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HomeMy WebLinkAbout22047_University Place Mall_DC680002_202010924_SG and GW ReportAECOM AECOM Technical Services of North Carolina, Inc. 919.461.1100 tel 1600 Perimeter Park Drive, Suite 400 919.461.1415 fax Morrisville, NC 27560 September 24, 2020 North Carolina Department of Environmental Quality Division of Waste Management — DSCA Program 1646 Mail Service Center Raleigh, NC 27699 Att: Mr. Mike Cunningham DSCA Project Manager Re: Soil Gas and Groundwater Sampling Report American Dry Cleaners DSCA Site ID #DC680002 201 South Estes Drive, Chapel Hill, Orange County, North Carolina Dear Mr. Cunningham: AECOM Technical Services of North Carolina, Inc. (includes legacy URS and legacy AECOM herein referred to as AECOM) is pleased to provide the attached Soil Gas and Groundwater Sampling Report for the American Dry Cleaners (#DC680002) site located at 201 South Estes Drive, Chapel Hill, North Carolina. This report includes documentation pertaining to the soil gas and limited groundwater sampling activities that were completed at the site in June and August 2020. The activities documented herein were completed in accordance with State Lead Authorization for Work (SLAW) 029, as approved on March 9, 2020. Assessment activities at the American Dry Cleaners site have identified groundwater contaminated with dry cleaning solvents (primarily tetrachloroethene [PCE] and associated breakdown products) that is migrating offsite to the east-southeast and beneath the Olin T. Binkley Baptist Church property. Soil gas assessment activities completed on the Olin T. Binkley Baptist Church property indicate contaminant concentrations exceeding the calculated soil gas to indoor air vapor intrusion risk levels. Based on the potential for vapor intrusion to affect indoor air quality due to groundwater and soil gas contaminant concentrations, indoor air samples have been collected in select preschool classrooms located in the education wing at the Olin T. Binkley Baptist Church since 2010, including: • June 2015 and January 2016 - Results of Indoor Air Sampling, dated February 2016; • June 2016 - Results of Indoor Air Sampling, dated July 2016; • December 2016 - Groundwater and Vapor Monitoring Report, dated January 2017; • June and December 2017 - Indoor Air and Soil Gas Sampling Report, dated January 2018; • June 2018, June and December 2018, January and February 2019 - Indoor Air, Soil Gas, and Groundwater Sampling Report, dated March 2019; • June 2019 - Indoor Air and Soil Gas Sampling Report, dated July 2019 and Updated Risk Calculator for the June 2019 Indoor Air Sampling Event letter, dated September 2019; and • December 2019 - Indoor Air, Soil Gas, and Ductwork Air Sampling Report, dated January 2020. As referenced in the above listed documents, indoor air results from each of the sampling events collected through December 2019 were within acceptable risk levels given current residential land use based on the presence of a church and daycare/preschool facility. AECOM Mr. Mike Cunningham American Dry Cleaners DC680002 September 24, 2020 Page 2 of 4 As part of vapor intrusion sampling activities, soil gas samples have been collected from permanent soil gas sample points SV-5 and SV-6R which are located in close proximity to the Olin T. Binkley Church preschool wing. However, during the most recent sampling event completed in December 2019, soil gas sampling point SV-6R could not be sampled due to the presence of water in the soil gas sample point. As the integrity of soil gas sampling point SV-6R has likely been affected by seepage of stormwater runoff around the seal within the annular space of the soil gas point, AECOM proposed to replace this soil gas sampling point in a fresh borehole in close proximity to soil gas sampling point SV-6R. Additionally, AECOM proposed to install three additional soil gas sampling points (SV-7, SV-8, and SV-9) to further evaluate potential vapor intrusion to affect indoor air quality in the portion of the church to the east of the education wing. Additionally, as many of the monitoring wells have not been sampled since 2013, AECOM proposed the collection of groundwater samples from six monitoring wells (MW-1, MW-3, MW-5, 2W-10, 2W-11, and 2W-12) located on the Olin T. Binkley Church property to further monitor plume stability and groundwater contaminant dynamics. On June 10, 2020, AECOM performed a limited groundwater sampling event pursuant to work authorized under SLAW029, dated March 9, 2020. Groundwater sampling was completed using standard purge and sample techniques using a disposable bailer, in accordance with the attached groundwater sampling SOP (Attachment 19). Groundwater samples were submitted to Pace Analytical Laboratory on June 10, 2020 for analysis of volatile organic compounds (VOCs) by Method 8260. An updated potentiometric surface contour map using depth to water levels gauged on June 6, 2020, is included as Attachment 6. Groundwater flow is to the southeast, which is consistent with historic groundwater flow data. Laboratory analysis of the groundwater samples indicated the presence of CVOCs above NC 2L Groundwater Quality Standards in monitoring wells MW-1, MW- 3, MW-5, 2W-10, 2W-11, and 2W-12. A groundwater quality summary map is included as Attachment 7. Groundwater analytical data is summarized in ADT Table 8. Groundwater -to - Indoor Air Risk Calculators are included in Attachment 16. According to the Mann -Kendall Trend Analysis worksheets, included in Attachment 17, concentrations of PCE are stable in monitoring well MW-3 and decreasing in monitoring wells 2W- 10 and 2W-11. Additionally, concentrations of TCE are decreasing in 2W-10 and demonstrate no trend in MW-3 and 2W-11. Soil gas quality monitoring has been occurring on the Olin T. Binkley Church property concurrent with the indoor air quality monitoring discussed in Section 2.0. Historical soil gas quality data has indicated the potential for vapor intrusion to affect indoor air quality above acceptable risk levels for residential and non-residential exposure. However, subsequent ongoing monitoring of indoor air quality, as discussed in section 2.0, has indicated that indoor air quality remains within acceptable levels for current property usage. As part of the continued monitoring of soil gas quality, AECOM collected a soil gas sample from soil gas monitoring point SV-5 on August 11, 2020. As previously documented a sample was not recently collected from soil gas sampling point SV-6R due to the presence of water inside the sample point and the sample point was considered to be damaged. Therefore, on August 11, 2020 a replacement sampling point (SV-6RR) was installed in the same location as SV-6R. Additionally, three soil gas points (SV-7, SV-8, and SV-9) were installed on August 11, 2020 along the western portion of the main church building. The newly installed soil gas sampling points were completed within a steel manhole with an approximate 18-inch square concrete pad at ground surface. Soil gas sampling points were installed in accordance with the attached soil gas installation SOP (Attachment 20). A=COM Mr. Mike Cunningham American Dry Cleaners DC680002 September 24, 2020 Page 3 of 4 Soil gas samples were collected from the five soil gas sampling points (SV-5, SV-6RR, SV-7, SV-8, and SV-9) into 6-liter summa canisters fitted with a 30-minute flow controller in accordance with the attached AECOM soil gas sampling SOP (Attachment 20). Each sample was analyzed for five DSCA contaminants of concern: PCE, TCE, cis-1,2-DCE, trans-1,2-DCE, and vinyl chloride using EPA Method TO-15. Sampling results and locations are shown on Attachment 14. A summary of the soil gas quality results, as entered into August 2019 DSCA risk calculators for both residential and non-residential exposure, is provided as follows: • SV-5 (8/11/20) — non-residential worker o Acceptable cumulative carcinogenic risk between 1E-04 and 1 E-05 (3.3E-05); and, o Unacceptable hazard index is greater than 1 (11). • SV-5 (8/11/20) - resident o Acceptable cumulative carcinogenic risk between 1 E-03 and 1 E-04 (1.7E-04); and, o Unacceptable hazard index is greater than 1 (42). • SV-6RR (8/11/20) — non-residential worker o Acceptable cumulative carcinogenic risk between 1 E-05 and 1 E-06 (3.2E-06); and, o Acceptable hazard index is less than 1 (0.96). • SV-6RR (8/11/20) - resident o Acceptable cumulative carcinogenic risk between 1 E-04 and 1 E-05 (4.9E-05); and, o Unacceptable hazard index is greater than 1 (12). • SV-7 (8/11/20) — non-residential worker o Acceptable cumulative carcinogenic risk less than 1E-06 (1.3E-09); and, o Acceptable hazard index is less than 1 (0.00035). • SV-7 (8/11/20) - resident o Acceptable cumulative carcinogenic risk less than 1 E-06 (1.7E-08); and, o Acceptable hazard index is less than 1 (0.0045). • SV-8 (8/11/20) — non-residential worker o No contaminants were detected above laboratory detection limits. • SV-8 (8/11/20) - resident o No contaminants were detected above laboratory detection limits. • SV-9 (8/11/20) — non-residential worker o Acceptable cumulative carcinogenic risk less than 1E-06 (7.9E-09); and, o Acceptable hazard index is less than 1 (0.0026). • SV-9 (8/11/20) - resident o Acceptable cumulative carcinogenic risk less than 1 E-06 (1.4E-07); and, o Acceptable hazard index is less than 1 (0.032). As indicated on Attachment 14, soil gas contaminant concentrations in SV-5 and SV-6RR continue to indicate a potential for vapor intrusion to affect indoor air quality above calculated risk levels for AECOM Mr. Mike Cunningham American Dry Cleaners DC680002 September 24, 2020 Page 4 of 4 both residential and non-residential exposure. Soil gas sampling results for SV-7, SV-8, and SV-9 indicate acceptable risk levels for both residential and non-residential exposure. Soil gas data is summarized in Analytical Data Table 4. Soil gas laboratory data is included as Attachment 15. DSCA soil gas risk calculators for residential and non-residential use are provided as Attachment 16. The results of the June 2020 limited groundwater sampling event indicate the contaminant plume is generally stable beneath the Olin T. Binkley Church property. Calculated vapor intrusion exposure risks associated with groundwater quality data collected from monitoring wells MW-3, 2W-10, 2W- 11, and 2W-12 exceed acceptable risk levels for both residential and non-residential use. The groundwater contaminant plume extends to monitoring well MW-1 located near the southern property boundary of the church downgradient from the American Dry Cleaners location. Soil gas quality data for samples SV-5 and SV-6RR exceed calculated acceptable vapor intrusion risk levels for residential use. Soil gas quality data for sample SV-5 exceeds calculated acceptable vapor intrusion risk levels for non-residential use. Soil gas quality data from the newly installed soil gas sampling points SV-7, SV-8, and SV-9 indicate acceptable vapor intrusion risk levels for both residential and non-residential use. During the time of this scope of work, indoor air and duct samples were not able to be collected due to access restrictions to the church building in association with Covid-19. Future indoor air and duct samples will be collected once normal operations resume with the preschool at the Olin T. Binkley Church. The work was done in accordance with AECOM Contract N16004, dated January 3, 2017, and in accordance with the scope and estimates provided in the approved SLAW029. If you have any questions or require additional information, please do not hesitate to call either Rob MacWilliams at 704-499-4839 or Nick Shore at 919-461-1485. Sincerely, AECOM TECHNICAL SERVICES OF NORTH CAROLINA, INC. Nick Shore, PG Project Manager Enclosures Robert H. MacWilliams, PG Program Manager ANALYTICAL DATA TABLES Analytical Data Tables for North Carolina Dry -Cleaning Solvent Cleanup Act Program Facility Name: American Dry Cleaners 201 South Estes Drive, Chapel Hill, Orange County DSCA ID No.: DC680002 Submittal Date: September 2020 Prepared By: AECOM Technical Services of North Carolina, Inc. 1600 Perimeter Park Drive, Suite 400, Morrisville, North Carolina Table of Contents DSCA ID No.: DC680002 Table/ Att. No. Description Check box if included Tables Table 1 Site Chronology ❑ Table 2 Analytical Data for Soil ❑ Table 3 Analytical Data for Sub -slab Gas ❑ Table 4 Analytical Data for Soil Gas ❑ Table 5 Analytical Data for Indoor and Outdoor Air ❑ Table 6 Monitoring Well Construction Data El Table 7 Groundwater Elevation Data El Table 8 Analytical Data for Groundwater El Table 9 Analytical Data for Surface Water ❑ Table 10 Water Well(s) Survey Data ❑ Table 11 Analytical Data for Water Supply Well(s) ❑ Table 12 Analytical Data for Natural Attenuation Parameters ❑ Attachments Att. 1 Site map showing location(s) of soil boring(s). ❑ Att2 Soil contaminant concentration maps showing the concentration at each sampling point. ❑ Att. 3 Soil isoconcentration maps. ❑ Att. 4 Site map showing location(s) of monitoring well(s). ❑ Att. 5 Well completion diagrams and records of construction submitted to state. ❑ Att. 6 Groundwater gradient map for each sampling event. 0 Att. 7 PCE concentration map showing the concentration at each sampling point and isoconcentration map. However, if there are significant plumes for other dry- cleaning contaminants, contaminant concentration maps for each chemical of concern should be included. 0 Att. 8 Groundwater concentration trend plots. ❑ Att. 9 Map showing location(s) of surface water sample(s) (if applicable). ❑ Att. 10 Surface water concentration map showing the concentration at each sampling point (if applicable). El Att. 11 USGS Quad map with plotted water well location(s) within the 1,500 foot and 0.5 mile radii of the site (if applicable). ❑ Att. 12 Site map showing location(s) of monitoring well(s) for natural attenuation parametc ❑ Att. 13 Site map showing location(s) of indoor air, outdoor air, or soil gas samples. ❑ Att. 14 Air and soil gas concentration map showing the concentration at each sampling point. El Att.15 Signed laboratory analytical reports including chain -of custody and quality assurance/quality control (QA/QC) documentation (only if not previously submitted). 0 Att. 16 DSCA Program Risk Calculators p Att. 17 Mann -Kendall Trend Analysis El Att. 18 IDW Disposal Manifest El Att. 19 SOP - Groundwater Sampling Using Disposable Bailers El Att. 20 SOP - Soil Gas Sampling El Att. 21 ❑ Note: 1. All maps must include a bar scale, north arrow, site name, DSCA ID No., and date. Table 1: Site Chronology DSCA ID No.: DC680002 Chronology of Events Date Instructions: Brief description of all significant events that have occurred since a problem was suspected at the facility. Commence with the first date a problem was suspected and continue through the most recent activity described in the current report. 04/01/95 Chlorinated compounds detected by Withers & Ravenel (W&R) during removal and closure of Underground Storage Tanks. 05/01/95 W&R complete preliminary investigation, install one monitoring well at the site. 08/08/95 W&R conduct Phase II Investigation, install eight monitoring wells as the site. 02/01/96 W&R complete Phase III Investigation, excavating a total of 400 cubic yards of contaminated soil. 12/06/07 ECS Carolinas, LLP conduct groundwater assessment. 07/10/08 W&R sampled existing wells and prepared Prioritization Assessment Report. 10/22/08 W&R installed five off -site monitoring wells on neighboring Olin T. Binkley Church property. Report on this date documents these activities. 02/17/09 W&R authorized to conduct aggressive fluid vapor recovery event. Report on this date documents these activities and result of post AFVR groundwater monitoring. Site placed in quarterly monitoring by DSCA program. 04/17/09 Second AFVR event authorized and post event groundwater monitoring documented in report issued on this date. 08/04/09 Groundwater monitoring report submitted to DSCA. 11/11/09 Third AFVR event authorized and post event groundwater monitoring documented in report issued on this date. 02/19/09 Groundwater monitoring report submitted to DSCA. 04/15/10 Fourth AFVR event authorized and post event groundwater monitoring documented in report issued on this date. 05/27/10 Outdoor air, indoor air and sub slab vapor sampling on church property documented in report issued on this date. 08/17/10 First semi-annual indoor air monitoring event at church documented in report issued on this date. 09/14/10 Groundwater monitoring report submitted to DSCA. 12/01/10 Fifth AFVR event authorized and post event groundwater monitoring documented in report issued on this date. 02/21/11 Groundwater monitoring report submitted to DSCA. 02/23/11 Second semi-annual indoor air monitoring event at church documented in report issued on this date. 03/08/11 Soil vapor sampling report for Harris Teeter property to the west. 06/09/11 W&R completes underground injection control permit application to inject Adventus product EHC, and receives UIC permit to conduct pilot test. 06/13/11 Groundwater monitoring report submitted to DSCA. 06/30/11 Indoor air sampling at Harris Teeter documented in report issued on this date. O1/07/12 Draft injection pilot test (three month post injection) issued on this date. 11/07/12 One-year post injection pilot test report issued on this date. 04/15/13 W&R conducts hydrogeological study to find permeable saturated zone for injection on church property. Bedrock was encountered above the surficial water table at most geoprobe drilling locations, which would preclude use of geoprobe to do injection. Report issued on this date documents the study and findings. 09/24/13 End of W&R involvement in project due to expiration of contract. 11/12/13 Groundwater Sampling Event, conducted by AECOM. 12/6/13 - 12/13/13 Indoor/Outdoor Air Sampling Event, Conducted by AECOM. Page 1 of 2 Table 1: Site Chronology DSCA ID No.: DC680002 Chronology of Events Instructions: Brief description of all significant events that have occurred since a problem was Date suspected at the facility. Commence with the first date a problem was suspected and continue through the most recent activity described in the current report. 02/07/14 Groundwater Sampling Event, conducted by AECOM. 06/27/14 Installation of 4 groundwater monitoring wells 2W-9, 2W-10, 2W-11, and 2W-12 07/08/14 Groundwater Sampling Event, conducted by AECOM. 08/22/14 Soil gas sampling event, conducted by AECOM 03/19/15 Indoor Air Sampling Event, conducted by AECOM 06/17/15 Indoor Air Sampling Event, conducted by AECOM 1 1/23/15 Groundwater samples collected from wells MW-2, MW-3, 2W-4, 2W-5, 2W-9, 2W-10, 2W-11, and 2W-12. O1/11/16 Indoor Air Sampling Event, conducted by AECOM 06/06/16 Indoor Air Sampling Event, conducted by AECOM Indoor Air (IA-2 and IA-3), Soil Vapor (SV-5 and SV-6), and Groundwater Sampling (MW-2, 2W-9, 2W-10, and 2W- 12/12/16 11) Event, conducted by URS. Two new soil vapor points (SV-5 and SV-6) were installed in the playground area of the Olin T. Binkley Memorial Church. 6/20/17 - Indoor Air (IA-2 and IA-3) and Soil Vapor (SV-5 and SV-6) sampling event was conducted by AECOM. 6/28/17 12/12/17 - Indoor Air (IA-2 and IA-3) and Soil Vapor (SV-5 and SV-6) sampling event was conducted by AECOM. 12/18/17 06/08/18 - Indoor Air (IA-2 and IA-3) and Soil Vapor (SV-5) sampling event was conducted by AECOM. Soil vapor sampling 06/15/18 point SV-6 had moisture in tubing and was not able to be sampled. 12/19/18 A soil vapor (SV-5) and limited groundwater sampling event of four wells (MW-2, 2W-9, 2W-10, and 2W-11) was conducted by AECOM. Soil vapor sampling point SV-6 had moisture in tubing and was not able to be sampled. 12/14/18 - Indoor Air (IA-2 and IA-3) and Soil Vapor (SV-5) sampling event was conducted by AECOM. 12/21/18 01/11/19 - Confirmatory 7-day indoor air samples (IA-2 and IA-3) were collected via Radiello samplers, and samples (IA-2[8-hr] O1/18/19 and IA-3[8-hr]) were collected via 6-liter summa canisters on January 11, 2019. '02/08/19 - Confirmatory 7-day indoor air samples (IA-2 and IA-3) were collected via Radiello samplersby AECOM. 02/15/19 02/14/19 Damaged monitoring well 2W-8 was abandoned by an NC Licensed Drilling contractor. 06/07/19 - Indoor Air (IA-2 and IA-3) and Soil Vapor (SV-5 and SV-6r) sampling event was conducted by AECOM. 06/14/19 AECOM collected indoor air samples (IA-2, IA-3, and IA-7 through IA-13), subslab soil gas samples (SSV-1 through 12/14/19 SSV-3), soil gas sample (SV-5), and duct samples (Duct-1 and Duct-2) from within the preschool wing of the Olin T. Binkley Memorial Church. 06/10/20 AECOM completed a limited groundwater sampling event. Monitoring wells sampled included: MW-1, MW-3, MW-5, 2W-10, 2W-11, and 2W-12. 08/11/20 AECOM installed soil gas sampling points SV-6rr, SV-7, SV-8, and SV-9 at the Olin T Binkley Memorial Church. Soil gas samples SV-5, SV-6rr, SV-7, SV-8, and SV-9 were collected. Page 2 of 2 Table 4: Analytical Data for Soil Gas DSCA ID No.: DC680002 N 0 ' y U N N A N O O N A i O iL p iL iL Q� U W O N Q In/m3] SV-1 4 0.5h 03/01/11 NA 31.3 NA NA NA 361 NA <1.3 147 13.8 NA NA SV-2 4 0.5h 03/01/11 NA <1.5 NA NA NA <2.5 NA <1.5 <2.0 <0.94 NA NA SV-3 4 0.5h 03/01/11 NA <1.4 NA NA NA 16.9 NA <1.4 1.8 <0.87 NA NA SV-4 3 0.5h 03/01/11 NA 1.6 NA NA NA <1.4 NA 10.1 5.5 <0.87 NA NA 7 0.5h 12/12/16 NA 16,000 NA NA NA 150,000 NA 410 35,000 1 <5.1 NA NA 7 0.5 h 06/28/17 NA 9,740 NA NA NA 75,800 NA 347 24,900 <10.2 NA NA 7 0.5 h 12/12/17 NA 11,000 NA NA NA 86,000 NA 260 23,000 <5.1 NA NA S V-5 7 0.5 h 06/15/18 NA 18,000 NA NA NA 140,000 NA 480 40,000 <51 NA NA 7 0.5 h 12/19/18 NA 9,800 NA NA NA 120,000 NA 390 24,000 <38 NA NA 7 0.5 h 06/14/19 NA 6,000 NA NA NA 93,000 NA 320 18,000 <38 NA NA 7 0.5 h 12/14/19 NA 5,600 NA NA NA 51,000 NA 230 9,600 <5.1 NA NA 7 0.5 h 08/11/20 NA 1,400 NA NA NA 45,000 NA 140 7,000 <38 NA NA 7 0.5h 12/12/16 NA 880 NA NA NA 31,000 NA 1 190 4,800 <5.1 NA NA SV-6 7 0.5 h 06/28/17 NA 262 NA NA NA 3,850 NA 154 484 <1.02 NA NA 7 0.5 h 12/12/17 NA 830 NA NA NA 21,000 NA 98 3,300 <5.1 NA NA SV-6r 7 0.5 h 06/14/19 NA 81 NA NA NA 13,000 NA 66 1,300 <5.1 NA NA SV6-rr 3.6 0.5 h 08/11/20 NA 15 NA NA NA 9,800 NA 15 350 <3.8 NA NA SV-7 5 0.5 h 08/11/20 NA <2 NA NA NA 6.2 NA <2 <2.7 <1.3 NA NA SV-8 3.5 0.5 h 08/11/20 NA <2 NA NA NA <3.4 NA <2 <2.7 <1.3 NA NA SV-9 4.75 0.5 h 08/11/20 NA <2 NA NA NA 8.8 NA <2 1.8J <1.3 NA NA SGOI 3.33 0.5h 07/09/14 NA 19 NA NA NA 330 NA <1.2 110 <0.77 NA <1.2 SG02 3.33 0.5h 07/09/14 NA 180 NA NA NA 130,000 NA <140 920 <90 NA <140 SG03 3.33 0.5h 07/09/14 NA <22 NA NA NA 11,000 NA <22 70 <14 NA <22 Indicate "G" for grab sample or for longer samples indicate the number of hours followed by "h". Page 1 of I Table 6: Monitoring Well Construction Data DSCA ID No.: DC680002 06- Well ID Date Installed (mm/dd/YY) Number of Samples Well Depth [feet] Well Diameter [inch] Screen Interval [feet] Status (Active/Inactive) HA-1 08/07/95 1 5.0 N/A 0.0-5.0 Inactive HA-2 08/07/95 1 7.0 N/A 2.0-7.0 Inactive 2W-1 05/23/95 1 8.5 2 3.1-8.1 Inactive 2W-2S 08/07/95 7 8.0 2 2.8-7.8 Active 2W-2D 08/08/95 3 14.0 2 3.4-13.4 Active 2W-3 08/08/95 1 21.5 2 6.0-21.0 Inactive 2W-4 08/07/95 6 9.5 2 4.0-9.0 Active 2W-5 08/10/95 16 9.2 2 3.8-8.8 Active 2W-6 08/08/95 16 13.0 2 7.2-12.2 Active 2W-7 08/08/95 7 9.0 2 3.5-8.5 Active 2W-8 08/10/95 2 9.0 2 3.5-8.5 Inactive 2W-9 6/27/14 4 13 2 8-13 Active 2W-10 6/27/14 5 13 2 8-13 Active 2W-11 6/27/14 5 13 2 8-13 Active 2W-12 6/27/14 3 12 2 7-12 Active MW-1 09/23/08 13 14.5 2 4.5-14.5 Active MW-2 09/23/08 17 28 2 18-28 Active MW-3 09/24/08 16 28 2 18-28 Active MW-4 09/24/08 6 33 2 23-33 Active MW-5 09/24/08 14 28 2 18-28 Active MW-6 09/12/08 1 15 2 5-15 Active Page 1 of 1 Table 7: Groundwater Elevation Data DSCA ID No.: DC680002 Groundwater Sampling Point Sampling Date (mm/dd/yy) TOC Elevation [feet] Depth to Water [feet bgs] Groundwater Elevation feet Depth to NAPL [feet bgs] NAPL Thickness [feet] Corrected* Groundwater Elevation [feet] 10/21/10 265.79 5.49 260.30 N/A N/A N/A 01/21/11 265.79 5.29 260.50 N/A N/A N/A 04/29/11 265.79 3.96 261.83 N/A N/A N/A 07/18/11 265.79 5.43 260.36 N/A N/A N/A 08/30/11 265.79 5.78 260.01 N/A N/A N/A 09/22/11 265.79 5.58 260.21 N/A N/A N/A 10/18/11 265.79 5.73 260.06 N/A N/A N/A 11/18/11 265.79 5.57 260.22 N/A N/A N/A 2W-2S 02/23/12 265.79 5.05 260.74 N/A N/A N/A 05/24/12 265.79 5.05 260.74 N/A N/A N/A 02/07/14 265.79 5.10 260.69 N/A N/A N/A 08/04/14 265.79 4.95 260.84 N/A N/A N/A 11/23/15 265.79 5.37 260.42 N/A N/A N/A 12/12/16 265.79 5.74 260.05 N/A N/A N/A 12/19/18 265.79 4.76 261.03 N/A N/A N/A 06/10/20 265.79 4.91 260.88 N/A N/A N/A 10/21/10 265.73 5.42 260.31 N/A N/A N/A 01/21/11 265.73 5.23 260.50 N/A N/A N/A 04/29/11 265.73 3.89 261.84 N/A N/A N/A 07/18/11 265.73 NA NA N/A N/A N/A 2W-2D 02/07/14 265.73 5.13 260.60 N/A N/A N/A 08/04/14 265.73 4.91 260.82 N/A N/A N/A 11/23/15 265.73 5.40 260.33 N/A N/A N/A 12/12/16 265.73 5.78 259.95 N/A N/A N/A 12/19/18 265.73 4.80 260.93 N/A N/A N/A 06/10/20 265.73 4.96 260.77 N/A N/A N/A 10/21/10 265.61 5.22 260.39 N/A N/A N/A 01/21/11 265.61 5.16 260.45 N/A N/A N/A 04/29/11 265.61 4.36 261.25 N/A N/A N/A 07/17/11 265.61 5.00 260.61 N/A N/A N/A 08/30/11 265.61 5.50 260.11 N/A N/A N/A 09/22/11 265.61 5.14 260.47 N/A N/A N/A 10/18/11 265.61 5.30 260.31 N/A N/A N/A 2W-4 11/18/11 265.61 5.25 260.36 N/A N/A N/A 02/23/12 265.61 5.95 259.66 N/A N/A N/A 05/24/12 265.61 4.73 260.88 N/A N/A N/A 02/07/14 265.61 5.30 260.31 N/A N/A N/A 08/04/14 265.61 5.25 260.36 N/A N/A N/A 11/23/15 265.61 5.25 260.36 N/A N/A N/A 12/12/16 265.61 5.49 260.12 N/A N/A N/A 12/19/18 265.61 4.95 260.66 N/A N/A N/A 10/21/10 264.53 4.73 259.80 N/A N/A N/A 01/21/11 264.53 4.57 259.96 N/A N/A N/A 04/29/11 264.53 4.22 260.31 N/A N/A N/A 07/18/11 264.53 4.33 260.20 N/A N/A N/A 08/30/11 264.53 4.80 259.73 N/A N/A N/A 09/22/11 264.53 4.23 260.30 N/A N/A N/A 10/18/11 264.53 4.45 260.08 N/A N/A N/A 11/18/11 264.53 4.00 260.53 N/A N/A N/A 2W-5 02/23/12 264.53 3.43 261.10 N/A N/A N/A 05/24/12 264.53 3.90 260.63 N/A N/A N/A 09/04/12 264.53 4.38 260.15 N/A N/A N/A 02/07/14 264.53 4.50 260.03 N/A N/A N/A 08/04/14 264.53 4.46 260.07 N/A N/A N/A 11/23/15 264.53 4.49 260.04 N/A N/A N/A 12/12/16 264.53 4.43 260.10 N/A N/A N/A 12/19/18 264.53 4.08 260.45 N/A N/A N/A 06/10/20 264.53 3.78 260.75 N/A N/A N/A Page 1 of4 Table 7: Groundwater Elevation Data DSCA ID No.: DC680002 Groundwater Sampling Point Sampling Date (mm/dd/yy) TOC Elevation [feet] Depth to Water [feet bgs] Elevation Groundwater feet Depth to NAPL [feet bgs] NAPL Thickness [feet] Corrected* Groundwater Elevation [feet] 10/21/10 264.77 6.01 258.76 N/A N/A N/A 01/21/11 264.77 5.56 259.21 N/A N/A N/A 04/29/11 264.77 5.41 259.36 N/A N/A N/A 07/18/11 264.77 5.50 259.27 N/A N/A N/A 08/30/11 264.77 6.06 258.71 N/A N/A N/A 09/22/11 264.77 5.36 259.41 N/A N/A N/A 10/18/11 264.77 5.95 258.82 N/A N/A N/A 11/18/11 264.77 5.85 258.92 N/A N/A N/A 2W-6 02/23/12 264.77 5.44 259.33 N/A N/A N/A 05/24/12 264.77 5.21 259.56 N/A N/A N/A 09/04/12 264.77 5.48 259.29 N/A N/A N/A 11/19/13 264.77 6.52 258.25 N/A N/A N/A 08/04/14 264.77 5.34 259.43 N/A N/A N/A 11/23/15 264.77 5.31 259.46 N/A N/A N/A 12/12/16 264.77 5.71 259.06 N/A N/A N/A 12/19/18 264.77 4.73 260.04 N/A N/A N/A 06/10/20 264.77 4.82 259.95 N/A N/A N/A 10/21/10 264.54 3.18 261.36 N/A N/A N/A 01/21/11 264.54 3.37 261.17 N/A N/A N/A 04/29/11 264.54 2.49 262.05 N/A N/A N/A 07/18/11 264.54 1.10 263.44 N/A N/A N/A 2W-7 11/19/13 264.54 5.15 259.39 N/A N/A N/A 08/04/14 264.54 2.93 261.61 N/A N/A N/A 11/23/15 264.54 3.75 260.79 N/A N/A N/A 12/12/16 264.54 5.24 259.30 N/A N/A N/A 06/10/20 264.54 1.88 262.66 N/A N/A N/A 10/21/10 266.32 6.05 260.27 N/A N/A N/A 01/21/11 266.32 6.27 260.05 N/A N/A N/A 04/29/11 266.32 4.83 261.49 N/A N/A N/A 07/18/11 266.32 6.15 260.17 N/A N/A N/A 08/30/11 266.32 6.50 259.82 N/A N/A N/A 09/22/11 266.32 6.33 259.99 N/A N/A N/A 2W-8 10/18/11 266.32 6.41 259.91 N/A N/A N/A 11/18/11 266.32 6.44 259.88 N/A N/A N/A 02/23/12 266.32 6.00 260.32 N/A N/A N/A 05/24/12 266.32 5.90 260.42 N/A N/A N/A 11/19/13 266.32 6.48 259.84 N/A N/A N/A 08/04/14 266.32 6.10 260.22 N/A N/A N/A 07/08/14 269.32 9.30 260.02 N/A N/A N/A 08/04/14 269.32 9.42 259.90 N/A N/A N/A 11/23/15 269.32 9.45 259.87 N/A N/A N/A 2W-9 12/12/16 269.32 9.51 259.81 N/A N/A N/A 12/19/18 269.32 8.04 261.28 N/A N/A N/A 06/10/20 269.32 8.30 261.02 N/A N/A N/A 07/08/14 268.73 9.50 259.23 N/A N/A N/A 08/04/14 268.73 9.25 259.48 N/A N/A N/A 11/23/15 268.73 9.30 259.43 N/A N/A N/A 2W-10 12/12/16 268.73 9.33 259.40 N/A N/A N/A 12/19/18 268.73 8.17 260.56 N/A N/A N/A 06/10/20 268.73 8.29 260.44 N/A N/A N/A 07/08/14 268.70 9.80 258.90 N/A N/A N/A 08/04/14 268.70 9.71 258.99 N/A N/A N/A 11/23/15 268.70 9.75 258.95 N/A N/A N/A 2W-11 12/12/16 268.70 9.78 258.92 N/A N/A N/A 12/19/18 268.70 9.00 259.70 N/A N/A N/A 06/10/20 268.70 9.11 259.59 N/A N/A N/A Page 2 of 4 Table 7: Groundwater Elevation Data DSCA ID No.: DC680002 Groundwater Sampling Point Sampling Date (mm/dd/yy) TOC Elevation [feet] Depth to Water [feet bgs] Elevation Groundwater feet Depth to NAPL [feet bgs] NAPL Thickness [feet] Corrected* Groundwater Elevation [feet] 07/08/14 267.52 8.70 258.82 N/A N/A N/A 08/04/14 267.52 8.60 258.92 N/A N/A N/A 2W-12 11/23/15 267.52 8.56 258.96 N/A N/A N/A 12/12/16 267.52 8.65 258.87 N/A N/A N/A 12/19/18 267.52 7.37 260.15 N/A N/A N/A 06/10/20 267.52 7.51 260.01 N/A N/A N/A 10/21/10 266.35 8.58 257.77 N/A N/A N/A 01/21/11 266.35 8.38 257.97 N/A N/A N/A 04/29/11 266.35 8.13 258.22 N/A N/A N/A 07/18/11 266.35 8.24 258.11 N/A N/A N/A 08/30/11 266.35 8.65 257.70 N/A N/A N/A 09/22/11 266.35 8.63 257.72 N/A N/A N/A 10/18/11 266.35 8.62 257.73 N/A N/A N/A MW-1 02/23/12 266.35 8.13 258.22 N/A N/A N/A 05/24/12 266.35 8.29 258.06 N/A N/A N/A 09/04/12 266.35 8.62 257.73 N/A N/A N/A 11/19/13 266.35 8.40 257.95 N/A N/A N/A 08/04/14 266.36 7.90 258.46 N/A N/A N/A 11/23/15 266.36 7.64 258.72 N/A N/A N/A 12/12/16 266.36 7.66 258.70 N/A N/A N/A 06/10/20 266.36 7.39 258.97 N/A N/A N/A 10/21/10 268.03 8.89 259.14 N/A N/A N/A 01/21/11 268.03 8.73 259.30 N/A N/A N/A 04/29/11 268.03 8.34 259.69 N/A N/A N/A 07/18/11 268.03 8.44 259.59 N/A N/A N/A 08/30/11 268.03 8.80 259.23 N/A N/A N/A 09/22/11 268.03 8.55 259.48 N/A N/A N/A 10/18/11 268.03 8.59 259.44 N/A N/A N/A 11/18/11 268.03 8.49 259.54 N/A N/A N/A MW-2 02/23/12 268.03 7.89 260.14 N/A N/A N/A 05/24/12 268.03 7.51 260.52 N/A N/A N/A 09/04/12 268.03 8.06 259.97 N/A N/A N/A 11/19/13 268.03 8.29 259.74 N/A N/A N/A 08/04/14 268.04 8.06 259.98 N/A N/A N/A 11/23/15 268.04 7.77 260.27 N/A N/A N/A 12/12/16 268.04 8.90 259.14 N/A N/A N/A 12/19/18 268.04 7.34 260.70 N/A N/A N/A 06/10/20 268.04 7.55 260.49 N/A N/A N/A 10/21/10 269.40 10.33 259.07 N/A N/A N/A 01/21/11 269.40 9.46 259.94 N/A N/A N/A 04/29/11 269.40 8.91 260.49 N/A N/A N/A 07/18/11 269.40 9.04 260.36 N/A N/A N/A 08/30/11 269.40 10.41 258.99 N/A N/A N/A 09/22/11 269.40 9.27 260.13 N/A N/A N/A 10/18/11 269.40 9.38 260.02 N/A N/A N/A MW-3 11/18/11 269.40 9.65 259.75 N/A N/A N/A 02/23/12 269.40 9.00 260.40 N/A N/A N/A 09/04/12 269.40 9.78 259.62 N/A N/A N/A 11/19/13 269.40 9.52 259.88 N/A N/A N/A 08/04/14 269.41 9.26 260.15 N/A N/A N/A 11/23/15 269.41 9.27 260.14 N/A N/A N/A 12/12/16 269.41 9.65 259.76 N/A N/A N/A 12/19/18 269.41 8.40 261.01 N/A N/A N/A 06/10/20 269.41 8.89 260.52 N/A N/A N/A Page 3 of 4 Table 7: Groundwater Elevation Data DSCA ID No.: DC680002 Groundwater Sampling Point Sampling Date (mm/dd/yy) TOC Elevation [feet] Depth to Water [feet bgs] Elevation Groundwater feet Depth to NAPL [feet bgs] NAPL Thickness [feet] Corrected* Groundwater Elevation [feet] 10/21/10 264.30 10.87 253.43 N/A N/A N/A 01/21/11 264.30 9.94 254.36 N/A N/A N/A 04/29/11 264.30 7.84 256.46 N/A N/A N/A 07/18/11 264.30 9.19 255.11 N/A N/A N/A 08/30/11 264.30 10.93 253.37 N/A N/A N/A 09/22/11 264.30 10.65 253.65 N/A N/A N/A MW-4 10/18/11 264.30 10.34 253.96 N/A N/A N/A 11/18/11 264.30 10.18 254.12 N/A N/A N/A 02/23/12 264.30 8.22 256.08 N/A N/A N/A 05/24/12 264.30 7.09 257.21 N/A N/A N/A 09/24/12 264.30 9.85 254.45 N/A N/A N/A 11/19/13 264.30 10.30 254.00 N/A N/A N/A 08/04/14 264.31 8.02 256.29 N/A N/A N/A 10/21/10 264.49 8.45 256.04 N/A N/A N/A 01/21/11 264.49 6.99 257.50 N/A N/A N/A 04/29/11 264.49 5.50 258.99 N/A N/A N/A 07/18/11 264.49 6.00 258.49 N/A N/A N/A 08/30/11 264.49 6.88 257.61 N/A N/A N/A 09/22/11 264.49 7.04 257.45 N/A N/A N/A 10/18/11 264.49 7.17 257.32 N/A N/A N/A MW-5 11/18/11 264.49 7.34 257.15 N/A N/A N/A 02/23/12 264.49 5.84 258.65 N/A N/A N/A 05/24/12 264.49 5.72 258.77 N/A N/A N/A 09/04/12 264.49 6.51 257.98 N/A N/A N/A 11/19/13 264.49 6.78 257.71 N/A N/A N/A 08/04/14 264.50 6.03 258.47 N/A N/A N/A 12/12/16 264.50 6.02 258.48 N/A N/A N/A 06/10/20 264.50 7.50 257.00 N/A N/A N/A 10/21/10 N/A 4.31 N/A N/A N/A N/A 01/21/11 N/A 4.23 N/A N/A N/A N/A 04/29/11 N/A 5.80 N/A N/A N/A N/A 07/18/11 N/A 2.79 N/A N/A N/A N/A MW-6 11/19/13 N/A 6.78 N/A N/A N/A N/A 08/04/14 264.50 3.05 261.45 N/A N/A N/A 11/23/15 264.50 4.46 260.04 N/A N/A N/A 12/12/16 264.50 5.85 258.65 N/A N/A N/A 06/10/20 264.50 2.48 262.02 N/A N/A N/A Page 4 of 4 Table 8: Analytical Data for Groundwater DSCA ID No.: DC680002 � � s o 0 G". O Q U O O i3 y N ,SJ .0 .0 y O ,. O O `� F' V T N N b ov. O 4 M U U U 1m9/Ll P- 1 1 <0.001 1 <0.001 <0.001 <0.001 1 <0.001 0.01 0.46 0.0016<0.001 <0.001 <0.01 <0.001 <0.001 <0.001 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS GP-4 02/14/13 <0.001 U.J <0.001 <0.001 <0.001 0.16 <0.001 <0.001 <0.001 0.0012 <0.001 0.0011 <0.001 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS P-5 1 1 7.551 <0.001 <0.001 7001 7 70.551 0.01 1 <0.001 70.001 70.51 70.001 70.001 70.001 <0.01 <0.01 ND 0.01 <0.01 <0.001 NS <0.001 7001 7001 70.331 7o.001 70.001 70.501 <0.01 <0.001 <0.001 <0.001 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS P- 1 1 70.001 1. 70.551 70.001 70.551 70.001 1 7 1 <0.001 <0.001 <0.01 <0.001 <0.001 <0.001 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS <0.001 <0.001 <0.001 <0.001 <0.001 70.001 <0.001 <0.001 <0.01 <0.001 <0.001 <0.001 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 5 NA < NA NA NA .11 NA NA < 1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA < NA NANNA NA NA < 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA p2W-1 05 5 NA 5.300 NA NA 7 .5 NA NA 2.72NA NA NA NA NA NA NA NA NA NA NA NA NA NA 08/95 NA <0.0050 NA NA<0.0050 NA NA <0.0050 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/06/07 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 10/21/10 <0.001 <0.001 <0.001 <0.0010.00066J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.01 <0.001 <0.001 0.0031J <0.01 <0.01 ND <0.001 0.00043J <0.001 NS 2W-2S 01/21/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.01 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.01 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 0.00037J <0.001 NS 07/18/11 <0.001 I <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.01 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 NS 02/07/14 <0.0005 <0.0005 <0.0005 <0.0005 NA <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.01 <0.01 <0.01 ND <0.0005 <0.0005 NA NA 08/95 NA <0.0010 NA NA NA <0.0010 NA NA <0.0010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2W-2D 12/06/07 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 02/07/14 <0.0005 <0.0005 <0.0005 <0.0005 NA <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.01 <0.01 <0.01 ND <0.0005 <0.0005 NA NA 2W-3 08/95 NA <0.001 NA NA NA 0.179 NA NA 0.003 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 08/95 NA <0.100 NA NA NA 6.09 NA NA 0.647 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/06/07 <0.001 I <0.001 <0.001 <0.001 0.023 0.0301 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 1.76 NA NA NA <0.001 NA NA NA 01/30/09 <0.001 0.479 <0.001 <0.001 <0.001 1.293 <0.001 0.00691 0.379 <0.001 <0.001 <0.001 NA <0.001 <0.001 NA NA NA NA <0.001 <0.001 NA NA 2W 4 02/07/14 <0.1 7.1 <0.1 <0.1 NA 2.9 <0.1 0.083J 1.8 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <2 <2 <2 ND <0.1 <0.1 NA NA 11/23/15 <0.001 0.132 <0.001 <0.001 70.005 0.00484 <0.005 0.00194 0.0078 0.0376 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 <0.005 <0.001 <0.0025 <0.001 NA 05/14/18 <0.001 0.0092 <0.001 <0.001 <0.002 0.0038 <0.001 0.00024J 0.0045 0.0033 <0.003 <0.001 NA <0.001 <0.001 <0.05 <0.02 <0.01 <0.002 <0.002 <0.002 <0.001 <0.001 Page 1 of 5 Table 8: Analytical Data for Groundwater DSCA ID No.: DC680002 � � s o w F' 7 N o CG 8 W F F F DC d N 4 U U U 1m9/Ll 12/06/07 <0.001 <0.001 <0.001 <0.001 1.52 15.1 <0.001 <0.001 2.55 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 01/30/09 <0.001 0.81 <0.001 <0.001 <0.001 0.991 <0.001 0.00683 0.429 0.329 <0.001 <0.001 NA <0.001 <0.001 NA NA NA NA <0.001 0.0041 NA NA 10/21/10 <0.02 0.239 <0.02 <0.02 <0.02 1.95 <0.02 0.0038 0.399 0.002 <0.02 <0.02 <0.02 <0.02 0.0012J <0.05 <0.01 <0.01 ND <0.02 0.00028J <0.001 NS 01/21/11 <0.02 1.42 <0.02 <0.02 <0.02 4.15 <0.02 0.116 1.77 0.0274 <0.02 <0.02 <0.02 <0.02 0.0059J <0.05 <0.01 <0.01 ND <0.02 <0.01 <0.001 NS 04/29/11 <0.02 1.9 <0.02 <0.02 <0.02 3.35 <0.02 0.0155J 1.63 0.256 <0.02 <0.02 <0.02 <0.02 <0.001 <0.05 <0.01 <0.01 ND <0.02 <0.01 0.0215J NS 07/18/11 <0.050 0.760 <0.050 <0.050 <0.050 3.4 <0.250 <0.05 0.990 0.060 <0.150 <0.050 <0.050 <0.050 <0.050 <2.0 <0.5 <0.5 ND <0.050 <0.12 <0.05 <0.001 08/30/11 0.0011 1.500 <0.001 <0.001 <0.001 0.082 <0.005 0.014 0.280 0.390 <0.003 <0.001 <0.001 0.005 <0.001 0.15 0.076 <0.01 I ND <0.001 <0.0025 <0.001 <0.001 09/22/11 <0.01 5.900 <0.01 <0.01 <0.01 0.65 <0.05 0.026 0.320 0.092 <0.03 <0.01 <0.01 0.012 <0.01 3.9 2 <0.1 ND <0.01 <0.025 <0.01 <0.01 2W 5 10/18/11 <0.01 0.034 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 0.540 <0.03 <0.01 <0.01 <0.01 <0.01 0.6 0.42 <0.1 ND <0.01 <0.025 <0.01 <0.01 11/18/11 <0.005 0.081 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.150 <0.015 <0.005 <0.005 <0.005 <0.005 0.45 0.25 <0.1 ND <0.005 <0.025 <0.01 <0.01 02/23/12 <0.01 0.013 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 0.006 <0.03 <0.01 <0.01 <0.01 <0.01 <0.05 <0.01 <0.1 ND <0.01 <0.025 <0.01 <0.01 05/24/12 <0.001 0.003 <0.001 <0.001 <0.001 <0.001 0.044 0.0016 <0.001 0.0041 <0.003 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/04/12 <0.001 0.002 <0.001 <0.001 <0.001 <0.001 1.5 0.0023 <0.001 0.0012 <0.003 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.01 ND <0.001 0.0086 <0.001 <0.001 02/07/14 0.00034J 0.018 <0.0005 <0.0005 NA <0.0005 0.0036 0.012 0.00044J 0.035 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.01 <0.01 <0.01 ND <0.0005 <0.0005 NA NA 11/23/15 <0.001 0.174 <0.001 <0.001 <0.005 <0.001 <0.005 0.00496 0.00108 0.0931 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 0.0247 <0.001 <0.0025 <0.001 NA 05/14/18 <0.005 0.47 <0.005 <0.005 <0.01 <0.005 0.0034J 0.01 <0.005 0.29 <0.015 <0.005 NA <0.005 <0.005 <0.25 0.013J <0.05 0.0093J <0.01 <0.01 <0.005 <0.005 08/95 NA <0.100 NA NA NA 1.77 NA NA 0.09600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/06/07 <0.001 <0.001 <0.001 <0.001 0.482 3.92 <0.001 <0.001 0.83800 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 01/30/09 <0.001 0.656 <0.001 <0.001 <0.001 0.903 <0.001 <0.001 0.21000 <0.001 <0.001 <0.001 NA <0.001 <0.001 NA NA NA NA <0.001 <0.001 NA NA 10/21/10 <0.002 0.401 <0.002 <0.002 <0.002 0.427 <0.002 <0.001 0.214 0.0373 <0.002 <0.002 <0.002 <0.002 <0.002 <0.05 <0.01 <0.01 ND <0.002 <0.001 <0.001 NS 01/21/11 <0.002 0.317 <0.002 <0.002 <0.002 0.346 <0.002 0.0015J 0.33 0.0035 <0.002 <0.002 <0.002 <0.002 <0.002 <0.05 <0.01 <0.01 ND <0.002 <0.01 <0.001 NS 04/29/11 <0.002 0.357 <0.002 <0.002 <0.002 3.41 <0.002 <0.001 0.316 <0.001 <0.002 <0.002 <0.002 <0.002 <0.002 <0.05 <0.01 <0.01 ND <0.002 <0.01 <0.001 NS 07/18/11 <0.05 0.280 <0.05 <0.05 <0.05 3.00 <0.250 <0.05 0.350 <0.05 <0.150 <0.05 <0.05 <0.05 <0.05 <2.5 <0.250 <0.025 ND <0.05 <0.120 <0.05 <0.001 2W_6 08/30/11 <0.001 0.240 <0.001 <0.001 <0.001 2.90 <0.005 0.0029 0.320 0.0016 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/22/11 <0.02 0.170 <0.02 <0.02 <0.02 1.70 <0.1 <0.02 0.190 <0.02 <0.06 <0.02 <0.02 <0.02 <0.02 <1.0 <0.2 <0.2 ND <0.02 <0.05 <0.02 <0.02 10/18/11 <0.025 0.25 <0.025 <0.025 <0.025 2.50 <0.120 <0.025 0.250 <0.02 <0.06 <0.025 <0.025 <0.025 <0.025 <1.0 <0.2 <0.2 ND <0.025 <0.05 <0.02 <0.02 11/18/11 <0.020 0.240 <0.020 <0.020 <0.020 1.80 <0.100 <0.020 0.220 <0.020 <0.06 <0.020 <0.020 <0.020 <0.020 <0.100 <0.200 <0.200 ND <0.020 <0.05 <0.02 <0.02 02/23/12 <0.020 0.160 <0.020 <0.020 <0.020 2.60 <0.100 <0.020 0.240 <0.020 <0.06 0.16 <0.020 <0.020 <0.020 <0.100 <0.200 <0.200 ND <0.020 <0.05 <0.02 <0.02 05/24/12 <0.01 0.170 <0.01 <0.01 <0.01 3.0 <0.01 <0.01 0..250 <0.01 <0.03 <0.01 <0.01 <0.01 <0.01 <0.5 <0.051 <<<000...251 <<<000.0..202555 <<N00..A002 1 <<N00/..A0021 09/04/12 <0.025 0.76 <0.025 <0.025 <0.025 0.84 <0.120 <0.025 0280<0.02 <0.06 <005 <0.025 <0.025 <0.025 <1.0 <0.2 NND DD <<<000.0..202515 <0.25 1.8 <0.25 <0.25 NA 2.10 <0.25 <0.25 .890 511/12/13 002 <0.25 <0.25 <0.25 <0.25 <0.25 <1 <0. 05/14/18 <0.005 0.4 <0.005 <0.005 <0.01 0.16 <0.005 0.0026J 0.140 . <0.015 <0.005 NA <0.005 <0.005 <0.25 <0.1 <0.05 <0.01 <0.01 <0.01 <0.005 <0.005 Page 2 of 5 Table 8: Analytical Data for Groundwater DSCA ID No.: DC680002 � � s o w F' 4 N z 4 U U U 1m9/Ll 08/95 NA <0.001 NA NA NA <0.001 NA NA <0.001 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/06/07 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 10/21/10 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0024J <0.01 <0.01 ND <0.001 0.00027J <0.001 NS 2W-7 01/21/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 07/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 10 ND <0.001 <0.0025 <0.001 NS 11/12/13 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 <0.005 <0.005 <0.002 <0.005 <0.005 <0.005 <0.005 <0.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA N/A 2W 8 12/06/07 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 11/12/13 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 <0.005 0.00032J <0.002 <0.005 <0.005 <0.005 <0.005 <0.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA N/A 07/08/14 <0.0025 0.6 <0.0025 <0.0025 NA 0.47 <0.0025 0.0052 0.24 0.0007J <0.0025 <0.0025 NA <0.0025 <0.0025 <0.050 <0.050 <0.050 ND 0.017J <0.0025 NA <0.0025 2W 9 11/23/15 <0.001 0.27 <0.001 <0.001 <0.005 0.316 <0.005 0.00404 0.129 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 <0.005 0.0251 <0.0025 <0.001 NA 12/12/16 <0.002 0.21 <0.002 <0.004 <0.008 0.22 <0.004 0.0037J 0.11 <0.008 <0.012 <0.002 NA <0.002 <0.002 <0.2 <0.08 <0.04 <0.008 0.013 <0.008 <0.002 NA 12/19/18 <0.001 0.149 <0.001 <0.001 <0.005 0.176 <0.001 0.00229 0.0862 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 <0.005 <0.005 <0.0025 <0.001 NA 07/08/14 <0.050 2.7 <0.050 <0.050 NA 7.2 <0.050 0.031J 3.5 <0.050 <0.050 <0.050 NA <0.050 <0.050 <1 71 <1 ND <0.050 <0.050 NA <0.050 11/23/15 <0.005 2.46 <0.005 <0.005 <0.025 3.1 <0.025 0.0247 4.27 <0.005 <0.015 <0.005 <0.005 <0.005 <0.005 <0.25 <0.05 <0.05 <0.025 <0.005 <0.0125 <0.005 NA 2W-10 12/12/16 <0.1 6.2 <0.1 <0.1 <0.2 0.053 <0.1 0.044J 0.049J <0.2 <0.3 <0.1 NA <0.1 <0.1 <5 <2 <1 <0.2 <0.2 <0.2 <0.1 NA 12/19/18 <0.005 1.93 <0.005 <0.005 <0.025 0.0482 <0.005 0.0126 0.036 0.0901 <0.015 <0.005 <0.005 <0.005 <0.005 <0.25 <0.05 <0.05 <0.025 <0.025 <0.0125 <0.005 NA 06/10/20 <0.0005 0.101 <0.0005 <0.0005 <0.0025 0.018 <0.0005 0.000473J 0.0365 0.0022 <0.0015 <0.0005 <0.0005 <0.0005 <0.0005 <0.025 <0.005 <0.005 <0.0025 <0.0005 <0.00125 <0.0005 NA 07/08/14 <0.025 0.87 <0.025 <0.025 NA 2.9 <0.025 0.0092J 0.69 <0.025 <0.025 <0.0025 NA <0.025 <0.025 <0.5 <0.5 <0.5 ND <0.025 <0.025 NA <0.025 11/23/15 <0.005 0.885 <0.005 <0.005 <0.025 0.312 <0.025 0.0115 2.26 <0.005 <0.015 <0.005 <0.005 <0.005 <0.005 <0.25 <0.05 <0.05 <0.025 <0.005 <0.0125 <0.005 NA 2W-11 12/12/16 <0.002 1.9 <0.002 <0.004 <0.008 0.074 <0.004 0.012J 0.21 0.000881 <0.012 <0.002 1 NA <0.002 0.0026J <0.2 <0.08 <0.04 <0.008 <0.008 0.0027J <0.004 NA 12/19/18 <0.001 0.314 <0.001 <0.001 <0.005 0.0178 <0.001 0.0008 0.0121 0.0982 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 <0.005 <0.005 <0.0025 <0.001 NA 06/10/20 <0.0005 0.0679 <0.0005 <0.0005 <0.0025 0.0114 <0.0005 0.000292J 0.0242 0.00143 <0.0015 <0.0005 <0.0005 <0.0005 <0.0005 <0.025 <0.005 <0.005 1 <0.0025 <0.0005 1 <0.00125 <0.0005 NA 07/08/14 <0.005 0.43 <0.005 <0.005 NA 1.1 <0.005 0.0028J 0.27 0.0043J <0.005 <0.0050 NA <0.005 <0.005 <0.1 <0.1 <0.1 ND <0.005 <0.005 NA <0.005 2W-12 11/23/15 <0.001 0.564 <0.001 <0.001 <0.005 1.17 <0.005 0.00749 0.249 <0.001 <0.003 <0.001 0.00107 <0.001 <0.001 <0.05 <0.01 <0.01 <0.005 <0.001 <0.0025 <0.001 NA 06/10/20 <0.0005 0.799 <0.0005 <0.0005 <0.0025 1.34 <0.0005 0.00531 0.228 <0.0005 <0.0015 <0.0005 0.0018 <0.0005 0.00103 <0.025 <0.005 <0.005 <0.0025 0.000147J <0.00125 <0.0005 NA 09/23/08 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 NA NA NA NA <0.005 NA NA NA 10/21/10 <0.001 <0.001 <0.001 <0.001 <0.001 0.00084J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0023J <0.01 <0.01 ND <0.001 0.00044J <0.001 NS 01/21/11 <0.001 <0.001 <0.001 <0.001 <0.001 0.00048J <0.001 <0.001 <0.00t <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0025J <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 <0.001 <0.001 <0.001 <0.001 <0.001 0.00061J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 07/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.00t <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 08/30/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 MW-1 09/22/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.00t <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 10/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 02/23/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.00t <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 05/24/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/04/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 11/12/13 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 <0.005 0.00036J 1 <0.002 <0.005 <0.005 <0.005 <0.005 <0.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA N/A 06/10/20 <0.0005 10.000141JI <0.0005 1 <0.0005 <0.0025 0.000738 1<0.0005 <0.0005 10.000442JI <0.0005 1 10.0015 <0.0005 1 <0.0005 <0.0005 1 <0.0005 1 <0.025 1 <0.005 <0.005 <0.0025 1 <0.0005 1 <0.00125 <0.0005 1 NA Page 3 of 5 Table 8: Analytical Data for Groundwater DSCA ID No.: DC680002 a � � o 4 N F F F >DC= d N 4 U U U 09/23/08 <0.005 0.799 <0.005 <0.005 <0.005 40.7 <0.005 0.0619 1.208 0.0191 <0.005 <0.005 NA 0.0693 <0.005 NA NA NA NA <0.005 NA NA NA 01/30/09 <0.001 0.8 <0.001 <0.001 <0.001 31.57 <0.001 0.046 1.886 0.00377 <0.001 <0.001 NA <0.001 0.0249 NA NA NA NA <0.001 <0.001 NA NA 10/21/10 <0.05 0.322 <0.05 <0.05 <0.05 4.63 <0.001 <0.001 0.451 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.01 <0.01 ND <0.001 <0.001 <0.001 NS 01/21/11 <0.05 1.29 <0.05 <0.05 <0.05 40.4 <0.001 0.0878 3.1 <0.05 <0.05 <0.05 <0.05 <0.05 0.0505 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 <0.05 1.46 <0.05 <0.05 <0.05 48.4 <0.001 <0.001 2.76 <0.05 <0.05 <0.05 <0.05 <0.05 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 0.198J NS 07/18/11 <1.0 <1.0 <1.0 <1.0 <1.0 34.0 <1.0 <1.0 2.6 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <50 <10 <10 ND <1.0 <2.5 <1.0 <1.0 08/30/11 <0.250 1.2 <0.250 <0.250 <0.250 40.0 <0.250 <0.250 3.6 <0.250 <0.750 <0.250 <0.250 <0.250 <0.250 <12 <2.5 <2.5 ND <0.250 <0.620 <0.250 <0.250 09/22/11 <0.250 7.2 <0.250 <0.250 <0.250 30.0 <0.250 <0.250 2.4 <0.250 <0.750 <0.250 <0.250 <0.250 <0.250 <12 <2.5 <2.5 ND <0.250 <0.620 <0.250 <0.250 MW-2 10/18/11 <0.250 15 <0.250 <0.250 <0.250 <0.250 <0.250 <0.250 <0.250 <0.250 <0.750 <0.250 <0.250 <0.250 <0.250 <12 <2.5 <2.5 ND <0.250 <0.620 <0.250 <0.250 11/18/11 <0.100 1.3 <0.100 <0.100 <0.100 40.0 <0.100 <0.100 3.2 <0.100 <0.300 <0.100 <0.100 <0.100 <0.100 <1.0 <1.0 <1.0 ND <0.100 <0.250 <0.100 <0.100 02/23/12 <0.100 1.2 <0.100 <0.100 <0.100 37.0 <0.100 <0.100 3.0 <0.100 <0.300 <0.100 <0.100 <0.100 <0.100 <1.0 <1.0 <1.0 ND <0.100 <0.250 <0.100 <0.100 05/24/12 <0.100 1.1 <0.100 <0.100 <0.100 37.0 <0.100 <0.100 2.6 <0.100 <0.300 <0.100 <0.100 <0.100 <0.100 <1.0 <1.0 <1.0 ND <0.100 <0.250 <0.100 <0.100 09/04/12 <0.250 1.1 <0.250 <0.250 <0.250 35.0 <0.250 <0.250 2.5 <0.250 <0.750 <0.250 <0.250 <0.250 <0.250 <12 <2.5 <2.5 ND <0.250 <0.620 <0.250 <0.250 11/12/13 <2.5 0.99 J <2.5 <2.5 NA 43.0 <2.5 <2.5 2.9 <1 <2.5 <2.5 <2.5 <2.5 <2.5 <10 <5 <5 ND <2.5 <2.5 NA NA 11/23/15 <0.005 0.6 <0.005 <0.005 <0.025 13.9 <0.025 0.0415 1.36 <0.005 <0.015 <0.005 <0.005 <0.005 0.0246 <0.25 <0.05 <0.05 <0.025 <0.025 <0.025 <0.005 NA 12/12/16 <0.01 0.5 <0.01 <0.01 <0.02 0.62 <0.01 0.00396J 0.21 0.0023J <0.03 <0.01 NA <0.01 <0.01 <0.5 <0.2 <0.1 <0.02 <0.02 <0.02 <0.01 NA 12/19/18 <0.001 0.736 <0.001 <0.001 <0.005 14.2 <0.001 0.0478 1.69 0.103 <0.003 <0.001 0.00211 <0.001 0.0228 <0.05 <0.01 <0.01 <0.005 <0.005 <0.0025 <0.001 NA 09/24/08 <0.005 1.8 <0.005 <0.005 <0.005 5.134 <0.005 <0.005 0.73 <0.005 <0.005 <0.005 NA <0.005 <0.005 NA NA NA NA <0.005 NA NA NA 01/30/09 <0.001 0.893 <0.001 <0.001 <0.001 3.073 <0.001 0.013 0.629 <0.001 <0.001 <0.001 NA <0.001 <0.001 NA NA NA NA <0.001 <0.001 NA NA 10/21/10 <0.005 0.68 <0.005 <0.005 <0.001 1.89 <0.005 0.0092J 0.392 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.05 <0.01 <0.01 ND <0.005 <0.001 <0.001 NS 01/21/11 <0.005 1.3 <0.005 <0.005 <0.001 1.86 <0.005 0.0172 0.408 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.25 <0.01 <0.01 ND <0.005 <0.01 <0.001 NS 04/29/11 <0.005 1.23 <0.005 <0.005 <0.001 1.42 <0.005 0.0148 0.319 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.25 <0.01 <0.01 ND <0.005 <0.01 <0.001 NS 07/18/11 <0.025 1.4 <0.025 <0.025 <0.025 1.3 <0.025 <0.025 0.42 <0.025 <0.075 <0.025 <0.025 <0.025 <0.025 <1.2 <0.25 <0.25 I ND <0.025 <0.062 <0.25 <0.25 08/30/11 <0.01 1.7 <0.01 <0.01 <0.01 1.8 <0.01 0.021 0.51 <0.001 <0.003 <0.01 <0.001 <0.01 <0.001 <0.500 <0.1 <0.1 ND <0.01 <0.025 <0.001 0.012 NM-3 09/22/11 <0.01 2.0 <0.01 <0.01 <0.01 1.7 <0.01 0.021 0.53 <0.001 <0.003 <0.01 <0.001 <0.01 <0.01 <0.500 <0.1 <0.1 ND <0.01 <0.025 <0.001 0.014 10/18/11 <0.01 2.1 <0.01 <0.01 <0.01 2.5 <0.01 0.028 0.67 <0.001 <0.003 <0.01 0.017 <0.01 <0.01 <0.500 <0.1 <0.1 ND <0.01 <0.025 <0.001 <0.001 11/18/11 <0.002 2.7 <0.002 <0.002 <0.002 4.4 <0.002 0.031 0.96 <0.002 <0.006 <0.002 0.027 <0.002 0.0027 <0.100 <0.20 <0.20 ND <0.002 <0.005 <0.002 <0.002 02/23/12 <0.025 2.8 <0.025 <0.025LNA 4.1 <0.025 0.032 1.1 <0.025 <0.075 <0.025 <0.025 <0.025 <0.025 <1.2 <0.025 <0.025 ND <0.025 <0.005 <0.025 <0.025 05/24/12 <0.050 2.9 <0.050 <0.050 3.3 <0.050 <0.050 1.6 <0.050 <0.150 <0.050 <0.050 <0.050 <0.050 <2.5 <0.050 <0.050 ND <0.050 <0.1 <0.050 <0.050 09/04/12 <0.025 4.3 <0.025 <0.025 6.6 <0.025 0.05 1.9 <0.025 <0.075 <0.025 0.031 <0.025 <0.025 <1.2 <0.025 <0.025 ND <0.025 <0.005 <0.025 <0.025 11/12/13 <0.5 1.5 <0.5 <0.5 5.9 <0.5 <0.5 0.73 <0.2 <0.5 <0.5 0.031J <0.5 <0.5 <2 <1 <1 ND <0.5 <0.5 NA NA 11/23/15 <0.001 0.8 <0.001 <0.001 1.58 <0.005 0.00934 0.335 <0.001 <0.003 <0.001 0.00742 <0.001 0.00106 <0.05 <0.01 <0.010 <0.005 <0.001 <0.0025 <0.001 NA 06/10/20 <0.0005 0.144 <0.0005 <0.0005 0.365 <0.0005 0.00153 0.0792 0.00358 <0.0015 <0.0005 0.00155 <0.0005 0.000241J <0.025 <0.005 1 <0.005 1 <0.0025 <0.0005 <0.00125 <0.0005 NA Page 4 of 5 Table 8: Analytical Data for Groundwater DSCA ID No.: DC680002 � � s o w F' 7 N o CG 8 W F F F DC d N 4 U U U 1m9/Ll 09/24/08 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 NA NA NA NA <0.005 NA NA NA 10/21/10 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0022J <0.01 <0.01 ND <0.001 0.00022J <0.001 NS 01/21/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS NM-4 04/29/11 <0.001 0.00031J <0.001 <0.001 <0.001 0.00071J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 07/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 11/12/13 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 <0.005 <0.005 <0.002 <0.005 <0.005 <0.005 <0.005 <0.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA <0.005 09/24/08 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 NA NA NA NA <0.005 NA NA NA 10/21/10 <0.001 <0.001 <0.001 <0.001 <0.001 0.00048J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0034J <0.01 <0.01 ND <0.001 <0.001 <0.001 <0.001 01/21/11 <0.001 <0.001 <0.001 <0.001 <0.001 0.00089J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 07/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 08/30/11 <0.001 <0.001 <0.001 <0.001 <0.001 0.0023 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/22/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 NM-5 10/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 11/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 02/23/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 05/24/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/04/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 11/19/13 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 <0.005 <0.005 <0.002 <0.005 <0.005 <0.005 <0.005 <0.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA N/A 06/10/20 <0.0005 0.000228J <0.0005 <0.0005 <0.0025 <0.0005 <0.0005 <0.0005 1 <0.0005 <0.0005 1 <0.0015 <0.0005 <0.0005 <0.0005 <0.0005 <0.025 <0.005 <0.005 <0.0025 <0.0005 <0.00125 <0.0005 NA MW-6 11/12/13 0.00031J <0.005 <0.005 70.005 NA <0.005 0.0027J <0.005 1 <0.005 <0.002 1 <0.005 <0.005 <0.005 <0.005 75.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA N/A Page 5 of 5 ATTACHMENT 6 GROUNDWATER CONTOUR MAP r I . it }_'I jA PC *. I F E � • :+ram r. M W-4 # (260.77) NM 411 D NM 2W-8 . 2W-2S & / ' (260.88) / f Harris Teeter Center ti I MW-3 f ' ti. (])160.52 2W4 @ ) ' 2W- ' • ' / 2W-5 T- ' - ' f FormL-rAmerican ; � � 2W- 0 / +� Dry -Cleaners Location ` ' 5 .4 46 4% -� MW-2 i ' • •,.�+ &0.49(D 2W- 1 Olin T.Bin ley Baptist 9hurch 257.0 ti 2W-766 t 260.01 / t 262. P %/.ti-` /2W4 51 / / 259.95 MW-1" 258.97 art- 6 .02 - - • t� r 10 i e I U LEGEND . z Monitoring Well Location, Identification and o F M 09 Groundwater Elevation (ft/msl) U y o Deep Monitoring Well Location, Identification C COO No U DMW-1 and Groundwater Elevation (ft/msl) - values in O N Q U Q o (29.87) parentheses not used in contouring a) Abandoned Monitoring Well Location a) ... a� Q Not Measured U NM 4- i — — Potentiometric Surface Contour (ft/msl) o °'Wvs (� -• - Inferred Groundwater Flow Direction 4, o N � M w V C 7 N Q� �M 8, m �" 2 2 ry ry C, �d - SW l IL 0 o 0 rV o � N N 00 0 0 Ln _ V) � � z o LL L° °z m a F U u? O 100 SHEET- APPROX. SCALE, ft. ATT. 6 ATTACHMENT 7 GROUNDWATER QUALITY MAP Ar W 2W-4 (05/14/2018) PCE - 3.8 µg/1 TCE - 4.5 µg/l cis-1,2-DCE - 9.2 µg/l trans-1,2-DCE - 0.24 J µg/l Vinyl chloride - 3.3 µg/l 2W-5 (05/14/2018) • • cis-1,2-DCE - 470 µg/l trans-1,2-DCE - 10 µg/l Vinyl chloride - 290 µg/l # Chloroethane - 9.3 J µg/l Toluene - 3.4 J µg/l 2-Butanone - 13 J µg/l 2W-2D (02/07/2014) BDL 2W-2S (02/07/2014) Harris Teeter Center Fornfer American - _ - -Cleaners Location ` I ; ' V. MW-2 (12/19/2018) • • \ 1 #� PCE - 14,200 µg/l TCE - 1,690 µg/1 cis-1,2-DCE - 736 µg/1 trans-1,2-DCE - 47.8 µg/1 ; .41- Vinyl chloride - 103 µg/1 1,1-DCE - 22.8 µg/l q�, dh . qL 1,1,2-Trichlorotrifluoroethane - / / f 4 2W-7 (11/12/2013) BDL MW-3 (11/12/2013) • ' Benzene - 0.31 J µg/l Toluene - 2.7 J µg/1. N.4 2W-6 (05/14/2018) • • 'CE - 160 µgd TCE - 140 µg/1 cis-1,2-DCE - 400 µg/l trans-1,2-DCE - 2.6 J µg/l Vinyl chloride - 11 µg/l y U 2W-8 (11/12/2013) LEGEND • • Z TCE - 0.32 J µg/l p Monitoring Well Location .— 81 No -' MW-3 (06/10/2020) Deep Monitoring Well Location �00 PCE - 365 µg/1 U TCE - 79.2 µg/l Abandoned Monitoring Well Location Q U Q cis-1,2-DCE - 144 µg/1 BDL Below Laboratory Detection Limits trans-1,2-DCE - 1.53 µg/l Vinyl chloride - 3.58 µg/l J Estimated Concentration Q v) 1,1-Dichloroethene - 0.241 J µg/1 µg/l micrograms per liter U 1,1,2-Trichlorotrifluoroethane - 1.55 µg/l 0 W vs — — Potentiometric Surface Contour (ft) Q vi Inferred Groundwater Flow Direction r � O z � MW-4 (11/12/2013) _N BDL � � J Area of PCE 2L Standard Exceedance Red highlighted text indicates concentrations 2W-9 (12/19/2018) above 2L Standards. PCE - 176 _ PCE - Tetrachloroethene a CE - 8612 µg/l TCE - Trichloroethene cis-1,2-DCE - 149 µg/1 DCE - Dichloroethene = ry trans-1,2-DCE - 2.29 µg/1 • • Groundwater analytical results exceed calculated 2 vapor intrusion risk for residential and non-residen- ❑ � � .. . tial exposure (DSCA Calculator Version 7 - August ¢ i ° U t ? _ 2019). • • Groundwater analytical results do not exceed f / calculated vapor intrusion risk for non-residential exposure but do exceed for residential exposure 2W-10 (06/10/2020) • • � (DSCA Calculator Version 7 -August 2019). PCE - 18 µg/1 TCE - 36.5 µg/l • • Groundwater analytical results do not exceed cis-1,2-DCE - 101 µg/l calculated vapor intrusion risk for residential and trans-1,2-DCE - 0.473 J µg/1 non-residential exposure (DSCA Calculator � Vinyl chloride - 2.2 µg/1 Version 7 - August 2019). Olin T. B ikley - BaptistAurch MW-5 (06/10/2020) • • cis-1,2-DCE - 0.228 J µg/1� / lied, 2W-11 (06/10/2029) • • PCE - 11.4 µg/1 TCE - 24.2 µg/l - cis-1,2-DCE - 67.9 µg/1 trans-1,2-DCE - 0.292 J µg/l S O o Vinyl chloride - 1.43 µg/l 0 0 r4 N O \ 2W-12 (06/10/2020) • o o M PCE - 1,340 µg/1 MW-1 (06/10/2020) • • _ V, Ln TCE - 228 µg/1 PCE - 0.738 µg/l cis-1,2-DCE - 799 µg/1 TCE - 0.442 J µg/l z trans-1,2-DCE - 5.31 µg/l cis-1 2-DCE - 0.141 J µg/1 - Chloroform - 0.147 J µg/1 100 1,1-Dichloroethene - 1.03 µg/l 0 SHEET: 1,1,2-Trichlorotrifluoroethane - 1.80 µg/1 ROX. SCALE, ft. ATT. 7 ATTACHMENT 14 SOIL VAPOR LOCATIONS AND RESULTS LEGEND Soil Gas Sample 0 Former Site Location SV-6 (6/28/171 00 PCE - 3,850 ug/m3 __j PCE -Tetrachloroethene TCE - 484 ug/m3 TCE -Trichloroethene cis-1,2-DCE - 262 ug/m3 cis-1,2-DCE - cis- 1,2-Dichloroethene trans 1,2 DCE 154 ug/m3 trans-1,2-DCE-trans-1,2-Dichloroethene SV-6(12/12/17) •• ug/m3 micrograms per cubic meter PCE - 21,000 ug/m3 J Estimated Concentration TCE - 3,300 ug/m3 09 Sample analytical results do not exceed cis-1,2-DCE - 830 ug/m3 calculated vapor intrusion risk for residential or trans-1,2-DCE - 98 Ug/m3 non-residential exposure - DSCA Indoor Air SV-6 (6/15/18) Risk Calculator, Version 7, August 2019. Not Sampled SV-6 (12/19/18) 99 Sample analytical results do not exceed Not Sampled calculated vapor intrusion risk for non- SV 6R (6/14/19) 100 residential exposure but do exceed for PCE-13,000 ug/m3 residential exposure - DSCA Indoor Air Risk TCE -1,300 ug/m3 Calculator, Version 7, August 2019. cis-1,2-DCE - 81 ug/m3 trans-1,2-DCE - 66 Ug/m3 00 Sample analytical results exceed calculated SV 6RR (8/11/20) • • + vapor intrusion risk for residential and non- PCE - 9,800 ug/m3 residential exposure - DSCA Indoor Air Risk TCE - 350 ug/m3 , Calculator, Version 7, August 2019. cis-1,2-DCE - 15 ug/m3 11 (8//20)/20) trans-1,2-DCE - 15 ug/m3 SV-7 PCE - (8/ u HARRIS TEETER � . CENTER t AMERICAN DR CLEANERS SV-5 (6/28/17) 00 PCE - 75,800 Ug/m3 r TICE - 24,900 Ug/m3 4 cis-1,2-DCE - 9,740 Ug/m3 �• trans 1,2 DCE 347 ug/m3 SV-8 (8/11/20) O O SV-5 (12/12/17) 00 BDL Q PCE - 86,000 Ug/m3 w TICE - 23,000 Ug/m3 OLIN T BINKLEY CIS-1,2-DCE-11,000 ug/m3 !� BAPTIST CHURCH trans-1,2-DCE - 260 Ug/m3 SV-9 (8/11/I a SV-5 (6/15/18) • • PCE-140,000 Ug/m3 ,. PCE - 8.8 ug/m3 2 TICE - 40,000 ug/m3 TICE 1.8 J ug/m3 p cis-1,2-DCE-18,000 ug/m3 ' 4 — 0 trans-1,2-DCE - 480 Ug/m3 SV-5 (12/19/18) • • PCE 120,000 ug/m3'� 0 TICE - 24,000 Ug/m3 t Z cis 1,2 DCE 9,800 Ug/m3 trans-1,2-DCE - 390 ug/m3 I ; SV-5 (6/14/19) 115 C�1 PCE - 93,000 Ug/m3 C TICE -18,000 Ug/m3 f cis-1,2-DCE - 6,000 Ug/m3 • !; - trans-1,2-DCE - 320 Ug/m3 r SV-5 (12/14/19) • • ;�� t PCE - 51,000 u /m3 TICE - 9,600 ug m3 j cis-1,2-DCE - 5,600 ug/m3 r p ) R t trans-1,2-DCE - 230 Ug/m3 �'; a< SV-5 (8/11/20) 00 PCE - 45,000 Ug/m3 i ! TICE - 7,000 Ug/m3 1 0 100 cis-1,2-DCE - 1,400 Ug/m3 trans-1,2-DCE -140 Ug/m3 Feet AECOM TECHNICAL SERVICES OF NORTH CAROLINA, INC 411%� OM 5925 CARNEGIE BOULEVARD, SUITE 370 CHARLOTTE, NC 28209 TEL: (704) 553-6150 FAX:(704) 553{751 y„q Soil Vapor Locations and Results American Dry Cleaners 201 South Estes Drive Chapel Hill, NC DSCA Site # DC680002 c m s= p Q U v v 9 Z CO N 0-10 SHEET: Attachment-14 ATTACHMENT 15 LABORATORY ANALYTICAL DATA REPORTS aceAnalytical o National Center for Testing & Innovation • #r ANALYTICAL REPORT June 22, 2020 AECOM - Raleigh, NC Sample Delivery Group Samples Received: Project Number: Description: Site: L1228253 06/11/2020 60628609 American Dry Cleaners (DC680002) DC680002 Report To: Nick Shore 1600 Perimeter Park Drive Suite 400 Morrisville. NC 27560 Entire Report Reviewed By: (211�o J Chris McCord Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. 4 V — 16 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 1 of 25 TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page 1 Fn Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 FS MW-1 L1228253-01 5 [Cn] MW-3 L1228253-02 7 MW-5 L1228253-03 9 Fr 2W-10 L1228253-04 11 2W-11 L1228253-05 13 RC 2W-12 L1228253-06 15 F, Qc: Quality Control Summary 17 Volatile Organic Compounds (GC/MS) by Method 8260D 17 rAl GI: Glossary of Terms 22 Al: Accreditations & Locations 23 FSC Sc: Sample Chain of Custody 24 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 2 of 25 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time MW-1 L1228253-01 GW T.Eischen 06/10/2010:30 06/11/2009:00 FP1 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time FTC Volatile Organic Compounds (GC/MS) by Method 8260D WG1492364 1 06/15/20 01:50 06/15/20 01:50 JHH Mt. Juliet, TN Collected by Collected date/time Received date/time M MW-3 L1228253-02 GW T.Eischen 06/10/2013:20 06/11/2009:00 Method Batch Dilution Preparation Analysis Analyst Location [Cn] date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260D WG1492364 1 06/15/20 02:09 06/15/20 02:09 JHH Mt. Juliet, TN FSr Volatile Organic Compounds (GC/MS) by Method 8260D WG1495099 10 06/18/2016:55 06/18/2016:55 BMB Mt. Juliet, TN 6 QC Collected by Collected date/time Received date/time MW-5 L1228253-03 GW T.Eischen 06/10/2012:45 06/11/2009:00 GI Method Batch Dilution Preparation Analysis Analyst Location date/time date/time FAI Volatile Organic Compounds (GC/MS) by Method 8260D WG1492364 1 06/15/20 02:29 06/15/20 02:29 JHH Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1495099 1 06/18/2017:14 06/18/2017:14 BMB Mt. Juliet, TN FSC Collected by Collected date/time Received date/time 2W-10 L1228253-04 GW T.Eischen 06/10/2013:50 06/11/2009:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260D WG1492364 1 06/15/20 02:48 06/15/20 02:48 JHH Mt. Juliet, TN Collected by Collected date/time Received date/time 2W-11 L1228253-05 GW T.Eischen 06/10/2014:20 06/11/2009:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260D WG1492364 1 06/15/20 03:07 06/15/20 03:07 JHH Mt. Juliet, TN Collected by Collected date/time Received date/time 2W-12 L1228253-06 GW T.Eischen 06/10/2012:00 06/11/2009:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260D WG1492364 1 06/15/20 03:26 06/15/20 03:26 JHH Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1495099 25 06/18/2017:34 06/18/2017:34 BMB Mt. Juliet, TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 3 of 25 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the FP1 appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. FSr FC-1 GI J ❑ Chris McCord FAI Project Manager FSC Report Revision History Level II Report - Version 1: 06/19/20 09:17 Sample Delivery Group (SDG) Narrative 2-Chloroethyl vinyl ether degrades under acidic conditions. Associated results were determined from the analysis of an acid -preserved sample. Lab Sample ID Project Sample ID Method L1228253-01 M W-1 8260D L1228253-02 MW-3 8260D L1228253-03 MW-5 8260D L1228253-04 2W-10 8260D L1228253-05 2W-11 8260D L1228253-06 2W-12 8260D ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 4 of 25 M W-1 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 06/10/20 10:30 L1228253 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time Acetone U 11.3 25.0 1 06/15/2020 01:50 WG1492364 Acrylonitrile U 0.671 5.00 1 06/15/2020 01:50 WG1492364 Benzene U 0.0941 0.500 1 06/15/2020 01:50 WG1492364 Bromobenzene U 0.118 0.500 1 06/15/2020 01:50 WG1492364 Bromodichloromethane U 0.136 0.500 1 06/15/2020 01:50 WG1492364 Bromochloromethane U 0.128 0.500 1 06/15/2020 01:50 WG1492364 Bromoform U 0.129 0.500 1 06/15/2020 01:50 WG1492364 Bromomethane U 0.605 2.50 1 06/15/2020 01:50 WG1492364 n-Butylbenzene U 0.157 0.500 1 06/15/2020 01:50 WG1492364 sec -Butyl benzene U 0.125 0.500 1 06/15/2020 01:50 WG1492364 ter[-Butylbenzene U 0.127 0.500 1 06/15/2020 01:50 WG1492364 Carbon disulfide U 0.0962 0.500 1 06/15/2020 01:50 WG1492364 Carbon tetrachloride U 0.128 0.500 1 06/15/2020 01:50 WG1492364 Chlorobenzene U 0.117 0.500 1 06/15/2020 01:50 WG1492364 Chlorodibromomethane U 0.140 0.500 1 06/15/2020 01:50 WG1492364 Chloroethane U 0.192 2.50 1 06/15/2020 01:50 WG1492364 2-Chloroethyl vinyl ether U 0.575 50.0 1 06/15/2020 01:50 WG1492364 Chloroform U 0.111 0.500 1 06/15/2020 01:50 WG1492364 Chloromethane U 0.960 1.25 1 06/15/2020 01:50 WG1492364 2-Chlorotoluene U 0.106 0.500 1 06/15/2020 01:50 WG1492364 4-Chlorotoluene U 0.114 0.500 1 06/15/2020 01:50 WG1492364 1,2-Dibromo-3-Chloropropane U 0.276 2.50 1 06/15/2020 01:50 WG1492364 1,2-Dibromoethane U 0.126 0.500 1 06/15/2020 01:50 WG1492364 Dibromomethane U 0.122 0.500 1 06/15/2020 01:50 WG1492364 1,2-Dichlorobenzene U 0.107 0.500 1 06/15/2020 01:50 WG1492364 1,3-Dichlorobenzene U 0.299 0.500 1 06/15/2020 01:50 WG1492364 1,4-Dichlorobenzene U 0.120 0.500 1 06/15/2020 01:50 WG1492364 Dichlorodifluoromethane U 0.374 2.50 1 06/15/2020 01:50 WG1492364 1,1-Dichloroethane U 0.100 0.500 1 06/15/2020 01:50 WG1492364 1,2-Dichloroethane U 0.0819 0.500 1 06/15/2020 01:50 WG1492364 M-Dichloroethene U 0.188 0.500 1 06/15/2020 01:50 WG1492364 cis-1,2-Dichloroethene 0.141 J 0.126 0.500 1 06/15/2020 01:50 WG1492364 trans-1,2-Dichloroethene U 0.149 0.500 1 06/15/2020 01:50 WG1492364 1,2-Dichloropropane U 0.149 0.500 1 06/15/2020 01:50 WG1492364 1,1-Dichloropropene U 0.142 0.500 1 06/15/2020 01:50 WG1492364 1,3-Dichloropropane U 0.109 1.00 1 06/15/2020 01:50 WG1492364 cis-1,3-Dichloropropene U 0.111 0.500 1 06/15/2020 01:50 WG1492364 trans-1,3-Dichloropropene U 0.118 0.500 1 06/15/2020 01:50 WG1492364 trans-1,4-Dichloro-2-butene U 0.467 5.00 1 06/15/2020 01:50 WG1492364 2,2-Dichloropropane U 0.161 0.500 1 06/15/2020 01:50 WG1492364 Di -isopropyl ether U 0.105 0.500 1 06/15/2020 01:50 WG1492364 Ethylbenzene U 0.137 0.500 1 06/15/2020 01:50 WG1492364 Hexachloro-1,3-butadiene U J0 0.337 1.00 1 06/15/2020 01:50 WG1492364 2-Hexanone U 0.787 5.00 1 06/15/2020 01:50 WG1492364 n-Hexane U 0.749 5.00 1 06/15/2020 01:50 WG1492364 lodomethane U 0.554 5.00 1 06/15/2020 01:50 WG1492364 Isopropylbenzene U 0.105 0.500 1 06/15/2020 01:50 WG1492364 p-Isopropyltoluene U 0.120 0.500 1 06/15/2020 01:50 WG1492364 2-Butanone (MEK) U 1.19 5.00 1 06/15/2020 01:50 WG1492364 Methylene Chloride U 0.430 2.50 1 06/15/2020 01:50 WG1492364 4-Methyl-2-pentanone (MIBK) U 0.478 5.00 1 06/15/2020 01:50 WG1492364 Methyl tert-butyl ether U 0.101 0.500 1 06/15/2020 01:50 WG1492364 Naphthalene U 0.174 2.50 1 06/15/2020 01:50 WG1492364 n-Propylbenzene U 0.0993 0.500 1 06/15/2020 01:50 WG1492364 Styrene U 0.118 0.500 1 06/15/2020 01:50 WG1492364 1,1,1,2-Tetrachloroethane U 0.147 0.500 1 06/15/2020 01:50 WG1492364 FP1 FTc FSS 4 Cn Fc F ql FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 5 of 25 M W-1 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 06/10/20 10:30 L1228253 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch F Analyte ug/I ug/I ug/I date / time 1,1,2,2-Tetrachloroethane U 0.133 0.500 1 06/15/2020 01:50 WG1492364 FTc 1,1,2-Trichlorotrifluoroethane U 0.180 0.500 1 06/15/2020 01:50 WG1492364 Tetrachloroethene 0.738 0.300 0.500 1 06/15/2020 01:50 WG1492364 Toluene U 0.278 0.500 1 06/15/2020 01:50 WG1492364 FS 1,2,3-Trichlorobenzene U 0.164 0.500 1 06/15/2020 01:50 WG1492364 1,2,4-Trichlorobenzene U J0 0.481 1.00 1 06/15/2020 01:50 WG1492364 Fn 1,1,1-Trichloroethane U 0.149 0.500 1 06/15/2020 01:50 WG1492364 1,1,2-Trichloroethane U 0.158 0.500 1 06/15/2020 01:50 WG1492364 Trichloroethene 0.442 J 0.190 0.500 1 06/15/2020 01:50 WG1492364 Trichlorofluoromethane U 0.160 2.50 1 06/15/2020 01:50 WG1492364 1,2,3-Trichloropropane U 0.237 2.50 1 06/15/2020 01:50 WG1492364 6 QC 1,2,4-Trimethylbenzene U 0.322 0.500 1 06/15/2020 01:50 WG1492364 1,2,3-Trimethyl benzene U 0.104 0.500 1 06/15/2020 01:50 WG1492364 1,3,5-Trimethyl benzene U 0.104 0.500 1 06/15/2020 01:50 WG1492364 GI Vinyl acetate U 0.692 5.00 1 06/15/2020 01:50 WG1492364 Vinyl chloride U 0.234 0.500 1 06/15/2020 01:50 WG1492364 FAI Xylenes, Total U 0.174 1.50 1 06/15/2020 01:50 WG1492364 (S) Toluene-d8 105 80.0-120 0611512020 01.50 WG1492364 (S) 4-Bromof/uorobenzene 95.5 77.0-126 0611512020 01:50 WG1492364 FSC (S)1,2-Dich/oroethane-d4 109 70.0-130 0611512020 01.50 WG1492364 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 6 of 25 MW-3 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 06/10/20 13:20 L1228253 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time Acetone U 11.3 25.0 1 06/15/2020 02:09 WG1492364 Acrylonitrile U 0.671 5.00 1 06/15/2020 02:09 WG1492364 Benzene U 0.0941 0.500 1 06/15/2020 02:09 WG1492364 Bromobenzene U 0.118 0.500 1 06/15/2020 02:09 WG1492364 Bromodichloromethane U 0.136 0.500 1 06/15/2020 02:09 WG1492364 Bromochloromethane U 0.128 0.500 1 06/15/2020 02:09 WG1492364 Bromoform U 0.129 0.500 1 06/15/2020 02:09 WG1492364 Bromomethane U 0.605 2.50 1 06/15/2020 02:09 WG1492364 n-Butylbenzene U 0.157 0.500 1 06/15/2020 02:09 WG1492364 sec -Butyl benzene U 0.125 0.500 1 06/15/2020 02:09 WG1492364 ter[-Butylbenzene U 0.127 0.500 1 06/15/2020 02:09 WG1492364 Carbon disulfide U 0.0962 0.500 1 06/15/2020 02:09 WG1492364 Carbon tetrachloride U 0.128 0.500 1 06/15/2020 02:09 WG1492364 Chlorobenzene U 0.117 0.500 1 06/15/2020 02:09 WG1492364 Chlorodibromomethane U 0.140 0.500 1 06/15/2020 02:09 WG1492364 Chloroethane U 0.192 2.50 1 06/15/2020 02:09 WG1492364 2-Chloroethyl vinyl ether U 0.575 50.0 1 06/15/2020 02:09 WG1492364 Chloroform U 0.111 0.500 1 06/15/2020 02:09 WG1492364 Chloromethane U 0.960 1.25 1 06/15/2020 02:09 WG1492364 2-Chlorotoluene U 0.106 0.500 1 06/15/2020 02:09 WG1492364 4-Chlorotoluene U 0.114 0.500 1 06/15/2020 02:09 WG1492364 1,2-Dibromo-3-Chloropropane U 0.276 2.50 1 06/15/2020 02:09 WG1492364 1,2-Dibromoethane U 0.126 0.500 1 06/15/2020 02:09 WG1492364 Dibromomethane U 0.122 0.500 1 06/15/2020 02:09 WG1492364 1,2-Dichlorobenzene U 0.107 0.500 1 06/15/2020 02:09 WG1492364 1,3-Dichlorobenzene U 0.299 0.500 1 06/15/2020 02:09 WG1492364 1,4-Dichlorobenzene U 0.120 0.500 1 06/15/2020 02:09 WG1492364 Dichlorodifluoromethane U 0.374 2.50 1 06/15/2020 02:09 WG1492364 1,1-Dichloroethane U 0.100 0.500 1 06/15/2020 02:09 WG1492364 1,2-Dichloroethane U 0.0819 0.500 1 06/15/2020 02:09 WG1492364 M-Dichloroethene 0.241 J 0.188 0.500 1 06/15/2020 02:09 WG1492364 cis-1,2-Dichloroethene 144 0.126 0.500 1 06/15/2020 02:09 WG1492364 trans-1,2-Dichloroethene 1.53 0.149 0.500 1 06/15/2020 02:09 WG1492364 1,2-Dichloropropane U 0.149 0.500 1 06/15/2020 02:09 WG1492364 1,1-Dichloropropene U 0.142 0.500 1 06/15/2020 02:09 WG1492364 1,3-Dichloropropane U 0.109 1.00 1 06/15/2020 02:09 WG1492364 cis-1,3-Dichloropropene U 0.111 0.500 1 06/15/2020 02:09 WG1492364 trans-1,3-Dichloropropene U 0.118 0.500 1 06/15/2020 02:09 WG1492364 trans-1,4-Dichloro-2-butene U 0.467 5.00 1 06/15/2020 02:09 WG1492364 2,2-Dichloropropane U 0.161 0.500 1 06/15/2020 02:09 WG1492364 Di -isopropyl ether U 0.105 0.500 1 06/15/2020 02:09 WG1492364 Ethylbenzene U 0.137 0.500 1 06/15/2020 02:09 WG1492364 Hexachloro-1,3-butadiene U J0 0.337 1.00 1 06/15/2020 02:09 WG1492364 2-Hexanone U 0.787 5.00 1 06/15/2020 02:09 WG1492364 n-Hexane U 0.749 5.00 1 06/15/2020 02:09 WG1492364 lodomethane U 0.554 5.00 1 06/15/2020 02:09 WG1492364 Isopropylbenzene U 0.105 0.500 1 06/15/2020 02:09 WG1492364 p-Isopropyltoluene U 0.120 0.500 1 06/15/2020 02:09 WG1492364 2-Butanone (MEK) U 1.19 5.00 1 06/15/2020 02:09 WG1492364 Methylene Chloride U 0.430 2.50 1 06/15/2020 02:09 WG1492364 4-Methyl-2-pentanone (MIBK) U 0.478 5.00 1 06/15/2020 02:09 WG1492364 Methyl tert-butyl ether U 0.101 0.500 1 06/15/2020 02:09 WG1492364 Naphthalene U 0.174 2.50 1 06/15/2020 02:09 WG1492364 n-Propylbenzene U 0.0993 0.500 1 06/15/2020 02:09 WG1492364 Styrene U 0.118 0.500 1 06/15/2020 02:09 WG1492364 1,1,1,2-Tetrachloroethane U 0.147 0.500 1 06/15/2020 02:09 WG1492364 FP1 FTc FSS 4 Cn Fc F ql FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 7 of 25 ONE LAB. NATIONWIDE. MW-3 SAMPLE RESULTS - 02 Collected date/time: 06/10/20 13:20 L1228253 Volatile Organic Compounds (GC/MS) by Method 8260D Analyte 1,1,2,2-TetrachIoroetha ne 1,1,2-TrichIorotrifluoroethane Tetrachloroethene Toluene 1,2,3-Trichlorobe nzene 1,2,4-Trichlorobenzene 1,1,1-Trich t o ro eth a n e 1,1,2-Trich I oroetha n e Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Tri methyl ben zen e 1,2,3-Trimethyl benzene 1,3,5-Trimethyl benzene Vinyl acetate Vinyl chloride Xylenes, Total (S) Toluene-d8 (S) Toluene-d8 (S) 4-Bromof/uorobenzene (S) 4-Bromofluorobenzene (S) 1,2-Dich/oroethone-d4 (S 1,2-Dich/oroethane-d4 Result ug/I Qualifier MDL ug/I RDL ug/I Dilution Analysis date / time IJ 0.133 0.500 1 06/15/2020 02:09 1.55 0.180 0.500 1 06/15/2020 02:09 365 3.00 5.00 10 06/18/202016:55 IJ 0.278 0.500 1 06/15/2020 02:09 IJ 0.164 0.500 1 06/15/2020 02:09 J J0 0.481 1.00 1 06/15/2020 02:09 IJ 0.149 0.500 1 06/15/2020 02:09 J 0.158 0.500 1 06/15/2020 02:09 79.2 0.190 0.500 1 06/15/2020 02:09 IJ 0.160 2.50 1 06/15/2020 02:09 IJ 0.237 2.50 1 06/15/2020 02:09 IJ 0.322 0.500 1 06/15/2020 02:09 IJ 0.104 0.500 1 06/15/2020 02:09 IJ 0.104 0.500 1 06/15/2020 02:09 IJ 0.692 5.00 1 06/15/2020 02:09 3.58 0.234 0.500 1 06/15/2020 02:09 IJ 0.174 1.50 1 06/15/2020 02:09 104 80.0-120 0611512020 02.09 104 80.0-120 061181202016:55 98.1 77.0-126 0611512020 02.09 101 77.0-126 061181202016:55 108 70.0-130 0611512020 02.09 105 70.0-130 061181202016:55 Batch WG1492364 WG1492364 WG1495099 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1492364 WG1495099 WG1492364 WG1495099 WG1492364 WG1495099 Fp FTc FS Fn N FC] F FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 8 of 25 MW-5 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE. Collected date/time: 06/10/20 12:45 L1228253 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time Acetone U 11.3 25.0 1 06/15/2020 02:29 WG1492364 Acrylonitrile U 0.671 5.00 1 06/15/2020 02:29 WG1492364 Benzene U 0.0941 0.500 1 06/15/2020 02:29 WG1492364 Bromobenzene U 0.118 0.500 1 06/15/2020 02:29 WG1492364 Bromodichloromethane U 0.136 0.500 1 06/15/2020 02:29 WG1492364 Bromochloromethane U 0.128 0.500 1 06/15/2020 02:29 WG1492364 Bromoform U 0.129 0.500 1 06/15/2020 02:29 WG1492364 Bromomethane U 0.605 2.50 1 06/15/2020 02:29 WG1492364 n-Butylbenzene U 0.157 0.500 1 06/15/2020 02:29 WG1492364 sec -Butyl benzene U 0.125 0.500 1 06/15/2020 02:29 WG1492364 ter[-Butylbenzene U 0.127 0.500 1 06/15/2020 02:29 WG1492364 Carbon disulfide U 0.0962 0.500 1 06/15/2020 02:29 WG1492364 Carbon tetrachloride U 0.128 0.500 1 06/15/2020 02:29 WG1492364 Chlorobenzene U 0.117 0.500 1 06/15/2020 02:29 WG1492364 Chlorodibromomethane U 0.140 0.500 1 06/15/2020 02:29 WG1492364 Chloroethane U 0.192 2.50 1 06/15/2020 02:29 WG1492364 2-Chloroethyl vinyl ether U 0.575 50.0 1 06/15/2020 02:29 WG1492364 Chloroform U 0.111 0.500 1 06/15/2020 02:29 WG1492364 Chloromethane U 0.960 1.25 1 06/15/2020 02:29 WG1492364 2-Chlorotoluene U 0.106 0.500 1 06/15/2020 02:29 WG1492364 4-Chlorotoluene U 0.114 0.500 1 06/15/2020 02:29 WG1492364 1,2-Dibromo-3-Chloropropane U 0.276 2.50 1 06/15/2020 02:29 WG1492364 1,2-Dibromoethane U 0.126 0.500 1 06/15/2020 02:29 WG1492364 Dibromomethane U 0.122 0.500 1 06/15/2020 02:29 WG1492364 1,2-Dichlorobenzene U 0.107 0.500 1 06/15/2020 02:29 WG1492364 1,3-Dichlorobenzene U 0.299 0.500 1 06/15/2020 02:29 WG1492364 1,4-Dichlorobenzene U 0.120 0.500 1 06/15/2020 02:29 WG1492364 Dichlorodifluoromethane U 0.374 2.50 1 06/15/2020 02:29 WG1492364 1,1-Dichloroethane U 0.100 0.500 1 06/15/2020 02:29 WG1492364 1,2-Dichloroethane U 0.0819 0.500 1 06/15/2020 02:29 WG1492364 M-Dichloroethene U 0.188 0.500 1 06/15/2020 02:29 WG1492364 cis-1,2-Dichloroethene 0.228 J 0.126 0.500 1 06/15/2020 02:29 WG1492364 trans-1,2-Dichloroethene U 0.149 0.500 1 06/15/2020 02:29 WG1492364 1,2-Dichloropropane U 0.149 0.500 1 06/15/2020 02:29 WG1492364 1,1-Dichloropropene U 0.142 0.500 1 06/15/2020 02:29 WG1492364 1,3-Dichloropropane U 0.109 1.00 1 06/15/2020 02:29 WG1492364 cis-1,3-Dichloropropene U 0.111 0.500 1 06/15/2020 02:29 WG1492364 trans-1,3-Dichloropropene U 0.118 0.500 1 06/15/2020 02:29 WG1492364 trans-1,4-Dichloro-2-butene U 0.467 5.00 1 06/15/2020 02:29 WG1492364 2,2-Dichloropropane U 0.161 0.500 1 06/15/2020 02:29 WG1492364 Di -isopropyl ether U 0.105 0.500 1 06/15/2020 02:29 WG1492364 Ethylbenzene U 0.137 0.500 1 06/15/2020 02:29 WG1492364 Hexachloro-1,3-butadiene U J0 0.337 1.00 1 06/15/2020 02:29 WG1492364 2-Hexanone U 0.787 5.00 1 06/15/2020 02:29 WG1492364 n-Hexane U 0.749 5.00 1 06/15/2020 02:29 WG1492364 lodomethane U 0.554 5.00 1 06/15/2020 02:29 WG1492364 Isopropylbenzene U 0.105 0.500 1 06/15/2020 02:29 WG1492364 p-Isopropyltoluene U 0.120 0.500 1 06/15/2020 02:29 WG1492364 2-Butanone (MEK) U 1.19 5.00 1 06/15/2020 02:29 WG1492364 Methylene Chloride U 0.430 2.50 1 06/15/2020 02:29 WG1492364 4-Methyl-2-pentanone (MIBK) U 0.478 5.00 1 06/15/2020 02:29 WG1492364 Methyl tert-butyl ether U 0.101 0.500 1 06/15/2020 02:29 WG1492364 Naphthalene U 0.174 2.50 1 06/15/2020 02:29 WG1492364 n-Propylbenzene U 0.0993 0.500 1 06/15/2020 02:29 WG1492364 Styrene U 0.118 0.500 1 06/15/2020 02:29 WG1492364 1,1,1,2-Tetrachloroethane U 0.147 0.500 1 06/15/2020 02:29 WG1492364 FP1 FTc FSS 4 Cn Fc F ql FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 9 of 25 MW-5 SAMPLE Collected date/time: 06/10/20 12:45 Volatile Organic Compounds (GC/MS) by Method 8260D RESULTS - 03 L1228253 ONE LAB. NATIONWIDE. Result Qualifier MDL RDL Dilution Analysis Batch F Analyte ug/I ug/I ug/I date / time 1,1,2,2-Tetrachloroethane U 0.133 0.500 1 06/15/2020 02:29 WG1492364 FTc 1,1,2-Trichlorotrifluoroethane U 0.180 0.500 1 06/15/2020 02:29 WG1492364 Tetrachloroethene U 0.300 0.500 1 06/18/202017:14 WG1495099 Toluene U 0.278 0.500 1 06/15/2020 02:29 WG1492364 FS 1,2,3-Trichlorobenzene U 0.164 0.500 1 06/15/2020 02:29 WG1492364 1,2,4-Trichlorobenzene U J0 0.481 1.00 1 06/15/2020 02:29 WG1492364 Fn 1,1,1-Trichloroethane U 0.149 0.500 1 06/15/2020 02:29 WG1492364 1,1,2-Trichloroethane U 0.158 0.500 1 06/15/2020 02:29 WG1492364 Trichloroethene U 0.190 0.500 1 06/15/2020 02:29 WG1492364 Trichlorofluoromethane U 0.160 2.50 1 06/15/2020 02:29 WG1492364 1,2,3-Trichloropropane U 0.237 2.50 1 06/15/2020 02:29 WG1492364 6 QC 1,2,4-Trimethylbenzene U 0.322 0.500 1 06/15/2020 02:29 WG1492364 1,2,3-Trimethyl benzene U 0.104 0.500 1 06/15/2020 02:29 WG1492364 1,3,5-Trimethyl benzene U 0.104 0.500 1 06/15/2020 02:29 WG1492364 GI Vinyl acetate U 0.692 5.00 1 06/15/2020 02:29 WG1492364 Vinyl chloride U 0.234 0.500 1 06/15/2020 02:29 WG1492364 FAI Xylenes, Total U 0.174 1.50 1 06/15/2020 02:29 WG1492364 (S) Toluene-d8 106 80.0-120 0611512020 02:29 WG1492364 (S) Toluene-d8 104 80.0-120 061181202017.74 WG1495099 FSC (S) 4-Bromof/uorobenzene 96.1 77.0-126 0611512020 02:29 WG1492364 (S) 4-Bromofluorobenzene 100 77.0-126 061181202017.74 WG1495099 (S)1,2-Dich/oroethane-d4 109 70.0-130 0611512020 02:29 WG1492364 (S)1,2-Dich/oroethane-d4 104 70.0-130 061181202017.74 WG1495099 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 10 of 25 2 W-10 SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE. Collected date/time: 06/10/20 13:50 L1228253 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time Acetone U 11.3 25.0 1 06/15/2020 02:48 WG1492364 Acrylonitrile U 0.671 5.00 1 06/15/2020 02:48 WG1492364 Benzene U 0.0941 0.500 1 06/15/2020 02:48 WG1492364 Bromobenzene U 0.118 0.500 1 06/15/2020 02:48 WG1492364 Bromodichloromethane U 0.136 0.500 1 06/15/2020 02:48 WG1492364 Bromochloromethane U 0.128 0.500 1 06/15/2020 02:48 WG1492364 Bromoform U 0.129 0.500 1 06/15/2020 02:48 WG1492364 Bromomethane U 0.605 2.50 1 06/15/2020 02:48 WG1492364 n-Butylbenzene U 0.157 0.500 1 06/15/2020 02:48 WG1492364 sec -Butyl benzene U 0.125 0.500 1 06/15/2020 02:48 WG1492364 ter[-Butylbenzene U 0.127 0.500 1 06/15/2020 02:48 WG1492364 Carbon disulfide U 0.0962 0.500 1 06/15/2020 02:48 WG1492364 Carbon tetrachloride U 0.128 0.500 1 06/15/2020 02:48 WG1492364 Chlorobenzene U 0.117 0.500 1 06/15/2020 02:48 WG1492364 Chlorodibromomethane U 0.140 0.500 1 06/15/2020 02:48 WG1492364 Chloroethane U 0.192 2.50 1 06/15/2020 02:48 WG1492364 2-Chloroethyl vinyl ether U 0.575 50.0 1 06/15/2020 02:48 WG1492364 Chloroform U 0.111 0.500 1 06/15/2020 02:48 WG1492364 Chloromethane U 0.960 1.25 1 06/15/2020 02:48 WG1492364 2-Chlorotoluene U 0.106 0.500 1 06/15/2020 02:48 WG1492364 4-Chlorotoluene U 0.114 0.500 1 06/15/2020 02:48 WG1492364 1,2-Dibromo-3-Chloropropane U 0.276 2.50 1 06/15/2020 02:48 WG1492364 1,2-Dibromoethane U 0.126 0.500 1 06/15/2020 02:48 WG1492364 Dibromomethane U 0.122 0.500 1 06/15/2020 02:48 WG1492364 1,2-Dichlorobenzene U 0.107 0.500 1 06/15/2020 02:48 WG1492364 1,3-Dichlorobenzene U 0.299 0.500 1 06/15/2020 02:48 WG1492364 1,4-Dichlorobenzene U 0.120 0.500 1 06/15/2020 02:48 WG1492364 Dichlorodifluoromethane U 0.374 2.50 1 06/15/2020 02:48 WG1492364 1,1-Dichloroethane U 0.100 0.500 1 06/15/2020 02:48 WG1492364 1,2-Dichloroethane U 0.0819 0.500 1 06/15/2020 02:48 WG1492364 M-Dichloroethene U 0.188 0.500 1 06/15/2020 02:48 WG1492364 cis-1,2-Dichloroethene 101 0.126 0.500 1 06/15/2020 02:48 WG1492364 trans-1,2-Dichloroethene 0.473 J 0.149 0.500 1 06/15/2020 02:48 WG1492364 1,2-Dichloropropane U 0.149 0.500 1 06/15/2020 02:48 WG1492364 1,1-Dichloropropene U 0.142 0.500 1 06/15/2020 02:48 WG1492364 1,3-Dichloropropane U 0.109 1.00 1 06/15/2020 02:48 WG1492364 cis-1,3-Dichloropropene U 0.111 0.500 1 06/15/2020 02:48 WG1492364 trans-1,3-Dichloropropene U 0.118 0.500 1 06/15/2020 02:48 WG1492364 trans-1,4-Dichloro-2-butene U 0.467 5.00 1 06/15/2020 02:48 WG1492364 2,2-Dichloropropane U 0.161 0.500 1 06/15/2020 02:48 WG1492364 Di -isopropyl ether U 0.105 0.500 1 06/15/2020 02:48 WG1492364 Ethylbenzene U 0.137 0.500 1 06/15/2020 02:48 WG1492364 Hexachloro-1,3-butadiene U J0 0.337 1.00 1 06/15/2020 02:48 WG1492364 2-Hexanone U 0.787 5.00 1 06/15/2020 02:48 WG1492364 n-Hexane U 0.749 5.00 1 06/15/2020 02:48 WG1492364 lodomethane U 0.554 5.00 1 06/15/2020 02:48 WG1492364 Isopropylbenzene U 0.105 0.500 1 06/15/2020 02:48 WG1492364 p-Isopropyltoluene U 0.120 0.500 1 06/15/2020 02:48 WG1492364 2-Butanone (MEK) U 1.19 5.00 1 06/15/2020 02:48 WG1492364 Methylene Chloride U 0.430 2.50 1 06/15/2020 02:48 WG1492364 4-Methyl-2-pentanone (MIBK) U 0.478 5.00 1 06/15/2020 02:48 WG1492364 Methyl tert-butyl ether U 0.101 0.500 1 06/15/2020 02:48 WG1492364 Naphthalene U 0.174 2.50 1 06/15/2020 02:48 WG1492364 n-Propylbenzene U 0.0993 0.500 1 06/15/2020 02:48 WG1492364 Styrene U 0.118 0.500 1 06/15/2020 02:48 WG1492364 1,1,1,2-Tetrachloroethane U 0.147 0.500 1 06/15/2020 02:48 WG1492364 FP1 FTc FSS 4 Cn Fc F ql FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 11 of 25 2 W-10 SAMPLE Collected date/time: 06/10/20 13:50 Volatile Organic Compounds (GC/MS) by Method 8260D RESULTS - 04 L1228253 ONE LAB. NATIONWIDE. f Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time l 1,1,2,2-Tetrachloroethane U 0.133 0.500 1 06/15/2020 02:48 WG1492364 f 1,1,2-Trichlorotrifluoroethane IJ 0.180 0.500 1 06/15/2020 02:48 WG1492364 Il Tetrachloroethene 18.0 0.300 0.500 1 06/15/2020 02:48 WG1492364 Toluene U 0.278 0.500 1 06/15/2020 02:48 WG1492364 1,2,3-Trichlorobenzene U 0.164 0.500 1 06/15/2020 02:48 WG1492364 1,2,4-Trichlorobenzene J J0 0.481 1.00 1 06/15/2020 02:48 WG1492364 f 1,1,1-Trichloroethane U 0.149 0.500 1 06/15/2020 02:48 WG1492364 Il 1,1,2-Trichloroethane J 0.158 0.500 1 06/15/2020 02:48 WG1492364 Trichloroethene 36.5 0.190 0.500 1 06/15/2020 02:48 WG1492364 I Trichlorofluoromethane U 0.160 2.50 1 06/15/2020 02:48 WG1492364 1,2,3-Trichloropropane U 0.237 2.50 1 06/15/2020 02:48 WG1492364 f 1,2,4-Trimethylbenzene U 0.322 0.500 1 06/15/2020 02:48 WG1492364 Il 1,2,3-Trimethyl benzene U 0.104 0.500 1 06/15/2020 02:48 WG1492364 1,3,5-Trimethyl benzene U 0.104 0.500 1 06/15/2020 02:48 WG1492364 Vinyl acetate U 0.692 5.00 1 06/15/2020 02:48 WG1492364 Vinyl chloride 2.20 0.234 0.500 1 06/15/2020 02:48 WG1492364 f Xylenes, Total U 0.174 1.50 1 06/15/2020 02:48 WG1492364 Il (S) Toluene-d8 105 80.0-120 0611512020 02.48 WG1492364 (S) 4-Bromof/uorobenzene 96.3 77.0-126 0611512020 02.48 WG1492364 (S)1,2-Dich/oroethone-d4 111 70.0-130 0611512020 02.48 WG1492364 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 12 of 25 2 W-11 SAMPLE RESULTS - 05 ONE LAB. NATIONWIDE. Collected date/time: 06/10/20 14:20 L1228253 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time Acetone U 11.3 25.0 1 06/15/2020 03:07 WG1492364 Acrylonitrile U 0.671 5.00 1 06/15/2020 03:07 WG1492364 Benzene U 0.0941 0.500 1 06/15/2020 03:07 WG1492364 Bromobenzene U 0.118 0.500 1 06/15/2020 03:07 WG1492364 Bromodichloromethane U 0.136 0.500 1 06/15/2020 03:07 WG1492364 Bromochloromethane U 0.128 0.500 1 06/15/2020 03:07 WG1492364 Bromoform U 0.129 0.500 1 06/15/2020 03:07 WG1492364 Bromomethane U 0.605 2.50 1 06/15/2020 03:07 WG1492364 n-Butylbenzene U 0.157 0.500 1 06/15/2020 03:07 WG1492364 sec -Butyl benzene U 0.125 0.500 1 06/15/2020 03:07 WG1492364 ter[-Butylbenzene U 0.127 0.500 1 06/15/2020 03:07 WG1492364 Carbon disulfide U 0.0962 0.500 1 06/15/2020 03:07 WG1492364 Carbon tetrachloride U 0.128 0.500 1 06/15/2020 03:07 WG1492364 Chlorobenzene U 0.117 0.500 1 06/15/2020 03:07 WG1492364 Chlorodibromomethane U 0.140 0.500 1 06/15/2020 03:07 WG1492364 Chloroethane U 0.192 2.50 1 06/15/2020 03:07 WG1492364 2-Chloroethyl vinyl ether U 0.575 50.0 1 06/15/2020 03:07 WG1492364 Chloroform U 0.111 0.500 1 06/15/2020 03:07 WG1492364 Chloromethane U 0.960 1.25 1 06/15/2020 03:07 WG1492364 2-Chlorotoluene U 0.106 0.500 1 06/15/2020 03:07 WG1492364 4-Chlorotoluene U 0.114 0.500 1 06/15/2020 03:07 WG1492364 1,2-Dibromo-3-Chloropropane U 0.276 2.50 1 06/15/2020 03:07 WG1492364 1,2-Dibromoethane U 0.126 0.500 1 06/15/2020 03:07 WG1492364 Dibromomethane U 0.122 0.500 1 06/15/2020 03:07 WG1492364 1,2-Dichlorobenzene U 0.107 0.500 1 06/15/2020 03:07 WG1492364 1,3-Dichlorobenzene U 0.299 0.500 1 06/15/2020 03:07 WG1492364 1,4-Dichlorobenzene U 0.120 0.500 1 06/15/2020 03:07 WG1492364 Dichlorodifluoromethane U 0.374 2.50 1 06/15/2020 03:07 WG1492364 1,1-Dichloroethane U 0.100 0.500 1 06/15/2020 03:07 WG1492364 1,2-Dichloroethane U 0.0819 0.500 1 06/15/2020 03:07 WG1492364 M-Dichloroethene U 0.188 0.500 1 06/15/2020 03:07 WG1492364 cis-1,2-Dichloroethene 67.9 0.126 0.500 1 06/15/2020 03:07 WG1492364 trans-1,2-Dichloroethene 0.292 J 0.149 0.500 1 06/15/2020 03:07 WG1492364 1,2-Dichloropropane U 0.149 0.500 1 06/15/2020 03:07 WG1492364 1,1-Dichloropropene U 0.142 0.500 1 06/15/2020 03:07 WG1492364 1,3-Dichloropropane U 0.109 1.00 1 06/15/2020 03:07 WG1492364 cis-1,3-Dichloropropene U 0.111 0.500 1 06/15/2020 03:07 WG1492364 trans-1,3-Dichloropropene U 0.118 0.500 1 06/15/2020 03:07 WG1492364 trans-1,4-Dichloro-2-butene U 0.467 5.00 1 06/15/2020 03:07 WG1492364 2,2-Dichloropropane U 0.161 0.500 1 06/15/2020 03:07 WG1492364 Di -isopropyl ether U 0.105 0.500 1 06/15/2020 03:07 WG1492364 Ethylbenzene U 0.137 0.500 1 06/15/2020 03:07 WG1492364 Hexachloro-1,3-butadiene U J0 0.337 1.00 1 06/15/2020 03:07 WG1492364 2-Hexanone U 0.787 5.00 1 06/15/2020 03:07 WG1492364 n-Hexane U 0.749 5.00 1 06/15/2020 03:07 WG1492364 lodomethane U 0.554 5.00 1 06/15/2020 03:07 WG1492364 Isopropylbenzene U 0.105 0.500 1 06/15/2020 03:07 WG1492364 p-Isopropyltoluene U 0.120 0.500 1 06/15/2020 03:07 WG1492364 2-Butanone (MEK) U 1.19 5.00 1 06/15/2020 03:07 WG1492364 Methylene Chloride U 0.430 2.50 1 06/15/2020 03:07 WG1492364 4-Methyl-2-pentanone (MIBK) U 0.478 5.00 1 06/15/2020 03:07 WG1492364 Methyl tert-butyl ether U 0.101 0.500 1 06/15/2020 03:07 WG1492364 Naphthalene U 0.174 2.50 1 06/15/2020 03:07 WG1492364 n-Propylbenzene U 0.0993 0.500 1 06/15/2020 03:07 WG1492364 Styrene U 0.118 0.500 1 06/15/2020 03:07 WG1492364 1,1,1,2-Tetrachloroethane U 0.147 0.500 1 06/15/2020 03:07 WG1492364 FP1 FTc FSS 4 Cn Fc F ql FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 13 of 25 2 W-11 SAMPLE Collected date/time: 06/10/20 14:20 Volatile Organic Compounds (GC/MS) by Method 8260D RESULTS - 05 L1228253 ONE LAB. NATIONWIDE. f Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time l 1,1,2,2-Tetrachloroethane U 0.133 0.500 1 06/15/2020 03:07 WG1492364 f 1,1,2-Trichlorotrifluoroethane U 0.180 0.500 1 06/15/2020 03:07 WG1492364 Il Tetrachloroethene 11.4 0.300 0.500 1 06/15/2020 03:07 WG1492364 Toluene U 0.278 0.500 1 06/15/2020 03:07 WG1492364 1,2,3-Trichlorobenzene IJ 0.164 0.500 1 06/15/2020 03:07 WG1492364 1,2,4-Trichlorobenzene IJ J0 0.481 1.00 1 06/15/2020 03:07 WG1492364 f 1,1,1-Trichloroethane U 0.149 0.500 1 06/15/2020 03:07 WG1492364 Il 1,1,2-Trichloroethane J 0.158 0.500 1 06/15/2020 03:07 WG1492364 Trichloroethene 24.2 0.190 0.500 1 06/15/2020 03:07 WG1492364 I Trichlorofluoromethane J 0.160 2.50 1 06/15/2020 03:07 WG1492364 1,2,3-Trichloropropane U 0.237 2.50 1 06/15/2020 03:07 WG1492364 f 1,2,4-Trimethylbenzene U 0.322 0.500 1 06/15/2020 03:07 WG1492364 Il 1,2,3-Trimethyl benzene U 0.104 0.500 1 06/15/2020 03:07 WG1492364 1,3,5-Trimethyl benzene U 0.104 0.500 1 06/15/2020 03:07 WG1492364 Vinyl acetate IJ 0.692 5.00 1 06/15/2020 03:07 WG1492364 Vinyl chloride 1.43 0.234 0.500 1 06/15/2020 03:07 WG1492364 f Xylenes, Total IJ 0.174 1.50 1 06/15/2020 03:07 WG1492364 Il (S) Toluene-d8 104 80.0-120 0611512020 03:07 WG1492364 (S) 4-Bromof/uorobenzene 96.4 77.0-126 0611512020 03:07 WG1492364 (S)1,2-Dich/oroethone-d4 112 70.0-130 0611512020 03:07 WG1492364 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 14 of 25 2 W -12 SAMPLE RESULTS - 06 ONE LAB. NATIONWIDE. Collected date/time: 06/10/20 12:00 L1228253 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time Acetone U 11.3 25.0 1 06/15/2020 03:26 WG1492364 Acrylonitrile U 0.671 5.00 1 06/15/2020 03:26 WG1492364 Benzene U 0.0941 0.500 1 06/15/2020 03:26 WG1492364 Bromobenzene U 0.118 0.500 1 06/15/2020 03:26 WG1492364 Bromodichloromethane U 0.136 0.500 1 06/15/2020 03:26 WG1492364 Bromochloromethane U 0.128 0.500 1 06/15/2020 03:26 WG1492364 Bromoform U 0.129 0.500 1 06/15/2020 03:26 WG1492364 Bromomethane U 0.605 2.50 1 06/15/2020 03:26 WG1492364 n-Butylbenzene U 0.157 0.500 1 06/15/2020 03:26 WG1492364 sec -Butyl benzene U 0.125 0.500 1 06/15/2020 03:26 WG1492364 ter[-Butylbenzene U 0.127 0.500 1 06/15/2020 03:26 WG1492364 Carbon disulfide U 0.0962 0.500 1 06/15/2020 03:26 WG1492364 Carbon tetrachloride U 0.128 0.500 1 06/15/2020 03:26 WG1492364 Chlorobenzene U 0.117 0.500 1 06/15/2020 03:26 WG1492364 Chlorodibromomethane U 0.140 0.500 1 06/15/2020 03:26 WG1492364 Chloroethane U 0.192 2.50 1 06/15/2020 03:26 WG1492364 2-Chloroethyl vinyl ether U 0.575 50.0 1 06/15/2020 03:26 WG1492364 Chloroform 0.147 J 0.111 0.500 1 06/15/2020 03:26 WG1492364 Chloromethane U 0.960 1.25 1 06/15/2020 03:26 WG1492364 2-Chlorotoluene U 0.106 0.500 1 06/15/2020 03:26 WG1492364 4-Chlorotoluene U 0.114 0.500 1 06/15/2020 03:26 WG1492364 1,2-Dibromo-3-Chloropropane U 0.276 2.50 1 06/15/2020 03:26 WG1492364 1,2-Dibromoethane U 0.126 0.500 1 06/15/2020 03:26 WG1492364 Dibromomethane U 0.122 0.500 1 06/15/2020 03:26 WG1492364 1,2-Dichlorobenzene U 0.107 0.500 1 06/15/2020 03:26 WG1492364 1,3-Dichlorobenzene U 0.299 0.500 1 06/15/2020 03:26 WG1492364 1,4-Dichlorobenzene U 0.120 0.500 1 06/15/2020 03:26 WG1492364 Dichlorodifluoromethane U 0.374 2.50 1 06/15/2020 03:26 WG1492364 1,1-Dichloroethane U 0.100 0.500 1 06/15/2020 03:26 WG1492364 1,2-Dichloroethane U 0.0819 0.500 1 06/15/2020 03:26 WG1492364 M-Dichloroethene 1.03 0.188 0.500 1 06/15/2020 03:26 WG1492364 cis-1,2-Dichloroethene 799 3.15 12.5 25 06/18/202017:34 WG1495099 trans-1,2-Dichloroethene 5.31 0.149 0.500 1 06/15/2020 03:26 WG1492364 1,2-Dichloropropane U 0.149 0.500 1 06/15/2020 03:26 WG1492364 1,1-Dichloropropene U 0.142 0.500 1 06/15/2020 03:26 WG1492364 1,3-Dichloropropane U 0.109 1.00 1 06/15/2020 03:26 WG1492364 cis-1,3-Dichloropropene U 0.111 0.500 1 06/15/2020 03:26 WG1492364 trans-1,3-Dichloropropene U 0.118 0.500 1 06/15/2020 03:26 WG1492364 trans-1,4-Dichloro-2-butene U 0.467 5.00 1 06/15/2020 03:26 WG1492364 2,2-Dichloropropane U 0.161 0.500 1 06/15/2020 03:26 WG1492364 Di -isopropyl ether U 0.105 0.500 1 06/15/2020 03:26 WG1492364 Ethylbenzene U 0.137 0.500 1 06/15/2020 03:26 WG1492364 Hexachloro-1,3-butadiene U J0 0.337 1.00 1 06/15/2020 03:26 WG1492364 2-Hexanone U 0.787 5.00 1 06/15/2020 03:26 WG1492364 n-Hexane U 0.749 5.00 1 06/15/2020 03:26 WG1492364 lodomethane U 0.554 5.00 1 06/15/2020 03:26 WG1492364 Isopropylbenzene U 0.105 0.500 1 06/15/2020 03:26 WG1492364 p-Isopropyltoluene U 0.120 0.500 1 06/15/2020 03:26 WG1492364 2-Butanone (MEK) U 1.19 5.00 1 06/15/2020 03:26 WG1492364 Methylene Chloride U 0.430 2.50 1 06/15/2020 03:26 WG1492364 4-Methyl-2-pentanone (MIBK) U 0.478 5.00 1 06/15/2020 03:26 WG1492364 Methyl tert-butyl ether U 0.101 0.500 1 06/15/2020 03:26 WG1492364 Naphthalene U 0.174 2.50 1 06/15/2020 03:26 WG1492364 n-Propylbenzene U 0.0993 0.500 1 06/15/2020 03:26 WG1492364 Styrene U 0.118 0.500 1 06/15/2020 03:26 WG1492364 1,1,1,2-Tetrachloroethane U 0.147 0.500 1 06/15/2020 03:26 WG1492364 FP1 FTc FSS 4 Cn Fc F ql FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 15 of 25 2 W -12 SAMPLE Collected date/time: 06/10/20 12:00 Volatile Organic Compounds (GC/MS) by Method 8260D RESULTS - 06 L1228253 ONE LAB. NATIONWIDE. Result Qualifier MDL RDL Dilution Analysis Batch F Analyte ug/I ug/I ug/I date / time 1,1,2,2-Tetrachloroethane U 0.133 0.500 1 06/15/2020 03:26 WG1492364 FTc 1,1,2-Trichlorotrifluoroethane 1.80 0.180 0.500 1 06/15/2020 03:26 WG1492364 Tetrachloroethene 1340 7.50 12.5 25 06/18/202017:34 WG1495099 Toluene U 0.278 0.500 1 06/15/2020 03:26 WG1492364 FS 1,2,3-Trichlorobenzene U 0.164 0.500 1 06/15/2020 03:26 WG1492364 1,2,4-Trichlorobenzene J J0 0.481 1.00 1 06/15/2020 03:26 WG1492364 Fn 1,1,1-Trichloroethane U 0.149 0.500 1 06/15/2020 03:26 WG1492364 1,1,2-Trichloroethane J 0.158 0.500 1 06/15/2020 03:26 WG1492364 Trichloroethene 228 4.75 12.5 25 06/18/202017:34 WG1495099 Trichlorofluoromethane J 0.160 2.50 1 06/15/2020 03:26 WG1492364 1,2,3-Trichloropropane U 0.237 2.50 1 06/15/2020 03:26 WG1492364 6 QC 1,2,4-Trimethylbenzene U 0.322 0.500 1 06/15/2020 03:26 WG1492364 1,2,3-Trimethyl benzene U 0.104 0.500 1 06/15/2020 03:26 WG1492364 1,3,5-Trimethyl benzene U 0.104 0.500 1 06/15/2020 03:26 WG1492364 GI Vinyl acetate IJ 0.692 5.00 1 06/15/2020 03:26 WG1492364 Vinyl chloride U 0.234 0.500 1 06/15/2020 03:26 WG1492364 FAI Xylenes, Total U 0.174 1.50 1 06/15/2020 03:26 WG1492364 (S) Toluene-d8 103 80.0-120 0611512020 03:26 WG1492364 (S Toluene-d8 103 80.0-120 061181202017.34 WG1495099 FSC (S) 4-Bromof/uorobenzene 98.9 77.0-126 0611512020 03:26 WG1492364 (S 4-Bromofluorobenzene 101 77.0-126 061181202017.34 WG1495099 (S) 1,2-Dich/oroethane-d4 108 70.0-130 0611512020 03:26 WG1492364 (S 1,2-Dich/oroethone-d4 104 70.0-130 061181202017.34 WG1495099 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 16 of 25 WG1492364 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260D L1228253-01,02,03,04,05,06 Method Blank (MB) (MB) R3540197-2 06/14/20 21:59 MB Result Analyte ug/I Acetone U Acrylonitrile U Benzene U Bromobenzene U Bromodichloromethane U Bromochloromethane U Bromoform U Bromomethane U n-Butylbenzene U sec -Butyl benzene U tert-Butylbenzene U Carbon disulfide U Carbon tetrachloride U Chlorobenzene U Chlorodibromomethane U Chloroethane U 2-Chloroethyl vinyl ether U Chloroform U Chloromethane U 2-Chlorotoluene U 4-Chlorotoluene U 1,2-Dibromo-3-Chloropropane U 1,2-Dibromoethane U Dibromomethane U 1,2-Dichlorobenzene U 1,3-Dichlorobenzene U 1,4-Dichlorobenzene U trans-1,4-Dichloro-2-butene U Dichlorodifluoromethane U 1,1-Dichloroethane U 1,2-Dichloroethane U 1,1-Dichloroethene U cis-1,2-Dichloroethene U trans-1,2-Dichloroethene U 1,2-Dichloropropane U 1,1-Dichloropropene U 1,3-Dichloropropane U cis-1,3-Dichloropropene U trans-1,3-Dichloropropene U 2,2-Dichloropropane U MB Qualifier MB MDL ug/I MB RDL ug/I 11.3 25.0 0.671 5.00 0.0941 0.500 0.118 0.500 0.136 0.500 0.128 0.500 0.129 0.500 0.605 2.50 0.157 0.500 0.125 0.500 0.127 0.500 0.0962 0.500 0.128 0.500 0.117 0.500 0.140 0.500 0.192 2.50 0.575 50.0 0.111 0.500 0.960 1.25 0.106 0.500 0.114 0.500 0.276 2.50 0.126 0.500 0.122 0.500 0.107 0.500 0.299 0.500 0.120 0.500 0.467 5.00 0.374 2.50 0.100 0.500 0.0819 0.500 0.188 0.500 0.126 0.500 0.149 0.500 0.149 0.500 0.142 0.500 0.109 1.00 0.111 0.500 0.118 0.500 0.161 0.500 FP1 FTC FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 17 of 25 WG1492364 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260D L1228253-01,02,03,04,05,06 Method Blank (MB) (MB) R3540197-2 06/14/20 21:59 MB Result Analyte ug/I Di -isopropyl ether U Ethylbenzene U Hexachloro-1,3-butadiene U 2-Hexanone U n-Hexane U lodomethane U Isopropylbenzene U p-Isopropyltoluene U 2-Butanone (MEK) U Methylene Chloride U 4-Methyl-2-pentanone (MIBK) U Methyl tert-butyl ether U Naphthalene U n-Propylbenzene U Styrene U 1,1,1,2-Tetrachloroethane U 1,1,2,2-Tetrachloroethane U Tetrachloroethene U Toluene U 1,1,2-Trichlorotrifluoroethane U 1,2,3-Trichlorobenzene U 1,2,4-Trichlorobenzene U 1,1,1-Trichloroethane U 1,1,2-Trichloroethane U Trichloroethene U Trichlorofluoromethane U 1,2,3-Trichloropropane U 1,2,3-Trimethyl benzene U 1,2,4-Trimethylbenzene U 1,3,5-Trimethyl benzene U Vinyl acetate U Vinyl chloride U Xylenes, Total U (S) Toluene-d8 104 (S) 4-Bromofluorobenzene 95.4 (S)1,2-Dich/oroethane-d4 110 MB Qualifier MB MDL MB RDL ug/I ug/I 0.105 0.500 0.137 0.500 0.337 1.00 0.787 5.00 0.749 5.00 0.554 5.00 0.105 0.500 0.120 0.500 1.19 5.00 0.430 2.50 0.478 5.00 0.101 0.500 0.174 2.50 0.0993 0.500 0.118 0.500 0.147 0.500 0.133 0.500 0.300 0.500 0.278 0.500 0.180 0.500 0.164 0.500 0.481 1.00 0.149 0.500 0.158 0.500 0.190 0.500 0.160 2.50 0.237 2.50 0.104 0.500 0.322 0.500 0.104 0.500 0.692 5.00 0.234 0.500 0.174 1.50 80.0-120 77.0-126 70.0-130 FP1 FTC FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 18 of 25 WG1492364 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260D L1228253-01,02,03,04,05,06 Laboratory Control Sample (LCS) (LCS) R3540197-1 06/14/20 21:01 Spike Amount Analyte ug/I Acetone Acrylonitrile Benzene Bromobenzene Bromodichloromethane Bromochloromethane Bromoform Bromomethane n-Butylbenzene sec -Butyl benzene tert-Butylbenzene Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene tra ns-1,4-Dich I oro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,1-Dichloropropene 1,3-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 2,2-Dichloropropane 25.0 25.0 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 25.0 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 LCS Result ug/I 21.0 25.9 4.92 4.73 4.80 5.44 4.36 5.24 4.54 4.60 4.69 4.72 4.88 5.14 4.88 5.12 24.6 4.72 6.02 4.85 4.89 3.71 5.01 5.01 5.05 4.93 4.98 3.67 5.05 4.98 5.30 4.90 4.78 5.05 5.40 5.04 5.00 4.67 4.67 4.95 LCS Rec. 84.0 104 98.4 94.6 96.0 109 87.2 105 90.8 92.0 93.8 94.4 97.6 103 97.6 102 98.4 94.4 120 97.0 97.8 74.2 100 100 101 98.6 99.6 73.4 101 99.6 106 98.0 95.6 101 108 101 100 93.4 93.4 99.0 Rec. Limits 19.0-160 55.0-149 70.0-123 73.0-121 75.0-120 76.0-122 68.0-132 10.0-160 73.0-125 75.0-125 76.0-124 61.0-128 68.0-126 80.0-121 77.0-125 47.0-150 51.0-160 73.0-120 41.0-142 76.0-123 75.0-122 58.0-134 80.0-122 80.0-120 79.0-121 79.0-120 79.0-120 33.0-144 51.0-149 70.0-126 70.0-128 71.0-124 73.0-120 73.0-120 77.0-125 74.0-126 80.0-120 80.0-123 78.0-124 58.0-130 LCS Qualifier FP1 FTC FSS 4 Cn FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 19 of 25 WG1492364 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260D L1228253-01,02,03,04,05,06 Laboratory Control Sample (LCS) (LCS) R3540197-1 06/14/20 21:01 Spike Amount Analyte ug/I Di -isopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone n-Hexane lodomethane Isopropylbenzene p-Isopropyltoluene 2-Butanone (MEK) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1, 2-Tet ra c h l o ro et h a n e 1,1,2,2-Tetrachloroetha ne Tetrachloroethene Toluene 1,1,2-Trichlorotrifluoroethane 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-T ri c h l o ro eth a n e 1,1,2-Trich I oroetha n e Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,3-Trim ethyl benzene 1,2,4-Tri methyl ben zen e 1,3,5-Trim ethyl benzene Vinyl acetate Vinyl chloride Xylenes, Total (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dich/oroethane-d4 5.00 5.00 5.00 25.0 5.00 25.0 5.00 5.00 25.0 5.00 25.0 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 5.00 25.0 5.00 15.0 LCS Result ug/I 5.26 5.08 3.33 23.4 5.12 24.8 4.90 4.71 23.4 5.11 25.0 5.18 4.09 4.91 4.85 5.05 4.71 5.14 4.79 4.53 3.70 3.76 5.36 5.09 5.26 4.88 5.37 4.47 4.73 4.80 21.2 5.54 14.8 LCS Rec 105 102 66.6 93.6 102 99.2 98.0 94.2 93.6 102 100 104 81.8 98.2 97.0 101 94.2 103 95.8 90.6 74.0 75.2 107 102 105 97.6 107 89.4 94.6 96.0 84.8 98.7 102 97.7 109 Rec. Limits LCS Qualifier 58.0-138 79.0-123 54.0-138 67.0-149 57.0-133 33.0-147 76.0-127 76.0-125 44.0-160 67.0-120 68.0-142 68.0-125 54.0-135 77.0-124 73.0-130 75.0-125 65.0-130 72.0-132 79.0-120 69.0-132 50.0-138 57.0-137 73.0-124 80.0-120 78.0-124 59.0-147 73.0-130 77.0-120 76.0-121 76.0-122 11.0-160 67.0-131 79.0-123 80.0-120 77.0-126 70.0-130 FP1 FTC FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 20 of 25 WG1495099 Volatile Organic Compounds (GC/MS) by Method 8260D Method Blank (MB) QUALITY CONTROL SUMMARY L1228253-02,03,06 ONE LAB. NATIONWIDE. (MB) R3540316-4 06/18/2013:07 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I cis-1,2-Dichloroethene U 0.126 0.500 Tetrachloroethene U 0.300 0.500 Trichloroethene U 0.190 0.500 (S) Toluene-d8 103 80.0-120 (S) 4-Bromofluorobenzene 98.0 77.0-126 (S)1,2-Dich/oroethane-d4 105 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3540316-1 06/18/20 11:49 • (LCSD) R3540316-2 06/18/2012:09 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % cis-1,2-Dichloroethene 5.00 5.19 5.44 104 109 73.0-120 4.70 20 Tetrachloroethene 5.00 5.78 5.80 116 116 72.0-132 0.345 20 Trichloroethene 5.00 5.67 5.76 113 115 78.0-124 1.57 20 (S) Toluene-d8 103 103 80.0-120 (S) 4-Bromofluorobenzene 101 101 77.0-126 (S)1,2-Dich/oroethone-d4 105 105 70.0-130 FP1 FTc FSS 4 Cn FSr �GI FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 21 of 25 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report ONE LAB. NATIONWIDE. The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions CP IP FTC FSS MDL Method Detection Limit. RDL Reported Detection Limit. [Cn] Rec. Recovery. RPD Relative Percent Difference. FSr SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be rqC detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the FAI laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or SC duplicated within these ranges. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J0 JO: The identification of the analyte is acceptable, but the reported concentration is an estimate. The calibration met method criteria. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 22 of 25 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 s Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T104704245-18-15 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA ME MT NO OR MN T ID t WI NY SD WY MI NV t NE IA OH PA T f IL Ills WV vA UT T CA�� T KS MO KY N NM O� AR SC T MS AL`7GA T TX * LA T AK q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60628609 L1228253 06/22/20 11:07 23 of 25 ,"Parry Name/Address: Billing Information: Analysis/Container/Preservative Chain of Custody Page 1 off p►ECOM VESC 1600 Perimeter Park Drive STE 400 i ylorrisville, NC 27560 L<B SCIE �NC �E s 3 1 hi t ;f�f Pro ecf + tiIe rt to: Email To: / repo I n C S o C G ✓I'1 �. �, J 1 0 @aecom.com 1 t2oss tmanon xa ❑� . ❑� Mount Mimi, 37322 i phone' 615758585E 5859 /State •. ~ Project - — — City/State Southern Cleaners (DC6700020 C hAPe ( // faxPlho615 758 58 .Par 615J58-5859 ■ 3 O X" Description: Collected: — __ -- --- —�-- � L# � ► aa�a5 3 Client Project rah Project J phone: 919�61-1100 C) Fax: 60627578 - A022 — Colle d by (print): Site/Facility ID # P.O. # � �5C �1 ! Acc[num: EN$RNC (Template: m , I I Prelogin: I I Cold by signature): Rush.P (Lab MUST Be Notified) sed Date Reults Nede_ E O " _Same Day _. ...20096 _Next Day ...__...._........_..... 1W% ': (/G O � _ V Emil? —No 2'jYes j J ! I I TSR: McCord Immediately Packed on Ice N _ Y T. _TDay .............................. 50% _Three Day ......- .................--25Y. -No. J FAX? _No _Yes Irf _J Cooler. Shipped Via: inns Sample ID Comp/Grab Matrix Depth Date Time I > n.,n.ycnntam;nan, vmpien nabonrvl %yub W�hz� v',� G 1p zozP 1 3C MW 3 X' o Mw-5 rZys .j 03 2W-la 3 50 3 oN ZDQ 3 _L—� + r -} 'Matrix: ss - soil GW- Groundwater WW - waste Water DW- Drinking water OT - Other pH Temp n,, Remarks: 9 �r ow Other Hold It / Relinquish"y:(Signature) Date., Time: Received by: (Signature) returned via: ❑UPS Condition: (lab use only) dEz ❑Courier ❑ _ --N ��� Cn� , Relinquished by: ignature) Date: Time: Received by: (Signature) emp: I Bottles Receiv "" --N' <O•b (ih orl;r • .5 Q CDC Seal Intact _Y _N NA Relinquished by : (Signature) Date: Time: Received for lab by: (Signatur Date: Time: PH Checked: NCF: J Q 7-, O 6�V NationalPace Analytical • • . Innovation Cooler Receipt F• Client: - 7677, L 140 3 Cooler Received/Opened On: 6 / / 20 Temperature: Received By: Montp Smith Si nature: Receipt Check List NP Yes No COC Seal Present / Intact? COC Signed / Accurate? Bottles arrive intact? Correct bottles used? Sufficient volume sent? If Applicable;, VOA Zero headspace? Preservation Correct / Checked? icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 August 18, 2020 Nick Shore AECOM-Morrisville NC 1600 Perimeter Park Drive Morrisville, NC 27560 Project Location: 201 S. Estes Dr, Chapel Hill, NC Client Job Number: Project Number: 60628609 Laboratory Work Order Number: 20HO614 Enclosed are results of analyses for samples received by the laboratory on August 11, 2020. If you have any questions concerning this report, please feel free to contact me. Sincerely, I,&, �. A�� Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 AECOM-Morrisville NC REPORT DATE: 8/18/2020 1600 Perimeter Park Drive Morrisville, NC 27560 PURCHASE ORDER NUMBER: 60628609 ATTN: Nick Shore PROJECT NUMBER: 60628609 ANALYTICAL SUMMARY WORK ORDER NUMBER: 20HO614 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 201 S. Estes Dr, Chapel Hill, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB SV-5 20HO614-01 Soil Gas EPATO-15 SV-9 20HO614-02 Soil Gas EPATO-15 SV-7 20HO614-03 Soil Gas EPATO-15 SV-8 20HO614-04 Soil Gas EPA TO-15 SV-6RR 20HO614-05 Soil Gas EPATO-15 Page 2 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. EPA TO-15 Qualifications: Elevated reporting limit due to high concentration of target compounds. Analyte & Samples(s) Qualified: 20HO614-01[SV-5], 20H0614-05[SV-6RR] Elevated reporting limit due to matrix interference. Analyte & Samples(s) Qualified: 20H0614-02[SV-9], 20HO614-03[SV-7], 20H0614-04[SV-8] The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. d� Lisa A. Worthington Technical Representative Page 3 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 201 S. Estes Dr, Chapel Hill, NC Date Received: 8/11/2020 Field Sample #: SV-5 Sample ID: 20HO614-01 Sample Matrix: Soil Gas Sampled: 8/ 10/2020 14:56 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1940 Canister Size: 6 liter Flow Controller ID: 4073 Sample Type: 30 min Work Order: 20HO614 Initial Vacuum(in Hg): -29.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -7.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 Sample Flags: RL-I I ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst cis-1,2-Dichloroethylene 350 15 5.1 1400 59 20 300 8/18/20 11:20 TPH trans-1,2-Dichloroethylene 34 15 4.4 140 59 18 300 8/18/20 11:20 TPH Tetrachloroethylene 6600 15 4.9 45000 100 33 300 8/18/20 11:20 TPH Trichloroethylene 1300 15 5.6 7000 81 30 300 8/18/20 11:20 TPH Vinyl Chloride ND 15 8.4 ND 38 21 300 8/18/20 11:20 TPH Surrogates 4-Bromofluorobenzene (1) % Recovery 114 % REC Limits 70-130 8/18/20 11:20 Page 4 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 201 S. Estes Dr, Chapel Hill, NC Sample Description/Location: Work Order: 20HO614 Date Received: 8/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: SV-9 Canister ID: 1179 Final Vacuum(in Hg): -6.5 Sample ID: 20HO614-02 Canister Size: 6 liter Receipt Vacuum(in Hg): -8.9 Sample Matrix: Soil Gas Flow Controller ID: 4370 Flow Controller Type: Fixed -Orifice Sampled: 8/10/2020 15:54 Sample Type: 30 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 Sample Flags: RL-12 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst cis-1,2-Dichloroethylene ND 0.50 0.17 ND 2.0 0.67 10 8/18/20 9:15 TPH trans-1,2-Dichloroethylene ND 0.50 0.15 ND 2.0 0.59 10 8/18/20 9:15 TPH Tetrachloroethylene 1.3 0.50 0.16 8.8 3.4 1.1 10 8/18/20 9:15 TPH Trichloroethylene 0.33 0.50 0.18 J 1.8 2.7 0.99 10 8/18/20 9:15 TPH Vinyl Chloride ND 0.50 0.28 ND 1.3 0.71 10 8/18/20 9:15 TPH Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 115 70-130 8/18/20 9:15 Page 5 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 201 S. Estes Dr, Chapel Hill, NC Sample Description/Location: Work Order: 20HO614 Date Received: 8/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: SV-7 Canister ID: 1955 Final Vacuum(in Hg): -6.5 Sample ID: 20HO614-03 Canister Size: 6 liter Receipt Vacuum(in Hg): -9.4 Sample Matrix: Soil Gas Flow Controller ID: 4283 Flow Controller Type: Fixed -Orifice Sampled: 8/10/2020 16:30 Sample Type: 30 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 Sample Flags: RL-12 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst cis-1,2-Dichloroethylene ND 0.50 0.17 ND 2.0 0.67 10 8/18/20 9:40 TPH trans-1,2-Dichloroethylene ND 0.50 0.15 ND 2.0 0.59 10 8/18/20 9:40 TPH Tetrachloroethylene 0.92 0.50 0.16 6.2 3.4 1.1 10 8/18/20 9:40 TPH Trichloroethylene ND 0.50 0.18 ND 2.7 0.99 10 8/18/20 9:40 TPH Vinyl Chloride ND 0.50 0.28 ND 1.3 0.71 10 8/18/20 9:40 TPH Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 115 70-130 8/18/20 9:40 Page 6 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 201 S. Estes Dr, Chapel Hill, NC Sample Description/Location: Work Order: 20HO614 Date Received: 8/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -29.5 Field Sample #: SV-8 Canister ID: 1929 Final Vacuum(in Hg): -5 Sample ID: 20HO614-04 Canister Size: 6 liter Receipt Vacuum(in Hg): -7.1 Sample Matrix: Soil Gas Flow Controller ID: 4369 Flow Controller Type: Fixed -Orifice Sampled: 8/10/2020 16:33 Sample Type: 30 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 Sample Flags: RL-12 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst cis-1,2-Dichloroethylene ND 0.50 0.17 ND 2.0 0.67 10 8/18/20 10:05 TPH trans-1,2-Dichloroethylene ND 0.50 0.15 ND 2.0 0.59 10 8/18/20 10:05 TPH Tetrachloroethylene ND 0.50 0.16 ND 3.4 1.1 10 8/18/20 10:05 TPH Trichloroethylene ND 0.50 0.18 ND 2.7 0.99 10 8/18/20 10:05 TPH Vinyl Chloride ND 0.50 0.28 ND 1.3 0.71 10 8/18/20 10:05 TPH Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 111 70-130 8/18/20 10:05 Page 7 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: 201 S. Estes Dr, Chapel Hill, NC Sample Description/Location: Work Order: 20HO614 Date Received: 8/11/2020 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: SV-6RR Canister ID: 1952 Final Vacuum(in Hg): -3.5 Sample ID: 20HO614-05 Canister Size: 6 liter Receipt Vacuum(in Hg): -5.7 Sample Matrix: Soil Gas Flow Controller ID: 4211 Flow Controller Type: Fixed -Orifice Sampled: 8/10/2020 14:58 Sample Type: 30 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 Sample Flags: RL-11 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst cis-1,2-Dichloroethylene 3.8 1.5 0.51 15 5.9 2.0 30 8/18/20 10:29 TPH trans-1,2-Dichloroethylene 3.7 1.5 0.44 15 5.9 1.8 30 8/18/20 10:29 TPH Tetrachloroethylene 1400 1.5 0.49 9800 10 3.3 30 8/18/20 10:29 TPH Trichloroethylene 66 1.5 0.56 350 8.1 3.0 30 8/18/20 10:29 TPH Vinyl Chloride ND 1.5 0.84 ND 3.8 2.1 30 8/18/20 10:29 TPH Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 115 70-130 8/18/20 10:29 Page 8 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep -EPA TO-15 Pre-Dil Pre-Dil Default Actual Pressure Pre Initial Final Injection Injection Lab Number [Field ID] Batch Dilution Dilution mL mL mL mL Date 20HO614-01 [SV-5] B264623 1.5 200 5 1000 200 200 08/17/20 20HO614-02 [SV-9] B264623 1.5 1 N/A 1000 200 30 08/17/20 20HO614-03 [SV-7] B264623 1.5 1 N/A 1000 200 30 08/17/20 20HO614-04 [SV-8] B264623 1.5 1 N/A 1000 200 30 08/17/20 20HO614-05 [SV-6RR] B264623 1.5 1 N/A 1000 200 10 08/17/20 Page 9 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD Analyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual Batch B264623 - TO-15 Prep Blank (B264623-BLK1) Prepared & Analyzed: 08/17/20 cis-1,2-Dichloroethylene ND 0.020 trans-1,2-Dichloroethylene ND 0.020 Tetrachloroethylene ND 0.020 Trichloroethylene ND 0.020 Vinyl Chloride ND 0.020 Surrogate: 4-Bromofluorobenzene (1) LCS (B264623-BS1) 9.29 8.00 116 Prepared & Analyzed: 08/17/20 70-130 cis-1,2-Dichloroethylene 5.36 5.00 107 70-130 trans-1,2-Dichloroethylene 5.40 5.00 108 70-130 Tetrachloroethylene 5.48 5.00 110 70-130 Trichloroethylene 4.84 5.00 96.9 70-130 Vinyl Chloride 5.09 5.00 102 70-130 Surrogate: 4-Bromofluorobenzene (1) 9.31 8.00 116 70-130 Page 10 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Note: Blank Subtraction is not performed unless otherwise noted FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). RL-11 Elevated reporting limit due to high concentration of target compounds. RL-12 Elevated reporting limit due to matrix interference. ANALYST TPH Thomas P. Hnitecki RAP Raisa A. Petraitis KKM Kerry K. McGee Page 11 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (S050383-ICV1) Lab File ID: J2020121.13 Analyzed: 07/19/20 19:25 Bromochloromethane (1) 192898 2.879 193615 2.876 100 60 - 140 0.0030 +/-0.50 1,4-Difluorobenzene(1) 923399 3.481 929583 3.478 99 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 813486 5.06 821357 5.06 99 60-140 0.0000 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S051436-CCVI) Lab File ID: J2023004.13 Analyzed: 08/17/20 14:14 Bromochloromethane (1) 123528 2.876 193615 2.876 64 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 710618 3.478 929583 3.478 76 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 639151 5.06 821357 5.06 78 60-140 0.0000 +/-0.50 LCS (B264623-BS1 ) Lab File ID: J2023006.13 Analyzed: 08/17/20 15:44 Bromochloromethane (1) 123746 2.879 123528 2.876 100 60 - 140 0.0030 +/-0.50 1,4-Difluorobenzene(1) 705969 3.481 710618 3.478 99 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 644075 5.06 639151 5.06 101 60-140 0.0000 +/-0.50 Blank (B264623-BLK1) Lab File ID: J2023009.13 Analyzed: 08/17/20 17:12 Bromochloromethane (1) 128482 2.867 123528 2.876 104 60 - 140 -0.0090 +/-0.50 1,4-Difluorobenzene(1) 726345 3.472 710618 3.478 102 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 637813 5.057 639151 5.06 100 60-140 -0.0030 +/-0.50 SV-9 (20110614-02 ) Lab File ID: J2023025.13 Analyzed: 08/18/20 09:15 Bromochloromethane (1) 120931 2.866 123528 2.876 98 60 - 140 -0.0100 +/-0.50 1,4-Difluorobenzene(1) 715656 3.487 710618 3.478 101 60-140 0.0090 +/-0.50 Chlorobenzene-d5(1) 686022 5.063 639151 5.06 107 60-140 0.0030 +/-0.50 SV-7 (20110614-03 ) Lab File ID: J2023026.13 Analyzed: 08/18/20 09:40 Bromochloromethane (1) 123172 2.867 123528 2.876 100 60 - 140 -0.0090 +/-0.50 1,4-Difluorobenzene(1) 679654 3.488 710618 3.478 96 60-140 0.0100 +/-0.50 Chlorobenzene-d5(1) 709583 5.063 639151 5.06 ill 60-140 0.0030 +/-0.50 SV-8 (20110614-04 ) Lab File ID: J2023027.D Analyzed: 08/18/20 10:05 Bromochloromethane (1) 117348 2.866 123528 2.876 95 60 - 140 -0.0100 +/-0.50 1,4-Difluorobenzene(1) 472744 3.497 710618 3.478 67 60-140 0.0190 +/-0.50 Chlorobenzene-d5(1) 702160 5.063 639151 5.06 110 60-140 0.0030 +/-0.50 SV-6RR (20110614-05) Lab File ID: J2023028.D Analyzed: 08/18/20 10:29 Bromochloromethane (1) 123286 2.873 123528 2.876 100 60 - 140 -0.0030 +/-0.50 1,4-Difluorobenzene(1) 750995 3.481 710618 3.478 106 60-140 0.0030 +/-0.50 Chlorobenzene-d5(1) 675765 5.06 639151 5.06 106 60-140 0.0000 +/-0.50 Page 12 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Diff RT Diff Limit Q SV-5 (20110614-01) Lab File ID: J2023030.D Analyzed: 08/18/20 11:20 Bromochloromethane (1) 125685 2.87 123528 2.876 102 60 - 140 -0.0060 +/-0.50 1,4-Difluorobenzene(1) 727158 3.475 710618 3.478 102 60-140 -0.0030 +/-0.50 Chlorobenzene-d5(1) 651794 5.057 639151 5.06 102 60-140 -0.0030 +/-0.50 Page 13 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S051436-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) cis-1,2-Dichloroethylene A 5.00 5.44 1.019309 1.108516 8.8 30 trans-1,2-Dichloroethylene A 5.00 5.53 1.070052 1.183214 10.6 30 Tetrachloroethylene A 5.00 5.67 0.5030711 0.5705469 13.4 30 Trichloroethylene A 5.00 4.92 0.2707074 0.2664227 -1.6 30 Vinyl Chloride A 5.00 5.23 0.7639505 0.7994171 4.6 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 14 of 18 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications EPA TO-15 in Air cis-1,2-Dichloroethylene AIHA,FL,NY,ME,NH,VA trans-1,2-Dichloroethylene AIHA,NJ,NY,ME,NH,VA Tetrachloroethylene AIHA,FL,NJ,NYM E,NH,VA Trichloroethylene AIHA,FL,NJ,NY,ME,NH,VA Vinyl Chloride AIHA,FL,NJ,NY,ME,NH,VA The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2017 100033 03/l/2022 MA Massachusetts DEP M-MA100 06/30/2021 CT Connecticut Department of Publilc Health PH-0567 09/30/2021 NY New York State Department of Health 10899 NELAP 04/1/2021 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2021 RI Rhode Island Department of Health LA000112 12/30/2020 NC North Carolina Div. of Water Quality 652 12/31/2020 NJ New Jersey DEP MA007 NELAP 06/30/2021 FL Florida Department of Health E871027 NELAP 06/30/2021 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2021 ME State of Maine 2011028 06/9/2021 VA Commonwealth of Virginia 460217 12/14/2020 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2020 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2021 NC-DW North Carolina Department of Health 25703 07/31/2021 PA Commonwealth of Pennsylvania DEP 68-05812 06/30/2021 MI Dept. of Env, Great Lakes, and Energy 9100 10/1/2020 Page 15 of 18 8/14/2020 Track your package or shipment with FedEx Tracking IMPORTANT! We are continuing to respond to the impact of COVID-19 around the world. See our latest updates, For COVID-19-related recipient closures, you can redirect packages, Ask FedEx, or contact the shipper. N&Xrq 149454204841 Delivered Thursday 8/ 3/2020 at 4-.40 pm DELIVERED Signature not regw-ec GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM R�:h:icli�,, NC US Multiple -piece Shipment 2 Piece sh:' . !.-nen TO EAS1 L.ONGh/lENDOW, MA (is TRACKING NUMBER SHIPPER CITY, STATE SHIP DATE STATUS DELIVERY DATE DESTINATION/RECIPIENT `.:CITY, STATE 1494Z4204841 DURHAM, NC V 1/202c 8/13i2D20 East Lcnymeadov, IVA (master 1 149454204852 f.1URi i/ V. NC Shipment Facts TRACKING NUMBER 91542048 {1 WEIGHT TOTAL SHIPMENT WEIGHT 3O 11.,si 13,�1 kg,-- STANDARD TRANSIT 8 �I'2.02U E/13i2020 MA SERVICE MASTER TRACKING NUMBER I ec,Ex Ground i 12 4i5-.2t4841 DIMENSIONS TOTALL PIECES I xiOx10irt 2 TERMS PACKAGING ' 1 hird Parly Pa( kage SHIP DATE ACTUAL DELIVERY 0 ! u 8/'1 =12020 4 40 � m .;.UE'F'i11/?020 https:l/www.fedex,comiapps/fedextrack/?action=track&tracknumbers=149454204841Mocale=en_US&cntry_code=us Page 17 of 18 U C: C:0 n MW tC =!StaD... I Have Not Confirmed Sample Container Numbers With Lab Staff Before Relinquishing Over ANALL-V-� C� AA. — I-Aa MC3 AL-rC3FlY Samples 'Doc#:278 .Rein 6 2017 Air Media Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any false �Statement will be brought to the attention of the Client - State True or False +` Client vl �[ r-v E ► Received By hf�—? Date 0 I '� 1;�-O Time How were the samples In Cooler On lee No Ice received? In Box T" Ambient Melted Ice Were samples within Temperature By Gun # Actual Temp - Compliance? 2-6°C By Blank # Actual Temp Was Custody Seal Intact? Were Samples Tampered with? Was COC Relinquished ? �� Does Chain Agree With Samples? Are there any loose caps/valves on any samples? Is COC in ink/ Legible? Did COC Include all Client Analysis I Sampler Name Pertinent Information? Project Are Sample Labels filled out and legible? Are there Rushes? V-- Samples are received within holding time? Proper Media Used? Are there Trip Blanks? -- ............. ID's t Collection Dates/Times r1 1 Who was notified? Individually Certified Cans? Is there enough Volume.?:. Page 18 of 18 1 ATTACHMENT 16 DSCA PROGRAM RISK CALCULATORS DSCA Soil Gas Risk Calculator - Cumulative Risk for Non -Residential Worker Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Date: 8/11/2020 Sample ID: SV-5 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m; Indoor AirCalculated Soil Gas Calculated Indoor Indoor Air Screening Level Non - CAS # Chemical Name: Concentration Air Concentration Concentration Level for Non - Calculated Carcinogenic a a for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR =1 E-06 Quotient 156-59-2 Dichloroeth lene, 1,2-cis- 1400 14 156-60-5 Dichloroet lene, 1,2-trans- 140 1.4 127-18-4 Tetrachloroeth lene 45000 450 4.7E+01 3.5E+01 9.5E-06 2.6E+00 79-01-46 Trichloroeth lene 000 70 1.8E0 2.3E-OS 0E+00 75-01- 1 Chloride 2.8+0 E+Vin 1 Cumulative: I 3.3E-05 I LIE+01 DSCA Soil Gas Risk Calculator - Cumulative Risk for Non -Residential Worker Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Date: 8/1112020 Sample ID: SV-6rr Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. 411 _... rt ,bone are in no/m3 Indoor Air Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chem Chemical Name: Concentration Air Concentration Screening Level for Non- Calculated Carcinogenic (ug/rn) (uP/rn) for Carcinogens @ Carcinogens @ Carcinogenic Risk Hazard Quotient TCR 1E06 THQ = 0.2 156-59-2 Dichloroethylene, 1,2-cis- 15 0.15 156-60-5 Dichloroethylene, 1,2-trans- 15 0.15 127-18-4 Tetrachloroethylene 9800 98 4.7E+01 3.5E+01 2.1E-06 5.6E-01 79-01-6 Trichloroethylene 350 3.5 3.0E+00 1.8E+00 1.2E-06 4.0E-Ol 75-01-4 Vinyl Chloride I 2.8E+00 8.8E+01 Cumulative: I 3.2E-06 I 9.6E-01 DSCA Soil Gas Risk Calculator - Cumulative Risk for Non -Residential Worker Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Date: 8/1112020 Sample ID: SV-7 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. 411 _... rt ,bone are in no/m3 Indoor Air Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chem Chemical Name: Concentration Air Concentration Screening Level for Non- Calculated Carcinogenic (uP/rn) for Carcinogens @ Carcinogens @ Carcinogenic Risk Hazard Quotient TCR 1E06 THQ = 0.2 156-59-2 Dichloroethylene, 1,2-cis- 156-60-5 Dichloroethylene, 1,2-trans- 127-18-4 Tetrachloroethylene 6.2 0.062 i 4.7E+01 3.5E+01 1.3E-09 3.5E-04 79-01-6 ITrlchloroethylene 3.0E+00 1.8E+00 75-01-4 Vinyl Chloride 2.8E+00 I 8.8E+01 Cumulative: I 1.3E-09 I 3.5E-04 DSCA Soil Gas Risk Calculator - Cumulative Risk for Non -Residential Worker Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Date: 8/1112020 Sample ID: SV-9 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. 411 _... rt ,bone are in no/m3 Indoor Air Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chem Chemical Name: Concentration Air Concentration Screening Level for Non- Calculated Carcinogenic (ug/rn) (uP/rn) for Carcinogens @ Carcinogens @ Carcinogenic Risk Hazard Quotient TCR 1E06 THQ = 0.2 156-59-2 Dichloroethylene, 1,2-cis- 156-60-5 Dichloroethylene, l,2-trans- 127-18-4 Tetrachloroethylene 8.8 0.088 4.7E+01 3.5E+01 1.9E-09 5.0E-04 79-01-6 Trichloroethylene 1.8 0.018 3.0E+00 1.8E+00 6.0E-09 2.1E-03 75-01-4 Vinyl Chloride 2.8E+00 I 8.8E+01 Cumulative: I 7.9E-09 I 2.6E-03 DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Date: 8/11/2020 Sample ID: SV-5 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. M concentrations are in ue/m' Indoor Air Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Air Concentration Screening Level for Non- Calculated Carcinogenic (ug/,n) (ug/m3) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR = I E-06 TH — 0 2 Quotient 156-59-2 Dichloroet lene, 1,2-cis- 1400 42 156-60-5 Dichloroeth lene, 1,2-trans- 140 4.2 127-18-4 Tetrachloroeth lene 45000 1350 1.1E+01 8.3E+00 1.3E-04 3.2E+01 79-011 Trichloroeth lene 700 21 4.8E-Ol 4.2E-01 4.4E-01 1.0E+01 75-01-4 Vin lChloride 1.7E-Ol 2.1E+01 Cumulative: I 1.7E-04 I 4.2E+01 DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Date: 8/1112020 Sample ID: SV-6rr Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All rnnrenirarinnc are m no/m3 Indoor An Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Air Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) s (ug/m) for Carcinogens @ Carcinogens @ Carcinogenic Risk Hazard Quotient TCR= 1E-06 THQ = 0.2 156-59-2 Dichloroethylene, 1,2-cis- 15 0.45 156-60-5 Dichloroethylene, 1,2-trans- 15 0.45 127-18-4 Tetrachloroethylene 9800 294 1.1E+01 8.3E+00 2.7E-05 7.0E+00 79-01-6 Trichloroethylene 350 10.5 4.8E-Ol 4.2E-01 2.2E-05 5.0E+00 75-01-4 Vinyl Chloride I 1.7E-01 2.1E+01 Cumulative: I 4.9E-05 I 1.2E+01 DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Date: 8/1112020 Sample ID: SV-7 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All rnnrenirarinnc are m no/m3 Indoor An Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Air Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) ; (ug/m) for Carcinogens @ Carcinogens @ Carcinogenic Risk Hazard Quotient TCR=1E-06 THQ — 0.2 156-59-2 Dichloroethylene, 1,2-cis- 156-60-5 Dichloroethylene, 1,2-trans- 127-18-4 Tetrachloroethylene 6.2 0.186 1.1E+01 8.3E+00 1.7E-08 4.5E-03 79-01-6 Trichloroethylene 4.8E-01 4.2E-01 75-01-4 Vinyl Chloride 1.7E-01 I 2.1E+01 Cumulative: I 1.7E-09 I 4.5E-03 DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Date: 8/1112020 Sample ID: SV-9 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All rnnrenirarinnc are m no/m3 Indoor An Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Air Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) ; (ug/m) for Carcinogens @ Carcinogens @ Carcinogenic Risk Hazard Quotient TCR=1E-06 THQ — 0.2 156-59-2 Dichloroethylene, 1,2-cis- 156-60-5 Dichloroethylene, 1,2-trans- 127-18-4 Tetrachloroethylene 8.8 0.264 1.1E I 8.3E+00 2.4E-08 6.3E-03 79-01-6 Trichloroethylene 1.8 0.054 4.8E-01 4.2E-01 LIE-07 2.6E-02 75-01-4 Vinyl Chloride 1.7E-01 I 2.1E+01 Cumulative: I 1.4E-07 I 3.2E-02 DSCA Indoor Air Risk Calculator- Cumulative Risk for Non -Residential Worker Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleanem, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Omnge County, North Carolina Sampling Date: 6/10/2020 Sample ID: MW-1 Average Groundwater Temperature ("C): 25 (Use de/autt of 25°C unless sits -specific data is available confimung Me groundwater temperetum during—stcass summercordilions.) Carcinogenic risk and hazard quotient cells highlighted In orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor Intrusion risk, no risk values are calculated forthese chemicals. Henry's Constant l Indoor An ndom_Idoor Av CalculatedNon- CAS# Chemical Name: Groundwater Concentration Henrys Constant a[25° used f Air Culated atim, Afr Concentratros Screening Level Screening Level fmNon- Calculated Carcinogenic (ug/L) (dnnensiovle 9) calculations (ugm� for Carcinogens C ® Carcvtogenic Risk Hazard ( ensiovless) ® TCR=1E-06 HQ 0 TH =0.2 Qvotievt 156-59-2 Dkhloroeth Irne, 1,2cis- 0.141 0.166802944 0.166802944 0.023519215 156-60-5 Dkhloroeth Irne, 1,2-trans- 0.383483238 0.383483238 127.18-0 Temchloroeth lene 0.738 0.723630417 0.723630417 0.534039248 4.7E+01 3.5E+01 1.1E-08 3.0E-03 79-01.6 Trichloroeth lene 0.442 0.402698283 0.402698283 0.177992641 3.0E+00 1.8E+00 6.0E-08 2.0E-02 75-014 Vinyl Chlorido 1.136549469 1.136549469 2.8E+00 8.8E+01 Cumulative: I 7.1E-08 I 2.3E-02 DSCA Indoor Air Risk Calculator -Cumulative Risk for Non -Residential Worker Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Dale: 6/10/2020 Sample ID: MW-8 Average Groundwater Temperature(oC): 25 (Use defeuttof25°C unless siteseecirc data is available confimung the ground-terlemp-tun, dung worst -case summercendillens.) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. Indoor Aa Groundwater Henrys Constant Henrys Constant C.1culated Indoor indoor Av S-.ing Level CalculatedNon- CASp Chemical Name: Con(ug/L) os at25° used f Air Concentration Screening Level for fm Non- Calculated Risk Carchrogenic (uglL) (dimensiovlesa) cakulatiovs (apJma) Carcinogens Carcvtogens @ Carcinogenic Hazard Quotient (dnnensionless) @TCR=1E-06 THO-02 75-354 Dichloroethvl-1,1- 0.241 L067048242 1.067048242 0.257158626 1.8E+02 2.9E-04 156-59-2 Dichlerecd lene. 1.2cis- 144 0.166802944 0.166802944 24.01962388 156-00.5 Dichloroethvlene, 1.2-trans- 1.53 0.383483238 0.383483238 0.586729354 127-184 Tetrachlomethvkoe 365 0.723630417 0.723630417 264.1251022 4.7E+01 3.5E+01 5.6E-06 1.5E+00 76-13.1 Trichloro-1,2,2-u luoroethane, 1,1,2- 1.55 21.50449714 21.50449714 33.33197056 4.4E+03 1.5E-03 79-01-6 Trichlom thvleoe 79.2 0.402698283 0.40269TI 19 31.89370401 3.0E+00 1.8E+00 I-05 N.29 3.6E+00 75-014 Vinyl Chloride 3.58 1.136549469 1.136549469 4.068847097 2.8E+00 8.8E11 1.5E-06 9.3E-03 Cumulative: I 1.8E-05 5.2E+00 DSCA Indoor Air Risk Calculator -Cumulative Risk for Non -Residential Worker Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Dale: 6/10/2020 Sample ID: MW5 Average Groundwater Temperature(oC): 25 (Use de/euttof25°C unless siteseecirc data is available confimung the ground-terleee—tun, dung worst -case summercendillens.) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do no[ pose a vapor intrusion risk, no risk values are calculated for these chemicals. Indoor Aa Growdwater Henrys Constant Henrys Constant C.1culated Indoor indoor Av Screening Level CalculatedNon- CASp Chemical Name: Con(ug/L) os at25° used f Air Concentration Screening Level for fm Non- Calculated Risk Carchrogenic (uglL) (dimensiovlesa) cakulatiovs (u�ms) Carcinogens Care. ogees @ Carcinogenic Hazard Quotient (dnnensionless) @TCR=1E-06 THO-02 156-59.2 Dichloroethvlene, I.Uis- 0.228 0.166802944 0.166802944 0.038031071 156-60-5 Dichlerecd lene. 1.2-tress- 0.383493239 0.393483238 127-18-4 Teuachloroethvlene 0.723630417 0.723630417 4.7E+01 3.5E+01 79-01-6 Trichlom thvleoe 0.402698283 0.402698283 3.0E+00 1.8E+00 75-01-4 Vinyl Chloride 1.136549469 1.136549469 2.8E+00 8.8E+01 Cumulative: I 0.0E+00 0.0E+00 DSCA Indoor Air Risk Calculator -Cumulative Risk for Non -Residential Worker Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Dale: 6/10/2020 Sample ID: 2W-10 Average Groundwater Temperature(oC): 25 (Use de/euttof25°C unless siteseecirc data is available confimung the ground-terleee-tun, dung worst -case summercendillens.) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do no[ pose a vapor intrusion risk, no risk values are calculated for these chemicals. Indoor Aa Growdwater Henrys Constant Henrys Constant C.1culated Indoor indoor Av S-.ing Level CalculatedNon- CASp Chemical Name: Con(ug/L) os at25° used f Air Concentration Screening Level for fm Non- Calculated Risk Carchrogenic (uglL) (dimensiovlesa) cakulatiovs (apJm') Carcinogens Carc. ogees @ Carcinogenic Hazard Quotient (dnnensionless) @TCR=1E-06 THO-02 156-59.2 Dichloroethvlen0.1.Uis- 101 0.166802944 0.166802944 16.9470973 156-60-5 Dichlerecd lene. 1.2-tress- 0.473 0.383493239 0.393483238 0.191387572 127-18-4 Teuachloroethvlene 18 0.723630417 0.723630417 13.02534751 4.7E+01 3.5E+01 2.8E-07 7.4E-02 79-01-6 Trichlom thvleoe 36.5 0.402698283 0.402698283 14.69948733 3.0E+00 1.8E+00 4.9E-06 1.7E+00 75-01-4 Vinyl Chloride 2.2 1.136549469 1.136549469 2.500408831 2.8E+00 8.8E+01 9.0E-07 5.7E-03 Cumulative: I 6.1E-06 1.8E+00 DSCA Indoor Air Risk Calculator -Cumulative Risk for Non -Residential Worker Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Dale: 6/10/2020 Sample ID: 2W-11 Average Groundwater Temperature(oC): 25 (Use default of25° C unless siteseecirc data is available confimung the ground-terleee-tun, dung worst -case summercendillens.) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do no[ pose a vapor intrusion risk, no risk values are calculated for these chemicals. Indoor Aa Growdwater Henrys Constant Henrys Constant C.1culated Indoor indoor Av S-.ing Level CalculatedNon- CASp Chemical Name: Con(ug/L) os at25° used f Air Concentration Screening Level for fm Non- Calculated Risk Carchrogenic (uglL) (dimensiovlesa) cakulatiovs (apJm') Carcinogens Carc. ogees @ Carcinogenic Hazard Quotient (dnnensionless) @TCR=1E-06 THO-02 156-59.2 Dichloroethvlen0.1.Uis- 67.9 0.166802944 0.166802944 11.32591987 156-60-5 Dichlerecd lane. 1.2-tress- 0.292 0.383493239 0.393483238 0.111977105 127-18-4 Teuachloroethvlene 11.4 0.723630417 0.723630417 8.249386754 4.7E+01 3.5E+01 1.7E-07 4.7E-02 79-01-6 Trichlom thvleoe 24.2 0.402698283 0.402698283 9.745298446 3.0E+00 1.8E+00 3.3E-06 1.1E+00 75-01-4 Vinyl Chloride 1.43 1.136549469 1.136549469 1.62526574 2.8E+00 8.8E+01 5.8E-07 3.7E-03 Cumulative: I 4.0E-06 1.2E+00 DSCA Indoor Air Risk Calculator -Cumulative Risk for Non -Residential Worker Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Dale: 6/10/2020 Sample ID: 2W-12 Average Groundwater Temperature(oC): 25 (Use defeuttof25°C unless siteseecirc data is available confimung the ground-terlemp-tun, dung worst -case summercendillens.) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. Indoor Aa Groundwater Hemy's Constant Hemy's Constant C.1culated Indoor indoor Av Screeting Level CalculatedNon- CASp Chemical Name: Concestrados at25° used f Air Concenaalion Screening Level for fm Non- Calculated Risk Carchrogenic (ugR.) (dimensiovlesa) cakulatiovs (apJm') Carcinogens Care. ogees @ Carcinogenic Hazard Quotient (dnnensionless) @TCR=1E-06 THO-02 67.66-3 Chloroform 0.147 0A50040883 0.150040883 0.02205601 5.3E-01 8.6E+01 4.1E-08 5.1E-05 75-354 Dichlom thvleoe. 1.1- 1.03 1.067048242 1.067048242 1.099059689 1.8E+02 1.3E-03 156-59-2 Dichloroethvlene, I.Uis- 799 0.166802944 0.166802944 133.2755519 156-60-5 Dichlerecd lene, 1.2-aaas- 5.31 0.383493239 0.393483238 2.036295993 127-184 Temchloroethvlene 1340 0.723630417 0.723630417 969.6647588 4.7E+01 3.5E+01 2.1E-05 5.5E+00 76-13-1 Tdchloro-1.2.2-.ifluoroethane, 1,12- l.8 21,50449714 21.50449714 38.70809485 4.4E+03 1.8E-03 79-01-6 Trichloroethvleoe 22I, 0.402698283 0.402698283 91.8152085 3.0E+00 1.8E+00 3.1E-05 1.0E+01 75-014 1 Vinvl Chloride 1 1.136549469 1 1.136549469 1 1 2.8E+00 I 8.8E+01 Cumulative: I 5.1E-05 1.6E+01 DSCA Indoor Air Risk Calculator -Cumulative Risk for Resident Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Date: 6/10/2020 Sample ID: MW-1 Average Groundwater Temperature (°C): 25 (Use default of 25°C unless sih-pecTc data is available corfimung the groundwater h,,hh—tum during -,Vasa summer -onions.) Carcinogen(, risk and hazard quotient cells highlighted In orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor Intrusion dsk, no risk values are calculated forthese chemicals. Henry's Covstant Calculated Indoor Air Indoor Av CalculatedNon- Groundwater Henrys Constant used f Indoor Av Scmening [,eve( Screenvtg Level Calculated Caroinogenic CAS# Chemical Name: Concevtratron a[25°C calculffiiovs Concentration for Carcinogens forNon- Carcinogenic Risk Hazard (ug/L) (dvnevsiovle 9) dira (evsiovless) @TCR=lEA6mo® Qmaevt (ap/mr) TH =0.2 156-59-2 Dichloroeth Irne, 1,2cis- 0.141 0.166802944 0A66802944 0.023519215 156-60-5 Dichkha t, 1,2-tmna- 0.383483238 0.383483238 127-184 Teuschloroeth lene 0.738 0.723630417 0.723630417 0.534039248 1.1E+01 8.3E+00 4.9E-08 1.3E-02 79-01.6 Trichloroeth lene 0.442 0.402698283 0.402698283 0.177992641 4.8E-01 4.2E-01 3.7E-07 8.5E-02 75-01-4 Vinyl Chlondc 1.136549469 1.136549469 1.7E-01 2.1E+01 Cumvlati— I 4.2E-07 9.8E-02 DSCA Indoor Air Risk Calculator -Cumulative Risk for Resident Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: Amenean Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Dale: 6/10/2020 Sample ID: MW-3 Average Groundwater Temperature(oC): 25 (Use de/euttef2VC unless sitespecirc data is available -firming the groundwatertemperature dung worst -case summercendillens.) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. Henrys Constant Cakulated Indoor Afr Indoor Aa Groundwater Henrys Constant used for Indoor A. Screening Level Screening Level Calculated CaleulatadNee- CAS# Chemical Name: Covoevtmdov at25°C calc.ionls Co(ug/reuov for Carcinogens for Nov- Caroinogenic Risk Carcinogenic (ug/L) (dimeneionlese) (dvnensiovless) (ug/m') ®TCR=18-06 CarHO-0. Q THO = 0.2 Hazffid Quotievt 75-354 Dichloroethvlene. 1.1- 0.241 1.067048242 1.067048242 0.257158626 4.2E+01 1.2E-03 156-59.2 Dichloroethvlene. I.Uis- 144 0.166802944 0.166802944 24.01962388 156-60-5 Dichloroethvlene. 1.2-taus- 1.53 0.383483238 0.383483238 0.586729354 127-18-4 Teuachloroethvlene 365 0.723630417 0.723630417 264.1251022 IAE+01 8.3E+00 2.4E-05 6.3E+00 76-13-1 Thohloro-1.2.2-tofluoroethane. 1.1.2. 1.55 21.50449714 21.50449714 33.33197056 1.0E+03 6.4E-03 79-01-6 Trichloroethvlrne 79.2 0.402698283 0.402698212 31.89370401 4.8E-0l 4.2E-0l 6.7E-05 1.5E+01 7NO Vint Chloride 3.58 1.136549469 1.136549469 4.068847097 1.7E-01 2.1E+01 2.4E-05 3.9E-02 Cumulative: I 1.2E-04 2.2E+01 DSCA Indoor Air Risk Calculator -Cumulative Risk for Resident Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: Amenean Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Dale: 6/10/2020 Sample ID: MW5 Average Groundwater Temperature(oC): 25 (Use deWftof2VC unless sitespecirc data is available —firming the groundwatertemperature during worst -case summercendillens.) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. Henrys Constant Cakulated Indoor Afr Indoor Groundwater Henrys Constant used for Indoor A. Screening Level Screening Level Calculated CaloulatedNon- CASq Chemical Name: Covicevtmdov at25°C calculations Co(ug/m tiov fm Carcinogens for Non- Carcinogenic Risk Carcinogenic (ug/L) (dimensiovlese) (dvnensiovless) (ug/m') ®TCR=1E06 —Ai Catch —0. Q THO = 0.2 Hazard Quotient 156-59-2 Dichloroethvlene. 1.2cis- 0.228 0.166802944 0.166802944 0.038031071 156-60.5 Dichloroethvlene, 1.2-mans- 0.383483238 0.383483238 127-184 TemechlomethAene 0.723630417 0.723630417 1.1E+01 8.3E+00 79-01.6 Tnchl—thvlene 0.402698283 0.402698283 4.8E-01 4.2E-01 75-014 VinA Chloride 1.136549469 1.136549469 1.7E-01 2.1E+01 Cumulative: I 0.0E+00 0.0E+00 DSCA Indoor Air Risk Calculator -Cumulative Risk for Resident Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: Amenean Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Dale: 6/10/2020 Sample ID: 2W-10 Average Groundwater Temperature(oC): 25 (Use deWftof2VC unless sitespecirc data is available -firming the groundrvalertemperature during worst -case summercendillens.) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. Henrys Constant Cakulated Indoor Afr Indoor Groundwater Henrys Constant used for Indoor A. Screening Level Screening Level Calculated CaloulatedNon- CASq Chemical Name: Covicevtmdov at25°C calculations Co(ug/m tiov fm Carcinogens for Non- Carcinogenic Risk Carcinogenic (ug/L) (dimensiovlese) (dvnensiovless) (ug/m') ®TCR=1E06 -Ai Catch -0. Q THO = 0.2 Hazard Quotient 156-59-2 Dichloroethvlene. 1.2cis- 101 0.166802944 0.166802944 16.8470973 156-60.5 Dichloroethvlene, 1.2-mans- 0.473 0.383483238 0.383483238 0.181387572 127-184 TemechlomethAene 18 0.723630417 0.723630417 13.02534751 1.1E+01 8.3E+00 1.2E-06 3.1E-01 79-01.6 Tnchl-thvlene 36.5 0.402698283 0.402698283 14.69848733 4.8E-01 4.2E-01 3.1E-05 7.0E+00 75-014 VinA Chloride 2.2 1.136549469 1.136549469 2.500408831 1.7E-01 2.1E+01 1.5E-05 2.4E-02 Cumulative: I 4.7E-05 7.4E+00 DSCA Indoor Air Risk Calculator -Cumulative Risk for Resident Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: Amenean Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Dale: 6/10/2020 Sample ID: 2W-11 Average Groundwater Temperature(oC): 25 (Use defvult of25° C unless sitespecirc data is available -firming the groundwatertemperature during worst -case summercendillens.) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. Henrys Constant Cakulated Indoor Afr Indoor Ai Groundwater Henrys Constant used for Indoor A. Screening Level Screening Level Calculated CaloulatedNon- CASq Chemical Name: Covicevtmdov at25°C calculadoos Concevtmtiov fm Carcinogens fm Non- Carcinogenic Risk Cmoinogenic (ug/L) (dimensiovlese) (dnnensionk.) (ug/m') ®TCR - IE-06 Carchrogens Q THO = 0.2 Hazard Quotient 156-59-2 Dwhlorecthvleuc. 1.2cis- 67.9 0.166802944 0.166802944 11.32591987 156-60.5 Dichloroethvlene, 1.2-mans- 0.292 0.383483238 0.383483238 0.111977105 127-184 TemachlomethAene 11.4 0.723630417 0.723630417 8.249386754 1.1E+01 8.3E+00 7.6E-07 2.0E-01 79-01.6 Tnchl-thvlene 24.2 0.402698283 0.402698283 9.745298446 4.8E-01 4.2E-01 2.0E-05 4.7E+00 75-014 VinA Chloride 1.43 1.136549469 1.136549469 1.62526574 1.7E-01 2.1E+01 9.7E-06 1.6E-02 Cumulative: I 3.1E-05 4.9E+00 DSCA Indoor Air Risk Calculator -Cumulative Risk for Resident Version 7, August 2019 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners, 210 South Estes Drive, Chapel Hill, Orange County, North Carolina Name/Address of Sampling Location: Olin T Binkley Memorial Church, 1712 Willow Drive, Chapel Hill, Orange County, North Carolina Sampling Dale: 6/10/2020 Sample ID: 2W-12 Average Groundwater Temperature(oC): 25 (Use deWftof2VC unless sitespecirc data is available -firming the groundwatertemperature during worst -case summercendillens.) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. Henrys Constant Cakulated Indoor Afr Indoor Groundwater Henrys Constant used for Indoor A. Screening Level Screening Level Calculated CalculetedNov- CASH Chemical Name: Cov(ug/L) ov a125°C calculations Co(ug/m tiov fm Carcinogens for Non- Caroinogenic Risk Carcinogenic (ug/L) (dimensiovlese) (dvnensiovless) (ug/m) ®TCR=1E06 -Ai Catch Q THO = 0.2 Hazffid Quotient 67-66-3 Chloroform 0.147 0.150040883 0.150040883 0.02205601 1.2E-01 2.0E+01 1.8E-07 2.2E-04 75-354 DichloroethYlrne. 1.1- 1.03 1.067048242 1.067048242 1.099059689 4.2E+01 5.3E-03 156-59-2 Diehlerecd lene. 1.2cis- 799 0.166802944 0.166802944 133.2755519 156-60.5 Dichloroethvlene. 1,2-mans- 5.31 0.383483238 0.383483238 2.036295993 127-184 Te-hlomethvlene 1340 0.723630417 0.723630417 969.6647588 1.1E+01 8.3E+00 9.0E-05 2.3E+01 76-13-1 Trichloro-1.2.2-uitluoroelhane. l.1.2- 1.8 21.50449714 2%50449714 38.70809485 1.0E+03 7.4E-03 79-01-6 Trichlomethvlene 226 0.402698283 0.402698283 91.8152085 4.8E-01 4.2E-01 1.9E-04 4.4E+01 75-014 Vinyl Chloride 1.136549469 1.136549469 1 1.7E-01 2.1E+01 Cumulative: I 2.8E-04 6.7E+0l ATTACHMENT 17 MANN-KENDALL TREND ANALYSIS MANN-KENDALL TOOLKIT for Constituent Trend Analysis Evaluation Date: June 2020 Job ID: 60628609 Facility Name: American Dry Cleaners (DC680002) Constituent: PCE Conducted By:AECOM Concentration Units: m /L Sampling PointlD: MW-2 I MW-3 I 2W-5 I 2W-6 I 2W-9 I 2W-10 I 2W-11 Sampling Event Sampling �. te PCE • • 1 09/23/08 40.7 5.134 2 01/30/09 31.57 3.073 0.991 0.903 3 10/21/10 4.63 1.89 1.95 0.427 4 01/21/11 40.4 1.86 4.15 0.346 5 04/29/11 48.4 1.42 3.35 3.41 6 07/18/11 34.0 1.3 3.4 3.00 7 08/30/11 40.0 1.8 0.082 2.90 8 09/22/11 30.0 1.7 0.65 1.70 9 10/18/11 0.125 2.5 0.005 2.50 10 11/18/11 40.0 4.4 0.0025 1.80 11 02/23/12 37.0 4.1 0.005 2.60 12 05/24/12 37.0 3.3 0.0005 3.0 13 09/04/12 35.0 6.6 0.0005 0.84 14 11/12/13 43.0 5.9 2.10 15 07/08/14 0.47 7.2 2.9 16 11/23/15 13.9 1.58 0.0005 0.316 3.1 0.312 17 12/12/16 0.62 0.22 0.053 0.074 18 12/19/18 14.2 0.176 0.0482 0.0178 19 06/10/20 0.365 0.0018 0.0114 20 Red text indicates one-half of laboratory detection limit. Coefficient of Variation 0.55 1 • - Mann -Kendall Statistic (S): Confidence Factor: ' Concentration Trend: Stable Stable Decreasing No Trend Decreasing Decreasing Decreasing 100 BMW-2 10 =MW-3 J �zw-5 � 1 -zw-s v 2W-9 C O 0.1 - -2W-10 R -zw-i 1 0.01 N C 0.001 - O C) 0.0001 02108 07/09 11/10 04112 08113 12114 05/16 09/17 02119 06/20 10/21 Sampling Date i Notes: 1. At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples. 2. Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>O) or decreasing (S<O): >95% = Increasing or Decreasing; >_ 90% = Probably Increasing or Probably Decreasing; < 90% and S>O = No Trend; < 90%, S:50, and COV >_ 1 = No Trend; < 90% and COV < 1 = Stable. 3. Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales, Ground Water, 41(3):355-367, 2003. DISCLAIMER: The GSI Mann -Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein. GSI Environmental Inc., www.gsi-net.com MANN-KENDALL TOOLKIT for Constituent Trend Analysis Evaluation Date: June 2020 Job ID: 60628609 Facility Name: American Dry Cleaners (DC680002) Constituent: TCE Conducted By:AECOM Concentration Units: m /L Sampling PointlD: MW-2 I MW-3 I 2W-5 I 2W-6 I 2W-9 I 2W-10 I 2W-11 Sampling Event Sampling �. te TCE • • 1 09/23/08 1.208 0.73 2.55 2 01/30/09 1.886 0.629 0.429 0.21000 3 10/21/10 0.451 0.392 0.399 0.214 4 01/21/11 3.1 0.408 1.77 0.33 5 04/29/11 2.76 0.319 1.63 0.316 6 07/18/11 2.6 0.42 0.990 0.350 7 08/30/11 3.6 0.51 0.280 0.320 8 09/22/11 2.4 0.53 0.320 0.190 9 10/18/11 0.125 0.67 0.005 0.250 10 11/18/11 3.2 0.96 0.0025 0.220 11 02/23/12 3.0 1.1 0.005 0.240 12 05/24/12 2.6 1.6 0.001 0.250 13 09/04/12 2.5 1.9 0.001 0.280 14 11/12/13 2.9 0.73 0.890 15 07/08/14 0.140 0.24 3.5 0.69 16 11/23/15 1.36 0.335 0.00108 0.129 4.27 2.26 17 12/12/16 0.21 0.11 0.049 0.21 18 12/19/18 1.69 0.0862 0.036 0.0121 19 06/10/20 0.0792 0.00365 0.0242 20 Red text indicates one-half of laboratory detection limit. Coefficient of Variation 0.52 1 • 0.60 Mann -Kendall Statistic (S): Confidence Factor: Concentration Trend: Stable No Trend Decreasing No Trend Decreasing Decreasing I No Trend 1 BMW-2 J -MW-3 _ 'F! -zw-s C1 �X `-� -zw-s 0.1 -2W-9 C 0 -2W-10 R 0.01 -2W-11 L r 0.001 O C) 0.0001 02108 07/09 11/10 04112 08113 12114 05/16 09/17 02119 06/20 10/21 Sampling Date Notes: 1. At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples. 2. Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing; >_ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S:50, and COV >_ 1 = No Trend; < 90% and COV < 1 = Stable. 3. Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales, Ground Water, 41(3):355-367, 2003. DISCLAIMER: The GSI Mann -Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein. GSI Environmental Inc., www.gsi-net.com ATTACHMENT 18 IDW DISPOSAL MANIFEST Please print or type. Fopn Approved. OMB No. 205M039 UNIFORM HAZARDOUS 1. Generator ID Number 2, Page 1 of 3. Emergency Response Phone 4. Manifest Tracking Number WASTE MANIFEST NICROW145706 1 1 255-31V443IMUM7As4 1 013311366 FL E 5. Generators Name and Mailing Address Generator's Site Address (if different than mejling address) Petitioner for DSl Ske DC` 2, Slaw-# 029 Ai<aeeracaaa Dirt' Cleaners DWM-DSCA 1646 Mail Se9iKip Cen-ter 201 S. rsies brave Genera rs o —91 -1100 Ralugh, NC 276-99-1646 Chapel Hill, ids. £7707 S® -ffl Ca29 6. Transporter l Company Name U.S. EPA ID Number !� 'y 5'Ag Sig ®o�FTS l� g+{ 9 { �yp��$ ,F—y § i'.�ITD a==ar JI'Mel ..F+_e'Wa far(S � i9-C SIC10198-5-5i"a&_'k2£ 7. Transporter 2 Company Name U.S. EPA ID Number 8. Designated Facility Name and Site Address U.S. EPA ID Number Crean Harbors Dee pa'aak, L.P. 2927 ladepepilence Parkway _ell ` 14-1378 Fadlit's Phone: 2 - 0-2300 La Porte ' 77571 I ¢ ga, 9b. U.S. DOT Description (including Proper Shipping Name, Hazard Class, ID Number, 10. Containers 11. Total 12. Unit HM and Packing Group (If any)) Ouantity WWoL 13. Waste Codes No. Type Cf.e.. 1. 's'l. x�-sa€S'si'i43s JC'�5$e E!3''gEs3r a,i7.s. X (etrasNorci a'flawr , 9, SGlii. ERG iff 171, W101 310 /(//Ic/✓1 P Z 2. Jul 3. 4. 14. Special Handlln Instructions an,,Additignal Info Non 9a_1} CH?92211 (liquids) I x _s%gall_ Emergency Res -pore¢_ Number #0B-25t� a- -324 jab# 2006-1 P 0# t00 Cuoraa.,;:Nu bar M60007950. 15. GENERATOWSIOFFEROR'S CERTIFICATION: I hereby declare that the contents of [his consignment are fully and accurately described above by the proper shipping name, and are classified, packaged, marked and labeled/placarded, and are In ail respects In proper condition for transport according to applicable International and national governmental regulations. If export shipment and I am the Primary Exporter, I certify that the contents of this consignment conform to the terms of the attached EPA Acknowledgment of Consent I cerfily that the waste minimization statement Identified in 40 CFR 26227(a) (if I am a large quantity generator) or (b) (if1 am a small quantity generator) is We. GemmtoesslOfierorl1s``Pdntedrryped Name r,.x )er �•�je,y 1;a heW D Signa� Month Day Year DGsA PC .huh0J ly <ifs : 6e,-0O 7 J i— 16. International Shipments ❑import to U.S. ❑Expartfrom U.S. Port ofentrylexit = Transporter signature (for exports only): Date leaving U.S.: W V. TrensporterAcknowledgmenl of Receipt of Materials Transporter 1 Pnntedlryped Name Signature Month , Day Year 5 // %S i 1+�4.`E. (,a1 /O d aTransporter 2 PrintedFryped Name Signature Month Day Year F 18. Discrepancy 18a. Discrepancy Indication Space ❑ Quantity ❑ Type ❑ Residue ❑ Paral Rejectlon Full Rejection Manifest Reference Number: 18b. Alternate Facility (or Generator) U.S. EPA ID Number J U LL Facility's Phone: 18c. Signature of Alternate Facility (or Generator) „ Month Day Year Q Z y19. Ha mndous Waste Report Management Method Codes (i.e., codes for hazardous waste treatment, disposal, and recycling systems) c 1. 2. 3. a. 20. Designated Facility Owner or Operator. Certification of receipt of hazardous materials covered by the manifestexcept as noted In Item 18a 1 Printedffyped Name Signature Month Day Year EPA Form 8700-22 (Rev. 12-M Previous editions are obsolete. DESIGNATED FACILITY TO EPA's e-MANIFEST SYSTEM CLEAN HARBORS ENVIRONMENTAL SERVICES, INC. LAND DISPOSAL RESTRICTION FORM LDRA MANIFEST NO OI? 3 �� 9l'grj ALE THE HAZARDOUS WASTES IDENTIFIED ON THE HAZARDOUS WASTE MANIFEST IDENTIFIED ABOVE AND BEARING THE EPA HAZARDOUS WASTE CODES LISTED BELOW ARE RESTRICTED WASTES WHICH ARE PROHIBITED FROM LAND DISPOSAL WITHOUT FURTHER TREATMENT UNDER THE LAND DISPOSAL RESTRICTIONS, 40 CFR PART 268.7 (a)(2), AND RCRA SECTION 3004(0). IN ACCORDANCE WITH 40 CFR 268.7(a), THE EPA WASTE CODE, WASTE SUBCATEGORY, AND TREATABILITY GROUPS, AS APPLICABLE, ARE INCLUDED BELOW. INSTRUCTIONS — COMPLETE ALL SECTIONS. REFER TO PAGE 3 OF THIS FORM FOR KEY TERMS/DEFINITIONS. Column 1 - Line Item: Enter the manifest line item number (e.g., 11a) that corresponds to the waste code(s). Column 2 - Waste Codes/Subcategory: Check off all applicable waste codes. For D001 through D043, also check applicable subcategory; for F001 through F005, check applicable constituents. Column 3 - Wastewater/Non-wastewater: Check off "WW" for wastewater and "Non-WW" for non -wastewaters. Column 4 - LDR Handling Code: Circle the appropriate handling code, as follows: 1 = The waste is a characteristic hazardous waste D001, D002, D003, D004-0011, or D018-43 which is intended for treatment/disposal in a CWA system, CWA-equivalent system, or Class I SDWA system. Underlying Hazardous Constituents (UHC's) are NOT required to be identified. 1A= The waste is a characteristic hazardous waste D001 High TOC Ignitable Liquids Subcategory (i.e., greater than or equal to lO %TOC). Pursuant to 40 CFR 268.40, the waste must be treated using organic recovery (RORGS) or combustion (CMBST) technology. UHC's are NOT required to be identified. 2 = The waste is a characteristic hazardous waste D001 (other than High TOC Ignitable Liquids), D002, D003 Explosive, Water Reactive or Other Reactive subcategory, D004-DO11. D012-17 non -wastewater, or D01 B-43 which is intended for treatment/disposal in a non-CWA system, non-CWA-equivalent system, or non -Class I SDWA system located in the United States. All UHC's which are reasonably expected to be present must be Identified, except for D001 waste that is Intended to be treated using organic recovery (RORGS) or combustion (CMBST) technologies. Identify UHC's by completing Sections I and IV of CHI Form LDR-1 Addendum and attach completed Addendum to this form. 3 = The waste is a characteristic (i.e., D-code) or listed (i.e., F-, K-, U-, or P-code) hazardous waste which is intended for export and treatmenUdisposal at a facility located outside the United States. LDR treatment standards do not apply to hazardous waste treated/disposed in a foreign country, and per USEPA guidance, the identification of UHC's (if applicable) is not required for hazardous waste that is intended to be exported. Note however that if the exported waste is subsequently returned for treatment/disposal in the United States, all applicable LDR regulations would apply and a revised LDR notification would be required. 4 = The waste meets the definition of hazardous debris pursuant to 40 CFR 268.2(h) and is intended for treatment/ disposal in compliance with the alternate debris treatment technologies of 40 CFR 268.45. In accordance With the requirements of 40 CFR 268.7(a)(2) : the contaminants subject to treatment (CSTT's) must be identified as part of this notification. Identify CSTTs by completing Section III and IV of the CHI Form LDR-1 Addendum and attach completed Addendum to this form. These constituents are being treated to comply with 40 CFR 268.45, 5 = The waste is a characteristic waste D003 Reactive Sulfide, Reactive Cyanide, or Unexploded Ordnance subcategory, a characteristic waste D012- 17 wastewater, or a listed (i.e., F-, K-, U-, or P-code) hazardous waste. UHC's are NOT required to be identified. 6 = The waste is a lab pack that is Intended for incineration using the alternative lab pack treatment standard under 40 CFR 268.42(c). UHC's are NOT required to be identified; however, the generator must complete and attach the lab pack certification statement on CHI Form LDR-LP. Note that in accordance with 40 CFR Part 268 Appendix IV, lab packs which contain waste codes 0009, F019, K003, K004, K005, K006, K062, K071, K100, K106, P010, P011, P012, P076, P078, U134, and U151 are not eligible for alternative lab pack treatment standard. =M= UnTC. IC TYC \IIII\CTC IC A CM.1 1.I,1J A 11—M Mn -AMA nT­n IhI A— 111M r„� r��,�r�•-'�r� SECTION I. CHARACTERISTIC WASTES D001 THROUGH D043 COLUMN 1: COLUMN 2: LINE ITEM WASTE CODE / SUBCATEGORY SEE MANIFEST [ ] DOOI Ignitables, except High TOC subcategory [ ] D001 High TOC Ignitable Liquids Subcategory (Greater than or equal to 10% TOC) [ ] D002 Corrosives [ ] D003 [ ] Reactive Sulfide, per 261.23 (a)(5) [ ] Reactive Cyanide, per 261.23(a)(5) [ ] Explosive, per 261.23(a)(6), (7) & (8) [ ] Water Reactive, per 261.23(a)(2), (3) & (4) [ ] Other Reactive, per 261.23(a)(1) [ j Unexploded Ordnance, Emergency Response [ ] D004 Arsenic [ ] D005 Barium [ ] D006 [ ] Cadmium [ ] Cadmium Containing Batteries [ ] D007 Chromium [ ] D008 [ ] Lead [ ] Lead Acid Batteries COLUMN 3: WASTEWATER/ NON -WASTEWATER []WW []Non-WW [ ] Non-WW only []WW []Non-WW [ ] WW [ ] Non-WW []WW []Non-WW [ ] WW [ ] Non-WW [ ] Non-WW only []WW []Non-WW []WW []Non-WW []WW []Non-WW [ ] WW [ ] Non-WW []WW []Non-WW [ ] Non-WW only [1WW []Non-WW []WW []Non-WW [ ]Non-WW only COLUMN 4: HANDLING CODE 1 2 3 4 6 1A 3 6 1 2 3 4 6 1 3 4 5 6 1 3 4 5 6 1 2 3 4 6 1 2 3 4 6 1 2 3 4 6 1 3 4 5 6 1 3 4 5 6 1 3 4 5 6 1 2 3 4 6 2 3 6 1 2 3 4 6 1 2 3 4 6 2 3 6 CHI Form LDR-1, Page 1 of 3 [Effective 2/28/00] CLEAN HARBORS ENVIRONMENTAL SERVICES, INC. LAND DISPOSAL RESTRICTION FORM LDR-1 MANIFEST NO O /33I/34f 4f Xr-E SECTION I. CHARACTERISTIC WASTES 0001-43 (CONTINUED) COLUMN 1: COLUMN 2: LINE ITEM WASTE CODE / SUBCATEGORY SEE MANIFEST [ ] D009 [ ] Low Mercury, less than 260 mg/kg Mercury [ ] High Mercury Organic Subcategory [ ] High Mercury Inorganic Subcategory [ ] D010 Selenium [ ] D011 Silver [ ] D012 Endrin [ ] D013 Undane [ ] D014 Methoxychlor [] D016 Toxaphene [ ] D016 2,4-D [ ] D017 2,4,5-TP (Silvex) [] D018 Benzene [ ] D019 Carbon tetrachloride [ ] D020 Chlordane [ ] D021 Chlorobenzene [ ] D022 Chloroform [ ] D023 o-Cresol [ ] D024 m-Cresol [ ] D025 p-Cresol [ ] D026 Cresol [ ] D027 1,4-Dichlorobenzene [ ] D028 1,2-Dichloroethane [ ] 0029 1,1-Dichloroethylene [ I D030 2,4-Dinitrotoluene [ ] D031 Heptachlor (and its epoxide) [ ] D032 Hexachlorobenzene [ ] D033 Hexachlorobutadiene [ ] D034 Hexachloroethane [ ] D035 Methyl ethyl ketone [ ] D036 Nitrobenzene [ ] D037 Pentachlorophenol [ ] D038 Pyridine [ ] D039 Tetrachloroethylene [ I D040 Trichloroethylene [ ] D041 2,4,5-Trichlorophenol [ ] D042 2,4,6-T6chlorophenol [ ] D043 Vinyl Chloride SECTION II. SPENT SOLVENT WASTES F001 THROUGH F005 COLUMN 1: COLUMN 2: LINE ITEM WASTE CODE / SUBCATEGORY SEE MANIFEST [ I Foot [,ZF002 [ ] F003 [ ] F004 [ ] F005 [ ] 1. ALL F001-F005 [ ] 2. Acetone [ ] 3. Benzene [ ] 4. n-Butyl alcohol [ ] 5. Carbon disulfide [ ] 6. Carbon tetrachloride [ ] 7. Chlorobenzene [ ] 8. o-Cresol [ ] 9. m-Cresol (difficult to distinguish from p-cresol [ ] 10. p-Cresol (difficult to distinguish from m-cresol) [ ] 11. Cresol - mixed isomers (sum of o-, m- and p-cresol) COLUMN 3: WASTEWATER/ NON -WASTEWATER [ ]WW [ ]Non-WW [ ] Non-WW only [ ] Non-WW only []WW []Non-WW []WW []Non-WW [IWW []Non-WW []WW I]Non-WW [ ] WW [ ] Non-WW []WW []Non-WW []WW []Non-WW []WW []Non-WW ( ] WW [ ] Non-WW [.]WW []Non-WW [ 1 WW [ 1 Non-WW []WW []Non-WW []WW []Non-WW [ ]WW [ ] Non-WW []WW []Non-WW []WW IINon-WW []WW [INon-WW []WW []Non-WW []WW []Non-WW [ I WW [ ]Non-WW [ ]WW [ 1 Non-WW []WW []Non-WW []WW [jNon-WW []WW []Non-WW []WW []Non-WW []WW []Non-WW []WW []Non-WW []WW []Non-WW []WW []Non-WW []WW []Non-WW []WW []Non-WW []WW []Non-WW [ ] WW [ ] Non-WW []WW []Non-WW COLUMN 3: WASTEWATER/ NON -WASTEWATER ( 1 WW Nor~ [ ] 12. Cyclohexanone [ ] 13. o-Dichlorobenzene [ ] 14.2-Ethoxyethanol(F005) only) [ ] 15. Ethyl acetate [ ] 16. Ethyl benzene [ ] 17. Ethyl ether [ ] 18. Isobutyl alcohol [ ] 19. Methanol [ ] 20. Methylene chloride [ ] 21. Methyl ethyl ketone [ ] 22. Methyl Isobutyl ketone f 1 23. Nitrobenzene [ ] 24. 2-Nitropropane (F005 only) COLUMN 4: HANDLING CODE 4 4 5 5 5 5 5 5 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 COLUMN 4: HANDLING CODE 3 4 fat 6 [ ] 25. Pyridine [ ] 26. Tetrachloroethylene [ ] 27. Toluene [ ] 28. 1,1,1-Trichloro- ethane [ ] 29.1,1,2-Trichloro- ethane [ ] 30. Trichloroethylene [ ] 31. 1,1,2-Trichloro- 1,2,2-trifluoroethane [ ] 32.Trichioromonofluoro- methane [ ] 33. Xylene - mixed isomers (sum of o-, m-, and p-xylene) CHI Form LDR-1, Page 2 of 3 [Effective 2128/00] CLEAN HARBORS ENVIRONMENTAL SERVICES, INC. p/33 ��T(of4 ,ALE LAND DISPOSAL RESTRICTION FORM LDR-1 MANIFEST NO SECTION III. CALIFORNIA LIST WASTES COLUMN 1: COLUMN 2: COLUMN 3: COLUMN 4: LINE ITEM WASTE CODE / SUBCATEGORY WASTEWATER/ HANDLING CODE SEE MANIFEST NON -WASTEWATER Hazardous waste containing one or more of the following [ ] W W [ ] Non-W W 1 2 3 4 6 California List constituents: [ ] ALL CALIFORNIA LIST CONSTITUENTS [ ] Liquids with nickel greater than or equal to 134 mg/I [ ] Liquids with thalllum greater than or equal to 130 mg/I [ ] Liquids with PCB's > or = 50 ppm [ ] Waste containing HOC's > or = 1,000 mg/kg SECTION IV. OTHER LISTED WASTES (F006-12 F019-F028 F037-38 F039 K- U- AND P-CODES) COLUMN 1: COLUMN 2: COLUMN 3: COLUMN 4: LINE ITEM WASTE CODE / SUBCATEGORY WASTEWATER/ HANDLING CODE SEE MANIFEST NON -WASTEWATER [] W W [] Non-W W 3 4 5 6 []WW []Non-WW 3 4 5 6 []WW []Non-WW 3 4 5 6 []WW []Non-WW 3 4 5 6 []WW []Non-WW 3 4 5 6 [ ] CHECK HERE IF ADDITIONAL LISTED WASTE CODES ARE PRESENT. COMPLETE AND ATTACH LDR-1 CONTINUATION SHEET. [ ] CHECK HERE IF WASTE CODE F039 (MULTISOURCE LEACHATE) IS PRESENT. IDENTIFY F039 CONSTITUENTS BY COMPLETING SECTIONS II AND IV OF CHI FORM LDR-1 ADDENDUM AND ATTACH COMPLETED ADDENDUM TO THIS FORM. SECTION V. CONTACT NAME AND DATE /�/)/ On behalf of DSCA �Pei�itioner Site ➢C(pg Q00z �,5 ""a/Z Print Name: N C✓ J " $ C P"I Date: 0� KEY TERMS/DEFINITIONS CLASS I SDWA SYSTEM means a Class I deep well facility regulated under the Safe Drinking Water Act (SDWA). CWA SYSTEM means a centralized wastewater treatment facility discharging under a Clean Water Act (CWA) permit. For example, a CWA facility would treat organic or inorganic aqueous wastes and discharge the treated effluent to the local sewer system. Examples of CWA treatment systems owned and operated by Clean Harbors include the wastewater treatment operations at Baltimore (including the CES system), Bristol, Chicago, Cincinnati and Cleveland. CWA-EQUIVALENT SYSTEM means a "zero discharge system" that engages in "CWA-equivalent" treatment before land disposal. Zeno - discharge facilities treat hazardous wastes using "CWA-equivalent" treatment methods, but do not discharge the treatment effluent to a sewer or water body (e.g., spray irrigation land farm). "CWA-equivalent" treatment methods means biological treatment for organics, alkaline chlorination, or ferrous sulfate precipitation for cyanide, precipitation/ sedimentation for metals, reduction of hexavalent chromium, or other treatment technology that can be demonstrated to perform equally or greater than these technologies. HIGH TOC IGNITABLE LIQUIDS SUBCATEGORY means an Ignitable liquid hazardous waste (waste code D001) which contains greater than or equal to 10% total organic carbon (TOC). Pursuant to 40 CFR 268.40, such wastes must be treated using organic recovery (RORGS) or combustion (CMBST) technology. Examples of RORGS technologies include the CES unit at Clean Harbors of Baltimore. Examples of CMBST technologies include hazardous waste fuel blending and subsequent reuse at a cement kiln, or destruction at a RCRA Incinerator. WASTEWATERS are wastes that contain less than 1% by weight total organic carbon (TOC) and less than 1% by weight total suspended solids (TSS). [See 40 CFR 268..2(f)] CHI Form LDR-1, Page 3 of 3 [Effective 2/28/001 ATTACHMENT 19 SOP - GROUNDWATER SAMPLING USING DISPOSABLE BAILERS ► ECOM AECOM — North Carolina Standard Operating Procedures Groundwater Sampling Using Disposable Bailers 1. Purpose and Scope Standard operating procedures to collect groundwater samples using disposable bailers. 2. Procedure 2.1 Required Equipment • HASP • Field Note Book and sampling logs. • Polypropylene rope, scissors (instrument to cut rope) • Bailer • Electronic water level indicator or oil -water interface probe • Collection container (5-gallon buck or similar container) • PPE • Sample bottles • Calculator • Water Quality Meter 2.2 Procedure 1. Review HASP. The field technician will don nitrile (or other HASP -approved gloves based on contaminants) gloves for all associated field work and sampling. 2. Open all wells to be sampled and allow equilibration time. Well caps should be placed adjacent to the monitoring wells on a clean area such as a small piece of plastic or towel. 3. Measure static water levels and total depth of well using the electronic water level indicator, or other similar device, and utilizing decontamination procedures to decontaminate the water level indicator before measuring water levels in the first well, between each well, and after completion of all water level measurements. 4. Calculate and record in the field book the volume of water in each well casing to be sampled. Sometimes this may be performed prior to field activity. Calculate borehole volume using formula: v = n r2 L Where: v = Volume L = Length of well, and r = Radius of well Groundwater Sampling Using Disposable Bailers () Revision June 7, 2017 PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET. 1/2 ► ECOM or use Cheat Sheet: Well Diameter (Inches) Gallons/Foot 2 0.16 3 0.37 4 0.65 5 1.02 6 1.47 7 2.00 8 2.61 9 3.30 10 4.08 12 5.87 14 8.00 16 10.50 18 13.20 20 16.30 24 23.50 36 52.90 5. Record the required purge volume in the field book (this should be three times the calculated volume of water in the well casing) and sample log. Purge at least the required volume of water from the monitoring well using a new or dedicated bailer and a new length of polypropylene rope secured tightly to the top of the bailer. 6. Place purge water in collection container for measurement purposes. Record in the field book the total amount of water purged from the well. Place purge water on ground, in 55- gallon drum or in other storage container as specified in work plan. If the well bails dry prior to the removal of three well volumes, record the amount of water purged, allow the well to recharge. It is not necessary to remove three well volumes from wells that bail dry. 7. Water level and water quality parameters (pH, specific conductance, dissolved oxygen and turbidity) need to be measured following purging. 8. Lower the bailer back into the well to collect sample. Place groundwater directly into laboratory supplied sample containers with appropriate preservatives (if required). If filtering is required for analysis, place water in unpreserved bottle, and request that laboratory filter sample. If additional groundwater is required to fill all necessary sample bottles, lower bailer back into well and collect additional groundwater. Seal container. 9. Label sample bottles — date, time, project identifier, sample location, depth (if required), required analysis, preservative (if used), and sampler's initials. Place samples in cooler with ice. Complete chain -of -custody form (supplied by the laboratory) and record site activities in field log book. Pack cooler for shipping or deliver samples to laboratory. Retain a copy of chain -of -custody and submit other copies with samples. Close and secure all wells. 3. Records List of the official records that are generated and support this procedure a. Field Notes b. Equipment Calibration Sheets AECOM Groundwater Sampling Using Disposable Bailers () Revision June 7, 2017 PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET. 2/2 ATTACHMENT 20 SOP - SOIL GAS SAMPLING tiLVMInnagine it. Del eed. AECOM — North Carolina Standard Operating Procedures Soil Gas Sampling 1. Purpose and Scope Standard operating procedure for the collection of soil gas samples using laboratory provided Summa canisters. 2. Procedure 2.1 Required Equipment: • Project Health and Safety Plan (HASP) • Work Plan • Summa Canister with a Flow Regulator from a certified laboratory (precalibrated for an 0.5 hour interval) • Field forms — Summa Canister Field Sampling Data Sheet • '/4" Stainless steel nuts and ferrules AMS Probe Kit or Hand Auger • 1/4" OD x 1/8" ID Teflon tubing • #2 driller sand Hydraulic cement or bentonite • Water • Ziplock bags Helium detector • Helium • Hand Vacuum Pump or Gilian GilAir Pump • Tedlar bags • Safety Cones • Laminated Sign to notify Air Sampling in progress • Chain of Custody (COC) • FedEx forms • Standard wrench set • Digital camera 2.2 AMS Soil Gas Sampling Method 1. Prior to sampling, locate any underground utilities to insure the safety of subsurface work conditions. 2. Use a 1'/2 inch stainless steel concrete bit and rotary hammer drill to core an entrance into the concrete or asphalt slab if needed. 3. Attach Teflon tubing to the barb tang of the retractable stainless steel screened soil gas vapor sampling tip. 4. Cut the tubing to the desired length so you can feed it through extra extension rods. 5. Attach the Retractable stainless steel screened soil gas vapor sampling tip to the extension rod. Place the extension drive adaptor to the opposite end of extension rod to protect threads when using the rotary hammer drill. Soil Gas Sampling (Rev1) Revision March 13, 2018 PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET. 1/4 AC^M Imagined. V Delivered. 6. Place the tip and the extension rod into the cored out hole and place the hammer drill in line with the extension drive adaptor. 7. Using the hammer drill, drive the tip and extension rod into the ground and add extension rods as needed to the desired depth beneath the ground surface. Fully tighten rods together to protect threads. 8. Using the jack supplied in the kit, jack out the extension rod a couple of inches to release the screen. 9. With the screen released, use a hand held vacuum pump to purge the subsurface air through the Teflon tubing. 10. After the soil gas vapor sampler is purged, connect the stainless steel summa canister to the Teflon tubing using air tight stainless steel fittings. Utilize the laboratory supplied flow controller to pull the sample over the desired time interval. 11. To remove the retractable stainless steel vapor sampling tip, use the jack supplied in the kit. Connect it under the extension drive adaptor and continue to jack the tip out of the ground fully. 12. Dissassemble the stainless steel vapor sampling tip. 13. Remove the Teflon tubing from the barb tang at the top of tip and dispose of the tubing. 14. Decontaminate the tip with soap that does not affect environmental parameters (Liquinox) and use a soft -bristle brush to wash away all dirt from the extensions and tip parts. Rinse with clean fresh water and let air dry. 2.3 Permanent Soil Gas Vapor Sampler: Permanent sampling tips can also be installed using the same method as described above. However, a different sampling tip is installed. The tip shown above is a permanent tip that can be used for multiple vapor monitoring events. The design is the same but uses a Teflon umbrella to seal the screen into place. (Bentonite can also be placed in the hole above the screen to provide a tighter seal for a longer period of time). Sampling from the permanent tips can be performed using the method described above. AECOM Soil Gas Sampling (Rev1) Revision March 13, 2018 PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET. 2/4 ACVM Imagine it. V Delivered. 2.4 AMS Vapor Implants Sampling Method 1. Prior to sampling, locate any underground utilities to insure the safety of subsurface work conditions. 2. Use a clean, stainless steel hand auger to auger down to the desired depth of soil gas vapor sampling beneath the ground surface. Note: Vapor implant should not be placed in saturated soils. 3. Attach Teflon tubing to the barbed tang of a 6" AMS Vapor Implant (AMS Item #21010). Make sure that the connection between the barbed end of the implant and the Teflon tubing is secure. 4. Lower the AMS Vapor Implant and attached tubing into the borehole until the Implant reaches the desired depth. The top of the vapor implant should be a minimum of five feet below ground surface. 5. Cut the tubing to the desired length so that you have approximately 2' of extra tubing to attach to the summa canister. 6. Using #2A filter sand, add enough sand to cover the 6" Implant and 2-3" above the Implant. Check the depth of sand using a measuring tape. 7. Add 10-12" of hydraulic cement or bentonite to the top of the sand to create a seal. Check the depth of sand using a measuring tape. If using bentonite, hydrate the bentonite to ensure a proper seal. Wait 2 hours or until the hydraulic cement has fully hardened, whichever is longer. 8. Use a hand held vacuum pump to purge the subsurface air through the Teflon tubing. Purge a minimum of one pore volume of the borehole. The pore volume should be a minimum of the volume of the tubing and sand filter pack. Calculate pore volume using formula: v = Tr ra2La + Tr rt2Lt where: v = Volume La = Length of sand -filled annular space, and ra = Radius of annular space Lt = Length of tubing, and rt = Radius of tubing 9. Thread the tubing through the helium leak test device (helium chamber). 10. Attach the helium detector to the helium leak test device. Attach the helium container to the leak test device using teflon tubing and fill the leak test device with helium until the helium detector reads >50%. 11. Use the hand pump to fill a 1 Liter tedlar bag with air from the sample port. 12. Close the tedlar bag and detach it from the pump. 13. Turn off the flow of helium into the helium leak test device. 14. Remove the helium detector from the leak test device and allow the helium detector reading to reach 0 ppm. 15. Insert the helium detector into the silicon tubing attached to the tedlar bag and open valve on the bag. 16. Record the reading. If the reading is below 10% of the value measured within the test device, proceed to the next step. If the reading is above 10%, repeat the leak test and reconstruct the sample point as necessary. AECOM Soil Gas Sampling (Rev1) Revision March 13, 2018 PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET. 3/4 Ima ine it. tiCVM Delge ed. 17. Be sure that the valve to the tedlar bag is open and that nothing is blocking the flow to the helium detector. The detector may produce false readings if the detector pump is strained or if methane is present in the soil gas. 18. After the helium test has been satisfactorily completed and soil gas vapor sampler is purged, connect the stainless steel summa canister to the Teflon tubing using air tight stainless steel fittings. Utilize the laboratory supplied flow controller to pull the sample over the desired time interval. 19. To remove the stainless steel Implant, break up the hydraulic seal. Tug gently on the Teflon tubing until the Implant is freed. 20. Remove the Teflon tubing from the barb and dispose of the tubing and the disposable stainless steel Implant. 21. Backfill borehole. Records a. Summa Canister Field Data Sheet b. Equipment Calibration Sheets 4. Attachments a. Summa Canister Field Data Sheet AECOM Soil Gas Sampling (Rev1) Revision March 13, 2018 PRINTED COPIES ARE UNCONTROLLED. CONTROLLED COPY IS AVAILABLE ON COMPANY INTRANET. 4/4 Summa Canister Sampling Field Data Sheet Site: Sam[ Date: Sample# Location Summa Canister ID Flow Controller ID Additional Tubing Added NO/ YES - How much NO/ YES - How much NO/ YES - How much NO/ YES - How much NO/ YES - How much Purge Time (Start) Purge Time (Stop) Total Purge Time (min) Purge Volume PID Test of Purge Air Initial Tracer Gas Results Pressure Gauge - before sampling Sample Time (Start) Sample Time (Stop) Total Sample Time (min) Pressure Gauge - after sampling Sample Volume Canister Pressure Went to Ambient Pressure? YES / NO YES / NO YES / NO YES / NO YES / NO Final Tracer Gas Results Associate Ambient Air Sample Number General Comments: