl (S)53 %05/05/20 12:57 321-60-804/30/20 16:5430-110 1
Terphenyl-d14 (S)63 %05/05/20 12:57 1718-51-004/30/20 16:5428-110 1
Phenol-d6 (S)83 %05/05/20 12:57 13127-88-304/30/20 16:5422-110 1
2-Fluorophenol (S)89 %05/05/20 12:57 367-12-404/30/20 16:5413-110 1
2,4,6-Tribromophenol (S)82 %05/05/20 12:57 118-79-604/30/20 16:5427-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Acetone ND ug/kg 04/30/20 20:38 67-64-104/30/20 14:321019.6 1
Benzene ND ug/kg 04/30/20 20:38 71-43-204/30/20 14:325.1 0.91 1
Bromobenzene ND ug/kg 04/30/20 20:38 108-86-104/30/20 14:325.1 1.4 1
Bromochloromethane ND ug/kg 04/30/20 20:38 74-97-504/30/20 14:325.1 1.2 1
Bromodichloromethane ND ug/kg 04/30/20 20:38 75-27-404/30/20 14:325.1 0.99 1
Bromoform ND ug/kg 04/30/20 20:38 75-25-204/30/20 14:325.1 2.5 1
Bromomethane ND ug/kg 04/30/20 20:38 74-83-9 IH04/30/20 14:3210.1 2.4 1
2-Butanone (MEK)ND ug/kg 04/30/20 20:38 78-93-304/30/20 14:3210112.1 1
n-Butylbenzene ND ug/kg 04/30/20 20:38 104-51-804/30/20 14:325.1 2.9 1
sec-Butylbenzene ND ug/kg 04/30/20 20:38 135-98-804/30/20 14:325.1 2.1 1
tert-Butylbenzene ND ug/kg 04/30/20 20:38 98-06-604/30/20 14:325.1 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-DUP-1 Lab ID:92475481005 Collected:04/28/20 00:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
Carbon tetrachloride ND ug/kg 04/30/20 20:38 56-23-504/30/20 14:325.1 0.97 1
Chlorobenzene ND ug/kg 04/30/20 20:38 108-90-704/30/20 14:325.1 0.98 1
Chloroethane ND ug/kg 04/30/20 20:38 75-00-304/30/20 14:3210.1 2.1 1
Chloroform ND ug/kg 04/30/20 20:38 67-66-304/30/20 14:325.1 1.1 1
Chloromethane ND ug/kg 04/30/20 20:38 74-87-304/30/20 14:3210.1 3.3 1
2-Chlorotoluene ND ug/kg 04/30/20 20:38 95-49-804/30/20 14:325.1 1.5 1
4-Chlorotoluene ND ug/kg 04/30/20 20:38 106-43-404/30/20 14:325.1 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/30/20 20:38 96-12-804/30/20 14:325.1 2.6 1
Dibromochloromethane ND ug/kg 04/30/20 20:38 124-48-104/30/20 14:325.1 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 04/30/20 20:38 106-93-404/30/20 14:325.1 1.1 1
Dibromomethane ND ug/kg 04/30/20 20:38 74-95-304/30/20 14:325.1 1.5 1
1,2-Dichlorobenzene ND ug/kg 04/30/20 20:38 95-50-104/30/20 14:325.1 1.8 1
1,3-Dichlorobenzene ND ug/kg 04/30/20 20:38 541-73-104/30/20 14:325.1 1.8 1
1,4-Dichlorobenzene ND ug/kg 04/30/20 20:38 106-46-704/30/20 14:325.1 1.8 1
Dichlorodifluoromethane ND ug/kg 04/30/20 20:38 75-71-804/30/20 14:3210.1 4.2 1
1,1-Dichloroethane ND ug/kg 04/30/20 20:38 75-34-304/30/20 14:325.1 0.74 1
1,2-Dichloroethane ND ug/kg 04/30/20 20:38 107-06-204/30/20 14:325.1 1.0 1
1,1-Dichloroethene ND ug/kg 04/30/20 20:38 75-35-404/30/20 14:325.1 1.2 1
cis-1,2-Dichloroethene ND ug/kg 04/30/20 20:38 156-59-204/30/20 14:325.1 0.88 1
trans-1,2-Dichloroethene ND ug/kg 04/30/20 20:38 156-60-504/30/20 14:325.1 0.99 1
1,2-Dichloropropane ND ug/kg 04/30/20 20:38 78-87-504/30/20 14:325.1 1.9 1
1,3-Dichloropropane ND ug/kg 04/30/20 20:38 142-28-904/30/20 14:325.1 1.9 1
2,2-Dichloropropane ND ug/kg 04/30/20 20:38 594-20-704/30/20 14:325.1 0.50 1
1,1-Dichloropropene ND ug/kg 04/30/20 20:38 563-58-604/30/20 14:325.1 2.1 1
cis-1,3-Dichloropropene ND ug/kg 04/30/20 20:38 10061-01-504/30/20 14:325.1 2.3 1
trans-1,3-Dichloropropene ND ug/kg 04/30/20 20:38 10061-02-604/30/20 14:325.1 0.89 1
Diisopropyl ether ND ug/kg 04/30/20 20:38 108-20-304/30/20 14:325.1 2.9 1
Ethylbenzene ND ug/kg 04/30/20 20:38 100-41-404/30/20 14:325.1 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/30/20 20:38 87-68-304/30/20 14:325.1 2.5 1
2-Hexanone ND ug/kg 04/30/20 20:38 591-78-604/30/20 14:3250.7 5.2 1
Isopropylbenzene (Cumene)ND ug/kg 04/30/20 20:38 98-82-804/30/20 14:325.1 1.5 1
p-Isopropyltoluene ND ug/kg 04/30/20 20:38 99-87-604/30/20 14:325.1 2.4 1
Methylene Chloride ND ug/kg 04/30/20 20:38 75-09-204/30/20 14:3220.3 6.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/30/20 20:38 108-10-104/30/20 14:3250.7 3.8 1
Methyl-tert-butyl ether ND ug/kg 04/30/20 20:38 1634-04-404/30/20 14:325.1 2.9 1
Naphthalene ND ug/kg 04/30/20 20:38 91-20-304/30/20 14:325.1 4.3 1
n-Propylbenzene ND ug/kg 04/30/20 20:38 103-65-104/30/20 14:325.1 1.7 1
Styrene ND ug/kg 04/30/20 20:38 100-42-504/30/20 14:325.1 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/30/20 20:38 630-20-604/30/20 14:325.1 1.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/30/20 20:38 79-34-504/30/20 14:325.1 1.8 1
Tetrachloroethene ND ug/kg 04/30/20 20:38 127-18-404/30/20 14:325.1 1.6 1
Toluene ND ug/kg 04/30/20 20:38 108-88-304/30/20 14:325.1 1.6 1
1,2,3-Trichlorobenzene ND ug/kg 04/30/20 20:38 87-61-604/30/20 14:325.1 3.6 1
1,2,4-Trichlorobenzene ND ug/kg 04/30/20 20:38 120-82-104/30/20 14:325.1 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-DUP-1 Lab ID:92475481005 Collected:04/28/20 00:00 Received:04/29/20 13:13 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Pace Analytical Services - Charlotte
8260D/5035A Volatile Organics
1,1,1-Trichloroethane ND ug/kg 04/30/20 20:38 71-55-604/30/20 14:325.1 0.88 1
1,1,2-Trichloroethane ND ug/kg 04/30/20 20:38 79-00-504/30/20 14:325.1 1.1 1
Trichloroethene ND ug/kg 04/30/20 20:38 79-01-604/30/20 14:325.1 1.3 1
Trichlorofluoromethane ND ug/kg 04/30/20 20:38 75-69-404/30/20 14:325.1 1.2 1
1,2,3-Trichloropropane ND ug/kg 04/30/20 20:38 96-18-404/30/20 14:325.1 1.7 1
1,2,4-Trimethylbenzene ND ug/kg 04/30/20 20:38 95-63-604/30/20 14:325.1 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/30/20 20:38 108-67-804/30/20 14:325.1 1.7 1
Vinyl acetate ND ug/kg 04/30/20 20:38 108-05-404/30/20 14:3250.7 16.5 1
Vinyl chloride ND ug/kg 04/30/20 20:38 75-01-404/30/20 14:3210.1 1.9 1
Xylene (Total)ND ug/kg 04/30/20 20:38 1330-20-704/30/20 14:3210.1 3.5 1
m&p-Xylene ND ug/kg 04/30/20 20:38 179601-23-104/30/20 14:3210.1 2.4 1
o-Xylene ND ug/kg 04/30/20 20:38 95-47-604/30/20 14:325.1 1.2 1
Surrogates
Toluene-d8 (S)103 %04/30/20 20:38 2037-26-504/30/20 14:3270-130 1
4-Bromofluorobenzene (S)101 %04/30/20 20:38 460-00-404/30/20 14:3270-130 1
1,2-Dichloroethane-d4 (S)102 %04/30/20 20:38 17060-07-004/30/20 14:3270-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.4 %04/29/20 17:090.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 68.0 %05/05/20 14:3505/05/20 14:261
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 05/04/20 11:48 18540-29-905/02/20 11:141.47 0.375 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-TRIP BLANK Lab ID:92475481006 Collected:04/28/20 00:00 Received:04/29/20 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 05/04/20 15:59 67-64-125.0 6.2 1
Benzene ND ug/L 05/04/20 15:59 71-43-21.0 0.15 1
Bromobenzene ND ug/L 05/04/20 15:59 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 05/04/20 15:59 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 05/04/20 15:59 75-27-41.0 0.26 1
Bromoform ND ug/L 05/04/20 15:59 75-25-21.0 0.62 1
Bromomethane ND ug/L 05/04/20 15:59 74-83-9 IH,L1,
v12.0 0.62 1
2-Butanone (MEK)ND ug/L 05/04/20 15:59 78-93-35.0 3.3 1
n-Butylbenzene ND ug/L 05/04/20 15:59 104-51-81.0 0.23 1
sec-Butylbenzene ND ug/L 05/04/20 15:59 135-98-81.0 0.20 1
tert-Butylbenzene ND ug/L 05/04/20 15:59 98-06-61.0 0.23 1
Carbon tetrachloride ND ug/L 05/04/20 15:59 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 05/04/20 15:59 108-90-71.0 0.23 1
Chloroethane ND ug/L 05/04/20 15:59 75-00-31.0 0.49 1
Chloroform ND ug/L 05/04/20 15:59 67-66-35.0 2.3 1
Chloromethane ND ug/L 05/04/20 15:59 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 05/04/20 15:59 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 05/04/20 15:59 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 05/04/20 15:59 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 05/04/20 15:59 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 05/04/20 15:59 106-93-41.0 0.26 1
Dibromomethane ND ug/L 05/04/20 15:59 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 05/04/20 15:59 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 05/04/20 15:59 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 05/04/20 15:59 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 05/04/20 15:59 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 05/04/20 15:59 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 05/04/20 15:59 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 05/04/20 15:59 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 05/04/20 15:59 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 05/04/20 15:59 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 05/04/20 15:59 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 05/04/20 15:59 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 05/04/20 15:59 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 05/04/20 15:59 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 05/04/20 15:59 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 05/04/20 15:59 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 05/04/20 15:59 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 05/04/20 15:59 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 05/04/20 15:59 87-68-31.0 0.44 1
2-Hexanone ND ug/L 05/04/20 15:59 591-78-65.0 0.57 1
Isopropylbenzene (Cumene)ND ug/L 05/04/20 15:59 98-82-81.0 0.20 1
p-Isopropyltoluene ND ug/L 05/04/20 15:59 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 05/04/20 15:59 75-09-25.0 3.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
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9800 Kincey Ave. Suite 100
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Page 31 of 65
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92475481
RMR-006
Sample:FG-TRIP BLANK Lab ID:92475481006 Collected:04/28/20 00:00 Received:04/29/20 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
4-Methyl-2-pentanone (MIBK)ND ug/L 05/04/20 15:59 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 05/04/20 15:59 1634-04-41.0 0.28 1
Naphthalene ND ug/L 05/04/20 15:59 91-20-31.0 0.35 1
n-Propylbenzene ND ug/L 05/04/20 15:59 103-65-11.0 0.18 1
Styrene ND ug/L 05/04/20 15:59 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 05/04/20 15:59 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 05/04/20 15:59 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 05/04/20 15:59 127-18-41.0 0.16 1
Toluene ND ug/L 05/04/20 15:59 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 05/04/20 15:59 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 05/04/20 15:59 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 05/04/20 15:59 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 05/04/20 15:59 79-00-51.0 0.24 1
Trichloroethene ND ug/L 05/04/20 15:59 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 05/04/20 15:59 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 05/04/20 15:59 96-18-41.0 0.35 1
1,2,4-Trimethylbenzene ND ug/L 05/04/20 15:59 95-63-61.0 0.17 1
1,3,5-Trimethylbenzene ND ug/L 05/04/20 15:59 108-67-81.0 0.20 1
Vinyl acetate ND ug/L 05/04/20 15:59 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 05/04/20 15:59 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 05/04/20 15:59 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 05/04/20 15:59 179601-23-12.0 0.41 1
o-Xylene ND ug/L 05/04/20 15:59 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)99 %05/04/20 15:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %05/04/20 15:59 17060-07-070-130 1
Toluene-d8 (S)99 %05/04/20 15:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1469565
3050B
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3524055-1
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 1.00 05/02/20 14:360.422
Barium mg/kg ND 2.50 05/02/20 14:361.25
Cadmium mg/kg ND 1.00 05/02/20 14:360.406
Chromium mg/kg ND 5.00 05/02/20 14:362.24
Lead mg/kg ND 2.00 05/02/20 14:361.00
Selenium mg/kg ND 2.50 05/02/20 14:361.01
Silver mg/kg ND 0.500 05/02/20 14:360.213
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3524055-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 99.0100 99.0 80.0-120
Barium mg/kg 100100 100 80.0-120
Cadmium mg/kg 106100 106 80.0-120
Chromium mg/kg 103100 103 80.0-120
Lead mg/kg 103100 103 80.0-120
Selenium mg/kg 101100 101 80.0-120
Silver mg/kg 21.020.0 105 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3524055-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92475481001
R3524055-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 25.3 77.6 75.0-12582.2 5.67 2025.32.78 101 107
Barium mg/kg MH25.3 115 75.0-125136 13.5 2025.340.7 186 213
Cadmium mg/kg 25.3 99.9 75.0-125106 5.69 2025.3ND 126 134
Chromium mg/kg 25.3 91.1 75.0-12596.9 5.06 2025.326.3 141 149
Lead mg/kg 25.3 90.4 75.0-12584.2 4.91 2025.347.1 161 154
Selenium mg/kg 25.3 91.7 75.0-12595.8 4.37 2025.3ND 116 121
Silver mg/kg 5.05 97.5 75.0-125102 4.49 205.05ND 24.6 25.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1470231
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3524556-1
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0400 05/04/20 19:240.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3524556-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.5380.500 108 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3524556-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92475481001
R3524556-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.631 93.7 75.0-12595.4 1.69 200.6310.0464 0.638 0.649
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
539075
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2873856
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/30/20 17:251.2
1,1,1-Trichloroethane ug/kg ND 5.0 04/30/20 17:250.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/30/20 17:251.7
1,1,2-Trichloroethane ug/kg ND 5.0 04/30/20 17:251.1
1,1-Dichloroethane ug/kg ND 5.0 04/30/20 17:250.74
1,1-Dichloroethene ug/kg ND 5.0 04/30/20 17:251.2
1,1-Dichloropropene ug/kg ND 5.0 04/30/20 17:252.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 04/30/20 17:253.6
1,2,3-Trichloropropane ug/kg ND 5.0 04/30/20 17:251.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/30/20 17:252.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 04/30/20 17:252.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/30/20 17:252.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/30/20 17:251.1
1,2-Dichlorobenzene ug/kg ND 5.0 04/30/20 17:251.8
1,2-Dichloroethane ug/kg ND 5.0 04/30/20 17:251.0
1,2-Dichloropropane ug/kg ND 5.0 04/30/20 17:251.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 04/30/20 17:251.7
1,3-Dichlorobenzene ug/kg ND 5.0 04/30/20 17:251.8
1,3-Dichloropropane ug/kg ND 5.0 04/30/20 17:251.9
1,4-Dichlorobenzene ug/kg ND 5.0 04/30/20 17:251.7
2,2-Dichloropropane ug/kg ND 5.0 04/30/20 17:250.49
2-Butanone (MEK)ug/kg ND 100 04/30/20 17:2511.9
2-Chlorotoluene ug/kg ND 5.0 04/30/20 17:251.5
2-Hexanone ug/kg ND 50.0 04/30/20 17:255.2
4-Chlorotoluene ug/kg ND 5.0 04/30/20 17:251.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/30/20 17:253.7
Acetone ug/kg ND 100 04/30/20 17:259.4
Benzene ug/kg ND 5.0 04/30/20 17:250.90
Bromobenzene ug/kg ND 5.0 04/30/20 17:251.4
Bromochloromethane ug/kg ND 5.0 04/30/20 17:251.2
Bromodichloromethane ug/kg ND 5.0 04/30/20 17:250.98
Bromoform ug/kg ND 5.0 04/30/20 17:252.4
Bromomethane ug/kg ND 10.0 IH04/30/20 17:252.4
Carbon tetrachloride ug/kg ND 5.0 04/30/20 17:250.96
Chlorobenzene ug/kg ND 5.0 04/30/20 17:250.97
Chloroethane ug/kg ND 10.0 04/30/20 17:252.1
Chloroform ug/kg ND 5.0 04/30/20 17:251.1
Chloromethane ug/kg ND 10.0 04/30/20 17:253.3
cis-1,2-Dichloroethene ug/kg ND 5.0 04/30/20 17:250.87
cis-1,3-Dichloropropene ug/kg ND 5.0 04/30/20 17:252.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2873856
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 04/30/20 17:252.5
Dibromomethane ug/kg ND 5.0 04/30/20 17:251.5
Dichlorodifluoromethane ug/kg ND 10.0 04/30/20 17:254.1
Diisopropyl ether ug/kg ND 5.0 04/30/20 17:252.9
Ethylbenzene ug/kg ND 5.0 04/30/20 17:251.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 04/30/20 17:252.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/30/20 17:251.4
m&p-Xylene ug/kg ND 10.0 04/30/20 17:252.4
Methyl-tert-butyl ether ug/kg ND 5.0 04/30/20 17:252.9
Methylene Chloride ug/kg ND 20.0 04/30/20 17:255.9
n-Butylbenzene ug/kg ND 5.0 04/30/20 17:252.8
n-Propylbenzene ug/kg ND 5.0 04/30/20 17:251.7
Naphthalene ug/kg ND 5.0 04/30/20 17:254.2
o-Xylene ug/kg ND 5.0 04/30/20 17:251.2
p-Isopropyltoluene ug/kg ND 5.0 04/30/20 17:252.4
sec-Butylbenzene ug/kg ND 5.0 04/30/20 17:252.1
Styrene ug/kg ND 5.0 04/30/20 17:251.5
tert-Butylbenzene ug/kg ND 5.0 04/30/20 17:251.7
Tetrachloroethene ug/kg ND 5.0 04/30/20 17:251.6
Toluene ug/kg ND 5.0 04/30/20 17:251.6
trans-1,2-Dichloroethene ug/kg ND 5.0 04/30/20 17:250.98
trans-1,3-Dichloropropene ug/kg ND 5.0 04/30/20 17:250.88
Trichloroethene ug/kg ND 5.0 04/30/20 17:251.3
Trichlorofluoromethane ug/kg ND 5.0 04/30/20 17:251.2
Vinyl acetate ug/kg ND 50.0 04/30/20 17:2516.3
Vinyl chloride ug/kg ND 10.0 04/30/20 17:251.9
Xylene (Total)ug/kg ND 10.0 04/30/20 17:253.5
1,2-Dichloroethane-d4 (S)%98 70-132 04/30/20 17:25
4-Bromofluorobenzene (S)%99 70-130 04/30/20 17:25
Toluene-d8 (S)%102 70-130 04/30/20 17:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2873857LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 51.650 103 70-130
1,1,1-Trichloroethane ug/kg 50.350 101 70-130
1,1,2,2-Tetrachloroethane ug/kg 49.950 100 55-130
1,1,2-Trichloroethane ug/kg 52.650 105 70-130
1,1-Dichloroethane ug/kg 50.650 101 68-130
1,1-Dichloroethene ug/kg 52.750 105 70-130
1,1-Dichloropropene ug/kg 53.250 106 70-130
1,2,3-Trichlorobenzene ug/kg 53.550 107 70-130
1,2,3-Trichloropropane ug/kg 50.350 101 70-130
1,2,4-Trichlorobenzene ug/kg 51.150 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2873857LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 52.350 105 69-130
1,2-Dibromo-3-chloropropane ug/kg 53.250 106 57-141
1,2-Dibromoethane (EDB)ug/kg 51.950 104 70-130
1,2-Dichlorobenzene ug/kg 52.750 105 70-130
1,2-Dichloroethane ug/kg 50.750 101 70-130
1,2-Dichloropropane ug/kg 52.050 104 70-130
1,3,5-Trimethylbenzene ug/kg 53.250 106 70-130
1,3-Dichlorobenzene ug/kg 51.950 104 70-130
1,3-Dichloropropane ug/kg 51.650 103 70-130
1,4-Dichlorobenzene ug/kg 52.250 104 70-130
2,2-Dichloropropane ug/kg 50.050 100 70-130
2-Butanone (MEK)ug/kg 110100 110 60-130
2-Chlorotoluene ug/kg 53.150 106 70-130
2-Hexanone ug/kg 105100 105 70-132
4-Chlorotoluene ug/kg 52.050 104 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 102100 102 69-130
Acetone ug/kg 115100 115 49-148
Benzene ug/kg 51.850 104 70-130
Bromobenzene ug/kg 51.850 104 70-130
Bromochloromethane ug/kg 50.450 101 70-130
Bromodichloromethane ug/kg 53.150 106 70-130
Bromoform ug/kg 50.950 102 68-136
Bromomethane ug/kg 65.5 IH5013160-140
Carbon tetrachloride ug/kg 52.450 105 70-130
Chlorobenzene ug/kg 51.250 102 70-130
Chloroethane ug/kg 59.750 119 51-147
Chloroform ug/kg 50.250 100 70-130
Chloromethane ug/kg 53.550 107 48-130
cis-1,2-Dichloroethene ug/kg 50.850 102 70-130
cis-1,3-Dichloropropene ug/kg 52.150 104 70-130
Dibromochloromethane ug/kg 52.250 104 70-130
Dibromomethane ug/kg 49.750 99 70-130
Dichlorodifluoromethane ug/kg 51.750 103 49-130
Diisopropyl ether ug/kg 52.750 105 66-130
Ethylbenzene ug/kg 49.250 98 70-130
Hexachloro-1,3-butadiene ug/kg 51.950 104 70-130
Isopropylbenzene (Cumene)ug/kg 51.450 103 70-130
m&p-Xylene ug/kg 98.8100 99 70-130
Methyl-tert-butyl ether ug/kg 52.650 105 70-130
Methylene Chloride ug/kg 49.450 99 50-137
n-Butylbenzene ug/kg 51.750 103 70-130
n-Propylbenzene ug/kg 50.650 101 70-130
Naphthalene ug/kg 55.850 112 70-131
o-Xylene ug/kg 51.350 103 70-130
p-Isopropyltoluene ug/kg 52.950 106 70-130
sec-Butylbenzene ug/kg 52.150 104 70-130
Styrene ug/kg 53.050 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2873857LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 45.850 92 69-130
Tetrachloroethene ug/kg 46.950 94 56-130
Toluene ug/kg 50.350 101 70-130
trans-1,2-Dichloroethene ug/kg 51.550 103 70-130
trans-1,3-Dichloropropene ug/kg 52.550 105 70-130
Trichloroethene ug/kg 52.150 104 70-141
Trichlorofluoromethane ug/kg 52.050 104 67-130
Vinyl acetate ug/kg 112100 112 10-136
Vinyl chloride ug/kg 59.250 118 67-130
Xylene (Total)ug/kg 150150 100 70-130
1,2-Dichloroethane-d4 (S)%98 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2873859MATRIX SPIKE SAMPLE:
MSSpike
Result
92475533002
1,1,1,2-Tetrachloroethane ug/kg 13.419.6 68 52-133ND
1,1,1-Trichloroethane ug/kg 15.619.6 80 49-137ND
1,1,2,2-Tetrachloroethane ug/kg 9.319.6 47 39-150ND
1,1,2-Trichloroethane ug/kg 18.119.6 92 48-140ND
1,1-Dichloroethane ug/kg 17.219.6 87 46-135ND
1,1-Dichloroethene ug/kg 18.819.6 96 38-149ND
1,1-Dichloropropene ug/kg 15.519.6 79 41-140ND
1,2,3-Trichlorobenzene ug/kg 9.119.6 46 10-158ND
1,2,3-Trichloropropane ug/kg 17.619.6 89 33-157ND
1,2,4-Trichlorobenzene ug/kg 9.119.6 47 10-155ND
1,2,4-Trimethylbenzene ug/kg 14.219.6 72 24-154ND
1,2-Dibromo-3-chloropropane ug/kg 15.319.6 78 33-158ND
1,2-Dibromoethane (EDB)ug/kg 18.019.6 92 40-136ND
1,2-Dichlorobenzene ug/kg 13.819.6 70 27-146ND
1,2-Dichloroethane ug/kg 18.019.6 92 49-140ND
1,2-Dichloropropane ug/kg 17.619.6 90 44-143ND
1,3,5-Trimethylbenzene ug/kg 14.119.6 72 40-144ND
1,3-Dichlorobenzene ug/kg 13.619.6 69 33-140ND
1,3-Dichloropropane ug/kg 18.219.6 93 47-147ND
1,4-Dichlorobenzene ug/kg 26.919.6 70 35-13913.1
2,2-Dichloropropane ug/kg 16.219.6 82 41-140ND
2-Butanone (MEK)ug/kg 43.5J39.3 95 10-181ND
2-Chlorotoluene ug/kg 15.119.6 77 38-147ND
2-Hexanone ug/kg 36.0J39.3 92 18-169ND
4-Chlorotoluene ug/kg 14.719.6 75 36-145ND
4-Methyl-2-pentanone (MIBK)ug/kg 38.3J39.3 98 16-175ND
Acetone ug/kg 76.6J M139.3 2 10-20076.0J
Benzene ug/kg 17.119.6 87 46-136ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
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Huntersville, NC 28078
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Page 38 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2873859MATRIX SPIKE SAMPLE:
MSSpike
Result
92475533002
Bromobenzene ug/kg 15.819.6 81 38-149ND
Bromochloromethane ug/kg 18.119.6 92 44-142ND
Bromodichloromethane ug/kg 13.219.6 67 41-140ND
Bromoform ug/kg 10.319.6 52 34-145ND
Bromomethane ug/kg 22.3 IH19.6 114 14-162ND
Carbon tetrachloride ug/kg 11.419.6 58 44-141ND
Chlorobenzene ug/kg 23.719.6 82 39-1417.7
Chloroethane ug/kg 22.219.6 113 10-182ND
Chloroform ug/kg 18.119.6 92 45-140ND
Chloromethane ug/kg 17.119.6 87 19-149ND
cis-1,2-Dichloroethene ug/kg 17.219.6 88 38-150ND
cis-1,3-Dichloropropene ug/kg 14.119.6 72 30-144ND
Dibromochloromethane ug/kg 11.719.6 60 36-145ND
Dibromomethane ug/kg 18.319.6 93 41-145ND
Dichlorodifluoromethane ug/kg 16.819.6 86 16-146ND
Diisopropyl ether ug/kg 18.119.6 92 41-143ND
Ethylbenzene ug/kg 14.519.6 74 35-144ND
Hexachloro-1,3-butadiene ug/kg 7.019.6 36 10-160ND
Isopropylbenzene (Cumene)ug/kg 15.719.6 67 30-1522.6J
m&p-Xylene ug/kg 29.639.3 75 33-145ND
Methyl-tert-butyl ether ug/kg 18.019.6 92 49-140ND
Methylene Chloride ug/kg 17.2J19.6 74 10-174ND
n-Butylbenzene ug/kg 11.919.6 55 10-160ND
n-Propylbenzene ug/kg 13.519.6 69 24-159ND
Naphthalene ug/kg 12.419.6 63 10-171ND
o-Xylene ug/kg 15.319.6 78 31-150ND
p-Isopropyltoluene ug/kg 12.619.6 64 21-154ND
sec-Butylbenzene ug/kg 15.219.6 57 19-1594.0J
Styrene ug/kg 15.619.6 80 15-152ND
tert-Butylbenzene ug/kg 12.119.6 61 31-141ND
Tetrachloroethene ug/kg 12.519.6 64 19-141ND
Toluene ug/kg 16.219.6 82 31-146ND
trans-1,2-Dichloroethene ug/kg 17.319.6 88 28-157ND
trans-1,3-Dichloropropene ug/kg 15.119.6 77 25-146ND
Trichloroethene ug/kg 21.919.6 112 34-149ND
Trichlorofluoromethane ug/kg 15.819.6 80 10-167ND
Vinyl acetate ug/kg ND39.3 12 10-200ND
Vinyl chloride ug/kg 20.019.6 102 36-155ND
Xylene (Total)ug/kg 44.958.9 76 29-148ND
1,2-Dichloroethane-d4 (S)%100 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
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Huntersville, NC 28078
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Page 39 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92475533001
2873858SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg 22.4J 3012.3J
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 160 3080.8J
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IH30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92475533001
2873858SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%103103
4-Bromofluorobenzene (S)%96100
Toluene-d8 (S)%100101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
539506
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92475481006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2875869
Associated Lab Samples:92475481006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 05/04/20 15:410.34
1,1,1-Trichloroethane ug/L ND 1.0 05/04/20 15:410.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 05/04/20 15:410.22
1,1,2-Trichloroethane ug/L ND 1.0 05/04/20 15:410.24
1,1-Dichloroethane ug/L ND 1.0 05/04/20 15:410.27
1,1-Dichloroethene ug/L ND 1.0 05/04/20 15:410.24
1,1-Dichloropropene ug/L ND 1.0 05/04/20 15:410.21
1,2,3-Trichlorobenzene ug/L ND 1.0 05/04/20 15:410.34
1,2,3-Trichloropropane ug/L ND 1.0 05/04/20 15:410.35
1,2,4-Trichlorobenzene ug/L ND 1.0 05/04/20 15:410.22
1,2,4-Trimethylbenzene ug/L ND 1.0 05/04/20 15:410.17
1,2-Dibromo-3-chloropropane ug/L ND 5.0 05/04/20 15:410.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 05/04/20 15:410.26
1,2-Dichlorobenzene ug/L ND 1.0 05/04/20 15:410.29
1,2-Dichloroethane ug/L ND 1.0 05/04/20 15:410.34
1,2-Dichloropropane ug/L ND 1.0 05/04/20 15:410.19
1,3,5-Trimethylbenzene ug/L ND 1.0 05/04/20 15:410.20
1,3-Dichlorobenzene ug/L ND 1.0 05/04/20 15:410.22
1,3-Dichloropropane ug/L ND 1.0 05/04/20 15:410.16
1,4-Dichlorobenzene ug/L ND 1.0 05/04/20 15:410.26
2,2-Dichloropropane ug/L ND 1.0 05/04/20 15:410.27
2-Butanone (MEK)ug/L ND 5.0 05/04/20 15:413.3
2-Chlorotoluene ug/L ND 1.0 05/04/20 15:410.20
2-Hexanone ug/L ND 5.0 05/04/20 15:410.57
4-Chlorotoluene ug/L ND 1.0 05/04/20 15:410.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 05/04/20 15:414.5
Acetone ug/L ND 25.0 05/04/20 15:416.2
Benzene ug/L ND 1.0 05/04/20 15:410.15
Bromobenzene ug/L ND 1.0 05/04/20 15:410.22
Bromochloromethane ug/L ND 1.0 05/04/20 15:410.34
Bromodichloromethane ug/L ND 1.0 05/04/20 15:410.26
Bromoform ug/L ND 1.0 05/04/20 15:410.62
Bromomethane ug/L ND 2.0 IH,v105/04/20 15:410.62
Carbon tetrachloride ug/L ND 1.0 05/04/20 15:410.22
Chlorobenzene ug/L ND 1.0 05/04/20 15:410.23
Chloroethane ug/L ND 1.0 05/04/20 15:410.49
Chloroform ug/L ND 5.0 05/04/20 15:412.3
Chloromethane ug/L ND 1.0 05/04/20 15:410.39
cis-1,2-Dichloroethene ug/L ND 1.0 05/04/20 15:410.29
cis-1,3-Dichloropropene ug/L ND 1.0 05/04/20 15:410.30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2875869
Associated Lab Samples:92475481006
Matrix:Water
AnalyzedMDL
Dibromochloromethane ug/L ND 1.0 05/04/20 15:410.41
Dibromomethane ug/L ND 1.0 05/04/20 15:410.46
Dichlorodifluoromethane ug/L ND 1.0 05/04/20 15:410.23
Diisopropyl ether ug/L ND 1.0 05/04/20 15:410.22
Ethylbenzene ug/L ND 1.0 05/04/20 15:410.26
Hexachloro-1,3-butadiene ug/L ND 1.0 05/04/20 15:410.44
Isopropylbenzene (Cumene)ug/L ND 1.0 05/04/20 15:410.20
m&p-Xylene ug/L ND 2.0 05/04/20 15:410.41
Methyl-tert-butyl ether ug/L ND 1.0 05/04/20 15:410.28
Methylene Chloride ug/L ND 5.0 05/04/20 15:413.7
n-Butylbenzene ug/L ND 1.0 05/04/20 15:410.23
n-Propylbenzene ug/L ND 1.0 05/04/20 15:410.18
Naphthalene ug/L ND 1.0 05/04/20 15:410.35
o-Xylene ug/L ND 1.0 05/04/20 15:410.22
p-Isopropyltoluene ug/L ND 1.0 05/04/20 15:410.21
sec-Butylbenzene ug/L ND 1.0 05/04/20 15:410.20
Styrene ug/L ND 1.0 05/04/20 15:410.27
tert-Butylbenzene ug/L ND 1.0 05/04/20 15:410.23
Tetrachloroethene ug/L ND 1.0 05/04/20 15:410.16
Toluene ug/L ND 1.0 05/04/20 15:410.24
trans-1,2-Dichloroethene ug/L ND 1.0 05/04/20 15:410.25
trans-1,3-Dichloropropene ug/L ND 1.0 05/04/20 15:410.31
Trichloroethene ug/L ND 1.0 05/04/20 15:410.22
Trichlorofluoromethane ug/L ND 1.0 05/04/20 15:410.31
Vinyl acetate ug/L ND 2.0 05/04/20 15:411.4
Vinyl chloride ug/L ND 1.0 05/04/20 15:410.24
Xylene (Total)ug/L ND 1.0 05/04/20 15:410.63
1,2-Dichloroethane-d4 (S)%94 70-130 05/04/20 15:41
4-Bromofluorobenzene (S)%97 70-130 05/04/20 15:41
Toluene-d8 (S)%102 70-130 05/04/20 15:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2875870LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 70-130
1,1,1-Trichloroethane ug/L 45.650 91 70-130
1,1,2,2-Tetrachloroethane ug/L 49.250 98 70-130
1,1,2-Trichloroethane ug/L 48.850 98 70-130
1,1-Dichloroethane ug/L 44.950 90 70-130
1,1-Dichloroethene ug/L 45.350 91 70-130
1,1-Dichloropropene ug/L 49.150 98 70-130
1,2,3-Trichlorobenzene ug/L 47.750 95 70-130
1,2,3-Trichloropropane ug/L 50.250 100 70-130
1,2,4-Trichlorobenzene ug/L 48.250 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2875870LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/L 47.150 94 70-131
1,2-Dibromo-3-chloropropane ug/L 52.350 105 70-130
1,2-Dibromoethane (EDB)ug/L 50.450 101 70-130
1,2-Dichlorobenzene ug/L 48.550 97 70-130
1,2-Dichloroethane ug/L 45.250 90 70-130
1,2-Dichloropropane ug/L 49.450 99 70-130
1,3,5-Trimethylbenzene ug/L 47.150 94 70-130
1,3-Dichlorobenzene ug/L 49.950 100 70-130
1,3-Dichloropropane ug/L 49.450 99 70-131
1,4-Dichlorobenzene ug/L 48.050 96 70-130
2,2-Dichloropropane ug/L 46.250 92 69-130
2-Butanone (MEK)ug/L 88.9100 89 64-135
2-Chlorotoluene ug/L 48.150 96 70-130
2-Hexanone ug/L 96.4100 96 66-135
4-Chlorotoluene ug/L 48.050 96 70-130
4-Methyl-2-pentanone (MIBK)ug/L 93.8100 94 70-130
Acetone ug/L 100100 100 61-157
Benzene ug/L 49.150 98 70-130
Bromobenzene ug/L 47.950 96 70-130
Bromochloromethane ug/L 50.150 100 70-130
Bromodichloromethane ug/L 50.950 102 70-130
Bromoform ug/L 52.150 104 70-130
Bromomethane ug/L 82.0 IH,L1,v15016438-130
Carbon tetrachloride ug/L 49.550 99 70-130
Chlorobenzene ug/L 47.850 96 70-130
Chloroethane ug/L 40.750 81 37-142
Chloroform ug/L 46.350 93 70-130
Chloromethane ug/L 43.550 87 48-130
cis-1,2-Dichloroethene ug/L 44.350 89 70-130
cis-1,3-Dichloropropene ug/L 50.850 102 70-130
Dibromochloromethane ug/L 51.250 102 70-130
Dibromomethane ug/L 48.650 97 70-130
Dichlorodifluoromethane ug/L 43.350 87 53-134
Diisopropyl ether ug/L 46.950 94 70-135
Ethylbenzene ug/L 45.950 92 70-130
Hexachloro-1,3-butadiene ug/L 51.250 102 68-132
Isopropylbenzene (Cumene)ug/L 48.550 97 70-130
m&p-Xylene ug/L 94.4100 94 70-130
Methyl-tert-butyl ether ug/L 48.450 97 70-130
Methylene Chloride ug/L 45.050 90 67-132
n-Butylbenzene ug/L 49.850 100 70-132
n-Propylbenzene ug/L 46.750 93 70-130
Naphthalene ug/L 48.350 97 70-130
o-Xylene ug/L 47.150 94 70-131
p-Isopropyltoluene ug/L 48.750 97 70-130
sec-Butylbenzene ug/L 47.650 95 70-130
Styrene ug/L 49.650 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2875870LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 41.350 83 66-130
Tetrachloroethene ug/L 48.350 97 69-130
Toluene ug/L 45.850 92 70-130
trans-1,2-Dichloroethene ug/L 46.050 92 70-130
trans-1,3-Dichloropropene ug/L 52.150 104 70-130
Trichloroethene ug/L 49.350 99 70-130
Trichlorofluoromethane ug/L 43.350 87 63-130
Vinyl acetate ug/L 95.8100 96 55-143
Vinyl chloride ug/L 50.650 101 70-131
Xylene (Total)ug/L 141150 94 70-130
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2875872MATRIX SPIKE SAMPLE:
MSSpike
Result
92475518006
1,1,1,2-Tetrachloroethane ug/L 22.220 111 73-134ND
1,1,1-Trichloroethane ug/L 21.520 107 82-143ND
1,1,2,2-Tetrachloroethane ug/L 22.420 112 70-136ND
1,1,2-Trichloroethane ug/L 21.220 106 70-135ND
1,1-Dichloroethane ug/L 22.620 113 70-139ND
1,1-Dichloroethene ug/L 22.820 114 70-154ND
1,1-Dichloropropene ug/L 22.220 111 70-149ND
1,2,3-Trichlorobenzene ug/L 23.820 119 70-135ND
1,2,3-Trichloropropane ug/L 22.120 111 71-137ND
1,2,4-Trichlorobenzene ug/L 24.620 123 73-140ND
1,2,4-Trimethylbenzene ug/L 23.520 117 71-142ND
1,2-Dibromo-3-chloropropane ug/L 23.720 118 65-134ND
1,2-Dibromoethane (EDB)ug/L 22.720 113 70-137ND
1,2-Dichlorobenzene ug/L 24.120 121 70-133ND
1,2-Dichloroethane ug/L 20.620 103 70-137ND
1,2-Dichloropropane ug/L 21.820 109 70-140ND
1,3,5-Trimethylbenzene ug/L 23.420 117 76-139ND
1,3-Dichlorobenzene ug/L 23.320 117 70-135ND
1,3-Dichloropropane ug/L 23.120 116 70-143ND
1,4-Dichlorobenzene ug/L 23.320 116 70-133ND
2,2-Dichloropropane ug/L 21.120 105 61-148ND
2-Butanone (MEK)ug/L 41.840 104 60-139ND
2-Chlorotoluene ug/L 23.520 117 70-144ND
2-Hexanone ug/L 44.340 111 65-138ND
4-Chlorotoluene ug/L 23.920 119 70-137ND
4-Methyl-2-pentanone (MIBK)ug/L 39.140 98 65-135ND
Acetone ug/L 43.140 108 60-148ND
Benzene ug/L 27.120 118 70-1513.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
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Page 45 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2875872MATRIX SPIKE SAMPLE:
MSSpike
Result
92475518006
Bromobenzene ug/L 24.320 122 70-136ND
Bromochloromethane ug/L 21.720 109 70-141ND
Bromodichloromethane ug/L 20.920 104 70-138ND
Bromoform ug/L 22.520 112 63-130ND
Bromomethane ug/L 32.0 M0,v12016015-152ND
Carbon tetrachloride ug/L 23.420 117 70-143ND
Chlorobenzene ug/L 23.920 120 70-138ND
Chloroethane ug/L 20.520 103 52-163ND
Chloroform ug/L 23.420 117 70-139ND
Chloromethane ug/L 17.120 86 41-139ND
cis-1,2-Dichloroethene ug/L 46.620 99 70-14126.9
cis-1,3-Dichloropropene ug/L 22.220 111 70-137ND
Dibromochloromethane ug/L 22.320 111 70-134ND
Dibromomethane ug/L 23.220 116 70-138ND
Dichlorodifluoromethane ug/L 16.920 84 47-155ND
Diisopropyl ether ug/L 33.120 115 63-14410.2
Ethylbenzene ug/L 22.920 114 66-153ND
Hexachloro-1,3-butadiene ug/L 27.4 v12013765-149ND
Isopropylbenzene (Cumene)ug/L 26.020 118 70-1392.4
m&p-Xylene ug/L 46.040 115 69-152ND
Methyl-tert-butyl ether ug/L 74.620 129 54-15648.9
Methylene Chloride ug/L 22.220 111 42-159ND
n-Butylbenzene ug/L 23.520 117 70-139ND
n-Propylbenzene ug/L 24.020 117 70-144ND
Naphthalene ug/L 25.620 125 61-148ND
o-Xylene ug/L 23.620 118 70-148ND
p-Isopropyltoluene ug/L 24.320 121 70-146ND
sec-Butylbenzene ug/L 23.820 117 70-141ND
Styrene ug/L 24.020 120 70-135ND
tert-Butylbenzene ug/L 19.420 97 70-130ND
Tetrachloroethene ug/L 24.820 114 59-1431.9
Toluene ug/L 21.820 106 59-148ND
trans-1,2-Dichloroethene ug/L 22.320 111 70-146ND
trans-1,3-Dichloropropene ug/L 21.020 105 70-135ND
Trichloroethene ug/L 29.720 121 70-1475.4
Trichlorofluoromethane ug/L 157 M120-11 70-148160
Vinyl acetate ug/L 46.440 116 49-151ND
Vinyl chloride ug/L 30.420 104 70-1569.6
Xylene (Total)ug/L 69.760 116 63-158ND
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
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Page 46 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92475518011
2875871SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L 0.64J 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2,4-Trimethylbenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3,5-Trimethylbenzene ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
Benzene ug/L 0.45J 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v130ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L 0.74J 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND v130ND
Isopropylbenzene (Cumene)ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92475518011
2875871SAMPLE DUPLICATE:
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
n-Butylbenzene ug/L ND 30ND
n-Propylbenzene ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
sec-Butylbenzene ug/L ND 30ND
Styrene ug/L ND 30ND
tert-Butylbenzene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L 1.0 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%9996
4-Bromofluorobenzene (S)%10097
Toluene-d8 (S)%98102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
538906
EPA 3546
EPA 8081B
8081 GCS Pesticides
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2873071
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Matrix:Solid
AnalyzedMDL
4,4'-DDD ug/kg ND 2.0 05/05/20 21:080.82
4,4'-DDE ug/kg ND 2.0 05/05/20 21:080.78
4,4'-DDT ug/kg ND 2.0 05/05/20 21:080.71
Aldrin ug/kg ND 2.0 05/05/20 21:080.71
alpha-BHC ug/kg ND 2.0 05/05/20 21:080.68
beta-BHC ug/kg ND 2.0 05/05/20 21:080.71
Chlordane (Technical)ug/kg ND 6.9 05/05/20 21:086.9
delta-BHC ug/kg ND 2.0 05/05/20 21:080.70
Dieldrin ug/kg ND 2.0 05/05/20 21:080.80
Endosulfan I ug/kg ND 2.0 05/05/20 21:080.79
Endosulfan II ug/kg ND 2.0 05/05/20 21:080.79
Endosulfan sulfate ug/kg ND 2.0 05/05/20 21:080.86
Endrin ug/kg ND 2.0 05/05/20 21:080.82
Endrin aldehyde ug/kg ND 2.0 05/05/20 21:080.77
Endrin ketone ug/kg ND 2.0 05/05/20 21:081.0
gamma-BHC (Lindane)ug/kg ND 2.0 05/05/20 21:080.81
Heptachlor ug/kg ND 2.0 05/05/20 21:080.65
Heptachlor epoxide ug/kg ND 2.0 05/05/20 21:080.66
Hexachlorobenzene ug/kg ND 2.0 05/05/20 21:080.65
Methoxychlor ug/kg ND 4.9 05/05/20 21:082.6
Mirex ug/kg ND 4.9 05/05/20 21:082.4
Toxaphene ug/kg ND 6.9 05/05/20 21:086.9
Decachlorobiphenyl (S)%112 10-130 05/05/20 21:08
Tetrachloro-m-xylene (S)%111 15-130 05/05/20 21:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2873072LABORATORY CONTROL SAMPLE:
LCSSpike
4,4'-DDD ug/kg 9.78.2 119 65-130
4,4'-DDE ug/kg 9.48.2 114 62-130
4,4'-DDT ug/kg 9.28.2 112 46-130
Aldrin ug/kg 8.28.2 100 46-130
alpha-BHC ug/kg 8.58.2 103 41-130
beta-BHC ug/kg 9.38.2 113 45-130
delta-BHC ug/kg 7.98.2 97 59-130
Dieldrin ug/kg 9.28.2 112 59-130
Endosulfan I ug/kg 9.48.2 115 60-130
Endosulfan II ug/kg 9.18.2 111 64-130
Endosulfan sulfate ug/kg 8.98.2 108 67-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2873072LABORATORY CONTROL SAMPLE:
LCSSpike
Endrin ug/kg 9.58.2 116 62-130
Endrin aldehyde ug/kg 7.98.2 97 52-130
Endrin ketone ug/kg 9.88.2 120 57-130
gamma-BHC (Lindane)ug/kg 8.68.2 105 47-130
Heptachlor ug/kg 7.88.2 95 48-130
Heptachlor epoxide ug/kg 8.38.2 102 56-130
Hexachlorobenzene ug/kg 8.38.2 101 40-130
Methoxychlor ug/kg 24.224.6 98 62-130
Mirex ug/kg 25.424.6 103 70-130
Decachlorobiphenyl (S)%111 10-130
Tetrachloro-m-xylene (S)%107 15-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2873073MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92475295005
2873074
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
4,4'-DDD ug/kg 11.9 123 36-130100 18 3012.3ND 14.6 12.2
4,4'-DDE ug/kg 11.9 119 26-13199 16 3012.3ND 14.2 12.1
4,4'-DDT ug/kg M1,R111.9 407 32-13196 121 3012.3ND 48.5 11.8
Aldrin ug/kg 11.9 100 28-13081 17 3012.3ND 11.9 10.0
alpha-BHC ug/kg 11.9 102 10-12386 15 3012.3ND 12.2 10.5
beta-BHC ug/kg 11.9 117 25-130100 12 3012.3ND 13.9 12.3
delta-BHC ug/kg 11.9 96 28-13080 15 3012.3ND 11.5 9.9
Dieldrin ug/kg 11.9 115 29-13092 18 3012.3ND 13.6 11.4
Endosulfan I ug/kg 11.9 115 31-130100 10 3012.3ND 13.7 12.3
Endosulfan II ug/kg 11.9 112 18-14190 18 3012.3ND 13.4 11.1
Endosulfan sulfate ug/kg 11.9 112 40-13090 19 3012.3ND 13.3 11.0
Endrin ug/kg 11.9 117 19-14794 19 3012.3ND 14.0 11.5
Endrin aldehyde ug/kg 11.9 102 25-13082 18 3012.3ND 12.1 10.1
Endrin ketone ug/kg 11.9 125 27-13498 21 3012.3ND 14.8 12.0
gamma-BHC (Lindane)ug/kg 11.9 101 30-13085 14 3012.3ND 12.0 10.4
Heptachlor ug/kg 11.9 96 33-13077 19 3012.3ND 11.4 9.5
Heptachlor epoxide ug/kg 11.9 100 33-13079 20 3012.3ND 11.9 9.7
Hexachlorobenzene ug/kg 11.9 101 10-14783 16 3012.3ND 12.0 10.2
Methoxychlor ug/kg 35.7 106 26-13381 23 3036.9ND 37.7 29.8
Mirex ug/kg 35.7 107 26-12587 17 3036.9ND 38.1 32.2
Decachlorobiphenyl (S)%116 10-13090
Tetrachloro-m-xylene (S)%105 15-13084
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
539069
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2873815
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 328 05/04/20 16:2875.1
1,2-Dichlorobenzene ug/kg ND 328 05/04/20 16:2870.9
1,3-Dichlorobenzene ug/kg ND 328 05/04/20 16:2873.8
1,4-Dichlorobenzene ug/kg ND 328 05/04/20 16:2872.1
1-Methylnaphthalene ug/kg ND 328 05/04/20 16:2887.3
2,2'-Oxybis(1-chloropropane)ug/kg ND 328 05/04/20 16:2891.1
2,4,5-Trichlorophenol ug/kg ND 328 v105/04/20 16:2885.1
2,4,6-Trichlorophenol ug/kg ND 328 v105/04/20 16:2882.4
2,4-Dichlorophenol ug/kg ND 328 05/04/20 16:28108
2,4-Dimethylphenol ug/kg ND 328 05/04/20 16:2881.7
2,4-Dinitrophenol ug/kg ND 1640 05/04/20 16:281050
2,4-Dinitrotoluene ug/kg ND 328 05/04/20 16:2886.8
2,6-Dinitrotoluene ug/kg ND 328 05/04/20 16:2885.7
2-Chloronaphthalene ug/kg ND 328 05/04/20 16:2873.0
2-Chlorophenol ug/kg ND 328 05/04/20 16:2876.3
2-Methylnaphthalene ug/kg ND 328 05/04/20 16:2883.4
2-Methylphenol(o-Cresol)ug/kg ND 328 05/04/20 16:2872.6
2-Nitroaniline ug/kg ND 1640 05/04/20 16:28165
2-Nitrophenol ug/kg ND 328 05/04/20 16:28101
3&4-Methylphenol(m&p Cresol)ug/kg ND 328 05/04/20 16:2882.5
3,3'-Dichlorobenzidine ug/kg ND 656 05/04/20 16:28228
3-Nitroaniline ug/kg ND 1640 05/04/20 16:28174
4,6-Dinitro-2-methylphenol ug/kg ND 656 05/04/20 16:28528
4-Bromophenylphenyl ether ug/kg ND 328 05/04/20 16:2886.0
4-Chloro-3-methylphenol ug/kg ND 656 05/04/20 16:28200
4-Chloroaniline ug/kg ND 656 05/04/20 16:28201
4-Chlorophenylphenyl ether ug/kg ND 328 05/04/20 16:2885.1
4-Nitroaniline ug/kg ND 656 05/04/20 16:28162
4-Nitrophenol ug/kg ND 1640 05/04/20 16:28523
Acenaphthene ug/kg ND 328 05/04/20 16:2884.3
Acenaphthylene ug/kg ND 328 05/04/20 16:2877.6
Aniline ug/kg ND 328 05/04/20 16:2873.6
Anthracene ug/kg ND 328 05/04/20 16:2885.0
Benzo(a)anthracene ug/kg ND 328 05/04/20 16:28104
Benzo(a)pyrene ug/kg ND 328 05/04/20 16:28142
Benzo(b)fluoranthene ug/kg ND 328 05/04/20 16:28132
Benzo(g,h,i)perylene ug/kg ND 328 05/04/20 16:28128
Benzo(k)fluoranthene ug/kg ND 328 05/04/20 16:28138
Benzoic Acid ug/kg ND 1640 05/04/20 16:28354
Benzyl alcohol ug/kg ND 656 05/04/20 16:28174
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
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Page 51 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2873815
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 328 05/04/20 16:2887.5
bis(2-Chloroethyl) ether ug/kg ND 328 05/04/20 16:2869.6
bis(2-Ethylhexyl)phthalate ug/kg ND 328 05/04/20 16:28107
Butylbenzylphthalate ug/kg ND 328 05/04/20 16:2887.3
Chrysene ug/kg ND 328 05/04/20 16:2895.2
Di-n-butylphthalate ug/kg ND 328 05/04/20 16:2880.9
Di-n-octylphthalate ug/kg ND 328 05/04/20 16:28187
Dibenz(a,h)anthracene ug/kg ND 328 05/04/20 16:28131
Dibenzofuran ug/kg ND 328 05/04/20 16:2882.0
Diethylphthalate ug/kg ND 328 05/04/20 16:2871.1
Dimethylphthalate ug/kg ND 328 05/04/20 16:2874.1
Fluoranthene ug/kg ND 328 05/04/20 16:2899.0
Fluorene ug/kg ND 328 05/04/20 16:2887.7
Hexachloro-1,3-butadiene ug/kg ND 328 05/04/20 16:2879.7
Hexachlorobenzene ug/kg ND 328 05/04/20 16:2883.2
Hexachlorocyclopentadiene ug/kg ND 328 v205/04/20 16:28131
Hexachloroethane ug/kg ND 328 05/04/20 16:2874.7
Indeno(1,2,3-cd)pyrene ug/kg ND 328 05/04/20 16:28150
Isophorone ug/kg ND 328 05/04/20 16:2871.2
N-Nitroso-di-n-propylamine ug/kg ND 328 05/04/20 16:2891.8
N-Nitrosodimethylamine ug/kg ND 328 05/04/20 16:2892.2
N-Nitrosodiphenylamine ug/kg ND 328 05/04/20 16:2883.6
Naphthalene ug/kg ND 328 05/04/20 16:2878.5
Nitrobenzene ug/kg ND 328 05/04/20 16:2878.3
Pentachlorophenol ug/kg ND 656 v105/04/20 16:28150
Phenanthrene ug/kg ND 328 05/04/20 16:2882.5
Phenol ug/kg ND 328 05/04/20 16:2878.3
Pyrene ug/kg ND 328 05/04/20 16:2890.2
Pyridine ug/kg ND 328 05/04/20 16:2882.9
2,4,6-Tribromophenol (S)%83 27-110 05/04/20 16:28
2-Fluorobiphenyl (S)%71 30-110 05/04/20 16:28
2-Fluorophenol (S)%68 13-110 05/04/20 16:28
Nitrobenzene-d5 (S)%69 23-110 05/04/20 16:28
Phenol-d6 (S)%75 22-110 05/04/20 16:28
Terphenyl-d14 (S)%101 28-110 05/04/20 16:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2873816LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 12101640 74 52-130
1,2-Dichlorobenzene ug/kg 12001640 73 51-130
1,3-Dichlorobenzene ug/kg 11501640 70 50-130
1,4-Dichlorobenzene ug/kg 12401640 75 49-130
1-Methylnaphthalene ug/kg 11301640 69 55-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2873816LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 11001640 67 30-130
2,4,5-Trichlorophenol ug/kg 12701640 78 55-130
2,4,6-Trichlorophenol ug/kg 12401640 76 57-130
2,4-Dichlorophenol ug/kg 12701640 77 56-130
2,4-Dimethylphenol ug/kg 12301640 75 51-130
2,4-Dinitrophenol ug/kg 57008200 70 27-133
2,4-Dinitrotoluene ug/kg 12301640 75 61-130
2,6-Dinitrotoluene ug/kg 12301640 75 60-130
2-Chloronaphthalene ug/kg 12001640 73 52-130
2-Chlorophenol ug/kg 12201640 74 54-130
2-Methylnaphthalene ug/kg 11701640 71 54-130
2-Methylphenol(o-Cresol)ug/kg 11901640 72 51-130
2-Nitroaniline ug/kg 22303280 68 51-130
2-Nitrophenol ug/kg 12401640 76 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 12201640 74 11-163
3,3'-Dichlorobenzidine ug/kg 25703280 78 10-132
3-Nitroaniline ug/kg 25703280 78 55-130
4,6-Dinitro-2-methylphenol ug/kg 26303280 80 47-142
4-Bromophenylphenyl ether ug/kg 11601640 71 59-130
4-Chloro-3-methylphenol ug/kg 23503280 72 55-130
4-Chloroaniline ug/kg 24703280 75 54-130
4-Chlorophenylphenyl ether ug/kg 11601640 71 58-130
4-Nitroaniline ug/kg 24903280 76 54-130
4-Nitrophenol ug/kg 62708200 77 48-130
Acenaphthene ug/kg 12101640 74 60-130
Acenaphthylene ug/kg 12201640 75 60-130
Aniline ug/kg 10801640 66 43-130
Anthracene ug/kg 12301640 75 63-130
Benzo(a)anthracene ug/kg 12701640 77 59-130
Benzo(a)pyrene ug/kg 12701640 78 57-130
Benzo(b)fluoranthene ug/kg 14001640 86 54-130
Benzo(g,h,i)perylene ug/kg 11101640 68 59-130
Benzo(k)fluoranthene ug/kg 12601640 77 54-130
Benzoic Acid ug/kg 43808200 53 19-130
Benzyl alcohol ug/kg 23103280 71 50-130
bis(2-Chloroethoxy)methane ug/kg 11001640 67 54-130
bis(2-Chloroethyl) ether ug/kg 10901640 66 48-130
bis(2-Ethylhexyl)phthalate ug/kg 11701640 72 45-134
Butylbenzylphthalate ug/kg 12701640 78 46-138
Chrysene ug/kg 11801640 72 58-130
Di-n-butylphthalate ug/kg 11901640 73 60-130
Di-n-octylphthalate ug/kg 12701640 78 53-130
Dibenz(a,h)anthracene ug/kg 11201640 68 59-130
Dibenzofuran ug/kg 11801640 72 60-130
Diethylphthalate ug/kg 11301640 69 60-130
Dimethylphthalate ug/kg 11401640 70 60-130
Fluoranthene ug/kg 12901640 78 65-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2873816LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 12001640 73 63-130
Hexachloro-1,3-butadiene ug/kg 12301640 75 46-130
Hexachlorobenzene ug/kg 12901640 79 58-130
Hexachlorocyclopentadiene ug/kg 874 v316405323-130
Hexachloroethane ug/kg 12001640 73 47-130
Indeno(1,2,3-cd)pyrene ug/kg 11601640 71 60-130
Isophorone ug/kg 11001640 67 49-130
N-Nitroso-di-n-propylamine ug/kg 11501640 70 47-130
N-Nitrosodimethylamine ug/kg 9481640 58 45-130
N-Nitrosodiphenylamine ug/kg 12001640 73 59-130
Naphthalene ug/kg 12101640 74 55-130
Nitrobenzene ug/kg 11401640 70 49-130
Pentachlorophenol ug/kg 2730 v132808310-132
Phenanthrene ug/kg 12201640 74 62-130
Phenol ug/kg 12601640 77 46-130
Pyrene ug/kg 13101640 80 53-130
Pyridine ug/kg 7931640 48 37-130
2,4,6-Tribromophenol (S)%94 27-110
2-Fluorobiphenyl (S)%75 30-110
2-Fluorophenol (S)%78 13-110
Nitrobenzene-d5 (S)%75 23-110
Phenol-d6 (S)%80 22-110
Terphenyl-d14 (S)%97 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2873819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92471459011
2873820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1690 63 18-13077 20 301690ND10701300
1,2-Dichlorobenzene ug/kg 1690 64 14-13075 15 301690ND10901270
1,3-Dichlorobenzene ug/kg 1690 63 12-13075 17 301690ND10601270
1,4-Dichlorobenzene ug/kg 1690 66 10-13078 17 301690ND11201320
1-Methylnaphthalene ug/kg 1690 58 12-13072 22 301690ND9811220
2,2'-Oxybis(1-
chloropropane)ug/kg 1690 59 10-13070 17 301690ND9981180
2,4,5-Trichlorophenol ug/kg 1690 72 13-13087 18 301690ND12301470
2,4,6-Trichlorophenol ug/kg 1690 69 17-13083 19 301690ND11701410
2,4-Dichlorophenol ug/kg 1690 66 10-13082 21 301690ND11301380
2,4-Dimethylphenol ug/kg 1690 64 10-13079 21 301690ND10801330
2,4-Dinitrophenol ug/kg 8470 18 10-13031 308470ND1560J2620
2,4-Dinitrotoluene ug/kg 1690 68 24-13083 21 301690ND11401410
2,6-Dinitrotoluene ug/kg 1690 68 23-13083 21 301690ND11401410
2-Chloronaphthalene ug/kg 1690 63 19-13079 22 301690ND10801340
2-Chlorophenol ug/kg 1690 68 10-13080 16 301690ND11501350
2-Methylnaphthalene ug/kg 1690 60 18-13074 22 301690ND10101260
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2873819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92471459011
2873820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol)ug/kg 1690 64 10-13079 21 301690ND10901330
2-Nitroaniline ug/kg 3390 63 17-13074 16 303390ND21302510
2-Nitrophenol ug/kg 1690 62 10-13078 23 301690ND10401320
3&4-Methylphenol(m&p
Cresol)ug/kg 1690 66 10-13079 18 301690ND11301340
3,3'-Dichlorobenzidine ug/kg 3390 65 10-13082 23 303390ND22102780
3-Nitroaniline ug/kg 3390 72 24-13085 17 303390ND24402880
4,6-Dinitro-2-methylphenol ug/kg R133904510-15266 37 303390ND15402230
4-Bromophenylphenyl ether ug/kg 1690 61 29-13074 20 301690ND10301250
4-Chloro-3-methylphenol ug/kg 3390 63 17-13077 21 303390ND21302620
4-Chloroaniline ug/kg 3390 65 14-13081 23 303390ND21902750
4-Chlorophenylphenyl ether ug/kg 1690 64 25-13076 18 301690ND10801290
4-Nitroaniline ug/kg 3390 72 22-13086 18 303390ND24302910
4-Nitrophenol ug/kg 8470 68 10-13084 20 308470ND57907110
Acenaphthene ug/kg 1690 65 20-13079 20 301690ND11001340
Acenaphthylene ug/kg 1690 66 25-13080 19 301690ND11101350
Aniline ug/kg 1690 62 10-13070 13 301690ND10401190
Anthracene ug/kg 1690 64 29-13077 18 301690ND10801300
Benzo(a)anthracene ug/kg 1690 66 19-13080 20 301690ND11101360
Benzo(a)pyrene ug/kg 1690 66 12-13080 20 301690ND11101350
Benzo(b)fluoranthene ug/kg 1690 73 14-13088 19 301690ND12401500
Benzo(g,h,i)perylene ug/kg 1690 58 10-13070 19 301690ND9811190
Benzo(k)fluoranthene ug/kg 1690 66 14-13079 19 301690ND11201350
Benzoic Acid ug/kg 8470 10 10-13010 308470ND811J822J
Benzyl alcohol ug/kg 3390 64 13-13075 16 303390ND21602530
bis(2-
Chloroethoxy)methane ug/kg 1690 58 16-13069 18 301690ND9761170
bis(2-Chloroethyl) ether ug/kg 1690 61 11-13073 18 301690ND10401240
bis(2-Ethylhexyl)phthalate ug/kg 1690 60 21-13078 27 301690ND10101330
Butylbenzylphthalate ug/kg 1690 63 23-13082 26 301690ND10701400
Chrysene ug/kg 1690 62 22-13075 20 301690ND10401280
Di-n-butylphthalate ug/kg 1690 60 30-13075 22 301690ND10201280
Di-n-octylphthalate ug/kg 1690 65 23-14277 17 301690ND11001310
Dibenz(a,h)anthracene ug/kg 1690 59 10-13075 24 301690ND10001270
Dibenzofuran ug/kg 1690 64 24-13077 20 301690ND10801310
Diethylphthalate ug/kg 1690 62 26-13075 20 301690ND10501280
Dimethylphthalate ug/kg 1690 64 22-13078 18 301690ND10901310
Fluoranthene ug/kg 1690 68 33-13080 17 301690ND11501360
Fluorene ug/kg 1690 65 22-13078 18 301690ND11001320
Hexachloro-1,3-butadiene ug/kg 1690 60 13-13078 25 301690ND10201320
Hexachlorobenzene ug/kg 1690 65 29-13080 20 301690ND11101350
Hexachlorocyclopentadiene ug/kg v316904510-13057 22 301690ND769964
Hexachloroethane ug/kg 1690 65 10-13075 14 301690ND11001270
Indeno(1,2,3-cd)pyrene ug/kg 1690 62 10-13076 20 301690ND10401280
Isophorone ug/kg 1690 57 13-13069 20 301690ND9621180
N-Nitroso-di-n-propylamine ug/kg 1690 63 12-13074 16 301690ND10601250
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/07/2020 10:14 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2873819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92471459011
2873820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/kg 1690 51 11-13061 19 301690ND8571030
N-Nitrosodiphenylamine ug/kg 1690 63 15-13077 20 301690ND10701310
Naphthalene ug/kg 1690 63 15-13075 17 301690ND10701270
Nitrobenzene ug/kg 1690 59 12-13072 20 301690ND9981220
Pentachlorophenol ug/kg v133907210-13090 22 303390ND24503060
Phenanthrene ug/kg 1690 63 27-13077 19 301690ND10701300
Phenol ug/kg 1690 68 10-13081 18 301690ND11501370
Pyrene ug/kg 1690 67 19-13083 22 301690ND11301410
Pyridine ug/kg 1690 46 10-13052 12 301690ND780880
2,4,6-Tribromophenol (S)%80 27-110102
2-Fluorobiphenyl (S)%61 30-11074
2-Fluorophenol (S)%69 13-11082
Nitrobenzene-d5 (S)%62 23-11076
Phenol-d6 (S)%71 22-11086
Terphenyl-d14 (S)%73 28-11098
REPORT OF LABORATORY ANALYSIS
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Page 56 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
538905
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92475353001
2873041SAMPLE DUPLICATE:
Percent Moisture %13.3 11 2514.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92475380002
2873042SAMPLE DUPLICATE:
Percent Moisture %91.9 0 2591.9
REPORT OF LABORATORY ANALYSIS
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Page 57 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1470312
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3524969-1
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 05/05/20 10:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3524969-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1213718-04
R3524969-3SAMPLE DUPLICATE:
Total Solids %96.9 0.150 1097.0
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 58 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1470313
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92475481005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3524990-1
Associated Lab Samples:92475481005
Matrix:Solid
AnalyzedMDL
Total Solids %ND 05/05/20 14:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3524990-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1214247-01
R3524990-3SAMPLE DUPLICATE:
Total Solids %83.0 0.452 1083.3
REPORT OF LABORATORY ANALYSIS
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Page 59 of 65
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92475481
RMR-006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1469626
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3524375-1
Associated Lab Samples:92475481001, 92475481002, 92475481003, 92475481004, 92475481005
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 05/04/20 10:030.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3524375-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.3510.0 93.5 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3524375-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1213718-04
R3524375-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg ML20.6 53.3 75.0-12556.6 6.05 2020.6ND 11.0 11.7
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3524375-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1213718-04
Chromium, Hexavalent mg/kg 744971 76.6 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1213718-01
R3524375-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.561J J1.79 200.551
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92475481005
R3524375-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92475481
RMR-006
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
RPD value was outside control limits.R1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 61 of 65
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92475481
RMR-006
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92475481001 538906 539457FG-1 (0-2)EPA 3546 EPA 8081B
92475481002 538906 539457FG-2 (0-2)EPA 3546 EPA 8081B
92475481003 538906 539457FG-3 (0-2)EPA 3546 EPA 8081B
92475481004 538906 539457FG-4 (0-2)EPA 3546 EPA 8081B
92475481005 538906 539457FG-DUP-1 EPA 3546 EPA 8081B
92475481001 1469565 1469565FG-1 (0-2)3050B EPA 6020B
92475481002 1469565 1469565FG-2 (0-2)3050B EPA 6020B
92475481003 1469565 1469565FG-3 (0-2)3050B EPA 6020B
92475481004 1469565 1469565FG-4 (0-2)3050B EPA 6020B
92475481005 1469565 1469565FG-DUP-1 3050B EPA 6020B
92475481001 1470231 1470231FG-1 (0-2)7471A EPA 7471B
92475481002 1470231 1470231FG-2 (0-2)7471A EPA 7471B
92475481003 1470231 1470231FG-3 (0-2)7471A EPA 7471B
92475481004 1470231 1470231FG-4 (0-2)7471A EPA 7471B
92475481005 1470231 1470231FG-DUP-1 7471A EPA 7471B
92475481001 539069 539677FG-1 (0-2)EPA 3546 EPA 8270E
92475481002 539069 539677FG-2 (0-2)EPA 3546 EPA 8270E
92475481003 539069 539677FG-3 (0-2)EPA 3546 EPA 8270E
92475481004 539069 539677FG-4 (0-2)EPA 3546 EPA 8270E
92475481005 539069 539677FG-DUP-1 EPA 3546 EPA 8270E
92475481001 539075 539100FG-1 (0-2)EPA 5035A EPA 8260D
92475481002 539075 539100FG-2 (0-2)EPA 5035A EPA 8260D
92475481003 539075 539100FG-3 (0-2)EPA 5035A EPA 8260D
92475481004 539075 539100FG-4 (0-2)EPA 5035A EPA 8260D
92475481005 539075 539100FG-DUP-1 EPA 5035A EPA 8260D
92475481006 539506FG-TRIP BLANK EPA 8260D
92475481001 538905FG-1 (0-2)ASTM D2974-87
92475481002 538905FG-2 (0-2)ASTM D2974-87
92475481003 538905FG-3 (0-2)ASTM D2974-87
92475481004 538905FG-4 (0-2)ASTM D2974-87
92475481005 538905FG-DUP-1 ASTM D2974-87
92475481001 1470312 1470312FG-1 (0-2)SM 2540 G SM 2540G
92475481002 1470312 1470312FG-2 (0-2)SM 2540 G SM 2540G
92475481003 1470312 1470312FG-3 (0-2)SM 2540 G SM 2540G
92475481004 1470312 1470312FG-4 (0-2)SM 2540 G SM 2540G
92475481005 1470313 1470313FG-DUP-1 SM 2540 G SM 2540G
92475481001 1469626 1469626FG-1 (0-2)3060A EPA 7199
92475481002 1469626 1469626FG-2 (0-2)3060A EPA 7199
92475481003 1469626 1469626FG-3 (0-2)3060A EPA 7199
92475481004 1469626 1469626FG-4 (0-2)3060A EPA 7199
92475481005 1469626 1469626FG-DUP-1 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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Page 62 of 65
Page 63 of 65
Page 64 of 65
Page 65 of 65

Appendix C
DEQ Risk Calculator

Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Prepared By:Hart & Hickman, PC
SPH
RWM
Site Wide Soil - Hypothetical Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
South Tryon Commercial
340 W. Tremont, Charlotte, Mecklenburg County
Division of Waste Management - Brownfields Program
South Tryon Commercial - BF No. 22007-18-060
December 2019
November 2019 EPA RSL Table
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: South Tryon Commercial - BF No. 22007-18-060
Exposure Unit ID: Site Wide Soil - Hypothetical Worst Case
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration to Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: December 2019Basis: November 2019 EPA RSL TableSite ID: South Tryon Commercial - BF No. 22007-18-060Exposure Unit ID: Site Wide Soil - Hypothetical Worst CaseExposure Point Concentration (mg/kg)Notes: CAS Number ChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion0.014 67-64-1 Acetonemg/kg0.0314 309-00-2 Aldrinmg/kg3.14 7440-38-2 Arsenic, Inorganic mg/kg74.9 7440-39-3 Bariummg/kg0.364 12789-03-6 Chlordane mg/kg74.9 16065-83-1 Chromium(III), Insoluble Salts mg/kg0.447 18540-29-9 Chromium(VI) mg/kg0.414 60-57-1 Dieldrinmg/kg0.0019 100-41-4 Ethylbenzene mg/kg47.1 7439-92-1 ~Lead and Compounds mg/kg0.0464 7439-97-6 ~Mercury (elemental) mg/kg0.0049 1330-20-7 Xylenesmg/kgInput Form 2ASoil Exposure Point Concentration TableDescription of Exposure Point Concentration Selection:North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: South Tryon Commercial - BF No. 22007-18-060
Exposure Unit ID: Site Wide Soil - Hypothetical Worst Case
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use* NC NC NC
Soil 4.2E-06 2.0E-02 NO
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: South Tryon Commercial - BF No. 22007-18-060
Exposure Unit ID: Site Wide Soil - Hypothetical Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.014 0.014 0.014 1.3E-08 7.1E-09 2.0E-08
309-00-2 Aldrin 0.0314 0.0314 0.0314 1.6E-07 6.9E-09 1.7E-07 9.0E-04 9.0E-04
7440-38-2 Arsenic, Inorganic 3.14 3.14 3.14 8.6E-07 1.8E-07 1.9E-11 1.0E-06 5.4E-03 1.1E-03 8.1E-07 6.5E-03
7440-39-3 Barium 74.9 74.9 74.9 3.2E-04 5.8E-07 3.2E-04
12789-03-6 Chlordane 0.364 0.364 0.364 3.9E-08 6.6E-09 1.8E-09 4.7E-08 6.2E-04 1.1E-04 7.3E-05 8.0E-04
16065-83-1 Chromium(III), Insoluble Salts 74.9 74.9 74.9 4.3E-05 4.3E-05
18540-29-9 Chromium(VI) 0.447 0.447 0.447 6.8E-08 5.2E-11 6.8E-08 1.3E-04 1.7E-08 1.3E-04
60-57-1 Dieldrin 0.414 0.414 0.414 2.0E-06 8.6E-07 2.6E-12 2.9E-06 7.1E-03 3.0E-03 1.0E-02
100-41-4 Ethylbenzene 0.0019 0.0019 0.0019 6.4E-12 6.4E-11 7.1E-11 1.6E-08 7.2E-08 8.8E-08
7439-92-1 ~Lead and Compounds 47.1 47.1 47.1 <SL** <SL** <SL**
7439-97-6 ~Mercury (elemental) 0.0464 0.0464 0.0464 9.6E-04 9.6E-04
1330-20-7 Xylenes 0.0049 0.0049 0.0049 2.1E-08 1.8E-06 1.9E-06
Cumulative: 4.2E-06 2.0E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator