22042_Matheson Ave_ Export Approval_Assessment Plan 20210504

May 4, 2021
Sent Via Email Mr. Dan Fitzpatrick BP NODA, LLC and BP Trail, LLC
3328 Peachtree Rd, NE, Suite 100 Atlanta, GA 30032 [e-mail]
Subject: Brownfields Soil Management Options Updated
Matheson Ave Brownfields Properties Charlotte, Mecklenburg County Brownfields Project Number: 22042-18-060 and 23015-19-060
Dear Mr. Fitzpatrick:
The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received and reviewed a request to export an approximate 2,000 cubic yards of soils from Matheson Ave II (22042-18-060) and Matheson Ave Creek (23015-19-060) (collectively, Matheson Ave)
Brownfields Properties. This request was submitted on your behalf by Mr. Eric Wysong of Apex
Engineering, LLC (Apex). DEQ understands the redevelopment on the Matheson Ave Brownfields Properties will be done jointly under the DEQ-approved Environmental Management Plan (EMP) dated November 26, 2019.
DEQ Brownfields reviewed the soil analytical data provided in the Brownfields Export Soil
Assessment Report Addendum dated May 3, 2021 prepared by Apex. Based on our review of the data, DEQ Brownfield’s agree that these soils may be exported as outlined in the table below. Stockpile Area Disposal Options
SP-03 Reeves, CDLF, MSWLF
SP-04 Reeves, CDLF, MSWLF SP-05 MSWLF
Reeves = Reeve’s LCID Landfill (Permit No. 60-S-LCID) CDLF = Construction & Demolition landfill MSWLF = Municipal Solid Waste landfill facility
Matheson Ave
May 4, 2021 Page 2

All soil export must be conducted under the DEQ Brownfields approved EMP. Per the Matheson
Ave EMP, the soils will be field screened during excavation prior to export from the property. If unanticipated impacts are identified during excavation, please refer to the EMP for further actions and cease transfer until appropriate characterization can be completed. In addition, in accordance with the approved EMP, annual Redevelopment Summary Reports will be submitted to DEQ Brownfields. Details related to the disposition of this soil including but not limited to, total
volume, general description of field screening efforts, etc. should be included with each Property’s Redevelopment Summary Report. Please be advised that this approval does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local
entities. If you have questions about this correspondence or require additional information, please feel free to contact me by phone at 704-661-0330 or by email at [e-mail]. Sincerely,
Carolyn Minnich Brownfields Project Manager
ec: Brownfields Property Management Unit Eric Wysong [e-mail] Stephen A. McCullers [e-mail]
Brownfields Export Soil Assessment Report – Addendum May 3, 2021 Matheson Ave II Page i

TABLE OF CONTENTS Section Page
1.0 INTRODUCTION ............................................................................................................. 1
2.0 SOIL SAMPLING ACTIVITIES ........................................................................................ 2
2.1 Sampling Methodology ........................................................................................ 2
2.2 Analytical Results ................................................................................................. 3
2.3 Risk Calculation ................................................................................................... 5
3.0 DISCUSSION .................................................................................................................. 7
4.0 CONCLUSIONS .............................................................................................................. 8
FIGURES Figure 1 Site Location Map Figure 2 Site Plan TABLES Table 1 Summary of Soil Analytical Detections Table 2 Metals Analytical Results – Matheson Sites and Reeves LCID
APPENDICES Appendix A Laboratory Analytical Report Appendix B NCDEQ Risk Calculator Output Sheets
Brownfields Export Soil Assessment Report – Addendum May 3, 2021 Matheson Ave II Page 1

1.0 INTRODUCTION
Maryland Apex Engineering, PC (Apex), a North Carolina licensed business entity of Apex
Companies, LLC, has prepared this Brownfields Export Soil Assessment Report Addendum on
behalf of the Brownfields Prospective Developers (PD), BP NODA, LLC and BP Trail, LLC. This
report documents sampling activities conducted prior to a proposed soil export at the Brownfields
sites located at 255 Matheson Avenue in Charlotte, North Carolina (the “Site”) (Figure 1). On
February 4th, 2019 and July 12th, 2019 Notices of Brownfields Property (NBP) were filed for the
Site to be developed for multi-family residential use and for development of a recreational
Greenway (Matheson Ave II and Matheson Ave Creek, respectively). Planned development
includes several multi-level residential buildings, associated amenities, a paved recreational path,
and a bridge over Little Sugar Creek. The Brownfields projects are being developed concurrently
under an Environmental Management Plan (EMP), approved and signed by the North Carolina
Department of Environmental Quality (NCDEQ) on November 27, 2019. Redevelopment
activities at the Site commenced in April 2020 and have consisted of land-clearing, grading,
construction of structural walls, construction of a bridge over Little Sugar Creek, utility work, and
initial construction of building foundations and split-walls.
Soil that is unsuitable for re-use due to geophysical properties has been generated from three
general areas in the southern portion of the Site from the excavation of soil around a sewer utility
installation and at the base of structural walls. See Figure 2 depicting the approximate locations
of the soil excavations and the resulting soil stockpile area. The stockpiled soil was determined
not suitable for re-use at the Site due to geophysical properties. Approximately 1,500 cubic yards
of the stockpiled soil was characterized for proposed export to the Reeves Land Clearing and
Inert Debris (Reeves LCID) landfill located at 2323 Salome Church Road in Charlotte, North
Carolina as documented in an April 1, 2021 dated Brownfields Export Soil Assessment Report.
Upon review of the Brownfields Soil Assessment Report, the NCDEQ approved export of the
characterized soil to Reeves LCID in an April 2, 2021 dated approval letter. The soil was
subsequently transported to Reeves LCID. However, approximately 3,000 cubic yards of soil
remained in the Site as it was anticipated the soil could be reused in non-structural applications
throughout the Site. Upon further review, it has been determined that the soil could not be re-
used onsite and will also require export. As such, the following report addendum documents
characterization activities performed on the remaining 3,000 cubic yards of soil. Assessment
activities were performed in accordance with the approved EMP following the characterization
requirements and analytical program as outlined in Part 1.A. Number 4 of the approved EMP.
Brownfields Export Soil Assessment Report – Addendum May 3, 2021 Matheson Ave II Page 2

2.0 SOIL SAMPLING ACTIVITIES
On April 7, 2021, Apex conducted soil sampling activities in accordance with the NCDEQ
approved EMP and in general accordance with the NCDEQ IHSB Guidelines for Assessment and
Cleanup of Contaminated Sites dated January 2020. The methodology and results are
summarized in the following sections.
2.1 Sampling Methodology
The stockpile area was surveyed by the onsite grading contractor and determined to comprise a
total of approximately 3,000 cubic yards of soil. The general locations of the excavated material
source areas and stockpile area are identified on the attached Figure 2.
The stockpile area was divided in thirds (SP-03, SP-04, and SP-05), each of which comprise an
estimated 1,000 cubic yards of soil. Each of the three areas was further divided into four
approximately equally sized quadrants based on a visual evaluation (SP-03a through SP-03d,
SP-04a through SP-04d, and SP-05a through SP-05d). At each quadrant, one grab soil sample
was collected at depths ranging from approximately two to six feet into the stockpile using a
decontaminated stainless-steel hand auger and an onsite track-mounted excavator. Each of the
grab soil samples were field screened for the presence of odor, staining, and elevated
photoionization detector (PID) readings. The stockpiled material was observed to consist
primarily of soil with some rock and woody vegetation included. A faint “rotten” odor was noted
during sampling, which is attributed to decay of organic material within the moist stockpiles. No
distinctive odors of an environmental concern were noted, such as petroleum or solvent odors,
and no staining was observed. There were no PID detections in any of the SP-03 grab samples.
PID readings ranged from non-detect to 0.1 parts per million (ppm) in the SP-04 grab samples
and non-detect to 0.2 ppm in the SP-05 grab samples.
The deepest grab sample from SP-03 and the grab samples with the highest PID detections from
SP-04 and SP-05 were selected and placed in laboratory-supplied sample containers, labeled,
and placed in a laboratory supplied cooler with ice. The samples were then hand delivered to
Pace Analytical in Huntersville, North Carolina under standard chain-of-custody protocol for
analysis of volatile organic compounds (VOCs) by EPA Method 8260D, preparation Method 5035.
After the selected VOC soil sample from each of the three stockpiles was collected and prepared,
the four grab soil samples from each stockpile were composited into one composite soil sample
per stockpile using a decontaminated stainless-steel bowl and spoon. The three composite soil
Brownfields Export Soil Assessment Report – Addendum May 3, 2021 Matheson Ave II Page 3

samples were placed in laboratory-supplied sample containers, labeled, and placed in a
laboratory supplied cooler with ice. The samples were then hand delivered to Pace Analytical in
Huntersville, North Carolina for analysis of semi-volatile organic compounds (SVOCs) by EPA
Method 8270E, hexavalent chromium by EPA Method 7199, metals (arsenic, barium, cadmium,
total chromium, lead, manganese, selenium, and silver) by EPA Method 6010D, mercury by EPA
Method 7471B, and Synthetic Precipitation Leaching Procedure (SPLP) by EPA Method 1312
followed by manganese analysis of the leachate by EPA Method 6010D. The SPLP and additional
manganese analysis of the leachate was performed as an added measure due to the proposed
export of the soil to an unlined landfill. As an added quality control measure, one duplicate soil
sample (SP-DUP) was collected from the SP-05 stockpile soil sample and analyzed for the same
parameters as the parent sample.
2.2 Analytical Results
The soil sample results were compared to the January 2021 NCDEQ Preliminary Soil
Remediation Goals (PSRGs) for Protection of Groundwater (PoG), Residential Health-Based
Direct Contact (Residential), and Industrial/Commercial Health-Based Direct Contact
(Industrial/Commercial). The results of the manganese analyses on the SPLP leachates were
compared to the 15A NCAC 2L Groundwater Quality Standard (2L Standard) for manganese.
The analytical detections are summarized as follows:
VOCs
Laboratory analytical detections of VOCs are summarized as follows:
• Cyclohexane, ethylbenzene, methylcyclohexane, toluene, and xylenes were detected in
the sample collected from SP-03, all at concentrations below applicable PSRGs. No other
VOCs were detected in SP-03;
• No VOCs were detected in the sample collected from SP-04;
• Acetone, 2-butanone, ethylbenzene, and toluene were detected in the sample collected
from SP-05, all at concentrations below applicable PSRGs. No other VOCs were detected
in SP-05; and,
• Acetone, ethylbenzene, and toluene were detected in the duplicate sample collected from
SP-05 (SP-DUP), all at concentrations below applicable PSRGs. No other VOCs were
detected in SP-DUP.
Brownfields Export Soil Assessment Report – Addendum May 3, 2021 Matheson Ave II Page 4

SVOCs
Laboratory analytical detections of SVOCs are summarized as follows:
• No SVOCs were detected in the samples collected from SP-03, SP-04, or the duplicate
sample collected from SP-05 (SP-DUP); and,
• Benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, chrysene, fluoranthene,
phenanthrene, and pyrene were detected in the sample collected from SP-05. All detected
concentrations were below applicable PSRGs with the exception of benzo(a)pyrene,
which was detected at an estimated J-flagged concentration of 0.224 milligrams per
kilogram (mg/kg), exceeding the Residential and PoG PSRGs of 0.11 mg/kg and 0.12
mg/kg respectively. No other SVOCs were detected in SP-05.
Metals
Laboratory analytical results did not identify detectable concentrations of silver in any of the four
samples (SP-03, SP-04, SP-05, and SP-DUP). Several metals were detected in each of the
samples, summarized as follows:
• Arsenic concentrations ranged from an estimated J-flag concentration of 0.77 mg/kg at
SP-04 to 2.0 mg/kg at SP-05. All detected concentrations of arsenic exceeded the
Residential PSRG but were below Industrial/Commercial and PoG PSRGs;
• Barium concentrations ranged from 75.3 mg/kg at SP-04 to 90.2 mg/kg at SP-03. All
detected concentrations of barium were below applicable PSRGs;
• Cadmium concentrations ranged from non-detect at SP-04 to 0.092 at SP-05. All detected
concentrations of cadmium were below applicable PSRGs;
• Total Chromium concentrations ranged from 38.1 mg/kg at SP-05 to 54.8 mg/kg at SP-03.
Hexavalent chromium was detected in SP-03 at an estimated J-flagged concentration of
0.636 mg/kg, which exceeded the Residential PSRG but was below Industrial/Commercial
and PoG PSRGs. Hexavalent chromium was not detected in any other sample and all
detected concentrations of total chromium were below applicable PSRGs for trivalent
chromium;
• Lead concentrations ranged from 9.8 mg/kg at SP-04 to 16.1 mg/kg at SP-05. All detected
concentrations of lead were below applicable PSRGs;
Brownfields Export Soil Assessment Report – Addendum May 3, 2021 Matheson Ave II Page 5

• Manganese concentrations ranged from 482 mg/kg at SP-05 to 636 mg/kg at SP-03. All
detected concentrations of manganese exceeded the Residential and PoG PSRGs, but
are below the Industrial/Commercial PSRG;
• Mercury concentrations ranged from 0.042 mg/kg at SP-03 to 0.068 mg/kg at SP-05. All
detected concentrations of mercury were below applicable PSRGs;
• Selenium concentrations ranged from 1.9 mg/kg at SP-05 to 2.0 mg/kg at SP-03, SP-04,
and SP-DUP. All detected concentrations of selenium were below applicable PSRGs;
and,
• Concentrations of manganese in the leachate following the SPLP were below the 2L
Standard of 50 micrograms per liter (µg/L) in SP-03 (13 µg/L), SP-04 (39 µg/L), and SP-05
(38 µg/L). However, the concentration of manganese in the leachate from the SP-05
duplicate sample (SP-DUP) was reported at 61 µg/L, exceeding the 2L Standard of 50
µg/L.
The analytical detections for the prior export soil sampling conducted in February 2021 (SP-01
and SP-02) were generally consistent with the analytical detections for the additional stockpile
samples analyzed in April 2021 (SP-03, SP-04, and SP-05) with the exception of the SVOC
detections in SP-05. The stockpiles associated with SP-01 and SP-02 were exported to Reeves
LCID in April 2021 under the April 2, 2021 dated NCDEQ approval. The soil associated with all
five stockpile samples were generated from the same general areas of the Site as show on
Figure 2 and the analytical detections for all five stockpiles are summarized in Table 1. The
complete laboratory analytical report for SP-03 through SP-05 is included as Appendix A.
2.3 Risk Calculation
In anticipation of a potential transfer to the Reeves LCID facility, the analytical data collected from
the soil proposed to be exported from the Site were compared to background metals
concentrations at the Reeves LCID (data obtained from Hart & Hickman’s Soil Management
Options Letter Report dated August 7, 2020; Manganese data provided February 19, 2021).
Metals concentrations between the Site and the Reeves LCID are generally similar and within the
range of expected naturally occurring concentrations. Concentrations of all metals except for
manganese and hexavalent chromium were slightly higher at the Reeves LCID than in the
Matheson Site soil. The metals results for the Matheson Site soils (SP-01 through SP-05) and
the prior Reeves LCID data are summarized in the attached Table 2.
Brownfields Export Soil Assessment Report – Addendum May 3, 2021 Matheson Ave II Page 6

The analytical results were further evaluated using the NCDEQ Risk Calculator (January 2021
version) by entering the highest concentrations of each VOC and SVOC detected in the February
and April 2021 stockpile sampling events and the highest concentration of each metal shown on
Table 2 to evaluate the risk associated with the proposed transfer of these soils (SP-03, SP-04,
and SP-05) combined with previously exported soils (SP-01 and SP-02) and reported metals
concentrations at the Reeves LCID. The risk calculator was used to evaluate the carcinogenic
and non-carcinogenic risks for residential direct contact, non-residential worker direct contact,
and construction worker exposure scenarios. The NCDEQ acceptable threshold for cumulative
carcinogenic risk is typically 1.0 x 10-4 and the acceptable threshold for cumulative non-
carcinogenic hazard is a hazard index equal to or less than 1.0. The results of the risk calculator
indicate the following:
• Residential direct contact with soil:
o Cumulative carcinogenic risk of 8.9 x 10-6
o Cumulative hazard index of 5.4 x 10-1
• Non-residential worker direct contact with soil:
o Cumulative carcinogenic risk of 1.2 x 10-6
o Cumulative hazard index of 3.7 x 10-2
• Construction worker direct contact with soil:
o Cumulative carcinogenic risk of 3.6 x 10-7
o Cumulative hazard index of 3.6
The results of the risk calculations indicate that calculated carcinogenic risk and non-carcinogenic
hazard for the worst-case scenario based on the February and April 2021 analytical results from
the Site combined with the Reeves LCID metals data are well below typical thresholds set by
NCDEQ for residential direct contact and non-residential worker direct contact exposure
scenarios. The construction worker direct contact cumulative hazard index is calculated at 3.6, a
result is largely driven by manganese concentrations that are presumed to be naturally-occurring.
Furthermore, construction worker exposure at the Reeves LCID is not considered a likely
exposure scenario once the soils have been placed. The output sheets from the NCDEQ Risk
Calculator are included as Appendix B.
Brownfields Export Soil Assessment Report – Addendum May 3, 2021 Matheson Ave II Page 7

3.0 DISCUSSION
Several VOCs and SVOCs were detected within the samples, all at concentrations below
applicable PSRGs, with the exception of benzo(a)pyrene at SP-05. The SP-05 sample contained
low concentrations of several SVOCs, all of which are polycyclic aromatic hydrocarbons (PAHs).
The PAHs detected in SP-05 are ubiquitous in urban environments as they form from the
incomplete combustion of organic materials such as coal, petroleum, and wood. Apex noted
limited amounts of woody debris and rock in the soil stockpiles, but no staining, coal, petroleum
odors, or partially burned materials were noted at the time of sampling. Based on the detection
of several PAHs in the SP-05 sample but not in the associated duplicate sample, the PAH impacts
to SP-05 are considered to be minimal in extent. Furthermore, cumulative risk calculations
including the highest reported concentrations of VOCs, SVOCs, and metals in all stockpile
samples fall below applicable risk thresholds for a residential exposure scenario, suggesting no
unacceptable risk is present for direct contact with this soil in a residential setting. However, no
SVOC data is available for the Reeves LCID and export of the SP-05 soil to Reeves LCID would
pose a risk of introducing a new contaminant at concentrations above applicable PSRGs,
specifically benzo(a)pyrene above its Residential and PoG PSRGs.
Arsenic and manganese were detected at concentrations exceeding the Residential and/or PoG
PSRGs in all samples and hexavalent chromium was detected at a concentration exceeding the
Residential PSRG in one sample (SP-03). The detected concentrations of arsenic and
manganese are consistent with data previously collected throughout the Site and are within the
range of expected background concentrations for the area. Although the J-flagged hexavalent
chromium detection in the SP-03 sample (0.636 mg/kg) is slightly higher than the highest
detection from the Reeves LCID (J-flagged 0.43 mg/kg), three of the five Reeves LCID samples
contained hexavalent chromium and only one of the five Matheson Site stockpile samples
contained hexavalent chromium. All hexavalent chromium detections from Reeves and Matheson
Site were estimated J-flagged results. Furthermore, there were no exceedances of the
hexavalent chromium PoG PSRG and the results of the risk calculator indicated cumulative risks
for residential and non-residential direct contact exposure scenarios are below applicable
thresholds. No other metals were detected at concentrations above PSRGs.
The concentrations of manganese detected in the SPLP leachates were below the applicable 2L
Standard in all of the samples with the exception of the SP-DUP sample. The mean average of
manganese concentration in leachate for SP-05 (38 µg/L) and the associated SP-DUP (61 µg/L)
Brownfields Export Soil Assessment Report – Addendum May 3, 2021 Matheson Ave II Page 8

calculates to be 49.5 µg/L, which is below the 2L Standard of 50 µg/L. Therefore, risk to
groundwater from leaching of manganese is not considered to be a concern with the Matheson
Site soil.
4.0 CONCLUSIONS
Apex has completed export soil sampling activities at the Matheson Ave Brownfields properties
located at 255 Avenue in Charlotte, North Carolina. Sampling included collection of three
stockpile samples (SP-03, SP-04, and SP-05) and one duplicate sample (SP-DUP) to
characterize Site soil for proposed offsite export to the Reeves LCID. The results of the export
soil sampling activities have identified low concentrations of VOCs and SVOCs below applicable
PSRGs, with the exception of benzo(a)pyrene in SP-05. Several metals were detected within soil
samples at concentrations within the expected range of naturally occurring background levels and
comparable to prior data available for Reeves LCID.
The analytical results of this assessment and the results from prior soil assessment at the Site
(February 2021; SP-01 and SP-02) were evaluated using the NCDEQ Risk Calculator by entering
the highest concentration for each of the detected VOCs and SVOCs at the Site and the highest
metals concentrations from the combined dataset, which also includes prior Reeves LCID metals
data. Based on the results of the risk calculations, the cumulative carcinogenic and non-
carcinogenic risk were determined to be below acceptable limits for direct contact soil exposure
scenarios including resident and non-residential worker. Additionally, SPLP analysis of
manganese in the Matheson Site stockpile samples show that manganese is not expected to
leach from this soil at a concentration great enough to create a groundwater quality concern.
Although results from the NCDEQ Risk Calculator indicate no unacceptable risk exists for export
of soil from SP-03, SP-04, and SP-05 to the Reeves LCID, export of soil from SP-05 to Reeves
LCID could result in the introduction of a new contaminant above its applicable PSRGs,
specifically benzo(a)pyrene. Based on the data available, Apex does not recommend export of
soil from SP-05 to the Reeves LCID. Based on the results of this assessment, export of soil from
SP-03 and SP-04 should pose no unacceptable risk to the Reeves LCID. As such, Apex requests
NCDEQ approval for the export of up to 2,000 cubic yards of soil from SP-03 and SP-04 to the
Reeves LCID.

FIGURES
USGS The National Map: National Boundaries Dataset, 3D Elevation Program,
Geographic Names Information System, National Hydrography Dataset,
National Land Cover Database, National Structures Dataset, and National
Transportation Dataset; U.S. Census Bureau - TIGER/Line
CHECK BY: EW
DRAWN BY: SP
DATE: 11/30/17
SCALE: AS SHOWN
CAD NO.: 510551-001
PRJ NO.: 510551-001
FIGURE
SITE LOCATION MAP
0$7+(621$9(,,$1'
0$7+(621$9(&5((.6,7(6
CHARLOTTE, NORTH CAROLINA
01,0002,000
Feet
1
SITE LOCATION
2
FigureSITE PLAN
MATHESON AVE II AND MATHESON AVE CREEK
SITES CHARLOTTE, NORTH CAROLINA
CHECKED BY: EW
DRAWN BY: CN
DATE APRIL 2021
SCALE Not to Scale
PROJECT NO. 510621.001
APPROXIMATE SOIL EXCAVATION AREAS
APPROXIMATE LOCATION OF SOIL STOCKPILES
LEGEND
BASE DRAWING TAKEN FROM KMLEY HORN EROSION CONTROL PLAN DATED 11/08/2019
BRIDGE – PARTIALLY DEVELOPED
BUILDING FOUNDATION –
PARTIALLY DEVELOPED
BUILDING FOUNDATION –
PARTIALLY DEVELOPED
BUILDING FOUNDATION –
PARTIALLY DEVELOPED
SP-04SP-05
SP-03

TABLES

TABLE 1
Soil Stockpile Analytical Detections - April 2021
Brownfields Project Numbers 22042-18-060 23015-19-060
255 Matheson Avenue
Charlotte, North Carolina
SP-01 SP-02
SP-DUP
(SP-02)SP-03 SP-04 SP-05
SP-DUP
(SP-05)
IHSB Residential PSRG
Standards
IHSB
Industrial/Commercia
l PSRG Standards
IHSB Protection of
Groundwater PSRG
Standards
Acetone < 0.0457 < 0.0391 < 0.0428 < 0.0399 < 0.0385 0.116 J 0.0895 J 12,000 140,000 25
Bromomethane <0.0113 0.0331 < 0.0105 < 0.0098 < 0.0095 < 0.0123 < 0.0115 1.4 6.4 0.050
2-Butanone (MEK)< 0.0342 < 0.0292 < 0.0320 < 0.0299 < 0.0288 0.0408 J < 0.0350 5,500 40,000 17
Cyclohexane < 0.0043 < 0.0037 < 0.0040 0.0059 J < 0.0036 < 0.0047 < 0.0044 1,400 5,800 NE
Ethylbenzene < 0.0033 < 0.0028 < 0.0031 0.0044 J < 0.0028 0.0117 0.0111 6.1 27 13
Methylcyclohexane 0.0328 < 0.0064 < 0.0070 0.0256 < 0.0063 < 0.0082 < 0.0077 NE NE NE
Methyl acetate < 0.0123 0.143 0.133 < 0.0108 < 0.0104 < 0.0135 < 0.0127 16,000 230,000 29
Toluene 0.0056 J 0.0041 J 0.0049 J 0.0073 < 0.0017 0.0565 0.0407 990 9,700 8.3
Xylene (Total)0.0062 J < 0.0035 < 0.0038 0.0171 < 0.0034 < 0.0044 < 0.0042 120 530 9.9
Benzo(a)anthracene < 0.135 < 0.130 < 0.138 < 0.138 < 0.141 0.257 J < 0.150 1.1 21 0.35
Benzo(a)pyrene < 0.183 < 0.177 < 0.188 < 0.143 < 0.146 0.224 J < 0.155 0.11 2.1 0.12
Benzo(b)fluoranthene < 0.170 < 0.164 < 0.175 < 0.138 < 0.141 0.257 J < 0.150 1.1 21 1.2
Chrysene < 0.123 < 0.118 < 0.126 < 0.150 < 0.154 0.254 J < 0.163 110 2,100 36
Fluoranthene < 0.128 < 0.123 < 0.131 < 0.141 < 0.145 0.603 < 0.154 480 6,000 670
Phenanthrene < 0.106 < 0.103 < 0.109 < 0.135 < 0.138 0.553 < 0.147 NE NE NE
Pyrene < 0.116 < 0.112 < 0.119 < 0.168 < 0.172 0.452 < 0.182 360 4,500 440
bis(2-Ethylhexyl)phthalate < 0.423 0.156 J < 0.434 < 0.160 < 0.164 < 0.159 < 0.174 39 160 14
Arsenic 2.9 2.4 J 2.1 J 1.1 J 0.77 J 2.0 2.0 J 0.68 3.0 5.8
Barium 93.7 86.8 85.5 90.2 75.3 85.8 85.7 3,100 47,000 580
Cadmium 0.093 0.087 J 0.079 J 0.067 J < 0.046 0.092 0.078 J 14 200 3.0
Chromium (III)39.3 48.3 41.7 54.8 46.3 38.1 40.9 23,000 350,000 360,000
Chromium (VI)< 0.329 < 0.345 < 0.324 0.636 J < 0.315 < 0.316 < 0.327 0.31 6.5 3.8
Lead 17.5 14.1 10.8 11.5 9.8 16.1 15.9 400 800 270
Manganese 578 746 685 636 576 482 503 380 5,600 65
Mercury 0.041 0.038 0.038 0.042 0.049 0.068 0.060 4.7 70 NE
Selenium < 0.46 < 0.48 < 0.46 2.0 2.0 1.9 2.0 78 1,200 2.1
Manganese 3.7 J 9.2 12 13 39 38 61
Notes:
Only analytes detected in one or more samples included on table above with the exception of hexavalent chromium, not detected in any sample
mg/kg = milligrams per kilogram
µg/L = micrograms per liter
NCDEQ = North Carolina Department of Environmental Quality
PSRG = Preliminary Soil Remediation Goals
IHSB Standards = Inactive Hazardous Sites Branch PSRG for residential/industrial health (January 2021)
VOCs = Volatile Organic Compounds
SVOCs = Semi-Volatile Organic Compounds
SPLP = Synthetic Precipitation Leaching Procedure
Bold / Underlined concentrations exceed the Residential PSRG
Bold / Italicized concentrations exceed the Protection of Groundwater PSRG
NE = PSRG not established
< = Result below laboratory method detection limit
J = Result is below laboratory reporting limit but above laboratory detectin limit; considered to be an estimated concentration
SP-DUP = Blind field soil duplicate (collected from SP-02)
50
Metals by USEPA Method 6010/7471/7199 (mg/kg)
SPLP (USEPA Method 1312) Manganese by USEPA Method 6010 (µg/L)15A NCAC 2L Groundwater Quality Standard
Analyte
SAMPLE ANALYTICAL RESULTS NCDEQ PSRG
VOCs by USEPA Method 8260 (mg/kg)
SVOCs by USEPA Method 8270 (mg/kg)
SAMPLE ANALYTICAL RESULTS
TABLE 2
Metals Analytical Results - Matheson Sites and Reeves LCID
Brownfields Project Numbers 22042-18-060 23015-19-060
255 Matheson Avenue
Charlotte, North Carolina
SP-01 SP-02
SP-DUP
(SP-02)SP-03 SP-04 SP-05
SP-DUP
(SP-05)BKG-R-01 BKG-R-02 BKG-R-03 BKG-R-04 BKG-R-05
Arsenic 2.9 2.4 J 2.1 J 1.1 J 0.77 J 2.0 2.0 J 3.0 1.9 2.6 2.2 1.9 0.68 3.0 5.8
Barium 93.7 86.8 85.5 90.2 75.3 85.8 85.7 120 77 J 91 J 130 150 3,100 47,000 580
Cadmium 0.093 0.087 J 0.079 J 0.067 J < 0.046 0.092 0.078 J 0.13 J 0.075 J < 0.044 0.1 J < 0.047 14 200 3.0
Chromium (III)39.3 48.3 41.7 54.8 46.3 38.1 40.9 57.76 35.72 45.76 46.57 57.67 23,000 350,000 360,000
Chromium (VI)< 0.329 < 0.345 < 0.324 0.636 J < 0.315 < 0.316 < 0.327 < 0.24 0.28 J < 0.24 0.43 J 0.33 J 0.31 6.5 3.8
Lead 17.5 14.1 10.8 11.5 9.8 16.1 15.9 15 10 12 29 6.7 400 800 270
Manganese 578 746 685 636 576 482 503 550 470 510 420 330 380 5,600 65
Mercury 0.041 0.038 0.038 0.042 0.049 0.068 0.060 0.097 0.03 J 0.047 J 0.07 0.055 J 4.7 70 NE
Selenium < 0.46 < 0.48 < 0.46 2.0 2.0 1.9 2.0 6.4 4.8 6.1 4.9 5.9 78 1,200 2.1
Silver < 0.23 < 0.24 < 0.23 < 0.24 < 0.23 < 0.19 < 0.20 0.54 J <0.055 <0.061 0.11 J <0.065 78 1,200 3.4
Notes:
1 Matheson Sites soil stockpile metals concentrations; stockpile samples collected February 2021 and exported to Reeves LCID in March 2021.
2 Matheson Sites soil stockpile metals concentrations; stockpile samples collected April 2021.
mg/kg = milligrams per kilogram
NCDEQ = North Carolina Department of Environmental Quality
PSRG = Preliminary Soil Remediation Goals
Bold / Underlined concentrations exceed the Residential PSRG
Bold / Italicized concentrations exceed the Protection of Groundwater PSRG
NE = PSRG not established
< = Result below laboratory method detection limit
J = Result is below laboratory reporting limit but above laboratory detectin limit; considered to be an estimated concentration
SP-DUP = Blind field soil duplicate (collected from SP-02)
3 Reeves Land Clearing and Inert Debris landfill, located at 2323 Salome Church Road, Charlotte, NC; data taken from Hart & Hickman background metals assessment for Reeve's LCID (Soil Management Options, dated August 7, 2020; Manganese data
provided 2/19/2021).
Residential
PSRG
Industrial /
Commercial
PSRG
Protection of
Groundwater
PSRG
Analyte
SAMPLE ANALYTICAL RESULTS (mg/kg) NCDEQ PSRG (mg/kg)
REEVES LCID 3MATHESON SITES
March 2021 1 April 2021 2

APPENDIX A

Laboratory Analytical Report
#=CL#
April 19, 2021
LIMS USE: FR - ERIC WYSONG
LIMS OBJECT ID: 92531940
92531940
Project:
Pace Project No.:
RE:
Eric Wysong
Apex Companies
5900-O Northwoods Business
Parkway
Charlotte, NC 28269
MATHESON AVENUE SITES
Dear Eric Wysong:
Enclosed are the analytical results for sample(s) received by the laboratory on April 08, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 50
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 50
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Lab ID Sample ID Matrix Date Collected Date Received
92531940001 SP-03 Solid 04/07/21 17:15 04/08/21 09:30
92531940002 SP-04 Solid 04/07/21 16:35 04/08/21 09:30
92531940003 SP-05 Solid 04/07/21 16:55 04/08/21 09:30
92531940004 SP-03B Solid 04/07/21 17:15 04/08/21 09:30
92531940005 SP-04C Solid 04/07/21 16:35 04/08/21 09:30
92531940006 SP-05D Solid 04/07/21 16:55 04/08/21 09:30
92531940007 SP-DUP-040721 Solid 04/07/21 00:00 04/08/21 09:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 50
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92531940001 SP-03 EPA 6010D 8 PASI-AKQ, RDT
EPA 6010D 1 PASI-ADS
EPA 7471B 1 PASI-ASOO
EPA 8270E 73 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANKAB
92531940002 SP-04 EPA 6010D 8 PASI-AKQ, RDT
EPA 6010D 1 PASI-ADS
EPA 7471B 1 PASI-ASOO
EPA 8270E 73 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANKAB
92531940003 SP-05 EPA 6010D 8 PASI-AKQ, RDT
EPA 6010D 1 PASI-ADS
EPA 7471B 1 PASI-ASOO
EPA 8270E 73 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANKAB
92531940004 SP-03B EPA 8260D 52 PASI-CCL
SW-846 1 PASI-CKDF
92531940005 SP-04C EPA 8260D 52 PASI-CCL
SW-846 1 PASI-CKDF
92531940006 SP-05D EPA 8260D 52 PASI-CCL
SW-846 1 PASI-CKDF
92531940007 SP-DUP-040721 EPA 6010D 8 PASI-AKQ, RDT
EPA 6010D 1 PASI-ADS
EPA 7471B 1 PASI-ASOO
EPA 8270E 73 PASI-CBPJ
EPA 8260D 52 PASI-CCL
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
EPA 7199 1 PANKAB
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 50
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-03 Lab ID:92531940001 Collected:04/07/21 17:15 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 1.1J mg/kg 04/15/21 12:52 7440-38-204/11/21 16:102.4 0.48 1
Barium 90.2 mg/kg 04/13/21 02:04 7440-39-304/11/21 16:100.96 0.24 1
Cadmium 0.067J mg/kg 04/15/21 12:52 7440-43-9 B04/11/21 16:100.096 0.048 1
Chromium 54.8 mg/kg 04/15/21 12:52 7440-47-304/11/21 16:100.48 0.24 1
Lead 11.5 mg/kg 04/15/21 12:52 7439-92-104/11/21 16:100.96 0.24 1
Manganese 636 mg/kg 04/15/21 12:52 7439-96-504/11/21 16:100.48 0.24 1
Selenium 2.0 mg/kg 04/15/21 12:52 7782-49-204/11/21 16:100.96 0.48 1
Silver ND mg/kg 04/15/21 12:52 7440-22-404/11/21 16:100.48 0.24 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1312; 04/12/21 15:15
Pace Analytical Services - Asheville
6010 MET ICP, SPLP
Manganese 0.013 mg/L 04/14/21 17:02 7439-96-504/14/21 01:400.0050 0.0034 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.042 mg/kg 04/13/21 16:01 7439-97-604/12/21 16:080.0030 0.0023 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Phenol ND ug/kg 04/09/21 12:57 108-95-204/08/21 15:524131841
bis(2-Chloroethyl) ether ND ug/kg 04/09/21 12:57 111-44-404/08/21 15:524131551
2-Chlorophenol ND ug/kg 04/09/21 12:57 95-57-804/08/21 15:524131551
2-Methylphenol(o-Cresol)ND ug/kg 04/09/21 12:57 95-48-704/08/21 15:524131691
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/09/21 12:57 15831-10-404/08/21 15:524131661
N-Nitroso-di-n-propylamine ND ug/kg 04/09/21 12:57 621-64-704/08/21 15:524131551
Hexachloroethane ND ug/kg 04/09/21 12:57 67-72-104/08/21 15:524131581
Nitrobenzene ND ug/kg 04/09/21 12:57 98-95-304/08/21 15:524131911
Isophorone ND ug/kg 04/09/21 12:57 78-59-104/08/21 15:524131841
2-Nitrophenol ND ug/kg 04/09/21 12:57 88-75-504/08/21 15:524131791
2,4-Dimethylphenol ND ug/kg 04/09/21 12:57 105-67-904/08/21 15:524131711
bis(2-Chloroethoxy)methane ND ug/kg 04/09/21 12:57 111-91-104/08/21 15:524131711
2,4-Dichlorophenol ND ug/kg 04/09/21 12:57 120-83-204/08/21 15:524131611
Naphthalene ND ug/kg 04/09/21 12:57 91-20-304/08/21 15:524131401
4-Chloroaniline ND ug/kg 04/09/21 12:57 106-47-804/08/21 15:528263241
Hexachloro-1,3-butadiene ND ug/kg 04/09/21 12:57 87-68-304/08/21 15:524131791
4-Chloro-3-methylphenol ND ug/kg 04/09/21 12:57 59-50-704/08/21 15:528262901
2-Methylnaphthalene ND ug/kg 04/09/21 12:57 91-57-604/08/21 15:524131651
Hexachlorocyclopentadiene ND ug/kg 04/09/21 12:57 77-47-404/08/21 15:524132371
2,4,6-Trichlorophenol ND ug/kg 04/09/21 12:57 88-06-204/08/21 15:524131701
2,4,5-Trichlorophenol ND ug/kg 04/09/21 12:57 95-95-404/08/21 15:524131891
2-Chloronaphthalene ND ug/kg 04/09/21 12:57 91-58-704/08/21 15:524131641
2-Nitroaniline ND ug/kg 04/09/21 12:57 88-74-404/08/21 15:5220603381
Dimethylphthalate ND ug/kg 04/09/21 12:57 131-11-304/08/21 15:524131501
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-03 Lab ID:92531940001 Collected:04/07/21 17:15 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthylene ND ug/kg 04/09/21 12:57 208-96-804/08/21 15:524131451
2,6-Dinitrotoluene ND ug/kg 04/09/21 12:57 606-20-204/08/21 15:524131511
3-Nitroaniline ND ug/kg 04/09/21 12:57 99-09-204/08/21 15:5220603241
Acenaphthene ND ug/kg 04/09/21 12:57 83-32-904/08/21 15:524131451
2,4-Dinitrophenol ND ug/kg 04/09/21 12:57 51-28-504/08/21 15:52206012801
4-Nitrophenol ND ug/kg 04/09/21 12:57 100-02-704/08/21 15:5220607981
Dibenzofuran ND ug/kg 04/09/21 12:57 132-64-904/08/21 15:524131491
2,4-Dinitrotoluene ND ug/kg 04/09/21 12:57 121-14-204/08/21 15:524131591
Diethylphthalate ND ug/kg 04/09/21 12:57 84-66-204/08/21 15:524131511
4-Chlorophenylphenyl ether ND ug/kg 04/09/21 12:57 7005-72-304/08/21 15:524131541
Fluorene ND ug/kg 04/09/21 12:57 86-73-704/08/21 15:524131451
4-Nitroaniline ND ug/kg 04/09/21 12:57 100-01-604/08/21 15:528263141
4,6-Dinitro-2-methylphenol ND ug/kg 04/09/21 12:57 534-52-104/08/21 15:528263851
N-Nitrosodiphenylamine ND ug/kg 04/09/21 12:57 86-30-604/08/21 15:524131461
4-Bromophenylphenyl ether ND ug/kg 04/09/21 12:57 101-55-304/08/21 15:524131591
Hexachlorobenzene ND ug/kg 04/09/21 12:57 118-74-104/08/21 15:524131611
Pentachlorophenol ND ug/kg 04/09/21 12:57 87-86-504/08/21 15:528264041
Phenanthrene ND ug/kg 04/09/21 12:57 85-01-804/08/21 15:524131351
Anthracene ND ug/kg 04/09/21 12:57 120-12-704/08/21 15:524131351
Di-n-butylphthalate ND ug/kg 04/09/21 12:57 84-74-204/08/21 15:524131391
Fluoranthene ND ug/kg 04/09/21 12:57 206-44-004/08/21 15:524131411
Pyrene ND ug/kg 04/09/21 12:57 129-00-004/08/21 15:524131681
Butylbenzylphthalate ND ug/kg 04/09/21 12:57 85-68-704/08/21 15:524131741
3,3'-Dichlorobenzidine ND ug/kg 04/09/21 12:57 91-94-1 IL04/08/21 15:528262791
Benzo(a)anthracene ND ug/kg 04/09/21 12:57 56-55-304/08/21 15:524131381
Chrysene ND ug/kg 04/09/21 12:57 218-01-904/08/21 15:524131501
bis(2-Ethylhexyl)phthalate ND ug/kg 04/09/21 12:57 117-81-704/08/21 15:524131601
Di-n-octylphthalate ND ug/kg 04/09/21 12:57 117-84-004/08/21 15:524131631
Benzo(b)fluoranthene ND ug/kg 04/09/21 12:57 205-99-204/08/21 15:524131381
Benzo(k)fluoranthene ND ug/kg 04/09/21 12:57 207-08-904/08/21 15:524131451
Benzo(a)pyrene ND ug/kg 04/09/21 12:57 50-32-804/08/21 15:524131431
Indeno(1,2,3-cd)pyrene ND ug/kg 04/09/21 12:57 193-39-504/08/21 15:524131631
Dibenz(a,h)anthracene ND ug/kg 04/09/21 12:57 53-70-304/08/21 15:524131591
Benzo(g,h,i)perylene ND ug/kg 04/09/21 12:57 191-24-204/08/21 15:524131601
Carbazole ND ug/kg 04/09/21 12:57 86-74-804/08/21 15:524131411
Acetophenone ND ug/kg 04/09/21 12:57 98-86-204/08/21 15:524131061
1,2,4,5-Tetrachlorobenzene ND ug/kg 04/09/21 12:57 95-94-304/08/21 15:524131011
2,3,4,6-Tetrachlorophenol ND ug/kg 04/09/21 12:57 58-90-204/08/21 15:524131031
Atrazine ND ug/kg 04/09/21 12:57 1912-24-904/08/21 15:524131331
Benzaldehyde ND ug/kg 04/09/21 12:57 100-52-704/08/21 15:524131381
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/09/21 12:57 108-60-104/08/21 15:524131961
Caprolactam ND ug/kg 04/09/21 12:57 105-60-2 v104/08/21 15:524132221
Biphenyl (Diphenyl)ND ug/kg 04/09/21 12:57 92-52-404/08/21 15:5241397.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-03 Lab ID:92531940001 Collected:04/07/21 17:15 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorobiphenyl (S)72 %04/09/21 12:57 321-60-804/08/21 15:5219-130 1
Terphenyl-d14 (S)69 %04/09/21 12:57 1718-51-004/08/21 15:5215-130 1
Phenol-d6 (S)73 %04/09/21 12:57 13127-88-304/08/21 15:5218-130 1
2-Fluorophenol (S)65 %04/09/21 12:57 367-12-404/08/21 15:5218-130 1
2,4,6-Tribromophenol (S)91 %04/09/21 12:57 118-79-604/08/21 15:5218-130 1
Nitrobenzene-d5 (S)77 %04/09/21 12:57 4165-60-004/08/21 15:5221-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.0 %04/08/21 17:19 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.5 %04/14/21 09:2304/14/21 09:131
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.636J mg/kg 04/12/21 00:36 18540-29-9 J04/10/21 13:331.24 0.317 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-04 Lab ID:92531940002 Collected:04/07/21 16:35 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 0.77J mg/kg 04/15/21 12:55 7440-38-204/11/21 16:102.3 0.46 1
Barium 75.3 mg/kg 04/13/21 02:07 7440-39-304/11/21 16:100.92 0.23 1
Cadmium ND mg/kg 04/15/21 12:55 7440-43-904/11/21 16:100.092 0.046 1
Chromium 46.3 mg/kg 04/15/21 12:55 7440-47-304/11/21 16:100.46 0.23 1
Lead 9.8 mg/kg 04/15/21 12:55 7439-92-104/11/21 16:100.92 0.23 1
Manganese 576 mg/kg 04/15/21 12:55 7439-96-504/11/21 16:100.46 0.23 1
Selenium 2.0 mg/kg 04/15/21 12:55 7782-49-204/11/21 16:100.92 0.46 1
Silver ND mg/kg 04/15/21 12:55 7440-22-404/11/21 16:100.46 0.23 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1312; 04/12/21 15:15
Pace Analytical Services - Asheville
6010 MET ICP, SPLP
Manganese 0.039 mg/L 04/14/21 17:22 7439-96-504/14/21 01:400.0050 0.0034 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.049 mg/kg 04/13/21 16:04 7439-97-604/12/21 16:080.0023 0.0018 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/09/21 13:58 83-32-904/08/21 15:524231491
Acenaphthylene ND ug/kg 04/09/21 13:58 208-96-804/08/21 15:524231491
Acetophenone ND ug/kg 04/09/21 13:58 98-86-204/08/21 15:524231091
Anthracene ND ug/kg 04/09/21 13:58 120-12-704/08/21 15:524231381
Atrazine ND ug/kg 04/09/21 13:58 1912-24-904/08/21 15:524231361
Benzaldehyde ND ug/kg 04/09/21 13:58 100-52-704/08/21 15:524231411
Benzo(a)anthracene ND ug/kg 04/09/21 13:58 56-55-304/08/21 15:524231411
Benzo(a)pyrene ND ug/kg 04/09/21 13:58 50-32-804/08/21 15:524231461
Benzo(b)fluoranthene ND ug/kg 04/09/21 13:58 205-99-204/08/21 15:524231411
Benzo(g,h,i)perylene ND ug/kg 04/09/21 13:58 191-24-204/08/21 15:524231641
Benzo(k)fluoranthene ND ug/kg 04/09/21 13:58 207-08-904/08/21 15:524231491
Biphenyl (Diphenyl)ND ug/kg 04/09/21 13:58 92-52-404/08/21 15:524231001
4-Bromophenylphenyl ether ND ug/kg 04/09/21 13:58 101-55-304/08/21 15:524231631
Butylbenzylphthalate ND ug/kg 04/09/21 13:58 85-68-704/08/21 15:524231781
Caprolactam ND ug/kg 04/09/21 13:58 105-60-2 v104/08/21 15:524232271
Carbazole ND ug/kg 04/09/21 13:58 86-74-804/08/21 15:524231451
4-Chloro-3-methylphenol ND ug/kg 04/09/21 13:58 59-50-704/08/21 15:528462971
4-Chloroaniline ND ug/kg 04/09/21 13:58 106-47-804/08/21 15:528463321
bis(2-Chloroethoxy)methane ND ug/kg 04/09/21 13:58 111-91-104/08/21 15:524231761
bis(2-Chloroethyl) ether ND ug/kg 04/09/21 13:58 111-44-404/08/21 15:524231591
2-Chloronaphthalene ND ug/kg 04/09/21 13:58 91-58-704/08/21 15:524231681
2-Chlorophenol ND ug/kg 04/09/21 13:58 95-57-804/08/21 15:524231591
4-Chlorophenylphenyl ether ND ug/kg 04/09/21 13:58 7005-72-304/08/21 15:524231581
Chrysene ND ug/kg 04/09/21 13:58 218-01-904/08/21 15:524231541
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-04 Lab ID:92531940002 Collected:04/07/21 16:35 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dibenz(a,h)anthracene ND ug/kg 04/09/21 13:58 53-70-304/08/21 15:524231631
Dibenzofuran ND ug/kg 04/09/21 13:58 132-64-904/08/21 15:524231531
3,3'-Dichlorobenzidine ND ug/kg 04/09/21 13:58 91-94-1 IL04/08/21 15:528462861
2,4-Dichlorophenol ND ug/kg 04/09/21 13:58 120-83-204/08/21 15:524231651
Diethylphthalate ND ug/kg 04/09/21 13:58 84-66-204/08/21 15:524231551
2,4-Dimethylphenol ND ug/kg 04/09/21 13:58 105-67-904/08/21 15:524231761
Dimethylphthalate ND ug/kg 04/09/21 13:58 131-11-304/08/21 15:524231541
Di-n-butylphthalate ND ug/kg 04/09/21 13:58 84-74-204/08/21 15:524231421
4,6-Dinitro-2-methylphenol ND ug/kg 04/09/21 13:58 534-52-104/08/21 15:528463951
2,4-Dinitrophenol ND ug/kg 04/09/21 13:58 51-28-504/08/21 15:52211013101
2,4-Dinitrotoluene ND ug/kg 04/09/21 13:58 121-14-204/08/21 15:524231631
2,6-Dinitrotoluene ND ug/kg 04/09/21 13:58 606-20-204/08/21 15:524231551
Di-n-octylphthalate ND ug/kg 04/09/21 13:58 117-84-004/08/21 15:524231671
bis(2-Ethylhexyl)phthalate ND ug/kg 04/09/21 13:58 117-81-704/08/21 15:524231641
Fluoranthene ND ug/kg 04/09/21 13:58 206-44-004/08/21 15:524231451
Fluorene ND ug/kg 04/09/21 13:58 86-73-704/08/21 15:524231491
Hexachloro-1,3-butadiene ND ug/kg 04/09/21 13:58 87-68-304/08/21 15:524231831
Hexachlorobenzene ND ug/kg 04/09/21 13:58 118-74-104/08/21 15:524231651
Hexachlorocyclopentadiene ND ug/kg 04/09/21 13:58 77-47-404/08/21 15:524232421
Hexachloroethane ND ug/kg 04/09/21 13:58 67-72-104/08/21 15:524231621
Indeno(1,2,3-cd)pyrene ND ug/kg 04/09/21 13:58 193-39-504/08/21 15:524231671
Isophorone ND ug/kg 04/09/21 13:58 78-59-104/08/21 15:524231881
2-Methylnaphthalene ND ug/kg 04/09/21 13:58 91-57-604/08/21 15:524231691
2-Methylphenol(o-Cresol)ND ug/kg 04/09/21 13:58 95-48-704/08/21 15:524231731
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/09/21 13:58 15831-10-404/08/21 15:524231701
Naphthalene ND ug/kg 04/09/21 13:58 91-20-304/08/21 15:524231441
2-Nitroaniline ND ug/kg 04/09/21 13:58 88-74-404/08/21 15:5221103461
3-Nitroaniline ND ug/kg 04/09/21 13:58 99-09-204/08/21 15:5221103321
4-Nitroaniline ND ug/kg 04/09/21 13:58 100-01-604/08/21 15:528463221
Nitrobenzene ND ug/kg 04/09/21 13:58 98-95-304/08/21 15:524231961
2-Nitrophenol ND ug/kg 04/09/21 13:58 88-75-504/08/21 15:524231831
4-Nitrophenol ND ug/kg 04/09/21 13:58 100-02-704/08/21 15:5221108181
N-Nitroso-di-n-propylamine ND ug/kg 04/09/21 13:58 621-64-704/08/21 15:524231591
N-Nitrosodiphenylamine ND ug/kg 04/09/21 13:58 86-30-604/08/21 15:524231501
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/09/21 13:58 108-60-104/08/21 15:524232011
Pentachlorophenol ND ug/kg 04/09/21 13:58 87-86-504/08/21 15:528464141
Phenanthrene ND ug/kg 04/09/21 13:58 85-01-804/08/21 15:524231381
Phenol ND ug/kg 04/09/21 13:58 108-95-204/08/21 15:524231881
Pyrene ND ug/kg 04/09/21 13:58 129-00-004/08/21 15:524231721
1,2,4,5-Tetrachlorobenzene ND ug/kg 04/09/21 13:58 95-94-304/08/21 15:524231031
2,3,4,6-Tetrachlorophenol ND ug/kg 04/09/21 13:58 58-90-204/08/21 15:524231061
2,4,5-Trichlorophenol ND ug/kg 04/09/21 13:58 95-95-404/08/21 15:524231941
2,4,6-Trichlorophenol ND ug/kg 04/09/21 13:58 88-06-204/08/21 15:524231741
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-04 Lab ID:92531940002 Collected:04/07/21 16:35 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorobiphenyl (S)73 %04/09/21 13:58 321-60-804/08/21 15:5219-130 1
Terphenyl-d14 (S)71 %04/09/21 13:58 1718-51-004/08/21 15:5215-130 1
Phenol-d6 (S)72 %04/09/21 13:58 13127-88-304/08/21 15:5218-130 1
2-Fluorophenol (S)67 %04/09/21 13:58 367-12-404/08/21 15:5218-130 1
2,4,6-Tribromophenol (S)89 %04/09/21 13:58 118-79-604/08/21 15:5218-130 1
Nitrobenzene-d5 (S)80 %04/09/21 13:58 4165-60-004/08/21 15:5221-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.5 %04/08/21 17:19 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.9 %04/14/21 09:2304/14/21 09:131
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 04/12/21 00:42 18540-29-904/10/21 13:331.24 0.315 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-05 Lab ID:92531940003 Collected:04/07/21 16:55 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 2.0 mg/kg 04/15/21 12:59 7440-38-204/11/21 16:101.9 0.39 1
Barium 85.8 mg/kg 04/13/21 02:10 7440-39-304/11/21 16:100.78 0.19 1
Cadmium 0.092 mg/kg 04/15/21 12:59 7440-43-9 B04/11/21 16:100.078 0.039 1
Chromium 38.1 mg/kg 04/15/21 12:59 7440-47-304/11/21 16:100.39 0.19 1
Lead 16.1 mg/kg 04/15/21 12:59 7439-92-104/11/21 16:100.78 0.19 1
Manganese 482 mg/kg 04/15/21 12:59 7439-96-504/11/21 16:100.39 0.19 1
Selenium 1.9 mg/kg 04/15/21 12:59 7782-49-204/11/21 16:100.78 0.39 1
Silver ND mg/kg 04/15/21 12:59 7440-22-404/11/21 16:100.39 0.19 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1312; 04/12/21 15:15
Pace Analytical Services - Asheville
6010 MET ICP, SPLP
Manganese 0.038 mg/L 04/14/21 17:25 7439-96-504/14/21 01:400.0050 0.0034 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.068 mg/kg 04/14/21 15:42 7439-97-604/12/21 16:080.0059 0.0045 2
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/09/21 14:58 83-32-904/08/21 15:524101441
Acenaphthylene ND ug/kg 04/09/21 14:58 208-96-804/08/21 15:524101441
Acetophenone ND ug/kg 04/09/21 14:58 98-86-204/08/21 15:524101061
Anthracene ND ug/kg 04/09/21 14:58 120-12-704/08/21 15:524101341
Atrazine ND ug/kg 04/09/21 14:58 1912-24-904/08/21 15:524101321
Benzaldehyde ND ug/kg 04/09/21 14:58 100-52-704/08/21 15:524101371
Benzo(a)anthracene 257J ug/kg 04/09/21 14:58 56-55-304/08/21 15:524101371
Benzo(a)pyrene 224J ug/kg 04/09/21 14:58 50-32-804/08/21 15:524101421
Benzo(b)fluoranthene 257J ug/kg 04/09/21 14:58 205-99-204/08/21 15:524101371
Benzo(g,h,i)perylene ND ug/kg 04/09/21 14:58 191-24-204/08/21 15:524101591
Benzo(k)fluoranthene ND ug/kg 04/09/21 14:58 207-08-904/08/21 15:524101441
Biphenyl (Diphenyl)ND ug/kg 04/09/21 14:58 92-52-404/08/21 15:5241097.1 1
4-Bromophenylphenyl ether ND ug/kg 04/09/21 14:58 101-55-304/08/21 15:524101581
Butylbenzylphthalate ND ug/kg 04/09/21 14:58 85-68-704/08/21 15:524101731
Caprolactam ND ug/kg 04/09/21 14:58 105-60-2 v104/08/21 15:524102201
Carbazole ND ug/kg 04/09/21 14:58 86-74-804/08/21 15:524101401
4-Chloro-3-methylphenol ND ug/kg 04/09/21 14:58 59-50-704/08/21 15:528202881
4-Chloroaniline ND ug/kg 04/09/21 14:58 106-47-804/08/21 15:528203221
bis(2-Chloroethoxy)methane ND ug/kg 04/09/21 14:58 111-91-104/08/21 15:524101701
bis(2-Chloroethyl) ether ND ug/kg 04/09/21 14:58 111-44-404/08/21 15:524101541
2-Chloronaphthalene ND ug/kg 04/09/21 14:58 91-58-704/08/21 15:524101631
2-Chlorophenol ND ug/kg 04/09/21 14:58 95-57-804/08/21 15:524101541
4-Chlorophenylphenyl ether ND ug/kg 04/09/21 14:58 7005-72-304/08/21 15:524101531
Chrysene 254J ug/kg 04/09/21 14:58 218-01-904/08/21 15:524101491
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-05 Lab ID:92531940003 Collected:04/07/21 16:55 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dibenz(a,h)anthracene ND ug/kg 04/09/21 14:58 53-70-304/08/21 15:524101581
Dibenzofuran ND ug/kg 04/09/21 14:58 132-64-904/08/21 15:524101481
3,3'-Dichlorobenzidine ND ug/kg 04/09/21 14:58 91-94-1 IL04/08/21 15:528202771
2,4-Dichlorophenol ND ug/kg 04/09/21 14:58 120-83-204/08/21 15:524101601
Diethylphthalate ND ug/kg 04/09/21 14:58 84-66-204/08/21 15:524101501
2,4-Dimethylphenol ND ug/kg 04/09/21 14:58 105-67-904/08/21 15:524101701
Dimethylphthalate ND ug/kg 04/09/21 14:58 131-11-304/08/21 15:524101491
Di-n-butylphthalate ND ug/kg 04/09/21 14:58 84-74-204/08/21 15:524101381
4,6-Dinitro-2-methylphenol ND ug/kg 04/09/21 14:58 534-52-104/08/21 15:528203821
2,4-Dinitrophenol ND ug/kg 04/09/21 14:58 51-28-504/08/21 15:52205012701
2,4-Dinitrotoluene ND ug/kg 04/09/21 14:58 121-14-204/08/21 15:524101581
2,6-Dinitrotoluene ND ug/kg 04/09/21 14:58 606-20-204/08/21 15:524101501
Di-n-octylphthalate ND ug/kg 04/09/21 14:58 117-84-004/08/21 15:524101611
bis(2-Ethylhexyl)phthalate ND ug/kg 04/09/21 14:58 117-81-704/08/21 15:524101591
Fluoranthene 603 ug/kg 04/09/21 14:58 206-44-004/08/21 15:524101401
Fluorene ND ug/kg 04/09/21 14:58 86-73-704/08/21 15:524101441
Hexachloro-1,3-butadiene ND ug/kg 04/09/21 14:58 87-68-304/08/21 15:524101781
Hexachlorobenzene ND ug/kg 04/09/21 14:58 118-74-104/08/21 15:524101601
Hexachlorocyclopentadiene ND ug/kg 04/09/21 14:58 77-47-404/08/21 15:524102351
Hexachloroethane ND ug/kg 04/09/21 14:58 67-72-104/08/21 15:524101561
Indeno(1,2,3-cd)pyrene ND ug/kg 04/09/21 14:58 193-39-504/08/21 15:524101611
Isophorone ND ug/kg 04/09/21 14:58 78-59-104/08/21 15:524101831
2-Methylnaphthalene ND ug/kg 04/09/21 14:58 91-57-604/08/21 15:524101641
2-Methylphenol(o-Cresol)ND ug/kg 04/09/21 14:58 95-48-704/08/21 15:524101681
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/09/21 14:58 15831-10-404/08/21 15:524101651
Naphthalene ND ug/kg 04/09/21 14:58 91-20-304/08/21 15:524101391
2-Nitroaniline ND ug/kg 04/09/21 14:58 88-74-404/08/21 15:5220503351
3-Nitroaniline ND ug/kg 04/09/21 14:58 99-09-204/08/21 15:5220503221
4-Nitroaniline ND ug/kg 04/09/21 14:58 100-01-604/08/21 15:528203121
Nitrobenzene ND ug/kg 04/09/21 14:58 98-95-304/08/21 15:524101901
2-Nitrophenol ND ug/kg 04/09/21 14:58 88-75-504/08/21 15:524101781
4-Nitrophenol ND ug/kg 04/09/21 14:58 100-02-704/08/21 15:5220507921
N-Nitroso-di-n-propylamine ND ug/kg 04/09/21 14:58 621-64-704/08/21 15:524101541
N-Nitrosodiphenylamine ND ug/kg 04/09/21 14:58 86-30-604/08/21 15:524101451
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/09/21 14:58 108-60-104/08/21 15:524101951
Pentachlorophenol ND ug/kg 04/09/21 14:58 87-86-504/08/21 15:528204011
Phenanthrene 553 ug/kg 04/09/21 14:58 85-01-804/08/21 15:524101341
Phenol ND ug/kg 04/09/21 14:58 108-95-204/08/21 15:524101831
Pyrene 452 ug/kg 04/09/21 14:58 129-00-004/08/21 15:524101661
1,2,4,5-Tetrachlorobenzene ND ug/kg 04/09/21 14:58 95-94-304/08/21 15:5241099.8 1
2,3,4,6-Tetrachlorophenol ND ug/kg 04/09/21 14:58 58-90-204/08/21 15:524101031
2,4,5-Trichlorophenol ND ug/kg 04/09/21 14:58 95-95-404/08/21 15:524101881
2,4,6-Trichlorophenol ND ug/kg 04/09/21 14:58 88-06-204/08/21 15:524101691
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-05 Lab ID:92531940003 Collected:04/07/21 16:55 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorobiphenyl (S)71 %04/09/21 14:58 321-60-804/08/21 15:5219-130 1
Terphenyl-d14 (S)63 %04/09/21 14:58 1718-51-004/08/21 15:5215-130 1
Phenol-d6 (S)77 %04/09/21 14:58 13127-88-304/08/21 15:5218-130 1
2-Fluorophenol (S)70 %04/09/21 14:58 367-12-404/08/21 15:5218-130 1
2,4,6-Tribromophenol (S)95 %04/09/21 14:58 118-79-604/08/21 15:5218-130 1
Nitrobenzene-d5 (S)71 %04/09/21 14:58 4165-60-004/08/21 15:5221-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.8 %04/08/21 17:19 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.7 %04/14/21 09:2304/14/21 09:131
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 04/12/21 00:47 18540-29-904/10/21 13:331.24 0.316 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-03B Lab ID:92531940004 Collected:04/07/21 17:15 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/09/21 05:28 67-64-104/08/21 15:5212439.9 1
Benzene ND ug/kg 04/09/21 05:28 71-43-204/08/21 15:526.2 2.5 1
Bromodichloromethane ND ug/kg 04/09/21 05:28 75-27-404/08/21 15:526.2 2.4 1
Bromoform ND ug/kg 04/09/21 05:28 75-25-204/08/21 15:526.2 2.2 1
Bromomethane ND ug/kg 04/09/21 05:28 74-83-904/08/21 15:5212.4 9.8 1
2-Butanone (MEK)ND ug/kg 04/09/21 05:28 78-93-304/08/21 15:5212429.9 1
Carbon disulfide ND ug/kg 04/09/21 05:28 75-15-004/08/21 15:5212.4 7.8 1
Carbon tetrachloride ND ug/kg 04/09/21 05:28 56-23-504/08/21 15:526.2 2.3 1
Chlorobenzene ND ug/kg 04/09/21 05:28 108-90-704/08/21 15:526.2 1.2 1
Chloroethane ND ug/kg 04/09/21 05:28 75-00-304/08/21 15:5212.4 4.8 1
Chloroform ND ug/kg 04/09/21 05:28 67-66-304/08/21 15:526.2 3.8 1
Chloromethane ND ug/kg 04/09/21 05:28 74-87-304/08/21 15:5212.4 5.2 1
Cyclohexane 5.9J ug/kg 04/09/21 05:28 110-82-704/08/21 15:526.2 3.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/09/21 05:28 96-12-804/08/21 15:526.2 2.4 1
Dibromochloromethane ND ug/kg 04/09/21 05:28 124-48-104/08/21 15:526.2 3.5 1
1,2-Dibromoethane (EDB)ND ug/kg 04/09/21 05:28 106-93-404/08/21 15:526.2 2.7 1
1,2-Dichlorobenzene ND ug/kg 04/09/21 05:28 95-50-104/08/21 15:526.2 2.2 1
1,3-Dichlorobenzene ND ug/kg 04/09/21 05:28 541-73-104/08/21 15:526.2 1.9 1
1,4-Dichlorobenzene ND ug/kg 04/09/21 05:28 106-46-704/08/21 15:526.2 1.6 1
Dichlorodifluoromethane ND ug/kg 04/09/21 05:28 75-71-804/08/21 15:5212.4 2.7 1
1,1-Dichloroethane ND ug/kg 04/09/21 05:28 75-34-304/08/21 15:526.2 2.6 1
1,2-Dichloroethane ND ug/kg 04/09/21 05:28 107-06-204/08/21 15:526.2 4.1 1
1,1-Dichloroethene ND ug/kg 04/09/21 05:28 75-35-404/08/21 15:526.2 2.6 1
cis-1,2-Dichloroethene ND ug/kg 04/09/21 05:28 156-59-204/08/21 15:526.2 2.1 1
trans-1,2-Dichloroethene ND ug/kg 04/09/21 05:28 156-60-504/08/21 15:526.2 2.2 1
1,2-Dichloropropane ND ug/kg 04/09/21 05:28 78-87-504/08/21 15:526.2 1.9 1
cis-1,3-Dichloropropene ND ug/kg 04/09/21 05:28 10061-01-504/08/21 15:526.2 1.7 1
trans-1,3-Dichloropropene ND ug/kg 04/09/21 05:28 10061-02-604/08/21 15:526.2 2.1 1
Ethylbenzene 4.4J ug/kg 04/09/21 05:28 100-41-404/08/21 15:526.2 2.9 1
2-Hexanone ND ug/kg 04/09/21 05:28 591-78-604/08/21 15:5262.2 6.0 1
Isopropylbenzene (Cumene)ND ug/kg 04/09/21 05:28 98-82-804/08/21 15:526.2 2.1 1
Methyl acetate ND ug/kg 04/09/21 05:28 79-20-904/08/21 15:5212.4 10.8 1
Methylcyclohexane 25.6 ug/kg 04/09/21 05:28 108-87-204/08/21 15:5212.4 6.5 1
Methylene Chloride ND ug/kg 04/09/21 05:28 75-09-204/08/21 15:5224.9 17.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/09/21 05:28 108-10-104/08/21 15:5262.2 6.0 1
Methyl-tert-butyl ether ND ug/kg 04/09/21 05:28 1634-04-404/08/21 15:526.2 2.3 1
Styrene ND ug/kg 04/09/21 05:28 100-42-504/08/21 15:526.2 1.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/09/21 05:28 79-34-504/08/21 15:526.2 1.6 1
Tetrachloroethene ND ug/kg 04/09/21 05:28 127-18-404/08/21 15:526.2 2.0 1
Toluene 7.3 ug/kg 04/09/21 05:28 108-88-304/08/21 15:526.2 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 04/09/21 05:28 87-61-604/08/21 15:526.2 5.0 1
1,2,4-Trichlorobenzene ND ug/kg 04/09/21 05:28 120-82-104/08/21 15:526.2 5.2 1
1,1,1-Trichloroethane ND ug/kg 04/09/21 05:28 71-55-604/08/21 15:526.2 3.2 1
1,1,2-Trichloroethane ND ug/kg 04/09/21 05:28 79-00-504/08/21 15:526.2 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-03B Lab ID:92531940004 Collected:04/07/21 17:15 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Trichloroethene ND ug/kg 04/09/21 05:28 79-01-604/08/21 15:526.2 1.6 1
Trichlorofluoromethane ND ug/kg 04/09/21 05:28 75-69-404/08/21 15:526.2 3.4 1
1,1,2-Trichlorotrifluoroethane ND ug/kg 04/09/21 05:28 76-13-104/08/21 15:526.2 3.5 1
Vinyl chloride ND ug/kg 04/09/21 05:28 75-01-404/08/21 15:5212.4 3.2 1
Xylene (Total)17.1 ug/kg 04/09/21 05:28 1330-20-704/08/21 15:5212.4 3.5 1
Surrogates
Toluene-d8 (S)102 %04/09/21 05:28 2037-26-504/08/21 15:5270-130 1
4-Bromofluorobenzene (S)108 %04/09/21 05:28 460-00-404/08/21 15:5269-134 1
1,2-Dichloroethane-d4 (S)109 %04/09/21 05:28 17060-07-004/08/21 15:5270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.6 %04/08/21 15:12 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-04C Lab ID:92531940005 Collected:04/07/21 16:35 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/09/21 05:46 67-64-104/08/21 15:5212038.5 1
Benzene ND ug/kg 04/09/21 05:46 71-43-204/08/21 15:526.0 2.4 1
Bromodichloromethane ND ug/kg 04/09/21 05:46 75-27-404/08/21 15:526.0 2.3 1
Bromoform ND ug/kg 04/09/21 05:46 75-25-204/08/21 15:526.0 2.1 1
Bromomethane ND ug/kg 04/09/21 05:46 74-83-904/08/21 15:5212.0 9.5 1
2-Butanone (MEK)ND ug/kg 04/09/21 05:46 78-93-304/08/21 15:5212028.8 1
Carbon disulfide ND ug/kg 04/09/21 05:46 75-15-004/08/21 15:5212.0 7.5 1
Carbon tetrachloride ND ug/kg 04/09/21 05:46 56-23-504/08/21 15:526.0 2.2 1
Chlorobenzene ND ug/kg 04/09/21 05:46 108-90-704/08/21 15:526.0 1.2 1
Chloroethane ND ug/kg 04/09/21 05:46 75-00-304/08/21 15:5212.0 4.6 1
Chloroform ND ug/kg 04/09/21 05:46 67-66-304/08/21 15:526.0 3.6 1
Chloromethane ND ug/kg 04/09/21 05:46 74-87-304/08/21 15:5212.0 5.0 1
Cyclohexane ND ug/kg 04/09/21 05:46 110-82-704/08/21 15:526.0 3.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/09/21 05:46 96-12-804/08/21 15:526.0 2.3 1
Dibromochloromethane ND ug/kg 04/09/21 05:46 124-48-104/08/21 15:526.0 3.4 1
1,2-Dibromoethane (EDB)ND ug/kg 04/09/21 05:46 106-93-404/08/21 15:526.0 2.6 1
1,2-Dichlorobenzene ND ug/kg 04/09/21 05:46 95-50-104/08/21 15:526.0 2.2 1
1,3-Dichlorobenzene ND ug/kg 04/09/21 05:46 541-73-104/08/21 15:526.0 1.9 1
1,4-Dichlorobenzene ND ug/kg 04/09/21 05:46 106-46-704/08/21 15:526.0 1.6 1
Dichlorodifluoromethane ND ug/kg 04/09/21 05:46 75-71-804/08/21 15:5212.0 2.6 1
1,1-Dichloroethane ND ug/kg 04/09/21 05:46 75-34-304/08/21 15:526.0 2.5 1
1,2-Dichloroethane ND ug/kg 04/09/21 05:46 107-06-204/08/21 15:526.0 4.0 1
1,1-Dichloroethene ND ug/kg 04/09/21 05:46 75-35-404/08/21 15:526.0 2.5 1
cis-1,2-Dichloroethene ND ug/kg 04/09/21 05:46 156-59-204/08/21 15:526.0 2.0 1
trans-1,2-Dichloroethene ND ug/kg 04/09/21 05:46 156-60-504/08/21 15:526.0 2.1 1
1,2-Dichloropropane ND ug/kg 04/09/21 05:46 78-87-504/08/21 15:526.0 1.8 1
cis-1,3-Dichloropropene ND ug/kg 04/09/21 05:46 10061-01-504/08/21 15:526.0 1.6 1
trans-1,3-Dichloropropene ND ug/kg 04/09/21 05:46 10061-02-604/08/21 15:526.0 2.1 1
Ethylbenzene ND ug/kg 04/09/21 05:46 100-41-404/08/21 15:526.0 2.8 1
2-Hexanone ND ug/kg 04/09/21 05:46 591-78-604/08/21 15:5259.9 5.8 1
Isopropylbenzene (Cumene)ND ug/kg 04/09/21 05:46 98-82-804/08/21 15:526.0 2.0 1
Methyl acetate ND ug/kg 04/09/21 05:46 79-20-904/08/21 15:5212.0 10.4 1
Methylcyclohexane ND ug/kg 04/09/21 05:46 108-87-204/08/21 15:5212.0 6.3 1
Methylene Chloride ND ug/kg 04/09/21 05:46 75-09-204/08/21 15:5224.0 16.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/09/21 05:46 108-10-104/08/21 15:5259.9 5.8 1
Methyl-tert-butyl ether ND ug/kg 04/09/21 05:46 1634-04-404/08/21 15:526.0 2.2 1
Styrene ND ug/kg 04/09/21 05:46 100-42-504/08/21 15:526.0 1.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/09/21 05:46 79-34-504/08/21 15:526.0 1.6 1
Tetrachloroethene ND ug/kg 04/09/21 05:46 127-18-404/08/21 15:526.0 1.9 1
Toluene ND ug/kg 04/09/21 05:46 108-88-304/08/21 15:526.0 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 04/09/21 05:46 87-61-604/08/21 15:526.0 4.8 1
1,2,4-Trichlorobenzene ND ug/kg 04/09/21 05:46 120-82-104/08/21 15:526.0 5.0 1
1,1,1-Trichloroethane ND ug/kg 04/09/21 05:46 71-55-604/08/21 15:526.0 3.1 1
1,1,2-Trichloroethane ND ug/kg 04/09/21 05:46 79-00-504/08/21 15:526.0 2.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-04C Lab ID:92531940005 Collected:04/07/21 16:35 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Trichloroethene ND ug/kg 04/09/21 05:46 79-01-604/08/21 15:526.0 1.5 1
Trichlorofluoromethane ND ug/kg 04/09/21 05:46 75-69-404/08/21 15:526.0 3.3 1
1,1,2-Trichlorotrifluoroethane ND ug/kg 04/09/21 05:46 76-13-104/08/21 15:526.0 3.3 1
Vinyl chloride ND ug/kg 04/09/21 05:46 75-01-404/08/21 15:5212.0 3.0 1
Xylene (Total)ND ug/kg 04/09/21 05:46 1330-20-704/08/21 15:5212.0 3.4 1
Surrogates
Toluene-d8 (S)100 %04/09/21 05:46 2037-26-504/08/21 15:5270-130 1
4-Bromofluorobenzene (S)108 %04/09/21 05:46 460-00-404/08/21 15:5269-134 1
1,2-Dichloroethane-d4 (S)108 %04/09/21 05:46 17060-07-004/08/21 15:5270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.1 %04/08/21 15:12 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-05D Lab ID:92531940006 Collected:04/07/21 16:55 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 116J ug/kg 04/09/21 06:04 67-64-104/08/21 15:5215549.9 1
Benzene ND ug/kg 04/09/21 06:04 71-43-204/08/21 15:527.8 3.1 1
Bromodichloromethane ND ug/kg 04/09/21 06:04 75-27-404/08/21 15:527.8 3.0 1
Bromoform ND ug/kg 04/09/21 06:04 75-25-204/08/21 15:527.8 2.7 1
Bromomethane ND ug/kg 04/09/21 06:04 74-83-904/08/21 15:5215.5 12.3 1
2-Butanone (MEK)40.8J ug/kg 04/09/21 06:04 78-93-304/08/21 15:5215537.3 1
Carbon disulfide ND ug/kg 04/09/21 06:04 75-15-004/08/21 15:5215.5 9.8 1
Carbon tetrachloride ND ug/kg 04/09/21 06:04 56-23-504/08/21 15:527.8 2.9 1
Chlorobenzene ND ug/kg 04/09/21 06:04 108-90-704/08/21 15:527.8 1.5 1
Chloroethane ND ug/kg 04/09/21 06:04 75-00-304/08/21 15:5215.5 6.0 1
Chloroform ND ug/kg 04/09/21 06:04 67-66-304/08/21 15:527.8 4.7 1
Chloromethane ND ug/kg 04/09/21 06:04 74-87-304/08/21 15:5215.5 6.5 1
Cyclohexane ND ug/kg 04/09/21 06:04 110-82-704/08/21 15:527.8 4.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/09/21 06:04 96-12-804/08/21 15:527.8 3.0 1
Dibromochloromethane ND ug/kg 04/09/21 06:04 124-48-104/08/21 15:527.8 4.4 1
1,2-Dibromoethane (EDB)ND ug/kg 04/09/21 06:04 106-93-404/08/21 15:527.8 3.4 1
1,2-Dichlorobenzene ND ug/kg 04/09/21 06:04 95-50-104/08/21 15:527.8 2.8 1
1,3-Dichlorobenzene ND ug/kg 04/09/21 06:04 541-73-104/08/21 15:527.8 2.4 1
1,4-Dichlorobenzene ND ug/kg 04/09/21 06:04 106-46-704/08/21 15:527.8 2.0 1
Dichlorodifluoromethane ND ug/kg 04/09/21 06:04 75-71-804/08/21 15:5215.5 3.4 1
1,1-Dichloroethane ND ug/kg 04/09/21 06:04 75-34-304/08/21 15:527.8 3.2 1
1,2-Dichloroethane ND ug/kg 04/09/21 06:04 107-06-204/08/21 15:527.8 5.1 1
1,1-Dichloroethene ND ug/kg 04/09/21 06:04 75-35-404/08/21 15:527.8 3.2 1
cis-1,2-Dichloroethene ND ug/kg 04/09/21 06:04 156-59-204/08/21 15:527.8 2.7 1
trans-1,2-Dichloroethene ND ug/kg 04/09/21 06:04 156-60-504/08/21 15:527.8 2.7 1
1,2-Dichloropropane ND ug/kg 04/09/21 06:04 78-87-504/08/21 15:527.8 2.3 1
cis-1,3-Dichloropropene ND ug/kg 04/09/21 06:04 10061-01-504/08/21 15:527.8 2.1 1
trans-1,3-Dichloropropene ND ug/kg 04/09/21 06:04 10061-02-604/08/21 15:527.8 2.7 1
Ethylbenzene 11.7 ug/kg 04/09/21 06:04 100-41-404/08/21 15:527.8 3.6 1
2-Hexanone ND ug/kg 04/09/21 06:04 591-78-604/08/21 15:5277.7 7.5 1
Isopropylbenzene (Cumene)ND ug/kg 04/09/21 06:04 98-82-804/08/21 15:527.8 2.6 1
Methyl acetate ND ug/kg 04/09/21 06:04 79-20-904/08/21 15:5215.5 13.5 1
Methylcyclohexane ND ug/kg 04/09/21 06:04 108-87-204/08/21 15:5215.5 8.2 1
Methylene Chloride ND ug/kg 04/09/21 06:04 75-09-204/08/21 15:5231.1 21.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/09/21 06:04 108-10-104/08/21 15:5277.7 7.5 1
Methyl-tert-butyl ether ND ug/kg 04/09/21 06:04 1634-04-404/08/21 15:527.8 2.9 1
Styrene ND ug/kg 04/09/21 06:04 100-42-504/08/21 15:527.8 2.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/09/21 06:04 79-34-504/08/21 15:527.8 2.1 1
Tetrachloroethene ND ug/kg 04/09/21 06:04 127-18-404/08/21 15:527.8 2.5 1
Toluene 56.5 ug/kg 04/09/21 06:04 108-88-304/08/21 15:527.8 2.2 1
1,2,3-Trichlorobenzene ND ug/kg 04/09/21 06:04 87-61-604/08/21 15:527.8 6.3 1
1,2,4-Trichlorobenzene ND ug/kg 04/09/21 06:04 120-82-104/08/21 15:527.8 6.5 1
1,1,1-Trichloroethane ND ug/kg 04/09/21 06:04 71-55-604/08/21 15:527.8 4.0 1
1,1,2-Trichloroethane ND ug/kg 04/09/21 06:04 79-00-504/08/21 15:527.8 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-05D Lab ID:92531940006 Collected:04/07/21 16:55 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Trichloroethene ND ug/kg 04/09/21 06:04 79-01-604/08/21 15:527.8 2.0 1
Trichlorofluoromethane ND ug/kg 04/09/21 06:04 75-69-404/08/21 15:527.8 4.3 1
1,1,2-Trichlorotrifluoroethane ND ug/kg 04/09/21 06:04 76-13-104/08/21 15:527.8 4.3 1
Vinyl chloride ND ug/kg 04/09/21 06:04 75-01-404/08/21 15:5215.5 3.9 1
Xylene (Total)ND ug/kg 04/09/21 06:04 1330-20-704/08/21 15:5215.5 4.4 1
Surrogates
Toluene-d8 (S)102 %04/09/21 06:04 2037-26-504/08/21 15:5270-130 1
4-Bromofluorobenzene (S)109 %04/09/21 06:04 460-00-404/08/21 15:5269-134 1
1,2-Dichloroethane-d4 (S)111 %04/09/21 06:04 17060-07-004/08/21 15:5270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.2 %04/08/21 15:12 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-DUP-040721 Lab ID:92531940007 Collected:04/07/21 00:00 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 2.0J mg/kg 04/15/21 13:02 7440-38-204/11/21 16:102.0 0.41 1
Barium 85.7 mg/kg 04/13/21 02:13 7440-39-304/11/21 16:100.81 0.20 1
Cadmium 0.078J mg/kg 04/15/21 13:02 7440-43-9 B04/11/21 16:100.081 0.041 1
Chromium 40.9 mg/kg 04/15/21 13:02 7440-47-304/11/21 16:100.41 0.20 1
Lead 15.9 mg/kg 04/15/21 13:02 7439-92-104/11/21 16:100.81 0.20 1
Manganese 503 mg/kg 04/15/21 13:02 7439-96-504/11/21 16:100.41 0.20 1
Selenium 2.0 mg/kg 04/15/21 13:02 7782-49-204/11/21 16:100.81 0.41 1
Silver ND mg/kg 04/15/21 13:02 7440-22-404/11/21 16:100.41 0.20 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1312; 04/12/21 15:15
Pace Analytical Services - Asheville
6010 MET ICP, SPLP
Manganese 0.061 mg/L 04/14/21 17:28 7439-96-504/14/21 01:400.0050 0.0034 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.060 mg/kg 04/13/21 16:09 7439-97-604/12/21 16:080.0074 0.0057 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/09/21 15:29 83-32-904/08/21 15:524491581
Acenaphthylene ND ug/kg 04/09/21 15:29 208-96-804/08/21 15:524491581
Acetophenone ND ug/kg 04/09/21 15:29 98-86-204/08/21 15:524491161
Anthracene ND ug/kg 04/09/21 15:29 120-12-704/08/21 15:524491471
Atrazine ND ug/kg 04/09/21 15:29 1912-24-904/08/21 15:524491441
Benzaldehyde ND ug/kg 04/09/21 15:29 100-52-704/08/21 15:524491501
Benzo(a)anthracene ND ug/kg 04/09/21 15:29 56-55-304/08/21 15:524491501
Benzo(a)pyrene ND ug/kg 04/09/21 15:29 50-32-804/08/21 15:524491551
Benzo(b)fluoranthene ND ug/kg 04/09/21 15:29 205-99-204/08/21 15:524491501
Benzo(g,h,i)perylene ND ug/kg 04/09/21 15:29 191-24-204/08/21 15:524491741
Benzo(k)fluoranthene ND ug/kg 04/09/21 15:29 207-08-904/08/21 15:524491581
Biphenyl (Diphenyl)ND ug/kg 04/09/21 15:29 92-52-404/08/21 15:524491061
4-Bromophenylphenyl ether ND ug/kg 04/09/21 15:29 101-55-304/08/21 15:524491731
Butylbenzylphthalate ND ug/kg 04/09/21 15:29 85-68-704/08/21 15:524491891
Caprolactam ND ug/kg 04/09/21 15:29 105-60-2 v104/08/21 15:524492411
Carbazole ND ug/kg 04/09/21 15:29 86-74-804/08/21 15:524491541
4-Chloro-3-methylphenol ND ug/kg 04/09/21 15:29 59-50-704/08/21 15:528983161
4-Chloroaniline ND ug/kg 04/09/21 15:29 106-47-804/08/21 15:528983531
bis(2-Chloroethoxy)methane ND ug/kg 04/09/21 15:29 111-91-104/08/21 15:524491861
bis(2-Chloroethyl) ether ND ug/kg 04/09/21 15:29 111-44-404/08/21 15:524491691
2-Chloronaphthalene ND ug/kg 04/09/21 15:29 91-58-704/08/21 15:524491781
2-Chlorophenol ND ug/kg 04/09/21 15:29 95-57-804/08/21 15:524491691
4-Chlorophenylphenyl ether ND ug/kg 04/09/21 15:29 7005-72-304/08/21 15:524491671
Chrysene ND ug/kg 04/09/21 15:29 218-01-904/08/21 15:524491631
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-DUP-040721 Lab ID:92531940007 Collected:04/07/21 00:00 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dibenz(a,h)anthracene ND ug/kg 04/09/21 15:29 53-70-304/08/21 15:524491731
Dibenzofuran ND ug/kg 04/09/21 15:29 132-64-904/08/21 15:524491621
3,3'-Dichlorobenzidine ND ug/kg 04/09/21 15:29 91-94-1 IL04/08/21 15:528983041
2,4-Dichlorophenol ND ug/kg 04/09/21 15:29 120-83-204/08/21 15:524491761
Diethylphthalate ND ug/kg 04/09/21 15:29 84-66-204/08/21 15:524491651
2,4-Dimethylphenol ND ug/kg 04/09/21 15:29 105-67-904/08/21 15:524491861
Dimethylphthalate ND ug/kg 04/09/21 15:29 131-11-304/08/21 15:524491631
Di-n-butylphthalate ND ug/kg 04/09/21 15:29 84-74-204/08/21 15:524491511
4,6-Dinitro-2-methylphenol ND ug/kg 04/09/21 15:29 534-52-104/08/21 15:528984191
2,4-Dinitrophenol ND ug/kg 04/09/21 15:29 51-28-504/08/21 15:52225013901
2,4-Dinitrotoluene ND ug/kg 04/09/21 15:29 121-14-204/08/21 15:524491731
2,6-Dinitrotoluene ND ug/kg 04/09/21 15:29 606-20-204/08/21 15:524491651
Di-n-octylphthalate ND ug/kg 04/09/21 15:29 117-84-004/08/21 15:524491771
bis(2-Ethylhexyl)phthalate ND ug/kg 04/09/21 15:29 117-81-704/08/21 15:524491741
Fluoranthene ND ug/kg 04/09/21 15:29 206-44-004/08/21 15:524491541
Fluorene ND ug/kg 04/09/21 15:29 86-73-704/08/21 15:524491581
Hexachloro-1,3-butadiene ND ug/kg 04/09/21 15:29 87-68-304/08/21 15:524491951
Hexachlorobenzene ND ug/kg 04/09/21 15:29 118-74-104/08/21 15:524491761
Hexachlorocyclopentadiene ND ug/kg 04/09/21 15:29 77-47-404/08/21 15:524492571
Hexachloroethane ND ug/kg 04/09/21 15:29 67-72-104/08/21 15:524491721
Indeno(1,2,3-cd)pyrene ND ug/kg 04/09/21 15:29 193-39-504/08/21 15:524491771
Isophorone ND ug/kg 04/09/21 15:29 78-59-104/08/21 15:524492001
2-Methylnaphthalene ND ug/kg 04/09/21 15:29 91-57-604/08/21 15:524491801
2-Methylphenol(o-Cresol)ND ug/kg 04/09/21 15:29 95-48-704/08/21 15:524491841
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/09/21 15:29 15831-10-404/08/21 15:524491811
Naphthalene ND ug/kg 04/09/21 15:29 91-20-304/08/21 15:524491521
2-Nitroaniline ND ug/kg 04/09/21 15:29 88-74-404/08/21 15:5222503681
3-Nitroaniline ND ug/kg 04/09/21 15:29 99-09-204/08/21 15:5222503531
4-Nitroaniline ND ug/kg 04/09/21 15:29 100-01-604/08/21 15:528983421
Nitrobenzene ND ug/kg 04/09/21 15:29 98-95-304/08/21 15:524492081
2-Nitrophenol ND ug/kg 04/09/21 15:29 88-75-504/08/21 15:524491951
4-Nitrophenol ND ug/kg 04/09/21 15:29 100-02-704/08/21 15:5222508691
N-Nitroso-di-n-propylamine ND ug/kg 04/09/21 15:29 621-64-704/08/21 15:524491691
N-Nitrosodiphenylamine ND ug/kg 04/09/21 15:29 86-30-604/08/21 15:524491591
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/09/21 15:29 108-60-104/08/21 15:524492141
Pentachlorophenol ND ug/kg 04/09/21 15:29 87-86-504/08/21 15:528984401
Phenanthrene ND ug/kg 04/09/21 15:29 85-01-804/08/21 15:524491471
Phenol ND ug/kg 04/09/21 15:29 108-95-204/08/21 15:524492001
Pyrene ND ug/kg 04/09/21 15:29 129-00-004/08/21 15:524491821
1,2,4,5-Tetrachlorobenzene ND ug/kg 04/09/21 15:29 95-94-304/08/21 15:524491091
2,3,4,6-Tetrachlorophenol ND ug/kg 04/09/21 15:29 58-90-204/08/21 15:524491131
2,4,5-Trichlorophenol ND ug/kg 04/09/21 15:29 95-95-404/08/21 15:524492061
2,4,6-Trichlorophenol ND ug/kg 04/09/21 15:29 88-06-204/08/21 15:524491851
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-DUP-040721 Lab ID:92531940007 Collected:04/07/21 00:00 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorobiphenyl (S)52 %04/09/21 15:29 321-60-804/08/21 15:5219-130 1
Terphenyl-d14 (S)47 %04/09/21 15:29 1718-51-004/08/21 15:5215-130 1
Phenol-d6 (S)54 %04/09/21 15:29 13127-88-304/08/21 15:5218-130 1
2-Fluorophenol (S)46 %04/09/21 15:29 367-12-404/08/21 15:5218-130 1
2,4,6-Tribromophenol (S)71 %04/09/21 15:29 118-79-604/08/21 15:5218-130 1
Nitrobenzene-d5 (S)47 %04/09/21 15:29 4165-60-004/08/21 15:5221-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 89.5J ug/kg 04/09/21 06:22 67-64-104/08/21 15:5214646.9 1
Benzene ND ug/kg 04/09/21 06:22 71-43-204/08/21 15:527.3 2.9 1
Bromodichloromethane ND ug/kg 04/09/21 06:22 75-27-404/08/21 15:527.3 2.8 1
Bromoform ND ug/kg 04/09/21 06:22 75-25-204/08/21 15:527.3 2.6 1
Bromomethane ND ug/kg 04/09/21 06:22 74-83-904/08/21 15:5214.6 11.5 1
2-Butanone (MEK)ND ug/kg 04/09/21 06:22 78-93-304/08/21 15:5214635.0 1
Carbon disulfide ND ug/kg 04/09/21 06:22 75-15-004/08/21 15:5214.6 9.2 1
Carbon tetrachloride ND ug/kg 04/09/21 06:22 56-23-504/08/21 15:527.3 2.7 1
Chlorobenzene ND ug/kg 04/09/21 06:22 108-90-704/08/21 15:527.3 1.4 1
Chloroethane ND ug/kg 04/09/21 06:22 75-00-304/08/21 15:5214.6 5.6 1
Chloroform ND ug/kg 04/09/21 06:22 67-66-304/08/21 15:527.3 4.4 1
Chloromethane ND ug/kg 04/09/21 06:22 74-87-304/08/21 15:5214.6 6.1 1
Cyclohexane ND ug/kg 04/09/21 06:22 110-82-704/08/21 15:527.3 4.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/09/21 06:22 96-12-804/08/21 15:527.3 2.8 1
Dibromochloromethane ND ug/kg 04/09/21 06:22 124-48-104/08/21 15:527.3 4.1 1
1,2-Dibromoethane (EDB)ND ug/kg 04/09/21 06:22 106-93-404/08/21 15:527.3 3.2 1
1,2-Dichlorobenzene ND ug/kg 04/09/21 06:22 95-50-104/08/21 15:527.3 2.6 1
1,3-Dichlorobenzene ND ug/kg 04/09/21 06:22 541-73-104/08/21 15:527.3 2.3 1
1,4-Dichlorobenzene ND ug/kg 04/09/21 06:22 106-46-704/08/21 15:527.3 1.9 1
Dichlorodifluoromethane ND ug/kg 04/09/21 06:22 75-71-804/08/21 15:5214.6 3.2 1
1,1-Dichloroethane ND ug/kg 04/09/21 06:22 75-34-304/08/21 15:527.3 3.0 1
1,2-Dichloroethane ND ug/kg 04/09/21 06:22 107-06-204/08/21 15:527.3 4.8 1
1,1-Dichloroethene ND ug/kg 04/09/21 06:22 75-35-404/08/21 15:527.3 3.0 1
cis-1,2-Dichloroethene ND ug/kg 04/09/21 06:22 156-59-204/08/21 15:527.3 2.5 1
trans-1,2-Dichloroethene ND ug/kg 04/09/21 06:22 156-60-504/08/21 15:527.3 2.6 1
1,2-Dichloropropane ND ug/kg 04/09/21 06:22 78-87-504/08/21 15:527.3 2.2 1
cis-1,3-Dichloropropene ND ug/kg 04/09/21 06:22 10061-01-504/08/21 15:527.3 2.0 1
trans-1,3-Dichloropropene ND ug/kg 04/09/21 06:22 10061-02-604/08/21 15:527.3 2.5 1
Ethylbenzene 11.1 ug/kg 04/09/21 06:22 100-41-404/08/21 15:527.3 3.4 1
2-Hexanone ND ug/kg 04/09/21 06:22 591-78-604/08/21 15:5273.0 7.0 1
Isopropylbenzene (Cumene)ND ug/kg 04/09/21 06:22 98-82-804/08/21 15:527.3 2.5 1
Methyl acetate ND ug/kg 04/09/21 06:22 79-20-904/08/21 15:5214.6 12.7 1
Methylcyclohexane ND ug/kg 04/09/21 06:22 108-87-204/08/21 15:5214.6 7.7 1
Methylene Chloride ND ug/kg 04/09/21 06:22 75-09-204/08/21 15:5229.2 20.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 50
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Sample:SP-DUP-040721 Lab ID:92531940007 Collected:04/07/21 00:00 Received:04/08/21 09:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/09/21 06:22 108-10-104/08/21 15:5273.0 7.0 1
Methyl-tert-butyl ether ND ug/kg 04/09/21 06:22 1634-04-404/08/21 15:527.3 2.7 1
Styrene ND ug/kg 04/09/21 06:22 100-42-504/08/21 15:527.3 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/09/21 06:22 79-34-504/08/21 15:527.3 1.9 1
Tetrachloroethene ND ug/kg 04/09/21 06:22 127-18-404/08/21 15:527.3 2.3 1
Toluene 40.7 ug/kg 04/09/21 06:22 108-88-304/08/21 15:527.3 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 04/09/21 06:22 87-61-604/08/21 15:527.3 5.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/09/21 06:22 120-82-104/08/21 15:527.3 6.1 1
1,1,1-Trichloroethane ND ug/kg 04/09/21 06:22 71-55-604/08/21 15:527.3 3.8 1
1,1,2-Trichloroethane ND ug/kg 04/09/21 06:22 79-00-504/08/21 15:527.3 2.4 1
Trichloroethene ND ug/kg 04/09/21 06:22 79-01-604/08/21 15:527.3 1.9 1
Trichlorofluoromethane ND ug/kg 04/09/21 06:22 75-69-404/08/21 15:527.3 4.0 1
1,1,2-Trichlorotrifluoroethane ND ug/kg 04/09/21 06:22 76-13-104/08/21 15:527.3 4.1 1
Vinyl chloride ND ug/kg 04/09/21 06:22 75-01-404/08/21 15:5214.6 3.7 1
Xylene (Total)ND ug/kg 04/09/21 06:22 1330-20-704/08/21 15:5214.6 4.2 1
Surrogates
Toluene-d8 (S)103 %04/09/21 06:22 2037-26-504/08/21 15:5270-130 1
4-Bromofluorobenzene (S)107 %04/09/21 06:22 460-00-404/08/21 15:5269-134 1
1,2-Dichloroethane-d4 (S)110 %04/09/21 06:22 17060-07-004/08/21 15:5270-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 26.0 %04/08/21 15:12 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 78.0 %04/14/21 09:1004/14/21 08:571
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 04/12/21 00:52 18540-29-904/10/21 13:331.28 0.327 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
613070
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3226848
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 04/13/21 15:010.0046
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3226849LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0900.083 108 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3226850MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92530715021
3226851
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg M1,R10.072 128 75-12590 37 200.0640.018 0.11 0.075
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
612829
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3225931
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 2.5 04/15/21 11:500.50
Barium mg/kg ND 1.0 04/13/21 01:110.25
Cadmium mg/kg 0.050J 0.10 04/15/21 11:500.050
Chromium mg/kg ND 0.50 04/15/21 11:500.25
Lead mg/kg ND 1.0 04/15/21 11:500.25
Manganese mg/kg ND 0.50 04/15/21 11:500.25
Selenium mg/kg ND 1.0 04/15/21 11:500.50
Silver mg/kg ND 0.50 04/15/21 11:500.25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3225932LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 47.950 96 80-120
Barium mg/kg 48.550 97 80-120
Cadmium mg/kg 48.650 97 80-120
Chromium mg/kg 49.550 99 80-120
Lead mg/kg 49.350 99 80-120
Manganese mg/kg 49.450 99 80-120
Selenium mg/kg 46.250 92 80-120
Silver mg/kg 24.425 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3225933MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92530814001
3225934
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 34.8 114 75-125108 4 2033.936.1 75.9 72.7
Barium mg/kg 34.8 98 75-12593 6 2033.99.6 43.1 40.6
Cadmium mg/kg 34.8 114 75-125112 5 2033.9ND 39.8 38.1
Chromium mg/kg M134.8 154 75-12559 2 2033.91600 1650 1620
Lead mg/kg 34.8 99 75-12596 3 2033.926.4 60.9 59.0
Manganese mg/kg M134.8 116 75-125-83 2 2033.92870 2910 2840
Selenium mg/kg M134.8 0 75-1250 2033.9ND ND ND
Silver mg/kg 17.4 106 75-125103 4 2016.95.2 23.6 22.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
613520
EPA 3010A
EPA 6010D
6010 MET SPLP
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3226897
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Matrix:Water
AnalyzedMDL
Manganese mg/L ND 0.0050 04/14/21 16:560.0034
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3229157LABORATORY CONTROL SAMPLE:
LCSSpike
Manganese mg/L 0.490.5 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3229158MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92531940001
3229159
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Manganese mg/L 0.5 96 75-12596 0 200.50.013 0.49 0.49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
612468
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92531940004, 92531940005, 92531940006, 92531940007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3224065
Associated Lab Samples:92531940004, 92531940005, 92531940006, 92531940007
Matrix:Solid
AnalyzedMDL
1,1,1-Trichloroethane ug/kg ND 5.0 04/09/21 01:512.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/09/21 01:511.3
1,1,2-Trichloroethane ug/kg ND 5.0 04/09/21 01:511.7
1,1,2-Trichlorotrifluoroethane ug/kg ND 5.0 04/09/21 01:512.8
1,1-Dichloroethane ug/kg ND 5.0 04/09/21 01:512.1
1,1-Dichloroethene ug/kg ND 5.0 04/09/21 01:512.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 04/09/21 01:514.0
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/09/21 01:514.2
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/09/21 01:511.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/09/21 01:512.2
1,2-Dichlorobenzene ug/kg ND 5.0 04/09/21 01:511.8
1,2-Dichloroethane ug/kg ND 5.0 04/09/21 01:513.3
1,2-Dichloropropane ug/kg ND 5.0 04/09/21 01:511.5
1,3-Dichlorobenzene ug/kg ND 5.0 04/09/21 01:511.6
1,4-Dichlorobenzene ug/kg ND 5.0 04/09/21 01:511.3
2-Butanone (MEK)ug/kg ND 100 04/09/21 01:5124.0
2-Hexanone ug/kg ND 50.0 04/09/21 01:514.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/09/21 01:514.8
Acetone ug/kg ND 100 04/09/21 01:5132.1
Benzene ug/kg ND 5.0 04/09/21 01:512.0
Bromodichloromethane ug/kg ND 5.0 04/09/21 01:511.9
Bromoform ug/kg ND 5.0 04/09/21 01:511.8
Bromomethane ug/kg ND 10.0 04/09/21 01:517.9
Carbon disulfide ug/kg ND 10.0 04/09/21 01:516.3
Carbon tetrachloride ug/kg ND 5.0 04/09/21 01:511.9
Chlorobenzene ug/kg ND 5.0 04/09/21 01:510.96
Chloroethane ug/kg ND 10.0 04/09/21 01:513.9
Chloroform ug/kg ND 5.0 04/09/21 01:513.0
Chloromethane ug/kg ND 10.0 04/09/21 01:514.2
cis-1,2-Dichloroethene ug/kg ND 5.0 04/09/21 01:511.7
cis-1,3-Dichloropropene ug/kg ND 5.0 04/09/21 01:511.4
Cyclohexane ug/kg ND 5.0 04/09/21 01:513.0
Dibromochloromethane ug/kg ND 5.0 04/09/21 01:512.8
Dichlorodifluoromethane ug/kg ND 10.0 04/09/21 01:512.2
Ethylbenzene ug/kg ND 5.0 04/09/21 01:512.3
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/09/21 01:511.7
Methyl acetate ug/kg ND 10.0 04/09/21 01:518.7
Methyl-tert-butyl ether ug/kg ND 5.0 04/09/21 01:511.9
Methylcyclohexane ug/kg ND 10.0 04/09/21 01:515.3
Methylene Chloride ug/kg ND 20.0 04/09/21 01:5113.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3224065
Associated Lab Samples:92531940004, 92531940005, 92531940006, 92531940007
Matrix:Solid
AnalyzedMDL
Styrene ug/kg ND 5.0 04/09/21 01:511.3
Tetrachloroethene ug/kg ND 5.0 04/09/21 01:511.6
Toluene ug/kg ND 5.0 04/09/21 01:511.4
trans-1,2-Dichloroethene ug/kg ND 5.0 04/09/21 01:511.8
trans-1,3-Dichloropropene ug/kg ND 5.0 04/09/21 01:511.7
Trichloroethene ug/kg ND 5.0 04/09/21 01:511.3
Trichlorofluoromethane ug/kg ND 5.0 04/09/21 01:512.8
Vinyl chloride ug/kg ND 10.0 04/09/21 01:512.5
Xylene (Total)ug/kg ND 10.0 04/09/21 01:512.8
1,2-Dichloroethane-d4 (S)%111 70-130 04/09/21 01:51
4-Bromofluorobenzene (S)%108 69-134 04/09/21 01:51
Toluene-d8 (S)%100 70-130 04/09/21 01:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3224066LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/kg 11401250 91 70-130
1,1,2,2-Tetrachloroethane ug/kg 12101250 97 70-130
1,1,2-Trichloroethane ug/kg 11801250 94 70-130
1,1,2-Trichlorotrifluoroethane ug/kg 11201250 90 67-130
1,1-Dichloroethane ug/kg 12201250 98 70-130
1,1-Dichloroethene ug/kg 12501250 100 70-130
1,2,3-Trichlorobenzene ug/kg 11301250 90 65-130
1,2,4-Trichlorobenzene ug/kg 10901250 87 68-130
1,2-Dibromo-3-chloropropane ug/kg 11001250 88 70-130
1,2-Dibromoethane (EDB)ug/kg 12301250 98 70-130
1,2-Dichlorobenzene ug/kg 11001250 88 70-130
1,2-Dichloroethane ug/kg 12101250 97 63-130
1,2-Dichloropropane ug/kg 12601250 101 70-130
1,3-Dichlorobenzene ug/kg 10801250 87 70-130
1,4-Dichlorobenzene ug/kg 10901250 87 70-130
2-Butanone (MEK)ug/kg 26602500 106 70-130
2-Hexanone ug/kg 27702500 111 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 26602500 106 70-130
Acetone ug/kg 26902500 108 69-130
Benzene ug/kg 12101250 97 70-130
Bromodichloromethane ug/kg 11901250 95 69-130
Bromoform ug/kg 11501250 92 70-130
Bromomethane ug/kg 11601250 93 52-130
Carbon disulfide ug/kg 12301250 98 67-130
Carbon tetrachloride ug/kg 11701250 93 70-130
Chlorobenzene ug/kg 11601250 92 70-130
Chloroethane ug/kg 12801250 103 65-130
Chloroform ug/kg 11201250 89 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3224066LABORATORY CONTROL SAMPLE:
LCSSpike
Chloromethane ug/kg 12501250 100 55-130
cis-1,2-Dichloroethene ug/kg 12701250 101 70-130
cis-1,3-Dichloropropene ug/kg 12201250 98 70-130
Cyclohexane ug/kg 13001250 104 70-134
Dibromochloromethane ug/kg 12001250 96 70-130
Dichlorodifluoromethane ug/kg 11601250 93 45-156
Ethylbenzene ug/kg 11301250 91 70-130
Isopropylbenzene (Cumene)ug/kg 11901250 95 70-130
Methyl acetate ug/kg 11001250 88 70-130
Methyl-tert-butyl ether ug/kg 11801250 94 70-130
Methylcyclohexane ug/kg 14001250 112 70-130
Methylene Chloride ug/kg 13301250 106 65-130
Styrene ug/kg 12501250 100 70-130
Tetrachloroethene ug/kg 11001250 88 70-130
Toluene ug/kg 11701250 93 70-130
trans-1,2-Dichloroethene ug/kg 12801250 102 70-130
trans-1,3-Dichloropropene ug/kg 12101250 97 68-130
Trichloroethene ug/kg 11001250 88 70-130
Trichlorofluoromethane ug/kg 10501250 84 70-130
Vinyl chloride ug/kg 11601250 93 61-130
Xylene (Total)ug/kg 35903750 96 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%107 69-134
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3224068MATRIX SPIKE SAMPLE:
MSSpike
Result
92531896004
1,1,1-Trichloroethane ug/kg 585514 114 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 571514 111 66-130ND
1,1,2-Trichloroethane ug/kg 586514 114 66-133ND
1,1,2-Trichlorotrifluoroethane ug/kg 525514 102 32-133ND
1,1-Dichloroethane ug/kg 564514 110 65-130ND
1,1-Dichloroethene ug/kg 594514 116 10-158ND
1,2,3-Trichlorobenzene ug/kg 602514 117 27-138ND
1,2,4-Trichlorobenzene ug/kg 567514 110 51-134ND
1,2-Dibromo-3-chloropropane ug/kg 479514 93 32-130ND
1,2-Dibromoethane (EDB)ug/kg 588514 115 70-130ND
1,2-Dichlorobenzene ug/kg 566514 110 69-130ND
1,2-Dichloroethane ug/kg 612514 119 59-130ND
1,2-Dichloropropane ug/kg 642514 125 70-130ND
1,3-Dichlorobenzene ug/kg 570514 111 70-130ND
1,4-Dichlorobenzene ug/kg 558514 109 68-130ND
2-Butanone (MEK)ug/kg 11801030 115 10-136ND
2-Hexanone ug/kg 12301030 119 10-144ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3224068MATRIX SPIKE SAMPLE:
MSSpike
Result
92531896004
4-Methyl-2-pentanone (MIBK)ug/kg 12301030 120 25-143ND
Acetone ug/kg 9581030 93 10-130ND
Benzene ug/kg 626514 122 67-130ND
Bromodichloromethane ug/kg 581514 113 64-130ND
Bromoform ug/kg 518514 101 62-130ND
Bromomethane ug/kg 530514 103 20-176ND
Carbon disulfide ug/kg 559514 109 42-130ND
Carbon tetrachloride ug/kg 573514 112 65-140ND
Chlorobenzene ug/kg 589514 115 70-130ND
Chloroethane ug/kg 237514 46 10-130ND
Chloroform ug/kg 547514 106 63-130ND
Chloromethane ug/kg 658514 128 58-130ND
cis-1,2-Dichloroethene ug/kg 609514 119 66-130ND
cis-1,3-Dichloropropene ug/kg 586514 114 67-130ND
Cyclohexane ug/kg 695514 135 70-158ND
Dibromochloromethane ug/kg 556514 108 67-130ND
Dichlorodifluoromethane ug/kg 585514 114 44-180ND
Ethylbenzene ug/kg 593514 115 66-130ND
Isopropylbenzene (Cumene)ug/kg 631514 123 69-135ND
Methyl acetate ug/kg 610514 119 49-152ND
Methyl-tert-butyl ether ug/kg 557514 109 65-130ND
Methylcyclohexane ug/kg 960514 187 24-200ND
Methylene Chloride ug/kg 623514 121 61-130ND
Styrene ug/kg 626514 122 70-132ND
Tetrachloroethene ug/kg 567514 109 70-1350.0050J mg/kg
Toluene ug/kg 607514 118 67-130ND
trans-1,2-Dichloroethene ug/kg 613514 119 69-130ND
trans-1,3-Dichloropropene ug/kg 568514 111 62-130ND
Trichloroethene ug/kg 578514 112 70-135ND
Trichlorofluoromethane ug/kg 196514 38 10-130ND
Vinyl chloride ug/kg 586514 114 61-148ND
Xylene (Total)ug/kg 18801540 122 63-132ND
1,2-Dichloroethane-d4 (S)%127 70-130
4-Bromofluorobenzene (S)%106 69-134
Toluene-d8 (S)%103 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92531896003
3224067SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1,2-Trichlorotrifluoroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92531896003
3224067SAMPLE DUPLICATE:
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon disulfide ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Cyclohexane ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
Methyl acetate ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylcyclohexane ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
Styrene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%110109
4-Bromofluorobenzene (S)%108106
Toluene-d8 (S)%102102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
612435
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3223767
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Matrix:Solid
AnalyzedMDL
1,2,4,5-Tetrachlorobenzene ug/kg ND 327 04/09/21 11:2679.6
2,2'-Oxybis(1-chloropropane)ug/kg ND 327 04/09/21 11:26155
2,3,4,6-Tetrachlorophenol ug/kg ND 327 04/09/21 11:2681.9
2,4,5-Trichlorophenol ug/kg ND 327 04/09/21 11:26150
2,4,6-Trichlorophenol ug/kg ND 327 04/09/21 11:26135
2,4-Dichlorophenol ug/kg ND 327 04/09/21 11:26128
2,4-Dimethylphenol ug/kg ND 327 04/09/21 11:26136
2,4-Dinitrophenol ug/kg ND 1630 04/09/21 11:261010
2,4-Dinitrotoluene ug/kg ND 327 04/09/21 11:26126
2,6-Dinitrotoluene ug/kg ND 327 04/09/21 11:26120
2-Chloronaphthalene ug/kg ND 327 04/09/21 11:26130
2-Chlorophenol ug/kg ND 327 04/09/21 11:26123
2-Methylnaphthalene ug/kg ND 327 04/09/21 11:26131
2-Methylphenol(o-Cresol)ug/kg ND 327 04/09/21 11:26134
2-Nitroaniline ug/kg ND 1630 04/09/21 11:26267
2-Nitrophenol ug/kg ND 327 04/09/21 11:26142
3&4-Methylphenol(m&p Cresol)ug/kg ND 327 04/09/21 11:26132
3,3'-Dichlorobenzidine ug/kg ND 653 IL04/09/21 11:26221
3-Nitroaniline ug/kg ND 1630 04/09/21 11:26256
4,6-Dinitro-2-methylphenol ug/kg ND 653 04/09/21 11:26305
4-Bromophenylphenyl ether ug/kg ND 327 04/09/21 11:26126
4-Chloro-3-methylphenol ug/kg ND 653 04/09/21 11:26230
4-Chloroaniline ug/kg ND 653 04/09/21 11:26256
4-Chlorophenylphenyl ether ug/kg ND 327 04/09/21 11:26122
4-Nitroaniline ug/kg ND 653 04/09/21 11:26249
4-Nitrophenol ug/kg ND 1630 04/09/21 11:26632
Acenaphthene ug/kg ND 327 04/09/21 11:26115
Acenaphthylene ug/kg ND 327 04/09/21 11:26115
Acetophenone ug/kg ND 327 04/09/21 11:2684.2
Anthracene ug/kg ND 327 04/09/21 11:26107
Atrazine ug/kg ND 327 04/09/21 11:26105
Benzaldehyde ug/kg ND 327 04/09/21 11:26109
Benzo(a)anthracene ug/kg ND 327 04/09/21 11:26109
Benzo(a)pyrene ug/kg ND 327 04/09/21 11:26113
Benzo(b)fluoranthene ug/kg ND 327 04/09/21 11:26109
Benzo(g,h,i)perylene ug/kg ND 327 04/09/21 11:26127
Benzo(k)fluoranthene ug/kg ND 327 04/09/21 11:26115
Biphenyl (Diphenyl)ug/kg ND 327 04/09/21 11:2677.4
bis(2-Chloroethoxy)methane ug/kg ND 327 04/09/21 11:26136
bis(2-Chloroethyl) ether ug/kg ND 327 04/09/21 11:26123
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3223767
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Matrix:Solid
AnalyzedMDL
bis(2-Ethylhexyl)phthalate ug/kg ND 327 04/09/21 11:26127
Butylbenzylphthalate ug/kg ND 327 04/09/21 11:26138
Caprolactam ug/kg ND 327 v104/09/21 11:26175
Carbazole ug/kg ND 327 04/09/21 11:26112
Chrysene ug/kg ND 327 04/09/21 11:26119
Di-n-butylphthalate ug/kg ND 327 04/09/21 11:26110
Di-n-octylphthalate ug/kg ND 327 04/09/21 11:26129
Dibenz(a,h)anthracene ug/kg ND 327 04/09/21 11:26126
Dibenzofuran ug/kg ND 327 04/09/21 11:26118
Diethylphthalate ug/kg ND 327 04/09/21 11:26120
Dimethylphthalate ug/kg ND 327 04/09/21 11:26119
Fluoranthene ug/kg ND 327 04/09/21 11:26112
Fluorene ug/kg ND 327 04/09/21 11:26115
Hexachloro-1,3-butadiene ug/kg ND 327 04/09/21 11:26142
Hexachlorobenzene ug/kg ND 327 04/09/21 11:26128
Hexachlorocyclopentadiene ug/kg ND 327 04/09/21 11:26187
Hexachloroethane ug/kg ND 327 04/09/21 11:26125
Indeno(1,2,3-cd)pyrene ug/kg ND 327 04/09/21 11:26129
Isophorone ug/kg ND 327 04/09/21 11:26146
N-Nitroso-di-n-propylamine ug/kg ND 327 04/09/21 11:26123
N-Nitrosodiphenylamine ug/kg ND 327 04/09/21 11:26116
Naphthalene ug/kg ND 327 04/09/21 11:26111
Nitrobenzene ug/kg ND 327 04/09/21 11:26151
Pentachlorophenol ug/kg ND 653 04/09/21 11:26320
Phenanthrene ug/kg ND 327 04/09/21 11:26107
Phenol ug/kg ND 327 04/09/21 11:26146
Pyrene ug/kg ND 327 04/09/21 11:26133
2,4,6-Tribromophenol (S)%78 18-130 04/09/21 11:26
2-Fluorobiphenyl (S)%69 19-130 04/09/21 11:26
2-Fluorophenol (S)%75 18-130 04/09/21 11:26
Nitrobenzene-d5 (S)%75 21-130 04/09/21 11:26
Phenol-d6 (S)%76 18-130 04/09/21 11:26
Terphenyl-d14 (S)%89 15-130 04/09/21 11:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3223768LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/kg 13101640 80 56-130
2,2'-Oxybis(1-chloropropane)ug/kg 13001640 79 38-130
2,3,4,6-Tetrachlorophenol ug/kg 15901640 97 51-133
2,4,5-Trichlorophenol ug/kg 15501640 94 49-130
2,4,6-Trichlorophenol ug/kg 14701640 90 50-130
2,4-Dichlorophenol ug/kg 15701640 95 51-130
2,4-Dimethylphenol ug/kg 16401640 100 53-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3223768LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrophenol ug/kg 81508200 99 39-130
2,4-Dinitrotoluene ug/kg 16001640 98 53-130
2,6-Dinitrotoluene ug/kg 15601640 95 55-130
2-Chloronaphthalene ug/kg 13901640 85 48-130
2-Chlorophenol ug/kg 14201640 87 54-130
2-Methylnaphthalene ug/kg 14201640 87 57-130
2-Methylphenol(o-Cresol)ug/kg 15101640 92 50-130
2-Nitroaniline ug/kg 28303280 86 49-130
2-Nitrophenol ug/kg 14601640 89 50-130
3&4-Methylphenol(m&p Cresol)ug/kg 15201640 93 50-130
3,3'-Dichlorobenzidine ug/kg 2950 IL32809047-130
3-Nitroaniline ug/kg 28903280 88 45-130
4,6-Dinitro-2-methylphenol ug/kg 31703280 97 50-142
4-Bromophenylphenyl ether ug/kg 13901640 85 55-130
4-Chloro-3-methylphenol ug/kg 31003280 95 52-130
4-Chloroaniline ug/kg 29803280 91 49-130
4-Chlorophenylphenyl ether ug/kg 15401640 94 53-130
4-Nitroaniline ug/kg 30603280 93 51-130
4-Nitrophenol ug/kg 81808200 100 40-130
Acenaphthene ug/kg 14801640 90 56-130
Acenaphthylene ug/kg 14501640 89 58-130
Acetophenone ug/kg 14401640 88 54-130
Anthracene ug/kg 14501640 88 60-130
Atrazine ug/kg 9961640 61 26-130
Benzaldehyde ug/kg 9791640 60 10-130
Benzo(a)anthracene ug/kg 15501640 95 59-130
Benzo(a)pyrene ug/kg 16001640 98 57-130
Benzo(b)fluoranthene ug/kg 17301640 106 54-130
Benzo(g,h,i)perylene ug/kg 16201640 99 59-130
Benzo(k)fluoranthene ug/kg 16301640 99 54-130
Biphenyl (Diphenyl)ug/kg 14001640 85 53-130
bis(2-Chloroethoxy)methane ug/kg 15001640 92 55-130
bis(2-Chloroethyl) ether ug/kg 14201640 86 53-130
bis(2-Ethylhexyl)phthalate ug/kg 15101640 92 58-130
Butylbenzylphthalate ug/kg 15301640 93 46-138
Caprolactam ug/kg 645 v116403916-130
Carbazole ug/kg 17701640 108 60-130
Chrysene ug/kg 15201640 93 57-130
Di-n-butylphthalate ug/kg 15001640 91 57-130
Di-n-octylphthalate ug/kg 15901640 97 57-130
Dibenz(a,h)anthracene ug/kg 16301640 99 60-130
Dibenzofuran ug/kg 15501640 94 54-130
Diethylphthalate ug/kg 15101640 92 55-130
Dimethylphthalate ug/kg 15101640 92 57-130
Fluoranthene ug/kg 15701640 96 57-130
Fluorene ug/kg 15001640 91 56-130
Hexachloro-1,3-butadiene ug/kg 13901640 85 41-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
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[phone]
Page 35 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3223768LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 14501640 88 53-130
Hexachlorocyclopentadiene ug/kg 13001640 79 23-130
Hexachloroethane ug/kg 13301640 81 48-130
Indeno(1,2,3-cd)pyrene ug/kg 16501640 101 61-130
Isophorone ug/kg 15101640 92 49-130
N-Nitroso-di-n-propylamine ug/kg 15701640 96 52-130
N-Nitrosodiphenylamine ug/kg 14101640 86 56-130
Naphthalene ug/kg 14301640 87 56-130
Nitrobenzene ug/kg 14001640 85 50-130
Pentachlorophenol ug/kg 29503280 90 33-130
Phenanthrene ug/kg 14501640 89 60-130
Phenol ug/kg 16101640 98 54-130
Pyrene ug/kg 14901640 91 61-130
2,4,6-Tribromophenol (S)%88 18-130
2-Fluorobiphenyl (S)%83 19-130
2-Fluorophenol (S)%84 18-130
Nitrobenzene-d5 (S)%84 21-130
Phenol-d6 (S)%88 18-130
Terphenyl-d14 (S)%74 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3223769MATRIX SPIKE SAMPLE:
MSSpike
Result
92531940001
1,2,4,5-Tetrachlorobenzene ug/kg 17102070 83 16-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 17202070 83 30-130ND
2,3,4,6-Tetrachlorophenol ug/kg 20002070 97 10-200ND
2,4,5-Trichlorophenol ug/kg 19202070 93 26-130ND
2,4,6-Trichlorophenol ug/kg 18302070 89 23-130ND
2,4-Dichlorophenol ug/kg 19802070 96 29-130ND
2,4-Dimethylphenol ug/kg 19502070 94 13-130ND
2,4-Dinitrophenol ug/kg 378010400 37 10-131ND
2,4-Dinitrotoluene ug/kg 19802070 95 28-130ND
2,6-Dinitrotoluene ug/kg 20102070 97 36-130ND
2-Chloronaphthalene ug/kg 17702070 85 27-130ND
2-Chlorophenol ug/kg 18402070 89 29-130ND
2-Methylnaphthalene ug/kg 19102070 92 29-130ND
2-Methylphenol(o-Cresol)ug/kg 19402070 94 20-130ND
2-Nitroaniline ug/kg 36304150 88 29-130ND
2-Nitrophenol ug/kg 19402070 93 26-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 21602070 104 10-176ND
3,3'-Dichlorobenzidine ug/kg 3710 IL41508915-130ND
3-Nitroaniline ug/kg 38304150 92 28-130ND
4,6-Dinitro-2-methylphenol ug/kg 34704150 84 15-132ND
4-Bromophenylphenyl ether ug/kg 17402070 84 35-130ND
4-Chloro-3-methylphenol ug/kg 42204150 102 30-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
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[phone]
Page 36 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3223769MATRIX SPIKE SAMPLE:
MSSpike
Result
92531940001
4-Chloroaniline ug/kg 37204150 90 28-130ND
4-Chlorophenylphenyl ether ug/kg 19402070 94 32-130ND
4-Nitroaniline ug/kg 42104150 102 30-130ND
4-Nitrophenol ug/kg 1050010400 101 17-130ND
Acenaphthene ug/kg 18502070 89 29-130ND
Acenaphthylene ug/kg 19002070 92 31-130ND
Acetophenone ug/kg 19402070 93 31-130ND
Anthracene ug/kg 18402070 89 33-130ND
Atrazine ug/kg 9472070 46 10-130ND
Benzaldehyde ug/kg 17002070 82 10-130ND
Benzo(a)anthracene ug/kg 19402070 92 32-130ND
Benzo(a)pyrene ug/kg 19402070 94 32-130ND
Benzo(b)fluoranthene ug/kg 20502070 99 33-130ND
Benzo(g,h,i)perylene ug/kg 20902070 101 28-130ND
Benzo(k)fluoranthene ug/kg 19502070 94 31-130ND
Biphenyl (Diphenyl)ug/kg 17502070 85 22-130ND
bis(2-Chloroethoxy)methane ug/kg 18502070 89 30-130ND
bis(2-Chloroethyl) ether ug/kg 18602070 90 68-130ND
bis(2-Ethylhexyl)phthalate ug/kg 17702070 86 40-130ND
Butylbenzylphthalate ug/kg 17602070 85 40-130ND
Caprolactam ug/kg 869 v120704210-130ND
Carbazole ug/kg 22802070 110 30-130ND
Chrysene ug/kg 19202070 91 30-130ND
Di-n-butylphthalate ug/kg 18602070 90 41-130ND
Di-n-octylphthalate ug/kg 19002070 91 42-130ND
Dibenz(a,h)anthracene ug/kg 20602070 100 27-130ND
Dibenzofuran ug/kg 19502070 94 32-130ND
Diethylphthalate ug/kg 19702070 95 40-130ND
Dimethylphthalate ug/kg 19302070 93 37-130ND
Fluoranthene ug/kg 20802070 97 26-130ND
Fluorene ug/kg 19702070 95 31-130ND
Hexachloro-1,3-butadiene ug/kg 18302070 88 20-130ND
Hexachlorobenzene ug/kg 18602070 90 29-130ND
Hexachlorocyclopentadiene ug/kg 15902070 77 10-130ND
Hexachloroethane ug/kg 17302070 84 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 21302070 103 28-130ND
Isophorone ug/kg 19002070 92 32-130ND
N-Nitroso-di-n-propylamine ug/kg 20402070 99 31-130ND
N-Nitrosodiphenylamine ug/kg 17002070 82 32-130ND
Naphthalene ug/kg 18802070 91 30-130ND
Nitrobenzene ug/kg 18702070 90 25-130ND
Pentachlorophenol ug/kg 34904150 84 10-130ND
Phenanthrene ug/kg 18702070 90 34-130ND
Phenol ug/kg 19902070 96 14-130ND
Pyrene ug/kg 18302070 86 31-130ND
2,4,6-Tribromophenol (S)%86 18-130
2-Fluorobiphenyl (S)%79 19-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
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Page 37 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3223769MATRIX SPIKE SAMPLE:
MSSpike
Result
92531940001
2-Fluorophenol (S)%79 18-130
Nitrobenzene-d5 (S)%85 21-130
Phenol-d6 (S)%86 18-130
Terphenyl-d14 (S)%66 15-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92531940002
3223770SAMPLE DUPLICATE:
1,2,4,5-Tetrachlorobenzene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,3,4,6-Tetrachlorophenol ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Acetophenone ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Atrazine ug/kg ND 30ND
Benzaldehyde ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92531940002
3223770SAMPLE DUPLICATE:
Biphenyl (Diphenyl)ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Caprolactam ug/kg ND 30ND
Carbazole ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2,4,6-Tribromophenol (S)%10889
2-Fluorobiphenyl (S)%9273
2-Fluorophenol (S)%8367
Nitrobenzene-d5 (S)%9480
Phenol-d6 (S)%9472
Terphenyl-d14 (S)%8471
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
612457
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92531940004, 92531940005, 92531940006, 92531940007
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92531592001
3223933SAMPLE DUPLICATE:
Percent Moisture %81.7 N202581.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92531970001
3223934SAMPLE DUPLICATE:
Percent Moisture %0.31 N22250.30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
612483
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92531940001, 92531940002, 92531940003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92531896006
3224139SAMPLE DUPLICATE:
Percent Moisture %11.3 N2102512.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92532064001
3224140SAMPLE DUPLICATE:
Percent Moisture %21.4 N222521.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1650596
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92531940001, 92531940002, 92531940003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3642101-1
Associated Lab Samples:92531940001, 92531940002, 92531940003
Matrix:Solid
AnalyzedMDL
Total Solids %0.00200 04/14/21 09:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3642101-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
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[phone]
Page 42 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1650600
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92531940007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3642082-1
Associated Lab Samples:92531940007
Matrix:Solid
AnalyzedMDL
Total Solids %0.00200 04/14/21 09:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3642082-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 99.9 85.0-115
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1648951
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3640835-1
Associated Lab Samples:92531940001, 92531940002, 92531940003, 92531940007
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 04/11/21 19:280.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3640835-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.7910.0 97.9 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3640835-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1336381-01
R3640835-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 24.2 79.6 75.0-12580.0 0.458 2024.21.60 20.9 21.0
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3640835-5MATRIX SPIKE SAMPLE:
MSSpike
Result
L1336381-01
Chromium, Hexavalent mg/kg 811779 104 75.0-1251.60
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1336381-02
R3640835-7SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.396J J2.48 200.406
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92531940007
R3640835-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 44 of 50
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92531940007
R3640835-9SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
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Page 45 of 50
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 50
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92531940
MATHESON AVENUE SITES
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92531940001 612829 612969SP-03 EPA 3050B EPA 6010D
92531940002 612829 612969SP-04 EPA 3050B EPA 6010D
92531940003 612829 612969SP-05 EPA 3050B EPA 6010D
92531940007 612829 612969SP-DUP-040721 EPA 3050B EPA 6010D
92531940001 613520 613536SP-03 EPA 3010A EPA 6010D
92531940002 613520 613536SP-04 EPA 3010A EPA 6010D
92531940003 613520 613536SP-05 EPA 3010A EPA 6010D
92531940007 613520 613536SP-DUP-040721 EPA 3010A EPA 6010D
92531940001 613070 613190SP-03 EPA 7471B EPA 7471B
92531940002 613070 613190SP-04 EPA 7471B EPA 7471B
92531940003 613070 613190SP-05 EPA 7471B EPA 7471B
92531940007 613070 613190SP-DUP-040721 EPA 7471B EPA 7471B
92531940001 612435 612615SP-03 EPA 3546 EPA 8270E
92531940002 612435 612615SP-04 EPA 3546 EPA 8270E
92531940003 612435 612615SP-05 EPA 3546 EPA 8270E
92531940007 612435 612615SP-DUP-040721 EPA 3546 EPA 8270E
92531940004 612468 612509SP-03B EPA 5035A/5030B EPA 8260D
92531940005 612468 612509SP-04C EPA 5035A/5030B EPA 8260D
92531940006 612468 612509SP-05D EPA 5035A/5030B EPA 8260D
92531940007 612468 612509SP-DUP-040721 EPA 5035A/5030B EPA 8260D
92531940001 612483SP-03 SW-846
92531940002 612483SP-04 SW-846
92531940003 612483SP-05 SW-846
92531940004 612457SP-03B SW-846
92531940005 612457SP-04C SW-846
92531940006 612457SP-05D SW-846
92531940007 612457SP-DUP-040721 SW-846
92531940001 1650596 1650596SP-03 SM 2540 G SM 2540G
92531940002 1650596 1650596SP-04 SM 2540 G SM 2540G
92531940003 1650596 1650596SP-05 SM 2540 G SM 2540G
92531940007 1650600 1650600SP-DUP-040721 SM 2540 G SM 2540G
92531940001 1648951 1648951SP-03 3060A EPA 7199
92531940002 1648951 1648951SP-04 3060A EPA 7199
92531940003 1648951 1648951SP-05 3060A EPA 7199
92531940007 1648951 1648951SP-DUP-040721 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/19/2021 03:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 50
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APPENDIX B

NCDEQ Risk Calculator Output Sheets
Exposure Point Concentrations
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID:
Exposure Unit ID:
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
0.116 J Flag Matheson SP-05 67-64-1 Acetone mg/kg
3 Reeves 01 7440-38-2 Arsenic, Inorganic mg/kg
150 Reeves 05 7440-39-3 Barium mg/kg
0.0331 Matheson SP-02 74-83-9 Bromomethane mg/kg
0.13 J Flag Reeves 01 7440-43-9 Cadmium (Diet)mg/kg
57.76 Reeves 01 16065-83-1 Chromium(III), Insoluble Salts mg/kg
0.636 J Flag Matheson SP-03 18540-29-9 Chromium(VI)mg/kg
0.0059 J Flag Matheson SP-03 110-82-7 Cyclohexane mg/kg
0.0117 Matheson SP-05 100-41-4 Ethylbenzene mg/kg
29 Reeve 04 7439-92-1 ~Lead and Compounds mg/kg
746 Matheson SP-02 7439-96-5 Manganese (Non-diet)mg/kg
0.097 Reeves 01 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
0.143 Matheson SP-02 79-20-9 Methyl Acetate mg/kg
0.0408 J Flag Matheson SP-05 78-93-3 Methyl Ethyl Ketone (2-Butanone)mg/kg
0.156 J Flag Matheson SP-02 117-81-7 ~Bis(2-ethylhexyl)phthalate mg/kg
0.257 J Flag Matheson SP-05 56-55-3 ~Benz[a]anthracene mg/kg
0.224 J Flag Matheson SP-05 50-32-8 ~Benzo[a]pyrene mg/kg
0.257 J Flag Matheson SP-05 205-99-2 ~Benzo[b]fluoranthene mg/kg
0.254 J Flag Matheson SP-05 218-01-9 ~Chrysene mg/kg
0.603 Matheson SP-05 206-44-0 ~Fluoranthene mg/kg
0.452 Matheson SP-05 129-00-0 ~Pyrene mg/kg
6.4 Reeves 01 7782-49-2 Selenium mg/kg
0.54 J Flag Reeves 01 7440-22-4 Silver mg/kg
0.0565 Matheson SP-05 108-88-3 Toluene mg/kg
0.0171 Matheson SP-03 1330-20-7 Xylenes mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID:
Exposure Unit ID:
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.116 0.116 0.116 1.6E-06 2.5E-07 1.9E-06
7440-38-2 Arsenic, Inorganic 3 3 3 3.9E-06 5.5E-07 7.7E-11 4.4E-06 7.7E-02 9.1E-03 3.2E-06 8.6E-02
7440-39-3 Barium 150 150 150 9.6E-03 4.8E-06 9.6E-03
74-83-9 Bromomethane 0.0331 0.0331 0.0331 3.0E-04 2.0E-03 2.3E-03
7440-43-9 Cadmium (Diet)0.13 0.13 0.13 1.4E-12 1.4E-12 1.7E-03 1.6E-04 2.1E-07 1.8E-03
16065-83-1 Chromium(III), Insoluble Salts 57.76 57.76 57.76 4.9E-04 4.9E-04
18540-29-9 Chromium(VI)0.636 0.636 0.636 2.1E-06 8.9E-10 2.1E-06 2.7E-03 1.0E-07 2.7E-03
110-82-7 Cyclohexane 0.0059 0.0059 0.0059 3.0E-07 3.0E-07
100-41-4 Ethylbenzene 0.0117 0.0117 0.0117 1.9E-10 1.7E-09 1.9E-09 1.5E-06 1.9E-06 3.4E-06
7439-92-1 ~Lead and Compounds 29 29 29 <SL**<SL**<SL**
7439-96-5 Manganese (Non-diet)746 746 746 4.0E-01 2.4E-04 4.0E-017487-94-7 ~Mercuric Chloride (and other Mercury salts)0.097 0.097 0.097 4.1E-03 5.2E-09 4.1E-03
79-20-9 Methyl Acetate 0.143 0.143 0.143 1.8E-06 1.8E-06
78-93-3 Methyl Ethyl Ketone (2-Butanone)0.0408 0.0408 0.0408 8.7E-07 6.0E-07 1.5E-06
117-81-7 ~Bis(2-ethylhexyl)phthalate 0.156 0.156 0.156 3.1E-09 8.8E-10 2.2E-15 4.0E-09 1.0E-04 2.4E-05 1.2E-04
56-55-3 ~Benz[a]anthracene 0.257 0.257 0.257 1.7E-07 5.6E-08 3.2E-09 2.3E-07
50-32-8 ~Benzo[a]pyrene 0.224 0.224 0.224 1.5E-06 4.9E-07 2.2E-12 2.0E-06 9.5E-03 2.9E-03 1.8E-06 1.2E-02
205-99-2 ~Benzo[b]fluoranthene 0.257 0.257 0.257 1.7E-07 5.6E-08 2.6E-13 2.2E-07
218-01-9 ~Chrysene 0.254 0.254 0.254 1.7E-09 5.5E-10 2.5E-15 2.2E-09
206-44-0 ~Fluoranthene 0.603 0.603 0.603 1.9E-04 5.9E-05 2.5E-04
129-00-0 ~Pyrene 0.452 0.452 0.452 1.9E-04 5.9E-05 2.5E-04
7782-49-2 Selenium 6.4 6.4 6.4 1.6E-02 5.2E-09 1.6E-02
7440-22-4 Silver 0.54 0.54 0.54 1.4E-03 1.4E-03
108-88-3 Toluene 0.0565 0.0565 0.0565 9.0E-06 2.4E-06 1.1E-05
1330-20-7 Xylenes 0.0171 0.0171 0.0171 1.1E-06 2.7E-05 2.8E-05
Cumulative: 8.9E-06 5.4E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening
level of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Non-Residential Worker Soil
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID:
Exposure Unit ID:
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient
Calculated Non-
Carcinogenic
Hazard
Quotient67-64-1 Acetone 0.116 0.116 0.116 1.1E-07 5.9E-08 1.7E-077440-38-2 Arsenic, Inorganic 3 3 3 8.3E-07 1.7E-07 1.8E-11 1.0E-06 5.1E-03 1.1E-03 7.7E-07 6.2E-03
7440-39-3 Barium 150 150 150 6.4E-04 1.2E-06 6.4E-04
74-83-9 Bromomethane 0.0331 0.0331 0.0331 2.0E-05 4.8E-04 5.0E-04
7440-43-9 Cadmium (Diet)0.13 0.13 0.13 3.2E-13 3.2E-13 1.1E-04 1.9E-05 5.0E-08 1.3E-0416065-83-1 Chromium(III), Insoluble Salts 57.76 57.76 57.76 3.3E-05 3.3E-05
18540-29-9 Chromium(VI)0.636 0.636 0.636 9.7E-08 7.3E-11 9.7E-08 1.8E-04 2.4E-08 1.8E-04
110-82-7 Cyclohexane 0.0059 0.0059 0.0059 7.1E-08 7.1E-08
100-41-4 Ethylbenzene 0.0117 0.0117 0.0117 3.9E-11 4.0E-10 4.3E-10 1.0E-07 4.4E-07 5.4E-07
7439-92-1 ~Lead and Compounds 29 29 29 <SL**<SL**<SL**
7439-96-5 Manganese (Non-diet)746 746 746 2.7E-02 5.7E-05 2.7E-02
7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.097 0.097 0.097 2.8E-04 1.2E-09 2.8E-04
79-20-9 Methyl Acetate 0.143 0.143 0.143 1.2E-07 1.2E-07
78-93-3 Methyl Ethyl Ketone (2-Butanone)0.0408 0.0408 0.0408 5.8E-08 1.4E-07 2.0E-07
117-81-7 ~Bis(2-ethylhexyl)phthalate 0.156 0.156 0.156 6.7E-10 2.8E-10 5.1E-16 9.5E-10 6.7E-06 2.8E-06 9.5E-06
56-55-3 ~Benz[a]anthracene 0.257 0.257 0.257 7.9E-09 4.3E-09 2.7E-10 1.2E-08
50-32-8 ~Benzo[a]pyrene 0.224 0.224 0.224 6.8E-08 3.8E-08 1.8E-13 1.1E-07 6.4E-04 3.5E-04 4.3E-07 9.9E-04
205-99-2 ~Benzo[b]fluoranthene 0.257 0.257 0.257 7.9E-09 4.3E-09 2.1E-14 1.2E-08
218-01-9 ~Chrysene 0.254 0.254 0.254 7.8E-11 4.3E-11 2.1E-16 1.2E-10
206-44-0 ~Fluoranthene 0.603 0.603 0.603 1.3E-05 7.1E-06 2.0E-05
129-00-0 ~Pyrene 0.452 0.452 0.452 1.3E-05 7.1E-06 2.0E-05
7782-49-2 Selenium 6.4 6.4 6.4 1.1E-03 1.2E-09 1.1E-037440-22-4 Silver 0.54 0.54 0.54 9.2E-05 9.2E-05108-88-3 Toluene 0.0565 0.0565 0.0565 6.0E-07 5.7E-07 1.2E-06
1330-20-7 Xylenes 0.0171 0.0171 0.0171 7.3E-08 6.4E-06 6.5E-06
Cumulative: 1.2E-06 3.7E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Construction Worker Soil
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID:
Exposure Unit ID:
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion Concentration
(mg/kg)
Dermal Concentration
(mg/kg)
Inhalation Concentration
(mg/kg)*
Ingestion Carcinogenic
Risk
Dermal Carcinogenic
Risk
Inhalation Carcinogenic
Risk
Calculated Carcinogenic
Risk
Ingestion Hazard
Quotient
Dermal Hazard
Quotient
Inhalation Hazard
Quotient
Calculated
Non-Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.116 0.116 0.116 1.7E-07 2.9E-07 4.6E-07
7440-38-2 Arsenic, Inorganic 3 3 3 1.1E-07 1.7E-08 4.0E-08 1.7E-07 1.8E-02 2.8E-03 4.5E-02 6.5E-027440-39-3 Barium 150 150 150 2.2E-03 6.7E-03 8.9E-03
74-83-9 Bromomethane 0.0331 0.0331 0.0331 2.0E-05 2.5E-04 2.7E-04
7440-43-9 Cadmium (Diet)0.13 0.13 0.13 7.2E-10 7.2E-10 7.7E-04 9.8E-05 2.9E-03 3.8E-03
16065-83-1 Chromium(III), Insoluble Salts 57.76 57.76 57.76 1.1E-04 2.6E-03 2.7E-03
18540-29-9 Chromium(VI)0.636 0.636 0.636 1.3E-08 1.6E-07 1.8E-07 3.7E-04 4.8E-04 8.5E-04
110-82-7 Cyclohexane 0.0059 0.0059 0.0059 3.3E-07 3.3E-07
100-41-4 Ethylbenzene 0.0117 0.0117 0.0117 5.2E-12 7.5E-11 8.0E-11 6.9E-07 2.4E-07 9.3E-07
7439-92-1 ~Lead and Compounds 29 29 29 <SL**<SL**<SL**7439-96-5 Manganese (Non-diet)746 746 746 9.2E-02 3.4E+00 3.4E+00
7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.097 0.097 0.097 1.4E-04 7.3E-05 2.2E-04
79-20-9 Methyl Acetate 0.143 0.143 0.143 4.2E-07 1.9E-04 1.9E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)0.0408 0.0408 0.0408 6.0E-08 3.6E-06 3.6E-06
117-81-7 ~Bis(2-ethylhexyl)phthalate 0.156 0.156 0.156 8.8E-11 2.8E-11 1.2E-12 1.2E-10 2.3E-05 7.4E-06 3.0E-05
56-55-3 ~Benz[a]anthracene 0.257 0.257 0.257 1.0E-09 4.3E-10 9.8E-11 1.6E-09
50-32-8 ~Benzo[a]pyrene 0.224 0.224 0.224 9.0E-09 3.8E-09 4.1E-10 1.3E-08 2.2E-03 9.2E-04 2.5E-02 2.8E-02
205-99-2 ~Benzo[b]fluoranthene 0.257 0.257 0.257 1.0E-09 4.3E-10 4.7E-11 1.5E-09
218-01-9 ~Chrysene 0.254 0.254 0.254 1.0E-11 4.3E-12 4.7E-13 1.5E-11206-44-0 ~Fluoranthene 0.603 0.603 0.603 1.8E-05 7.4E-06 2.5E-05
129-00-0 ~Pyrene 0.452 0.452 0.452 4.4E-06 1.9E-06 6.3E-06
7782-49-2 Selenium 6.4 6.4 6.4 3.8E-03 7.2E-05 3.8E-03
7440-22-4 Silver 0.54 0.54 0.54 3.2E-04 3.2E-04108-88-3 Toluene 0.0565 0.0565 0.0565 2.1E-07 2.8E-06 3.0E-06
1330-20-7 Xylenes 0.0171 0.0171 0.0171 1.3E-07 7.9E-06 8.0E-06
Cumulative: 3.6E-07 3.6E+00
Output Form 2E
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator