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HomeMy WebLinkAbout22047_University Place Mall_DC680002_20190307_IA, SG, and GW ReportAECOM AECOM Technical Services of North Carolina, Inc. 919.461.1100 tel 1600 Perimeter Park Drive, Suite 400 919.461.1415 fax Morrisville, NC 27560 March 7, 2019 North Carolina Department of Environmental Quality Division of Waste Management — DSCA Program 1646 Mail Service Center Raleigh, NC 27699 Att: Mr. Mike Cunningham DSCA Project Manager Re: Indoor Air, Soil Gas, and Groundwater Sampling Report American Dry Cleaners DSCA Site ID #DC680002 201 South Estes Drive, Chapel Hill, Orange County, North Carolina Dear Mr. Cunningham: AECOM Technical Services of North Carolina, Inc. (includes legacy URS and legacy AECOM herein referred to as AECOM) is pleased to provide the attached Indoor Air, Soil Gas, and Groundwater Sampling Report for the American Dry Cleaners (#DC680002) site located at 201 South Estes Drive, Chapel Hill, North Carolina. This report includes documentation pertaining to the indoor air and soil gas sampling activities that were completed at the site in June and December 2018, as well as follow-up indoor air sampling events completed in January and February 2019. In addition to the soil gas and indoor air sampling activities, this report also includes the findings of a limited groundwater sampling event completed in December 2018. The activities documented herein were completed in accordance with State Lead Authorization for Work (SLAW) 027, as approved on February 9, 2018, and change order 027A, approved on January 31, 2019. Due to the potential risk of vapor intrusion from tetrachloroethene (PCE) contaminated groundwater to affect indoor air quality at the western portion of the Olin T. Binkley Church, periodic monitoring of soil gas and indoor air quality was implemented in June 2017. This included the installation and sampling of two permanent soil gas sampling points (SV-5 and SV-6) at the locations shown on Attachment 14. Comprehensive information specific to the installation and initial sampling of soil gas sampling points SV-5 and SV-6 in December 2016 is on file in the Groundwater and Vapor Monitoring Report, dated January 18, 2018. Pursuant to SLAW 027, soil gas sampling points SV-5 and SV-6 were sampled on June 15, 2018, and December 19, 2018. During both sampling events soil gas sampling point SV-6 produced moisture in the tubing indicating that the soil gas sampling point was most likely flooded from infiltrate from the surface. AECOM plans to reinstall soil gas sampling point SV-6 during the June 2019 sampling event. The soil gas samples collected from SV-5 were analyzed for five DSCA contaminants of concern: PCE, trichloroethene (TCE), cis-1,2-dichloroethene (DCE), trans-1,2-DCE, and vinyl chloride using EPA Method TO-15 LL. A summary of the soil gas quality results, as entered into the DSCA risk calculators, is provided as follows: SV-5 (6/15/18) — non-residential worker o Unacceptable cumulative carcinogenic risk of 1.6E-04; and, o Unacceptable hazard index of 54. SV-5 (6/15/18) - resident o Unacceptable cumulative carcinogenic risk of 2.9E-03; and, o Unacceptable hazard index of 680. AECOM Mr. Mike Cunningham American Dry Cleaners — DC680002 March 7, 2019 Page 2 of 5 SV-5 (12/19/18) — non-residential worker o Unacceptable cumulative carcinogenic risk of 1.1E-04; and, o Unacceptable hazard index of 34. SV-5 (12/19/18) - resident o Unacceptable cumulative carcinogenic risk of 1.8E-03; and, o Unacceptable hazard index of 430. Permanent soil gas points SV-5 and SV-6 were installed to monitor soil gas in relation to indoor air concentrations. Since SV-5 was installed in June 2017, concentrations of PCE have increased from 75,000 micrograms per liter (µg/m3) to 120,000 µg/m3 in December 2018. TCE concentrations have remained steady ranging from 24,900 µg/m3 to 24,000 µg/m3, with the exception of June 2018 at 40,000 µg/m3. Due to water in the tubing during the June and December 2018 sampling events, limited data are available for SV-6. Concentrations of PCE have increased from 3,850 µg/m3 to 21,000 µg/m3 in between June and December 2018. TCE concentrations increased from 484 µg/m3 to 3,300 µg/m3 between June and December 2018. As part of continued evaluation of potential vapor intrusion risk to the preschool located at the Olin T. Binkley Church, two indoor air samples (IA-2 and IA-3) were collected concurrent with the soil gas samples in June and December 2018. Each indoor air sample was collected using a passive Radiello sampler deployed for a period of 7 days from within the preschool located at the Olin T. Binkley Church. Sampling results and locations are shown on Attachment 14. A summary of the indoor air quality results, as entered into DSCA risk calculators, is provided as follows: • IA-2 (6/8/18 - 6/15/18) — non-residential worker o Acceptable cumulative carcinogenic risk of 5.9E-08; and, o Acceptable hazard index of 0.016. • IA-2 (6/8/18 - 6/15/18) - resident o Cumulative carcinogenic risk less than 1E-06 (2.6E-07); and o Cumulative hazard index is less than 1 (0.067). • IA-2 (12/14/18 - 12/21/18) - non-residential worker o Cumulative carcinogenic risk less than 1E-06 (7.3E-07); and o Cumulative hazard index is less than 1 (0.24). • IA-2 (12/14/18 - 12/21/18) - resident o Cumulative carcinogenic risk between 1E-05 and lE-06 (4.4E-06); and o Cumulative hazard index is 1 (1.0) • IA-3 (6/8/18 - 6/15/18) - non-residential worker o Cumulative carcinogenic risk less than 1E-06 (6.1E-08); and o Cumulative hazard index is less than 1 (0.017). • IA-3 (6/8/18 - 6/15/18) - resident o Cumulative carcinogenic risk less than 1E-06 (2.7E-07); and o Cumulative hazard index is less than 1 (0.07). • IA-3 (12/14/18 - 12/21/18) - non-residential worker o Cumulative carcinogenic risk less thanlE-06 (8.3E-07); and o Cumulative hazard index is less than 1 (0.27). AECOM Mr. Mike Cunningham American Dry Cleaners — DC680002 March 7, 2019 Page 3 of 5 IA-3 (12/14/18 - 12/21/18) - resident o Cumulative carcinogenic risk is between 1E-05 and 1E-06 (4.9E-06); and o Cumulative hazard index is greater than 1 (1.1). The analytical results of the December 2018 sampling event indicated an exceedance of acceptable risk for residential exposure, as calculated using the DSCA Risk Calculator. AECOM discussed the December 2018 indoor air sampling results with Mr. Mike Cunningham of DSCA, and recommended to immediately resample the designated indoor air sampling locations to confirm if the December 2018 indoor air sampling data was representative of actual indoor air quality or possibly attributable to extraneous factors such as fugitive emissions from products containing similar contaminants, and/or materials introduced into the vicinity of the sample locations. Two indoor air samples (IA-2 and IA-3) were collected in January and February 2019 using 7-day Radiello samplers. A summary of the indoor air quality results, as entered into DSCA risk calculators, is provided as follows: • IA-2 (1/11/19 - 1/18/19) — non-residential worker o Cumulative carcinogenic risk less than 1E-06 (5.9E-07); and o Cumulative hazard index is less than 1 (0.2). • IA-2 (1/11/19 - 1/18/19) - resident o Cumulative carcinogenic risk between 1E-05 and 1E-06 (3.6E-06); and o Cumulative hazard index is less than 1 (0.83). • IA-2 (2/8/19 - 2/15/19) - non-residential worker o Cumulative carcinogenic risk less than 1E-06 (5.9E-07); and o Cumulative hazard index is less than 1 (0.2). • IA-2 (2/8/19 - 2/15/19) - resident o Cumulative carcinogenic risk between 1E-05 and 1E-06 (3.6E-06); and o Cumulative hazard index is less than 1 (0.83). • IA-3 (1/11/19 - 1/18/19) - non-residential worker o Cumulative carcinogenic risk less than 1E-06 (5.2E-07); and o Cumulative hazard index is less than 1 (0.17). • IA-3 (1/11/19 - 1/18/19) - resident o Cumulative carcinogenic risk between 1E-05 and 1E-06 (3.1E-06); and o Cumulative hazard index is less than 1 (0.73). • IA-3 (2/8/19 - 2/15/19) - non-residential worker o Cumulative carcinogenic risk less than 1E-06 (5.7E-07); and o Cumulative hazard index is less than 1 (0.19). • IA-3 (2/8/19 - 2/15/19) - resident o Cumulative carcinogenic risk is between 1E-05 and 1E-06 (3.5E-06); and o Cumulative hazard index is less than 1 (0.81). In addition to the collection of the Radiello samples deployed over a duration of seven days, AECOM deployed two 8-hour summa samples (IA-2 [8-hr] and IA-3 [8-hr]) within the two designated indoor air sampling locations on January 11, 2019. Results from the January 2019 re -sampling were received by AECOM on January 24, 2019, and indicated that contaminant concentrations were lower than that observed in December 2018 and within acceptable calculated risk levels for residential exposure. Results are shown on Attachment 14. A summary of the indoor air quality results, as entered into DSCA risk calculators, is provided as follows: AECOM Mr. Mike Cunningham American Dry Cleaners — DC680002 March 7, 2019 Page 4 of 5 • IA-2 (1/11/19) — non-residential worker o Cumulative carcinogenic risk less than 1E-06 (8.OE-08); and o Cumulative hazard index is less than 1 (0.025). • IA-2 (1/11/19) - resident o Cumulative carcinogenic risk less than 1E-06 (4.4E-07); and o Cumulative hazard index is less than 1 (0.11). • IA-3 (1/11/19) - non-residential worker o Cumulative carcinogenic risk less than 1E-06 (TOE-08); and o Cumulative hazard index is less than 1 (0.022). • IA-3 (1/11/19) - resident o Cumulative carcinogenic risk less than 1E-06 (3.8E-07); and o Cumulative hazard index is less than 1 (0.091). When comparing the 8-hour summa samples to the Radiello samples, concentrations of PCE and TCE are generally similar. Overall, PCE and TCE concentrations from the summa samples are slightly lower relative to the concentrations of the Radiello samples. Indoor air sampling results are summarized on Attachment 14. On December 19, 2018, AECOM performed a limited groundwater sampling event pursuant to work authorized under SLAW027, dated February 9, 2018. Sampling was completed using standard purge and sample techniques, in accordance with standard purge methods. An updated potentiometric surface contour map using depth to water levels gauged on December 19, 2018, is included as Attachment 6. Laboratory analysis of the groundwater samples indicated the presence of chlorinated volatile organic compounds (CVOCs) above NC 2L Groundwater Quality Standards in monitoring wells MW-2, 2W-9, 2W-10, and 2W-11. A groundwater quality summary map is included as Attachment 7. Groundwater analytical data is summarized in ADT Table 8. During the December 2018 groundwater sampling event, an older monitoring well installed by Withers and Ravanel (2W-8) was observed to be damaged. Monitoring well 2W-8 is located within the entryway to the shopping center and is north of the contaminant plume. The well has been sampled two times (December 2007 and November 2013), with only a trace level of TCE (0.00032 J micrograms per liter) detected during the November 2013 sampling event. The well appeared to be filled with sediment and a water level meter could not be advanced down the well likely indicative of a cracked PVC casing. AECOM recommended to DSCA that this well should be properly abandoned in order to reduce the likelihood of storm water impacts to the monitoring well and comply with NCAC 2C guidelines. On February 14, 2019, 2W-8 was abandoned by Regional Probing Services, a North Carolina Licensed Well Driller. The well abandonment record is included as Attachment 5. According to the Mann -Kendall Trend Analysis worksheets, included in Attachment 18, concentrations of PCE are stable in monitoring well MW-2, and decreasing in monitoring wells 2W-9, 2W-10, and 2W- 11. Additionally, concentrations of TCE are stable in monitoring well MW-2, decreasing in 2W-9, and demonstrate no trend in 2W-10 and 2W-11. Concentrations of PCE and TCE indicated groundwater concentrations continue to decrease during the December 2018 sampling event. As documented above, soil gas contaminant concentrations continue to present an unacceptable cumulative carcinogenic risk and hazard index, the indoor air samples collected in June 2018were within acceptable residential exposure ranges. The December 2018 indoor air samples indicated an exceedance AECOM Mr. Mike Cunningham American Dry Cleaners — DC680002 March 7, 2019 Page 5 of 5 of residential risk. Two additional indoor air sampling events were completed in January 2019 and February 2019 to determine if concentrations remained above acceptable risk levels. Both confirmatory sampling events indicated indoor air concentrations of PCE and TCE had slightly decreased, and acceptable risk levels for residential use. Due to the continued potential risk of vapor intrusion, semiannual indoor air sampling and soil gas sampling should continue in 2019. The work was done in accordance with AECOM Contract N16004, dated January 3, 2017, and in accordance with the scope and estimates provided in the approved SLAW027. If you have any questions or require additional information, please do not hesitate to call either Rob MacWilliams at 704-499-4839 or Nick Shore at 919-461-1485. Sincerely, AECOM TECHNICAL SERVICES OF NORTH CAROLINA, INC. Nick Shore, PG Project Manager Enclosures Robert H. MacWilliams, PG Program Manager ANALYTICAL DATA TABLES Analytical Data Tables for North Carolina Dry -Cleaning Solvent Cleanup Act Program Facility Name: American Dry Cleaners 201 South Estes Drive, Chapel Hill, Orange County DSCA ID No.: DC680002 Submittal Date: March 2019 Prepared By: AECOM Technical Services of North Carolina, Inc. 1600 Perimeter Park Drive, Suite 400, Morrisville, North Carolina Table of Contents DSCA ID No.: DC680002 Table/ Att. No. Check box Description if included Tables Table 1 Site Chronology 0 Table 2 Analytical Data for Soil ❑ Table 3 Analytical Data for Sub -slab Gas ❑ Table 4 Analytical Data for Soil Gas 0 Table 5 Analytical Data for Indoor and Outdoor Air 0 Table 6 Monitoring Well Construction Data 0 Table 7 Groundwater Elevation Data 0 Table 8 Analytical Data for Groundwater 0 Table 9 Analytical Data for Surface Water ❑ Table 10 Water Well(s) Survey Data ❑ Table 11 Analytical Data for Water Supply Well(s) ❑ Table 12 Analytical Data for Natural Attenuation Parameters ❑ Attachments Att. 1 Site map showing location(s) of soil boring(s). ❑ Att2 Soil contaminant concentration maps showing the concentration at each sampling point. ❑ Att. 3 Soil isoconcentration maps. ❑ Att. 4 Site map showing location(s) of monitoring well(s). ❑ Att. 5 Well completion diagrams and records of construction submitted to state. 0 Att. 6 Groundwater gradient map for each sampling event. 0 Att. 7 PCE concentration map showing the concentration at each sampling point and isoconcentration map. However, if there are significant plumes for other dry- cleaning contaminants, contaminant concentration maps for each chemical of concern should be included. 0 Att. 8 Groundwater concentration trend plots. ❑ Att. 9 Map showing location(s) of surface water sample(s) (if applicable). ❑ Att. 10 Surface water concentration map showing the concentration at each sampling point (if applicable). Att. 11 USGS Quad map with plotted water well location(s) within the 1,500 foot and 0.5 mile radii of the site (if applicable). ❑ Att. 12 Site map showing location(s) of monitoring well(s) for natural attenuation parametc ❑ Att. 13 Site map showing location(s) of indoor air, outdoor air, or soil gas samples. ❑ Att. 14 Air and soil gas concentration map showing the concentration at each sampling point. 0 Att.15 Signed laboratory analytical reports including chain -of custody and quality assurance/quality control (QA/QC) documentation (only if not previously submitted). 0 Att. 16 DSCA Program Risk Calculators 0 Att. 17 Indoor Air Building Survey Form 0 Att. 18 Mann -Kendall Trend Analysis 0 Att. 19 ❑ Att. 20 ❑ Att. 21 ❑ Note: 1. All maps must include a bar scale, north arrow, site name, DSCA ID No., and date. Table 1: Site Chronology DSCA ID No.: DC680002 Chronology of Events Date Instructions: Brief description of all significant events that have occurred since a problem was suspected at the facility. Commence with the first date a problem was suspected and continue through the most recent activity described in the current report. 04/01/95 Chlorinated compounds detected by Withers & Ravenel (W&R) during removal and closure of Underground Storage Tanks. 05/01/95 W&R complete preliminary investigation, install one monitoring well at the site. 08/08/95 W&R conduct Phase II Investigation, install eight monitoring wells as the site. 02/01/96 W&R complete Phase III Investigation, excavating a total of 400 cubic yards of contaminated soil. 12/06/07 ECS Carolinas, LLP conduct groundwater assessment. 07/10/08 W&R sampled existing wells and prepared Prioritization Assessment Report. 10/22/08 W&R installed five off -site monitoring wells on neighboring Olin T. Binkley Church property. Report on this date documents these activities. 02/17/09 W&R authorized to conduct aggressive fluid vapor recovery event. Report on this date documents these activities and result of post AFVR groundwater monitoring. Site placed in quarterly monitoring by DSCA program. 04/17/09 Second AFVR event authorized and post event groundwater monitoring documented in report issued on this date. 08/04/09 Groundwater monitoring report submitted to DSCA. 11/11/09 Third AFVR event authorized and post event groundwater monitoring documented in report issued on this date. 02/19/09 Groundwater monitoring report submitted to DSCA. 04/15/10 Fourth AFVR event authorized and post event groundwater monitoring documented in report issued on this date. 05/27/10 Outdoor air, indoor air and sub slab vapor sampling on church property documented in report issued on this date. 08/17/10 First semi-annual indoor air monitoring event at church documented in report issued on this date. 09/14/10 Groundwater monitoring report submitted to DSCA. 12/01/10 Fifth AFVR event authorized and post event groundwater monitoring documented in report issued on this date. 02/21/11 Groundwater monitoring report submitted to DSCA. 02/23/11 Second semi-annual indoor air monitoring event at church documented in report issued on this date. 03/08/11 Soil vapor sampling report for Harris Teeter property to the west. 06/09/11 W&R completes underground injection control permit application to inject Adventus product EHC, and receives UIC permit to conduct pilot test. 06/13/11 Groundwater monitoring report submitted to DSCA. 06/30/11 Indoor air sampling at Harris Teeter documented in report issued on this date. O1/07/12 Draft injection pilot test (three month post injection) issued on this date. 11/07/12 One-year post injection pilot test report issued on this date. 04/15/13 W&R conducts hydrogeological study to find permeable saturated zone for injection on church property. Bedrock was encountered above the surficial water table at most geoprobe drilling locations, which would preclude use of geoprobe to do injection. Report issued on this date documents the study and findings. 09/24/13 End of W&R involvement in project due to expiration of contract. 11/12/13 Groundwater Sampling Event, conducted by AECOM. 12/6/13 - 12/13/13 Indoor/Outdoor Air Sampling Event, Conducted by AECOM. Page 1 of 2 Table 1: Site Chronology DSCA ID No.: DC680002 Chronology of Events Date Instructions: Brief description of all significant events that have occurred since a problem was suspected at the facility. Commence with the first date a problem was suspected and continue through the most recent activity described in the current report. 02/07/14 Groundwater Sampling Event, conducted by AECOM. 06/27/14 Installation of 4 groundwater monitoring wells 2W-9, 2W-10, 2W-11, and 2W-12 07/08/14 Groundwater Sampling Event, conducted by AECOM. 08/22/14 Soil gas sampling event, conducted by AECOM 03/19/15 Indoor Air Sampling Event, conducted by AECOM 06/17/15 Indoor Air Sampling Event, conducted by AECOM 1 1/23/15 Groundwater samples collected from wells MW-2, MW-3, 2W-4, 2W-5, 2W-9, 2W-10, 2W-11, and 2W-12. O1/11/16 Indoor Air Sampling Event, conducted by AECOM 06/06/16 Indoor Air Sampling Event, conducted by AECOM 12/12/16 Indoor Air (IA-2 and IA-3), Soil Vapor (SV-5 and SV-6), and Groundwater Sampling (MW-2, 2W-9, 2W-10, and 2W- 11) Event, conducted by URS. Two new soil vapor points (SV-5 and SV-6) were installed in the playground area of the Olin T. Binkley Memorial Church. 6/20/17 - 6/28/17 Indoor Air (IA-2 and IA-3) and Soil Vapor (SV-5 and SV-6) sampling event was conducted by AECOM. 12/12/17 - 12/18/17 Indoor Air (IA-2 and IA-3) and Soil Vapor (SV-5 and SV-6) sampling event was conducted by AECOM. 06/08/18 - 06/15/18 Indoor Air (IA-2 and IA-3) and Soil Vapor (SV-5) sampling event was conducted by AECOM. Soil vapor sampling point SV-6 had moisture in tubing and was not able to be sampled. 12/19/18 A soil vapor (SV-5) and limited groundwater sampling event of four wells (MW-2, 2W-9, 2W-10, and 2W-11) was conducted by AECOM. Soil vapor sampling point SV-6 had moisture in tubing and was not able to be sampled. 12/14/18 - 12/21/18 Indoor Air (IA-2 and IA-3) and Soil Vapor (SV-5) sampling event was conducted by AECOM. 01/11/19 - O1/18/19 Confirmatory 7-day indoor air samples (IA-2 and IA-3) were collected via Radiello samplers, and samples (IA-2[8-hr] and IA-3[8-hr]) were collected via 6-liter summa canisters on January 11, 2019. '02/08/19 - 02/15/19 Confirmatory 7-day indoor air samples (IA-2 and IA-3) were collected via Radiello samplersby AECOM. 02/14/19 Damaged monitoring well 2W-8 was abandoned by an NC Licensed Drilling contractor. Page 2 of 2 Table 4: Analytical Data for Soil Gas DSCA ID No.: DC680002 N ' N N A i O M iL p iL iL Q� U W O N Q In/m3] SV-1 4 0.5h 03/01/11 NA 31.3 NA NA NA 361 NA <1.3 147 13.8 NA NA SV-2 4 0.5h 03/01/11 NA <1.5 NA NA NA <2.5 NA <1.5 <2.0 <0.94 NA NA SV-3 4 0.5h 03/01/11 NA <1.4 NA NA NA 16.9 NA <1.4 1.8 <0.87 NA NA SV-4 3 0.5h 03/01/11 NA 1.6 NA NA NA <1.4 NA 10.1 5.5 <0.87 NA NA 7 0.5h 12/12/16 NA 16,000 NA NA NA 150,000 NA 410 35,000 1 <5.1 NA NA 7 0.5 h 06/28/17 NA 9,740 NA NA NA 75,800 NA 347 24,900 <10.2 NA NA SV-5 7 0.5 h 12/12/17 NA 11,000 NA NA NA 86,000 NA 260 23,000 <5.1 NA NA 7 0.5 h 06/15/18 NA 18,000 NA NA NA 140,000 NA 480 40,000 <51 NA NA 7 0.5 h 12/19/18 NA 9,800 NA NA NA 120,000 NA 390 24,000 <38 NA NA 7 0.5h 12/12/16 NA 880 NA NA NA 31,000 NA 190 4,800 <5.1 NA NA SV-6 7 0.5 h 06/28/17 NA 262 NA NA NA 3,850 NA 154 484 <1.02 NA NA 7 0.5 h 12/12/17 NA 830 NA NA NA 21,000 NA 98 3,300 <5.1 NA NA SGOI 3.33 0.5h 07/09/14 NA 19 NA NA NA 330 NA <1.2 110 1 <0.77 NA <1.2 SG02 3.33 0.5h 07/09/14 NA 180 NA NA NA 130,000 NA <140 920 <90 NA <140 SG03 3.33 0.5h 07/09/14 NA <22 NA NA NA 11,000 NA <22 70 <14 NA <22 Indicate "G" for grab sample or for longer samples indicate the number of hours followed by "h". Page 1 of I Table 5: Analytical Data for Indoor and Outdoor Air DSCA ID No.: DC680002 A C O m^ Q N N y « W L t o Td o r itl O y 3 05/04/10 AD SU 8h ND ND ND ND NA 9.3 7.3 ND ND ND ND IA -I 07/22/10 AD P 7d NA ND NA NA NA 14 NA ND 0.93 ND NA 01/28/11 AD P 7d NA 0.13 NA NA NA 6.1 NA ND 6.6 ND NA 05/04/10 AD SU 8h ND ND ND ND NA 7.4 7.4 ND 10.8 ND ND 08/23/11 AD P 34d NA 0.14 NA NA NA 10.0 NA ND 1.0 ND NA 08/30/11 AD P 7d NA 0.33 NA NA NA 11.0 NA ND 1.3 ND NA 09/22/11 AD P 23d NA 0.13 NA NA NA 9.2 NA ND 0.96 ND NA 11/18/11 AD P 30d NA 0.075 NA NA NA 5.2 NA ND 0.58 ND NA 11/30/11 AD P 13d NA ND NA NA NA 3.6 NA ND 0.45 ND NA 03/01/12 AD P 10d NA ND NA NA NA 3.5 NA ND 0.41 ND NA 06/01/12 AD P 8d NA ND NA NA NA 5.1 NA ND 0.48 ND NA 09/04/12 AD P 5d NA 0.24 NA NA NA 10.0 NA ND 1.30 ND NA 12/13/13 AD P 7d NA 0.18 NA NA NA 4.9 NA ND 0.56 ND NA 03/19/15 AD P 7d NA <0.32 NA NA NA 1.9 NA <0.33 0.22 <0.44 NA IA-2 06/17/15 AD P 7d NA <0.32 NA NA NA 4 NA <0.33 0.47 <0.44 NA 01/11/16 AD P 8d NA <0.28 NA NA NA 2.4 NA <0.29 0.23 <0.28 NA 06/13/16 AD P 7d NA <0.32 NA NA NA 3.9 NA <0.33 0.39 <0.44 NA 12/12/16 AD P 7d NA <0.32 NA NA NA 4.0 NA <0.34 0.46 <0.45 NA 06/20/17 AD P 7d NA <0.28 NA NA NA 3.1 NA <0.29 0.35 <0.39 NA 12/18/17 AD P 7d NA <0.32 NA NA NA 4.3 NA <0.33 0.59 <0.44 NA 06/15/18 AD P 7d NA <0.24 NA NA NA 2.8 NA <1.2 <0.29 <0.15 NA 12/21/18 AD P 7d NA <0.24 NA NA NA 4.6 NA <1.2 1.9 <0.15 NA Ol/11/19 AD SU 8h NA <0.14 NA NA NA 1.4 NA <0.14 0.15J <0.09 NA Ol/18/19 AD P 7d NA <0.24 NA NA NA 2.6 NA <1.2 1.6 <0.15 NA 02/15/19 AD P 7d NA <0.24 NA NA NA 2.5 NA <1.2 1.6 <0.15 NA 05/04/10 AD SU 8h 9.5 ND 3.0 ND NA 4.6 22.6 ND 8.8 ND 18.7 07/22/10 AD P 7d NA ND NA NA NA 12 NA ND 0.75 ND NA 01/28/11 AD P 7d NA 0.15 NA NA NA 7.1 NA ND 0.8 ND NA 08/23/11 AD P 34d NA 0.14 NA NA NA 9.8 NA ND 0.99 ND NA 08/30/11 AD P 7d NA 0.31 NA NA NA 12.0 NA ND 1.20 ND NA 09/22/11 AD P 23d NA 0.11 NA NA NA 8.1 NA ND 0.88 ND NA 11/18/11 AD P 30d NA 0.093 NA NA NA 6.2 NA ND 0.75 ND NA 11/30/11 AD P 13d NA ND NA NA NA 4.1 NA ND 0.51 ND NA 03/01/12 AD P 10d NA ND NA NA NA 3.8 NA ND 0.44 ND NA 06/01/12 AD P 8d NA ND NA NA NA 5.5 NA ND 0.50 ND NA 09/04/12 AD P 5d NA 0.28 NA NA NA 12.0 NA ND 1.50 ND NA 12/13/13 AD P 7d NA 0.19 NA NA NA 5.9 NA ND 0.68 ND NA IA-3 03/19/15 AD P 7d NA <0.32 NA NA NA 1.8 NA <0.33 0.21 <0.44 1 NA 06/17/15 AD P 7d NA <0.32 NA NA NA 4.4 NA <0.33 1 0.5 <0.44 NA 01/11/16 AD P 8d NA <0.28 NA NA NA 2.4 NA <0.29 0.24 <0.39 NA 06/13/16 AD P 7d NA <0.32 NA NA NA 3.4 NA <0.33 0.36 <0.44 NA 12/12/16 AD P 7d NA <0.32 NA NA NA 3.2 NA <0.34 0.34 <0.45 NA 06/20/17 AD P 7d NA <0.28 NA NA NA 3.2 NA <0.29 0.38 <0.39 NA 12/18/17 AD P 7d NA <0.32 NA NA NA 4.5 NA <0.33 0.59 <0.44 NA 06/15/18 AD P 7d NA <0.24 NA NA NA 2.9 NA <1.2 <0.29 <0.15 I NA 12/21/18 AD P 7d NA <0.24 NA NA NA 5.9 NA <1.2 1 2.1 <0.15 NA 01/11/19 AD SU 8-h NA <0.16 NA NA NA 1.4 NA <0.16 0.12J <0.01 NA 01/18/19 AD P 7d NA <0.24 NA NA NA 2.3 NA <1.2 1.4 <0.15 NA 02/15/19 AD P 7d NA <0.24 NA NA NA 1.8 NA <1.2 1.6 <0.15 NA IA4 05/04/10 AD SU 8h 0.8 ND ND ND NA 3.9 4.7 ND ND ND ND IA-5 05/04/10 AD SU 8h ND ND ND ND NA ND 1.5 ND ND ND ND 07/22/10 AD P 7d NA ND NA NA NA 5.1 NA ND 0.45 ND NA 06/15/11 AD SU 8h NA 3.9 NA NA NA 4.1 NA ND 0.18 ND NA IA-6 01/10/12 AD SU 8h NA 2.4 NA NA NA 1.6 NA ND 0.23 ND NA HT-IA-1 03/19/15 AD P 7d NA <0.32 NA NA NA 0.88 NA 10 C <0.14 <0.44 NA HT-IA-2 03/19/15 AD P 7d NA <0.32 NA NA NA 3.8 NA 9.0 C <0.14 <0.44 NA BG-1 05/04/10 AD SU 8h ND ND ND 0.98 NA ND 1.5 ND ND ND ND BG-2 05/04/10 AD SU 8h ND ND ND ND NA ND ND ND 1.8 ND ND OAA-1 12/13/13 AD P 7d NA ND NA NA NA ND NA ND ND I ND NA Notes: ' Indicate T" for former or current dry-cleaning facility, "AD" for adjacent space, "R" for residence, "C" for commercial not adjacent space. If sample was taken outdoors, leave blank. 3 Indicate 'SU' for summa canister, 'TC' for flux chambers, "T" for tedlar bags, 'T" for passive samplers, "O" for other. Pagel of4 Table 5(2): Additional Data for Indoor and Outdoor Air CA ID No.: DC680002 Is dry-cleaning facility at the site: Operating ❑ Pick-up Only ❑ Abandoned 0 If facility is operating, solvents used are: Perc ❑ Petroleum ❑ Green Earth ❑ Other ❑ For the active or former dry-cleaning space, describe the type and location of the air handling/HVAC unit (for example - a shared unit supplying two adjacent spaces; unit located on the root): - The air handling/HVAC unit(s) are located on the roof of the Hams Teeter building. For any indoor air spaces tested, describe the current use of the space (for example - an ABC liquor store adjacent to the dry-cleaner, a residence approximately 200 feet from the dry-cleaner, etc.): Harris Teeter (former American Dry -Cleaners). Olin T. Binkley Baptist Church preschool facility located 150 feet east (down gradient) of farmer American Dry Cleaners. For any other indoor spaces tested, describe the type and location of the air handling/HVAC unit (for example - a shared unit supplying two adjacent spaces; unit located on the roof): Olin T. Binkley Baptist Church - One air handling/HVAC unit is located on the roof of the west wing where the preschool classrooms are located. - One air handling/HVAC unit is located on the ground along the south wall where the preschool classrooms are located. - Three air handling/HVAC units are located on the roof of the east wing where the church offices are located. - One air handling/HVAC unit is located on the ground along the north wall of the east wing where church sactuary is located. Sampling location map that indicates where all indoor air samples were collected. The map should clearly indicate the names/types of businesses and residence names sampled and in the vicinity of the subject site that may be of concern. Page 3 of 4 Table 5(3): Additional Data for Indoor and Outdoor Air 1 SCA ID No.: DC680002 Sample ID Name and Address for Sampling Location Property Owner Name, Address, and Phone Number Tenant Name, Address, and Phones Number IA-2 Olin T. Binkley Baptist Church Olin T. Binkley Baptist Church 1712 Willow Drive, Chapel Hill, NC 27514 1712 Willow Drive, Chapel Hill, NC 27514 919-9424964(office) Dale Osborne (Pastor) 919-923-3874 (cell) IA 3 HT-IA-1 Frank Rinaldo Harris Teeter, 2110 S Estes Drive, Chapel Hill, NC 27514 Madison University Mall LLC 2001 Pennsylvania Ave, NW Washington DC 20005 Jeff Hoffinan (Store Manager) 919-933-5700 (Work) HT-IA-1 (202) 741-3857 Page 4 of 4 Table 6: Monitoring Well Construction Data DSCA ID No.: DC680002 Well ID Date Installed (mm/dd/YY) Number of Samples Well Depth [feet] Well Diameter [inch] Screen Interval [feet] Status (Active/Inactive) HA-1 08/07/95 1 5.0 N/A 0.0-5.0 Inactive HA-2 08/07/95 1 7.0 N/A 2.0-7.0 Inactive 2W-1 05/23/95 1 8.5 2 3.1-8.1 Inactive 2W-2S 08/07/95 7 8.0 2 2.8-7.8 Active 2W-2D 08/08/95 3 14.0 2 3.4-13.4 Active 2W-3 08/08/95 1 21.5 2 6.0-21.0 Inactive 2W-4 08/07/95 6 9.5 2 4.0-9.0 Active 2W-5 08/10/95 16 9.2 2 3.8-8.8 Active 2W-6 08/08/95 16 13.0 2 7.2-12.2 Active 2W-7 08/08/95 7 9.0 2 3.5-8.5 Active 2W-8 08/10/95 2 9.0 2 3.5-8.5 Inactive 2W-9 6/27/14 4 13 2 8-13 Active 2W-10 6/27/14 4 13 2 8-13 Active 2W-11 6/27/14 4 13 2 8-13 Active 2W-12 6/27/14 2 12 2 7-12 Active MW-1 09/23/08 12 14.5 2 4.5-14.5 Active MW-2 09/23/08 17 28 2 18-28 Active MW-3 09/24/08 15 28 2 18-28 Active MW-4 09/24/08 6 33 2 23-33 Active MW-5 09/24/08 13 28 2 18-28 Active MW-6 09/12/08 1 15 2 5-15 Active Page 1 of 1 Table 7: Groundwater Elevation Data DSCA ID No.: DC680002 Groundwater Sampling Point Sampling Date (mrn/dd/yy) TOC Elevation [feet] Depth to Water [feet bgs] Groundwater Elevation [feet] Depth to NAPL [feet bgs] NAPL Thickness [feet] Corrected* Groundwater Elevation [feet] 2W-2S 10/21/10 265.79 5.49 260.30 N/A N/A N/A O1/21/11 265.79 5.29 260.50 N/A N/A N/A 04/29/11 265.79 3.96 261.83 N/A N/A N/A 07/18/11 265.79 5.43 260.36 N/A N/A N/A 08/30/11 265.79 5.78 260.01 N/A N/A N/A 09/22/11 265.79 5.58 260.21 N/A N/A N/A 10/18/11 265.79 5.73 260.06 N/A N/A N/A 11/18/11 265.79 5.57 260.22 N/A N/A N/A 02/23/12 265.79 5.05 260.74 N/A N/A N/A 05/24/12 265.79 5.05 260.74 N/A N/A N/A 02/07/14 265.79 5.10 260.69 N/A N/A N/A 08/04/14 265.79 4.95 260.84 N/A N/A N/A 11/23/15 265.79 5.37 260.42 N/A N/A N/A 12/12/16 265.79 5.74 260.05 N/A N/A N/A 12/19/18 265.79 4.76 261.03 N/A N/A N/A 2W-2D 10/21/10 265.73 5.42 260.31 N/A N/A N/A O1/21/11 265.73 5.23 260.50 N/A N/A N/A 04/29/11 265.73 3.89 261.84 N/A N/A N/A 07/18/11 265.73 NA NA N/A N/A N/A 02/07/14 265.73 5.13 260.60 N/A N/A N/A 08/04/14 265.73 4.91 260.82 N/A N/A N/A 11/23/15 265.73 5.40 260.33 N/A N/A N/A 12/12/16 265.73 5.78 259.95 N/A N/A N/A 12/19/18 265.73 4.80 260.93 N/A N/A N/A 10/21/10 265.61 5.22 260.39 N/A N/A N/A O1/21/11 265.61 5.16 260.45 N/A N/A N/A 04/29/11 265.61 4.36 261.25 N/A N/A N/A 07/17/11 265.61 5.00 260.61 N/A N/A N/A 08/30/11 265.61 5.50 260.11 N/A N/A N/A 09/22/11 265.61 5.14 260.47 N/A N/A N/A 10/18/11 265.61 5.30 260.31 N/A N/A N/A 'W-4 11/18/11 265.61 5.25 260.36 N/A N/A N/A 02/23/12 265.61 5.95 259.66 N/A N/A N/A 05/24/12 265.61 4.73 260.88 N/A N/A N/A 02/07/14 265.61 5.30 260.31 N/A N/A N/A 08/04/14 265.61 5.25 260.36 N/A N/A N/A 11/23/15 265.61 5.25 260.36 N/A N/A N/A 12/12/16 265.61 5.49 260.12 N/A N/A N/A 12/19/18 265.61 4.95 260.66 N/A N/A N/A 10/21/10 264.53 4.73 259.80 N/A N/A N/A O1/21/11 264.53 4.57 259.96 N/A N/A N/A 04/29/11 264.53 4.22 260.31 N/A N/A N/A 07/18/11 264.53 4.33 260.20 N/A N/A N/A 08/30/11 264.53 4.80 259.73 N/A N/A N/A 09/22/11 264.53 4.23 260.30 N/A N/A N/A 10/18/11 264.53 4.45 260.08 N/A N/A N/A 11/18/11 264.53 4.00 260.53 N/A N/A N/A 2W-5 02/23/12 264.53 3.43 261.10 N/A N/A N/A 05/24/12 264.53 3.90 260.63 N/A N/A N/A 09/04/12 264.53 4.38 260.15 N/A N/A N/A 02/07/14 264.53 4.50 260.03 N/A N/A N/A 08/04/14 264.53 4.46 260.07 N/A N/A N/A 11/23/15 264.53 4.49 260.04 N/A N/A N/A 12/12/16 264.53 4.43 260.10 N/A N/A N/A 12/19/18 264.53 4.08 260.45 N/A N/A N/A Page 1 of 4 Table 7: Groundwater Elevation Data DSCA ID No.: DC680002 Groundwater Sampling Point Sampling Date (mrn/dd/yy) TOC Elevation [feet] Depth to Water [feet bgs] Groundwater Elevation [feet] Depth to NAPL [feet bgs] NAPL Thickness [feet] Corrected* Groundwater Elevation [feet] 2W-6 10/21/10 264.77 6.01 258.76 N/A N/A N/A O1/21/11 264.77 5.56 259.21 N/A N/A N/A 04/29/11 264.77 5.41 259.36 N/A N/A N/A 07/18/11 264.77 5.50 259.27 N/A N/A N/A 08/30/11 264.77 6.06 258.71 N/A N/A N/A 09/22/11 264.77 5.36 259.41 N/A N/A N/A 10/18/11 264.77 5.95 258.82 N/A N/A N/A 11/18/11 264.77 5.85 258.92 N/A N/A N/A 02/23/12 264.77 5.44 259.33 N/A N/A N/A 05/24/12 264.77 5.21 259.56 N/A N/A N/A 09/04/12 264.77 5.48 259.29 N/A N/A N/A 11/19/13 264.77 6.52 258.25 N/A N/A N/A 08/04/14 264.77 5.34 259.43 N/A N/A N/A 11/23/15 264.77 5.31 259.46 N/A N/A N/A 12/12/16 264.77 5.71 259.06 N/A N/A N/A 12/19/18 264.77 4.73 260.04 N/A N/A N/A 2W-7 10/21/10 264.54 3.18 261.36 N/A N/A N/A O1/21/11 264.54 3.37 261.17 N/A N/A N/A 04/29/11 264.54 2.49 262.05 N/A N/A N/A 07/18/11 264.54 1.10 263.44 N/A N/A N/A 11/19/13 264.54 5.15 259.39 N/A N/A N/A 08/04/14 264.54 2.93 261.61 N/A N/A N/A 11/23/15 264.54 3.75 260.79 N/A N/A N/A 12/12/16 264.54 5.24 259.30 N/A N/A N/A 10/21/10 266.32 6.05 260.27 N/A N/A N/A O1/21/11 266.32 6.27 260.05 N/A N/A N/A 04/29/11 266.32 4.83 261.49 N/A N/A N/A 07/18/11 266.32 6.15 260.17 N/A N/A N/A 08/30/11 266.32 6.50 259.82 N/A N/A N/A 2W-8 09/22/11 266.32 6.33 259.99 N/A N/A N/A 10/18/11 266.32 6.41 259.91 N/A N/A N/A 11/18/11 266.32 6.44 259.88 N/A N/A N/A 02/23/12 266.32 6.00 260.32 N/A N/A N/A 05/24/12 266.32 5.90 260.42 N/A N/A N/A 11/19/13 266.32 6.48 259.84 N/A N/A N/A 08/04/14 266.32 6.10 260.22 N/A N/A N/A 07/08/14 269.32 9.30 260.02 N/A N/A N/A 08/04/14 269.32 9.42 259.90 N/A N/A N/A 2W-9 11/23/15 269.32 9.45 259.87 N/A N/A N/A 12/12/16 269.32 9.51 259.81 N/A N/A N/A 12/19/18 269.32 8.04 261.28 N/A N/A N/A 07/08/14 268.73 9.50 259.23 N/A N/A N/A 08/04/14 268.73 9.25 259.48 N/A N/A N/A 2W-10 11/23/15 268.73 9.30 259.43 N/A N/A N/A 12/12/16 268.73 9.33 259.40 N/A N/A N/A 12/19/18 268.73 8.17 260.56 N/A N/A N/A 07/08/14 268.70 9.80 258.90 N/A N/A N/A 08/04/14 268.70 9.71 258.99 N/A N/A N/A 2W-11 11/23/15 268.70 9.75 258.95 N/A N/A N/A 12/12/16 268.70 9.78 258.92 N/A N/A N/A 12/19/18 268.70 9.00 259.70 N/A N/A N/A 07/08/14 267.52 8.70 258.82 N/A N/A N/A 08/04/14 267.52 8.60 258.92 1 N/A N/A N/A 2W-12 1 11/23/15 1 267.52 1 8.56 1 258.96 N/A N/A N/A 12/12/16 267.52 8.65 258.87 N/A N/A N/A 12/19/18 267.52 7.37 260.15 N/A N/A N/A Page 2 of 4 Table 7: Groundwater Elevation Data DSCA ID No.: DC680002 Groundwater Sampling Point Sampling Date (mrn/dd/yy) TOC Elevation [feet] Depth to Water [feet bgs] Groundwater Elevation [feet] Depth to NAPL [feet bgs] NAPL Thickness [feet] Corrected* Groundwater Elevation [feet] MW-1 10/21/10 266.35 8.58 257.77 N/A N/A N/A O1/21/11 266.35 8.38 257.97 N/A N/A N/A 04/29/11 266.35 8.13 258.22 N/A N/A N/A 07/18/11 266.35 8.24 258.11 N/A N/A N/A 08/30/11 266.35 8.65 257.70 N/A N/A N/A 09/22/11 266.35 8.63 257.72 N/A N/A N/A 10/18/11 266.35 8.62 257.73 N/A N/A N/A 02/23/12 266.35 8.13 258.22 N/A N/A N/A 05/24/12 266.35 8.29 258.06 N/A N/A N/A 09/04/12 266.35 8.62 257.73 N/A N/A N/A 11/19/13 266.35 8.40 257.95 N/A N/A N/A 08/04/14 266.36 7.90 258.46 N/A N/A N/A 11/23/15 266.36 7.64 258.72 N/A N/A N/A 12/12/16 266.36 7.66 258.70 N/A N/A N/A MW-2 10/21/10 268.03 8.89 259.14 N/A N/A N/A O1/21/11 268.03 8.73 259.30 N/A N/A N/A 04/29/11 268.03 8.34 259.69 N/A N/A N/A 07/18/11 268.03 8.44 259.59 N/A N/A N/A 08/30/11 268.03 8.80 259.23 N/A N/A N/A 09/22/11 268.03 8.55 259.48 N/A N/A N/A 10/18/11 268.03 8.59 259.44 N/A N/A N/A 11/18/11 268.03 8.49 259.54 N/A N/A N/A 02/23/12 268.03 7.89 260.14 N/A N/A N/A 05/24/12 268.03 7.51 260.52 N/A N/A N/A 09/04/12 268.03 8.06 259.97 N/A N/A N/A 11/19/13 268.03 8.29 259.74 N/A N/A N/A 08/04/14 268.04 8.06 259.98 N/A N/A N/A 11/23/15 268.04 7.77 260.27 N/A N/A N/A 12/12/16 268.04 8.90 259.14 N/A N/A N/A 12/19/18 268.04 7.34 260.70 N/A N/A N/A 10/21/10 269.40 10.33 259.07 N/A N/A N/A O1/21/11 269.40 9.46 259.94 N/A N/A N/A 04/29/11 269.40 8.91 260.49 N/A N/A N/A 07/18/11 269.40 9.04 260.36 N/A N/A N/A 08/30/11 269.40 10.41 258.99 N/A N/A N/A 09/22/11 269.40 9.27 260.13 N/A N/A N/A 10/18/11 269.40 9.38 260.02 N/A N/A N/A MW-3 11/18/11 269.40 9.65 259.75 N/A N/A N/A 02/23/12 269.40 9.00 260.40 N/A N/A N/A 09/04/12 269.40 9.78 259.62 N/A N/A N/A 11/19/13 269.40 9.52 259.88 N/A N/A N/A 08/04/14 269.41 9.26 260.15 N/A N/A N/A 11/23/15 269.41 9.27 260.14 N/A N/A N/A 12/12/16 269.41 9.65 259.76 N/A N/A N/A 12/19/18 269.41 8.40 261.01 N/A N/A N/A 10/21/10 264.30 10.87 253.43 N/A N/A N/A O1/21/11 264.30 9.94 254.36 N/A N/A N/A 04/29/11 264.30 7.84 256.46 N/A N/A N/A 07/18/11 264.30 9.19 255.11 N/A N/A N/A 08/30/11 264.30 10.93 253.37 N/A N/A N/A 09/22/11 264.30 10.65 253.65 N/A N/A N/A MW-4 10/18/11 264.30 10.34 253.96 N/A N/A N/A 11/18/11 264.30 10.18 254.12 N/A N/A N/A 02/23/12 264.30 8.22 256.08 N/A N/A N/A 05/24/12 264.30 7.09 257.21 N/A N/A N/A 09/24/12 264.30 1 9.85 1 254.45 1 N/A N/A N/A 11/19/13 264.30 10.30 254.00 N/A N/A N/A 88/04/14 264.31 8.02 256.29 N/A N/A N/A Page 3 of 4 Table 7: Groundwater Elevation Data DSCA ID No.: DC680002 Groundwater Sampling Point Sampling Date (mrn/dd/yy) TOC Elevation [feet] Depth to Water [feet bgs] Groundwater Elevation [feet] Depth to NAPL [feet bgs] NAPL Thickness [feet] Corrected* Groundwater Elevation [feet] MW-5 10/21/10 264.49 8.45 256.04 N/A N/A N/A O1/21/11 264.49 6.99 257.50 N/A N/A N/A 04/29/11 264.49 5.50 258.99 N/A N/A N/A 07/18/11 264.49 6.00 258.49 N/A N/A N/A 08/30/11 264.49 6.88 257.61 N/A N/A N/A 09/22/11 264.49 7.04 257.45 N/A N/A N/A 10/18/11 264.49 7.17 257.32 N/A N/A N/A 11/18/11 264.49 7.34 257.15 N/A N/A N/A 02/23/12 264.49 5.84 258.65 N/A N/A N/A 05/24/12 264.49 5.72 258.77 N/A N/A N/A 09/04/12 264.49 6.51 257.98 N/A N/A N/A 11/19/13 264.49 6.78 257.71 N/A N/A N/A 08/04/14 264.50 6.03 258.47 N/A N/A N/A 12/12/16 264.50 6.02 258.48 N/A N/A N/A MW-6 10/21/10 N/A 4.31 N/A N/A N/A N/A O1/21/11 N/A 4.23 N/A N/A N/A N/A 04/29/11 N/A 5.80 N/A N/A N/A N/A 07/18/11 N/A 2.79 N/A N/A N/A N/A 11/19/13 N/A 6.78 N/A N/A N/A N/A 08/04/14 1 264.50 1 3.05 1 261.45 N/A N/A N/A 11/23/15 264.50 4.46 260.04 N/A N/A N/A 12/12/16 264.50 5.85 258.65 N/A N/A N/A Page 4 of 4 Table 8: Analytical Data for Groundwater DSCA ID No.: DC680002 O 0 o > o N N V1 N U N Lam. A N O U N N A Q Y -Z O U F F� o Oi. o F E- 3 'O bo N N� :2 u L' 0 y ci 9 tiC d cv 7 I U I U U [mg/L] V) 13 <0.001 1.8 <0.001 <0.001 <0.001 1.2 <0.001 0 6 1 <0.001 <0.001 <0.01 <0.001 <0.001 <0.001 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS <0.001 <0.001 70.331 7001 77001 8 <0.001 <0.001 <0.001 <0.001 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 70.001 <0.001 <0.001 <0.001 <0.001 0.0 6 <0.001 <0.001 <0.01 <0.001 <0.001 <0.001 <0.01 <0.01 ND 10.01 <0.001 NS <0.001 <0.001 <0.001 <0.001 7o.001 0. 0.0 1 70.001 7001 701 <0.001 <0.001 <0.001 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS <0.001 <0.001 <0.001 <0.001 <0.001 0.0 2 <0.001 <0.001 <0.01 <0.001 <0.001 <0.001 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS <0.001 0.150 <0.001 <0.001 <0.001 0.44 <0.001 <0.001 <0.001 <0.001 <0.01 <0.001 <0.001 <0.001 <0.01 <0.01 ND <0.001 I <0.01 <0.001 NS HA- 5 NA < 1 NA NA NA 0.01 NA NA < NA NA NA NA NA NA NA NA NA NA NA NA NA NA HA-7-0 5 NA <• 0 NA NA NA 6.7 NA NA < NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2W- 0 5 NA NA NA NA 76. NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 08/95 NA <0.0050 NA NA NA <0.0050 NA NA <0.0050 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/06/07 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 10/21/10 <0.001 <0.001 <0.001 <0.001 <0.001 0.00066J <0.001 <0.001 I <0.001 <0.001 <0.001 <0.001 <0.01 <0.001 <0.001 0.0031J <0.01 <0.01 ND <0.001 0.00043J <0.001 NS 2W-2S 01/21/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.01 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.01 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 0.00037J <0.001 NS 07/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.01 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 NS 02/07/14 1 <0.0005 <0.0005 <0.0005 <0.0005 NA <0.0005 1 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 1 <0.0005 <0.0005 <0.0005 <0.0005 <0.01 <0.01 <0.01 ND <0.0005 <0.0005 NA NA 08/95 NA <0.0010 NA NA NA <0.0010 NA NA <0.0010 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2W-2D 12/06/07 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 I NA <0.001 I <0.001 <0.001 NA NA NA <0.001 NA NA NA 02/07/14 <0.0005 <0.0005 <0.0005 <0.0005 NA <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.01 <0.01 <0.01 ND <0.0005 <0.0005 NA NA 2W-3 08/95 NA <0.001 NA NA NA 0.179 NA NA 0.003 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 08/95 NA <0.100 NA NA NA 6.09 NA NA 0.647 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/06/07 <0.001 <0.001 <0.001 <0.001 0.023 0.0301 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 1.76 NA NA NA <0.001 NA NA NA 2W4 01/30/09 <0.001 0.479 <0.001 <0.001 <0.001 1.293 <0.001 0.00691 1 0.379 <0.001 <0.001 <0.001 NA <0.001 <0.001 NA NA NA NA <0.001 <0.001 NA NA 02/07/14 <0.1 7.1 <0.1 <0.1 NA 2.9 <0.1 0.083J 1.8 <0.1 <0.1 <0.1 1 <0.1 <0.1 <0.1 <2 <2 <2 ND <0.1 <0.1 NA NA 11/23/15 <0.001 0.132 <0.001 <0.001 <0.005 0.00484 <0.005 0.00194 0.0078 0.0376 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 <0.005 <0.001 <0.0025 <0.001 NA 05/14/18 <0.001 0.0092 <0.001 <0.001 <0.002 0.0038 <0.001 0.00024J 0.0045 0.0033 <0.003 <0.001 NA <0.001 <0.001 <0.05 <0.02 <0.01 <0.002 <0.002 <0.002 <0.001 I <0.001 12/06/07 <0.001 <0.001 <0.001 <0.001 1.52 1 15.1 <0.001 <0.001 2.55 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 01/30/09 <0.001 0.81 <0.001 <0.001 <0.001 0.991 <0.001 0.00683 0.429 0.329 <0.001 <0.001 NA <0.001 <0.001 NA NA NA NA <0.001 0.0041 NA NA 10/21/10 <0.02 0.239 <0.02 <0.02 <0.02 1.95 <0.02 0.0038 1 0.399 0.002 <0.02 <0.02 <0.02 <0.02 0.0012J <0.05 <0.01 <0.01 ND <0.02 0.00028J <0.001 NS 01/21/11 <0.02 1.42 <0.02 <0.02 <0.02 4.15 <0.02 0.116 1.77 0.0274 <0.02 <0.02 <0.02 <0.02 0.0059J <0.05 <0.01 <0.01 ND <0.02 <0.01 <0.001 NS 04/29/11 <0.02 1.9 <0.02 <0.02 <0.02 3.35 <0.02 0.0155J 1.63 0.256 <0.02 <0.02 <0.02 <0.02 <0.001 <0.05 <0.01 <0.01 ND <0.02 <0.01 0.0215J NS 07/18/11 <0.050 0.760 <0.050 <0.050 <0.050 3.4 <0.250 <0.05 0.990 0.060 <0.150 <0.050 <0.050 <0.050 <0.050 <2.0 <0.5 <0.5 ND <0.050 <0.12 <0.05 <0.001 08/30/11 0.0011 1.500 <0.001 <0.001 <0.001 1 0.082 <0.005 0.014 0.280 1 0.390 <0.003 <0.001 <0.001 0.005 <0.001 0.15 0.076 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/22/11 <0.01 5.900 <0.01 <0.01 <0.01 0.65 <0.05 0.026 0.320 0.092 <0.03 <0.01 <0.01 0.012 <0.01 3.9 2 <0.1 ND <0.01 <0.025 <0.01 <0.01 2W 5 10/18/11 <0.01 0.034 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 0.540 <0.03 <0.01 <0.01 <0.01 <0.01 0.6 0.42 <0.1 ND <0.01 1 <0.025 <0.01 <0.01 11/18/11 <0.005 0.081 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.150 <0.015 <0.005 <0.005 <0.005 <0.005 0.45 0.25 <0.1 ND <0.005 <0.025 <0.01 <0.01 02/23/12 <0.01 0.013 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 0.006 <0.03 <0.01 <0.01 <0.01 <0.01 <0.05 <0.01 <0.1 ND <0.01 <0.025 <0.01 <0.01 05/24/12 <0.001 0.003 <0.001 <0.001 <0.001 <0.001 0.044 0.0016 <0.001 0.0041 <0.003 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/04/12 <0.001 0.002 <0.001 <0.001 <0.001 <0.001 1.5 0.0023 <0.001 0.0012 <0.003 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.01 ND <0.001 0.0086 <0.001 <0.001 02/07/14 0.00034J 0.018 <0.0005 <0.0005 NA <0.0005 0.0036 0.012 0.00044J 0.035 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.01 <0.01 <0.01 ND <0.0005 <0.0005 NA NA 11/23/15 <0.001 0.174 <0.001 <0.001 <0.005 <0.001 <0.005 0.00496 0.00108 0.0931 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 0.0247 <0.001 <0.0025 <0.001 NA 05/14/18 <0.005 0.47 <0.005 <0.005 <0.01 <0.005 0.0034J 0.01 <0.005 0.29 <0.015 <0.005 NA <0.005 1 <0.005 <0.25 0.013J <0.05 1 0.0093J I <0.01 I <0.01 1 <0.005 1<0.005 Page 1 of 4 Table 8: Analytical Data for Groundwater DSCA ID No.: DC680002 O 0 N U Oi. L' Q 9 tiC d N 7 U I U U [mg/L] cn 08/95 NA <0.100 NA NA NA 1.77 NA NA 0.09600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/06/07 <0.001 <0.001 <0.001 <0.001 0.482 3.92 <0.001 <0.001 0.83800 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 01/30/09 <0.001 0.656 <0.001 <0.001 <0.001 0.903 <0.001 <0.001 0.21000 <0.001 <0.001 <0.001 NA <0.001 <0.001 NA NA NA NA <0.001 <0.001 NA NA 10/21/10 <0.002 0.401 <0.002 <0.002 <0.002 0.427 <0.002 <0.001 0.214 0.0373 <0.002 <0.002 <0.002 <0.002 <0.002 <0.05 <0.01 <0.01 ND <0.002 <0.001 <0.001 NS 01/21/11 <0.002 0.317 <0.002 <0.002 <0.002 0.346 <0.002 0.0015J 0.33 0.0035 <0.002 <0.002 <0.002 <0.002 <0.002 <0.05 <0.01 <0.01 ND <0.002 <0.01 <0.001 NS 04/29/11 <0.002 0.357 <0.002 <0.002 <0.002 3.41 <0.002 <0.001 0.316 <0.001 I <0.002 <0.002 <0.002 1 <0.002 <0.002 <0.05 <0.01 I <0.01 ND <0.002 1 <0.01 <0.001 NS 07/18/11 <0.05 0.280 <0.05 <0.05 <0.05 3.00 <0.250 <0.05 0.350 <0.05 <0.150 <0.05 <0.05 <0.05 <0.05 <2.5 <0.250 <0.025 ND <0.05 <0.120 <0.05 <0.001 2W-6 08/30/11 <0.001 0.240 <0.001 <0.001 <0.001 2.90 <0.005 0.0029 0.320 0.0016 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/22/11 <0.02 0.170 <0.02 <0.02 <0.02 1.70 <0.1 <0.02 0.190 <0.02 <0.06 <0.02 <0.02 <0.02 <0.02 <1.0 <0.2 <0.2 ND <0.02 <0.05 <0.02 <0.02 10/18/11 <0.025 0.25 <0.025 <0.025 <0.025 2.50 <0.120 <0.025 0.250 <0.02 <0.06 <0.025 <0.025 <0.025 <0.025 <1.0 <0.2 <0.2 ND <0.025 <0.05 <0.02 <0.02 11/18/11 <0.020 0.240 <0.020 <0.020 <0.020 1.80 <0.100 <0.020 0.220 <0.020 <0.06 <0.020 <0.020 <0.020 <0.020 <0.100 <0.200 <0.200 ND <0.020 <0.05 <0.02 <0.02 02/23/12 <0.020 0.160 <0.020 <0.020 <0.020 2.60 <0.100 <0.020 0.240 <0.020 <0.06 0.16 <0.020 <0.020 <0.020 <0.100 <0.200 <0.200 ND <0.020 <0.05 <0.02 <0.02 05/24/12 <0.01 0.170 <0.01 <0.01 <0.01 3.0 <0.01 <0.01 0.250 <0.01 <0.03 <0.01 <0.01 <0.01 <0.01 <0.5 <0.01 <0.1 ND <0.01 <0.025 <0.01 <0.01 09/04/12 <0.025 0.76 <0.025 <0.025 <0.025 0.84 <0.120 <0.025 0.280 <0.02 <0.06 <0.025 <0.025 <0.025 <0.025 <1.0 <0.2 <0.2 ND <0.025 <0.05 <0.02 <0.02 11/12/13 <0.25 1.8 <0.25 <0.25 NA 2.10 <0.25 <0.25 0.890 0.052 J <0.25 <0.25 <0.25 <0.25 <0.25 <1 <0.5 <0.5 ND <0.25 <0.25 NA N/A 05/14/18 <0.005 0.4 <0.005 <0.005 <0.01 0.16 <0.005 0.0026J 0.140 0.011 <0.015 <0.005 NA <0.005 <0.005 <0.25 <0.1 <0.05 <0.01 <0.01 <0.01 <0.005 <0.005 08/95 NA <0.001 NA NA NA <0.001 NA NA <0.001 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/06/07 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 10/21/10 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 I <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0024J <0.01 <0.01 ND <0.001 0.00027J <0.001 NS 2W-7 01/21/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 I <0.001 1 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 1 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 07/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 10 ND <0.001 <0.0025 <0.001 NS 11/12/13 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 <0.005 <0.005 <0.002 <0.005 <0.005 <0.005 <0.005 <0.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA N/A 2W 8 12/06/07 <0.001 <0.001 I <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 NA <0.001 <0.001 <0.001 NA NA NA <0.001 NA NA NA 11/12/13 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 <0.005 1 0.00032J <0.002 <0.005 <0.005 1 <0.005 <0.005 <0.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA N/A 07/08/14 <0.0025 0.6 <0.0025 <0.0025 NA 0.47 <0.0025 0.0052 0.24 0.0007J <0.0025 <0.0025 NA <0.0025 <0.0025 1 <0.050 <0.050 <0.050 ND 0.017J <0.0025 NA <0.0025 2W 9 11/23/15 <0.001 0.27 <0.001 <0.001 <0.005 0.316 <0.005 0.00404 0.129 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 <0.005 0.0251 <0.0025 <0.001 NA 12/12/16 <0.002 0.21 <0.002 <0.004 <0.008 0.22 <0.004 0.0037J 0.11 <0.008 <0.012 <0.002 NA <0.002 <0.002 <0.2 <0.08 <0.04 <0.008 0.013 <0.008 <0.002 NA 12/19/18 <0.001 1 0.149 <0.001 <0.001 <0.005 0.176 1 <0.001 0.00229 0.0862 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 <0.005 <0.005 <0.0025 <0.001 NA 07/08/14 <0.050 2.7 <0.050 <0.050 NA 7.2 <0.050 0.031J 3.5 <0.050 <0.050 <0.050 NA 1 <0.050 <0.050 <1 <1 <1 I ND <0.050 <0.050 NA <0.050 11/23/15 <0.005 2.46 <0.005 <0.005 <0.025 3.1 <0.025 0.0247 4.27 <0.005 <0.015 <0.005 <0.005 <0.005 <0.005 <0.25 <0.05 <0.05 <0.025 <0.005 <0.0125 <0.005 NA 2W-10 12/12/16 <0.1 6.2 <0.1 <0.1 <0.2 0.053 <0.1 0.044J 0.049J <0.2 <0.3 <0.1 NA <0.1 <0.1 <5 <2 <1 <0.2 <0.2 <0.2 <0.1 NA 12/19/18 <0.005 1.93 <0.005 <0.005 <0.025 0.0482 <0.005 0.0126 0.036 0.0901 <0.015 <0.005 <0.005 <0.005 <0.005 <0.25 <0.05 <0.05 <0.025 <0.025 <0.0125 <0.005 NA 07/08/14 <0.025 0.87 <0.025 <0.025 NA 2.9 <0.025 0.0092J 0.69 <0.025 <0.025 <0.0025 NA <0.025 <0.025 <0.5 <0.5 <0.5 ND <0.025 <0.025 NA <0.025 11/23/15 <0.005 0.885 <0.005 <0.005 <0.025 0.312 <0.025 0.0115 2.26 <0.005 <0.015 <0.005 <0.005 <0.005 <0.005 <0.25 <0.05 <0.05 <0.025 <0.005 <0.0125 <0.005 NA 2W-11 12/12/16 <0.002 1.9 <0.002 <0.004 <0.008 0.074 <0.004 0.012J 0.21 0.00088J <0.012 <0.002 NA <0.002 0.0026J <0.2 <0.08 <0.04 <0.008 <0.008 0.0027J <0.004 NA 12/19/18 <0.001 0.314 <0.001 <0.001 <0.005 0.0178 <0.001 0.0008 0.0121 0.0982 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 <0.005 <0.005 <0.0025 <0.001 NA 07/08/14 <0.005 0.43 <0.005 <0.005 NA 1.1 <0.005 0.0028J 0.27 0.0043J <0.005 <0.0050 NA <0.005 <0.005 <0.1 <0.1 <0.1 ND <0.005 <0.005 NA <0.005 2W 12 11/23/15 <0.001 0.564 <0.001 <0.001 <0.005 1.17 <0.005 0.00749 0.249 <0.001 <0.003 <0.001 0.00107 <0.001 <0.001 <0.05 <0.01 <0.01 <0.005 <0.001 <0.0025 <0.001 NA Page 2 of 4 Table 8: Analytical Data for Groundwater DSCA ID No.: DC680002 O 0 o > o N N V1 N U N Lam. A N O U N N A Q Y O Oi. N� ^ -Z 0 U F F� " o o F E- 3 'O bo N u L' y ° O cv 7 U I U U [mg/L] Con 09/23/08 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 NA NA NA NA <0.005 NA NA NA 10/21/10 <0.001 <0.001 <0.001 <0.001 <0.001 0.00084J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0023J <0.01 <0.01 ND <0.001 0.00044J <0.001 NS 01/21/11 <0.001 <0.001 <0.001 <0.001 <0.001 0.00048J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0025J <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 <0.001 <0.001 <0.001 <0.001 <0.001 0.00061J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 07/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 Mw-1 08/30/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 1 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/22/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 10/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 02/23/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 05/24/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/04/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 11/12/13 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 <0.005 0.00036J <0.002 <0.005 <0.005 <0.005 <0.005 <0.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA N/A 09/23/08 <0.005 0.799 <0.005 <0.005 <0.005 40.7 <0.005 0.0619 1.208 0.0191 <0.005 <0.005 NA 0.0693 <0.005 NA NA NA NA <0.005 NA NA NA 01/30/09 <0.001 0.8 <0.001 <0.001 <0.001 31.57 <0.001 0.046 1.886 0.00377 <0.001 <0.001 NA <0.001 0.0249 NA NA NA NA <0.001 <0.001 NA NA 10/21/10 <0.05 0.322 <0.05 <0.05 <0.05 4.63 <0.001 <0.001 0.451 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.01 <0.01 ND <0.001 <0.001 <0.001 NS 01/21/11 <0.05 1.29 <0.05 <0.05 <0.05 40.4 <0.001 0.0878 3.1 <0.05 <0.05 <0.05 <0.05 <0.05 0.0505 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 <0.05 1.46 <0.05 <0.05 <0.05 48.4 <0.001 <0.001 2.76 <0.05 <0.05 <0.05 <0.05 <0.05 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 0.198J NS 07/18/11 <1.0 <1.0 <1.0 <1.0 <1.0 34.0 <1.0 <1.0 2.6 <1.0 <3.0 <1.0 <1.0 <1.0 <1.0 <50 <10 <10 ND <1.0 <2.5 <1.0 <1.0 08/30/11 <0.250 1.2 <0.250 <0.250 <0.250 40.0 <0.250 <0.250 3.6 <0.250 <0.750 <0.250 <0.250 <0.250 <0.250 <12 <2.5 <2.5 ND <0.250 <0.620 <0.250 <0.250 09/22/11 <0.250 7.2 <0.250 <0.250 <0.250 30.0 <0.250 <0.250 2.4 <0.250 <0.750 <0.250 <0.250 <0.250 <0.250 <12 <2.5 <2.5 ND <0.250 <0.620 <0.250 <0.250 Mw-2 10/18/11 <0.250 1 15 <0.250 <0.250 <0.250 <0.250 1 <0.250 <0.250 <0.250 <0.250 <0.750 1 <0.250 <0.250 <0.250 <0.250 <12 <2.5 <2.5 ND <0.250 <0.620 <0.250 <0.250 11/18/11 <0.100 1.3 <0.100 <0.100 <0.100 40.0 <0.100 <0.100 3.2 <0.100 <0.300 <0.100 <0.100 <0.100 <0.100 <1.0 <1.0 <1.0 ND I <0.100 <0.250 <0.100 <0.100 02/23/12 <0.100 1.2 <0.100 <0.100 <0.100 37.0 <0.100 <0.100 3.0 <0.100 <0.300 <0.100 <0.100 <0.100 <0.100 <1.0 <1.0 <1.0 ND <0.100 <0.250 <0.100 <0.100 05/24/12 <0.100 1.1 <0.100 <0.100 <0.100 37.0 <0.100 1 <0.100 2.6 <0.100 <0.300 <0.100 <0.100 <0.100 <0.100 <1.0 <1.0 <1.0 ND <0.100 1 <0.250 <0.100 <0.100 09/04/12 <0.250 1.1 <0.250 <0.250 <0.250 35.0 <0.250 <0.250 2.5 <0.250 <0.750 <0.250 <0.250 <0.250 <0.250 <12 <2.5 <2.5 ND <0.250 <0.620 <0.250 <0.250 11/12/13 <2.5 0.99 J <2.5 <2.5 NA 43.0 <2.5 <2.5 2.9 <1 <2.5 <2.5 <2.5 <2.5 <2.5 <10 <5 <5 ND <2.5 <2.5 NA NA 11/23/15 <0.005 0.6 <0.005 <0.005 <0.025 13.9 <0.025 0.0415 1.36 <0.005 <0.015 <0.005 <0.005 <0.005 0.0246 <0.25 <0.05 <0.05 <0.025 <0.025 <0.025 <0.005 NA 12/12/16 <0.01 0.5 <0.01 <0.01 <0.02 0.62 <0.01 0.00396J 0.21 0.0023J <0.03 <0.01 NA <0.01 <0.01 <0.5 <0.2 <0.1 <0.02 <0.02 <0.02 <0.01 NA 12/19/18 <0.001 0.736 <0.001 <0.001 <0.005 14.2 <0.001 0.0478 1.69 0.103 <0.003 <0.001 0.00211 <0.001 0.0228 <0.05 <0.01 <0.01 <0.005 <0.005 <0.0025 <0.001 NA 09/24/08 <0.005 1.8 <0.005 <0.005 <0.005 5.134 <0.005 <0.005 0.73 <0.005 <0.005 <0.005 NA <0.005 <0.005 NA NA NA NA <0.005 NA NA NA 01/30/09 <0.001 0.893 <0.001 <0.001 <0.001 3.073 <0.001 0.013 0.629 <0.001 <0.001 <0.001 NA <0.001 <0.001 NA NA NA NA <0.001 <0.001 NA NA 10/21/10 <0.005 0.68 <0.005 <0.005 <0.001 1.89 <0.005 0.0092J 0.392 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.05 <0.01 <0.01 ND <0.005 <0.001 <0.001 NS 01/21/11 <0.005 1.3 <0.005 <0.005 <0.001 1.86 <0.005 0.0172 0.408 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.25 <0.01 I <0.01 ND <0.005 <0.01 <0.001 NS 04/29/11 <0.005 1.23 <0.005 <0.005 <0.001 1.42 <0.005 0.0148 0.319 <0.005 <0.001 <0.005 <0.005 <0.005 <0.005 <0.25 <0.01 <0.01 ND <0.005 <0.01 <0.001 NS 07/18/11 <0.025 1.4 <0.025 <0.025 <0.025 1.3 <0.025 <0.025 0.42 <0.025 <0.075 <0.025 <0.025 <0.025 <0.025 <1.2 <0.25 <0.25 ND <0.025 <0.062 <0.25 <0.25 08/30/11 <0.01 1.7 <0.01 <0.01 <0.01 1.8 <0.01 0.021 0.51 <0.001 <0.003 <0.01 <0.001 <0.01 <0.001 <0.500 <0.1 <0.1 ND I <0.01 <0.025 <0.001 0.012 M'-3 09/22/11 <0.01 2.0 <0.01 <0.01 <0.01 1.7 <0.01 0.021 0.53 <0.001 <0.003 <0.01 <0.001 <0.01 <0.01 <0.500 <0.1 <0.1 ND <0.01 <0.025 <0.001 0.014 10/18/11 <0.01 2.1 <0.01 <0.01 <0.01 2.5 <0.01 0.028 0.67 <0.001 <0.003 <0.01 0.017 <0.01 <0.01 <0.500 <0.1 <0.1 ND <0.01 <0.025 <0.001 <0.001 11/18/11 <0.002 2.7 <0.002 <0.002 <0.002 4.4 <0.002 0.031 0.96 <0.002 <0.006 <0.002 0.027 <0.002 0.0027 <0.100 <0.20 <0.20 ND <0.002 <0.005 <0.002 <0.002 02/23/12 <0.025 2.8 <0.025 <0.025 <0.025 4.1 <0.025 0.032 1.1 <0.025 <0.075 <0.025 <0.025 <0.025 <0.025 <1.2 <0.025 <0.025 ND <0.025 <0.005 <0.025 <0.025 05/24/12 <0.050 2.9 <0.050 <0.050 <0.050 3.3 <0.050 <0.050 1.6 <0.050 <0.150 <0.050 <0.050 <0.050 <0.050 <2.5 <0.050 <0.050 ND <0.050 1 <0.1 <0.050 <0.050 09/04/12 <0.025 4.3 <0.025 <0.025 <0.025 6.6 <0.025 0.05 1.9 <0.025 <0.075 <0.025 0.031 <0.025 <0.025 <1.2 <0.025 <0.025 ND <0.025 <0.005 <0.025 <0.025 11/12/13 <0.5 1 1.5 <0.5 <0.5 NA 5.9 <0.5 <0.5 0.73 <0.2 <0.5 1 <0.5 1 0.031J <0.5 <0.5 <2 <1 <1 ND <0.5 1 <0.5 1 NA NA 11/23/15 <0.001 1 0.756 <0.001 <0.001 <0.005 1.58 <0.005 0.00934 0.335 1 <0.001 <0.003 1 <0.001 1 0.00742 <0.001 0.00106 <0.05 <0.01 <0.010 <0.005 <0.001 <0.0025 1 <0.001 NA Pagc 3 of 4 Table 8: Analytical Data for Groundwater DSCA ID No.: DC680002 O 0 N U Oi. L' Q 9 tiC d N 7 U I U U [mg/L] 09/24/08 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 NA NA NA NA <0.005 NA NA NA 10/21/10 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0022J <0.01 <0.01 ND <0.001 0.00022J <0.001 NS MW4 01/21/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 <0.001 0.00031J <0.001 <0.001 <0.001 0.00071J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 07/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 11/12/13 <0.005 1 <0.005 <0.005 <0.005 NA <0.005 1 <0.005 <0.005 <0.005 1 <0.002 <0.005 1 <0.005 <0.005 <0.005 1 <0.005 <0.02 <0.01 <0.01 I ND <0.005 <0.005 NA <0.005 09/24/08 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 NA NA NA NA <0.005 NA NA NA 10/21/10 <0.001 <0.001 <0.001 <0.001 <0.001 0.00048J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 0.0034J <0.01 <0.01 ND <0.001 <0.001 <0.001 <0.001 01/21/11 <0.001 <0.001 <0.001 <0.001 <0.001 0.00089J <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 04/29/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.25 <0.01 <0.01 ND <0.001 <0.01 <0.001 NS 07/18/11 <0.001 <0.001 I <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 I <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND I <0.001 <0.0025 <0.001 <0.001 08/30/11 <0.001 <0.001 <0.001 <0.001 <0.001 0.0023 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 MW-5 09/22/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 10/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 11/18/11 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 02/23/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 05/24/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 09/04/12 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.005 <0.001 <0.001 I <0.001 <0.003 <0.001 <0.001 <0.001 <0.001 <0.05 <0.01 <0.01 ND <0.001 <0.0025 <0.001 <0.001 11/19/13 <0.005 <0.005 <0.005 <0.005 NA <0.005 <0.005 <0.005 <0.005 <0.002 <0.005 <0.005 <0.005 <0.005 <0.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA N/A MW-6 11/12/13 0.00031J <0.005 <0.005 <0.005 NA <0.005 0.0027J <0.005 <0.005 <0.002 <0.005 <0.005 <0.005 <0.005 <0.005 <0.02 <0.01 <0.01 ND <0.005 <0.005 NA N/A Page 4 of 4 ATTACHMENT 5 MONITORING WELL ABANDONMENT RECORD WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: Lawrence D. Opper Well Contractor Name (or well owner personally abandoning well on his/her property) 3322-A NC Well Contractor Certification Number Regional Probing Services Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. County, State, Variance, etc.) ifknown 3. Well use (check well use): Water Supply Well: ❑Agricultural ❑Municipal/Public ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑Industrial/Commercial ❑Residential Water Supply (shared) ❑Irrigation Non -Water Supply Well: El Aquifer Recharge ❑Aquifer Storage and Recovery ❑Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling El Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage El Subsidence Control ❑Tracer El Other (explain under 7g) 4. Date well(s) abandoned: 2/14/2019 5a. Well location: American Dry Cleaners DC680002 Facility/Owner Name Facility ID# (if applicable) 201 S. Estes Street, Chapel Hill Physical Address, City, and Zip Orange County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 35.929785 N 79.025835 W CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well construction record(s) if available. For multiple injection or non -water supply wells ONLY with the same constructionlabandonment, you can submit one form. 6a. Well ID#: 2W-8 6b. Total well depth: 9 (ftJ 6c. Borehole diameter: Well Dlam 2.0 (in.) 6d. Water level below ground surface: 3 (ft.) 6e. Outer casing length (if known): 6f. Inner casing/tubing length (if known): 3.5 6g. Screen length (if known): 5 (ft.) For Internal Use ONLY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: 1 For multiple injection or non -water supply wells ONLY with the same construction/abandonment, you can submit one form. 7b. Approximate volume of water remaining in well(s): (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: 7d. Amount of disinfectant used: 7e. Sealing materials used (check all that apply): ❑ Neat Cement Grout 0 Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑ Concrete Grout ❑ Drill Cuttings ❑ Specialty Grout ❑ Gravel ❑ Bentonite Slurry ❑ Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: Bentonite 1.4 Ibs/ ft 7g. Provide a brief description of the abandonment procedure: Filled/ hydrated, capped with concrete. Well was partially filled with silt. 8. Certification: Lawrence Opper :" ' ..... -0 2/24/2019 Signature of Certified Well Contractor or Well Owner Date By signing this form, I hereby certify that the well(s) was (were) abandoned in accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 10a. For All Wells: Submit this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Iniection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Quality, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Iniection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. Form GW-30 North Carolina Department of Environment and Natural Resources - Division of Water Quality Revised March 2013 ATTACHMENT 6 GROUNDWATER GRADIENT MAP wF LEGEND r U • z CIO + Monitoring Well Location, Identification and p 8xo IllpF M 09 oo Groundwater Elevation (ft/msl) o U _ y i 4 Deep Mnitoring Well Location, Identification Q d U r * DMW-1 and Groundwater Elevation (ft/msl) - values in U U Q _ (29•87) parentheses not used in contouring IIi � cd a) k y NM Not Measured cd Q - - — — Potentiometric Surface Contour (ft/msl) Q 0 U k Q Inferred Groundwater Flow Direction _ N b All w • Ar- u �_ U N 60.93' aM # �J 2W-2D 2W-8 a$ 2W-2S �NM -• - �, o 261.03 / ¢o�� F Harris Teeter Center MW-3 ti. (@261.01 p (2 0.60.1 6) (5)261.28 2W-9 � �4 � � ~� •� 2W_5 /Olin T. Binkleyrl . * W-10 / Baptist Church r / 260.45 60.56 � . •��,, Former American � 1 MW-2 / •-,4 '# a' Dry -Cleaners Location ✓ 2W ��� 260.70� ® ®259.70 �. F ' do ti ® -2W-12 N O 2W-7 / 260.15 :. # -6 / 260.04 �: lied, - fir. /� •_ f MW- 1 #f NM 'Ahr- r ` _6 - - � N o •� i N 4 y N Z_ 00 r # ft Ln G° °z t _ m a r ' 0 50 a y � - � : • 10 �i SHEET: APPROX. SCALE, ft. ATT. 6 ATTACHMENT 7 GROUNDWATER QUALITY SUMMARY MAP 2W-2D (02/07/2014) 2W`2S (02/07/2014) • • 2W-8 (11/12/2013) BDL TCE - 0.32 J µg/1 dn F go— , 3 2W-4 (05/14/2018) PCE - 3.8 µg/1 TCE - 4.5 µg/1 cis-1,2-DCE - 9.2 µg/l Ittrans-1,2-DCE - 0.24 J µg/1 Vinyl chloride - 3.3 µg/1 �- Ap 2W-5 (05/14/2018) • • Harris Teeter Center cis-1,2-DCE - 470 µg/l trans-1,2-DCE - 10 µg/l Vinyl chloride - 290 µg/1 # Chloroethane - 9.3 J µg/l Toluene - 3.4 J µg/l 2-Butanone - 13 J µg/l -1110i Former American 4P Dry -Cleaners Location MW-2 (12/19/2018) 2-t4h PCE - 14,200 µg/l TCE - 1,690 µg/1 cis-1,2-DCE - 736 µg/l trans-1,2-DCE - 47.8 µg/1 _ Vinyl chloride - 103 µg/1 1,1-DCE - 22.8 µg/1 , # 1,1,2-Trichlorotrifluoroethane - 2.11 µg/l 4%j 2W-7 (11/12/2013) •. BDL MW-1 (11/12/2013) • Benzene - 0.31 J µg/l Toluene - 2.7 J µg/1 s � 2W-6 (05/14/2018) • • .'CE - 160 µgd TCE - 140 µg/1 cis-1,2-DCE - 400 µgd trans-1,2-DCE - 2.6 J µg/l Vinyl chloride - 11 µg/1 F Olin T. Binkley Baptist Church •• MW-3 (11/23/2015) • • PCE - 1,580 µg/l TCE - 335 µg/1 cis-1,2-DCE - 756 µg/1 trans-1,2-DCE - 9.34 µg/l 1,1,2-Trichlorotrifluoroethane - 7.42 µg/l Pv e 2W-12 (11/23/2015) 004 PCE - 1,170 µg/1 TCE - 249 µg/l cis-1,2-DCE - 564 µg/1 trans-1,2-DCE - 7.49 µg/l 1,1,2-Trichlorotrifluoroethane - 1.07 µg/l We MW-4 (11/12/2013) • • BDL 2 W-9 (12/19/20181 • • PCE - 176 µg/1 TCE - 86.2 µg/1 cis-1,2-DCE - 149 µg/l trans-1,2-DCE - 2.29 µg/l 2W-10 (12/19/2018) • • PCE - 48.2 µg/1 TCE - 36.0 µg/1 cis-1,2-DCE - 1,930 µg/l trans-1,2-DCE - 12.6 µg/1 Vinyl chloride - 90.1 µg/1 MW-5 (11/19/2013) BDL 2W-11 (12/19/2018� • • PCE - 17.8 µg/1 TCE - 12.1 µg/1 cis-1,2-DCE - 314 µg/1 trans-1,2-DCE - 8.00 µg/1 Vinyl chloride - 98.2 µg/l MW-1 (11/12/2013) • • TCE - 0.36 J µg/l 1. r LEGEND Monitoring Well Location Deep Monitoring Well Location BDL Below Laboratory Detection Limits µg/1 micrograms per liter — — Potentiometric Surface Contour (ft) 4 Inferred Groundwater Flow Direction J Area of PCE 2L Standard Exceedance Red highlighted text indicates concentrations above 2L Standards. PCE - Tetrachloroethene TCE - Trichloroethene DCE - Dichloroethene 09 Groundwater analytical results exceed calculated vapor intrusion risk for residential and non-residen- tial exposure (DSCA Calculator Version 6 - November 2017). • • Groundwater analytical results do not exceed calculated vapor intrusion risk for non-residential exposure but do exceed for residential exposure (DSCA Calculator Version 6 - November 2017). 09 Groundwater analytical results do not exceed calculated vapor intrusion risk for residential and non-residential exposure (DSCA Calculator Version 6 - November 2017). U =U dQUQ Cd Nk Qun U o �WQ w� 0 N V C R VYmr.iM V32 VryN ¢Z°U? lied, S 0 0 N N i \ \ N M 0 0 U) � z o ILL °z m ° F - � U W o 0 50 SHEET: APPROX. SCALE, ft. ATT. 7 ATTACHMENT 14 INDOOR AIR / SOIL GAS ANALYTICAL RESULTS MAP ram: \NUSu'1A lrrrSvvuu-r\ualaw JGr1A3 UaIa1ZUu\USGAWIIBS\A erican ury Ueaners 8oi5-uuunJire UaIa\ivia s\ uib\r i indoor Air Doll vapor Kesuns Ma .mxa LEGEND y' Soil Gas Sample • Indoor/Ambient Air Sample 0 Site Location PCE-Tetrachloroethene WILLOW DRIVE TCE - Trichloroethene cis-1,2-DCE - cis-1,2-Dichloroethene trans-1,2-DCE - trans-1,2-Dichloroethene ug/m3 micrograms per cubic meter J - estimated concentration Sample does not exceed acceptable00 w. non-residential or residential risk. SV-6 (6/28/17) Sample exceeds acceptable residential risk PCE - 3,850 ug/m3 - • • based on the DSCA Groundwater to TCE - 484 ug/m3 M Indoor Air Resident Risk Calculator. cis-1,2-DCE - 262 ug/m3 Sample exceeds acceptable non-residen- trans-1,2-DCE - 154 ug/m3 00 tial risk based on the DSCA Groundwa- SV-6 (12/12/17) • • ter to Indoor Air Non -Residential Risk PCE - 21,000 ug/m3 Calculator. TCE - 3,300 ug/m3 cis-1,2-DCE - 830 ug/m3 IA-3 (6/12/17 - 6/20/17) • • trans-1,2-DCE - 98 ug/m3 � SV-6 (6/15/18) PCE - 3.2 ug/m3 Sampled TCE - 0.38 ug/m3 Not S SV-6 ample/18) IA-3 (12/11/17-12/18/17) • • Not Sampled PCE - 4.5 ug/m3 HARRIS TEETER TCE - 0.59 ug/m3 -CENTER a . IA-3 (6/8/18 - 6/15/18) 00 PCE - 2.9 ug/m3 09 '` : IA-3 (12/14/18-12/21/18) 00 PCE - 5.9 ug/m3 ! ! TCE - 2.1 ug/m3 ;! IA-3 (8-hr) (1/11/19) 00 !� OQ PCE - 1.4 ug/m3 _ AMF, ICA RY TCE - 0.12 J ug/m3 R LEA IA-3 (1/11/19 - 1/18/19) • • PCE - 2.3 ug/m3 0 TCE - 1.4 ug/m3 j 'S► ' O IA-3 (2/8/19 - 2/15/19) • • W !� �{ ` + PCE - 1.8 ug/m3 A, TCE - 1.6 ug/m3 PCE - 75,800 ug/m3 T. BIN EY -,� TCE - 24,900 ug/m3 Q • F cis-1,2-DCE - 9,740 ug/m3 ,, AP fST CHURCH i x I�4• trans-1,2-DCE - 347 ug/m3wwj f SV-5 (12/12/17) e e r O PCE - 86,000 ug/m3 / TCE - 23,000 ug/m3 IA-2 (6/12/17 - 6/20/17) F" cis-1,2-DCE - 11,000 ug/m3 PCE - 3.1 ug/m3 trans-1,2-DCE - 260 ug/m3 TCE - 0.35 ug/m3 Z SV-5 (6/15/18) 00 IA-2 (12/11/17-12/18/17) • • PCE - 140,000 ug/m3 PCE - 4.3 ug/m3 TCE - 40,000 ug/m3 TCE - 0.59 ug/m3 cis-1,2-DCE - 18,000 ug/m3 IA-2 (6/8/18 - 6/15/18) A O trans-1,2-DCE - 480 ug/m3 PCE - 2.8 ug/m3 SV-5 (12/19/18) 00 1 IA-2 (12/14/18-12/21/18) 00 I PCE - 120,000 ug/m3 PCE - 4.6 ug/m3 TCE - 24,000 ug/m3 { TCE - 1.9 ug/m3 cis-1,2-DCE - 9,800 ug/m3 IA-2 (8-hr) (1/11/19) 00 trans-1,2-DCE - 390 ug/m3 PCE - 1.4 ug/m3 TCE - 0.15 J ug/m3 t l r IA-2 (1/11/19-1/18/19) 00�? = PCE - 2.6 ug/m3 TCE - 1.6 ug/m3 0 100 IA-2 (2/8/19 - 2/15/19) 00 y PCE - 2.5 ug/m3 •` TCE - 1.6 ug/m3 Feet Indoor Air/Soil Gas Results Map T A AECOM TECHNICAL SERVICES N N �COMOFNORTHCAROLINA, INC American Dry Cleaners pa a z 5925 CARNEGIE BOULEVARD, SUITE 370 CHARLOTTE,NC 28209 r`DE 201 South Estes Drive TEL: (704) 553-6150 7� �7('1 U •q Z o C FAX: (704) 553-6151 Door Chapel Hill, 1V C � U U k' �' 10 SHEET: DSCA Site # DC680002 Attachment 14 ATTACHMENT 15 LABORATORY ANALYTICAL REPORTS icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 June 26, 2018 Nick Shore AECOM-Morrisville NC 1600 Perimeter Park Drive Morrisville, NC 27560 Project Location: DC680002 (Chapel Hill) Client Job Number: Project Number: 60535849 Laboratory Work Order Number: 18F1081 Enclosed are results of analyses for samples received by the laboratory on June 18, 2018. If you have any questions concerning this report, please feel free to contact me. Sincerely, I,&, �. A�� Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 AECOM-Morrisville NC REPORT DATE: 6/26/2018 1600 Perimeter Park Drive Morrisville, NC 27560 PURCHASE ORDER NUMBER: 60535849 ATTN: Nick Shore PROJECT NUMBER: 60535849 ANALYTICAL SUMMARY WORK ORDER NUMBER: 18F1081 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: DC680002 (Chapel Hill) FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB IA-2 18F1081-01 Indoor air RAD 130 IA-3 18171081-02 Indoor air RAD 130 SV-5 18171081-03 Soil Gas EPATO-15 Page 2 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method Radiello RAD-130 - The sampling rates for trichloroethene and tetrachloroethene are as follows: trichloroethene = 69 mL/min, tetrachloroethene = 59 mL/min. The theoretical sampling rates for vinyl chloride, trans-1,2-dichloroethene, and cis-1,2-dichloroethene are estimated using Graham's Law and are as follows: vinyl chloride = 103 mL/min, trans-1,2-dichloroethene = 83 mL/min, cis-1,2-dichloroethene = 83 mL/min. The results for these 3 compounds are estimated values. EPA TO-15 Qualifications Elevated reporting limit due to high concentration of target compounds. Analyte & Samples(s) Qualified: 18F1081-03[SV-51 The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. 4Z�14__ VWWLO_� Lisa A. Worthington Project Manager Page 3 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: DC680002 (Chapel Hill) Sample Description/Location: Work Order: 18F1081 Date Received: 6/18/2018 Sub Description/Location: Field Sample #: IA-2 Sample ID: 18F1081-01 Sample Matrix: Indoor air Flow Controller ID: Sampled: 6/15/2018 11:45 Sample Type: Air Volume L: 10165 RAD 130 Total µg ug/m3 Date/Time Analyte Results RL MDL Flag/Qua[ Results ILL MDL Dilution Analyzed Analyst Vinyl Chloride ND 0.16 ND 0.15 1 6/25/18 12:58 CJM trans-1,2-Dichloroethene ND 1.0 ND 1.2 1 6/25/18 12:58 CJM cis-1,2-Dichloroethene ND 0.20 ND 0.24 1 6/25/18 12:58 CJM Tichloroethene ND 0.20 ND 0.29 1 6/25/18 12:58 CJM Tetrachloroethene 1.7 0.20 2.8 0.33 1 6/25/18 12:58 CJM Page 4 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: DC680002 (Chapel Hill) Sample Description/Location: Work Order: 18171081 Date Received: 6/18/2018 Sub Description/Location: Field Sample #: IA-3 Sample ID: 18F1081-02 Sample Matrix: Indoor air Flow Controller ID: Sampled: 6/15/2018 11:50 Sample Type: Air Volume L: 10165 RAD 130 Total µg ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Vinyl Chloride ND 0.16 ND 0.15 1 6/25/18 12:34 CJM trans-1,2-Dichloroethene ND 1.0 ND 1.2 1 6/25/18 12:34 CJM cis-1,2-Dichloroethene ND 0.20 ND 0.24 1 6/25/18 12:34 CJM Tichloroethene ND 0.20 ND 0.29 1 6/25/18 12:34 CJM Tetrachloroethene 1.8 0.20 2.9 0.33 1 6/25/18 12:34 CJM Page 5 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: DC680002 (Chapel Hill) Sample Description/Location: Work Order: 18171081 Date Received: 6/18/2018 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: SV-5 Canister ID: 1672 Final Vacuum(in Hg): -6 Sample ID: 18F1081-03 Canister Size: 6 liter Receipt Vacuum(in Hg): -8.7 Sample Matrix: Soil Gas Flow Controller ID: 4291 Flow Controller Type: Fixed -Orifice Sampled: 6/15/2018 12:50 Sample Type: 30 min Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 Sample Flags: RL-11 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst cis-1,2-Dichloroethylene 4500 20 8.2 18000 79 32 400 6/22/18 20:58 BRF trans-1,2-Dichloroethylene 120 20 8.0 480 79 32 400 6/22/18 20:58 BRF Tetrachloroethylene 20000 200 110 140000 1400 750 4000 6/22/18 21:34 BRF Trichloroethylene 7500 20 8.1 40000 110 43 400 6/22/18 20:58 BRF Vinyl Chloride ND 20 13 ND 51 32 400 6/22/18 20:58 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 94.9 70-130 6/22/18 20:58 4-Bromofluorobenzene(1) 108 70-130 6/22/18 21:34 Page 6 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep -EPA TO-15 Pre-Dil Pre-Dil Default Actual Pressure Pre Initial Final Injection Injection Lab Number [Field ID] Batch Dilution Dilution mL mL mL mL Date 18F1081-03[SV-5] B206533 2 200 5 1000 400 400 06/22/18 18F1081-03RE1[SV--5] B206533 2 200 5 1000 400 40 06/22/18 Prep Method: Radiello-RAD 130 Lab Number [Field ID] Batch Initial [Cartridge Final [mL] Date 18F1081-01 [IA-2] B206503 1.00 2.00 06/25/18 18F1081-02 [IA-3] B206503 1.00 2.00 06/25/18 Page 7 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Miscellaneous Air Analyses - Quality Control Total µg ug/m3 Spike Level Source %REC RPD nalyte Results RL Results RL Total µg Result %REC Limits RPD Limit Flag/Qua Batch B206503 - Radiello Blank (B206503-BLK1) Prepared & Analyzed: 06/25/18 Vinyl Chloride ND 0.16 trans-1,2-Dichloroethene ND 1.0 cis-1,2-Dichloroethene ND 0.20 Trichloroethene ND 0.20 Tetrachloroethene ND 0.20 LCS (B206503-BSI) Prepared & Analyzed: 06/25/18 Vinyl Chloride 7.45 0.16 0.41 10.0 74.5 40-140 trans-1,2-Dichloroethene 7.83 1.0 10.0 78.3 40-140 cis-1,2-Dichloroethene 7.75 0.20 10.0 77.5 40-140 Trichloroethene 6.75 0.20 10.0 67.5 40-140 Tetrachloroethene 6.50 0.20 10.0 65.0 40-140 LCS Dup (B206503-BSD1) Prepared & Analyzed: 06/25/18 Vinyl Chloride 6.86 0.16 0.41 10.0 68.6 40-140 8.25 30 trans-1,2-Dichloroethene 7.88 1.0 10.0 78.8 40-140 0.713 30 cis-1,2-Dichloroethene 7.91 0.20 10.0 79.1 40-140 2.07 30 Trichloroethene 6.99 0.20 10.0 69.9 40-140 3.47 30 Tetrachloroethene 6.79 0.20 10.0 67.9 40-140 4.27 30 Page 8 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD Analyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual Batch B206533 - TO-15 Prep Blank (B206533-BLKI) Prepared & Analyzed: 06/22/18 cis-1,2-Dichloroethylene ND 0.035 trans-1,2-Dichloroethylene ND 0.035 Tetrachloroethylene ND 0.035 Trichloroethylene ND 0.035 Vinyl Chloride ND 0.035 Surrogate: 4-Bromofluorobenzene (1) 7.67 8.00 95.9 70-130 LCS (B206533-BSI) Prepared & Analyzed: 06/22/18 cis-1,2-Dichloroethylene 5.96 5.00 119 70-130 trans-1,2-Dichloroethylene 5.63 5.00 113 70-130 Tetrachloroethylene 5.72 5.00 114 70-130 Trichloroethylene 6.00 5.00 120 70-130 Vinyl Chloride 5.50 5.00 110 70-130 Surrogate: 4-Bromofluorobenzene (1) 7.75 8.00 96.9 70-130 Duplicate (B206533-DUPl) Source: 18F1081-03RE1 Prepared & Analyzed: 06/22/18 cis-1,2-Dichloroethylene 3100 200 12000 790 3300 6.04 25 trans-1,2-Dichloroethylene ND 200 ND 790 ND 25 Tetrachloroethylene 19000 200 130000 1400 20000 7.93 25 Trichloroethylene 5100 200 28000 1100 5400 4.11 25 Vinyl Chloride ND 200 ND 510 ND 25 Surrogate: 4-Bromofluorobenzene (1) 8.54 8.00 107 70-130 Page 9 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 * FAX 413/525-6405 " TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. RL-11 Elevated reporting limit due to high concentration of target compounds. ANALYST PEB Paula E. Blakeborough KKM Kerry K. McGee KDM Karly D. Monette IMR Irina Raducan CJM Christian J. Merchant BRF Brittany R. Fisk Page 10 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (S024524-ICV1) Lab File ID: G062019.13 Analyzed: 06/21/18 01:03 Bromochloromethane (1) 145324 8.563 132100 8.563 110 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 412402 10.471 384286 10.471 107 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 267512 15.257 245397 15.263 109 60-140 -0.0060 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S024618-CCVI) Lab File ID: G062204.1) Analyzed: 06/22/18 11:03 Bromochloromethane (1) 140694 8.563 132100 8.563 107 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 397039 10.477 384286 10.471 103 60 - 140 0.0060 +/-0.50 Chlorobenzene-d5(1) 252927 15.263 245397 15.263 103 60-140 0.0000 +/-0.50 LCS (B206533-BS1 ) Lab File ID: G062205.13 Analyzed: 06/22/18 11:39 Bromochloromethane (1) 144686 8.563 140694 8.563 103 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 407752 10.477 397039 10.477 103 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 267045 15.263 252927 15.263 106 60-140 0.0000 +/-0.50 Blank (B206533-BLK1) Lab File ID: G062209.13 Analyzed: 06/22/18 14:09 Bromochloromethane (1) 127368 8.569 140694 8.563 91 60 - 140 0.0060 +/-0.50 1,4-Difluorobenzene (1) 328982 10.477 397039 10.477 83 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 202263 15.263 252927 15.263 80 60-140 0.0000 +/-0.50 SV-5 (18F1081-03 ) Lab File ID: G062218.13 Analyzed: 06/22/18 20:58 Bromochloromethane (1) 156139 8.563 140694 8.563 ill 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 397576 10.471 397039 10.477 100 60 - 140 -0.0060 +/-0.50 Chlorobenzene-d5 (1) 248499 15.263 252927 15.263 98 60 - 140 0.0000 +/-0.50 SV-5 (18F1081-03RE1) Lab File ID: G062219.D Analyzed: 06/22/18 21:34 Bromochloromethane (1) 139718 8.563 140694 8.563 99 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 363011 10.471 397039 10.477 91 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 235534 15.263 252927 15.263 93 60-140 0.0000 +/-0.50 Duplicate (B206533-DUP1) Lab File ID: G062220.D Analyzed: 06/22/18 22:10 Bromochloromethane (1) 136213 8.569 140694 8.563 97 60 - 140 0.0060 +/-0.50 1,4-Difluorobenzene(1) 351673 10.477 397039 10.477 89 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 233300 15.263 252927 15.263 92 60-140 0.0000 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY RAD 130 Reference Reference Area % RT Diff Internal Standard Response RT Response RT Area % Limits RT Diff Limit Q Blank (B206503-BLK1 Lab File ID: B0625004.D Analyzed: 06/25/18 10:58 2-Fluorotoluene 7644063 13.463 6581909 13.463 116 50-200 0.0000 +/-0.50 Page 11 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY RAD 130 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Diff RT Diff Limit Q LCS (B206503-BS1 Lab File ID: B0625005.1) Analyzed: 06/25/18 11:22 2-Fluorotoluene 6709368 13.462 6581909 13.463 102 50-200 -0.0010 +/-0.50 LCS Dup (B206503-BSD1) Lab File ID: B0625006.D Analyzed: 06/25/18 11:46 2-Fluorotoluene 7120248 13.46 6581909 13.463 108 50-200 -0.0030 +/-0.50 IA-3 (18F1081-02 ) Lab File ID: B0625008.D Analyzed: 06/25/18 12:34 2-Fluorotoluene 7917735 13.462 6581909 13.463 120 50-200 -0.0010 +/-0.50 IA-2 (18F1081-01 ) Lab File ID: B0625009.D Analyzed: 06/25/18 12:58 2-Fluorotoluene 7937254 13.461 6581909 13.463 121 50-200 -0.0020 +/-0.50 Page 12 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S024618-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) cis-1,2-Dichloroethylene A 5.00 5.58 0.7528265 0.8395184 11.5 30 trans-1,2-Dichloroethylene A 5.00 5.26 0.7430221 0.7824413 5.3 30 Tetrachloroethylene A 5.00 5.43 0.3718453 0.4038604 8.6 30 Trichloroethylene A 5.00 5.61 0.2775193 0.3113528 12.2 30 Vinyl Chloride A 5.00 5.27 0.4694811 0.4944404 5.3 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 13 of 17 icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications EPA TO-15 in Air cis-1,2-Dichloroethylene AIHA,FL,NY,VA trans-1,2-Dichloroethylene AIHA,NJ,NY,VA Tetrachloroethylene AIHA,FL,NJ,NY,VA Trichloroethylene AIHA,FL,NJ,NY,VA Vinyl Chloride AIHA,FL,NJ,NY,VA The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2018 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LA000112 12/30/2018 NC North Carolina Div. of Water Quality 652 12/31/2018 NJ New Jersey DEP MA007 NELAP 06/30/2019 FL Florida Department of Health E871027 NELAP 06/30/2018 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2018 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2018 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2018 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2019 NC-DW North Carolina Department of Health 25703 07/31/2018 Page 14 of 17 16 m c�_ S U R O M a h... _..__. :. .... ++ 0 Lab Receipt Pressure a o Final Pressure ` m E- _ initial Pressure U C � � O L3J an mui O M ce 00 Q �e Z I N X [ a � D � Q n Q r N 5 Q O �. I E -- �1 �CQ T 49 � a � cAl E� h E s��C 2 E UO .a ar R 5 CY .a OS OL! F- U a µ. O O O m m rr 1 ,I — a � � m a � m `. a cse a v U U Page 15 of 17 6/21/2018 FedEx I Tracking, Shipping, and Locations E3,AbjM0tt[ber McLOGIN Welcome to PASSWORD FedEx ID USER (HTTPS://W W W.FEDEX.COMIFCL/WEB/JSP/FokGOTPASSWORD,JSP? APPNAME=FCLFSM&LOCALE=US EN&STEP30RL=HTTPS%3A%2F%2FWWW.FEDEX,COM%2FSHIPF 0 0GO exclusive benefits RATE SNIP TRACK LOCATIONS when you open a FedEx account, TRACKNGID 772502794133 CREATE ACCOUNT (HTTPS:// W W W.FEDEX.COM/EN- USlCREATE- ACCOUNT.HTML) TRACK MULTIPLE TRACKING NUMBERS I NEED HELP? (KrTP:pW W W.FEDEX.COM/US/TRACKING/P—OUICKHELP.HTML) Delivered Wednesday 6/20/2018 at 12:55 pm DELIVERED Signed for by: RPETRAITIS Add to Watch List FROM Raleigh, NC US TO LAST LONGMEADOW, MA US SEE FULL DETAILS https:f/www,fedex,com/en-us/home.html I Page 16 of 17 Received By PR Data (n Time How were the samples In Cooler 'on ice No Ice received? In Box -T- Ambient Melted Ice Were samples within Temperature By Gun # Actual Temp - Compliance? 2-6'C t 3 P By Blank # Actual Temp - Was Custody Seal Intact? 4,-�VA Were Samples Tampered with? tQ FA Was COC Relinquished ? -T-w Does Chain Agree With Samples? Are there any loose caps/valves on any samples? - Is COC in ink/ Legible? -I Did COC Include all Client z Analysis T Sam ler Name w Pertinent Information? Project -T- Are Sample Labels filled out and legible? Are there Rushes? I Samples are received within Folding time? Proper Media Used? Are there Trip Blanks? P ID's Collection Dates/Times i _:I:_ Who was notified? t Individually Certified Cans? Is there enough Volume? Summa Cans Nut/Ferrule IC Train Tedlar Baqs Tubing TO-17 Tubes T-Connector Radiello Syringe Pufs/TO-11 s Tedlar O �FaceAnalXical o National Center for Testing & Innovation ANALYTICAL REPORT December 31, 2018 AECOM - Raleigh, NC Sample Delivery Group: Samples Received: Project Number: Description: Site: Report To: L1055119 12/20/2018 60566538 American Dry Cleaners DC680002 DC680002 Stephanie Hempel 1600 Perimeter Park Drive Suite 400 Morrisville. NC 27560 Entire Report Reviewed By: �� �4 J Chris McCord Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. V 0 TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page CID Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 FS 2W-9 L1055119-01 5 [Cn] 2W-10 L1055119-02 7 2W-11 L1055119-03 9 Fr MW-2 L1055119-04 11 Qc: Quality Control Summary 13 RC Volatile Organic Compounds (GC/MS) by Method 8260B 13 F GI: Glossary of Terms 19 Al: Accreditations & Locations 20 rAI Sc: Sample Chain of Custody 21 FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 2 of 22 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time 2W-9 L1055119-01 GW Stephanie Hempel 12/19/1813:15 12/20/18 09:30 FP1 Method Batch Dilution Preparation Analysis Analyst date/time date/time FTC Volatile Organic Compounds (GC/MS) by Method 8260B WG1214884 1 12/22/18 01:27 12/22/18 01:27 TJJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1215213 5 12/23/1818:14 12/23/1818:14 BMB Collected by Collected date/time Received date/time 2W-10 L1055119-02 GW Stephanie Hempel 12/19/1813:30 12/20/18 09:30 4 n Method Batch Dilution Preparation Analysis Analyst date/time Fdate/time Volatile Organic Compounds (GC/MS) by Method 8260E WG1214884 5 12/22/18 01:47 12/22/18 01:47 GLN Volatile Organic Compounds (GC/MS) by Method 8260E WG1216589 100 12/27/18 20:09 12/27/18 20:09 JHH RC Collected by Collected date/time Received date/time F 2W-11 L1055119-03 GW Stephanie Hempel 12/19/1813:50 12/20/18 09:30 Method Batch Dilution Preparation Analysis Analyst FAI date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260B WG1214884 1 12/22/18 02:07 12/22/18 02:07 TJJ Volatile Organic Compounds (GC/MS) by Method 8260B WG1215213 5 12/23/1818:53 12/23/1818:53 BMB FSC Collected by Collected date/time Received date/time MW-2 L1055119-04 GW Stephanie Hempel 12/19/1814:20 12/20/18 09:30 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 8260E WG1214884 1 12/22/18 02:26 12/22/18 02:26 BMB Volatile Organic Compounds (GC/MS) by Method 8260E WG1215213 10 12/23/1819:12 12/23/1819:12 BMB Volatile Organic Compounds (GC/MS) by Method 8260E WG1216589 200 12/27/18 20:28 12/27/18 20:28 JHH ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 3 of 22 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. C-L I �'J��j V,-"---j Chris McCord Project Manager FP1 FTC FSS FSr FC-1 F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 4 of 22 2W-9 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 12/19/18 13:15 L1055119 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch u Analyte mg/I mg/I date /time Acetone ND 0.0500 1 12/22/2018 01:27 WG1214884 FTc Acrolein ND 0.0500 1 12/22/2018 01:27 WG1214884 Acrylonitrile ND 0.0100 1 12/22/2018 01:27 WG1214884 F Benzene ND 0.00100 1 12/22/2018 01:27 WG1214884 Bromobenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 Bromodichloromethane ND 0.00100 1 12/22/2018 01:27 WG1214884 rCn Bromoform ND 0.00100 1 12/22/2018 01:27 WG1214884 Bromomethane ND 0.00500 1 12/22/2018 01:27 WG1214884 n-Butylbenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 sec -Butyl benzene ND 0.00100 1 12/22/2018 01:27 WG1214884 ter[-Butylbenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 Fc Carbon tetrachloride ND 0.00100 1 12/22/2018 01:27 WG1214884 Chlorobenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 Fq Chlorodibromomethane ND 0.00100 1 12/22/2018 01:27 WG1214884 Chloroethane ND 0.00500 1 12/22/2018 01:27 WG1214884 Chloroform ND 0.00500 1 12/22/2018 01:27 WG1214884 FAI Chloromethane ND 0.00250 1 12/22/2018 01:27 WG1214884 2-Chlorotoluene ND 0.00100 1 12/22/2018 01:27 WG1214884 F 4-Chlorotoluene ND 0.00100 1 12/22/2018 01:27 WG1214884 1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/22/2018 01:27 WG1214884 1,2-Dibromoethane ND 0.00100 1 12/22/2018 01:27 WG1214884 Dibromomethane ND 0.00100 1 12/22/2018 01:27 WG1214884 1,2-Dichlorobenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 1,3-Dichlorobenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 1,4-Dichlorobenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 Dichlorodifluoromethane ND 0.00500 1 12/22/2018 01:27 WG1214884 1,1-Dichloroethane ND 0.00100 1 12/22/2018 01:27 WG1214884 1,2-Dichloroethane ND 0.00100 1 12/22/2018 01:27 WG1214884 1,1-Dichloroethene ND 0.00100 1 12/22/2018 01:27 WG1214884 cis-1,2-Dichloroethene 0.149 0.00100 1 12/22/2018 01:27 WG1214884 trans-1,2-Dichloroethene 0.00229 0.00100 1 12/22/2018 01:27 WG1214884 1,2-Dichloropropane ND 0.00100 1 12/22/2018 01:27 WG1214884 1,1-Dichloropropene ND 0.00100 1 12/22/2018 01:27 WG1214884 1,3-Dichloropropane ND 0.00100 1 12/22/2018 01:27 WG1214884 cis-1,3-Dichloropropene ND 0.00100 1 12/22/2018 01:27 WG1214884 trans-1,3-Dichloropropene ND 0.00100 1 12/22/2018 01:27 WG1214884 2,2-Dichloropropane ND 0.00100 1 12/22/2018 01:27 WG1214884 Di -isopropyl ether ND 0.00100 1 12/22/2018 01:27 WG1214884 Ethylbenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 Hexachloro-1,3-butadiene ND 0.00100 1 12/22/2018 01:27 WG1214884 Isopropylbenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 p-Isopropyltoluene ND 0.00100 1 12/22/2018 01:27 WG1214884 2-Butanone (MEK) ND 0.0100 1 12/22/2018 01:27 WG1214884 Methylene Chloride ND 0.00500 1 12/22/2018 01:27 WG1214884 4-Methyl-2-pentanone (MIBK) ND 0.0100 1 12/22/2018 01:27 WG1214884 Methyl tert-butyl ether ND 0.00100 1 12/22/2018 01:27 WG1214884 Naphthalene ND 0.00500 1 12/22/2018 01:27 WG1214884 n-Propylbenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 Styrene ND 0.00100 1 12/22/2018 01:27 WG1214884 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/22/2018 01:27 WG1214884 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/22/2018 01:27 WG1214884 1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/22/2018 01:27 WG1214884 Tetrachloroethene 0.176 0.00500 5 12/23/201818:14 WG1215213 Toluene ND 0.00100 1 12/22/2018 01:27 WG1214884 1,2,3-Trichlorobenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 1,2,4-Trichlorobenzene ND 0.00100 1 12/22/2018 01:27 WG1214884 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 5 of 22 ONE LAB. NATIONWIDE. 2W-9 SAMPLE RESULTS - 01 Collected date/time: 12/19/18 13:15 L1055119 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Analyte mg/I mg/I 1,1,1-Trichloroethane ND 0.00100 1,1,2-Trichloroethane ND 0.00100 Trichloroethene 0.0862 0.00100 Trichlorofluoromethane ND 0.00500 1,2,3-Trichloropropane ND 0.00250 1,2,4-Trimethyl ben zene ND 0.00100 1,2,3-Trimethyl benzene ND 0.00100 1,3,5-Trimethyl benzene ND 0.00100 Vinyl chloride ND 0.00100 Xylenes, Total ND 0.00300 (S) Toluene-d8 104 80.0-120 (S) Toluene-d8 102 80.0-120 (S) Dibromofluoromethane 98.2 75.0-120 (S) Dibromofluoromethane 98.7 75.0-120 (S) 4-Bromof/uorobenzene 93.0 77.0-126 (S) 4-Bromofluorobenzene 109 77.0-126 Dilution Analysis date / time 12/22/2018 01:27 12/22/2018 01:27 12/22/2018 01:27 12/22/2018 01:27 12/22/2018 01:27 12/22/2018 01:27 12/22/2018 01:27 12/22/2018 01:27 12/22/2018 01:27 12/22/2018 01:27 1212212018 01:27 121231201818.14 1212212018 01:27 121231201818.14 1212212018 01:27 121231201818.14 Batch WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1215213 WG1214884 WG1215213 WG1214884 WG1215213 Fp FTc FS Fn N FC] F ql FAI FSC ACCOUNT: PROJECT: SDG: AECOM - Raleigh, NC 60566538 L1055119 DATE/TIME: PAGE: 12/31/1815:20 6 of 22 2 W -10 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 12/19/18 13:30 L1055119 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time Acetone ND 0.250 5 12/22/2018 01:47 WG1214884 Acrolein ND 0.250 5 12/22/2018 01:47 WG1214884 Acrylonitrile ND 0.0500 5 12/22/2018 01:47 WG1214884 Benzene ND 0.00500 5 12/22/2018 01:47 WG1214884 Bromobenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 Bromodichloromethane ND 0.00500 5 12/22/2018 01:47 WG1214884 Bromoform ND 0.00500 5 12/22/2018 01:47 WG1214884 Bromomethane ND 0.0250 5 12/22/2018 01:47 WG1214884 n-Butylbenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 sec -Butyl benzene ND 0.00500 5 12/22/2018 01:47 WG1214884 ter[-Butylbenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 Carbon tetrachloride ND 0.00500 5 12/22/2018 01:47 WG1214884 Chlorobenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 Chlorodibromomethane ND 0.00500 5 12/22/2018 01:47 WG1214884 Chloroethane ND 0.0250 5 12/22/2018 01:47 WG1214884 Chloroform ND 0.0250 5 12/22/2018 01:47 WG1214884 Chloromethane ND 0.0125 5 12/22/2018 01:47 WG1214884 2-Chlorotoluene ND 0.00500 5 12/22/2018 01:47 WG1214884 4-Chlorotoluene ND 0.00500 5 12/22/2018 01:47 WG1214884 1,2-Dibromo-3-Chloropropane ND 0.0250 5 12/22/2018 01:47 WG1214884 1,2-Dibromoethane ND 0.00500 5 12/22/2018 01:47 WG1214884 Dibromomethane ND 0.00500 5 12/22/2018 01:47 WG1214884 1,2-Dichlorobenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 1,3-Dichlorobenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 1,4-Dichlorobenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 Dichlorodifluoromethane ND 0.0250 5 12/22/2018 01:47 WG1214884 1,1-Dichloroethane ND 0.00500 5 12/22/2018 01:47 WG1214884 1,2-Dichloroethane ND 0.00500 5 12/22/2018 01:47 WG1214884 1,1-Dichloroethene ND 0.00500 5 12/22/2018 01:47 WG1214884 cis-1,2-Dichloroethene 1.93 0.100 100 12/27/2018 20:09 WG1216589 trans-1,2-Dichloroethene 0.0126 0.00500 5 12/22/2018 01:47 WG1214884 1,2-Dichloropropane ND 0.00500 5 12/22/2018 01:47 WG1214884 1,1-Dichloropropene ND 0.00500 5 12/22/2018 01:47 WG1214884 1,3-Dichloropropane ND 0.00500 5 12/22/2018 01:47 WG1214884 cis-1,3-Dichloropropene ND 0.00500 5 12/22/2018 01:47 WG1214884 trans-1,3-Dichloropropene ND 0.00500 5 12/22/2018 01:47 WG1214884 2,2-Dichloropropane ND 0.00500 5 12/22/2018 01:47 WG1214884 Di -isopropyl ether ND 0.00500 5 12/22/2018 01:47 WG1214884 Ethylbenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 Hexachloro-1,3-butadiene ND 0.00500 5 12/22/2018 01:47 WG1214884 Isopropylbenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 p-Isopropyltoluene ND 0.00500 5 12/22/2018 01:47 WG1214884 2-Butanone (MEK) ND 0.0500 5 12/22/2018 01:47 WG1214884 Methylene Chloride ND 0.0250 5 12/22/2018 01:47 WG1214884 4-Methyl-2-pentanone (MIBK) ND 0.0500 5 12/22/2018 01:47 WG1214884 Methyl tert-butyl ether ND 0.00500 5 12/22/2018 01:47 WG1214884 Naphthalene ND 0.0250 5 12/22/2018 01:47 WG1214884 n-Propylbenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 Styrene ND 0.00500 5 12/22/2018 01:47 WG1214884 1,1,1,2-Tetrachloroethane ND 0.00500 5 12/22/2018 01:47 WG1214884 1,1,2,2-Tetrachloroethane ND 0.00500 5 12/22/2018 01:47 WG1214884 1,1,2-Trichlorotrifluoroethane ND 0.00500 5 12/22/2018 01:47 WG1214884 Tetrachloroethene 0.0482 0.00500 5 12/22/2018 01:47 WG1214884 Toluene ND 0.00500 5 12/22/2018 01:47 WG1214884 1,2,3-Trichlorobenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 1,2,4-Trichlorobenzene ND 0.00500 5 12/22/2018 01:47 WG1214884 FP1 FTc FSS 4 Cn Fc F ql FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 7 of 22 ONE LAB. NATIONWIDE. 2W-10 SAMPLE RESULTS - 02 Collected date/time: 12/19/18 13:30 L1055119 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier Analyte mg/I 1,1,1-Trich Io roetha ne 1,1,2-Trich I oroetha n e Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Tri methyl ben zen e 1,2,3-Trimethyl benzene 1,3,5-Trimethyl benzene Vinyl chloride Xylenes, Total (S) Toluene-d8 (S) Toluene-d8 (S) Dibromofluoromethane (S) Dibromofluoromethane (S) 4-Bromof/uorobenzene (S) 4-Bromofluorobenzene ND ND 0.0360 ND ND ND ND ND 0.0901 ND 104 102 95.5 99.4 91.4 97.5 RDL mg/I Dilution Analysis date / time 0.00500 5 12/22/2018 01:47 0.00500 5 12/22/2018 01:47 0.00500 5 12/22/2018 01:47 0.0250 5 12/22/2018 01:47 0.0125 5 12/22/2018 01:47 0.00500 5 12/22/2018 01:47 0.00500 5 12/22/2018 01:47 0.00500 5 12/22/2018 01:47 0.00500 5 12/22/2018 01:47 0.0150 5 12/22/2018 01:47 80.0-120 1212212018 01.47 80.0-120 1212712018 20:09 75.0-120 1212212018 01.47 75.0-120 1212712018 20:09 77.0-126 1212212018 01.47 77.0-126 1212712018 20:09 Batch WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1216589 WG1214884 WG1216589 WG1214884 WG1216589 Fp FTc FS Fn N FC] F FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 8 of 22 2 W-11 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE. Collected date/time: 12/19/18 13:50 L1055119 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch u Analyte mg/I mg/I date /time Acetone ND 0.0500 1 12/22/2018 02:07 WG1214884 FTc Acrolein ND 0.0500 1 12/22/2018 02:07 WG1214884 Acrylonitrile ND 0.0100 1 12/22/2018 02:07 WG1214884 F Benzene ND 0.00100 1 12/22/2018 02:07 WG1214884 Bromobenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 Bromodichloromethane ND 0.00100 1 12/22/2018 02:07 WG1214884 rCn Bromoform ND 0.00100 1 12/22/2018 02:07 WG1214884 Bromomethane ND 0.00500 1 12/22/2018 02:07 WG1214884 n-Butylbenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 sec -Butyl benzene ND 0.00100 1 12/22/2018 02:07 WG1214884 ter[-Butylbenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 Fc Carbon tetrachloride ND 0.00100 1 12/22/2018 02:07 WG1214884 Chlorobenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 Fq Chlorodibromomethane ND 0.00100 1 12/22/2018 02:07 WG1214884 Chloroethane ND 0.00500 1 12/22/2018 02:07 WG1214884 Chloroform ND 0.00500 1 12/22/2018 02:07 WG1214884 FAI Chloromethane ND 0.00250 1 12/22/2018 02:07 WG1214884 2-Chlorotoluene ND 0.00100 1 12/22/2018 02:07 WG1214884 F 4-Chlorotoluene ND 0.00100 1 12/22/2018 02:07 WG1214884 1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/22/2018 02:07 WG1214884 1,2-Dibromoethane ND 0.00100 1 12/22/2018 02:07 WG1214884 Dibromomethane ND 0.00100 1 12/22/2018 02:07 WG1214884 1,2-Dichlorobenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 1,3-Dichlorobenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 1,4-Dichlorobenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 Dichlorodifluoromethane ND 0.00500 1 12/22/2018 02:07 WG1214884 1,1-Dichloroethane ND 0.00100 1 12/22/2018 02:07 WG1214884 1,2-Dichloroethane ND 0.00100 1 12/22/2018 02:07 WG1214884 1,1-Dichloroethene ND 0.00100 1 12/22/2018 02:07 WG1214884 cis-1,2-Dichloroethene 0.314 0.00500 5 12/23/201818:53 WG1215213 trans-1,2-Dichloroethene 0.00800 0.00100 1 12/22/2018 02:07 WG1214884 1,2-Dichloropropane ND 0.00100 1 12/22/2018 02:07 WG1214884 1,1-Dichloropropene ND 0.00100 1 12/22/2018 02:07 WG1214884 1,3-Dichloropropane ND 0.00100 1 12/22/2018 02:07 WG1214884 cis-1,3-Dichloropropene ND 0.00100 1 12/22/2018 02:07 WG1214884 trans-1,3-Dichloropropene ND 0.00100 1 12/22/2018 02:07 WG1214884 2,2-Dichloropropane ND 0.00100 1 12/22/2018 02:07 WG1214884 Di -isopropyl ether ND 0.00100 1 12/22/2018 02:07 WG1214884 Ethylbenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 Hexachloro-1,3-butadiene ND 0.00100 1 12/22/2018 02:07 WG1214884 Isopropylbenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 p-Isopropyltoluene ND 0.00100 1 12/22/2018 02:07 WG1214884 2-Butanone (MEK) ND 0.0100 1 12/22/2018 02:07 WG1214884 Methylene Chloride ND 0.00500 1 12/22/2018 02:07 WG1214884 4-Methyl-2-pentanone (MIBK) ND 0.0100 1 12/22/2018 02:07 WG1214884 Methyl tert-butyl ether ND 0.00100 1 12/22/2018 02:07 WG1214884 Naphthalene ND 0.00500 1 12/22/2018 02:07 WG1214884 n-Propylbenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 Styrene ND 0.00100 1 12/22/2018 02:07 WG1214884 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/22/2018 02:07 WG1214884 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/22/2018 02:07 WG1214884 1,1,2-Trichlorotrifluoroethane ND 0.00100 1 12/22/2018 02:07 WG1214884 Tetrachloroethene 0.0178 0.00100 1 12/22/2018 02:07 WG1214884 Toluene ND 0.00100 1 12/22/2018 02:07 WG1214884 1,2,3-Trichlorobenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 1,2,4-Trichlorobenzene ND 0.00100 1 12/22/2018 02:07 WG1214884 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 9 of 22 ONE LAB. NATIONWIDE. 2W-11 SAMPLE RESULTS - 03 Collected date/time: 12/19/18 13:50 L1055119 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Analyte mg/I mg/I 1,1,1-Trichloroethane ND 0.00100 1,1,2-Trichloroethane ND 0.00100 Trichloroethene 0.0121 0.00100 Trichlorofluoromethane ND 0.00500 1,2,3-Trichloropropane ND 0.00250 1,2,4-Trimethyl ben zene ND 0.00100 1,2,3-Trimethyl benzene ND 0.00100 1,3,5-Trimethyl benzene ND 0.00100 Vinyl chloride 0.0982 0.00100 Xylenes, Total ND 0.00300 (S) Toluene-d8 104 80.0-120 (S) Toluene-d8 99.7 80.0-120 (S) Dibromofluoromethane 97.5 75.0-120 (S) Dibromofluoromethane 102 75.0-120 (S) 4-Bromof/uorobenzene 93.8 77.0-126 (S) 4-Bromofluorobenzene 107 77.0-126 Dilution Analysis date / time 12/22/2018 02:07 12/22/2018 02:07 12/22/2018 02:07 12/22/2018 02:07 12/22/2018 02:07 12/22/2018 02:07 12/22/2018 02:07 12/22/2018 02:07 12/22/2018 02:07 12/22/2018 02:07 1212212018 02:07 121231201818.53 1212212018 02:07 121231201818.53 1212212018 02:07 121231201818.53 Batch WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1214884 WG1215213 WG1214884 WG1215213 WG1214884 WG1215213 Fp FTc FS Fn FC] F ql FAI FSC ACCOUNT: PROJECT: SDG: AECOM - Raleigh, NC 60566538 L1055119 DATE/TIME: PAGE: 12/31/1815:20 10 of 22 MW-2 SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE. Collected date/time: 12/19/18 14:20 L1055119 Volatile Organic Compounds (GC/MS) by Method 8260B Result Qualifier RDL Dilution Analysis Batch u Analyte mg/I mg/I date /time Acetone ND 0.0500 1 12/22/2018 02:26 WG1214884 FTc Acrolein ND 0.0500 1 12/22/2018 02:26 WG1214884 Acrylonitrile ND 0.0100 1 12/22/2018 02:26 WG1214884 F Benzene ND 0.00100 1 12/22/2018 02:26 WG1214884 Bromobenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 Bromodichloromethane ND 0.00100 1 12/22/2018 02:26 WG1214884 rCn Bromoform ND 0.00100 1 12/22/2018 02:26 WG1214884 Bromomethane ND 0.00500 1 12/22/2018 02:26 WG1214884 n-Butylbenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 sec -Butyl benzene ND 0.00100 1 12/22/2018 02:26 WG1214884 ter[-Butylbenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 Fc Carbon tetrachloride ND 0.00100 1 12/22/2018 02:26 WG1214884 Chlorobenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 Fq Chlorodibromomethane ND 0.00100 1 12/22/2018 02:26 WG1214884 Chloroethane ND 0.00500 1 12/22/2018 02:26 WG1214884 Chloroform ND 0.00500 1 12/22/2018 02:26 WG1214884 FAI Chloromethane ND 0.00250 1 12/22/2018 02:26 WG1214884 2-Chlorotoluene ND 0.00100 1 12/22/2018 02:26 WG1214884 F 4-Chlorotoluene ND 0.00100 1 12/22/2018 02:26 WG1214884 1,2-Dibromo-3-Chloropropane ND 0.00500 1 12/22/2018 02:26 WG1214884 1,2-Dibromoethane ND 0.00100 1 12/22/2018 02:26 WG1214884 Dibromomethane ND 0.00100 1 12/22/2018 02:26 WG1214884 1,2-Dichlorobenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 1,3-Dichlorobenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 1,4-Dichlorobenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 Dichlorodifluoromethane ND 0.00500 1 12/22/2018 02:26 WG1214884 1,1-Dichloroethane ND 0.00100 1 12/22/2018 02:26 WG1214884 1,2-Dichloroethane ND 0.00100 1 12/22/2018 02:26 WG1214884 1,1-Dichloroethene 0.0228 0.00100 1 12/22/2018 02:26 WG1214884 cis-1,2-Dichloroethene 0.736 0.0100 10 12/23/201819:12 WG1215213 trans-1,2-Dichloroethene 0.0478 0.00100 1 12/22/2018 02:26 WG1214884 1,2-Dichloropropane ND 0.00100 1 12/22/2018 02:26 WG1214884 1,1-Dichloropropene ND 0.00100 1 12/22/2018 02:26 WG1214884 1,3-Dichloropropane ND 0.00100 1 12/22/2018 02:26 WG1214884 cis-1,3-Dichloropropene ND 0.00100 1 12/22/2018 02:26 WG1214884 trans-1,3-Dichloropropene ND 0.00100 1 12/22/2018 02:26 WG1214884 2,2-Dichloropropane ND 0.00100 1 12/22/2018 02:26 WG1214884 Di -isopropyl ether ND 0.00100 1 12/22/2018 02:26 WG1214884 Ethylbenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 Hexachloro-1,3-butadiene ND 0.00100 1 12/22/2018 02:26 WG1214884 Isopropylbenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 p-Isopropyltoluene ND 0.00100 1 12/22/2018 02:26 WG1214884 2-Butanone (MEK) ND 0.0100 1 12/22/2018 02:26 WG1214884 Methylene Chloride ND 0.00500 1 12/22/2018 02:26 WG1214884 4-Methyl-2-pentanone (MIBK) ND 0.0100 1 12/22/2018 02:26 WG1214884 Methyl tert-butyl ether ND 0.00100 1 12/22/2018 02:26 WG1214884 Naphthalene ND 0.00500 1 12/22/2018 02:26 WG1214884 n-Propylbenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 Styrene ND 0.00100 1 12/22/2018 02:26 WG1214884 1,1,1,2-Tetrachloroethane ND 0.00100 1 12/22/2018 02:26 WG1214884 1,1,2,2-Tetrachloroethane ND 0.00100 1 12/22/2018 02:26 WG1214884 1,1,2-Trichlorotrifluoroethane 0.00211 0.00100 1 12/22/2018 02:26 WG1214884 Tetrachloroethene 14.2 0.200 200 12/27/2018 20:28 WG1216589 Toluene ND 0.00100 1 12/22/2018 02:26 WG1214884 1,2,3-Trichlorobenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 1,2,4-Trichlorobenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 11 of 22 MW-2 SAMPLE Collected date/time: 12/19/18 14:20 Volatile Organic Compounds (GC/MS) by Method 8260B RESULTS - 04 L1055119 ONE LAB. NATIONWIDE. f Result Qualifier RDL Dilution Analysis Batch Analyte mg/I mg/I date / time l 1,1,1-Trichloroethane ND 0.00100 1 12/22/2018 02:26 WG1214884 f 1,1,2-Trichloroethane ND 0.00100 1 12/22/2018 02:26 WG1214884 Il Trichloroethene 1.69 0.0100 10 12/23/201819:12 WG1215213 Trichlorofluoromethane ND 0.00500 1 12/22/2018 02:26 WG1214884 1,2,3-Trichloropropane ND 0.00250 1 12/22/2018 02:26 WG1214884 1,2,4-Trimethylbenzene ND 0.00100 1 12/22/2018 02:26 WG1214884 f 1,2,3-Trimethyl benzene ND 0.00100 1 12/22/2018 02:26 WG1214884 Il 1,3,5-Trimethyl benzene ND 0.00100 1 12/22/2018 02:26 WG1214884 Vinyl chloride 0.103 0.00100 1 12/22/2018 02:26 WG1214884 I Xylenes, Total ND 0.00300 1 12/22/2018 02:26 WG1214884 (S) Toluene-d8 112 80.0-120 1212212018 0216 WG1214884 f (S) Toluene-d8 96.4 80.0-120 121231201819.12 WG1215213 Il (S)Toluene-d8 107 80.0-120 121271201820:28 WG1216589 (S) Dibromofluoromethane 85.5 75.0-120 1212212018 02:26 WG1214884 (S) Dibromofluoromethane 98.1 75.0-120 121231201819.12 WG1215213 (S)Dibromofluoromethane 101 75.0-120 121271201820:28 WG1216589 f (S) 4-Bromofluorobenzene 90.9 77.0-126 1212212018 02:26 WG1214884 Il (S) 4-Bromofluorobenzene 107 77.0-126 121231201819.12 WG1215213 (S)4-Bromofluorobenzene 94.6 77.0-126 121271201820:28 WG1216589 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 12 of 22 WG1214884 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260B L1055119-01,02,03,04 Method Blank (MB) (MB) R3370682-3 12/22/18 00:27 MB Result MB Qualifier Analvte mq/I Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec -Butyl benzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,1-Dichloropropene 1,3-Dichloropropane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 2,2-Dichloropropane Di -isopropyl ether Ethylbenzene Hexachloro-1,3-butadiene U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U MB MDL mg/I 0.0100 0.00887 0.00187 0.000331 0.000352 0.000380 0.000469 0.000866 0.000361 0.000365 0.000399 0.000379 0.000348 0.000327 0.000453 0.000324 0.000276 0.000375 0.000351 0.00133 0.000381 0.000346 0.000349 0.000220 0.000274 0.000551 0.000259 0.000361 0.000398 0.000260 0.000396 0.000306 0.000352 0.000366 0.000418 0.000419 0.000321 0.000320 0.000384 0.000256 MB RDL mg/I 0.0500 0.0500 0.0100 0.00100 0.00100 0.00100 0.00100 0.00500 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00500 0.00500 0.00250 0.00100 0.00100 0.00500 0.00100 0.00100 0.00100 0.00100 0.00100 0.00500 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 0.00100 FP1 FTC FSS [Cn] FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/18 15:20 13 of 22 WG1214884 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260B L1055119-01,02,03,04 Method Blank (MB) (MB) R3370682-3 12/22/18 00:27 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Isopropylbenzene U 0.000326 0.00100 p-Isopropyltoluene U 0.000350 0.00100 2-Butanone (MEK) U 0.00393 0.0100 Methylene Chloride U 0.00100 0.00500 4-Methyl-2-pentanone (MIBK) U 0.00214 0.0100 Methyl tert-butyl ether U 0.000367 0.00100 Naphthalene U 0.00100 0.00500 n-Propylbenzene U 0.000349 0.00100 Styrene U 0.000307 0.00100 1,1,1,2-Tetrachloroethane U 0.000385 0.00100 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0.000412 0.00100 1,1,2-Trichlorotrifluoroethane U 0.000303 0.00100 1,2,3-Trichlorobenzene U 0.000230 0.00100 1,2,4-Trichlorobenzene U 0.000355 0.00100 1,1,1-Trichloroethane U 0.000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0.00100 Trichlorofluoromethane U 0.00120 0.00500 1,2,3-Trichloropropane U 0.000807 0.00250 1,2,3-Trimethyl benzene U 0.000321 0.00100 1,2,4-Trimethylbenzene U 0.000373 0.00100 1,3,5-Trimethyl benzene U 0.000387 0.00100 Vinyl chloride U 0.000259 0.00100 Xylenes, Total U 0.00106 0.00300 (S) Toluene-d8 105 80.0-120 (S) Dibromofluoromethane 101 75.0-120 (S) 4-Bromof/uorobenzene 90.7 77.0-126 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3370682-1 12/21/18 23:07 • (LCSD) R3370682-2 12/21/18 23:27 Spike Amount LCS Result LCSD Result Analyte mg/I mg/I mg/I Acetone 0.125 0.107 0.102 Acrolein 0.125 0.0946 0.103 Acrylonitrile 0.125 0.113 0.116 Benzene 0.0250 0.0226 0.0233 ACCOUNT: AECOM - Raleigh, NC LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 86.0 81.6 19.0-160 5.27 27 75.6 82.7 10.0-160 8.87 26 90.7 92.4 55.0-149 1.89 20 90.4 93.4 70.0-123 3.29 20 PROJECT: SDG: DATE/TIME: PAGE: 60566538 L1055119 12/31/18 15:20 14 of 22 FP1 FTc FSS 4 Cn FSr �GI FAI [Sc WG1214884 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260B L1055119-01,02,03,04 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3370682-1 12/21/18 23:07 • (LCSD) R3370682-2 12/21/18 23:27 Spike Amount LCS Result LCSD Result Analyte mg/I mg/I mg/I Bromobenzene 0.0250 0.0218 0.0225 Bromodichloromethane 0.0250 0.0211 0.0216 Bromoform 0.0250 0.0222 0.0231 Bromomethane 0.0250 0.0261 0.0270 n-Butylbenzene 0.0250 0.0233 0.0229 sec -Butyl benzene 0.0250 0.0237 0.0240 tert-Butylbenzene 0.0250 0.0234 0.0240 Carbon tetrachloride 0.0250 0.0232 0.0234 Chlorobenzene 0.0250 0.0253 0.0267 Chlorodibromomethane 0.0250 0.0239 0.0250 Chloroethane 0.0250 0.0249 0.0264 Chloroform 0.0250 0.0230 0.0232 Chloromethane 0.0250 0.0250 0.0259 2-Chlorotoluene 0.0250 0.0243 0.0248 4-Chlorotoluene 0.0250 0.0241 0.0253 1,2-Dibromo-3-Chloropropane 0.0250 0.0201 0.0206 1,2-Dibromoethane 0.0250 0.0239 0.0244 Dibromomethane 0.0250 0.0233 0.0235 1,2-Dichlorobenzene 0.0250 0.0228 0.0234 1,3-Dichlorobenzene 0.0250 0.0235 0.0248 1,4-Dichlorobenzene 0.0250 0.0243 0.0249 Dichlorodifluoromethane 0.0250 0.0269 0.0284 1,1-Dichloroethane 0.0250 0.0230 0.0233 1,2-Dichloroethane 0.0250 0.0222 0.0223 1,1-Dichloroethene 0.0250 0.0243 0.0239 cis-1,2-Dichloroethene 0.0250 0.0231 0.0235 trans-1,2-Dichloroethene 0.0250 0.0241 0.0244 1,2-Dichloropropane 0.0250 0.0243 0.0248 1,1-Dichloropropene 0.0250 0.0221 0.0228 1,3-Dichloropropane 0.0250 0.0242 0.0258 cis-1,3-Dichloropropene 0.0250 0.0233 0.0241 trans-1,3-Dichloropropene 0.0250 0.0240 0.0257 2,2-Dichloropropane 0.0250 0.0224 0.0225 Di -isopropyl ether 0.0250 0.0221 0.0227 Ethylbenzene 0.0250 0.0252 0.0263 Hexachloro-1,3-butadiene 0.0250 0.0186 0.0184 Isopropylbenzene 0.0250 0.0229 0.0231 p-Isopropyltoluene 0.0250 0.0233 0.0237 2-Butanone (MEK) 0.125 0.104 0.107 Methylene Chloride 0.0250 0.0248 0.0246 ACCOUNT: AECOM - Raleigh, NC LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 87.1 89.9 73.0-121 3.14 20 84.3 86.4 75.0-120 2.40 20 88.7 92.4 68.0-132 4.16 20 105 108 10.0-160 3.39 25 93.1 91.6 73.0-125 1.63 20 94.8 96.0 75.0-125 1.28 20 93.6 96.0 76.0-124 2.55 20 92.7 93.7 68.0-126 1.05 20 101 107 80.0-121 5.34 20 95.7 99.8 77.0-125 4.24 20 99.5 106 47.0-150 5.99 20 92.1 92.6 73.0-120 0.517 20 99.9 104 41.0-142 3.63 20 97.1 99.1 76.0-123 2.09 20 96.4 101 75.0-122 4.74 20 80.5 82.3 58.0-134 2.24 20 95.5 97.6 80.0-122 2.12 20 93.2 94.0 80.0-120 0.822 20 91.2 93.4 79.0-121 2.46 20 94.1 99.1 79.0-120 5.20 20 97.1 99.6 79.0-120 2.55 20 108 114 51.0-149 5.38 20 92.1 93.1 70.0-126 1.08 20 88.9 89.1 70.0-128 0.185 20 97.3 95.7 71.0-124 1.70 20 92.5 94.1 73.0-120 1.64 20 96.5 97.4 73.0-120 0.928 20 97.2 99.4 77.0-125 2.23 20 88.4 91.3 74.0-126 3.31 20 96.7 103 80.0-120 6.55 20 93.4 96.5 80.0-123 3.35 20 96.1 103 78.0-124 6.77 20 89.7 89.9 58.0-130 0.236 20 88.4 90.7 58.0-138 2.58 20 101 105 79.0-123 4.38 20 74.6 73.7 54.0-138 1.10 20 91.5 92.4 76.0-127 0.989 20 93.1 94.8 76.0-125 1.80 20 83.0 85.4 44.0-160 2.79 20 99.1 98.4 67.0-120 0.637 20 PROJECT: SDG: DATE/TIME: PAGE: 60566538 L1055119 12/31/18 15:20 15 of 22 FP1 FTC FSS [Cn] FSr �GI FAI FSC WG1214884 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 8260B L1055119-01,02,03,04 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1(LCS) R3370682-1 12/21/18 23:07 • (LCSD) R3370682-2 12/21/18 23:27 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % FTC 4-Methyl-2-pentanone (MIBK) 0.125 0.117 0.124 93.7 99.0 68.0-142 5.50 20 Methyl tert-butyl ether 0.0250 0.0239 0.0240 95.5 96.2 68.0-125 0.726 20 FSS Naphthalene 0.0250 0.0180 0.0179 71.9 71.4 54.0-135 0.629 20 n-Propylbenzene 0.0250 0.0220 0.0229 87.9 91.7 77.0-124 4.21 20 Styrene 0.0250 0.0225 0.0233 90.2 93.1 73.0-130 3.15 20 [Cn] 1,1,1,2-Tetrachloroethane 0.0250 0.0236 0.0247 94.4 98.6 75.0-125 4.44 20 1,1,2,2-Tetrachloroethane 0.0250 0.0209 0.0218 83.5 87.2 65.0-130 4.30 20 FSr Tetrachloroethene 0.0250 0.0252 0.0258 101 103 72.0-132 2.23 20 Toluene 0.0250 0.0249 0.0256 99.5 102 79.0-120 2.72 20 1,1,2-Trichlorotrifluoroethane 0.0250 0.0270 0.0265 108 106 69.0-132 1.63 20 1,2,3-Trichlorobenzene 0.0250 0.0187 0.0181 74.8 72.4 50.0-138 3.24 20 1,2,4-Trichlorobenzene 0.0250 0.0190 0.0190 75.9 75.8 57.0-137 0.0644 20 7G1 1,1,1-Trichloroethane 0.0250 0.0237 0.0243 94.9 97.2 73.0-124 2.42 20 1,1,2-Trichloroethane 0.0250 0.0260 0.0273 104 109 80.0-120 4.73 20 Trichloroethene 0.0250 0.0254 0.0262 101 105 78.0-124 3.08 20 FAI Trichlorofluoromethane 0.0250 0.0270 0.0275 108 110 59.0-147 2.09 20 1,2,3-Trichloropropane 0.0250 0.0231 0.0238 92.4 95.3 73.0-130 3.11 20 FSC 1,2,3-Trimethylbenzene 0.0250 0.0240 0.0242 95.8 96.8 77.0-120 1.04 20 1,2,4-Trimethylbenzene 0.0250 0.0233 0.0233 93.1 93.4 76.0-121 0.234 20 1,3,5-Trimethyl benzene 0.0250 0.0233 0.0241 93.4 96.3 76.0-122 3.05 20 Vinyl chloride 0.0250 0.0257 0.0270 103 108 67.0-131 4.80 20 Xylenes, Total 0.0750 0.0750 0.0781 100 104 79.0-123 4.05 20 (S) Toluene-d8 103 105 80.0-120 (S) DibromoFluoromethane 97.9 95.9 75.0-120 (S) 4-Bromof/uorobenzene 87.5 89.5 77.0-126 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/18 15:20 16 of 22 WG1215213 Volatile Organic Compounds (GC/MS) by Method 8260B Method Blank (MB) QUALITY CONTROL SUMMARY 1-1055119-01,03,04 ONE LAB. NATIONWIDE. (MB) R3371686-3 12/23/1816:27 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I cis-1,2-Dichloroethene U 0.000260 0.00100 Tetrachloroethene U 0.000372 0.00100 Trichloroethene U 0.000398 0.00100 (S) Toluene-d8 101 80.0-120 (S) Dibromofluoromethane 99.6 75.0-120 (S) 4-Bromof/uorobenzene 109 77.0-126 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3371686-1 12/23/1815:28 • (LCSD) R3371686-2 12/23/1815:48 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I % % % % % cis-1,2-Dichloroethene 0.0250 0.0252 0.0244 101 97.4 73.0-120 3.53 20 Tetrachloroethene 0.0250 0.0192 0.0196 76.6 78.5 72.0-132 2.38 20 Trichloroethene 0.0250 0.0221 0.0222 88.6 88.8 78.0-124 0.246 20 (S) Toluene-d8 99.5 99.4 80.0-120 (S) Dibromofluoromethane 100 101 75.0-120 (S) 4-Bromofluorobenzene 112 113 77.0-126 FP1 FTc FSS 4 Cn FSr �GI FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/18 15:20 17 of 22 WG1216589 Volatile Organic Compounds (GC/MS) by Method 8260B Method Blank (MB) (MB) R3371912-3 12/27/18 19:24 MB Result Analyte mg/I cis-1,2-Dichloroethene U Tetrachloroethene U (S) Toluene-d8 106 (S) Dibromofluoromethane 99.0 (S) 4-Bromofluorobenzene 95.0 QUALITY CONTROL SUMMARY 1-1055119-02,04 MB Qualifier MB MDL MB RDL mg/I mg/I 0.000260 0.00100 0.000372 0.00100 80.0-120 75.0-120 77.0-126 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3371912-1 12/27/1818:24 • (LCSD) R3371912-2 12/27/1818:44 Spike Amount LCS Result LCSD Result LCS Rec. Analyte mg/1 mg/I mg/I % cis-1,2-Dichloroethene 0.0250 0.0239 0.0242 95.5 Tetrachloroethene 0.0250 0.0246 0.0240 98.6 (S) Toluene-d8 (S) Dibromofluoromethane (S) 4-Bromofluorobenzene 105 96.7 91.8 LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD 96.7 73.0-120 1.28 96.1 72.0-132 2.59 101 80.0-120 98.2 75.0-120 94.3 77.0-126 RPD Limits 20 20 ONE LAB. NATIONWIDE. FP1 FTc FSS 4 Cn FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/18 15:20 18 of 22 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. FP1 FTC FSS [Cn] FSr 6 QC FAI FSC Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 19 of 22 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 5 Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T 104704245-17-14 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA ME MT NO OR MN T ID t WI NY SD WY MI NV t NE IA OH PA T f IL Ills WV vA UT T CA�� T KS MO KY N NM O� AR SC T MS AL`7GA T TX * LA T AK q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: AECOM - Raleigh, NC 60566538 L1055119 12/31/1815:20 20 of 22 :OMpany+ N@rne/Address: AECOM 1600 Perimeter Park Drive STE 400 Morfiisville, NC 27550 Repart LO' Stephanie Hemple Prole[t American Dry Cleaners DC680002 Dextiption Phone: 919-461-1100 client Prolea Fax; 60566536 Collected by (Iprintj: Site/Facility I D p Billing Information_ I rnall tephanie.hernple aecom.com Cotiected: Lab Project4 Collected by lslg atu Rush? (Lab MIJ5t IJIe Notified same day-._ ........... .......... 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Time: R ed for lah by: j 'gnat rare) bate: Time; pH Checked: NCF; ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 December 27, 2018 Nick Shore AECOM-Morrisville NC 1600 Perimeter Park Drive Morrisville, NC 27560 Project Location: DC680002 - American Cleaners Client Job Number: Project Number: 60566538 Laboratory Work Order Number: 18L1167 Enclosed are results of analyses for samples received by the laboratory on December 21, 2018. If you have any questions concerning this report, please feel free to contact me. Sincerely, I,&, �. A�� Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 AECOM-Morrisville NC REPORT DATE: 12/27/2018 1600 Perimeter Park Drive Morrisville, NC 27560 PURCHASE ORDER NUMBER: 60566538 ATTN: Nick Shore PROJECT NUMBER: 60566538 ANALYTICAL SUMMARY WORK ORDER NUMBER: 18L1167 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: DC680002 - American Cleaners FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB IA-2 (Radiello 106TB) 18L1167-01 Indoor air IA-3 (Radiello 107TB) 18L1167-02 Indoor air RAD 130 RAD 130 Page 2 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method Radiello RAD-130 - The sampling rates for trichloroethene and tetrachloroethene are as follows: trichloroethene = 69 mL/min, tetrachloroethene = 59 mL/min. The theoretical sampling rates for vinyl chloride, 1, 1 -dichloroethene, trans-1,2-dichloroethene, and cis-1,2-dichloroethene are estimated using Graham's Law and are as follows: vinyl chloride = 103 mL/min, 1, 1 -dichloroethene = 83 mL/min, trans-1,2-dichloroethene = 83 mUmin, cis-1,2-dichloroethene = 83 mL/min. The results for these 4 compounds are estimated values. RAD 130 Qualifications Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. Analyte & Samples(s) Qualified: Vinyl Chloride B219989-BSDI The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. 4Z�14__ VWWLO_� Lisa A. Worthington Project Manager Page 3 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: DC680002 - American Cleaners Sample Description/Location: Work Order: 18L1167 Date Received: 12/21/2018 Sub Description/Location: Field Sample #: IA-2 (Radiello 106TB) Sample ID: 18L1167-01 Sample Matrix: Indoor air Flow Controller ID: Sampled: 12/21/2018 12:20 Sample Type: Air Volume L: 10080 RAD 130 Total µg ug/m3 Date/Time Analyte Results RL MDL Flag/Qua[ Results ILL MDL Dilution Analyzed Analyst Vinyl Chloride ND 0.16 ND 0.15 1 12/26/18 16:35 IMR 1,1-Dichloroethene ND 1.0 ND 1.2 1 12/26/18 16:35 IMR trans-1,2-Dichloroethene ND 1.0 ND 1.2 1 12/26/18 16:35 IMR cis-1,2-Dichloroethene ND 0.20 ND 0.24 1 12/26/18 16:35 IMR Tichloroethene 1.3 0.20 1.9 0.29 1 12/26/18 16:35 IMR Tetrachloroethene 2.8 0.20 4.6 0.34 1 12/26/18 16:35 IMR Page 4 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Project Location: DC680002 - American Cleaners Date Received: 12/21/2018 Field Sample #: IA-3 (Radiello 107TB) Sample ID: 18L1167-02 Sample Matrix: Indoor air Sampled: 12/21 /2018 12:15 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Flow Controller ID: Sample Type: Air Volume L: 10080 Work Order: 18L1167 RAD 130 Total µg ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results ILL MDL Dilution Analyzed Analyst Vinyl Chloride ND 0.16 ND 0.15 1 12/26/18 16:58 IMR 1,1-Dichloroethene ND 1.0 ND 1.2 1 12/26/18 16:58 IMR trans-1,2-Dichloroethene ND 1.0 ND 1.2 1 12/26/18 16:58 IMR cis-1,2-Dichloroethene ND 0.20 ND 0.24 1 12/26/18 16:58 IMR Tichloroethene 1.5 0.20 2.1 0.29 1 12/26/18 16:58 IMR Tetrachloroethene 3.5 0.20 5.9 0.34 1 12/26/18 16:58 IMR Page 5 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: Radiello-RAD 130 Lab Number [Field ID] Batch Initial [Cartridge Final [mL] Date 18L1167-01 [IA-2 (Radiello 106TB)] B219989 1.00 2.00 12/26/18 18L1167-02 [IA-3 (Radiello 107TB)] B219989 1.00 2.00 12/26/18 Page 6 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Miscellaneous Air Analyses - Quality Control Total µg ug/m3 Spike Level Source %REC RPD .nalyte Results RL Results RL Total µg Result %REC Limits RPD Limit Flag/Qua Batch B219989 - Radiello Blank (B219989-BLK1) Prepared & Analyzed: 12/26/18 Vinyl Chloride ND 0.16 1,1-Dichloroethene ND 1.0 trans-1,2-Dichloroethene ND 1.0 cis-1,2-Dichloroethene ND 0.20 Trichloroethene ND 0.20 Tetrachloroethene ND 0.20 LCS (B219989-BS1) Prepared & Analyzed: 12/26/18 Vinyl Chloride 4.14 0.16 0.41 10.0 41.4 40-140 111-Dichloroethene 6.85 1.0 10.0 68.5 40-140 trans-1,2-Dichloroethene 6.94 1.0 10.0 69.4 40-140 cis-1,2-Dichloroethene 8.00 0.20 10.0 80.0 40-140 Trichloroethene 8.28 0.20 10.0 82.8 40-140 Tetrachloroethene 8.18 0.20 10.0 81.8 40-140 LCS Dup (B219989-BSD1) Prepared & Analyzed: 12/26/18 Vinyl Chloride 3.75 0.16 0.41 10.0 37.5 * 40-140 9.89 30 L-07 1,1-Dichloroethene 6.01 1.0 10.0 60.1 40-140 13.1 30 trans-1,2-Dichloroethene 6.35 1.0 10.0 63.5 40-140 8.87 30 cis-1,2-Dichloroethene 7.43 0.20 10.0 74.3 40-140 7.34 30 Trichloroethene 7.73 0.20 10.0 77.3 40-140 6.92 30 Tetrachloroethene 7.95 0.20 10.0 79.5 40-140 2.75 30 Page 7 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. ANALYST PEB Paula E. Blakeborough KKM Kerry K. McGee IMR Irina Raducan CJM Christian J. Merchant Page 8 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 INTERNAL STANDARD AREA AND RT SUMMARY RAD 130 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Difi RT Diff Limit Q LCS (B219989-BS1 Lab File ID: B1226002.D Analyzed: 12/26/18 15:12 2-Fluorotoluene 7943386 13.478 8683837 13.479 91 50-200 -0.0010 +/-0.50 LCS Dup (B219989-BSDI) Lab File ID: B1226003.D Analyzed: 12/26/18 15:35 2-Fluorotoluene 8936297 13.473 8683837 13.479 103 50-200 -0.0060 +/-0.50 Blank (B219989-BLK1) Lab File ID: B1226004.D Analyzed: 12/26/18 16:11 2-Fluorotoluene 7671156 13.475 8683837 13.479 88 50-200 -0.0040 +/-0.50 IA-2 (Radiello 106TB) (181,1167-01 ) Lab File ID: B1226005.D Analyzed: 12/26/18 16:35 2-Fluorotoluene 7746646 13.471 8683837 13.479 89 50 - 200 -0.0080 +1-0.50 IA-3 (Radiello 107TB) (18L1167-02 ) Lab File ID: B1226006.D Analyzed: 12/26/18 16:58 2-Fluorotoluene 8643550 13.466 8683837 13.479 100 50-200 -0.0130 +/-0.50 Page 9 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CONTINUING CALIBRATION CHECK COMPOUND TYPE RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 10 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications No certified Analyses included in this Report The CON -TEST Environmental Laboratory operates under the following certifications and accreditation Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2019 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LA000112 12/30/2019 NC North Carolina Div. of Water Quality 652 12/31/2019 NJ New Jersey DEP MA007 NELAP 06/30/2019 FL Florida Department of Health E871027 NELAP 06/30/2019 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2019 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2019 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2019 NC-DW North Carolina Department of Health 25703 07/31/2019 Page 11 of 14 aM 3 c a s t <, o' Q O E l7OmW Y Z = L V _j O :Ei^CO R z D Z. G Q U X It a 0 ❑❑ li U. � IIt CO 11 11 o°'i v am in m iow; o 1A V)ACOO CO aLab Receipt Pressure ro � Final Pressure 0 0- 5 (U A Initial Pressure JAJ 1 U'a/i d _ C+ CL _ a E o ,A 4W v a r, w + Ci m > C a m a V'yA'� i^ C , CC 3 O EOE Cl ? M vx x da Z Z •atl+ CO 6.0 L N ° 3 a E a d A ILE c c _ C� •yO^ V Z E❑❑ 0 3 ? w c . E H ❑ ❑ ❑ ❑ 0 yO.. 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In Box y Ambient Melted Ice Were samples within Temperature By Gun # Actual Temp - Compliance? 2-6°C By Blank # ��_ Actual Temp - Was Custody Seal Intact? Were Samples Tampered with? Was COC Relinquished ? �_ Does Chain Agree With Samples? T Are there any loose caps/valves on any samples? F Is COC in ink/ Legible?-T— Did COC Include all Client Analysis I Sampler Name Pertinent Information? Project i ID`s Collection Dates/Times T_ Are Sample Labels filled out and legible? _F Are there Rushes? E. Who was notified? Samples are received within holding time? T Proper Media Used? _r Individually Certified Cans? Are there Trip Blanks? 1= Is there enough Volume? AM Summa Cans Nut/Ferrule IC Train Tedlar Batts Tubing TO-17 Tubes T-Connector Radiello Syringe Pufs/TO-11 s Tedlar Comments: ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 December 27, 2018 Nick Shore AECOM-Morrisville NC 1600 Perimeter Park Drive Morrisville, NC 27560 Project Location: Chapel Hill, NC Client Job Number: Project Number: DC680002 Laboratory Work Order Number: 18L1068 Enclosed are results of analyses for samples received by the laboratory on December 20, 2018. If you have any questions concerning this report, please feel free to contact me. Sincerely, I,&, �. A�� Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 13 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 AECOM-Morrisville NC REPORT DATE: 12/27/2018 1600 Perimeter Park Drive Morrisville, NC 27560 PURCHASE ORDER NUMBER: 60566538 ATTN: Nick Shore PROJECT NUMBER: DC680002 ANALYTICAL SUMMARY WORK ORDER NUMBER: 18L1068 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Chapel Hill, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB SG-5 18L1068-01 Soil Gas EPA TO-15 Page 2 of 13 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. EPA TO-15 Qualifications: Elevated reporting limit due to high concentration of target compounds. Analyte & Samples(s) Qualified: 18L1068-01[SG-5] The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Project Manager Page 3 of 13 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Chapel Hill, NC Sample Description/Location: Date Received: 12/20/2018 Sub Description/Location: Field Sample #: SG-5 Canister ID: 1204 Sample ID: 181,1068-01 Canister Size: 6 liter Sample Matrix: Soil Gas Flow Controller ID: 4197 Sampled: 12/19/2018 15:13 Sample Type: 30 min Work Order: 181,1068 Initial Vacuum(in Hg): -24 Final Vacuum(in Hg): -1 Receipt Vacuum(in Hg): -5.5 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 Sample Flags: RL-11 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst cis-1,2-Dichloroethylene 2500 15 6.1 9800 59 24 300 12/27/18 12:08 BRF trans-1,2-Dichloroethylene 99 15 6.1 390 59 24 300 12/27/18 12:08 BRF Tetrachloroethylene 18000 60 33 120000 410 230 1200 12/27/18 4:05 BRF Trichloroethylene 4400 15 6.1 24000 81 33 300 12/27/18 12:08 BRF Vinyl Chloride ND 15 9.4 ND 38 24 300 12/27/18 12:08 BRF Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 92.4 70-130 94.5 70-130 12/27/18 12:08 12/27/18 4:05 Page 4 of 13 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep -EPA TO-15 Pre-Dil Pre-Dil Default Actual Pressure Pre Initial Final Injection Injection Lab Number [Field ID[ Batch Dilution Dilution mL mL mL mL Date 18L1068-01 [SG-5] B220123 1.5 200 5 1000 400 400 12/26/18 18L1068-01RE1 [SG-5] B220123 1.5 200 5 1000 400 100 12/26/18 Page 5 of 13 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD Analyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual Batch B220123 - TO-15 Prep Blank (B220123-BLKl) Prepared & Analyzed: 12/26/18 cis-1,2-Dichloroethylene ND 0.10 trans-1,2-Dichloroethylene ND 0.10 Tetrachloroethylene ND 0.10 Trichloroethylene ND 0.10 Vinyl Chloride ND 0.10 Surrogate: 4-Bromofluorobenzene (1) LCS (B220123-BSI) 7.63 8.00 95.4 Prepared & Analyzed: 12/26/18 70-130 cis-1,2-Dichloroethylene 5.36 5.00 107 70-130 trans-1,2-Dichloroethylene 5.77 5.00 115 70-130 Tetrachloroethylene 5.79 5.00 116 70-130 Trichloroethylene 5.26 5.00 105 70-130 Vinyl Chloride 5.25 5.00 105 70-130 Surrogate: 4-Bromofluorobenzene (1) 7.74 8.00 96.7 70-130 Page 6 of 13 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. RL-11 Elevated reporting limit due to high concentration of target compounds. ANALYST RAP Raisa A. Petraitis PEB Paula E. Blakeborough KKM Kerry K. McGee BRF Brittany R. Fisk Page 7 of 13 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (S029991-ICV1) Lab File ID: B120417.D Analyzed: 12/04/18 22:13 Bromochloromethane (1) 80510 5.072 82524 5.077 98 60 - 140 -0.0050 +/-0.50 1,4-Difluorobenzene (1) 180031 6.292 183364 6.291 98 60 - 140 0.0010 +/-0.50 Chlorobenzene-d5(1) 157522 9.891 164139 9.89 96 60-140 0.0010 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S030757-CCV1) Lab File ID: 13122609.13 Analyzed: 12/26/18 20:27 Bromochloromethane (1) 96523 5.074 82524 5.077 117 60 - 140 -0.0030 +/-0.50 1,4-Difluorobenzene (1) 229944 6.294 183364 6.291 125 60 - 140 0.0030 +/-0.50 Chlorobenzene-d5(1) 197534 9.887 164139 9.89 120 60-140 -0.0030 +/-0.50 LCS (B220123-BS1 ) Lab File ID: B122610.D Analyzed: 12/26/18 20:54 Bromochloromethane (1) 92152 5.07 96523 5.074 95 60 - 140 -0.0040 +/-0.50 1,4-Difluorobenzene (1) 215672 6.29 229944 6.294 94 60 - 140 -0.0040 +/-0.50 Chlorobenzene-d5(1) 190832 9.889 197534 9.887 97 60-140 0.0020 +/-0.50 Blank (B220123-BLK1) Lab File ID: B 122614.13 Analyzed: 12/26/18 22:57 Bromochloromethane (1) 98221 5.072 96523 5.074 102 60 - 140 -0.0020 +/-0.50 1,4-Difluorobenzene (1) 231618 6.292 229944 6.294 101 60 - 140 -0.0020 +/-0.50 Chlorobenzene-d5(1) 203736 9.891 197534 9.887 103 60-140 0.0040 +/-0.50 SG-5 (18L1068-01RE1) Lab File ID: B122624.D Analyzed: 12/27/18 04:05 Bromochloromethane (1) 98866 5.076 96523 5.074 102 60 - 140 0.0020 +/-0.50 1,4-Difluorobenzene (1) 241135 6.296 229944 6.294 105 60 - 140 0.0020 +/-0.50 Chlorobenzene-d5(1) 212591 9.889 197534 9.887 108 60-140 0.0020 +/-0.50 SG-5 (18L1068-01) Lab File ID: B122641.D Analyzed: 12/27/18 12:08 Bromochloromethane (1) 83218 5.072 96523 5.074 86 60 - 140 -0.0020 +/-0.50 1,4-Difluorobenzene (1) 187615 6.292 229944 6.294 82 60 - 140 -0.0020 +/-0.50 Chlorobenzene-d5(1) 162339 9.891 197534 9.887 82 60-140 0.0040 +/-0.50 Page 8 of 13 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S030757-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) cis-1,2-Dichloroethylene A 5.00 4.59 0.6369715 0.5844493 -8.2 30 trans-1,2-Dichloroethylene L 5.00 4.16 0.5990668 0.5273935 -16.9 30 Tetrachloroethylene A 5.00 5.27 0.3710352 0.3910942 5.4 30 Trichlomethylene A 5.00 4.35 0.2710247 0.2356052 -13.1 30 Vinyl Chloride A 5.00 6.07 0.5200947 0.6317251 21.5 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 9 of 13 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications EPA TO-15 in Air cis-1,2-Dichloroethylene AIHA,FL,NY,VA trans-1,2-Dichloroethylene AIHA,NJ,NY,VA Tetrachloroethylene AIHA,FL,NJ,NY,VA Trichloroethylene AIHA,FL,NJ,NY,VA Vinyl Chloride AIHA,FL,NJ,NY,VA The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2019 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LA000112 12/30/2019 NC North Carolina Div. of Water Quality 652 12/31/2019 NJ New Jersey DEP MA007 NELAP 06/30/2019 FL Florida Department of Health E871027 NELAP 06/30/2019 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2019 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2019 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2019 NC-DW North Carolina Department of Health 25703 07/31/2019 Page 10 of 13 E CL m. c`6s a N Rc°f cOm o o a Co py y U Li C c 2 a c3 a o Lab Receipt Pressure d 2 o Final Pressure m N y initial Pressure E o ii M MQ n LU Q cii N � Q 7 � Q cc 1jr O a u o V 0 M^ O • M Q X >S p a o o s a .� H x .- e E E C G � C F E _ ,yam C: 3 Z U N .. i- 0 '.. .� .E Q � V c 6: � 'U ° Q E c o Gi L iCri x s Page 11 of 13 12/25/2018 Track your package or shipment with FedEx Tracking 774037088636 Delivered Monday 12/24/2018 at 11:40 are DELIVERED Signed for by: GRACHEAL GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM TO Rekeigl', NC US hasp Long.-nPadov,,, !,�A US Multiple -piece Shipment 5 Piece shipment TRACKING NUMBER SHIPPER CITY, STATE SNIP DATE STATUS DELIVERY GATE DESTINATION/RECIPIENT CITY, STATE 17407088599 (master ) DJRHAh1, NC 12,/2U/2018 12/2421018 EAST LONGMEADOV4 , IMA 774037087835 DU€;HAkl, NC 12/20,, 2C18 12/24r2018 EAST LGNGMEADOA� MA 774037088636 DJRI IAIvl, NC 12/20/2018 12/24:/2018 EAST LONGMEADOVV, NIA 77403708S810 DURHAM, NC 12/20/2018 12/24/2018 EAST I ONGMEADOW, MA 774037089470 D[ R11AM, NC 12/20,/2018 12/24/2018 EAST LONGMEA"101Y, MIA Shipment Facts TRACKING NUMBER SERVICE REFERENCE 774037088636 Fec'Ex Grouxt 80 MASTER TRACKING NUMBER WEIGHT DIMENSIONS 774037088599 16ILS / 6.8 kgs 2 2 x 14x9 ill. TOTAL PIECES TOTAL SHIPMENT WEIGHT TERMS 5 75 lbs / 34.02 kgs Third Party PACKAGING STANDARD TRANSIT SHIP DATE Package 10 L 12124/20] 8 TILL i 2/20/?018 https://www.fedex.com/a ppstfedextrackl?action =track&tracknumbers=774037088636&locale=en_US&Cntry_code=us Page 12 of 13 I Have Not Confirmed Sample Container Numbers With Lab Staff Before C 00 n mm UE S t Relinquishing Over [-aA�E3C3FlAk-rc>Fly Samples Doc# 278 Reu 6 2017 Air Media Sample Receipt Checklist - (Rejection Criteria Listing - using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State True or False Client Received By C)L2S Date Time (J,.k40 How were the samples In Cooler On Ice No Ice received? In Box t-- Ambient Melted Ice Were samples within Temperature By Gun # Actual Temp - Compliance? 2-6°C two, By Blank # Actua[ Temp - Was Custody Seal Intact? Were Samples Tampered with? N(A Was COC Relinquished ? Does Chain Agree With Samples? Are there any loose caps/valves on any samples? Is CDC in ink/ Legible?__-- Did COC Include all Client -T Analysis i Sampler Name T Pertinent Information? Project ID's �� Collection Dates/Times T' Are Sample Labels filled out and legible? Are there Rushes? _E Who was notified? Samples are received within holding time? Y Proper Media Used? - — Individually Certified Cans? Are there Trip Blanks? F Is there enough Volume? w _ Summa Cans li 'a- Nut/Ferrule IC Train Tedlar Baqs Tubing TO-17 Tubes T-Connector°' -: Radiello Syringe Pufs/TO-11 s Tedlar Comments: ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 January 22, 2019 Nick Shore AECOM-Morrisville NC 1600 Perimeter Park Drive Morrisville, NC 27560 Project Location: Chapel Hill, NC Client Job Number: Project Number: 60566538 Laboratory Work Order Number: 19A1036 Enclosed are results of analyses for samples received by the laboratory on January 18, 2019. If you have any questions concerning this report, please feel free to contact me. Sincerely, I,&, �. A�� Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 AECOM-Morrisville NC REPORT DATE: 1/22/2019 1600 Perimeter Park Drive Morrisville, NC 27560 PURCHASE ORDER NUMBER: 60566538 ATTN: Nick Shore PROJECT NUMBER: 60566538 ANALYTICAL SUMMARY WORK ORDER NUMBER: 19A1036 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Chapel Hill, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB IA-2 19A1036-01 Air RAD 130 IA-3 19A1036-02 Air RAD 130 Page 2 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method Radiello RAD-130 - The sampling rates for trichloroethene and tetrachloroethene are as follows: trichloroethene = 69 mL/min, tetrachloroethene = 59 mL/min. The theoretical sampling rates for vinyl chloride, trans-1,2-dichloroethene, and cis-1,2-dichloroethene are estimated using Graham's Law and are as follows: vinyl chloride = 103 mL/min, trans-1,2-dichloroethene = 83 mL/min, cis-1,2-dichloroethene = 83 mL/min. The results for these 3 compounds are estimated values. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. 4Z�14__ VWWLO_� Lisa A. Worthington Project Manager Page 3 of 14 ,con -testy ANALYTICAL LABORATORY Project Location: Chapel Hill, NC Date Received: 1/18/2019 Field Sample #: IA-2 Sample ID: 19A1036-01 Sample Matrix: Air Sampled: 1/18/2019 08:45 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Flow Controller ID: Sample Type: Air Volume L: 10075 Work Order: 19A1036 RAD 130 Total µg ug/m3 Date/Time Analyte Results RL MDL Flag/Qua[ Results ILL MDL Dilution Analyzed Analyst Vinyl Chloride ND 0.16 ND 0.15 1 1/22/19 13:29 IMR trans-1,2-Dichloroethene ND 1.0 ND 1.2 1 1/22/19 13:29 IMR cis-1,2-Dichloroethene ND 0.20 ND 0.24 1 1/22/19 13:29 IMR Tichloroethene 1.1 0.20 1.6 0.29 1 1/22/19 13:29 IMR Tetrachloroethene 1.5 0.20 2.6 0.34 1 1/22/19 13:29 IMR Page 4 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Chapel Hill, NC Sample Description/Location: Work Order: 19A1036 Date Received: l/18/2019 Sub Description/Location: Field Sample #: IA-3 Sample ID: 19A1036-02 Sample Matrix: Air Flow Controller ID: Sampled: 1/18/2019 08:50 Sample Type: Air Volume L: 10075 RAD 130 Total µg ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results ILL MDL Dilution Analyzed Analyst Vinyl Chloride ND 0.16 ND 0.15 1 1/22/19 13:52 IMR trans-1,2-Dichloroethene ND 1.0 ND 1.2 1 1/22/19 13:52 IMR cis-1,2-Dichloroethene ND 0.20 ND 0.24 1 1/22/19 13:52 IMR Tichloroethene 0.97 0.20 1.4 0.29 1 1/22/19 13:52 IMR Tetrachloroethene 1.3 0.20 2.3 0.34 1 1/22/19 13:52 IMR Page 5 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: Radiello-RAD 130 Lab Number [Field ID] Batch Initial [Cartridge Final [mL] Date 19A1036-01 [IA-2] B221755 1.00 2.00 01/22/19 19A1036-02 [IA-3] B221755 1.00 2.00 01/22/19 Page 6 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Miscellaneous Air Analyses - Quality Control Total µg ug/m3 Spike Level Source %REC RPD ,nalyte Results RL Results RL Total µg Result %REC Limits RPD Limit Flag/Qua Batch B221755 - Radiello Blank (B221755-BLK1) Prepared & Analyzed: 01/22/19 Vinyl Chloride ND 0.16 trans-1,2-Dichloroethene ND 1.0 cis-1,2-Dichloroethene ND 0.20 Trichloroethene ND 0.20 Tetrachloroethene ND 0.20 LCS (B221755-BS1) Prepared & Analyzed: 01/22/19 Vinyl Chloride 8.30 0.16 0.41 10.0 83.0 40-140 trans-1,2-Dichloroethene 8.33 1.0 10.0 83.3 40-140 cis-1,2-Dichloroethene 9.80 0.20 10.0 98.0 40-140 Trichloroethene 9.42 0.20 10.0 94.2 40-140 Tetrachloroethene 9.38 0.20 10.0 93.8 40-140 LCS Dup (B221755-BSD1) Prepared & Analyzed: 01/22/19 Vinyl Chloride 7.46 0.16 0.41 10.0 74.6 40-140 10.7 30 trans-1,2-Dichloroethene 7.46 1.0 10.0 74.6 40-140 11.0 30 cis-1,2-Dichloroethene 8.68 0.20 10.0 86.8 40-140 12.1 30 Trichloroethene 8.16 0.20 10.0 81.6 40-140 14.4 30 Tetrachloroethene 8.26 0.20 10.0 82.6 40-140 12.8 30 Page 7 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. ANALYST RAP Raisa A. Petraitis KKM Kerry K. McGee IMR Irina Raducan CJM Christian J. Merchant Page 8 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 INTERNAL STANDARD AREA AND RT SUMMARY RAD 130 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Difi RT Diff Limit Q LCS (B221755-BS1 Lab File ID: 130122002.1) Analyzed: O1/22/19 12:10 2-Fluorotoluene 8685458 13.47 7219611 13.464 120 50-200 0.0060 +/-0.50 LCS Dup (B221755-BSD1) Lab File ID: B0I22003.D Analyzed: 01/22/19 12:33 2-Fluorotoluene 9263501 13.468 7219611 13.464 128 50-200 0.0040 +/-0.50 Blank (B221755-BLK1) Lab File ID: B0122004.D Analyzed: 01/22/19 13:06 2-Fluorotoluene 8095880 13.473 7219611 13.464 112 50-200 0.0090 +/-0.50 IA-2 (19A1036-01) Lab File ID: B0122005.D Analyzed: 01/22/19 13:29 2-Fluorotoluene 7794244 13.469 7219611 13.464 108 50-200 0.0050 +/-0.50 IA-3 (19A1036-02 ) Lab File ID: 130122006.13 Analyzed: 01/22/19 13:52 2-Fluorotoluene 8184252 13.465 7219611 13.464 113 50-200 0.0010 +/-0.50 Page 9 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CONTINUING CALIBRATION CHECK COMPOUND TYPE RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 10 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications No certified Analyses included in this Report The CON -TEST Environmental Laboratory operates under the following certifications and accreditation Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2019 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LA000112 12/30/2019 NC North Carolina Div. of Water Quality 652 12/31/2019 NJ New Jersey DEP MA007 NELAP 06/30/2019 FL Florida Department of Health E871027 NELAP 06/30/2019 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2019 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2019 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2019 NC-DW North Carolina Department of Health 25703 07/31/2019 Page 11 of 14 7.N - 47 4 = Ru i N W G O m W m I.E. N E �,,, L m m i 3 0 o Ij V E a `a � ,E c CL r m 3 ° E a o E o m c Q u m E W °1 On ..E� �c E vc 00 a �3Ed o ,n 0 o Lab Receipt Pressure Q y o an Final Pressure z4 a U.1 Initial Pressure ouni H N j M m UJ q, V) �I J Y Q i z � � m c�[ o o © ❑ ❑❑ '❑ E O c c E E �..... u LLJ a IK ©© W w Zj t7 u m a s O r+f j O Z Z O El a ea n © >, o 9 o �� E cW. ul m w LT u z a �_ rG PO OJ N E V e G G i/1 N ai c m , Eca S N U p 111 ra Ad tkZ « E !Y �e o a a, n v a E ca d "u a L v sr u v c"i v v v F u .o v a > 25 [ a N Z to Ij 9 u° O m� Z L �a m m a }� O= II Niimm u It gmN� 1 Co N<dNOm0 fillc C E 3 jr-, C v o E a ? d u ' I� 'cs c ui N c m C 49 V L u r Ld u a c 0 T c m a LA 0 L, Jl -q ;O Z � D C V Z ❑ ❑ < � a N c 6- o Gr a ❑ ❑ ❑ a " 3 ❑ ❑ ❑ c v n 0 Ui V c w u e o ❑ ❑ ❑ a �Y E e�" E E "�. -0 ,U N r c nn ,� • vn c ,.+ rn .� on A Pape 12 of 14 1 1/19/2019 Track your package or shipment with FedEx Tracking 774247696475�ti Delivered Saturday 1 /19/2019 at 10.1 i are FROM Raleigl;, NC US Shipment Facts TRACKING NUMBER 774247696475 DIMENSIONS 17x11x15 in. TOTAL SHIPMENT WEIGHT 24.9 Ibs / 11.29 kgs PACKAGING your Packaging SHIP DATE 0 Fri 1/18/2019 DELIVERED Signed for by. B.BDDA GET STATUS UPDATES OBTAIN PROOF OF DELIVERY TO EAST LONGMEADOW, MA US SERVICE WEIGHT Fe.dFx Priority Overnight 24.9 Ibs / 11 29 kgs DELIVERED TO TOTAL PIECES Shipping/Receiving 1 TERMS SHIPPER REFERENCE Third Party 80 SPECIAL HANDLING SECTION STANDARD TRANSIT For Saturday Delivery 1 i 19/2019 by 12,00 pm ACTUAL DELIVERY Sat 1/19/2019 10:17 any "ravel History Saturday,1/19/2019 10:17 am EAST LONGMEADOW, MA Delivered 9:33 am W INDSOR LOCKS, CT On FedEx vehicle for delivery 9:23 am WINDSOR LOCKS, CT Al local FedEx facility hftps://www.fedex.com/apps/fedextrack/?action =track&tracknumbe rs=7742476964 75&locale=en_US&cntry_code=us Local Scan Time Page 13 of 14 Received By How were the samples received? Were samples within Temperature Compliance? 2-60C Was Custody Seal Intact? Was COC Relinquished ? Date In Cooler i In Box By Gun # By Blank # ram_ Are there any loose caps/valves on any samples? Is COC in ink/ Legible? -f Time On Ice' i No Ice Ambient Melted Ice ! Actual Temp - Actual Temp - Were Samples Tampered with? Does Chain Agree With Samples? Did COC Include all Client Analysis Pertinent Information? Project I- ID's r Are Sample Labels filled out and legible? F Are there Rushes? F Who was notified? Sampler Name fi Collection Dates/Times —t-� - Samples are received within holding time? --- Proper Media Used? -T-- Individually Certified Cans? Are there Trip Blanks? r Is there enough Volume? .. „f- Summa Cans Nut/Ferrule IC Train Tedlar Bags Tubing TO-17 Tubes T-Connector , . I. Radiello �rt,J Syringe PufsfTO-11 s I I Tedlar Comments: ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 January 24, 2019 Nick Shore AECOM-Morrisville NC 1600 Perimeter Park Drive Morrisville, NC 27560 Project Location: Chapel Hill, NC Client Job Number: Project Number: 60566538 Laboratory Work Order Number: 19AO860 Enclosed are results of analyses for samples received by the laboratory on January 16, 2019. If you have any questions concerning this report, please feel free to contact me. Sincerely, I,&, �. A�� Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 AECOM-Morrisville NC REPORT DATE: 1/24/2019 1600 Perimeter Park Drive Morrisville, NC 27560 PURCHASE ORDER NUMBER: 60566538 ATTN: Nick Shore PROJECT NUMBER: 60566538 ANALYTICAL SUMMARY WORK ORDER NUMBER: 19AO860 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Chapel Hill, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB IA-2 (8-HR) IA-3 (8-HR) 19AO860-01 Indoor air 19AO860-02 Indoor air EPA TO-15 EPA TO-15 Page 2 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Project Manager Page 3 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Chapel Hill, NC Sample Description/Location: Work Order: 19A0860 Date Received: 1/16/2019 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: IA-2 (8-HR) Canister ID: 2193 Final Vacuum(in Hg): -14 Sample ID: 19AO860-01 Canister Size: 6 liter Receipt Vacuum(in Hg): -12.8 Sample Matrix: Indoor air Flow Controller ID: 3052 Flow Controller Type: Fixed -Orifice Sampled: 1/11/2019 14:25 Sample Type: 8 hr Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst cis-1,2-Dichloroethylene ND 0.035 0.014 ND 0.14 0.057 0.702 1/22/19 4:20 BRF trans-1,2-Dichloroethylene ND 0.035 0.014 ND 0.14 0.056 0.702 1/22/19 4:20 BRF Tetrachloroethylene 0.21 0.035 0.020 1.4 0.24 0.13 0.702 1/22/19 4:20 BRF Trichloroethylene 0.027 0.035 0.014 J 0.15 0.19 0.076 0.702 1/22/19 4:20 BRF Vinyl Chloride ND 0.035 0.022 ND 0.090 0.057 0.702 1/22/19 4:20 BRF Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 85.9 70-130 1/22/19 4:20 Page 4 of 14 ,con -testy ANALYTICAL LABORATORY Project Location: Chapel Hill, NC Date Received: l/16/2019 Field Sample #: IA-3 (8-HR) Sample ID: 19AO860-02 Sample Matrix: Indoor air Sampled: 1 /11/2019 14:30 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1013 Canister Size: 6 liter Flow Controller ID: 3250 Sample Type: 8 hr Work Order: 19A0860 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -15 Receipt Vacuum(in Hg): -14.2 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst cis-1,2-Dichloroethylene ND 0.040 0.016 ND 0.16 0.065 0.8 1/22/19 5:08 BRF trans-1,2-Dichloroethylene ND 0.040 0.016 ND 0.16 0.064 0.8 1/22/19 5:08 BRF Tetrachloroethylene 0.21 0.040 0.022 1.4 0.27 0.15 0.8 1/22/19 5:08 BRF Trichloroethylene 0.023 0.040 0.016 J 0.12 0.21 0.087 0.8 1/22/19 5:08 BRF Vinyl Chloride ND 0.040 0.025 ND 0.10 0.064 0.8 1/22/19 5:08 BRF Surrogates 4-Bromofluorobenzene (1) % Recovery 86.1 % REC Limits 70-130 1/22/19 5:08 Page 5 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep -EPA TO-15 Pre-Dil Pre-Dil Default Actual Pressure Pre Initial Final Injection Injection Lab Number [Field ID] Batch Dilution Dilution mL mL mL mL Date 19AO860-01 [IA-2 (8-HR)] B221765 1.5 1 N/A 1000 400 855 01/21/19 19AO860-02 [IA-3 (8-HR)] B221765 2 1 N/A 1000 400 1000 01/21/19 Page 6 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD Analyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual Batch B221765 - TO-15 Prep Blank (B221765-BLK1) Prepared & Analyzed: 01/21/19 cis-1,2-Dichloroethylene ND 0.035 trans-1,2-Dichloroethylene ND 0.035 Tetrachloroethylene ND 0.035 Trichloroethylene ND 0.035 Vinyl Chloride ND 0.035 Surrogate: 4-Bromofluorobenzene (1) LCS (B221765-BS1) 6.81 8.00 85.1 Prepared & Analyzed: 01/21/19 70-130 cis-1,2-Dichloroethylene 5.42 5.00 108 70-130 trans-1,2-Dichloroethylene 6.34 5.00 127 70-130 Tetrachloroethylene 4.64 5.00 92.7 70-130 Trichloroethylene 5.08 5.00 102 70-130 Vinyl Chloride 5.63 5.00 113 70-130 Surrogate: 4-Bromofluorobenzene (1) 7.02 8.00 87.7 70-130 Page 7 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). ANALYST RAP Raisa A. Petraitis PEB Paula E. Blakeborough KKM Kerry K. McGee BRF Brittany R. Fisk Page 8 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (S028828-ICV1) Lab File ID: F102923.13 Analyzed: 10/30/18 04:10 Bromochloromethane (1) 178163 8.64 173242 8.637 103 60 - 140 0.0030 +/-0.50 1,4-Difluorobenzene (1) 535471 10.409 508001 10.409 105 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 489391 14.775 471214 14.778 104 60-140 -0.0030 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S031512-CCVI) Lab File ID: F012104.D Analyzed: 01/21/19 14:39 Bromochloromethane (1) 109756 8.624 173242 8.637 63 60 - 140 -0.0130 +/-0.50 1,4-Difluorobenzene (1) 355459 10.392 508001 10.409 70 60 - 140 -0.0170 +/-0.50 Chlorobenzene-d5(1) 331512 14.759 471214 14.778 70 60-140 -0.0190 +/-0.50 LCS (B221765-BS1 ) Lab File ID: F012105.13 Analyzed: 01/21/19 15:18 Bromochloromethane (1) 109450 8.627 109756 8.624 100 60 - 140 0.0030 +/-0.50 1,4-Difluorobenzene (1) 351668 10.392 355459 10.392 99 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 329543 14.759 331512 14.759 99 60-140 0.0000 +/-0.50 Blank (B221765-BLK1) Lab File ID: F012108.D Analyzed: 01/21/19 18:08 Bromochloromethane (1) 108527 8.627 109756 8.624 99 60 - 140 0.0030 +/-0.50 1,4-Difluorobenzene (1) 343329 10.396 355459 10.392 97 60 - 140 0.0040 +/-0.50 Chlorobenzene-d5(1) 321438 14.759 331512 14.759 97 60-140 0.0000 +/-0.50 IA-2 (8-HR) (19A0860-01) Lab File ID: F012123.D Analyzed: 01/22/19 04:20 Bromochloromethane (1) 102119 8.621 109756 8.624 93 60 - 140 -0.0030 +/-0.50 1,4-Difluorobenzene(1) 309786 10.392 355459 10.392 87 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 293134 14.756 331512 14.759 88 60-140 -0.0030 +/-0.50 IA-3 (8-HR) (19A0860-02) Lab File ID: F012124.D Analyzed: 01/22/19 05:08 Bromochloromethane (1) 102827 8.624 109756 8.624 94 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 315996 10.389 355459 10.392 89 60-140 -0.0030 +/-0.50 Chlorobenzene-d5(1) 298072 14.759 331512 14.759 90 60-140 0.0000 +/-0.50 Page 9 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S031512-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) cis-1,2-Dichloroethylene A 5.00 5.94 0.7692606 0.9144211 18.9 30 trans-1,2-Dichloroethylene A 5.00 6.08 0.6973638 0.8475528 21.5 30 Tetrachloroethylene A 5.00 5.11 0.4524124 0.4627139 2.3 30 Trichlomethylene A 5.00 5.56 0.2796892 0.3110165 11.2 30 Vinyl Chloride A 5.00 6.25 0.6840267 0.8545938 24.9 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 10 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications EPA TO-15 in Air cis-1,2-Dichloroethylene AIHA,FL,NY,VA trans-1,2-Dichloroethylene AIHA,NJ,NY,VA Tetrachloroethylene AIHA,FL,NJ,NY,VA Trichloroethylene AIHA,FL,NJ,NY,VA Vinyl Chloride AIHA,FL,NJ,NY,VA The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2019 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LA000112 12/30/2019 NC North Carolina Div. of Water Quality 652 12/31/2019 NJ New Jersey DEP MA007 NELAP 06/30/2019 FL Florida Department of Health E871027 NELAP 06/30/2019 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2019 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2019 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2019 NC-DW North Carolina Department of Health 25703 07/31/2019 Page 11 of 14 -5_ CL to in M ' o O i r '^ n a °' -E .2 c a '� ° y c W E 1= 0 Ca am% Epep sit E y 10 H p U M o� a cc,v ae a, 0. �!} C _ ° Gan E O Q Lab Receipt Pressure c 2 y Final Pressure E W Initial Pressure N _ U mN u O 4i QJ N CY v � o � }' 2 � Q >_ cc 0 El El JLi J �+ M cY 4 3 Cr v � Q O n � E 2 x O M t/'1 vE Ncj ® N 3U = I 4 L? O O X C W w- d � E a #A V 2 €O Y r aEG E Z .. Y > fj c ��pp V E E Q ro O m (v (y U Q _w 5 O m O � � Q y x xx x z o 0 V1 z cc � c70mQ Y CA � o JOE, z W v OC]a°3a.a�.0 a R 3f II Co a ti �Qav am � m � 0 4S 0 2 U Q Cil ❑ ❑ Q Q Q7 d £ Q E O E 2 Q c �_ T C ro � 2 E w Uj is c a Cr- J E E g E a c LE 9 cc CDF in I a iT /✓ ✓T .- 73 L .1 N N C E U V M MIX x (Y x C> Page 12 of 14 1/18/2019 Track your package or shipment with FedEx Tracking N&E-r"j-. 's 774211166239 Delivered Friday 1/18/2019 at 11A6 am DELIVERED Signed for by: PRACHEAL GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM TO Raleigh, NC US East Longmeadow, MA U5 Shipment Facts TRACKING NUMBER SERVICE REFERENCE 774211166239 FedEx Ground 80 WEIGHT DIMENSIONS TOTAL PIECES 15 Ibs / 6.8 kgs 21x14x9 in. 1 TERMS PACKAGING STANDARD TRANSIT Third Party Package 0 1/18/2019 SHIP DATE ACTUAL. DELIVERY (D Fri 1/18/2019 11.16 ann Wed 1/16/2019 Travel History Local Scan Time v Friday,1/18/2p19 11:16 am East Longmeadow, MA Delivered 5:09 am CHICOPEE, MA an FedEx vehicle for delivery 5,00 am CHICOPEE, MA At local FedEx facility 12.A2 am MIDDLETOWN, CT Departed FedEx location Thursday,1/1712019 https://www.fedex.com/apps/fedextrackl?action=track&tracknumbers=774211166239&locale=en_US&cntry_code=us Page 13 of 14 I I Have Not Confirmed Sample Container Numbers With Lab Staff Before Relinquishing Over Samples . ............. ..... ..... ........ ..... ... ....... D60 278' R17 Fier 6 20 1. ... 1. . 1,.,..''.. .1. .1 ..'. . . .. .... ........ ... Air Media Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State True or False Client PLQKL-1"-\ Received By pp_-, Date Time How were the samples In Cooler On Ice No Ice received? In Box --T- Ambient Melted Ice Were samples within Temperature By Gun # Actual Temp - Compliance? 2-6'C 01) By Blank ft Actual Temp - Was Custody Seal Intact? A Were Samples Tampered with? Was COC Relinquished ? Does Chain Agree With Samples? -E. Are there any loose caps/valves on any samples? Is COC in ink/ Legible? -V Did COC Include all Client Analysis Sampler Name Pertinent Information? Project 7k— ID's Collection Dates/Times Are Sample Labels filled out and legible? —F Are there Rushes? E Who was notified? Samples are received within holding time? :L Proper Media Used? Individually Certified Cans? Are there Trip Blanks? F— Is there enough Volume? 71— ML��� Summa Cans (AJ Nut/Ferrule IC Train Tedlar Baqs Tubing TO-1 7 Tubes T-Connector Radiello Syringe Pufs/TO-1 1 s Tedlar %,*urnmenx.5-. ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 February 21, 2019 Nick Shore AECOM-Morrisville NC 1600 Perimeter Park Drive Morrisville, NC 27560 Project Location: Chapel Hill, NC Client Job Number: Project Number: 60566538 Laboratory Work Order Number: 19BO758 Enclosed are results of analyses for samples received by the laboratory on February 15, 2019. If you have any questions concerning this report, please feel free to contact me. Sincerely, I,&, �. A�� Kerry K. McGee Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 AECOM-Morrisville NC REPORT DATE: 2/21/2019 1600 Perimeter Park Drive Morrisville, NC 27560 PURCHASE ORDER NUMBER: 60566538 ATTN: Nick Shore PROJECT NUMBER: 60566538 ANALYTICAL SUMMARY WORK ORDER NUMBER: 19BO758 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Chapel Hill, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB IA-2 19BO758-01 Indoor air IA-3 19BO758-02 Indoor air RAD 130 RAD 130 Page 2 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method Radiello RAD-130 - The sampling rates for trichloroethene and tetrachloroethene are as follows: trichloroethene = 69 mL/min, tetrachloroethene = 59 mL/min. The theoretical sampling rates for vinyl chloride, trans-1,2-dichloroethene, and cis-1,2-dichloroethene are estimated using Graham's Law and are as follows: vinyl chloride = 103 mL/min, trans-1,2-dichloroethene = 83 mL/min, cis-1,2-dichloroethene = 83 mL/min. The results for these 3 compounds are estimated values. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. 4Z�14__ VWWLO_� Lisa A. Worthington Project Manager Page 3 of 14 ,con -testy ANALYTICAL LABORATORY Project Location: Chapel Hill, NC Date Received: 2/15/2019 Field Sample #: IA-2 Sample ID: 19BO758-01 Sample Matrix: Indoor air Sampled: 2/ 15/2019 13:00 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Flow Controller ID: Sample Type: Air Volume L: 10080 Work Order: 19BO758 RAD 130 Total µg ug/m3 Date/Time Analyte Results RL MDL Flag/Qua[ Results ILL MDL Dilution Analyzed Analyst Vinyl Chloride ND 0.16 ND 0.15 1 2/20/19 15:46 IMR trans-1,2-Dichloroethene ND 1.0 ND 1.2 1 2/20/19 15:46 IMR cis-1,2-Dichloroethene ND 0.20 ND 0.24 1 2/20/19 15:46 IMR Tichloroethene 1.1 0.20 1.6 0.29 1 2/20/19 15:46 IMR Tetrachloroethene 1.5 0.20 2.5 0.34 1 2/20/19 15:46 IMR Page 4 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Chapel Hill, NC Sample Description/Location: Work Order: 19BO758 Date Received: 2/15/2019 Sub Description/Location: Field Sample #: IA-3 Sample ID: 19BO758-02 Sample Matrix: Indoor air Flow Controller ID: Sampled: 2/15/2019 13:05 Sample Type: Air Volume L: 10080 RAD 130 Total µg ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results ILL MDL Dilution Analyzed Analyst Vinyl Chloride ND 0.16 ND 0.15 1 2/20/19 16:10 IMR trans-1,2-Dichloroethene ND 1.0 ND 1.2 1 2/20/19 16:10 IMR cis-1,2-Dichloroethene ND 0.20 ND 0.24 1 2/20/19 16:10 IMR Tichloroethene 1.1 0.20 1.6 0.29 1 2/20/19 16:10 IMR Tetrachloroethene 1.1 0.20 1.8 0.34 1 2/20/19 16:10 IMR Page 5 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: Radiello-RAD 130 Lab Number [Field ID] Batch Initial [Cartridge Final [mL] Date 19B0758-01 [IA-2] B223980 1.00 2.00 02/20/19 19B0758-02 [IA-3] B223980 1.00 2.00 02/20/19 Page 6 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Miscellaneous Air Analyses - Quality Control Total µg ug/m3 Spike Level Source %REC RPD ,nalyte Results RL Results RL Total µg Result %REC Limits RPD Limit Flag/Qua Batch B223980 - Radiello Blank (B223980-BLK1) Prepared & Analyzed: 02/20/19 Vinyl Chloride ND 0.16 trans-1,2-Dichloroethene ND 1.0 cis-1,2-Dichloroethene ND 0.20 Trichloroethene ND 0.20 Tetrachloroethene ND 0.20 LCS (B223980-BSI) Prepared & Analyzed: 02/20/19 Vinyl Chloride 7.62 0.16 0.41 10.0 76.2 40-140 trans-1,2-Dichloroethene 8.07 1.0 10.0 80.7 40-140 cis-1,2-Dichloroethene 8.54 0.20 10.0 85.4 40-140 Trichloroethene 7.83 0.20 10.0 78.3 40-140 Tetrachloroethene 7.50 0.20 10.0 75.0 40-140 LCS Dup (B223980-BSD1) Prepared & Analyzed: 02/20/19 Vinyl Chloride 7.69 0.16 0.41 10.0 76.9 40-140 0.914 30 trans-1,2-Dichloroethene 7.96 1.0 10.0 79.6 40-140 1.40 30 cis-1,2-Dichloroethene 8.66 0.20 10.0 86.6 40-140 1.40 30 Trichloroethene 8.01 0.20 10.0 80.1 40-140 2.32 30 Tetrachloroethene 7.91 0.20 10.0 79.1 40-140 5.37 30 Page 7 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. ANALYST RAP Raisa A. Petraitis KKM Kerry K. McGee IMR Irina Raducan CLA Catherine L. Amrich Page 8 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 INTERNAL STANDARD AREA AND RT SUMMARY RAD 130 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Diff RT Diff Limit Q LCS (B223980-BS1 Lab File ID: 130220002.1) Analyzed: 02/20/19 14:23 2-Fluorotoluene 8270419 13.442 7442237 13.439 111 50-200 0.0030 +/-0.50 LCS Dup (B223980-BSD1) Lab File ID: B0220003.D Analyzed: 02/20/19 14:59 2-Fluorotoluene 7909885 13.44 7442237 13.439 106 50-200 0.0010 +/-0.50 Blank (B223980-BLK1) Lab File ID: B0220004.D Analyzed: 02/20/19 15:22 2-Fluorotoluene 7081383 13.439 7442237 13.439 95 50-200 0.0000 +/-0.50 IA-2 (19110758-01 ) Lab File ID: B0220005.D Analyzed: 02/20/19 15:46 2-Fluorotoluene 7718608 13.442 7442237 13.439 104 50-200 0.0030 +/-0.50 IA-3 (19B0758-02 ) Lab File ID: 130220006.13 Analyzed: 02/20/19 16:10 2-Fluorotoluene 7422287 13.443 7442237 13.439 100 50 - 200 0.0040 +/-0.50 Page 9 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CONTINUING CALIBRATION CHECK COMPOUND TYPE RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 10 of 14 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications No certified Analyses included in this Report The CON -TEST Environmental Laboratory operates under the following certifications and accreditation Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2019 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2020 RI Rhode Island Department of Health LA000112 12/30/2019 NC North Carolina Div. of Water Quality 652 12/31/2019 NJ New Jersey DEP MA007 NELAP 06/30/2019 FL Florida Department of Health E871027 NELAP 06/30/2019 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2019 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2019 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2019 NC-DW North Carolina Department of Health 25703 07/31/2019 Page 11 of 14 T a :. �+ Ir 'p w a s 't7 W C a C W N BEN:: a `a .�.p yo. affi���+' y Ot O -=to � a d ` � � 0 C r V W � � e o Eoamra � � E•• p(I 3 ?°.Eoa If ,e r d N d T a �� a e a L'" d o Lab Receipt Pressure q° Final Pressure v n ro _ Pressure EInitial u eLn i LN 3 N g NC V1 Ln wog ona X X J a z aj a a o` E ❑ ❑❑IUOF U ; O S V en v :: z z 0�r N CLra❑❑❑ U- fo ass- 4 ; o o E o a n E u z a V � a � M {l4 N d in R C O w N a t11 {(} V Q 0 M In a Cto a O X E C1+ E C O d zZ o m d _ N O O tl U o Ln to a = u U w, Q Ln U Ln Qy M z V_ Z R E O o ;; C Q C a n a: E Ei Z E � a.+ 0 W1 a 0 q .I q 01< o E m = m ...I z ccr C N •l"7 G +' Q7 d H 11, U a o .Ol a .OS a o o° E ro � v ar 1 n o go,m z o C7 4A 7 m z u n�Qj6�r a % G V1 — It N Oa 0 (--1 ❑ L Q It II m 11 II ffi m tj o a m pII L U Q d o � r Q El❑ 0 R O +a+ u A ❑ to u v c u° V U 2 P v Cr C Cr -IC,a o a .0 Ca O c Ir CrW j? ` LA m u E E IL a, a C J a o >•- o ❑ 1❑ c'$ro 0 0 m fa a i A� K 7 U '=M El O _ N CO U a z ❑ ❑ N E 8 l7 � U C yJ i b a n ❑ ❑ ❑ 't7 N V E E E E E E V ♦— I � I 1 I I u a T V C eu 1 10 k'1 M w Page 12 of 14 2116l2019 Track your package or shipment with FedEx Tracking 7744873764411�` Delivered Saturday 2/16/2019 at 10.15 am DELIVERED Signed for by: B.BECCA GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM Raleigh, NC US Multiple -piece Shipment 774487376257 RALEIGH, NC 2/15/2019 77448737 6717 RALEIGH, NC 2/ 15/2019 774487376739 RALEIGH, NC 774487376831 RALEIGH, NC Shipment Facts TRACKING NUMBER 774487376441 2/15/2019 2/15/2019 TO EAST LONGMEADOW, MA US 6 Piece shipment 2/1b/2019 EAST LONGMEADOW, MA 2/16/2019 EAST LONGMEADOW, MA 2/16/2019 EAST LONGMEADOW, MA 2/16/2019 EAST LONGMEADOW, MA SERVICE MASTER TRACKING NUMBER FedEx Priority Overnight 774487376441 WEIGHT DELIVERED TO TOTAL PIECES 15 Ibs / 6 8 tags Shipping"Receivoig 6 https:llwww.fedex.com/apps/fedextrackl?action=track&tracknumbers=774487376441 &locale=en_US&cntry_code=us Page 13 of 14 Client /-(-0Cc)j- Received By Date How were the samples In Cooler r received? In Box Were samples within Temperature By Gun # Compliance? 2-6°C 'T By Blank # Was Custody Seal Intact?ri Was COC Relinquished ? Are there any loose caps/valves on any samples? Is COC in ink/ Legible? - 1 % 1 1 C1 Time = s On Ice T No Ice Ambient Melted Ice Actual Temp - . Actual Temp - Were Samples Tampered with? frR. Does Chain Agree With Samples? -T- Did COC Include all Client - Analysis k Sampler Name Pertinent Information? Project ID's Collection Dates[Times T Are Sample Labels filled out and legible? I I Are there Rushes? F Who was notified? Samples are received within holding time? T Proper Media Used? j Individually Certified Cans?_ Are there Trip Blanks? Is there enough Volume? i Summa Cans Nut/Ferrule IC Train Tedlar Baqs Tubing TO-17 Tubes T-Connector Radiello 2 Syringe Pufs/T0-11s Tedlar ATTACHMENT 16 DSCA PROGRAM RISK CALCULATORS DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 6/15/2018 Sample ID: IA-2 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic 3 (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 2.8 1.1E+O1 8.3E+00 2.6E-07 6.7E-02 79-01-6 Trichloroeth lene 4.8E-Ol 4.2E-Ol 75-01-4 Vinyl Chloride 1.7E-01 2.1E+01 Cumulative: I 2.6E-07 I6.7E-02 DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 12/21/2018 Sample ID: IA-2 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic 3 (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 4.6 1.1E+O1 8.3E+00 4.3E-07 1.1E-Ol 79-01-6 Trichloroeth lene 1.9 4.8E-01 4.2E-01 4.0E-06 9.1E-Ol 75-01-4 1 Vinyl Chloride 1.7E-01 2.1E+01 Cumulative: I 4.4E-06 I1.0E+00 DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 1/18/219 Sample ID: IA-2 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic 3 (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 2.6 1.1E+O1 8.3E+00 2.4E-07 6.2E-02 79-01-6 Trichloroeth lene 1.6 4.8E-01 4.2E-0] 3.3E-06 7.7E-Ol 75-01-4 Vinyl Chloride 1.7E-01 2.1E+01 Cumulative: I 3.6E-06 I8.3E-Ol DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 1/11/2019 Sample ID: IA-2 (8-hr) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic 3 (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 1.4 1.1E+O1 8.3E+00 1.3E-07 3.4E-02 79-01-6 Trichloroeth lene 0.15 4.8E-01 4.2E-01 3.1E-07 7.2E-02 75-01-4 1 Vinyl Chloride 1.7E-01 I 2.1E+01 Cumulative: I 4.4E-07 I1.1E-01 DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 2/15/2019 Sample ID: IA-2 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic 3 (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 2.5 1.1E+O1 8.3E+00 2.3E-07 6.0E-02 79-01-6 Trichloroeth lene 1.6 4.8E-01 4.2E-01 3.3E-06 7.7E-Ol 75-01-4 Vinyl Chloride 1.7E-01 2.1E+01 Cumulative: I 3.6E-06 I8.3E-Ol DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 6/15/2018 Sample ID: IA-3 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic 3 (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 2.9 1.1E+O1 8.3E+00 2.7E-07 7.0E-02 79-01-6 Trichloroeth lene 4.8E-Ol 4.2E-Ol 75-01-4 Vinyl Chloride 1.7E-01 2.1E+01 Cumulative: I 2.7E-07 I7.0E-02 DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 12/21/2018 Sample ID: IA-3 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic 3 (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 5.9 1.1E+O1 8.3E+00 5.5E-07 1.4E-Ol 79-01-6 Trichloroeth lene 2.1 4.8E-Ol 4.2E-0] 4.4E-06 1.0E+00 75-01-4 Vinyl Chloride 1.7E-01 I 2.1E+01 Cumulative: I 4.9E-06 I1.1E+00 DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 1/18/2019 Sample ID: IA-3 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic 3 (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 2.3 1.1E+O1 8.3E+00 2.1E-07 5.5E-02 79-01-6 Trichloroeth lene 1.4 4.8E-01 4.2E-01 2.9E-06 6.7E-01 75-01-4 Vinyl Chloride 1.7E-01 2.1E+01 Cumulative: I 3.1E-06 I7.3E-Ol DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 1/11/2019 Sample ID: IA-3 (8-hr) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic 3 (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 1.4 1.1E+O1 8.3E+00 1.3E-07 3.4E-02 79-01-6 Trichloroeth lene 0.12 4.8E-01 4.2E-01 2.5E-07 5.8E-02 75-01-4 1 Vinyl Chloride 1.7E-01 I 2.1E+01 Cumulative: I 3.8E-07 I9.1E-02 DSCA Indoor Air Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 2/15/2019 Sample ID: IA-3 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic 3 (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 1.8 1.1E+O1 8.3E+00 1.7E-07 4.3E-02 79-01-6 Trichloroeth lene 1.6 4.8E-01 4.2E-01 3.3E-06 7.7E-Ol 75-01-4 1 Vinyl Chloride 1.7E-01 2.1E+01 Cumulative: I 3.5E-06 I8.1E-Ol DSCA Indoor Air Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 6/15/2018 Sample ID: IA-2 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/ms Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 2.8 4.7E+O1 3.5E+O1 5.9E-08 1.6E-02 79-01-6 Trichloroeth lene 3.0E+00 1.8E+00 75-01-4 Vinyl Chloride 2.8E+00 8.8E+01 Cumulative: I 5.9E-08 I1.6E-02 DSCA Indoor Air Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 12/21/2018 Sample ID: IA-2 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/ms Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 4.6 4.7E+O1 3.5E+O1 9.8E-OS 2.6E-02 79-01-6 Trichloroeth lene 1.9 3.0E+00 1.8E+00 6.4E-07 2.2E-Ol 75-01-4 1 Vinyl Chloride 2.8E+00 8.8E+01 Cumulative: I 7.3E-07 I2.4E-Ol DSCA Indoor Air Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 1/18/2019 Sample ID: IA-2 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/ms Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 2.6 4.7E+01 3.5E+01 5.5E-05 1.5E-02 79-01-6 Trichloroeth lene l.6 3.0E+00 1.8E+00 5.3E-07 1.8E-01 75-01-4 Vinyl Chloride 2.8E+00 I 8.8E+01 Cumulative: I 5.9E-07 I2.0E-Ol DSCA Indoor Air Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 1/18/2019 Sample ID: IA-2 (8-hr) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/ms Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 1.4 4.7E+01 3.5E+O1 3.0E-OS 8.0E-03 79-01-6 Trichloroeth lene F. 3.0E+00 1.8E+06 5.0E-08 1.7E-02 75-01-4 Vinyl Chloride 2.8E+00 I 8.8E+01 Cumulative: I 8.0E-08 I2.5E-02 DSCA Indoor Air Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 2/15/2019 Sample ID: IA-2 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/ms Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 2.5 4.7E+01 3.5E+01 5.3E-05 1.4E-02 79-01-6 Trichloroeth lene 1.6 3.0E+00 1.8E+00 5.3E-07 1.8E-Ol 75-01-4 Vinyl Chloride 2.8E+00 I 8.8E+01 Cumulative: I 5.9E-07 I2.0E-Ol DSCA Indoor Air Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 6/15/2018 Sample ID: IA-3 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/ms Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 2.9 4.7E+O1 3.5E+O1 6.1E-OS 1.7E-02 79-01-6 Trichloroeth lene 3.0E+00 1.8E+00 75-01-4 Vinyl Chloride 2.8E+00 8.8E+01 Cumulative: I 6.1E-08 I1.7E-02 DSCA Indoor Air Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 12/21/2018 Sample ID: IA-3 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/ms Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 5.9 4.7E+O1 3.5E+O1 1.3E-07 3.4E-02 79-01-6 Trichloroeth lene 2.1 3.0E+00 1.8E+00 7.0E-07 2.4E-Ol 75-01-4 1 Vinyl Chloride I 2.8E+00 I 8.8E+01 Cumulative: I 8.3E-07 I2.7E-Ol DSCA Indoor Air Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 1/18/2019 Sample ID: IA-3 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/ms Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 2.3 4.7E+O1 3.5E+O1 4.9E-OS 1.3E-02 79-01-6 Trichloroeth lene 1.4 3.0E+00 1.8E+00 4.7E-07 1.6E-Ol 75-01-4 Vinyl Chloride 2.8E+00 8.8E+01 Cumulative: I 5.2E-07 I1.7E-0 l DSCA Indoor Air Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 1/18/2019 Sample ID: IA-3 (8-hr) Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/ms Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 1.4 4.7E+01 3.5E+O1 3.0E-OS 8.0E-03 79-01-6 Trichloroeth lene 0.12 3.0E+00 1.8E+06 4.0E-08 1.4E-02 75-01-4 Vinyl Chloride I 2.8E+00 I 8.8E+01 Cumulative: I 7.0E-08 I2.2E-02 DSCA Indoor Air Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 2/15/2019 Sample ID: IA-3 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/ms Indoor Air Indoor Air Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Screening Level for Non- Calculated Carcinogenic s (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient THQ = 0.2 156-59-2 Dichloroeth lene, 1,2-cis- 156-60-5 Dichloroeth lene, 1,2-trans- 127-18-4 Tetrachloroeth lene 1.8 4.7E+O1 3.5E+O1 3.8E-OS 1.0E-02 79-01-6 Trichloroeth lene 1.6 3.0E+00 1.8E+00 5.3E-07 1.8E-Ol 75-01-4 Vinyl Chloride 2.8E+00 8.8E+01 Cumulative: I 5.7E-07 I1.9E-0 l DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 6/15/2018 Sample ID: SV-5 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m' Indoor Air Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Air Concentration Screening Level for Non- Calculated Carcinogenic (ug/m3) (ug/m3) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR = 1E-06 TH = 0.2 Quotient 156-59-2 Dichloroeth lene, 1,2-cis- 18000 540 156-60-5 Dichloroeth lene, 1,2-trans- 480 14.4 127-18-4 Tetrachloroeth lene 140000 4200 1.1E+01 8.3E+00 3.9E-04 1.0E+02 79-01-6 Trichloroeth lene 40000 1200 4.8E-01 4.2E-01 2.5E-03 5.8E+02 75-01-4 Vinyl Chloride 1.7E-01 2.1E+01 Cumulative: I 2.9E-03 I 6.8E+02 DSCA Soil Gas Risk Calculator - Cumulative Risk for Resident Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 12/19/2018 Sample ID: SV-5 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m' Indoor Air Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Air Concentration Screening Level for Non- Calculated Carcinogenic (ug/m3) (ug/m3) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR = 1E-06 TH = 0.2 Quotient 156-59-2 Dichloroeth lene, 1,2-cis- 9800 294 156-60-5 Dichloroeth lene, 1,2-trans- 390 11.7 127-18-4 Tetrachloroeth lene 120000 3600 1.1E+01 8.3E+00 3.3E-04 8.6E+01 79-01-6 Trichloroeth lene 24000 720 4.8E-01 4.2E-01 1.5E-03 3.5E+02 75-01-4 Vinyl Chloride 1.7E-01 2.1E+01 Cumulative: I 1.8E-03 I 4.3E+02 DSCA Soil Gas Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 6/15/2018 Sample ID: SV-5 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in us/ms Indoor Air Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Air Concentration Screening Level for Non - Calculated Carcinogenic a a (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient 156-59-2 Dichloroeth lene, 1,2-cis- 18000 180 156-60-5 Dichloroeth lene, 1,2-trans- 480 4.8 127-18-4 Tetrachloroeth lene I40000 1400 4.7E+01 3.5E+01 3.0E-05 8.0E+00 79-01-6 Trichloroeth lene 40000 400 3.0E+00 1.8E+00 1.3E-04 4.6E+01 75-01-4 Vinyl Chloride I I 2.8E+00 i 8.8E+01 Cumulative: I 1.6E-04 I 5.4E+01 DSCA Soil Gas Risk Calculator - Cumulative Risk for Non -Residential Worker Version 6, November 2017 DSCA ID No: DC680002 Name/Address of DSCA Site: American Dry Cleaners 201 S. Estes Drive, Chapel Hill, Orange County, NC Name/Address of Sampling Location: 1712 Willow Drive, Chapel Hill, Orange County, NC Sampling Date: 12/19/2018 Sample ID: SV-5 Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in us/ms Indoor Air Soil Gas Calculated Indoor Indoor Air Screening Level Calculated Non - CAS # Chemical Name: Concentration Air Concentration Screening Level for Non - Calculated Carcinogenic a a (ug/m) for Carcinogens Carcinogens @ Carcinogenic Risk Hazard @ TCR= 1E-06 Quotient 156-59-2 Dichloroeth lene, 1,2-cis- 9800 98 156-60-5 Dichloroeth lene, 1,2-trans- 390 3.9 127-18-4 Tetrachloroeth lene I20000 1200 4.7E+01 3.5E+01 2.5E-05 6.8E+00 79-01-6 Trichloroeth lene 24000 240 3.0E+00 1.8E+00 8.0E-05 2.7E+01 75-01-4 Vinyl Chloride I I 2.8E+00 i 8.8E+01 Cumulative: I 1.1E-04 I 3.4E+01 ATTACHMENT 17 INDOOR AIR SAMPLING BUILDING SURVEY FORMS AECOM Technical Services of North Carolina, Inc. PECOM Form adapted from NJDEP Guidance INDOOR AIR BUILDING SURVEY and SAMPLING FORM Preparer's name:S� -PA ( V'_ kNCW2 C_ Date: J;;� 1 y 1\8 Preparer's affiliation: AC^.('nA, \ Phone #: q�°� _ �--1(Q k Site Name: Ajnn,CNg1C pjj Ct_CA►JipS---,,S Case #: xpp a Part I - Occupants Building Address: tT}\Q tA3 j j 1 Qv,, �4 xi 4 NC1 t-A Property Contact: j-), )pT�,jr- Owner / Renter / other: 4\Agaa Contact's Phone: home ( ) work 6la) fILQ —1-19 cell ( ) # of Building occupants: Children under age 13 O Children age 13-18 Adults \S Part II — Building Characteristics Building type: residential / multi -family residential /office /strip mal commercia / industrial Describe building: C fl�_C_ �k \_31 Z F_ Year constructed: 'lq (01A— Sensitive population: day care / nursing home / hospital / school / other (specify): Type of construction: full basement / partial basement / walk -out basement / crawl space / ab on grade Slab description o=Ievel multiple levels / not applicable Number of floors below grade: () Number of floors at or above grade: Depth of basement below grade surface: ft. Basement size: ft? N\ A Basement floor construction: concrete / dirt / floating / stone / other (specify): } Foundation walls: poured concrete cinder blocks / stone / other (specify) Basement sump present? Yes /No Sump pump? Yes /No Water in sump? Yes /No JJ 1 A Elevator present? Yes/)DCo Type of heating system (circle all that apply): of air circulate hot air radiation wood steam radiation eat pum hot water radiation kerosene heater electric baseboard o r specify):} Type of ventilation system (circle all that apply): tral air condition g mechanical fans `bathroom ventilation fan individua ai on-ditioning units kitchen range hoo an ou si a -atr intake other (specify): Type of ' ' ed (cir all that apply): Natural g / (1_ectrfcy fuel oil / wood / coal / solar / kerosene Are the basement walls or floor sealed with waterproof paint or epoxy coatings? Yes /6 Is there a whole house fan? Yes No Septic system? Yes / Yes (but not used) No Irrigation/private well? Yes / Yes (but not used No Type of ground cover outside of building gras / concrete / spha / other (specify) tNa�_C!-1 %y,�, n�A_-,o N� Existing subsurface depressurization (radon) system in place? Yes No 1 active /passive Sub -slab vapor/moisture barrier in place? Yes o Type of barrier: — xrz, ma , (---§Zrz i 3x_Dei Ol s Part III - Outside Contaminant Sources Contaminated site (1000-ft. radius): F:c\C2, 'C>C' Other stationary sources nearby (gas stations, emission stacks, etc.): R\1f1 Heavy vehicular traffic nearby (or other mobile sources): Part IV — Indoor Contaminant Sources Identify all potential indoor sources found in the building (including attached garages) and the location of the source (floor and room). In the event these source(s) are removed prior to the indoor air sampling event please document accordingly. Any ventilation implemented after removal of the items should be completed at least 24 hours prior to the commencement of the indoor air sampling event. Potential Sources Location(s) Removed (Yes f No 1 NA) Gasoline storage cans Gas -powered equipment Kerosene storage cans Paints / thinners / strippers t-- Cleaning solvents Oven cleaners Carpet / upholstery cleaners Other house cleaning products Moth balls Polishes / waxes Insecticides Furniture / floor polish Nail polish / polish remover Hairspray Cologne / perfume Air fresheners Fuel tank (inside building) NA Wood stove or fireplace NA New furniture 1 upholstery New carpeting / flooring NA Hobbies - glues, paints, etc. 0 Part V — Miscellaneous Items Do any occupants of the building smoke? Yes No How often? Last time someone smoked in the building? hours /days ago Does the building have an attached garage directly connected to living space? Yes/'t�l If so, is a car usually parked in the garage? Yes !No ���� Are gas -powered equipment or cans of gasoline/fuels stored in the garage? Yes /No Do the occupants of the building have their clothes dry cleaned? Yes /No If yes, how often? weekly / monthly / 3-4 times a year Have the drapes, rugs, etc. been dry cleaned? Yes No Do any of the occupants use solvents in work? Yes No If yes, what types of solvents are used? If yes, are their clothes washed at work? Yes /& Have any pesticides/herbicides been applied around the building or in the yard? If so, when and which chemicals? Has there ever been a fire in the building? Yes /E O If yes, when? Has painting or staining been done in the building in the last 6 months? If yes, when Part VI — Sampling Information and where? Yes e Yes /6° Sample Technician: Phone number: &5 "(p \ - Sample Sourc : Indoor Ai / Sub -Slab / Near Slab Soil Gas / Exterior Soil Gas Sampler Type: Stainless Steel Canister / Other (specify): Rpc>j F-1 t L� Analytical Method: TO-15 SIM / TO-15 full scan / other:iRhi�� L-zh Cert. Laboratory: ('O�— 7 �'S Sample locations (floor, room): RovM 6 Field ID # III - 1 Oho t \3Field ID # i4<DC X\rl Field ID # Jg_ - 3 (�C>>}—T� Field ID # Were NJ DEP "Instructions for Occupants" followed? If not, describe modifications: es No 3 Provide Drawing of Sample Location(s) in Building Part VII - Meteorological Conditions Was there significant precipitation within 72 hours prior to (or during) the sampling event? OYesNo Describe the general weather conditions: ti 1a° F -IC- -Q,\14\tJL-a C0_ --,�t-c�4` Part VIII — General Observations Provide any information that may be pertinent to the sampling event and may assist in the data interpretation process. 4 DWM INDOOR AIR BUILDING SURVEY and SAMPLING FORM Site Name: �► c� �c Preparer's name: R Preparer's affiliation:��p Part I - Occupants Date: Phone #: Building Address: �v� Property Contact: -7 Owner / Renter / then �nL Contact's Phone: home ( ) work cell ( ) # of Building occupants: Children underage 13 -,-?c-z Children age 13-18 Adults; Part II — Building Characteristics Building type: residential / multi -family residential / office / strip mall / ommercia / industrial 1—S-t o2�, 3U-C k, SPL-) - L5_,,.1CL v Describe building: C 1�.�C .rl 1. _ Year constructed: Sensitive population: y car / nursing home / hospital / school / other (specify): Number of floors below grade: (full basement / crawl space / slab :ongra ) Number of floors at or above grade: _` Depth of basement below grade surface: ft. Basement size: ft �, R Basement floor construction: concrete / dirt / floating / stone / other (specify):$ Foundation walls: poured concrete / coder bloc / stone / other (specify) Basement sump present? Yes / No Sump pump? Yes / No Water in sump? Yes / No N1 (� Type o inMstem�circle all that apply): of ' ' ulati hot air radiation wood steam radiation eat pum hot water radiation kerosene heater electric baseboard other (specify)it{��a-. Type of v a system (ci�le all that apply): al air conditiomn mechanical fans bathroom ventilation fan individual air conditioning units kitchen range hood fan ou si other (specify): Type of d (circl ll that apply): Natural g / ect / fuel oil / wood / coal / solar / kerosene Are the basement walls or floor sealed with waterproof paint or epoxy coatings? Yes 18 Is there a whole house fan? Yes Co Septic system? Yes / Yes (but not used) No Irrigation/private well? Yes / Yes (but not used) No Type of ground cover outside of building: Cgr�as�s)(Fcrete)� �haltother (specify) Existing subsurface depressurization (radon) system in place? Yes / No , active /passive Sub -slab vapor/moisture barrier in place? Type of barrier: Part III - Outside Contaminant Sources Yes / No Other stationary sources nearby (gas stations, emission stacks, etc.): V Heavy vehicular traffic nearby (or other mobile sources): =, . - - Part IV — Indoor Contaminant Sources Identify all potential indoor sources found in the building (including attached garages), the location of the source (floor and room), and whether the item was removed from the building 48 hours prior to indoor air sampling event. Any ventilation implemented after removal of the items should be completed at least 24 hours prior to the commencement of the indoor air sampling event. Potential Sources Location(s) Removed (Yes / No / NA) Gasoline storage cans Gas -powered equipment Kerosene storage cans Paints / thinners / strippers Cleaning solvents Oven cleaners Carpet / upholstery cleaners Other housecleaning products Moth balls Polishes / waxes Insecticides Furniture / floor polish Nail polish / polish remover Hairspray Cologne / perfume Air fresheners Fuel tank (inside building) NA Wood stove or fireplace NA New furniture / upholstery New carpeting / flooring NA Hobbies - glues, paints, etc. — -Z J fvC' Part V - Miscellaneous Items Do any occupants of the building smoke? Yes / No How often? Last time someone smoked in the building? hours / days ago Does the building have an attached garage directly connected to living space? Yes /(A' If so, is a car usually parked in the garage? Yes / No Are gas -powered equipment or cans of gasoline/fuels stored in the garage? Yes / No Do the occupants of the building have their clothes dry cleaned? (�e-s % No If yes, how often? weekly / monthly / 3-4 times a year yCz, Do any of the occupants use solvents in work? Yes :1Vo If yes, what types of solvents are used? If yes, are their clothes washed at work? Yes / No Have any pesticides/herbicides been applied around the building or in the yard? Yes 1. If so, when and which chemicals? �^ Has there ever been a fire in the building? Yes / No . If yes, when? Has painting or staining been done in the building in the last 6 months? Yes 146 If yes, when and where? Part VI - Sampling Information Sample Technician: S. _tAeC,;\(xz , _ Phone number: I )��15 _ - - 35p Sample Source: Indoor A / Sub -Slab / Near Slab Soil Gas / Exterior Soil Gas Sampler Type: Tedlar bag / Sorbent /, Stainless Steel Canister / Other (specify): 1`2" \ !1'1-L- C--� Analytical Method: 0-15 TO-17 / other: Sample locations (floor, room): Field ID # _LE�s_ - Field ID # i �� - -3 Were "Instructions for Occupants" followed? If not, describe modifications: P V Cert. Laboratory: Field ID # I P�` - a_ ( R - 1� \2D� Field ID # 1 P) - 3 L 8 — P, Yes I No Provide Drawing of Sample Location(s) in Building LOB- f\ —\ \ o ZJ S CSC Hcx> k.-S FoC c s C, -k 8) Part VII - Meteorological Conditions Was there significant precipitation within 12 hours prior to (or during) the sampling event? Yes No Describe the general weather conditions: -,/ ' O - L SM Pk2� C c., mil_ a aFM\-X-K-Z'■ - y Part VIII - General Observations Provide any information that may be pertinent to the sampling event and may assist in the data interpretation process. (Adapted from the NJDEP Vapor Intrusion Guidance, October 2005) AECOM Technical Services of North Carolina, Inc. PECOM Form adapted from NJDEP Guidance INDOOR AIR BUILDING SURVEY and SAMPLING FORM Preparer's name: �7 ; F��rll�ll�^� j�41Q4� Date: 10t Preparer's affiliation: _ [��Y\ Phone #: Site Name: Case #: Part I - Occupants Building Address: Property Contact: Owner 1 Renter / ther i3�����_[,� Contact's Phone: home ( ) work 6t5) cell ( ) # of Building occupants: Children under age 13 L,-LU Children age 13-18 Adults .,_ � Part II - Building Characteristics Building type: residential / multi -family residential / office / strip mall 1 ommercia / industrial Describe building: 1 15.U)a�-\ t�� ,1Et)cAgV Year constructed: Sensitive population: ay car nursing home / hospital / school / other (specify): Type of construction: full basement / partial basement / walk -out basement / crawl space 1 ab on grade Slab description: n71eve� multiple levels / not applicable �S('�-� -L-�\J C L' t -S %0� Number of floors below grade: () Number of floors at or above grade: Depth of basement below grade surface: ft. Basement size: ftz A Basement floor construction: concrete / dirt / floating / stone / other (specify):{ Foundation walls: poured concrete / nder block / stone / other (specify) Basement sump present? Yes No Sump pump? Yes No Water in sump? Yes/ Elevator present? Ye 10 Type of heatin s stem (circle all that apply): hot • ircul hot air radiation wood steam radiation ea p hot water radiation kerosene heater electric baseboard specify): ZCo \ L 42, 1 r l Type o4inivi lations stem (circle all that apply): al air conditio ing mechanical fans athroom ventilation f ns ua air conditioning units kitchen range hoo an outside air intake other (specify): Type of fuel utilized (cir le all that apply): atural g 1 ect 1 fuel oil / wood / coal / solar / kerosene Are the basement walls or floor sealed with waterproof paint or epoxy coatings? Yes Is there a whole house fan? Yes I/ 0 J Septic system? Yes I Yews (but not used) No Irrigation/private well? Yes 1 Yes (but not used) Type of ground cover outside of buildin . gras / oncre aspha / other (specify) Existing subsurface depressurization (radon) system in place? Yes 1F) Sub -slab vapor/moisture barrier in place? Yes I(!57) Type of barrier: Part III - Outside Contaminant Sources Contaminated site (1000-ft. radius): Other stationary sources nearby (gas stations, emission stacks, etc.):tl� Heavy vehicular traffic nearby (or other mobile sources): Part IV — Indoor Contaminant Sources active 1 passive Identify all potential indoor sources found in the building (including attached garages) and the location of the source (floor and room). In the event these source(s) are removed prior to the indoor air sampling event please document accordingly. Any ventilation implemented after removal of the items should be completed at least 24 hours prior to the commencement of the indoor air sampling event. Potential Sources Location(s) Removed (Yes / No / NA) Gasoline storage cans Gas -powered equipment Kerosene storage cans Paints / thinners / strippers Cleaning solvents 2 VSA_ C. i d Oven cleaners Carpet / upholstery cleaners Other house cleaning products Moth balls Polishes / waxes Insecticides Furniture / floor polish Nail polish / polish remover Hairspray Cologne / perfume Air fresheners Fuel tank (inside building) NA Wood stove or fireplace NA New furniture / upholstery New carpeting / flooring NA Hobbies - glues, paints, etc. -- N 2 Part V — Miscellaneous Items Do any occupants of the building smoke? Yes No How often? Last time someone smoked in the building? hours 1 days ago Does the building have an attached garage directly connected to living space? Yes 10 If so, is a car usually parked in the garage? Yes /No Are gas -powered equipment or cans of gasoline/fuels stored in the garage? Yes I No Do the occupants of the building have their clothes dry cleaned? Yey No If yes, how often? weekly / monthly / 3-4 times a year Have the drapes, rugs, etc. been dry cleaned? Yes S Do any of the occupants use solvents in work? Yes No If yes, what types of solvents are used? If yes, are their clothes washed at work? Yes I No Have any pesticides/herbicides been applied around the building or in the yard? Yes /(S If so, when and which chemicals? Has there ever been a fire in the building? Yes I6) If yes, when? Has painting or staining been done in the building in the last 6 months? Yes /0 If yes, when and where? Part VI — Sampling Information Sample Technician: -ram, yvzs,�\P _ �_ Phone number: An LN(,, 1 - t!ZQ <- Sample Source ndoor Ai / Sub -Slab / Near Slab Soil Gas / Exterior Soil Gas Sampler Type: Stainless Steel Canister / Other (specify): Analytical Method: TO-] 5 SIM / TO-15 full scan / other: D \ Cert. Laboratory: Sample locations (floor, room): Field ID # I F - - a Field ID # Field ID # 11� - 3 Field ID # Were NJ DEP "Instructions for Occupants" followed? (Ees!y No If not, describe modifications:._ _ b£C 0( �5 3 Provide Drawing of Sample Location(s) in Building SCC S1 k C- NNP P — �00 MS g Part VII - Meteoroloizical Conditions Was there significant precipitation within 72 hours prior to (or during) the sampling event? P No Describe the general weather conditions: z; kb PBiCc\ ( � \c)R —\ c�, P15, IMP o-LNn . — (a �" ;= e o<-X�LC7--,%s Mc - Part VIII — General Observations Provide any information that may be pertinent to the sampling event and may assist in the data interpretation process. 4 ATTACHMENT 18 MANN-KENDALL TREND ANALYSIS MANN-KENDALL TOOLKIT for Constituent Trend Analysis Evaluation Date: I March 2019 Job ID: 60566538 Facility Name: JAmerican Dry Cleaners (DC680002) Constituent: PC Conducted By: AECOM Concentration Units: mg/L Sampling Point ID: MW-2 MW-3 2W-5 2W-6 2W-9 2W-10 2W-11 .. - 1 09/23/08 40.7 5.134 2 01/30/09 31.57 3.073 0.991 0.903 3 10/21/10 4.63 1.89 1.95 0.427 4 01/21/11 40.4 1.86 4.15 0.346 5 04/29/11 48.4 1.42 3.35 3.41 6 07/18/11 34.0 1.3 3.4 3.00 7 08/30/11 40.0 1.8 0.082 2.90 8 09/22/11 30.0 1.7 0.65 1.70 9 10/18/11 0.125 2.5 0.005 2.50 10 11/18/11 40.0 4.4 0.0025 1.80 11 02/23/12 37.0 4.1 0.005 2.60 12 05/24/12 37.0 3.3 0.0005 3.0 13 09/04/12 35.0 6.6 0.0005 0.84 14 11/12/13 43.0 5.9 2.10 15 07/08/14 0.47 7.2 2.9 16 11/23/15 13.9 1.58 0.0005 0.316 3.1 0.312 17 12/12/16 0.62 0.22 0.053 0.074 18 12/19/18 14.2 0.176 0.0482 0.0178 19 20 Red text indicates one-half of laboratory detection limit. Coefficient of Variation: Mann -Kendall Statistic (S): Confidence Factor: Concentration Trend: 100 M W-2 10 BMW-3 J -2W-5 E 1 0oo, _zw-5 v 2W-9 C O 0.1 -zw-io M-2W-11 0.01 O U c 0.001 _ O C) 0.0001 02108 07/09 11/10 04/12 08113 12114 05116 09117 02119 06120 Sampling Date Notes: 1. At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples. 2. Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing; >_ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S50, and COV >_ 1 = No Trend; < 90% and COV < 1 = Stable. 3. Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales, Ground Water, 41(3):355-367, 2003. DISCLAIMER: The GSI Mann -Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product, however, no party, including without limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein. GSI Environmental Inc., www.gsi-net.com MANN-KENDALL TOOLKIT for Constituent Trend Analysis Evaluation Date: I March 2019 Job ID: 60566538 Facility Name: JAmerican Dry Cleaners (DC680002) Constituent: TCE Conducted By: AECOM Concentration Units: mg/L Sampling Point ID: MW-2 MW-3 2W-5 2W-6 2W-9 2W-10 2W-11 1 09/23/08 1.208 0.73 2.55 2 01/30/09 1.886 0.629 0.429 0.21000 3 10/21/10 0.451 0.392 0.399 0.214 4 01/21/11 3.1 0.408 1.77 0.33 5 04/29/11 2.76 0.319 1.63 0.316 6 07/18/11 2.6 0.42 0.990 0.350 7 08/30/11 3.6 0.51 0.280 0.320 8 09/22/11 2.4 0.53 0.320 0.190 9 10/18/11 0.125 0.67 0.005 0.250 10 11/18/11 3.2 0.96 0.0025 0.220 11 02/23/12 3.0 1.1 0.005 0.240 12 05/24/12 2.6 1.6 0.001 0.250 13 09/04/12 2.5 1.9 0.001 0.280 14 11/12/13 2.9 0.73 0.890 15 07/08/14 0.140 0.24 3.5 0.69 16 11/23/15 1.36 0.335 0.00108 0.129 4.27 2.26 17 12/12/16 0.21 0.11 0.049 0.21 18 12/19/18 1.69 0.0862 0.036 0.0121 19 20 Red text indicates one-half of laboratory detection limit. Coefficient of Variation: I Mann -Kendall Statistic (S): Confidence Factor: Concentration Trend: - 10 M W-2 BMW-3 J 1 -2W-5 _2W-5 0.1^2W-9 C O -zw-io 0.01 -2W-11 C O 0.001 O C) 0.0001 02108 07109 11/10 04/12 08113 12114 05116 09117 02/19 06120 Sampling Date Notes: 1. At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples. 2. Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing; >_ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S50, and COV >_ 1 = No Trend; < 90% and COV < 1 = Stable. 3. Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales, Ground Water, 41(3):355-367, 2003. DISCLAIMER: The GSI Mann -Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product, however, no party, including without limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein. GSI Environmental Inc., www.gsi-net.com