22030_Durafiber Brownfields Assessment Report_20200722

Via Email

July 22, 2020

NCDEQ – Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attn: Mr. Bill Schmithorst, PG

Re: Brownfields Assessment Report
Salisbury Investments
7401 Statesville Boulevard
Salisbury, North Carolina
Brownfields Project No. 22030-18-080
H&H Project No. FDP-058

Dear Mr. Schmithorst:

On behalf of Salisbury Investments I, LLC, enclosed please find a copy of the Brownfields
Assessment Report prepared for the Salisbury Investments Brownfields property located in
Salisbury, Rowan County.

Should you have questions or need additional information, please do not hesitate to contact us at
[phone].

Sincerely,
Hart & Hickman, PC
Haley Martin, PG Ralph McGee, PG
Assistant Project Geologist Project Manager

Enclosure:

cc: Ms. MariJon Owens, Forsite Development (Via Email)
Mr. Steve Hart, PG, H&H (Via Email)
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Brownfields Assessment Report
Salisbury Investments
7401 Statesville Boulevard
Salisbury, North Carolina
Brownfields Project No. 22030-18-080
H&H Job No. FDP-058

Table of Contents

1.0 Introduction .............................................................................................................................1 
1.1 Background Information .......................................................................................................2 
1.2 Previous Assessment Activities .............................................................................................2 
2.0 Brownfields Assessment Activities ........................................................................................7 
3.0 Soil Assessment Activities .......................................................................................................9 
3.1 Soil Sampling Methodologies ...............................................................................................9 
3.2 Soil Sampling Analytical Results ........................................................................................11 
4.0 Groundwater Assessment Activities ....................................................................................13 
4.1 Groundwater Sampling Activities .......................................................................................13 
4.2 Groundwater Sample Analytical Results .............................................................................14 
5.0 Surface Water Assessment Activities ..................................................................................18 
5.1 Surface Water Sampling Activities .....................................................................................18 
5.2 Surface Water Analytical Results ........................................................................................19 
6.0 Sub-Slab Soil Vapor Assessment Activities ........................................................................20 
6.1 Sub-Slab Soil Vapor Sampling Activities ...........................................................................20 
6.2 Sub-Slab Soil Vapor Sample Analytical Results .................................................................22 
6.3 Vapor Intrusion Evaluation .................................................................................................22 
7.0 Quality Assurance – Quality Control ..................................................................................24 
7.1 Trip Blank ............................................................................................................................24 
7.2 Laboratory Duplicates .........................................................................................................24 
8.0 Summary and Conclusions ..................................................................................................26 

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List of Tables

Table 1 Summary of Soil Analytical Data
Table 2 Well Construction and Groundwater Elevation Data
Table 3 Summary of Groundwater Analytical Data
Table 4 Summary of Surface Water Analytical Data
Table 5 Summary of Sub-Slab Soil Vapor Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Detailed Site Map
Figure 4 Sample Location Map
Figure 5 Shallow Groundwater Hydraulic Gradient Map

List of Appendices

Appendix A Boring Logs
Appendix B Laboratory Analytical Reports
Appendix C Groundwater & Surface Water Sampling Forms
Appendix D DEQ Risk Calculators

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Brownfields Assessment Report
Salisbury Investments
7401 Statesville Boulevard
Salisbury, North Carolina
Brownfields Project No. 22030-18-080
H&H Job No. FDP-058

1.0 Introduction

On behalf of Salisbury Investments I, LLC (Prospective Developer or PD), Hart & Hickman, PC
(H&H) has prepared this report to document assessment activities recently completed at the
Salisbury Investments Brownfields property (Brownfields Project No. 22030-18-080) located at
7401 Statesville Boulevard in Salisbury, Rowan County, North Carolina (Site). The Site consists
of five parcels totaling approximately 538 acres of land located approximately six miles west of
downtown Salisbury. A Site location map is provided as Figure 1, and the Site and surrounding
area are shown in Figure 2.

The Site is improved with an approximate two million square foot (sq ft) industrial
manufacturing facility. The industrial manufacturing facility encompasses approximately 170
acres of land in the central portion of the Site and includes administrative offices, warehouse
areas, production areas, shipping and receiving areas, chemical storage areas, a training building,
a maintenance building, and a wastewater treatment plant. Other Site improvements include
concrete-paved parking areas, paved and gravel covered access roads, loading areas, railroad
spurs, landscaped areas, and a former recreational clubhouse building with a pond. Remaining
portions of the Site consist of undeveloped wooded land. A detailed Site map is provided as
Figure 3.

Proposed redevelopment of the Brownfields property includes adaptive reuse of the existing
warehouses and training buildings within the industrial manufacturing facility for commercial
and industrial purposes. In addition, the wastewater treatment plant will continue operations and
may be used to treat third-party wastewater.
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1.1 Background Information

The Site was comprised of undeveloped vacant land from at least the late 1940s until grading and
construction of the industrial facility began in the mid-1960s. Manufacturing operations began
on the Site by 1966. The facility was historically utilized for manufacturing polymer filament
fibers and polymer chips. The polymer materials were made by combining terephthalic acid and
ethylene glycol into a molten mixture and processing the mixture into filament fibers or chips as
the material cooled. Plant operations have historically included manufacturing process units, raw
materials and finished products shipping units, a wastewater treatment plant, chemical recovery
units, a construction debris landfill, and chemical recovery waste landfills.

Polymer manufacturing operations were originally conducted at the Site by Celanese under the
name Fibers Industries, Inc. In the late 1980s, Celanese was purchased by Hoechst and the name
of the facility was changed to Hoechst-Celanese. Site manufacturing operations continued as
Hoechst-Celanese until the late 1990s or early 2000s when it became KoSa. The Site was
purchased by Invista (a subsidiary of Dupont) and operations continued as Invista S.A.R.L (a
subsidiary of Koch Industries) until the early 2010s when Performance Fibers, Inc. operations
began. In 2016, Performance Fibers changed its name to Durafiber Technologies. Durafiber
Technologies operations continued at the Site until September 2017.

The Site buildings are vacant and have been unoccupied since Durafiber Technologies vacated
the Site in 2017. A portion of the Site is leased for exterior storage of tractor trailers. The
wastewater treatment facility remains in operation with limited staff.

1.2 Previous Assessment Activities

RCRA Assessment and Remediation
Extensive assessment, remediation, and monitoring activities have been conducted at the Site
since the early 1980s. A brief summary of the historical assessment and remedial activities is
provided below.
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In the late 1960s, a glycol recovery unit bottoms landfill (GRUB landfill) opened east of the
manufacturing facility and received waste extracted from glycol recovery operations until the
mid-1970s. In addition, chromate reduction unit (CRU) basins opened east of the facility as part
of the water-cooling system in the early to mid-1970s. The CRU basins received waste until the
mid-1980s. Waste materials disposed in both the GRUB landfill and CRU basins were removed
and transported off-Site and the waste areas were permanently closed in the mid-1980s. The
GRUB landfill was subsequently designated as a solid waste management unit (SWMU) during a
facility investigation in the early 1990s. In 1993, the U.S. Environmental Protection Agency
(EPA) agreed that removal of impacted subsurface soil in the CRU area was not practical and
that groundwater extraction was adequate to remediate impacts in the CRU.

In the early 1990s, during a Resource Conservation and Recovery Act Facility Investigation
(RCRA RFI), the Dowtherm heat transfer area, the heat transfer fluid storage area, and the
wastewater polishing ponds were identified as additional SWMUs. The Dowtherm (a mixture of
1,1-biphenyl and biphenyl ether) heater system was utilized for the production of polyester resins
and fibers used in the manufacturing process. Releases associated with storage, operations, and
maintenance resulted in the SWMU designation for the Dowtherm heat transfer system area.
The polishing ponds received effluent from the plant wastewater treatment system and were
estimated to contain approximately 85,000 cubic yards of sludge material that was identified as a
potential source of groundwater impacts identified east of the manufacturing facility. In 1994
and 1995, sludge was removed from two of the wastewater polishing ponds and was disposed of
off-Site. Subsequently, a sludge dewatering system was installed to minimize the entry of sludge
into the polishing ponds, although Durafiber may not have used the sludge dewatering system
after it took over operations at the Site.

On April 6, 1990, Hoechst Celanese Corporation entered into a RCRA 3008(h) Administrative
Order on Consent (AOC) with the EPA to complete assessment and remedial activities for
protection of human health and the environment from impacts associated with historical
manufacturing operations at the Site. On October 4, 2000, CNA Holdings, LLC (formerly
Hoechst Celanese Corporation) entered into a Final AOC with the EPA.
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Hoechst Celanese Corporation completed voluntary groundwater assessment activities at the Site
to evaluate the potential for impacts associated with manufacturing operations as early as 1981.
Based on assessment results, several organic and inorganic compounds were identified in Site
groundwater. The GRUB landfill area, the CRU basins, the Dowtherm heat transfer area, and the
wastewater polishing ponds were identified as the primary sources for impacts identified in
groundwater. Free product Dowtherm was also identified in the subsurface in the Dowtherm
SWMU area. By the late 1980s and early 1990s, groundwater extraction systems were installed
in and around these source areas as well as along the eastern Site boundary to control migration
of impacted groundwater.

As part of the assessment activities in the early to mid-1990s, Hoechst Celanese sampled water
supply wells north and east of the facility on a voluntary basis. Subsequent to the sampling and
analysis of these wells, Hoechst Celanese determined that City of Salisbury water would be
provided to residents east of Second Creek near the Spring Hills subdivision and at specific
locations along Highway 70 north of the plant. Private wells in the Spring Hills subdivision and
ten private wells along Highway 70 were subsequently abandoned and restrictions against the
drilling of new wells in the area have been implemented.

Historically, 1,4-dioxane has been detected above the North Carolina Department of
Environmental Quality (DEQ) 2B Surface Water Standard (2B Standard) in Second Creek
located along the eastern Site boundary. Concentrations of 1,4-dioxane decreased to levels
below the 2B Standard for a period of time in the 2000s, but increased to levels above the 2B
Standard in the 2010s. The increases in 1,4-dioxane concentrations in the Second Creek were
attributed to Durafiber processes discharging to the wastewater treatment plant polishing ponds
because an increase in concentrations was also observed in the pond effluent during this
timeframe.

The GRUB landfill, CRU basin, and eastern Site boundary groundwater extraction systems
operated until 2004. In 2011, groundwater extraction activities in the Dowtherm SWMU area
were discontinued. Annual groundwater monitoring for natural attenuation and plume stability is
the currently approved action for addressing impacts in Site groundwater. Constituents
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monitored in groundwater include chlorobenzene, 1,2-dichlorobenzene, 1,4-dichlorobenzene,
1,1-biphenyl, biphenyl ether, ethylene glycol, and 1,4-dioxane.

May 2018 Phase I ESA
H&H completed Phase I Environmental Site Assessment (ESA) activities at the Site in May
2018. Results of the Phase I ESA identified residual soil, groundwater, and surface water
impacts associated with historical industrial and manufacturing operations to be environmental
concerns in connection with the Site.

2019 Annual Groundwater Monitoring Report
In September 2019, annual groundwater monitoring activities were completed at the Site by
AECOM on behalf of CNA Holdings. The September 2019 groundwater monitoring data
indicates that target constituents of concern are present at concentrations exceeding the DEQ 2L
Groundwater Standards (2L Standards) in Site groundwater and above the DEQ 2B Standards in
samples collected from Second Creek. During the September 2019 sampling event, no
compounds were detected in groundwater above the Site-specific “trigger levels”, except for
chlorobenzene in well S-58 only (see well location in Figure 4). However, chlorobenzene
concentrations in well S-58 appear to be decreasing or stable since 2011.

The “trigger levels” were determined based on the maximum detected concentrations of
constituents in groundwater during a Risk Assessment performed in 1998. The trigger levels
were established as part of the request to terminate active remedial actions and are levels that, if
exceeded, could trigger additional active remedial actions. The trigger levels have periodically
been exceeded, but not for an extended period of time (except well S-58) and no additional
active remediation has been performed since shut down of the groundwater extraction systems.
The recent groundwater and surface water sampling activities are documented in the 2019
Annual Groundwater Monitoring Report prepared by AECOM dated February 14, 2020.

Brownfields
The PD obtained the Site through Durafiber bankruptcy proceedings in April 2018. To address
environmental concerns associated with historical Site use, the PD elected to enter the Site into
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the DEQ Brownfields Program and received eligibility in a letter dated September 24, 2018. A
meeting was held at the Site with DEQ Brownfields personnel in December 2018. In an email
dated April 6, 2020, the DEQ Brownfields Program requested additional assessment to evaluate
environmental conditions at the Site. Based on subsequent correspondence, DEQ Brownfields
provided concurrence on the additional assessment in an email dated May 1, 2020. To address
DEQ Brownfields requests for additional assessment, H&H prepared a Brownfields Assessment
Work Plan (Work Plan) for DEQ review and approval. The Work Plan received DEQ approval
in an email dated May 27, 2020.

Brownfields assessment activities described herein were completed to further evaluate potential
risks associated with future use of the Site and included sampling and analysis of soil,
groundwater, surface water, and sub-slab soil vapor. A summary of methods and results of the
Brownfields assessment activities conducted in accordance with the Work Plan is provided in the
following sections.
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2.0 Brownfields Assessment Activities

H&H conducted the Brownfields assessment activities in June 2020, As part of the assessment
activities, soil samples were collected in the area of the fuel oil storage secondary containment
system, cooling tower, and Dowtherm heating units. Groundwater samples were collected from
eight (8) existing groundwater monitoring wells located downgradient of the manufacturing
facility and in the vicinity of the polishing ponds located in the southeastern portion of the Site.
To address the potential for structural vapor intrusion into existing Site buildings, H&H
completed sub-slab soil vapor sampling in the filament and staple warehouses, maintenance
shop, and training building.

Prior to conducting field activities, H&H contacted North Carolina 811, the public utility locator,
to mark subsurface utilities at the Site. H&H also contracted with a private utility locator to
mark utilities which were not identified by the public locator. The private utility locator also
utilized ground penetrating radar (GPR) survey techniques to identify and mark utilities. In
addition, H&H directed the drilling contractor to hand clear each boring to a depth of
approximately 5 feet below ground surface (ft bgs) to further screen the boring locations for the
presence of subsurface utilities.

The assessment activities were performed in general accordance with the DEQ Inactive
Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup of Contaminated Sites
(Guidelines) dated January 2020, the DEQ Division of Waste Management (DWM) Vapor
Intrusion Guidance (VI Guidance) dated March 2018, most recent versions of the U.S.
Environmental Protection Agency (EPA) Region IV Science and Ecosystem Support Division
(SESD) Field Branches Quality System and Technical Procedures guidance, and the DEQ-
approved Work Plan.
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Details of the soil assessment activities are provided in Section 3.0; groundwater assessment
activities are summarized in Section 4.0; the surface water assessment activities are described in
Section 5.0; a summary of the sub-slab soil vapor assessment activities are provided in Section
6.0; quality assurance and quality control measures are detailed in Section 7.0; and summary and
conclusions based on results of the assessment activities are provided in Section 8.0.
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3.0 Soil Assessment Activities

On June 9, 2020, H&H contracted with Mid-South Environmental (Mid-South) to advance soil
borings at the Site in the area near the Dowtherm heating units, fuel oil storage secondary
containment system, and cooling tower. In addition, two (2) background soil samples were
collected for laboratory analysis to establish Site-specific background concentrations for
naturally occurring metals. Soil sample locations are depicted on Figure 4.

Soil borings were advanced at the Site using decontaminated stainless steel hand augers or a
track-mounted drill rig capable in utilizing direct push technology (DPT) drilling techniques.
Continuous soil samples were collected from the center of the hand auger bucket or from acetate
lined macrocore DPT sleeves at each boring. Soil samples were logged for lithologic
description, observed for obvious evidence of staining and unusual odors, and field screened for
the presence of volatile organic vapors using a calibrated photoionization detector (PID). Boring
logs including lithologic descriptions and field screening results for each soil boring are provided
in Appendix A.

Details of the soil sampling activities and results are provided in the following sections.

3.1 Soil Sampling Methodologies

Dowtherm Heating Units
Three (3) soil borings (SB-1 through SB-3) were advanced to approximately 15 ft bgs in the
vicinity of previous soil borings DTHA-4, DTHA-5, and DTHA-8 advanced by others in the
mid-1980s adjacent to the Dowtherm systems (Figure 4). Field screening results did not identify
obvious evidence of impact in soil borings SB-1 and SB-2. As such, H&H collected a sample
from both of the borings from a similar depth interval (6 ft to 8 ft) as soil samples collected in the
mid-1980s. During boring advancement of SB-3, field screening results indicated PID readings
up to 212 parts per million (ppm). Based on field screening results, H&H collected a grab soil
sample for laboratory analysis from the 2 ft to 4 ft depth interval where the highest PID reading
was measured.
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Fuel Oil Storage
Two (2) soil borings (SB-4 and SB-5) were advanced to a depth of approximately 10 ft bgs
adjacent to each side of the aboveground storage tank (AST) secondary containment basin
located in the southeastern portion of the manufacturing facility (Figure 4). Prior to boring
advancement, depth to the base of the AST secondary containment system was measured at 4 ft
bgs. During boring advancement, soil samples were field screened in two-foot intervals from
each boring. Field screening results did not identify field evidence of impact in the soil samples.
As such, soil samples for laboratory analysis were collected from the depth interval (6 ft to 8 ft)
interpreted to be below the base of the AST secondary containment system.

Cooling Tower
Two (2) soil borings (SB-6 and SB-7) were advanced on the eastern and downgradient side of
the cooling tower located in the southeastern portion of the manufacturing facility (Figure 4).
Soil borings were advanced to approximately 3 ft bgs. Field screening results did not identify
field evidence of impact in the soil samples. As such, a soil sample was collected for laboratory
analysis from the 2 ft to 3 ft depth interval.

Laboratory Analysis
Soil samples selected for laboratory analysis in each evaluation area were collected directly into
laboratory supplied glassware, labeled with the sample identification, date, time, and requested
analysis and placed in a laboratory supplied cooler with ice. The soil samples were delivered to
Pace Analytical (Pace) under standard chain of custody protocols. Soil samples SB-1 through
SB-5 were submitted for analysis of volatile organic compounds (VOCs) by EPA Method 8260,
semi-volatile organic compounds (SVOCs) by EPA Method 8270, and Resource Conservation
and Recovery Act (RCRA) metals plus hexavalent chromium by EPA Methods 6020/7471/7199.
The cooling tower soil samples (SB-6 and SB-7) were submitted for analysis of total chromium
by EPA Method 6020 and hexavalent chromium by EPA Method 7199.

Background Samples
In addition to the soil samples described above, H&H also collected two (2) shallow background
soil samples to evaluate Site-specific background concentrations for naturally occurring metals.
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Soil sample locations (denoted by BG nomenclature) are depicted on Figure 4. Background soil
sample BG-1 was collected from 2-3 ft bgs in the western portion of the Site, and background
soil sample BG-2 was collected from 2-3 ft bgs in the southern portion of the Site. Background
soil samples were submitted for laboratory analysis of RCRA metals plus hexavalent chromium
by EPA Methods 6020/7471/7199.

Quality Assurance/Quality Control (QA/QC)
For QA/QC purposes, a duplicate soil sample (labeled SB-DUP) was submitted to the laboratory
from the SB-3 sample location.

Following sampling activities, the soil borings were properly abandoned and the surfaces were
repaired similar to pre-drilling conditions. Additionally, the soil sample locations were estimated
using a hand-held global positioning system (GPS) unit.

3.2 Soil Sampling Analytical Results

A tabular summary of the soil sample analytical results is presented in Table 1 and the laboratory
analytical reports and chain of custody records are provided in Appendix B. The laboratory
analytical results were compared to the most recent version of the DEQ IHSB
Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) dated December 2019. In
addition to the PSRGs, metals results were compared to published concentrations for naturally
occurring metals in North Carolina soil as well as Site-specific background levels in soil samples
BG-1 and BG-2.

VOCs
Low levels of several compounds including n-butylbenzene (0.0498 milligrams per kilogram
[mg/kg]), sec-butylbenzene (0.0395 mg/kg), 2-chlorotoluene (0.278 mg/kg), p-isopropyltoluene
(0.0608 mg/kg), naphthalene (up to 0.014 mg/kg), 1,2,4-trimethylbenzene (up to 0.105 mg/kg),
and 1,3,5-trimehtylbenzene (up to 0.0783 mg/kg) were detected at concentrations above the
laboratory method detection limits, but well below the Industrial/Commercial PSRGs in soil
sample SB-3 and its duplicate soil sample (SB-DUP) collected in the southern portion of the
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Dowtherm heat transfer area (Figure 4). In addition, low levels of tetrachloroethene (PCE;
0.0640 mg/kg), trichloroethene (TCE; 0.0741 mg/kg), vinyl chloride (0.0029 J mg/kg), 2-
chlorotoluene (0.0206 mg/kg), and cis-1,2-dichloroethene (0.0158 mg/kg) were detected at
concentrations above the laboratory method detection limits, but well below the IHSB
Industrial/Commercial PSRGs in soil sample SB-5 collected adjacent and downgradient of the
fuel oil storage tanks. Note that the J-flag designation (J) indicates the compound was detected
at a concentration above the laboratory method detection limit, but below the laboratory
reporting limit resulting in the laboratory estimating the concentration. No other VOCs were
detected at concentrations above the laboratory method detection limits, and no VOCs were
detected at concentrations above the DEQ IHSB Industrial/Commercial PSRGs in soil samples
collected at the Site.

SVOCs
A low level of phenol (0.163 J mg/kg) was detected at a concentration above the laboratory
method detection limit, but well below the IHSB Industrial/Commercial PSRG in the SB-3
duplicate soil sample collected near the Dowtherm heat transfer area. No other SVOCs were
detected at concentrations above the laboratory detection limits in the remaining soil samples
collected at the Site.

Metals
As expected, due to the natural presence of metals in soil, several metals were detected above
laboratory method detection limits in each soil sample collected at the Site. The detected metals
concentrations are within established concentrations for naturally occurring metals in North
Carolina soil (Dragun & Chekiri 2005), consistent with Site-specific ranges, and/or below IHSB
Industrial/Commercial PSRGs. Total chromium was detected in cooling tower sample SB-6 at a
concentration above Site-specific background, but speciation of the chromium did not indicate
hexavalent chromium above the DEQ IHSB Industrial/Commercial PSRG.
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4.0 Groundwater Assessment Activities

On June 10, 2020, H&H collected groundwater samples from eight (8) existing groundwater
monitoring wells located downgradient of the manufacturing facility and in the vicinity of the
polishing ponds located in the southeastern portion of the Site. Locations of the sampled existing
monitoring wells are depicted on Figure 4, and are described further below:
 topographically downgradient of the polishing ponds (R-30, TT-34, and YY-37);
 topographically downgradient of the manufacturing facility (GG-43 and DD-40);
 topographically downgradient of the former GRUB landfill (Z-90); and
 topographically downgradient of the water treatment facility (SS-58 and RR-102).
Details of the groundwater sampling activities and results are provided in the following sections.

4.1 Groundwater Sampling Activities

Prior to sampling, H&H located each groundwater monitoring well planned for sampling. Each
monitoring well is constructed with an above ground well housing with the exception of YY-37
which is completed in a flush-mount man hole. Upon locating the wells, H&H removed the
expandable well caps and observed a dedicated submersible pump within each monitor well with
the exception of well YY-37. With the exception of the historically impacted monitoring wells
S-58 and Z-90, and the deeper well RR-102, the submersible pumps were removed from each
well and placed within dedicated plastic bags. Each well was then allowed to equilibrate to static
conditions.

Following stabilization of groundwater levels, a decontaminated electronic water level indicator
was used to measure the depth to the water table relative to the tops of well casings and the
ground surface at each of the eight wells to be sampled. Depth to groundwater ranged from
approximately 7.5 ft bgs downgradient of the polishing ponds at monitor well TT-34 to
approximately 30.5 ft bgs downgradient of the manufacturing facility at monitor well GG-43.
Based on depth to water table measurements, groundwater flow direction was estimated to be
toward the southeast. A shallow groundwater hydraulic gradient map is provided as Figure 5,
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and well construction and groundwater elevation information is provided in Table 2.

Groundwater samples were collected utilizing low flow/low stress purging and sampling
techniques using a peristaltic pump and dedicated polyethylene tubing. The intake point of the
pump tubing was placed in the approximate mid-portion of the screened interval of each well,
and groundwater was removed at a rate no greater than 200 milliliters per minute. H&H utilized
calibrated water quality meters to collect measurements of pH, temperature, dissolved oxygen,
oxidation reduction potential, turbidity, and specific conductivity at three to five-minute intervals
during the purging process. Purging was considered complete when field parameters stabilized
(pH ± 0.1 Standard Units, conductivity varied no more than 5%, and turbidity was near or less
than 10 Nephelometric Turbidity Units [NTUs]). Groundwater sampling forms completed by
sampling personnel are provided in Appendix C.

Once groundwater parameters stabilized, groundwater samples for VOC analysis were collected
directly into laboratory supplied sample containers using the “soda straw” method to minimize
volatile loss through the peristaltic pump head. Groundwater samples submitted for remaining
analyses were collected directly into laboratory supplied glassware directly from the sample
tubing discharge. The sample containers were labeled with the sample identification, date, time,
and requested analysis, and placed in a laboratory supplied cooler with ice. The samples were
delivered to Pace under standard chain of custody protocols for analysis of VOCs by EPA
Method 8260, SVOCs by EPA Method 8270, RCRA metals by EPA Method 6020/7471, and
hexavalent chromium by EPA Method 7199. For QA/QC purposes, a dedicated groundwater
sample (labeled GW-DUP) was collected from well S-58.

Following collection of groundwater samples, dedicated submersible wells were placed back
within the monitor wells and the wells were secured.

4.2 Groundwater Sample Analytical Results

A tabular summary of the groundwater sample laboratory analytical results is presented in
Table 3. Copies of the laboratory analytical report and chain of custody records are provided in
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Appendix B. Groundwater data were compared to the DEQ 15A NCAC 02L .0202 Groundwater
Standards (2L Standards) dated April 2013 and the DEQ DWM Non-Residential Vapor Intrusion
Groundwater Screening Levels (GWSLs) dated February 2018. Summary of the groundwater
assessment results is provided below.

VOCs
Laboratory analytical results indicate that several compounds including benzene (up to 61.2
micrograms per liter [µg/L]), chlorobenzene (12,500 µg/L), and 1,4-dichlorobenzene (up to 140
µg/L) were detected at concentrations above the DEQ 2L Standards in the S-58 groundwater
sample and its duplicate sample collected downgradient of the wastewater treatment plant. The
chlorobenzene concentration also exceeds the DEQ DWM Non-Residential Vapor Intrusion
GWSL. No compounds were detected at concentrations above the 2L Standards or the GWSLs
in groundwater samples collected from monitor wells GG-43 and DD-40 located downgradient
to the manufacturing areas and upgradient of the waste water treatment plant area, or in the
RR-102 groundwater sample collected downgradient of the wastewater treatment plant aeration
and clarifier units.

Groundwater sample laboratory analytical results also identified 2-butanone (239 J µg/L),
chlorobenzene (1,500 µg/L), 1,2-dichlorobenzene (18.2 J µg/L), and cis-1,2-dichloroethene (27.3
J µg/L) at concentrations above the laboratory method detection limits in monitoring well Z-90
located downgradient of the former GRUB landfill. The chlorobenzene concentration detected
in the Z-90 sample exceeds the 2L Standard and DEQ DWM Non-Residential GWSL. No other
compounds were detected at concentrations above the 2L Standards or DEQ DWM Non-
Residential Vapor Intrusion GWSLs in the groundwater sample collected downgradient of the
former GRUB landfill.

As noted above, three groundwater samples (TT-34, YY-37, and R-30) were collected east and
downgradient of the polishing ponds located in the eastern portion of the Site. Groundwater
sample laboratory analytical results indicate that chlorobenzene (53.4 µg/L) and
1,2-dichlorobenzene (248 µg/L) were detected at concentrations above the 2L Standards, but
below the DEQ DWM Non-Residential GWSLs in groundwater sample YY-37. No other
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compounds were detected at concentrations above the 2L Standards or DEQ DWM Non-
Residential Vapor Intrusion GWSLs in the groundwater samples collected downgradient of the
polishing ponds.

SVOCs
Several SVOCs were detected at concentrations above the laboratory method detection limits in
the groundwater sample collected downgradient of the wastewater treatment plant (S-58), the
waste disposal area (Z-90), and one well (YY-37) located downgradient of the polishing ponds.
Laboratory analytical results indicate that 1,4-dichlorobenzene (120 µg/L) was detected in the
S-58 groundwater sample at a concentration above the 2L Standard of 6 µg/L and slightly above
the DEQ DWM Non-Residential GWSL of 110 µg/L. In addition, bis(2-ethylhexyl)phthalate
(up to 4.6 J µg/L) was detected in S-58 and its duplicate groundwater sample GW-DUP at
concentrations slightly above the DEQ 2L Standards of 6 µg/L and 3 µg/L, respectively. There
is no established DEQ DWM Vapor Intrusion GWSL for bis(2-ethylhexyl) phthalate. No other
SVOCs were detected at concentrations above the 2L Standard or DEQ DWM Non-Residential
Vapor Intrusion GWSLs in samples collected downgradient of the wastewater treatment plant.

Phenol (2,730 µg/L) was detected at a concentration above the DEQ 2L Standard of 30 µg/L in
the Z-90 groundwater sample collected downgradient of the former GRUB landfill. There is no
established DEQ DWM Vapor Intrusion GWSL for phenol. No other SVOCs were detected at
concentrations above the 2L Standard or DEQ DWM Non-Residential Vapor Intrusion GWSLs
in the Z-90 groundwater sample.

Laboratory analytical results indicate that 1,2-dichlorobenzene (185 µg/L) was detected as a
SVOC at a concentration above the DEQ 2L Standard of 20 µg/L, but well below the DEQ
DWM Non-Residential GWSL of 2,200 µg/L in the YY-37 groundwater sample collected
downgradient of the polishing ponds. No other SVOCs were detected at concentrations above
the DEQ 2L Standards or the DEQ DWM Non-Residential Vapor Intrusion GWSLs in
groundwater samples collected downgradient of the polishing ponds.
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Metals
Several metals were detected at concentrations above the laboratory method detection limits in
the groundwater samples collected at the Site. Total chromium was detected at concentrations
above the DEQ 2L Standard of 10 µg/L in the Z-90 (13.6 µg/L), DD-40 (10.6 µg/L), GG-43 (190
µg/L), and RR-102 (69.4 µg/L) groundwater samples. Speciation of the chromium did not
indicate hexavalent chromium above the DEQ 2L Standard of 10 µg/L in groundwater samples
collected at the Site.

Barium (3,020 µg/L) and cadmium (9.66 µg/L) were also detected in the Z-90 groundwater
sample at concentrations above the DEQ 2L Standards of 700 µg/L and 2 µg/L, respectively.
Low levels of several other metals including arsenic (up to 2.98 J µg/L), lead (up to 4.80 J µg/L),
and selenium (up to 1.83 J µg/L) were detected at concentrations above the laboratory method
detection limits, but below the 2L Standards in remaining groundwater samples collected at the
Site.
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5.0 Surface Water Assessment Activities

On June 9, 2020, H&H collected two (2) surface water samples from Second Creek. H&H
collected one upgradient surface water sample (SW-1) near the southeastern property boundary
and one downgradient surface water sample (SW-4) near the northeastern property boundary
(Figure 4). Due to inundated low lying areas in the northeastern portion of the Site, surface
water sampling location SW-4 was adjusted slightly upgradient from the location proposed in the
Work Plan.

Details of the surface water sampling activities and results are provided in the following sections. 

5.1 Surface Water Sampling Activities

Surface water samples were collected in order from downstream to upstream and were collected
utilizing a peristaltic pump and dedicated polyethylene tubing. The intake point of the sample
tubing was placed in the approximate center of Second Creek at each sample location. H&H
utilized water quality meters to collect measurements of pH, temperature, dissolved oxygen,
oxidation reduction potential, turbidity, and specific conductivity during the sampling process.
Surface water sampling forms completed by sampling personnel are provided in Appendix C.

Similar to the groundwater samples, surface water samples for VOC analysis were collected
directly into laboratory supplied sample containers using the “soda straw” method to minimize
volatile loss through the peristaltic pump head. Surface water samples submitted for remaining
analyses were collected directly into laboratory supplied glassware directly from the sample
tubing discharge. The sample containers were labeled with the sample identification, date, time,
and requested analysis and place in a laboratory supplied cooler with ice. The samples were
delivered to Pace under standard chain of custody protocols for analysis of VOCs by EPA
Method 8260, SVOCs by EPA Method 8270, RCRA metals plus hexavalent chromium by EPA
Method 6020/7470/7199, and total hardness by EPA Method 2340. The samples were analyzed
for total hardness to allow calculation of hardness dependent surface water standards. For
QA/QC purposes, a duplicate surface water sample (labeled SW-DUP) was collected at sample
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location SW-4.

5.2 Surface Water Analytical Results

A tabular summary of the surface water sample laboratory analytical results is presented in
Table 4. Copies of the laboratory analytical report and chain of custody records are provided in
Appendix B. Groundwater data were compared to the DEQ 15A NCAC 02B .0211 Surface
Water Quality Standards (2B Standards) dated June 2019 for a Class C surface water body.
Hardness-dependent 2B Standards were calculated using the background sample hardness value
of 43 mg/L at sample SW-1. A summary of the surface water assessment results is provided
below.

No organic compounds were detected at concentrations above laboratory method detection limits
in the surface water samples collected at the Site.

Low levels of several metals including barium (up to 52.9 µg/L), hexavalent chromium (up to
0.115 µg/L), and trivalent chromium (up to 2.09 µg/L) were detected at concentrations above the
laboratory method detection limits, but below the DEQ 2B Standards in surface water samples
collected at the Site. No other compounds were detected at concentrations above the laboratory
method detection limits in the surface water samples collected at the Site.
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6.0 Sub-Slab Soil Vapor Assessment Activities

In June 2020, H&H completed sub-slab soil vapor assessment activities at the Site to evaluate the
potential for structural vapor intrusion. As part of the soil gas assessment activities, eleven (11)
temporary sub-slab soil vapor points (SS-1 through SS-11) were installed within the filament and
staple warehouses, maintenance shop, and training building of the manufacturing facility. Three
sample points (SS-1 through SS-3) were installed in the eastern portion of the filament
warehouse, four sample points (SS-4 through SS-7) were installed in the eastern portion of the
staple warehouse, two samples (SS-8 and SS-9) were installed in the maintenance building
located in the northeastern portion of the manufacturing facility, and two samples (SS-10 and
SS-11) were installed in the training building located in southern portion of the manufacturing
facility. Locations of the sub-slab soil vapor samples are depicted on Figure 4. For QA/QC
purposes, a duplicate sample (labeled SS-DUP) was collected at SS-3.

Details of the assessment activities and results are provided in the following sections.

6.1 Sub-Slab Soil Vapor Sampling Activities

The temporary sampling points were installed using a rotary hammer drill and 1½-inch diameter
drill bit to advance a pilot hole into the concrete slab to a depth of approximately 1¾ inches
below the slab surface. A drill guide was then placed within the pilot hole, and a 5/8-inch
diameter drill bit was utilized to advance a boring through the concrete slab to approximately 6
inches into the underlying soil/gravel beneath the slab. Loose concrete cuttings were removed
from each boring, and a Cox-Colvin Vapor Pin™ (vapor pin) assembly (brass sampling point
and silicone sleeve) was seated in the borehole using an installation/extraction tool and dead
blow hammer.

Following vapor pin installation, Teflon sample tubing was connected to the barbed end of the
vapor pin. A laboratory supplied batch certified 1-liter stainless steel Summa sample canister
was connected to an in-line flow controller with a vacuum gauge and the flow controller was
connected to the sample tubing using a brass nut and ferrule assembly to form an air-tight seal.
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The flow regulator was pre-set by the laboratory to regulate the vapor intake rate to
approximately 100 milliliters per minute.

Prior to collection of the sub-slab soil vapor samples, a leak check was conducted by
constructing a shroud around the sample train at each sampling point and flooding the air within
the shroud with helium gas. Helium concentrations inside the shroud were measured using a
calibrated helium gas detector and maintained at concentrations of approximately 20% for the
duration of the leak check. Using a syringe and three-way valve, the Teflon sample tubing was
purged and a sample was collected from the sample tubing outside the shroud into a Tedlar bag
and analyzed using the helium gas detector to ensure that helium concentrations were less than
10% of the helium concentrations measure within the shroud. Each sub-slab sampling point
passed the helium leak check criteria.

Following a successful leak check, the intake valve on the Summa canister was fully opened to
begin collection of the sub-slab soil vapor sample. Vacuum readings on the Summa canister
were recorded prior to and following the sampling period to ensure adequate sample volume was
collected. A vacuum was maintained within each summa canister at the conclusion of the
sampling event per laboratory standard operating procedures.

After sample collection, the flow controller valve was closed and disconnected from the canister.
The canisters were placed in laboratory supplied shipping containers, properly labeled and
shipped under standard chain-of-custody protocols to ConTest Analytical Laboratory for analysis
of VOCs by EPA Method TO-15. Upon receipt of the samples, the laboratory recorded the final
received vacuum pressure for each Summa canister.

Following collection of the sub-slab soil vapor samples, the vapor pins were removed and the
concrete surface was patched to match the surrounding area. Each sample location was
estimated by measuring from known benchmarks within the facility (e.g., doors, exterior walls,
hallways, etc.).
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6.2 Sub-Slab Soil Vapor Sample Analytical Results

A tabular summary of the soil gas sample analytical results is provided as Table 5. The
laboratory analytical report and chain of custody records are provided in Appendix B. The
analytical results were compared to DEQ DWM Non-Residential Vapor Intrusion Sub-slab and
Exterior Soil Gas Screening Levels (SGSLs) dated February 2018.

Laboratory analytical results for the soil gas samples indicate the presence of several compounds
at concentrations above the laboratory method detection limits in each sample. However, no
VOCs were detected at concentrations exceeding the DEQ DWM Non-Residential SGSLs in the
sub-slab soil vapor samples collected at the Site.

6.3 Vapor Intrusion Evaluation

The DEQ DWM Vapor Intrusion SGSLs used for comparison to the laboratory analytical results
are conservative and based upon a cumulative lifetime incremental carcinogenic risk (LICR) of
1 x 10-5 for potential carcinogenic effects and a cumulative hazard quotient (HQ) of 0.2 for
potential non-carcinogenic effects. Vapor intrusion mitigation or additional assessment is not
typically warranted if the calculated cumulative LICR is less than 1 x 10-4 and a calculated
cumulative Hazard Index (HI) is less than 1.0 (the HI is the sum of the individual compound
HQs).

H&H utilized the DEQ Risk Calculator (December 2019) assuming a non-residential land use
scenario to further evaluate potential cumulative risks for the soil gas to indoor air vapor
intrusion pathway. H&H calculated the cumulative risks using the highest concentration of any
compound detected in any sub-slab soil vapor sample collected at the Site to model the potential
for vapor intrusion under a hypothetical “worst-case” scenario.

Risk calculator results indicate that under a hypothetical worst-case scenario for the soil gas to
indoor air vapor intrusion pathway for a non-residential use, the cumulative LICR is 5.7 x 10-7
and the cumulative HI is 0.007. Risk calculator results for the soil gas to indoor air vapor
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intrusion pathway do not exceed acceptable risk levels under a non-residential land use scenario.
Based on evaluation of sub-slab soil vapor data and risk calculation results, there does not appear
to be a significant risk of structural vapor intrusion for the main warehouse, maintenance, and
training buildings at the Site. Copies of the completed risk calculators are provided in
Appendix D.
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7.0 Quality Assurance – Quality Control

For quality assurance and quality control purposes (QA/QC), non-dedicated equipment and tools
were decontaminated prior to use at each boring or sampling location or following exposure to
soil or groundwater. Field QA/QC samples were analyzed along with the investigative samples
to determine potential variability introduced in sampling, handling, shipping, and analysis. Two
trip blanks accompanied the groundwater and surface water samples during shipment and
sampling and were submitted for analysis of VOCs by EPA Method 8260. In addition, H&H
collected duplicate soil, groundwater, surface water, and sub-slab soil vapor samples to evaluate
the ability of the laboratory to reproduce sample results. Duplicate samples were submitted to the
laboratory for the same analysis as the corresponding parent sample.

7.1 Trip Blank

The trip blanks were prepared by the laboratory and consisted of certified-clean sample
containers filled with analyte-free water. The trip blanks accompanied the empty groundwater
and surface water laboratory sample containers to the Site, remained within the sample coolers
containing groundwater and surface water samples during sampling, and traveled back to the
laboratory with the groundwater and surface water samples field samples. The purpose of a trip
blank is to evaluate sample handling conditions and the potential for external contaminants to
compromise investigative samples during transit. Laboratory analytical results of the trip blanks
did not indicate the presence of VOCs at concentrations above the laboratory method detection
limits (Appendix B).

7.2 Laboratory Duplicates

Duplicate samples were collected to evaluate the precision of the field sampling procedures,
sample matrix variability, and analytical reproducibility. Duplicate soil, surface water, and
groundwater samples were collected directly into individual laboratory supplied sample
containers using sampling methodologies described in previous sections. The duplicate sub-slab
soil vapor sample was collected concurrently with the parent sample using a laboratory supplied
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T-fitting which allows for collection of two sub-slab soil vapor samples from one sampling point
simultaneously. The samples were analyzed for the same parameters as the parent samples, and
the analytical results were compared with those of the parent sample. The analytical results of
the parent sample and the duplicate sample were used to evaluate the cumulative precision of the
analytical method, sample matrix, and sample collection techniques.

Duplicate sample laboratory analytical results for each sample media are presented in the
summary tables (Table 1, Table 3, Table 4, and Table 5). Review of the duplicate sample results
in comparison to the parent sample results for each media sampled indicates that there was no
significant variability and confirm adequate sampling and laboratory reproducibility for soil,
surface water, and sub-slab vapor.

Groundwater duplicate sample results in comparison to the parent groundwater sample results
indicate that naphthalene by EPA Method 8260 was not detected above the laboratory method
detection limit (<35.2 µg/L) in the S-58 parent groundwater samples, but was detected at a
concentration of 567 1g µg/L in the S-58 duplicate groundwater sample GW-DUP. The “1g
flag” indicates that the detection of naphthalene in the duplicate groundwater sample is carryover
from the previous sample analyzed. Aside from the carryover naphthalene detection reported in
the duplicate groundwater sample, there was no significant variability and confirm adequate
sampling and laboratory reproducibility for the groundwater data. Please note that both the S-58
parent sample and its duplicate sample were diluted by a factor of 100 for the VOC analysis by
EPA Method 8260.
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8.0 Summary and Conclusions

H&H completed Brownfields assessment activities at the Salisbury Investments Brownfields
property located in Salisbury, Rowan County in accordance with the DEQ Brownfields approved
Work Plan dated May 19, 2020. Brownfields assessment activities included collection of soil,
groundwater, surface water, and sub-slab soil vapor samples for laboratory analysis to further
evaluate potential risks associated with the proposed uses of the Site. A brief summary of the
Brownfields assessment activities is provided below.

 Results of soil assessment activities completed in the vicinity of the Dowtherm heaters,
fuel oil storage tanks, and cooling tower did not identify compounds at concentrations
above the DEQ IHSB Commercial/Industrial PSRGs.

 Results of groundwater assessment activities identified benzene, chlorobenzene,
1,4-dichlorobenzene, bis(2-ethylhexyl)phthalate, and total chromium at concentrations
exceeding the DEQ 2L Standards in samples collected downgradient of the wastewater
treatment plant (S-58 and RR-102). The chlorobenzene concentration in S-58 also
exceed the DEQ DWM Non-Residential Vapor Intrusion GWSLs.

In addition, the organic compounds chlorobenzene and phenol were detected in
groundwater at concentrations exceeding the DEQ 2L Standards (and the DEQ DWM
Non-Residential Vapor Intrusion GWSL in the case of chlorobenzene) in the Z-90
groundwater sample collected downgradient of a former GRUB landfill. The metals
barium, cadmium, and total chromium were also detected at concentrations above the
DEQ 2L Standards in the groundwater sample collected downgradient of the former
GRUB landfill.

Three groundwater samples were collected along the eastern Site boundary and
downgradient of the polishing ponds. Chlorobenzene and 1,2-dichlorobenzene were
detected at concentrations above the DEQ 2L Standards in one (YY-37) of the three
polishing pond area groundwater samples.
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 Results of surface water assessment activities did not identify organic or inorganic
compounds at concentrations above the DEQ 2B Standards in samples collected from
upgradient and downgradient locations within on-Site portions of Second Creek.

 Results of sub-slab soil vapor assessment activities completed within the filament and
staple warehouses, maintenance building, and training building did not identify
compounds at concentrations above the DEQ DWM Non-Residential Vapor Intrusion
SGSLs. Hypothetical risk calculator results confirm that the soil gas to indoor air vapor
intrusion pathway does not pose an unacceptable risk for potential vapor intrusion in
these buildings under a non-residential use scenario.

In summary, results of soil assessment activities completed at the Site indicate that there is no
evidence of significant impacts in the areas of the fuel oil storage tanks, Dowtherm areas, or
cooling tower. Proposed redevelopment plans do not currently include significant disturbance to
soil. However, if significant soil disturbance does occur, it can be managed in accordance with a
DEQ Brownfields approved Environmental Management Plan (EMP).

Results of groundwater assessment activities indicate that groundwater impacts were identified at
concentrations above the DEQ groundwater quality or vapor intrusion screening criteria in areas
downgradient of a former GRUB landfill, the wastewater treatment plant, and the polishing
ponds. Groundwater impacts are being addressed by CNA Holdings, LLC under purview of the
EPA. Similar to soil, proposed redevelopment plans do not include activities that will encounter
groundwater. Vapor intrusion may need to be evaluated further if future enclosed buildings are
constructed in these areas.

Hypothetical worst-case scenario risk calculator results for the sub-slab soil vapor to indoor air
vapor intrusion pathways indicate that there does not appear to be a significant risk of structural
vapor intrusion into Site buildings planned for occupancy as part of the proposed redevelopment.

Table 1Summary of Soil Analytical DataSalisbury Investments Salisbury, North CarolinaH&H Job No. FDP-058Evaluation AreaSample IDSB-1 SB-2 SB-4 SB-5 SB-6 SB-7 BG-1 BG-2DateDepth (ft bgs)6-8 6-8 2-4 2-4 6-8 6-8 2-3 2-3 2-3 2-3Sample Type Range Mean Range MeanUnitsVOCs (8260D)n-Butylbenzene<0.0039 <0.00430.0498<0.0034 <0.0025 <0.0026 NA NA NA NA12,000-- -- -- --sec-Butylbenzene<0.0045 <0.00510.0395<0.0039 <0.0030 <0.0030 NA NA NA NA23,000-- -- -- --2-Chlorotoluene<0.0051 <0.0057 <0.00460.0278<0.00330.0206NA NA NA NA4,700-- -- -- --cis-1,2-Dichloroethene<0.0041 <0.0046 <0.0037 <0.0035 <0.00270.0158NA NA NA NA470-- -- -- --p-Isopropyltoluene<0.0039 <0.0044 <0.00360.0608<0.0026 <0.0026 NA NA NA NANE-- -- -- --Naphthalene<0.004 <0.00450.0140 0.0085<0.0026 <0.0027 NA NA NA NA18-- -- -- --Tetrachloroethene<0.0035 <0.0040 <0.0032 <0.0031 <0.00230.0640NA NA NA NA82-- -- -- --Trichloroethene<0.0045 <0.0050 <0.0040 <0.0039 <0.00290.0741NA NA NA NA4-- -- -- --1,2,4-Trimethylbenzene<0.0051 <0.00580.1050 0.0425<0.0034 <0.0034 NA NA NA NA370-- -- -- --1,3,5-Trimethylbenzene<0.0043 <0.00480.0783 0.0298<0.0028 <0.0028 NA NA NA NA320-- -- -- --Vinyl chloride<0.0027 <0.0031 <0.0025 <0.0024 <0.00180.0029 JNA NA NA NA1.7-- -- -- --SVOCs (8270E)Phenol<0.108 <0.112 <0.1120.163 J<0.0986 <0.0979 NA NA NA NA49,000-- -- -- --Metals (6020B/7471B/7199) Arsenic<0.583 <0.5980.820 J 0.618 J 0.745 J<0.555 NA NA <0.525 <0.5753.0All BDL --1.0 - 18 4.8Barium 241 111 183 155 156 86.9NA NA34.6 38.747,00034.6 - 38.7 36.7 50 - 1,000 356Cadmium<0.561 <0.576 <0.596 <0.579 <0.539 <0.534 NA NA <0.505 <0.553200All BDL --1.0 - 10 4Chromium (Total) 58.1 19.4 9.66 12.8 22.8 74.5 118 14.5 66.0 17.4NE17.4 - 66 41.7 7.0 - 300 65Chromium, Hexavalent 1.14 J<0.362 <0.375 <0.364 <0.339 <0.3350.977 J<0.332 <0.317 <0.3476.5All BDL --NS NSChromium, Trivalent 57.0 19.4 9.66 12.8 22.8 74.5 117 14.5 66.0 17.4 350,000 17.4 - 66 41.7 NS NSLead<1.383.88 4.16 3.63 4.06 2.45 JNA NA2.69 2.32 J8002.32 - 2.69 2.51 ND - 50 16Mercury<0.0249 <0.0255 <0.0264 <0.0257 <0.02390.0348 JNA NA0.0461 J 0.06309.70.0461 - 0.063 0.109 0.03 - 0.52 0.12Selenium<1.40 <1.43 <1.48 <1.44 <1.34 <1.33 NA NA <1.26 <1.381,200All BDL --<0.1 - 0.8 0.42Silver<0.294 <0.302 <0.313 <0.304 <0.283 <0.280 NA NA <0.265 <0.2901,200All BDL --ND - 5.0 NSNotes:1) NC Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) dated December 20192) Range and mean values of background metals for North Carolina soils obtained from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. Compound concentrations reported to the laboratory method detection limits. Aside from metals, only those compounds detected in at least one sample are shown in the table above. Concentrations are reported in milligrams per kilograms (mg/kg). Laboratory analytical methods are shown in parentheses.VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic Compoundsft bgs = feet below ground surface; BDL = Below Method Detection Limits; NS = Not Specified; NA = Not Analyzed; -- = Not Applicable; NE = Not Established; ND = Not DetectedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. 6/9/2020Industrial / Commercial PSRGs (1)SB-3 / SB-DUPRegional Background Metals in Soils (2)Site-Specific Background Metals in SoilScreening Criteriamg/kgCooling Tower6/9/2020BackgroundFuel Oil Storage 6/9/2020Grab6/9/2020Dowtherm AreaS:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-058 Durafiber Celanese Salisbury\Brownfields\Assessment\Tables\Data Table FDP-058Table 1 (Page 1 of 1)Hart & Hickman, PC
Table 2Well Construction and Groundwater Elevation DataSalisbury InvestmentsSalisbury, North CarolinaH&H Job No. FDP-058R-30 Polishing Ponds Saprolite/Soil 2 11/20/1981 25-3030 666.90 669.2618.79 650.47S-58 Water Treatment Facility Transition/Shallow Rock 2 6/27/1986 53-5858 687.30 688.7318.66 670.07Z-90 Downgradient of Manufacturing Facility Transition/Shallow Rock 2 4/26/1988 80-9090 682.98 683.9818.58 665.40DD-40 Water Treatment Facility Saprolite/Soil 2 6/29/1986 35-4040 694.46 696.0418.31 677.73GG-43 Downgradient of Manufacturing Facility Saprolite/Soil 2 5/8/1987 38-4343 713.10 715.0432.69 682.35RR-102 Polishing Ponds Saprolite/Soil 2 5/5/1989 92.5-102.5102.5 678.03 679.9815.11 664.87TT-34 Polishing Ponds Saprolite/Soil 2 5/9/1989 24-3434 658.42 663.3012.55 650.75YY-37 Polishing Ponds Saprolite/Soil 2 12/10/1990 27-3737 666.95 668.3818.19 650.19Notes:1) Depth to water measured by H&H on 6/10/2020. Depth to water measured relative to top of casing. Well construction information taken from Draft RFI and Site Stabilization Completion Report prepared by RUST Environmental & Infrastructure Inc. rdataed February 21, 1996. ft = Feet; bTOC = Below Top of CasingDepth to Water (ft bTOC) (1)Elevation (ft bTOC)Screen Interval (ft)Total Depth (ft)Ground Surface Elevation (ft)Top of Casing Elevation (ft)Well ID Site Area Screened ZoneDiameter (inches)Date InstalledS:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-058 Durafiber Celanese Salisbury\Brownfields\Assessment\Tables\Data Table FDP-0587/8/2020Table 2 (Page 1 of 1)Hart & Hickman, PC
Table 3Summary of Groundwater Analytical DataSalisbury Investments Salisbury, North CarolinaH&H Job No. FDP-058Sample IDR-30 Z-90 DD-40 GG-43 RR-102 TT-34 YY-37Date6/10/2020 6/10/2020 6/10/2020 6/10/2020 6/10/2020 6/10/2020 6/10/20206/10/2020 6/10/2020UnitsVOCs (8260B)Benzene<0.1561.2 J 58.4 J<7.5 <0.15 <0.15 <0.15 <0.15 <0.30169Bromodichloromethane<0.26 <25.6 <25.6 <12.8 <0.260.35 J<0.26 <0.26 <0.51138Bromomethane<0.62 <62.0 <62.0 <31.0 <0.622.6<0.62 <0.62 <1.2NE 152-Butanone (MEK)<3.3 <333 <333239 J<3.3 <3.3 <3.3 <3.3 <6.74,000 1,900,000Chlorobenzene<0.2312,50012,5001,500<0.23 <0.23 <0.23 <0.2353.450 3401,2-Dichlorobenzene<0.29 <29.1 <29.118.2 J<0.290.40 J<0.29 <0.2924820 2,2001,4-Dichlorobenzene<0.26140 137<12.9 <0.26 <0.26 <0.26 <0.263.6 6 110cis-1,2-Dichloroethylene<0.29 <29.1 <29.127.3 J<0.29 <0.29 <0.29 <0.291.0 J 70 NENaphthalene <0.35 <35.2 567 1g <17.6 <0.35 <0.35 <0.35 <0.35 <0.706150SVOCs (8270D)Benzoic Acid<19.5 <19.5 <19.514,600<19.5 <19.5 <19.5 <19.5 <19.530,000 NEBenzyl alcohol<2.6 <2.6 <2.61,780<2.6 <2.6 <2.6 <2.6 <2.6NE NE4-Chloroaniline<2.8 <2.8 <2.8 <57.0 <2.8 <2.8 <2.8 <2.8 <2.8NE NE2-Chlorophenol<1.414.8 13.5<28.8 <1.4 <1.4 <1.4 <1.4 <1.4NE NE1,2-Dichlorobenzene<1.42.1 J<1.4 <27.0 <1.4 <1.4 <1.4 <1.418520 2,2001,4-Dichlorobenzene<1.512093.5<30.4 <1.5 <1.5 <1.5 <1.53.1 J 6 110bis(2-Ethylhexyl)phthalate<2.03.7 J 4.6 J<39.6 <2.0 <2.0 <2.0 <2.0 <2.03NE3&4-Methylphenol (m&p Cresol)<1.21.3 J<1.258.9 J<1.2 <1.2 <1.2 <1.2 <1.2NE NENaphthalene<1.6 <1.6 <1.6 <32.8 <1.6 <1.6 <1.6 <1.6 <1.66 150Phenol<1.5 <1.53.3 J2,730<1.5 <1.5 <1.5 <1.52.3 J 30 NERCRA Metals (6020A-B, 7470A)Arsenic<0.735 <0.7351.18 J 2.98<0.735 <0.735 <0.735 <0.735 <0.73510--Barium146 115 1183,020101 71.2 30.5 108 93.3 700--Cadmium<0.478 <0.4780.629 J9.66<0.478 <0.478 <0.478 <0.478 <0.4782--Chromium<1.49 <1.49 <1.4913.6 10.6 190 69.44.96<1.4910--Chromium, Hexavalent<0.0400 <0.0400 <0.0400 <0.04003.86 3.97 9.51 0.16<0.0400NE--Chromium, Trivalent<1.49 <1.49 <1.4913.6 6.7 186 59.9 4.8<1.49NE--Lead<2.49 <2.49 <2.494.80 J<2.49 <2.49 <2.493.74 J<2.4915--Mercury<0.100 <0.100 <0.100 <0.100 <0.100 <0.100 <0.100 <0.100 <0.10010.75Selenium1.29 J 1.03 J<0.6571.33 J 1.12 J 1.52 J 1.12 J 1.22 J 1.83 J 20--Silver<0.513 <0.513 <0.513 <0.513 <0.513 <0.513 <0.513 <0.513 <0.51320--Turbidity (NTU)12.2 9.00 6.52 9.76 8.40 10.2 12.7-- --Notes:1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Quality Standards (2L Standards) dated April 20132) NC DEQ Division of Waste Management (DWM) Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSLs) dated February 2018With the exception of metals, only constituents detected in at least one sample are shown.Concentrations are reported in micrograms per liter (µg/L).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.Bold indicates concentration exceeds DEQ 2L Standard.Underlined indicates concentration exceeds DEQ DWM Non-Residential Vapor Intrusion GWSLsVOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic Compounds; NTU = Nephelometric Turbidity Units; NE = Not Established; -- = Not Applicable1g = Compound concentration was detected due to laboratory carryover from a previously analyzed sample. J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. 2L Standards (1)3.91S-58 / GW-DUPNon-Residential GWSLs(2)µg/LS:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-058 Durafiber Celanese Salisbury\Brownfields\Assessment\Tables\Data Table FDP-058_Updated.xlsx7/16/2020Table 3 (Page 1 of 1) Hart & Hickman, PC
Table 4Summary of Surface Water Analytical DataSalisbury Investments Salisbury, North CarolinaH&H Job No. FDP-058Area of ConcernUpstream Sample IDSW-1Sample Date06/09/20AcuteChronicUnitsVOCs (8260)BDLBDLBDL----SVOCs (8270)BDLBDLBDL----Metals (6020/7470)Arsenic<0.735 <0.735 <0.735340 150Barium 52.9 52.0 52.6 NE NECadmium<0.478 <0.478 <0.4781.31 (2)0.22 (2) Chromium1.93 J2.042.15NENEChromium, Hexavalent0.1010.1150.0555 J1611Chromium, Trivalent1.831.932.09285.43 (2) 37.13 (2)Lead<2.49 <2.492.65 J25.48 (2)0.99 (2)Mercury<0.100 <0.100 <0.1000.012 0.012Selenium<0.657 <0.657 <0.65755Silver<0.513 <0.513 <0.5130.75 (2) 0.06HardnessCalcium (6020)10,70010,90010,900NENEMagnesium (6020)3,9904,1204,110NENETotal Hardness (2340)43,00044,10044,100----Turbidity (NTU)44.3-- --Notes:1)North Carolina 15A NCAC 2B Surface Water Quality Standards (2B Standards) for Class C Surface Waters dated June 20192)2B Standards calculated using the Hardness-Dependent Metal Calculator dated June 10, 2019 and an in-stream hardness value of 43 mg/L (SW-1). Samples were collected from Second Creek, a Class C surface water bodyCompound concentrations are reported to the laboratory method detection limit.Concentrations are reported in micrograms per liter (µg/L).Laboratory analytical methods are shown in parentheses.Hardness-dependent metals include cadmium, trivalent chromium, lead, and silver.VOCs = Volatile Organic Compounds; SVOCs = Semi-VOCs; NTU = Nephelometric Turbidity UnitsNE = Not Established; BDL = Below Method Detection Limits; -- = Not ApplicableJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. 29.0DownstreamScreening CriteriaSW-4 / SW-DUP 2B Standards (1)06/09/20µg/LS:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-058 Durafiber Celanese Salisbury\Brownfields\Assessment\Tables\Data Table FDP-0587/8/2020Table 4 (Page 1 of 1)Hart & Hickman, PC
Table 5Summary of Sub-Slab Soil Vapor Analytical DataSalisbury Investments Salisbury, North CarolinaH&H Job No. FDP-058Evaluation AreaSample IDSS-1 SS-2 SS-4 SS-5 SS-6 SS-7 SS-8 SS-9 SS-10 SS-11Sample DateSlab Thickness (in)16 9 12 14 18 17 8 12 11 12UnitsVOCs (TO-15)Acetone (2) 120 380 360 340 86 110 190 120 210 290 460 230 2,700,000Benzene1.0<0.26 <0.260.40<0.26 <0.26 <0.260.51 J 0.31 J<0.26 <0.260.59 J 1,6002-Butanone (MEK)7.3 J 6.6 J 7.4 J 8.3 J 5.3 J 8.7 J 12 J 6.0 J 8.1 J 16 J 60 5.5 J 440,000Carbon Disulfide2.7 J<0.43 <0.43 <0.43 <0.43 <0.43 <0.435.9 J<0.43 <0.43 <0.43 <0.4361,000Carbon Tetrachloride0.83 J<0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.412,000Chloroform3.9<0.36 <0.36 <0.36 <0.36 <0.36 <0.364.8<0.361.0<0.36 <0.36530 Dichlorodifluoromethane (Freon 12)3.1 2.1 2.5 2.5 2.1 1.9 1.9 1.7 1.9 1.9<0.431.9 8,8001,1-Dichloroethane17<0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.257,7001,1-Dichloroethylene210<0.43 <0.43 <0.43 <0.43 <0.43 <0.43 <0.43 <0.43 <0.43 <0.43 <0.4318,000cis-1,2-Dichloroethylene<0.32 <0.32 <0.32 <0.32 <0.32 <0.32 <0.321.0<0.32 <0.32 <0.32 <0.32NEEthanol (2)1,000 630 910 690 560 860 900 530 560 3,600 1,700 750 NEEthyl Acetate12<0.54 <0.54 <0.54 <0.547.8<0.54 <0.545.6 10<0.5411 6,100Ethylbenzene0.50 J<0.50 <0.50 <0.50 <0.500.56 J<0.50 <0.501.1 0.66 J 1.2 2.4 4,9004-Ethyltoluene<0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.602.4 0.73 J 2.0 5.9 NEHeptane0.82<0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.481.1 35,0002-Hexanone (MBK)<0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.4815<0.482,600Isopropanol200 220 170 160 22 22 36 21 21 42 70 17 J 18,000Methylene Chloride8.4 1.3 J 1.8 J 1.3 J 1.7 J 6.7 J 1.4 J 2.6 J 1.5 J 2.3 J 2.2 J 5.6 J 53,0004-Methyl-2-pentanone (MIBK)<0.43 <0.432.5 2.8<0.43 <0.43 <0.43 <0.43 <0.4314<0.4334 260,000Naphthalene<0.80 <0.80 <0.80 <0.800.82 J<0.80 <0.800.88 J 4.5 5.7 4.0 9.2 260Styrene0.63 J<0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.530.92 0.90 1.3 2.4 88,000Tetrachloroethylene75 2.2 9.7 9.5 610 0.84 J 260 1.3 J 33 530 69 3.9 3,500Tetrahydrofuran<0.59 <0.59 <0.59 <0.59 <0.59 <0.59 <0.599.1<0.59 <0.59 <0.59 <0.59180,000Toluene4.0 1.3 0.68 J 0.63 J 1.3 4.6 1.6 1.5 3.0 2.5 3.1 7.4 440,0001,1,1-Trichloroethane4.2 13 2.6 2.5 0.79 J<0.412.9<0.41 <0.411.1<0.41 <0.41440,000Trichloroethylene17<0.43 <0.43 <0.43 <0.43 <0.43 <0.430.82 J<0.43 <0.43 <0.43 <0.43180 Trichlorofluoromethane (Freon 11)3.6 J 1.9 J 2.0 J 2.0 J 2.1 J 1.7 J 1.6 J 1.3 J 1.6 J 2.1 J 3.1 J 1.5 J NE1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)<1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <1.23.8 J<1.2440,0001,2,4-Trimethylbenzene<0.63 <0.63 <0.63 <0.63 <0.63 <0.63 <0.63 <0.63 <0.63 <0.63 <0.6325 5,3001,3,5-Trimethylbenzene<0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.624.6 1.3 4.0 12 5,300m&p-Xylene1.7 J 2.0 1.2 J 1.5 J 1.1 J 1.8 J 1.3 J 1.2 J 10 3.9 8.3 21 8,800o-Xylene0.69 J 0.69 J<0.54 <0.54 <0.540.82 J 0.57 J 0.61 J 3.4 1.4 2.9 7.1 8,800Notes:1) North Carolina Department of Environment Quality (DEQ) Division of Waste Management (DWM) Non-Residential Sub-slab and Exterior Soil Gas Screening Levels (SGSLs) dated February 20182) Concentrations were reported with the V-06 laboratory qualifier. V-06 = Continuing calibration verification did not meet method specifications and was biased on the high side for the compound. Only constituents detected in at least one sample are shown in the table above.Compound concentrations are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory detection limits.Laboratory analytical method is shown in parentheses. J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. VOCs = Volatile Organic Compounds; in = Inches; NE = Not Established 6/9/2020 6/9/2020Non-Residential SGSLs (1)µg/m3SS-3 / SS-DUPFilament WarehouseStaple Warehouse Maintenance Building Training Building6/10/2020136/9/2020S:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-058 Durafiber Celanese Salisbury\Brownfields\Assessment\Tables\Data Table FDP-0587/8/2020Table 5 (Page 1 of 1) Hart & Hickman, PC
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
ROWAN MILLS, NORTH CAROLINA 1991
TITLE
PROJECT
SITE LOCATION MAP
SALISBURY INVESTMENTS
7401 STATESVILLE BOULEVARD
SALISBURY, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
5/11/2020 0
1FDP-058
REVISION NO. 0
JOB NO. FDP-058
DATE: 7-7-20
FIGURE NO. 2
SALISBURY INVESTMENTS
7401 STATESVILLE BOULEVARD
SALISBURY, NORTH CAROLINA
SITE MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
SECOND CREEK
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
STATES
V
I
L
L
E

B
O
U
L
E
V
A
R
D
OL
D

U
.
S
.

H
W
Y

7
0
HWY 801CELANESE DRIVEPARKS ROADNOTES:
1.AERIAL IMAGERY OBTAINED FROM NC ONEMAP,
2019.
2.PARCEL DATA OBTAINED FROM ROWAN COUNTY
GIS, 2020.
ALLISON BROS. RACE CARS
(7920 STATESVILLE BOULEVARD)
RESIDENTIAL
AGRICULTURAL
LAND
AGRICULTURAL
LAND
RURAL
RESIDENTIAL
UNDEVELOPED
WOODED LAND MERIDIAN AUTOMOTIVE SYSTEMS
(6701 STATESVILLE BOULEVARD)
DUKE POWER
SUBSTATION
AGRICULTURAL
LAND
RESIDENTIALUNDEVELOPED
WOODED LANDAGRICULTURAL
LAND
FORMER DURAFIBER
TECHNOLOGIES FACILITY
S:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-058 Durafiber Celanese Salisbury\Figures\Site Map.dwg, FIG 2, 7/8/2020 5:49:09 PM, sperry
CELANESE DRIVEFORMER GRUB LANDFILL
POLISHING
POND
POLISHING
POND
POLISHING
POND
POLISHING
POND
(2) AERATION BASINS
DIGESTOR
PROCESS
WATER POND
GROUNDWATER
REMEDIATION SYSTEM
ABANDONED AERATION BASIN
PARKING
PARKING
REC CLUBHOUSE
FIBER
LAKE
STAPLE WAREHOUSE
FILAMENT
WAREHOUSE
EQUALIZATION TANKS
(FORMER CRU BASIN)
CLARIFIER
FUEL OIL STORAGE
GLYCOL RECOVERY UNIT
UTILITIES
POLYMER SPINNING
POLYMER SPINNING
DOW REBOILERS
DOW STORAGE
DOW BOILERS
DOW STORAGE
GLYCOL STORAGE
GLYCOL RECOVERY STORAGE
WASTE WATER
TREATMENT PLANT
DOWTHERM AREA
REVISION NO. 0
JOB NO. FDP-058
DATE: 7-8-20
FIGURE NO. 3
SALISBURY INVESTMENTS
7401 STATESVILLE BOULEVARD
SALISBURY, NORTH CAROLINA
DETAILED SITE MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1.AERIAL IMAGERY OBTAINED FROM NC ONEMAP,
2019.
2.PARCEL DATA OBTAINED FROM ROWAN COUNTY
GIS, 2020.
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
SECOND CREEK
RAILROAD SPUR
S:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-058 Durafiber Celanese Salisbury\Figures\Detailed Site Map.dwg, FIG 3, 7/16/2020 11:33:21 AM, sperry
POLISHING
POND
POLISHING
POND
POLISHING
POND
POLISHING
POND
DIGESTOR
PROCESS
WATER
POND
ABANDONED AERATION BASIN
REC CLUBHOUSE
FIBER
LAKE
STAPLE WAREHOUSE
FILAMENT
WAREHOUSE
CLARIFIER
DOW STORAGE
SB-1
SB-2
SB-3
SB-4 SB-5
SB-6
SB-7
SS-2
SS-5
SS-1
SS-3
SS-4
SS-6
SS-7
SS-8
SS-9
SS-10
SS-11
SW-4
SW-1
BG-1
BG-2
UNDEVELOPED
PARKING
PARKINGCELANESE DRIVETT-34
YY-37
R-30
Z-90
RR-102
S-58
DD-40
GG-43
FORMER GRUB LANDFILL
DOWTHERM AREA
WASTE WATER
TREATMENT PLANT
DOW REBOILERS
DOW STORAGE
DOW BOILERS
FUEL OIL STORAGE
MAINTENANCE BUILDING
TRAINING BUILDING EQUALIZATION TANKS
(FORMER CRU BASIN)
REVISION NO. 0
JOB NO. FDP-058
DATE: 7-8-20
FIGURE NO. 4
SALISBURY INVESTMENTS
7401 STATESVILLE BOULEVARD
SALISBURY, NORTH CAROLINA
SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1.AERIAL IMAGERY OBTAINED FROM NC ONEMAP,
2019.
2.PARCEL DATA OBTAINED FROM ROWAN COUNTY
GIS, 2020.
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
SECOND CREEK
RAILROAD SPUR
DOWTHERM AREA SOIL SAMPLE
FUEL OIL STORAGE SOIL SAMPLE
COOLING TOWER SOIL SAMPLE
BACKGROUND SOIL SAMPLE
GROUNDWATER MONITORING WELL
SURFACE WATER SAMPLE
SUB-SLAB SOIL VAPOR SAMPLE
S:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-058 Durafiber Celanese Salisbury\Figures\Sample Location Map.dwg, FIG 4, 7/16/2020 12:23:08 PM, sperry
(682.35)
TT-34
YY-37
R-30
(650.75)
(650.47)
Z-90
RR-102
S-58
DD-40
GG-43
(650.19)
(677.78)
(670.07)
(669.87)*
(665.40)*
REVISION NO. 0
JOB NO. FDP-058
DATE: 7-8-20
FIGURE NO. 5
SALISBURY INVESTMENTS
7401 STATESVILLE BOULEVARD
SALISBURY, NORTH CAROLINA
SHALLOW GROUNDWATER
HYDRAULIC GRADIENT MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1.AERIAL IMAGERY OBTAINED FROM NC ONEMAP,
2019.
2.PARCEL DATA OBTAINED FROM ROWAN COUNTY
GIS, 2020.
3.MONITORING WELLS GAUGED BY H&H ON 6/10/2020.
* GROUNDWATER ELEVATIONS FROM DEEPER
MONITORING WELLS RR-102 AND Z-90 NOT USED IN
CONTOURING.
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
SECOND CREEK
RAILROAD SPUR
GROUNDWATER MONITORING WELL
GROUNDWATER ELEVATION (FT)
INFERRED GROUNDWATER
ELEVATION CONTOUR (FT)
INFERRED GROUNDWATER FLOW
DIRECTION
680
(682.35)
POLISHING
POND
POLISHING
POND
POLISHING
POND
POLISHING
POND
PROCESS
WATER
POND
FIBER
LAKE 680
670
660
650
S:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-058 Durafiber Celanese Salisbury\Figures\Sample Location Map.dwg, FIG 5, 7/16/2020 11:36:12 AM, sperry

Appendix A

Boring Logs
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
ForSite Development Partners
FDP-058
7401 Statesville Boulevard,Salisbury, NC
BORING LOG
Boring No.
Page:
BG-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/9/20
6/9/20
Mid-South Environmental
Other
Hand Auger
Don Warren
Haley Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') Sandy SILT (ML); medium stiff, moist, brown, with organics
(3') Boring terminated
6.5
3.2 BG-1(2-3)
0
1
2
3
4
5
Grab
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
ForSite Development Partners
FDP-058
7401 Statesville Boulevard,Salisbury, NC
BORING LOG
Boring No.
Page:
BG-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/9/20
6/9/20
Mid-South Environmental
Other
Hand Auger
Don Warren
Haley Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') SILT (ML); some clay, soft, wet, brown
(0.5') SILT (ML); medium stiff, moist, dark red and orange
(3') Boring terminated
7.8
8.4 BG-2(2-3)
0
1
2
3
4
5
Grab
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
ForSite Development Partners
FDP-058
7401 Statesville Boulevard,Salisbury, NC
BORING LOG
Boring No.
Page:
SB-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/9/20
6/9/20
Mid-South Environmental
Direct Push
Geoprobe 54 DT
Don Warren
Haley Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
15.0
2.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Poorly graded GRAVEL with sand (GP); some coarse sand, dense, dry, debris
(3') SILT (ML); soft, moist, greenish-gray
(6') SILT (ML); soft, moist, light greenish-brown
(15') Boring terminated
6.5
7.8
9.7
11.9
7.2
8.8
8.8
8.2
SB-1(6-8)
0
5
10
15
20
Grab
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
ForSite Development Partners
FDP-058
7401 Statesville Boulevard,Salisbury, NC
BORING LOG
Boring No.
Page:
SB-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/9/20
6/9/20
Mid-South Environmental
Direct Push
Geoprobe 54 DT
Don Warren
Haley Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
15.0
2.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Poorly graded GRAVEL with sand (GP); some coarse sand
(2') SILT (ML); medium stiff, moist, dark greenish-gray, slight odor
(5') SILT (ML); soft, dry, brown
(6') SILT (ML); medium stiff, moist, gray-tan
(14') Silty SAND (SM); loose, wet, light greenish-brown
(15') Boring terminated
10.7
15.5
15.8
15.1
13.2
11.7
9.9
SB-2(6-8)
0
5
10
15
20
Grab
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
ForSite Development Partners
FDP-058
7401 Statesville Boulevard,Salisbury, NC
BORING LOG
Boring No.
Page:
SB-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/9/20
6/9/20
Mid-South Environmental
Direct Push
Geoprobe 54 DT
Don Warren
Haley Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
15.0
2.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
(0') Poorly graded GRAVEL with sand (GP); some coarse sand
(2') Sandy SILT (ML); soft, moist, dark reddish-gray
(8') SILT (ML); soft, moist, gray and tan
(12') As Above: Poor Recovery (30%)
(15') Boring terminated
212.3
25.3
17.4
21.7
22.4
23.3
SB-3(2-4)
0
5
10
15
20
Grab
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
ForSite Development Partners
FDP-058
7401 Statesville Boulevard,Salisbury, NC
BORING LOG
Boring No.
Page:
SB-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/9/20
6/9/20
Mid-South Environmental
Direct Push
Geoprobe 54 DT
Don Warren
Haley Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
10.0
2.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
(0') Silty GRAVEL (GM)
(2') SILT (ML); some clay, stiff, wet, brown and red, with mica
(6') As Above: some gray, slight odor
(8') As Above: saturated
(10') Boring terminated
12.7
13.8
16.7
12.7
SB-4(6-8)
0
5
10
15
Grab
NOTES: Hole precleared to 5.0' using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
ForSite Development Partners
FDP-058
7401 Statesville Boulevard,Salisbury, NC
BORING LOG
Boring No.
Page:
SB-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/9/20
6/9/20
Mid-South Environmental
Direct Push
Geoprobe 54 DT
Don Warren
Haley Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
10.0
2.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
(0') Concrete
(0.5') SILT (ML); some clay, stiff, moist, pale reddish, (fill)
(8') SILT (ML); little clay, stiff, moist, pale reddish-brown
(10') Boring terminated
12.7
12.0
11.1
11.4
11.6
SB-5(6-8)
0
5
10
15
Grab
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
ForSite Development Partners
FDP-058
7401 Statesville Boulevard,Salisbury, NC
BORING LOG
Boring No.
Page:
SB-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/9/20
6/9/20
Mid-South Environmental
Other
Hand Auger
Don Warren
Haley Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') Poorly graded GRAVEL (GP)
(0.5') SILT (ML); some clay, stiff, moist, pale reddish, with mica
(3') Boring terminated
16.0
13.5 SB-6(2-3)
0
1
2
3
4
5
Grab
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
ForSite Development Partners
FDP-058
7401 Statesville Boulevard,Salisbury, NC
BORING LOG
Boring No.
Page:
SB-7
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/9/20
6/9/20
Mid-South Environmental
Other
Hand Auger
Don Warren
Haley Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.25
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') Poorly graded GRAVEL (GP)
(0.5') SILT (ML); some clay, stiff, moist, pale reddish
(3') Boring terminated
16.6
16.2 SB-7(2-3)
0
1
2
3
4
5
Grab

Appendix B

Laboratory Analytical Reports
#=CL#
June 18, 2020
LIMS USE: FR - RALPH MCGEE
LIMS OBJECT ID: 92481197
92481197
Project:
Pace Project No.:
RE:
Ralph McGee
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
FDP-058
Dear Ralph McGee:
Enclosed are the analytical results for sample(s) received by the laboratory on June 10, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang for
[e-mail]
Project Manager
Kevin Godwin
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 69
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92481197
FDP-058
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 69
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92481197
FDP-058
Lab ID Sample ID Matrix Date Collected Date Received
92481197001 SB-1(6-8)Solid 06/09/20 09:35 06/10/20 10:20
92481197002 SB-2(6-8)Solid 06/09/20 10:15 06/10/20 10:20
92481197003 SB-3(2-4)Solid 06/09/20 10:45 06/10/20 10:20
92481197004 SB-4(6-8)Solid 06/09/20 11:15 06/10/20 10:20
92481197005 SB-5(6-8)Solid 06/09/20 12:10 06/10/20 10:20
92481197006 SB-DUP Solid 06/09/20 00:00 06/10/20 10:20
92481197007 SB-6(2-3)Solid 06/09/20 12:15 06/10/20 10:20
92481197008 SB-7(2-3)Solid 06/09/20 12:20 06/10/20 10:20
92481197009 BG-1(2-3)Solid 06/09/20 08:30 06/10/20 10:20
92481197010 BG-2(2-3)Solid 06/09/20 13:00 06/10/20 10:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 69
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92481197
FDP-058
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92481197001 SB-1(6-8)EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92481197002 SB-2(6-8)EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92481197003 SB-3(2-4)EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92481197004 SB-4(6-8)EPA 6020B 7 PANLD
EPA 7471B 1 PANABL
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92481197005 SB-5(6-8)EPA 6020B 7 PANLD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92481197006 SB-DUP EPA 6020B 7 PANLD
EPA 7471B 1 PANTCT
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 69
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92481197
FDP-058
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92481197007 SB-6(2-3)EPA 6020B 1 PANLD
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92481197008 SB-7(2-3)EPA 6020B 1 PANLD
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92481197009 BG-1(2-3)EPA 6020B 7 PANLD
EPA 7471B 1 PANTCT
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92481197010 BG-2(2-3)EPA 6020B 7 PANLD
EPA 7471B 1 PANTCT
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-1(6-8)Lab ID:92481197001 Collected:06/09/20 09:35 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND mg/kg 06/14/20 18:51 7440-38-206/13/20 08:241.38 0.583 5
Barium 241 mg/kg 06/14/20 18:51 7440-39-3 ML06/13/20 08:243.46 1.73 5
Cadmium ND mg/kg 06/14/20 18:51 7440-43-9 PH06/13/20 08:241.38 0.561 5
Chromium 58.1 mg/kg 06/14/20 18:51 7440-47-306/13/20 08:246.91 3.10 5
Lead ND mg/kg 06/14/20 18:51 7439-92-106/13/20 08:242.76 1.38 5
Selenium ND mg/kg 06/14/20 18:51 7782-49-206/13/20 08:243.46 1.40 5
Silver ND mg/kg 06/14/20 18:51 7440-22-406/13/20 08:240.691 0.294 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 06/12/20 09:00 7439-97-606/11/20 20:250.0553 0.0249 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/11/20 17:26 83-32-906/10/20 15:394531171
Acenaphthylene ND ug/kg 06/11/20 17:26 208-96-806/10/20 15:394531071
Aniline ND ug/kg 06/11/20 17:26 62-53-306/10/20 15:394531021
Anthracene ND ug/kg 06/11/20 17:26 120-12-706/10/20 15:394531181
Benzo(a)anthracene ND ug/kg 06/11/20 17:26 56-55-306/10/20 15:394531441
Benzo(a)pyrene ND ug/kg 06/11/20 17:26 50-32-806/10/20 15:394531961
Benzo(b)fluoranthene ND ug/kg 06/11/20 17:26 205-99-206/10/20 15:394531831
Benzo(g,h,i)perylene ND ug/kg 06/11/20 17:26 191-24-206/10/20 15:394531771
Benzo(k)fluoranthene ND ug/kg 06/11/20 17:26 207-08-906/10/20 15:394531911
Benzoic Acid ND ug/kg 06/11/20 17:26 65-85-006/10/20 15:3922604891
Benzyl alcohol ND ug/kg 06/11/20 17:26 100-51-606/10/20 15:399062401
4-Bromophenylphenyl ether ND ug/kg 06/11/20 17:26 101-55-306/10/20 15:394531191
Butylbenzylphthalate ND ug/kg 06/11/20 17:26 85-68-706/10/20 15:394531211
4-Chloro-3-methylphenol ND ug/kg 06/11/20 17:26 59-50-706/10/20 15:399062761
4-Chloroaniline ND ug/kg 06/11/20 17:26 106-47-806/10/20 15:399062771
bis(2-Chloroethoxy)methane ND ug/kg 06/11/20 17:26 111-91-106/10/20 15:394531211
bis(2-Chloroethyl) ether ND ug/kg 06/11/20 17:26 111-44-406/10/20 15:3945396.2 1
2-Chloronaphthalene ND ug/kg 06/11/20 17:26 91-58-706/10/20 15:394531011
2-Chlorophenol ND ug/kg 06/11/20 17:26 95-57-806/10/20 15:394531051
4-Chlorophenylphenyl ether ND ug/kg 06/11/20 17:26 7005-72-306/10/20 15:394531181
Chrysene ND ug/kg 06/11/20 17:26 218-01-906/10/20 15:394531321
Dibenz(a,h)anthracene ND ug/kg 06/11/20 17:26 53-70-306/10/20 15:394531811
Dibenzofuran ND ug/kg 06/11/20 17:26 132-64-906/10/20 15:394531131
1,2-Dichlorobenzene ND ug/kg 06/11/20 17:26 95-50-106/10/20 15:3945398.0 1
1,3-Dichlorobenzene ND ug/kg 06/11/20 17:26 541-73-106/10/20 15:394531021
1,4-Dichlorobenzene ND ug/kg 06/11/20 17:26 106-46-706/10/20 15:3945399.7 1
3,3'-Dichlorobenzidine ND ug/kg 06/11/20 17:26 91-94-106/10/20 15:399063161
2,4-Dichlorophenol ND ug/kg 06/11/20 17:26 120-83-206/10/20 15:394531501
Diethylphthalate ND ug/kg 06/11/20 17:26 84-66-206/10/20 15:3945398.3 1
2,4-Dimethylphenol ND ug/kg 06/11/20 17:26 105-67-906/10/20 15:394531131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-1(6-8)Lab ID:92481197001 Collected:06/09/20 09:35 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/11/20 17:26 131-11-306/10/20 15:394531021
Di-n-butylphthalate ND ug/kg 06/11/20 17:26 84-74-206/10/20 15:394531121
4,6-Dinitro-2-methylphenol ND ug/kg 06/11/20 17:26 534-52-106/10/20 15:399067301
2,4-Dinitrophenol ND ug/kg 06/11/20 17:26 51-28-506/10/20 15:39226014501
2,4-Dinitrotoluene ND ug/kg 06/11/20 17:26 121-14-206/10/20 15:394531201
2,6-Dinitrotoluene ND ug/kg 06/11/20 17:26 606-20-2 L2,v206/10/20 15:394531181
Di-n-octylphthalate ND ug/kg 06/11/20 17:26 117-84-0 v106/10/20 15:394532581
bis(2-Ethylhexyl)phthalate ND ug/kg 06/11/20 17:26 117-81-706/10/20 15:394531481
Fluoranthene ND ug/kg 06/11/20 17:26 206-44-006/10/20 15:394531371
Fluorene ND ug/kg 06/11/20 17:26 86-73-706/10/20 15:394531211
Hexachloro-1,3-butadiene ND ug/kg 06/11/20 17:26 87-68-306/10/20 15:394531101
Hexachlorobenzene ND ug/kg 06/11/20 17:26 118-74-106/10/20 15:394531151
Hexachlorocyclopentadiene ND ug/kg 06/11/20 17:26 77-47-406/10/20 15:394531811
Hexachloroethane ND ug/kg 06/11/20 17:26 67-72-106/10/20 15:394531031
Indeno(1,2,3-cd)pyrene ND ug/kg 06/11/20 17:26 193-39-506/10/20 15:394532071
Isophorone ND ug/kg 06/11/20 17:26 78-59-106/10/20 15:3945398.4 1
1-Methylnaphthalene ND ug/kg 06/11/20 17:26 90-12-006/10/20 15:394531211
2-Methylnaphthalene ND ug/kg 06/11/20 17:26 91-57-606/10/20 15:394531151
2-Methylphenol(o-Cresol)ND ug/kg 06/11/20 17:26 95-48-706/10/20 15:394531001
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/11/20 17:26 15831-10-406/10/20 15:394531141
Naphthalene ND ug/kg 06/11/20 17:26 91-20-306/10/20 15:394531081
2-Nitroaniline ND ug/kg 06/11/20 17:26 88-74-406/10/20 15:3922602281
3-Nitroaniline ND ug/kg 06/11/20 17:26 99-09-206/10/20 15:3922602401
4-Nitroaniline ND ug/kg 06/11/20 17:26 100-01-606/10/20 15:399062241
Nitrobenzene ND ug/kg 06/11/20 17:26 98-95-306/10/20 15:394531081
2-Nitrophenol ND ug/kg 06/11/20 17:26 88-75-506/10/20 15:394531401
4-Nitrophenol ND ug/kg 06/11/20 17:26 100-02-706/10/20 15:3922607221
N-Nitrosodimethylamine ND ug/kg 06/11/20 17:26 62-75-906/10/20 15:394531271
N-Nitroso-di-n-propylamine ND ug/kg 06/11/20 17:26 621-64-706/10/20 15:394531271
N-Nitrosodiphenylamine ND ug/kg 06/11/20 17:26 86-30-606/10/20 15:394531161
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/11/20 17:26 108-60-106/10/20 15:394531261
Pentachlorophenol ND ug/kg 06/11/20 17:26 87-86-506/10/20 15:399062071
Phenanthrene ND ug/kg 06/11/20 17:26 85-01-806/10/20 15:394531141
Phenol ND ug/kg 06/11/20 17:26 108-95-206/10/20 15:394531081
Pyrene ND ug/kg 06/11/20 17:26 129-00-006/10/20 15:394531251
Pyridine ND ug/kg 06/11/20 17:26 110-86-106/10/20 15:394531151
1,2,4-Trichlorobenzene ND ug/kg 06/11/20 17:26 120-82-106/10/20 15:394531041
2,4,5-Trichlorophenol ND ug/kg 06/11/20 17:26 95-95-406/10/20 15:394531181
2,4,6-Trichlorophenol ND ug/kg 06/11/20 17:26 88-06-206/10/20 15:394531141
Surrogates
Nitrobenzene-d5 (S)40 %06/11/20 17:26 4165-60-006/10/20 15:3923-110 1
2-Fluorobiphenyl (S)38 %06/11/20 17:26 321-60-806/10/20 15:3930-110 1
Terphenyl-d14 (S)40 %06/11/20 17:26 1718-51-006/10/20 15:3928-110 1
Phenol-d6 (S)42 %06/11/20 17:26 13127-88-306/10/20 15:3922-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-1(6-8)Lab ID:92481197001 Collected:06/09/20 09:35 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)42 %06/11/20 17:26 367-12-406/10/20 15:3913-110 1
2,4,6-Tribromophenol (S)36 %06/11/20 17:26 118-79-606/10/20 15:3927-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/15/20 18:56 67-64-106/15/20 15:0014353.2 1
Benzene ND ug/kg 06/15/20 18:56 71-43-206/15/20 15:007.1 5.0 1
Bromobenzene ND ug/kg 06/15/20 18:56 108-86-106/15/20 15:007.1 4.8 1
Bromochloromethane ND ug/kg 06/15/20 18:56 74-97-506/15/20 15:007.1 5.4 1
Bromodichloromethane ND ug/kg 06/15/20 18:56 75-27-406/15/20 15:007.1 4.7 1
Bromoform ND ug/kg 06/15/20 18:56 75-25-206/15/20 15:007.1 3.9 1
Bromomethane ND ug/kg 06/15/20 18:56 74-83-906/15/20 15:0014.3 11.2 1
2-Butanone (MEK)ND ug/kg 06/15/20 18:56 78-93-306/15/20 15:0014360.5 1
n-Butylbenzene ND ug/kg 06/15/20 18:56 104-51-806/15/20 15:007.1 3.9 1
sec-Butylbenzene ND ug/kg 06/15/20 18:56 135-98-806/15/20 15:007.1 4.5 1
tert-Butylbenzene ND ug/kg 06/15/20 18:56 98-06-606/15/20 15:007.1 3.8 1
Carbon tetrachloride ND ug/kg 06/15/20 18:56 56-23-506/15/20 15:007.1 3.2 1
Chlorobenzene ND ug/kg 06/15/20 18:56 108-90-706/15/20 15:007.1 4.6 1
Chloroethane ND ug/kg 06/15/20 18:56 75-00-306/15/20 15:0014.3 7.5 1
Chloroform ND ug/kg 06/15/20 18:56 67-66-306/15/20 15:007.1 3.5 1
Chloromethane ND ug/kg 06/15/20 18:56 74-87-306/15/20 15:0014.3 10.0 1
2-Chlorotoluene ND ug/kg 06/15/20 18:56 95-49-806/15/20 15:007.1 5.1 1
4-Chlorotoluene ND ug/kg 06/15/20 18:56 106-43-406/15/20 15:007.1 4.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/15/20 18:56 96-12-806/15/20 15:007.1 6.6 1
Dibromochloromethane ND ug/kg 06/15/20 18:56 124-48-106/15/20 15:007.1 3.8 1
1,2-Dibromoethane (EDB)ND ug/kg 06/15/20 18:56 106-93-406/15/20 15:007.1 5.0 1
Dibromomethane ND ug/kg 06/15/20 18:56 74-95-306/15/20 15:007.1 3.6 1
1,2-Dichlorobenzene ND ug/kg 06/15/20 18:56 95-50-106/15/20 15:007.1 4.2 1
1,3-Dichlorobenzene ND ug/kg 06/15/20 18:56 541-73-106/15/20 15:007.1 5.9 1
1,4-Dichlorobenzene ND ug/kg 06/15/20 18:56 106-46-706/15/20 15:007.1 5.4 1
Dichlorodifluoromethane ND ug/kg 06/15/20 18:56 75-71-806/15/20 15:0014.3 2.5 1
1,1-Dichloroethane ND ug/kg 06/15/20 18:56 75-34-306/15/20 15:007.1 3.1 1
1,2-Dichloroethane ND ug/kg 06/15/20 18:56 107-06-206/15/20 15:007.1 2.9 1
1,1-Dichloroethene ND ug/kg 06/15/20 18:56 75-35-406/15/20 15:007.1 2.2 1
cis-1,2-Dichloroethene ND ug/kg 06/15/20 18:56 156-59-206/15/20 15:007.1 4.1 1
trans-1,2-Dichloroethene ND ug/kg 06/15/20 18:56 156-60-506/15/20 15:007.1 3.1 1
1,2-Dichloropropane ND ug/kg 06/15/20 18:56 78-87-506/15/20 15:007.1 4.4 1
1,3-Dichloropropane ND ug/kg 06/15/20 18:56 142-28-906/15/20 15:007.1 4.9 1
2,2-Dichloropropane ND ug/kg 06/15/20 18:56 594-20-706/15/20 15:007.1 3.9 1
1,1-Dichloropropene ND ug/kg 06/15/20 18:56 563-58-606/15/20 15:007.1 3.4 1
cis-1,3-Dichloropropene ND ug/kg 06/15/20 18:56 10061-01-506/15/20 15:007.1 4.6 1
trans-1,3-Dichloropropene ND ug/kg 06/15/20 18:56 10061-02-606/15/20 15:007.1 6.0 1
Diisopropyl ether ND ug/kg 06/15/20 18:56 108-20-306/15/20 15:007.1 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-1(6-8)Lab ID:92481197001 Collected:06/09/20 09:35 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/15/20 18:56 100-41-406/15/20 15:007.1 6.7 1
Hexachloro-1,3-butadiene ND ug/kg 06/15/20 18:56 87-68-306/15/20 15:007.1 6.8 1
2-Hexanone ND ug/kg 06/15/20 18:56 591-78-606/15/20 15:0071.3 14.2 1
Isopropylbenzene (Cumene)ND ug/kg 06/15/20 18:56 98-82-806/15/20 15:007.1 4.5 1
p-Isopropyltoluene ND ug/kg 06/15/20 18:56 99-87-606/15/20 15:007.1 3.9 1
Methylene Chloride ND ug/kg 06/15/20 18:56 75-09-206/15/20 15:0028.5 10.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/15/20 18:56 108-10-106/15/20 15:0071.3 60.4 1
Methyl-tert-butyl ether ND ug/kg 06/15/20 18:56 1634-04-406/15/20 15:007.1 4.6 1
Naphthalene ND ug/kg 06/15/20 18:56 91-20-306/15/20 15:007.1 4.0 1
n-Propylbenzene ND ug/kg 06/15/20 18:56 103-65-106/15/20 15:007.1 4.9 1
Styrene ND ug/kg 06/15/20 18:56 100-42-506/15/20 15:007.1 3.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/15/20 18:56 630-20-606/15/20 15:007.1 4.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/15/20 18:56 79-34-506/15/20 15:007.1 6.3 1
Tetrachloroethene ND ug/kg 06/15/20 18:56 127-18-406/15/20 15:007.1 3.5 1
Toluene ND ug/kg 06/15/20 18:56 108-88-306/15/20 15:007.1 4.1 1
1,2,3-Trichlorobenzene ND ug/kg 06/15/20 18:56 87-61-606/15/20 15:007.1 4.4 1
1,2,4-Trichlorobenzene ND ug/kg 06/15/20 18:56 120-82-106/15/20 15:007.1 4.0 1
1,1,1-Trichloroethane ND ug/kg 06/15/20 18:56 71-55-606/15/20 15:007.1 2.9 1
1,1,2-Trichloroethane ND ug/kg 06/15/20 18:56 79-00-506/15/20 15:007.1 5.3 1
Trichloroethene ND ug/kg 06/15/20 18:56 79-01-606/15/20 15:007.1 4.5 1
Trichlorofluoromethane ND ug/kg 06/15/20 18:56 75-69-406/15/20 15:007.1 1.8 1
1,2,3-Trichloropropane ND ug/kg 06/15/20 18:56 96-18-406/15/20 15:007.1 5.8 1
1,2,4-Trimethylbenzene ND ug/kg 06/15/20 18:56 95-63-606/15/20 15:007.1 5.1 1
1,3,5-Trimethylbenzene ND ug/kg 06/15/20 18:56 108-67-806/15/20 15:007.1 4.3 1
Vinyl acetate ND ug/kg 06/15/20 18:56 108-05-406/15/20 15:0071.3 6.2 1
Vinyl chloride ND ug/kg 06/15/20 18:56 75-01-406/15/20 15:0014.3 2.7 1
Xylene (Total)ND ug/kg 06/15/20 18:56 1330-20-706/15/20 15:0014.3 4.1 1
m&p-Xylene ND ug/kg 06/15/20 18:56 179601-23-106/15/20 15:0014.3 11.0 1
o-Xylene ND ug/kg 06/15/20 18:56 95-47-606/15/20 15:007.1 4.1 1
Surrogates
Toluene-d8 (S)101 %06/15/20 18:56 2037-26-506/15/20 15:0070-130 1
4-Bromofluorobenzene (S)98 %06/15/20 18:56 460-00-406/15/20 15:0070-130 1
1,2-Dichloroethane-d4 (S)102 %06/15/20 18:56 17060-07-006/15/20 15:0070-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.3 %06/10/20 16:550.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 72.3 %06/14/20 00:3206/14/20 00:191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-1(6-8)Lab ID:92481197001 Collected:06/09/20 09:35 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.14J mg/kg 06/16/20 20:00 18540-29-9 J06/16/20 12:301.38 0.353 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-2(6-8)Lab ID:92481197002 Collected:06/09/20 10:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND mg/kg 06/14/20 19:14 7440-38-206/13/20 08:241.42 0.598 5
Barium 111 mg/kg 06/14/20 19:14 7440-39-306/13/20 08:243.55 1.77 5
Cadmium ND mg/kg 06/14/20 19:14 7440-43-906/13/20 08:241.42 0.576 5
Chromium 19.4 mg/kg 06/14/20 19:14 7440-47-306/13/20 08:247.09 3.18 5
Lead 3.88 mg/kg 06/14/20 19:14 7439-92-106/13/20 08:242.84 1.42 5
Selenium ND mg/kg 06/14/20 19:14 7782-49-206/13/20 08:243.55 1.43 5
Silver ND mg/kg 06/14/20 19:14 7440-22-406/13/20 08:240.709 0.302 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 06/12/20 09:02 7439-97-606/11/20 20:250.0567 0.0255 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/11/20 18:27 83-32-906/10/20 15:394671201
Acenaphthylene ND ug/kg 06/11/20 18:27 208-96-806/10/20 15:394671111
Aniline ND ug/kg 06/11/20 18:27 62-53-306/10/20 15:394671051
Anthracene ND ug/kg 06/11/20 18:27 120-12-706/10/20 15:394671211
Benzo(a)anthracene ND ug/kg 06/11/20 18:27 56-55-306/10/20 15:394671491
Benzo(a)pyrene ND ug/kg 06/11/20 18:27 50-32-806/10/20 15:394672021
Benzo(b)fluoranthene ND ug/kg 06/11/20 18:27 205-99-206/10/20 15:394671881
Benzo(g,h,i)perylene ND ug/kg 06/11/20 18:27 191-24-206/10/20 15:394671831
Benzo(k)fluoranthene ND ug/kg 06/11/20 18:27 207-08-906/10/20 15:394671971
Benzoic Acid ND ug/kg 06/11/20 18:27 65-85-006/10/20 15:3923405041
Benzyl alcohol ND ug/kg 06/11/20 18:27 100-51-606/10/20 15:399342481
4-Bromophenylphenyl ether ND ug/kg 06/11/20 18:27 101-55-306/10/20 15:394671231
Butylbenzylphthalate ND ug/kg 06/11/20 18:27 85-68-706/10/20 15:394671241
4-Chloro-3-methylphenol ND ug/kg 06/11/20 18:27 59-50-706/10/20 15:399342851
4-Chloroaniline ND ug/kg 06/11/20 18:27 106-47-806/10/20 15:399342861
bis(2-Chloroethoxy)methane ND ug/kg 06/11/20 18:27 111-91-106/10/20 15:394671251
bis(2-Chloroethyl) ether ND ug/kg 06/11/20 18:27 111-44-406/10/20 15:3946799.2 1
2-Chloronaphthalene ND ug/kg 06/11/20 18:27 91-58-706/10/20 15:394671041
2-Chlorophenol ND ug/kg 06/11/20 18:27 95-57-806/10/20 15:394671091
4-Chlorophenylphenyl ether ND ug/kg 06/11/20 18:27 7005-72-306/10/20 15:394671211
Chrysene ND ug/kg 06/11/20 18:27 218-01-906/10/20 15:394671361
Dibenz(a,h)anthracene ND ug/kg 06/11/20 18:27 53-70-306/10/20 15:394671871
Dibenzofuran ND ug/kg 06/11/20 18:27 132-64-906/10/20 15:394671171
1,2-Dichlorobenzene ND ug/kg 06/11/20 18:27 95-50-106/10/20 15:394671011
1,3-Dichlorobenzene ND ug/kg 06/11/20 18:27 541-73-106/10/20 15:394671051
1,4-Dichlorobenzene ND ug/kg 06/11/20 18:27 106-46-706/10/20 15:394671031
3,3'-Dichlorobenzidine ND ug/kg 06/11/20 18:27 91-94-106/10/20 15:399343261
2,4-Dichlorophenol ND ug/kg 06/11/20 18:27 120-83-206/10/20 15:394671541
Diethylphthalate ND ug/kg 06/11/20 18:27 84-66-206/10/20 15:394671011
2,4-Dimethylphenol ND ug/kg 06/11/20 18:27 105-67-906/10/20 15:394671161
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-2(6-8)Lab ID:92481197002 Collected:06/09/20 10:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/11/20 18:27 131-11-306/10/20 15:394671061
Di-n-butylphthalate ND ug/kg 06/11/20 18:27 84-74-206/10/20 15:394671151
4,6-Dinitro-2-methylphenol ND ug/kg 06/11/20 18:27 534-52-106/10/20 15:399347531
2,4-Dinitrophenol ND ug/kg 06/11/20 18:27 51-28-506/10/20 15:39234014901
2,4-Dinitrotoluene ND ug/kg 06/11/20 18:27 121-14-206/10/20 15:394671241
2,6-Dinitrotoluene ND ug/kg 06/11/20 18:27 606-20-2 L2,v206/10/20 15:394671221
Di-n-octylphthalate ND ug/kg 06/11/20 18:27 117-84-0 v106/10/20 15:394672661
bis(2-Ethylhexyl)phthalate ND ug/kg 06/11/20 18:27 117-81-706/10/20 15:394671531
Fluoranthene ND ug/kg 06/11/20 18:27 206-44-006/10/20 15:394671411
Fluorene ND ug/kg 06/11/20 18:27 86-73-706/10/20 15:394671251
Hexachloro-1,3-butadiene ND ug/kg 06/11/20 18:27 87-68-306/10/20 15:394671141
Hexachlorobenzene ND ug/kg 06/11/20 18:27 118-74-106/10/20 15:394671191
Hexachlorocyclopentadiene ND ug/kg 06/11/20 18:27 77-47-406/10/20 15:394671871
Hexachloroethane ND ug/kg 06/11/20 18:27 67-72-106/10/20 15:394671061
Indeno(1,2,3-cd)pyrene ND ug/kg 06/11/20 18:27 193-39-506/10/20 15:394672141
Isophorone ND ug/kg 06/11/20 18:27 78-59-106/10/20 15:394671021
1-Methylnaphthalene ND ug/kg 06/11/20 18:27 90-12-006/10/20 15:394671241
2-Methylnaphthalene ND ug/kg 06/11/20 18:27 91-57-606/10/20 15:394671191
2-Methylphenol(o-Cresol)ND ug/kg 06/11/20 18:27 95-48-706/10/20 15:394671031
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/11/20 18:27 15831-10-406/10/20 15:394671181
Naphthalene ND ug/kg 06/11/20 18:27 91-20-306/10/20 15:394671121
2-Nitroaniline ND ug/kg 06/11/20 18:27 88-74-406/10/20 15:3923402351
3-Nitroaniline ND ug/kg 06/11/20 18:27 99-09-206/10/20 15:3923402481
4-Nitroaniline ND ug/kg 06/11/20 18:27 100-01-606/10/20 15:399342311
Nitrobenzene ND ug/kg 06/11/20 18:27 98-95-306/10/20 15:394671121
2-Nitrophenol ND ug/kg 06/11/20 18:27 88-75-506/10/20 15:394671441
4-Nitrophenol ND ug/kg 06/11/20 18:27 100-02-706/10/20 15:3923407451
N-Nitrosodimethylamine ND ug/kg 06/11/20 18:27 62-75-906/10/20 15:394671311
N-Nitroso-di-n-propylamine ND ug/kg 06/11/20 18:27 621-64-706/10/20 15:394671311
N-Nitrosodiphenylamine ND ug/kg 06/11/20 18:27 86-30-606/10/20 15:394671191
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/11/20 18:27 108-60-106/10/20 15:394671301
Pentachlorophenol ND ug/kg 06/11/20 18:27 87-86-506/10/20 15:399342141
Phenanthrene ND ug/kg 06/11/20 18:27 85-01-806/10/20 15:394671181
Phenol ND ug/kg 06/11/20 18:27 108-95-206/10/20 15:394671121
Pyrene ND ug/kg 06/11/20 18:27 129-00-006/10/20 15:394671291
Pyridine ND ug/kg 06/11/20 18:27 110-86-106/10/20 15:394671181
1,2,4-Trichlorobenzene ND ug/kg 06/11/20 18:27 120-82-106/10/20 15:394671071
2,4,5-Trichlorophenol ND ug/kg 06/11/20 18:27 95-95-406/10/20 15:394671211
2,4,6-Trichlorophenol ND ug/kg 06/11/20 18:27 88-06-206/10/20 15:394671171
Surrogates
Nitrobenzene-d5 (S)40 %06/11/20 18:27 4165-60-006/10/20 15:3923-110 1
2-Fluorobiphenyl (S)35 %06/11/20 18:27 321-60-806/10/20 15:3930-110 1
Terphenyl-d14 (S)37 %06/11/20 18:27 1718-51-006/10/20 15:3928-110 1
Phenol-d6 (S)43 %06/11/20 18:27 13127-88-306/10/20 15:3922-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-2(6-8)Lab ID:92481197002 Collected:06/09/20 10:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)43 %06/11/20 18:27 367-12-406/10/20 15:3913-110 1
2,4,6-Tribromophenol (S)40 %06/11/20 18:27 118-79-606/10/20 15:3927-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/15/20 19:15 67-64-106/15/20 15:0016059.7 1
Benzene ND ug/kg 06/15/20 19:15 71-43-206/15/20 15:008.0 5.6 1
Bromobenzene ND ug/kg 06/15/20 19:15 108-86-106/15/20 15:008.0 5.4 1
Bromochloromethane ND ug/kg 06/15/20 19:15 74-97-506/15/20 15:008.0 6.1 1
Bromodichloromethane ND ug/kg 06/15/20 19:15 75-27-406/15/20 15:008.0 5.2 1
Bromoform ND ug/kg 06/15/20 19:15 75-25-206/15/20 15:008.0 4.3 1
Bromomethane ND ug/kg 06/15/20 19:15 74-83-906/15/20 15:0016.0 12.6 1
2-Butanone (MEK)ND ug/kg 06/15/20 19:15 78-93-306/15/20 15:0016067.8 1
n-Butylbenzene ND ug/kg 06/15/20 19:15 104-51-806/15/20 15:008.0 4.3 1
sec-Butylbenzene ND ug/kg 06/15/20 19:15 135-98-806/15/20 15:008.0 5.1 1
tert-Butylbenzene ND ug/kg 06/15/20 19:15 98-06-606/15/20 15:008.0 4.3 1
Carbon tetrachloride ND ug/kg 06/15/20 19:15 56-23-506/15/20 15:008.0 3.6 1
Chlorobenzene ND ug/kg 06/15/20 19:15 108-90-706/15/20 15:008.0 5.2 1
Chloroethane ND ug/kg 06/15/20 19:15 75-00-306/15/20 15:0016.0 8.5 1
Chloroform ND ug/kg 06/15/20 19:15 67-66-306/15/20 15:008.0 4.0 1
Chloromethane ND ug/kg 06/15/20 19:15 74-87-306/15/20 15:0016.0 11.2 1
2-Chlorotoluene ND ug/kg 06/15/20 19:15 95-49-806/15/20 15:008.0 5.7 1
4-Chlorotoluene ND ug/kg 06/15/20 19:15 106-43-406/15/20 15:008.0 5.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/15/20 19:15 96-12-806/15/20 15:008.0 7.4 1
Dibromochloromethane ND ug/kg 06/15/20 19:15 124-48-106/15/20 15:008.0 4.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/15/20 19:15 106-93-406/15/20 15:008.0 5.6 1
Dibromomethane ND ug/kg 06/15/20 19:15 74-95-306/15/20 15:008.0 4.0 1
1,2-Dichlorobenzene ND ug/kg 06/15/20 19:15 95-50-106/15/20 15:008.0 4.7 1
1,3-Dichlorobenzene ND ug/kg 06/15/20 19:15 541-73-106/15/20 15:008.0 6.6 1
1,4-Dichlorobenzene ND ug/kg 06/15/20 19:15 106-46-706/15/20 15:008.0 6.0 1
Dichlorodifluoromethane ND ug/kg 06/15/20 19:15 75-71-806/15/20 15:0016.0 2.8 1
1,1-Dichloroethane ND ug/kg 06/15/20 19:15 75-34-306/15/20 15:008.0 3.5 1
1,2-Dichloroethane ND ug/kg 06/15/20 19:15 107-06-206/15/20 15:008.0 3.3 1
1,1-Dichloroethene ND ug/kg 06/15/20 19:15 75-35-406/15/20 15:008.0 2.5 1
cis-1,2-Dichloroethene ND ug/kg 06/15/20 19:15 156-59-206/15/20 15:008.0 4.6 1
trans-1,2-Dichloroethene ND ug/kg 06/15/20 19:15 156-60-506/15/20 15:008.0 3.5 1
1,2-Dichloropropane ND ug/kg 06/15/20 19:15 78-87-506/15/20 15:008.0 5.0 1
1,3-Dichloropropane ND ug/kg 06/15/20 19:15 142-28-906/15/20 15:008.0 5.5 1
2,2-Dichloropropane ND ug/kg 06/15/20 19:15 594-20-706/15/20 15:008.0 4.4 1
1,1-Dichloropropene ND ug/kg 06/15/20 19:15 563-58-606/15/20 15:008.0 3.8 1
cis-1,3-Dichloropropene ND ug/kg 06/15/20 19:15 10061-01-506/15/20 15:008.0 5.2 1
trans-1,3-Dichloropropene ND ug/kg 06/15/20 19:15 10061-02-606/15/20 15:008.0 6.8 1
Diisopropyl ether ND ug/kg 06/15/20 19:15 108-20-306/15/20 15:008.0 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-2(6-8)Lab ID:92481197002 Collected:06/09/20 10:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/15/20 19:15 100-41-406/15/20 15:008.0 7.5 1
Hexachloro-1,3-butadiene ND ug/kg 06/15/20 19:15 87-68-306/15/20 15:008.0 7.6 1
2-Hexanone ND ug/kg 06/15/20 19:15 591-78-606/15/20 15:0080.0 15.9 1
Isopropylbenzene (Cumene)ND ug/kg 06/15/20 19:15 98-82-806/15/20 15:008.0 5.1 1
p-Isopropyltoluene ND ug/kg 06/15/20 19:15 99-87-606/15/20 15:008.0 4.4 1
Methylene Chloride ND ug/kg 06/15/20 19:15 75-09-206/15/20 15:0032.0 11.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/15/20 19:15 108-10-106/15/20 15:0080.0 67.7 1
Methyl-tert-butyl ether ND ug/kg 06/15/20 19:15 1634-04-406/15/20 15:008.0 5.1 1
Naphthalene ND ug/kg 06/15/20 19:15 91-20-306/15/20 15:008.0 4.5 1
n-Propylbenzene ND ug/kg 06/15/20 19:15 103-65-106/15/20 15:008.0 5.5 1
Styrene ND ug/kg 06/15/20 19:15 100-42-506/15/20 15:008.0 3.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/15/20 19:15 630-20-606/15/20 15:008.0 5.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/15/20 19:15 79-34-506/15/20 15:008.0 7.1 1
Tetrachloroethene ND ug/kg 06/15/20 19:15 127-18-406/15/20 15:008.0 4.0 1
Toluene ND ug/kg 06/15/20 19:15 108-88-306/15/20 15:008.0 4.6 1
1,2,3-Trichlorobenzene ND ug/kg 06/15/20 19:15 87-61-606/15/20 15:008.0 4.9 1
1,2,4-Trichlorobenzene ND ug/kg 06/15/20 19:15 120-82-106/15/20 15:008.0 4.5 1
1,1,1-Trichloroethane ND ug/kg 06/15/20 19:15 71-55-606/15/20 15:008.0 3.2 1
1,1,2-Trichloroethane ND ug/kg 06/15/20 19:15 79-00-506/15/20 15:008.0 6.0 1
Trichloroethene ND ug/kg 06/15/20 19:15 79-01-606/15/20 15:008.0 5.0 1
Trichlorofluoromethane ND ug/kg 06/15/20 19:15 75-69-406/15/20 15:008.0 2.0 1
1,2,3-Trichloropropane ND ug/kg 06/15/20 19:15 96-18-406/15/20 15:008.0 6.5 1
1,2,4-Trimethylbenzene ND ug/kg 06/15/20 19:15 95-63-606/15/20 15:008.0 5.8 1
1,3,5-Trimethylbenzene ND ug/kg 06/15/20 19:15 108-67-806/15/20 15:008.0 4.8 1
Vinyl acetate ND ug/kg 06/15/20 19:15 108-05-406/15/20 15:0080.0 6.9 1
Vinyl chloride ND ug/kg 06/15/20 19:15 75-01-406/15/20 15:0016.0 3.1 1
Xylene (Total)ND ug/kg 06/15/20 19:15 1330-20-706/15/20 15:0016.0 4.6 1
m&p-Xylene ND ug/kg 06/15/20 19:15 179601-23-106/15/20 15:0016.0 12.3 1
o-Xylene ND ug/kg 06/15/20 19:15 95-47-606/15/20 15:008.0 4.6 1
Surrogates
Toluene-d8 (S)100 %06/15/20 19:15 2037-26-506/15/20 15:0070-130 1
4-Bromofluorobenzene (S)100 %06/15/20 19:15 460-00-406/15/20 15:0070-130 1
1,2-Dichloroethane-d4 (S)104 %06/15/20 19:15 17060-07-006/15/20 15:0070-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.7 %06/10/20 16:550.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 70.5 %06/14/20 00:3206/14/20 00:191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-2(6-8)Lab ID:92481197002 Collected:06/09/20 10:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 06/16/20 20:05 18540-29-906/16/20 12:301.42 0.362 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-3(2-4)Lab ID:92481197003 Collected:06/09/20 10:45 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.820J mg/kg 06/14/20 19:34 7440-38-2 J06/13/20 08:241.47 0.620 5
Barium 183 mg/kg 06/14/20 19:34 7440-39-306/13/20 08:243.67 1.84 5
Cadmium ND mg/kg 06/14/20 19:34 7440-43-906/13/20 08:241.47 0.596 5
Chromium 9.66 mg/kg 06/14/20 19:34 7440-47-306/13/20 08:247.35 3.29 5
Lead 4.16 mg/kg 06/14/20 19:34 7439-92-106/13/20 08:242.94 1.47 5
Selenium ND mg/kg 06/14/20 19:34 7782-49-206/13/20 08:243.67 1.48 5
Silver ND mg/kg 06/14/20 19:34 7440-22-406/13/20 08:240.735 0.313 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 06/12/20 09:05 7439-97-606/11/20 20:250.0588 0.0264 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/11/20 18:57 83-32-906/10/20 15:394701211
Acenaphthylene ND ug/kg 06/11/20 18:57 208-96-806/10/20 15:394701111
Aniline ND ug/kg 06/11/20 18:57 62-53-306/10/20 15:394701061
Anthracene ND ug/kg 06/11/20 18:57 120-12-706/10/20 15:394701221
Benzo(a)anthracene ND ug/kg 06/11/20 18:57 56-55-306/10/20 15:394701501
Benzo(a)pyrene ND ug/kg 06/11/20 18:57 50-32-806/10/20 15:394702041
Benzo(b)fluoranthene ND ug/kg 06/11/20 18:57 205-99-206/10/20 15:394701901
Benzo(g,h,i)perylene ND ug/kg 06/11/20 18:57 191-24-206/10/20 15:394701841
Benzo(k)fluoranthene ND ug/kg 06/11/20 18:57 207-08-906/10/20 15:394701981
Benzoic Acid ND ug/kg 06/11/20 18:57 65-85-006/10/20 15:3923505071
Benzyl alcohol ND ug/kg 06/11/20 18:57 100-51-606/10/20 15:399412491
4-Bromophenylphenyl ether ND ug/kg 06/11/20 18:57 101-55-306/10/20 15:394701231
Butylbenzylphthalate ND ug/kg 06/11/20 18:57 85-68-706/10/20 15:394701251
4-Chloro-3-methylphenol ND ug/kg 06/11/20 18:57 59-50-706/10/20 15:399412861
4-Chloroaniline ND ug/kg 06/11/20 18:57 106-47-806/10/20 15:399412881
bis(2-Chloroethoxy)methane ND ug/kg 06/11/20 18:57 111-91-106/10/20 15:394701261
bis(2-Chloroethyl) ether ND ug/kg 06/11/20 18:57 111-44-406/10/20 15:3947099.9 1
2-Chloronaphthalene ND ug/kg 06/11/20 18:57 91-58-706/10/20 15:394701051
2-Chlorophenol ND ug/kg 06/11/20 18:57 95-57-806/10/20 15:394701091
4-Chlorophenylphenyl ether ND ug/kg 06/11/20 18:57 7005-72-306/10/20 15:394701221
Chrysene ND ug/kg 06/11/20 18:57 218-01-906/10/20 15:394701371
Dibenz(a,h)anthracene ND ug/kg 06/11/20 18:57 53-70-306/10/20 15:394701881
Dibenzofuran ND ug/kg 06/11/20 18:57 132-64-906/10/20 15:394701181
1,2-Dichlorobenzene ND ug/kg 06/11/20 18:57 95-50-106/10/20 15:394701021
1,3-Dichlorobenzene ND ug/kg 06/11/20 18:57 541-73-106/10/20 15:394701061
1,4-Dichlorobenzene ND ug/kg 06/11/20 18:57 106-46-706/10/20 15:394701031
3,3'-Dichlorobenzidine ND ug/kg 06/11/20 18:57 91-94-106/10/20 15:399413281
2,4-Dichlorophenol ND ug/kg 06/11/20 18:57 120-83-206/10/20 15:394701551
Diethylphthalate ND ug/kg 06/11/20 18:57 84-66-206/10/20 15:394701021
2,4-Dimethylphenol ND ug/kg 06/11/20 18:57 105-67-906/10/20 15:394701171
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-3(2-4)Lab ID:92481197003 Collected:06/09/20 10:45 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/11/20 18:57 131-11-306/10/20 15:394701061
Di-n-butylphthalate ND ug/kg 06/11/20 18:57 84-74-206/10/20 15:394701161
4,6-Dinitro-2-methylphenol ND ug/kg 06/11/20 18:57 534-52-106/10/20 15:399417581
2,4-Dinitrophenol ND ug/kg 06/11/20 18:57 51-28-506/10/20 15:39235015001
2,4-Dinitrotoluene ND ug/kg 06/11/20 18:57 121-14-206/10/20 15:394701251
2,6-Dinitrotoluene ND ug/kg 06/11/20 18:57 606-20-2 L2,v206/10/20 15:394701231
Di-n-octylphthalate ND ug/kg 06/11/20 18:57 117-84-0 v106/10/20 15:394702681
bis(2-Ethylhexyl)phthalate ND ug/kg 06/11/20 18:57 117-81-706/10/20 15:394701541
Fluoranthene ND ug/kg 06/11/20 18:57 206-44-006/10/20 15:394701421
Fluorene ND ug/kg 06/11/20 18:57 86-73-706/10/20 15:394701261
Hexachloro-1,3-butadiene ND ug/kg 06/11/20 18:57 87-68-306/10/20 15:394701141
Hexachlorobenzene ND ug/kg 06/11/20 18:57 118-74-106/10/20 15:394701191
Hexachlorocyclopentadiene ND ug/kg 06/11/20 18:57 77-47-406/10/20 15:394701881
Hexachloroethane ND ug/kg 06/11/20 18:57 67-72-106/10/20 15:394701071
Indeno(1,2,3-cd)pyrene ND ug/kg 06/11/20 18:57 193-39-506/10/20 15:394702151
Isophorone ND ug/kg 06/11/20 18:57 78-59-106/10/20 15:394701021
1-Methylnaphthalene ND ug/kg 06/11/20 18:57 90-12-006/10/20 15:394701251
2-Methylnaphthalene ND ug/kg 06/11/20 18:57 91-57-606/10/20 15:394701201
2-Methylphenol(o-Cresol)ND ug/kg 06/11/20 18:57 95-48-706/10/20 15:394701041
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/11/20 18:57 15831-10-406/10/20 15:394701181
Naphthalene ND ug/kg 06/11/20 18:57 91-20-306/10/20 15:394701131
2-Nitroaniline ND ug/kg 06/11/20 18:57 88-74-406/10/20 15:3923502371
3-Nitroaniline ND ug/kg 06/11/20 18:57 99-09-206/10/20 15:3923502491
4-Nitroaniline ND ug/kg 06/11/20 18:57 100-01-606/10/20 15:399412321
Nitrobenzene ND ug/kg 06/11/20 18:57 98-95-306/10/20 15:394701121
2-Nitrophenol ND ug/kg 06/11/20 18:57 88-75-506/10/20 15:394701451
4-Nitrophenol ND ug/kg 06/11/20 18:57 100-02-706/10/20 15:3923507501
N-Nitrosodimethylamine ND ug/kg 06/11/20 18:57 62-75-906/10/20 15:394701321
N-Nitroso-di-n-propylamine ND ug/kg 06/11/20 18:57 621-64-706/10/20 15:394701321
N-Nitrosodiphenylamine ND ug/kg 06/11/20 18:57 86-30-606/10/20 15:394701201
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/11/20 18:57 108-60-106/10/20 15:394701311
Pentachlorophenol ND ug/kg 06/11/20 18:57 87-86-506/10/20 15:399412151
Phenanthrene ND ug/kg 06/11/20 18:57 85-01-806/10/20 15:394701181
Phenol ND ug/kg 06/11/20 18:57 108-95-206/10/20 15:394701121
Pyrene ND ug/kg 06/11/20 18:57 129-00-006/10/20 15:394701291
Pyridine ND ug/kg 06/11/20 18:57 110-86-106/10/20 15:394701191
1,2,4-Trichlorobenzene ND ug/kg 06/11/20 18:57 120-82-106/10/20 15:394701081
2,4,5-Trichlorophenol ND ug/kg 06/11/20 18:57 95-95-406/10/20 15:394701221
2,4,6-Trichlorophenol ND ug/kg 06/11/20 18:57 88-06-206/10/20 15:394701181
Surrogates
Nitrobenzene-d5 (S)55 %06/11/20 18:57 4165-60-006/10/20 15:3923-110 1
2-Fluorobiphenyl (S)44 %06/11/20 18:57 321-60-806/10/20 15:3930-110 1
Terphenyl-d14 (S)47 %06/11/20 18:57 1718-51-006/10/20 15:3928-110 1
Phenol-d6 (S)58 %06/11/20 18:57 13127-88-306/10/20 15:3922-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-3(2-4)Lab ID:92481197003 Collected:06/09/20 10:45 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)59 %06/11/20 18:57 367-12-406/10/20 15:3913-110 1
2,4,6-Tribromophenol (S)58 %06/11/20 18:57 118-79-606/10/20 15:3927-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/15/20 19:33 67-64-106/15/20 15:0012948.2 1
Benzene ND ug/kg 06/15/20 19:33 71-43-206/15/20 15:006.5 4.6 1
Bromobenzene ND ug/kg 06/15/20 19:33 108-86-106/15/20 15:006.5 4.4 1
Bromochloromethane ND ug/kg 06/15/20 19:33 74-97-506/15/20 15:006.5 4.9 1
Bromodichloromethane ND ug/kg 06/15/20 19:33 75-27-406/15/20 15:006.5 4.2 1
Bromoform ND ug/kg 06/15/20 19:33 75-25-206/15/20 15:006.5 3.5 1
Bromomethane ND ug/kg 06/15/20 19:33 74-83-906/15/20 15:0012.9 10.2 1
2-Butanone (MEK)ND ug/kg 06/15/20 19:33 78-93-306/15/20 15:0012954.8 1
n-Butylbenzene 49.8 ug/kg 06/15/20 19:33 104-51-806/15/20 15:006.5 3.5 1
sec-Butylbenzene 39.5 ug/kg 06/15/20 19:33 135-98-806/15/20 15:006.5 4.1 1
tert-Butylbenzene ND ug/kg 06/15/20 19:33 98-06-606/15/20 15:006.5 3.5 1
Carbon tetrachloride ND ug/kg 06/15/20 19:33 56-23-506/15/20 15:006.5 2.9 1
Chlorobenzene ND ug/kg 06/15/20 19:33 108-90-706/15/20 15:006.5 4.2 1
Chloroethane ND ug/kg 06/15/20 19:33 75-00-306/15/20 15:0012.9 6.8 1
Chloroform ND ug/kg 06/15/20 19:33 67-66-306/15/20 15:006.5 3.2 1
Chloromethane ND ug/kg 06/15/20 19:33 74-87-306/15/20 15:0012.9 9.1 1
2-Chlorotoluene ND ug/kg 06/15/20 19:33 95-49-806/15/20 15:006.5 4.6 1
4-Chlorotoluene ND ug/kg 06/15/20 19:33 106-43-406/15/20 15:006.5 4.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/15/20 19:33 96-12-806/15/20 15:006.5 6.0 1
Dibromochloromethane ND ug/kg 06/15/20 19:33 124-48-106/15/20 15:006.5 3.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/15/20 19:33 106-93-406/15/20 15:006.5 4.6 1
Dibromomethane ND ug/kg 06/15/20 19:33 74-95-306/15/20 15:006.5 3.2 1
1,2-Dichlorobenzene ND ug/kg 06/15/20 19:33 95-50-106/15/20 15:006.5 3.8 1
1,3-Dichlorobenzene ND ug/kg 06/15/20 19:33 541-73-106/15/20 15:006.5 5.3 1
1,4-Dichlorobenzene ND ug/kg 06/15/20 19:33 106-46-706/15/20 15:006.5 4.8 1
Dichlorodifluoromethane ND ug/kg 06/15/20 19:33 75-71-806/15/20 15:0012.9 2.2 1
1,1-Dichloroethane ND ug/kg 06/15/20 19:33 75-34-306/15/20 15:006.5 2.8 1
1,2-Dichloroethane ND ug/kg 06/15/20 19:33 107-06-206/15/20 15:006.5 2.6 1
1,1-Dichloroethene ND ug/kg 06/15/20 19:33 75-35-406/15/20 15:006.5 2.0 1
cis-1,2-Dichloroethene ND ug/kg 06/15/20 19:33 156-59-206/15/20 15:006.5 3.7 1
trans-1,2-Dichloroethene ND ug/kg 06/15/20 19:33 156-60-506/15/20 15:006.5 2.8 1
1,2-Dichloropropane ND ug/kg 06/15/20 19:33 78-87-506/15/20 15:006.5 4.0 1
1,3-Dichloropropane ND ug/kg 06/15/20 19:33 142-28-906/15/20 15:006.5 4.5 1
2,2-Dichloropropane ND ug/kg 06/15/20 19:33 594-20-706/15/20 15:006.5 3.6 1
1,1-Dichloropropene ND ug/kg 06/15/20 19:33 563-58-606/15/20 15:006.5 3.1 1
cis-1,3-Dichloropropene ND ug/kg 06/15/20 19:33 10061-01-506/15/20 15:006.5 4.2 1
trans-1,3-Dichloropropene ND ug/kg 06/15/20 19:33 10061-02-606/15/20 15:006.5 5.5 1
Diisopropyl ether ND ug/kg 06/15/20 19:33 108-20-306/15/20 15:006.5 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-3(2-4)Lab ID:92481197003 Collected:06/09/20 10:45 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/15/20 19:33 100-41-406/15/20 15:006.5 6.0 1
Hexachloro-1,3-butadiene ND ug/kg 06/15/20 19:33 87-68-306/15/20 15:006.5 6.1 1
2-Hexanone ND ug/kg 06/15/20 19:33 591-78-606/15/20 15:0064.6 12.8 1
Isopropylbenzene (Cumene)ND ug/kg 06/15/20 19:33 98-82-806/15/20 15:006.5 4.1 1
p-Isopropyltoluene ND ug/kg 06/15/20 19:33 99-87-606/15/20 15:006.5 3.6 1
Methylene Chloride ND ug/kg 06/15/20 19:33 75-09-206/15/20 15:0025.8 9.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/15/20 19:33 108-10-106/15/20 15:0064.6 54.7 1
Methyl-tert-butyl ether ND ug/kg 06/15/20 19:33 1634-04-406/15/20 15:006.5 4.1 1
Naphthalene 14.0 ug/kg 06/15/20 19:33 91-20-306/15/20 15:006.5 3.6 1
n-Propylbenzene ND ug/kg 06/15/20 19:33 103-65-106/15/20 15:006.5 4.5 1
Styrene ND ug/kg 06/15/20 19:33 100-42-506/15/20 15:006.5 3.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/15/20 19:33 630-20-606/15/20 15:006.5 4.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/15/20 19:33 79-34-506/15/20 15:006.5 5.7 1
Tetrachloroethene ND ug/kg 06/15/20 19:33 127-18-406/15/20 15:006.5 3.2 1
Toluene ND ug/kg 06/15/20 19:33 108-88-306/15/20 15:006.5 3.7 1
1,2,3-Trichlorobenzene ND ug/kg 06/15/20 19:33 87-61-606/15/20 15:006.5 4.0 1
1,2,4-Trichlorobenzene ND ug/kg 06/15/20 19:33 120-82-106/15/20 15:006.5 3.6 1
1,1,1-Trichloroethane ND ug/kg 06/15/20 19:33 71-55-606/15/20 15:006.5 2.6 1
1,1,2-Trichloroethane ND ug/kg 06/15/20 19:33 79-00-506/15/20 15:006.5 4.8 1
Trichloroethene ND ug/kg 06/15/20 19:33 79-01-606/15/20 15:006.5 4.0 1
Trichlorofluoromethane ND ug/kg 06/15/20 19:33 75-69-406/15/20 15:006.5 1.6 1
1,2,3-Trichloropropane ND ug/kg 06/15/20 19:33 96-18-406/15/20 15:006.5 5.3 1
1,2,4-Trimethylbenzene 105 ug/kg 06/15/20 19:33 95-63-606/15/20 15:006.5 4.7 1
1,3,5-Trimethylbenzene 78.3 ug/kg 06/15/20 19:33 108-67-806/15/20 15:006.5 3.9 1
Vinyl acetate ND ug/kg 06/15/20 19:33 108-05-406/15/20 15:0064.6 5.6 1
Vinyl chloride ND ug/kg 06/15/20 19:33 75-01-406/15/20 15:0012.9 2.5 1
Xylene (Total)ND ug/kg 06/15/20 19:33 1330-20-706/15/20 15:0012.9 3.7 1
m&p-Xylene ND ug/kg 06/15/20 19:33 179601-23-106/15/20 15:0012.9 9.9 1
o-Xylene ND ug/kg 06/15/20 19:33 95-47-606/15/20 15:006.5 3.7 1
Surrogates
Toluene-d8 (S)99 %06/15/20 19:33 2037-26-506/15/20 15:0070-130 1
4-Bromofluorobenzene (S)102 %06/15/20 19:33 460-00-406/15/20 15:0070-130 1
1,2-Dichloroethane-d4 (S)102 %06/15/20 19:33 17060-07-006/15/20 15:0070-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.5 %06/10/20 16:550.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 68.1 %06/14/20 00:3206/14/20 00:191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-3(2-4)Lab ID:92481197003 Collected:06/09/20 10:45 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 06/16/20 20:10 18540-29-906/16/20 12:301.47 0.375 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-4(6-8)Lab ID:92481197004 Collected:06/09/20 11:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.745J mg/kg 06/14/20 19:37 7440-38-2 J06/13/20 08:241.33 0.561 5
Barium 156 mg/kg 06/14/20 19:37 7440-39-306/13/20 08:243.32 1.66 5
Cadmium ND mg/kg 06/14/20 19:37 7440-43-906/13/20 08:241.33 0.539 5
Chromium 22.8 mg/kg 06/14/20 19:37 7440-47-306/13/20 08:246.64 2.98 5
Lead 4.06 mg/kg 06/14/20 19:37 7439-92-106/13/20 08:242.66 1.33 5
Selenium ND mg/kg 06/14/20 19:37 7782-49-206/13/20 08:243.32 1.34 5
Silver ND mg/kg 06/14/20 19:37 7440-22-406/13/20 08:240.664 0.283 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 06/12/20 09:07 7439-97-606/11/20 20:250.0531 0.0239 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/12/20 08:53 83-32-906/10/20 15:394131061
Acenaphthylene ND ug/kg 06/12/20 08:53 208-96-806/10/20 15:3941397.8 1
Aniline ND ug/kg 06/12/20 08:53 62-53-306/10/20 15:3941392.7 1
Anthracene ND ug/kg 06/12/20 08:53 120-12-706/10/20 15:394131071
Benzo(a)anthracene ND ug/kg 06/12/20 08:53 56-55-306/10/20 15:394131311
Benzo(a)pyrene ND ug/kg 06/12/20 08:53 50-32-806/10/20 15:394131791
Benzo(b)fluoranthene ND ug/kg 06/12/20 08:53 205-99-206/10/20 15:394131661
Benzo(g,h,i)perylene ND ug/kg 06/12/20 08:53 191-24-206/10/20 15:394131611
Benzo(k)fluoranthene ND ug/kg 06/12/20 08:53 207-08-906/10/20 15:394131741
Benzoic Acid ND ug/kg 06/12/20 08:53 65-85-006/10/20 15:3920704461
Benzyl alcohol ND ug/kg 06/12/20 08:53 100-51-606/10/20 15:398262191
4-Bromophenylphenyl ether ND ug/kg 06/12/20 08:53 101-55-306/10/20 15:394131081
Butylbenzylphthalate ND ug/kg 06/12/20 08:53 85-68-706/10/20 15:394131101
4-Chloro-3-methylphenol ND ug/kg 06/12/20 08:53 59-50-706/10/20 15:398262521
4-Chloroaniline ND ug/kg 06/12/20 08:53 106-47-806/10/20 15:398262531
bis(2-Chloroethoxy)methane ND ug/kg 06/12/20 08:53 111-91-106/10/20 15:394131101
bis(2-Chloroethyl) ether ND ug/kg 06/12/20 08:53 111-44-406/10/20 15:3941387.7 1
2-Chloronaphthalene ND ug/kg 06/12/20 08:53 91-58-706/10/20 15:3941392.0 1
2-Chlorophenol ND ug/kg 06/12/20 08:53 95-57-806/10/20 15:3941396.1 1
4-Chlorophenylphenyl ether ND ug/kg 06/12/20 08:53 7005-72-306/10/20 15:394131071
Chrysene ND ug/kg 06/12/20 08:53 218-01-906/10/20 15:394131201
Dibenz(a,h)anthracene ND ug/kg 06/12/20 08:53 53-70-306/10/20 15:394131651
Dibenzofuran ND ug/kg 06/12/20 08:53 132-64-906/10/20 15:394131031
1,2-Dichlorobenzene ND ug/kg 06/12/20 08:53 95-50-106/10/20 15:3941389.4 1
1,3-Dichlorobenzene ND ug/kg 06/12/20 08:53 541-73-106/10/20 15:3941393.0 1
1,4-Dichlorobenzene ND ug/kg 06/12/20 08:53 106-46-706/10/20 15:3941390.9 1
3,3'-Dichlorobenzidine ND ug/kg 06/12/20 08:53 91-94-106/10/20 15:398262881
2,4-Dichlorophenol ND ug/kg 06/12/20 08:53 120-83-206/10/20 15:394131361
Diethylphthalate ND ug/kg 06/12/20 08:53 84-66-206/10/20 15:3941389.6 1
2,4-Dimethylphenol ND ug/kg 06/12/20 08:53 105-67-906/10/20 15:394131031
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-4(6-8)Lab ID:92481197004 Collected:06/09/20 11:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/12/20 08:53 131-11-306/10/20 15:3941393.4 1
Di-n-butylphthalate ND ug/kg 06/12/20 08:53 84-74-206/10/20 15:394131021
4,6-Dinitro-2-methylphenol ND ug/kg 06/12/20 08:53 534-52-106/10/20 15:398266661
2,4-Dinitrophenol ND ug/kg 06/12/20 08:53 51-28-506/10/20 15:39207013201
2,4-Dinitrotoluene ND ug/kg 06/12/20 08:53 121-14-206/10/20 15:394131091
2,6-Dinitrotoluene ND ug/kg 06/12/20 08:53 606-20-2 L206/10/20 15:394131081
Di-n-octylphthalate ND ug/kg 06/12/20 08:53 117-84-006/10/20 15:394132351
bis(2-Ethylhexyl)phthalate ND ug/kg 06/12/20 08:53 117-81-706/10/20 15:394131351
Fluoranthene ND ug/kg 06/12/20 08:53 206-44-006/10/20 15:394131251
Fluorene ND ug/kg 06/12/20 08:53 86-73-706/10/20 15:394131111
Hexachloro-1,3-butadiene ND ug/kg 06/12/20 08:53 87-68-306/10/20 15:394131001
Hexachlorobenzene ND ug/kg 06/12/20 08:53 118-74-106/10/20 15:394131051
Hexachlorocyclopentadiene ND ug/kg 06/12/20 08:53 77-47-406/10/20 15:394131651
Hexachloroethane ND ug/kg 06/12/20 08:53 67-72-106/10/20 15:3941394.1 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/12/20 08:53 193-39-506/10/20 15:394131891
Isophorone ND ug/kg 06/12/20 08:53 78-59-106/10/20 15:3941389.7 1
1-Methylnaphthalene ND ug/kg 06/12/20 08:53 90-12-006/10/20 15:394131101
2-Methylnaphthalene ND ug/kg 06/12/20 08:53 91-57-606/10/20 15:394131051
2-Methylphenol(o-Cresol)ND ug/kg 06/12/20 08:53 95-48-706/10/20 15:3941391.5 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/12/20 08:53 15831-10-406/10/20 15:394131041
Naphthalene ND ug/kg 06/12/20 08:53 91-20-306/10/20 15:3941398.9 1
2-Nitroaniline ND ug/kg 06/12/20 08:53 88-74-406/10/20 15:3920702081
3-Nitroaniline ND ug/kg 06/12/20 08:53 99-09-206/10/20 15:3920702191
4-Nitroaniline ND ug/kg 06/12/20 08:53 100-01-606/10/20 15:398262041
Nitrobenzene ND ug/kg 06/12/20 08:53 98-95-306/10/20 15:3941398.6 1
2-Nitrophenol ND ug/kg 06/12/20 08:53 88-75-506/10/20 15:394131281
4-Nitrophenol ND ug/kg 06/12/20 08:53 100-02-706/10/20 15:3920706581
N-Nitrosodimethylamine ND ug/kg 06/12/20 08:53 62-75-906/10/20 15:394131161
N-Nitroso-di-n-propylamine ND ug/kg 06/12/20 08:53 621-64-706/10/20 15:394131161
N-Nitrosodiphenylamine ND ug/kg 06/12/20 08:53 86-30-606/10/20 15:394131051
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/12/20 08:53 108-60-106/10/20 15:394131151
Pentachlorophenol ND ug/kg 06/12/20 08:53 87-86-506/10/20 15:398261891
Phenanthrene ND ug/kg 06/12/20 08:53 85-01-806/10/20 15:394131041
Phenol ND ug/kg 06/12/20 08:53 108-95-206/10/20 15:3941398.6 1
Pyrene ND ug/kg 06/12/20 08:53 129-00-006/10/20 15:394131141
Pyridine ND ug/kg 06/12/20 08:53 110-86-106/10/20 15:394131051
1,2,4-Trichlorobenzene ND ug/kg 06/12/20 08:53 120-82-106/10/20 15:3941394.6 1
2,4,5-Trichlorophenol ND ug/kg 06/12/20 08:53 95-95-406/10/20 15:394131071
2,4,6-Trichlorophenol ND ug/kg 06/12/20 08:53 88-06-206/10/20 15:394131041
Surrogates
Nitrobenzene-d5 (S)40 %06/12/20 08:53 4165-60-006/10/20 15:3923-110 1
2-Fluorobiphenyl (S)55 %06/12/20 08:53 321-60-806/10/20 15:3930-110 1
Terphenyl-d14 (S)62 %06/12/20 08:53 1718-51-006/10/20 15:3928-110 1
Phenol-d6 (S)63 %06/12/20 08:53 13127-88-306/10/20 15:3922-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-4(6-8)Lab ID:92481197004 Collected:06/09/20 11:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)69 %06/12/20 08:53 367-12-406/10/20 15:3913-110 1
2,4,6-Tribromophenol (S)69 %06/12/20 08:53 118-79-606/10/20 15:3927-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/15/20 19:51 67-64-106/15/20 15:0093.4 34.8 1
Benzene ND ug/kg 06/15/20 19:51 71-43-206/15/20 15:004.7 3.3 1
Bromobenzene ND ug/kg 06/15/20 19:51 108-86-106/15/20 15:004.7 3.2 1
Bromochloromethane ND ug/kg 06/15/20 19:51 74-97-506/15/20 15:004.7 3.5 1
Bromodichloromethane ND ug/kg 06/15/20 19:51 75-27-406/15/20 15:004.7 3.1 1
Bromoform ND ug/kg 06/15/20 19:51 75-25-206/15/20 15:004.7 2.5 1
Bromomethane ND ug/kg 06/15/20 19:51 74-83-906/15/20 15:009.3 7.3 1
2-Butanone (MEK)ND ug/kg 06/15/20 19:51 78-93-306/15/20 15:0093.4 39.6 1
n-Butylbenzene ND ug/kg 06/15/20 19:51 104-51-806/15/20 15:004.7 2.5 1
sec-Butylbenzene ND ug/kg 06/15/20 19:51 135-98-806/15/20 15:004.7 3.0 1
tert-Butylbenzene ND ug/kg 06/15/20 19:51 98-06-606/15/20 15:004.7 2.5 1
Carbon tetrachloride ND ug/kg 06/15/20 19:51 56-23-506/15/20 15:004.7 2.1 1
Chlorobenzene ND ug/kg 06/15/20 19:51 108-90-706/15/20 15:004.7 3.0 1
Chloroethane ND ug/kg 06/15/20 19:51 75-00-306/15/20 15:009.3 4.9 1
Chloroform ND ug/kg 06/15/20 19:51 67-66-306/15/20 15:004.7 2.3 1
Chloromethane ND ug/kg 06/15/20 19:51 74-87-306/15/20 15:009.3 6.6 1
2-Chlorotoluene ND ug/kg 06/15/20 19:51 95-49-806/15/20 15:004.7 3.3 1
4-Chlorotoluene ND ug/kg 06/15/20 19:51 106-43-406/15/20 15:004.7 3.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/15/20 19:51 96-12-806/15/20 15:004.7 4.3 1
Dibromochloromethane ND ug/kg 06/15/20 19:51 124-48-106/15/20 15:004.7 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 06/15/20 19:51 106-93-406/15/20 15:004.7 3.3 1
Dibromomethane ND ug/kg 06/15/20 19:51 74-95-306/15/20 15:004.7 2.3 1
1,2-Dichlorobenzene ND ug/kg 06/15/20 19:51 95-50-106/15/20 15:004.7 2.8 1
1,3-Dichlorobenzene ND ug/kg 06/15/20 19:51 541-73-106/15/20 15:004.7 3.9 1
1,4-Dichlorobenzene ND ug/kg 06/15/20 19:51 106-46-706/15/20 15:004.7 3.5 1
Dichlorodifluoromethane ND ug/kg 06/15/20 19:51 75-71-806/15/20 15:009.3 1.6 1
1,1-Dichloroethane ND ug/kg 06/15/20 19:51 75-34-306/15/20 15:004.7 2.1 1
1,2-Dichloroethane ND ug/kg 06/15/20 19:51 107-06-206/15/20 15:004.7 1.9 1
1,1-Dichloroethene ND ug/kg 06/15/20 19:51 75-35-406/15/20 15:004.7 1.5 1
cis-1,2-Dichloroethene ND ug/kg 06/15/20 19:51 156-59-206/15/20 15:004.7 2.7 1
trans-1,2-Dichloroethene ND ug/kg 06/15/20 19:51 156-60-506/15/20 15:004.7 2.0 1
1,2-Dichloropropane ND ug/kg 06/15/20 19:51 78-87-506/15/20 15:004.7 2.9 1
1,3-Dichloropropane ND ug/kg 06/15/20 19:51 142-28-906/15/20 15:004.7 3.2 1
2,2-Dichloropropane ND ug/kg 06/15/20 19:51 594-20-706/15/20 15:004.7 2.6 1
1,1-Dichloropropene ND ug/kg 06/15/20 19:51 563-58-606/15/20 15:004.7 2.2 1
cis-1,3-Dichloropropene ND ug/kg 06/15/20 19:51 10061-01-506/15/20 15:004.7 3.0 1
trans-1,3-Dichloropropene ND ug/kg 06/15/20 19:51 10061-02-606/15/20 15:004.7 3.9 1
Diisopropyl ether ND ug/kg 06/15/20 19:51 108-20-306/15/20 15:004.7 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-4(6-8)Lab ID:92481197004 Collected:06/09/20 11:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/15/20 19:51 100-41-406/15/20 15:004.7 4.4 1
Hexachloro-1,3-butadiene ND ug/kg 06/15/20 19:51 87-68-306/15/20 15:004.7 4.4 1
2-Hexanone ND ug/kg 06/15/20 19:51 591-78-606/15/20 15:0046.7 9.3 1
Isopropylbenzene (Cumene)ND ug/kg 06/15/20 19:51 98-82-806/15/20 15:004.7 3.0 1
p-Isopropyltoluene ND ug/kg 06/15/20 19:51 99-87-606/15/20 15:004.7 2.6 1
Methylene Chloride ND ug/kg 06/15/20 19:51 75-09-206/15/20 15:0018.7 6.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/15/20 19:51 108-10-106/15/20 15:0046.7 39.5 1
Methyl-tert-butyl ether ND ug/kg 06/15/20 19:51 1634-04-406/15/20 15:004.7 3.0 1
Naphthalene ND ug/kg 06/15/20 19:51 91-20-306/15/20 15:004.7 2.6 1
n-Propylbenzene ND ug/kg 06/15/20 19:51 103-65-106/15/20 15:004.7 3.2 1
Styrene ND ug/kg 06/15/20 19:51 100-42-506/15/20 15:004.7 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/15/20 19:51 630-20-606/15/20 15:004.7 3.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/15/20 19:51 79-34-506/15/20 15:004.7 4.1 1
Tetrachloroethene ND ug/kg 06/15/20 19:51 127-18-406/15/20 15:004.7 2.3 1
Toluene ND ug/kg 06/15/20 19:51 108-88-306/15/20 15:004.7 2.7 1
1,2,3-Trichlorobenzene ND ug/kg 06/15/20 19:51 87-61-606/15/20 15:004.7 2.9 1
1,2,4-Trichlorobenzene ND ug/kg 06/15/20 19:51 120-82-106/15/20 15:004.7 2.6 1
1,1,1-Trichloroethane ND ug/kg 06/15/20 19:51 71-55-606/15/20 15:004.7 1.9 1
1,1,2-Trichloroethane ND ug/kg 06/15/20 19:51 79-00-506/15/20 15:004.7 3.5 1
Trichloroethene ND ug/kg 06/15/20 19:51 79-01-606/15/20 15:004.7 2.9 1
Trichlorofluoromethane ND ug/kg 06/15/20 19:51 75-69-406/15/20 15:004.7 1.2 1
1,2,3-Trichloropropane ND ug/kg 06/15/20 19:51 96-18-406/15/20 15:004.7 3.8 1
1,2,4-Trimethylbenzene ND ug/kg 06/15/20 19:51 95-63-606/15/20 15:004.7 3.4 1
1,3,5-Trimethylbenzene ND ug/kg 06/15/20 19:51 108-67-806/15/20 15:004.7 2.8 1
Vinyl acetate ND ug/kg 06/15/20 19:51 108-05-406/15/20 15:0046.7 4.0 1
Vinyl chloride ND ug/kg 06/15/20 19:51 75-01-406/15/20 15:009.3 1.8 1
Xylene (Total)ND ug/kg 06/15/20 19:51 1330-20-706/15/20 15:009.3 2.7 1
m&p-Xylene ND ug/kg 06/15/20 19:51 179601-23-106/15/20 15:009.3 7.2 1
o-Xylene ND ug/kg 06/15/20 19:51 95-47-606/15/20 15:004.7 2.7 1
Surrogates
Toluene-d8 (S)100 %06/15/20 19:51 2037-26-506/15/20 15:0070-130 1
4-Bromofluorobenzene (S)101 %06/15/20 19:51 460-00-406/15/20 15:0070-130 1
1,2-Dichloroethane-d4 (S)103 %06/15/20 19:51 17060-07-006/15/20 15:0070-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.8 %06/10/20 16:550.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 75.3 %06/14/20 00:3206/14/20 00:191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-4(6-8)Lab ID:92481197004 Collected:06/09/20 11:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 06/16/20 20:16 18540-29-906/16/20 12:301.33 0.339 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-5(6-8)Lab ID:92481197005 Collected:06/09/20 12:10 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND mg/kg 06/14/20 19:41 7440-38-206/13/20 08:241.32 0.555 5
Barium 86.9 mg/kg 06/14/20 19:41 7440-39-306/13/20 08:243.29 1.64 5
Cadmium ND mg/kg 06/14/20 19:41 7440-43-906/13/20 08:241.32 0.534 5
Chromium 74.5 mg/kg 06/14/20 19:41 7440-47-306/13/20 08:246.58 2.95 5
Lead 2.45J mg/kg 06/14/20 19:41 7439-92-1 J06/13/20 08:242.63 1.32 5
Selenium ND mg/kg 06/14/20 19:41 7782-49-206/13/20 08:243.29 1.33 5
Silver ND mg/kg 06/14/20 19:41 7440-22-406/13/20 08:240.658 0.280 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0348J mg/kg 06/14/20 17:40 7439-97-6 J06/12/20 09:200.0526 0.0237 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/12/20 09:20 83-32-906/10/20 15:394101061
Acenaphthylene ND ug/kg 06/12/20 09:20 208-96-806/10/20 15:3941097.1 1
Aniline ND ug/kg 06/12/20 09:20 62-53-306/10/20 15:3941092.1 1
Anthracene ND ug/kg 06/12/20 09:20 120-12-706/10/20 15:394101061
Benzo(a)anthracene ND ug/kg 06/12/20 09:20 56-55-306/10/20 15:394101301
Benzo(a)pyrene ND ug/kg 06/12/20 09:20 50-32-806/10/20 15:394101781
Benzo(b)fluoranthene ND ug/kg 06/12/20 09:20 205-99-206/10/20 15:394101651
Benzo(g,h,i)perylene ND ug/kg 06/12/20 09:20 191-24-206/10/20 15:394101601
Benzo(k)fluoranthene ND ug/kg 06/12/20 09:20 207-08-906/10/20 15:394101731
Benzoic Acid ND ug/kg 06/12/20 09:20 65-85-006/10/20 15:3920504421
Benzyl alcohol ND ug/kg 06/12/20 09:20 100-51-606/10/20 15:398202171
4-Bromophenylphenyl ether ND ug/kg 06/12/20 09:20 101-55-306/10/20 15:394101081
Butylbenzylphthalate ND ug/kg 06/12/20 09:20 85-68-706/10/20 15:394101091
4-Chloro-3-methylphenol ND ug/kg 06/12/20 09:20 59-50-706/10/20 15:398202501
4-Chloroaniline ND ug/kg 06/12/20 09:20 106-47-806/10/20 15:398202511
bis(2-Chloroethoxy)methane ND ug/kg 06/12/20 09:20 111-91-106/10/20 15:394101091
bis(2-Chloroethyl) ether ND ug/kg 06/12/20 09:20 111-44-406/10/20 15:3941087.1 1
2-Chloronaphthalene ND ug/kg 06/12/20 09:20 91-58-706/10/20 15:3941091.3 1
2-Chlorophenol ND ug/kg 06/12/20 09:20 95-57-806/10/20 15:3941095.4 1
4-Chlorophenylphenyl ether ND ug/kg 06/12/20 09:20 7005-72-306/10/20 15:394101061
Chrysene ND ug/kg 06/12/20 09:20 218-01-906/10/20 15:394101191
Dibenz(a,h)anthracene ND ug/kg 06/12/20 09:20 53-70-306/10/20 15:394101641
Dibenzofuran ND ug/kg 06/12/20 09:20 132-64-906/10/20 15:394101031
1,2-Dichlorobenzene ND ug/kg 06/12/20 09:20 95-50-106/10/20 15:3941088.7 1
1,3-Dichlorobenzene ND ug/kg 06/12/20 09:20 541-73-106/10/20 15:3941092.3 1
1,4-Dichlorobenzene ND ug/kg 06/12/20 09:20 106-46-706/10/20 15:3941090.2 1
3,3'-Dichlorobenzidine ND ug/kg 06/12/20 09:20 91-94-106/10/20 15:398202861
2,4-Dichlorophenol ND ug/kg 06/12/20 09:20 120-83-206/10/20 15:394101351
Diethylphthalate ND ug/kg 06/12/20 09:20 84-66-206/10/20 15:3941089.0 1
2,4-Dimethylphenol ND ug/kg 06/12/20 09:20 105-67-906/10/20 15:394101021
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-5(6-8)Lab ID:92481197005 Collected:06/09/20 12:10 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/12/20 09:20 131-11-306/10/20 15:3941092.7 1
Di-n-butylphthalate ND ug/kg 06/12/20 09:20 84-74-206/10/20 15:394101011
4,6-Dinitro-2-methylphenol ND ug/kg 06/12/20 09:20 534-52-106/10/20 15:398206611
2,4-Dinitrophenol ND ug/kg 06/12/20 09:20 51-28-506/10/20 15:39205013101
2,4-Dinitrotoluene ND ug/kg 06/12/20 09:20 121-14-206/10/20 15:394101091
2,6-Dinitrotoluene ND ug/kg 06/12/20 09:20 606-20-2 L206/10/20 15:394101071
Di-n-octylphthalate ND ug/kg 06/12/20 09:20 117-84-006/10/20 15:394102341
bis(2-Ethylhexyl)phthalate ND ug/kg 06/12/20 09:20 117-81-706/10/20 15:394101341
Fluoranthene ND ug/kg 06/12/20 09:20 206-44-006/10/20 15:394101241
Fluorene ND ug/kg 06/12/20 09:20 86-73-706/10/20 15:394101101
Hexachloro-1,3-butadiene ND ug/kg 06/12/20 09:20 87-68-306/10/20 15:3941099.7 1
Hexachlorobenzene ND ug/kg 06/12/20 09:20 118-74-106/10/20 15:394101041
Hexachlorocyclopentadiene ND ug/kg 06/12/20 09:20 77-47-406/10/20 15:394101641
Hexachloroethane ND ug/kg 06/12/20 09:20 67-72-106/10/20 15:3941093.4 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/12/20 09:20 193-39-506/10/20 15:394101881
Isophorone ND ug/kg 06/12/20 09:20 78-59-106/10/20 15:3941089.1 1
1-Methylnaphthalene ND ug/kg 06/12/20 09:20 90-12-006/10/20 15:394101091
2-Methylnaphthalene ND ug/kg 06/12/20 09:20 91-57-606/10/20 15:394101041
2-Methylphenol(o-Cresol)ND ug/kg 06/12/20 09:20 95-48-706/10/20 15:3941090.8 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/12/20 09:20 15831-10-406/10/20 15:394101031
Naphthalene ND ug/kg 06/12/20 09:20 91-20-306/10/20 15:3941098.2 1
2-Nitroaniline ND ug/kg 06/12/20 09:20 88-74-406/10/20 15:3920502061
3-Nitroaniline ND ug/kg 06/12/20 09:20 99-09-206/10/20 15:3920502171
4-Nitroaniline ND ug/kg 06/12/20 09:20 100-01-606/10/20 15:398202031
Nitrobenzene ND ug/kg 06/12/20 09:20 98-95-306/10/20 15:3941097.9 1
2-Nitrophenol ND ug/kg 06/12/20 09:20 88-75-506/10/20 15:394101271
4-Nitrophenol ND ug/kg 06/12/20 09:20 100-02-706/10/20 15:3920506541
N-Nitrosodimethylamine ND ug/kg 06/12/20 09:20 62-75-906/10/20 15:394101151
N-Nitroso-di-n-propylamine ND ug/kg 06/12/20 09:20 621-64-706/10/20 15:394101151
N-Nitrosodiphenylamine ND ug/kg 06/12/20 09:20 86-30-606/10/20 15:394101051
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/12/20 09:20 108-60-106/10/20 15:394101141
Pentachlorophenol ND ug/kg 06/12/20 09:20 87-86-506/10/20 15:398201881
Phenanthrene ND ug/kg 06/12/20 09:20 85-01-806/10/20 15:394101031
Phenol ND ug/kg 06/12/20 09:20 108-95-206/10/20 15:3941097.9 1
Pyrene ND ug/kg 06/12/20 09:20 129-00-006/10/20 15:394101131
Pyridine ND ug/kg 06/12/20 09:20 110-86-106/10/20 15:394101041
1,2,4-Trichlorobenzene ND ug/kg 06/12/20 09:20 120-82-106/10/20 15:3941093.9 1
2,4,5-Trichlorophenol ND ug/kg 06/12/20 09:20 95-95-406/10/20 15:394101061
2,4,6-Trichlorophenol ND ug/kg 06/12/20 09:20 88-06-206/10/20 15:394101031
Surrogates
Nitrobenzene-d5 (S)74 %06/12/20 09:20 4165-60-006/10/20 15:3923-110 1
2-Fluorobiphenyl (S)65 %06/12/20 09:20 321-60-806/10/20 15:3930-110 1
Terphenyl-d14 (S)79 %06/12/20 09:20 1718-51-006/10/20 15:3928-110 1
Phenol-d6 (S)67 %06/12/20 09:20 13127-88-306/10/20 15:3922-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-5(6-8)Lab ID:92481197005 Collected:06/09/20 12:10 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)71 %06/12/20 09:20 367-12-406/10/20 15:3913-110 1
2,4,6-Tribromophenol (S)76 %06/12/20 09:20 118-79-606/10/20 15:3927-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/16/20 01:02 67-64-106/15/20 17:0095.1 35.5 1
Benzene ND ug/kg 06/16/20 01:02 71-43-206/15/20 17:004.8 3.4 1
Bromobenzene ND ug/kg 06/16/20 01:02 108-86-106/15/20 17:004.8 3.2 1
Bromochloromethane ND ug/kg 06/16/20 01:02 74-97-506/15/20 17:004.8 3.6 1
Bromodichloromethane ND ug/kg 06/16/20 01:02 75-27-406/15/20 17:004.8 3.1 1
Bromoform ND ug/kg 06/16/20 01:02 75-25-206/15/20 17:004.8 2.6 1
Bromomethane ND ug/kg 06/16/20 01:02 74-83-906/15/20 17:009.5 7.5 1
2-Butanone (MEK)ND ug/kg 06/16/20 01:02 78-93-306/15/20 17:0095.1 40.3 1
n-Butylbenzene ND ug/kg 06/16/20 01:02 104-51-806/15/20 17:004.8 2.6 1
sec-Butylbenzene ND ug/kg 06/16/20 01:02 135-98-806/15/20 17:004.8 3.0 1
tert-Butylbenzene ND ug/kg 06/16/20 01:02 98-06-606/15/20 17:004.8 2.5 1
Carbon tetrachloride ND ug/kg 06/16/20 01:02 56-23-506/15/20 17:004.8 2.1 1
Chlorobenzene ND ug/kg 06/16/20 01:02 108-90-706/15/20 17:004.8 3.1 1
Chloroethane ND ug/kg 06/16/20 01:02 75-00-306/15/20 17:009.5 5.0 1
Chloroform ND ug/kg 06/16/20 01:02 67-66-306/15/20 17:004.8 2.3 1
Chloromethane ND ug/kg 06/16/20 01:02 74-87-306/15/20 17:009.5 6.7 1
2-Chlorotoluene 20.6 ug/kg 06/16/20 01:02 95-49-806/15/20 17:004.8 3.4 1
4-Chlorotoluene ND ug/kg 06/16/20 01:02 106-43-406/15/20 17:004.8 3.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/16/20 01:02 96-12-806/15/20 17:004.8 4.4 1
Dibromochloromethane ND ug/kg 06/16/20 01:02 124-48-106/15/20 17:004.8 2.6 1
1,2-Dibromoethane (EDB)ND ug/kg 06/16/20 01:02 106-93-406/15/20 17:004.8 3.4 1
Dibromomethane ND ug/kg 06/16/20 01:02 74-95-306/15/20 17:004.8 2.4 1
1,2-Dichlorobenzene ND ug/kg 06/16/20 01:02 95-50-106/15/20 17:004.8 2.8 1
1,3-Dichlorobenzene ND ug/kg 06/16/20 01:02 541-73-106/15/20 17:004.8 3.9 1
1,4-Dichlorobenzene ND ug/kg 06/16/20 01:02 106-46-706/15/20 17:004.8 3.6 1
Dichlorodifluoromethane ND ug/kg 06/16/20 01:02 75-71-806/15/20 17:009.5 1.6 1
1,1-Dichloroethane ND ug/kg 06/16/20 01:02 75-34-306/15/20 17:004.8 2.1 1
1,2-Dichloroethane ND ug/kg 06/16/20 01:02 107-06-206/15/20 17:004.8 1.9 1
1,1-Dichloroethene ND ug/kg 06/16/20 01:02 75-35-406/15/20 17:004.8 1.5 1
cis-1,2-Dichloroethene 15.8 ug/kg 06/16/20 01:02 156-59-206/15/20 17:004.8 2.7 1
trans-1,2-Dichloroethene ND ug/kg 06/16/20 01:02 156-60-506/15/20 17:004.8 2.1 1
1,2-Dichloropropane ND ug/kg 06/16/20 01:02 78-87-506/15/20 17:004.8 3.0 1
1,3-Dichloropropane ND ug/kg 06/16/20 01:02 142-28-906/15/20 17:004.8 3.3 1
2,2-Dichloropropane ND ug/kg 06/16/20 01:02 594-20-706/15/20 17:004.8 2.6 1
1,1-Dichloropropene ND ug/kg 06/16/20 01:02 563-58-606/15/20 17:004.8 2.3 1
cis-1,3-Dichloropropene ND ug/kg 06/16/20 01:02 10061-01-506/15/20 17:004.8 3.1 1
trans-1,3-Dichloropropene ND ug/kg 06/16/20 01:02 10061-02-606/15/20 17:004.8 4.0 1
Diisopropyl ether ND ug/kg 06/16/20 01:02 108-20-306/15/20 17:004.8 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-5(6-8)Lab ID:92481197005 Collected:06/09/20 12:10 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/16/20 01:02 100-41-406/15/20 17:004.8 4.5 1
Hexachloro-1,3-butadiene ND ug/kg 06/16/20 01:02 87-68-306/15/20 17:004.8 4.5 1
2-Hexanone ND ug/kg 06/16/20 01:02 591-78-606/15/20 17:0047.6 9.4 1
Isopropylbenzene (Cumene)ND ug/kg 06/16/20 01:02 98-82-806/15/20 17:004.8 3.0 1
p-Isopropyltoluene ND ug/kg 06/16/20 01:02 99-87-606/15/20 17:004.8 2.6 1
Methylene Chloride ND ug/kg 06/16/20 01:02 75-09-206/15/20 17:0019.0 7.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/16/20 01:02 108-10-106/15/20 17:0047.6 40.2 1
Methyl-tert-butyl ether ND ug/kg 06/16/20 01:02 1634-04-406/15/20 17:004.8 3.0 1
Naphthalene ND ug/kg 06/16/20 01:02 91-20-306/15/20 17:004.8 2.7 1
n-Propylbenzene ND ug/kg 06/16/20 01:02 103-65-106/15/20 17:004.8 3.3 1
Styrene ND ug/kg 06/16/20 01:02 100-42-506/15/20 17:004.8 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/16/20 01:02 630-20-606/15/20 17:004.8 3.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/16/20 01:02 79-34-506/15/20 17:004.8 4.2 1
Tetrachloroethene 64.0 ug/kg 06/16/20 01:02 127-18-406/15/20 17:004.8 2.4 1
Toluene ND ug/kg 06/16/20 01:02 108-88-306/15/20 17:004.8 2.7 1
1,2,3-Trichlorobenzene ND ug/kg 06/16/20 01:02 87-61-606/15/20 17:004.8 2.9 1
1,2,4-Trichlorobenzene ND ug/kg 06/16/20 01:02 120-82-106/15/20 17:004.8 2.7 1
1,1,1-Trichloroethane ND ug/kg 06/16/20 01:02 71-55-606/15/20 17:004.8 1.9 1
1,1,2-Trichloroethane ND ug/kg 06/16/20 01:02 79-00-506/15/20 17:004.8 3.5 1
Trichloroethene 74.1 ug/kg 06/16/20 01:02 79-01-606/15/20 17:004.8 3.0 1
Trichlorofluoromethane ND ug/kg 06/16/20 01:02 75-69-406/15/20 17:004.8 1.2 1
1,2,3-Trichloropropane ND ug/kg 06/16/20 01:02 96-18-406/15/20 17:004.8 3.9 1
1,2,4-Trimethylbenzene ND ug/kg 06/16/20 01:02 95-63-606/15/20 17:004.8 3.4 1
1,3,5-Trimethylbenzene ND ug/kg 06/16/20 01:02 108-67-806/15/20 17:004.8 2.8 1
Vinyl acetate ND ug/kg 06/16/20 01:02 108-05-406/15/20 17:0047.6 4.1 1
Vinyl chloride 2.9J ug/kg 06/16/20 01:02 75-01-406/15/20 17:009.5 1.8 1
Xylene (Total)ND ug/kg 06/16/20 01:02 1330-20-706/15/20 17:009.5 2.7 1
m&p-Xylene ND ug/kg 06/16/20 01:02 179601-23-106/15/20 17:009.5 7.3 1
o-Xylene ND ug/kg 06/16/20 01:02 95-47-606/15/20 17:004.8 2.7 1
Surrogates
Toluene-d8 (S)99 %06/16/20 01:02 2037-26-506/15/20 17:0070-130 1
4-Bromofluorobenzene (S)100 %06/16/20 01:02 460-00-406/15/20 17:0070-130 1
1,2-Dichloroethane-d4 (S)101 %06/16/20 01:02 17060-07-006/15/20 17:0070-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.6 %06/10/20 17:290.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 76.0 %06/14/20 00:3206/14/20 00:191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-5(6-8)Lab ID:92481197005 Collected:06/09/20 12:10 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 06/16/20 20:31 18540-29-906/16/20 12:301.32 0.335 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-DUP Lab ID:92481197006 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 0.618J mg/kg 06/14/20 19:44 7440-38-2 J06/13/20 08:241.43 0.602 5
Barium 155 mg/kg 06/14/20 19:44 7440-39-306/13/20 08:243.56 1.78 5
Cadmium ND mg/kg 06/14/20 19:44 7440-43-906/13/20 08:241.43 0.579 5
Chromium 12.8 mg/kg 06/14/20 19:44 7440-47-306/13/20 08:247.13 3.19 5
Lead 3.63 mg/kg 06/14/20 19:44 7439-92-106/13/20 08:242.85 1.43 5
Selenium ND mg/kg 06/14/20 19:44 7782-49-206/13/20 08:243.56 1.44 5
Silver ND mg/kg 06/14/20 19:44 7440-22-406/13/20 08:240.713 0.304 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 06/14/20 17:43 7439-97-606/12/20 09:200.0570 0.0257 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/12/20 09:47 83-32-906/10/20 15:394701211
Acenaphthylene ND ug/kg 06/12/20 09:47 208-96-806/10/20 15:394701111
Aniline ND ug/kg 06/12/20 09:47 62-53-306/10/20 15:394701061
Anthracene ND ug/kg 06/12/20 09:47 120-12-706/10/20 15:394701221
Benzo(a)anthracene ND ug/kg 06/12/20 09:47 56-55-306/10/20 15:394701501
Benzo(a)pyrene ND ug/kg 06/12/20 09:47 50-32-806/10/20 15:394702041
Benzo(b)fluoranthene ND ug/kg 06/12/20 09:47 205-99-206/10/20 15:394701901
Benzo(g,h,i)perylene ND ug/kg 06/12/20 09:47 191-24-206/10/20 15:394701841
Benzo(k)fluoranthene ND ug/kg 06/12/20 09:47 207-08-906/10/20 15:394701981
Benzoic Acid ND ug/kg 06/12/20 09:47 65-85-006/10/20 15:3923505071
Benzyl alcohol ND ug/kg 06/12/20 09:47 100-51-606/10/20 15:399412491
4-Bromophenylphenyl ether ND ug/kg 06/12/20 09:47 101-55-306/10/20 15:394701231
Butylbenzylphthalate ND ug/kg 06/12/20 09:47 85-68-706/10/20 15:394701251
4-Chloro-3-methylphenol ND ug/kg 06/12/20 09:47 59-50-706/10/20 15:399412871
4-Chloroaniline ND ug/kg 06/12/20 09:47 106-47-806/10/20 15:399412881
bis(2-Chloroethoxy)methane ND ug/kg 06/12/20 09:47 111-91-106/10/20 15:394701261
bis(2-Chloroethyl) ether ND ug/kg 06/12/20 09:47 111-44-406/10/20 15:3947099.9 1
2-Chloronaphthalene ND ug/kg 06/12/20 09:47 91-58-706/10/20 15:394701051
2-Chlorophenol ND ug/kg 06/12/20 09:47 95-57-806/10/20 15:394701091
4-Chlorophenylphenyl ether ND ug/kg 06/12/20 09:47 7005-72-306/10/20 15:394701221
Chrysene ND ug/kg 06/12/20 09:47 218-01-906/10/20 15:394701371
Dibenz(a,h)anthracene ND ug/kg 06/12/20 09:47 53-70-306/10/20 15:394701881
Dibenzofuran ND ug/kg 06/12/20 09:47 132-64-906/10/20 15:394701181
1,2-Dichlorobenzene ND ug/kg 06/12/20 09:47 95-50-106/10/20 15:394701021
1,3-Dichlorobenzene ND ug/kg 06/12/20 09:47 541-73-106/10/20 15:394701061
1,4-Dichlorobenzene ND ug/kg 06/12/20 09:47 106-46-706/10/20 15:394701031
3,3'-Dichlorobenzidine ND ug/kg 06/12/20 09:47 91-94-106/10/20 15:399413281
2,4-Dichlorophenol ND ug/kg 06/12/20 09:47 120-83-206/10/20 15:394701551
Diethylphthalate ND ug/kg 06/12/20 09:47 84-66-206/10/20 15:394701021
2,4-Dimethylphenol ND ug/kg 06/12/20 09:47 105-67-906/10/20 15:394701171
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-DUP Lab ID:92481197006 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/12/20 09:47 131-11-306/10/20 15:394701061
Di-n-butylphthalate ND ug/kg 06/12/20 09:47 84-74-206/10/20 15:394701161
4,6-Dinitro-2-methylphenol ND ug/kg 06/12/20 09:47 534-52-106/10/20 15:399417581
2,4-Dinitrophenol ND ug/kg 06/12/20 09:47 51-28-506/10/20 15:39235015001
2,4-Dinitrotoluene ND ug/kg 06/12/20 09:47 121-14-206/10/20 15:394701251
2,6-Dinitrotoluene ND ug/kg 06/12/20 09:47 606-20-2 L206/10/20 15:394701231
Di-n-octylphthalate ND ug/kg 06/12/20 09:47 117-84-006/10/20 15:394702681
bis(2-Ethylhexyl)phthalate ND ug/kg 06/12/20 09:47 117-81-706/10/20 15:394701541
Fluoranthene ND ug/kg 06/12/20 09:47 206-44-006/10/20 15:394701421
Fluorene ND ug/kg 06/12/20 09:47 86-73-706/10/20 15:394701261
Hexachloro-1,3-butadiene ND ug/kg 06/12/20 09:47 87-68-306/10/20 15:394701141
Hexachlorobenzene ND ug/kg 06/12/20 09:47 118-74-106/10/20 15:394701191
Hexachlorocyclopentadiene ND ug/kg 06/12/20 09:47 77-47-406/10/20 15:394701881
Hexachloroethane ND ug/kg 06/12/20 09:47 67-72-106/10/20 15:394701071
Indeno(1,2,3-cd)pyrene ND ug/kg 06/12/20 09:47 193-39-506/10/20 15:394702151
Isophorone ND ug/kg 06/12/20 09:47 78-59-106/10/20 15:394701021
1-Methylnaphthalene ND ug/kg 06/12/20 09:47 90-12-006/10/20 15:394701251
2-Methylnaphthalene ND ug/kg 06/12/20 09:47 91-57-606/10/20 15:394701201
2-Methylphenol(o-Cresol)ND ug/kg 06/12/20 09:47 95-48-706/10/20 15:394701041
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/12/20 09:47 15831-10-406/10/20 15:394701181
Naphthalene ND ug/kg 06/12/20 09:47 91-20-306/10/20 15:394701131
2-Nitroaniline ND ug/kg 06/12/20 09:47 88-74-406/10/20 15:3923502371
3-Nitroaniline ND ug/kg 06/12/20 09:47 99-09-206/10/20 15:3923502491
4-Nitroaniline ND ug/kg 06/12/20 09:47 100-01-606/10/20 15:399412321
Nitrobenzene ND ug/kg 06/12/20 09:47 98-95-306/10/20 15:394701121
2-Nitrophenol ND ug/kg 06/12/20 09:47 88-75-506/10/20 15:394701451
4-Nitrophenol ND ug/kg 06/12/20 09:47 100-02-706/10/20 15:3923507501
N-Nitrosodimethylamine ND ug/kg 06/12/20 09:47 62-75-906/10/20 15:394701321
N-Nitroso-di-n-propylamine ND ug/kg 06/12/20 09:47 621-64-706/10/20 15:394701321
N-Nitrosodiphenylamine ND ug/kg 06/12/20 09:47 86-30-606/10/20 15:394701201
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/12/20 09:47 108-60-106/10/20 15:394701311
Pentachlorophenol ND ug/kg 06/12/20 09:47 87-86-506/10/20 15:399412151
Phenanthrene ND ug/kg 06/12/20 09:47 85-01-806/10/20 15:394701181
Phenol 163J ug/kg 06/12/20 09:47 108-95-206/10/20 15:394701121
Pyrene ND ug/kg 06/12/20 09:47 129-00-006/10/20 15:394701291
Pyridine ND ug/kg 06/12/20 09:47 110-86-106/10/20 15:394701191
1,2,4-Trichlorobenzene ND ug/kg 06/12/20 09:47 120-82-106/10/20 15:394701081
2,4,5-Trichlorophenol ND ug/kg 06/12/20 09:47 95-95-406/10/20 15:394701221
2,4,6-Trichlorophenol ND ug/kg 06/12/20 09:47 88-06-206/10/20 15:394701181
Surrogates
Nitrobenzene-d5 (S)52 %06/12/20 09:47 4165-60-006/10/20 15:3923-110 1
2-Fluorobiphenyl (S)42 %06/12/20 09:47 321-60-806/10/20 15:3930-110 1
Terphenyl-d14 (S)54 %06/12/20 09:47 1718-51-006/10/20 15:3928-110 1
Phenol-d6 (S)49 %06/12/20 09:47 13127-88-306/10/20 15:3922-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-DUP Lab ID:92481197006 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)53 %06/12/20 09:47 367-12-406/10/20 15:3913-110 1
2,4,6-Tribromophenol (S)63 %06/12/20 09:47 118-79-606/10/20 15:3927-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/16/20 01:20 67-64-106/15/20 17:0012446.2 1
Benzene ND ug/kg 06/16/20 01:20 71-43-206/15/20 17:006.2 4.4 1
Bromobenzene ND ug/kg 06/16/20 01:20 108-86-106/15/20 17:006.2 4.2 1
Bromochloromethane ND ug/kg 06/16/20 01:20 74-97-506/15/20 17:006.2 4.7 1
Bromodichloromethane ND ug/kg 06/16/20 01:20 75-27-406/15/20 17:006.2 4.1 1
Bromoform ND ug/kg 06/16/20 01:20 75-25-206/15/20 17:006.2 3.3 1
Bromomethane ND ug/kg 06/16/20 01:20 74-83-906/15/20 17:0012.4 9.8 1
2-Butanone (MEK)ND ug/kg 06/16/20 01:20 78-93-306/15/20 17:0012452.5 1
n-Butylbenzene ND ug/kg 06/16/20 01:20 104-51-806/15/20 17:006.2 3.4 1
sec-Butylbenzene ND ug/kg 06/16/20 01:20 135-98-806/15/20 17:006.2 3.9 1
tert-Butylbenzene ND ug/kg 06/16/20 01:20 98-06-606/15/20 17:006.2 3.3 1
Carbon tetrachloride ND ug/kg 06/16/20 01:20 56-23-506/15/20 17:006.2 2.8 1
Chlorobenzene ND ug/kg 06/16/20 01:20 108-90-706/15/20 17:006.2 4.0 1
Chloroethane ND ug/kg 06/16/20 01:20 75-00-306/15/20 17:0012.4 6.6 1
Chloroform ND ug/kg 06/16/20 01:20 67-66-306/15/20 17:006.2 3.1 1
Chloromethane ND ug/kg 06/16/20 01:20 74-87-306/15/20 17:0012.4 8.7 1
2-Chlorotoluene 27.8 ug/kg 06/16/20 01:20 95-49-806/15/20 17:006.2 4.4 1
4-Chlorotoluene ND ug/kg 06/16/20 01:20 106-43-406/15/20 17:006.2 4.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/16/20 01:20 96-12-806/15/20 17:006.2 5.8 1
Dibromochloromethane ND ug/kg 06/16/20 01:20 124-48-106/15/20 17:006.2 3.3 1
1,2-Dibromoethane (EDB)ND ug/kg 06/16/20 01:20 106-93-406/15/20 17:006.2 4.4 1
Dibromomethane ND ug/kg 06/16/20 01:20 74-95-306/15/20 17:006.2 3.1 1
1,2-Dichlorobenzene ND ug/kg 06/16/20 01:20 95-50-106/15/20 17:006.2 3.7 1
1,3-Dichlorobenzene ND ug/kg 06/16/20 01:20 541-73-106/15/20 17:006.2 5.1 1
1,4-Dichlorobenzene ND ug/kg 06/16/20 01:20 106-46-706/15/20 17:006.2 4.6 1
Dichlorodifluoromethane ND ug/kg 06/16/20 01:20 75-71-806/15/20 17:0012.4 2.1 1
1,1-Dichloroethane ND ug/kg 06/16/20 01:20 75-34-306/15/20 17:006.2 2.7 1
1,2-Dichloroethane ND ug/kg 06/16/20 01:20 107-06-206/15/20 17:006.2 2.5 1
1,1-Dichloroethene ND ug/kg 06/16/20 01:20 75-35-406/15/20 17:006.2 1.9 1
cis-1,2-Dichloroethene ND ug/kg 06/16/20 01:20 156-59-206/15/20 17:006.2 3.5 1
trans-1,2-Dichloroethene ND ug/kg 06/16/20 01:20 156-60-506/15/20 17:006.2 2.7 1
1,2-Dichloropropane ND ug/kg 06/16/20 01:20 78-87-506/15/20 17:006.2 3.9 1
1,3-Dichloropropane ND ug/kg 06/16/20 01:20 142-28-906/15/20 17:006.2 4.3 1
2,2-Dichloropropane ND ug/kg 06/16/20 01:20 594-20-706/15/20 17:006.2 3.4 1
1,1-Dichloropropene ND ug/kg 06/16/20 01:20 563-58-606/15/20 17:006.2 3.0 1
cis-1,3-Dichloropropene ND ug/kg 06/16/20 01:20 10061-01-506/15/20 17:006.2 4.0 1
trans-1,3-Dichloropropene ND ug/kg 06/16/20 01:20 10061-02-606/15/20 17:006.2 5.2 1
Diisopropyl ether ND ug/kg 06/16/20 01:20 108-20-306/15/20 17:006.2 2.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-DUP Lab ID:92481197006 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/16/20 01:20 100-41-406/15/20 17:006.2 5.8 1
Hexachloro-1,3-butadiene ND ug/kg 06/16/20 01:20 87-68-306/15/20 17:006.2 5.9 1
2-Hexanone ND ug/kg 06/16/20 01:20 591-78-606/15/20 17:0062.0 12.3 1
Isopropylbenzene (Cumene)ND ug/kg 06/16/20 01:20 98-82-806/15/20 17:006.2 3.9 1
p-Isopropyltoluene 60.8 ug/kg 06/16/20 01:20 99-87-606/15/20 17:006.2 3.4 1
Methylene Chloride ND ug/kg 06/16/20 01:20 75-09-206/15/20 17:0024.8 9.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/16/20 01:20 108-10-106/15/20 17:0062.0 52.4 1
Methyl-tert-butyl ether ND ug/kg 06/16/20 01:20 1634-04-406/15/20 17:006.2 4.0 1
Naphthalene 8.5 ug/kg 06/16/20 01:20 91-20-306/15/20 17:006.2 3.5 1
n-Propylbenzene ND ug/kg 06/16/20 01:20 103-65-106/15/20 17:006.2 4.3 1
Styrene ND ug/kg 06/16/20 01:20 100-42-506/15/20 17:006.2 2.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/16/20 01:20 630-20-606/15/20 17:006.2 4.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/16/20 01:20 79-34-506/15/20 17:006.2 5.5 1
Tetrachloroethene ND ug/kg 06/16/20 01:20 127-18-406/15/20 17:006.2 3.1 1
Toluene ND ug/kg 06/16/20 01:20 108-88-306/15/20 17:006.2 3.5 1
1,2,3-Trichlorobenzene ND ug/kg 06/16/20 01:20 87-61-606/15/20 17:006.2 3.8 1
1,2,4-Trichlorobenzene ND ug/kg 06/16/20 01:20 120-82-106/15/20 17:006.2 3.5 1
1,1,1-Trichloroethane ND ug/kg 06/16/20 01:20 71-55-606/15/20 17:006.2 2.5 1
1,1,2-Trichloroethane ND ug/kg 06/16/20 01:20 79-00-506/15/20 17:006.2 4.6 1
Trichloroethene ND ug/kg 06/16/20 01:20 79-01-606/15/20 17:006.2 3.9 1
Trichlorofluoromethane ND ug/kg 06/16/20 01:20 75-69-406/15/20 17:006.2 1.5 1
1,2,3-Trichloropropane ND ug/kg 06/16/20 01:20 96-18-406/15/20 17:006.2 5.0 1
1,2,4-Trimethylbenzene 42.5 ug/kg 06/16/20 01:20 95-63-606/15/20 17:006.2 4.5 1
1,3,5-Trimethylbenzene 29.8 ug/kg 06/16/20 01:20 108-67-806/15/20 17:006.2 3.7 1
Vinyl acetate ND ug/kg 06/16/20 01:20 108-05-406/15/20 17:0062.0 5.4 1
Vinyl chloride ND ug/kg 06/16/20 01:20 75-01-406/15/20 17:0012.4 2.4 1
Xylene (Total)ND ug/kg 06/16/20 01:20 1330-20-706/15/20 17:0012.4 3.5 1
m&p-Xylene ND ug/kg 06/16/20 01:20 179601-23-106/15/20 17:0012.4 9.5 1
o-Xylene ND ug/kg 06/16/20 01:20 95-47-606/15/20 17:006.2 3.5 1
Surrogates
Toluene-d8 (S)98 %06/16/20 01:20 2037-26-506/15/20 17:0070-130 1
4-Bromofluorobenzene (S)102 %06/16/20 01:20 460-00-406/15/20 17:0070-130 1
1,2-Dichloroethane-d4 (S)98 %06/16/20 01:20 17060-07-006/15/20 17:0070-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.1 %06/10/20 17:290.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 70.1 %06/14/20 00:3206/14/20 00:191
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-DUP Lab ID:92481197006 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 06/16/20 20:36 18540-29-906/16/20 12:301.43 0.364 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-6(2-3)Lab ID:92481197007 Collected:06/09/20 12:15 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Chromium 118 mg/kg 06/14/20 19:47 7440-47-306/13/20 08:246.59 2.95 5
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 75.9 %06/14/20 00:3206/14/20 00:191
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.977J mg/kg 06/16/20 20:42 18540-29-9 J06/16/20 12:301.32 0.336 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:SB-7(2-3)Lab ID:92481197008 Collected:06/09/20 12:20 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Chromium 14.5 mg/kg 06/14/20 19:50 7440-47-306/13/20 08:246.52 2.92 5
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 76.7 %06/14/20 00:3206/14/20 00:191
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 06/16/20 20:47 18540-29-906/16/20 12:301.30 0.332 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:BG-1(2-3)Lab ID:92481197009 Collected:06/09/20 08:30 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND mg/kg 06/14/20 19:54 7440-38-206/13/20 08:241.24 0.525 5
Barium 34.6 mg/kg 06/14/20 19:54 7440-39-306/13/20 08:243.11 1.55 5
Cadmium ND mg/kg 06/14/20 19:54 7440-43-906/13/20 08:241.24 0.505 5
Chromium 66.0 mg/kg 06/14/20 19:54 7440-47-306/13/20 08:246.22 2.79 5
Lead 2.69 mg/kg 06/14/20 19:54 7439-92-106/13/20 08:242.49 1.24 5
Selenium ND mg/kg 06/14/20 19:54 7782-49-206/13/20 08:243.11 1.26 5
Silver ND mg/kg 06/14/20 19:54 7440-22-406/13/20 08:240.622 0.265 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0461J mg/kg 06/14/20 17:46 7439-97-6 J06/12/20 09:200.0498 0.0224 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.4 %06/14/20 00:3206/14/20 00:191
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 06/16/20 20:52 18540-29-906/16/20 12:301.24 0.317 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 69
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481197
FDP-058
Sample:BG-2(2-3)Lab ID:92481197010 Collected:06/09/20 13:00 Received:06/10/20 10:20 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND mg/kg 06/14/20 19:57 7440-38-206/13/20 08:241.36 0.575 5
Barium 38.7 mg/kg 06/14/20 19:57 7440-39-306/13/20 08:243.40 1.70 5
Cadmium ND mg/kg 06/14/20 19:57 7440-43-906/13/20 08:241.36 0.553 5
Chromium 17.4 mg/kg 06/14/20 19:57 7440-47-306/13/20 08:246.81 3.05 5
Lead 2.32J mg/kg 06/14/20 19:57 7439-92-1 J06/13/20 08:242.72 1.36 5
Selenium ND mg/kg 06/14/20 19:57 7782-49-206/13/20 08:243.40 1.38 5
Silver ND mg/kg 06/14/20 19:57 7440-22-406/13/20 08:240.681 0.290 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0630 mg/kg 06/14/20 17:48 7439-97-606/12/20 09:200.0545 0.0245 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 73.4 %06/14/20 00:3206/14/20 00:191
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 06/16/20 20:57 18540-29-906/16/20 12:301.36 0.347 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1491387
3051
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004, 92481197005, 92481197006, 92481197007,
92481197008, 92481197009, 92481197010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3538552-1
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004, 92481197005, 92481197006, 92481197007,
92481197008, 92481197009, 92481197010
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 1.00 06/14/20 18:450.422
Barium mg/kg ND 2.50 06/14/20 18:451.25
Cadmium mg/kg ND 1.00 06/14/20 18:450.406
Chromium mg/kg ND 5.00 06/14/20 18:452.24
Lead mg/kg ND 2.00 06/14/20 18:451.00
Selenium mg/kg ND 2.50 06/14/20 18:451.01
Silver mg/kg ND 0.500 06/14/20 18:450.213
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3538552-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 102100 102 80.0-120
Barium mg/kg 103100 103 80.0-120
Cadmium mg/kg 111100 111 80.0-120
Chromium mg/kg 106100 106 80.0-120
Lead mg/kg 108100 108 80.0-120
Selenium mg/kg 107100 107 80.0-120
Silver mg/kg 21.220.0 106 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3538552-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481197001
R3538552-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 27.6 90.7 75.0-12585.2 6.22 2027.6ND 125 118
Barium mg/kg ML27.6 52.8 75.0-12573.5 8.74 2027.6241 314 342
Cadmium mg/kg 27.6 103 75.0-12597.7 5.60 2027.6ND 143 135
Chromium mg/kg 27.6 114 75.0-12593.3 14.5 2027.658.1 216 187
Lead mg/kg 27.6 102 75.0-12595.2 7.15 2027.6ND 141 132
Selenium mg/kg 27.6 95.5 75.0-12588.1 8.03 2027.6ND 132 122
Silver mg/kg 5.53 101 75.0-12595.3 5.75 205.53ND 27.9 26.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1491313
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3537893-1
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0400 06/12/20 07:590.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3537893-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.5410.500 108 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3537893-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1228166-01
R3537893-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.644 112 75.0-12596.2 14.7 200.6440.0370 0.761 0.656
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1491494
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481197005, 92481197006, 92481197009, 92481197010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3538549-1
Associated Lab Samples:92481197005, 92481197006, 92481197009, 92481197010
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0400 06/14/20 17:050.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3538549-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.5220.500 104 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3538549-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1227566-26
R3538549-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.575 94.3 75.0-12599.6 5.46 200.575ND 0.543 0.573
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
546519
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2909061
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 2.5 06/15/20 11:571.6
1,1,1-Trichloroethane ug/kg ND 2.5 06/15/20 11:571.0
1,1,2,2-Tetrachloroethane ug/kg ND 2.5 06/15/20 11:572.2
1,1,2-Trichloroethane ug/kg ND 2.5 06/15/20 11:571.9
1,1-Dichloroethane ug/kg ND 2.5 06/15/20 11:571.1
1,1-Dichloroethene ug/kg ND 2.5 06/15/20 11:570.78
1,1-Dichloropropene ug/kg ND 2.5 06/15/20 11:571.2
1,2,3-Trichlorobenzene ug/kg ND 2.5 06/15/20 11:571.5
1,2,3-Trichloropropane ug/kg ND 2.5 06/15/20 11:572.0
1,2,4-Trichlorobenzene ug/kg ND 2.5 06/15/20 11:571.4
1,2,4-Trimethylbenzene ug/kg ND 2.5 06/15/20 11:571.8
1,2-Dibromo-3-chloropropane ug/kg ND 2.5 06/15/20 11:572.3
1,2-Dibromoethane (EDB)ug/kg ND 2.5 06/15/20 11:571.8
1,2-Dichlorobenzene ug/kg ND 2.5 06/15/20 11:571.5
1,2-Dichloroethane ug/kg ND 2.5 06/15/20 11:571.0
1,2-Dichloropropane ug/kg ND 2.5 06/15/20 11:571.6
1,3,5-Trimethylbenzene ug/kg ND 2.5 06/15/20 11:571.5
1,3-Dichlorobenzene ug/kg ND 2.5 06/15/20 11:572.1
1,3-Dichloropropane ug/kg ND 2.5 06/15/20 11:571.7
1,4-Dichlorobenzene ug/kg ND 2.5 06/15/20 11:571.9
2,2-Dichloropropane ug/kg ND 2.5 06/15/20 11:571.4
2-Butanone (MEK)ug/kg ND 50.0 06/15/20 11:5721.2
2-Chlorotoluene ug/kg ND 2.5 06/15/20 11:571.8
2-Hexanone ug/kg ND 25.0 06/15/20 11:575.0
4-Chlorotoluene ug/kg ND 2.5 06/15/20 11:571.6
4-Methyl-2-pentanone (MIBK)ug/kg ND 25.0 06/15/20 11:5721.2
Acetone ug/kg ND 50.0 06/15/20 11:5718.6
Benzene ug/kg ND 2.5 06/15/20 11:571.8
Bromobenzene ug/kg ND 2.5 06/15/20 11:571.7
Bromochloromethane ug/kg ND 2.5 06/15/20 11:571.9
Bromodichloromethane ug/kg ND 2.5 06/15/20 11:571.6
Bromoform ug/kg ND 2.5 06/15/20 11:571.4
Bromomethane ug/kg ND 5.0 06/15/20 11:573.9
Carbon tetrachloride ug/kg ND 2.5 06/15/20 11:571.1
Chlorobenzene ug/kg ND 2.5 06/15/20 11:571.6
Chloroethane ug/kg ND 5.0 06/15/20 11:572.6
Chloroform ug/kg ND 2.5 06/15/20 11:571.2
Chloromethane ug/kg ND 5.0 06/15/20 11:573.5
cis-1,2-Dichloroethene ug/kg ND 2.5 06/15/20 11:571.4
cis-1,3-Dichloropropene ug/kg ND 2.5 06/15/20 11:571.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2909061
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 2.5 06/15/20 11:571.3
Dibromomethane ug/kg ND 2.5 06/15/20 11:571.2
Dichlorodifluoromethane ug/kg ND 5.0 06/15/20 11:570.86
Diisopropyl ether ug/kg ND 2.5 06/15/20 11:571.0
Ethylbenzene ug/kg ND 2.5 06/15/20 11:572.3
Hexachloro-1,3-butadiene ug/kg ND 2.5 06/15/20 11:572.4
Isopropylbenzene (Cumene)ug/kg ND 2.5 06/15/20 11:571.6
m&p-Xylene ug/kg ND 5.0 06/15/20 11:573.8
Methyl-tert-butyl ether ug/kg ND 2.5 06/15/20 11:571.6
Methylene Chloride ug/kg ND 10.0 06/15/20 11:573.7
n-Butylbenzene ug/kg ND 2.5 06/15/20 11:571.4
n-Propylbenzene ug/kg ND 2.5 06/15/20 11:571.7
Naphthalene ug/kg ND 2.5 06/15/20 11:571.4
o-Xylene ug/kg ND 2.5 06/15/20 11:571.4
p-Isopropyltoluene ug/kg ND 2.5 06/15/20 11:571.4
sec-Butylbenzene ug/kg ND 2.5 06/15/20 11:571.6
Styrene ug/kg ND 2.5 06/15/20 11:571.2
tert-Butylbenzene ug/kg ND 2.5 06/15/20 11:571.3
Tetrachloroethene ug/kg ND 2.5 06/15/20 11:571.2
Toluene ug/kg ND 2.5 06/15/20 11:571.4
trans-1,2-Dichloroethene ug/kg ND 2.5 06/15/20 11:571.1
trans-1,3-Dichloropropene ug/kg ND 2.5 06/15/20 11:572.1
Trichloroethene ug/kg ND 2.5 06/15/20 11:571.6
Trichlorofluoromethane ug/kg ND 2.5 06/15/20 11:570.62
Vinyl acetate ug/kg ND 25.0 06/15/20 11:572.2
Vinyl chloride ug/kg ND 5.0 06/15/20 11:570.96
Xylene (Total)ug/kg ND 5.0 06/15/20 11:571.4
1,2-Dichloroethane-d4 (S)%105 70-132 06/15/20 11:57
4-Bromofluorobenzene (S)%101 70-130 06/15/20 11:57
Toluene-d8 (S)%99 70-130 06/15/20 11:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2909062LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 628625 101 70-130
1,1,1-Trichloroethane ug/kg 617625 99 70-130
1,1,2,2-Tetrachloroethane ug/kg 608625 97 55-130
1,1,2-Trichloroethane ug/kg 612625 98 70-130
1,1-Dichloroethane ug/kg 600625 96 68-130
1,1-Dichloroethene ug/kg 640625 102 70-130
1,1-Dichloropropene ug/kg 622625 100 70-130
1,2,3-Trichlorobenzene ug/kg 594625 95 70-130
1,2,3-Trichloropropane ug/kg 603625 96 70-130
1,2,4-Trichlorobenzene ug/kg 596625 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2909062LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 590625 94 69-130
1,2-Dibromo-3-chloropropane ug/kg 622625 100 57-141
1,2-Dibromoethane (EDB)ug/kg 613625 98 70-130
1,2-Dichlorobenzene ug/kg 592625 95 70-130
1,2-Dichloroethane ug/kg 539625 86 70-130
1,2-Dichloropropane ug/kg 607625 97 70-130
1,3,5-Trimethylbenzene ug/kg 614625 98 70-130
1,3-Dichlorobenzene ug/kg 603625 97 70-130
1,3-Dichloropropane ug/kg 599625 96 70-130
1,4-Dichlorobenzene ug/kg 582625 93 70-130
2,2-Dichloropropane ug/kg 600625 96 70-130
2-Butanone (MEK)ug/kg 12601250 101 60-130
2-Chlorotoluene ug/kg 626625 100 70-130
2-Hexanone ug/kg 12701250 101 70-132
4-Chlorotoluene ug/kg 609625 97 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 12401250 99 69-130
Acetone ug/kg 12501250 100 49-148
Benzene ug/kg 594625 95 70-130
Bromobenzene ug/kg 621625 99 70-130
Bromochloromethane ug/kg 667625 107 70-130
Bromodichloromethane ug/kg 593625 95 70-130
Bromoform ug/kg 644625 103 68-136
Bromomethane ug/kg 711625 114 60-140
Carbon tetrachloride ug/kg 653625 105 70-130
Chlorobenzene ug/kg 603625 96 70-130
Chloroethane ug/kg 589625 94 51-147
Chloroform ug/kg 617625 99 70-130
Chloromethane ug/kg 506625 81 48-130
cis-1,2-Dichloroethene ug/kg 615625 98 70-130
cis-1,3-Dichloropropene ug/kg 606625 97 70-130
Dibromochloromethane ug/kg 648625 104 70-130
Dibromomethane ug/kg 621625 99 70-130
Dichlorodifluoromethane ug/kg 596625 95 49-130
Diisopropyl ether ug/kg 592625 95 66-130
Ethylbenzene ug/kg 563625 90 70-130
Hexachloro-1,3-butadiene ug/kg 643625 103 70-130
Isopropylbenzene (Cumene)ug/kg 615625 98 70-130
m&p-Xylene ug/kg 11501250 92 70-130
Methyl-tert-butyl ether ug/kg 628625 101 70-130
Methylene Chloride ug/kg 617625 99 50-137
n-Butylbenzene ug/kg 613625 98 70-130
n-Propylbenzene ug/kg 608625 97 70-130
Naphthalene ug/kg 613625 98 70-131
o-Xylene ug/kg 614625 98 70-130
p-Isopropyltoluene ug/kg 603625 97 70-130
sec-Butylbenzene ug/kg 606625 97 70-130
Styrene ug/kg 642625 103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2909062LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 589625 94 69-130
Tetrachloroethene ug/kg 616625 99 56-130
Toluene ug/kg 620625 99 70-130
trans-1,2-Dichloroethene ug/kg 628625 100 70-130
trans-1,3-Dichloropropene ug/kg 576625 92 70-130
Trichloroethene ug/kg 628625 101 70-141
Trichlorofluoromethane ug/kg 599625 96 67-130
Vinyl acetate ug/kg 12201250 98 10-136
Vinyl chloride ug/kg 662625 106 67-130
Xylene (Total)ug/kg 17701880 94 70-130
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2909063MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481260010
2909064
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 597 107 52-133106 14 30689ND637732
1,1,1-Trichloroethane ug/kg 597 100 49-137105 19 30689ND597725
1,1,2,2-Tetrachloroethane ug/kg 597 98 39-15098 15 30689ND584676
1,1,2-Trichloroethane ug/kg 597 115 48-140106 6 30689ND688730
1,1-Dichloroethane ug/kg 597 91 46-13595 19 30689ND545658
1,1-Dichloroethene ug/kg 597 99 38-149108 22 30689ND593742
1,1-Dichloropropene ug/kg 597 102 41-140108 20 30689ND611747
1,2,3-Trichlorobenzene ug/kg 597 64 10-15872 25 30689ND384494
1,2,3-Trichloropropane ug/kg 597 95 33-15799 18 30689ND568682
1,2,4-Trichlorobenzene ug/kg 597 83 10-15589 21 30689ND494611
1,2,4-Trimethylbenzene ug/kg 597 99 24-154108 23 30689ND590746
1,2-Dibromo-3-
chloropropane ug/kg 597 67 33-15871 20 30689ND398486
1,2-Dibromoethane (EDB)ug/kg 597 101 40-136103 16 30689ND603708
1,2-Dichlorobenzene ug/kg 597 97 27-146102 20 30689ND578703
1,2-Dichloroethane ug/kg 597 88 49-14092 19 30689ND524632
1,2-Dichloropropane ug/kg 597 103 44-143106 17 30689ND613727
1,3,5-Trimethylbenzene ug/kg 597 106 40-144111 19 30689ND632765
1,3-Dichlorobenzene ug/kg 597 100 33-140109 22 30689ND597748
1,3-Dichloropropane ug/kg 597 102 47-147105 17 30689ND611722
1,4-Dichlorobenzene ug/kg 597 97 35-139102 19 30689ND579703
2,2-Dichloropropane ug/kg 597 87 41-14092 20 30689ND522635
2-Butanone (MEK)ug/kg 1190 30 10-18121 23 301380ND363288
2-Chlorotoluene ug/kg 597 105 38-147111 20 30689ND629767
2-Hexanone ug/kg 1190 71 18-16973 18 301380ND8461010
4-Chlorotoluene ug/kg 597 102 36-145110 22 30689ND610760
4-Methyl-2-pentanone
(MIBK)ug/kg R111903616-17598 103 301380ND4321350
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2909063MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481260010
2909064
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acetone ug/kg 1190 47 10-20033 19 301380ND556461
Benzene ug/kg 597 101 46-136107 20 30689ND605736
Bromobenzene ug/kg 597 104 38-149110 20 30689ND622759
Bromochloromethane ug/kg 597 105 44-142109 18 30689ND626753
Bromodichloromethane ug/kg 597 88 41-14097 25 30689ND524671
Bromoform ug/kg 597 97 34-14596 13 30689ND580664
Bromomethane ug/kg 597 100 14-16295 9 30689ND599656
Carbon tetrachloride ug/kg 597 107 44-141114 21 30689ND636786
Chlorobenzene ug/kg 597 107 39-141109 17 30689ND636752
Chloroethane ug/kg 597 22 10-18223 22 30689ND129160
Chloroform ug/kg 597 93 45-140100 21 30689ND558687
Chloromethane ug/kg 597 81 19-14989 23 30689ND484610
cis-1,2-Dichloroethene ug/kg 597 97 38-150102 20 30689ND577705
cis-1,3-Dichloropropene ug/kg 597 95 30-144100 20 30689ND564689
Dibromochloromethane ug/kg 597 104 36-145105 15 30689ND620723
Dibromomethane ug/kg 597 104 41-145104 15 30689ND620718
Dichlorodifluoromethane ug/kg 597 82 16-14690 24 30689ND488619
Diisopropyl ether ug/kg 597 90 41-14395 20 30689ND536654
Ethylbenzene ug/kg 597 99 35-144102 17 30689ND592701
Hexachloro-1,3-butadiene ug/kg 597 106 10-160117 24 30689ND634804
Isopropylbenzene
(Cumene)ug/kg 597 107 30-152112 18 30689ND641769
m&p-Xylene ug/kg 1190 101 33-145104 17 301380ND12101430
Methyl-tert-butyl ether ug/kg 597 95 49-140100 20 30689ND568691
Methylene Chloride ug/kg 597 96 10-174100 19 30689ND571691
n-Butylbenzene ug/kg 597 103 10-160111 22 30689ND615765
n-Propylbenzene ug/kg 597 105 24-159110 19 30689ND624755
Naphthalene ug/kg 597 59 10-17164 23 30689ND349441
o-Xylene ug/kg 597 108 31-150112 18 30689ND643768
p-Isopropyltoluene ug/kg 597 101 21-154109 21 30689ND605749
sec-Butylbenzene ug/kg 597 103 19-159111 22 30689ND613761
Styrene ug/kg 597 109 15-152111 16 30689ND648763
tert-Butylbenzene ug/kg 597 103 31-141107 18 30689ND614738
Tetrachloroethene ug/kg 597 110 19-141115 18 30689ND658791
Toluene ug/kg 597 108 31-146114 20 30689ND642782
trans-1,2-Dichloroethene ug/kg 597 101 28-157105 18 30689ND602723
trans-1,3-Dichloropropene ug/kg 597 86 25-14692 21 30689ND514634
Trichloroethene ug/kg 597 110 34-149115 18 30689ND655789
Trichlorofluoromethane ug/kg 597 22 10-16722 14 30689ND133153
Vinyl acetate ug/kg 1190 84 10-20089 20 301380ND10001230
Vinyl chloride ug/kg 597 105 36-155114 22 30689ND625783
Xylene (Total)ug/kg 1780 103 29-148106 17 302070ND18502200
1,2-Dichloroethane-d4 (S)%113 70-132114
4-Bromofluorobenzene (S)%102 70-13099
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
547418
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481197005, 92481197006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2913428
Associated Lab Samples:92481197005, 92481197006
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/16/20 00:253.3
1,1,1-Trichloroethane ug/kg ND 5.0 06/16/20 00:252.0
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/16/20 00:254.4
1,1,2-Trichloroethane ug/kg ND 5.0 06/16/20 00:253.7
1,1-Dichloroethane ug/kg ND 5.0 06/16/20 00:252.2
1,1-Dichloroethene ug/kg ND 5.0 06/16/20 00:251.6
1,1-Dichloropropene ug/kg ND 5.0 06/16/20 00:252.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/16/20 00:253.1
1,2,3-Trichloropropane ug/kg ND 5.0 06/16/20 00:254.1
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/16/20 00:252.8
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/16/20 00:253.6
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/16/20 00:254.6
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/16/20 00:253.5
1,2-Dichlorobenzene ug/kg ND 5.0 06/16/20 00:253.0
1,2-Dichloroethane ug/kg ND 5.0 06/16/20 00:252.0
1,2-Dichloropropane ug/kg ND 5.0 06/16/20 00:253.1
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/16/20 00:253.0
1,3-Dichlorobenzene ug/kg ND 5.0 06/16/20 00:254.1
1,3-Dichloropropane ug/kg ND 5.0 06/16/20 00:253.5
1,4-Dichlorobenzene ug/kg ND 5.0 06/16/20 00:253.8
2,2-Dichloropropane ug/kg ND 5.0 06/16/20 00:252.8
2-Butanone (MEK)ug/kg ND 100 06/16/20 00:2542.4
2-Chlorotoluene ug/kg ND 5.0 06/16/20 00:253.6
2-Hexanone ug/kg ND 50.0 06/16/20 00:259.9
4-Chlorotoluene ug/kg ND 5.0 06/16/20 00:253.2
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/16/20 00:2542.3
Acetone ug/kg ND 100 06/16/20 00:2537.3
Benzene ug/kg ND 5.0 06/16/20 00:253.5
Bromobenzene ug/kg ND 5.0 06/16/20 00:253.4
Bromochloromethane ug/kg ND 5.0 06/16/20 00:253.8
Bromodichloromethane ug/kg ND 5.0 06/16/20 00:253.3
Bromoform ug/kg ND 5.0 06/16/20 00:252.7
Bromomethane ug/kg ND 10.0 06/16/20 00:257.9
Carbon tetrachloride ug/kg ND 5.0 06/16/20 00:252.2
Chlorobenzene ug/kg ND 5.0 06/16/20 00:253.2
Chloroethane ug/kg ND 10.0 06/16/20 00:255.3
Chloroform ug/kg ND 5.0 06/16/20 00:252.5
Chloromethane ug/kg ND 10.0 06/16/20 00:257.0
cis-1,2-Dichloroethene ug/kg ND 5.0 06/16/20 00:252.9
cis-1,3-Dichloropropene ug/kg ND 5.0 06/16/20 00:253.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2913428
Associated Lab Samples:92481197005, 92481197006
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 06/16/20 00:252.7
Dibromomethane ug/kg ND 5.0 06/16/20 00:252.5
Dichlorodifluoromethane ug/kg ND 10.0 06/16/20 00:251.7
Diisopropyl ether ug/kg ND 5.0 06/16/20 00:252.0
Ethylbenzene ug/kg ND 5.0 06/16/20 00:254.7
Hexachloro-1,3-butadiene ug/kg ND 5.0 06/16/20 00:254.7
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/16/20 00:253.2
m&p-Xylene ug/kg ND 10.0 06/16/20 00:257.7
Methyl-tert-butyl ether ug/kg ND 5.0 06/16/20 00:253.2
Methylene Chloride ug/kg ND 20.0 06/16/20 00:257.4
n-Butylbenzene ug/kg ND 5.0 06/16/20 00:252.7
n-Propylbenzene ug/kg ND 5.0 06/16/20 00:253.4
Naphthalene ug/kg ND 5.0 06/16/20 00:252.8
o-Xylene ug/kg ND 5.0 06/16/20 00:252.8
p-Isopropyltoluene ug/kg ND 5.0 06/16/20 00:252.8
sec-Butylbenzene ug/kg ND 5.0 06/16/20 00:253.2
Styrene ug/kg ND 5.0 06/16/20 00:252.4
tert-Butylbenzene ug/kg ND 5.0 06/16/20 00:252.7
Tetrachloroethene ug/kg ND 5.0 06/16/20 00:252.5
Toluene ug/kg ND 5.0 06/16/20 00:252.9
trans-1,2-Dichloroethene ug/kg ND 5.0 06/16/20 00:252.2
trans-1,3-Dichloropropene ug/kg ND 5.0 06/16/20 00:254.2
Trichloroethene ug/kg ND 5.0 06/16/20 00:253.1
Trichlorofluoromethane ug/kg ND 5.0 06/16/20 00:251.2
Vinyl acetate ug/kg ND 50.0 06/16/20 00:254.3
Vinyl chloride ug/kg ND 10.0 06/16/20 00:251.9
Xylene (Total)ug/kg ND 10.0 06/16/20 00:252.8
1,2-Dichloroethane-d4 (S)%102 70-132 06/16/20 00:25
4-Bromofluorobenzene (S)%101 70-130 06/16/20 00:25
Toluene-d8 (S)%99 70-130 06/16/20 00:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2913429LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12201250 97 70-130
1,1,1-Trichloroethane ug/kg 12001250 96 70-130
1,1,2,2-Tetrachloroethane ug/kg 12101250 97 55-130
1,1,2-Trichloroethane ug/kg 11901250 95 70-130
1,1-Dichloroethane ug/kg 11601250 93 68-130
1,1-Dichloroethene ug/kg 12401250 99 70-130
1,1-Dichloropropene ug/kg 12201250 97 70-130
1,2,3-Trichlorobenzene ug/kg 11201250 89 70-130
1,2,3-Trichloropropane ug/kg 11901250 95 70-130
1,2,4-Trichlorobenzene ug/kg 11101250 89 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2913429LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 11601250 93 69-130
1,2-Dibromo-3-chloropropane ug/kg 12301250 98 57-141
1,2-Dibromoethane (EDB)ug/kg 12101250 97 70-130
1,2-Dichlorobenzene ug/kg 11601250 92 70-130
1,2-Dichloroethane ug/kg 10301250 83 70-130
1,2-Dichloropropane ug/kg 11501250 92 70-130
1,3,5-Trimethylbenzene ug/kg 12101250 97 70-130
1,3-Dichlorobenzene ug/kg 11701250 94 70-130
1,3-Dichloropropane ug/kg 11801250 94 70-130
1,4-Dichlorobenzene ug/kg 11501250 92 70-130
2,2-Dichloropropane ug/kg 11101250 88 70-130
2-Butanone (MEK)ug/kg 23202500 93 60-130
2-Chlorotoluene ug/kg 12901250 104 70-130
2-Hexanone ug/kg 24202500 97 70-132
4-Chlorotoluene ug/kg 12101250 97 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 23102500 93 69-130
Acetone ug/kg 22602500 91 49-148
Benzene ug/kg 11501250 92 70-130
Bromobenzene ug/kg 12401250 99 70-130
Bromochloromethane ug/kg 13501250 108 70-130
Bromodichloromethane ug/kg 11201250 90 70-130
Bromoform ug/kg 12401250 99 68-136
Bromomethane ug/kg 13701250 110 60-140
Carbon tetrachloride ug/kg 12401250 99 70-130
Chlorobenzene ug/kg 12001250 96 70-130
Chloroethane ug/kg 11701250 94 51-147
Chloroform ug/kg 11801250 95 70-130
Chloromethane ug/kg 9961250 80 48-130
cis-1,2-Dichloroethene ug/kg 11901250 95 70-130
cis-1,3-Dichloropropene ug/kg 11601250 92 70-130
Dibromochloromethane ug/kg 12501250 100 70-130
Dibromomethane ug/kg 12201250 98 70-130
Dichlorodifluoromethane ug/kg 11701250 94 49-130
Diisopropyl ether ug/kg 11101250 89 66-130
Ethylbenzene ug/kg 11101250 89 70-130
Hexachloro-1,3-butadiene ug/kg 12101250 96 70-130
Isopropylbenzene (Cumene)ug/kg 12101250 96 70-130
m&p-Xylene ug/kg 22702500 91 70-130
Methyl-tert-butyl ether ug/kg 12201250 98 70-130
Methylene Chloride ug/kg 11601250 93 50-137
n-Butylbenzene ug/kg 11501250 92 70-130
n-Propylbenzene ug/kg 11901250 95 70-130
Naphthalene ug/kg 12101250 97 70-131
o-Xylene ug/kg 12401250 99 70-130
p-Isopropyltoluene ug/kg 11701250 94 70-130
sec-Butylbenzene ug/kg 11701250 94 70-130
Styrene ug/kg 12701250 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2913429LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 11801250 94 69-130
Tetrachloroethene ug/kg 12101250 97 56-130
Toluene ug/kg 12201250 97 70-130
trans-1,2-Dichloroethene ug/kg 12001250 96 70-130
trans-1,3-Dichloropropene ug/kg 11001250 88 70-130
Trichloroethene ug/kg 12201250 98 70-141
Trichlorofluoromethane ug/kg 12001250 96 67-130
Vinyl acetate ug/kg 22802500 91 10-136
Vinyl chloride ug/kg 12901250 103 67-130
Xylene (Total)ug/kg 35103750 94 70-130
1,2-Dichloroethane-d4 (S)%92 70-132
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2914200MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481674006
2914201
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 548 89 52-13396 22 30631ND485608
1,1,1-Trichloroethane ug/kg 548 87 49-13799 27 30631ND476623
1,1,2,2-Tetrachloroethane ug/kg 548 84 39-15089 19 30631ND462561
1,1,2-Trichloroethane ug/kg 548 87 48-14097 24 30631ND479609
1,1-Dichloroethane ug/kg 548 82 46-13593 27 30631ND449588
1,1-Dichloroethene ug/kg 548 92 38-14985 5 30631ND506534
1,1-Dichloropropene ug/kg 548 93 41-140104 25 30631ND508653
1,2,3-Trichlorobenzene ug/kg 548 63 10-15862 12 30631ND347390
1,2,3-Trichloropropane ug/kg 548 84 33-15786 16 30631ND463544
1,2,4-Trichlorobenzene ug/kg 548 82 10-15585 18 30631ND447533
1,2,4-Trimethylbenzene ug/kg 548 92 24-154101 23 30631ND502635
1,2-Dibromo-3-
chloropropane ug/kg 548 55 33-15861 24 30631ND303385
1,2-Dibromoethane (EDB)ug/kg 548 84 40-13694 25 30631ND458590
1,2-Dichlorobenzene ug/kg 548 86 27-14696 25 30631ND473606
1,2-Dichloroethane ug/kg 548 77 49-14086 26 30631ND421545
1,2-Dichloropropane ug/kg 548 89 44-14399 25 30631ND486625
1,3,5-Trimethylbenzene ug/kg 548 95 40-144106 25 30631ND521669
1,3-Dichlorobenzene ug/kg 548 89 33-14099 24 30631ND490622
1,3-Dichloropropane ug/kg 548 88 47-14797 24 30631ND480610
1,4-Dichlorobenzene ug/kg 548 88 35-13998 25 30631ND483619
2,2-Dichloropropane ug/kg 548 73 41-14081 24 30631ND399510
2-Butanone (MEK)ug/kg 1100 26 10-18130 29 301260ND284381
2-Chlorotoluene ug/kg 548 92 38-147103 24 3063112.8 519 661
2-Hexanone ug/kg 1100 61 18-16967 23 301260ND670843
4-Chlorotoluene ug/kg 548 93 36-145105 26 30631ND510660
4-Methyl-2-pentanone
(MIBK)ug/kg 1100 82 16-17592 25 301260ND9031160
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2914200MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481674006
2914201
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acetone ug/kg R111002910-20039 41 301260ND338514
Benzene ug/kg 548 90 46-13699 24 30631ND491625
Bromobenzene ug/kg 548 91 38-149101 25 30631ND498638
Bromochloromethane ug/kg 548 90 44-14299 24 30631ND492623
Bromodichloromethane ug/kg 548 78 41-14089 26 30631ND429559
Bromoform ug/kg 548 77 34-14586 26 30631ND420545
Bromomethane ug/kg 548 85 14-16294 24 30631ND466591
Carbon tetrachloride ug/kg 548 93 44-141102 24 30631ND507646
Chlorobenzene ug/kg 548 90 39-141101 25 30631ND494638
Chloroethane ug/kg 548 21 10-18225 30 30631ND114155
Chloroform ug/kg 548 82 45-14094 27 30631ND451591
Chloromethane ug/kg 548 88 19-149100 26 30631ND484628
cis-1,2-Dichloroethene ug/kg 548 86 38-15097 26 30631ND472612
cis-1,3-Dichloropropene ug/kg 548 82 30-14492 26 30631ND447583
Dibromochloromethane ug/kg 548 83 36-14595 27 30631ND457599
Dibromomethane ug/kg 548 82 41-14591 25 30631ND448577
Dichlorodifluoromethane ug/kg 548 109 16-146123 26 30631ND595773
Diisopropyl ether ug/kg 548 81 41-14390 24 30631ND446569
Ethylbenzene ug/kg 548 87 35-14497 25 30631ND477611
Hexachloro-1,3-butadiene ug/kg 548 100 10-160112 25 30631ND547705
Isopropylbenzene
(Cumene)ug/kg 548 94 30-152106 26 30631ND517670
m&p-Xylene ug/kg 1100 88 33-14598 24 301260ND9661230
Methyl-tert-butyl ether ug/kg 548 84 49-14093 23 30631ND462584
Methylene Chloride ug/kg 548 88 10-17495 22 30631ND483601
n-Butylbenzene ug/kg 548 96 10-160109 26 30631ND528685
n-Propylbenzene ug/kg 548 94 24-159105 25 30631ND516661
Naphthalene ug/kg 548 50 10-17153 18 30631ND277333
o-Xylene ug/kg 548 93 31-150103 25 30631ND507652
p-Isopropyltoluene ug/kg 548 94 21-154105 25 30631ND515662
sec-Butylbenzene ug/kg 548 96 19-159107 24 30631ND528672
Styrene ug/kg 548 91 15-152102 25 30631ND500645
tert-Butylbenzene ug/kg 548 93 31-141103 24 30631ND510647
Tetrachloroethene ug/kg 548 96 19-141107 25 30631ND527675
Toluene ug/kg 548 94 31-146104 24 30631ND514657
trans-1,2-Dichloroethene ug/kg 548 91 28-157100 23 30631ND501630
trans-1,3-Dichloropropene ug/kg 548 76 25-14685 25 30631ND415534
Trichloroethene ug/kg 548 96 34-149106 25 30631ND524670
Trichlorofluoromethane ug/kg 548 21 10-16725 30 30631ND116158
Vinyl acetate ug/kg 1100 68 10-20074 23 301260ND742939
Vinyl chloride ug/kg 548 109 36-155121 25 30631ND596766
Xylene (Total)ug/kg 1640 90 29-148100 24 301900ND14701880
1,2-Dichloroethane-d4 (S)%113 70-132116
4-Bromofluorobenzene (S)%101 70-130100
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
546425
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004, 92481197005, 92481197006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2908583
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004, 92481197005, 92481197006
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 327 06/11/20 13:5374.9
1,2-Dichlorobenzene ug/kg ND 327 06/11/20 13:5370.7
1,3-Dichlorobenzene ug/kg ND 327 06/11/20 13:5373.6
1,4-Dichlorobenzene ug/kg ND 327 06/11/20 13:5371.9
1-Methylnaphthalene ug/kg ND 327 06/11/20 13:5387.0
2,2'-Oxybis(1-chloropropane)ug/kg ND 327 06/11/20 13:5390.8
2,4,5-Trichlorophenol ug/kg ND 327 06/11/20 13:5384.9
2,4,6-Trichlorophenol ug/kg ND 327 06/11/20 13:5382.1
2,4-Dichlorophenol ug/kg ND 327 06/11/20 13:53108
2,4-Dimethylphenol ug/kg ND 327 06/11/20 13:5381.4
2,4-Dinitrophenol ug/kg ND 1630 06/11/20 13:531040
2,4-Dinitrotoluene ug/kg ND 327 06/11/20 13:5386.5
2,6-Dinitrotoluene ug/kg ND 327 v206/11/20 13:5385.4
2-Chloronaphthalene ug/kg ND 327 06/11/20 13:5372.8
2-Chlorophenol ug/kg ND 327 06/11/20 13:5376.0
2-Methylnaphthalene ug/kg ND 327 06/11/20 13:5383.2
2-Methylphenol(o-Cresol)ug/kg ND 327 06/11/20 13:5372.4
2-Nitroaniline ug/kg ND 1630 06/11/20 13:53164
2-Nitrophenol ug/kg ND 327 06/11/20 13:53101
3&4-Methylphenol(m&p Cresol)ug/kg ND 327 06/11/20 13:5382.2
3,3'-Dichlorobenzidine ug/kg ND 653 06/11/20 13:53228
3-Nitroaniline ug/kg ND 1630 06/11/20 13:53173
4,6-Dinitro-2-methylphenol ug/kg ND 653 06/11/20 13:53527
4-Bromophenylphenyl ether ug/kg ND 327 06/11/20 13:5385.7
4-Chloro-3-methylphenol ug/kg ND 653 06/11/20 13:53199
4-Chloroaniline ug/kg ND 653 06/11/20 13:53200
4-Chlorophenylphenyl ether ug/kg ND 327 06/11/20 13:5384.9
4-Nitroaniline ug/kg ND 653 06/11/20 13:53161
4-Nitrophenol ug/kg ND 1630 06/11/20 13:53521
Acenaphthene ug/kg ND 327 06/11/20 13:5384.1
Acenaphthylene ug/kg ND 327 06/11/20 13:5377.3
Aniline ug/kg ND 327 06/11/20 13:5373.4
Anthracene ug/kg ND 327 06/11/20 13:5384.8
Benzo(a)anthracene ug/kg ND 327 06/11/20 13:53104
Benzo(a)pyrene ug/kg ND 327 06/11/20 13:53142
Benzo(b)fluoranthene ug/kg ND 327 06/11/20 13:53132
Benzo(g,h,i)perylene ug/kg ND 327 06/11/20 13:53128
Benzo(k)fluoranthene ug/kg ND 327 06/11/20 13:53138
Benzoic Acid ug/kg ND 1630 06/11/20 13:53352
Benzyl alcohol ug/kg ND 653 06/11/20 13:53173
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2908583
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004, 92481197005, 92481197006
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 327 06/11/20 13:5387.2
bis(2-Chloroethyl) ether ug/kg ND 327 06/11/20 13:5369.4
bis(2-Ethylhexyl)phthalate ug/kg ND 327 06/11/20 13:53107
Butylbenzylphthalate ug/kg ND 327 06/11/20 13:5387.0
Chrysene ug/kg ND 327 06/11/20 13:5394.9
Di-n-butylphthalate ug/kg ND 327 06/11/20 13:5380.6
Di-n-octylphthalate ug/kg ND 327 v106/11/20 13:53186
Dibenz(a,h)anthracene ug/kg ND 327 06/11/20 13:53131
Dibenzofuran ug/kg ND 327 06/11/20 13:5381.7
Diethylphthalate ug/kg ND 327 06/11/20 13:5370.9
Dimethylphthalate ug/kg ND 327 06/11/20 13:5373.9
Fluoranthene ug/kg ND 327 06/11/20 13:5398.7
Fluorene ug/kg ND 327 06/11/20 13:5387.4
Hexachloro-1,3-butadiene ug/kg ND 327 06/11/20 13:5379.4
Hexachlorobenzene ug/kg ND 327 06/11/20 13:5383.0
Hexachlorocyclopentadiene ug/kg ND 327 06/11/20 13:53131
Hexachloroethane ug/kg ND 327 06/11/20 13:5374.5
Indeno(1,2,3-cd)pyrene ug/kg ND 327 06/11/20 13:53150
Isophorone ug/kg ND 327 06/11/20 13:5371.0
N-Nitroso-di-n-propylamine ug/kg ND 327 06/11/20 13:5391.5
N-Nitrosodimethylamine ug/kg ND 327 06/11/20 13:5391.9
N-Nitrosodiphenylamine ug/kg ND 327 06/11/20 13:5383.4
Naphthalene ug/kg ND 327 06/11/20 13:5378.2
Nitrobenzene ug/kg ND 327 06/11/20 13:5378.0
Pentachlorophenol ug/kg ND 653 06/11/20 13:53150
Phenanthrene ug/kg ND 327 06/11/20 13:5382.3
Phenol ug/kg ND 327 06/11/20 13:5378.0
Pyrene ug/kg ND 327 06/11/20 13:5389.9
Pyridine ug/kg ND 327 06/11/20 13:5382.7
2,4,6-Tribromophenol (S)%56 27-110 06/11/20 13:53
2-Fluorobiphenyl (S)%56 30-110 06/11/20 13:53
2-Fluorophenol (S)%61 13-110 06/11/20 13:53
Nitrobenzene-d5 (S)%57 23-110 06/11/20 13:53
Phenol-d6 (S)%61 22-110 06/11/20 13:53
Terphenyl-d14 (S)%72 28-110 06/11/20 13:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2908584LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10701660 65 52-130
1,2-Dichlorobenzene ug/kg 12001660 72 51-130
1,3-Dichlorobenzene ug/kg 12001660 72 50-130
1,4-Dichlorobenzene ug/kg 12401660 75 49-130
1-Methylnaphthalene ug/kg 11201660 68 55-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2908584LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 14401660 87 30-130
2,4,5-Trichlorophenol ug/kg 11401660 69 55-130
2,4,6-Trichlorophenol ug/kg 11501660 70 57-130
2,4-Dichlorophenol ug/kg 11501660 69 56-130
2,4-Dimethylphenol ug/kg 11601660 70 51-130
2,4-Dinitrophenol ug/kg 55408280 67 27-133
2,4-Dinitrotoluene ug/kg 12001660 72 61-130
2,6-Dinitrotoluene ug/kg 853 L2,v316605260-130
2-Chloronaphthalene ug/kg 12201660 74 52-130
2-Chlorophenol ug/kg 12201660 74 54-130
2-Methylnaphthalene ug/kg 11501660 69 54-130
2-Methylphenol(o-Cresol)ug/kg 12601660 76 51-130
2-Nitroaniline ug/kg 25403310 77 51-130
2-Nitrophenol ug/kg 12001660 72 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 12301660 74 11-163
3,3'-Dichlorobenzidine ug/kg 22503310 68 10-132
3-Nitroaniline ug/kg 22003310 66 55-130
4,6-Dinitro-2-methylphenol ug/kg 26003310 78 47-142
4-Bromophenylphenyl ether ug/kg 11001660 67 59-130
4-Chloro-3-methylphenol ug/kg 23203310 70 55-130
4-Chloroaniline ug/kg 23403310 71 54-130
4-Chlorophenylphenyl ether ug/kg 11001660 66 58-130
4-Nitroaniline ug/kg 25103310 76 54-130
4-Nitrophenol ug/kg 57908280 70 48-130
Acenaphthene ug/kg 12501660 75 60-130
Acenaphthylene ug/kg 12701660 76 60-130
Aniline ug/kg 12101660 73 43-130
Anthracene ug/kg 12401660 75 63-130
Benzo(a)anthracene ug/kg 12601660 76 59-130
Benzo(a)pyrene ug/kg 13101660 79 57-130
Benzo(b)fluoranthene ug/kg 12701660 77 54-130
Benzo(g,h,i)perylene ug/kg 13301660 81 59-130
Benzo(k)fluoranthene ug/kg 12601660 76 54-130
Benzoic Acid ug/kg 46908280 57 19-130
Benzyl alcohol ug/kg 24103310 73 50-130
bis(2-Chloroethoxy)methane ug/kg 12001660 72 54-130
bis(2-Chloroethyl) ether ug/kg 12301660 74 48-130
bis(2-Ethylhexyl)phthalate ug/kg 13901660 84 45-134
Butylbenzylphthalate ug/kg 13901660 84 46-138
Chrysene ug/kg 12501660 75 58-130
Di-n-butylphthalate ug/kg 13201660 80 60-130
Di-n-octylphthalate ug/kg 1450 v116608853-130
Dibenz(a,h)anthracene ug/kg 12701660 76 59-130
Dibenzofuran ug/kg 11601660 70 60-130
Diethylphthalate ug/kg 12101660 73 60-130
Dimethylphthalate ug/kg 11901660 72 60-130
Fluoranthene ug/kg 12201660 74 65-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2908584LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 11801660 71 63-130
Hexachloro-1,3-butadiene ug/kg 9151660 55 46-130
Hexachlorobenzene ug/kg 11501660 69 58-130
Hexachlorocyclopentadiene ug/kg 8541660 52 23-130
Hexachloroethane ug/kg 12401660 75 47-130
Indeno(1,2,3-cd)pyrene ug/kg 13501660 82 60-130
Isophorone ug/kg 11701660 71 49-130
N-Nitroso-di-n-propylamine ug/kg 11901660 72 47-130
N-Nitrosodimethylamine ug/kg 13001660 79 45-130
N-Nitrosodiphenylamine ug/kg 12901660 78 59-130
Naphthalene ug/kg 11901660 72 55-130
Nitrobenzene ug/kg 12201660 74 49-130
Pentachlorophenol ug/kg 23303310 70 10-132
Phenanthrene ug/kg 12601660 76 62-130
Phenol ug/kg 13901660 84 46-130
Pyrene ug/kg 12801660 77 53-130
Pyridine ug/kg 10501660 63 37-130
2,4,6-Tribromophenol (S)%69 27-110
2-Fluorobiphenyl (S)%66 30-110
2-Fluorophenol (S)%72 13-110
Nitrobenzene-d5 (S)%67 23-110
Phenol-d6 (S)%74 22-110
Terphenyl-d14 (S)%79 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2908585MATRIX SPIKE SAMPLE:
MSSpike
Result
92480879001
1,2,4-Trichlorobenzene ug/kg 11102070 54 18-130ND
1,2-Dichlorobenzene ug/kg 12902070 63 14-130ND
1,3-Dichlorobenzene ug/kg 12702070 61 12-130ND
1,4-Dichlorobenzene ug/kg 13402070 65 10-130ND
1-Methylnaphthalene ug/kg 11202070 54 12-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 16002070 78 10-130ND
2,4,5-Trichlorophenol ug/kg 12602070 61 13-130ND
2,4,6-Trichlorophenol ug/kg 12402070 60 17-130ND
2,4-Dichlorophenol ug/kg 12602070 61 10-130ND
2,4-Dimethylphenol ug/kg 11702070 57 10-130ND
2,4-Dinitrophenol ug/kg 676010300 66 10-130ND
2,4-Dinitrotoluene ug/kg 13202070 64 24-130ND
2,6-Dinitrotoluene ug/kg 949 v320704623-130ND
2-Chloronaphthalene ug/kg 12002070 58 19-130ND
2-Chlorophenol ug/kg 13602070 66 10-130ND
2-Methylnaphthalene ug/kg 11402070 55 18-130ND
2-Methylphenol(o-Cresol)ug/kg 13202070 64 10-130ND
2-Nitroaniline ug/kg 28204120 68 17-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
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Huntersville, NC 28078
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Page 56 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2908585MATRIX SPIKE SAMPLE:
MSSpike
Result
92480879001
2-Nitrophenol ug/kg 13502070 66 10-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 13402070 65 10-130ND
3,3'-Dichlorobenzidine ug/kg 20104120 49 10-130ND
3-Nitroaniline ug/kg 24704120 60 24-130ND
4,6-Dinitro-2-methylphenol ug/kg 29504120 72 10-152ND
4-Bromophenylphenyl ether ug/kg 10202070 50 29-130ND
4-Chloro-3-methylphenol ug/kg 25704120 62 17-130ND
4-Chloroaniline ug/kg 25504120 62 14-130ND
4-Chlorophenylphenyl ether ug/kg 10102070 49 25-130ND
4-Nitroaniline ug/kg 26804120 65 22-130ND
4-Nitrophenol ug/kg 627010300 61 10-130ND
Acenaphthene ug/kg 12102070 59 20-130ND
Acenaphthylene ug/kg 12602070 61 25-130ND
Aniline ug/kg 9752070 47 10-130ND
Anthracene ug/kg 11402070 55 29-130ND
Benzo(a)anthracene ug/kg 11602070 56 19-130ND
Benzo(a)pyrene ug/kg 11302070 55 12-130ND
Benzo(b)fluoranthene ug/kg 11302070 55 14-130ND
Benzo(g,h,i)perylene ug/kg 11902070 58 10-130ND
Benzo(k)fluoranthene ug/kg 11202070 54 14-130ND
Benzoic Acid ug/kg 442010300 43 10-130ND
Benzyl alcohol ug/kg 27404120 66 13-130ND
bis(2-Chloroethoxy)methane ug/kg 13002070 63 16-130ND
bis(2-Chloroethyl) ether ug/kg 13702070 67 11-130ND
bis(2-Ethylhexyl)phthalate ug/kg 14102070 69 21-130ND
Butylbenzylphthalate ug/kg 13702070 66 23-130ND
Chrysene ug/kg 11902070 58 22-130ND
Di-n-butylphthalate ug/kg 12002070 58 30-130ND
Di-n-octylphthalate ug/kg 1410 v120706923-142ND
Dibenz(a,h)anthracene ug/kg 11702070 57 10-130ND
Dibenzofuran ug/kg 11502070 56 24-130ND
Diethylphthalate ug/kg 12702070 62 26-130ND
Dimethylphthalate ug/kg 13102070 64 22-130ND
Fluoranthene ug/kg 10702070 52 33-130ND
Fluorene ug/kg 11402070 55 22-130ND
Hexachloro-1,3-butadiene ug/kg 8972070 43 13-130ND
Hexachlorobenzene ug/kg 10902070 53 29-130ND
Hexachlorocyclopentadiene ug/kg 8142070 39 10-130ND
Hexachloroethane ug/kg 12602070 61 10-130ND
Indeno(1,2,3-cd)pyrene ug/kg 11702070 57 10-130ND
Isophorone ug/kg 13102070 64 13-130ND
N-Nitroso-di-n-propylamine ug/kg 13502070 65 12-130ND
N-Nitrosodimethylamine ug/kg 13302070 64 11-130ND
N-Nitrosodiphenylamine ug/kg 12402070 60 15-130ND
Naphthalene ug/kg 12702070 62 15-130ND
Nitrobenzene ug/kg 12902070 63 12-130ND
Pentachlorophenol ug/kg 24304120 59 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
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Huntersville, NC 28078
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Page 57 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2908585MATRIX SPIKE SAMPLE:
MSSpike
Result
92480879001
Phenanthrene ug/kg 11602070 56 27-130ND
Phenol ug/kg 14902070 72 10-130ND
Pyrene ug/kg 12802070 62 19-130ND
Pyridine ug/kg 5662070 27 10-130ND
2,4,6-Tribromophenol (S)%57 27-110
2-Fluorobiphenyl (S)%50 30-110
2-Fluorophenol (S)%66 13-110
Nitrobenzene-d5 (S)%63 23-110
Phenol-d6 (S)%67 22-110
Terphenyl-d14 (S)%66 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92481197001
2908586SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND v230ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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Page 58 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92481197001
2908586SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND v130ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%2936
2-Fluorobiphenyl (S)%3238
2-Fluorophenol (S)%3642
Nitrobenzene-d5 (S)%3540
Phenol-d6 (S)%3642
Terphenyl-d14 (S)%3440
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
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Page 59 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
546498
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92480879001
2908942SAMPLE DUPLICATE:
Percent Moisture %18.2 8 2519.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92481197004
2908943SAMPLE DUPLICATE:
Percent Moisture %19.9 1 2519.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
546505
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481197005, 92481197006
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92481197005
2908991SAMPLE DUPLICATE:
Percent Moisture %20.8 1 2520.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92480742007
2909007SAMPLE DUPLICATE:
Percent Moisture %96.9 1 2597.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
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Huntersville, NC 28078
[phone]
Page 61 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1491975
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004, 92481197005, 92481197006, 92481197007,
92481197008, 92481197009, 92481197010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3538806-1
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004, 92481197005, 92481197006, 92481197007,
92481197008, 92481197009, 92481197010
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 06/14/20 00:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3538806-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92481197001
R3538806-3SAMPLE DUPLICATE:
Total Solids %72.1 0.364 1072.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
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Huntersville, NC 28078
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Page 62 of 69
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481197
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1492872
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004, 92481197005, 92481197006, 92481197007,
92481197008, 92481197009, 92481197010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3539614-1
Associated Lab Samples:92481197001, 92481197002, 92481197003, 92481197004, 92481197005, 92481197006, 92481197007,
92481197008, 92481197009, 92481197010
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 06/16/20 17:230.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3539614-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.7010.0 97.0 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3539614-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1227566-21
R3539614-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 21.4 86.3 75.0-12590.0 4.13 2021.4ND 18.5 19.3
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3539614-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1227566-21
Chromium, Hexavalent mg/kg 678814 83.3 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1227566-20
R3539614-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92481197010
R3539614-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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Page 63 of 69
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92481197
FDP-058
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
The analyte failed the method required serial dilution test and/or subsequent post-spike criteria. These failures indicate
matrix interference.PH
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 64 of 69
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92481197
FDP-058
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92481197001 1491387 1491387SB-1(6-8)3051 EPA 6020B
92481197002 1491387 1491387SB-2(6-8)3051 EPA 6020B
92481197003 1491387 1491387SB-3(2-4)3051 EPA 6020B
92481197004 1491387 1491387SB-4(6-8)3051 EPA 6020B
92481197005 1491387 1491387SB-5(6-8)3051 EPA 6020B
92481197006 1491387 1491387SB-DUP 3051 EPA 6020B
92481197007 1491387 1491387SB-6(2-3)3051 EPA 6020B
92481197008 1491387 1491387SB-7(2-3)3051 EPA 6020B
92481197009 1491387 1491387BG-1(2-3)3051 EPA 6020B
92481197010 1491387 1491387BG-2(2-3)3051 EPA 6020B
92481197001 1491313 1491313SB-1(6-8)7471A EPA 7471B
92481197002 1491313 1491313SB-2(6-8)7471A EPA 7471B
92481197003 1491313 1491313SB-3(2-4)7471A EPA 7471B
92481197004 1491313 1491313SB-4(6-8)7471A EPA 7471B
92481197005 1491494 1491494SB-5(6-8)7471A EPA 7471B
92481197006 1491494 1491494SB-DUP 7471A EPA 7471B
92481197009 1491494 1491494BG-1(2-3)7471A EPA 7471B
92481197010 1491494 1491494BG-2(2-3)7471A EPA 7471B
92481197001 546425 546649SB-1(6-8)EPA 3546 EPA 8270E
92481197002 546425 546649SB-2(6-8)EPA 3546 EPA 8270E
92481197003 546425 546649SB-3(2-4)EPA 3546 EPA 8270E
92481197004 546425 546649SB-4(6-8)EPA 3546 EPA 8270E
92481197005 546425 546649SB-5(6-8)EPA 3546 EPA 8270E
92481197006 546425 546649SB-DUP EPA 3546 EPA 8270E
92481197001 546519 547401SB-1(6-8)EPA 5035A/5030B EPA 8260D
92481197002 546519 547401SB-2(6-8)EPA 5035A/5030B EPA 8260D
92481197003 546519 547401SB-3(2-4)EPA 5035A/5030B EPA 8260D
92481197004 546519 547401SB-4(6-8)EPA 5035A/5030B EPA 8260D
92481197005 547418 547524SB-5(6-8)EPA 5035A/5030B EPA 8260D
92481197006 547418 547524SB-DUP EPA 5035A/5030B EPA 8260D
92481197001 546498SB-1(6-8)ASTM D2974-87
92481197002 546498SB-2(6-8)ASTM D2974-87
92481197003 546498SB-3(2-4)ASTM D2974-87
92481197004 546498SB-4(6-8)ASTM D2974-87
92481197005 546505SB-5(6-8)ASTM D2974-87
92481197006 546505SB-DUP ASTM D2974-87
92481197001 1491975 1491975SB-1(6-8)SM 2540 G SM 2540G
92481197002 1491975 1491975SB-2(6-8)SM 2540 G SM 2540G
92481197003 1491975 1491975SB-3(2-4)SM 2540 G SM 2540G
92481197004 1491975 1491975SB-4(6-8)SM 2540 G SM 2540G
92481197005 1491975 1491975SB-5(6-8)SM 2540 G SM 2540G
92481197006 1491975 1491975SB-DUP SM 2540 G SM 2540G
92481197007 1491975 1491975SB-6(2-3)SM 2540 G SM 2540G
92481197008 1491975 1491975SB-7(2-3)SM 2540 G SM 2540G
92481197009 1491975 1491975BG-1(2-3)SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
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Page 65 of 69
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92481197
FDP-058
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92481197010 1491975 1491975BG-2(2-3)SM 2540 G SM 2540G
92481197001 1492872 1492872SB-1(6-8)3060A EPA 7199
92481197002 1492872 1492872SB-2(6-8)3060A EPA 7199
92481197003 1492872 1492872SB-3(2-4)3060A EPA 7199
92481197004 1492872 1492872SB-4(6-8)3060A EPA 7199
92481197005 1492872 1492872SB-5(6-8)3060A EPA 7199
92481197006 1492872 1492872SB-DUP 3060A EPA 7199
92481197007 1492872 1492872SB-6(2-3)3060A EPA 7199
92481197008 1492872 1492872SB-7(2-3)3060A EPA 7199
92481197009 1492872 1492872BG-1(2-3)3060A EPA 7199
92481197010 1492872 1492872BG-2(2-3)3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/18/2020 05:08 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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#=CL#
July 13, 2020
LIMS USE: FR - RALPH MCGEE
LIMS OBJECT ID: 92481464
92481464
Project:
Pace Project No.:
RE:
Ralph McGee
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
FDP-058
Dear Ralph McGee:
Enclosed are the analytical results for sample(s) received by the laboratory on June 11, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
Report revised 7/13/20 to correct reporting errors for S-58 and GW-Dup.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 81
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92481464
FDP-058
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 81
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92481464
FDP-058
Lab ID Sample ID Matrix Date Collected Date Received
92481464001 R-30 Water 06/10/20 13:45 06/11/20 12:44
92481464002 S-58 Water 06/10/20 16:30 06/11/20 12:44
92481464003 Z-90 Water 06/10/20 15:15 06/11/20 12:44
92481464004 DD-40 Water 06/10/20 16:45 06/11/20 12:44
92481464005 GG-43 Water 06/10/20 11:15 06/11/20 12:44
92481464006 RR-102 Water 06/10/20 15:00 06/11/20 12:44
92481464007 TT-34 Water 06/10/20 09:25 06/11/20 12:44
92481464008 YY-37 Water 06/10/20 11:55 06/11/20 12:44
92481464009 GW-Dup Water 06/10/20 00:00 06/11/20 12:44
92481464010 Trip Blank-1 Water 06/10/20 00:00 06/11/20 12:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 81
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92481464
FDP-058
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92481464001 R-30 EPA 6020B 7 PANLD
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
92481464002 S-58 EPA 6020B 7 PANLD
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
92481464003 Z-90 EPA 6020B 7 PANLD, RDS
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
92481464004 DD-40 EPA 6020B 7 PANLD
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
92481464005 GG-43 EPA 6020B 7 PANLD
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
92481464006 RR-102 EPA 6020B 7 PANLD
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
92481464007 TT-34 EPA 6020B 7 PANLD
EPA 7470A 1 PANABL
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
92481464008 YY-37 EPA 6020B 7 PANLD
EPA 7470A 1 PANABL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 81
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92481464
FDP-058
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
92481464009 GW-Dup EPA 6020B 7 PANLAT, LD
EPA 7470A 1 PANTCT
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
92481464010 Trip Blank-1 EPA 8260D 63 PASI-CSAS
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:R-30 Lab ID:92481464001 Collected:06/10/20 13:45 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/17/20 23:21 7440-38-206/17/20 16:452.00 0.735 1
Barium 146 ug/L 06/17/20 23:21 7440-39-306/17/20 16:4520.0 7.78 1
Cadmium ND ug/L 06/17/20 23:21 7440-43-906/17/20 16:451.00 0.478 1
Chromium ND ug/L 06/17/20 23:21 7440-47-306/17/20 16:452.00 1.49 1
Lead ND ug/L 06/17/20 23:21 7439-92-106/17/20 16:455.00 2.49 1
Selenium 1.29J ug/L 06/17/20 23:21 7782-49-2 J06/17/20 16:452.00 0.657 1
Silver ND ug/L 06/17/20 23:21 7440-22-406/17/20 16:452.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/15/20 11:19 7439-97-606/14/20 19:000.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/16/20 18:56 83-32-906/15/20 20:0810.0 1.4 1
Acenaphthylene ND ug/L 06/16/20 18:56 208-96-806/15/20 20:0810.0 1.5 1
Aniline ND ug/L 06/16/20 18:56 62-53-306/15/20 20:0810.0 1.6 1
Anthracene ND ug/L 06/16/20 18:56 120-12-706/15/20 20:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 06/16/20 18:56 56-55-306/15/20 20:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 06/16/20 18:56 50-32-806/15/20 20:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/16/20 18:56 205-99-206/15/20 20:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/16/20 18:56 191-24-206/15/20 20:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/16/20 18:56 207-08-906/15/20 20:0810.0 1.5 1
Benzoic Acid ND ug/L 06/16/20 18:56 65-85-006/15/20 20:0850.0 19.5 1
Benzyl alcohol ND ug/L 06/16/20 18:56 100-51-606/15/20 20:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/16/20 18:56 101-55-306/15/20 20:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 06/16/20 18:56 85-68-706/15/20 20:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/16/20 18:56 59-50-706/15/20 20:0810.0 2.8 1
4-Chloroaniline ND ug/L 06/16/20 18:56 106-47-806/15/20 20:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/20 18:56 111-91-106/15/20 20:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/16/20 18:56 111-44-406/15/20 20:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 06/16/20 18:56 91-58-706/15/20 20:0810.0 1.4 1
2-Chlorophenol ND ug/L 06/16/20 18:56 95-57-806/15/20 20:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/16/20 18:56 7005-72-306/15/20 20:0810.0 1.5 1
Chrysene ND ug/L 06/16/20 18:56 218-01-906/15/20 20:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/16/20 18:56 53-70-306/15/20 20:0810.0 1.6 1
Dibenzofuran ND ug/L 06/16/20 18:56 132-64-906/15/20 20:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/16/20 18:56 95-50-106/15/20 20:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/16/20 18:56 541-73-106/15/20 20:0810.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/16/20 18:56 106-46-706/15/20 20:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/16/20 18:56 91-94-106/15/20 20:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/16/20 18:56 120-83-206/15/20 20:0810.0 1.5 1
Diethylphthalate ND ug/L 06/16/20 18:56 84-66-206/15/20 20:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/16/20 18:56 105-67-906/15/20 20:0810.0 1.5 1
Dimethylphthalate ND ug/L 06/16/20 18:56 131-11-306/15/20 20:0810.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:R-30 Lab ID:92481464001 Collected:06/10/20 13:45 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/16/20 18:56 84-74-206/15/20 20:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/20 18:56 534-52-106/15/20 20:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/16/20 18:56 51-28-506/15/20 20:0850.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/16/20 18:56 121-14-206/15/20 20:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/16/20 18:56 606-20-206/15/20 20:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/16/20 18:56 117-84-006/15/20 20:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/16/20 18:56 117-81-706/15/20 20:086.0 2.0 1
Fluoranthene ND ug/L 06/16/20 18:56 206-44-006/15/20 20:0810.0 1.6 1
Fluorene ND ug/L 06/16/20 18:56 86-73-706/15/20 20:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/16/20 18:56 87-68-306/15/20 20:0810.0 1.6 1
Hexachlorobenzene ND ug/L 06/16/20 18:56 118-74-106/15/20 20:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/16/20 18:56 77-47-406/15/20 20:0810.0 2.4 1
Hexachloroethane ND ug/L 06/16/20 18:56 67-72-106/15/20 20:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/20 18:56 193-39-506/15/20 20:0810.0 1.7 1
Isophorone ND ug/L 06/16/20 18:56 78-59-106/15/20 20:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 06/16/20 18:56 90-12-006/15/20 20:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 06/16/20 18:56 91-57-606/15/20 20:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/16/20 18:56 95-48-706/15/20 20:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/16/20 18:56 15831-10-406/15/20 20:0810.0 1.2 1
Naphthalene ND ug/L 06/16/20 18:56 91-20-306/15/20 20:0810.0 1.6 1
2-Nitroaniline ND ug/L 06/16/20 18:56 88-74-406/15/20 20:0820.0 3.0 1
3-Nitroaniline ND ug/L 06/16/20 18:56 99-09-206/15/20 20:0820.0 2.8 1
4-Nitroaniline ND ug/L 06/16/20 18:56 100-01-606/15/20 20:0820.0 3.1 1
Nitrobenzene ND ug/L 06/16/20 18:56 98-95-306/15/20 20:0810.0 1.5 1
2-Nitrophenol ND ug/L 06/16/20 18:56 88-75-506/15/20 20:0810.0 1.7 1
4-Nitrophenol ND ug/L 06/16/20 18:56 100-02-706/15/20 20:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/16/20 18:56 62-75-906/15/20 20:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/20 18:56 621-64-706/15/20 20:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/16/20 18:56 86-30-606/15/20 20:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/16/20 18:56 108-60-106/15/20 20:0810.0 1.3 1
Pentachlorophenol ND ug/L 06/16/20 18:56 87-86-506/15/20 20:0820.0 2.8 1
Phenanthrene ND ug/L 06/16/20 18:56 85-01-806/15/20 20:0810.0 1.4 1
Phenol ND ug/L 06/16/20 18:56 108-95-206/15/20 20:0810.0 1.5 1
Pyrene ND ug/L 06/16/20 18:56 129-00-006/15/20 20:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/16/20 18:56 120-82-106/15/20 20:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/16/20 18:56 95-95-406/15/20 20:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/16/20 18:56 88-06-206/15/20 20:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)50 %06/16/20 18:56 4165-60-006/15/20 20:0813-130 1
2-Fluorobiphenyl (S)46 %06/16/20 18:56 321-60-806/15/20 20:0813-130 1
Terphenyl-d14 (S)72 %06/16/20 18:56 1718-51-006/15/20 20:0825-130 1
Phenol-d6 (S)30 %06/16/20 18:56 13127-88-306/15/20 20:0810-130 1
2-Fluorophenol (S)32 %06/16/20 18:56 367-12-406/15/20 20:0810-130 1
2,4,6-Tribromophenol (S)52 %06/16/20 18:56 118-79-606/15/20 20:0810-137 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:R-30 Lab ID:92481464001 Collected:06/10/20 13:45 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/17/20 01:43 67-64-125.0 6.2 1
Benzene ND ug/L 06/17/20 01:43 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/17/20 01:43 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/17/20 01:43 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/17/20 01:43 75-27-41.0 0.26 1
Bromoform ND ug/L 06/17/20 01:43 75-25-21.0 0.62 1
Bromomethane ND ug/L 06/17/20 01:43 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 06/17/20 01:43 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/17/20 01:43 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/17/20 01:43 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/17/20 01:43 75-00-31.0 0.49 1
Chloroform ND ug/L 06/17/20 01:43 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/17/20 01:43 74-87-3 v31.0 0.39 1
2-Chlorotoluene ND ug/L 06/17/20 01:43 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/17/20 01:43 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/20 01:43 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/17/20 01:43 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/20 01:43 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/17/20 01:43 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/17/20 01:43 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/17/20 01:43 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/17/20 01:43 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/17/20 01:43 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/17/20 01:43 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/17/20 01:43 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/17/20 01:43 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/17/20 01:43 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/17/20 01:43 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/17/20 01:43 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/17/20 01:43 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/17/20 01:43 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/17/20 01:43 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/17/20 01:43 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/17/20 01:43 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/17/20 01:43 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/17/20 01:43 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/17/20 01:43 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/17/20 01:43 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/17/20 01:43 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/17/20 01:43 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/20 01:43 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/17/20 01:43 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/17/20 01:43 91-20-31.0 0.35 1
Styrene ND ug/L 06/17/20 01:43 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/20 01:43 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 8 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:R-30 Lab ID:92481464001 Collected:06/10/20 13:45 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/17/20 01:43 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/17/20 01:43 127-18-41.0 0.16 1
Toluene ND ug/L 06/17/20 01:43 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/17/20 01:43 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/17/20 01:43 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/17/20 01:43 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/17/20 01:43 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/17/20 01:43 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/17/20 01:43 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/17/20 01:43 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/17/20 01:43 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 06/17/20 01:43 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/17/20 01:43 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/17/20 01:43 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/17/20 01:43 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %06/17/20 01:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %06/17/20 01:43 17060-07-070-130 1
Toluene-d8 (S)97 %06/17/20 01:43 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 06/15/20 16:46 18540-29-906/15/20 16:460.100 0.0400 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:S-58 Lab ID:92481464002 Collected:06/10/20 16:30 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/17/20 23:24 7440-38-206/17/20 16:452.00 0.735 1
Barium 115 ug/L 06/17/20 23:24 7440-39-306/17/20 16:4520.0 7.78 1
Cadmium ND ug/L 06/17/20 23:24 7440-43-906/17/20 16:451.00 0.478 1
Chromium ND ug/L 06/17/20 23:24 7440-47-306/17/20 16:452.00 1.49 1
Lead ND ug/L 06/17/20 23:24 7439-92-106/17/20 16:455.00 2.49 1
Selenium 1.03J ug/L 06/17/20 23:24 7782-49-2 J06/17/20 16:452.00 0.657 1
Silver ND ug/L 06/17/20 23:24 7440-22-406/17/20 16:452.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/15/20 11:21 7439-97-606/14/20 19:000.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/16/20 19:21 83-32-906/15/20 20:0810.0 1.4 1
Acenaphthylene ND ug/L 06/16/20 19:21 208-96-806/15/20 20:0810.0 1.5 1
Aniline ND ug/L 06/16/20 19:21 62-53-306/15/20 20:0810.0 1.6 1
Anthracene ND ug/L 06/16/20 19:21 120-12-706/15/20 20:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 06/16/20 19:21 56-55-306/15/20 20:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 06/16/20 19:21 50-32-806/15/20 20:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/16/20 19:21 205-99-206/15/20 20:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/16/20 19:21 191-24-206/15/20 20:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/16/20 19:21 207-08-906/15/20 20:0810.0 1.5 1
Benzoic Acid ND ug/L 06/16/20 19:21 65-85-006/15/20 20:0850.0 19.5 1
Benzyl alcohol ND ug/L 06/16/20 19:21 100-51-606/15/20 20:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/16/20 19:21 101-55-306/15/20 20:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 06/16/20 19:21 85-68-706/15/20 20:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/16/20 19:21 59-50-706/15/20 20:0810.0 2.8 1
4-Chloroaniline ND ug/L 06/16/20 19:21 106-47-806/15/20 20:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/20 19:21 111-91-106/15/20 20:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/16/20 19:21 111-44-406/15/20 20:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 06/16/20 19:21 91-58-706/15/20 20:0810.0 1.4 1
2-Chlorophenol 14.8 ug/L 06/16/20 19:21 95-57-806/15/20 20:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/16/20 19:21 7005-72-306/15/20 20:0810.0 1.5 1
Chrysene ND ug/L 06/16/20 19:21 218-01-906/15/20 20:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/16/20 19:21 53-70-306/15/20 20:0810.0 1.6 1
Dibenzofuran ND ug/L 06/16/20 19:21 132-64-906/15/20 20:0810.0 1.3 1
1,2-Dichlorobenzene 2.1J ug/L 06/16/20 19:21 95-50-106/15/20 20:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/16/20 19:21 541-73-106/15/20 20:0810.0 1.4 1
1,4-Dichlorobenzene 120 ug/L 06/16/20 19:21 106-46-706/15/20 20:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/16/20 19:21 91-94-106/15/20 20:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/16/20 19:21 120-83-206/15/20 20:0810.0 1.5 1
Diethylphthalate ND ug/L 06/16/20 19:21 84-66-206/15/20 20:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/16/20 19:21 105-67-906/15/20 20:0810.0 1.5 1
Dimethylphthalate ND ug/L 06/16/20 19:21 131-11-306/15/20 20:0810.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:S-58 Lab ID:92481464002 Collected:06/10/20 16:30 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/16/20 19:21 84-74-206/15/20 20:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/20 19:21 534-52-106/15/20 20:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/16/20 19:21 51-28-506/15/20 20:0850.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/16/20 19:21 121-14-206/15/20 20:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/16/20 19:21 606-20-206/15/20 20:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/16/20 19:21 117-84-006/15/20 20:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate 3.7J ug/L 06/16/20 19:21 117-81-706/15/20 20:086.0 2.0 1
Fluoranthene ND ug/L 06/16/20 19:21 206-44-006/15/20 20:0810.0 1.6 1
Fluorene ND ug/L 06/16/20 19:21 86-73-706/15/20 20:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/16/20 19:21 87-68-306/15/20 20:0810.0 1.6 1
Hexachlorobenzene ND ug/L 06/16/20 19:21 118-74-106/15/20 20:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/16/20 19:21 77-47-406/15/20 20:0810.0 2.4 1
Hexachloroethane ND ug/L 06/16/20 19:21 67-72-106/15/20 20:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/20 19:21 193-39-506/15/20 20:0810.0 1.7 1
Isophorone ND ug/L 06/16/20 19:21 78-59-106/15/20 20:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 06/16/20 19:21 90-12-006/15/20 20:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 06/16/20 19:21 91-57-606/15/20 20:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/16/20 19:21 95-48-706/15/20 20:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)1.3J ug/L 06/16/20 19:21 15831-10-406/15/20 20:0810.0 1.2 1
Naphthalene ND ug/L 06/16/20 19:21 91-20-306/15/20 20:0810.0 1.6 1
2-Nitroaniline ND ug/L 06/16/20 19:21 88-74-406/15/20 20:0820.0 3.0 1
3-Nitroaniline ND ug/L 06/16/20 19:21 99-09-206/15/20 20:0820.0 2.8 1
4-Nitroaniline ND ug/L 06/16/20 19:21 100-01-606/15/20 20:0820.0 3.1 1
Nitrobenzene ND ug/L 06/16/20 19:21 98-95-306/15/20 20:0810.0 1.5 1
2-Nitrophenol ND ug/L 06/16/20 19:21 88-75-506/15/20 20:0810.0 1.7 1
4-Nitrophenol ND ug/L 06/16/20 19:21 100-02-706/15/20 20:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/16/20 19:21 62-75-906/15/20 20:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/20 19:21 621-64-706/15/20 20:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/16/20 19:21 86-30-606/15/20 20:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/16/20 19:21 108-60-106/15/20 20:0810.0 1.3 1
Pentachlorophenol ND ug/L 06/16/20 19:21 87-86-506/15/20 20:0820.0 2.8 1
Phenanthrene ND ug/L 06/16/20 19:21 85-01-806/15/20 20:0810.0 1.4 1
Phenol ND ug/L 06/16/20 19:21 108-95-206/15/20 20:0810.0 1.5 1
Pyrene ND ug/L 06/16/20 19:21 129-00-006/15/20 20:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/16/20 19:21 120-82-106/15/20 20:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/16/20 19:21 95-95-406/15/20 20:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/16/20 19:21 88-06-206/15/20 20:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)99 %06/16/20 19:21 4165-60-006/15/20 20:0813-130 1
2-Fluorobiphenyl (S)93 %06/16/20 19:21 321-60-806/15/20 20:0813-130 1
Terphenyl-d14 (S)146 %06/16/20 19:21 1718-51-0 S006/15/20 20:0825-130 1
Phenol-d6 (S)53 %06/16/20 19:21 13127-88-306/15/20 20:0810-130 1
2-Fluorophenol (S)40 %06/16/20 19:21 367-12-406/15/20 20:0810-130 1
2,4,6-Tribromophenol (S)75 %06/16/20 19:21 118-79-606/15/20 20:0810-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:S-58 Lab ID:92481464002 Collected:06/10/20 16:30 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/17/20 14:04 67-64-12500617100
Benzene 61.2J ug/L 06/17/20 14:04 71-43-210015.0 100
Bromobenzene ND ug/L 06/17/20 14:04 108-86-110022.0 100
Bromochloromethane ND ug/L 06/17/20 14:04 74-97-510034.3 100
Bromodichloromethane ND ug/L 06/17/20 14:04 75-27-410025.6 100
Bromoform ND ug/L 06/17/20 14:04 75-25-210061.7 100
Bromomethane ND ug/L 06/17/20 14:04 74-83-9 v220062.0 100
2-Butanone (MEK)ND ug/L 06/17/20 14:04 78-93-3500333100
Carbon tetrachloride ND ug/L 06/17/20 14:04 56-23-510022.4 100
Chlorobenzene 12500 ug/L 06/17/20 14:04 108-90-7 M110023.3 100
Chloroethane ND ug/L 06/17/20 14:04 75-00-310049.0 100
Chloroform ND ug/L 06/17/20 14:04 67-66-3500234100
Chloromethane ND ug/L 06/17/20 14:04 74-87-3 v210038.9 100
2-Chlorotoluene ND ug/L 06/17/20 14:04 95-49-810020.3 100
4-Chlorotoluene ND ug/L 06/17/20 14:04 106-43-410020.4 100
1,2-Dibromo-3-chloropropane ND ug/L 06/17/20 14:04 96-12-850025.7 100
Dibromochloromethane ND ug/L 06/17/20 14:04 124-48-110041.3 100
1,2-Dibromoethane (EDB)ND ug/L 06/17/20 14:04 106-93-410025.8 100
Dibromomethane ND ug/L 06/17/20 14:04 74-95-310045.9 100
1,2-Dichlorobenzene ND ug/L 06/17/20 14:04 95-50-110029.1 100
1,3-Dichlorobenzene ND ug/L 06/17/20 14:04 541-73-110021.7 100
1,4-Dichlorobenzene 140 ug/L 06/17/20 14:04 106-46-710025.8 100
Dichlorodifluoromethane ND ug/L 06/17/20 14:04 75-71-810022.6 100
1,1-Dichloroethane ND ug/L 06/17/20 14:04 75-34-310026.8 100
1,2-Dichloroethane ND ug/L 06/17/20 14:04 107-06-210033.6 100
1,1-Dichloroethene ND ug/L 06/17/20 14:04 75-35-410024.5 100
cis-1,2-Dichloroethene ND ug/L 06/17/20 14:04 156-59-210029.1 100
trans-1,2-Dichloroethene ND ug/L 06/17/20 14:04 156-60-510025.4 100
1,2-Dichloropropane ND ug/L 06/17/20 14:04 78-87-510018.7 100
1,3-Dichloropropane ND ug/L 06/17/20 14:04 142-28-910015.8 100
2,2-Dichloropropane ND ug/L 06/17/20 14:04 594-20-710027.0 100
1,1-Dichloropropene ND ug/L 06/17/20 14:04 563-58-610021.3 100
cis-1,3-Dichloropropene ND ug/L 06/17/20 14:04 10061-01-510029.6 100
trans-1,3-Dichloropropene ND ug/L 06/17/20 14:04 10061-02-610030.9 100
Diisopropyl ether ND ug/L 06/17/20 14:04 108-20-310021.8 100
Ethylbenzene ND ug/L 06/17/20 14:04 100-41-410025.6 100
Hexachloro-1,3-butadiene ND ug/L 06/17/20 14:04 87-68-310043.8 100
2-Hexanone ND ug/L 06/17/20 14:04 591-78-650056.8 100
p-Isopropyltoluene ND ug/L 06/17/20 14:04 99-87-610021.2 100
Methylene Chloride ND ug/L 06/17/20 14:04 75-09-2500369100
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/20 14:04 108-10-1500453100
Methyl-tert-butyl ether ND ug/L 06/17/20 14:04 1634-04-410027.5 100
Naphthalene ND ug/L 06/17/20 14:04 91-20-310035.2 100
Styrene ND ug/L 06/17/20 14:04 100-42-510026.7 100
1,1,1,2-Tetrachloroethane ND ug/L 06/17/20 14:04 630-20-610034.0 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:S-58 Lab ID:92481464002 Collected:06/10/20 16:30 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/17/20 14:04 79-34-510022.2 100
Tetrachloroethene ND ug/L 06/17/20 14:04 127-18-410016.2 100
Toluene ND ug/L 06/17/20 14:04 108-88-310024.4 100
1,2,3-Trichlorobenzene ND ug/L 06/17/20 14:04 87-61-610034.4 100
1,2,4-Trichlorobenzene ND ug/L 06/17/20 14:04 120-82-110021.8 100
1,1,1-Trichloroethane ND ug/L 06/17/20 14:04 71-55-610017.5 100
1,1,2-Trichloroethane ND ug/L 06/17/20 14:04 79-00-510023.6 100
Trichloroethene ND ug/L 06/17/20 14:04 79-01-610022.0 100
Trichlorofluoromethane ND ug/L 06/17/20 14:04 75-69-410031.1 100
1,2,3-Trichloropropane ND ug/L 06/17/20 14:04 96-18-410034.7 100
Vinyl acetate ND ug/L 06/17/20 14:04 108-05-4200145100
Vinyl chloride ND ug/L 06/17/20 14:04 75-01-410024.2 100
Xylene (Total)ND ug/L 06/17/20 14:04 1330-20-710063.0 100
m&p-Xylene ND ug/L 06/17/20 14:04 179601-23-120041.0 100
o-Xylene ND ug/L 06/17/20 14:04 95-47-610022.0 100
Surrogates
4-Bromofluorobenzene (S)97 %06/17/20 14:04 460-00-470-130 100
1,2-Dichloroethane-d4 (S)101 %06/17/20 14:04 17060-07-070-130 100
Toluene-d8 (S)101 %06/17/20 14:04 2037-26-570-130 100
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 06/15/20 16:54 18540-29-906/15/20 16:540.100 0.0400 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:Z-90 Lab ID:92481464003 Collected:06/10/20 15:15 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.98 ug/L 06/17/20 23:27 7440-38-206/17/20 16:452.00 0.735 1
Barium 3020 ug/L 06/18/20 10:13 7440-39-306/17/20 16:45100038950
Cadmium 9.66 ug/L 06/17/20 23:27 7440-43-906/17/20 16:451.00 0.478 1
Chromium 13.6 ug/L 06/17/20 23:27 7440-47-306/17/20 16:452.00 1.49 1
Lead 4.80J ug/L 06/17/20 23:27 7439-92-1 J06/17/20 16:455.00 2.49 1
Selenium 1.33J ug/L 06/17/20 23:27 7782-49-2 J06/17/20 16:452.00 0.657 1
Silver ND ug/L 06/17/20 23:27 7440-22-406/17/20 16:452.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/15/20 11:23 7439-97-606/14/20 19:000.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/17/20 14:01 83-32-906/15/20 20:0820028.4 20
Acenaphthylene ND ug/L 06/17/20 14:01 208-96-806/15/20 20:0820029.4 20
Aniline ND ug/L 06/17/20 14:01 62-53-306/15/20 20:0820032.8 20
Anthracene ND ug/L 06/17/20 14:01 120-12-706/15/20 20:0820031.2 20
Benzo(a)anthracene ND ug/L 06/17/20 14:01 56-55-306/15/20 20:0820030.4 20
Benzo(a)pyrene ND ug/L 06/17/20 14:01 50-32-806/15/20 20:0820035.2 20
Benzo(b)fluoranthene ND ug/L 06/17/20 14:01 205-99-206/15/20 20:0820034.0 20
Benzo(g,h,i)perylene ND ug/L 06/17/20 14:01 191-24-206/15/20 20:0820031.8 20
Benzo(k)fluoranthene ND ug/L 06/17/20 14:01 207-08-906/15/20 20:0820029.4 20
Benzoic Acid 14600 ug/L 06/17/20 14:59 65-85-006/15/20 20:08250097550
Benzyl alcohol 1780 ug/L 06/17/20 14:01 100-51-606/15/20 20:0840052.8 20
4-Bromophenylphenyl ether ND ug/L 06/17/20 14:01 101-55-306/15/20 20:0820023.4 20
Butylbenzylphthalate ND ug/L 06/17/20 14:01 85-68-706/15/20 20:0820037.4 20
4-Chloro-3-methylphenol ND ug/L 06/17/20 14:01 59-50-706/15/20 20:0820055.6 20
4-Chloroaniline ND ug/L 06/17/20 14:01 106-47-806/15/20 20:0840057.0 20
bis(2-Chloroethoxy)methane ND ug/L 06/17/20 14:01 111-91-106/15/20 20:0820026.8 20
bis(2-Chloroethyl) ether ND ug/L 06/17/20 14:01 111-44-406/15/20 20:0820034.6 20
2-Chloronaphthalene ND ug/L 06/17/20 14:01 91-58-706/15/20 20:0820027.6 20
2-Chlorophenol ND ug/L 06/17/20 14:01 95-57-806/15/20 20:0820028.8 20
4-Chlorophenylphenyl ether ND ug/L 06/17/20 14:01 7005-72-306/15/20 20:0820029.8 20
Chrysene ND ug/L 06/17/20 14:01 218-01-906/15/20 20:0820027.6 20
Dibenz(a,h)anthracene ND ug/L 06/17/20 14:01 53-70-306/15/20 20:0820031.6 20
Dibenzofuran ND ug/L 06/17/20 14:01 132-64-906/15/20 20:0820026.8 20
1,2-Dichlorobenzene ND ug/L 06/17/20 14:01 95-50-106/15/20 20:0820027.0 20
1,3-Dichlorobenzene ND ug/L 06/17/20 14:01 541-73-106/15/20 20:0820027.8 20
1,4-Dichlorobenzene ND ug/L 06/17/20 14:01 106-46-706/15/20 20:0820030.4 20
3,3'-Dichlorobenzidine ND ug/L 06/17/20 14:01 91-94-106/15/20 20:0840054.2 20
2,4-Dichlorophenol ND ug/L 06/17/20 14:01 120-83-206/15/20 20:0820030.0 20
Diethylphthalate ND ug/L 06/17/20 14:01 84-66-206/15/20 20:0820031.4 20
2,4-Dimethylphenol ND ug/L 06/17/20 14:01 105-67-906/15/20 20:0820030.0 20
Dimethylphthalate ND ug/L 06/17/20 14:01 131-11-306/15/20 20:0820027.8 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 14 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:Z-90 Lab ID:92481464003 Collected:06/10/20 15:15 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/17/20 14:01 84-74-206/15/20 20:0820032.0 20
4,6-Dinitro-2-methylphenol ND ug/L 06/17/20 14:01 534-52-106/15/20 20:0840089.6 20
2,4-Dinitrophenol ND ug/L 06/17/20 14:01 51-28-506/15/20 20:08100014520
2,4-Dinitrotoluene ND ug/L 06/17/20 14:01 121-14-206/15/20 20:0820034.2 20
2,6-Dinitrotoluene ND ug/L 06/17/20 14:01 606-20-206/15/20 20:0820034.8 20
Di-n-octylphthalate ND ug/L 06/17/20 14:01 117-84-006/15/20 20:0820044.0 20
bis(2-Ethylhexyl)phthalate ND ug/L 06/17/20 14:01 117-81-706/15/20 20:0812039.6 20
Fluoranthene ND ug/L 06/17/20 14:01 206-44-006/15/20 20:0820031.6 20
Fluorene ND ug/L 06/17/20 14:01 86-73-706/15/20 20:0820028.8 20
Hexachloro-1,3-butadiene ND ug/L 06/17/20 14:01 87-68-306/15/20 20:0820031.2 20
Hexachlorobenzene ND ug/L 06/17/20 14:01 118-74-106/15/20 20:0820026.4 20
Hexachlorocyclopentadiene ND ug/L 06/17/20 14:01 77-47-406/15/20 20:0820048.2 20
Hexachloroethane ND ug/L 06/17/20 14:01 67-72-106/15/20 20:0820026.8 20
Indeno(1,2,3-cd)pyrene ND ug/L 06/17/20 14:01 193-39-506/15/20 20:0820033.4 20
Isophorone ND ug/L 06/17/20 14:01 78-59-106/15/20 20:0820026.0 20
1-Methylnaphthalene ND ug/L 06/17/20 14:01 90-12-006/15/20 20:0820028.0 20
2-Methylnaphthalene ND ug/L 06/17/20 14:01 91-57-606/15/20 20:0820028.2 20
2-Methylphenol(o-Cresol)ND ug/L 06/17/20 14:01 95-48-706/15/20 20:0820024.4 20
3&4-Methylphenol(m&p Cresol)58.9J ug/L 06/17/20 14:01 15831-10-406/15/20 20:0820023.6 20
Naphthalene ND ug/L 06/17/20 14:01 91-20-306/15/20 20:0820032.8 20
2-Nitroaniline ND ug/L 06/17/20 14:01 88-74-406/15/20 20:0840060.8 20
3-Nitroaniline ND ug/L 06/17/20 14:01 99-09-206/15/20 20:0840055.8 20
4-Nitroaniline ND ug/L 06/17/20 14:01 100-01-606/15/20 20:0840062.6 20
Nitrobenzene ND ug/L 06/17/20 14:01 98-95-306/15/20 20:0820029.8 20
2-Nitrophenol ND ug/L 06/17/20 14:01 88-75-506/15/20 20:0820033.2 20
4-Nitrophenol ND ug/L 06/17/20 14:01 100-02-706/15/20 20:08100018820
N-Nitrosodimethylamine ND ug/L 06/17/20 14:01 62-75-906/15/20 20:0820036.6 20
N-Nitroso-di-n-propylamine ND ug/L 06/17/20 14:01 621-64-706/15/20 20:0820025.6 20
N-Nitrosodiphenylamine ND ug/L 06/17/20 14:01 86-30-606/15/20 20:0820027.6 20
2,2'-Oxybis(1-chloropropane)ND ug/L 06/17/20 14:01 108-60-106/15/20 20:0820026.2 20
Pentachlorophenol ND ug/L 06/17/20 14:01 87-86-506/15/20 20:0840056.4 20
Phenanthrene ND ug/L 06/17/20 14:01 85-01-806/15/20 20:0820028.8 20
Phenol 2730 ug/L 06/17/20 14:59 108-95-206/15/20 20:0850077.0 50
Pyrene ND ug/L 06/17/20 14:01 129-00-006/15/20 20:0820029.8 20
1,2,4-Trichlorobenzene ND ug/L 06/17/20 14:01 120-82-106/15/20 20:0820031.6 20
2,4,5-Trichlorophenol ND ug/L 06/17/20 14:01 95-95-406/15/20 20:0820030.6 20
2,4,6-Trichlorophenol ND ug/L 06/17/20 14:01 88-06-206/15/20 20:0820028.6 20
Surrogates
Nitrobenzene-d5 (S)0 %06/17/20 14:01 4165-60-0 D3,S406/15/20 20:0813-130 20
2-Fluorobiphenyl (S)0 %06/17/20 14:01 321-60-8 S406/15/20 20:0813-130 20
Terphenyl-d14 (S)0 %06/17/20 14:01 1718-51-0 S406/15/20 20:0825-130 20
Phenol-d6 (S)0 %06/17/20 14:01 13127-88-3 S406/15/20 20:0810-130 20
2-Fluorophenol (S)0 %06/17/20 14:01 367-12-4 S406/15/20 20:0810-130 20
2,4,6-Tribromophenol (S)0 %06/17/20 14:01 118-79-6 S406/15/20 20:0810-137 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:Z-90 Lab ID:92481464003 Collected:06/10/20 15:15 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/17/20 06:12 67-64-1125030850
Benzene ND ug/L 06/17/20 06:12 71-43-250.0 7.5 50
Bromobenzene ND ug/L 06/17/20 06:12 108-86-150.0 11.0 50
Bromochloromethane ND ug/L 06/17/20 06:12 74-97-550.0 17.2 50
Bromodichloromethane ND ug/L 06/17/20 06:12 75-27-450.0 12.8 50
Bromoform ND ug/L 06/17/20 06:12 75-25-250.0 30.8 50
Bromomethane ND ug/L 06/17/20 06:12 74-83-9 v210031.0 50
2-Butanone (MEK)239J ug/L 06/17/20 06:12 78-93-325016650
Carbon tetrachloride ND ug/L 06/17/20 06:12 56-23-550.0 11.2 50
Chlorobenzene 1500 ug/L 06/17/20 06:12 108-90-750.0 11.6 50
Chloroethane ND ug/L 06/17/20 06:12 75-00-350.0 24.5 50
Chloroform ND ug/L 06/17/20 06:12 67-66-325011750
Chloromethane ND ug/L 06/17/20 06:12 74-87-3 v250.0 19.4 50
2-Chlorotoluene ND ug/L 06/17/20 06:12 95-49-850.0 10.2 50
4-Chlorotoluene ND ug/L 06/17/20 06:12 106-43-450.0 10.2 50
1,2-Dibromo-3-chloropropane ND ug/L 06/17/20 06:12 96-12-825012.8 50
Dibromochloromethane ND ug/L 06/17/20 06:12 124-48-150.0 20.6 50
1,2-Dibromoethane (EDB)ND ug/L 06/17/20 06:12 106-93-450.0 12.9 50
Dibromomethane ND ug/L 06/17/20 06:12 74-95-350.0 23.0 50
1,2-Dichlorobenzene 18.2J ug/L 06/17/20 06:12 95-50-150.0 14.6 50
1,3-Dichlorobenzene ND ug/L 06/17/20 06:12 541-73-150.0 10.8 50
1,4-Dichlorobenzene ND ug/L 06/17/20 06:12 106-46-750.0 12.9 50
Dichlorodifluoromethane ND ug/L 06/17/20 06:12 75-71-850.0 11.3 50
1,1-Dichloroethane ND ug/L 06/17/20 06:12 75-34-350.0 13.4 50
1,2-Dichloroethane ND ug/L 06/17/20 06:12 107-06-250.0 16.8 50
1,1-Dichloroethene ND ug/L 06/17/20 06:12 75-35-450.0 12.2 50
cis-1,2-Dichloroethene 27.3J ug/L 06/17/20 06:12 156-59-250.0 14.6 50
trans-1,2-Dichloroethene ND ug/L 06/17/20 06:12 156-60-550.0 12.7 50
1,2-Dichloropropane ND ug/L 06/17/20 06:12 78-87-550.0 9.4 50
1,3-Dichloropropane ND ug/L 06/17/20 06:12 142-28-950.0 7.9 50
2,2-Dichloropropane ND ug/L 06/17/20 06:12 594-20-750.0 13.5 50
1,1-Dichloropropene ND ug/L 06/17/20 06:12 563-58-650.0 10.6 50
cis-1,3-Dichloropropene ND ug/L 06/17/20 06:12 10061-01-550.0 14.8 50
trans-1,3-Dichloropropene ND ug/L 06/17/20 06:12 10061-02-650.0 15.4 50
Diisopropyl ether ND ug/L 06/17/20 06:12 108-20-350.0 10.9 50
Ethylbenzene ND ug/L 06/17/20 06:12 100-41-450.0 12.8 50
Hexachloro-1,3-butadiene ND ug/L 06/17/20 06:12 87-68-350.0 21.9 50
2-Hexanone ND ug/L 06/17/20 06:12 591-78-625028.4 50
p-Isopropyltoluene ND ug/L 06/17/20 06:12 99-87-650.0 10.6 50
Methylene Chloride ND ug/L 06/17/20 06:12 75-09-225018450
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/20 06:12 108-10-125022650
Methyl-tert-butyl ether ND ug/L 06/17/20 06:12 1634-04-450.0 13.8 50
Naphthalene ND ug/L 06/17/20 06:12 91-20-350.0 17.6 50
Styrene ND ug/L 06/17/20 06:12 100-42-550.0 13.4 50
1,1,1,2-Tetrachloroethane ND ug/L 06/17/20 06:12 630-20-650.0 17.0 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:Z-90 Lab ID:92481464003 Collected:06/10/20 15:15 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/17/20 06:12 79-34-550.0 11.1 50
Tetrachloroethene ND ug/L 06/17/20 06:12 127-18-450.0 8.1 50
Toluene ND ug/L 06/17/20 06:12 108-88-350.0 12.2 50
1,2,3-Trichlorobenzene ND ug/L 06/17/20 06:12 87-61-650.0 17.2 50
1,2,4-Trichlorobenzene ND ug/L 06/17/20 06:12 120-82-150.0 10.9 50
1,1,1-Trichloroethane ND ug/L 06/17/20 06:12 71-55-650.0 8.8 50
1,1,2-Trichloroethane ND ug/L 06/17/20 06:12 79-00-550.0 11.8 50
Trichloroethene ND ug/L 06/17/20 06:12 79-01-650.0 11.0 50
Trichlorofluoromethane ND ug/L 06/17/20 06:12 75-69-450.0 15.6 50
1,2,3-Trichloropropane ND ug/L 06/17/20 06:12 96-18-450.0 17.4 50
Vinyl acetate ND ug/L 06/17/20 06:12 108-05-410072.5 50
Vinyl chloride ND ug/L 06/17/20 06:12 75-01-450.0 12.1 50
Xylene (Total)ND ug/L 06/17/20 06:12 1330-20-750.0 31.5 50
m&p-Xylene ND ug/L 06/17/20 06:12 179601-23-110020.5 50
o-Xylene ND ug/L 06/17/20 06:12 95-47-650.0 11.0 50
Surrogates
4-Bromofluorobenzene (S)97 %06/17/20 06:12 460-00-4 D370-130 50
1,2-Dichloroethane-d4 (S)105 %06/17/20 06:12 17060-07-070-130 50
Toluene-d8 (S)100 %06/17/20 06:12 2037-26-570-130 50
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 06/15/20 17:01 18540-29-906/15/20 17:010.100 0.0400 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:DD-40 Lab ID:92481464004 Collected:06/10/20 16:45 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/17/20 23:30 7440-38-206/17/20 16:452.00 0.735 1
Barium 101 ug/L 06/17/20 23:30 7440-39-306/17/20 16:4520.0 7.78 1
Cadmium ND ug/L 06/17/20 23:30 7440-43-906/17/20 16:451.00 0.478 1
Chromium 10.6 ug/L 06/17/20 23:30 7440-47-306/17/20 16:452.00 1.49 1
Lead ND ug/L 06/17/20 23:30 7439-92-106/17/20 16:455.00 2.49 1
Selenium 1.12J ug/L 06/17/20 23:30 7782-49-2 J06/17/20 16:452.00 0.657 1
Silver ND ug/L 06/17/20 23:30 7440-22-406/17/20 16:452.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/15/20 11:25 7439-97-606/14/20 19:000.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/16/20 20:12 83-32-906/15/20 20:0810.0 1.4 1
Acenaphthylene ND ug/L 06/16/20 20:12 208-96-806/15/20 20:0810.0 1.5 1
Aniline ND ug/L 06/16/20 20:12 62-53-306/15/20 20:0810.0 1.6 1
Anthracene ND ug/L 06/16/20 20:12 120-12-706/15/20 20:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 06/16/20 20:12 56-55-306/15/20 20:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 06/16/20 20:12 50-32-806/15/20 20:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/16/20 20:12 205-99-206/15/20 20:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/16/20 20:12 191-24-206/15/20 20:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/16/20 20:12 207-08-906/15/20 20:0810.0 1.5 1
Benzoic Acid ND ug/L 06/16/20 20:12 65-85-006/15/20 20:0850.0 19.5 1
Benzyl alcohol ND ug/L 06/16/20 20:12 100-51-606/15/20 20:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/16/20 20:12 101-55-306/15/20 20:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 06/16/20 20:12 85-68-706/15/20 20:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/16/20 20:12 59-50-706/15/20 20:0810.0 2.8 1
4-Chloroaniline ND ug/L 06/16/20 20:12 106-47-806/15/20 20:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/20 20:12 111-91-106/15/20 20:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/16/20 20:12 111-44-406/15/20 20:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 06/16/20 20:12 91-58-706/15/20 20:0810.0 1.4 1
2-Chlorophenol ND ug/L 06/16/20 20:12 95-57-806/15/20 20:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/16/20 20:12 7005-72-306/15/20 20:0810.0 1.5 1
Chrysene ND ug/L 06/16/20 20:12 218-01-906/15/20 20:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/16/20 20:12 53-70-306/15/20 20:0810.0 1.6 1
Dibenzofuran ND ug/L 06/16/20 20:12 132-64-906/15/20 20:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/16/20 20:12 95-50-106/15/20 20:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/16/20 20:12 541-73-106/15/20 20:0810.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/16/20 20:12 106-46-706/15/20 20:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/16/20 20:12 91-94-106/15/20 20:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/16/20 20:12 120-83-206/15/20 20:0810.0 1.5 1
Diethylphthalate ND ug/L 06/16/20 20:12 84-66-206/15/20 20:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/16/20 20:12 105-67-906/15/20 20:0810.0 1.5 1
Dimethylphthalate ND ug/L 06/16/20 20:12 131-11-306/15/20 20:0810.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:DD-40 Lab ID:92481464004 Collected:06/10/20 16:45 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/16/20 20:12 84-74-206/15/20 20:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/20 20:12 534-52-106/15/20 20:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/16/20 20:12 51-28-506/15/20 20:0850.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/16/20 20:12 121-14-206/15/20 20:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/16/20 20:12 606-20-206/15/20 20:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/16/20 20:12 117-84-006/15/20 20:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/16/20 20:12 117-81-706/15/20 20:086.0 2.0 1
Fluoranthene ND ug/L 06/16/20 20:12 206-44-006/15/20 20:0810.0 1.6 1
Fluorene ND ug/L 06/16/20 20:12 86-73-706/15/20 20:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/16/20 20:12 87-68-306/15/20 20:0810.0 1.6 1
Hexachlorobenzene ND ug/L 06/16/20 20:12 118-74-106/15/20 20:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/16/20 20:12 77-47-406/15/20 20:0810.0 2.4 1
Hexachloroethane ND ug/L 06/16/20 20:12 67-72-106/15/20 20:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/20 20:12 193-39-506/15/20 20:0810.0 1.7 1
Isophorone ND ug/L 06/16/20 20:12 78-59-106/15/20 20:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 06/16/20 20:12 90-12-006/15/20 20:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 06/16/20 20:12 91-57-606/15/20 20:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/16/20 20:12 95-48-706/15/20 20:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/16/20 20:12 15831-10-406/15/20 20:0810.0 1.2 1
Naphthalene ND ug/L 06/16/20 20:12 91-20-306/15/20 20:0810.0 1.6 1
2-Nitroaniline ND ug/L 06/16/20 20:12 88-74-406/15/20 20:0820.0 3.0 1
3-Nitroaniline ND ug/L 06/16/20 20:12 99-09-206/15/20 20:0820.0 2.8 1
4-Nitroaniline ND ug/L 06/16/20 20:12 100-01-606/15/20 20:0820.0 3.1 1
Nitrobenzene ND ug/L 06/16/20 20:12 98-95-306/15/20 20:0810.0 1.5 1
2-Nitrophenol ND ug/L 06/16/20 20:12 88-75-506/15/20 20:0810.0 1.7 1
4-Nitrophenol ND ug/L 06/16/20 20:12 100-02-706/15/20 20:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/16/20 20:12 62-75-906/15/20 20:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/20 20:12 621-64-706/15/20 20:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/16/20 20:12 86-30-606/15/20 20:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/16/20 20:12 108-60-106/15/20 20:0810.0 1.3 1
Pentachlorophenol ND ug/L 06/16/20 20:12 87-86-506/15/20 20:0820.0 2.8 1
Phenanthrene ND ug/L 06/16/20 20:12 85-01-806/15/20 20:0810.0 1.4 1
Phenol ND ug/L 06/16/20 20:12 108-95-206/15/20 20:0810.0 1.5 1
Pyrene ND ug/L 06/16/20 20:12 129-00-006/15/20 20:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/16/20 20:12 120-82-106/15/20 20:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/16/20 20:12 95-95-406/15/20 20:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/16/20 20:12 88-06-206/15/20 20:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)76 %06/16/20 20:12 4165-60-006/15/20 20:0813-130 1
2-Fluorobiphenyl (S)71 %06/16/20 20:12 321-60-806/15/20 20:0813-130 1
Terphenyl-d14 (S)128 %06/16/20 20:12 1718-51-006/15/20 20:0825-130 1
Phenol-d6 (S)42 %06/16/20 20:12 13127-88-306/15/20 20:0810-130 1
2-Fluorophenol (S)49 %06/16/20 20:12 367-12-406/15/20 20:0810-130 1
2,4,6-Tribromophenol (S)87 %06/16/20 20:12 118-79-606/15/20 20:0810-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:DD-40 Lab ID:92481464004 Collected:06/10/20 16:45 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/17/20 03:30 67-64-125.0 6.2 1
Benzene ND ug/L 06/17/20 03:30 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/17/20 03:30 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/17/20 03:30 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/17/20 03:30 75-27-41.0 0.26 1
Bromoform ND ug/L 06/17/20 03:30 75-25-21.0 0.62 1
Bromomethane ND ug/L 06/17/20 03:30 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 06/17/20 03:30 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/17/20 03:30 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/17/20 03:30 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/17/20 03:30 75-00-31.0 0.49 1
Chloroform ND ug/L 06/17/20 03:30 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/17/20 03:30 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 06/17/20 03:30 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/17/20 03:30 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/20 03:30 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/17/20 03:30 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/20 03:30 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/17/20 03:30 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/17/20 03:30 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/17/20 03:30 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/17/20 03:30 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/17/20 03:30 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/17/20 03:30 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/17/20 03:30 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/17/20 03:30 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/17/20 03:30 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/17/20 03:30 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/17/20 03:30 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/17/20 03:30 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/17/20 03:30 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/17/20 03:30 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/17/20 03:30 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/17/20 03:30 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/17/20 03:30 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/17/20 03:30 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/17/20 03:30 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/17/20 03:30 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/17/20 03:30 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/17/20 03:30 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/20 03:30 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/17/20 03:30 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/17/20 03:30 91-20-31.0 0.35 1
Styrene ND ug/L 06/17/20 03:30 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/20 03:30 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:DD-40 Lab ID:92481464004 Collected:06/10/20 16:45 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/17/20 03:30 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/17/20 03:30 127-18-41.0 0.16 1
Toluene ND ug/L 06/17/20 03:30 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/17/20 03:30 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/17/20 03:30 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/17/20 03:30 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/17/20 03:30 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/17/20 03:30 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/17/20 03:30 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/17/20 03:30 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/17/20 03:30 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 06/17/20 03:30 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/17/20 03:30 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/17/20 03:30 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/17/20 03:30 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)97 %06/17/20 03:30 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %06/17/20 03:30 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/20 03:30 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 3.86 ug/L 06/15/20 21:33 18540-29-906/15/20 21:332.00 0.800 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:GG-43 Lab ID:92481464005 Collected:06/10/20 11:15 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/17/20 23:34 7440-38-206/17/20 16:452.00 0.735 1
Barium 71.2 ug/L 06/17/20 23:34 7440-39-306/17/20 16:4520.0 7.78 1
Cadmium ND ug/L 06/17/20 23:34 7440-43-906/17/20 16:451.00 0.478 1
Chromium 190 ug/L 06/17/20 23:34 7440-47-306/17/20 16:452.00 1.49 1
Lead ND ug/L 06/17/20 23:34 7439-92-106/17/20 16:455.00 2.49 1
Selenium 1.52J ug/L 06/17/20 23:34 7782-49-2 J06/17/20 16:452.00 0.657 1
Silver ND ug/L 06/17/20 23:34 7440-22-406/17/20 16:452.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/15/20 11:27 7439-97-606/14/20 19:000.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/16/20 20:38 83-32-906/15/20 20:0810.0 1.4 1
Acenaphthylene ND ug/L 06/16/20 20:38 208-96-806/15/20 20:0810.0 1.5 1
Aniline ND ug/L 06/16/20 20:38 62-53-306/15/20 20:0810.0 1.6 1
Anthracene ND ug/L 06/16/20 20:38 120-12-706/15/20 20:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 06/16/20 20:38 56-55-306/15/20 20:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 06/16/20 20:38 50-32-806/15/20 20:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/16/20 20:38 205-99-206/15/20 20:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/16/20 20:38 191-24-206/15/20 20:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/16/20 20:38 207-08-906/15/20 20:0810.0 1.5 1
Benzoic Acid ND ug/L 06/16/20 20:38 65-85-006/15/20 20:0850.0 19.5 1
Benzyl alcohol ND ug/L 06/16/20 20:38 100-51-606/15/20 20:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/16/20 20:38 101-55-306/15/20 20:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 06/16/20 20:38 85-68-706/15/20 20:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/16/20 20:38 59-50-706/15/20 20:0810.0 2.8 1
4-Chloroaniline ND ug/L 06/16/20 20:38 106-47-806/15/20 20:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/16/20 20:38 111-91-106/15/20 20:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/16/20 20:38 111-44-406/15/20 20:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 06/16/20 20:38 91-58-706/15/20 20:0810.0 1.4 1
2-Chlorophenol ND ug/L 06/16/20 20:38 95-57-806/15/20 20:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/16/20 20:38 7005-72-306/15/20 20:0810.0 1.5 1
Chrysene ND ug/L 06/16/20 20:38 218-01-906/15/20 20:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/16/20 20:38 53-70-306/15/20 20:0810.0 1.6 1
Dibenzofuran ND ug/L 06/16/20 20:38 132-64-906/15/20 20:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/16/20 20:38 95-50-106/15/20 20:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/16/20 20:38 541-73-106/15/20 20:0810.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/16/20 20:38 106-46-706/15/20 20:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/16/20 20:38 91-94-106/15/20 20:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/16/20 20:38 120-83-206/15/20 20:0810.0 1.5 1
Diethylphthalate ND ug/L 06/16/20 20:38 84-66-206/15/20 20:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/16/20 20:38 105-67-906/15/20 20:0810.0 1.5 1
Dimethylphthalate ND ug/L 06/16/20 20:38 131-11-306/15/20 20:0810.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:GG-43 Lab ID:92481464005 Collected:06/10/20 11:15 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/16/20 20:38 84-74-206/15/20 20:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/16/20 20:38 534-52-106/15/20 20:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/16/20 20:38 51-28-506/15/20 20:0850.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/16/20 20:38 121-14-206/15/20 20:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/16/20 20:38 606-20-206/15/20 20:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/16/20 20:38 117-84-006/15/20 20:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/16/20 20:38 117-81-706/15/20 20:086.0 2.0 1
Fluoranthene ND ug/L 06/16/20 20:38 206-44-006/15/20 20:0810.0 1.6 1
Fluorene ND ug/L 06/16/20 20:38 86-73-706/15/20 20:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/16/20 20:38 87-68-306/15/20 20:0810.0 1.6 1
Hexachlorobenzene ND ug/L 06/16/20 20:38 118-74-106/15/20 20:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/16/20 20:38 77-47-406/15/20 20:0810.0 2.4 1
Hexachloroethane ND ug/L 06/16/20 20:38 67-72-106/15/20 20:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/16/20 20:38 193-39-506/15/20 20:0810.0 1.7 1
Isophorone ND ug/L 06/16/20 20:38 78-59-106/15/20 20:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 06/16/20 20:38 90-12-006/15/20 20:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 06/16/20 20:38 91-57-606/15/20 20:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/16/20 20:38 95-48-706/15/20 20:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/16/20 20:38 15831-10-406/15/20 20:0810.0 1.2 1
Naphthalene ND ug/L 06/16/20 20:38 91-20-306/15/20 20:0810.0 1.6 1
2-Nitroaniline ND ug/L 06/16/20 20:38 88-74-406/15/20 20:0820.0 3.0 1
3-Nitroaniline ND ug/L 06/16/20 20:38 99-09-206/15/20 20:0820.0 2.8 1
4-Nitroaniline ND ug/L 06/16/20 20:38 100-01-606/15/20 20:0820.0 3.1 1
Nitrobenzene ND ug/L 06/16/20 20:38 98-95-306/15/20 20:0810.0 1.5 1
2-Nitrophenol ND ug/L 06/16/20 20:38 88-75-506/15/20 20:0810.0 1.7 1
4-Nitrophenol ND ug/L 06/16/20 20:38 100-02-706/15/20 20:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/16/20 20:38 62-75-906/15/20 20:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/16/20 20:38 621-64-706/15/20 20:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/16/20 20:38 86-30-606/15/20 20:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/16/20 20:38 108-60-106/15/20 20:0810.0 1.3 1
Pentachlorophenol ND ug/L 06/16/20 20:38 87-86-506/15/20 20:0820.0 2.8 1
Phenanthrene ND ug/L 06/16/20 20:38 85-01-806/15/20 20:0810.0 1.4 1
Phenol ND ug/L 06/16/20 20:38 108-95-206/15/20 20:0810.0 1.5 1
Pyrene ND ug/L 06/16/20 20:38 129-00-006/15/20 20:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/16/20 20:38 120-82-106/15/20 20:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/16/20 20:38 95-95-406/15/20 20:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/16/20 20:38 88-06-206/15/20 20:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)58 %06/16/20 20:38 4165-60-006/15/20 20:0813-130 1
2-Fluorobiphenyl (S)54 %06/16/20 20:38 321-60-806/15/20 20:0813-130 1
Terphenyl-d14 (S)115 %06/16/20 20:38 1718-51-006/15/20 20:0825-130 1
Phenol-d6 (S)33 %06/16/20 20:38 13127-88-306/15/20 20:0810-130 1
2-Fluorophenol (S)41 %06/16/20 20:38 367-12-406/15/20 20:0810-130 1
2,4,6-Tribromophenol (S)62 %06/16/20 20:38 118-79-606/15/20 20:0810-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:GG-43 Lab ID:92481464005 Collected:06/10/20 11:15 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/17/20 03:48 67-64-125.0 6.2 1
Benzene ND ug/L 06/17/20 03:48 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/17/20 03:48 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/17/20 03:48 74-97-51.0 0.34 1
Bromodichloromethane 0.35J ug/L 06/17/20 03:48 75-27-41.0 0.26 1
Bromoform ND ug/L 06/17/20 03:48 75-25-21.0 0.62 1
Bromomethane 2.6 ug/L 06/17/20 03:48 74-83-9 v32.0 0.62 1
2-Butanone (MEK)ND ug/L 06/17/20 03:48 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/17/20 03:48 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/17/20 03:48 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/17/20 03:48 75-00-31.0 0.49 1
Chloroform ND ug/L 06/17/20 03:48 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/17/20 03:48 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 06/17/20 03:48 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/17/20 03:48 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/20 03:48 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/17/20 03:48 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/20 03:48 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/17/20 03:48 74-95-31.0 0.46 1
1,2-Dichlorobenzene 0.40J ug/L 06/17/20 03:48 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/17/20 03:48 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/17/20 03:48 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/17/20 03:48 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/17/20 03:48 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/17/20 03:48 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/17/20 03:48 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/17/20 03:48 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/17/20 03:48 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/17/20 03:48 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/17/20 03:48 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/17/20 03:48 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/17/20 03:48 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/17/20 03:48 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/17/20 03:48 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/17/20 03:48 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/17/20 03:48 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/17/20 03:48 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/17/20 03:48 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/17/20 03:48 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/17/20 03:48 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/20 03:48 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/17/20 03:48 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/17/20 03:48 91-20-31.0 0.35 1
Styrene ND ug/L 06/17/20 03:48 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/20 03:48 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:GG-43 Lab ID:92481464005 Collected:06/10/20 11:15 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/17/20 03:48 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/17/20 03:48 127-18-41.0 0.16 1
Toluene ND ug/L 06/17/20 03:48 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/17/20 03:48 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/17/20 03:48 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/17/20 03:48 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/17/20 03:48 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/17/20 03:48 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/17/20 03:48 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/17/20 03:48 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/17/20 03:48 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 06/17/20 03:48 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/17/20 03:48 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/17/20 03:48 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/17/20 03:48 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)89 %06/17/20 03:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %06/17/20 03:48 17060-07-070-130 1
Toluene-d8 (S)102 %06/17/20 03:48 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 3.97 ug/L 06/15/20 21:41 18540-29-906/15/20 21:410.500 0.200 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:RR-102 Lab ID:92481464006 Collected:06/10/20 15:00 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/17/20 23:37 7440-38-206/17/20 16:452.00 0.735 1
Barium 30.5 ug/L 06/17/20 23:37 7440-39-306/17/20 16:4520.0 7.78 1
Cadmium ND ug/L 06/17/20 23:37 7440-43-906/17/20 16:451.00 0.478 1
Chromium 69.4 ug/L 06/17/20 23:37 7440-47-306/17/20 16:452.00 1.49 1
Lead ND ug/L 06/17/20 23:37 7439-92-106/17/20 16:455.00 2.49 1
Selenium 1.12J ug/L 06/17/20 23:37 7782-49-2 J06/17/20 16:452.00 0.657 1
Silver ND ug/L 06/17/20 23:37 7440-22-406/17/20 16:452.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/15/20 11:29 7439-97-606/14/20 19:000.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/17/20 12:05 83-32-906/15/20 20:0810.0 1.4 1
Acenaphthylene ND ug/L 06/17/20 12:05 208-96-806/15/20 20:0810.0 1.5 1
Aniline ND ug/L 06/17/20 12:05 62-53-306/15/20 20:0810.0 1.6 1
Anthracene ND ug/L 06/17/20 12:05 120-12-706/15/20 20:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 06/17/20 12:05 56-55-306/15/20 20:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 06/17/20 12:05 50-32-806/15/20 20:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/17/20 12:05 205-99-206/15/20 20:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/17/20 12:05 191-24-206/15/20 20:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/17/20 12:05 207-08-906/15/20 20:0810.0 1.5 1
Benzoic Acid ND ug/L 06/17/20 12:05 65-85-006/15/20 20:0850.0 19.5 1
Benzyl alcohol ND ug/L 06/17/20 12:05 100-51-606/15/20 20:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/17/20 12:05 101-55-306/15/20 20:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 06/17/20 12:05 85-68-706/15/20 20:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/17/20 12:05 59-50-706/15/20 20:0810.0 2.8 1
4-Chloroaniline ND ug/L 06/17/20 12:05 106-47-806/15/20 20:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/17/20 12:05 111-91-106/15/20 20:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/17/20 12:05 111-44-406/15/20 20:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 06/17/20 12:05 91-58-706/15/20 20:0810.0 1.4 1
2-Chlorophenol ND ug/L 06/17/20 12:05 95-57-806/15/20 20:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/17/20 12:05 7005-72-306/15/20 20:0810.0 1.5 1
Chrysene ND ug/L 06/17/20 12:05 218-01-906/15/20 20:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/17/20 12:05 53-70-306/15/20 20:0810.0 1.6 1
Dibenzofuran ND ug/L 06/17/20 12:05 132-64-906/15/20 20:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/17/20 12:05 95-50-106/15/20 20:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/17/20 12:05 541-73-106/15/20 20:0810.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/17/20 12:05 106-46-706/15/20 20:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/17/20 12:05 91-94-106/15/20 20:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/17/20 12:05 120-83-206/15/20 20:0810.0 1.5 1
Diethylphthalate ND ug/L 06/17/20 12:05 84-66-206/15/20 20:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/17/20 12:05 105-67-906/15/20 20:0810.0 1.5 1
Dimethylphthalate ND ug/L 06/17/20 12:05 131-11-306/15/20 20:0810.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:RR-102 Lab ID:92481464006 Collected:06/10/20 15:00 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/17/20 12:05 84-74-206/15/20 20:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/17/20 12:05 534-52-106/15/20 20:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/17/20 12:05 51-28-506/15/20 20:0850.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/17/20 12:05 121-14-206/15/20 20:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/17/20 12:05 606-20-206/15/20 20:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/17/20 12:05 117-84-006/15/20 20:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/17/20 12:05 117-81-706/15/20 20:086.0 2.0 1
Fluoranthene ND ug/L 06/17/20 12:05 206-44-006/15/20 20:0810.0 1.6 1
Fluorene ND ug/L 06/17/20 12:05 86-73-706/15/20 20:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/17/20 12:05 87-68-306/15/20 20:0810.0 1.6 1
Hexachlorobenzene ND ug/L 06/17/20 12:05 118-74-106/15/20 20:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/17/20 12:05 77-47-406/15/20 20:0810.0 2.4 1
Hexachloroethane ND ug/L 06/17/20 12:05 67-72-106/15/20 20:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/17/20 12:05 193-39-506/15/20 20:0810.0 1.7 1
Isophorone ND ug/L 06/17/20 12:05 78-59-106/15/20 20:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 06/17/20 12:05 90-12-006/15/20 20:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 06/17/20 12:05 91-57-606/15/20 20:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/17/20 12:05 95-48-706/15/20 20:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/17/20 12:05 15831-10-406/15/20 20:0810.0 1.2 1
Naphthalene ND ug/L 06/17/20 12:05 91-20-306/15/20 20:0810.0 1.6 1
2-Nitroaniline ND ug/L 06/17/20 12:05 88-74-406/15/20 20:0820.0 3.0 1
3-Nitroaniline ND ug/L 06/17/20 12:05 99-09-206/15/20 20:0820.0 2.8 1
4-Nitroaniline ND ug/L 06/17/20 12:05 100-01-606/15/20 20:0820.0 3.1 1
Nitrobenzene ND ug/L 06/17/20 12:05 98-95-306/15/20 20:0810.0 1.5 1
2-Nitrophenol ND ug/L 06/17/20 12:05 88-75-506/15/20 20:0810.0 1.7 1
4-Nitrophenol ND ug/L 06/17/20 12:05 100-02-706/15/20 20:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/17/20 12:05 62-75-906/15/20 20:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/17/20 12:05 621-64-706/15/20 20:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/17/20 12:05 86-30-606/15/20 20:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/17/20 12:05 108-60-106/15/20 20:0810.0 1.3 1
Pentachlorophenol ND ug/L 06/17/20 12:05 87-86-506/15/20 20:0820.0 2.8 1
Phenanthrene ND ug/L 06/17/20 12:05 85-01-806/15/20 20:0810.0 1.4 1
Phenol ND ug/L 06/17/20 12:05 108-95-206/15/20 20:0810.0 1.5 1
Pyrene ND ug/L 06/17/20 12:05 129-00-006/15/20 20:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/17/20 12:05 120-82-106/15/20 20:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/17/20 12:05 95-95-406/15/20 20:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/17/20 12:05 88-06-206/15/20 20:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)75 %06/17/20 12:05 4165-60-006/15/20 20:0813-130 1
2-Fluorobiphenyl (S)71 %06/17/20 12:05 321-60-806/15/20 20:0813-130 1
Terphenyl-d14 (S)122 %06/17/20 12:05 1718-51-006/15/20 20:0825-130 1
Phenol-d6 (S)41 %06/17/20 12:05 13127-88-306/15/20 20:0810-130 1
2-Fluorophenol (S)54 %06/17/20 12:05 367-12-406/15/20 20:0810-130 1
2,4,6-Tribromophenol (S)84 %06/17/20 12:05 118-79-606/15/20 20:0810-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:RR-102 Lab ID:92481464006 Collected:06/10/20 15:00 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/17/20 04:06 67-64-125.0 6.2 1
Benzene ND ug/L 06/17/20 04:06 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/17/20 04:06 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/17/20 04:06 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/17/20 04:06 75-27-41.0 0.26 1
Bromoform ND ug/L 06/17/20 04:06 75-25-21.0 0.62 1
Bromomethane ND ug/L 06/17/20 04:06 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 06/17/20 04:06 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/17/20 04:06 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/17/20 04:06 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/17/20 04:06 75-00-31.0 0.49 1
Chloroform ND ug/L 06/17/20 04:06 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/17/20 04:06 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 06/17/20 04:06 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/17/20 04:06 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/20 04:06 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/17/20 04:06 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/20 04:06 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/17/20 04:06 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/17/20 04:06 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/17/20 04:06 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/17/20 04:06 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/17/20 04:06 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/17/20 04:06 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/17/20 04:06 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/17/20 04:06 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/17/20 04:06 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/17/20 04:06 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/17/20 04:06 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/17/20 04:06 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/17/20 04:06 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/17/20 04:06 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/17/20 04:06 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/17/20 04:06 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/17/20 04:06 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/17/20 04:06 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/17/20 04:06 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/17/20 04:06 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/17/20 04:06 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/17/20 04:06 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/20 04:06 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/17/20 04:06 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/17/20 04:06 91-20-31.0 0.35 1
Styrene ND ug/L 06/17/20 04:06 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/20 04:06 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:RR-102 Lab ID:92481464006 Collected:06/10/20 15:00 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/17/20 04:06 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/17/20 04:06 127-18-41.0 0.16 1
Toluene ND ug/L 06/17/20 04:06 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/17/20 04:06 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/17/20 04:06 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/17/20 04:06 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/17/20 04:06 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/17/20 04:06 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/17/20 04:06 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/17/20 04:06 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/17/20 04:06 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 06/17/20 04:06 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/17/20 04:06 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/17/20 04:06 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/17/20 04:06 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)95 %06/17/20 04:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %06/17/20 04:06 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/20 04:06 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 9.51 ug/L 06/15/20 21:48 18540-29-906/15/20 21:481.00 0.400 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:TT-34 Lab ID:92481464007 Collected:06/10/20 09:25 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/17/20 23:40 7440-38-206/17/20 16:452.00 0.735 1
Barium 108 ug/L 06/17/20 23:40 7440-39-306/17/20 16:4520.0 7.78 1
Cadmium ND ug/L 06/17/20 23:40 7440-43-906/17/20 16:451.00 0.478 1
Chromium 4.96 ug/L 06/17/20 23:40 7440-47-306/17/20 16:452.00 1.49 1
Lead 3.74J ug/L 06/17/20 23:40 7439-92-1 J06/17/20 16:455.00 2.49 1
Selenium 1.22J ug/L 06/17/20 23:40 7782-49-2 J06/17/20 16:452.00 0.657 1
Silver ND ug/L 06/17/20 23:40 7440-22-406/17/20 16:452.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/15/20 11:47 7439-97-606/14/20 19:000.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/17/20 12:34 83-32-906/15/20 20:0810.0 1.4 1
Acenaphthylene ND ug/L 06/17/20 12:34 208-96-806/15/20 20:0810.0 1.5 1
Aniline ND ug/L 06/17/20 12:34 62-53-306/15/20 20:0810.0 1.6 1
Anthracene ND ug/L 06/17/20 12:34 120-12-706/15/20 20:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 06/17/20 12:34 56-55-306/15/20 20:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 06/17/20 12:34 50-32-806/15/20 20:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/17/20 12:34 205-99-206/15/20 20:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/17/20 12:34 191-24-206/15/20 20:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/17/20 12:34 207-08-906/15/20 20:0810.0 1.5 1
Benzoic Acid ND ug/L 06/17/20 12:34 65-85-006/15/20 20:0850.0 19.5 1
Benzyl alcohol ND ug/L 06/17/20 12:34 100-51-606/15/20 20:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/17/20 12:34 101-55-306/15/20 20:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 06/17/20 12:34 85-68-706/15/20 20:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/17/20 12:34 59-50-706/15/20 20:0810.0 2.8 1
4-Chloroaniline ND ug/L 06/17/20 12:34 106-47-806/15/20 20:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/17/20 12:34 111-91-106/15/20 20:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/17/20 12:34 111-44-406/15/20 20:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 06/17/20 12:34 91-58-706/15/20 20:0810.0 1.4 1
2-Chlorophenol ND ug/L 06/17/20 12:34 95-57-806/15/20 20:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/17/20 12:34 7005-72-306/15/20 20:0810.0 1.5 1
Chrysene ND ug/L 06/17/20 12:34 218-01-906/15/20 20:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/17/20 12:34 53-70-306/15/20 20:0810.0 1.6 1
Dibenzofuran ND ug/L 06/17/20 12:34 132-64-906/15/20 20:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/17/20 12:34 95-50-106/15/20 20:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/17/20 12:34 541-73-106/15/20 20:0810.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/17/20 12:34 106-46-706/15/20 20:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/17/20 12:34 91-94-106/15/20 20:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/17/20 12:34 120-83-206/15/20 20:0810.0 1.5 1
Diethylphthalate ND ug/L 06/17/20 12:34 84-66-206/15/20 20:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/17/20 12:34 105-67-906/15/20 20:0810.0 1.5 1
Dimethylphthalate ND ug/L 06/17/20 12:34 131-11-306/15/20 20:0810.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:TT-34 Lab ID:92481464007 Collected:06/10/20 09:25 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/17/20 12:34 84-74-206/15/20 20:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/17/20 12:34 534-52-106/15/20 20:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/17/20 12:34 51-28-506/15/20 20:0850.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/17/20 12:34 121-14-206/15/20 20:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/17/20 12:34 606-20-206/15/20 20:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/17/20 12:34 117-84-006/15/20 20:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/17/20 12:34 117-81-706/15/20 20:086.0 2.0 1
Fluoranthene ND ug/L 06/17/20 12:34 206-44-006/15/20 20:0810.0 1.6 1
Fluorene ND ug/L 06/17/20 12:34 86-73-706/15/20 20:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/17/20 12:34 87-68-306/15/20 20:0810.0 1.6 1
Hexachlorobenzene ND ug/L 06/17/20 12:34 118-74-106/15/20 20:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/17/20 12:34 77-47-406/15/20 20:0810.0 2.4 1
Hexachloroethane ND ug/L 06/17/20 12:34 67-72-106/15/20 20:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/17/20 12:34 193-39-506/15/20 20:0810.0 1.7 1
Isophorone ND ug/L 06/17/20 12:34 78-59-106/15/20 20:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 06/17/20 12:34 90-12-006/15/20 20:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 06/17/20 12:34 91-57-606/15/20 20:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/17/20 12:34 95-48-706/15/20 20:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/17/20 12:34 15831-10-406/15/20 20:0810.0 1.2 1
Naphthalene ND ug/L 06/17/20 12:34 91-20-306/15/20 20:0810.0 1.6 1
2-Nitroaniline ND ug/L 06/17/20 12:34 88-74-406/15/20 20:0820.0 3.0 1
3-Nitroaniline ND ug/L 06/17/20 12:34 99-09-206/15/20 20:0820.0 2.8 1
4-Nitroaniline ND ug/L 06/17/20 12:34 100-01-606/15/20 20:0820.0 3.1 1
Nitrobenzene ND ug/L 06/17/20 12:34 98-95-306/15/20 20:0810.0 1.5 1
2-Nitrophenol ND ug/L 06/17/20 12:34 88-75-506/15/20 20:0810.0 1.7 1
4-Nitrophenol ND ug/L 06/17/20 12:34 100-02-706/15/20 20:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/17/20 12:34 62-75-906/15/20 20:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/17/20 12:34 621-64-706/15/20 20:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/17/20 12:34 86-30-606/15/20 20:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/17/20 12:34 108-60-106/15/20 20:0810.0 1.3 1
Pentachlorophenol ND ug/L 06/17/20 12:34 87-86-506/15/20 20:0820.0 2.8 1
Phenanthrene ND ug/L 06/17/20 12:34 85-01-806/15/20 20:0810.0 1.4 1
Phenol ND ug/L 06/17/20 12:34 108-95-206/15/20 20:0810.0 1.5 1
Pyrene ND ug/L 06/17/20 12:34 129-00-006/15/20 20:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/17/20 12:34 120-82-106/15/20 20:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/17/20 12:34 95-95-406/15/20 20:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/17/20 12:34 88-06-206/15/20 20:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)106 %06/17/20 12:34 4165-60-006/15/20 20:0813-130 1
2-Fluorobiphenyl (S)99 %06/17/20 12:34 321-60-806/15/20 20:0813-130 1
Terphenyl-d14 (S)145 %06/17/20 12:34 1718-51-0 S306/15/20 20:0825-130 1
Phenol-d6 (S)57 %06/17/20 12:34 13127-88-306/15/20 20:0810-130 1
2-Fluorophenol (S)76 %06/17/20 12:34 367-12-406/15/20 20:0810-130 1
2,4,6-Tribromophenol (S)102 %06/17/20 12:34 118-79-606/15/20 20:0810-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:TT-34 Lab ID:92481464007 Collected:06/10/20 09:25 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/17/20 04:24 67-64-125.0 6.2 1
Benzene ND ug/L 06/17/20 04:24 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/17/20 04:24 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/17/20 04:24 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/17/20 04:24 75-27-41.0 0.26 1
Bromoform ND ug/L 06/17/20 04:24 75-25-21.0 0.62 1
Bromomethane ND ug/L 06/17/20 04:24 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 06/17/20 04:24 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/17/20 04:24 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/17/20 04:24 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/17/20 04:24 75-00-31.0 0.49 1
Chloroform ND ug/L 06/17/20 04:24 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/17/20 04:24 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 06/17/20 04:24 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/17/20 04:24 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/17/20 04:24 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/17/20 04:24 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/17/20 04:24 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/17/20 04:24 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/17/20 04:24 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/17/20 04:24 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/17/20 04:24 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/17/20 04:24 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/17/20 04:24 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/17/20 04:24 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/17/20 04:24 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/17/20 04:24 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/17/20 04:24 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/17/20 04:24 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/17/20 04:24 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/17/20 04:24 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/17/20 04:24 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/17/20 04:24 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/17/20 04:24 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/17/20 04:24 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/17/20 04:24 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/17/20 04:24 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/17/20 04:24 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/17/20 04:24 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/17/20 04:24 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/20 04:24 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/17/20 04:24 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/17/20 04:24 91-20-31.0 0.35 1
Styrene ND ug/L 06/17/20 04:24 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/17/20 04:24 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:TT-34 Lab ID:92481464007 Collected:06/10/20 09:25 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/17/20 04:24 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/17/20 04:24 127-18-41.0 0.16 1
Toluene ND ug/L 06/17/20 04:24 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/17/20 04:24 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/17/20 04:24 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/17/20 04:24 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/17/20 04:24 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/17/20 04:24 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/17/20 04:24 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/17/20 04:24 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/17/20 04:24 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 06/17/20 04:24 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/17/20 04:24 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/17/20 04:24 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/17/20 04:24 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)101 %06/17/20 04:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)107 %06/17/20 04:24 17060-07-070-130 1
Toluene-d8 (S)100 %06/17/20 04:24 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.160 ug/L 06/15/20 20:15 18540-29-906/15/20 20:150.100 0.0400 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:YY-37 Lab ID:92481464008 Collected:06/10/20 11:55 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/17/20 23:44 7440-38-206/17/20 16:452.00 0.735 1
Barium 93.3 ug/L 06/17/20 23:44 7440-39-306/17/20 16:4520.0 7.78 1
Cadmium ND ug/L 06/17/20 23:44 7440-43-906/17/20 16:451.00 0.478 1
Chromium ND ug/L 06/17/20 23:44 7440-47-306/17/20 16:452.00 1.49 1
Lead ND ug/L 06/17/20 23:44 7439-92-106/17/20 16:455.00 2.49 1
Selenium 1.83J ug/L 06/17/20 23:44 7782-49-2 J06/17/20 16:452.00 0.657 1
Silver ND ug/L 06/17/20 23:44 7440-22-406/17/20 16:452.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/15/20 10:44 7439-97-606/14/20 19:000.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/17/20 13:03 83-32-906/15/20 20:0810.0 1.4 1
Acenaphthylene ND ug/L 06/17/20 13:03 208-96-806/15/20 20:0810.0 1.5 1
Aniline ND ug/L 06/17/20 13:03 62-53-306/15/20 20:0810.0 1.6 1
Anthracene ND ug/L 06/17/20 13:03 120-12-706/15/20 20:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 06/17/20 13:03 56-55-306/15/20 20:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 06/17/20 13:03 50-32-806/15/20 20:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/17/20 13:03 205-99-206/15/20 20:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/17/20 13:03 191-24-206/15/20 20:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/17/20 13:03 207-08-906/15/20 20:0810.0 1.5 1
Benzoic Acid ND ug/L 06/17/20 13:03 65-85-006/15/20 20:0850.0 19.5 1
Benzyl alcohol ND ug/L 06/17/20 13:03 100-51-606/15/20 20:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/17/20 13:03 101-55-306/15/20 20:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 06/17/20 13:03 85-68-706/15/20 20:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/17/20 13:03 59-50-706/15/20 20:0810.0 2.8 1
4-Chloroaniline ND ug/L 06/17/20 13:03 106-47-806/15/20 20:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/17/20 13:03 111-91-106/15/20 20:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/17/20 13:03 111-44-406/15/20 20:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 06/17/20 13:03 91-58-706/15/20 20:0810.0 1.4 1
2-Chlorophenol ND ug/L 06/17/20 13:03 95-57-806/15/20 20:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/17/20 13:03 7005-72-306/15/20 20:0810.0 1.5 1
Chrysene ND ug/L 06/17/20 13:03 218-01-906/15/20 20:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/17/20 13:03 53-70-306/15/20 20:0810.0 1.6 1
Dibenzofuran ND ug/L 06/17/20 13:03 132-64-906/15/20 20:0810.0 1.3 1
1,2-Dichlorobenzene 185 ug/L 06/17/20 14:30 95-50-106/15/20 20:0820.0 2.7 2
1,3-Dichlorobenzene ND ug/L 06/17/20 13:03 541-73-106/15/20 20:0810.0 1.4 1
1,4-Dichlorobenzene 3.1J ug/L 06/17/20 13:03 106-46-706/15/20 20:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/17/20 13:03 91-94-106/15/20 20:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/17/20 13:03 120-83-206/15/20 20:0810.0 1.5 1
Diethylphthalate ND ug/L 06/17/20 13:03 84-66-206/15/20 20:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/17/20 13:03 105-67-906/15/20 20:0810.0 1.5 1
Dimethylphthalate ND ug/L 06/17/20 13:03 131-11-306/15/20 20:0810.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:YY-37 Lab ID:92481464008 Collected:06/10/20 11:55 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/17/20 13:03 84-74-206/15/20 20:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/17/20 13:03 534-52-106/15/20 20:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/17/20 13:03 51-28-506/15/20 20:0850.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/17/20 13:03 121-14-206/15/20 20:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/17/20 13:03 606-20-206/15/20 20:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/17/20 13:03 117-84-006/15/20 20:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/17/20 13:03 117-81-706/15/20 20:086.0 2.0 1
Fluoranthene ND ug/L 06/17/20 13:03 206-44-006/15/20 20:0810.0 1.6 1
Fluorene ND ug/L 06/17/20 13:03 86-73-706/15/20 20:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/17/20 13:03 87-68-306/15/20 20:0810.0 1.6 1
Hexachlorobenzene ND ug/L 06/17/20 13:03 118-74-106/15/20 20:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/17/20 13:03 77-47-406/15/20 20:0810.0 2.4 1
Hexachloroethane ND ug/L 06/17/20 13:03 67-72-106/15/20 20:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/17/20 13:03 193-39-506/15/20 20:0810.0 1.7 1
Isophorone ND ug/L 06/17/20 13:03 78-59-106/15/20 20:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 06/17/20 13:03 90-12-006/15/20 20:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 06/17/20 13:03 91-57-606/15/20 20:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/17/20 13:03 95-48-706/15/20 20:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/17/20 13:03 15831-10-406/15/20 20:0810.0 1.2 1
Naphthalene ND ug/L 06/17/20 13:03 91-20-306/15/20 20:0810.0 1.6 1
2-Nitroaniline ND ug/L 06/17/20 13:03 88-74-406/15/20 20:0820.0 3.0 1
3-Nitroaniline ND ug/L 06/17/20 13:03 99-09-206/15/20 20:0820.0 2.8 1
4-Nitroaniline ND ug/L 06/17/20 13:03 100-01-606/15/20 20:0820.0 3.1 1
Nitrobenzene ND ug/L 06/17/20 13:03 98-95-306/15/20 20:0810.0 1.5 1
2-Nitrophenol ND ug/L 06/17/20 13:03 88-75-506/15/20 20:0810.0 1.7 1
4-Nitrophenol ND ug/L 06/17/20 13:03 100-02-706/15/20 20:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/17/20 13:03 62-75-906/15/20 20:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/17/20 13:03 621-64-706/15/20 20:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/17/20 13:03 86-30-606/15/20 20:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/17/20 13:03 108-60-106/15/20 20:0810.0 1.3 1
Pentachlorophenol ND ug/L 06/17/20 13:03 87-86-506/15/20 20:0820.0 2.8 1
Phenanthrene ND ug/L 06/17/20 13:03 85-01-806/15/20 20:0810.0 1.4 1
Phenol 2.3J ug/L 06/17/20 13:03 108-95-206/15/20 20:0810.0 1.5 1
Pyrene ND ug/L 06/17/20 13:03 129-00-006/15/20 20:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/17/20 13:03 120-82-106/15/20 20:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/17/20 13:03 95-95-406/15/20 20:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/17/20 13:03 88-06-206/15/20 20:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)102 %06/17/20 13:03 4165-60-006/15/20 20:0813-130 1
2-Fluorobiphenyl (S)97 %06/17/20 13:03 321-60-806/15/20 20:0813-130 1
Terphenyl-d14 (S)139 %06/17/20 13:03 1718-51-0 S006/15/20 20:0825-130 1
Phenol-d6 (S)57 %06/17/20 13:03 13127-88-306/15/20 20:0810-130 1
2-Fluorophenol (S)76 %06/17/20 13:03 367-12-406/15/20 20:0810-130 1
2,4,6-Tribromophenol (S)98 %06/17/20 13:03 118-79-606/15/20 20:0810-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:YY-37 Lab ID:92481464008 Collected:06/10/20 11:55 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/17/20 15:34 67-64-150.0 12.3 2
Benzene ND ug/L 06/17/20 15:34 71-43-22.0 0.30 2
Bromobenzene ND ug/L 06/17/20 15:34 108-86-12.0 0.44 2
Bromochloromethane ND ug/L 06/17/20 15:34 74-97-52.0 0.69 2
Bromodichloromethane ND ug/L 06/17/20 15:34 75-27-42.0 0.51 2
Bromoform ND ug/L 06/17/20 15:34 75-25-22.0 1.2 2
Bromomethane ND ug/L 06/17/20 15:34 74-83-9 v24.0 1.2 2
2-Butanone (MEK)ND ug/L 06/17/20 15:34 78-93-310.0 6.7 2
Carbon tetrachloride ND ug/L 06/17/20 15:34 56-23-52.0 0.45 2
Chlorobenzene 53.4 ug/L 06/17/20 15:34 108-90-72.0 0.47 2
Chloroethane ND ug/L 06/17/20 15:34 75-00-32.0 0.98 2
Chloroform ND ug/L 06/17/20 15:34 67-66-310.0 4.7 2
Chloromethane ND ug/L 06/17/20 15:34 74-87-3 v22.0 0.78 2
2-Chlorotoluene ND ug/L 06/17/20 15:34 95-49-82.0 0.41 2
4-Chlorotoluene ND ug/L 06/17/20 15:34 106-43-42.0 0.41 2
1,2-Dibromo-3-chloropropane ND ug/L 06/17/20 15:34 96-12-810.0 0.51 2
Dibromochloromethane ND ug/L 06/17/20 15:34 124-48-12.0 0.83 2
1,2-Dibromoethane (EDB)ND ug/L 06/17/20 15:34 106-93-42.0 0.52 2
Dibromomethane ND ug/L 06/17/20 15:34 74-95-32.0 0.92 2
1,2-Dichlorobenzene 248 ug/L 06/17/20 15:34 95-50-12.0 0.58 2
1,3-Dichlorobenzene ND ug/L 06/17/20 15:34 541-73-12.0 0.43 2
1,4-Dichlorobenzene 3.6 ug/L 06/17/20 15:34 106-46-72.0 0.52 2
Dichlorodifluoromethane ND ug/L 06/17/20 15:34 75-71-82.0 0.45 2
1,1-Dichloroethane ND ug/L 06/17/20 15:34 75-34-32.0 0.54 2
1,2-Dichloroethane ND ug/L 06/17/20 15:34 107-06-22.0 0.67 2
1,1-Dichloroethene ND ug/L 06/17/20 15:34 75-35-42.0 0.49 2
cis-1,2-Dichloroethene 1.0J ug/L 06/17/20 15:34 156-59-22.0 0.58 2
trans-1,2-Dichloroethene ND ug/L 06/17/20 15:34 156-60-52.0 0.51 2
1,2-Dichloropropane ND ug/L 06/17/20 15:34 78-87-52.0 0.37 2
1,3-Dichloropropane ND ug/L 06/17/20 15:34 142-28-92.0 0.32 2
2,2-Dichloropropane ND ug/L 06/17/20 15:34 594-20-72.0 0.54 2
1,1-Dichloropropene ND ug/L 06/17/20 15:34 563-58-62.0 0.43 2
cis-1,3-Dichloropropene ND ug/L 06/17/20 15:34 10061-01-52.0 0.59 2
trans-1,3-Dichloropropene ND ug/L 06/17/20 15:34 10061-02-62.0 0.62 2
Diisopropyl ether ND ug/L 06/17/20 15:34 108-20-32.0 0.44 2
Ethylbenzene ND ug/L 06/17/20 15:34 100-41-42.0 0.51 2
Hexachloro-1,3-butadiene ND ug/L 06/17/20 15:34 87-68-32.0 0.88 2
2-Hexanone ND ug/L 06/17/20 15:34 591-78-610.0 1.1 2
p-Isopropyltoluene ND ug/L 06/17/20 15:34 99-87-62.0 0.42 2
Methylene Chloride ND ug/L 06/17/20 15:34 75-09-210.0 7.4 2
4-Methyl-2-pentanone (MIBK)ND ug/L 06/17/20 15:34 108-10-110.0 9.1 2
Methyl-tert-butyl ether ND ug/L 06/17/20 15:34 1634-04-42.0 0.55 2
Naphthalene ND ug/L 06/17/20 15:34 91-20-32.0 0.70 2
Styrene ND ug/L 06/17/20 15:34 100-42-52.0 0.53 2
1,1,1,2-Tetrachloroethane ND ug/L 06/17/20 15:34 630-20-62.0 0.68 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:YY-37 Lab ID:92481464008 Collected:06/10/20 11:55 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/17/20 15:34 79-34-52.0 0.44 2
Tetrachloroethene ND ug/L 06/17/20 15:34 127-18-42.0 0.32 2
Toluene ND ug/L 06/17/20 15:34 108-88-32.0 0.49 2
1,2,3-Trichlorobenzene ND ug/L 06/17/20 15:34 87-61-62.0 0.69 2
1,2,4-Trichlorobenzene ND ug/L 06/17/20 15:34 120-82-12.0 0.44 2
1,1,1-Trichloroethane ND ug/L 06/17/20 15:34 71-55-62.0 0.35 2
1,1,2-Trichloroethane ND ug/L 06/17/20 15:34 79-00-52.0 0.47 2
Trichloroethene ND ug/L 06/17/20 15:34 79-01-62.0 0.44 2
Trichlorofluoromethane ND ug/L 06/17/20 15:34 75-69-42.0 0.62 2
1,2,3-Trichloropropane ND ug/L 06/17/20 15:34 96-18-42.0 0.69 2
Vinyl acetate ND ug/L 06/17/20 15:34 108-05-44.0 2.9 2
Vinyl chloride ND ug/L 06/17/20 15:34 75-01-42.0 0.48 2
Xylene (Total)ND ug/L 06/17/20 15:34 1330-20-72.0 1.3 2
m&p-Xylene ND ug/L 06/17/20 15:34 179601-23-14.0 0.82 2
o-Xylene ND ug/L 06/17/20 15:34 95-47-62.0 0.44 2
Surrogates
4-Bromofluorobenzene (S)96 %06/17/20 15:34 460-00-470-130 2
1,2-Dichloroethane-d4 (S)103 %06/17/20 15:34 17060-07-070-130 2
Toluene-d8 (S)101 %06/17/20 15:34 2037-26-570-130 2
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 06/15/20 20:25 18540-29-906/15/20 20:250.100 0.0400 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:GW-Dup Lab ID:92481464009 Collected:06/10/20 00:00 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 1.18J ug/L 06/18/20 00:26 7440-38-2 J06/17/20 16:452.00 0.735 1
Barium 118 ug/L 06/18/20 00:26 7440-39-306/17/20 16:4520.0 7.78 1
Cadmium 0.629J ug/L 06/18/20 00:26 7440-43-9 J06/17/20 16:451.00 0.478 1
Chromium ND ug/L 06/18/20 00:26 7440-47-306/17/20 16:452.00 1.49 1
Lead ND ug/L 06/18/20 00:26 7439-92-106/17/20 16:455.00 2.49 1
Selenium ND ug/L 06/18/20 02:13 7782-49-206/17/20 16:452.00 0.657 1
Silver ND ug/L 06/18/20 00:26 7440-22-406/17/20 16:452.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/15/20 21:13 7439-97-606/15/20 11:220.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/17/20 13:32 83-32-906/15/20 20:0810.0 1.4 1
Acenaphthylene ND ug/L 06/17/20 13:32 208-96-806/15/20 20:0810.0 1.5 1
Aniline ND ug/L 06/17/20 13:32 62-53-306/15/20 20:0810.0 1.6 1
Anthracene ND ug/L 06/17/20 13:32 120-12-706/15/20 20:0810.0 1.6 1
Benzo(a)anthracene ND ug/L 06/17/20 13:32 56-55-306/15/20 20:0810.0 1.5 1
Benzo(a)pyrene ND ug/L 06/17/20 13:32 50-32-806/15/20 20:0810.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/17/20 13:32 205-99-206/15/20 20:0810.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/17/20 13:32 191-24-206/15/20 20:0810.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/17/20 13:32 207-08-906/15/20 20:0810.0 1.5 1
Benzoic Acid ND ug/L 06/17/20 13:32 65-85-006/15/20 20:0850.0 19.5 1
Benzyl alcohol ND ug/L 06/17/20 13:32 100-51-606/15/20 20:0820.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/17/20 13:32 101-55-306/15/20 20:0810.0 1.2 1
Butylbenzylphthalate ND ug/L 06/17/20 13:32 85-68-706/15/20 20:0810.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/17/20 13:32 59-50-706/15/20 20:0810.0 2.8 1
4-Chloroaniline ND ug/L 06/17/20 13:32 106-47-806/15/20 20:0820.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/17/20 13:32 111-91-106/15/20 20:0810.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/17/20 13:32 111-44-406/15/20 20:0810.0 1.7 1
2-Chloronaphthalene ND ug/L 06/17/20 13:32 91-58-706/15/20 20:0810.0 1.4 1
2-Chlorophenol 13.5 ug/L 06/17/20 13:32 95-57-806/15/20 20:0810.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/17/20 13:32 7005-72-306/15/20 20:0810.0 1.5 1
Chrysene ND ug/L 06/17/20 13:32 218-01-906/15/20 20:0810.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/17/20 13:32 53-70-306/15/20 20:0810.0 1.6 1
Dibenzofuran ND ug/L 06/17/20 13:32 132-64-906/15/20 20:0810.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/17/20 13:32 95-50-106/15/20 20:0810.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/17/20 13:32 541-73-106/15/20 20:0810.0 1.4 1
1,4-Dichlorobenzene 93.5 ug/L 06/17/20 13:32 106-46-706/15/20 20:0810.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/17/20 13:32 91-94-106/15/20 20:0820.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/17/20 13:32 120-83-206/15/20 20:0810.0 1.5 1
Diethylphthalate ND ug/L 06/17/20 13:32 84-66-206/15/20 20:0810.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/17/20 13:32 105-67-906/15/20 20:0810.0 1.5 1
Dimethylphthalate ND ug/L 06/17/20 13:32 131-11-306/15/20 20:0810.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:GW-Dup Lab ID:92481464009 Collected:06/10/20 00:00 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/17/20 13:32 84-74-206/15/20 20:0810.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/17/20 13:32 534-52-106/15/20 20:0820.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/17/20 13:32 51-28-506/15/20 20:0850.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/17/20 13:32 121-14-206/15/20 20:0810.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/17/20 13:32 606-20-206/15/20 20:0810.0 1.7 1
Di-n-octylphthalate ND ug/L 06/17/20 13:32 117-84-006/15/20 20:0810.0 2.2 1
bis(2-Ethylhexyl)phthalate 4.6J ug/L 06/17/20 13:32 117-81-706/15/20 20:086.0 2.0 1
Fluoranthene ND ug/L 06/17/20 13:32 206-44-006/15/20 20:0810.0 1.6 1
Fluorene ND ug/L 06/17/20 13:32 86-73-706/15/20 20:0810.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/17/20 13:32 87-68-306/15/20 20:0810.0 1.6 1
Hexachlorobenzene ND ug/L 06/17/20 13:32 118-74-106/15/20 20:0810.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/17/20 13:32 77-47-406/15/20 20:0810.0 2.4 1
Hexachloroethane ND ug/L 06/17/20 13:32 67-72-106/15/20 20:0810.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/17/20 13:32 193-39-506/15/20 20:0810.0 1.7 1
Isophorone ND ug/L 06/17/20 13:32 78-59-106/15/20 20:0810.0 1.3 1
1-Methylnaphthalene ND ug/L 06/17/20 13:32 90-12-006/15/20 20:0810.0 1.4 1
2-Methylnaphthalene ND ug/L 06/17/20 13:32 91-57-606/15/20 20:0810.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/17/20 13:32 95-48-706/15/20 20:0810.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/17/20 13:32 15831-10-406/15/20 20:0810.0 1.2 1
Naphthalene ND ug/L 06/17/20 13:32 91-20-306/15/20 20:0810.0 1.6 1
2-Nitroaniline ND ug/L 06/17/20 13:32 88-74-406/15/20 20:0820.0 3.0 1
3-Nitroaniline ND ug/L 06/17/20 13:32 99-09-206/15/20 20:0820.0 2.8 1
4-Nitroaniline ND ug/L 06/17/20 13:32 100-01-606/15/20 20:0820.0 3.1 1
Nitrobenzene ND ug/L 06/17/20 13:32 98-95-306/15/20 20:0810.0 1.5 1
2-Nitrophenol ND ug/L 06/17/20 13:32 88-75-506/15/20 20:0810.0 1.7 1
4-Nitrophenol ND ug/L 06/17/20 13:32 100-02-706/15/20 20:0850.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/17/20 13:32 62-75-906/15/20 20:0810.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/17/20 13:32 621-64-706/15/20 20:0810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/17/20 13:32 86-30-606/15/20 20:0810.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/17/20 13:32 108-60-106/15/20 20:0810.0 1.3 1
Pentachlorophenol ND ug/L 06/17/20 13:32 87-86-506/15/20 20:0820.0 2.8 1
Phenanthrene ND ug/L 06/17/20 13:32 85-01-806/15/20 20:0810.0 1.4 1
Phenol 3.3J ug/L 06/17/20 13:32 108-95-206/15/20 20:0810.0 1.5 1
Pyrene ND ug/L 06/17/20 13:32 129-00-006/15/20 20:0810.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/17/20 13:32 120-82-106/15/20 20:0810.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/17/20 13:32 95-95-406/15/20 20:0810.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/17/20 13:32 88-06-206/15/20 20:0810.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)77 %06/17/20 13:32 4165-60-006/15/20 20:0813-130 1
2-Fluorobiphenyl (S)76 %06/17/20 13:32 321-60-806/15/20 20:0813-130 1
Terphenyl-d14 (S)119 %06/17/20 13:32 1718-51-006/15/20 20:0825-130 1
Phenol-d6 (S)43 %06/17/20 13:32 13127-88-306/15/20 20:0810-130 1
2-Fluorophenol (S)52 %06/17/20 13:32 367-12-406/15/20 20:0810-130 1
2,4,6-Tribromophenol (S)74 %06/17/20 13:32 118-79-606/15/20 20:0810-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:GW-Dup Lab ID:92481464009 Collected:06/10/20 00:00 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/18/20 16:36 67-64-12500617100
Benzene 58.4J ug/L 06/18/20 16:36 71-43-210015.0 100
Bromobenzene ND ug/L 06/18/20 16:36 108-86-110022.0 100
Bromochloromethane ND ug/L 06/18/20 16:36 74-97-510034.3 100
Bromodichloromethane ND ug/L 06/18/20 16:36 75-27-410025.6 100
Bromoform ND ug/L 06/18/20 16:36 75-25-210061.7 100
Bromomethane ND ug/L 06/18/20 16:36 74-83-920062.0 100
2-Butanone (MEK)ND ug/L 06/18/20 16:36 78-93-3500333100
Carbon tetrachloride ND ug/L 06/18/20 16:36 56-23-510022.4 100
Chlorobenzene 12500 ug/L 06/18/20 16:36 108-90-710023.3 100
Chloroethane ND ug/L 06/18/20 16:36 75-00-3 v210049.0 100
Chloroform ND ug/L 06/18/20 16:36 67-66-3500234100
Chloromethane ND ug/L 06/18/20 16:36 74-87-310038.9 100
2-Chlorotoluene ND ug/L 06/18/20 16:36 95-49-810020.3 100
4-Chlorotoluene ND ug/L 06/18/20 16:36 106-43-410020.4 100
1,2-Dibromo-3-chloropropane ND ug/L 06/18/20 16:36 96-12-850025.7 100
Dibromochloromethane ND ug/L 06/18/20 16:36 124-48-110041.3 100
1,2-Dibromoethane (EDB)ND ug/L 06/18/20 16:36 106-93-410025.8 100
Dibromomethane ND ug/L 06/18/20 16:36 74-95-310045.9 100
1,2-Dichlorobenzene ND ug/L 06/18/20 16:36 95-50-110029.1 100
1,3-Dichlorobenzene ND ug/L 06/18/20 16:36 541-73-110021.7 100
1,4-Dichlorobenzene 137 ug/L 06/18/20 16:36 106-46-710025.8 100
Dichlorodifluoromethane ND ug/L 06/18/20 16:36 75-71-8 v210022.6 100
1,1-Dichloroethane ND ug/L 06/18/20 16:36 75-34-310026.8 100
1,2-Dichloroethane ND ug/L 06/18/20 16:36 107-06-210033.6 100
1,1-Dichloroethene ND ug/L 06/18/20 16:36 75-35-410024.5 100
cis-1,2-Dichloroethene ND ug/L 06/18/20 16:36 156-59-210029.1 100
trans-1,2-Dichloroethene ND ug/L 06/18/20 16:36 156-60-510025.4 100
1,2-Dichloropropane ND ug/L 06/18/20 16:36 78-87-510018.7 100
1,3-Dichloropropane ND ug/L 06/18/20 16:36 142-28-910015.8 100
2,2-Dichloropropane ND ug/L 06/18/20 16:36 594-20-710027.0 100
1,1-Dichloropropene ND ug/L 06/18/20 16:36 563-58-610021.3 100
cis-1,3-Dichloropropene ND ug/L 06/18/20 16:36 10061-01-510029.6 100
trans-1,3-Dichloropropene ND ug/L 06/18/20 16:36 10061-02-610030.9 100
Diisopropyl ether ND ug/L 06/18/20 16:36 108-20-310021.8 100
Ethylbenzene ND ug/L 06/18/20 16:36 100-41-410025.6 100
Hexachloro-1,3-butadiene ND ug/L 06/18/20 16:36 87-68-310043.8 100
2-Hexanone ND ug/L 06/18/20 16:36 591-78-650056.8 100
p-Isopropyltoluene ND ug/L 06/18/20 16:36 99-87-610021.2 100
Methylene Chloride ND ug/L 06/18/20 16:36 75-09-2500369100
4-Methyl-2-pentanone (MIBK)ND ug/L 06/18/20 16:36 108-10-1500453100
Methyl-tert-butyl ether ND ug/L 06/18/20 16:36 1634-04-410027.5 100
Naphthalene 567 ug/L 06/18/20 16:36 91-20-3 1g,v310035.2 100
Styrene ND ug/L 06/18/20 16:36 100-42-510026.7 100
1,1,1,2-Tetrachloroethane ND ug/L 06/18/20 16:36 630-20-610034.0 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:GW-Dup Lab ID:92481464009 Collected:06/10/20 00:00 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/18/20 16:36 79-34-510022.2 100
Tetrachloroethene ND ug/L 06/18/20 16:36 127-18-410016.2 100
Toluene ND ug/L 06/18/20 16:36 108-88-310024.4 100
1,2,3-Trichlorobenzene ND ug/L 06/18/20 16:36 87-61-6 v210034.4 100
1,2,4-Trichlorobenzene ND ug/L 06/18/20 16:36 120-82-110021.8 100
1,1,1-Trichloroethane ND ug/L 06/18/20 16:36 71-55-610017.5 100
1,1,2-Trichloroethane ND ug/L 06/18/20 16:36 79-00-510023.6 100
Trichloroethene ND ug/L 06/18/20 16:36 79-01-610022.0 100
Trichlorofluoromethane ND ug/L 06/18/20 16:36 75-69-4 v210031.1 100
1,2,3-Trichloropropane ND ug/L 06/18/20 16:36 96-18-4 M1,R110034.7 100
Vinyl acetate ND ug/L 06/18/20 16:36 108-05-4200145100
Vinyl chloride ND ug/L 06/18/20 16:36 75-01-410024.2 100
Xylene (Total)ND ug/L 06/18/20 16:36 1330-20-710063.0 100
m&p-Xylene ND ug/L 06/18/20 16:36 179601-23-120041.0 100
o-Xylene ND ug/L 06/18/20 16:36 95-47-610022.0 100
Surrogates
4-Bromofluorobenzene (S)93 %06/18/20 16:36 460-00-470-130 100
1,2-Dichloroethane-d4 (S)85 %06/18/20 16:36 17060-07-070-130 100
Toluene-d8 (S)102 %06/18/20 16:36 2037-26-570-130 100
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND ug/L 06/15/20 20:32 18540-29-906/15/20 20:320.100 0.0400 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:Trip Blank-1 Lab ID:92481464010 Collected:06/10/20 00:00 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/16/20 13:19 67-64-125.0 6.2 1
Benzene ND ug/L 06/16/20 13:19 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/16/20 13:19 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/16/20 13:19 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/16/20 13:19 75-27-41.0 0.26 1
Bromoform ND ug/L 06/16/20 13:19 75-25-21.0 0.62 1
Bromomethane ND ug/L 06/16/20 13:19 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 06/16/20 13:19 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/16/20 13:19 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/16/20 13:19 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/16/20 13:19 75-00-3 v21.0 0.49 1
Chloroform ND ug/L 06/16/20 13:19 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/16/20 13:19 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 06/16/20 13:19 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/16/20 13:19 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/16/20 13:19 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/16/20 13:19 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/16/20 13:19 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/16/20 13:19 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/16/20 13:19 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/16/20 13:19 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/16/20 13:19 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/16/20 13:19 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/16/20 13:19 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/16/20 13:19 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/16/20 13:19 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/16/20 13:19 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/16/20 13:19 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/16/20 13:19 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/16/20 13:19 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/16/20 13:19 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/16/20 13:19 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/16/20 13:19 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/16/20 13:19 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/16/20 13:19 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/16/20 13:19 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/16/20 13:19 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/16/20 13:19 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/16/20 13:19 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/16/20 13:19 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/16/20 13:19 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/16/20 13:19 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/16/20 13:19 91-20-3 v21.0 0.35 1
Styrene ND ug/L 06/16/20 13:19 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/16/20 13:19 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481464
FDP-058
Sample:Trip Blank-1 Lab ID:92481464010 Collected:06/10/20 00:00 Received:06/11/20 12:44 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/16/20 13:19 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/16/20 13:19 127-18-41.0 0.16 1
Toluene ND ug/L 06/16/20 13:19 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/16/20 13:19 87-61-6 v21.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/16/20 13:19 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/16/20 13:19 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/16/20 13:19 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/16/20 13:19 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/16/20 13:19 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/16/20 13:19 96-18-4 v21.0 0.35 1
Vinyl acetate ND ug/L 06/16/20 13:19 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 06/16/20 13:19 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/16/20 13:19 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/16/20 13:19 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/16/20 13:19 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)91 %06/16/20 13:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)84 %06/16/20 13:19 17060-07-070-130 1
Toluene-d8 (S)107 %06/16/20 13:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1493080
3015
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481464001, 92481464002, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007,
92481464008, 92481464009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3539883-1
Associated Lab Samples:92481464001, 92481464002, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007,
92481464008, 92481464009
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 2.00 06/17/20 20:030.735
Barium ug/L ND 20.0 06/17/20 20:037.78
Cadmium ug/L ND 1.00 06/17/20 20:030.478
Chromium ug/L ND 2.00 06/17/20 20:031.49
Lead ug/L ND 5.00 06/17/20 20:032.49
Selenium ug/L ND 2.00 06/17/20 20:030.657
Silver ug/L ND 2.00 06/17/20 20:030.513
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3539883-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 49.250.0 98.4 80.0-120
Barium ug/L 47.450.0 94.9 80.0-120
Cadmium ug/L 52.850.0 106 80.0-120
Chromium ug/L 51.550.0 103 80.0-120
Lead ug/L 50.350.0 101 80.0-120
Selenium ug/L 52.350.0 105 80.0-120
Silver ug/L 51.450.0 103 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3539883-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1228294-01
R3539883-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 50.0 101 75.0-12598.8 2.49 2050.00.871 51.5 50.3
Barium ug/L 50.0 95.6 75.0-12597.4 0.321 2050.0231 279 280
Cadmium ug/L 50.0 106 75.0-125107 0.525 2050.0ND 53.1 53.4
Chromium ug/L 50.0 106 75.0-125104 1.68 2050.0ND 53.1 52.2
Lead ug/L 50.0 103 75.0-125102 0.787 2050.0ND 51.5 51.1
Selenium ug/L 50.0 109 75.0-125107 1.54 2050.0ND 54.5 53.7
Silver ug/L 50.0 105 75.0-125104 0.983 2050.0ND 52.6 52.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1492418
7470A
EPA 7470A
Mercury 7470A
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481464001, 92481464002, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007,
92481464008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3538769-1
Associated Lab Samples:92481464001, 92481464002, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007,
92481464008
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.200 06/15/20 10:000.100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3538769-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 3.243.00 108 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3538769-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481464008
R3538769-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 3.00 89.5 75.0-12594.1 5.12 203.00ND 2.68 2.82
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1492419
7470A
EPA 7470A
Mercury 7470A
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481464009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3538982-1
Associated Lab Samples:92481464009
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.200 06/15/20 20:200.100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3538982-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.623.00 87.3 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3538982-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1228693-29
R3538982-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 3.00 107 75.0-125101 5.36 203.00ND 3.20 3.03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
547453
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481464010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2913513
Associated Lab Samples:92481464010
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/16/20 12:080.34
1,1,1-Trichloroethane ug/L ND 1.0 06/16/20 12:080.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/16/20 12:080.22
1,1,2-Trichloroethane ug/L ND 1.0 06/16/20 12:080.24
1,1-Dichloroethane ug/L ND 1.0 06/16/20 12:080.27
1,1-Dichloroethene ug/L ND 1.0 06/16/20 12:080.24
1,1-Dichloropropene ug/L ND 1.0 06/16/20 12:080.21
1,2,3-Trichlorobenzene ug/L ND 1.0 v206/16/20 12:080.34
1,2,3-Trichloropropane ug/L ND 1.0 v206/16/20 12:080.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/16/20 12:080.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 06/16/20 12:080.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/16/20 12:080.26
1,2-Dichlorobenzene ug/L ND 1.0 06/16/20 12:080.29
1,2-Dichloroethane ug/L ND 1.0 06/16/20 12:080.34
1,2-Dichloropropane ug/L ND 1.0 06/16/20 12:080.19
1,3-Dichlorobenzene ug/L ND 1.0 06/16/20 12:080.22
1,3-Dichloropropane ug/L ND 1.0 06/16/20 12:080.16
1,4-Dichlorobenzene ug/L ND 1.0 06/16/20 12:080.26
2,2-Dichloropropane ug/L ND 1.0 06/16/20 12:080.27
2-Butanone (MEK)ug/L ND 5.0 06/16/20 12:083.3
2-Chlorotoluene ug/L ND 1.0 06/16/20 12:080.20
2-Hexanone ug/L ND 5.0 06/16/20 12:080.57
4-Chlorotoluene ug/L ND 1.0 06/16/20 12:080.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/16/20 12:084.5
Acetone ug/L ND 25.0 06/16/20 12:086.2
Benzene ug/L ND 1.0 06/16/20 12:080.15
Bromobenzene ug/L ND 1.0 06/16/20 12:080.22
Bromochloromethane ug/L ND 1.0 06/16/20 12:080.34
Bromodichloromethane ug/L ND 1.0 06/16/20 12:080.26
Bromoform ug/L ND 1.0 06/16/20 12:080.62
Bromomethane ug/L ND 2.0 06/16/20 12:080.62
Carbon tetrachloride ug/L ND 1.0 06/16/20 12:080.22
Chlorobenzene ug/L ND 1.0 06/16/20 12:080.23
Chloroethane ug/L ND 1.0 v206/16/20 12:080.49
Chloroform ug/L ND 5.0 06/16/20 12:082.3
Chloromethane ug/L ND 1.0 06/16/20 12:080.39
cis-1,2-Dichloroethene ug/L ND 1.0 06/16/20 12:080.29
cis-1,3-Dichloropropene ug/L ND 1.0 06/16/20 12:080.30
Dibromochloromethane ug/L ND 1.0 06/16/20 12:080.41
Dibromomethane ug/L ND 1.0 06/16/20 12:080.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 47 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2913513
Associated Lab Samples:92481464010
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 06/16/20 12:080.23
Diisopropyl ether ug/L ND 1.0 06/16/20 12:080.22
Ethylbenzene ug/L ND 1.0 06/16/20 12:080.26
Hexachloro-1,3-butadiene ug/L ND 1.0 06/16/20 12:080.44
m&p-Xylene ug/L ND 2.0 06/16/20 12:080.41
Methyl-tert-butyl ether ug/L ND 1.0 06/16/20 12:080.28
Methylene Chloride ug/L ND 5.0 06/16/20 12:083.7
Naphthalene ug/L ND 1.0 v206/16/20 12:080.35
o-Xylene ug/L ND 1.0 06/16/20 12:080.22
p-Isopropyltoluene ug/L ND 1.0 06/16/20 12:080.21
Styrene ug/L ND 1.0 06/16/20 12:080.27
Tetrachloroethene ug/L ND 1.0 06/16/20 12:080.16
Toluene ug/L ND 1.0 06/16/20 12:080.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/16/20 12:080.25
trans-1,3-Dichloropropene ug/L ND 1.0 06/16/20 12:080.31
Trichloroethene ug/L ND 1.0 06/16/20 12:080.22
Trichlorofluoromethane ug/L ND 1.0 06/16/20 12:080.31
Vinyl acetate ug/L ND 2.0 06/16/20 12:081.4
Vinyl chloride ug/L ND 1.0 06/16/20 12:080.24
Xylene (Total)ug/L ND 1.0 06/16/20 12:080.63
1,2-Dichloroethane-d4 (S)%79 70-130 06/16/20 12:08
4-Bromofluorobenzene (S)%92 70-130 06/16/20 12:08
Toluene-d8 (S)%102 70-130 06/16/20 12:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2913514LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.350 101 70-130
1,1,1-Trichloroethane ug/L 46.850 94 70-130
1,1,2,2-Tetrachloroethane ug/L 40.850 82 70-130
1,1,2-Trichloroethane ug/L 53.550 107 70-130
1,1-Dichloroethane ug/L 48.050 96 70-130
1,1-Dichloroethene ug/L 49.750 99 70-130
1,1-Dichloropropene ug/L 49.450 99 70-130
1,2,3-Trichlorobenzene ug/L 39.1 v3507870-130
1,2,3-Trichloropropane ug/L 38.7 v3507770-130
1,2,4-Trichlorobenzene ug/L 46.950 94 70-130
1,2-Dibromo-3-chloropropane ug/L 45.550 91 70-130
1,2-Dibromoethane (EDB)ug/L 50.850 102 70-130
1,2-Dichlorobenzene ug/L 57.050 114 70-130
1,2-Dichloroethane ug/L 42.850 86 70-130
1,2-Dichloropropane ug/L 50.350 101 70-130
1,3-Dichlorobenzene ug/L 54.350 109 70-130
1,3-Dichloropropane ug/L 48.450 97 70-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2913514LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 57.550 115 70-130
2,2-Dichloropropane ug/L 50.050 100 69-130
2-Butanone (MEK)ug/L 93.7100 94 64-135
2-Chlorotoluene ug/L 49.550 99 70-130
2-Hexanone ug/L 88.2100 88 66-135
4-Chlorotoluene ug/L 53.250 106 70-130
4-Methyl-2-pentanone (MIBK)ug/L 99.0100 99 70-130
Acetone ug/L 94.1100 94 61-157
Benzene ug/L 54.450 109 70-130
Bromobenzene ug/L 55.250 110 70-130
Bromochloromethane ug/L 52.550 105 70-130
Bromodichloromethane ug/L 50.150 100 70-130
Bromoform ug/L 48.450 97 70-130
Bromomethane ug/L 50.750 101 38-130
Carbon tetrachloride ug/L 52.450 105 70-130
Chlorobenzene ug/L 52.450 105 70-130
Chloroethane ug/L 36.0 v3507237-142
Chloroform ug/L 45.650 91 70-130
Chloromethane ug/L 42.650 85 48-130
cis-1,2-Dichloroethene ug/L 47.050 94 70-130
cis-1,3-Dichloropropene ug/L 50.950 102 70-130
Dibromochloromethane ug/L 50.250 100 70-130
Dibromomethane ug/L 54.750 109 70-130
Dichlorodifluoromethane ug/L 44.150 88 53-134
Diisopropyl ether ug/L 51.350 103 70-135
Ethylbenzene ug/L 48.650 97 70-130
Hexachloro-1,3-butadiene ug/L 53.550 107 68-132
m&p-Xylene ug/L 98.6100 99 70-130
Methyl-tert-butyl ether ug/L 47.050 94 70-130
Methylene Chloride ug/L 49.250 98 67-132
Naphthalene ug/L 39.1 v3507870-130
o-Xylene ug/L 51.050 102 70-131
p-Isopropyltoluene ug/L 58.750 117 70-130
Styrene ug/L 54.650 109 70-130
Tetrachloroethene ug/L 53.650 107 69-130
Toluene ug/L 53.150 106 70-130
trans-1,2-Dichloroethene ug/L 48.550 97 70-130
trans-1,3-Dichloropropene ug/L 51.650 103 70-130
Trichloroethene ug/L 55.550 111 70-130
Trichlorofluoromethane ug/L 42.650 85 63-130
Vinyl acetate ug/L 103100 103 55-143
Vinyl chloride ug/L 56.750 113 70-131
Xylene (Total)ug/L 150150 100 70-130
1,2-Dichloroethane-d4 (S)%83 70-130
4-Bromofluorobenzene (S)%91 70-130
Toluene-d8 (S)%104 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2913515MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481368011
2913516
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 98 73-13495 4 302019.6 18.9
1,1,1-Trichloroethane ug/L 20 99 82-14395 4 3020ND19.7 18.9
1,1,2,2-Tetrachloroethane ug/L 20 89 70-13685 4 3020ND17.8 17.1
1,1,2-Trichloroethane ug/L 20 97 70-13595 2 3020ND19.4 19.0
1,1-Dichloroethane ug/L 20 100 70-13998 3 3020ND20.0 19.5
1,1-Dichloroethene ug/L 20 104 70-154104 0 3020ND21.4 21.3
1,1-Dichloropropene ug/L 20 100 70-14999 1 302020.0 19.7
1,2,3-Trichlorobenzene ug/L M1,v3207270-13566 8 302014.4 13.3
1,2,3-Trichloropropane ug/L 20 85 71-13784 2 302017.0 16.7
1,2,4-Trichlorobenzene ug/L 20 83 73-14078 6 302016.5 15.6
1,2-Dibromo-3-
chloropropane ug/L 20 85 65-13481 4 302017.0 16.2
1,2-Dibromoethane (EDB)ug/L 20 98 70-13795 3 302019.6 19.0
1,2-Dichlorobenzene ug/L 20 99 70-13394 5 302019.8 18.9
1,2-Dichloroethane ug/L v3209170-13789 2 3020ND18.1 17.8
1,2-Dichloropropane ug/L 20 100 70-14099 1 302020.0 19.8
1,3-Dichlorobenzene ug/L 20 98 70-13596 2 302019.7 19.2
1,3-Dichloropropane ug/L 20 96 70-14389 7 302019.1 17.9
1,4-Dichlorobenzene ug/L 20 99 70-13398 1 302019.8 19.6
2,2-Dichloropropane ug/L 20 98 61-14898 0 302019.7 19.6
2-Butanone (MEK)ug/L 40 106 60-13996 10 3040ND42.3 38.3
2-Chlorotoluene ug/L 20 98 70-14494 4 302019.6 18.8
2-Hexanone ug/L 40 88 65-13885 3 304035.3 34.1
4-Chlorotoluene ug/L 20 96 70-13792 5 302019.3 18.4
4-Methyl-2-pentanone
(MIBK)ug/L 40 94 65-13594 0 304037.8 37.6
Acetone ug/L 40 97 60-14893 3 304038.6 37.4
Benzene ug/L 20 98 70-15199 1 302019.7 19.9
Bromobenzene ug/L 20 100 70-13697 4 302020.0 19.3
Bromochloromethane ug/L 20 107 70-141101 5 302021.3 20.2
Bromodichloromethane ug/L 20 99 70-13898 1 302019.7 19.6
Bromoform ug/L 20 88 63-13083 5 302017.5 16.7
Bromomethane ug/L 20 119 15-152116 3 302023.9 23.2
Carbon tetrachloride ug/L 20 101 70-143102 1 3020ND20.3 20.4
Chlorobenzene ug/L 20 99 70-13898 1 302019.7 19.6
Chloroethane ug/L 20 92 52-16391 1 3020ND18.5 18.3
Chloroform ug/L 20 98 70-13993 5 3020ND20.8 19.7
Chloromethane ug/L 20 88 41-13987 1 302017.7 17.4
cis-1,2-Dichloroethene ug/L 20 100 70-14197 2 3020ND20.8 20.3
cis-1,3-Dichloropropene ug/L 20 95 70-13796 1 302018.9 19.1
Dibromochloromethane ug/L 20 95 70-13492 3 302019.0 18.5
Dibromomethane ug/L 20 101 70-138100 2 302020.2 19.9
Dichlorodifluoromethane ug/L 20 86 47-15587 1 3020ND17.2 17.5
Diisopropyl ether ug/L 20 103 63-14499 4 302020.6 19.8
Ethylbenzene ug/L 20 92 66-15392 0 302018.4 18.4
Hexachloro-1,3-butadiene ug/L 20 94 65-14990 5 302018.9 18.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2913515MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481368011
2913516
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 93 69-15293 1 304037.3 37.1
Methyl-tert-butyl ether ug/L 20 95 54-15690 5 302019.0 18.0
Methylene Chloride ug/L 20 105 42-159104 1 3020ND21.1 20.8
Naphthalene ug/L v3207361-14865 11 302014.6 13.1
o-Xylene ug/L 20 97 70-14894 3 302019.5 18.8
p-Isopropyltoluene ug/L 20 106 70-146102 3 302021.2 20.5
Styrene ug/L 20 98 70-13596 2 302019.5 19.2
Tetrachloroethene ug/L 20 113 59-143115 1 302036.3 58.8 59.2
Toluene ug/L 20 96 59-14895 0 302019.1 19.1
trans-1,2-Dichloroethene ug/L 20 102 70-146101 1 3020ND20.4 20.2
trans-1,3-Dichloropropene ug/L 20 93 70-13593 1 302018.7 18.6
Trichloroethene ug/L 20 105 70-147107 2 3020ND21.7 22.1
Trichlorofluoromethane ug/L 20 93 70-14895 2 302018.6 18.9
Vinyl acetate ug/L 40 98 49-15194 4 304039.3 37.5
Vinyl chloride ug/L 20 114 70-156113 0 3020ND22.8 22.7
Xylene (Total)ug/L 60 95 63-15893 2 306056.8 55.9
1,2-Dichloroethane-d4 (S)%94 70-13093
4-Bromofluorobenzene (S)%95 70-13096
Toluene-d8 (S)%98 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
547618
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481464001, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2914297
Associated Lab Samples:92481464001, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/17/20 00:490.34
1,1,1-Trichloroethane ug/L ND 1.0 06/17/20 00:490.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/17/20 00:490.22
1,1,2-Trichloroethane ug/L ND 1.0 06/17/20 00:490.24
1,1-Dichloroethane ug/L ND 1.0 06/17/20 00:490.27
1,1-Dichloroethene ug/L ND 1.0 06/17/20 00:490.24
1,1-Dichloropropene ug/L ND 1.0 06/17/20 00:490.21
1,2,3-Trichlorobenzene ug/L ND 1.0 06/17/20 00:490.34
1,2,3-Trichloropropane ug/L ND 1.0 06/17/20 00:490.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/17/20 00:490.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 06/17/20 00:490.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/17/20 00:490.26
1,2-Dichlorobenzene ug/L ND 1.0 06/17/20 00:490.29
1,2-Dichloroethane ug/L ND 1.0 06/17/20 00:490.34
1,2-Dichloropropane ug/L ND 1.0 06/17/20 00:490.19
1,3-Dichlorobenzene ug/L ND 1.0 06/17/20 00:490.22
1,3-Dichloropropane ug/L ND 1.0 06/17/20 00:490.16
1,4-Dichlorobenzene ug/L ND 1.0 06/17/20 00:490.26
2,2-Dichloropropane ug/L ND 1.0 06/17/20 00:490.27
2-Butanone (MEK)ug/L ND 5.0 06/17/20 00:493.3
2-Chlorotoluene ug/L ND 1.0 06/17/20 00:490.20
2-Hexanone ug/L ND 5.0 06/17/20 00:490.57
4-Chlorotoluene ug/L ND 1.0 06/17/20 00:490.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/17/20 00:494.5
Acetone ug/L ND 25.0 06/17/20 00:496.2
Benzene ug/L ND 1.0 06/17/20 00:490.15
Bromobenzene ug/L ND 1.0 06/17/20 00:490.22
Bromochloromethane ug/L ND 1.0 06/17/20 00:490.34
Bromodichloromethane ug/L ND 1.0 06/17/20 00:490.26
Bromoform ug/L ND 1.0 06/17/20 00:490.62
Bromomethane ug/L ND 2.0 v206/17/20 00:490.62
Carbon tetrachloride ug/L ND 1.0 06/17/20 00:490.22
Chlorobenzene ug/L ND 1.0 06/17/20 00:490.23
Chloroethane ug/L ND 1.0 06/17/20 00:490.49
Chloroform ug/L ND 5.0 06/17/20 00:492.3
Chloromethane ug/L ND 1.0 v306/17/20 00:490.39
cis-1,2-Dichloroethene ug/L ND 1.0 06/17/20 00:490.29
cis-1,3-Dichloropropene ug/L ND 1.0 06/17/20 00:490.30
Dibromochloromethane ug/L ND 1.0 06/17/20 00:490.41
Dibromomethane ug/L ND 1.0 06/17/20 00:490.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2914297
Associated Lab Samples:92481464001, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 06/17/20 00:490.23
Diisopropyl ether ug/L ND 1.0 06/17/20 00:490.22
Ethylbenzene ug/L ND 1.0 06/17/20 00:490.26
Hexachloro-1,3-butadiene ug/L ND 1.0 06/17/20 00:490.44
m&p-Xylene ug/L ND 2.0 06/17/20 00:490.41
Methyl-tert-butyl ether ug/L ND 1.0 06/17/20 00:490.28
Methylene Chloride ug/L ND 5.0 06/17/20 00:493.7
Naphthalene ug/L ND 1.0 06/17/20 00:490.35
o-Xylene ug/L ND 1.0 06/17/20 00:490.22
p-Isopropyltoluene ug/L ND 1.0 06/17/20 00:490.21
Styrene ug/L ND 1.0 06/17/20 00:490.27
Tetrachloroethene ug/L ND 1.0 06/17/20 00:490.16
Toluene ug/L ND 1.0 06/17/20 00:490.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/17/20 00:490.25
trans-1,3-Dichloropropene ug/L ND 1.0 06/17/20 00:490.31
Trichloroethene ug/L ND 1.0 06/17/20 00:490.22
Trichlorofluoromethane ug/L ND 1.0 06/17/20 00:490.31
Vinyl acetate ug/L ND 2.0 06/17/20 00:491.4
Vinyl chloride ug/L ND 1.0 06/17/20 00:490.24
Xylene (Total)ug/L ND 1.0 06/17/20 00:490.63
1,2-Dichloroethane-d4 (S)%102 70-130 06/17/20 00:49
4-Bromofluorobenzene (S)%95 70-130 06/17/20 00:49
Toluene-d8 (S)%98 70-130 06/17/20 00:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2914298LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.350 103 70-130
1,1,1-Trichloroethane ug/L 48.850 98 70-130
1,1,2,2-Tetrachloroethane ug/L 53.050 106 70-130
1,1,2-Trichloroethane ug/L 47.850 96 70-130
1,1-Dichloroethane ug/L 51.050 102 70-130
1,1-Dichloroethene ug/L 56.450 113 70-130
1,1-Dichloropropene ug/L 50.850 102 70-130
1,2,3-Trichlorobenzene ug/L 52.850 106 70-130
1,2,3-Trichloropropane ug/L 49.150 98 70-130
1,2,4-Trichlorobenzene ug/L 63.150 126 70-130
1,2-Dibromo-3-chloropropane ug/L 47.350 95 70-130
1,2-Dibromoethane (EDB)ug/L 54.750 109 70-130
1,2-Dichlorobenzene ug/L 60.450 121 70-130
1,2-Dichloroethane ug/L 47.650 95 70-130
1,2-Dichloropropane ug/L 50.950 102 70-130
1,3-Dichlorobenzene ug/L 59.350 119 70-130
1,3-Dichloropropane ug/L 55.550 111 70-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2914298LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 58.350 117 70-130
2,2-Dichloropropane ug/L 50.950 102 69-130
2-Butanone (MEK)ug/L 88.7100 89 64-135
2-Chlorotoluene ug/L 59.050 118 70-130
2-Hexanone ug/L 100100 100 66-135
4-Chlorotoluene ug/L 56.950 114 70-130
4-Methyl-2-pentanone (MIBK)ug/L 93.1100 93 70-130
Acetone ug/L 91.2100 91 61-157
Benzene ug/L 51.250 102 70-130
Bromobenzene ug/L 61.550 123 70-130
Bromochloromethane ug/L 54.650 109 70-130
Bromodichloromethane ug/L 44.950 90 70-130
Bromoform ug/L 42.250 84 70-130
Bromomethane ug/L 46.0 v3509238-130
Carbon tetrachloride ug/L 47.650 95 70-130
Chlorobenzene ug/L 54.250 108 70-130
Chloroethane ug/L 42.850 86 37-142
Chloroform ug/L 51.650 103 70-130
Chloromethane ug/L 30.0 v3506048-130
cis-1,2-Dichloroethene ug/L 50.450 101 70-130
cis-1,3-Dichloropropene ug/L 48.950 98 70-130
Dibromochloromethane ug/L 48.650 97 70-130
Dibromomethane ug/L 47.250 94 70-130
Dichlorodifluoromethane ug/L 40.150 80 53-134
Diisopropyl ether ug/L 52.350 105 70-135
Ethylbenzene ug/L 52.450 105 70-130
Hexachloro-1,3-butadiene ug/L 58.950 118 68-132
m&p-Xylene ug/L 102100 102 70-130
Methyl-tert-butyl ether ug/L 50.350 101 70-130
Methylene Chloride ug/L 54.450 109 67-132
Naphthalene ug/L 54.650 109 70-130
o-Xylene ug/L 53.150 106 70-131
p-Isopropyltoluene ug/L 60.550 121 70-130
Styrene ug/L 53.750 107 70-130
Tetrachloroethene ug/L 49.750 99 69-130
Toluene ug/L 47.650 95 70-130
trans-1,2-Dichloroethene ug/L 53.650 107 70-130
trans-1,3-Dichloropropene ug/L 43.950 88 70-130
Trichloroethene ug/L 47.950 96 70-130
Trichlorofluoromethane ug/L 41.750 83 63-130
Vinyl acetate ug/L 103100 103 55-143
Vinyl chloride ug/L 48.750 97 70-131
Xylene (Total)ug/L 155150 104 70-130
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2914299MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481464001
2914300
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 85 73-13496 12 3020ND17.1 19.2
1,1,1-Trichloroethane ug/L 20 92 82-14399 8 3020ND18.4 19.9
1,1,2,2-Tetrachloroethane ug/L 20 92 70-136105 13 3020ND18.3 21.0
1,1,2-Trichloroethane ug/L 20 84 70-13593 11 3020ND16.8 18.7
1,1-Dichloroethane ug/L 20 92 70-139102 10 3020ND18.5 20.4
1,1-Dichloroethene ug/L 20 100 70-154113 12 3020ND20.1 22.6
1,1-Dichloropropene ug/L 20 97 70-149106 8 3020ND19.4 21.1
1,2,3-Trichlorobenzene ug/L 20 80 70-13591 12 3020ND16.1 18.1
1,2,3-Trichloropropane ug/L 20 83 71-13795 13 3020ND16.7 18.9
1,2,4-Trichlorobenzene ug/L 20 91 73-140104 14 3020ND18.2 20.9
1,2-Dibromo-3-
chloropropane ug/L 20 77 65-13490 16 3020ND15.4 18.1
1,2-Dibromoethane (EDB)ug/L 20 89 70-137100 12 3020ND17.8 20.0
1,2-Dichlorobenzene ug/L 20 97 70-133113 15 3020ND19.5 22.6
1,2-Dichloroethane ug/L 20 85 70-13794 11 3020ND17.0 18.9
1,2-Dichloropropane ug/L 20 96 70-140105 10 3020ND19.1 21.1
1,3-Dichlorobenzene ug/L 20 93 70-135108 15 3020ND18.5 21.6
1,3-Dichloropropane ug/L 20 93 70-143106 14 3020ND18.5 21.2
1,4-Dichlorobenzene ug/L 20 90 70-133105 15 3020ND18.0 21.0
2,2-Dichloropropane ug/L 20 101 61-148109 8 3020ND20.1 21.8
2-Butanone (MEK)ug/L 40 84 60-13992 9 3040ND33.6 36.7
2-Chlorotoluene ug/L 20 95 70-144108 12 3020ND19.1 21.5
2-Hexanone ug/L 40 83 65-13897 16 3040ND33.0 38.8
4-Chlorotoluene ug/L 20 96 70-137113 16 3020ND19.2 22.6
4-Methyl-2-pentanone
(MIBK)ug/L 40 81 65-13591 11 3040ND32.4 36.3
Acetone ug/L 40 82 60-14894 14 3040ND32.6 37.6
Benzene ug/L 20 91 70-151108 17 3020ND18.2 21.7
Bromobenzene ug/L 20 100 70-136106 5 3020ND20.0 21.1
Bromochloromethane ug/L 20 100 70-141107 7 3020ND20.0 21.3
Bromodichloromethane ug/L 20 84 70-13888 5 3020ND16.8 17.6
Bromoform ug/L 20 83 63-13086 3 3020ND16.7 17.2
Bromomethane ug/L 20 78 15-15294 19 3020ND15.6 18.8
Carbon tetrachloride ug/L 20 86 70-14398 13 3020ND17.2 19.7
Chlorobenzene ug/L 20 89 70-138103 14 3020ND17.8 20.6
Chloroethane ug/L 20 87 52-16398 12 3020ND17.4 19.7
Chloroform ug/L 20 87 70-139103 18 3020ND17.3 20.7
Chloromethane ug/L 20 64 41-13973 14 3020ND12.9 14.8
cis-1,2-Dichloroethene ug/L 20 91 70-141102 12 3020ND18.2 20.5
cis-1,3-Dichloropropene ug/L 20 87 70-137103 17 3020ND17.4 20.6
Dibromochloromethane ug/L 20 86 70-13499 14 3020ND17.3 19.8
Dibromomethane ug/L 20 83 70-13894 12 3020ND16.6 18.8
Dichlorodifluoromethane ug/L 20 71 47-15580 12 3020ND14.2 16.0
Diisopropyl ether ug/L 20 91 63-14499 8 3020ND18.3 19.8
Ethylbenzene ug/L 20 91 66-153104 13 3020ND18.1 20.7
Hexachloro-1,3-butadiene ug/L 20 101 65-149111 10 3020ND20.2 22.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2914299MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481464001
2914300
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 90 69-152102 12 3040ND35.9 40.6
Methyl-tert-butyl ether ug/L 20 90 54-15695 6 3020ND18.0 19.0
Methylene Chloride ug/L 20 91 42-159102 11 3020ND18.2 20.4
Naphthalene ug/L 20 78 61-14891 15 3020ND15.6 18.2
o-Xylene ug/L 20 88 70-148104 17 3020ND17.7 20.9
p-Isopropyltoluene ug/L 20 98 70-146114 15 3020ND19.6 22.8
Styrene ug/L 20 89 70-135108 20 3020ND17.8 21.7
Tetrachloroethene ug/L 20 90 59-143103 14 3020ND18.0 20.7
Toluene ug/L 20 88 59-14898 10 3020ND17.7 19.5
trans-1,2-Dichloroethene ug/L 20 100 70-146110 10 3020ND19.9 22.0
trans-1,3-Dichloropropene ug/L 20 80 70-13591 13 3020ND15.9 18.1
Trichloroethene ug/L 20 88 70-147103 16 3020ND17.6 20.6
Trichlorofluoromethane ug/L v3208670-14890 4 3020ND17.2 18.0
Vinyl acetate ug/L 40 88 49-15198 11 3040ND35.2 39.1
Vinyl chloride ug/L 20 95 70-156102 7 3020ND19.0 20.5
Xylene (Total)ug/L 60 89 63-158103 14 3060ND53.6 61.5
1,2-Dichloroethane-d4 (S)%105 70-13099
4-Bromofluorobenzene (S)%98 70-130102
Toluene-d8 (S)%95 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
547850
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481464002, 92481464008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2915083
Associated Lab Samples:92481464002, 92481464008
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/17/20 12:520.34
1,1,1-Trichloroethane ug/L ND 1.0 06/17/20 12:520.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/17/20 12:520.22
1,1,2-Trichloroethane ug/L ND 1.0 06/17/20 12:520.24
1,1-Dichloroethane ug/L ND 1.0 06/17/20 12:520.27
1,1-Dichloroethene ug/L ND 1.0 06/17/20 12:520.24
1,1-Dichloropropene ug/L ND 1.0 06/17/20 12:520.21
1,2,3-Trichlorobenzene ug/L ND 1.0 06/17/20 12:520.34
1,2,3-Trichloropropane ug/L ND 1.0 06/17/20 12:520.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/17/20 12:520.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 06/17/20 12:520.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/17/20 12:520.26
1,2-Dichlorobenzene ug/L ND 1.0 06/17/20 12:520.29
1,2-Dichloroethane ug/L ND 1.0 06/17/20 12:520.34
1,2-Dichloropropane ug/L ND 1.0 06/17/20 12:520.19
1,3-Dichlorobenzene ug/L ND 1.0 06/17/20 12:520.22
1,3-Dichloropropane ug/L ND 1.0 06/17/20 12:520.16
1,4-Dichlorobenzene ug/L ND 1.0 06/17/20 12:520.26
2,2-Dichloropropane ug/L ND 1.0 06/17/20 12:520.27
2-Butanone (MEK)ug/L ND 5.0 06/17/20 12:523.3
2-Chlorotoluene ug/L ND 1.0 06/17/20 12:520.20
2-Hexanone ug/L ND 5.0 06/17/20 12:520.57
4-Chlorotoluene ug/L ND 1.0 06/17/20 12:520.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/17/20 12:524.5
Acetone ug/L ND 25.0 06/17/20 12:526.2
Benzene ug/L ND 1.0 06/17/20 12:520.15
Bromobenzene ug/L ND 1.0 06/17/20 12:520.22
Bromochloromethane ug/L ND 1.0 06/17/20 12:520.34
Bromodichloromethane ug/L ND 1.0 06/17/20 12:520.26
Bromoform ug/L ND 1.0 06/17/20 12:520.62
Bromomethane ug/L ND 2.0 v206/17/20 12:520.62
Carbon tetrachloride ug/L ND 1.0 06/17/20 12:520.22
Chlorobenzene ug/L ND 1.0 06/17/20 12:520.23
Chloroethane ug/L ND 1.0 06/17/20 12:520.49
Chloroform ug/L ND 5.0 06/17/20 12:522.3
Chloromethane ug/L ND 1.0 v206/17/20 12:520.39
cis-1,2-Dichloroethene ug/L ND 1.0 06/17/20 12:520.29
cis-1,3-Dichloropropene ug/L ND 1.0 06/17/20 12:520.30
Dibromochloromethane ug/L ND 1.0 06/17/20 12:520.41
Dibromomethane ug/L ND 1.0 06/17/20 12:520.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2915083
Associated Lab Samples:92481464002, 92481464008
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 06/17/20 12:520.23
Diisopropyl ether ug/L ND 1.0 06/17/20 12:520.22
Ethylbenzene ug/L ND 1.0 06/17/20 12:520.26
Hexachloro-1,3-butadiene ug/L ND 1.0 06/17/20 12:520.44
m&p-Xylene ug/L ND 2.0 06/17/20 12:520.41
Methyl-tert-butyl ether ug/L ND 1.0 06/17/20 12:520.28
Methylene Chloride ug/L ND 5.0 06/17/20 12:523.7
Naphthalene ug/L ND 1.0 06/17/20 12:520.35
o-Xylene ug/L ND 1.0 06/17/20 12:520.22
p-Isopropyltoluene ug/L ND 1.0 06/17/20 12:520.21
Styrene ug/L ND 1.0 06/17/20 12:520.27
Tetrachloroethene ug/L ND 1.0 06/17/20 12:520.16
Toluene ug/L ND 1.0 06/17/20 12:520.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/17/20 12:520.25
trans-1,3-Dichloropropene ug/L ND 1.0 06/17/20 12:520.31
Trichloroethene ug/L ND 1.0 06/17/20 12:520.22
Trichlorofluoromethane ug/L ND 1.0 06/17/20 12:520.31
Vinyl acetate ug/L ND 2.0 06/17/20 12:521.4
Vinyl chloride ug/L ND 1.0 06/17/20 12:520.24
Xylene (Total)ug/L ND 1.0 06/17/20 12:520.63
1,2-Dichloroethane-d4 (S)%103 70-130 06/17/20 12:52
4-Bromofluorobenzene (S)%95 70-130 06/17/20 12:52
Toluene-d8 (S)%101 70-130 06/17/20 12:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2915084LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.650 89 70-130
1,1,1-Trichloroethane ug/L 46.050 92 70-130
1,1,2,2-Tetrachloroethane ug/L 44.950 90 70-130
1,1,2-Trichloroethane ug/L 41.550 83 70-130
1,1-Dichloroethane ug/L 48.350 97 70-130
1,1-Dichloroethene ug/L 50.150 100 70-130
1,1-Dichloropropene ug/L 47.850 96 70-130
1,2,3-Trichlorobenzene ug/L 46.850 94 70-130
1,2,3-Trichloropropane ug/L 44.050 88 70-130
1,2,4-Trichlorobenzene ug/L 50.750 101 70-130
1,2-Dibromo-3-chloropropane ug/L 42.050 84 70-130
1,2-Dibromoethane (EDB)ug/L 48.250 96 70-130
1,2-Dichlorobenzene ug/L 50.050 100 70-130
1,2-Dichloroethane ug/L 44.750 89 70-130
1,2-Dichloropropane ug/L 45.650 91 70-130
1,3-Dichlorobenzene ug/L 47.850 96 70-130
1,3-Dichloropropane ug/L 48.450 97 70-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2915084LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 47.350 95 70-130
2,2-Dichloropropane ug/L 48.950 98 69-130
2-Butanone (MEK)ug/L 88.3100 88 64-135
2-Chlorotoluene ug/L 47.350 95 70-130
2-Hexanone ug/L 92.3100 92 66-135
4-Chlorotoluene ug/L 47.550 95 70-130
4-Methyl-2-pentanone (MIBK)ug/L 87.7100 88 70-130
Acetone ug/L 91.2100 91 61-157
Benzene ug/L 45.550 91 70-130
Bromobenzene ug/L 46.750 93 70-130
Bromochloromethane ug/L 48.450 97 70-130
Bromodichloromethane ug/L 42.250 84 70-130
Bromoform ug/L 44.650 89 70-130
Bromomethane ug/L 37.4 v3507538-130
Carbon tetrachloride ug/L 43.850 88 70-130
Chlorobenzene ug/L 45.750 91 70-130
Chloroethane ug/L 41.050 82 37-142
Chloroform ug/L 48.750 97 70-130
Chloromethane ug/L 37.9 v2507648-130
cis-1,2-Dichloroethene ug/L 47.450 95 70-130
cis-1,3-Dichloropropene ug/L 46.250 92 70-130
Dibromochloromethane ug/L 48.350 97 70-130
Dibromomethane ug/L 42.950 86 70-130
Dichlorodifluoromethane ug/L 44.450 89 53-134
Diisopropyl ether ug/L 48.950 98 70-135
Ethylbenzene ug/L 44.450 89 70-130
Hexachloro-1,3-butadiene ug/L 51.750 103 68-132
m&p-Xylene ug/L 89.0100 89 70-130
Methyl-tert-butyl ether ug/L 45.650 91 70-130
Methylene Chloride ug/L 51.050 102 67-132
Naphthalene ug/L 45.450 91 70-130
o-Xylene ug/L 44.750 89 70-131
p-Isopropyltoluene ug/L 50.650 101 70-130
Styrene ug/L 45.650 91 70-130
Tetrachloroethene ug/L 44.950 90 69-130
Toluene ug/L 41.750 83 70-130
trans-1,2-Dichloroethene ug/L 50.650 101 70-130
trans-1,3-Dichloropropene ug/L 42.450 85 70-130
Trichloroethene ug/L 43.150 86 70-130
Trichlorofluoromethane ug/L 39.250 78 63-130
Vinyl acetate ug/L 96.6100 97 55-143
Vinyl chloride ug/L 47.450 95 70-131
Xylene (Total)ug/L 134150 89 70-130
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2915085MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481464002
2915086
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 95 73-13492 3 302000ND18901840
1,1,1-Trichloroethane ug/L 2000 104 82-14385 20 302000ND20801700
1,1,2,2-Tetrachloroethane ug/L 2000 95 70-13692 4 302000ND19001830
1,1,2-Trichloroethane ug/L 2000 83 70-13582 1 302000ND16601640
1,1-Dichloroethane ug/L 2000 109 70-13993 15 302000ND21701870
1,1-Dichloroethene ug/L 2000 123 70-154102 18 302000ND24502050
1,1-Dichloropropene ug/L 2000 111 70-14997 14 302000ND22201930
1,2,3-Trichlorobenzene ug/L 2000 86 70-13584 3 302000ND17201670
1,2,3-Trichloropropane ug/L 2000 89 71-13790 1 302000ND17901800
1,2,4-Trichlorobenzene ug/L 2000 97 73-14098 0 302000ND19501960
1,2-Dibromo-3-
chloropropane ug/L 2000 85 65-13485 1 302000ND16901700
1,2-Dibromoethane (EDB)ug/L 2000 101 70-13796 5 302000ND20201930
1,2-Dichlorobenzene ug/L 2000 104 70-13398 6 302000ND20801970
1,2-Dichloroethane ug/L 2000 95 70-13787 9 302000ND19101750
1,2-Dichloropropane ug/L 2000 99 70-14095 4 302000ND19801900
1,3-Dichlorobenzene ug/L 2000 101 70-13599 2 302000ND20101980
1,3-Dichloropropane ug/L 2000 100 70-14396 4 302000ND20001910
1,4-Dichlorobenzene ug/L 2000 101 70-13393 8 30200014021602000
2,2-Dichloropropane ug/L 2000 111 61-14897 13 302000ND22201950
2-Butanone (MEK)ug/L 4000 88 60-13982 7 304000ND35103280
2-Chlorotoluene ug/L 2000 110 70-144102 7 302000ND22002050
2-Hexanone ug/L 4000 91 65-13892 1 304000ND36403670
4-Chlorotoluene ug/L 2000 93 70-137101 8 302000ND18702020
4-Methyl-2-pentanone
(MIBK)ug/L 4000 84 65-13581 4 304000ND33603230
Acetone ug/L 4000 87 60-14882 5 304000ND34703290
Benzene ug/L 2000 106 70-15196 10 30200061.2J 2180 1970
Bromobenzene ug/L 2000 103 70-136102 1 302000ND20502040
Bromochloromethane ug/L 2000 113 70-141100 12 302000ND22501990
Bromodichloromethane ug/L 2000 87 70-13881 7 302000ND17401620
Bromoform ug/L 2000 90 63-13087 3 302000ND18001740
Bromomethane ug/L v3200011115-152104 7 302000ND22302080
Carbon tetrachloride ug/L 2000 95 70-14386 10 302000ND18901720
Chlorobenzene ug/L M1200015070-138117 4 302000125001550014800
Chloroethane ug/L 2000 103 52-16381 23 302000ND20501630
Chloroform ug/L 2000 100 70-13988 12 302000ND20001760
Chloromethane ug/L v320006641-13960 9 302000ND13101200
cis-1,2-Dichloroethene ug/L 2000 107 70-14194 12 302000ND21301890
cis-1,3-Dichloropropene ug/L 2000 97 70-13790 8 302000ND19501800
Dibromochloromethane ug/L 2000 93 70-13492 2 302000ND18601830
Dibromomethane ug/L 2000 91 70-13888 4 302000ND18301750
Dichlorodifluoromethane ug/L 2000 85 47-15574 14 302000ND17001480
Diisopropyl ether ug/L 2000 103 63-14493 10 302000ND20701870
Ethylbenzene ug/L 2000 102 66-15394 8 302000ND20401880
Hexachloro-1,3-butadiene ug/L 2000 104 65-14994 10 302000ND20701880
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2915085MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481464002
2915086
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 4000 99 69-15294 5 304000ND39803770
Methyl-tert-butyl ether ug/L 2000 99 54-15689 10 302000ND19701780
Methylene Chloride ug/L 2000 102 42-15991 12 302000ND20501820
Naphthalene ug/L 2000 85 61-14887 2 302000ND17001730
o-Xylene ug/L 2000 98 70-14893 5 302000ND19601860
p-Isopropyltoluene ug/L 2000 108 70-146103 4 302000ND21502060
Styrene ug/L 2000 96 70-13596 0 302000ND19201930
Tetrachloroethene ug/L 2000 99 59-14396 3 302000ND19801920
Toluene ug/L 2000 94 59-14891 4 302000ND18901810
trans-1,2-Dichloroethene ug/L 2000 116 70-14698 16 302000ND23201970
trans-1,3-Dichloropropene ug/L 2000 90 70-13582 9 302000ND17901640
Trichloroethene ug/L 2000 101 70-14790 12 302000ND20301790
Trichlorofluoromethane ug/L 2000 94 70-14881 15 302000ND18701620
Vinyl acetate ug/L 4000 102 49-15191 12 304000ND40703630
Vinyl chloride ug/L 2000 105 70-15690 15 302000ND21001810
Xylene (Total)ug/L 6000 99 63-15894 5 306000ND59305620
1,2-Dichloroethane-d4 (S)%95 70-13098
4-Bromofluorobenzene (S)%95 70-13096
Toluene-d8 (S)%98 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
548122
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481464009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2916174
Associated Lab Samples:92481464009
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/18/20 13:370.34
1,1,1-Trichloroethane ug/L ND 1.0 06/18/20 13:370.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/18/20 13:370.22
1,1,2-Trichloroethane ug/L ND 1.0 06/18/20 13:370.24
1,1-Dichloroethane ug/L ND 1.0 06/18/20 13:370.27
1,1-Dichloroethene ug/L ND 1.0 06/18/20 13:370.24
1,1-Dichloropropene ug/L ND 1.0 06/18/20 13:370.21
1,2,3-Trichlorobenzene ug/L ND 1.0 v206/18/20 13:370.34
1,2,3-Trichloropropane ug/L ND 1.0 06/18/20 13:370.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/18/20 13:370.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 06/18/20 13:370.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/18/20 13:370.26
1,2-Dichlorobenzene ug/L ND 1.0 06/18/20 13:370.29
1,2-Dichloroethane ug/L ND 1.0 06/18/20 13:370.34
1,2-Dichloropropane ug/L ND 1.0 06/18/20 13:370.19
1,3-Dichlorobenzene ug/L ND 1.0 06/18/20 13:370.22
1,3-Dichloropropane ug/L ND 1.0 06/18/20 13:370.16
1,4-Dichlorobenzene ug/L ND 1.0 06/18/20 13:370.26
2,2-Dichloropropane ug/L ND 1.0 06/18/20 13:370.27
2-Butanone (MEK)ug/L ND 5.0 06/18/20 13:373.3
2-Chlorotoluene ug/L ND 1.0 06/18/20 13:370.20
2-Hexanone ug/L ND 5.0 06/18/20 13:370.57
4-Chlorotoluene ug/L ND 1.0 06/18/20 13:370.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/18/20 13:374.5
Acetone ug/L ND 25.0 06/18/20 13:376.2
Benzene ug/L ND 1.0 06/18/20 13:370.15
Bromobenzene ug/L ND 1.0 06/18/20 13:370.22
Bromochloromethane ug/L ND 1.0 06/18/20 13:370.34
Bromodichloromethane ug/L ND 1.0 06/18/20 13:370.26
Bromoform ug/L ND 1.0 06/18/20 13:370.62
Bromomethane ug/L ND 2.0 06/18/20 13:370.62
Carbon tetrachloride ug/L ND 1.0 06/18/20 13:370.22
Chlorobenzene ug/L ND 1.0 06/18/20 13:370.23
Chloroethane ug/L ND 1.0 v206/18/20 13:370.49
Chloroform ug/L ND 5.0 06/18/20 13:372.3
Chloromethane ug/L ND 1.0 06/18/20 13:370.39
cis-1,2-Dichloroethene ug/L ND 1.0 06/18/20 13:370.29
cis-1,3-Dichloropropene ug/L ND 1.0 06/18/20 13:370.30
Dibromochloromethane ug/L ND 1.0 06/18/20 13:370.41
Dibromomethane ug/L ND 1.0 06/18/20 13:370.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2916174
Associated Lab Samples:92481464009
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 v206/18/20 13:370.23
Diisopropyl ether ug/L ND 1.0 06/18/20 13:370.22
Ethylbenzene ug/L ND 1.0 06/18/20 13:370.26
Hexachloro-1,3-butadiene ug/L ND 1.0 06/18/20 13:370.44
m&p-Xylene ug/L ND 2.0 06/18/20 13:370.41
Methyl-tert-butyl ether ug/L ND 1.0 06/18/20 13:370.28
Methylene Chloride ug/L ND 5.0 06/18/20 13:373.7
Naphthalene ug/L ND 1.0 v206/18/20 13:370.35
o-Xylene ug/L ND 1.0 06/18/20 13:370.22
p-Isopropyltoluene ug/L ND 1.0 06/18/20 13:370.21
Styrene ug/L ND 1.0 06/18/20 13:370.27
Tetrachloroethene ug/L ND 1.0 06/18/20 13:370.16
Toluene ug/L ND 1.0 06/18/20 13:370.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/18/20 13:370.25
trans-1,3-Dichloropropene ug/L ND 1.0 06/18/20 13:370.31
Trichloroethene ug/L ND 1.0 06/18/20 13:370.22
Trichlorofluoromethane ug/L ND 1.0 v206/18/20 13:370.31
Vinyl acetate ug/L ND 2.0 06/18/20 13:371.4
Vinyl chloride ug/L ND 1.0 06/18/20 13:370.24
Xylene (Total)ug/L ND 1.0 06/18/20 13:370.63
1,2-Dichloroethane-d4 (S)%86 70-130 06/18/20 13:37
4-Bromofluorobenzene (S)%93 70-130 06/18/20 13:37
Toluene-d8 (S)%103 70-130 06/18/20 13:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2916175LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 46.950 94 70-130
1,1,1-Trichloroethane ug/L 45.450 91 70-130
1,1,2,2-Tetrachloroethane ug/L 42.850 86 70-130
1,1,2-Trichloroethane ug/L 48.750 97 70-130
1,1-Dichloroethane ug/L 46.250 92 70-130
1,1-Dichloroethene ug/L 47.550 95 70-130
1,1-Dichloropropene ug/L 47.650 95 70-130
1,2,3-Trichlorobenzene ug/L 37.6 v3507570-130
1,2,3-Trichloropropane ug/L 40.550 81 70-130
1,2,4-Trichlorobenzene ug/L 43.950 88 70-130
1,2-Dibromo-3-chloropropane ug/L 46.950 94 70-130
1,2-Dibromoethane (EDB)ug/L 48.150 96 70-130
1,2-Dichlorobenzene ug/L 50.850 102 70-130
1,2-Dichloroethane ug/L 41.850 84 70-130
1,2-Dichloropropane ug/L 49.250 98 70-130
1,3-Dichlorobenzene ug/L 51.550 103 70-130
1,3-Dichloropropane ug/L 46.050 92 70-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2916175LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 51.250 102 70-130
2,2-Dichloropropane ug/L 48.150 96 69-130
2-Butanone (MEK)ug/L 100100 100 64-135
2-Chlorotoluene ug/L 46.450 93 70-130
2-Hexanone ug/L 91.6100 92 66-135
4-Chlorotoluene ug/L 48.150 96 70-130
4-Methyl-2-pentanone (MIBK)ug/L 95.2100 95 70-130
Acetone ug/L 103100 103 61-157
Benzene ug/L 48.850 98 70-130
Bromobenzene ug/L 49.650 99 70-130
Bromochloromethane ug/L 50.650 101 70-130
Bromodichloromethane ug/L 47.750 95 70-130
Bromoform ug/L 46.550 93 70-130
Bromomethane ug/L 46.550 93 38-130
Carbon tetrachloride ug/L 47.850 96 70-130
Chlorobenzene ug/L 49.050 98 70-130
Chloroethane ug/L 34.2 v3506837-142
Chloroform ug/L 43.650 87 70-130
Chloromethane ug/L 41.750 83 48-130
cis-1,2-Dichloroethene ug/L 46.250 92 70-130
cis-1,3-Dichloropropene ug/L 47.750 95 70-130
Dibromochloromethane ug/L 47.750 95 70-130
Dibromomethane ug/L 49.850 100 70-130
Dichlorodifluoromethane ug/L 39.6 v3507953-134
Diisopropyl ether ug/L 50.350 101 70-135
Ethylbenzene ug/L 45.450 91 70-130
Hexachloro-1,3-butadiene ug/L 48.050 96 68-132
m&p-Xylene ug/L 92.2100 92 70-130
Methyl-tert-butyl ether ug/L 45.650 91 70-130
Methylene Chloride ug/L 48.650 97 67-132
Naphthalene ug/L 38.0 v3507670-130
o-Xylene ug/L 47.450 95 70-131
p-Isopropyltoluene ug/L 52.150 104 70-130
Styrene ug/L 50.850 102 70-130
Tetrachloroethene ug/L 50.150 100 69-130
Toluene ug/L 46.850 94 70-130
trans-1,2-Dichloroethene ug/L 46.850 94 70-130
trans-1,3-Dichloropropene ug/L 46.650 93 70-130
Trichloroethene ug/L 51.650 103 70-130
Trichlorofluoromethane ug/L 39.9 v3508063-130
Vinyl acetate ug/L 106100 106 55-143
Vinyl chloride ug/L 52.550 105 70-131
Xylene (Total)ug/L 140150 93 70-130
1,2-Dichloroethane-d4 (S)%85 70-130
4-Bromofluorobenzene (S)%93 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2916176MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481464009
2916177
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 100 73-13499 2 302000ND20101970
1,1,1-Trichloroethane ug/L 2000 98 82-14398 0 302000ND19501960
1,1,2,2-Tetrachloroethane ug/L 2000 94 70-13673 25 302000ND18801460
1,1,2-Trichloroethane ug/L 2000 104 70-135102 2 302000ND20902040
1,1-Dichloroethane ug/L 2000 100 70-13999 1 302000ND20001990
1,1-Dichloroethene ug/L 2000 106 70-154104 2 302000ND21302080
1,1-Dichloropropene ug/L 2000 104 70-149102 2 302000ND20802050
1,2,3-Trichlorobenzene ug/L v320008570-13590 5 302000ND17101790
1,2,3-Trichloropropane ug/L M1,R120009171-13765 34 302000ND18201290
1,2,4-Trichlorobenzene ug/L 2000 99 73-140102 3 302000ND19702040
1,2-Dibromo-3-
chloropropane ug/L 2000 98 65-13494 4 302000ND19501880
1,2-Dibromoethane (EDB)ug/L 2000 104 70-137102 2 302000ND20802030
1,2-Dichlorobenzene ug/L 2000 110 70-133108 1 302000ND22002170
1,2-Dichloroethane ug/L 2000 87 70-13785 2 302000ND17401700
1,2-Dichloropropane ug/L 2000 106 70-140104 2 302000ND21302090
1,3-Dichlorobenzene ug/L 2000 111 70-135107 3 302000ND22202140
1,3-Dichloropropane ug/L 2000 99 70-14396 3 302000ND19701920
1,4-Dichlorobenzene ug/L 2000 109 70-133106 3 30200013723202260
2,2-Dichloropropane ug/L 2000 97 61-148100 4 302000ND19302010
2-Butanone (MEK)ug/L 4000 105 60-13999 5 304000ND41803980
2-Chlorotoluene ug/L 2000 108 70-14494 13 302000ND21501880
2-Hexanone ug/L 4000 98 65-13892 6 304000ND39103670
4-Chlorotoluene ug/L 2000 106 70-13795 11 302000ND21201900
4-Methyl-2-pentanone
(MIBK)ug/L 4000 107 65-13599 7 304000ND42603970
Acetone ug/L 4000 101 60-14896 6 304000ND40603830
Benzene ug/L 2000 104 70-151105 1 30200058.4J 2140 2150
Bromobenzene ug/L 2000 113 70-136125 10 302000ND22602500
Bromochloromethane ug/L 2000 110 70-141108 2 302000ND22002160
Bromodichloromethane ug/L 2000 99 70-138100 1 302000ND19902010
Bromoform ug/L 2000 93 63-13094 1 302000ND18601880
Bromomethane ug/L 2000 104 15-152105 1 302000ND20802100
Carbon tetrachloride ug/L 2000 103 70-143105 2 302000ND20602100
Chlorobenzene ug/L 2000 107 70-13891 2 302000125001460014300
Chloroethane ug/L v320009652-16391 6 302000ND19301820
Chloroform ug/L 2000 97 70-13995 2 302000ND19501900
Chloromethane ug/L 2000 93 41-13988 6 302000ND18701750
cis-1,2-Dichloroethene ug/L 2000 98 70-14199 0 302000ND19701970
cis-1,3-Dichloropropene ug/L 2000 101 70-137101 0 302000ND20202020
Dibromochloromethane ug/L 2000 100 70-13497 3 302000ND20001950
Dibromomethane ug/L 2000 109 70-138107 2 302000ND21802150
Dichlorodifluoromethane ug/L v320009147-15583 9 302000ND18201660
Diisopropyl ether ug/L 2000 106 63-144103 2 302000ND21102060
Ethylbenzene ug/L 2000 101 66-15398 2 302000ND20101970
Hexachloro-1,3-butadiene ug/L 2000 110 65-149115 4 302000ND22002300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2916176MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481464009
2916177
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 4000 101 69-15299 2 304000ND40503970
Methyl-tert-butyl ether ug/L 2000 95 54-15693 2 302000ND19101870
Methylene Chloride ug/L 2000 107 42-159104 3 302000ND21402080
Naphthalene ug/L v320006461-14861 4 30200056718501780
o-Xylene ug/L 2000 105 70-148102 3 302000ND21102040
p-Isopropyltoluene ug/L 2000 114 70-146109 4 302000ND22702190
Styrene ug/L 2000 109 70-135108 1 302000ND21802150
Tetrachloroethene ug/L 2000 107 59-143114 6 302000ND21502270
Toluene ug/L 2000 102 59-148104 3 302000ND20302090
trans-1,2-Dichloroethene ug/L 2000 103 70-146101 2 302000ND20602020
trans-1,3-Dichloropropene ug/L 2000 97 70-13597 0 302000ND19401940
Trichloroethene ug/L 2000 113 70-147111 2 302000ND22602220
Trichlorofluoromethane ug/L v3200010070-14895 6 302000ND20101900
Vinyl acetate ug/L 4000 109 49-151107 1 304000ND43404280
Vinyl chloride ug/L 2000 123 70-156115 6 302000ND24602300
Xylene (Total)ug/L 6000 103 63-158100 2 306000ND61606010
1,2-Dichloroethane-d4 (S)%86 70-13088
4-Bromofluorobenzene (S)%95 70-13091
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
547414
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481464001, 92481464002, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007,
92481464008, 92481464009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2913400
Associated Lab Samples:92481464001, 92481464002, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007,
92481464008, 92481464009
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 06/16/20 11:161.6
1,2-Dichlorobenzene ug/L ND 10.0 06/16/20 11:161.4
1,3-Dichlorobenzene ug/L ND 10.0 06/16/20 11:161.4
1,4-Dichlorobenzene ug/L ND 10.0 06/16/20 11:161.5
1-Methylnaphthalene ug/L ND 10.0 06/16/20 11:161.4
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/16/20 11:161.3
2,4,5-Trichlorophenol ug/L ND 10.0 06/16/20 11:161.5
2,4,6-Trichlorophenol ug/L ND 10.0 06/16/20 11:161.4
2,4-Dichlorophenol ug/L ND 10.0 06/16/20 11:161.5
2,4-Dimethylphenol ug/L ND 10.0 06/16/20 11:161.5
2,4-Dinitrophenol ug/L ND 50.0 06/16/20 11:167.3
2,4-Dinitrotoluene ug/L ND 10.0 06/16/20 11:161.7
2,6-Dinitrotoluene ug/L ND 10.0 06/16/20 11:161.7
2-Chloronaphthalene ug/L ND 10.0 06/16/20 11:161.4
2-Chlorophenol ug/L ND 10.0 06/16/20 11:161.4
2-Methylnaphthalene ug/L ND 10.0 06/16/20 11:161.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/16/20 11:161.2
2-Nitroaniline ug/L ND 20.0 06/16/20 11:163.0
2-Nitrophenol ug/L ND 10.0 06/16/20 11:161.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/16/20 11:161.2
3,3'-Dichlorobenzidine ug/L ND 20.0 06/16/20 11:162.7
3-Nitroaniline ug/L ND 20.0 06/16/20 11:162.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 06/16/20 11:164.5
4-Bromophenylphenyl ether ug/L ND 10.0 06/16/20 11:161.2
4-Chloro-3-methylphenol ug/L ND 10.0 06/16/20 11:162.8
4-Chloroaniline ug/L ND 20.0 06/16/20 11:162.8
4-Chlorophenylphenyl ether ug/L ND 10.0 06/16/20 11:161.5
4-Nitroaniline ug/L ND 20.0 06/16/20 11:163.1
4-Nitrophenol ug/L ND 50.0 06/16/20 11:169.4
Acenaphthene ug/L ND 10.0 06/16/20 11:161.4
Acenaphthylene ug/L ND 10.0 06/16/20 11:161.5
Aniline ug/L ND 10.0 06/16/20 11:161.6
Anthracene ug/L ND 10.0 06/16/20 11:161.6
Benzo(a)anthracene ug/L ND 10.0 06/16/20 11:161.5
Benzo(a)pyrene ug/L ND 10.0 06/16/20 11:161.8
Benzo(b)fluoranthene ug/L ND 10.0 06/16/20 11:161.7
Benzo(g,h,i)perylene ug/L ND 10.0 06/16/20 11:161.6
Benzo(k)fluoranthene ug/L ND 10.0 06/16/20 11:161.5
Benzoic Acid ug/L ND 50.0 06/16/20 11:1619.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
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Huntersville, NC 28078
[phone]
Page 67 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2913400
Associated Lab Samples:92481464001, 92481464002, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007,
92481464008, 92481464009
Matrix:Water
AnalyzedMDL
Benzyl alcohol ug/L ND 20.0 06/16/20 11:162.6
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/16/20 11:161.3
bis(2-Chloroethyl) ether ug/L ND 10.0 06/16/20 11:161.7
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/16/20 11:162.0
Butylbenzylphthalate ug/L ND 10.0 06/16/20 11:161.9
Chrysene ug/L ND 10.0 06/16/20 11:161.4
Di-n-butylphthalate ug/L ND 10.0 06/16/20 11:161.6
Di-n-octylphthalate ug/L ND 10.0 06/16/20 11:162.2
Dibenz(a,h)anthracene ug/L ND 10.0 06/16/20 11:161.6
Dibenzofuran ug/L ND 10.0 06/16/20 11:161.3
Diethylphthalate ug/L ND 10.0 06/16/20 11:161.6
Dimethylphthalate ug/L ND 10.0 06/16/20 11:161.4
Fluoranthene ug/L ND 10.0 06/16/20 11:161.6
Fluorene ug/L ND 10.0 06/16/20 11:161.4
Hexachloro-1,3-butadiene ug/L ND 10.0 06/16/20 11:161.6
Hexachlorobenzene ug/L ND 10.0 06/16/20 11:161.3
Hexachlorocyclopentadiene ug/L ND 10.0 06/16/20 11:162.4
Hexachloroethane ug/L ND 10.0 06/16/20 11:161.3
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/16/20 11:161.7
Isophorone ug/L ND 10.0 06/16/20 11:161.3
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/16/20 11:161.3
N-Nitrosodimethylamine ug/L ND 10.0 06/16/20 11:161.8
N-Nitrosodiphenylamine ug/L ND 10.0 06/16/20 11:161.4
Naphthalene ug/L ND 10.0 06/16/20 11:161.6
Nitrobenzene ug/L ND 10.0 06/16/20 11:161.5
Pentachlorophenol ug/L ND 20.0 06/16/20 11:162.8
Phenanthrene ug/L ND 10.0 06/16/20 11:161.4
Phenol ug/L ND 10.0 06/16/20 11:161.5
Pyrene ug/L ND 10.0 06/16/20 11:161.5
2,4,6-Tribromophenol (S)%87 10-137 06/16/20 11:16
2-Fluorobiphenyl (S)%80 13-130 06/16/20 11:16
2-Fluorophenol (S)%61 10-130 06/16/20 11:16
Nitrobenzene-d5 (S)%85 13-130 06/16/20 11:16
Phenol-d6 (S)%49 10-130 06/16/20 11:16
Terphenyl-d14 (S)%115 25-130 06/16/20 11:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2913401LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 39.950 80 30-130
1,2-Dichlorobenzene ug/L 39.550 79 30-130
1,3-Dichlorobenzene ug/L 38.350 77 20-130
1,4-Dichlorobenzene ug/L 40.850 82 30-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
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Page 68 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2913401LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/L 45.050 90 30-130
2,2'-Oxybis(1-chloropropane)ug/L 47.350 95 20-130
2,4,5-Trichlorophenol ug/L 52.150 104 40-130
2,4,6-Trichlorophenol ug/L 49.850 100 40-130
2,4-Dichlorophenol ug/L 51.350 103 31-130
2,4-Dimethylphenol ug/L 53.650 107 30-130
2,4-Dinitrophenol ug/L 262250 105 30-130
2,4-Dinitrotoluene ug/L 54.550 109 49-130
2,6-Dinitrotoluene ug/L 55.450 111 50-130
2-Chloronaphthalene ug/L 43.650 87 30-130
2-Chlorophenol ug/L 46.850 94 30-130
2-Methylnaphthalene ug/L 46.350 93 30-130
2-Methylphenol(o-Cresol)ug/L 46.050 92 30-130
2-Nitroaniline ug/L 105100 105 40-130
2-Nitrophenol ug/L 49.950 100 20-130
3&4-Methylphenol(m&p Cresol)ug/L 44.850 90 20-130
3,3'-Dichlorobenzidine ug/L 107100 107 10-150
3-Nitroaniline ug/L 111100 111 40-130
4,6-Dinitro-2-methylphenol ug/L 114100 114 40-130
4-Bromophenylphenyl ether ug/L 50.350 101 30-130
4-Chloro-3-methylphenol ug/L 107100 107 30-130
4-Chloroaniline ug/L 105100 105 20-130
4-Chlorophenylphenyl ether ug/L 48.750 97 20-130
4-Nitroaniline ug/L 111100 111 40-130
4-Nitrophenol ug/L 154250 62 10-130
Acenaphthene ug/L 46.950 94 30-130
Acenaphthylene ug/L 48.750 97 30-130
Aniline ug/L 44.950 90 20-130
Anthracene ug/L 51.550 103 50-130
Benzo(a)anthracene ug/L 54.450 109 50-130
Benzo(a)pyrene ug/L 55.150 110 50-130
Benzo(b)fluoranthene ug/L 55.550 111 50-130
Benzo(g,h,i)perylene ug/L 47.050 94 50-130
Benzo(k)fluoranthene ug/L 55.950 112 50-130
Benzoic Acid ug/L 65.3250 26 10-130
Benzyl alcohol ug/L 101100 101 20-130
bis(2-Chloroethoxy)methane ug/L 49.850 100 30-130
bis(2-Chloroethyl) ether ug/L 48.550 97 30-130
bis(2-Ethylhexyl)phthalate ug/L 57.250 114 50-130
Butylbenzylphthalate ug/L 58.450 117 50-150
Chrysene ug/L 52.550 105 50-130
Di-n-butylphthalate ug/L 55.250 110 50-130
Di-n-octylphthalate ug/L 55.350 111 50-130
Dibenz(a,h)anthracene ug/L 48.650 97 40-130
Dibenzofuran ug/L 47.350 95 40-130
Diethylphthalate ug/L 53.850 108 40-130
Dimethylphthalate ug/L 52.450 105 40-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
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Page 69 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2913401LABORATORY CONTROL SAMPLE:
LCSSpike
Fluoranthene ug/L 52.750 105 30-130
Fluorene ug/L 50.650 101 20-130
Hexachloro-1,3-butadiene ug/L 37.150 74 10-130
Hexachlorobenzene ug/L 50.150 100 30-130
Hexachlorocyclopentadiene ug/L 36.850 74 10-150
Hexachloroethane ug/L 37.650 75 10-130
Indeno(1,2,3-cd)pyrene ug/L 48.050 96 40-130
Isophorone ug/L 54.050 108 30-130
N-Nitroso-di-n-propylamine ug/L 54.750 109 30-130
N-Nitrosodimethylamine ug/L 39.750 79 10-130
N-Nitrosodiphenylamine ug/L 50.850 102 30-130
Naphthalene ug/L 43.250 86 20-130
Nitrobenzene ug/L 48.250 96 20-130
Pentachlorophenol ug/L 116100 116 10-140
Phenanthrene ug/L 50.150 100 50-130
Phenol ug/L 31.150 62 10-130
Pyrene ug/L 57.450 115 50-130
2,4,6-Tribromophenol (S)%95 10-137
2-Fluorobiphenyl (S)%77 13-130
2-Fluorophenol (S)%61 10-130
Nitrobenzene-d5 (S)%86 13-130
Phenol-d6 (S)%52 10-130
Terphenyl-d14 (S)%116 25-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2913402MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481368002
2913403
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 85 30-13082 3 3050ND42.5 41.2
1,2-Dichlorobenzene ug/L 50 83 30-13081 3 3050ND41.7 40.6
1,3-Dichlorobenzene ug/L 50 82 20-13082 1 3050ND41.2 40.9
1,4-Dichlorobenzene ug/L 50 83 30-13083 1 3050ND41.6 41.3
1-Methylnaphthalene ug/L 50 88 30-13087 1 3050ND43.8 43.4
2,2'-Oxybis(1-
chloropropane)ug/L 50 85 20-13087 1 3050ND42.7 43.3
2,4,5-Trichlorophenol ug/L 50 98 40-13093 5 3050ND49.0 46.4
2,4,6-Trichlorophenol ug/L 50 95 40-13093 2 3050ND47.5 46.5
2,4-Dichlorophenol ug/L 50 94 31-13092 2 3050ND47.0 46.0
2,4-Dimethylphenol ug/L 50 99 30-130100 1 3050ND49.5 50.1
2,4-Dinitrophenol ug/L 250 82 30-13072 13 30250ND205180
2,4-Dinitrotoluene ug/L 50 111 49-13099 11 3050ND55.3 49.3
2,6-Dinitrotoluene ug/L 50 101 50-13096 4 3050ND50.3 48.2
2-Chloronaphthalene ug/L 50 93 30-13089 4 3050ND46.4 44.5
2-Chlorophenol ug/L 50 88 30-13088 0 3050ND44.1 43.9
2-Methylnaphthalene ug/L 50 91 30-13090 0 3050ND45.3 45.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
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Huntersville, NC 28078
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Page 70 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2913402MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481368002
2913403
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol)ug/L 50 85 30-13082 3 3050ND42.5 41.2
2-Nitroaniline ug/L 100 99 40-13096 3 30100ND99.4 96.1
2-Nitrophenol ug/L 50 95 20-13095 1 3050ND47.3 47.6
3&4-Methylphenol(m&p
Cresol)ug/L 50 80 20-13078 2 3050ND40.0 39.2
3,3'-Dichlorobenzidine ug/L 100 109 10-150100 9 30100ND10999.9
3-Nitroaniline ug/L 100 104 40-13096 7 30100ND10496.5
4,6-Dinitro-2-methylphenol ug/L 100 97 40-13084 15 30100ND97.3 84.0
4-Bromophenylphenyl ether ug/L 50 91 30-13087 4 3050ND45.4 43.7
4-Chloro-3-methylphenol ug/L 100 93 30-13092 1 30100ND93.4 92.4
4-Chloroaniline ug/L 100 95 20-13093 2 30100ND94.9 93.5
4-Chlorophenylphenyl ether ug/L 50 90 20-13087 3 3050ND45.1 43.5
4-Nitroaniline ug/L 100 114 40-130101 12 30100ND114101
4-Nitrophenol ug/L 250 62 10-13056 9 30250ND154141
Acenaphthene ug/L 50 96 30-13093 3 3050ND47.8 46.5
Acenaphthylene ug/L 50 97 30-13094 3 3050ND48.7 47.2
Aniline ug/L 50 76 20-13073 5 3050ND38.1 36.3
Anthracene ug/L 50 105 50-13097 7 3050ND52.4 48.6
Benzo(a)anthracene ug/L 50 112 50-130100 11 3050ND56.2 50.1
Benzo(a)pyrene ug/L 50 112 50-130100 11 3050ND56.2 50.2
Benzo(b)fluoranthene ug/L 50 110 50-130100 9 3050ND55.0 50.2
Benzo(g,h,i)perylene ug/L 50 116 50-130106 9 3050ND57.9 53.1
Benzo(k)fluoranthene ug/L 50 116 50-130100 15 3050ND57.8 49.9
Benzoic Acid ug/L 250 38 10-13042 10 30250ND95.7 106
Benzyl alcohol ug/L 100 85 20-13081 4 30100ND84.9 81.3
bis(2-
Chloroethoxy)methane ug/L 50 93 30-13090 3 3050ND46.6 45.2
bis(2-Chloroethyl) ether ug/L 50 92 30-13090 1 3050ND45.8 45.2
bis(2-Ethylhexyl)phthalate ug/L 50 114 50-130103 10 3050ND56.9 51.6
Butylbenzylphthalate ug/L 50 113 50-150103 9 3050ND56.3 51.7
Chrysene ug/L 50 113 50-130102 11 3050ND56.7 50.8
Di-n-butylphthalate ug/L 50 108 50-13098 10 3050ND54.1 49.0
Di-n-octylphthalate ug/L 50 118 50-130108 9 3050ND59.1 54.0
Dibenz(a,h)anthracene ug/L 50 119 40-130108 10 3050ND59.4 53.9
Dibenzofuran ug/L 50 95 40-13091 4 3050ND47.6 45.5
Diethylphthalate ug/L 50 98 40-13087 11 3050ND49.0 43.7
Dimethylphthalate ug/L 50 93 40-13086 7 3050ND46.4 43.1
Fluoranthene ug/L 50 109 30-13099 10 3050ND54.6 49.5
Fluorene ug/L 50 97 20-13093 4 3050ND48.4 46.6
Hexachloro-1,3-butadiene ug/L 50 75 10-13074 2 3050ND37.7 37.0
Hexachlorobenzene ug/L 50 94 30-13089 5 3050ND47.1 44.6
Hexachlorocyclopentadiene ug/L 50 77 10-15076 1 3050ND38.7 38.2
Hexachloroethane ug/L 50 83 10-13083 0 3050ND41.4 41.5
Indeno(1,2,3-cd)pyrene ug/L 50 115 40-130105 9 3050ND57.4 52.4
Isophorone ug/L 50 94 30-13093 1 3050ND46.9 46.5
N-Nitroso-di-n-propylamine ug/L 50 93 30-13092 1 3050ND46.4 45.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
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[phone]
Page 71 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2913402MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481368002
2913403
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/L 50 81 10-13078 4 3050ND40.7 39.2
N-Nitrosodiphenylamine ug/L 50 101 30-13097 4 3050ND50.4 48.7
Naphthalene ug/L 50 89 20-13088 1 3050ND44.6 43.9
Nitrobenzene ug/L 50 95 20-13095 0 3050ND47.7 47.7
Pentachlorophenol ug/L 100 99 10-14089 10 30100ND98.8 89.3
Phenanthrene ug/L 50 103 50-13095 8 3050ND51.4 47.4
Phenol ug/L 50 55 10-13054 3 3050ND27.7 27.0
Pyrene ug/L 50 106 50-13097 9 3050ND53.0 48.6
2,4,6-Tribromophenol (S)%103 10-13795
2-Fluorobiphenyl (S)%89 13-13084
2-Fluorophenol (S)%68 10-13067
Nitrobenzene-d5 (S)%96 13-13093
Phenol-d6 (S)%53 10-13052
Terphenyl-d14 (S)%116 25-130101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
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Page 72 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481464
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1491175
7199
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481464001, 92481464002, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007,
92481464008, 92481464009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3539076-1
Associated Lab Samples:92481464001, 92481464002, 92481464003, 92481464004, 92481464005, 92481464006, 92481464007,
92481464008, 92481464009
Matrix:Water
AnalyzedMDL
Chromium, Hexavalent ug/L ND 0.100 06/15/20 14:010.0400
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3539076-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent ug/L 0.4910.500 98.2 90.0-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3539076-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1227922-02
R3539076-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent ug/L 1.00 101 90.0-110102 0.653 201.00ND 1.01 1.02
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3539076-6MATRIX SPIKE SAMPLE:
MSSpike
Result
92481464005
Chromium, Hexavalent ug/L 5.12 E,MH1.00 126 90.0-1103.86
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1227236-01
R3539076-3SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L 0.0899J J0.607 200.0905
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92481464006
R3539076-8SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L 9.52 0.141 209.51
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
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Huntersville, NC 28078
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Page 73 of 81
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92481464
FDP-058
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Detection due to carryover from previously analyzed sample.1g
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
Surrogate recovery not evaluated against control limits due to sample dilution.S4
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
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[phone]
Page 74 of 81
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92481464
FDP-058
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92481464001 1493080 1493080R-30 3015 EPA 6020B
92481464002 1493080 1493080S-58 3015 EPA 6020B
92481464003 1493080 1493080Z-90 3015 EPA 6020B
92481464004 1493080 1493080DD-40 3015 EPA 6020B
92481464005 1493080 1493080GG-43 3015 EPA 6020B
92481464006 1493080 1493080RR-102 3015 EPA 6020B
92481464007 1493080 1493080TT-34 3015 EPA 6020B
92481464008 1493080 1493080YY-37 3015 EPA 6020B
92481464009 1493080 1493080GW-Dup 3015 EPA 6020B
92481464001 1492418 1492418R-30 7470A EPA 7470A
92481464002 1492418 1492418S-58 7470A EPA 7470A
92481464003 1492418 1492418Z-90 7470A EPA 7470A
92481464004 1492418 1492418DD-40 7470A EPA 7470A
92481464005 1492418 1492418GG-43 7470A EPA 7470A
92481464006 1492418 1492418RR-102 7470A EPA 7470A
92481464007 1492418 1492418TT-34 7470A EPA 7470A
92481464008 1492418 1492418YY-37 7470A EPA 7470A
92481464009 1492419 1492419GW-Dup 7470A EPA 7470A
92481464001 547414 547527R-30 EPA 3510C EPA 8270E
92481464002 547414 547527S-58 EPA 3510C EPA 8270E
92481464003 547414 547527Z-90 EPA 3510C EPA 8270E
92481464004 547414 547527DD-40 EPA 3510C EPA 8270E
92481464005 547414 547527GG-43 EPA 3510C EPA 8270E
92481464006 547414 547527RR-102 EPA 3510C EPA 8270E
92481464007 547414 547527TT-34 EPA 3510C EPA 8270E
92481464008 547414 547527YY-37 EPA 3510C EPA 8270E
92481464009 547414 547527GW-Dup EPA 3510C EPA 8270E
92481464001 547618R-30 EPA 8260D
92481464002 547850S-58 EPA 8260D
92481464003 547618Z-90 EPA 8260D
92481464004 547618DD-40 EPA 8260D
92481464005 547618GG-43 EPA 8260D
92481464006 547618RR-102 EPA 8260D
92481464007 547618TT-34 EPA 8260D
92481464008 547850YY-37 EPA 8260D
92481464009 548122GW-Dup EPA 8260D
92481464010 547453Trip Blank-1 EPA 8260D
92481464001 1491175 1491175R-30 7199 EPA 7199
92481464002 1491175 1491175S-58 7199 EPA 7199
92481464003 1491175 1491175Z-90 7199 EPA 7199
92481464004 1491175 1491175DD-40 7199 EPA 7199
92481464005 1491175 1491175GG-43 7199 EPA 7199
92481464006 1491175 1491175RR-102 7199 EPA 7199
92481464007 1491175 1491175TT-34 7199 EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 75 of 81
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92481464
FDP-058
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92481464008 1491175 1491175YY-37 7199 EPA 7199
92481464009 1491175 1491175GW-Dup 7199 EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/13/2020 04:54 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 81
Page 77 of 81
Page 78 of 81
Page 79 of 81
Page 80 of 81
Page 81 of 81
#=CL#
June 17, 2020
LIMS USE: FR - RALPH MCGEE
LIMS OBJECT ID: 92481193
92481193
Project:
Pace Project No.:
RE:
Ralph McGee
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
FDP-058
Dear Ralph McGee:
Enclosed are the analytical results for sample(s) received by the laboratory on June 10, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 43
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92481193
FDP-058
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 43
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92481193
FDP-058
Lab ID Sample ID Matrix Date Collected Date Received
92481193001 SW-1 Water 06/09/20 16:20 06/10/20 10:20
92481193002 SW-4 Water 06/09/20 14:45 06/10/20 10:20
92481193003 SW-DUP Water 06/09/20 00:00 06/10/20 10:20
92481193004 Trip Blank Water 06/09/20 00:00 06/10/20 10:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 43
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92481193
FDP-058
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92481193001 SW-1 EPA 6020B 9 PANLD
EPA 7470A 1 PANSD
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
SM2340-97 1 PANLD
92481193002 SW-4 EPA 6020B 9 PANLD
EPA 7470A 1 PANSD
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
SM2340-97 1 PANLD
92481193003 SW-DUP EPA 6020B 9 PANLD
EPA 7470A 1 PANSD
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
EPA 7199 1 PANGB
SM2340-97 1 PANLD
92481193004 Trip Blank EPA 8260D 63 PASI-CSAS
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-1 Lab ID:92481193001 Collected:06/09/20 16:20 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/15/20 21:35 7440-38-206/15/20 16:342.00 0.735 1
Barium 52.9 ug/L 06/15/20 21:35 7440-39-306/15/20 16:3420.0 7.78 1
Cadmium ND ug/L 06/15/20 21:35 7440-43-906/15/20 16:341.00 0.478 1
Calcium 10700 ug/L 06/15/20 21:35 7440-70-206/15/20 16:3410004801
Chromium 1.93J ug/L 06/15/20 21:23 7440-47-3 J06/15/20 16:342.00 1.49 1
Lead ND ug/L 06/15/20 21:35 7439-92-106/15/20 16:345.00 2.49 1
Magnesium 3990 ug/L 06/15/20 21:35 7439-95-406/15/20 16:3410004651
Selenium ND ug/L 06/15/20 21:35 7782-49-206/15/20 16:342.00 0.657 1
Silver ND ug/L 06/15/20 21:35 7440-22-406/15/20 16:342.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/12/20 19:34 7439-97-606/12/20 09:060.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/12/20 12:23 83-32-906/11/20 11:3910.0 1.4 1
Acenaphthylene ND ug/L 06/12/20 12:23 208-96-806/11/20 11:3910.0 1.5 1
Aniline ND ug/L 06/12/20 12:23 62-53-306/11/20 11:3910.0 1.6 1
Anthracene ND ug/L 06/12/20 12:23 120-12-706/11/20 11:3910.0 1.6 1
Benzo(a)anthracene ND ug/L 06/12/20 12:23 56-55-306/11/20 11:3910.0 1.5 1
Benzo(a)pyrene ND ug/L 06/12/20 12:23 50-32-806/11/20 11:3910.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/12/20 12:23 205-99-206/11/20 11:3910.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/12/20 12:23 191-24-206/11/20 11:3910.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/12/20 12:23 207-08-906/11/20 11:3910.0 1.5 1
Benzoic Acid ND ug/L 06/12/20 12:23 65-85-006/11/20 11:3950.0 19.5 1
Benzyl alcohol ND ug/L 06/12/20 12:23 100-51-606/11/20 11:3920.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/12/20 12:23 101-55-306/11/20 11:3910.0 1.2 1
Butylbenzylphthalate ND ug/L 06/12/20 12:23 85-68-706/11/20 11:3910.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/12/20 12:23 59-50-706/11/20 11:3910.0 2.8 1
4-Chloroaniline ND ug/L 06/12/20 12:23 106-47-806/11/20 11:3920.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/12/20 12:23 111-91-106/11/20 11:3910.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/12/20 12:23 111-44-406/11/20 11:3910.0 1.7 1
2-Chloronaphthalene ND ug/L 06/12/20 12:23 91-58-706/11/20 11:3910.0 1.4 1
2-Chlorophenol ND ug/L 06/12/20 12:23 95-57-806/11/20 11:3910.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/12/20 12:23 7005-72-306/11/20 11:3910.0 1.5 1
Chrysene ND ug/L 06/12/20 12:23 218-01-906/11/20 11:3910.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/12/20 12:23 53-70-306/11/20 11:3910.0 1.6 1
Dibenzofuran ND ug/L 06/12/20 12:23 132-64-906/11/20 11:3910.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/12/20 12:23 95-50-106/11/20 11:3910.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/12/20 12:23 541-73-106/11/20 11:3910.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/12/20 12:23 106-46-706/11/20 11:3910.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/12/20 12:23 91-94-106/11/20 11:3920.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/12/20 12:23 120-83-206/11/20 11:3910.0 1.5 1
Diethylphthalate ND ug/L 06/12/20 12:23 84-66-206/11/20 11:3910.0 1.6 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 5 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-1 Lab ID:92481193001 Collected:06/09/20 16:20 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
2,4-Dimethylphenol ND ug/L 06/12/20 12:23 105-67-906/11/20 11:3910.0 1.5 1
Dimethylphthalate ND ug/L 06/12/20 12:23 131-11-306/11/20 11:3910.0 1.4 1
Di-n-butylphthalate ND ug/L 06/12/20 12:23 84-74-206/11/20 11:3910.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/12/20 12:23 534-52-106/11/20 11:3920.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/12/20 12:23 51-28-506/11/20 11:3950.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/12/20 12:23 121-14-206/11/20 11:3910.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/12/20 12:23 606-20-206/11/20 11:3910.0 1.7 1
Di-n-octylphthalate ND ug/L 06/12/20 12:23 117-84-006/11/20 11:3910.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/12/20 12:23 117-81-706/11/20 11:396.0 2.0 1
Fluoranthene ND ug/L 06/12/20 12:23 206-44-006/11/20 11:3910.0 1.6 1
Fluorene ND ug/L 06/12/20 12:23 86-73-706/11/20 11:3910.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/12/20 12:23 87-68-306/11/20 11:3910.0 1.6 1
Hexachlorobenzene ND ug/L 06/12/20 12:23 118-74-106/11/20 11:3910.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/12/20 12:23 77-47-406/11/20 11:3910.0 2.4 1
Hexachloroethane ND ug/L 06/12/20 12:23 67-72-106/11/20 11:3910.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/12/20 12:23 193-39-506/11/20 11:3910.0 1.7 1
Isophorone ND ug/L 06/12/20 12:23 78-59-106/11/20 11:3910.0 1.3 1
1-Methylnaphthalene ND ug/L 06/12/20 12:23 90-12-006/11/20 11:3910.0 1.4 1
2-Methylnaphthalene ND ug/L 06/12/20 12:23 91-57-606/11/20 11:3910.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/12/20 12:23 95-48-706/11/20 11:3910.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/12/20 12:23 15831-10-406/11/20 11:3910.0 1.2 1
Naphthalene ND ug/L 06/12/20 12:23 91-20-306/11/20 11:3910.0 1.6 1
2-Nitroaniline ND ug/L 06/12/20 12:23 88-74-406/11/20 11:3920.0 3.0 1
3-Nitroaniline ND ug/L 06/12/20 12:23 99-09-206/11/20 11:3920.0 2.8 1
4-Nitroaniline ND ug/L 06/12/20 12:23 100-01-606/11/20 11:3920.0 3.1 1
Nitrobenzene ND ug/L 06/12/20 12:23 98-95-306/11/20 11:3910.0 1.5 1
2-Nitrophenol ND ug/L 06/12/20 12:23 88-75-506/11/20 11:3910.0 1.7 1
4-Nitrophenol ND ug/L 06/12/20 12:23 100-02-706/11/20 11:3950.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/12/20 12:23 62-75-906/11/20 11:3910.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/12/20 12:23 621-64-706/11/20 11:3910.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/12/20 12:23 86-30-606/11/20 11:3910.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/12/20 12:23 108-60-106/11/20 11:3910.0 1.3 1
Pentachlorophenol ND ug/L 06/12/20 12:23 87-86-506/11/20 11:3920.0 2.8 1
Phenanthrene ND ug/L 06/12/20 12:23 85-01-806/11/20 11:3910.0 1.4 1
Phenol ND ug/L 06/12/20 12:23 108-95-206/11/20 11:3910.0 1.5 1
Pyrene ND ug/L 06/12/20 12:23 129-00-006/11/20 11:3910.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/12/20 12:23 120-82-106/11/20 11:3910.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/12/20 12:23 95-95-406/11/20 11:3910.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/12/20 12:23 88-06-206/11/20 11:3910.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)52 %06/12/20 12:23 4165-60-006/11/20 11:3913-130 1
2-Fluorobiphenyl (S)40 %06/12/20 12:23 321-60-806/11/20 11:3913-130 1
Terphenyl-d14 (S)103 %06/12/20 12:23 1718-51-006/11/20 11:3925-130 1
Phenol-d6 (S)32 %06/12/20 12:23 13127-88-306/11/20 11:3910-130 1
2-Fluorophenol (S)41 %06/12/20 12:23 367-12-406/11/20 11:3910-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 6 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-1 Lab ID:92481193001 Collected:06/09/20 16:20 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Surrogates
2,4,6-Tribromophenol (S)70 %06/12/20 12:23 118-79-606/11/20 11:3910-137 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/16/20 07:06 67-64-125.0 6.2 1
Benzene ND ug/L 06/16/20 07:06 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/16/20 07:06 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/16/20 07:06 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/16/20 07:06 75-27-41.0 0.26 1
Bromoform ND ug/L 06/16/20 07:06 75-25-2 L2,v11.0 0.62 1
Bromomethane ND ug/L 06/16/20 07:06 74-83-9 v12.0 0.62 1
2-Butanone (MEK)ND ug/L 06/16/20 07:06 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/16/20 07:06 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/16/20 07:06 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/16/20 07:06 75-00-31.0 0.49 1
Chloroform ND ug/L 06/16/20 07:06 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/16/20 07:06 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 06/16/20 07:06 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/16/20 07:06 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/16/20 07:06 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/16/20 07:06 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/16/20 07:06 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/16/20 07:06 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/16/20 07:06 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/16/20 07:06 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/16/20 07:06 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/16/20 07:06 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/16/20 07:06 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/16/20 07:06 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/16/20 07:06 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/16/20 07:06 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/16/20 07:06 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/16/20 07:06 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/16/20 07:06 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/16/20 07:06 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/16/20 07:06 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/16/20 07:06 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/16/20 07:06 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/16/20 07:06 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/16/20 07:06 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/16/20 07:06 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/16/20 07:06 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/16/20 07:06 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/16/20 07:06 75-09-25.0 3.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-1 Lab ID:92481193001 Collected:06/09/20 16:20 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
4-Methyl-2-pentanone (MIBK)ND ug/L 06/16/20 07:06 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/16/20 07:06 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/16/20 07:06 91-20-31.0 0.35 1
Styrene ND ug/L 06/16/20 07:06 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/16/20 07:06 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 06/16/20 07:06 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/16/20 07:06 127-18-41.0 0.16 1
Toluene ND ug/L 06/16/20 07:06 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/16/20 07:06 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/16/20 07:06 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/16/20 07:06 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/16/20 07:06 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/16/20 07:06 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/16/20 07:06 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/16/20 07:06 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/16/20 07:06 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 06/16/20 07:06 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/16/20 07:06 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/16/20 07:06 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/16/20 07:06 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)94 %06/16/20 07:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %06/16/20 07:06 17060-07-070-130 1
Toluene-d8 (S)101 %06/16/20 07:06 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.101 ug/L 06/15/20 16:09 18540-29-906/15/20 16:090.100 0.0400 1
Analytical Method: SM2340-97 Preparation Method: SM2340B
Pace National - Mt. Juliet
Calculated Results
Hardness, Total(SM 2340B)43000 ug/L 06/15/20 21:3506/15/20 21:35250012001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-4 Lab ID:92481193002 Collected:06/09/20 14:45 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/15/20 21:38 7440-38-206/15/20 16:342.00 0.735 1
Barium 52.0 ug/L 06/15/20 21:38 7440-39-306/15/20 16:3420.0 7.78 1
Cadmium ND ug/L 06/15/20 21:38 7440-43-906/15/20 16:341.00 0.478 1
Calcium 10900 ug/L 06/15/20 21:38 7440-70-206/15/20 16:3410004801
Chromium 2.04 ug/L 06/15/20 21:26 7440-47-306/15/20 16:342.00 1.49 1
Lead ND ug/L 06/15/20 21:38 7439-92-106/15/20 16:345.00 2.49 1
Magnesium 4120 ug/L 06/15/20 21:38 7439-95-406/15/20 16:3410004651
Selenium ND ug/L 06/15/20 21:38 7782-49-206/15/20 16:342.00 0.657 1
Silver ND ug/L 06/15/20 21:38 7440-22-406/15/20 16:342.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/12/20 19:36 7439-97-606/12/20 09:060.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/12/20 12:52 83-32-906/11/20 11:3910.0 1.4 1
Acenaphthylene ND ug/L 06/12/20 12:52 208-96-806/11/20 11:3910.0 1.5 1
Aniline ND ug/L 06/12/20 12:52 62-53-306/11/20 11:3910.0 1.6 1
Anthracene ND ug/L 06/12/20 12:52 120-12-706/11/20 11:3910.0 1.6 1
Benzo(a)anthracene ND ug/L 06/12/20 12:52 56-55-306/11/20 11:3910.0 1.5 1
Benzo(a)pyrene ND ug/L 06/12/20 12:52 50-32-806/11/20 11:3910.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/12/20 12:52 205-99-206/11/20 11:3910.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/12/20 12:52 191-24-206/11/20 11:3910.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/12/20 12:52 207-08-906/11/20 11:3910.0 1.5 1
Benzoic Acid ND ug/L 06/12/20 12:52 65-85-006/11/20 11:3950.0 19.5 1
Benzyl alcohol ND ug/L 06/12/20 12:52 100-51-606/11/20 11:3920.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/12/20 12:52 101-55-306/11/20 11:3910.0 1.2 1
Butylbenzylphthalate ND ug/L 06/12/20 12:52 85-68-706/11/20 11:3910.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/12/20 12:52 59-50-706/11/20 11:3910.0 2.8 1
4-Chloroaniline ND ug/L 06/12/20 12:52 106-47-806/11/20 11:3920.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/12/20 12:52 111-91-106/11/20 11:3910.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/12/20 12:52 111-44-406/11/20 11:3910.0 1.7 1
2-Chloronaphthalene ND ug/L 06/12/20 12:52 91-58-706/11/20 11:3910.0 1.4 1
2-Chlorophenol ND ug/L 06/12/20 12:52 95-57-806/11/20 11:3910.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/12/20 12:52 7005-72-306/11/20 11:3910.0 1.5 1
Chrysene ND ug/L 06/12/20 12:52 218-01-906/11/20 11:3910.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/12/20 12:52 53-70-306/11/20 11:3910.0 1.6 1
Dibenzofuran ND ug/L 06/12/20 12:52 132-64-906/11/20 11:3910.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/12/20 12:52 95-50-106/11/20 11:3910.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/12/20 12:52 541-73-106/11/20 11:3910.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/12/20 12:52 106-46-706/11/20 11:3910.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/12/20 12:52 91-94-106/11/20 11:3920.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/12/20 12:52 120-83-206/11/20 11:3910.0 1.5 1
Diethylphthalate ND ug/L 06/12/20 12:52 84-66-206/11/20 11:3910.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-4 Lab ID:92481193002 Collected:06/09/20 14:45 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
2,4-Dimethylphenol ND ug/L 06/12/20 12:52 105-67-906/11/20 11:3910.0 1.5 1
Dimethylphthalate ND ug/L 06/12/20 12:52 131-11-306/11/20 11:3910.0 1.4 1
Di-n-butylphthalate ND ug/L 06/12/20 12:52 84-74-206/11/20 11:3910.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/12/20 12:52 534-52-106/11/20 11:3920.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/12/20 12:52 51-28-506/11/20 11:3950.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/12/20 12:52 121-14-206/11/20 11:3910.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/12/20 12:52 606-20-206/11/20 11:3910.0 1.7 1
Di-n-octylphthalate ND ug/L 06/12/20 12:52 117-84-006/11/20 11:3910.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/12/20 12:52 117-81-706/11/20 11:396.0 2.0 1
Fluoranthene ND ug/L 06/12/20 12:52 206-44-006/11/20 11:3910.0 1.6 1
Fluorene ND ug/L 06/12/20 12:52 86-73-706/11/20 11:3910.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/12/20 12:52 87-68-306/11/20 11:3910.0 1.6 1
Hexachlorobenzene ND ug/L 06/12/20 12:52 118-74-106/11/20 11:3910.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/12/20 12:52 77-47-406/11/20 11:3910.0 2.4 1
Hexachloroethane ND ug/L 06/12/20 12:52 67-72-106/11/20 11:3910.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/12/20 12:52 193-39-506/11/20 11:3910.0 1.7 1
Isophorone ND ug/L 06/12/20 12:52 78-59-106/11/20 11:3910.0 1.3 1
1-Methylnaphthalene ND ug/L 06/12/20 12:52 90-12-006/11/20 11:3910.0 1.4 1
2-Methylnaphthalene ND ug/L 06/12/20 12:52 91-57-606/11/20 11:3910.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/12/20 12:52 95-48-706/11/20 11:3910.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/12/20 12:52 15831-10-406/11/20 11:3910.0 1.2 1
Naphthalene ND ug/L 06/12/20 12:52 91-20-306/11/20 11:3910.0 1.6 1
2-Nitroaniline ND ug/L 06/12/20 12:52 88-74-406/11/20 11:3920.0 3.0 1
3-Nitroaniline ND ug/L 06/12/20 12:52 99-09-206/11/20 11:3920.0 2.8 1
4-Nitroaniline ND ug/L 06/12/20 12:52 100-01-606/11/20 11:3920.0 3.1 1
Nitrobenzene ND ug/L 06/12/20 12:52 98-95-306/11/20 11:3910.0 1.5 1
2-Nitrophenol ND ug/L 06/12/20 12:52 88-75-506/11/20 11:3910.0 1.7 1
4-Nitrophenol ND ug/L 06/12/20 12:52 100-02-706/11/20 11:3950.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/12/20 12:52 62-75-906/11/20 11:3910.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/12/20 12:52 621-64-706/11/20 11:3910.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/12/20 12:52 86-30-606/11/20 11:3910.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/12/20 12:52 108-60-106/11/20 11:3910.0 1.3 1
Pentachlorophenol ND ug/L 06/12/20 12:52 87-86-506/11/20 11:3920.0 2.8 1
Phenanthrene ND ug/L 06/12/20 12:52 85-01-806/11/20 11:3910.0 1.4 1
Phenol ND ug/L 06/12/20 12:52 108-95-206/11/20 11:3910.0 1.5 1
Pyrene ND ug/L 06/12/20 12:52 129-00-006/11/20 11:3910.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/12/20 12:52 120-82-106/11/20 11:3910.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/12/20 12:52 95-95-406/11/20 11:3910.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/12/20 12:52 88-06-206/11/20 11:3910.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)77 %06/12/20 12:52 4165-60-006/11/20 11:3913-130 1
2-Fluorobiphenyl (S)65 %06/12/20 12:52 321-60-806/11/20 11:3913-130 1
Terphenyl-d14 (S)115 %06/12/20 12:52 1718-51-006/11/20 11:3925-130 1
Phenol-d6 (S)43 %06/12/20 12:52 13127-88-306/11/20 11:3910-130 1
2-Fluorophenol (S)57 %06/12/20 12:52 367-12-406/11/20 11:3910-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-4 Lab ID:92481193002 Collected:06/09/20 14:45 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Surrogates
2,4,6-Tribromophenol (S)86 %06/12/20 12:52 118-79-606/11/20 11:3910-137 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/16/20 07:24 67-64-125.0 6.2 1
Benzene ND ug/L 06/16/20 07:24 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/16/20 07:24 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/16/20 07:24 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/16/20 07:24 75-27-41.0 0.26 1
Bromoform ND ug/L 06/16/20 07:24 75-25-2 L2,v11.0 0.62 1
Bromomethane ND ug/L 06/16/20 07:24 74-83-9 v12.0 0.62 1
2-Butanone (MEK)ND ug/L 06/16/20 07:24 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/16/20 07:24 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/16/20 07:24 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/16/20 07:24 75-00-31.0 0.49 1
Chloroform ND ug/L 06/16/20 07:24 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/16/20 07:24 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 06/16/20 07:24 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/16/20 07:24 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/16/20 07:24 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/16/20 07:24 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/16/20 07:24 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/16/20 07:24 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/16/20 07:24 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/16/20 07:24 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/16/20 07:24 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/16/20 07:24 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/16/20 07:24 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/16/20 07:24 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/16/20 07:24 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/16/20 07:24 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/16/20 07:24 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/16/20 07:24 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/16/20 07:24 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/16/20 07:24 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/16/20 07:24 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/16/20 07:24 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/16/20 07:24 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/16/20 07:24 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/16/20 07:24 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/16/20 07:24 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/16/20 07:24 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/16/20 07:24 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/16/20 07:24 75-09-25.0 3.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-4 Lab ID:92481193002 Collected:06/09/20 14:45 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
4-Methyl-2-pentanone (MIBK)ND ug/L 06/16/20 07:24 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/16/20 07:24 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/16/20 07:24 91-20-31.0 0.35 1
Styrene ND ug/L 06/16/20 07:24 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/16/20 07:24 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 06/16/20 07:24 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/16/20 07:24 127-18-41.0 0.16 1
Toluene ND ug/L 06/16/20 07:24 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/16/20 07:24 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/16/20 07:24 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/16/20 07:24 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/16/20 07:24 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/16/20 07:24 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/16/20 07:24 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/16/20 07:24 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/16/20 07:24 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 06/16/20 07:24 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/16/20 07:24 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/16/20 07:24 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/16/20 07:24 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)97 %06/16/20 07:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %06/16/20 07:24 17060-07-070-130 1
Toluene-d8 (S)101 %06/16/20 07:24 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.115 ug/L 06/15/20 16:31 18540-29-906/15/20 16:310.100 0.0400 1
Analytical Method: SM2340-97 Preparation Method: SM2340B
Pace National - Mt. Juliet
Calculated Results
Hardness, Total(SM 2340B)44100 ug/L 06/15/20 21:3806/15/20 21:38250012001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-DUP Lab ID:92481193003 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/15/20 21:41 7440-38-206/15/20 16:342.00 0.735 1
Barium 52.6 ug/L 06/15/20 21:41 7440-39-306/15/20 16:3420.0 7.78 1
Cadmium ND ug/L 06/15/20 21:41 7440-43-906/15/20 16:341.00 0.478 1
Calcium 10900 ug/L 06/15/20 21:41 7440-70-206/15/20 16:3410004801
Chromium 2.15 ug/L 06/15/20 21:30 7440-47-306/15/20 16:342.00 1.49 1
Lead 2.65J ug/L 06/15/20 21:41 7439-92-1 J06/15/20 16:345.00 2.49 1
Magnesium 4110 ug/L 06/15/20 21:41 7439-95-406/15/20 16:3410004651
Selenium ND ug/L 06/15/20 21:41 7782-49-206/15/20 16:342.00 0.657 1
Silver ND ug/L 06/15/20 21:41 7440-22-406/15/20 16:342.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/12/20 19:38 7439-97-606/12/20 09:060.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/12/20 10:55 83-32-906/11/20 11:3910.0 1.4 1
Acenaphthylene ND ug/L 06/12/20 10:55 208-96-806/11/20 11:3910.0 1.5 1
Aniline ND ug/L 06/12/20 10:55 62-53-306/11/20 11:3910.0 1.6 1
Anthracene ND ug/L 06/12/20 10:55 120-12-706/11/20 11:3910.0 1.6 1
Benzo(a)anthracene ND ug/L 06/12/20 10:55 56-55-306/11/20 11:3910.0 1.5 1
Benzo(a)pyrene ND ug/L 06/12/20 10:55 50-32-806/11/20 11:3910.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/12/20 10:55 205-99-206/11/20 11:3910.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/12/20 10:55 191-24-206/11/20 11:3910.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/12/20 10:55 207-08-906/11/20 11:3910.0 1.5 1
Benzoic Acid ND ug/L 06/12/20 10:55 65-85-006/11/20 11:3950.0 19.5 1
Benzyl alcohol ND ug/L 06/12/20 10:55 100-51-606/11/20 11:3920.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/12/20 10:55 101-55-306/11/20 11:3910.0 1.2 1
Butylbenzylphthalate ND ug/L 06/12/20 10:55 85-68-706/11/20 11:3910.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/12/20 10:55 59-50-706/11/20 11:3910.0 2.8 1
4-Chloroaniline ND ug/L 06/12/20 10:55 106-47-806/11/20 11:3920.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/12/20 10:55 111-91-106/11/20 11:3910.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/12/20 10:55 111-44-406/11/20 11:3910.0 1.7 1
2-Chloronaphthalene ND ug/L 06/12/20 10:55 91-58-706/11/20 11:3910.0 1.4 1
2-Chlorophenol ND ug/L 06/12/20 10:55 95-57-806/11/20 11:3910.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/12/20 10:55 7005-72-306/11/20 11:3910.0 1.5 1
Chrysene ND ug/L 06/12/20 10:55 218-01-906/11/20 11:3910.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/12/20 10:55 53-70-306/11/20 11:3910.0 1.6 1
Dibenzofuran ND ug/L 06/12/20 10:55 132-64-906/11/20 11:3910.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/12/20 10:55 95-50-106/11/20 11:3910.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/12/20 10:55 541-73-106/11/20 11:3910.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/12/20 10:55 106-46-706/11/20 11:3910.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/12/20 10:55 91-94-106/11/20 11:3920.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/12/20 10:55 120-83-206/11/20 11:3910.0 1.5 1
Diethylphthalate ND ug/L 06/12/20 10:55 84-66-206/11/20 11:3910.0 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-DUP Lab ID:92481193003 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
2,4-Dimethylphenol ND ug/L 06/12/20 10:55 105-67-906/11/20 11:3910.0 1.5 1
Dimethylphthalate ND ug/L 06/12/20 10:55 131-11-306/11/20 11:3910.0 1.4 1
Di-n-butylphthalate ND ug/L 06/12/20 10:55 84-74-206/11/20 11:3910.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/12/20 10:55 534-52-106/11/20 11:3920.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/12/20 10:55 51-28-506/11/20 11:3950.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/12/20 10:55 121-14-206/11/20 11:3910.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/12/20 10:55 606-20-206/11/20 11:3910.0 1.7 1
Di-n-octylphthalate ND ug/L 06/12/20 10:55 117-84-006/11/20 11:3910.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/12/20 10:55 117-81-706/11/20 11:396.0 2.0 1
Fluoranthene ND ug/L 06/12/20 10:55 206-44-006/11/20 11:3910.0 1.6 1
Fluorene ND ug/L 06/12/20 10:55 86-73-706/11/20 11:3910.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/12/20 10:55 87-68-306/11/20 11:3910.0 1.6 1
Hexachlorobenzene ND ug/L 06/12/20 10:55 118-74-106/11/20 11:3910.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/12/20 10:55 77-47-406/11/20 11:3910.0 2.4 1
Hexachloroethane ND ug/L 06/12/20 10:55 67-72-106/11/20 11:3910.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/12/20 10:55 193-39-506/11/20 11:3910.0 1.7 1
Isophorone ND ug/L 06/12/20 10:55 78-59-106/11/20 11:3910.0 1.3 1
1-Methylnaphthalene ND ug/L 06/12/20 10:55 90-12-006/11/20 11:3910.0 1.4 1
2-Methylnaphthalene ND ug/L 06/12/20 10:55 91-57-606/11/20 11:3910.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/12/20 10:55 95-48-706/11/20 11:3910.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/12/20 10:55 15831-10-406/11/20 11:3910.0 1.2 1
Naphthalene ND ug/L 06/12/20 10:55 91-20-306/11/20 11:3910.0 1.6 1
2-Nitroaniline ND ug/L 06/12/20 10:55 88-74-406/11/20 11:3920.0 3.0 1
3-Nitroaniline ND ug/L 06/12/20 10:55 99-09-206/11/20 11:3920.0 2.8 1
4-Nitroaniline ND ug/L 06/12/20 10:55 100-01-606/11/20 11:3920.0 3.1 1
Nitrobenzene ND ug/L 06/12/20 10:55 98-95-306/11/20 11:3910.0 1.5 1
2-Nitrophenol ND ug/L 06/12/20 10:55 88-75-506/11/20 11:3910.0 1.7 1
4-Nitrophenol ND ug/L 06/12/20 10:55 100-02-706/11/20 11:3950.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/12/20 10:55 62-75-906/11/20 11:3910.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/12/20 10:55 621-64-706/11/20 11:3910.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/12/20 10:55 86-30-606/11/20 11:3910.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/12/20 10:55 108-60-106/11/20 11:3910.0 1.3 1
Pentachlorophenol ND ug/L 06/12/20 10:55 87-86-506/11/20 11:3920.0 2.8 1
Phenanthrene ND ug/L 06/12/20 10:55 85-01-806/11/20 11:3910.0 1.4 1
Phenol ND ug/L 06/12/20 10:55 108-95-206/11/20 11:3910.0 1.5 1
Pyrene ND ug/L 06/12/20 10:55 129-00-006/11/20 11:3910.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/12/20 10:55 120-82-106/11/20 11:3910.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/12/20 10:55 95-95-406/11/20 11:3910.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/12/20 10:55 88-06-206/11/20 11:3910.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)71 %06/12/20 10:55 4165-60-006/11/20 11:3913-130 1
2-Fluorobiphenyl (S)58 %06/12/20 10:55 321-60-806/11/20 11:3913-130 1
Terphenyl-d14 (S)105 %06/12/20 10:55 1718-51-006/11/20 11:3925-130 1
Phenol-d6 (S)42 %06/12/20 10:55 13127-88-306/11/20 11:3910-130 1
2-Fluorophenol (S)54 %06/12/20 10:55 367-12-406/11/20 11:3910-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-DUP Lab ID:92481193003 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Surrogates
2,4,6-Tribromophenol (S)82 %06/12/20 10:55 118-79-606/11/20 11:3910-137 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/16/20 07:42 67-64-125.0 6.2 1
Benzene ND ug/L 06/16/20 07:42 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/16/20 07:42 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/16/20 07:42 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/16/20 07:42 75-27-41.0 0.26 1
Bromoform ND ug/L 06/16/20 07:42 75-25-2 L2,v11.0 0.62 1
Bromomethane ND ug/L 06/16/20 07:42 74-83-9 v12.0 0.62 1
2-Butanone (MEK)ND ug/L 06/16/20 07:42 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/16/20 07:42 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/16/20 07:42 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/16/20 07:42 75-00-31.0 0.49 1
Chloroform ND ug/L 06/16/20 07:42 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/16/20 07:42 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 06/16/20 07:42 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/16/20 07:42 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/16/20 07:42 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/16/20 07:42 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/16/20 07:42 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/16/20 07:42 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/16/20 07:42 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/16/20 07:42 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/16/20 07:42 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/16/20 07:42 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/16/20 07:42 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/16/20 07:42 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/16/20 07:42 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/16/20 07:42 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/16/20 07:42 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/16/20 07:42 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/16/20 07:42 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/16/20 07:42 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/16/20 07:42 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/16/20 07:42 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/16/20 07:42 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/16/20 07:42 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/16/20 07:42 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/16/20 07:42 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/16/20 07:42 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/16/20 07:42 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/16/20 07:42 75-09-25.0 3.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:SW-DUP Lab ID:92481193003 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
4-Methyl-2-pentanone (MIBK)ND ug/L 06/16/20 07:42 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/16/20 07:42 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/16/20 07:42 91-20-31.0 0.35 1
Styrene ND ug/L 06/16/20 07:42 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/16/20 07:42 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 06/16/20 07:42 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/16/20 07:42 127-18-41.0 0.16 1
Toluene ND ug/L 06/16/20 07:42 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/16/20 07:42 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/16/20 07:42 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/16/20 07:42 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/16/20 07:42 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/16/20 07:42 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/16/20 07:42 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/16/20 07:42 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/16/20 07:42 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 06/16/20 07:42 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/16/20 07:42 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/16/20 07:42 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/16/20 07:42 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)94 %06/16/20 07:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)112 %06/16/20 07:42 17060-07-070-130 1
Toluene-d8 (S)103 %06/16/20 07:42 2037-26-570-130 1
Analytical Method: EPA 7199 Preparation Method: 7199
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.0555J ug/L 06/15/20 16:39 18540-29-9 J06/15/20 16:390.100 0.0400 1
Analytical Method: SM2340-97 Preparation Method: SM2340B
Pace National - Mt. Juliet
Calculated Results
Hardness, Total(SM 2340B)44100 ug/L 06/15/20 21:4106/15/20 21:41250012001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:Trip Blank Lab ID:92481193004 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/15/20 15:37 67-64-125.0 6.2 1
Benzene ND ug/L 06/15/20 15:37 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/15/20 15:37 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/15/20 15:37 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/15/20 15:37 75-27-41.0 0.26 1
Bromoform ND ug/L 06/15/20 15:37 75-25-21.0 0.62 1
Bromomethane ND ug/L 06/15/20 15:37 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 06/15/20 15:37 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/15/20 15:37 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/15/20 15:37 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/15/20 15:37 75-00-31.0 0.49 1
Chloroform ND ug/L 06/15/20 15:37 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/15/20 15:37 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 06/15/20 15:37 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/15/20 15:37 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/15/20 15:37 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/15/20 15:37 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/15/20 15:37 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/15/20 15:37 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/15/20 15:37 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/15/20 15:37 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/15/20 15:37 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/15/20 15:37 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/15/20 15:37 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/15/20 15:37 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/15/20 15:37 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/15/20 15:37 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/15/20 15:37 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/15/20 15:37 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/15/20 15:37 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/15/20 15:37 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/15/20 15:37 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/15/20 15:37 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/15/20 15:37 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/15/20 15:37 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/15/20 15:37 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/15/20 15:37 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/15/20 15:37 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/15/20 15:37 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/15/20 15:37 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/15/20 15:37 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/15/20 15:37 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/15/20 15:37 91-20-31.0 0.35 1
Styrene ND ug/L 06/15/20 15:37 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/15/20 15:37 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92481193
FDP-058
Sample:Trip Blank Lab ID:92481193004 Collected:06/09/20 00:00 Received:06/10/20 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/15/20 15:37 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/15/20 15:37 127-18-41.0 0.16 1
Toluene ND ug/L 06/15/20 15:37 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/15/20 15:37 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/15/20 15:37 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/15/20 15:37 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/15/20 15:37 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/15/20 15:37 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/15/20 15:37 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/15/20 15:37 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/15/20 15:37 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 06/15/20 15:37 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/15/20 15:37 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/15/20 15:37 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/15/20 15:37 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)93 %06/15/20 15:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %06/15/20 15:37 17060-07-070-130 1
Toluene-d8 (S)103 %06/15/20 15:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 18 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1491232
3015
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481193001, 92481193002, 92481193003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3538961-1
Associated Lab Samples:92481193001, 92481193002, 92481193003
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 2.00 06/15/20 19:580.735
Barium ug/L ND 20.0 06/15/20 19:587.78
Cadmium ug/L ND 1.00 06/15/20 19:580.478
Calcium ug/L ND 1000 06/15/20 19:58480
Lead ug/L ND 5.00 06/15/20 19:582.49
Magnesium ug/L ND 1000 06/15/20 19:58465
Selenium ug/L ND 2.00 06/15/20 19:580.657
Silver ug/L ND 2.00 06/15/20 19:580.513
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3538974-1
Associated Lab Samples:92481193001, 92481193002, 92481193003
Matrix:Water
AnalyzedMDL
Chromium ug/L ND 2.00 06/15/20 21:011.49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3538961-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 49.850.0 99.6 80.0-120
Barium ug/L 46.550.0 93.0 80.0-120
Cadmium ug/L 50.250.0 100 80.0-120
Calcium ug/L 48405000 96.7 80.0-120
Lead ug/L 49.350.0 98.6 80.0-120
Magnesium ug/L 49005000 98.0 80.0-120
Selenium ug/L 49.850.0 99.6 80.0-120
Silver ug/L 49.750.0 99.4 80.0-120
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3538974-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 49.250.0 98.4 80.0-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3538961-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
R3538961-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 50.0 99.8 75.0-12596.2 0.707 2050.0 254 253
Barium ug/L 50.0 106 75.0-12598.4 3.98 2050.0 92.9 89.3
Cadmium ug/L 50.0 100 75.0-125101 0.690 2050.0 50.2 50.5
Calcium ug/L 5000 79.1 75.0-12587.6 1.09 2050003910039600
Lead ug/L 50.0 99.5 75.0-12599.6 0.036 2050.0 49.8 49.8
Magnesium ug/L 5000 80.2 75.0-12593.3 1.93 2050003340034100
Selenium ug/L 50.0 103 75.0-125111 7.74 2050.0 51.3 55.4
Silver ug/L 50.0 101 75.0-125100 1.39 2050.0 50.7 50.0
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3538974-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
R3538974-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium ug/L 50.0 93.3 75.0-12594.9 1.64 2050.0 46.7 47.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1491239
7470A
EPA 7470A
Mercury 7470A
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481193001, 92481193002, 92481193003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3538205-1
Associated Lab Samples:92481193001, 92481193002, 92481193003
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.200 06/12/20 19:050.100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3538205-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 3.123.00 104 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3538205-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
R3538205-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 3.00 106 75.0-125103 2.41 203.00 3.18 3.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
547329
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481193004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2912925
Associated Lab Samples:92481193004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/15/20 12:370.34
1,1,1-Trichloroethane ug/L ND 1.0 06/15/20 12:370.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/15/20 12:370.22
1,1,2-Trichloroethane ug/L ND 1.0 06/15/20 12:370.24
1,1-Dichloroethane ug/L ND 1.0 06/15/20 12:370.27
1,1-Dichloroethene ug/L ND 1.0 06/15/20 12:370.24
1,1-Dichloropropene ug/L ND 1.0 06/15/20 12:370.21
1,2,3-Trichlorobenzene ug/L ND 1.0 06/15/20 12:370.34
1,2,3-Trichloropropane ug/L ND 1.0 06/15/20 12:370.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/15/20 12:370.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 06/15/20 12:370.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/15/20 12:370.26
1,2-Dichlorobenzene ug/L ND 1.0 06/15/20 12:370.29
1,2-Dichloroethane ug/L ND 1.0 06/15/20 12:370.34
1,2-Dichloropropane ug/L ND 1.0 06/15/20 12:370.19
1,3-Dichlorobenzene ug/L ND 1.0 06/15/20 12:370.22
1,3-Dichloropropane ug/L ND 1.0 06/15/20 12:370.16
1,4-Dichlorobenzene ug/L ND 1.0 06/15/20 12:370.26
2,2-Dichloropropane ug/L ND 1.0 06/15/20 12:370.27
2-Butanone (MEK)ug/L ND 5.0 06/15/20 12:373.3
2-Chlorotoluene ug/L ND 1.0 06/15/20 12:370.20
2-Hexanone ug/L ND 5.0 06/15/20 12:370.57
4-Chlorotoluene ug/L ND 1.0 06/15/20 12:370.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/15/20 12:374.5
Acetone ug/L ND 25.0 06/15/20 12:376.2
Benzene ug/L ND 1.0 06/15/20 12:370.15
Bromobenzene ug/L ND 1.0 06/15/20 12:370.22
Bromochloromethane ug/L ND 1.0 06/15/20 12:370.34
Bromodichloromethane ug/L ND 1.0 06/15/20 12:370.26
Bromoform ug/L ND 1.0 06/15/20 12:370.62
Bromomethane ug/L ND 2.0 06/15/20 12:370.62
Carbon tetrachloride ug/L ND 1.0 06/15/20 12:370.22
Chlorobenzene ug/L ND 1.0 06/15/20 12:370.23
Chloroethane ug/L ND 1.0 06/15/20 12:370.49
Chloroform ug/L ND 5.0 06/15/20 12:372.3
Chloromethane ug/L ND 1.0 06/15/20 12:370.39
cis-1,2-Dichloroethene ug/L ND 1.0 06/15/20 12:370.29
cis-1,3-Dichloropropene ug/L ND 1.0 06/15/20 12:370.30
Dibromochloromethane ug/L ND 1.0 06/15/20 12:370.41
Dibromomethane ug/L ND 1.0 06/15/20 12:370.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2912925
Associated Lab Samples:92481193004
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 06/15/20 12:370.23
Diisopropyl ether ug/L ND 1.0 06/15/20 12:370.22
Ethylbenzene ug/L ND 1.0 06/15/20 12:370.26
Hexachloro-1,3-butadiene ug/L ND 1.0 06/15/20 12:370.44
m&p-Xylene ug/L ND 2.0 06/15/20 12:370.41
Methyl-tert-butyl ether ug/L ND 1.0 06/15/20 12:370.28
Methylene Chloride ug/L ND 5.0 06/15/20 12:373.7
Naphthalene ug/L ND 1.0 06/15/20 12:370.35
o-Xylene ug/L ND 1.0 06/15/20 12:370.22
p-Isopropyltoluene ug/L ND 1.0 06/15/20 12:370.21
Styrene ug/L ND 1.0 06/15/20 12:370.27
Tetrachloroethene ug/L ND 1.0 06/15/20 12:370.16
Toluene ug/L ND 1.0 06/15/20 12:370.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/15/20 12:370.25
trans-1,3-Dichloropropene ug/L ND 1.0 06/15/20 12:370.31
Trichloroethene ug/L ND 1.0 06/15/20 12:370.22
Trichlorofluoromethane ug/L ND 1.0 06/15/20 12:370.31
Vinyl acetate ug/L ND 2.0 06/15/20 12:371.4
Vinyl chloride ug/L ND 1.0 06/15/20 12:370.24
Xylene (Total)ug/L ND 1.0 06/15/20 12:370.63
1,2-Dichloroethane-d4 (S)%102 70-130 06/15/20 12:37
4-Bromofluorobenzene (S)%91 70-130 06/15/20 12:37
Toluene-d8 (S)%97 70-130 06/15/20 12:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2912926LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.250 94 70-130
1,1,1-Trichloroethane ug/L 44.650 89 70-130
1,1,2,2-Tetrachloroethane ug/L 48.350 97 70-130
1,1,2-Trichloroethane ug/L 44.350 89 70-130
1,1-Dichloroethane ug/L 46.250 92 70-130
1,1-Dichloroethene ug/L 49.250 98 70-130
1,1-Dichloropropene ug/L 48.050 96 70-130
1,2,3-Trichlorobenzene ug/L 53.150 106 70-130
1,2,3-Trichloropropane ug/L 45.350 91 70-130
1,2,4-Trichlorobenzene ug/L 58.150 116 70-130
1,2-Dibromo-3-chloropropane ug/L 45.150 90 70-130
1,2-Dibromoethane (EDB)ug/L 48.550 97 70-130
1,2-Dichlorobenzene ug/L 52.250 104 70-130
1,2-Dichloroethane ug/L 44.450 89 70-130
1,2-Dichloropropane ug/L 46.650 93 70-130
1,3-Dichlorobenzene ug/L 51.850 104 70-130
1,3-Dichloropropane ug/L 49.550 99 70-131
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2912926LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 49.750 99 70-130
2,2-Dichloropropane ug/L 49.450 99 69-130
2-Butanone (MEK)ug/L 88.4100 88 64-135
2-Chlorotoluene ug/L 50.850 102 70-130
2-Hexanone ug/L 93.6100 94 66-135
4-Chlorotoluene ug/L 50.050 100 70-130
4-Methyl-2-pentanone (MIBK)ug/L 90.1100 90 70-130
Acetone ug/L 90.9100 91 61-157
Benzene ug/L 46.250 92 70-130
Bromobenzene ug/L 51.650 103 70-130
Bromochloromethane ug/L 50.350 101 70-130
Bromodichloromethane ug/L 42.450 85 70-130
Bromoform ug/L 43.750 87 70-130
Bromomethane ug/L 47.750 95 38-130
Carbon tetrachloride ug/L 44.150 88 70-130
Chlorobenzene ug/L 47.450 95 70-130
Chloroethane ug/L 40.150 80 37-142
Chloroform ug/L 45.950 92 70-130
Chloromethane ug/L 39.450 79 48-130
cis-1,2-Dichloroethene ug/L 45.350 91 70-130
cis-1,3-Dichloropropene ug/L 45.950 92 70-130
Dibromochloromethane ug/L 46.650 93 70-130
Dibromomethane ug/L 43.550 87 70-130
Dichlorodifluoromethane ug/L 41.250 82 53-134
Diisopropyl ether ug/L 47.650 95 70-135
Ethylbenzene ug/L 48.450 97 70-130
Hexachloro-1,3-butadiene ug/L 53.350 107 68-132
m&p-Xylene ug/L 94.1100 94 70-130
Methyl-tert-butyl ether ug/L 47.050 94 70-130
Methylene Chloride ug/L 49.350 99 67-132
Naphthalene ug/L 52.650 105 70-130
o-Xylene ug/L 49.750 99 70-131
p-Isopropyltoluene ug/L 52.750 105 70-130
Styrene ug/L 52.350 105 70-130
Tetrachloroethene ug/L 49.450 99 69-130
Toluene ug/L 44.550 89 70-130
trans-1,2-Dichloroethene ug/L 49.650 99 70-130
trans-1,3-Dichloropropene ug/L 43.650 87 70-130
Trichloroethene ug/L 43.250 86 70-130
Trichlorofluoromethane ug/L 39.150 78 63-130
Vinyl acetate ug/L 94.9100 95 55-143
Vinyl chloride ug/L 46.050 92 70-131
Xylene (Total)ug/L 144150 96 70-130
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2912927MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92480225003
2912928
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 86 73-13482 5 3020ND17.2 16.4
1,1,1-Trichloroethane ug/L 20 91 82-14390 1 3020ND18.1 18.0
1,1,2,2-Tetrachloroethane ug/L 20 88 70-13685 4 3020ND17.6 17.0
1,1,2-Trichloroethane ug/L 20 83 70-13573 12 3020ND16.6 14.7
1,1-Dichloroethane ug/L 20 94 70-13988 7 3020ND18.8 17.6
1,1-Dichloroethene ug/L 20 106 70-15496 10 3020ND21.3 19.2
1,1-Dichloropropene ug/L 20 93 70-14993 1 3020ND18.5 18.6
1,2,3-Trichlorobenzene ug/L 20 95 70-13577 21 3020ND18.9 15.3
1,2,3-Trichloropropane ug/L 20 90 71-13783 7 3020ND17.9 16.7
1,2,4-Trichlorobenzene ug/L 20 113 73-14094 19 3020ND22.6 18.8
1,2-Dibromo-3-
chloropropane ug/L 20 89 65-13483 7 3020ND17.7 16.5
1,2-Dibromoethane (EDB)ug/L 20 94 70-13786 9 3020ND18.8 17.1
1,2-Dichlorobenzene ug/L 20 110 70-13390 20 3020ND22.0 18.1
1,2-Dichloroethane ug/L 20 83 70-13782 1 3020ND16.7 16.5
1,2-Dichloropropane ug/L 20 94 70-14087 9 3020ND18.9 17.3
1,3-Dichlorobenzene ug/L 20 106 70-13587 20 3020ND21.3 17.4
1,3-Dichloropropane ug/L 20 95 70-14390 6 3020ND19.1 18.0
1,4-Dichlorobenzene ug/L 20 103 70-13391 12 3020ND20.6 18.3
2,2-Dichloropropane ug/L 20 96 61-14896 0 3020ND19.1 19.2
2-Butanone (MEK)ug/L 40 86 60-13983 3 3040ND34.4 33.2
2-Chlorotoluene ug/L 20 111 70-14495 15 3020ND22.2 19.1
2-Hexanone ug/L 40 89 65-13882 8 3040ND35.5 32.7
4-Chlorotoluene ug/L 20 105 70-13781 25 3020ND21.0 16.3
4-Methyl-2-pentanone
(MIBK)ug/L 40 82 65-13577 6 3040ND32.6 30.8
Acetone ug/L 40 85 60-14887 2 3040ND34.0 34.7
Benzene ug/L 20 90 70-15192 2 3020ND18.0 18.3
Bromobenzene ug/L 20 107 70-13695 12 3020ND21.4 19.0
Bromochloromethane ug/L 20 99 70-14194 5 3020ND19.9 18.8
Bromodichloromethane ug/L 20 78 70-13876 3 3020ND15.6 15.2
Bromoform ug/L 20 81 63-13082 1 3020ND16.3 16.5
Bromomethane ug/L 20 126 15-152109 15 3020ND25.3 21.8
Carbon tetrachloride ug/L 20 89 70-14385 5 3020ND17.8 17.0
Chlorobenzene ug/L 20 90 70-13887 4 3020ND18.0 17.3
Chloroethane ug/L 20 91 52-16387 4 3020ND18.1 17.4
Chloroform ug/L 20 87 70-13987 0 3020ND17.5 17.4
Chloromethane ug/L 20 68 41-13976 11 3020ND13.6 15.1
cis-1,2-Dichloroethene ug/L 20 93 70-14190 3 3020ND18.5 18.1
cis-1,3-Dichloropropene ug/L 20 90 70-13784 6 3020ND17.9 16.9
Dibromochloromethane ug/L 20 92 70-13482 11 3020ND18.3 16.4
Dibromomethane ug/L 20 80 70-13886 8 3020ND15.9 17.3
Dichlorodifluoromethane ug/L 20 74 47-15570 4 3020ND14.7 14.1
Diisopropyl ether ug/L 20 92 63-14487 5 3020ND18.4 17.5
Ethylbenzene ug/L 20 96 66-15388 9 3020ND19.2 17.5
Hexachloro-1,3-butadiene ug/L 20 112 65-14990 21 3020ND22.4 18.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2912927MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92480225003
2912928
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 94 69-15286 9 3040ND37.5 34.3
Methyl-tert-butyl ether ug/L 20 91 54-15687 5 3020ND18.3 17.5
Methylene Chloride ug/L 20 93 42-15989 4 3020ND18.6 17.8
Naphthalene ug/L 20 96 61-14876 22 3020ND19.1 15.3
o-Xylene ug/L 20 89 70-14886 3 3020ND17.8 17.2
p-Isopropyltoluene ug/L 20 117 70-14692 24 3020ND23.4 18.3
Styrene ug/L 20 95 70-13587 9 3020ND19.1 17.4
Tetrachloroethene ug/L 20 93 59-14384 9 3020ND18.6 16.9
Toluene ug/L 20 84 59-14884 0 3020ND16.8 16.7
trans-1,2-Dichloroethene ug/L 20 96 70-14696 0 3020ND19.2 19.2
trans-1,3-Dichloropropene ug/L 20 76 70-13577 0 3020ND15.3 15.3
Trichloroethene ug/L 20 90 70-14787 3 3020ND17.9 17.5
Trichlorofluoromethane ug/L v1208470-14880 5 3020ND16.9 16.0
Vinyl acetate ug/L 40 92 49-15189 4 3040ND36.8 35.4
Vinyl chloride ug/L 20 98 70-15691 7 3020ND19.6 18.3
Xylene (Total)ug/L 60 92 63-15886 7 3060ND55.2 51.5
1,2-Dichloroethane-d4 (S)%104 70-13096
4-Bromofluorobenzene (S)%93 70-13094
Toluene-d8 (S)%96 70-13094
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
547374
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481193001, 92481193002, 92481193003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2913166
Associated Lab Samples:92481193001, 92481193002, 92481193003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/15/20 23:180.34
1,1,1-Trichloroethane ug/L ND 1.0 06/15/20 23:180.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/15/20 23:180.22
1,1,2-Trichloroethane ug/L ND 1.0 06/15/20 23:180.24
1,1-Dichloroethane ug/L ND 1.0 06/15/20 23:180.27
1,1-Dichloroethene ug/L ND 1.0 06/15/20 23:180.24
1,1-Dichloropropene ug/L ND 1.0 06/15/20 23:180.21
1,2,3-Trichlorobenzene ug/L ND 1.0 06/15/20 23:180.34
1,2,3-Trichloropropane ug/L ND 1.0 06/15/20 23:180.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/15/20 23:180.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 06/15/20 23:180.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/15/20 23:180.26
1,2-Dichlorobenzene ug/L ND 1.0 06/15/20 23:180.29
1,2-Dichloroethane ug/L ND 1.0 06/15/20 23:180.34
1,2-Dichloropropane ug/L ND 1.0 06/15/20 23:180.19
1,3-Dichlorobenzene ug/L ND 1.0 06/15/20 23:180.22
1,3-Dichloropropane ug/L ND 1.0 06/15/20 23:180.16
1,4-Dichlorobenzene ug/L ND 1.0 06/15/20 23:180.26
2,2-Dichloropropane ug/L ND 1.0 06/15/20 23:180.27
2-Butanone (MEK)ug/L ND 5.0 06/15/20 23:183.3
2-Chlorotoluene ug/L ND 1.0 06/15/20 23:180.20
2-Hexanone ug/L ND 5.0 06/15/20 23:180.57
4-Chlorotoluene ug/L ND 1.0 06/15/20 23:180.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/15/20 23:184.5
Acetone ug/L ND 25.0 06/15/20 23:186.2
Benzene ug/L ND 1.0 06/15/20 23:180.15
Bromobenzene ug/L ND 1.0 06/15/20 23:180.22
Bromochloromethane ug/L ND 1.0 06/15/20 23:180.34
Bromodichloromethane ug/L ND 1.0 06/15/20 23:180.26
Bromoform ug/L ND 1.0 v106/15/20 23:180.62
Bromomethane ug/L 2.7 2.0 v106/15/20 23:180.62
Carbon tetrachloride ug/L ND 1.0 06/15/20 23:180.22
Chlorobenzene ug/L ND 1.0 06/15/20 23:180.23
Chloroethane ug/L ND 1.0 06/15/20 23:180.49
Chloroform ug/L ND 5.0 06/15/20 23:182.3
Chloromethane ug/L ND 1.0 06/15/20 23:180.39
cis-1,2-Dichloroethene ug/L ND 1.0 06/15/20 23:180.29
cis-1,3-Dichloropropene ug/L ND 1.0 06/15/20 23:180.30
Dibromochloromethane ug/L ND 1.0 06/15/20 23:180.41
Dibromomethane ug/L ND 1.0 06/15/20 23:180.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2913166
Associated Lab Samples:92481193001, 92481193002, 92481193003
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 06/15/20 23:180.23
Diisopropyl ether ug/L ND 1.0 06/15/20 23:180.22
Ethylbenzene ug/L ND 1.0 06/15/20 23:180.26
Hexachloro-1,3-butadiene ug/L 0.89J 1.0 06/15/20 23:180.44
m&p-Xylene ug/L ND 2.0 06/15/20 23:180.41
Methyl-tert-butyl ether ug/L ND 1.0 06/15/20 23:180.28
Methylene Chloride ug/L ND 5.0 06/15/20 23:183.7
Naphthalene ug/L ND 1.0 06/15/20 23:180.35
o-Xylene ug/L ND 1.0 06/15/20 23:180.22
p-Isopropyltoluene ug/L ND 1.0 06/15/20 23:180.21
Styrene ug/L ND 1.0 06/15/20 23:180.27
Tetrachloroethene ug/L ND 1.0 06/15/20 23:180.16
Toluene ug/L ND 1.0 06/15/20 23:180.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/15/20 23:180.25
trans-1,3-Dichloropropene ug/L ND 1.0 06/15/20 23:180.31
Trichloroethene ug/L ND 1.0 06/15/20 23:180.22
Trichlorofluoromethane ug/L ND 1.0 06/15/20 23:180.31
Vinyl acetate ug/L ND 2.0 06/15/20 23:181.4
Vinyl chloride ug/L ND 1.0 06/15/20 23:180.24
Xylene (Total)ug/L ND 1.0 06/15/20 23:180.63
1,2-Dichloroethane-d4 (S)%103 70-130 06/15/20 23:18
4-Bromofluorobenzene (S)%91 70-130 06/15/20 23:18
Toluene-d8 (S)%100 70-130 06/15/20 23:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2913167LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 44.950 90 70-130
1,1,1-Trichloroethane ug/L 42.950 86 70-130
1,1,2,2-Tetrachloroethane ug/L 45.250 90 70-130
1,1,2-Trichloroethane ug/L 42.050 84 70-130
1,1-Dichloroethane ug/L 44.350 89 70-130
1,1-Dichloroethene ug/L 48.850 98 70-130
1,1-Dichloropropene ug/L 43.650 87 70-130
1,2,3-Trichlorobenzene ug/L 45.050 90 70-130
1,2,3-Trichloropropane ug/L 43.250 86 70-130
1,2,4-Trichlorobenzene ug/L 47.550 95 70-130
1,2-Dibromo-3-chloropropane ug/L 45.650 91 70-130
1,2-Dibromoethane (EDB)ug/L 50.050 100 70-130
1,2-Dichlorobenzene ug/L 49.650 99 70-130
1,2-Dichloroethane ug/L 41.650 83 70-130
1,2-Dichloropropane ug/L 42.950 86 70-130
1,3-Dichlorobenzene ug/L 47.550 95 70-130
1,3-Dichloropropane ug/L 49.050 98 70-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2913167LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 49.650 99 70-130
2,2-Dichloropropane ug/L 43.850 88 69-130
2-Butanone (MEK)ug/L 87.8100 88 64-135
2-Chlorotoluene ug/L 48.550 97 70-130
2-Hexanone ug/L 96.9100 97 66-135
4-Chlorotoluene ug/L 42.350 85 70-130
4-Methyl-2-pentanone (MIBK)ug/L 88.9100 89 70-130
Acetone ug/L 93.9100 94 61-157
Benzene ug/L 43.750 87 70-130
Bromobenzene ug/L 49.650 99 70-130
Bromochloromethane ug/L 46.950 94 70-130
Bromodichloromethane ug/L 38.050 76 70-130
Bromoform ug/L 33.5 L2,v1506770-130
Bromomethane ug/L 35.3 v1507138-130
Carbon tetrachloride ug/L 42.050 84 70-130
Chlorobenzene ug/L 46.750 93 70-130
Chloroethane ug/L 37.550 75 37-142
Chloroform ug/L 42.750 85 70-130
Chloromethane ug/L 35.150 70 48-130
cis-1,2-Dichloroethene ug/L 43.350 87 70-130
cis-1,3-Dichloropropene ug/L 43.150 86 70-130
Dibromochloromethane ug/L 39.050 78 70-130
Dibromomethane ug/L 42.950 86 70-130
Dichlorodifluoromethane ug/L 33.750 67 53-134
Diisopropyl ether ug/L 46.050 92 70-135
Ethylbenzene ug/L 45.050 90 70-130
Hexachloro-1,3-butadiene ug/L 46.350 93 68-132
m&p-Xylene ug/L 88.9100 89 70-130
Methyl-tert-butyl ether ug/L 44.850 90 70-130
Methylene Chloride ug/L 47.450 95 67-132
Naphthalene ug/L 47.250 94 70-130
o-Xylene ug/L 45.250 90 70-131
p-Isopropyltoluene ug/L 49.450 99 70-130
Styrene ug/L 45.250 90 70-130
Tetrachloroethene ug/L 45.450 91 69-130
Toluene ug/L 42.650 85 70-130
trans-1,2-Dichloroethene ug/L 46.650 93 70-130
trans-1,3-Dichloropropene ug/L 39.150 78 70-130
Trichloroethene ug/L 42.550 85 70-130
Trichlorofluoromethane ug/L 35.350 71 63-130
Vinyl acetate ug/L 93.0100 93 55-143
Vinyl chloride ug/L 41.850 84 70-131
Xylene (Total)ug/L 134150 89 70-130
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%93 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2913188MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481156002
2913189
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 98 73-134106 8 3020ND19.6 21.2
1,1,1-Trichloroethane ug/L 20 104 82-143104 0 3020ND20.9 20.8
1,1,2,2-Tetrachloroethane ug/L 20 100 70-136106 6 3020ND19.9 21.2
1,1,2-Trichloroethane ug/L 20 92 70-13597 5 3020ND18.4 19.4
1,1-Dichloroethane ug/L 20 108 70-139112 4 3020ND21.6 22.4
1,1-Dichloroethene ug/L 20 123 70-154122 1 3020ND24.6 24.3
1,1-Dichloropropene ug/L 20 114 70-149109 4 3020ND22.7 21.8
1,2,3-Trichlorobenzene ug/L 20 98 70-135107 8 3020ND19.6 21.4
1,2,3-Trichloropropane ug/L 20 91 71-13799 9 3020ND18.1 19.8
1,2,4-Trichlorobenzene ug/L 20 113 73-140120 6 3020ND22.6 24.0
1,2-Dibromo-3-
chloropropane ug/L 20 90 65-13486 4 3020ND17.9 17.2
1,2-Dibromoethane (EDB)ug/L 20 101 70-137114 12 3020ND20.2 22.8
1,2-Dichlorobenzene ug/L 20 105 70-133111 5 3020ND21.1 22.1
1,2-Dichloroethane ug/L 20 98 70-13798 1 3020ND19.7 19.5
1,2-Dichloropropane ug/L 20 106 70-140106 0 3020ND21.1 21.2
1,3-Dichlorobenzene ug/L 20 103 70-135109 5 3020ND20.7 21.8
1,3-Dichloropropane ug/L 20 100 70-143108 8 3020ND20.0 21.7
1,4-Dichlorobenzene ug/L 20 101 70-133112 9 3020ND20.3 22.3
2,2-Dichloropropane ug/L 20 111 61-148110 1 3020ND22.2 21.9
2-Butanone (MEK)ug/L 40 96 60-139100 4 3040ND38.3 40.0
2-Chlorotoluene ug/L 20 106 70-144111 5 3020ND21.1 22.2
2-Hexanone ug/L 40 97 65-138101 3 3040ND38.9 40.3
4-Chlorotoluene ug/L 20 87 70-137109 23 3020ND17.4 21.8
4-Methyl-2-pentanone
(MIBK)ug/L 40 93 65-13594 0 3040ND37.3 37.5
Acetone ug/L 40 104 60-148102 2 3040ND41.5 40.6
Benzene ug/L 20 107 70-151112 5 3020ND21.3 22.5
Bromobenzene ug/L 20 108 70-136108 1 3020ND21.7 21.5
Bromochloromethane ug/L 20 113 70-141114 0 3020ND22.6 22.7
Bromodichloromethane ug/L 20 91 70-13895 4 3020ND18.3 19.0
Bromoform ug/L 20 90 63-13094 4 3020ND18.0 18.8
Bromomethane ug/L 20 115 15-152102 12 3020ND23.0 20.3
Carbon tetrachloride ug/L 20 100 70-143100 0 3020ND20.0 20.0
Chlorobenzene ug/L 20 100 70-138108 8 3020ND20.1 21.7
Chloroethane ug/L 20 112 52-163104 7 3020ND22.4 20.8
Chloroform ug/L 20 105 70-139102 3 3020ND21.0 20.4
Chloromethane ug/L 20 90 41-13986 5 3020ND17.9 17.1
cis-1,2-Dichloroethene ug/L 20 108 70-141108 0 3020ND21.6 21.7
cis-1,3-Dichloropropene ug/L 20 101 70-13799 2 3020ND20.1 19.8
Dibromochloromethane ug/L 20 94 70-134102 8 3020ND18.9 20.4
Dibromomethane ug/L 20 98 70-138100 2 3020ND19.6 19.9
Dichlorodifluoromethane ug/L 20 87 47-15585 2 3020ND17.5 17.1
Diisopropyl ether ug/L 20 106 63-144106 0 3020ND21.2 21.3
Ethylbenzene ug/L 20 100 66-153108 7 3020ND20.1 21.6
Hexachloro-1,3-butadiene ug/L 20 113 65-149124 9 3020ND22.6 24.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2913188MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92481156002
2913189
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 99 69-152105 6 3040ND39.6 42.1
Methyl-tert-butyl ether ug/L 20 102 54-156103 1 3020ND20.4 20.6
Methylene Chloride ug/L 20 107 42-159108 1 3020ND21.4 21.6
Naphthalene ug/L 20 94 61-148102 8 3020ND18.9 20.4
o-Xylene ug/L 20 101 70-148107 6 3020ND20.2 21.4
p-Isopropyltoluene ug/L 20 111 70-146114 3 3020ND22.2 22.9
Styrene ug/L 20 102 70-135109 7 3020ND20.5 21.9
Tetrachloroethene ug/L 20 97 59-14399 2 3020ND19.3 19.7
Toluene ug/L 20 97 59-14899 2 3020ND19.4 19.8
trans-1,2-Dichloroethene ug/L 20 109 70-146113 3 3020ND21.7 22.5
trans-1,3-Dichloropropene ug/L 20 84 70-13595 11 3020ND16.9 18.9
Trichloroethene ug/L 20 100 70-147107 7 3020ND20.0 21.4
Trichlorofluoromethane ug/L v1209670-14897 0 3020ND19.3 19.3
Vinyl acetate ug/L 40 101 49-151100 0 3040ND40.2 40.0
Vinyl chloride ug/L 20 109 70-156110 1 3020ND21.8 22.0
Xylene (Total)ug/L 60 100 63-158106 6 3060ND59.7 63.5
1,2-Dichloroethane-d4 (S)%100 70-13092
4-Bromofluorobenzene (S)%99 70-130102
Toluene-d8 (S)%97 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
546578
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92481193001, 92481193002, 92481193003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2909220
Associated Lab Samples:92481193001, 92481193002, 92481193003
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 06/12/20 12:491.6
1,2-Dichlorobenzene ug/L ND 10.0 06/12/20 12:491.4
1,3-Dichlorobenzene ug/L ND 10.0 06/12/20 12:491.4
1,4-Dichlorobenzene ug/L ND 10.0 06/12/20 12:491.5
1-Methylnaphthalene ug/L ND 10.0 06/12/20 12:491.4
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/12/20 12:491.3
2,4,5-Trichlorophenol ug/L ND 10.0 06/12/20 12:491.5
2,4,6-Trichlorophenol ug/L ND 10.0 06/12/20 12:491.4
2,4-Dichlorophenol ug/L ND 10.0 06/12/20 12:491.5
2,4-Dimethylphenol ug/L ND 10.0 06/12/20 12:491.5
2,4-Dinitrophenol ug/L ND 50.0 06/12/20 12:497.3
2,4-Dinitrotoluene ug/L ND 10.0 06/12/20 12:491.7
2,6-Dinitrotoluene ug/L ND 10.0 06/12/20 12:491.7
2-Chloronaphthalene ug/L ND 10.0 06/12/20 12:491.4
2-Chlorophenol ug/L ND 10.0 06/12/20 12:491.4
2-Methylnaphthalene ug/L ND 10.0 06/12/20 12:491.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/12/20 12:491.2
2-Nitroaniline ug/L ND 20.0 06/12/20 12:493.0
2-Nitrophenol ug/L ND 10.0 06/12/20 12:491.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/12/20 12:491.2
3,3'-Dichlorobenzidine ug/L ND 20.0 06/12/20 12:492.7
3-Nitroaniline ug/L ND 20.0 06/12/20 12:492.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 06/12/20 12:494.5
4-Bromophenylphenyl ether ug/L ND 10.0 06/12/20 12:491.2
4-Chloro-3-methylphenol ug/L ND 10.0 06/12/20 12:492.8
4-Chloroaniline ug/L ND 20.0 06/12/20 12:492.8
4-Chlorophenylphenyl ether ug/L ND 10.0 06/12/20 12:491.5
4-Nitroaniline ug/L ND 20.0 06/12/20 12:493.1
4-Nitrophenol ug/L ND 50.0 06/12/20 12:499.4
Acenaphthene ug/L ND 10.0 06/12/20 12:491.4
Acenaphthylene ug/L ND 10.0 06/12/20 12:491.5
Aniline ug/L ND 10.0 06/12/20 12:491.6
Anthracene ug/L ND 10.0 06/12/20 12:491.6
Benzo(a)anthracene ug/L ND 10.0 06/12/20 12:491.5
Benzo(a)pyrene ug/L ND 10.0 06/12/20 12:491.8
Benzo(b)fluoranthene ug/L ND 10.0 06/12/20 12:491.7
Benzo(g,h,i)perylene ug/L ND 10.0 06/12/20 12:491.6
Benzo(k)fluoranthene ug/L ND 10.0 06/12/20 12:491.5
Benzoic Acid ug/L ND 50.0 06/12/20 12:4919.5
Benzyl alcohol ug/L ND 20.0 06/12/20 12:492.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2909220
Associated Lab Samples:92481193001, 92481193002, 92481193003
Matrix:Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/12/20 12:491.3
bis(2-Chloroethyl) ether ug/L ND 10.0 06/12/20 12:491.7
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/12/20 12:492.0
Butylbenzylphthalate ug/L ND 10.0 06/12/20 12:491.9
Chrysene ug/L ND 10.0 06/12/20 12:491.4
Di-n-butylphthalate ug/L ND 10.0 06/12/20 12:491.6
Di-n-octylphthalate ug/L ND 10.0 06/12/20 12:492.2
Dibenz(a,h)anthracene ug/L ND 10.0 06/12/20 12:491.6
Dibenzofuran ug/L ND 10.0 06/12/20 12:491.3
Diethylphthalate ug/L ND 10.0 06/12/20 12:491.6
Dimethylphthalate ug/L ND 10.0 06/12/20 12:491.4
Fluoranthene ug/L ND 10.0 06/12/20 12:491.6
Fluorene ug/L ND 10.0 06/12/20 12:491.4
Hexachloro-1,3-butadiene ug/L ND 10.0 06/12/20 12:491.6
Hexachlorobenzene ug/L ND 10.0 06/12/20 12:491.3
Hexachlorocyclopentadiene ug/L ND 10.0 06/12/20 12:492.4
Hexachloroethane ug/L ND 10.0 06/12/20 12:491.3
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/12/20 12:491.7
Isophorone ug/L ND 10.0 06/12/20 12:491.3
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/12/20 12:491.3
N-Nitrosodimethylamine ug/L ND 10.0 06/12/20 12:491.8
N-Nitrosodiphenylamine ug/L ND 10.0 06/12/20 12:491.4
Naphthalene ug/L ND 10.0 06/12/20 12:491.6
Nitrobenzene ug/L ND 10.0 06/12/20 12:491.5
Pentachlorophenol ug/L ND 20.0 06/12/20 12:492.8
Phenanthrene ug/L ND 10.0 06/12/20 12:491.4
Phenol ug/L ND 10.0 06/12/20 12:491.5
Pyrene ug/L ND 10.0 06/12/20 12:491.5
2,4,6-Tribromophenol (S)%78 10-137 06/12/20 12:49
2-Fluorobiphenyl (S)%65 13-130 06/12/20 12:49
2-Fluorophenol (S)%65 10-130 06/12/20 12:49
Nitrobenzene-d5 (S)%77 13-130 06/12/20 12:49
Phenol-d6 (S)%49 10-130 06/12/20 12:49
Terphenyl-d14 (S)%101 25-130 06/12/20 12:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2909221LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 33.750 67 30-130
1,2-Dichlorobenzene ug/L 33.050 66 30-130
1,3-Dichlorobenzene ug/L 30.550 61 20-130
1,4-Dichlorobenzene ug/L 32.950 66 30-130
1-Methylnaphthalene ug/L 41.050 82 30-130
2,2'-Oxybis(1-chloropropane)ug/L 44.650 89 20-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2909221LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 49.450 99 40-130
2,4,6-Trichlorophenol ug/L 47.950 96 40-130
2,4-Dichlorophenol ug/L 50.050 100 31-130
2,4-Dimethylphenol ug/L 52.750 105 30-130
2,4-Dinitrophenol ug/L 277250 111 30-130
2,4-Dinitrotoluene ug/L 51.950 104 49-130
2,6-Dinitrotoluene ug/L 53.250 106 50-130
2-Chloronaphthalene ug/L 40.050 80 30-130
2-Chlorophenol ug/L 47.250 94 30-130
2-Methylnaphthalene ug/L 41.650 83 30-130
2-Methylphenol(o-Cresol)ug/L 46.650 93 30-130
2-Nitroaniline ug/L 101100 101 40-130
2-Nitrophenol ug/L 48.750 97 20-130
3&4-Methylphenol(m&p Cresol)ug/L 44.050 88 20-130
3,3'-Dichlorobenzidine ug/L 109100 109 10-150
3-Nitroaniline ug/L 109100 109 40-130
4,6-Dinitro-2-methylphenol ug/L 102100 102 40-130
4-Bromophenylphenyl ether ug/L 45.150 90 30-130
4-Chloro-3-methylphenol ug/L 107100 107 30-130
4-Chloroaniline ug/L 102100 102 20-130
4-Chlorophenylphenyl ether ug/L 45.350 91 20-130
4-Nitroaniline ug/L 110100 110 40-130
4-Nitrophenol ug/L 193250 77 10-130
Acenaphthene ug/L 44.250 88 30-130
Acenaphthylene ug/L 45.850 92 30-130
Aniline ug/L 46.250 92 20-130
Anthracene ug/L 47.050 94 50-130
Benzo(a)anthracene ug/L 50.350 101 50-130
Benzo(a)pyrene ug/L 50.750 101 50-130
Benzo(b)fluoranthene ug/L 52.950 106 50-130
Benzo(g,h,i)perylene ug/L 51.150 102 50-130
Benzo(k)fluoranthene ug/L 49.250 98 50-130
Benzoic Acid ug/L 185250 74 10-130
Benzyl alcohol ug/L 96.7100 97 20-130
bis(2-Chloroethoxy)methane ug/L 47.350 95 30-130
bis(2-Chloroethyl) ether ug/L 46.150 92 30-130
bis(2-Ethylhexyl)phthalate ug/L 53.950 108 50-130
Butylbenzylphthalate ug/L 54.750 109 50-150
Chrysene ug/L 49.050 98 50-130
Di-n-butylphthalate ug/L 51.550 103 50-130
Di-n-octylphthalate ug/L 58.350 117 50-130
Dibenz(a,h)anthracene ug/L 51.450 103 40-130
Dibenzofuran ug/L 44.550 89 40-130
Diethylphthalate ug/L 50.750 101 40-130
Dimethylphthalate ug/L 49.850 100 40-130
Fluoranthene ug/L 50.150 100 30-130
Fluorene ug/L 48.150 96 20-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2909221LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 27.550 55 10-130
Hexachlorobenzene ug/L 44.650 89 30-130
Hexachlorocyclopentadiene ug/L 28.150 56 10-150
Hexachloroethane ug/L 27.450 55 10-130
Indeno(1,2,3-cd)pyrene ug/L 51.250 102 40-130
Isophorone ug/L 50.350 101 30-130
N-Nitroso-di-n-propylamine ug/L 49.750 99 30-130
N-Nitrosodimethylamine ug/L 40.850 82 10-130
N-Nitrosodiphenylamine ug/L 45.750 91 30-130
Naphthalene ug/L 40.350 81 20-130
Nitrobenzene ug/L 46.250 92 20-130
Pentachlorophenol ug/L 103100 103 10-140
Phenanthrene ug/L 46.050 92 50-130
Phenol ug/L 33.350 67 10-130
Pyrene ug/L 46.950 94 50-130
2,4,6-Tribromophenol (S)%95 10-137
2-Fluorobiphenyl (S)%79 13-130
2-Fluorophenol (S)%77 10-130
Nitrobenzene-d5 (S)%91 13-130
Phenol-d6 (S)%63 10-130
Terphenyl-d14 (S)%108 25-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2909222MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92471460028
2909223
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 44 30-13040 10 3050ND22.0 20.0
1,2-Dichlorobenzene ug/L 50 41 30-13041 1 3050ND20.5 20.7
1,3-Dichlorobenzene ug/L 50 37 20-13039 6 3050ND18.3 19.3
1,4-Dichlorobenzene ug/L 50 40 30-13041 5 3050ND19.8 20.7
1-Methylnaphthalene ug/L 50 61 30-13050 21 3050ND30.7 25.0
2,2'-Oxybis(1-
chloropropane)
ug/L 50 67 20-13063 6 3050ND33.6 31.7
2,4,5-Trichlorophenol ug/L 50 82 40-13071 14 3050ND40.8 35.6
2,4,6-Trichlorophenol ug/L 50 78 40-13069 12 3050ND39.0 34.7
2,4-Dichlorophenol ug/L 50 77 31-13067 14 3050ND38.7 33.5
2,4-Dimethylphenol ug/L 50 82 30-13071 14 3050ND40.8 35.5
2,4-Dinitrophenol ug/L 250 95 30-13085 11 30250ND237212
2,4-Dinitrotoluene ug/L 50 94 49-13082 14 3050ND46.8 40.8
2,6-Dinitrotoluene ug/L 50 94 50-13082 13 3050ND47.1 41.2
2-Chloronaphthalene ug/L 50 60 30-13050 18 3050ND30.1 25.2
2-Chlorophenol ug/L 50 64 30-13063 2 3050ND32.2 31.4
2-Methylnaphthalene ug/L 50 60 30-13051 18 3050ND30.2 25.3
2-Methylphenol(o-Cresol)ug/L 50 69 30-13061 13 3050ND34.6 30.3
2-Nitroaniline ug/L 100 90 40-13078 14 30100ND89.9 78.5
REPORT OF LABORATORY ANALYSIS
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Page 35 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2909222MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92471460028
2909223
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitrophenol ug/L 50 71 20-13067 6 3050ND35.6 33.5
3&4-Methylphenol(m&p
Cresol)ug/L M15014620-130129 13 3050ND73.0 64.4
3,3'-Dichlorobenzidine ug/L 100 99 10-15086 14 30100ND99.0 86.0
3-Nitroaniline ug/L 100 97 40-13084 13 30100ND96.5 84.3
4,6-Dinitro-2-methylphenol ug/L 100 88 40-13080 9 30100ND88.3 80.4
4-Bromophenylphenyl ether ug/L 50 77 30-13068 12 3050ND38.5 34.0
4-Chloro-3-methylphenol ug/L 100 87 30-13072 18 30100ND86.9 72.3
4-Chloroaniline ug/L 100 82 20-13070 15 30100ND81.6 70.2
4-Chlorophenylphenyl ether ug/L 50 76 20-13065 16 3050ND37.9 32.3
4-Nitroaniline ug/L 100 102 40-13089 14 30100ND10288.5
4-Nitrophenol ug/L 250 61 10-13051 18 30250ND153128
Acenaphthene ug/L 50 72 30-13060 19 3050ND36.2 30.0
Acenaphthylene ug/L 50 75 30-13063 17 3050ND37.5 31.7
Aniline ug/L 50 63 20-13059 7 3050ND31.7 29.5
Anthracene ug/L 50 83 50-13075 10 3050ND41.5 37.7
Benzo(a)anthracene ug/L 50 94 50-13082 13 3050ND46.8 41.1
Benzo(a)pyrene ug/L 50 92 50-13080 14 3050ND46.2 40.1
Benzo(b)fluoranthene ug/L 50 94 50-13085 11 3050ND47.2 42.3
Benzo(g,h,i)perylene ug/L 50 93 50-13080 15 3050ND46.4 39.9
Benzo(k)fluoranthene ug/L 50 90 50-13079 13 3050ND45.1 39.4
Benzoic Acid ug/L 250 52 10-13043 18 30250ND130109
Benzyl alcohol ug/L 100 73 20-13066 10 30100ND73.0 65.9
bis(2-
Chloroethoxy)methane
ug/L 50 75 30-13067 11 3050ND37.7 33.7
bis(2-Chloroethyl) ether ug/L 50 67 30-13067 1 3050ND33.7 33.4
bis(2-Ethylhexyl)phthalate ug/L 50 102 50-13089 14 3050ND50.8 44.3
Butylbenzylphthalate ug/L 50 101 50-15088 14 3050ND50.7 44.1
Chrysene ug/L 50 91 50-13080 14 3050ND45.6 39.8
Di-n-butylphthalate ug/L 50 96 50-13084 13 3050ND48.0 42.2
Di-n-octylphthalate ug/L 50 110 50-13094 16 3050ND54.9 46.9
Dibenz(a,h)anthracene ug/L 50 93 40-13081 14 3050ND46.6 40.4
Dibenzofuran ug/L 50 73 40-13063 14 3050ND36.3 31.6
Diethylphthalate ug/L 50 92 40-13081 12 3050ND45.8 40.5
Dimethylphthalate ug/L 50 89 40-13077 14 3050ND44.4 38.6
Fluoranthene ug/L 50 93 30-13083 11 3050ND46.5 41.5
Fluorene ug/L 50 81 20-13070 14 3050ND40.3 35.1
Hexachloro-1,3-butadiene ug/L 50 36 10-13034 6 3050ND17.9 16.9
Hexachlorobenzene ug/L 50 78 30-13070 12 3050ND39.2 35.0
Hexachlorocyclopentadiene ug/L 50 39 10-15031 23 3050ND19.6 15.5
Hexachloroethane ug/L 50 33 10-13036 8 3050ND16.5 17.9
Indeno(1,2,3-cd)pyrene ug/L 50 93 40-13080 14 3050ND46.4 40.1
Isophorone ug/L 50 84 30-13073 14 3050ND41.9 36.3
N-Nitroso-di-n-propylamine ug/L 50 83 30-13072 14 3050ND41.5 36.1
N-Nitrosodimethylamine ug/L 50 50 10-13054 8 3050ND24.9 27.0
N-Nitrosodiphenylamine ug/L 50 78 30-13070 11 3050ND39.2 35.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/17/2020 05:51 PM
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[phone]
Page 36 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2909222MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92471460028
2909223
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Naphthalene ug/L 50 57 20-13051 12 3050ND28.5 25.3
Nitrobenzene ug/L 50 70 20-13066 5 3050ND34.8 33.1
Pentachlorophenol ug/L 100 91 10-14081 12 30100ND91.3 80.8
Phenanthrene ug/L 50 81 50-13073 10 3050ND40.5 36.6
Phenol ug/L 50 45 10-13041 10 3050ND22.7 20.6
Pyrene ug/L 50 86 50-13075 13 3050ND42.9 37.6
2,4,6-Tribromophenol (S)%89 10-13780
2-Fluorobiphenyl (S)%68 13-13058
2-Fluorophenol (S)%49 10-13051
Nitrobenzene-d5 (S)%74 13-13071
Phenol-d6 (S)%46 10-13042
Terphenyl-d14 (S)%108 25-13093
REPORT OF LABORATORY ANALYSIS
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Page 37 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92481193
FDP-058
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1491175
7199
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92481193001, 92481193002, 92481193003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3539076-1
Associated Lab Samples:92481193001, 92481193002, 92481193003
Matrix:Water
AnalyzedMDL
Chromium, Hexavalent ug/L ND 0.100 06/15/20 14:010.0400
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3539076-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent ug/L 0.4910.500 98.2 90.0-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3539076-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1227922-02
R3539076-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent ug/L 1.00 101 90.0-110102 0.653 201.00ND 1.01 1.02
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3539076-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1228652-05
Chromium, Hexavalent ug/L 5.12 E,MH1.00 126 90.0-1103.86
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1227236-01
R3539076-3SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L 0.0899J J0.607 200.0905
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1228652-06
R3539076-8SAMPLE DUPLICATE:
Chromium, Hexavalent ug/L 9.52 0.141 209.51
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92481193
FDP-058
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biased
high.MH
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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Page 39 of 43
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92481193
FDP-058
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92481193001 1491232 1491232SW-1 3015 EPA 6020B
92481193002 1491232 1491232SW-4 3015 EPA 6020B
92481193003 1491232 1491232SW-DUP 3015 EPA 6020B
92481193001 1491239 1491239SW-1 7470A EPA 7470A
92481193002 1491239 1491239SW-4 7470A EPA 7470A
92481193003 1491239 1491239SW-DUP 7470A EPA 7470A
92481193001 546578 546918SW-1 EPA 3510C EPA 8270E
92481193002 546578 546918SW-4 EPA 3510C EPA 8270E
92481193003 546578 546918SW-DUP EPA 3510C EPA 8270E
92481193001 547374SW-1 EPA 8260D
92481193002 547374SW-4 EPA 8260D
92481193003 547374SW-DUP EPA 8260D
92481193004 547329Trip Blank EPA 8260D
92481193001 1491175 1491175SW-1 7199 EPA 7199
92481193002 1491175 1491175SW-4 7199 EPA 7199
92481193003 1491175 1491175SW-DUP 7199 EPA 7199
92481193001 1491232 1491232SW-1 SM2340B SM2340-97
92481193002 1491232 1491232SW-4 SM2340B SM2340-97
92481193003 1491232 1491232SW-DUP SM2340B SM2340-97
REPORT OF LABORATORY ANALYSIS
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Page 40 of 43
Page 41 of 43
Page 42 of 43
Page 43 of 43
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
June 22, 2020
Ralph McGee
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
Project Location: Salisbury, NC
Client Job Number:
Project Number: FDP-058
Laboratory Work Order Number: 20F0582
Enclosed are results of analyses for samples received by the laboratory on June 11, 2020. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
6/22/2020Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
ATTN: Ralph McGee
FDP-058
20F0582
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Salisbury, NC
SS-1 20F0582-01 Sub Slab EPA TO-15
SS-2 20F0582-02 Sub Slab EPA TO-15
SS-3 20F0582-03 Sub Slab EPA TO-15
SS-4 20F0582-04 Sub Slab EPA TO-15
SS-5 20F0582-05 Sub Slab EPA TO-15
SS-6 20F0582-06 Sub Slab EPA TO-15
SS-7 20F0582-07 Sub Slab EPA TO-15
SS-8 20F0582-08 Sub Slab EPA TO-15
SS-9 20F0582-09 Sub Slab EPA TO-15
SS-10 20F0582-10 Sub Slab EPA TO-15
SS-11 20F0582-11 Sub Slab EPA TO-15
SS-Dup 20F0582-12 Sub Slab EPA TO-15
Page 2 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Reported result is estimated. Value reported over verified calibration range.
Analyte & Samples(s) Qualified:
Ethanol
B260278-DUP1
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be
biased on the low side.
Analyte & Samples(s) Qualified:
Propene
20F0582-01[SS-1], 20F0582-02[SS-2], 20F0582-03[SS-3], 20F0582-04[SS-4], 20F0582-05[SS-5], 20F0582-06[SS-6], 20F0582-07[SS-7], 20F0582-08[SS-8],
20F0582-09[SS-9], 20F0582-10[SS-10], 20F0582-11[SS-11], 20F0582-12[SS-Dup], B260278-BLK1, B260278-BS1, B260278-DUP1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
Acetone, Ethanol
20F0582-01[SS-1], 20F0582-02[SS-2], 20F0582-03[SS-3], 20F0582-04[SS-4], 20F0582-05[SS-5], 20F0582-06[SS-6], 20F0582-07[SS-7], 20F0582-08[SS-8],
20F0582-09[SS-9], 20F0582-10[SS-10], 20F0582-11[SS-11], 20F0582-12[SS-Dup], B260278-BS1, B260278-DUP1, S049482-CCV1, 20F0582-01RE1[SS-1],
20F0582-02RE1[SS-2], 20F0582-03RE1[SS-3], 20F0582-04RE1[SS-4], 20F0582-05RE1[SS-5], 20F0582-06RE1[SS-6], 20F0582-07RE1[SS-7], 20F0582-08RE1[SS-8],
20F0582-09RE1[SS-9], 20F0582-10RE1[SS-10], 20F0582-11RE1[SS-11], 20F0582-12RE1[SS-Dup], B260459-BS1, B260459-DUP1, S049551-CCV1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 3 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-1
Sample ID: 20F0582-01
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -24.7
Final Vacuum(in Hg): -3.3
Receipt Vacuum(in Hg): -6
Sampled: 6/10/2020 09:41
Canister ID: 2240
Flow Controller ID: 4225
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 49 8.0 6/17/20 15:09 BRFV-06 120 4192.8 6.6
Benzene 0.33 0.20 6/17/20 15:09 BRF1.0 40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 15:09 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 15:09 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 15:09 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 15:09 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 15:09 BRFND40.440.15 0.32
2-Butanone (MEK)2.5 8.0 6/17/20 15:09 BRFJ7.3 4240.37 1.1
Carbon Disulfide 0.86 2.0 6/17/20 15:09 BRFJ2.7 46.20.14 0.43
Carbon Tetrachloride 0.13 0.20 6/17/20 15:09 BRFJ0.83 41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 15:09 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 15:09 BRFND40.530.20 0.52
Chloroform 0.81 0.20 6/17/20 15:09 BRF3.9 40.980.074 0.36
Chloromethane ND 0.40 6/17/20 15:09 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 15:09 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 15:09 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 15:09 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 15:09 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 15:09 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 15:09 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.62 0.20 6/17/20 15:09 BRF3.1 40.990.087 0.43
1,1-Dichloroethane 4.2 0.20 6/17/20 15:09 BRF17 40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 15:09 BRFND40.810.076 0.31
1,1-Dichloroethylene 53 0.20 6/17/20 15:09 BRF210 40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/17/20 15:09 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 15:09 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 15:09 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 15:09 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 15:09 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 15:09 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 15:09 BRFND47.21.3 4.6
Ethanol 560 40 6/19/20 16:19 BRFV-06 1000 20751834
Ethyl Acetate 3.3 0.20 6/17/20 15:09 BRF12 40.720.15 0.54
Ethylbenzene 0.12 0.20 6/17/20 15:09 BRFJ0.50 40.870.12 0.50
4-Ethyltoluene ND 0.20 6/17/20 15:09 BRFND40.980.12 0.60
Heptane 0.20 0.20 6/17/20 15:09 BRF0.82 40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 15:09 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 15:09 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/17/20 15:09 BRFND40.820.12 0.48
Isopropanol 80 8.0 6/17/20 15:09 BRF200 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 15:09 BRFND40.720.10 0.36
Methylene Chloride 2.4 2.0 6/17/20 15:09 BRF8.4 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 6/17/20 15:09 BRFND40.820.10 0.43
Naphthalene ND 0.20 6/17/20 15:09 BRFND41.00.15 0.80
Propene ND 8.0 6/17/20 15:09 BRFL-03 ND 4140.37 0.64
Styrene 0.15 0.20 6/17/20 15:09 BRFJ0.63 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 15:09 BRFND41.40.089 0.61
Page 4 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-1
Sample ID: 20F0582-01
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -24.7
Final Vacuum(in Hg): -3.3
Receipt Vacuum(in Hg): -6
Sampled: 6/10/2020 09:41
Canister ID: 2240
Flow Controller ID: 4225
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 11 0.20 6/17/20 15:09 BRF75 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/17/20 15:09 BRFND40.590.20 0.59
Toluene 1.1 0.20 6/17/20 15:09 BRF4.0 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 15:09 BRFND41.50.14 1.0
1,1,1-Trichloroethane 0.78 0.20 6/17/20 15:09 BRF4.2 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 15:09 BRFND41.10.082 0.45
Trichloroethylene 3.2 0.20 6/17/20 15:09 BRF17 41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.65 0.80 6/17/20 15:09 BRFJ3.6 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/17/20 15:09 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/17/20 15:09 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 6/17/20 15:09 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 15:09 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 15:09 BRFND40.510.13 0.32
m&p-Xylene 0.39 0.40 6/17/20 15:09 BRFJ1.7 41.70.23 1.00
o-Xylene 0.16 0.20 6/17/20 15:09 BRFJ0.69 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)104 6/19/20 16:1970-130
4-Bromofluorobenzene (1)102 6/17/20 15:0970-130
Page 5 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-2
Sample ID: 20F0582-02
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -3.5
Receipt Vacuum(in Hg): -5.1
Sampled: 6/10/2020 09:13
Canister ID: 2307
Flow Controller ID: 4224
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 160 8.0 6/17/20 15:50 BRFV-06 380 4192.8 6.6
Benzene ND 0.20 6/17/20 15:50 BRFND40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 15:50 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 15:50 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 15:50 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 15:50 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 15:50 BRFND40.440.15 0.32
2-Butanone (MEK)2.3 8.0 6/17/20 15:50 BRFJ6.6 4240.37 1.1
Carbon Disulfide ND 2.0 6/17/20 15:50 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/17/20 15:50 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 15:50 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 15:50 BRFND40.530.20 0.52
Chloroform ND 0.20 6/17/20 15:50 BRFND40.980.074 0.36
Chloromethane ND 0.40 6/17/20 15:50 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 15:50 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 15:50 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 15:50 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 15:50 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 15:50 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 15:50 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.43 0.20 6/17/20 15:50 BRF2.1 40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/17/20 15:50 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 15:50 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/17/20 15:50 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/17/20 15:50 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 15:50 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 15:50 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 15:50 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 15:50 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 15:50 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 15:50 BRFND47.21.3 4.6
Ethanol 330 20 6/19/20 16:59 BRFV-06 630 10388.9 17
Ethyl Acetate ND 0.20 6/17/20 15:50 BRFND40.720.15 0.54
Ethylbenzene ND 0.20 6/17/20 15:50 BRFND40.870.12 0.50
4-Ethyltoluene ND 0.20 6/17/20 15:50 BRFND40.980.12 0.60
Heptane ND 0.20 6/17/20 15:50 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 15:50 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 15:50 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/17/20 15:50 BRFND40.820.12 0.48
Isopropanol 91 8.0 6/17/20 15:50 BRF220 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 15:50 BRFND40.720.10 0.36
Methylene Chloride 0.37 2.0 6/17/20 15:50 BRFJ1.3 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 6/17/20 15:50 BRFND40.820.10 0.43
Naphthalene ND 0.20 6/17/20 15:50 BRFND41.00.15 0.80
Propene ND 8.0 6/17/20 15:50 BRFL-03 ND 4140.37 0.64
Styrene ND 0.20 6/17/20 15:50 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 15:50 BRFND41.40.089 0.61
Page 6 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-2
Sample ID: 20F0582-02
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -3.5
Receipt Vacuum(in Hg): -5.1
Sampled: 6/10/2020 09:13
Canister ID: 2307
Flow Controller ID: 4224
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.32 0.20 6/17/20 15:50 BRF2.2 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/17/20 15:50 BRFND40.590.20 0.59
Toluene 0.34 0.20 6/17/20 15:50 BRF1.3 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 15:50 BRFND41.50.14 1.0
1,1,1-Trichloroethane 2.3 0.20 6/17/20 15:50 BRF13 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 15:50 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 6/17/20 15:50 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.33 0.80 6/17/20 15:50 BRFJ1.9 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/17/20 15:50 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/17/20 15:50 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 6/17/20 15:50 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 15:50 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 15:50 BRFND40.510.13 0.32
m&p-Xylene 0.46 0.40 6/17/20 15:50 BRF2.0 41.70.23 1.00
o-Xylene 0.16 0.20 6/17/20 15:50 BRFJ0.69 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 6/19/20 16:5970-130
4-Bromofluorobenzene (1)102 6/17/20 15:5070-130
Page 7 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-3
Sample ID: 20F0582-03
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -6
Receipt Vacuum(in Hg): -8.1
Sampled: 6/10/2020 08:36
Canister ID: 2105
Flow Controller ID: 4090
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 150 8.0 6/17/20 17:11 BRFV-06 360 4192.8 6.6
Benzene ND 0.20 6/17/20 17:11 BRFND40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 17:11 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 17:11 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 17:11 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 17:11 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 17:11 BRFND40.440.15 0.32
2-Butanone (MEK)2.5 8.0 6/17/20 17:11 BRFJ7.4 4240.37 1.1
Carbon Disulfide ND 2.0 6/17/20 17:11 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/17/20 17:11 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 17:11 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 17:11 BRFND40.530.20 0.52
Chloroform ND 0.20 6/17/20 17:11 BRFND40.980.074 0.36
Chloromethane ND 0.40 6/17/20 17:11 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 17:11 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 17:11 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 17:11 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 17:11 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 17:11 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 17:11 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.51 0.20 6/17/20 17:11 BRF2.5 40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/17/20 17:11 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 17:11 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/17/20 17:11 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/17/20 17:11 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 17:11 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 17:11 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 17:11 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 17:11 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 17:11 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 17:11 BRFND47.21.3 4.6
Ethanol 480 40 6/19/20 17:38 BRFV-06 910 20751834
Ethyl Acetate ND 0.20 6/17/20 17:11 BRFND40.720.15 0.54
Ethylbenzene ND 0.20 6/17/20 17:11 BRFND40.870.12 0.50
4-Ethyltoluene ND 0.20 6/17/20 17:11 BRFND40.980.12 0.60
Heptane ND 0.20 6/17/20 17:11 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 17:11 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 17:11 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/17/20 17:11 BRFND40.820.12 0.48
Isopropanol 70 8.0 6/17/20 17:11 BRF170 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 17:11 BRFND40.720.10 0.36
Methylene Chloride 0.53 2.0 6/17/20 17:11 BRFJ1.8 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)0.61 0.20 6/17/20 17:11 BRF2.5 40.820.10 0.43
Naphthalene ND 0.20 6/17/20 17:11 BRFND41.00.15 0.80
Propene ND 8.0 6/17/20 17:11 BRFL-03 ND 4140.37 0.64
Styrene ND 0.20 6/17/20 17:11 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 17:11 BRFND41.40.089 0.61
Page 8 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-3
Sample ID: 20F0582-03
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -6
Receipt Vacuum(in Hg): -8.1
Sampled: 6/10/2020 08:36
Canister ID: 2105
Flow Controller ID: 4090
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 1.4 0.20 6/17/20 17:11 BRF9.7 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/17/20 17:11 BRFND40.590.20 0.59
Toluene 0.18 0.20 6/17/20 17:11 BRFJ0.68 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 17:11 BRFND41.50.14 1.0
1,1,1-Trichloroethane 0.48 0.20 6/17/20 17:11 BRF2.6 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 17:11 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 6/17/20 17:11 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.36 0.80 6/17/20 17:11 BRFJ2.0 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/17/20 17:11 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/17/20 17:11 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 6/17/20 17:11 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 17:11 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 17:11 BRFND40.510.13 0.32
m&p-Xylene 0.28 0.40 6/17/20 17:11 BRFJ1.2 41.70.23 1.00
o-Xylene ND 0.20 6/17/20 17:11 BRFND40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 6/19/20 17:3870-130
4-Bromofluorobenzene (1)102 6/17/20 17:1170-130
Page 9 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-4
Sample ID: 20F0582-04
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -4.5
Receipt Vacuum(in Hg): -5.6
Sampled: 6/9/2020 12:25
Canister ID: 2315
Flow Controller ID: 4131
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 36 8.0 6/17/20 17:51 BRFV-06 86 4192.8 6.6
Benzene ND 0.20 6/17/20 17:51 BRFND40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 17:51 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 17:51 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 17:51 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 17:51 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 17:51 BRFND40.440.15 0.32
2-Butanone (MEK)1.8 8.0 6/17/20 17:51 BRFJ5.3 4240.37 1.1
Carbon Disulfide ND 2.0 6/17/20 17:51 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/17/20 17:51 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 17:51 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 17:51 BRFND40.530.20 0.52
Chloroform ND 0.20 6/17/20 17:51 BRFND40.980.074 0.36
Chloromethane ND 0.40 6/17/20 17:51 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 17:51 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 17:51 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 17:51 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 17:51 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 17:51 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 17:51 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.43 0.20 6/17/20 17:51 BRF2.1 40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/17/20 17:51 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 17:51 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/17/20 17:51 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/17/20 17:51 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 17:51 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 17:51 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 17:51 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 17:51 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 17:51 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 17:51 BRFND47.21.3 4.6
Ethanol 290 20 6/17/20 18:31 BRFV-06 560 10388.9 17
Ethyl Acetate ND 0.20 6/17/20 17:51 BRFND40.720.15 0.54
Ethylbenzene ND 0.20 6/17/20 17:51 BRFND40.870.12 0.50
4-Ethyltoluene ND 0.20 6/17/20 17:51 BRFND40.980.12 0.60
Heptane ND 0.20 6/17/20 17:51 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 17:51 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 17:51 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/17/20 17:51 BRFND40.820.12 0.48
Isopropanol 8.9 8.0 6/17/20 17:51 BRF22 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 17:51 BRFND40.720.10 0.36
Methylene Chloride 0.48 2.0 6/17/20 17:51 BRFJ1.7 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 6/17/20 17:51 BRFND40.820.10 0.43
Naphthalene 0.16 0.20 6/17/20 17:51 BRFJ0.82 41.00.15 0.80
Propene ND 8.0 6/17/20 17:51 BRFL-03 ND 4140.37 0.64
Styrene ND 0.20 6/17/20 17:51 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 17:51 BRFND41.40.089 0.61
Page 10 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-4
Sample ID: 20F0582-04
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -4.5
Receipt Vacuum(in Hg): -5.6
Sampled: 6/9/2020 12:25
Canister ID: 2315
Flow Controller ID: 4131
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 90 0.20 6/17/20 17:51 BRF610 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/17/20 17:51 BRFND40.590.20 0.59
Toluene 0.35 0.20 6/17/20 17:51 BRF1.3 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 17:51 BRFND41.50.14 1.0
1,1,1-Trichloroethane 0.14 0.20 6/17/20 17:51 BRFJ0.79 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 17:51 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 6/17/20 17:51 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.38 0.80 6/17/20 17:51 BRFJ2.1 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/17/20 17:51 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/17/20 17:51 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 6/17/20 17:51 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 17:51 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 17:51 BRFND40.510.13 0.32
m&p-Xylene 0.26 0.40 6/17/20 17:51 BRFJ1.1 41.70.23 1.00
o-Xylene ND 0.20 6/17/20 17:51 BRFND40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)102 6/17/20 18:3170-130
4-Bromofluorobenzene (1)102 6/17/20 17:5170-130
Page 11 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-5
Sample ID: 20F0582-05
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -4.5
Receipt Vacuum(in Hg): -6
Sampled: 6/9/2020 13:21
Canister ID: 2096
Flow Controller ID: 4352
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 45 8.0 6/17/20 19:12 BRFV-06 110 4192.8 6.6
Benzene ND 0.20 6/17/20 19:12 BRFND40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 19:12 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 19:12 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 19:12 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 19:12 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 19:12 BRFND40.440.15 0.32
2-Butanone (MEK)3.0 8.0 6/17/20 19:12 BRFJ8.7 4240.37 1.1
Carbon Disulfide ND 2.0 6/17/20 19:12 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/17/20 19:12 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 19:12 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 19:12 BRFND40.530.20 0.52
Chloroform ND 0.20 6/17/20 19:12 BRFND40.980.074 0.36
Chloromethane ND 0.40 6/17/20 19:12 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 19:12 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 19:12 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 19:12 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 19:12 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 19:12 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 19:12 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.38 0.20 6/17/20 19:12 BRF1.9 40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/17/20 19:12 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 19:12 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/17/20 19:12 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/17/20 19:12 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 19:12 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 19:12 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 19:12 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 19:12 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 19:12 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 19:12 BRFND47.21.3 4.6
Ethanol 450 40 6/20/20 8:29 BRFV-06 860 20751834
Ethyl Acetate 2.2 0.20 6/17/20 19:12 BRF7.8 40.720.15 0.54
Ethylbenzene 0.13 0.20 6/17/20 19:12 BRFJ0.56 40.870.12 0.50
4-Ethyltoluene ND 0.20 6/17/20 19:12 BRFND40.980.12 0.60
Heptane ND 0.20 6/17/20 19:12 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 19:12 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 19:12 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/17/20 19:12 BRFND40.820.12 0.48
Isopropanol 8.8 8.0 6/17/20 19:12 BRF22 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 19:12 BRFND40.720.10 0.36
Methylene Chloride 1.9 2.0 6/17/20 19:12 BRFJ6.7 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 6/17/20 19:12 BRFND40.820.10 0.43
Naphthalene ND 0.20 6/17/20 19:12 BRFND41.00.15 0.80
Propene ND 8.0 6/17/20 19:12 BRFL-03 ND 4140.37 0.64
Styrene ND 0.20 6/17/20 19:12 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 19:12 BRFND41.40.089 0.61
Page 12 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-5
Sample ID: 20F0582-05
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -4.5
Receipt Vacuum(in Hg): -6
Sampled: 6/9/2020 13:21
Canister ID: 2096
Flow Controller ID: 4352
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.12 0.20 6/17/20 19:12 BRFJ0.84 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/17/20 19:12 BRFND40.590.20 0.59
Toluene 1.2 0.20 6/17/20 19:12 BRF4.6 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 19:12 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 6/17/20 19:12 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 19:12 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 6/17/20 19:12 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.31 0.80 6/17/20 19:12 BRFJ1.7 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/17/20 19:12 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/17/20 19:12 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 6/17/20 19:12 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 19:12 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 19:12 BRFND40.510.13 0.32
m&p-Xylene 0.41 0.40 6/17/20 19:12 BRF1.8 41.70.23 1.00
o-Xylene 0.19 0.20 6/17/20 19:12 BRFJ0.82 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 6/20/20 8:2970-130
4-Bromofluorobenzene (1)102 6/17/20 19:1270-130
Page 13 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-6
Sample ID: 20F0582-06
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -6.5
Receipt Vacuum(in Hg): -7.3
Sampled: 6/9/2020 12:54
Canister ID: 2338
Flow Controller ID: 4113
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 81 8.0 6/17/20 19:53 BRFV-06 190 4192.8 6.6
Benzene ND 0.20 6/17/20 19:53 BRFND40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 19:53 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 19:53 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 19:53 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 19:53 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 19:53 BRFND40.440.15 0.32
2-Butanone (MEK)4.2 8.0 6/17/20 19:53 BRFJ12 4240.37 1.1
Carbon Disulfide ND 2.0 6/17/20 19:53 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/17/20 19:53 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 19:53 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 19:53 BRFND40.530.20 0.52
Chloroform ND 0.20 6/17/20 19:53 BRFND40.980.074 0.36
Chloromethane ND 0.40 6/17/20 19:53 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 19:53 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 19:53 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 19:53 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 19:53 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 19:53 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 19:53 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.38 0.20 6/17/20 19:53 BRF1.9 40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/17/20 19:53 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 19:53 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/17/20 19:53 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/17/20 19:53 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 19:53 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 19:53 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 19:53 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 19:53 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 19:53 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 19:53 BRFND47.21.3 4.6
Ethanol 480 20 6/19/20 18:56 BRFV-06 900 10388.9 17
Ethyl Acetate ND 0.20 6/17/20 19:53 BRFND40.720.15 0.54
Ethylbenzene ND 0.20 6/17/20 19:53 BRFND40.870.12 0.50
4-Ethyltoluene ND 0.20 6/17/20 19:53 BRFND40.980.12 0.60
Heptane ND 0.20 6/17/20 19:53 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 19:53 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 19:53 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/17/20 19:53 BRFND40.820.12 0.48
Isopropanol 14 8.0 6/17/20 19:53 BRF36 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 19:53 BRFND40.720.10 0.36
Methylene Chloride 0.40 2.0 6/17/20 19:53 BRFJ1.4 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 6/17/20 19:53 BRFND40.820.10 0.43
Naphthalene ND 0.20 6/17/20 19:53 BRFND41.00.15 0.80
Propene ND 8.0 6/17/20 19:53 BRFL-03 ND 4140.37 0.64
Styrene ND 0.20 6/17/20 19:53 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 19:53 BRFND41.40.089 0.61
Page 14 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-6
Sample ID: 20F0582-06
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -6.5
Receipt Vacuum(in Hg): -7.3
Sampled: 6/9/2020 12:54
Canister ID: 2338
Flow Controller ID: 4113
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 38 0.20 6/17/20 19:53 BRF260 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/17/20 19:53 BRFND40.590.20 0.59
Toluene 0.42 0.20 6/17/20 19:53 BRF1.6 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 19:53 BRFND41.50.14 1.0
1,1,1-Trichloroethane 0.52 0.20 6/17/20 19:53 BRF2.9 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 19:53 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 6/17/20 19:53 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.28 0.80 6/17/20 19:53 BRFJ1.6 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/17/20 19:53 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/17/20 19:53 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 6/17/20 19:53 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 19:53 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 19:53 BRFND40.510.13 0.32
m&p-Xylene 0.30 0.40 6/17/20 19:53 BRFJ1.3 41.70.23 1.00
o-Xylene 0.13 0.20 6/17/20 19:53 BRFJ0.57 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 6/19/20 18:5670-130
4-Bromofluorobenzene (1)103 6/17/20 19:5370-130
Page 15 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-7
Sample ID: 20F0582-07
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -6.9
Sampled: 6/9/2020 11:54
Canister ID: 2333
Flow Controller ID: 4356
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 52 8.0 6/17/20 20:33 BRFV-06 120 4192.8 6.6
Benzene 0.16 0.20 6/17/20 20:33 BRFJ0.51 40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 20:33 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 20:33 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 20:33 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 20:33 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 20:33 BRFND40.440.15 0.32
2-Butanone (MEK)2.0 8.0 6/17/20 20:33 BRFJ6.0 4240.37 1.1
Carbon Disulfide 1.9 2.0 6/17/20 20:33 BRFJ5.9 46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/17/20 20:33 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 20:33 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 20:33 BRFND40.530.20 0.52
Chloroform 0.98 0.20 6/17/20 20:33 BRF4.8 40.980.074 0.36
Chloromethane ND 0.40 6/17/20 20:33 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 20:33 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 20:33 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 20:33 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 20:33 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 20:33 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 20:33 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.35 0.20 6/17/20 20:33 BRF1.7 40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/17/20 20:33 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 20:33 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/17/20 20:33 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene 0.26 0.20 6/17/20 20:33 BRF1.0 40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 20:33 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 20:33 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 20:33 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 20:33 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 20:33 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 20:33 BRFND47.21.3 4.6
Ethanol 280 20 6/19/20 19:36 BRFV-06 530 10388.9 17
Ethyl Acetate ND 0.20 6/17/20 20:33 BRFND40.720.15 0.54
Ethylbenzene ND 0.20 6/17/20 20:33 BRFND40.870.12 0.50
4-Ethyltoluene ND 0.20 6/17/20 20:33 BRFND40.980.12 0.60
Heptane ND 0.20 6/17/20 20:33 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 20:33 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 20:33 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/17/20 20:33 BRFND40.820.12 0.48
Isopropanol 8.5 8.0 6/17/20 20:33 BRF21 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 20:33 BRFND40.720.10 0.36
Methylene Chloride 0.74 2.0 6/17/20 20:33 BRFJ2.6 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 6/17/20 20:33 BRFND40.820.10 0.43
Naphthalene 0.17 0.20 6/17/20 20:33 BRFJ0.88 41.00.15 0.80
Propene ND 8.0 6/17/20 20:33 BRFL-03 ND 4140.37 0.64
Styrene ND 0.20 6/17/20 20:33 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 20:33 BRFND41.40.089 0.61
Page 16 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-7
Sample ID: 20F0582-07
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -6.9
Sampled: 6/9/2020 11:54
Canister ID: 2333
Flow Controller ID: 4356
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.20 0.20 6/17/20 20:33 BRFJ1.3 41.40.11 0.75
Tetrahydrofuran 3.1 0.20 6/17/20 20:33 BRF9.1 40.590.20 0.59
Toluene 0.40 0.20 6/17/20 20:33 BRF1.5 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 20:33 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 6/17/20 20:33 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 20:33 BRFND41.10.082 0.45
Trichloroethylene 0.15 0.20 6/17/20 20:33 BRFJ0.82 41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.24 0.80 6/17/20 20:33 BRFJ1.3 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/17/20 20:33 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/17/20 20:33 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 6/17/20 20:33 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 20:33 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 20:33 BRFND40.510.13 0.32
m&p-Xylene 0.28 0.40 6/17/20 20:33 BRFJ1.2 41.70.23 1.00
o-Xylene 0.14 0.20 6/17/20 20:33 BRFJ0.61 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 6/19/20 19:3670-130
4-Bromofluorobenzene (1)102 6/17/20 20:3370-130
Page 17 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-8
Sample ID: 20F0582-08
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -5.1
Sampled: 6/9/2020 10:09
Canister ID: 2295
Flow Controller ID: 4328
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 90 8.0 6/17/20 21:14 BRFV-06 210 4192.8 6.6
Benzene 0.096 0.20 6/17/20 21:14 BRFJ0.31 40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 21:14 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 21:14 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 21:14 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 21:14 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 21:14 BRFND40.440.15 0.32
2-Butanone (MEK)2.7 8.0 6/17/20 21:14 BRFJ8.1 4240.37 1.1
Carbon Disulfide ND 2.0 6/17/20 21:14 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/17/20 21:14 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 21:14 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 21:14 BRFND40.530.20 0.52
Chloroform ND 0.20 6/17/20 21:14 BRFND40.980.074 0.36
Chloromethane ND 0.40 6/17/20 21:14 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 21:14 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 21:14 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 21:14 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 21:14 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 21:14 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 21:14 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.38 0.20 6/17/20 21:14 BRF1.9 40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/17/20 21:14 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 21:14 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/17/20 21:14 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/17/20 21:14 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 21:14 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 21:14 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 21:14 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 21:14 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 21:14 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 21:14 BRFND47.21.3 4.6
Ethanol 300 20 6/19/20 20:15 BRFV-06 560 10388.9 17
Ethyl Acetate 1.6 0.20 6/17/20 21:14 BRF5.6 40.720.15 0.54
Ethylbenzene 0.26 0.20 6/17/20 21:14 BRF1.1 40.870.12 0.50
4-Ethyltoluene 0.48 0.20 6/17/20 21:14 BRF2.4 40.980.12 0.60
Heptane ND 0.20 6/17/20 21:14 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 21:14 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 21:14 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/17/20 21:14 BRFND40.820.12 0.48
Isopropanol 8.6 8.0 6/17/20 21:14 BRF21 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 21:14 BRFND40.720.10 0.36
Methylene Chloride 0.42 2.0 6/17/20 21:14 BRFJ1.5 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 6/17/20 21:14 BRFND40.820.10 0.43
Naphthalene 0.86 0.20 6/17/20 21:14 BRF4.5 41.00.15 0.80
Propene ND 8.0 6/17/20 21:14 BRFL-03 ND 4140.37 0.64
Styrene 0.22 0.20 6/17/20 21:14 BRF0.92 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 21:14 BRFND41.40.089 0.61
Page 18 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-8
Sample ID: 20F0582-08
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -5.1
Sampled: 6/9/2020 10:09
Canister ID: 2295
Flow Controller ID: 4328
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 4.9 0.20 6/17/20 21:14 BRF33 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/17/20 21:14 BRFND40.590.20 0.59
Toluene 0.79 0.20 6/17/20 21:14 BRF3.0 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 21:14 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 6/17/20 21:14 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 21:14 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 6/17/20 21:14 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.28 0.80 6/17/20 21:14 BRFJ1.6 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/17/20 21:14 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/17/20 21:14 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene 0.94 0.20 6/17/20 21:14 BRF4.6 40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 21:14 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 21:14 BRFND40.510.13 0.32
m&p-Xylene 2.4 0.40 6/17/20 21:14 BRF10 41.70.23 1.00
o-Xylene 0.78 0.20 6/17/20 21:14 BRF3.4 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)106 6/19/20 20:1570-130
4-Bromofluorobenzene (1)105 6/17/20 21:1470-130
Page 19 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-9
Sample ID: 20F0582-09
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28.7
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -5.7
Sampled: 6/9/2020 10:36
Canister ID: 2230
Flow Controller ID: 4340
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 120 8.0 6/17/20 21:55 BRFV-06 290 4192.8 6.6
Benzene ND 0.20 6/17/20 21:55 BRFND40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 21:55 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 21:55 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 21:55 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 21:55 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 21:55 BRFND40.440.15 0.32
2-Butanone (MEK)5.3 8.0 6/17/20 21:55 BRFJ16 4240.37 1.1
Carbon Disulfide ND 2.0 6/17/20 21:55 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/17/20 21:55 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 21:55 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 21:55 BRFND40.530.20 0.52
Chloroform 0.21 0.20 6/17/20 21:55 BRF1.0 40.980.074 0.36
Chloromethane ND 0.40 6/17/20 21:55 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 21:55 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 21:55 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 21:55 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 21:55 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 21:55 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 21:55 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.39 0.20 6/17/20 21:55 BRF1.9 40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/17/20 21:55 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 21:55 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/17/20 21:55 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/17/20 21:55 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 21:55 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 21:55 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 21:55 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 21:55 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 21:55 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 21:55 BRFND47.21.3 4.6
Ethanol 1900 80 6/19/20 20:54 BRFV-06 3600 401503667
Ethyl Acetate 2.8 0.20 6/17/20 21:55 BRF10 40.720.15 0.54
Ethylbenzene 0.15 0.20 6/17/20 21:55 BRFJ0.66 40.870.12 0.50
4-Ethyltoluene 0.15 0.20 6/17/20 21:55 BRFJ0.73 40.980.12 0.60
Heptane ND 0.20 6/17/20 21:55 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 21:55 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 21:55 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/17/20 21:55 BRFND40.820.12 0.48
Isopropanol 17 8.0 6/17/20 21:55 BRF42 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 21:55 BRFND40.720.10 0.36
Methylene Chloride 0.67 2.0 6/17/20 21:55 BRFJ2.3 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)3.5 0.20 6/17/20 21:55 BRF14 40.820.10 0.43
Naphthalene 1.1 0.20 6/17/20 21:55 BRF5.7 41.00.15 0.80
Propene ND 8.0 6/17/20 21:55 BRFL-03 ND 4140.37 0.64
Styrene 0.21 0.20 6/17/20 21:55 BRF0.90 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 21:55 BRFND41.40.089 0.61
Page 20 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-9
Sample ID: 20F0582-09
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28.7
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -5.7
Sampled: 6/9/2020 10:36
Canister ID: 2230
Flow Controller ID: 4340
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 79 0.20 6/17/20 21:55 BRF530 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/17/20 21:55 BRFND40.590.20 0.59
Toluene 0.66 0.20 6/17/20 21:55 BRF2.5 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 21:55 BRFND41.50.14 1.0
1,1,1-Trichloroethane 0.21 0.20 6/17/20 21:55 BRF1.1 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 21:55 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 6/17/20 21:55 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.38 0.80 6/17/20 21:55 BRFJ2.1 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/17/20 21:55 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/17/20 21:55 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene 0.26 0.20 6/17/20 21:55 BRF1.3 40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 21:55 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 21:55 BRFND40.510.13 0.32
m&p-Xylene 0.90 0.40 6/17/20 21:55 BRF3.9 41.70.23 1.00
o-Xylene 0.33 0.20 6/17/20 21:55 BRF1.4 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 6/19/20 20:5470-130
4-Bromofluorobenzene (1)103 6/17/20 21:5570-130
Page 21 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-10
Sample ID: 20F0582-10
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -5.3
Sampled: 6/9/2020 09:33
Canister ID: 2300
Flow Controller ID: 4332
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 190 8.0 6/17/20 23:17 BRFV-06 460 4192.8 6.6
Benzene ND 0.20 6/17/20 23:17 BRFND40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 23:17 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 23:17 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 23:17 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 23:17 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 23:17 BRFND40.440.15 0.32
2-Butanone (MEK)20 8.0 6/17/20 23:17 BRF60 4240.37 1.1
Carbon Disulfide ND 2.0 6/17/20 23:17 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/17/20 23:17 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 23:17 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 23:17 BRFND40.530.20 0.52
Chloroform ND 0.20 6/17/20 23:17 BRFND40.980.074 0.36
Chloromethane ND 0.40 6/17/20 23:17 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 23:17 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 23:17 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 23:17 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 23:17 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 23:17 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 23:17 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 6/17/20 23:17 BRFND40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/17/20 23:17 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 23:17 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/17/20 23:17 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/17/20 23:17 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 23:17 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 23:17 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 23:17 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 23:17 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 23:17 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 23:17 BRFND47.21.3 4.6
Ethanol 900 40 6/19/20 22:17 BRFV-06 1700 20751834
Ethyl Acetate ND 0.20 6/17/20 23:17 BRFND40.720.15 0.54
Ethylbenzene 0.27 0.20 6/17/20 23:17 BRF1.2 40.870.12 0.50
4-Ethyltoluene 0.41 0.20 6/17/20 23:17 BRF2.0 40.980.12 0.60
Heptane ND 0.20 6/17/20 23:17 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 23:17 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 23:17 BRFND4280.35 1.2
2-Hexanone (MBK)3.7 0.20 6/17/20 23:17 BRF15 40.820.12 0.48
Isopropanol 29 8.0 6/17/20 23:17 BRF70 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 23:17 BRFND40.720.10 0.36
Methylene Chloride 0.64 2.0 6/17/20 23:17 BRFJ2.2 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 6/17/20 23:17 BRFND40.820.10 0.43
Naphthalene 0.76 0.20 6/17/20 23:17 BRF4.0 41.00.15 0.80
Propene ND 8.0 6/17/20 23:17 BRFL-03 ND 4140.37 0.64
Styrene 0.31 0.20 6/17/20 23:17 BRF1.3 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 23:17 BRFND41.40.089 0.61
Page 22 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-10
Sample ID: 20F0582-10
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -5.3
Sampled: 6/9/2020 09:33
Canister ID: 2300
Flow Controller ID: 4332
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 10 0.20 6/17/20 23:17 BRF69 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/17/20 23:17 BRFND40.590.20 0.59
Toluene 0.82 0.20 6/17/20 23:17 BRF3.1 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 23:17 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 6/17/20 23:17 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 23:17 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 6/17/20 23:17 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.54 0.80 6/17/20 23:17 BRFJ3.1 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)0.50 0.80 6/17/20 23:17 BRFJ3.8 46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/17/20 23:17 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene 0.80 0.20 6/17/20 23:17 BRF4.0 40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 23:17 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 23:17 BRFND40.510.13 0.32
m&p-Xylene 1.9 0.40 6/17/20 23:17 BRF8.3 41.70.23 1.00
o-Xylene 0.68 0.20 6/17/20 23:17 BRF2.9 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 6/19/20 22:1770-130
4-Bromofluorobenzene (1)104 6/17/20 23:1770-130
Page 23 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-11
Sample ID: 20F0582-11
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28.3
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -4.3
Sampled: 6/9/2020 09:05
Canister ID: 2101
Flow Controller ID: 4332
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 96 8.0 6/17/20 23:58 BRFV-06 230 4192.8 6.6
Benzene 0.18 0.20 6/17/20 23:58 BRFJ0.59 40.640.082 0.26
Benzyl chloride ND 0.20 6/17/20 23:58 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/17/20 23:58 BRFND41.30.074 0.49
Bromoform ND 0.20 6/17/20 23:58 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/17/20 23:58 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/17/20 23:58 BRFND40.440.15 0.32
2-Butanone (MEK)1.9 8.0 6/17/20 23:58 BRFJ5.5 4240.37 1.1
Carbon Disulfide ND 2.0 6/17/20 23:58 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/17/20 23:58 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/17/20 23:58 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/17/20 23:58 BRFND40.530.20 0.52
Chloroform ND 0.20 6/17/20 23:58 BRFND40.980.074 0.36
Chloromethane ND 0.40 6/17/20 23:58 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/17/20 23:58 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/17/20 23:58 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/17/20 23:58 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/17/20 23:58 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/17/20 23:58 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/17/20 23:58 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.39 0.20 6/17/20 23:58 BRF1.9 40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/17/20 23:58 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/17/20 23:58 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/17/20 23:58 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/17/20 23:58 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/17/20 23:58 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/17/20 23:58 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/17/20 23:58 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/17/20 23:58 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/17/20 23:58 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/17/20 23:58 BRFND47.21.3 4.6
Ethanol 400 20 6/19/20 22:58 BRFV-06 750 10388.9 17
Ethyl Acetate 3.0 0.20 6/17/20 23:58 BRF11 40.720.15 0.54
Ethylbenzene 0.56 0.20 6/17/20 23:58 BRF2.4 40.870.12 0.50
4-Ethyltoluene 1.2 0.20 6/17/20 23:58 BRF5.9 40.980.12 0.60
Heptane 0.28 0.20 6/17/20 23:58 BRF1.1 40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/17/20 23:58 BRFND42.10.092 0.98
Hexane ND 8.0 6/17/20 23:58 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/17/20 23:58 BRFND40.820.12 0.48
Isopropanol 7.1 8.0 6/17/20 23:58 BRFJ17 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/17/20 23:58 BRFND40.720.10 0.36
Methylene Chloride 1.6 2.0 6/17/20 23:58 BRFJ5.6 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)8.2 0.20 6/17/20 23:58 BRF34 40.820.10 0.43
Naphthalene 1.8 0.20 6/17/20 23:58 BRF9.2 41.00.15 0.80
Propene ND 8.0 6/17/20 23:58 BRFL-03 ND 4140.37 0.64
Styrene 0.55 0.20 6/17/20 23:58 BRF2.4 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/17/20 23:58 BRFND41.40.089 0.61
Page 24 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-11
Sample ID: 20F0582-11
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -28.3
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -4.3
Sampled: 6/9/2020 09:05
Canister ID: 2101
Flow Controller ID: 4332
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.58 0.20 6/17/20 23:58 BRF3.9 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/17/20 23:58 BRFND40.590.20 0.59
Toluene 2.0 0.20 6/17/20 23:58 BRF7.4 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/17/20 23:58 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 6/17/20 23:58 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/17/20 23:58 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 6/17/20 23:58 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.27 0.80 6/17/20 23:58 BRFJ1.5 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/17/20 23:58 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene 5.2 0.20 6/17/20 23:58 BRF25 40.980.13 0.63
1,3,5-Trimethylbenzene 2.3 0.20 6/17/20 23:58 BRF12 40.980.13 0.62
Vinyl Acetate ND 4.0 6/17/20 23:58 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/17/20 23:58 BRFND40.510.13 0.32
m&p-Xylene 4.8 0.40 6/17/20 23:58 BRF21 41.70.23 1.00
o-Xylene 1.6 0.20 6/17/20 23:58 BRF7.1 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)106 6/19/20 22:5870-130
4-Bromofluorobenzene (1)105 6/17/20 23:5870-130
Page 25 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-Dup
Sample ID: 20F0582-12
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -6
Receipt Vacuum(in Hg): -8.1
Sampled: 6/10/2020 00:00
Canister ID: 2122
Flow Controller ID: 4090
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 140 8.0 6/18/20 0:39 BRFV-06 340 4192.8 6.6
Benzene 0.12 0.20 6/18/20 0:39 BRFJ0.40 40.640.082 0.26
Benzyl chloride ND 0.20 6/18/20 0:39 BRFND41.00.052 0.27
Bromodichloromethane ND 0.20 6/18/20 0:39 BRFND41.30.074 0.49
Bromoform ND 0.20 6/18/20 0:39 BRFND42.10.090 0.93
Bromomethane ND 0.40 6/18/20 0:39 BRFND41.60.14 0.53
1,3-Butadiene ND 0.20 6/18/20 0:39 BRFND40.440.15 0.32
2-Butanone (MEK)2.8 8.0 6/18/20 0:39 BRFJ8.3 4240.37 1.1
Carbon Disulfide ND 2.0 6/18/20 0:39 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 6/18/20 0:39 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 6/18/20 0:39 BRFND40.920.098 0.45
Chloroethane ND 0.20 6/18/20 0:39 BRFND40.530.20 0.52
Chloroform ND 0.20 6/18/20 0:39 BRFND40.980.074 0.36
Chloromethane ND 0.40 6/18/20 0:39 BRFND40.830.14 0.28
Cyclohexane ND 0.20 6/18/20 0:39 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 6/18/20 0:39 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 6/18/20 0:39 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 6/18/20 0:39 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 6/18/20 0:39 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 6/18/20 0:39 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.50 0.20 6/18/20 0:39 BRF2.5 40.990.087 0.43
1,1-Dichloroethane ND 0.20 6/18/20 0:39 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 6/18/20 0:39 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 6/18/20 0:39 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 6/18/20 0:39 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 6/18/20 0:39 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 6/18/20 0:39 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 6/18/20 0:39 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 6/18/20 0:39 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 6/18/20 0:39 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 6/18/20 0:39 BRFND47.21.3 4.6
Ethanol 360 20 6/20/20 0:20 BRFV-06 690 10388.9 17
Ethyl Acetate ND 0.20 6/18/20 0:39 BRFND40.720.15 0.54
Ethylbenzene ND 0.20 6/18/20 0:39 BRFND40.870.12 0.50
4-Ethyltoluene ND 0.20 6/18/20 0:39 BRFND40.980.12 0.60
Heptane ND 0.20 6/18/20 0:39 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.20 6/18/20 0:39 BRFND42.10.092 0.98
Hexane ND 8.0 6/18/20 0:39 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 6/18/20 0:39 BRFND40.820.12 0.48
Isopropanol 66 8.0 6/18/20 0:39 BRF160 4200.37 0.90
Methyl tert-Butyl Ether (MTBE)ND 0.20 6/18/20 0:39 BRFND40.720.10 0.36
Methylene Chloride 0.38 2.0 6/18/20 0:39 BRFJ1.3 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)0.69 0.20 6/18/20 0:39 BRF2.8 40.820.10 0.43
Naphthalene ND 0.20 6/18/20 0:39 BRFND41.00.15 0.80
Propene ND 8.0 6/18/20 0:39 BRFL-03 ND 4140.37 0.64
Styrene ND 0.20 6/18/20 0:39 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 6/18/20 0:39 BRFND41.40.089 0.61
Page 26 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Salisbury, NC
Date Received: 6/11/2020
Work Order: 20F0582Sample Description/Location:
Field Sample #: SS-Dup
Sample ID: 20F0582-12
Sample Matrix: Sub Slab
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -6
Receipt Vacuum(in Hg): -8.1
Sampled: 6/10/2020 00:00
Canister ID: 2122
Flow Controller ID: 4090
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 1.4 0.20 6/18/20 0:39 BRF9.5 41.40.11 0.75
Tetrahydrofuran ND 0.20 6/18/20 0:39 BRFND40.590.20 0.59
Toluene 0.17 0.20 6/18/20 0:39 BRFJ0.63 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 6/18/20 0:39 BRFND41.50.14 1.0
1,1,1-Trichloroethane 0.45 0.20 6/18/20 0:39 BRF2.5 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 6/18/20 0:39 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 6/18/20 0:39 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.36 0.80 6/18/20 0:39 BRFJ2.0 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 6/18/20 0:39 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 6/18/20 0:39 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 6/18/20 0:39 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 6/18/20 0:39 BRFND4140.12 0.44
Vinyl Chloride ND 0.20 6/18/20 0:39 BRFND40.510.13 0.32
m&p-Xylene 0.34 0.40 6/18/20 0:39 BRFJ1.5 41.70.23 1.00
o-Xylene ND 0.20 6/18/20 0:39 BRFND40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 6/20/20 0:2070-130
4-Bromofluorobenzene (1)103 6/18/20 0:3970-130
Page 27 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
20F0582-01 [SS-1]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-02 [SS-2]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-03 [SS-3]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-04 [SS-4]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-04RE1 [SS-4]B260278 1.5 1 N/A 1000 400 60 06/17/20
20F0582-05 [SS-5]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-06 [SS-6]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-07 [SS-7]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-08 [SS-8]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-09 [SS-9]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-10 [SS-10]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-11 [SS-11]B260278 1.5 1 N/A 1000 400 150 06/17/20
20F0582-12 [SS-Dup]B260278 1.5 1 N/A 1000 400 150 06/17/20
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
20F0582-01RE1 [SS-1]B260459 1.5 1 N/A 1000 400 30 06/19/20
20F0582-02RE1 [SS-2]B260459 1.5 1 N/A 1000 400 60 06/19/20
20F0582-03RE1 [SS-3]B260459 1.5 1 N/A 1000 400 30 06/19/20
20F0582-05RE1 [SS-5]B260459 1.5 1 N/A 1000 400 30 06/19/20
20F0582-06RE1 [SS-6]B260459 1.5 1 N/A 1000 400 60 06/19/20
20F0582-07RE1 [SS-7]B260459 1.5 1 N/A 1000 400 60 06/19/20
20F0582-08RE1 [SS-8]B260459 1.5 1 N/A 1000 400 60 06/19/20
20F0582-09RE1 [SS-9]B260459 1.5 1 N/A 1000 400 15 06/19/20
20F0582-10RE1 [SS-10]B260459 1.5 1 N/A 1000 400 30 06/19/20
20F0582-11RE1 [SS-11]B260459 1.5 1 N/A 1000 400 60 06/19/20
20F0582-12RE1 [SS-Dup]B260459 1.5 1 N/A 1000 400 60 06/19/20
Page 28 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B260278 - TO-15 Prep
Blank (B260278-BLK1)Prepared & Analyzed: 06/17/20
0.80NDAcetone
0.020NDBenzene
0.020NDBenzyl chloride
0.020NDBromodichloromethane
0.020NDBromoform
0.020NDBromomethane
0.020ND1,3-Butadiene
0.80ND2-Butanone (MEK)
0.20NDCarbon Disulfide
0.020NDCarbon Tetrachloride
0.020NDChlorobenzene
0.020NDChloroethane
0.020NDChloroform
0.040NDChloromethane
0.020NDCyclohexane
0.020NDDibromochloromethane
0.020ND1,2-Dibromoethane (EDB)
0.020ND1,2-Dichlorobenzene
0.020ND1,3-Dichlorobenzene
0.020ND1,4-Dichlorobenzene
0.020NDDichlorodifluoromethane (Freon 12)
0.020ND1,1-Dichloroethane
0.020ND1,2-Dichloroethane
0.020ND1,1-Dichloroethylene
0.020NDcis-1,2-Dichloroethylene
0.020NDtrans-1,2-Dichloroethylene
0.020ND1,2-Dichloropropane
0.020NDcis-1,3-Dichloropropene
0.020NDtrans-1,3-Dichloropropene
0.020ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.20ND1,4-Dioxane
0.80NDEthanol
0.020NDEthyl Acetate
0.020NDEthylbenzene
0.020ND4-Ethyltoluene
0.020NDHeptane
0.020NDHexachlorobutadiene
0.80NDHexane
0.020ND2-Hexanone (MBK)
0.80NDIsopropanol
0.020NDMethyl tert-Butyl Ether (MTBE)
0.20NDMethylene Chloride
0.020ND4-Methyl-2-pentanone (MIBK)
0.020NDNaphthalene
0.80 L-03NDPropene
0.020NDStyrene
Page 29 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B260278 - TO-15 Prep
Blank (B260278-BLK1)Prepared & Analyzed: 06/17/20
0.020ND1,1,2,2-Tetrachloroethane
0.020NDTetrachloroethylene
0.020NDTetrahydrofuran
0.020NDToluene
0.020ND1,2,4-Trichlorobenzene
0.020ND1,1,1-Trichloroethane
0.020ND1,1,2-Trichloroethane
0.020NDTrichloroethylene
0.080NDTrichlorofluoromethane (Freon 11)
0.080ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.020ND1,2,4-Trimethylbenzene
0.020ND1,3,5-Trimethylbenzene
0.40NDVinyl Acetate
0.020NDVinyl Chloride
0.040NDm&p-Xylene
0.020NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1018.04
LCS (B260278-BS1)Prepared & Analyzed: 06/17/20
5.00 V-0670-1301195.94Acetone
5.00 70-13083.54.18Benzene
5.00 70-13093.24.66Benzyl chloride
5.00 70-13095.54.78Bromodichloromethane
5.00 70-1301045.22Bromoform
5.00 70-13089.54.47Bromomethane
5.00 70-1301065.301,3-Butadiene
5.00 70-13081.14.062-Butanone (MEK)
5.00 70-13070.73.53Carbon Disulfide
5.00 70-1301035.15Carbon Tetrachloride
5.00 70-13086.64.33Chlorobenzene
5.00 70-1301055.27Chloroethane
5.00 70-13077.63.88Chloroform
5.00 70-13099.64.98Chloromethane
5.00 70-13076.33.82Cyclohexane
5.00 70-13097.14.86Dibromochloromethane
5.00 70-13088.44.421,2-Dibromoethane (EDB)
5.00 70-13090.14.511,2-Dichlorobenzene
5.00 70-13094.94.741,3-Dichlorobenzene
5.00 70-13090.74.531,4-Dichlorobenzene
5.00 70-13085.54.27Dichlorodifluoromethane (Freon 12)
5.00 70-13075.03.751,1-Dichloroethane
5.00 70-13090.34.521,2-Dichloroethane
5.00 70-13081.24.061,1-Dichloroethylene
5.00 70-13075.43.77cis-1,2-Dichloroethylene
5.00 70-13077.33.86trans-1,2-Dichloroethylene
5.00 70-13081.54.081,2-Dichloropropane
Page 30 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B260278 - TO-15 Prep
LCS (B260278-BS1)Prepared & Analyzed: 06/17/20
5.00 70-13084.84.24cis-1,3-Dichloropropene
5.00 70-13095.84.79trans-1,3-Dichloropropene
5.00 70-13088.84.441,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
5.00 70-13075.03.751,4-Dioxane
5.00 V-0670-1301135.67Ethanol
5.00 70-13073.53.68Ethyl Acetate
5.00 70-13087.64.38Ethylbenzene
5.00 70-13089.54.484-Ethyltoluene
5.00 70-13086.64.33Heptane
5.00 70-13087.14.36Hexachlorobutadiene
5.00 70-13098.14.90Hexane
5.00 70-13099.84.992-Hexanone (MBK)
5.00 70-1301065.29Isopropanol
5.00 70-13075.93.79Methyl tert-Butyl Ether (MTBE)
5.00 70-13079.43.97Methylene Chloride
5.00 70-13099.54.974-Methyl-2-pentanone (MIBK)
5.00 70-13084.24.21Naphthalene
5.00 L-0370-13068.53.42Propene *
5.00 70-13086.94.34Styrene
5.00 70-13088.34.411,1,2,2-Tetrachloroethane
5.00 70-13090.34.52Tetrachloroethylene
5.00 70-13072.73.63Tetrahydrofuran
5.00 70-13086.64.33Toluene
5.00 70-13078.83.941,2,4-Trichlorobenzene
5.00 70-13091.94.601,1,1-Trichloroethane
5.00 70-13086.04.301,1,2-Trichloroethane
5.00 70-13085.44.27Trichloroethylene
5.00 70-1301055.24Trichlorofluoromethane (Freon 11)
5.00 70-13072.13.601,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-13089.74.491,2,4-Trimethylbenzene
5.00 70-13091.34.571,3,5-Trimethylbenzene
5.00 70-13086.44.32Vinyl Acetate
5.00 70-13099.44.97Vinyl Chloride
10.0 70-13092.89.28m&p-Xylene
5.00 70-13093.04.65o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1078.52
Page 31 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B260278 - TO-15 Prep
Duplicate (B260278-DUP1)Prepared & Analyzed: 06/17/20 Source: 20F0582-02
8.0 160 25 V-060.501160Acetone19380
0.20 ND 25NDBenzene0.64ND
0.20 ND 25NDBenzyl chloride 1.0ND
0.20 ND 25NDBromodichloromethane1.3ND
0.20 ND 25NDBromoform2.1ND
0.20 ND 25NDBromomethane0.78ND
0.20 ND 25ND1,3-Butadiene 0.44ND
8.0 2.3 25 J1.062.32-Butanone (MEK)246.7
2.0 ND 25NDCarbon Disulfide 6.2ND
0.20 ND 25NDCarbon Tetrachloride 1.3ND
0.20 ND 25NDChlorobenzene0.92ND
0.20 ND 25NDChloroethane0.53ND
0.20 ND 25NDChloroform0.98ND
0.40 ND 25NDChloromethane0.83ND
0.20 ND 25NDCyclohexane0.69ND
0.20 ND 25NDDibromochloromethane1.7ND
0.20 ND 25ND1,2-Dibromoethane (EDB)1.5ND
0.20 ND 25ND1,2-Dichlorobenzene 1.2ND
0.20 ND 25ND1,3-Dichlorobenzene 1.2ND
0.20 ND 25ND1,4-Dichlorobenzene 1.2ND
0.20 0.43 251.870.42Dichlorodifluoromethane (Freon 12)0.992.1
0.20 ND 25ND1,1-Dichloroethane 0.81ND
0.20 ND 25ND1,2-Dichloroethane 0.81ND
0.20 ND 25ND1,1-Dichloroethylene 0.79ND
0.20 ND 25NDcis-1,2-Dichloroethylene 0.79ND
0.20 ND 25NDtrans-1,2-Dichloroethylene 0.79ND
0.20 ND 25ND1,2-Dichloropropane 0.92ND
0.20 ND 25NDcis-1,3-Dichloropropene 0.91ND
0.20 ND 25NDtrans-1,3-Dichloropropene 0.91ND
0.20 ND 25ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
1.4ND
2.0 ND 25ND1,4-Dioxane 7.2ND
8.0 360 25 E, V-064.46340Ethanol15640
0.20 ND 25NDEthyl Acetate 0.72ND
0.20 ND 25NDEthylbenzene0.87ND
0.20 ND 25ND4-Ethyltoluene 0.98ND
0.20 ND 25NDHeptane0.82ND
0.20 ND 25NDHexachlorobutadiene2.1ND
8.0 ND 25NDHexane28ND
0.20 ND 25ND2-Hexanone (MBK)0.82ND
8.0 91 251.2090Isopropanol20220
0.20 ND 25NDMethyl tert-Butyl Ether (MTBE)0.72ND
2.0 0.37 25 J3.310.36Methylene Chloride 6.91.2
0.20 ND 25ND4-Methyl-2-pentanone (MIBK)0.82ND
0.20 ND 25NDNaphthalene1.0ND
8.0 ND 25 L-03NDPropene14ND
0.20 ND 25NDStyrene0.85ND
Page 32 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B260278 - TO-15 Prep
Duplicate (B260278-DUP1)Prepared & Analyzed: 06/17/20 Source: 20F0582-02
0.20 ND 25ND1,1,2,2-Tetrachloroethane 1.4ND
0.20 0.32 251.230.33Tetrachloroethylene 1.42.2
0.20 ND 25NDTetrahydrofuran0.59ND
0.20 0.34 254.600.36Toluene 0.751.3
0.20 ND 25ND1,2,4-Trichlorobenzene 1.5ND
0.20 2.3 250.6962.31,1,1-Trichloroethane 1.113
0.20 ND 25ND1,1,2-Trichloroethane 1.1ND
0.20 ND 25NDTrichloroethylene1.1ND
0.80 0.33 25 J0.000.33Trichlorofluoromethane (Freon 11)4.51.9
0.80 ND 25ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
6.1ND
0.20 ND 25ND1,2,4-Trimethylbenzene 0.98ND
0.20 ND 25ND1,3,5-Trimethylbenzene 0.98ND
4.0 ND 25NDVinyl Acetate 14ND
0.20 ND 25NDVinyl Chloride 0.51ND
0.40 0.46 250.000.46m&p-Xylene 1.72.0
0.20 0.16 25 J7.230.17o-Xylene 0.870.75
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1018.05
Batch B260459 - TO-15 Prep
Blank (B260459-BLK1)Prepared & Analyzed: 06/19/20
0.80NDEthanol
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1048.28
LCS (B260459-BS1)Prepared & Analyzed: 06/19/20
5.00 V-0670-1301266.32Ethanol
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1088.60
Page 33 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B260459 - TO-15 Prep
Duplicate (B260459-DUP1)Prepared & Analyzed: 06/19/20 Source: 20F0582-11RE1
20 400 25 V-061.07400Ethanol38760
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1068.51
Page 34 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Note: Blank Subtraction is not performed unless otherwise noted
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
FLAG/QUALIFIER SUMMARY
Reported result is estimated. Value reported over verified calibration range.E
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this
compound is likely to be biased on the low side.
L-03
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for
this compound.
V-06
Page 35 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYST
Rebecca FaustRLF
Raisa A. PetraitisRAP
PDF Management StationSTATION
Kerry K. McGeeKKM
Brittany R. FiskBRF
Page 36 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S048688-ICV1 )Lab File ID: G2014217.D Analyzed: 05/22/20 06:45
Bromochloromethane (1)382161 8.521 362753 8.527 60 - 140105 -0.0060 +/-0.50
1,4-Difluorobenzene (1)1261285 10.302 1218329 10.301 60 - 140104 0.0010 +/-0.50
Chlorobenzene-d5 (1)1132393 14.679 1094382 14.679 60 - 140103 0.0000 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S049482-CCV1 )Lab File ID: G2016904.D Analyzed: 06/17/20 10:57
Bromochloromethane (1)363828 8.527 362753 8.527 60 - 140100 0.0000 +/-0.50
1,4-Difluorobenzene (1)967440 10.302 1218329 10.301 60 - 14079 0.0010 +/-0.50
Chlorobenzene-d5 (1)850081 14.679 1094382 14.679 60 - 14078 0.0000 +/-0.50
LCS (B260278-BS1 )Lab File ID: G2016906.D Analyzed: 06/17/20 12:17
Bromochloromethane (1)370239 8.527 363828 8.527 60 - 140102 0.0000 +/-0.50
1,4-Difluorobenzene (1)987818 10.301 967440 10.302 60 - 140102 -0.0010 +/-0.50
Chlorobenzene-d5 (1)876094 14.679 850081 14.679 60 - 140103 0.0000 +/-0.50
Blank (B260278-BLK1 )Lab File ID: G2016909.D Analyzed: 06/17/20 14:28
Bromochloromethane (1)320393 8.534 363828 8.527 60 - 14088 0.0070 +/-0.50
1,4-Difluorobenzene (1)909236 10.301 967440 10.302 60 - 14094 -0.0010 +/-0.50
Chlorobenzene-d5 (1)804688 14.679 850081 14.679 60 - 14095 0.0000 +/-0.50
SS-1 (20F0582-01 )Lab File ID: G2016910.D Analyzed: 06/17/20 15:09
Bromochloromethane (1)317630 8.527 363828 8.527 60 - 14087 0.0000 +/-0.50
1,4-Difluorobenzene (1)917082 10.301 967440 10.302 60 - 14095 -0.0010 +/-0.50
Chlorobenzene-d5 (1)807908 14.679 850081 14.679 60 - 14095 0.0000 +/-0.50
SS-2 (20F0582-02 )Lab File ID: G2016911.D Analyzed: 06/17/20 15:50
Bromochloromethane (1)323023 8.527 363828 8.527 60 - 14089 0.0000 +/-0.50
1,4-Difluorobenzene (1)916552 10.301 967440 10.302 60 - 14095 -0.0010 +/-0.50
Chlorobenzene-d5 (1)814874 14.679 850081 14.679 60 - 14096 0.0000 +/-0.50
Duplicate (B260278-DUP1 )Lab File ID: G2016912.D Analyzed: 06/17/20 16:31
Bromochloromethane (1)323388 8.527 363828 8.527 60 - 14089 0.0000 +/-0.50
1,4-Difluorobenzene (1)900870 10.301 967440 10.302 60 - 14093 -0.0010 +/-0.50
Chlorobenzene-d5 (1)785739 14.679 850081 14.679 60 - 14092 0.0000 +/-0.50
SS-3 (20F0582-03 )Lab File ID: G2016913.D Analyzed: 06/17/20 17:11
Bromochloromethane (1)324172 8.527 363828 8.527 60 - 14089 0.0000 +/-0.50
1,4-Difluorobenzene (1)904374 10.302 967440 10.302 60 - 14093 0.0000 +/-0.50
Chlorobenzene-d5 (1)800288 14.673 850081 14.679 60 - 14094 -0.0060 +/-0.50
Page 37 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SS-4 (20F0582-04 )Lab File ID: G2016914.D Analyzed: 06/17/20 17:51
Bromochloromethane (1)330881 8.527 363828 8.527 60 - 14091 0.0000 +/-0.50
1,4-Difluorobenzene (1)935723 10.301 967440 10.302 60 - 14097 -0.0010 +/-0.50
Chlorobenzene-d5 (1)825083 14.679 850081 14.679 60 - 14097 0.0000 +/-0.50
SS-4 (20F0582-04RE1 )Lab File ID: G2016915.D Analyzed: 06/17/20 18:31
Bromochloromethane (1)325507 8.527 363828 8.527 60 - 14089 0.0000 +/-0.50
1,4-Difluorobenzene (1)917851 10.301 967440 10.302 60 - 14095 -0.0010 +/-0.50
Chlorobenzene-d5 (1)796377 14.679 850081 14.679 60 - 14094 0.0000 +/-0.50
SS-5 (20F0582-05 )Lab File ID: G2016916.D Analyzed: 06/17/20 19:12
Bromochloromethane (1)328126 8.527 363828 8.527 60 - 14090 0.0000 +/-0.50
1,4-Difluorobenzene (1)928479 10.302 967440 10.302 60 - 14096 0.0000 +/-0.50
Chlorobenzene-d5 (1)821590 14.679 850081 14.679 60 - 14097 0.0000 +/-0.50
SS-6 (20F0582-06 )Lab File ID: G2016917.D Analyzed: 06/17/20 19:53
Bromochloromethane (1)331471 8.521 363828 8.527 60 - 14091 -0.0060 +/-0.50
1,4-Difluorobenzene (1)930718 10.301 967440 10.302 60 - 14096 -0.0010 +/-0.50
Chlorobenzene-d5 (1)823535 14.673 850081 14.679 60 - 14097 -0.0060 +/-0.50
SS-7 (20F0582-07 )Lab File ID: G2016918.D Analyzed: 06/17/20 20:33
Bromochloromethane (1)325048 8.527 363828 8.527 60 - 14089 0.0000 +/-0.50
1,4-Difluorobenzene (1)922799 10.301 967440 10.302 60 - 14095 -0.0010 +/-0.50
Chlorobenzene-d5 (1)819339 14.679 850081 14.679 60 - 14096 0.0000 +/-0.50
SS-8 (20F0582-08 )Lab File ID: G2016919.D Analyzed: 06/17/20 21:14
Bromochloromethane (1)333167 8.521 363828 8.527 60 - 14092 -0.0060 +/-0.50
1,4-Difluorobenzene (1)940675 10.302 967440 10.302 60 - 14097 0.0000 +/-0.50
Chlorobenzene-d5 (1)839695 14.679 850081 14.679 60 - 14099 0.0000 +/-0.50
SS-9 (20F0582-09 )Lab File ID: G2016920.D Analyzed: 06/17/20 21:55
Bromochloromethane (1)338258 8.521 363828 8.527 60 - 14093 -0.0060 +/-0.50
1,4-Difluorobenzene (1)961153 10.301 967440 10.302 60 - 14099 -0.0010 +/-0.50
Chlorobenzene-d5 (1)856411 14.679 850081 14.679 60 - 140101 0.0000 +/-0.50
SS-10 (20F0582-10 )Lab File ID: G2016922.D Analyzed: 06/17/20 23:17
Bromochloromethane (1)341802 8.521 363828 8.527 60 - 14094 -0.0060 +/-0.50
1,4-Difluorobenzene (1)963920 10.302 967440 10.302 60 - 140100 0.0000 +/-0.50
Chlorobenzene-d5 (1)872338 14.673 850081 14.679 60 - 140103 -0.0060 +/-0.50
SS-11 (20F0582-11 )Lab File ID: G2016923.D Analyzed: 06/17/20 23:58
Bromochloromethane (1)341316 8.527 363828 8.527 60 - 14094 0.0000 +/-0.50
1,4-Difluorobenzene (1)974911 10.301 967440 10.302 60 - 140101 -0.0010 +/-0.50
Chlorobenzene-d5 (1)860520 14.672 850081 14.679 60 - 140101 -0.0070 +/-0.50
Page 38 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SS-Dup (20F0582-12 )Lab File ID: G2016924.D Analyzed: 06/18/20 00:39
Bromochloromethane (1)343082 8.521 363828 8.527 60 - 14094 -0.0060 +/-0.50
1,4-Difluorobenzene (1)975678 10.302 967440 10.302 60 - 140101 0.0000 +/-0.50
Chlorobenzene-d5 (1)857612 14.673 850081 14.679 60 - 140101 -0.0060 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S049551-CCV1 )Lab File ID: G2017104.D Analyzed: 06/19/20 10:10
Bromochloromethane (1)351820 8.521 362753 8.527 60 - 14097 -0.0060 +/-0.50
1,4-Difluorobenzene (1)993496 10.302 1218329 10.301 60 - 14082 0.0010 +/-0.50
Chlorobenzene-d5 (1)882982 14.679 1094382 14.679 60 - 14081 0.0000 +/-0.50
LCS (B260459-BS1 )Lab File ID: G2017106.D Analyzed: 06/19/20 11:29
Bromochloromethane (1)353367 8.528 351820 8.521 60 - 140100 0.0070 +/-0.50
1,4-Difluorobenzene (1)998531 10.302 993496 10.302 60 - 140101 0.0000 +/-0.50
Chlorobenzene-d5 (1)891669 14.679 882982 14.679 60 - 140101 0.0000 +/-0.50
Blank (B260459-BLK1 )Lab File ID: G2017112.D Analyzed: 06/19/20 15:40
Bromochloromethane (1)348889 8.527 351820 8.521 60 - 14099 0.0060 +/-0.50
1,4-Difluorobenzene (1)948609 10.301 993496 10.302 60 - 14095 -0.0010 +/-0.50
Chlorobenzene-d5 (1)841030 14.673 882982 14.679 60 - 14095 -0.0060 +/-0.50
SS-1 (20F0582-01RE1 )Lab File ID: G2017113.D Analyzed: 06/19/20 16:19
Bromochloromethane (1)344896 8.528 351820 8.521 60 - 14098 0.0070 +/-0.50
1,4-Difluorobenzene (1)934967 10.302 993496 10.302 60 - 14094 0.0000 +/-0.50
Chlorobenzene-d5 (1)838937 14.679 882982 14.679 60 - 14095 0.0000 +/-0.50
SS-2 (20F0582-02RE1 )Lab File ID: G2017114.D Analyzed: 06/19/20 16:59
Bromochloromethane (1)343194 8.527 351820 8.521 60 - 14098 0.0060 +/-0.50
1,4-Difluorobenzene (1)923394 10.301 993496 10.302 60 - 14093 -0.0010 +/-0.50
Chlorobenzene-d5 (1)825685 14.679 882982 14.679 60 - 14094 0.0000 +/-0.50
SS-3 (20F0582-03RE1 )Lab File ID: G2017115.D Analyzed: 06/19/20 17:38
Bromochloromethane (1)346063 8.527 351820 8.521 60 - 14098 0.0060 +/-0.50
1,4-Difluorobenzene (1)929577 10.301 993496 10.302 60 - 14094 -0.0010 +/-0.50
Chlorobenzene-d5 (1)828695 14.679 882982 14.679 60 - 14094 0.0000 +/-0.50
SS-6 (20F0582-06RE1 )Lab File ID: G2017117.D Analyzed: 06/19/20 18:56
Bromochloromethane (1)348148 8.527 351820 8.521 60 - 14099 0.0060 +/-0.50
1,4-Difluorobenzene (1)937643 10.301 993496 10.302 60 - 14094 -0.0010 +/-0.50
Chlorobenzene-d5 (1)836800 14.679 882982 14.679 60 - 14095 0.0000 +/-0.50
Page 39 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SS-7 (20F0582-07RE1 )Lab File ID: G2017118.D Analyzed: 06/19/20 19:36
Bromochloromethane (1)344344 8.527 351820 8.521 60 - 14098 0.0060 +/-0.50
1,4-Difluorobenzene (1)919835 10.301 993496 10.302 60 - 14093 -0.0010 +/-0.50
Chlorobenzene-d5 (1)832017 14.679 882982 14.679 60 - 14094 0.0000 +/-0.50
SS-8 (20F0582-08RE1 )Lab File ID: G2017119.D Analyzed: 06/19/20 20:15
Bromochloromethane (1)346751 8.528 351820 8.521 60 - 14099 0.0070 +/-0.50
1,4-Difluorobenzene (1)934249 10.302 993496 10.302 60 - 14094 0.0000 +/-0.50
Chlorobenzene-d5 (1)837959 14.673 882982 14.679 60 - 14095 -0.0060 +/-0.50
SS-9 (20F0582-09RE1 )Lab File ID: G2017120.D Analyzed: 06/19/20 20:54
Bromochloromethane (1)345717 8.527 351820 8.521 60 - 14098 0.0060 +/-0.50
1,4-Difluorobenzene (1)926796 10.302 993496 10.302 60 - 14093 0.0000 +/-0.50
Chlorobenzene-d5 (1)829021 14.679 882982 14.679 60 - 14094 0.0000 +/-0.50
SS-10 (20F0582-10RE1 )Lab File ID: G2017122.D Analyzed: 06/19/20 22:17
Bromochloromethane (1)345039 8.528 351820 8.521 60 - 14098 0.0070 +/-0.50
1,4-Difluorobenzene (1)926800 10.302 993496 10.302 60 - 14093 0.0000 +/-0.50
Chlorobenzene-d5 (1)835815 14.673 882982 14.679 60 - 14095 -0.0060 +/-0.50
SS-11 (20F0582-11RE1 )Lab File ID: G2017123.D Analyzed: 06/19/20 22:58
Bromochloromethane (1)346048 8.527 351820 8.521 60 - 14098 0.0060 +/-0.50
1,4-Difluorobenzene (1)927654 10.301 993496 10.302 60 - 14093 -0.0010 +/-0.50
Chlorobenzene-d5 (1)832466 14.673 882982 14.679 60 - 14094 -0.0060 +/-0.50
Duplicate (B260459-DUP1 )Lab File ID: G2017124.D Analyzed: 06/19/20 23:39
Bromochloromethane (1)349487 8.528 351820 8.521 60 - 14099 0.0070 +/-0.50
1,4-Difluorobenzene (1)940846 10.302 993496 10.302 60 - 14095 0.0000 +/-0.50
Chlorobenzene-d5 (1)845639 14.679 882982 14.679 60 - 14096 0.0000 +/-0.50
SS-Dup (20F0582-12RE1 )Lab File ID: G2017125.D Analyzed: 06/20/20 00:20
Bromochloromethane (1)353496 8.521 351820 8.521 60 - 140100 0.0000 +/-0.50
1,4-Difluorobenzene (1)945733 10.301 993496 10.302 60 - 14095 -0.0010 +/-0.50
Chlorobenzene-d5 (1)843488 14.673 882982 14.679 60 - 14096 -0.0060 +/-0.50
SS-5 (20F0582-05RE1 )Lab File ID: G2017131.D Analyzed: 06/20/20 08:29
Bromochloromethane (1)393835 8.521 351820 8.521 60 - 140112 0.0000 +/-0.50
1,4-Difluorobenzene (1)1039551 10.295 993496 10.302 60 - 140105 -0.0070 +/-0.50
Chlorobenzene-d5 (1)910778 14.672 882982 14.679 60 - 140103 -0.0070 +/-0.50
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S049482-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
1.121259A 36.3 *306.82 0.82266825.00Acetone
0.7831473A -5.0 304.75 0.82440025.00Benzene
0.865414A 4.8 305.24 0.82605635.00Benzyl chloride
0.609288A 9.6 305.48 0.55614585.00Bromodichloromethane
0.5555461A 20.5 306.02 0.46122335.00Bromoform
0.6361072A -0.8 304.96 0.64115985.00Bromomethane
0.5499962A 20.5 306.02 0.45644285.001,3-Butadiene
1.325387A -10.5 304.48 1.4802815.002-Butanone (MEK)
1.824651A -22.8 303.86 2.3638395.00Carbon Disulfide
0.5369387A 21.6 306.08 0.4414015.00Carbon Tetrachloride
0.821198A 0.6 305.03 0.81644235.00Chlorobenzene
0.3587585A 16.1 305.80 0.30900575.00Chloroethane
1.476777A -12.1 304.40 1.6799065.00Chloroform
0.6368636A 12.7 305.64 0.56501915.00Chloromethane
0.3288729A -11.6 304.42 0.37192755.00Cyclohexane
0.6259545A 13.4 305.67 0.55196925.00Dibromochloromethane
0.5580739A 3.3 305.16 0.54045415.001,2-Dibromoethane (EDB)
0.5797622A -4.0 304.80 0.60370175.001,2-Dichlorobenzene
0.683756A 4.4 305.22 0.65479615.001,3-Dichlorobenzene
0.6751394A 0.6 305.03 0.67080595.001,4-Dichlorobenzene
1.742063A -4.0 304.80 1.8137055.00Dichlorodifluoromethane (Freon 12)
1.218118A -17.2 304.14 1.4712475.001,1-Dichloroethane
0.9822356A 1.8 305.09 0.96489415.001,2-Dichloroethane
1.082767A -9.0 304.55 1.1896185.001,1-Dichloroethylene
0.9033499A -14.9 304.26 1.0613395.00cis-1,2-Dichloroethylene
0.9263102A -14.2 304.29 1.0791155.00trans-1,2-Dichloroethylene
0.2947209A -5.9 304.70 0.31332535.001,2-Dichloropropane
0.4804978A 3.5 305.17 0.46440925.00cis-1,3-Dichloropropene
0.4108559A 10.1 305.50 0.37331385.00trans-1,3-Dichloropropene
1.860686A 7.1 305.36 1.7373125.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.1309617A -20.0 304.00 0.16374425.001,4-Dioxane
0.1999978A 42.5 *307.12 0.14034935.00Ethanol
0.219264A -13.7 304.32 0.25402915.00Ethyl Acetate
1.364209A 2.0 305.10 1.3373675.00Ethylbenzene
1.364824A 1.5 305.08 1.3446935.004-Ethyltoluene
0.2476391A 1.6 305.08 0.24364065.00Heptane
0.3055502A -11.1 304.44 0.34366515.00Hexachlorobutadiene
0.859206A 12.1 305.60 0.8511285.00Hexane
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S049482-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.6155366A 8.3 305.42 0.56820545.002-Hexanone (MBK)
1.131475A 19.9 306.00 0.94374645.00Isopropanol
1.783388A -12.6 304.37 2.0415655.00Methyl tert-Butyl Ether (MTBE)
0.7875546A -10.5 304.48 0.87971495.00Methylene Chloride
0.6145175A 12.0 305.60 0.54861895.004-Methyl-2-pentanone (MIBK)
0.7278346A -17.6 304.12 0.88329815.00Naphthalene
0.5196346A -21.6 303.92 0.6624285.00Propene
0.7826341A 2.0 305.10 0.76762715.00Styrene
0.7707124A -2.0 304.90 0.78629065.001,1,2,2-Tetrachloroethane
0.4502554A 5.3 305.27 0.42754535.00Tetrachloroethylene
0.2747276A -21.2 303.94 0.34883345.00Tetrahydrofuran
1.054859A -1.3 304.94 1.0687755.00Toluene
0.3264348A -18.4 304.08 0.39999385.001,2,4-Trichlorobenzene
0.5408898A 13.2 305.66 0.47779075.001,1,1-Trichloroethane
0.3669467A -0.5 304.98 0.36861165.001,1,2-Trichloroethane
0.3423882A -2.8 304.86 0.35242275.00Trichloroethylene
1.729235A 17.4 305.87 1.4726645.00Trichlorofluoromethane (Freon 11)
1.354754A -17.8 304.11 1.6471355.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
1.06538A 1.2 305.06 1.0530955.001,2,4-Trimethylbenzene
1.127324A 4.7 305.24 1.0766625.001,3,5-Trimethylbenzene
2.174619A 1.5 305.08 2.1419175.00Vinyl Acetate
0.7347164A 12.7 305.63 0.65208365.00Vinyl Chloride
1.068005A 7.1 3010.7 0.996829110.0m&p-Xylene
1.104032A 8.4 305.42 1.0182835.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S049551-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.1931397A 37.6 *306.88 0.14034935.00Ethanol
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 43 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,ME,NHAcetone
AIHA,FL,NJ,NY,ME,NH,VABenzene
AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride
AIHA,NJ,NY,ME,NH,VABromodichloromethane
AIHA,NJ,NY,ME,NH,VABromoform
AIHA,FL,NJ,NY,ME,NHBromomethane
AIHA,NJ,NY,ME,NH,VA1,3-Butadiene
AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
AIHA,NJ,NY,ME,NH,VACarbon Disulfide
AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride
AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene
AIHA,FL,NJ,NY,ME,NH,VAChloroethane
AIHA,FL,NJ,NY,ME,NH,VAChloroform
AIHA,FL,NJ,NY,ME,NH,VAChloromethane
AIHA,NJ,NY,ME,NH,VACyclohexane
AIHA,NY,ME,NHDibromochloromethane
AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
AIHA,NY,ME,NHtrans-1,3-Dichloropropene
AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,ME,NH,VA1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,ME,NH,VAHeptane
AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene
AIHA,FL,NJ,NY,ME,NH,VAHexane
AIHA2-Hexanone (MBK)
AIHA,NY,ME,NHIsopropanol
AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride
AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
AIHAPropene
AIHA,FL,NJ,NY,ME,NH,VAStyrene
AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
Page 44 of 49
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,ME,NH,VAToluene
AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene
AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride
AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene
AIHA,FL,NJ,NY,ME,NH,VAo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2021
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2021
LAO00112Rhode Island Department of HealthRI 12/30/2020
652North Carolina Div. of Water QualityNC 12/31/2020
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2021
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2021
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2021
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Appendix C

Groundwater & Surface Water Sampling Forms
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record/DVW8SGDWHG://201Job No:Well ID:Water Volume Pumping DOTemp. S. Cond. pHORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/FDP-058Former Durafiber Technologies FacilitySalisbury,NC6/10/20669.2630.0017.25HHM2780F, scattered rain showersPumpremovedprior to sampling12:4012:4512:5012:5513:0013:0513:1013:2013:2513:3013:3513:4017.2517.2617.2617.2617.2617.2617.2617.2617.2617.2617.2617.260.0 mL2.25 L4.5 L8.25 L150 mL/min1501501501501501501501501501501503.231.580.920.910.950.820.780.760.620.780.720.7119.619.819.819.419.819.819.919.919.920.019.619.6293.3294.1295.3294.2295.8293.2293.4293.0290.9290.0290.26.476.366.296.216.186.176.156.156.156.156.156.1542.822.111.1-7.7-15.4-15.8-15.3-16.3-18.2-20.1-20.4-21.2109.0078.1028.2035.1048.9032.0028.0029.1026.2012.20YSI Pro Plus & Hach 2100QHexavalent chromium(lab required)VOCs(8260)-x3VOAs(HCl); SVOCs(8270)- x2 100mL Amber(unpres); Metals(6020/7470)- x1 250mLplastic(HNO3)Hexavalent chromium(7199)-x150mLplastic(HNO3)PeristalticPVC2-inch13:45Pace AnalyticalR-30NA2530Polyethylene bgs290.0
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record/DVW8SGDWHG://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/FDP-058Former Durafiber Technologies FacilitySalisbury,NC6/10/20868.7358.0015.91HHM83F, scattered rain showersStatedpurge at 15:35 - elevated turbidityduringinitialpurge; Dedicated submersiblepumpwas not removedprior to sampling15:5516:0016:0516:1016:1516:2017.8217.8217.8217.8217.8517.882.5 L5L125 mL/min1251251251251250.210.220.220.250.230.2124.125.425.525.024.924.7946.0957.0957.0955.0955.0955.06.166.206.206.216.226.22-82.5-83.5-84.1-83.5-83.4-83.05.309.952.332.103.913.91YSI Pro Plus & Hach 2100QHexavalent chromium(lab required)VOCs(8260)-x3VOAs(HCl); SVOCs(8270)- x2 100mL Amber(unpres); Metals(6020/7470)- x1 250mLplastic(HNO3)Hexavalent chromium(7199)-x150mLplastic(HNO3)PeristalticStainless Steel2-inch16:30Pace AnalyticalS-58NA5358Polyethylene bgs
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record/DVW8SGDWHG://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/FDP-058Former Durafiber Technologies FacilitySalisbury,NC6/10/20683.9890.0016.58MRV8280 F, sunnyOdorTubingset on topof dedicated submersiblepump; left wellpumpingat 14:00 to set tubingin other wells while turbiditydrops(returned at 15:05)12:5513:0013:0513:1013:2013:3013:4013:5014:0015:0515:1015:1516.5816.5816.5816.5816.5816.5816.5816.5816.5816.5816.5816.580.0 L0.81.62.43.23.75.25.76.212.713.213.7160 mL/min1601601601001001001001001001001004.860.890.520.400.350.190.170.170.140.130.120.1121.823.923.923.624.322.723.423.924.323.823.023.13,240.03,193.03,197.03,198.03,263.03,297.03,301.03,328.03,355.03,333.03,335.04.294.394.384.394.414.474.484.504.524.554.554.55111.3113.0105.1105.1102.389.097.698.798.1102.699.3100.2141.40107.6089.6086.50162.00189.0085.0078.9067.8020.8016.5214.89Turbidityat 9.0 NTU at time of metals samplingYSI Pro Plus & Hach 2100QHexavalent chromium(lab required)VOCs(8260)-x3VOAs(HCl); SVOCs(8270)- x2 100mL Amber(unpres); Metals(6020/7470)- x1 250mLplastic(HNO3)Hexavalent chromium(7199)-x150mLplastic(HNO3)PeristalticStainless Steel2-inch15:15Pace AnalyticalZ-90NA8090Polyethylene bgs3,347.0
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record/DVW8SGDWHG://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/FDP-058Former Durafiber Technologies FacilitySalisbury,NC6/10/20696.0440.0014.31MRV3883F, scattered rain showersPumpremovedprior to sampling; ORP sensor disfunctional startingat 16:10, unable to calibrate15:5015:5516:0016:1016:2016:3516:4016:4515.0515.5615.8516.4816.9017.0117.0317.030.0 L0.51.02.03.04.04.55.0100 mL/min1001001001001001001005.694.143.762.712.732.112.062.0723.022.823.423.323.123.323.523.4180.5159.7158.0157.6156.8156.0155.4155.26.486.576.586.476.306.266.276.2966.060.359.91,494.01,410.01,400.01,369.21,250.079.2265.4061.5755.7028.5716.806.656.52YSI Pro Plus & Hach 2100QHexavalent chromium(lab required)VOCs(8260)-x3VOAs(HCl); SVOCs(8270)- x2 100mL Amber(unpres); Metals(6020/7470)- x1 250mLplastic(HNO3)Hexavalent chromium(7199)-x150mLplastic(HNO3)PeristalticStainless Steel2-inch16:45Pace AnalyticalDD-40NA3540Polyethylene bgs
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record/DVW8SGDWHG://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/FDP-058Former Durafiber Technologies FacilitySalisbury,NC6/10/20715.0443.0031.25MRV4180 F, mostly sunnyRemoved pump on 6/9/2010:3010:3510:4010:4510:5010:5511:0011:1011:1531.2731.2731.2731.2731.2731.2731.2731.2731.270.0 L0.51.01.52.02.53.03.54.0100 mL/min1001001001001001001001004.733.563.683.423.713.473.363.173.0924.024.524.725.425.426.127.128.227.1211.3211.1212.1210.6211.6207.7209.1210.1209.85.775.705.725.755.785.765.795.805.7759.362.663.763.263.865.164.765.165.141.8331.5818.8424.8520.5814.2012.809.899.76YSI Pro Plus & Hach 2100QHexavalent chromium(lab required)VOCs(8260)-x3VOAs(HCl); SVOCs(8270)- x2 100mL Amber(unpres); Metals(6020/7470)- x1 250mLplastic(HNO3)Hexavalent chromium(7199)-x150mLplastic(HNO3)PeristalticStainless Steel2-inch11:15Pace AnalyticalGG-43NA3843Polyethylene bgs
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(S/cm)(SU)(mV)(NTU)Stabilization CriteriaLOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________ Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: ) Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name: Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________ Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________Type of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________ NOTES:R SAMPLING PARAMETERS
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record/DVW8SGDWHG://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/FDP-058Former Durafiber Technologies FacilitySalisbury,NC6/10/20663.3034.0010.82HHM2780F, sunnyDedicated submersiblepumpremovedprior to sampling08:4508:5008:5509:0009:0509:1009:1509:2011.6212.0012.0212.0412.0612.0612.0612.080.0 mL2.25 L4.5 L170 mL/min1501501501501501501503.923.984.004.024.003.923.903.9319.219.519.820.020.019.920.220.2133.5133.6133.7133.0132.9132.6132.6133.05.355.155.115.035.035.035.035.03125.0133.5132.5128.9128.4127.7132.1130.741.5020.2017.6014.4013.7012.6011.3010.20YSI Pro Plus & Hach 2100QHexavalent chromium(lab required)VOCs(8260)-x3VOAs(HCl); SVOCs(8270)- x2 100mL Amber(unpres); Metals(6020/7470)- x1 250mLplastic(HNO3)Hexavalent chromium(7199)-x150mLplastic(HNO3)PeristalticPVC2-inch09:25Pace AnalyticalTT-34NA2434Polyethylene bgs
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record/DVW8SGDWHG://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/FDP-058Former Durafiber Technologies FacilitySalisbury,NC6/10/20668.3837.0017.21HHM3080 F, sunnyNopumpin the well - flush mount well locatedin the roadway10:5511:0011:0511:1011:1511:2011:2511:3011:3511:4011:4517.7417.7417.7417.7617.7617.7617.7717.7717.7717.7717.780.0 mL7501.5L4.57.5150 mL/min1501501501501501501501501501500.210.480.430.400.390.260.240.230.250.260.2719.920.420.420.020.020.020.020.020.120.020.1762.0762.0769.0772.0773.0772.0777.0782.0773.0771.06.136.146.136.156.156.166.166.166.176.186.182.852.2-28.2-33.7-36.8-38.2-37.9-38.9-38.1-38.0-37.8122.0083.9060.3054.6043.8044.2039.1032.0023.0019.8012.70Turbidityat 9.0 NTU at time of metals samplingYSI Pro Plus & Hach 2100QHexavalent chromium(lab required)VOCs(8260)-x3VOAs(HCl); SVOCs(8270)- x2 100mL Amber(unpres); Metals(6020/7470)- x1 250mLplastic(HNO3)Hexavalent chromium(7199)-x150mLplastic(HNO3)PeristalticPVC2-inch11:55Pace AnalyticalYY-37NA2737Polyethylene bgs769.0
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)LOH6:6DPSOLQJ/RJ6:)RUP
'DWH
FDP-058 SW-4 & SW-DUP 06/09/20
Former Durafiber Technologies Facility Salisbury, NC
Poly
✔
✔
✔
~20 feet NM
14:45 6.73 26.6 146.1 105.4 29.0
✔
✔
Sunny, 80s
VOCs (8260) - x3 VOAs (HCl); SVOCs (8270) - x2 100mL Amber (unpres);
Metals (6020/7470) - x1 250mL plastic (HNO3); Hexavalent chromium (7199) - x1 50 mL plastic (HNO3)
Field filtered hexavalent chromium per EPA Method.
HHM 6/9/20 14:45

Appendix D

DEQ Risk Calculators
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Site Wide Sub-Slab Soil Vapor - Hypothetical Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
Salisbury Investments
7401 Statesville Boulevard, Salisbury, Rowan County
Division of Waste Management - Brownfields Program
22030-18-080
December 2019
November 2019 EPA RSL Table
Prepared By:Matt Vawter
Ralph McGee, PG
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: 22030-18-080
Exposure Unit ID: Site Wide Sub-Slab Soil Vapor - Hypothetical Worst Case
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration to Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: 22030-18-080
Exposure Unit ID: Site Wide Sub-Slab Soil Vapor - Hypothetical Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: December 2019Basis: November 2019 EPA RSL TableSite ID: 22030-18-080Exposure Unit ID: Site Wide Sub-Slab Soil Vapor - Hypothetical Worst Case Description of Exposure Point Concentration Selection:Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.Exposure Point Concentration (ug/m3)Notes: CAS Number ChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion460SS-1067-64-1 Acetoneug/m31SS-171-43-2 Benzeneug/m35.9SS-175-15-0 Carbon Disulfideug/m30.83SS-156-23-5 Carbon Tetrachlorideug/m34.8SS-767-66-3 Chloroformug/m33.1SS-175-71-8 Dichlorodifluoromethaneug/m317SS-175-34-3 Dichloroethane, 1,1-ug/m3210SS-175-35-4 Dichloroethylene, 1,1-ug/m31SS-7156-59-2 Dichloroethylene, 1,2-cis-ug/m312SS-1141-78-6 Ethyl Acetateug/m32.4SS-11100-41-4 Ethylbenzeneug/m39.1SS-7109-99-9 ~Tetrahydrofuranug/m31.1SS-11142-82-5 Heptane, N-ug/m315SS-10591-78-6 Hexanone, 2-ug/m3220SS-267-63-0 Isopropanolug/m360SS-1078-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m334SS-11108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m38.4SS-175-09-2 Methylene Chlorideug/m39.2SS-1191-20-3 ~Naphthaleneug/m32.4SS-11100-42-5 Styreneug/m3610SS-4127-18-4 Tetrachloroethyleneug/m37.4SS-11108-88-3 Tolueneug/m33.8SS-1076-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-ug/m313SS-271-55-6 Trichloroethane, 1,1,1-ug/m317SS-179-01-6 Trichloroethyleneug/m33.6SS-175-69-4 Trichlorofluoromethaneug/m325SS-1195-63-6 Trimethylbenzene, 1,2,4-ug/m312SS-11108-67-8 Trimethylbenzene, 1,3,5-ug/m328.1SS-111330-20-7 Xylenesug/m3Input Form 2DSoil Gas Exposure Point Concentration TableNorth Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: 22030-18-080
Exposure Unit ID: Site Wide Sub-Slab Soil Vapor - Hypothetical Worst Case
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use* NC NC NC
Soil NC NC NC
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 5.7E-07 7.0E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: December 2019
Basis: November 2019 EPA RSL Table
Site ID: 22030-18-080
Exposure Unit ID: Site Wide Sub-Slab Soil Vapor - Hypothetical Worst Case
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 460 4.6 - 2.7E+04 3.4E-05
71-43-2 Benzene 1 0.01 1.6E+00 2.6E+01 6.4E-09 7.6E-05
75-15-0 Carbon Disulfide 5.9 0.059 - 6.1E+02 1.9E-05
56-23-5 Carbon Tetrachloride 0.83 0.0083 2.0E+00 8.8E+01 4.1E-09 1.9E-05
67-66-3 Chloroform 4.8 0.048 5.3E-01 8.6E+01 9.0E-08 1.1E-04
75-71-8 Dichlorodifluoromethane 3.1 0.031 - 8.8E+01 7.1E-05
75-34-3 Dichloroethane, 1,1- 17 0.17 7.7E+00 - 2.2E-08
75-35-4 Dichloroethylene, 1,1- 210 2.1 - 1.8E+02 2.4E-03
156-59-2 Dichloroethylene, 1,2-cis- 1 0.01 - -
141-78-6 Ethyl Acetate 12 0.12 - 6.1E+01 3.9E-04
100-41-4 Ethylbenzene 2.4 0.024 4.9E+00 8.8E+02 4.9E-09 5.5E-06
109-99-9 ~Tetrahydrofuran 9.1 0.091 - 1.8E+03 1.0E-05
142-82-5 Heptane, N- 1.1 0.011 - 3.5E+02 6.3E-06
591-78-6 Hexanone, 2- 15 0.15 - 2.6E+01 1.1E-03
67-63-0 Isopropanol 220 2.2 - 1.8E+02 2.5E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone) 60 0.6 - 4.4E+03 2.7E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 34 0.34 - 2.6E+03 2.6E-05
75-09-2 Methylene Chloride 8.4 0.084 1.2E+03 5.3E+02 6.8E-11 3.2E-05
91-20-3 ~Naphthalene 9.2 0.092 3.6E-01 2.6E+00 2.6E-07 7.0E-03
100-42-5 Styrene 2.4 0.024 - 8.8E+02 5.5E-06
127-18-4 Tetrachloroethylene 610 6.1 4.7E+01 3.5E+01 1.3E-07 3.5E-02
108-88-3 Toluene 7.4 0.074 - 4.4E+03 3.4E-06
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 3.8 0.038 - 4.4E+03 1.7E-06
71-55-6 Trichloroethane, 1,1,1- 13 0.13 - 4.4E+03 5.9E-06
79-01-6 Trichloroethylene 17 0.17 3.0E+00 1.8E+00 5.7E-08 1.9E-02
75-69-4 Trichlorofluoromethane 3.6 0.036 - -
95-63-6 Trimethylbenzene, 1,2,4- 25 0.25 - 5.3E+01 9.5E-04
108-67-8 Trimethylbenzene, 1,3,5- 12 0.12 - 5.3E+01 4.6E-04
1330-20-7 Xylenes 28.1 0.281 - 8.8E+01 6.4E-04
Cumulative: 5.7E-07 7.0E-02
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator