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HomeMy WebLinkAbout23052_Southern Steel_Haz Treatment WP_DEQ Approval 2021.03.31.docx March 31, 2021 Sent Via E-mail Bo Cappleman Hart & Hickman 2923 South Tryon St, Suite 100 Charlotte, NC 28203 rcappleman@harthickman.com Subject: Hazardous Soil Removal & Treatment Work Plan Approval Former Southern Steel Facility Charlotte, Mecklenburg County Brownfields Project No. 23052-19-060 Dear Mr. Bo Cappleman: The North Carolina Department of Environmental Quality (DEQ) Brownfields Program received the Hazardous Soil Removal and Treatment Work Plan dated March 30, 2021 Work Plan). DEQ Brownfield comments to previous revisions dated March 18, 2021 of this Work Plan have been addressed; therefore, the Work Plan is approved. OR simply: The Work Plan has been reviewed and is approved. Please be advised that this approval from DEQ Brownfields does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local entities. If you have any questions, please feel free to contact me at 704-661-0330, or via e-mail at Carolyn.Minnich@ncdenr.gov. Sincerely, Carolyn Minnich Brownfields Project Manager ec: Travis Thomas travis.thomas@robyhome.com Trent Haston Trent.Haston@andrewroby.com Chris S. Walker chris.walker@alexanderricks.com Ms. Carolyn Minnich March 30, 2021 Page 2 S:\AAA-Master Projects\Roby Realty (ANR)\ANR-007 - 3015 Wilkinson Blvd (former Southern Steel)\Soil Stabilization Work Plan\Hazardous Soil Removal & Treatment Work Plan - Southern Steel (3-30-21).doc In March 2019, H&H performed soil sampling as part of a Phase II Environmental Site Assessment. Lead was detected in four soil samples that were collected in the central and western portions of the Site at concentrations above the DEQ Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs). Lead detections in the samples were sufficiently high such that waste characterization sampling was warranted. Therefore, in September and October 2019, H&H performed soil characterization sampling at the Site to evaluate soil conditions in areas that may be disturbed during grading activities associated with the proposed Site redevelopment. Laboratory analytical results indicated the presence of lead in leachate from composite soil samples B1-A (13.5 mg/L), B1-B (26.0 mg/L), Comp-1 (11.4 mg/L), and Comp-3 (5.8 mg/L) at concentrations above the Environmental Protection Agency (EPA) Toxicity Characteristic Leaching Procedure (TCLP) regulatory level of 5.0 mg/L. Based on the TCLP lead data and recent civil engineering plans which depict the proposed warehouse buildings, characteristically hazardous soil may be present in an approximate 0.3-acre area to a depth of at least 4 feet below ground surface (ft bgs) within and adjacent to the west, north, and east of the proposed Building 1 in the western portion of the Site (see Figure 2). TCLP data from the September and October 2019 soil characterization sampling is summarized in Table 1. An Environmental Management Plan (EMP) was executed for the Site on March 5, 2021. The EMP designated the approximate 0.3-acre area containing characteristically hazardous soil as “Area 1.” Soil within Area 1 that is disturbed during redevelopment activities will be managed in accordance with protocol outlined in the following section. 2.0 Scope of Work 2.1 Soil Removal and Stockpiling Based on the proposed Site redevelopment plans, soil within Area 1 will be disturbed during grading, installation of aggregate piers, construction of foundation footers, and installation of subgrade utilities. As such, H&H will utilize a submeter global positioning system (GPS) device to mark the perimeter of Area 1 using wooden stakes and flagging so that soil removed from Ms. Carolyn Minnich March 30, 2021 Page 3 S:\AAA-Master Projects\Roby Realty (ANR)\ANR-007 - 3015 Wilkinson Blvd (former Southern Steel)\Soil Stabilization Work Plan\Hazardous Soil Removal & Treatment Work Plan - Southern Steel (3-30-21).doc Area 1 can be properly segregated and stockpiled in accordance with Figure 1 of the DEQ- approved EMP (NCBP Diagram for Temporary Containment of Impacted or Potentially Impacted Soil). The proposed stockpile location is depicted on Figure 2; however, please note that this location is subject to change based on Site conditions at the time of stockpiling (i.e., due to equipment staging areas, construction traffic, etc.). The soil stockpile will include soil from depth intervals that were not previously tested by TCLP. For example, initial grading will include the removal of the top 6 to 12 inches of organic-rich soil along Area 1, and installation of aggregate piers will generate soil cuttings from depths of approximately 0 to 20 ft bgs. Therefore, the soil removed and stockpiled from Area 1 will be characterized as described below to evaluate the extent of treatment via lead stabilization that will be required. Upon completion of soil excavation activities in Area 1, the soil stockpile will be subdivided into approximate 100 cubic yard sections. One composite soil sample (consisting of five evenly spaced sample aliquots) will be collected per approximately 100 cubic yard section using a decontaminated stainless steel hand auger or trowel. Each composite soil sample will be thoroughly homogenized in a stainless steel or glass bowl prior to placement in dedicated laboratory-supplied sample containers, which will be labeled with the sample identification, date, and requested analysis, and placed in a laboratory-supplied cooler with ice. The samples will be delivered to a North Carolina-certified laboratory under standard chain-of-custody protocols and analyzed for total lead by EPA Method 6020. If the results of total lead analysis indicate potentially hazardous levels of lead in a sample based on the “Rule of 20” (i.e., greater than 100 mg/kg), the sample will be analyzed for TCLP lead by EPA Method 6020 to confirm which portions of the stockpile contain characteristically hazardous levels of lead. The total lead data will also be compared to the DEQ Residential and Non-Residential Preliminary Soil Remediation Goals (PSRGs) to evaluate whether the material will require an impervious cap or placement of two feet of clean fill on top of the soil after placement in other areas of the Site. If the location of soil disposition is not covered with an impervious surface, the soil conditions will be further evaluated during final grade sampling. Ms. Carolyn Minnich March 30, 2021 Page 4 S:\AAA-Master Projects\Roby Realty (ANR)\ANR-007 - 3015 Wilkinson Blvd (former Southern Steel)\Soil Stabilization Work Plan\Hazardous Soil Removal & Treatment Work Plan - Southern Steel (3-30-21).doc TCLP analytical data will be compared to the EPA TCLP regulatory level of 5.0 mg/L. If lead is not detected in composite sample leachate at a concentration above 5.0 mg/L, then the soil from the corresponding stockpile section will be placed in an area of the Site that requires fill material. The locations(s) of Area 1 soil disposition have not yet been determined but will be surveyed in the field and added to the Brownfields Plat. A cut/fill analysis which depicts fill areas (i.e., potential areas of soil disposition) is included as Appendix A. Portions of the soil stockpile where lead is detected in composite sample leachate at concentrations above the EPA TCLP regulatory level of 5.0 mg/L will be treated by lead stabilization as described below. 2.2 Soil Amendment Bench Testing Soil stabilization will be conducted by mixing EnviroBlend, Free Flow, or an equivalent lead- stabilizing amendment with the impacted soil on-Site at the proposed stockpile location in the southeastern portion of the Site (see Figure 2). The blending compound is a magnesium oxide powder blend that stabilizes and binds soil metals to reduce metal leachability and render the soil non-hazardous prior to placement in a designated area on the Site or transporting off-Site to a permitted Subtitle D Landfill for disposal as non-hazardous waste. Prior to conducting soil removal and stabilization activities, a bench test will be conducted by the compound manufacturer to determine the proper dosage of amendment to use during stabilization activities. H&H will provide a soil sample from the location exhibiting the highest TCLP lead concentration detected in the hazardous soil stockpile for the bench testing. Based on the bench test results, the recommended amount of amendment measured in percent by weight will be added to the soil stockpile and mixed as discussed below. EnviroBlend and Free Flow product specifications is provided in Appendix B. Ms. Carolyn Minnich March 30, 2021 Page 5 S:\AAA-Master Projects\Roby Realty (ANR)\ANR-007 - 3015 Wilkinson Blvd (former Southern Steel)\Soil Stabilization Work Plan\Hazardous Soil Removal & Treatment Work Plan - Southern Steel (3-30-21).doc 2.3 Soil Stabilization During stabilization activities, H&H will direct the contractor to mix soil within the stockpile using an excavator. Prior to and during excavation and mixing, the soil will be dampened with a mist or fine spray to mitigate dust emissions. After blending of the amendment and soils is completed, the stabilized material will remain in place, and confirmation samples will be collected as described below. After confirmation sampling, the treated soil will be covered with plastic and protected from rainfall to prevent run- off while awaiting confirmation sampling results. 2.4 Post-Stabilization Soil Sampling Upon completion of treatment activities, H&H will collect confirmatory samples to confirm that the soil has been treated to non-hazardous lead levels. The treated soil stockpile will be subdivided into approximate 100 cubic yard sections. Post-treatment confirmation samples will be collected with a decontaminated stainless steel hand auger or trowel at a rate of one composite sample (consisting of five evenly spaced sample aliquots) per approximately 100 cubic yard section. Each composite soil sample will be thoroughly homogenized in a stainless steel or glass bowl prior to placement in dedicated laboratory-supplied sample containers, which will be labeled with the sample identification, date, and requested analysis, and placed in a laboratory- supplied cooler with ice. The samples will be delivered to a North Carolina-certified laboratory under standard chain-of-custody protocols and analyzed for TCLP lead by EPA Method 6020 to confirm that lead is not detected above the EPA TCLP regulatory level of 5.0 mg/L. If lead is detected in the leachate at a concentration below 5.0 mg/L, no further treatment or sampling will be performed. 2.5 Quality Assurance/Quality Control Non-dedicated equipment and tools will be decontaminated prior to use at each sampling location or following exposure to soil. For quality assurance and quality control purposes Ms. Carolyn Minnich March 30, 2021 Page 6 S:\AAA-Master Projects\Roby Realty (ANR)\ANR-007 - 3015 Wilkinson Blvd (former Southern Steel)\Soil Stabilization Work Plan\Hazardous Soil Removal & Treatment Work Plan - Southern Steel (3-30-21).doc (QA/QC), H&H will duplicate soil samples for TCLP lead analysis by EPA Method 6020 during pre-stabilization and post-stabilization soil sampling (two total duplicate samples). Duplicate soil samples will be collected at a rate of one per 20 samples per day. Laboratory QA/QC procedures will be employed to ensure appropriate sample handling and analysis and to aid in the review and validation of the analytical data. QA/QC procedures will be conducted in accordance with the method protocols and will include regular equipment maintenance, equipment calibrations, and adherence to specific sample custody and data management procedures. Samples will be analyzed in conjunction with appropriate blanks, laboratory duplicates, continuing calibration standards, surrogate standards, and matrix spiking standards in accordance with approved methodologies to monitor both instrument and analyst performance. H&H will request that the laboratory reporting limits be equal to or below applicable screening criteria. Additionally, H&H will request that the laboratory include estimated concentrations for compounds that are detected at levels above the laboratory method detection limit, but below the laboratory reporting limit (J Flags). 2.6 Treated Soil Disposition Option 1: After the impacted soil has been determined to be non-hazardous based on confirmation sampling results, the treated soil will be placed in a designated area which will be surveyed in the field and depicted on the Brownfields survey plat. The area(s) and depth of soil placement have not yet been determined, but areas could include paved parking areas or driveways, beneath building foundations, or unpaved areas. Option 2: Alternatively, the stabilized soil will be transported to a Subtitle D landfill (likely the Republic Services landfill in Concord, North Carolina) for disposal. A non-hazardous waste profile will be completed and submitted to the disposal facility. The soil will be loaded onto trucks at the stockpile location and transported for disposal at the waste disposal facility. H&H will maintain Ms. Carolyn Minnich March 30, 2021 Page 7 S:\AAA-Master Projects\Roby Realty (ANR)\ANR-007 - 3015 Wilkinson Blvd (former Southern Steel)\Soil Stabilization Work Plan\Hazardous Soil Removal & Treatment Work Plan - Southern Steel (3-30-21).doc copies of disposal manifests and certified weight tickets for each truckload of stabilized material that is hauled off for disposal. 2.7 Reporting Following completion of the proposed activities, H&H will document the soil treatment and placement activities in a report. The report will include a description of the stockpile sampling activities, the laboratory analytical reports, a figure depicting sample locations and the final soil disposition location, a tabular summary and discussion of the analytical data in comparison to regulatory screening levels, the quantity of soil excavated, the quantity of soil treated, field logs, a photograph log, laboratory analytical data with chain of custody records, and conclusions concerning our activities. A DEQ Brownfields-approved EMP is in place for the Site and proposed redevelopment activities are anticipated to begin in the near term. We appreciate your prompt review of this Work Plan. Should you have any questions or need additional information, please do not hesitate to contact us at (704) 586-0007. Sincerely, Hart & Hickman, PC Bo Cappleman, PG Christine E. Schaefer Due Diligence Manager Senior Project Environmental Scientist Attachments cc: Mr. Trent Haston, Wilkinson Steel Yard, LLC Tables Table 1 Summary of Composite Soil Sample Analytical Results Former Southern Steel Facility Brownfields Project No. 23052-19-060 3015 Wilkinson Boulevard Charlotte, North Carolina H&H Job No. ANR-007 Area of Site Sample ID B1-A B1-B B1-C B2-A B2-B B2-C B3-A B3-B B3-C Comp-1 Comp-2 Comp-3 Comp-4 Comp-5 Comp-6 Sample Date 9/24/2019 9/24/2019 9/24/2019 9/24/2019 9/24/2019 9/24/2019 9/24/2019 9/24/2019 9/24/2019 10/30/2019 10/30/2019 10/30/2019 10/30/2019 10/30/2019 10/30/2019 Sample Type Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Composite Sample Depth (ft bgs)0-4 0-4 0-4 0-4 0-4 0-4 0-4 0-4 0-4 0-4 0-4 0-4 0-4 0-4 0-4 Metals (6010D/7470A TCLP) Arsenic <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 0.0070 J 0.016 J <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 5.0 Barium 0.51 0.53 0.53 0.95 0.59 0.70 0.50 0.41 0.52 0.90 0.75 0.76 0.90 0.63 0.72 100 Cadmium 0.0015 J 0.0015 J 0.0013 J <0.00040 0.0040 J 0.0043 J 0.0028 J 0.0050 <0.00040 0.0054 0.0036 J 0.0028 J 0.0034 J 0.0030 J 0.0036 J 1.0 Chromium (total)<0.0010 0.0038 J <0.0010 <0.0010 0.0044 J <0.0010 <0.0010 0.0020 J <0.0010 0.031 J 0.015 J 0.011 J 0.011 J 0.025 J 0.0057 J 5.0 Lead 13.5 26.0 4.3 0.78 0.43 2.2 0.19 0.13 0.017 J 11.4 4.5 5.8 4.0 1.8 2.5 5.0 Mercury <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 0.2 Selenium <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 0.0056 J <0.0047 <0.0047 <0.0047 <0.0047 <0.0047 0.0078 J 0.024 J <0.0047 0.0088 J 1.0 Silver <0.0025 <0.0025 <0.0025 0.0028 J <0.0025 <0.0025 0.0042 J 0.0031 J <0.0025 <0.0025 <0.0025 <0.0025 <0.0025 <0.0025 <0.0025 5.0 Laboratory analytical methods are shown in parentheses. Notes 1) EPA Maximum Concentration of Contaminants for Toxicity Characteristic Leaching Procedure (TCLP) regulatory level (November 2004). J = estimated concentration above the laboratory method detection limit but below the laboratory reporting limit Soil concentrations are reported in miligrams per liter (mg/L). Compound concentrations are reported to the laboratory method detection limit. Bold indicates an exceedance of EPA's Maximum Concentration of Contaminants for TCLP regulatory level. ft bgs = feet below ground surface Proposed Building No. 1 Proposed Building No. 2 Proposed Building No. 3 EPA TCLP Regulatory Level (mg/L)1 Area Between Proposed Building Nos.1 and 2 S:\AAA-Master Projects\Roby Realty (ANR)\ANR-007 - 3015 Wilkinson Blvd (former Southern Steel)\Soil Assessment\Tables\Soil Table 2/13/2020 Table 1 Hart & Hickman, PC Figures 0 2000 4000 APPROXIMATE SCALE IN FEETN U.S.G.S. QUADRANGLE MAP QUADRANGLE 7.5 MINUTE SERIES (TOPOGRAPHIC) CHARLOTTE WEST, NORTH CAROLINA 1996 TITLE PROJECT SITE LOCATION MAP FORMER SOUTHERN STEEL FACILITY3015 WILKINSON BOULEVARDCHARLOTTE, NORTH CAROLINA DATE: JOB NO: REVISION NO: FIGURE: 2-12-20 0 1ANR-007 SITE ANDREW JACKSON HIGHWAY ASHLEY ROAD ASHLEY ROADASHLEY ROADASHLEY ROAD WILKINSON BOULEVARD WEYLAND AVENUEREVISION NO. 0 JOB NO. ANR-007 DATE: 3-10-21 FIGURE NO. 2 FORMER SOUTHERN STEEL FACILITY 3015 WILKINSON BOULEVARD CHARLOTTE, NORTH CAROLINA SITE MAP LEGEND SITE PROPERTY BOUNDARY RAILROAD TRACKS COMPOSITE SOIL BORING APPROXIMATE EXTENT OF HAZARDOUS LEVELS OF LEAD AT 0-4 FT BGS (AREA 1) PROPOSED BUILDING FOOTPRINT COMP-1 COMP-3 B1-B B1-A B1-A-2 B1-A-3 B1-A-4 B1-B-1 B1-B-3 B1-B-2 B1-B-4 A B DC A B DC B1-A-1 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) License # C-1269 / #C-245 Geology NOTES 1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG COUNTY GIS. 2. ONLY SOIL SAMPLE LOCATIONS INDICATING LEAD IN LEACHATE AT CONCENTRATIONS ABOVE THE ENVIRONMENTAL PROTECTION AGENCY TOXICITY CHARACTERISTIC LEACHING PROCEDURE REGULATORY LEVEL ARE SHOWN. 3. COMPOSITE SAMPLES ARE COMPRISED OF SOIL ALIQUOTS FROM 0-2 FEET BELOW GROUND SURFACE (BGS) AND 2-4 FEET BGS FROM EACH COMPOSITE SOIL BORING IN EACH AREA. 4. SAMPLE LOCATIONS ESTIMATED USING TRIMBLE GPS. 5. PROPOSED REDEVELOPMENT PLAN WAS PREPARED BY AMERICAN ENGINEERING ASSOCIATES - SOUTHEAST P.A. AND PROVIDED BY THE PROSPECTIVE DEVELOPER.ASHLEY ROADASHLEY ROAD WILKINSON BOULEVARD WEYLAND AVENUEQUIKTRIP (3025 WILKINSON BLVD) MECKLENBURG COUNTY ABC (2915 WILKINSON BLVD) MECKLENBURG COUNTY SCHOOLS B U S MAINTENANCE FACILITY (3101 WILKINSON BLVD) EASTWAY WRECKER SERVICES (2801 WILKINSON BLVD) MULTI-TENANT STRIP MALL SHELL GAS STATION (3000 WILKINSON BLVD) BAR-B-Q KING (2900 WILKINSON BLVD) PARKER VETERINARY HOSPITAL (2820 WILKINSON BLVD) QUICK AUTO SALES (2926 WILKINSON BLVD) PROPOSED BUILDING 1 PROPOSED BUILDING 2 PROPOSED BUILDING 3 A DC B PROPOSED SOIL STOCKPILE AND BLENDING AREA S:\AAA-Master Projects\Roby Realty (ANR)\ANR-007 - 3015 Wilkinson Blvd (former Southern Steel)\Soil Stabilization Work Plan\Figures\Site and Sample Location Map.dwg, 3/11/2021 10:04:26 AM, DWG To PDF.pc3 Appendix A Cut/Fill Analysis PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCE PCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCE P C C E P C C E PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCE PCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOE OE OE OE OE OE OEOEOEOE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEG G G G G G G G G G G G G G G G G G G G G G G G G G G G GGGGGGGGGGGGGGGW W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W W DYH OEOEOEOEOE OE OE OE OE OE OE OE OE OE OE OEOEOEOEG WWWWSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSOEOEOEEX. 15" RCP EX. 15" RCPEX. 18" RCP OE OE OE OE OE OE OE OE OE OE OE OE OEOEOEOEOEOEOEOE OEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE OE PCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCEPCCE50' EX. R/WDAVID L. WILLIAMS D.B. 11826, PG. 825 TAX PARCEL #117-011-15 EX. 30"RCP LP 10'x70'35'x35'10'x70'35 ' x 3 5 ' 35'x35' 10'x70'35'x35'10'x70' 20' TRANSITIONAL SETBACK Concrete PARCEL 1 QUIKTRIP CORPORATION MB. 54, PG. 565 DB. 29066, PG. 563 TAX PARCEL #11701122 TOTAL AREA: 118,875 SF (2.73 AC)N01°45'56"E 144.08'S03°19'33"W 144.02'PP EX. 30" Curb & GutterEX. 30" RCP EX. Concrete Sidewalk 75' FUTURE R/WWMWM OE OE OE OE OE OE OE OE OE OE OE OE OE OE EX. 36"RCPEX. 36"RCP E X . 1 8 " R C P SSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSSLP 8" TERROEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEOEAsphalt FH SS SS S03°19'33"W 608.56'(TOTAL)EXISTING REGIONALSTORMWATERMANAGEMENT BASINDRY DETENTIONPP LOT 1 MB 61, PG 61 MECKLENBURG COUNTY ABC DB. 30170, PG. 567 TAX PARCEL #11701122 EX . P D E S03°24'51"W 337.71'2 0 ' T R A N S I T I O N A L S E T B A C K PARCEL 4 MB 57, PG 114 WILKINSON HOLDINGS I, LLC DB. 27179, PG. 152 TAX PARCEL #11701124 TOTAL AREA: 39,028 SF (0.896 AC) FUTURE RIGHT-OF-WAY9,971 SF (0.229 AC)S12°28'49"E 143 .01 '(TOTAL)S86°35'09"W 120.50' S86°35'09"W 323.33'S86°35'09"W 288.32' N86°38'06"W 43.11' TOP OF BANK FIELD LOCATED EX. HEADWALL N88°05'56"W 651.56' N88°05'56"W 109.64' S76°00'03 " W 2038.30' G R O U N D 2037.98' G R I D NGS MONUMENT "254 AZ MK" NC GRID NAD83 N: 541,723.45 FT (37.5984387° / 37°35'54.3 8 " N ) E: 1,437,993.26 FT (84.0318138° / -84°01'54 . 5 3 " E ) CGF: 0.99984316 CONTROL CORNER NC CORNER NAD83 N: 541,230.37 (37.5984387° / 37°35'34.62 " N ) E: 1,436,015.50 (-84.0331665° / 84°01'59 . 4 " E )EX. 54" CMPCONTROL CORNER NC CORNER NAD83 N: 541,255.63 E: 1,435,254.72 S 2 4 ° 5 6 '2 2 " E 25 0 . 0 1 ' LP 30' CROSS ACCESS AND UTILITIESPERMANENT DETENTION EASEMENT EX. 20' PCCE TO WILKINSON BLVD 36' CROSS ACCESS AND UTILITIESPERMANENT DETENTION EASEMENTPPPP STOPSIGN DO NOTENTER SIGN S S S S EX. Concrete Sidewalk EX. PDES N1°34'50"E 340.79'EX. 18" RCPEX. 54" CMPEX. RCP EX. 2 4 " R C P E X . R C P E X . R C PEX. RCP EX. RCP EX. RCP EX. RCP EX . R C P R/W R/W R/WR/W R/W R/W R/W R/W R/W R/W R/W R/W R/W R/W R/W R/W R/W R/W R/W SS SS SS SS SS SS SS SS SS SS SS SS SS SS SS SS SS SS SS SS SS SS SS SS F U T U R E R I G H T - O F -W A Y S LOT 2 MB 61, PG 61 END SPOT 1, LLC DB. 33272, PG. 665 TAX PARCEL #11701122 GRAVEL GRAVEL METAL RETAINING WALL EX. 24" RCPAPPROX. LOCATION END OF PIPE AS PER PREVIOUS SURVEY. POSSIBLY BURIED INV. 725.49 EX. 36"RCP RIM:731.72 IN(A):724.72 IN(B):724.60 OUT:724.66 RIM:730.24 IN(A):726.09 IN(B):726.33 OUT:726.00 RIM:733.17 IN:728.82 OUT:728.72 RIM:729.45 IN:723.21 OUT:723.10 INV:723.01 (B) (A) (B)(A)20' STREAMSIDE ZONE15'UPLANDZONE35' SWIM BUFFERTOP OF BANK FIELD LOCATED 35' SWIM BUFFER20' STREAMSIDE ZONE15'UPLANDZONEWD732 730730729 731732 733 72572672772872972372372472572672772872973 0 731 733732732 733 732 732 740 73 0 732 730 729 728725 729 730 731 7 3 2 733 731 731 731 732 73373 4 7457 3 2 735 740 73 1 745 7 3 3 7 3 4 735 2 4 " R C P 24" RCP 24" RCP 24" RCP15" RCP15" RCP15" RCP15" RCPA1-CB A2-DIA4-DI A3-DI A6-DI A5-DI A7-DI A8-DI BUILDING CBUILDING BBUILDING A EX. DRY DETENTION POND LP: 731.34 LP: 732.30 LP: 732.23 LP: 732.12 LP: 732.42 LP: 732.16 LP: 732.69 LP: 732.03 QUIK TRIP ABC STORE HP: 732.79 HP: 732.82 HP: 734.05 HP: 733.47 HP: 733.54 733.51 734.25 734.25 733.23733.23 732.99 732.99 733.06 733.26733.74 733.22 -2:1-2:1 100' NORFOLK SOUTHERN R/W733.11 733.11733.10 733.10 TC: 733.47FL: 732.97 TC: 733.09FL: 732.59 TC: 733.51FL: 733.01 TC: 734.08FL: 733.58 TC: 733.46FL: 732.96 TC: 733.50FL: 733.00 TC: 733.55FL: 733.05 TC: 734.11FL: 733.61 TC: 734.21FL: 733.71 TC: 734.11FL: 733.61 TC: 733.52FL: 733.02 TC: 733.39 FL: 732.89 TC: 734.03FL: 733.53 TC: 733.62FL: 733.12 TC: 733.60FL: 733.10 TC: 733.57FL: 733.07 TC: 733.60FL: 733.10 TC: 733.60 FL: 733.10 TC: 733.12 FL: 732.62 TC: 733.08FL: 732.58 TC: 733.53FL: 733.03 TC: 733.53 FL: 733.03 TC: 733.50FL: 733.00 TC: 733.69FL: 733.19 TC: 734.11FL: 733.61 TC: 734.11 FL: 733.61 TC: 732.97FL: 732.47 TC: 732.33FL: 731.83 TC: 733.53FL: 733.03 TC: 733.53FL: 733.03 TC: 733.00FL: 732.50 TC: 733.57FL: 733.07 TC: 733.55FL: 733.05 TC: 733.60 FL: 733.10 TC: 733.60FL: 733.10 TC: 733.60 FL: 733.10 TC: 733.19FL: 732.69 TC: 733.12FL: 732.62 TC: 733.01FL: 732.51 TC: 732.47FL: 731.97 TC: 732.31FL: 731.81 TC: 735.00FL: 734.50MEET EX.TC: 734.03FL: 733.53MEET EX.TC: 732.68FL: 732.18 MEET EX. TC: 731.63FL: 731.13MEET EX. TC: 731.24FL: 730.74 MEET EX. TC: 732.08FL: 731.58MEET EX. TC: 733.26 FL: 732.76MEET EX. TC: 731.92FL: 731.42MEET EX. -1.00%-5.49% -1.01%-0.76%-1.00%-2.18% -1.23% -2.00%-3.00%-1.00%-1.00%-1.30%-1.69%-1.00%-1.00%-1.00%-3.65%-1.79%-2.71%-1.00%-2.14%-1.67%-1.16%-1.37%-1.59%-1.00%-1.00%-1.84%-1.47%-1.47%-1.19%-1.19%-1.28%-1.18%-1.31%-1.31%-1.16%-2.00%-2.00%-1.00%-2.00%-1.59%-1.00%-2.16%-1.00%-1.72% -1.11%-0.45%-1.49% -0.89%-0.43%-2.00% -1.54%-1.00%-2.00% -2.00%0.00%-0.95% -1.68%0.53%WILKINSON BLVD (US-29 / NC-74) 100' NCDOT PUBLIC R/W 730.52 CONVERT EX. CB TO DI EX. 20' PCCE TO WILKINSON BLVDPB 57 PG 114 732 733 733 73 3 733734 734ADJUST EX JBRIM TO GRADE -1.00%-1.00%-0.95% -1.00%3.76%3.76%-2.00%-1.00%EX. ACCESS EASEMENTPB 57 PG 114 100' R/WEX. CBRIM: 733.17INV IN: 728.82INV OUT: 728.72 EX. CBRIM: 731.72INV IN: 724.72INV IN: 724.60INV OUT: 724.66 EX. JB A-9RIM: 729.45INV IN: 723.21INV OUT: 723.10 EX. FES A-10INV OUT: 723.01 EX. CBRIM: 730.30INV OUT: 726.60 EX. CB EX. CB EX. CB EX. JB EX. CBRIM: 734.92INV OUT: 730.07EX. CBRIM: 734.94INV IN: 729.53INV OUT: 729.53 EX.OUTLETSTRUCTURE EX. 36" RCPEX. 36" RCPEX. 2 4 " R C P E X . 1 5 " H D P E EX CBRIM: 730.43INV OUT: 724.93 EX CB EX CB EX CB EX 15" HDPE EX 15" HDPE EX 15" HD P E EX CB EX. 36" RCP EX. 18" RCP EX. 12" RCPEX. PDEEX . P D E EX . 1 5 " R C PEX. 18" RCPEX. 1.5' CURB & GUTTER EX. 1.5' CURB & GUTTER EX. 1.5' CURB & GUTTER EX. 1.5' CURB & GUTTER EX. ASPHALT EX. ASPHALTEX. 1.5' CURB & GUTTEREX. 1.5' CURB & GUTTEREX. ASPHALT EX. CONC. EX. CONC.DRIVEWAY EX. ASPHALTDRIVEWAY EX. 2.0' CURB & GUTTER EX. 2.0' CURB & GUTTER EX. CONC. PAVEMENT EX. 2.0' CURB & GUTTER EX. 2.0' CURB & GUTTER EX. CONC. PAVEMENT EX. CONC.DRIVEWAY EX. ASPHALTEX. 2.5' CURB & GUTTEREX. CBRIM: 730.24INV IN: 726.09INV IN: 726.33INV OUT: 726.00 -1.00%-1.29%-2.00%TC: 733.14FL: 732.64 -2.53% 732 -1.00%-1.00%-1.00%TC: 733.56 FL: 733.06 733734733733731.05 732.07 733.67 733.37 733.27 733.08 732.98733.59 733.34 733.34 733.91 733.85 733.85 734.05 -1.00%733.67 731.12 731.15 732.17 733.47 732.66 TC: 734.11 FL: 733.61 TC: 733.67FL: 733.17 TC: 733.57FL: 733.07 TC: 733.22FL: 732.72 TC: 733.22FL: 732.72 TC: 733.50FL: 733.00 733 73 3 73 3 734734 7327337 3 2 733-1.71%-1.00%-1.00%TC: 733.35 FL: 732.85 TC: 733.19 FL: 732.69 TC: 734.20FL: 733.70 734.25 733.57 FFE = 733.67 FFE = 734.25 FFE = 733.74 731.88 732.77 731 EX. 24" RCPINV: 729.45 EX. 24" RCP BEGINNIGLOCATION UNKNOWN REMOVE EX. 24" RCP UNDERPROPOSED PAVEMENT. PLUG PIPE END PER NCDOT STD. 840.71 10" HDPE ROOF DRAIN@ MIN. 1.0% 8" HDPEROOF DRAIN @ MIN. 1.0% 8" HDPE ROOF DRAIN @ MIN. 1.0% 8" HDPEROOF DRAIN @ MIN. 1.0% 8" HDPEROOF DRAIN@ MIN. 1.0% 10" HDPE ROOF DRAIN @ MIN. 1.0% 10" HDPEROOF DRAIN @ MIN. 1.0% 8" HDPE ROOF DRAIN@ MIN. 1.0% 8" HDPEROOF DRAIN@ MIN. 1.0% 10" HDPEROOF DRAIN@ MIN. 1.0% 10" HDPE ROOF DRAIN @ MIN. 1.0% 8" HDPE ROOF DRAIN @ MIN. 1.0% 8" HDPE ROOF DRAIN @ MIN. 1.0% 8" HDPEROOF DRAIN@ MIN. 1.0% 8" HDPEROOF DRAIN@ MIN. 1.0% 10" HDPEROOF DRAIN@ MIN. 1.0%8" HDPEROOF DRAIN @ MIN. 1.0% 8" HDPEROOF DRAIN@ MIN. 1.0% R2-COGRND = 733.62 INV = 730.73 R4-COGRND = 733.62INV = 729.80 R6-COGRND = 733.62 INV = 729.45 R9-CO GRND = 733.62INV = 728.92 R8-COGRND = 733.62 INV = 729.33 R14-CO GRND = 733.55INV = 728.92 R13-CO GRND = 733.55INV = 729.33 R11-COGRND = 733.55INV = 729.45 R21-CO GRND = 734.13INV = 729.55R16-DSGRND = 733.55INV = 729.32 R19-COGRND = 733.19INV = 728.85 R18-COGRND = 733.55 INV = 729.31 R23-COGRND = 734.13INV = 729.54 R24-COGRND = 733.69INV = 729.08 R26-CO GRND = 733.76INV = 729.61 R29-CO GRND = 733.52 INV = 729.14 R28-CO GRND = 734.21 INV = 729.61 ROOF DRAINS DISCHARGE TOGRADE ALONG FRONT OF THEBUILDING SEE SHEET C5.1 FOR TRIBUTARY AREAS ROOF DRAINS DISCHARGE TOGRADE ALONG FRONT OF THEBUILDING SEE SHEET C5.1 FOR TRIBUTARY AREAS ROOF DRAINS DISCHARGE TOGRADE ALONG FRONT OF THEBUILDING SEE SHEET C5.1 FOR TRIBUTARY AREAS R15-DSGRND = 730.13INV = 729.38 R17-DSGRND = 730.13INV = 729.37 R10-DSGRND = 730.27 INV = 729.51 R12-DSGRND = 730.15 INV = 729.39 R22-DSGRND = 730.36 INV = 729.60 R20-DSGRND = 730.37INV = 729.61 R25-DS GRND = 730.43INV = 729.67 R27-DS GRND = 730.43INV = 729.67 R1-DS GRND = 731.55INV = 730.79 R3-DSGRND = 730.62 INV = 729.86 R5-DSGRND = 730.27 INV = 729.51 R7-DS GRND = 730.15INV = 729.39 EX. 5' CONC. SIDEWALKEX. 5' CONC. SIDEWALKWILKINSON BLVD (US-29 / NC-74) 100' NCDOT PUBLIC R/W TC: 735.24 FL: 734.74 UGEUGEUGEUGEUGE UGE UGE UGE UGE UGE UGE UGE UGE UGE UGE UGEUGEUGEUGEUGE UGE UGE UTUTUTUT UT UT UT UT UT UT UT UT UT UT UGEUGEUGEUGEUGE UGE UGE UGE UGE UGE UGE UGE UGE UGE UGEUGEUGEUGEUGEUGEUGEUGEUGEUGEUGEUGEUGEUGEUGEUGEUGEUGE UGE UGE UTUTUTUT UT UT UT UTUTUTUT UT UT UT UT UT UT UT UT UT UTUTUTUTUTUTUTUTUTUTUTUTUTUTUTUTUTUT UT UT UT AREA 1 CUT/FILL ANALYSIS -- PROPOSED TREE PROTECTION FENCE ( IN FEET ) 0 GRAPHIC SCALE 1 inch = 30 ft. 15 30 6030 LOCATION MAP SCALE: 1" = 1,500' Wilkinson Blvd Remount RoadDonald Ross Road As h l e y RoadWest Blv d N C- 1 6 0 Greenland Ave SITE To I-77 To I-485 Old Steele Creek RdWeyland AveUE UE DROP INLET & PIPE CATCH BASIN & PIPE STORM DRAIN MANHOLE & PIPED POWER LINE (UNDERGROUND) LEGEND: R/W e e e G G E E SS SS FO FO FO W W EASEMENT RIGHT-OF-WAY SETBACK GAS LINE POWER LINE (OVERHEAD) SANITARY SEWER PIPE STORM DRAIN PIPE TELEPHONE LINE (UNDERGROUND) WATER LINE PROPERTY LINE X X FENCE TP TP 680 677 680 677 EX. MAJOR CONTOUR EX. MINOR CONTOUR TO WILKINSON BLVDINTERSECTION WITHASHLEY ROADPROPOSED CONCRETE PAVEMENT PROPOSED HEAVY DUTY ASPHALT PAVEMENT PROPOSED STANDARD ASPHALTPAVEMENT 4-13-20 1 1 1 1 2 Elevations Table Number 1 2 3 4 5 6 7 8 9 Minimum Elevation -4.00 -3.00 -2.00 -1.00 0.00 1.00 2.00 3.00 4.00 Maximum Elevation -3.00 -2.00 -1.00 0.00 1.00 2.00 3.00 4.00 5.00 Area 1455.05 2737.22 5259.51 15276.05 28434.38 27936.75 35301.14 24552.73 1725.18 Color American Engineering Associates - Southeast, P.A.8008 Corporate Center Dr - Suite 110Charlotte, NC 28226704-375-2438AMERICANEngineeringFIRM # C-3881 *** 3 Days Before Digging *** North Carolina 811 811 or 1-800-632-4949 Remote Ticket Entry http://nc811.org/remoteticketentry.htm L ARPONISSEFO ENGINE RE 33046 SEAL JOB NUMBER: DATE: DRAWN BY: CHECKED BY: C190079 CT CDA 2-21-2020 2-21-20 1-28-2021 NOTES: 1.PRIOR TO PLACEMENT OF FILL MATERIAL WITHIN PROPOSED BUILDING FOOTPRINTS,UP TO 1 FT OF CUT WILL OCCUR TO REMOVE STRUCTURALLY UNSUITABLE SOILS WITHHIGH ORGANIC CONTENT. 2.AREA 1 NOTED BELOW CONTAINS POTENTIALLY HAZARDOUS LEVELS OF LEAD. SOILSREMOVED FROM THIS AREA MUST BE STOCKPILED IN ACCORDANCE WITH THEDEQ-APPROVED ENVIRONMENTAL MANAGEMENT PLAN AND CHARACTERIZED PRIORTO EXPORT FROM THE SITE OR PRIOR TO PLACEMENT IN A DESIGNATED AREA ON THESITE. Appendix B EnviroBlend and Free Flow Product Specifications Determining the Right EnviroBlend® chemistry for your site. An overview of our complimentary treatability study services Treatability Study Instructions EnviroBlend is not a one-size-fits all approach as we have a family of chemistries that are tailor-made for each unique application. The most effective and preferred method for determining the best EnviroBlend chemistry and dosage rate for your application is through a complimentary treatability study. To complete a treatability study, we kindly request that you follow the steps below: 1. Please obtain a 2 lb. representative sample from your site and send it directly to our 3rd party lab at the following address: Ursus Remediation Testing & Technologies, LLC 1204 Springdale Street Mount Horeb, WI 53572 The sample can be collected and put in any type of packaging (i.e., Ziplock bag), and can be shipped as-is (it does NOT have to be on ice, etc.). 2. The attached form should be filled out to the best of your ability. Please print this out and include in your sample to the lab. Please also email a copy to cgehret@premiermagnesia.com so that we can track the sample. We can usually turn the results around in a 2-3 business days. EnviroBlend® Overview For over 40 years, EnviroBlend has been a trusted name in heavy metals stabilization. Our family of chemistries are successful in stabilizing lead, cadmium, arsenic, hexavalent chromium, zinc, nickel, copper and more. We can treat to regulatory goals such as the Toxicity Characteristic Leaching Procedure (TCLP), the Synthetic Precipitate Procedure (SPLP), the Multiple Extraction Procedure (MEP) and the California Wet Test (CalWet). We also have treatment reagents for industrial acid gas emissions and odor control. EnviroBlend products are custom made to perform in a wide range of waste matrices and are available in dry (milled or granular) and slurry form. They can be used on remediation sites in-situ or ex-situ for soil and/or groundwater. Our foundry and industrial products are available as in-line treatment for the elimination of hazardous waste generation. If you have questions, please contact Charis Gehret at cgehret@premiermagnesia.com . EnviroBlend® Application and Handling EnviroBlend® Application EnviroBlend® is a dry granular or milled material that can be purchased in 2000# Supersacks or bulk. The single consideration with treatment is making sure product is homogeneously mixed within the matrix (soil, waste, etc.). There is no preferred method for mixing. Generally, clients utilize excavators, track hoes, backhoes, rotary-head mixers, pug-mills, or agricultural tillers. If not using a batch plant or pug mill, it is advisable to parcel out soil if not already residing in cells or piles. This will allow for more careful metering of amendment. This is an example of the steps for batch-mixing: 1. Excavate a pile of contaminated waste/soil of a set amount – for example 100 tons, etc. 2. Add the EnviroBlend at the required dosage. For example, if a 2% dosage rate of EnviroBlend has been determined to be needed, it would necessitate that you add 2 tons of EnviroBlend per each 100 tons of soil. 3. Mix soil/EnviroBlend pile thoroughly with any of the previously mentioned equipment so that it becomes a homogenous mix. 4. Once complete, you can sample immediately for TCLP. There no cure time and no additives (e.g. water) or activator(s) need be mixed with the product for treatment Some products are offered in slurry form, for these products please see Slurry Application. EnviroBlend® Handling and Shelf Life Store product in a dry, protected place. Do not allow water to penetrate impoundment, silo, or Supersack. Significant or repeated exposure to precipitation may cause the product to clump or form a crust. With bulk piles of product, ground and top coverage tarps are recommended to keep product dry from precipitation and from wicking moisture from the ground. For Supersacks, even though sacks are water resistant and shrink-wrapped to pallets, tarping or covered storage of Supersacks is recommended to prevent product exposure to precipitation or ponded water – on the ground or on the sack – especially for prolonged (months) product staging time. EnviroBlend® Application Guidelines and Storage and Handling - 2019 Note that there is no specific shelf life, but if EnviroBlend is kept completely dry with no moisture exposure, it could last up to 6 months. However, any hydration could compromise chemical effectiveness, so it is best to purchase product as needed, and not for long term storage. For additional information about EnviroBlend products for environmental treatment applications, please contact Charis Gehret at cgehret@premiermagnesia.com. Bench Scale Treatability Study Form Sample labeled as: ______________ Anticipated Sample Arrival Date: ______________ Sample shipping address: Enclose form in the box and Email completed form to: URSUS 1204 Springdale St. cgehret@premiermagnesia.com Mount Horeb, WI 53572 (608) 437-7413 Premier Contact: Customer Name/Location: Contact Name/phone and Email: Type of Industry: Dust, Sand or Metals Source/Location Name: Metal(s) of Concern: Note: Required Regulatory Goals: (check each that applies) Metals/Test TLCP TCLP/UTS SPLP STLC MEP Other (List) Lead Arsenic Cadmium Zinc Chromium Nickel Current Product Used: Current Dosage Rate: Special Instructions: SAFETY DATA SHEET 1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAKING Product identifier Product Name ENVIROBLENDÒ CS Other means of identification Product Code ENVIROBLENDÒ CS Synonyms None Recommended use of the chemical and restrictions on use used for heavy metals remediation. Uses advised against No information available Details of the supplier of the safety data sheet Emergency telephone number 24 Hour Emergency Phone Number Chemtrec 1-800-424-9300 Emergency Telephone Chemtrec 1-800-424-9300 2. HAZARDS IDENTIFICATION Classification OSHA Regulatory Status Product dust is classified as a "nuisance particulate, not otherwise regulated" as specified by ACGHI and OSHA. The excessive, long-term inhalation of mineral dusts may contribute to the development of industrial bronchitis, reduced breathing capacity, and may lead to the increased susceptibility to lung disease. Contact with water may cause product to swell, generate some heat and burst its container. Low toxicity. Not a dangerous substance or mixture according to the Globally Harmonized System (GHS) Label elements Emergency Overview Causes mild irritation to the eyes Low toxicity by skin contact. Chronic overexposure by inhalation of airborne particulate may irritate upper respiratory system as well as the throat. Ingestion is an unlikely route of exposure. If ingested in large amounts it may cause irritation, nausea, vomiting, diarrhea, abdominal pain, black stool, pink urine, coma and possibly death. Hazards not otherwise classified (HNOC) Other Information Unknown Acute Toxicity 100% of the mixture consists of ingredient(s) of unknown toxicity Manufacturer Address The product contains no substances which at their given concentration, are considered to be hazardous to health _____________________________________________________________________________________________ Appearance Fine powder to fine granular Page 1 / 7 Physical state Solid Odor Odorless Issue Date 02-Dec-2014 Revision Date 24-March-2017 Version 1 Premier Magnesia, LLC, 75 Giles Place, Waynesville, NC 28786 Company Phone Number 828-452-4784 Recommended Use A specialty blend of magnesium oxide, magnesium hydroxide _____________________________________________________________________________________________ 3. COMPOSITION/INFORMATION ON INGREDIENTS Chemical Name CAS No.Weight-%Trade Secret Magnesium Oxide 1309-48-4 70 Magnesium Hydroxide 1309-42-8 30 4. FIRST AID MEASURES First aid measures Eye contact Rinse thoroughly with plenty of water, also under the eyelids. Skin Contact Wash with soap and water. Low toxicity by skin contact. Inhalation Move victim to fresh air. If breathing has stopped, give artificial respiration. Get medical attention immediately. Ingestion Ingestion is an unlikely route of exposure. If ingested in sufficient quantity and victim is conscious, give 1-2 glasses of water or milk. Never give anything by mouth to an unconscious person. Leave decision to induce vomiting to qualified medical personnel, since particles may be aspirated into the lungs. Seek immediate medical attention. Most important symptoms and effects, both acute and delayed Symptoms No information available. Indication of any immediate medical attention and special treatment needed Note to physicians Treat symptomatically. 5. FIRE-FIGHTING MEASURES Suitable extinguishing media Use extinguishing measures that are appropriate to local circumstances and the surrounding environment. Unsuitable extinguishing media Water reacts with magnesium oxide producing magnesium hydroxide and heat. Do not allow water to get inside containers: reaction with water will cause product to swell, generate heat, and burst its container. If contact is unavoidable, use sufficient water to safely absorb the heat that may be generated. Specific hazards arising from the chemical No information available. Explosion data Sensitivity to Mechanical Impact None. Sensitivity to Static Discharge None. Protective equipment and precautions for firefighters Firefighters should wear NIOSH approved, positive pressure, self-contained breathing apparatus and full protective clothing when appropriate. 6. ACCIDENTAL RELEASE MEASURES Personal precautions, protective equipment and emergency procedures _____________________________________________________________________________________________ Personal precautions Ensure adequate ventilation, especially in confined areas. Page 2 / 7 Environmental precautions ENVIROBLENDÒ CS Revision Date 24-March-2017 _____________________________________________________________________________________________ Environmental precautions See Section 12 for additional ecological information. Methods and material for containment and cleaning up Methods for containment Prevent further leakage or spillage if safe to do so. Methods for cleaning up Carefully clean up and place material into a suitable container, being careful to avoid creating excessive dust. If conditions warrant, clean up personnel should wear approved respiratory protection, gloves and goggles to prevent irritation from contact and/or inhalation. 7. HANDLING AND STORAGE Precautions for safe handling Advice on safe handling Use personal protective equipment as required. Conditions for safe storage, including any incompatibilities Storage Conditions Keep container tightly closed in a dry and well-ventilated place. Avoid generation of dust. Do not allow water to get inside containers; reaction with water will cause product to swell, generate heat and burst its container. Exposed, unprotected magnesium oxide will absorb moisture and carbon dioxide from the air. Incompatible materials Magnesium Oxide component is soluble in aqueous acids generating heat and steam; violent reaction or ignition with interhalogens (e.g., bromine pentifluoride; chlorine trifluoride). Incandescent reaction with phosphorus pentachloride. 8. EXPOSURE CONTROLS/PERSONAL PROTECTION Control parameters Exposure Guidelines This product, as supplied, does not contain any hazardous materials with occupational exposure limits established by the region specific regulatory bodies. Chemical Name ACGIH TLV OSHA PEL NIOSH IDLH Magnesium Oxide 1309-48-4 TWA: 10 mg/m3 inhalable fraction TWA: 15 mg/m3 fume, total particulate (vacated) TWA: 10 mg/m3 fume and total particulate IDLH: 750 mg/m3 fume NIOSH IDLH Provide workers with NIOSH approved respirators in accordance with requirements of 29 CFR 1910. 134 for level of exposure incurred. Appropriate engineering controls Engineering Controls Provide sufficient ventilation, in both volume and air flow patterns to control mist/dust concentrations below allowable exposure limits. Showers. Eyewash stations. Individual protection measures, such as personal protective equipment Eye/face protection Avoid contact with eyes. The use of eye protection is recommended. Skin and body protection The use of eye protection, gloves and long sleeve clothing is recommended. Respiratory protection Provide workers with NIOSH approved respirators in accordance with requirements of 29 CFR 1910. 134 for level of exposure incurred. General Hygiene Considerations _____________________________________________________________________________________________ Wash hands thoroughly after handling. 9. PHYSICAL AND CHEMICAL PROPERTIES Page 3 / 7 Information on basic physical and chemical properties ENVIROBLENDÒ CS Revision Date 24-March-2017 _____________________________________________________________________________________________ Physical state Solid Explosive properties No information available Oxidizing properties No information available Other Information Softening point No information available Molecular weight No information available VOC Content (%)No information available Density No information available Bulk density 70-80lb/ft3 10. STABILITY AND REACTIVITY Reactivity Chemical stability Stable under recommended storage conditions. Possibility of Hazardous Reactions None under normal processing. Hazardous polymerization Hazardous polymerization does not occur. Conditions to avoid Extremes of temperature and direct sunlight. Incompatible materials Magnesium Oxide component is soluble in aqueous acids generating heat and steam; violent reaction or ignition with interhalogens (e.g., bromine pentifluoride; chlorine trifluoride). Incandescent reaction with phosphorus pentachloride. Hazardous Decomposition Products Heat and steam. 11. TOXICOLOGICAL INFORMATION Appearance Fine powder to fine granular Odor Odorless Color Brownish Odor threshold No information available Property Values Remarks • Method pH 10-11 Melting point/freezing point Melting pt >2100 °C Melting pt >3800 °F Boiling point / boiling range No information available Flash point No information available Evaporation rate Not Applicable Flammability (solid, gas)No information available Flammability Limit in Air Upper flammability limit:No information available Lower flammability limit:No information available Vapor pressure No information available Vapor density No information available Specific Gravity 3.56 g/cc Water solubility Slight <1% Solubility in other solvents No information available Partition coefficient No information available Autoignition temperature No information available Decomposition temperature No information available Kinematic viscosity _____________________________________________________________________________________________ No information available Dynamic viscosity No information available Page 4 / 7 No data available ENVIROBLENDÒ CS Revision Date 24-March-2017 _____________________________________________________________________________________________ Information on likely routes of exposure Product Information Magnesium Oxide # 1309-48-4 Magnesium Hydroxide #1309-42-8 Product does not present an acute toxicity hazard based on known or supplied information. Inhalation Inhalation of fume (not MgO dust particulate) produced upon decomposition of magnesium compounds can produce a febrile reaction and leukocytosis in humans. Eye contact Irritating to eyes. Skin Contact Low toxicity by skin contact. Ingestion Ingestion is an unlikely route of exposure. If ingested in large amounts it may cause irritation, nausea, vomiting, diarrhea, abdominal pain, black stool, pink urine, coma and possibly death. Chemical Name Oral LD50 Dermal LD50 Inhalation LC50 Magnesium Hydroxide 1309-42-8 = 8500 mg/kg ( Rat )-- Information on toxicological effects Symptoms No information available. Delayed and immediate effects as well as chronic effects from short and long-term exposure Sensitization No information available. Germ cell mutagenicity No information available. Carcinogenicity No information available. Reproductive toxicity No information available. STOT - single exposure No information available. STOT - repeated exposure No information available. Aspiration hazard No information available. Numerical measures of toxicity - Product Information Unknown Acute Toxicity 100% of the mixture consists of ingredient(s) of unknown toxicity 12. ECOLOGICAL INFORMATION Ecotoxicity No data available on any adverse effects of this material on the environment 100% of the mixture consists of components(s) of unknown hazards to the aquatic environment Persistence and degradability No information available. Bioaccumulation No information available. Other adverse effects No information available _____________________________________________________________________________________________ 13. DISPOSAL CONSIDERATIONS Waste treatment methods Page 5 / 7 Disposal of wastes This product does not exhibit any characteristics of a hazardous waste. The product is suitable for landfill disposal. Follow all applicable federal, state and local regulations for safe disposal. ENVIROBLENDÒ CS Revision Date 24-March-2017 _____________________________________________________________________________________________ Contaminated packaging Do not reuse container. 14. TRANSPORT INFORMATION DOT Not regulated Not regulated by DOT as a hazardous material. No hazard class, label or placard required, no UN or NA number assigned. 15. REGULATORY INFORMATION International Inventories TSCA Complies Chemical Name TSCA DSL/NDSL EINECS/ELI NCS ENCS IECSC KECL PICCS AICS Magnesium Oxide X X X X X X X X Magnesium Hydroxide X X X X X X X X X - Listed TSCA - United States Toxic Substances Control Act Section 8(b) Inventory DSL/NDSL - Canadian Domestic Substances List/Non-Domestic Substances List EINECS/ELINCS - European Inventory of Existing Chemical Substances/European List of Notified Chemical Substances ENCS - Japan Existing and New Chemical Substances IECSC - China Inventory of Existing Chemical Substances KECL - Korean Existing and Evaluated Chemical Substances PICCS - Philippines Inventory of Chemicals and Chemical Substances AICS - Australian Inventory of Chemical Substances US Federal Regulations SARA 313 This product does not contain any substances reportable under Sections 302, 304 or 313. Sections 311 and 312 do apply. (Routine Reporting and Chemical Inventories) SARA 311/312 Hazard Categories Acute health hazard No Chronic Health Hazard No Fire hazard No Sudden release of pressure hazard No _____________________________________________________________________________________________ Reactive Hazard No CWA (Clean Water Act) This product does not contain any substances regulated as pollutants pursuant to the Clean Water Act (40 CFR 122.21 and 40 CFR 122.42) Page 6 / 7 CERCLA This material, as supplied, does not contain any substances regulated as hazardous substances under the Comprehensive Environmental Response Compensation and Liability Act (CERCLA) (40 CFR 302) or the Superfund Amendments and Reauthorization Act (SARA) (40 CFR 355). There may be specific reporting requirements at the local, regional, or state level pertaining to releases of this material ENVIROBLENDÒ CS Revision Date 24-March-2017 _____________________________________________________________________________________________ US State Regulations California Proposition 65 This product does not contain chemicals known to the State of California to cause cancer, birthdefects or other reproductive toxins. U.S. State Right-to-Know Regulations Chemical Name New Jersey Massachusetts Pennsylvania Magnesium Oxide 1309-48-4 X X X U.S. EPA Label Information EPA Pesticide Registration Number Not Applicable 16. OTHER INFORMATION Issue Date 02-Dec-2014 Revision Note No information available Disclaimer at the date of its publication. The information given is designed only as a guidance for safe handling, use, processing, storage, transportation, disposal and release and is not to be considered a warranty or quality specification. The information relates only to the specific material designated and may not be valid for such material used in combination with any other materials or in any process, unless specified in the text. End of Safety Data Sheet NFPA Health hazards 1 Flammability 0 Instability 0 _____________________________________________________________________________________________ Physical and Chemical Properties - HMIS Health hazards 0 Flammability 0 Page 7 / 7 Physical hazards 0 Personal protection X ENVIROBLENDÒ CS Revision Date 24-March-2017 Revision Date 24-March-2017 The information provided in this Safety Data Sheet is correct to the best of our knowledge, information and belief Free Flow—Rockford, LLC. • 4920 Forest Hills Rd, Suite 200 • Loves Park, IL 61111 Phone: 815-636-0166 • Fax: 815-636.0560 www.freeflowtech.com FF-200® SPECIFICATIONS SHEET FF-200® Free Flow 200 (FF-200®) chemistry has proven to be an effective and economical alternative to traditional blends for lead stabilization in soils and sludges. FF-200 is easy to handle in the field and provides effective non-reversing fixation of the lead at low dosages. It has been used effectively in diesel-fuel spill clean-ups and additionally as a fast-acting absorbent on airport runways for hydraulic oil. The fine texture of FF-200® allows penetration in the open cracks and crevices of concrete or asphalt and quick absorption of oils or fuel, leaving a non- slick surface. Physical Properties  Molecular Formula: Mixture  Appearance: White gray powder  Specific Gravity: 2.6  pH: 12.0  Flashpoint: Noncombustible  Odor: None  Loss on Ignition: 0.8 percent Advantages  Custom Blending / Packaging  User Friendly Chemistries  Cost Effectiveness Typical Sieve Analysis % Passing 20 Mesh 95% Passing 40 Mesh 87% Passing 100 Mesh 35% Passing 200 Mesh 15%  Effective for oil spill cleanup  Reduced application rate  Absorbs quickly Free Flow Technologies, Ltd. FF-200 Chemistry Free Flow 200® is a proprietary blend of stabilizing reagents that fixate heavy metals in waste or soil across a wide range of pH conditions using a combination of sulfate, carbonate and hydroxide precipitation chemistry. How It Works When moisture comes into contact with soil or waste stabilized with Free Flow 200®, soluble sulfates are immediately released to initiate fixation reactions with lead and barium by the following reactions: Pb+2(aq) + SO4-2(aq) → PbSO4 (s) Ksp = 1.6 x 10-8 Ba+2(aq) + SO4-2(aq) → BaSO4 (s) Ksp = 1.1 x 10-10 The sulfate reaction is a preliminary sweep reaction that precipitates the most soluble lead with the soluble sulfate anion. Precipitation of remaining lead and other heavy metals proceeds by slow-release car- bonate and hydroxide components that react with acidity and heavy metals to further fixate the metals via the reaction shown below: Pb+2 (aq) + 2 OH- (aq) → Pb(OH)2 (s) Ksp = 1.2 x 10-15 Although the above reactions are described for lead, the reagent performs similar for fixation of other heavy metals such as cadmium, trivalent chromium, cobalt, copper, nickel, silver, and zinc. Through a combination of the chemical reactions described above, Free Flow 200® is able to stabilize heavy metals in soil and waste across a wide range of pH values to meet the objectives of the SPLP or TCLP in remediation applications. Free Flow Technologies, Ltd. • 4920 Forest Hills Rd • Suite 200 • Loves Park, IL 61111 Phone: 815-636-0166 • Fax: 815-636.0560 www.freeflowtech.com SDS – FF-100® - 200® - 300® – Page 1 Free Flow - Rockford, L.L.C. A Free Flow Technologies, Ltd. Company SAFETY DATA SHEET (SDS) OSHA Hazard Communication Standard 29 CFR 1910.1200. Prepared to GHS Trade Name: Free Flow 100®, Free Flow 200®, Free Flow 300® Product CAS: None Recommended use: Stabilize RCRA Metals Company Identification: Free Flow Technologies, Inc. For information call: (815) 636-0166 4920 Forest Hills Rd, Suite 200 Emergency Contact: Timothy Danzer Loves Park, Illinois 61111 Fax: (815) 636-0560 GHS07 Acute Toxicity Classification of the substance:  H303 Acute Toxicity, category 5 (oral)  H313 Acute Toxicity, category 5 (dermal)  H332 Acute Toxicity, category 4 (inhalation)  H315 Skin, eye irritation, category 2  H317 Skin sensitization, category 1  H335 Specific Target Organ Toxicity, category 3 (single exposure, respiratory tract irritation) WARNING Hazard Statements:  H303 May be harmful if swallowed  H313 May be harmful in contact with skin  H332 Harmful if inhaled  H315 Causes skin irritation  H317 May cause an allergic skin reaction  H335 May cause respiratory irritation Precautionary Statements: Prevention P261 Avoid breathing dust. P264 Wash hands thoroughly after handling. P271 Use only outdoors or in a well-ventilated area. P272 Contaminated work clothing should not be allowed out of the workplace. SECTION 1 – PRODUCT AND COMPANY IDENTIFICATION SECTION 2 – HAZARD(S) IDENTIFICATION SDS – FF-100® - 200® - 300® – Page 2 Free Flow - Rockford, L.L.C. A Free Flow Technologies, Ltd. Company Prevention cont. P280 Wear protective gloves, safety glasses, and protective clothing such as long sleeves and pant cuffs over shoes to minimize skin contact. Response P302+P352 IF ON SKIN: Wash with plenty of soap and water. P304+P340 IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing. P312 Call a POISON CENTER or doctor/physician if you feel unwell. P321 Specific treatment, see supplemental first aid information. P332+P313 If skin irritation occurs: Get medical advice/attention. P362+P364 Take off contaminated clothing and wash it before reuse. Storage/Disposal P403+P233 Store in a well-ventilated place. Keep container tightly closed. P501 Dispose of container in accordance with local, regional, national, and/or international regulations. Hazards Ratings HMIS Chemical Name CAS Approx. % (w/w) LD50 LC50 Phosphate Compounds 7758-23-8 0 - 80 Not Available Not Available Calcium Oxide 1305-78-8 10 - 70 Not Available Not Available Sulfur Trioxide 7446-11-9 0 - 40 Not Available Not Available Silicon Dioxide 60676-86-0 2.5 – 15 Not Available Not Available Aluminum Oxide – Non-fibrous 1344-28-1 0.5 - 5 Not Available Not Available Iron Oxide 1309-37-1 0.5 - 5 Rat, oral, >5000 mg/kg Not Available Sodium Bicarbonate 144-55-8 0 - 70 Mouse, oral, 3360 mg/kg Not Available Magnesium Oxide 1309-48-4 0 - 60 Not Available Not Available SECTION 3 – COMPOSITION, INFORMATION ON INGREDIENTS SECTION 2 – HAZARD(S) IDENTIFICATION (CONT.) (CONT.) 1 SDS – FF-100® - 200® - 300® – Page 3 Free Flow - Rockford, L.L.C. A Free Flow Technologies, Ltd. Company After Eye Contact: Flush eyes with water while lifting lids. Seek medical attention. After Skin Contact: Wash skin with soap and water, remove contaminated clothing and shoes. If irritation develops, seek medical attention. After Ingestion: Dilute with water, fruit juice or vinegar. Seek medical attention. After Inhalation: Remove to fresh air, if irritation develops, seek medical attention. Most important symptoms and effects, both acute and delayed. Refer to Section 11 – Toxicological Information Indication of any immediate medical attention and special treatment needed. All treatments should be based on observed signs and symptoms of distress in the patient. Consideration should be given to the possibility that overexposure to materials other than this product may have occurred. Suitable extinguishing equipment: This material is noncombustible. Extinguishing equipment that is not appropriate for a particular situation: Do not use water on adjacent fires. Extinguish adjacent fires with dry chemical or CO2. Specific hazards that develop from the chemical during the fire: No specific hazards are identified. Protective equipment or precautions for firefighters: No special measures required. Personal precautions, protective equipment and emergency procedures: Wear protective equipment to prevent skin exposure and inhalation. Keep unprotected persons away. Environmental Precautions: Avoid runoff to waterways and sewers. Methods and materials used for containment and cleanup: Use appropriate protective equipment while using dry cleanup methods (sweep/shovel) which minimize dusting. Reclaim in watertight containers. Small amounts may be flushed with water to drain. SECTION 4 – FIRST AID MEASURES SECTION 5 – FIRE FIGHTING MEASURES SECTION 6 – ACCIDENTAL RELEASE MEASURES SDS – FF-100® - 200® - 300® – Page 4 Free Flow - Rockford, L.L.C. A Free Flow Technologies, Ltd. Company Precautions for safe handling: Swells when wet, may expand the container. Keep eyewash bottles available throughout work area. Conditions for safe storage, including any incompatibilities: Store away from water or acids. Control Parameters Component Formula CAS PEL TLV _ Phosphate Compounds Ca(H2PO4)2H2O 7758-23-8 Not established Not established Calcium Oxide CaO 1305-78-8 5 mg/m3 2 mg/m3 Sulfur Trioxide SO3 7446-11-9 1 mg/m3 0.2 mg/m3 Silicon Dioxide** SiO2 60676-86-0 0.1 mg/m3* 0.1 mg/m3* Aluminum Oxide Al2O3 1344-28-1 10 mg/m3+ 10 mg/m3+ Iron Oxide** Fe2O3 1309-37-1 15 mg/m3 5 mg/m3 Sodium Bicarbonate NaHCO3 144-55-8 15 mg/m3* 10 mg/m3* Magnesium Oxide MgO 1309-48-4 15 mg/m3* 10 mg/m3* * Respirable Dust + 5 mg/M3 as Respirable Fraction **Silicon Dioxide and Iron Oxide are listed by IARC as potential carcinogens. Exposure Controls Engineering Controls: Use general and local exhaust to keep dust levels within acceptable limits. Personal Protective Equipment Pictograms: Breathing Protection: Use NIOSH approved dust respirator when exposure limits exceeded. Hand Protection: Wear gloves to minimize skin contact. Eye Protection: Wear tight fitting goggles. Skin Protection: Wear long sleeves, gloves, and pant cuffs over shoes to minimize skin contact. SECTION 8 – EXPOSURE CONTROLS AND PERSONAL PROTECTION SECTION 7 – HANDLING AND STORAGE SDS – FF-100® - 200® - 300® – Page 5 Free Flow - Rockford, L.L.C. A Free Flow Technologies, Ltd. Company Appearance: White-gray powder. Boiling Point: N/A Odor: Odorless Flammable, Lower Limit: N/A Odor Threshold: N/A Flammable, Upper Limit: N/A Solubility: N/A Flash Point: N/A Partition Coefficient: Not determined. Auto Ignition Temperature: N/A pH: 6.0 – 12.0 Freezing/Melting Point: N/A Density: 80 – 85 lbs/ft3 Viscosity: N/A Vapor Pressure: N/A Decomposition Temp.: N/A Vapor Density: N/A Evaporation Rate: N/A Molecular Formula: Mixture Reactivity: No dangerous reactions known under conditions of normal use. Chemical Stability: Stable, keep dry. Thermal decomposition/conditions to be avoided: Avoid extreme temperatures. Possibility of hazardous reactions: Contains calcium oxide and may react with water or acid to produce heat. Incompatible materials: Water, strong acids. Toxicological Effects Component Formula LD50 LC50 _ Phosphate Compounds Ca(H2PO4)2H2O Not Available Not Available Calcium Oxide CaO Not Available Not Available Sulfur Trioxide SO3 Not Available Not Available Silicon Dioxide** SiO2 Not Available Not Available Aluminum Oxide Al2O3 Not Available Not Available Iron Oxide** Fe2O3 rat, oral, >5000 mg/kg Not Available Sodium Bicarbonate NaHCO3 mouse, oral, 3360 mg/kg Not Available Magnesium Oxide MgO Not Available Not Available **Silicon Dioxide and Iron Oxide are listed by IARC as potential carcinogens. SECTION 9 – PHYSICAL AND CHEMICAL PROPERTIES SECTION 10 – STABILITY AND REACTIVITY SECTION 11 – TOXICOLOGICAL INFORMATION SDS – FF-100® - 200® - 300® – Page 6 Free Flow - Rockford, L.L.C. A Free Flow Technologies, Ltd. Company Routes of exposure Absorbed through skin. Dermal contact. Eye contact. Inhalation. Ingestion. Potential health effects Eye: Acute: May cause mild eye irritation Chronic: No data available Skin: Acute: Causes skin irritation Chronic: Repeated and prolonged exposure may cause dermatitis Ingestion: Acute: May cause irritation Chronic: No data available Inhalation: Acute: May cause respiratory irritation Chronic: No data available Symptoms from exposure Target Organs: Eyes, respiratory passages, skin, digestive tract. Pre-existing respiratory diseases including asthma and emphysema may also be aggravated. Eye: May cause irritation/inflammation and tissue damage. Skin: May cause irritation to moist skin. Ingestion: May cause ulceration to the digestive tract. Inhalation: May cause irritation/inflammation to nasal and upper respiratory passages. Toxicity: No further relevant information available. Persistence and degradability: No further relevant information available. Bioaccumulative potential: No further relevant information available. Mobility in soil: No further relevant information available. SECTION 12 – ECOLOGICAL INFORMATION SECTION 11 – TOXICOLOGICAL INFORMATION (CONT.) SDS – FF-100® - 200® - 300® – Page 7 Free Flow - Rockford, L.L.C. A Free Flow Technologies, Ltd. Company Recommended Waste Treatment Methods: No treatment necessary. Recommended Package Disposal: Dispose of in container in accordance with local, regional, national, and/or international regulations. UN Number: N/A UN proper shipping name: N/A Transport Hazard class: N/A Packing group number: N/A Environmental hazards: N/A Special Precautions: To prevent dust, cover product with tarp if not in bulk bag container. SARA Title III - Section 302 Extremely Hazardous Material - None SARA Title III – Section 31/312 – Hazard Categories: Fire Hazard – No Sudden Release of Pressure – No Reactivity Hazard – Yes Immediate Health Hazard – Yes Delayed Health Hazard - Yes SARA Title III – Section 313 - This material is not subject to the toxic chemical reporting requirements of Section 313 of Title III of the Superfund Amendments and Reauthorization Act of 1986 and 40 CFR Part 372. Information herein is based on data believed to be accurate at the time of the preparation. No warranty or representation, express or implied, is made to the accuracy or completeness of the SDS. No responsibility can be assumed by vendor for any damage or injury resulting from misuse, failure to follow recommended practices, or from any hazards inherent in the nature of the product. SECTION 13 – DISPOSAL CONSIDERATIONS SECTION 14 – TRANSPORT INFORMATION SECTION 15 – REGULATORY INFORMATION SECTION 16 – ADDITIONAL INFORMATION SDS – FF-100® - 200® - 300® – Page 8 Free Flow - Rockford, L.L.C. A Free Flow Technologies, Ltd. Company SDS Effective: 12/1/2014 SECTION 16 – ADDITIONAL INFORMATION (CONT.)