23081_Kroehler Mnfg Brownfields Assessment Report_ 20200804

Via Email
August 4, 2020
NCDEQ – Division of Waste Management Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646 Attn: Mr. Bill Schmithorst, PG
Re: Brownfield Assessment Report
Kroehler Manufacturing Charlotte, North Carolina Brownfields Project No. 23081-19-060 H&H Project No. BCP-145

Dear Mr. Schmithorst: On behalf of BIN – MR3412 LLC, enclosed is a copy of the Brownfields Assessment Report prepared for the Kroehler Manufacturing property (Brownfields Project No. 23081-19-060) for
your review and record.
Should you have any questions or need additional information, please do not hesitate to contact us at [phone].
Sincerely,
Hart & Hickman, PC

Ralph McGee, PG Alexis McKenzie, EI Project Manager Project Engineer Enclosure

cc: Mr. Pete Kidwell, Beacon Partners (Via Email) Mr. Miller Otstott, Beacon Partners (Via Email) Ms. Mary Katherine Stukes, Moore & Van Allen, PLLC (Via Email)
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Brownfields Assessment Report Kroehler Manufacturing
Charlotte, North Carolina Brownfields Project No. 23081-19-060 H&H Job No. BCP-145
Table of Contents
1.0 Introduction .............................................................................................................................1
1.1 Background ............................................................................................................................1
1.2 Previous Environmental Assessments ...................................................................................2
1.3 Brownfields Program .............................................................................................................4
2.0 Brownfields Assessment Activities ........................................................................................5
3.0 Receptor Survey ......................................................................................................................6
4.0 Soil Sampling Activities ..........................................................................................................9
4.1 Soil Sampling Methodology ..................................................................................................9
4.2 Soil Sampling Analytical Results ........................................................................................11
5.0 Groundwater Sampling Activities .......................................................................................13
5.1 Groundwater Sampling Methodologies ...............................................................................13
5.2 Groundwater Sampling Analytical Results .........................................................................15
5.3 Vapor Intrusion Evaluation .................................................................................................16
6.0 Quality Assurance – Quality Control ..................................................................................18
6.1 Trip Blank ............................................................................................................................18
6.2 Field Duplicates ...................................................................................................................18
7.0 Summary and Conclusions...................................................................................................19

List of Tables
Table 1 Summary of Soil Analytical Data
Table 2 Summary of Well Construction and Groundwater Elevation Data
Table 3 Summary of Groundwater Analytical Data
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List of Figures
Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Receptor Survey Map
Figure 4 Sample Location Map
List of Appendices
Appendix A Brownfields Property Receptor Survey Form
Appendix B Boring Logs
Appendix C Laboratory Analytical Report
Appendix D Field Sampling Forms
Appendix E DEQ Risk Calculator (July 2020)
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Brownfields Assessment Report Kroehler Manufacturing
Charlotte, North Carolina Brownfields Project No. 23081-19-060 H&H Job No. BCP-145
1.0 Introduction

On behalf of BIN – MR3412 LLC (Prospective Developer or PD), Hart & Hickman, PC (H&H)
has prepared this report to document Brownfields assessment activities completed at the
Kroehler Manufacturing Brownfields property (Brownfields Project No. 23081-19-060) located
at 3412 Monroe Road in Charlotte, Mecklenburg County, North Carolina (Site or subject Site).
The Site consists of one approximately 6.75-acre parcel of land located in a mixed industrial and
residential area southeast of uptown Charlotte. A Site location map is provided as Figure 1, and
the Site and surrounding area are shown in Figure 2.

The Site is developed with an approximately 121,000-square foot (sq ft) industrial warehouse
building constructed in 1950. An addition including a lower level basement was constructed on
the southwestern portion of the original warehouse building in the mid to late-1950s. The Site
building consists of a two-story office area, a show room, employee break areas, warehouse
space, two loading dock areas, and an out of use boiler room. Other improvements to the Site
include asphalt parking areas and access drives, outdoor storage areas, former and active railway
spurs, and landscaped and naturally vegetated areas.

A description of the Site history and previous assessment activities completed at the Site is
provided in the following sections.

1.1 Background
Prior to 1950, the Site consisted of undeveloped agricultural land. In the 1950s, the Site was
developed with the existing industrial warehouse facility which was occupied by Kroehler
Manufacturing for furniture manufacturing operations until 1985. Greenline Corporation then
occupied the facility for conveyor component manufacturing operations until the early 2000s.
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The property was most recently occupied by Party Reflections, a party equipment rental
company. Party reflections vacated the Site in June 2020.

Monroe Road is located adjacent to the north with residential and commercial use development
located beyond. The adjacent properties located to the east, south, and west consist of primarily
industrial and commercial use development. The adjacent property located to the southeast and
topographically upgradient of the Site was occupied by Atlantic Envelope from the 1960s
through the mid to late 2010s. Historically, the facility received violations related to hazardous
waste generation and handling practices associated with envelope manufacturing operations. No
release incidents were reported in the environmental databases in connection with the Atlantic
Envelope facility.

1.2 Previous Environmental Assessments
In August and September 2019, H&H conducted Phase I and II Environmental Site Assessment
(ESA) activities at the Site. The results of the Phase I and II ESA activities are documented in a
Phase I and II ESA Report prepared by H&H dated October 7, 2019. Results of the Phase I ESA
identified several areas of potential environmental concern based on historical Site uses. Phase
II ESA activities included collection of six soil samples and one downgradient to cross-gradient
groundwater sample for laboratory analysis in areas of concern to evaluate the potential for
impact. The historical sample locations are depicted on Figure 4.

Phase II ESA soil sample laboratory analytical results indicated the presence of volatile organic
compounds (VOCs) and semi-VOCs (SVOCs) at concentrations above the North Carolina
Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB)
Protection of Groundwater Preliminary Soil Remediation Goals (PRSGs) in a deep soil sample
(SB-2) collected adjacent to a former sump that was located south of the Site building. A low
level of the polynuclear aromatic hydrocarbon (PAH) benzo(a)pyrene was detected at a
concentration above the DEQ IHSB Residential PSRG in a soil sample (SB-5) collected adjacent
to one floor drain in the basement in the southern portion of the Site warehouse building. No
compounds were detected at concentrations above the DEQ IHSB Industrial/Commercial PSRGs
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in soil samples collected in areas of potential environmental concern at the Site.

H&H collected one groundwater sample for laboratory analysis from a temporary groundwater
monitoring well (TMW-2) installed adjacent to the former sump south of the warehouse
building. Groundwater sample laboratory analytical results identified low levels of 1,1-
dichloroethane, benzene, naphthalene, and 1-methylnaphthalene at concentrations above the
DEQ 15A NCAC 2L Groundwater Standards (2L Standards). No other compounds were
detected at concentrations above the 2L Standards, and no compounds were detected in Site
groundwater at concentrations above the DEQ Division of Waste Management (DWM) Vapor
Intrusion Groundwater Screening Levels (GWSLs).

To address environmental concerns at the Site identified during previous assessment activities,
the PD elected to enter the Site into the DEQ Brownfields Program as part of property
transaction due diligence. The Site received a letter of eligibility on February 3, 2020
(Brownfields Project No. 23081-79-060). In addition to entering the Site into the Brownfields
Program, the PD elected to complete vapor intrusion assessment activities as part of property
transaction due diligence activities to evaluate the potential for structural vapor intrusion into the
existing Site building. Vapor intrusion assessment activities were completed by H&H in
December 2019 and documented in a Vapor Intrusion Assessment Report dated February 17,
2020.

Vapor intrusion assessment activities included collection of sub-slab soil vapor samples for
laboratory analysis within the Site building to determine if volatile compounds are present at
levels that pose unacceptable vapor intrusion risks. In addition, co-located sub-slab radon
samples and indoor air radon samples were collected for laboratory analysis to establish
Site-specific attenuation factors from sub-slab vapor to indoor air within the Site building.
Sub-slab soil vapor sample laboratory analytical results indicate that several compounds were
detected at concentrations above the laboratory method detection limits in each sample. No
compounds were detected at concentrations above the DEQ DWM Residential or Non-
Residential Vapor Intrusion Sub-slab and Exterior Soil Gas Screening Levels (SGSLs). This is
consistent with results of previous soil and groundwater assessment activities completed at the
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Site.

Hypothetical worst-case risk calculator results for the sub-slab soil vapor to indoor air pathway
indicated that calculated cumulative carcinogenic and non-carcinogenic risk are well below the
DEQ and EPA acceptable levels for residential and non-residential uses. Predicted indoor air
concentrations using the most conservative attenuation factor based on the radon measurements
and the highest compound concentrations detected in any sub-slab soil vapor sample also
indicate that no predicted indoor air concentration exceeds the DEQ DWM Vapor Intrusion
Residential or Non-Residential Indoor Air Screening Levels (IASLs). As expected, hypothetical
worst-case calculated cumulative carcinogenic and non-carcinogenic risks based on the predicted
indoor air concentrations are orders of magnitude below the DEQ and EPA acceptable levels.

1.3 Brownfields Program
As noted above, the Site received eligibility into the DEQ Brownfields Program via a Letter of
Eligibility dated February 3, 2020. The PD elected to participate in the Brownfields Program
Redevelopment Now option to expedite the Brownfields process. As part of the process, a
kick-off/data gap meeting was held on May 14, 2020 with the PD, counsel for the PD, DEQ
Brownfields personnel, and H&H to discuss historical uses of the Site, available historical
environmental information, proposed redevelopment plans, data gaps, and a proposed schedule
for completion of the Brownfields Agreement. Based on conversations with DEQ Brownfields
during the kick-off meeting, H&H prepared a Brownfields Assessment Work Plan (Work Plan)
dated June 11, 2020 . The Work Plan received DEQ-approval in an email dated June 18, 2020.

Current redevelopment plans included renovations to the Site building and surrounding surfaces
for adaptive reuse as a multi-tenant commercial building. In accordance with the DEQ-approved
Work Plan, H&H conducted soil and groundwater assessment activities at the Site to evaluate
potential risk to future tenants and to assist in management of Site media during redevelopment
activities. Summary of the Brownfields assessment activities completed at the Site is provided in
the following sections.
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2.0 Brownfields Assessment Activities

In June 2020, H&H completed soil assessment activities to evaluate the potential for impacts
near on-Site rail spurs and to establish Site-specific background levels for metals. H&H also
completed groundwater assessment activities to evaluate subsurface conditions in areas
upgradient and downgradient of the Site building. In addition, a receptor survey was completed
to obtain information about land use, water supply, basements, underground utilities, drains, and
surface water bodies in the vicinity of the Site.

The assessment activities were performed in general accordance with the DEQ IHSB Guidelines
for Assessment and Cleanup (Guidelines) dated January 2020, the DEQ DWM Vapor Intrusion
Guidance (VI Guidance) dated March 2018, the most recent versions of the U.S. Environmental
Protection Agency (EPA) Region IV Science and Ecosystem Support Division (SESD) Field
Branches Quality System and Technical Procedures guidance, and the DEQ-approved Work
Plan dated June 11, 2020.

Prior to conducting field activities, H&H contacted North Carolina 811, the public utility locator,
to mark subsurface utilities located on the Site. H&H also contracted with a private utility
locator to screen proposed sample locations for subgrade utilities that may not have been marked
by the public locator. Additionally, boring locations were hand cleared to approximately 5 feet
(ft) below the ground surface (bgs) prior to use of mechanical drilling equipment to further
screen the boring locations for the presence of subsurface utilities. In accordance with
Mecklenburg County rules, H&H also reopened the previously obtained Subsurface
Investigation Permit (SIP) from Mecklenburg County (SIP No. 70002675) prior to temporary
monitoring well installation and sampling.

Receptor survey activities are discussed in Section 3.0; soil assessment activities are summarized
in Section 4.0; groundwater assessment activities and results are included in Section 5.0; a
discussion of the quality assurance/quality control practices is provided in Section 6.0; and
summary and conclusions based on results of the Brownfields assessment activities are provided
in Section 7.0.
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3.0 Receptor Survey

On June 25, 2020 H&H completed receptor survey activities at the Site and nearby area in
accordance with DEQ Brownfields Program guidance. Receptor survey activities included a
pedestrian and vehicular survey to identify possible water supply wells, basements, utility
manways and chases, storm sewers, other underground utilities, drains, and surface water within
a 1,500-ft radius of the Site. H&H also utilized the information from the online Mecklenburg
County Well Information System and DEQ Source Water Assessment Program (SWAP) for
potential potable water sources in the area. In addition, H&H identified the locations of main
underground and aboveground utilities, and land use and zoning in the areas of the Site using
available Mecklenburg County online resources. A copy of the completed Brownfields Property
Receptor Survey form is provided as Appendix A and a receptor survey map is provided as
Figure 3. The results of the receptor survey are summarized below.

Site and Surrounding Properties
As previously mentioned, the Site is comprised of one parcel totaling approximately 6.75-acres
of land located in a mixed commercial, industrial, and residential area of Charlotte.
Development on the surrounding properties primarily consists of industrial use to the east, south,
and west with residential and commercial development to the north, across Monroe Road. The
Site is bordered to the southwest and west with an active railroad spur.

Zoning
The Site is zoned for I-2 for heavy industrial use. The adjacent properties to the east and west
are zoned for heavy industrial use (I-2) and the properties to the south are zoned for light
industrial use (I-1). The properties located along the northern side of Monroe Road are zoned for
business and office use (B-2 and O-2) with multi-family and single-family residential zoning
located beyond (R-22 MF and R-4).

Municipal Water Availability
Municipal water supplied by Charlotte Water is available to the Site and surrounding area. H&H
did not identify sources of public drinking water within 1,500 ft of the Site based on review of
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information available on the DEQ SWAP and Mecklenburg County Well Information System
geographic information system (GIS) maps, as well as review of the Annual Water Quality
Report published by the City of Charlotte. The City of Charlotte obtains raw water from Lake
Norman and Mountain Island Lake which are located approximately 17 and 12 miles northwest
of the Site, respectively. H&H observed the service area map published by Mecklenburg County
which indicated that municipal water is available to the Site and the surrounding area within a
1,500 ft radius of the Site. Additionally, H&H observed municipal water meters for the Site and
surrounding properties during receptor survey reconnaissance activities.

Water Supply Wells
H&H conducted a pedestrian and vehicular survey of properties within a 1,500 ft radius of the
Site to identify potential water supply wells. H&H also utilized the DEQ SWAP GIS map to
identify potential potable water supply wells located within a 1,500 ft radius of the Site. No
private water supply wells were identified within a 1,500 ft radius of the Site.

Surface Water Bodies
A ponded section of an unnamed tributary of Briar Creek is located approximately 500 feet south
of the Site. The unnamed tributary flows in a southwestern direction toward Briar Creek located
approximately 4,000 feet to the southwest of the Site.

Topographic gradient and surface drainage in the southern portion of the Site generally slopes in
a southwestern direction towards the pond located south of the Site. Topographic gradient and
surface drainage in the northern and central portions of the Site generally slope in a northwestern
direction towards Briar Creek.

Based on the NC DEQ classification system, Briar Creek is a Class C surface water body. A
Class C surface water body is defined as “waters protected for uses such as secondary recreation,
fishing, wildlife, fish consumption, aquatic life including propagation, survival and maintenance
of biological integrity, and agriculture. Secondary recreation includes wading, boating, and other
uses involving human body contact with water where such activities take place in an infrequent,
unorganized, or incidental manner”. Briar Creek flows southwest through Mecklenburg County
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and discharges into Little Sugar Creek approximately 4 miles southwest of the Site.

Subsurface Structures
H&H contacted North Carolina 811, the public utility locator, to mark subsurface utilities located
on the Site and conducted a visual reconnaissance in the Site area to identify potential subsurface
structures within 1,000 ft of the Site. H&H observed evidence of subsurface utilities including
sanitary sewer, storm sewer, municipal water, natural gas, and/or electrical on and nearby
adjacent properties. Locations of subsurface structures at the Site are included in Figure 3. In
addition, H&H observed several structures with crawlspaces and/or potential basements within
a 1,500 ft radius of the Site during visual reconnaissance.

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4.0 Soil Sampling Activities
Two on-Site rail spurs have been used as part of historical manufacturing and distribution
operations at the Site. The rail spur located in the southern and eastern portions of the Site has
been abandoned and is no longer in use. The rail spur along the southwestern and western Site
boundaries has not been abandoned and remains an active rail. The locations of the active and
inactive rail spurs are shown in Figure 2.

On June 24, 2020, H&H collected two composite soil samples to evaluate the potential for
impact in shallow soil along the active and inactive rail spurs. In addition, two background
samples were collected in areas that appeared to be unaffected by historical uses at the Site. A
description of the soil sampling activities and results are included below.

4.1 Soil Sampling Methodology
Background Soil Sampling Activities
H&H advanced two (2) shallow soil borings (BKG-1 and BKG-2) for collection of soil samples
for laboratory analysis from areas at the Site that do not appear to have been affected by
historical uses to establish ranges for naturally occurring background concentrations of metals.
Background soil boring locations (denoted by BKG nomenclature) are shown in Figure 4.

The soil borings were advanced utilizing a decontaminated stainless-steel hand auger.
Continuous soil samples were collected from the center of the hand auger bucket at each boring.
Soil samples were logged for lithological description and field screened for indication of
potential impacts by observation for staining, odors, and the presence of organic vapors using a
calibrated photoionization detector (PID). Field screening results did not indicate obvious
evidence of potential impacts in either background soil boring. Boring logs documenting the
lithology and field screening results are included as Appendix B.

One soil sample was collected from composite sample BKG-1 for laboratory analysis from a
depth interval of 2-4 ft bgs. The soil sample was collected during advancement of temporary
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monitoring well TMW-3 and was advanced slightly deeper than the 3-foot depth described in the
Work Plan. Background sample BKG-2 was collected from a depth of approximately 1-3 ft bgs.

Soil samples selected for laboratory analysis were placed directly into dedicated laboratory
supplied sample containers, labeled with the sample identification, date, time, and requested
analysis, and placed in a laboratory supplied cooler with ice. The background soil samples were
submitted to Pace Analytical (Pace) under standard chain of custody protocols for analysis of
Resource Conservation and Recovery Act (RCRA) metals plus hexavalent chromium by EPA
Methods 6020/7471/7199.

Rail Spur Soil Sampling Activities
H&H collected shallow composite soil samples (COMP-1 and COMP-2) for laboratory analysis
to evaluate the potential for impact along the two on-Site railroad spur corridors. Composite soil
sample COMP-1 was collected to represent soil conditions along the active railroad spur in the
southwestern and western portions of the Site, and COMP-2 was collected to represent soil
conditions near the out of use rail spur located in the southern and eastern portions of the Site.
Composite soil samples for each railroad spur were comprised of five (5) soil samples collected
from aliquot soil borings advanced along each rail spur. The aliquot soil boring locations are
shown in Figure 4.

One soil sample was collected from 0-2 ft bgs at each aliquot soil boring location. The aliquot
soil borings were advanced using a decontaminated stainless steel hand auger. Continuous soil
samples were collected from the center of the hand auger bucket at each soil boring and
described for lithologic purposes, observed for the presence of staining and odors, and field
screened for elevated volatile organic vapors using a calibrated PID. Soil in the area of each rail
spur generally consisted of reddish-brown silty clay. H&H did not observe staining or odors,
and field screening results did not indicate obvious evidence of potential impacts in aliquot soil
samples collected adjacent to the rail spurs.

Following field screening, the soil sample aliquots were combined and homogenized to form one
composite soil sample representative of shallow soil near each rail spur. Soil samples selected
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for laboratory analysis were collected directly into laboratory supplied glassware, labeled with
the sample identification, date, time, and requested analysis and placed in a laboratory supplied
cooler with ice. The samples were delivered to Pace under standard chain of custody protocols
for analysis of semi-volatile organic compounds (SVOCs) by EPA Method 8270 and RCRA
metals plus hexavalent chromium by EPA Method 6020/7471/7199. In addition, one grab soil
sample was collected from an undisturbed portion of an aliquot sample for each rail spur and was
submitted for laboratory analysis of volatile organic compounds (VOCs) by EPA Method 8260.

Following sampling activities, the soil borings were properly abandoned and the surface was
repaired similar to pre-assessment conditions. Additionally, the soil sample locations were
estimated using a hand-held global positioning system (GPS) unit.

4.2 Soil Sampling Analytical Results
A tabular summary of the soil sample analytical results is presented in Table 1, and the
laboratory analytical report and chain of custody record is provided in Appendix C. Laboratory
analytical results were compared to the DEQ IHSB Residential and Industrial/Commercial
PSRGs dated December 2019. In addition to the PSRGs, metals results were compared to
published concentrations for naturally occurring metals in North Carolina soil (Dragun &
Chekiri, 2005) and Site-specific background levels represented by background soil samples
BKG-1 and BKG-2. A summary of the laboratory analytical results is provided below.

VOCs
Laboratory analytical results indicate several VOCs were detected in the samples collected along
the active and inactive rail spurs. Bromomethane (up to 0.0115 milligrams per kilogram
[mg/kg]), p-isopropyltoluene (up to 0.101 mg/kg), naphthalene (up to 0.124 mg/kg), and toluene
(0.0036 J mg/kg) were detected in at least one of the rail spur composite soil samples. No VOCs
were detected at concentrations above the DEQ IHSB Residential or Industrial/Commercial
PSRGs in either soil sample collected along the rail spur corridors.
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SVOCs
Low levels of several SVOCs including benzo(a)anthracene (1.010 J mg/kg),
benzo(b)fluoranthene (0.897 J mg/kg), chrysene (0.804 J mg/kg), fluoranthene 1.760 J mg/kg),
phenanthrene (1.620 J mg/kg), and pyrene (1.430 J mg/kg) were detected at laboratory estimated
concentrations above the laboratory method detection limits, but below the laboratory reporting
limits (J-Flag) in composite soil sample COMP-1 (active rail spur). Pyrene (0.575 J mg/kg) was
also detected above the laboratory method detection limit in composite sample COMP-2
(inactive rail spur). No SVOCs were detected at concentrations above the DEQ IHSB
Residential and Industrial/Commercial PSRGs in either soil sample collected along the rail spur
corridors.
Metals
As expected, due to the naturally occurring metals in soils, multiple metals were detected at
concentrations below the DEQ IHSB PSRGs, with the exception of arsenic. Arsenic was
detected along the active railroad at concentrations up to 7.02 mg/kg and along the inactive rail
spur at a concentration of 6.14 mg/kg. The detected concentrations exceed both the DEQ IHSB
Industrial/Commercial PSRG and Site-specific background range. However, the arsenic
concentrations detected in the rail spur composite soil samples are within the published range for
North Carolina soil, as documented in Elements in North Carolina Soils by Drugan and Chekiri
(2005; see Table 1), and are likely representative of background conditions.
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5.0 Groundwater Sampling Activities
On June 24 and 25, 2020, H&H and Innovative Environmental Technologies (IET) installed
three (3) temporary groundwater monitoring wells at the Site (TMW-3 through TMW-5). Two
temporary monitoring wells (TMW-4 and TMW-5) were installed along the northwestern and
downgradient side of the Site building, and one temporary monitoring well (TMW-3) was
installed near the southeastern corner of the Site on the upgradient side of the building. The
location of TMW-3 was relocated in the field due to inaccessibility to mobilize a drill rig to the
location described in the Work Plan. DEQ provided approval for the alternate TMW-3 location
in an email dated June 23, 2020. The three temporary monitoring well locations (denoted by
TMW nomenclature) are shown in Figure 4. Summary of the groundwater sampling methods
and results is provided in the following sections.
5.1 Groundwater Sampling Methodologies
The temporary groundwater monitoring well borings were advanced with a track-mounted drill
rig capable of utilizing direct push technology (DPT) drilling techniques to a depth at which
sufficient groundwater was encountered. During boring advancement, continuous soil samples
were collected from each boring using acetate lined macro core sleeves and logged for lithologic
description and field screened for the presence of staining, odors, and the presence of organic
vapors using a calibrated PID. No obvious evidence of impacts were observed during field
screening.
Each temporary monitoring well was constructed of 1-inch diameter PVC well screen set to
bracket the water table with a 1-inch diameter PVC well casing to the ground surface. A sand
filter pack was placed from the bottom of the borings to approximately 2 ft above the top of each
well screen. The temporary wells were completed by placing a minimum of 2 ft of hydrated
bentonite seal above the sand filter pack. Boring logs including the temporary well diagrams,
lithologic description, and field screening results are included as Appendix B.
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Once the temporary monitoring wells were installed, the wells were allowed to equilibrate to
static conditions, and a decontaminated electronic water level indicator was used to measure the
depth to the water table relative to the ground surface and to the top of the well casing in each
well. The elevation of the ground surface and top of casing for each well was surveyed relative
to an arbitrary on-Site datum. Using the measured depths to the water table and survey
measurements, H&H calculated groundwater elevations at each well location and estimated
groundwater flow direction at the Site to be toward the northwest. A tabular summary of the
groundwater elevation data is included as Table 2.

The wells were developed by removing a minimum of 3 to 5 volumes and until field parameters
stabilized (pH± 0.1 Standard Units [SU] and conductivity varies no more than 5%). After
development, groundwater samples were collected utilizing low flow/low stress purging
techniques using a peristaltic pump and dedicated polyethylene tubing. The intake point of the
pump tubing was placed in the approximate mid-portion of the screened interval of the well, and
groundwater was removed at a rate no greater than 200 milliliters per minute. H&H utilized
water quality meters to collect measurements of pH, temperature, dissolved oxygen, oxidation
reduction potential, turbidity, and specific conductivity at three to five-minute intervals during
the purging process. Purging was considered complete when the field parameters stabilized (pH
± 0.1 SU, conductivity varied no more than 5%, and turbidity was less than 10 Nephelometric
Turbidity Units [NTUs]). Field sampling forms are included as Appendix D.

Once groundwater parameters stabilized, groundwater samples for VOC analysis were collected
directly into laboratory supplied sample containers using the “soda straw” method to eliminate
the potential for volatile compound loss through the pump head. Samples collected for the
remaining analyses were collected directly into laboratory supplied sample containers from the
dedicated sample tubing discharge. The sample containers were labeled with the sample
identification, date, time, and requested analysis, and placed in a laboratory supplied cooler with
ice. The groundwater samples were delivered to Pace under standard chain of custody protocols
for analyses of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and RCRA metals
by EPA Methods 6020/7471.
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Following installation and sampling activities, the groundwater sample locations were estimated
using a hand-held GPS unit. Following surveying activities, the temporary monitoring wells
were properly abandoned by a licensed well driller.

5.2 Groundwater Sampling Analytical Results

A tabular summary of the groundwater analytical data is provided as Table 3, and a copy of the
laboratory analytical report is provided in Appendix C. Groundwater analytical results were
compared to the DEQ 15A NCAC 2L Groundwater Quality Standards (2L Standards) and the
DEQ DWM Residential and Non-Residential Vapor Intrusion GWSLs. A summary of the
laboratory analytical results is provided below.

VOCs
Several VOCs including chloroform (4.9 J micrograms per liter [µg/L]), 1,1-dichloroethene (1.5
µg/L) and trichloroethene (TCE; 1.7 µg/L) were detected above the laboratory method detection
limits, but below the 2L Standards in downgradient well TMW-4 located west of the Site
building (Figure 4). The concentration of TCE detected in the TMW-4 groundwater sample is
slightly above the DEQ DWM Residential Vapor Intrusion GWSL of 1.0 µg/L, but below the
DEQ DWM Non-Residential Vapor Intrusion GWSL of 4.4 µg/L. No VOCs were detected at
concentrations above the laboratory method detection limits in other Brownfields assessment
groundwater samples.

SVOCs
No SVOCs were detected at concentrations above the laboratory method detection limits in
Brownfields assessment groundwater samples collected at the Site.

Metals
Barium was detected in each groundwater sample (up to 80.0 µg/L) at concentrations well below
the 2L Standard of 700 µg/L. Chromium was detected in TMW-3, upgradient of the building at
a concentration of 4.90 µg/L, which is below the 2L Standard of 10 µg/L. No other metals were
detected at concentrations above the laboratory detection limits in groundwater samples collected
16
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at the Site.

5.3 Vapor Intrusion Evaluation
The DEQ DWM Vapor Intrusion GWSLs used for comparison to the laboratory analytical
results are conservative and based upon a cumulative lifetime incremental carcinogenic risk
(LICR) of 1 x 10-5 for potential carcinogenic effects and a cumulative hazard quotient (HQ) of
0.2 for potential non-carcinogenic effects. Vapor intrusion mitigation or additional assessment is
not typically warranted if the calculated cumulative LICR is 1 x 10-4 or less and a calculated
cumulative Hazard Index (HI) of 1.0 or less. The HI is the sum of HQs for each individual target
compound.

As discussed in Section 1.2, results of the vapor intrusion assessment activities completed by
H&H in December 2019 did not indicate the potential for structural vapor intrusion into the
existing Site building at unacceptable levels. Based on the TCE concentration detected in TMW-
4, H&H utilized the DEQ Risk Calculator (July 2020) to confirm cumulative risks associated
with compound concentrations detected in the groundwater do not exceed acceptable levels.

The current planned use of the Site includes upfit for adaptive reuse as a multi-tenant
commercial building. Future redevelopment of the Site may include razing the existing Site
building for construction of multi-family residential use. Therefore, H&H used the highest
compound concentrations detected in any groundwater sample to simulate the hypothetical
“worst-case” scenario for both residential and non-residential uses. A copy of the completed risk
calculator is provided in Appendix E.

The results of the risk calculation assuming a residential-use scenario indicate a cumulative
worst case LICR of 7.5 x 10-6 and a HI of 0.34. The risk calculation results assuming a non-
residential scenario indicate a LICR of 1.6 x 10-6 and a HI of 0.082. Risk calculator results
indicate the worst-case LICR and HI under both use scenarios are well below the DEQ and EPA
acceptable risk levels and confirm the results of the vapor intrusion assessment indicating no
significant risk of structural vapor intrusion into the existing Site building. Because TCE was
17
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detected in Site groundwater at a concentration slightly above the DEQ DWM Residential Vapor
Intrusion GWSL, additional vapor intrusion assessment may be warranted in the event
redevelopment for residential use occurs in the future.
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6.0 Quality Assurance – Quality Control

For quality assurance and quality control purposes (QA/QC), field QA/QC samples were
analyzed along with the investigative samples to determine the potential variability introduced in
sampling, handling, shipping, and analysis. One trip blank was submitted for analysis of VOCs
by EPA Method 8260 for the groundwater sample shipment. To evaluate the reproducibility of
the sample results, H&H collected one duplicate soil sample and one duplicate groundwater
sample for laboratory analysis.

6.1 Trip Blank
The trip blank was prepared by the laboratory and consisted of certified-clean sample containers
filled with analyte-free water. The trip blank accompanied the empty laboratory sample
containers to the Site, remained within the sample cooler during sampling, and traveled back to
the laboratory with field samples. The purpose of a trip blank is to evaluate sample handling
conditions and the potential for external contaminants to compromise investigative samples
during transit. Laboratory analytical results of the trip blank did not indicate the presence of
VOCs above the laboratory method detection limits.

6.2 Field Duplicates

Field duplicate samples were collected to evaluate the precision of the field sampling procedures,
sample matrix variability, and analytical reproducibility. For VOC analytes, duplicate soil and
groundwater samples were collected directly into individual sample containers using sampling
methodologies described in previous sections. The samples were analyzed for the same
parameters as the parent samples, and the analytical results were compared with those of the
parent sample. The analytical results of the parent sample and the duplicate sample were used to
evaluate the cumulative precision because of the limitations of the analytical method, sample
matrix, and sample collection techniques. The results of the duplicate samples collected from
each sample medium are presented in the summary tables. As shown in Tables 1 and Table 3, the
duplicate sample results did not indicate significant variability compared with the results of the
parent samples.
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7.0 Summary and Conclusions

H&H has completed Brownfields assessment activities at the Kroehler Manufacturing
Brownfields property located in Charlotte, North Carolina. The assessment activities were
conducted in accordance with the DEQ Brownfields approved Work Plan dated June 11, 2020.
Brownfields assessment activities included collection of soil and groundwater samples for
laboratory analysis to evaluate the potential for impacts associated with historical on-Site and
nearby off-Site uses. In addition, receptor survey activities were completed to obtain
information about land use, water supply, basements, underground utilities, drains, and surface
water bodies in the vicinity of the Site. A brief summary of the Brownfields assessment
activities is provided below.

Soil Sampling
Laboratory analytical results did not indicate the presence organic compounds at concentrations
above the DEQ IHSB Residential and Industrial/Commercial PSRGs in soil samples collected in
the area of on-Site rail spur corridors. Arsenic was detected at a concentration above the DEQ
IHSB Residential and Industrial/Commercial PSRG and the Site-specific background range in
the composite soil sample collected near the active rail spur along the western and southwestern
Site boundaries. However, the arsenic concentration is within the published range of naturally
occurring levels in North Carolina soil and is likely representative of background conditions. No
other compounds were detected at concentrations above the DEQ IHSB PSRGs in Brownfields
assessment soil samples collected at the Site.

Groundwater Sampling
Laboratory analytical results did not indicate the presence of organic or inorganic compounds at
concentrations above the DEQ 2L Groundwater Quality Standards in Brownfields assessment
groundwater samples collected at the Site. TCE (1.7 µg/L) was detected in groundwater sample
TMW-4 collected downgradient and west of the Site building at a concentration slightly
exceeding the DEQ DWM Residential Vapor Intrusion GWSL of 1.0 µg/L, but below the Non-
Residential GWSL of 4.4 µg/L. No other compounds were detected at concentrations above the
DEQ DWM GWSLs in Brownfields assessment groundwater samples collected at the Site.
20
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Results of vapor intrusion risk evaluation using the DEQ Rick Calculator confirm that there are
no risks of structural vapor intrusion into the existing Site building. However, because the TCE
concentration in groundwater downgradient of the Site building exceeds the DEQ DWM
Residential Vapor Intrusion GWSL, additional assessment may be warranted prior to future
redevelopment for residential uses.

In summary, results of the Brownfields assessment activities did not identify significant exposure
risks to future Site workers or to future Site users. In addition, Brownfields assessment results
indicate that Site media can be managed in accordance with a DEQ Brownfields Program
approved Environmental Management Plan.

Table 1Summary of Soil Analytical DataKroehler ManufacturingCharlotte, North CarolinaBrownfields Project No. 23081-19-060H&H Job No. BCP-145 Location Sample IDBKG-1 BKG-2 Sample Date6/24/2020 6/24/2020 Depth (ft bgs)2-4 1-3Sample TypeGrab Composite Grab Composite Grab Composite Grab Grab Range Range Mean UnitsVOCs (8260B)Bromomethane 0.0115NA <0.0086 NA0.0101 JNA NA NA1.4 6.4-- -- --p-Isopropyltoluene 0.0129NA0.101NA <0.0035 NA NA NANE NE-- -- --Naphthalene 0.124NA0.0059NA0.0078NA NA NA4.1 18-- -- --Toluene<0.0031 NA0.0036 JNA <0.0036 NA NA NA990 9,700-- -- --SVOCs (8270D)Benzo(a)anthraceneNA1.040 JNA <0.629 NA <0.657 NA NA1.1 21-- -- --Benzo(b)fluorantheneNA0.897 JNA <0.796 NA <0.832 NA NA1.1 21-- -- --ChryseneNA0.804 JNA <0.574 NA <0.599 NA NA110 2,100-- -- --FluorantheneNA1.760 JNA <0.597 NA <0.624 NA NA480 6,000-- -- --PhenanthreneNA1.620 JNA <0.498 NA <0.520 NA NANE NE-- -- --PyreneNA1.430 JNA <0.544 NA0.575 JNA NA360 4,500-- -- --Metals (6020D/717471B/7199)ArsenicNA7.02NA6.44NA6.14<0.5722.810.68 3.0 ND - 2.811.0 - 18 4.8BariumNA133NA106NA99.617.4 39.33,100 47,000 17.4 - 39.350-1000 356CadmiumNA1.07 JNA1.37NA <0.528<0.550 <0.47514 200 ND1.0 - 10 4.3Chromium (Total)NA34.8NA19.5NA17.64.66 J 24.3NE NE 4.66 J - 24.37.0 - 300 65Hexavalent ChromiumNA <0.309 NA <0.316 NA <0.332<0.346 <0.2980.31 6.5 NDNS NSTrivalent ChromiumNA34.8NA19.5NA17.64.66 J 24.323,000 350,000 4.66 J - 24.3NS NSLeadNA183NA101NA16.47.92 12.6400 800 7.92 - 12.6ND - 50 16MercuryNA0.0390 JNA0.0370 JNA0.0417 J<0.02440.0267 J2.3 9.7 ND - 0.0267 J0.03 - 0.52 0.121SeleniumNA <1.22 NA <1.25 NA <1.31<1.37 <1.1878 1,200 ND<0.1 - 0.8 0.42SilverNA <0.258 NA <0.264 NA <0.277<0.289 <0.24978 1,200 NDND - 5.0 NSNotes:Compounds are reported to the laboratory method detection limit. With the exception of metals, only constituents detected in at least one sample are shown in the table above.Soil concentrations are reported in milligrams per kilogram (mg/kg).Bold indicates concentration exceeds the Residential PSRG.Underline indicates concentration exceeds the Industrial/Commercial PSRG.VOCs = volatile organic compounds; SVOCs = semi-VOCs; ft bgs = feet below ground surface -- = Not Applicable; NA = Not Analyzed; NE = Not Established; ND = Non Detect; NS = Not SpecifiedJ = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. Laboratory analytical methods are shown in parentheses.2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Drugan and Chekiri, 2005.mg/kgBackground Soil1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (December 2019). Active Rail Spur Inactive Rail SpurCOMP-1/COMP-DUP6/24/2020 6/24/2020COMP-20-2Regional Background Metals in Soil (2)0-2Industrial/Commercial PSRGs (1)Residential PSRGs (1)Site-Specfic Background Metals in SoilS:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-145 Monroe Road\Report\Tables\data tables_rev17/31/2020Table 1 (Page 1 of 1)Hart & Hickman, PC
Table 2Summary of Well Construction and Groundwater Elevation DataKroehler ManufacturingCharlotte, North CarolinaBrownfields Project No. 23081-19-060H&H Job No. BCP-145Well ID TOC Elevation (ft) Total Depth (ft) Screen Length (ft)Screened interval (ft bgs)Static Depth to Groundwater (ft below TOC)Groundwater Elevation (ft below TOC)TMW-3* 100.00 40 10 30-40 32.24 67.76TMW-4 97.60 40 10 30-40 30.41 67.19TMW-5 98.18 33 10 23-33 30.11 68.07 Notes:TMW = temporary monitoring well; TOC = top of casing; ft = feet; bgs = below ground surfaceDepth to groundwater measurements collected on June 25, 2020.*TOC elevation measured relative to TMW-3 set at an arbitrary elevation of 100.00.S:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-145 Monroe Road\Report\Tables\data tables_rev17/31/2020Table 2 (Page 1 of 1)Hart & Hickman, PC
Table 3Summary of Groundwater Analytical DataKroehler ManufacturingCharlotte, North CarolinaBrownfields Project No. 23081-19-060H&H Job No. BCP-145Sample IDTMW-3 TMW-4Date6/25/2020 6/25/2020LocationUpgradient DowngradientUnitsVOCs (8260B)Chloroform<2.34.9 J<2.3 <2.370 8.1 361,1-Dichloroethene<0.241.5<0.24 <0.24350 39 160Trichloroethene<0.221.7<0.22 <0.223 1.0 4.4SVOCs (8270D)ALL BDL ALL BDL ALL BDL ALL BDL -- -- --Metals (6020/7470)Arsenic<0.735 <0.735 <0.735 <0.73510-- --Barium74.4 34.1 80.0 79.7700-- --Cadmium<0.478 <0.478 <0.478 <0.4782-- --Chromium (total)4.90<1.49 <1.49 <1.4910-- --Lead<2.49 <2.49 <2.49 <2.4915-- --Mercury<0.100 <0.100 <0.100 <0.1001 0.18 75Selenium<0.657 <0.657 <0.657 <0.65720-- --Silver<0.513 <0.513 <0.513 <0.51320-- --Notes:1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) (April 2013).2) DEQ Division of Waste Management (DWM) Vapor Intrusion Groundwater Screening Level (GWSLs) (February 2018)Compounds are reported to the laboratory method detection limits. With the exception of metals, only constituents detected in at least one sample are shown in the table above.Concentrations are reported in micrograms per liter (µg/L).Laboratory analytical methods are shown in parentheses.Underline indicates concentration exceeds the Residential GWSL. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds-- = not applicable; BDL = below laboratory method detection limits; NE = not establishedJ = compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.µg/LDowngradient6/25/20202L Standards (1)Residential GWSLs(2) Non-Residential GWSLs(2)TMW-5/DUP-1S:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-145 Monroe Road\Report\Tables\data tables_rev17/31/2020Table 3 (Page 1 of 1)Hart & Hickman, PC
TITLE
PROJECT
SITE LOCATION MAP
KROEHLER MANUFACTURING3412 MONROE ROADCHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
5-22-20 0
1BCP-145
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE EAST, NC, 1991
706704
702700 696
708
710
70
8 712714712710714716
718
7
0
4
7
0
67087107
0
4
7
0
2
70
0
698
696
696
694
692
7
0
6704702700
698
698
REVISION NO. 0
JOB NO. BCP-145
DATE: 6-4-20
FIGURE NO. 2
KROEHLER MANUFACTURING
3412 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
SITE MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
RAILROAD
TOPOGRAPHIC CONTOUR AND
ELEVATION (FT ABOVE MSL)
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
704
MO
N
R
O
E

R
O
A
DMO
N
R
O
E

R
O
A
D
CHIPL
E
Y

A
V
E
N
U
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CHIPL
E
Y
A
V
E
N
U
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FOR
T
U
N
E
S
T
R
E
E
T
FOR
T
U
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E
S
T
R
E
E
T
DOMI
N
O C
O
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R
T
DOMI
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O
C
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PRO AM DRIVEPRO AM DRIVELAT
R
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B
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D
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LAT
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D
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NOTES:
1.AERIAL IMAGERY AND LIDAR ELEVATION DATA
OBTAINED FROM MECKLENBURG COUNTY GIS
(2019).
2.FT ABOVE MSL = FEET ABOVE MEAN SEA LEVEL
CAROLINA PRODUCTS
(1132 PRO AM DRIVE)
THE DOG KNOWLEDGE
(1110 PRO AM DRIVE)
ATLANTIC SELF STORAGE AND
PENSKE TRUCK RENTAL
(3434 MONROE ROAD)
(FORMER ATLANTIC ENVELOPE)
TECHNOCOM
(3330 MONROE ROAD)
ATLANTIC SWEETENER
(512 DOMINO COURT)
RESIDENTIAL
LOADING DOCKS
LOADING DOCKS
FORMER DRUM STORAGE
BUILDING AND SUMP
LOWER LEVEL
BASEMENT
ABANDONED
RAILROAD SPUR
ACTIVE
RAILROAD SPUR
\\hhfs01\MasterFiles\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-145 Monroe Road\Figures\BF Site Map.dwg, 7/29/2020 3:08:40 PM, amckenzie
1,500 FT
1,500 FT
REVISION NO. 0
JOB NO. BCP-145
DATE: 7-24-20
FIGURE NO. 3
KROEHLER MANUFACTURING
3412 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
RECEPTOR SURVEY MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
RAILROAD
WATER LINE
UNDERGROUND ELECTRIC LINE
NATURAL GAS LINE
SANITARY SEWER LINE
BURIED TELECOMMUNICATION LINE
INDUSTRIAL USE
RESIDENTIAL USE
COMMERCIAL/OFFICE USE
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1.AERIAL IMAGERY AND LIDAR ELEVATION DATA
OBTAINED FROM MECKLENBURG COUNTY GIS
(2019).
2.ZONING OBTAINED FROM MECKLENBURG COUNTY
GIS (2019).S:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-145 Monroe Road\Figures\BF Site Map.dwg, 8/4/2020 11:51:36 AM, amckenzie
IAR-4
SSR-4
SSV-4
IAR-3
SSR-3SSV-3
IAR-2
SSR-2SSV-2
IAR-1
SSR-1SSV-1
SB-5
SB-4
SB-3
SB-6
TMW-2/SB-2
TMW-1/SB-1
COMP-2
COMP-1
TMW-3/BKG-1
TMW-4
TMW-5
BKG-2
REVISION NO. 0
JOB NO. BCP-145
DATE: 7-29-20
FIGURE NO. 4
KROEHLER MANUFACTURING
3412 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
RAILROAD
FLOOR DRAIN
HISTORICAL SOIL BORING LOCATION
(SEPTEMBER 2019)
HISTORICAL CO-LOCATED SOIL
BORING/TEMPORARY MONITORING WELL
LOCATION (SEPTEMBER 2019)
HISTORICAL SUB-SLAB SOIL VAPOR
MONITORING POINT (DECEMBER 2019)
HISTORICAL CO-LOCATED SUB-SLAB AND
INDOOR AIR RADON SAMPLE LOCATION
(DECEMBER 2019)
ALIQUOT SOIL BORING LOCATION
BACKGROUND SOIL BORING LOCATION
TEMPORARY GROUNDWATER MONITORING
WELL LOCATION
CO-LOCATED TEMPORARY GROUNDWATER
MONITORING WELL AND BACKGROUND SOIL
BORING LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 GeologyMO
N
R
O
E

R
O
A
DMO
N
R
O
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R
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A
D
CHIPL
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Y

A
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CHIPL
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Y
A
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U
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FOR
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FOR
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DOMI
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DOMI
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PRO AM DRIVEPRO AM DRIVELAT
R
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B
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LAT
R
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B
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D
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NOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS (2019).
2.PREVIOUS SOIL AND GROUNDWATER SAMPLES
COLLECTED BY H&H IN SEPTEMBER 2019.
3.SUB-SLAB SOIL VAPOR AND RADON SAMPLES
COLLECTED BY H&H IN DECEMBER 2019.S:\AAA-Master Projects\Beacon Partners- BEP or BCP\BCP-145 Monroe Road\Figures\BF Site Map.dwg, 7/31/2020 7:29:43 AM, amckenzie

Appendix A

Brownfields Property Receptor Survey Form
a. Provide occupancy and use information.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
NASize of Property (acres)
% of property that is wooded/brush
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the
information requested below. Distances are measured from the site property boundary unless otherwise indicated
by the DEQ Brownfield’s Project Manager (PM).
Site:
Address:
City:
County:
Brownfields Project Number:
Date
Property and Building Characteristics
Current Usage Proposed UsageSurface Conditions
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air
return, and design considerations (e.g. positive pressure?).
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets
as needed. If numerous buildings are on-site, consult with your PM as only information on specific buildings may
be needed.
b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings
(e.g. windows, bay doors), and height (number of stories).
% of property that is covered by buildings
Rev. 09/2015 Page 1 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East
West
Utilities
Is there a septic system on-site? (Y or N) _________
Please provide the utility providers for the subject property
a. Natural Gas ___________________________
b. Sewer ___________________________
c. Electricity ___________________________
d. Other __________________________
For surrounding properties, please complete the following table with available information.
Zoning/Land Use
DirectionDistance
(ft)Address
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with
the subject property.
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
Is there a basement within 1,000 ft of the Property
Please provide information on the following land uses in the vicinity of the subject site, including a map of the
surrounding areas. If specific receptors are present, please provide addresses of the facilities.
Proposed Usage Current Use/Occupant
For the subject property, please provide a map of known buried utilites. If available, include depth to top,
construction material, and diameter of the utilities. In addition, please provide the following information on utilty
providers. If additional assessment is required, the public utility locators should be contacted. This information
can then be added to a site map.
Y/N *
Is a school or daycare center within 1,000 ft of the
Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific
addresses.
Distance
(ft)
Is there a residence within 1,000 ft of the Property?
Utility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is a sanitary sewer within 100 ft of the Property boundary?
Rev. 09/2015 Page 2 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public ______ Private ______
Surface Water & Wetlands
Distance
(ft)Direction AddressY/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a
minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if
water supply or irrigation wells may be present. Information from applicable databases can and should be
utilized; however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the
requested radius, please provide a map of the well locations. If needed, please attach a separate table to list all
wells. Please note, the PM may opt for a more extensive water supply well survey if needed.
Are there surface water features on the
property? (If yes, please complete a. to d.)
Provide Information regarding Surface Water
and Wetlands
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public,
please include the water providers name.
a. Is the water body naturally developed or
man-made?
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property
boundary?Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in
the vicinity of the Property.
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
b. List the uses of the water body.
c. What is the source of the water for the
water body?
d. What is the nature of the bottom of the
water body (e.g., rocky or concrete bottom,
drainage ways or impoundments)
If no on-site surface water features, what is the
nearest surface water body?
Are there any wetlands present on the
property? If no wetlands on-site, are wetlands
suspected on adjoining properties?
Rev. 09/2015 Page 3 of 3

Appendix B

Boring Logs
NOTES: Hole precleared to 5.0' on 6/24/20 by IET using hand auger. Background soil sample BKG-1 collected from 2-4 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-145
3412 Monroe Road, Charlotte, NC
WELL LOG
Well No.
Page:
TMW-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/24/20
6/24/20
IET
Direct Push
Powerprobe 9510
TR
Alexis McKenzie
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
40.0 Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
40.0
1.0
0.020
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Pellets
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
40
(0') Silty CLAY (CL); medium plasticity, soft, slightly moist, light brown, tan
(5') Silty CLAY (CL); medium plasticity, soft, slightly moist, light brown, black mottling
(18') As Above: moist, orange-ish
(28') As Above: tan
16.1
17.8
17.4
27.9
30.8
32.6
24.6
16.4
28.5
24.2
12.5
BKG-1
0
5
10
15
20
25
30
35
40
(40') Boring terminated
NOTES: Hole precleared to 5.0' on 6/24/20 by IET using hand auger. Drill rig refusal at 40 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-145
3412 Monroe Road, Charlotte, NC
WELL LOG
Well No.
Page:
TMW-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/24/20
6/24/20
IET
Direct Push
Powerprobe 9510
TR
Alexis McKenzie
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
40.0 Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
40.0
1.0
0.020
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Pellets
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
40
(0') Asphalt
(0.5') Silty CLAY (CL); medium plasticity, stiff, dry, dark reddish-brown
(12') As Above: slightly orange
(16') As Above: light brown
(24') As Above: moist, saprolite
11.2
8.5
7.5
40.1
32.6
38.5
46.9
45.5
30.8
19.7
18.9
0
5
10
15
20
25
30
35
40
(40') Boring terminated
NOTES: Hole precleared to 5.0' on 6/24/20 by IET using hand auger. Drill rig refusal at 33 ft bgs.
generated using GroundLogs.online
Client:
Project:
Address:
Beacon Partners
BCP-145
3412 Monroe Road, Charlotte, NC
WELL LOG
Well No.
Page:
TMW-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
6/24/20
6/24/20
IET
Direct Push
Powerprobe 9510
TR
Alexis McKenzie
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
33.0 Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
33.0
1.0
0.020
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Pellets
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
40
(0') Asphalt
(0.25') Poorly graded GRAVEL (GP)
(0.5') Silty CLAY (CL); medium plasticity, soft, slightly moist, reddish-brown
(5') As Above: dark brown
(6') Silty CLAY (CL); medium plasticity, medium stiff, slightly moist, reddish-
brown
(15') As Above: orange-red, soft
(21') Clayey SILT (ML); soft, slightly moist, light brown, tan
(33') Boring terminated
28.2
22.2
20.3
78.0
42.6
30.6
20.1
33.9
32.7
32.6
0
5
10
15
20
25
30
35
40

Appendix C

Laboratory Analytical Report
#=CL#
July 31, 2020
LIMS USE: FR - ALEXIS MCKENZIE
LIMS OBJECT ID: 92483554
92483554
Project:
Pace Project No.:
RE:
Alexis McKenzie
Hart & Hickman
2923 S Tryon Street
Suite 100
Charlotte, NC 28203
BCP-145
Dear Alexis McKenzie:
Enclosed are the analytical results for sample(s) received by the laboratory on June 25, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
Report revised 7/31/20 to include re-run results for TMW-5 EPA 6020 Chromium.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 85
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92483554
BCP-145
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 85
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92483554
BCP-145
Lab ID Sample ID Matrix Date Collected Date Received
92483554001 TMW-3 Water 06/25/20 09:50 06/25/20 13:30
92483554002 TMW-4 Water 06/25/20 08:40 06/25/20 13:30
92483554003 TMW-5 Water 06/25/20 07:05 06/25/20 13:30
92483554004 DUP-1 Water 06/25/20 00:00 06/25/20 13:30
92483554005 COMP-1 Solid 06/24/20 16:25 06/25/20 13:30
92483554006 COMP-2 Solid 06/24/20 16:30 06/25/20 13:30
92483554007 COMP-DUP Solid 06/24/20 00:00 06/25/20 13:30
92483554008 BKG-1 Solid 06/24/20 16:10 06/25/20 13:30
92483554009 BKG-2 Solid 06/24/20 16:15 06/25/20 13:30
92483554010 TRIP BLANK Water 06/24/20 00:00 06/25/20 13:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 85
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92483554
BCP-145
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92483554001 TMW-3 EPA 6020B 7 PANLD
EPA 7470A 1 PANTCT
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92483554002 TMW-4 EPA 6020B 7 PANLD
EPA 7470A 1 PANTCT
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92483554003 TMW-5 EPA 6020B 7 PANJPD, LD
EPA 7470A 1 PANTCT
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92483554004 DUP-1 EPA 6020B 7 PANLD
EPA 7470A 1 PANTRB
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92483554005 COMP-1 EPA 6020B 7 PANLAT
EPA 7471B 1 PANTRB
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92483554006 COMP-2 EPA 6020B 7 PANLAT
EPA 7471B 1 PANTRB
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92483554007 COMP-DUP EPA 6020B 7 PANLAT
EPA 7471B 1 PANTRB
EPA 8270E 75 PASI-CPKS
EPA 8260D 70 PASI-CSAS
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 85
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92483554
BCP-145
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92483554008 BKG-1 EPA 6020B 7 PANLAT
EPA 7471B 1 PANTRB
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92483554009 BKG-2 EPA 6020B 7 PANLAT
EPA 7471B 1 PANTRB
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92483554010 TRIP BLANK EPA 8260D 63 PASI-CSAS
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-3 Lab ID:92483554001 Collected:06/25/20 09:50 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/30/20 17:14 7440-38-206/30/20 10:422.00 0.735 1
Barium 74.4 ug/L 06/30/20 17:14 7440-39-306/30/20 10:4220.0 7.78 1
Cadmium ND ug/L 06/30/20 17:14 7440-43-906/30/20 10:421.00 0.478 1
Chromium 4.90 ug/L 06/30/20 17:14 7440-47-306/30/20 10:422.00 1.49 1
Lead ND ug/L 06/30/20 17:14 7439-92-106/30/20 10:425.00 2.49 1
Selenium ND ug/L 06/30/20 17:14 7782-49-206/30/20 10:422.00 0.657 1
Silver ND ug/L 06/30/20 17:14 7440-22-406/30/20 10:422.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/29/20 18:45 7439-97-606/29/20 09:180.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/28/20 18:23 83-32-906/26/20 16:5410.0 1.4 1
Acenaphthylene ND ug/L 06/28/20 18:23 208-96-806/26/20 16:5410.0 1.5 1
Aniline ND ug/L 06/28/20 18:23 62-53-306/26/20 16:5410.0 1.6 1
Anthracene ND ug/L 06/28/20 18:23 120-12-706/26/20 16:5410.0 1.6 1
Benzo(a)anthracene ND ug/L 06/28/20 18:23 56-55-306/26/20 16:5410.0 1.5 1
Benzo(a)pyrene ND ug/L 06/28/20 18:23 50-32-806/26/20 16:5410.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/28/20 18:23 205-99-206/26/20 16:5410.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/28/20 18:23 191-24-206/26/20 16:5410.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/28/20 18:23 207-08-906/26/20 16:5410.0 1.5 1
Benzoic Acid ND ug/L 06/28/20 18:23 65-85-006/26/20 16:5450.0 19.5 1
Benzyl alcohol ND ug/L 06/28/20 18:23 100-51-606/26/20 16:5420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/28/20 18:23 101-55-306/26/20 16:5410.0 1.2 1
Butylbenzylphthalate ND ug/L 06/28/20 18:23 85-68-706/26/20 16:5410.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/28/20 18:23 59-50-706/26/20 16:5410.0 2.8 1
4-Chloroaniline ND ug/L 06/28/20 18:23 106-47-806/26/20 16:5420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/28/20 18:23 111-91-106/26/20 16:5410.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/28/20 18:23 111-44-406/26/20 16:5410.0 1.7 1
2-Chloronaphthalene ND ug/L 06/28/20 18:23 91-58-706/26/20 16:5410.0 1.4 1
2-Chlorophenol ND ug/L 06/28/20 18:23 95-57-806/26/20 16:5410.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/28/20 18:23 7005-72-306/26/20 16:5410.0 1.5 1
Chrysene ND ug/L 06/28/20 18:23 218-01-906/26/20 16:5410.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/28/20 18:23 53-70-306/26/20 16:5410.0 1.6 1
Dibenzofuran ND ug/L 06/28/20 18:23 132-64-906/26/20 16:5410.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/28/20 18:23 95-50-106/26/20 16:5410.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/28/20 18:23 541-73-106/26/20 16:5410.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/28/20 18:23 106-46-706/26/20 16:5410.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/28/20 18:23 91-94-106/26/20 16:5420.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/28/20 18:23 120-83-206/26/20 16:5410.0 1.5 1
Diethylphthalate ND ug/L 06/28/20 18:23 84-66-206/26/20 16:5410.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/28/20 18:23 105-67-906/26/20 16:5410.0 1.5 1
Dimethylphthalate ND ug/L 06/28/20 18:23 131-11-306/26/20 16:5410.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-3 Lab ID:92483554001 Collected:06/25/20 09:50 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/28/20 18:23 84-74-206/26/20 16:5410.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/28/20 18:23 534-52-106/26/20 16:5420.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/28/20 18:23 51-28-506/26/20 16:5450.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/28/20 18:23 121-14-206/26/20 16:5410.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/28/20 18:23 606-20-206/26/20 16:5410.0 1.7 1
Di-n-octylphthalate ND ug/L 06/28/20 18:23 117-84-006/26/20 16:5410.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/28/20 18:23 117-81-706/26/20 16:546.0 2.0 1
Fluoranthene ND ug/L 06/28/20 18:23 206-44-006/26/20 16:5410.0 1.6 1
Fluorene ND ug/L 06/28/20 18:23 86-73-706/26/20 16:5410.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/28/20 18:23 87-68-306/26/20 16:5410.0 1.6 1
Hexachlorobenzene ND ug/L 06/28/20 18:23 118-74-106/26/20 16:5410.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/28/20 18:23 77-47-406/26/20 16:5410.0 2.4 1
Hexachloroethane ND ug/L 06/28/20 18:23 67-72-106/26/20 16:5410.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/28/20 18:23 193-39-506/26/20 16:5410.0 1.7 1
Isophorone ND ug/L 06/28/20 18:23 78-59-106/26/20 16:5410.0 1.3 1
1-Methylnaphthalene ND ug/L 06/28/20 18:23 90-12-006/26/20 16:5410.0 1.4 1
2-Methylnaphthalene ND ug/L 06/28/20 18:23 91-57-606/26/20 16:5410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/28/20 18:23 95-48-706/26/20 16:5410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/28/20 18:23 15831-10-406/26/20 16:5410.0 1.2 1
Naphthalene ND ug/L 06/28/20 18:23 91-20-306/26/20 16:5410.0 1.6 1
2-Nitroaniline ND ug/L 06/28/20 18:23 88-74-406/26/20 16:5420.0 3.0 1
3-Nitroaniline ND ug/L 06/28/20 18:23 99-09-206/26/20 16:5420.0 2.8 1
4-Nitroaniline ND ug/L 06/28/20 18:23 100-01-606/26/20 16:5420.0 3.1 1
Nitrobenzene ND ug/L 06/28/20 18:23 98-95-306/26/20 16:5410.0 1.5 1
2-Nitrophenol ND ug/L 06/28/20 18:23 88-75-506/26/20 16:5410.0 1.7 1
4-Nitrophenol ND ug/L 06/28/20 18:23 100-02-706/26/20 16:5450.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/28/20 18:23 62-75-906/26/20 16:5410.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/28/20 18:23 621-64-706/26/20 16:5410.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/28/20 18:23 86-30-606/26/20 16:5410.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/28/20 18:23 108-60-106/26/20 16:5410.0 1.3 1
Pentachlorophenol ND ug/L 06/28/20 18:23 87-86-506/26/20 16:5420.0 2.8 1
Phenanthrene ND ug/L 06/28/20 18:23 85-01-806/26/20 16:5410.0 1.4 1
Phenol ND ug/L 06/28/20 18:23 108-95-206/26/20 16:5410.0 1.5 1
Pyrene ND ug/L 06/28/20 18:23 129-00-006/26/20 16:5410.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/28/20 18:23 120-82-106/26/20 16:5410.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/28/20 18:23 95-95-406/26/20 16:5410.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/28/20 18:23 88-06-206/26/20 16:5410.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)49 %06/28/20 18:23 4165-60-006/26/20 16:5413-130 1
2-Fluorobiphenyl (S)48 %06/28/20 18:23 321-60-806/26/20 16:5413-130 1
Terphenyl-d14 (S)78 %06/28/20 18:23 1718-51-006/26/20 16:5425-130 1
Phenol-d6 (S)28 %06/28/20 18:23 13127-88-306/26/20 16:5410-130 1
2-Fluorophenol (S)35 %06/28/20 18:23 367-12-406/26/20 16:5410-130 1
2,4,6-Tribromophenol (S)52 %06/28/20 18:23 118-79-606/26/20 16:5410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-3 Lab ID:92483554001 Collected:06/25/20 09:50 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/26/20 03:47 67-64-125.0 6.2 1
Benzene ND ug/L 06/26/20 03:47 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/26/20 03:47 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/26/20 03:47 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/26/20 03:47 75-27-41.0 0.26 1
Bromoform ND ug/L 06/26/20 03:47 75-25-21.0 0.62 1
Bromomethane ND ug/L 06/26/20 03:47 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 06/26/20 03:47 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/26/20 03:47 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/26/20 03:47 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/26/20 03:47 75-00-31.0 0.49 1
Chloroform ND ug/L 06/26/20 03:47 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/26/20 03:47 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 06/26/20 03:47 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/26/20 03:47 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/26/20 03:47 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/26/20 03:47 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/26/20 03:47 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/26/20 03:47 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/26/20 03:47 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/26/20 03:47 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/26/20 03:47 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/26/20 03:47 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/26/20 03:47 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/26/20 03:47 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/26/20 03:47 75-35-4 v21.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/26/20 03:47 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/26/20 03:47 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/26/20 03:47 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/26/20 03:47 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/26/20 03:47 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/26/20 03:47 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/26/20 03:47 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/26/20 03:47 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/26/20 03:47 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/26/20 03:47 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/26/20 03:47 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/26/20 03:47 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/26/20 03:47 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/26/20 03:47 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/26/20 03:47 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/26/20 03:47 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/26/20 03:47 91-20-31.0 0.35 1
Styrene ND ug/L 06/26/20 03:47 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/26/20 03:47 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-3 Lab ID:92483554001 Collected:06/25/20 09:50 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/26/20 03:47 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/26/20 03:47 127-18-41.0 0.16 1
Toluene ND ug/L 06/26/20 03:47 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/26/20 03:47 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/26/20 03:47 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/26/20 03:47 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/26/20 03:47 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/26/20 03:47 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/26/20 03:47 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/26/20 03:47 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/26/20 03:47 108-05-4 IK2.0 1.4 1
Vinyl chloride ND ug/L 06/26/20 03:47 75-01-4 v21.0 0.24 1
Xylene (Total)ND ug/L 06/26/20 03:47 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/26/20 03:47 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/26/20 03:47 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)98 %06/26/20 03:47 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/26/20 03:47 17060-07-070-130 1
Toluene-d8 (S)99 %06/26/20 03:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-4 Lab ID:92483554002 Collected:06/25/20 08:40 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/30/20 17:18 7440-38-206/30/20 10:422.00 0.735 1
Barium 34.1 ug/L 06/30/20 17:18 7440-39-306/30/20 10:4220.0 7.78 1
Cadmium ND ug/L 06/30/20 17:18 7440-43-906/30/20 10:421.00 0.478 1
Chromium ND ug/L 06/30/20 17:18 7440-47-306/30/20 10:422.00 1.49 1
Lead ND ug/L 06/30/20 17:18 7439-92-106/30/20 10:425.00 2.49 1
Selenium ND ug/L 06/30/20 17:18 7782-49-206/30/20 10:422.00 0.657 1
Silver ND ug/L 06/30/20 17:18 7440-22-406/30/20 10:422.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/29/20 18:47 7439-97-606/29/20 09:180.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/28/20 18:49 83-32-906/26/20 16:5410.0 1.4 1
Acenaphthylene ND ug/L 06/28/20 18:49 208-96-806/26/20 16:5410.0 1.5 1
Aniline ND ug/L 06/28/20 18:49 62-53-306/26/20 16:5410.0 1.6 1
Anthracene ND ug/L 06/28/20 18:49 120-12-706/26/20 16:5410.0 1.6 1
Benzo(a)anthracene ND ug/L 06/28/20 18:49 56-55-306/26/20 16:5410.0 1.5 1
Benzo(a)pyrene ND ug/L 06/28/20 18:49 50-32-806/26/20 16:5410.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/28/20 18:49 205-99-206/26/20 16:5410.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/28/20 18:49 191-24-206/26/20 16:5410.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/28/20 18:49 207-08-906/26/20 16:5410.0 1.5 1
Benzoic Acid ND ug/L 06/28/20 18:49 65-85-006/26/20 16:5450.0 19.5 1
Benzyl alcohol ND ug/L 06/28/20 18:49 100-51-606/26/20 16:5420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/28/20 18:49 101-55-306/26/20 16:5410.0 1.2 1
Butylbenzylphthalate ND ug/L 06/28/20 18:49 85-68-706/26/20 16:5410.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/28/20 18:49 59-50-706/26/20 16:5410.0 2.8 1
4-Chloroaniline ND ug/L 06/28/20 18:49 106-47-806/26/20 16:5420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/28/20 18:49 111-91-106/26/20 16:5410.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/28/20 18:49 111-44-406/26/20 16:5410.0 1.7 1
2-Chloronaphthalene ND ug/L 06/28/20 18:49 91-58-706/26/20 16:5410.0 1.4 1
2-Chlorophenol ND ug/L 06/28/20 18:49 95-57-806/26/20 16:5410.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/28/20 18:49 7005-72-306/26/20 16:5410.0 1.5 1
Chrysene ND ug/L 06/28/20 18:49 218-01-906/26/20 16:5410.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/28/20 18:49 53-70-306/26/20 16:5410.0 1.6 1
Dibenzofuran ND ug/L 06/28/20 18:49 132-64-906/26/20 16:5410.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/28/20 18:49 95-50-106/26/20 16:5410.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/28/20 18:49 541-73-106/26/20 16:5410.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/28/20 18:49 106-46-706/26/20 16:5410.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/28/20 18:49 91-94-106/26/20 16:5420.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/28/20 18:49 120-83-206/26/20 16:5410.0 1.5 1
Diethylphthalate ND ug/L 06/28/20 18:49 84-66-206/26/20 16:5410.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/28/20 18:49 105-67-906/26/20 16:5410.0 1.5 1
Dimethylphthalate ND ug/L 06/28/20 18:49 131-11-306/26/20 16:5410.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-4 Lab ID:92483554002 Collected:06/25/20 08:40 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/28/20 18:49 84-74-206/26/20 16:5410.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/28/20 18:49 534-52-106/26/20 16:5420.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/28/20 18:49 51-28-506/26/20 16:5450.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/28/20 18:49 121-14-206/26/20 16:5410.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/28/20 18:49 606-20-206/26/20 16:5410.0 1.7 1
Di-n-octylphthalate ND ug/L 06/28/20 18:49 117-84-006/26/20 16:5410.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/28/20 18:49 117-81-706/26/20 16:546.0 2.0 1
Fluoranthene ND ug/L 06/28/20 18:49 206-44-006/26/20 16:5410.0 1.6 1
Fluorene ND ug/L 06/28/20 18:49 86-73-706/26/20 16:5410.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/28/20 18:49 87-68-306/26/20 16:5410.0 1.6 1
Hexachlorobenzene ND ug/L 06/28/20 18:49 118-74-106/26/20 16:5410.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/28/20 18:49 77-47-406/26/20 16:5410.0 2.4 1
Hexachloroethane ND ug/L 06/28/20 18:49 67-72-106/26/20 16:5410.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/28/20 18:49 193-39-506/26/20 16:5410.0 1.7 1
Isophorone ND ug/L 06/28/20 18:49 78-59-106/26/20 16:5410.0 1.3 1
1-Methylnaphthalene ND ug/L 06/28/20 18:49 90-12-006/26/20 16:5410.0 1.4 1
2-Methylnaphthalene ND ug/L 06/28/20 18:49 91-57-606/26/20 16:5410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/28/20 18:49 95-48-706/26/20 16:5410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/28/20 18:49 15831-10-406/26/20 16:5410.0 1.2 1
Naphthalene ND ug/L 06/28/20 18:49 91-20-306/26/20 16:5410.0 1.6 1
2-Nitroaniline ND ug/L 06/28/20 18:49 88-74-406/26/20 16:5420.0 3.0 1
3-Nitroaniline ND ug/L 06/28/20 18:49 99-09-206/26/20 16:5420.0 2.8 1
4-Nitroaniline ND ug/L 06/28/20 18:49 100-01-606/26/20 16:5420.0 3.1 1
Nitrobenzene ND ug/L 06/28/20 18:49 98-95-306/26/20 16:5410.0 1.5 1
2-Nitrophenol ND ug/L 06/28/20 18:49 88-75-506/26/20 16:5410.0 1.7 1
4-Nitrophenol ND ug/L 06/28/20 18:49 100-02-706/26/20 16:5450.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/28/20 18:49 62-75-906/26/20 16:5410.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/28/20 18:49 621-64-706/26/20 16:5410.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/28/20 18:49 86-30-606/26/20 16:5410.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/28/20 18:49 108-60-106/26/20 16:5410.0 1.3 1
Pentachlorophenol ND ug/L 06/28/20 18:49 87-86-506/26/20 16:5420.0 2.8 1
Phenanthrene ND ug/L 06/28/20 18:49 85-01-806/26/20 16:5410.0 1.4 1
Phenol ND ug/L 06/28/20 18:49 108-95-206/26/20 16:5410.0 1.5 1
Pyrene ND ug/L 06/28/20 18:49 129-00-006/26/20 16:5410.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/28/20 18:49 120-82-106/26/20 16:5410.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/28/20 18:49 95-95-406/26/20 16:5410.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/28/20 18:49 88-06-206/26/20 16:5410.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)54 %06/28/20 18:49 4165-60-006/26/20 16:5413-130 1
2-Fluorobiphenyl (S)49 %06/28/20 18:49 321-60-806/26/20 16:5413-130 1
Terphenyl-d14 (S)100 %06/28/20 18:49 1718-51-006/26/20 16:5425-130 1
Phenol-d6 (S)31 %06/28/20 18:49 13127-88-306/26/20 16:5410-130 1
2-Fluorophenol (S)38 %06/28/20 18:49 367-12-406/26/20 16:5410-130 1
2,4,6-Tribromophenol (S)58 %06/28/20 18:49 118-79-606/26/20 16:5410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-4 Lab ID:92483554002 Collected:06/25/20 08:40 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/26/20 04:05 67-64-125.0 6.2 1
Benzene ND ug/L 06/26/20 04:05 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/26/20 04:05 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/26/20 04:05 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/26/20 04:05 75-27-41.0 0.26 1
Bromoform ND ug/L 06/26/20 04:05 75-25-21.0 0.62 1
Bromomethane ND ug/L 06/26/20 04:05 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 06/26/20 04:05 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/26/20 04:05 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/26/20 04:05 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/26/20 04:05 75-00-31.0 0.49 1
Chloroform 4.9J ug/L 06/26/20 04:05 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/26/20 04:05 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 06/26/20 04:05 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/26/20 04:05 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/26/20 04:05 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/26/20 04:05 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/26/20 04:05 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/26/20 04:05 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/26/20 04:05 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/26/20 04:05 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/26/20 04:05 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/26/20 04:05 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/26/20 04:05 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/26/20 04:05 107-06-21.0 0.34 1
1,1-Dichloroethene 1.5 ug/L 06/26/20 04:05 75-35-4 v31.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/26/20 04:05 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/26/20 04:05 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/26/20 04:05 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/26/20 04:05 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/26/20 04:05 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/26/20 04:05 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/26/20 04:05 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/26/20 04:05 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/26/20 04:05 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/26/20 04:05 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/26/20 04:05 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/26/20 04:05 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/26/20 04:05 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/26/20 04:05 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/26/20 04:05 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/26/20 04:05 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/26/20 04:05 91-20-31.0 0.35 1
Styrene ND ug/L 06/26/20 04:05 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/26/20 04:05 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
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Page 12 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-4 Lab ID:92483554002 Collected:06/25/20 08:40 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/26/20 04:05 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/26/20 04:05 127-18-41.0 0.16 1
Toluene ND ug/L 06/26/20 04:05 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/26/20 04:05 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/26/20 04:05 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/26/20 04:05 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/26/20 04:05 79-00-51.0 0.24 1
Trichloroethene 1.7 ug/L 06/26/20 04:05 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/26/20 04:05 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/26/20 04:05 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/26/20 04:05 108-05-4 IK2.0 1.4 1
Vinyl chloride ND ug/L 06/26/20 04:05 75-01-4 v21.0 0.24 1
Xylene (Total)ND ug/L 06/26/20 04:05 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/26/20 04:05 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/26/20 04:05 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)100 %06/26/20 04:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %06/26/20 04:05 17060-07-070-130 1
Toluene-d8 (S)99 %06/26/20 04:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-5 Lab ID:92483554003 Collected:06/25/20 07:05 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/30/20 17:21 7440-38-206/30/20 10:422.00 0.735 1
Barium 80.0 ug/L 06/30/20 17:21 7440-39-306/30/20 10:4220.0 7.78 1
Cadmium ND ug/L 06/30/20 17:21 7440-43-906/30/20 10:421.00 0.478 1
Chromium ND ug/L 07/30/20 15:17 7440-47-307/29/20 21:112.00 1.49 1
Lead ND ug/L 06/30/20 17:21 7439-92-106/30/20 10:425.00 2.49 1
Selenium ND ug/L 06/30/20 17:21 7782-49-206/30/20 10:422.00 0.657 1
Silver ND ug/L 06/30/20 17:21 7440-22-406/30/20 10:422.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/29/20 18:53 7439-97-606/29/20 09:180.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/28/20 19:14 83-32-906/26/20 16:5410.0 1.4 1
Acenaphthylene ND ug/L 06/28/20 19:14 208-96-806/26/20 16:5410.0 1.5 1
Aniline ND ug/L 06/28/20 19:14 62-53-306/26/20 16:5410.0 1.6 1
Anthracene ND ug/L 06/28/20 19:14 120-12-706/26/20 16:5410.0 1.6 1
Benzo(a)anthracene ND ug/L 06/28/20 19:14 56-55-306/26/20 16:5410.0 1.5 1
Benzo(a)pyrene ND ug/L 06/28/20 19:14 50-32-806/26/20 16:5410.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/28/20 19:14 205-99-206/26/20 16:5410.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/28/20 19:14 191-24-206/26/20 16:5410.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/28/20 19:14 207-08-906/26/20 16:5410.0 1.5 1
Benzoic Acid ND ug/L 06/28/20 19:14 65-85-006/26/20 16:5450.0 19.5 1
Benzyl alcohol ND ug/L 06/28/20 19:14 100-51-606/26/20 16:5420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/28/20 19:14 101-55-306/26/20 16:5410.0 1.2 1
Butylbenzylphthalate ND ug/L 06/28/20 19:14 85-68-706/26/20 16:5410.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/28/20 19:14 59-50-706/26/20 16:5410.0 2.8 1
4-Chloroaniline ND ug/L 06/28/20 19:14 106-47-806/26/20 16:5420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/28/20 19:14 111-91-106/26/20 16:5410.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/28/20 19:14 111-44-406/26/20 16:5410.0 1.7 1
2-Chloronaphthalene ND ug/L 06/28/20 19:14 91-58-706/26/20 16:5410.0 1.4 1
2-Chlorophenol ND ug/L 06/28/20 19:14 95-57-806/26/20 16:5410.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/28/20 19:14 7005-72-306/26/20 16:5410.0 1.5 1
Chrysene ND ug/L 06/28/20 19:14 218-01-906/26/20 16:5410.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/28/20 19:14 53-70-306/26/20 16:5410.0 1.6 1
Dibenzofuran ND ug/L 06/28/20 19:14 132-64-906/26/20 16:5410.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/28/20 19:14 95-50-106/26/20 16:5410.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/28/20 19:14 541-73-106/26/20 16:5410.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/28/20 19:14 106-46-706/26/20 16:5410.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/28/20 19:14 91-94-106/26/20 16:5420.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/28/20 19:14 120-83-206/26/20 16:5410.0 1.5 1
Diethylphthalate ND ug/L 06/28/20 19:14 84-66-206/26/20 16:5410.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/28/20 19:14 105-67-906/26/20 16:5410.0 1.5 1
Dimethylphthalate ND ug/L 06/28/20 19:14 131-11-306/26/20 16:5410.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 14 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-5 Lab ID:92483554003 Collected:06/25/20 07:05 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/28/20 19:14 84-74-206/26/20 16:5410.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/28/20 19:14 534-52-106/26/20 16:5420.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/28/20 19:14 51-28-506/26/20 16:5450.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/28/20 19:14 121-14-206/26/20 16:5410.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/28/20 19:14 606-20-206/26/20 16:5410.0 1.7 1
Di-n-octylphthalate ND ug/L 06/28/20 19:14 117-84-006/26/20 16:5410.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/28/20 19:14 117-81-706/26/20 16:546.0 2.0 1
Fluoranthene ND ug/L 06/28/20 19:14 206-44-006/26/20 16:5410.0 1.6 1
Fluorene ND ug/L 06/28/20 19:14 86-73-706/26/20 16:5410.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/28/20 19:14 87-68-306/26/20 16:5410.0 1.6 1
Hexachlorobenzene ND ug/L 06/28/20 19:14 118-74-106/26/20 16:5410.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/28/20 19:14 77-47-406/26/20 16:5410.0 2.4 1
Hexachloroethane ND ug/L 06/28/20 19:14 67-72-106/26/20 16:5410.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/28/20 19:14 193-39-506/26/20 16:5410.0 1.7 1
Isophorone ND ug/L 06/28/20 19:14 78-59-106/26/20 16:5410.0 1.3 1
1-Methylnaphthalene ND ug/L 06/28/20 19:14 90-12-006/26/20 16:5410.0 1.4 1
2-Methylnaphthalene ND ug/L 06/28/20 19:14 91-57-606/26/20 16:5410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/28/20 19:14 95-48-706/26/20 16:5410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/28/20 19:14 15831-10-406/26/20 16:5410.0 1.2 1
Naphthalene ND ug/L 06/28/20 19:14 91-20-306/26/20 16:5410.0 1.6 1
2-Nitroaniline ND ug/L 06/28/20 19:14 88-74-406/26/20 16:5420.0 3.0 1
3-Nitroaniline ND ug/L 06/28/20 19:14 99-09-206/26/20 16:5420.0 2.8 1
4-Nitroaniline ND ug/L 06/28/20 19:14 100-01-606/26/20 16:5420.0 3.1 1
Nitrobenzene ND ug/L 06/28/20 19:14 98-95-306/26/20 16:5410.0 1.5 1
2-Nitrophenol ND ug/L 06/28/20 19:14 88-75-506/26/20 16:5410.0 1.7 1
4-Nitrophenol ND ug/L 06/28/20 19:14 100-02-706/26/20 16:5450.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/28/20 19:14 62-75-906/26/20 16:5410.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/28/20 19:14 621-64-706/26/20 16:5410.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/28/20 19:14 86-30-606/26/20 16:5410.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/28/20 19:14 108-60-106/26/20 16:5410.0 1.3 1
Pentachlorophenol ND ug/L 06/28/20 19:14 87-86-506/26/20 16:5420.0 2.8 1
Phenanthrene ND ug/L 06/28/20 19:14 85-01-806/26/20 16:5410.0 1.4 1
Phenol ND ug/L 06/28/20 19:14 108-95-206/26/20 16:5410.0 1.5 1
Pyrene ND ug/L 06/28/20 19:14 129-00-006/26/20 16:5410.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/28/20 19:14 120-82-106/26/20 16:5410.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/28/20 19:14 95-95-406/26/20 16:5410.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/28/20 19:14 88-06-206/26/20 16:5410.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)44 %06/28/20 19:14 4165-60-006/26/20 16:5413-130 1
2-Fluorobiphenyl (S)41 %06/28/20 19:14 321-60-806/26/20 16:5413-130 1
Terphenyl-d14 (S)94 %06/28/20 19:14 1718-51-006/26/20 16:5425-130 1
Phenol-d6 (S)36 %06/28/20 19:14 13127-88-306/26/20 16:5410-130 1
2-Fluorophenol (S)40 %06/28/20 19:14 367-12-406/26/20 16:5410-130 1
2,4,6-Tribromophenol (S)46 %06/28/20 19:14 118-79-606/26/20 16:5410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-5 Lab ID:92483554003 Collected:06/25/20 07:05 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/26/20 04:23 67-64-125.0 6.2 1
Benzene ND ug/L 06/26/20 04:23 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/26/20 04:23 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/26/20 04:23 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/26/20 04:23 75-27-41.0 0.26 1
Bromoform ND ug/L 06/26/20 04:23 75-25-21.0 0.62 1
Bromomethane ND ug/L 06/26/20 04:23 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 06/26/20 04:23 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/26/20 04:23 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/26/20 04:23 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/26/20 04:23 75-00-31.0 0.49 1
Chloroform ND ug/L 06/26/20 04:23 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/26/20 04:23 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 06/26/20 04:23 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/26/20 04:23 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/26/20 04:23 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/26/20 04:23 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/26/20 04:23 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/26/20 04:23 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/26/20 04:23 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/26/20 04:23 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/26/20 04:23 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/26/20 04:23 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/26/20 04:23 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/26/20 04:23 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/26/20 04:23 75-35-4 v21.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/26/20 04:23 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/26/20 04:23 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/26/20 04:23 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/26/20 04:23 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/26/20 04:23 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/26/20 04:23 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/26/20 04:23 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/26/20 04:23 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/26/20 04:23 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/26/20 04:23 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/26/20 04:23 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/26/20 04:23 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/26/20 04:23 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/26/20 04:23 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/26/20 04:23 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/26/20 04:23 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/26/20 04:23 91-20-31.0 0.35 1
Styrene ND ug/L 06/26/20 04:23 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/26/20 04:23 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TMW-5 Lab ID:92483554003 Collected:06/25/20 07:05 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/26/20 04:23 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/26/20 04:23 127-18-41.0 0.16 1
Toluene ND ug/L 06/26/20 04:23 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/26/20 04:23 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/26/20 04:23 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/26/20 04:23 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/26/20 04:23 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/26/20 04:23 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/26/20 04:23 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/26/20 04:23 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/26/20 04:23 108-05-4 IK2.0 1.4 1
Vinyl chloride ND ug/L 06/26/20 04:23 75-01-4 v21.0 0.24 1
Xylene (Total)ND ug/L 06/26/20 04:23 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/26/20 04:23 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/26/20 04:23 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)99 %06/26/20 04:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/26/20 04:23 17060-07-070-130 1
Toluene-d8 (S)98 %06/26/20 04:23 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:DUP-1 Lab ID:92483554004 Collected:06/25/20 00:00 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND ug/L 06/30/20 17:25 7440-38-206/30/20 10:422.00 0.735 1
Barium 79.7 ug/L 06/30/20 17:25 7440-39-306/30/20 10:4220.0 7.78 1
Cadmium ND ug/L 06/30/20 17:25 7440-43-906/30/20 10:421.00 0.478 1
Chromium ND ug/L 06/30/20 17:25 7440-47-306/30/20 10:422.00 1.49 1
Lead ND ug/L 06/30/20 17:25 7439-92-106/30/20 10:425.00 2.49 1
Selenium ND ug/L 06/30/20 17:25 7782-49-206/30/20 10:422.00 0.657 1
Silver ND ug/L 06/30/20 17:25 7440-22-406/30/20 10:422.00 0.513 1
Analytical Method: EPA 7470A Preparation Method: 7470A
Pace National - Mt. Juliet
Mercury 7470A
Mercury ND ug/L 06/30/20 08:04 7439-97-606/29/20 20:000.200 0.100 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 06/28/20 19:40 83-32-906/26/20 16:5410.0 1.4 1
Acenaphthylene ND ug/L 06/28/20 19:40 208-96-806/26/20 16:5410.0 1.5 1
Aniline ND ug/L 06/28/20 19:40 62-53-306/26/20 16:5410.0 1.6 1
Anthracene ND ug/L 06/28/20 19:40 120-12-706/26/20 16:5410.0 1.6 1
Benzo(a)anthracene ND ug/L 06/28/20 19:40 56-55-306/26/20 16:5410.0 1.5 1
Benzo(a)pyrene ND ug/L 06/28/20 19:40 50-32-806/26/20 16:5410.0 1.8 1
Benzo(b)fluoranthene ND ug/L 06/28/20 19:40 205-99-206/26/20 16:5410.0 1.7 1
Benzo(g,h,i)perylene ND ug/L 06/28/20 19:40 191-24-206/26/20 16:5410.0 1.6 1
Benzo(k)fluoranthene ND ug/L 06/28/20 19:40 207-08-906/26/20 16:5410.0 1.5 1
Benzoic Acid ND ug/L 06/28/20 19:40 65-85-006/26/20 16:5450.0 19.5 1
Benzyl alcohol ND ug/L 06/28/20 19:40 100-51-606/26/20 16:5420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 06/28/20 19:40 101-55-306/26/20 16:5410.0 1.2 1
Butylbenzylphthalate ND ug/L 06/28/20 19:40 85-68-706/26/20 16:5410.0 1.9 1
4-Chloro-3-methylphenol ND ug/L 06/28/20 19:40 59-50-706/26/20 16:5410.0 2.8 1
4-Chloroaniline ND ug/L 06/28/20 19:40 106-47-806/26/20 16:5420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 06/28/20 19:40 111-91-106/26/20 16:5410.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 06/28/20 19:40 111-44-406/26/20 16:5410.0 1.7 1
2-Chloronaphthalene ND ug/L 06/28/20 19:40 91-58-706/26/20 16:5410.0 1.4 1
2-Chlorophenol ND ug/L 06/28/20 19:40 95-57-806/26/20 16:5410.0 1.4 1
4-Chlorophenylphenyl ether ND ug/L 06/28/20 19:40 7005-72-306/26/20 16:5410.0 1.5 1
Chrysene ND ug/L 06/28/20 19:40 218-01-906/26/20 16:5410.0 1.4 1
Dibenz(a,h)anthracene ND ug/L 06/28/20 19:40 53-70-306/26/20 16:5410.0 1.6 1
Dibenzofuran ND ug/L 06/28/20 19:40 132-64-906/26/20 16:5410.0 1.3 1
1,2-Dichlorobenzene ND ug/L 06/28/20 19:40 95-50-106/26/20 16:5410.0 1.4 1
1,3-Dichlorobenzene ND ug/L 06/28/20 19:40 541-73-106/26/20 16:5410.0 1.4 1
1,4-Dichlorobenzene ND ug/L 06/28/20 19:40 106-46-706/26/20 16:5410.0 1.5 1
3,3'-Dichlorobenzidine ND ug/L 06/28/20 19:40 91-94-106/26/20 16:5420.0 2.7 1
2,4-Dichlorophenol ND ug/L 06/28/20 19:40 120-83-206/26/20 16:5410.0 1.5 1
Diethylphthalate ND ug/L 06/28/20 19:40 84-66-206/26/20 16:5410.0 1.6 1
2,4-Dimethylphenol ND ug/L 06/28/20 19:40 105-67-906/26/20 16:5410.0 1.5 1
Dimethylphthalate ND ug/L 06/28/20 19:40 131-11-306/26/20 16:5410.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:DUP-1 Lab ID:92483554004 Collected:06/25/20 00:00 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 06/28/20 19:40 84-74-206/26/20 16:5410.0 1.6 1
4,6-Dinitro-2-methylphenol ND ug/L 06/28/20 19:40 534-52-106/26/20 16:5420.0 4.5 1
2,4-Dinitrophenol ND ug/L 06/28/20 19:40 51-28-506/26/20 16:5450.0 7.3 1
2,4-Dinitrotoluene ND ug/L 06/28/20 19:40 121-14-206/26/20 16:5410.0 1.7 1
2,6-Dinitrotoluene ND ug/L 06/28/20 19:40 606-20-206/26/20 16:5410.0 1.7 1
Di-n-octylphthalate ND ug/L 06/28/20 19:40 117-84-006/26/20 16:5410.0 2.2 1
bis(2-Ethylhexyl)phthalate ND ug/L 06/28/20 19:40 117-81-706/26/20 16:546.0 2.0 1
Fluoranthene ND ug/L 06/28/20 19:40 206-44-006/26/20 16:5410.0 1.6 1
Fluorene ND ug/L 06/28/20 19:40 86-73-706/26/20 16:5410.0 1.4 1
Hexachloro-1,3-butadiene ND ug/L 06/28/20 19:40 87-68-306/26/20 16:5410.0 1.6 1
Hexachlorobenzene ND ug/L 06/28/20 19:40 118-74-106/26/20 16:5410.0 1.3 1
Hexachlorocyclopentadiene ND ug/L 06/28/20 19:40 77-47-406/26/20 16:5410.0 2.4 1
Hexachloroethane ND ug/L 06/28/20 19:40 67-72-106/26/20 16:5410.0 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 06/28/20 19:40 193-39-506/26/20 16:5410.0 1.7 1
Isophorone ND ug/L 06/28/20 19:40 78-59-106/26/20 16:5410.0 1.3 1
1-Methylnaphthalene ND ug/L 06/28/20 19:40 90-12-006/26/20 16:5410.0 1.4 1
2-Methylnaphthalene ND ug/L 06/28/20 19:40 91-57-606/26/20 16:5410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 06/28/20 19:40 95-48-706/26/20 16:5410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 06/28/20 19:40 15831-10-406/26/20 16:5410.0 1.2 1
Naphthalene ND ug/L 06/28/20 19:40 91-20-306/26/20 16:5410.0 1.6 1
2-Nitroaniline ND ug/L 06/28/20 19:40 88-74-406/26/20 16:5420.0 3.0 1
3-Nitroaniline ND ug/L 06/28/20 19:40 99-09-206/26/20 16:5420.0 2.8 1
4-Nitroaniline ND ug/L 06/28/20 19:40 100-01-606/26/20 16:5420.0 3.1 1
Nitrobenzene ND ug/L 06/28/20 19:40 98-95-306/26/20 16:5410.0 1.5 1
2-Nitrophenol ND ug/L 06/28/20 19:40 88-75-506/26/20 16:5410.0 1.7 1
4-Nitrophenol ND ug/L 06/28/20 19:40 100-02-706/26/20 16:5450.0 9.4 1
N-Nitrosodimethylamine ND ug/L 06/28/20 19:40 62-75-906/26/20 16:5410.0 1.8 1
N-Nitroso-di-n-propylamine ND ug/L 06/28/20 19:40 621-64-706/26/20 16:5410.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 06/28/20 19:40 86-30-606/26/20 16:5410.0 1.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 06/28/20 19:40 108-60-106/26/20 16:5410.0 1.3 1
Pentachlorophenol ND ug/L 06/28/20 19:40 87-86-506/26/20 16:5420.0 2.8 1
Phenanthrene ND ug/L 06/28/20 19:40 85-01-806/26/20 16:5410.0 1.4 1
Phenol ND ug/L 06/28/20 19:40 108-95-206/26/20 16:5410.0 1.5 1
Pyrene ND ug/L 06/28/20 19:40 129-00-006/26/20 16:5410.0 1.5 1
1,2,4-Trichlorobenzene ND ug/L 06/28/20 19:40 120-82-106/26/20 16:5410.0 1.6 1
2,4,5-Trichlorophenol ND ug/L 06/28/20 19:40 95-95-406/26/20 16:5410.0 1.5 1
2,4,6-Trichlorophenol ND ug/L 06/28/20 19:40 88-06-206/26/20 16:5410.0 1.4 1
Surrogates
Nitrobenzene-d5 (S)48 %06/28/20 19:40 4165-60-006/26/20 16:5413-130 1
2-Fluorobiphenyl (S)40 %06/28/20 19:40 321-60-806/26/20 16:5413-130 1
Terphenyl-d14 (S)79 %06/28/20 19:40 1718-51-006/26/20 16:5425-130 1
Phenol-d6 (S)30 %06/28/20 19:40 13127-88-306/26/20 16:5410-130 1
2-Fluorophenol (S)36 %06/28/20 19:40 367-12-406/26/20 16:5410-130 1
2,4,6-Tribromophenol (S)49 %06/28/20 19:40 118-79-606/26/20 16:5410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:DUP-1 Lab ID:92483554004 Collected:06/25/20 00:00 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/26/20 04:41 67-64-125.0 6.2 1
Benzene ND ug/L 06/26/20 04:41 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/26/20 04:41 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/26/20 04:41 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/26/20 04:41 75-27-41.0 0.26 1
Bromoform ND ug/L 06/26/20 04:41 75-25-21.0 0.62 1
Bromomethane ND ug/L 06/26/20 04:41 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 06/26/20 04:41 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/26/20 04:41 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/26/20 04:41 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/26/20 04:41 75-00-31.0 0.49 1
Chloroform ND ug/L 06/26/20 04:41 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/26/20 04:41 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 06/26/20 04:41 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/26/20 04:41 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/26/20 04:41 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 06/26/20 04:41 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/26/20 04:41 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/26/20 04:41 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/26/20 04:41 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/26/20 04:41 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/26/20 04:41 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/26/20 04:41 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/26/20 04:41 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/26/20 04:41 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/26/20 04:41 75-35-4 v21.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/26/20 04:41 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/26/20 04:41 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/26/20 04:41 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/26/20 04:41 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/26/20 04:41 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/26/20 04:41 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/26/20 04:41 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/26/20 04:41 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/26/20 04:41 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/26/20 04:41 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/26/20 04:41 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/26/20 04:41 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/26/20 04:41 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/26/20 04:41 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/26/20 04:41 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/26/20 04:41 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/26/20 04:41 91-20-31.0 0.35 1
Styrene ND ug/L 06/26/20 04:41 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/26/20 04:41 630-20-61.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:DUP-1 Lab ID:92483554004 Collected:06/25/20 00:00 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/26/20 04:41 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/26/20 04:41 127-18-41.0 0.16 1
Toluene ND ug/L 06/26/20 04:41 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/26/20 04:41 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/26/20 04:41 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/26/20 04:41 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/26/20 04:41 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/26/20 04:41 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/26/20 04:41 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/26/20 04:41 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/26/20 04:41 108-05-4 IK2.0 1.4 1
Vinyl chloride ND ug/L 06/26/20 04:41 75-01-4 v21.0 0.24 1
Xylene (Total)ND ug/L 06/26/20 04:41 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/26/20 04:41 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/26/20 04:41 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)99 %06/26/20 04:41 460-00-470-130 1
1,2-Dichloroethane-d4 (S)92 %06/26/20 04:41 17060-07-070-130 1
Toluene-d8 (S)99 %06/26/20 04:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-1 Lab ID:92483554005 Collected:06/24/20 16:25 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 7.02 mg/kg 06/30/20 22:07 7440-38-206/29/20 17:521.21 0.512 5
Barium 133 mg/kg 07/01/20 14:07 7440-39-306/29/20 17:526.06 3.03 10
Cadmium 1.07J mg/kg 06/30/20 22:07 7440-43-9 J06/29/20 17:521.21 0.492 5
Chromium 34.8 mg/kg 06/30/20 22:07 7440-47-306/29/20 17:526.06 2.72 5
Lead 183 mg/kg 07/01/20 14:07 7439-92-106/29/20 17:524.85 2.42 10
Selenium ND mg/kg 06/30/20 22:07 7782-49-206/29/20 17:523.03 1.22 5
Silver ND mg/kg 06/30/20 22:07 7440-22-406/29/20 17:520.606 0.258 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0390J mg/kg 06/30/20 09:27 7439-97-6 J06/29/20 21:510.0485 0.0218 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/30/20 19:02 83-32-906/26/20 15:4619004895
Acenaphthylene ND ug/kg 06/30/20 19:02 208-96-806/26/20 15:4619004505
Aniline ND ug/kg 06/30/20 19:02 62-53-306/26/20 15:4619004275
Anthracene ND ug/kg 06/30/20 19:02 120-12-706/26/20 15:4619004935
Benzo(a)anthracene 1040J ug/kg 06/30/20 19:02 56-55-306/26/20 15:4619006055
Benzo(a)pyrene ND ug/kg 06/30/20 19:02 50-32-806/26/20 15:4619008245
Benzo(b)fluoranthene 897J ug/kg 06/30/20 19:02 205-99-206/26/20 15:4619007665
Benzo(g,h,i)perylene ND ug/kg 06/30/20 19:02 191-24-206/26/20 15:4619007435
Benzo(k)fluoranthene ND ug/kg 06/30/20 19:02 207-08-906/26/20 15:4619008015
Benzoic Acid ND ug/kg 06/30/20 19:02 65-85-006/26/20 15:46950020505
Benzyl alcohol ND ug/kg 06/30/20 19:02 100-51-606/26/20 15:46380010105
4-Bromophenylphenyl ether ND ug/kg 06/30/20 19:02 101-55-306/26/20 15:4619004995
Butylbenzylphthalate ND ug/kg 06/30/20 19:02 85-68-706/26/20 15:4619005065
4-Chloro-3-methylphenol ND ug/kg 06/30/20 19:02 59-50-706/26/20 15:46380011605
4-Chloroaniline ND ug/kg 06/30/20 19:02 106-47-806/26/20 15:46380011605
bis(2-Chloroethoxy)methane ND ug/kg 06/30/20 19:02 111-91-106/26/20 15:4619005075
bis(2-Chloroethyl) ether ND ug/kg 06/30/20 19:02 111-44-406/26/20 15:4619004045
2-Chloronaphthalene ND ug/kg 06/30/20 19:02 91-58-706/26/20 15:4619004235
2-Chlorophenol ND ug/kg 06/30/20 19:02 95-57-806/26/20 15:4619004425
4-Chlorophenylphenyl ether ND ug/kg 06/30/20 19:02 7005-72-306/26/20 15:4619004945
Chrysene 804J ug/kg 06/30/20 19:02 218-01-906/26/20 15:4619005525
Dibenz(a,h)anthracene ND ug/kg 06/30/20 19:02 53-70-306/26/20 15:4619007605
Dibenzofuran ND ug/kg 06/30/20 19:02 132-64-906/26/20 15:4619004755
1,2-Dichlorobenzene ND ug/kg 06/30/20 19:02 95-50-106/26/20 15:4619004115
1,3-Dichlorobenzene ND ug/kg 06/30/20 19:02 541-73-106/26/20 15:4619004285
1,4-Dichlorobenzene ND ug/kg 06/30/20 19:02 106-46-706/26/20 15:4619004185
3,3'-Dichlorobenzidine ND ug/kg 06/30/20 19:02 91-94-106/26/20 15:46380013205
2,4-Dichlorophenol ND ug/kg 06/30/20 19:02 120-83-206/26/20 15:4619006285
Diethylphthalate ND ug/kg 06/30/20 19:02 84-66-206/26/20 15:4619004125
2,4-Dimethylphenol ND ug/kg 06/30/20 19:02 105-67-906/26/20 15:4619004735
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-1 Lab ID:92483554005 Collected:06/24/20 16:25 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/30/20 19:02 131-11-306/26/20 15:4619004305
Di-n-butylphthalate ND ug/kg 06/30/20 19:02 84-74-206/26/20 15:4619004695
4,6-Dinitro-2-methylphenol ND ug/kg 06/30/20 19:02 534-52-106/26/20 15:46380030605
2,4-Dinitrophenol ND ug/kg 06/30/20 19:02 51-28-506/26/20 15:46950060705
2,4-Dinitrotoluene ND ug/kg 06/30/20 19:02 121-14-206/26/20 15:4619005035
2,6-Dinitrotoluene ND ug/kg 06/30/20 19:02 606-20-206/26/20 15:4619004975
Di-n-octylphthalate ND ug/kg 06/30/20 19:02 117-84-006/26/20 15:46190010805
bis(2-Ethylhexyl)phthalate ND ug/kg 06/30/20 19:02 117-81-706/26/20 15:4619006225
Fluoranthene 1760J ug/kg 06/30/20 19:02 206-44-0 L206/26/20 15:4619005745
Fluorene ND ug/kg 06/30/20 19:02 86-73-706/26/20 15:4619005095
Hexachloro-1,3-butadiene ND ug/kg 06/30/20 19:02 87-68-306/26/20 15:4619004625
Hexachlorobenzene ND ug/kg 06/30/20 19:02 118-74-106/26/20 15:4619004835
Hexachlorocyclopentadiene ND ug/kg 06/30/20 19:02 77-47-406/26/20 15:4619007605
Hexachloroethane ND ug/kg 06/30/20 19:02 67-72-106/26/20 15:4619004335
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/20 19:02 193-39-506/26/20 15:4619008705
Isophorone ND ug/kg 06/30/20 19:02 78-59-106/26/20 15:4619004135
1-Methylnaphthalene ND ug/kg 06/30/20 19:02 90-12-006/26/20 15:4619005065
2-Methylnaphthalene ND ug/kg 06/30/20 19:02 91-57-606/26/20 15:4619004845
2-Methylphenol(o-Cresol)ND ug/kg 06/30/20 19:02 95-48-706/26/20 15:4619004215
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/30/20 19:02 15831-10-406/26/20 15:4619004785
Naphthalene ND ug/kg 06/30/20 19:02 91-20-306/26/20 15:4619004555
2-Nitroaniline ND ug/kg 06/30/20 19:02 88-74-406/26/20 15:4695009565
3-Nitroaniline ND ug/kg 06/30/20 19:02 99-09-206/26/20 15:46950010105
4-Nitroaniline ND ug/kg 06/30/20 19:02 100-01-606/26/20 15:4638009395
Nitrobenzene ND ug/kg 06/30/20 19:02 98-95-306/26/20 15:4619004545
2-Nitrophenol ND ug/kg 06/30/20 19:02 88-75-506/26/20 15:4619005875
4-Nitrophenol ND ug/kg 06/30/20 19:02 100-02-706/26/20 15:46950030305
N-Nitrosodimethylamine ND ug/kg 06/30/20 19:02 62-75-906/26/20 15:4619005345
N-Nitroso-di-n-propylamine ND ug/kg 06/30/20 19:02 621-64-706/26/20 15:4619005325
N-Nitrosodiphenylamine ND ug/kg 06/30/20 19:02 86-30-606/26/20 15:4619004855
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/30/20 19:02 108-60-106/26/20 15:4619005285
Pentachlorophenol ND ug/kg 06/30/20 19:02 87-86-506/26/20 15:4638008705
Phenanthrene 1620J ug/kg 06/30/20 19:02 85-01-806/26/20 15:4619004795
Phenol ND ug/kg 06/30/20 19:02 108-95-206/26/20 15:4619004545
Pyrene 1430J ug/kg 06/30/20 19:02 129-00-006/26/20 15:4619005235
Pyridine ND ug/kg 06/30/20 19:02 110-86-106/26/20 15:4619004815
1,2,4-Trichlorobenzene ND ug/kg 06/30/20 19:02 120-82-106/26/20 15:4619004355
2,4,5-Trichlorophenol ND ug/kg 06/30/20 19:02 95-95-406/26/20 15:4619004945
2,4,6-Trichlorophenol ND ug/kg 06/30/20 19:02 88-06-206/26/20 15:4619004775
Surrogates
Nitrobenzene-d5 (S)43 %06/30/20 19:02 4165-60-0 D306/26/20 15:4623-110 5
2-Fluorobiphenyl (S)43 %06/30/20 19:02 321-60-806/26/20 15:4630-110 5
Terphenyl-d14 (S)48 %06/30/20 19:02 1718-51-006/26/20 15:4628-110 5
Phenol-d6 (S)28 %06/30/20 19:02 13127-88-306/26/20 15:4622-110 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-1 Lab ID:92483554005 Collected:06/24/20 16:25 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)26 %06/30/20 19:02 367-12-406/26/20 15:4613-110 5
2,4,6-Tribromophenol (S)33 %06/30/20 19:02 118-79-606/26/20 15:4627-110 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/29/20 17:04 67-64-106/29/20 10:4510739.9 1
Benzene ND ug/kg 06/29/20 17:04 71-43-206/29/20 10:455.4 3.8 1
Bromobenzene ND ug/kg 06/29/20 17:04 108-86-106/29/20 10:455.4 3.6 1
Bromochloromethane ND ug/kg 06/29/20 17:04 74-97-506/29/20 10:455.4 4.1 1
Bromodichloromethane ND ug/kg 06/29/20 17:04 75-27-406/29/20 10:455.4 3.5 1
Bromoform ND ug/kg 06/29/20 17:04 75-25-206/29/20 10:455.4 2.9 1
Bromomethane 11.5 ug/kg 06/29/20 17:04 74-83-9 v206/29/20 10:4510.7 8.4 1
2-Butanone (MEK)ND ug/kg 06/29/20 17:04 78-93-306/29/20 10:4510745.4 1
n-Butylbenzene ND ug/kg 06/29/20 17:04 104-51-806/29/20 10:455.4 2.9 1
sec-Butylbenzene ND ug/kg 06/29/20 17:04 135-98-806/29/20 10:455.4 3.4 1
tert-Butylbenzene ND ug/kg 06/29/20 17:04 98-06-606/29/20 10:455.4 2.9 1
Carbon tetrachloride ND ug/kg 06/29/20 17:04 56-23-506/29/20 10:455.4 2.4 1
Chlorobenzene ND ug/kg 06/29/20 17:04 108-90-706/29/20 10:455.4 3.5 1
Chloroethane ND ug/kg 06/29/20 17:04 75-00-306/29/20 10:4510.7 5.7 1
Chloroform ND ug/kg 06/29/20 17:04 67-66-306/29/20 10:455.4 2.6 1
Chloromethane ND ug/kg 06/29/20 17:04 74-87-306/29/20 10:4510.7 7.5 1
2-Chlorotoluene ND ug/kg 06/29/20 17:04 95-49-806/29/20 10:455.4 3.8 1
4-Chlorotoluene ND ug/kg 06/29/20 17:04 106-43-406/29/20 10:455.4 3.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/29/20 17:04 96-12-806/29/20 10:455.4 5.0 1
Dibromochloromethane ND ug/kg 06/29/20 17:04 124-48-106/29/20 10:455.4 2.9 1
1,2-Dibromoethane (EDB)ND ug/kg 06/29/20 17:04 106-93-406/29/20 10:455.4 3.8 1
Dibromomethane ND ug/kg 06/29/20 17:04 74-95-306/29/20 10:455.4 2.7 1
1,2-Dichlorobenzene ND ug/kg 06/29/20 17:04 95-50-106/29/20 10:455.4 3.2 1
1,3-Dichlorobenzene ND ug/kg 06/29/20 17:04 541-73-106/29/20 10:455.4 4.4 1
1,4-Dichlorobenzene ND ug/kg 06/29/20 17:04 106-46-706/29/20 10:455.4 4.0 1
Dichlorodifluoromethane ND ug/kg 06/29/20 17:04 75-71-806/29/20 10:4510.7 1.8 1
1,1-Dichloroethane ND ug/kg 06/29/20 17:04 75-34-306/29/20 10:455.4 2.4 1
1,2-Dichloroethane ND ug/kg 06/29/20 17:04 107-06-2 v206/29/20 10:455.4 2.2 1
1,1-Dichloroethene ND ug/kg 06/29/20 17:04 75-35-406/29/20 10:455.4 1.7 1
cis-1,2-Dichloroethene ND ug/kg 06/29/20 17:04 156-59-206/29/20 10:455.4 3.1 1
trans-1,2-Dichloroethene ND ug/kg 06/29/20 17:04 156-60-506/29/20 10:455.4 2.3 1
1,2-Dichloropropane ND ug/kg 06/29/20 17:04 78-87-506/29/20 10:455.4 3.3 1
1,3-Dichloropropane ND ug/kg 06/29/20 17:04 142-28-906/29/20 10:455.4 3.7 1
2,2-Dichloropropane ND ug/kg 06/29/20 17:04 594-20-706/29/20 10:455.4 2.9 1
1,1-Dichloropropene ND ug/kg 06/29/20 17:04 563-58-606/29/20 10:455.4 2.6 1
cis-1,3-Dichloropropene ND ug/kg 06/29/20 17:04 10061-01-506/29/20 10:455.4 3.5 1
trans-1,3-Dichloropropene ND ug/kg 06/29/20 17:04 10061-02-606/29/20 10:455.4 4.5 1
Diisopropyl ether ND ug/kg 06/29/20 17:04 108-20-306/29/20 10:455.4 2.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-1 Lab ID:92483554005 Collected:06/24/20 16:25 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/29/20 17:04 100-41-406/29/20 10:455.4 5.0 1
Hexachloro-1,3-butadiene ND ug/kg 06/29/20 17:04 87-68-306/29/20 10:455.4 5.1 1
2-Hexanone ND ug/kg 06/29/20 17:04 591-78-606/29/20 10:4553.5 10.6 1
Isopropylbenzene (Cumene)ND ug/kg 06/29/20 17:04 98-82-806/29/20 10:455.4 3.4 1
p-Isopropyltoluene 12.9 ug/kg 06/29/20 17:04 99-87-606/29/20 10:455.4 3.0 1
Methylene Chloride ND ug/kg 06/29/20 17:04 75-09-206/29/20 10:4521.4 7.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/29/20 17:04 108-10-106/29/20 10:4553.5 45.3 1
Methyl-tert-butyl ether ND ug/kg 06/29/20 17:04 1634-04-406/29/20 10:455.4 3.4 1
Naphthalene 124 ug/kg 06/29/20 17:04 91-20-306/29/20 10:455.4 3.0 1
n-Propylbenzene ND ug/kg 06/29/20 17:04 103-65-106/29/20 10:455.4 3.7 1
Styrene ND ug/kg 06/29/20 17:04 100-42-506/29/20 10:455.4 2.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/29/20 17:04 630-20-606/29/20 10:455.4 3.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/29/20 17:04 79-34-506/29/20 10:455.4 4.7 1
Tetrachloroethene ND ug/kg 06/29/20 17:04 127-18-406/29/20 10:455.4 2.7 1
Toluene ND ug/kg 06/29/20 17:04 108-88-306/29/20 10:455.4 3.1 1
1,2,3-Trichlorobenzene ND ug/kg 06/29/20 17:04 87-61-606/29/20 10:455.4 3.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/29/20 17:04 120-82-106/29/20 10:455.4 3.0 1
1,1,1-Trichloroethane ND ug/kg 06/29/20 17:04 71-55-606/29/20 10:455.4 2.2 1
1,1,2-Trichloroethane ND ug/kg 06/29/20 17:04 79-00-506/29/20 10:455.4 4.0 1
Trichloroethene ND ug/kg 06/29/20 17:04 79-01-606/29/20 10:455.4 3.3 1
Trichlorofluoromethane ND ug/kg 06/29/20 17:04 75-69-406/29/20 10:455.4 1.3 1
1,2,3-Trichloropropane ND ug/kg 06/29/20 17:04 96-18-406/29/20 10:455.4 4.4 1
1,2,4-Trimethylbenzene ND ug/kg 06/29/20 17:04 95-63-606/29/20 10:455.4 3.9 1
1,3,5-Trimethylbenzene ND ug/kg 06/29/20 17:04 108-67-806/29/20 10:455.4 3.2 1
Vinyl acetate ND ug/kg 06/29/20 17:04 108-05-406/29/20 10:4553.5 4.6 1
Vinyl chloride ND ug/kg 06/29/20 17:04 75-01-406/29/20 10:4510.7 2.1 1
Xylene (Total)ND ug/kg 06/29/20 17:04 1330-20-706/29/20 10:4510.7 3.1 1
m&p-Xylene ND ug/kg 06/29/20 17:04 179601-23-106/29/20 10:4510.7 8.2 1
o-Xylene ND ug/kg 06/29/20 17:04 95-47-606/29/20 10:455.4 3.1 1
Surrogates
Toluene-d8 (S)99 %06/29/20 17:04 2037-26-506/29/20 10:4570-130 1
4-Bromofluorobenzene (S)97 %06/29/20 17:04 460-00-406/29/20 10:4570-130 1
1,2-Dichloroethane-d4 (S)112 %06/29/20 17:04 17060-07-006/29/20 10:4570-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.6 %06/25/20 16:360.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 82.5 %06/30/20 16:1806/30/20 16:091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-1 Lab ID:92483554005 Collected:06/24/20 16:25 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 07/02/20 16:32 18540-29-907/01/20 19:051.21 0.309 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-2 Lab ID:92483554006 Collected:06/24/20 16:30 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 6.14 mg/kg 06/30/20 22:10 7440-38-206/29/20 17:521.30 0.549 5
Barium 99.6 mg/kg 06/30/20 22:10 7440-39-306/29/20 17:523.25 1.63 5
Cadmium ND mg/kg 06/30/20 22:10 7440-43-906/29/20 17:521.30 0.528 5
Chromium 17.6 mg/kg 06/30/20 22:10 7440-47-306/29/20 17:526.50 2.91 5
Lead 16.4 mg/kg 06/30/20 22:10 7439-92-106/29/20 17:522.60 1.30 5
Selenium ND mg/kg 06/30/20 22:10 7782-49-206/29/20 17:523.25 1.31 5
Silver ND mg/kg 06/30/20 22:10 7440-22-406/29/20 17:520.650 0.277 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0417J mg/kg 06/30/20 09:30 7439-97-6 J06/29/20 21:510.0520 0.0234 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/30/20 19:29 83-32-906/26/20 15:4620605315
Acenaphthylene ND ug/kg 06/30/20 19:29 208-96-806/26/20 15:4620604895
Aniline ND ug/kg 06/30/20 19:29 62-53-306/26/20 15:4620604645
Anthracene ND ug/kg 06/30/20 19:29 120-12-706/26/20 15:4620605355
Benzo(a)anthracene ND ug/kg 06/30/20 19:29 56-55-306/26/20 15:4620606575
Benzo(a)pyrene ND ug/kg 06/30/20 19:29 50-32-806/26/20 15:4620608945
Benzo(b)fluoranthene ND ug/kg 06/30/20 19:29 205-99-206/26/20 15:4620608325
Benzo(g,h,i)perylene ND ug/kg 06/30/20 19:29 191-24-206/26/20 15:4620608075
Benzo(k)fluoranthene ND ug/kg 06/30/20 19:29 207-08-906/26/20 15:4620608695
Benzoic Acid ND ug/kg 06/30/20 19:29 65-85-006/26/20 15:461030022305
Benzyl alcohol ND ug/kg 06/30/20 19:29 100-51-606/26/20 15:46413010905
4-Bromophenylphenyl ether ND ug/kg 06/30/20 19:29 101-55-306/26/20 15:4620605425
Butylbenzylphthalate ND ug/kg 06/30/20 19:29 85-68-706/26/20 15:4620605505
4-Chloro-3-methylphenol ND ug/kg 06/30/20 19:29 59-50-706/26/20 15:46413012605
4-Chloroaniline ND ug/kg 06/30/20 19:29 106-47-806/26/20 15:46413012605
bis(2-Chloroethoxy)methane ND ug/kg 06/30/20 19:29 111-91-106/26/20 15:4620605515
bis(2-Chloroethyl) ether ND ug/kg 06/30/20 19:29 111-44-406/26/20 15:4620604385
2-Chloronaphthalene ND ug/kg 06/30/20 19:29 91-58-706/26/20 15:4620604605
2-Chlorophenol ND ug/kg 06/30/20 19:29 95-57-806/26/20 15:4620604805
4-Chlorophenylphenyl ether ND ug/kg 06/30/20 19:29 7005-72-306/26/20 15:4620605365
Chrysene ND ug/kg 06/30/20 19:29 218-01-906/26/20 15:4620605995
Dibenz(a,h)anthracene ND ug/kg 06/30/20 19:29 53-70-306/26/20 15:4620608265
Dibenzofuran ND ug/kg 06/30/20 19:29 132-64-906/26/20 15:4620605165
1,2-Dichlorobenzene ND ug/kg 06/30/20 19:29 95-50-106/26/20 15:4620604475
1,3-Dichlorobenzene ND ug/kg 06/30/20 19:29 541-73-106/26/20 15:4620604655
1,4-Dichlorobenzene ND ug/kg 06/30/20 19:29 106-46-706/26/20 15:4620604545
3,3'-Dichlorobenzidine ND ug/kg 06/30/20 19:29 91-94-106/26/20 15:46413014405
2,4-Dichlorophenol ND ug/kg 06/30/20 19:29 120-83-206/26/20 15:4620606825
Diethylphthalate ND ug/kg 06/30/20 19:29 84-66-206/26/20 15:4620604485
2,4-Dimethylphenol ND ug/kg 06/30/20 19:29 105-67-906/26/20 15:4620605145
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-2 Lab ID:92483554006 Collected:06/24/20 16:30 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/30/20 19:29 131-11-306/26/20 15:4620604675
Di-n-butylphthalate ND ug/kg 06/30/20 19:29 84-74-206/26/20 15:4620605095
4,6-Dinitro-2-methylphenol ND ug/kg 06/30/20 19:29 534-52-106/26/20 15:46413033305
2,4-Dinitrophenol ND ug/kg 06/30/20 19:29 51-28-506/26/20 15:461030065905
2,4-Dinitrotoluene ND ug/kg 06/30/20 19:29 121-14-206/26/20 15:4620605475
2,6-Dinitrotoluene ND ug/kg 06/30/20 19:29 606-20-206/26/20 15:4620605405
Di-n-octylphthalate ND ug/kg 06/30/20 19:29 117-84-006/26/20 15:46206011805
bis(2-Ethylhexyl)phthalate ND ug/kg 06/30/20 19:29 117-81-706/26/20 15:4620606765
Fluoranthene ND ug/kg 06/30/20 19:29 206-44-0 L206/26/20 15:4620606245
Fluorene ND ug/kg 06/30/20 19:29 86-73-706/26/20 15:4620605525
Hexachloro-1,3-butadiene ND ug/kg 06/30/20 19:29 87-68-306/26/20 15:4620605025
Hexachlorobenzene ND ug/kg 06/30/20 19:29 118-74-106/26/20 15:4620605245
Hexachlorocyclopentadiene ND ug/kg 06/30/20 19:29 77-47-406/26/20 15:4620608265
Hexachloroethane ND ug/kg 06/30/20 19:29 67-72-106/26/20 15:4620604705
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/20 19:29 193-39-506/26/20 15:4620609455
Isophorone ND ug/kg 06/30/20 19:29 78-59-106/26/20 15:4620604485
1-Methylnaphthalene ND ug/kg 06/30/20 19:29 90-12-006/26/20 15:4620605505
2-Methylnaphthalene ND ug/kg 06/30/20 19:29 91-57-606/26/20 15:4620605255
2-Methylphenol(o-Cresol)ND ug/kg 06/30/20 19:29 95-48-706/26/20 15:4620604575
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/30/20 19:29 15831-10-406/26/20 15:4620605195
Naphthalene ND ug/kg 06/30/20 19:29 91-20-306/26/20 15:4620604945
2-Nitroaniline ND ug/kg 06/30/20 19:29 88-74-406/26/20 15:461030010405
3-Nitroaniline ND ug/kg 06/30/20 19:29 99-09-206/26/20 15:461030010905
4-Nitroaniline ND ug/kg 06/30/20 19:29 100-01-606/26/20 15:46413010205
Nitrobenzene ND ug/kg 06/30/20 19:29 98-95-306/26/20 15:4620604935
2-Nitrophenol ND ug/kg 06/30/20 19:29 88-75-506/26/20 15:4620606385
4-Nitrophenol ND ug/kg 06/30/20 19:29 100-02-706/26/20 15:461030032905
N-Nitrosodimethylamine ND ug/kg 06/30/20 19:29 62-75-906/26/20 15:4620605805
N-Nitroso-di-n-propylamine ND ug/kg 06/30/20 19:29 621-64-706/26/20 15:4620605785
N-Nitrosodiphenylamine ND ug/kg 06/30/20 19:29 86-30-606/26/20 15:4620605275
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/30/20 19:29 108-60-106/26/20 15:4620605745
Pentachlorophenol ND ug/kg 06/30/20 19:29 87-86-506/26/20 15:4641309455
Phenanthrene ND ug/kg 06/30/20 19:29 85-01-806/26/20 15:4620605205
Phenol ND ug/kg 06/30/20 19:29 108-95-206/26/20 15:4620604935
Pyrene 575J ug/kg 06/30/20 19:29 129-00-006/26/20 15:4620605685
Pyridine ND ug/kg 06/30/20 19:29 110-86-106/26/20 15:4620605225
1,2,4-Trichlorobenzene ND ug/kg 06/30/20 19:29 120-82-106/26/20 15:4620604735
2,4,5-Trichlorophenol ND ug/kg 06/30/20 19:29 95-95-406/26/20 15:4620605365
2,4,6-Trichlorophenol ND ug/kg 06/30/20 19:29 88-06-206/26/20 15:4620605195
Surrogates
Nitrobenzene-d5 (S)40 %06/30/20 19:29 4165-60-0 D306/26/20 15:4623-110 5
2-Fluorobiphenyl (S)39 %06/30/20 19:29 321-60-806/26/20 15:4630-110 5
Terphenyl-d14 (S)43 %06/30/20 19:29 1718-51-006/26/20 15:4628-110 5
Phenol-d6 (S)17 %06/30/20 19:29 13127-88-3 S506/26/20 15:4622-110 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-2 Lab ID:92483554006 Collected:06/24/20 16:30 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)12 %06/30/20 19:29 367-12-4 S506/26/20 15:4613-110 5
2,4,6-Tribromophenol (S)23 %06/30/20 19:29 118-79-6 S506/26/20 15:4627-110 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/29/20 17:22 67-64-106/29/20 10:4512647.0 1
Benzene ND ug/kg 06/29/20 17:22 71-43-206/29/20 10:456.3 4.5 1
Bromobenzene ND ug/kg 06/29/20 17:22 108-86-106/29/20 10:456.3 4.3 1
Bromochloromethane ND ug/kg 06/29/20 17:22 74-97-506/29/20 10:456.3 4.8 1
Bromodichloromethane ND ug/kg 06/29/20 17:22 75-27-406/29/20 10:456.3 4.1 1
Bromoform ND ug/kg 06/29/20 17:22 75-25-206/29/20 10:456.3 3.4 1
Bromomethane 10.1J ug/kg 06/29/20 17:22 74-83-9 v206/29/20 10:4512.6 9.9 1
2-Butanone (MEK)ND ug/kg 06/29/20 17:22 78-93-306/29/20 10:4512653.5 1
n-Butylbenzene ND ug/kg 06/29/20 17:22 104-51-806/29/20 10:456.3 3.4 1
sec-Butylbenzene ND ug/kg 06/29/20 17:22 135-98-806/29/20 10:456.3 4.0 1
tert-Butylbenzene ND ug/kg 06/29/20 17:22 98-06-606/29/20 10:456.3 3.4 1
Carbon tetrachloride ND ug/kg 06/29/20 17:22 56-23-506/29/20 10:456.3 2.8 1
Chlorobenzene ND ug/kg 06/29/20 17:22 108-90-706/29/20 10:456.3 4.1 1
Chloroethane ND ug/kg 06/29/20 17:22 75-00-306/29/20 10:4512.6 6.7 1
Chloroform ND ug/kg 06/29/20 17:22 67-66-306/29/20 10:456.3 3.1 1
Chloromethane ND ug/kg 06/29/20 17:22 74-87-306/29/20 10:4512.6 8.9 1
2-Chlorotoluene ND ug/kg 06/29/20 17:22 95-49-806/29/20 10:456.3 4.5 1
4-Chlorotoluene ND ug/kg 06/29/20 17:22 106-43-406/29/20 10:456.3 4.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/29/20 17:22 96-12-806/29/20 10:456.3 5.9 1
Dibromochloromethane ND ug/kg 06/29/20 17:22 124-48-106/29/20 10:456.3 3.4 1
1,2-Dibromoethane (EDB)ND ug/kg 06/29/20 17:22 106-93-406/29/20 10:456.3 4.5 1
Dibromomethane ND ug/kg 06/29/20 17:22 74-95-306/29/20 10:456.3 3.1 1
1,2-Dichlorobenzene ND ug/kg 06/29/20 17:22 95-50-106/29/20 10:456.3 3.7 1
1,3-Dichlorobenzene ND ug/kg 06/29/20 17:22 541-73-106/29/20 10:456.3 5.2 1
1,4-Dichlorobenzene ND ug/kg 06/29/20 17:22 106-46-706/29/20 10:456.3 4.7 1
Dichlorodifluoromethane ND ug/kg 06/29/20 17:22 75-71-806/29/20 10:4512.6 2.2 1
1,1-Dichloroethane ND ug/kg 06/29/20 17:22 75-34-306/29/20 10:456.3 2.8 1
1,2-Dichloroethane ND ug/kg 06/29/20 17:22 107-06-2 v206/29/20 10:456.3 2.6 1
1,1-Dichloroethene ND ug/kg 06/29/20 17:22 75-35-406/29/20 10:456.3 2.0 1
cis-1,2-Dichloroethene ND ug/kg 06/29/20 17:22 156-59-206/29/20 10:456.3 3.6 1
trans-1,2-Dichloroethene ND ug/kg 06/29/20 17:22 156-60-506/29/20 10:456.3 2.7 1
1,2-Dichloropropane ND ug/kg 06/29/20 17:22 78-87-506/29/20 10:456.3 3.9 1
1,3-Dichloropropane ND ug/kg 06/29/20 17:22 142-28-906/29/20 10:456.3 4.4 1
2,2-Dichloropropane ND ug/kg 06/29/20 17:22 594-20-706/29/20 10:456.3 3.5 1
1,1-Dichloropropene ND ug/kg 06/29/20 17:22 563-58-606/29/20 10:456.3 3.0 1
cis-1,3-Dichloropropene ND ug/kg 06/29/20 17:22 10061-01-506/29/20 10:456.3 4.1 1
trans-1,3-Dichloropropene ND ug/kg 06/29/20 17:22 10061-02-606/29/20 10:456.3 5.3 1
Diisopropyl ether ND ug/kg 06/29/20 17:22 108-20-306/29/20 10:456.3 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-2 Lab ID:92483554006 Collected:06/24/20 16:30 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/29/20 17:22 100-41-406/29/20 10:456.3 5.9 1
Hexachloro-1,3-butadiene ND ug/kg 06/29/20 17:22 87-68-306/29/20 10:456.3 6.0 1
2-Hexanone ND ug/kg 06/29/20 17:22 591-78-606/29/20 10:4563.1 12.5 1
Isopropylbenzene (Cumene)ND ug/kg 06/29/20 17:22 98-82-806/29/20 10:456.3 4.0 1
p-Isopropyltoluene ND ug/kg 06/29/20 17:22 99-87-606/29/20 10:456.3 3.5 1
Methylene Chloride ND ug/kg 06/29/20 17:22 75-09-206/29/20 10:4525.2 9.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/29/20 17:22 108-10-106/29/20 10:4563.1 53.3 1
Methyl-tert-butyl ether ND ug/kg 06/29/20 17:22 1634-04-406/29/20 10:456.3 4.0 1
Naphthalene 7.8 ug/kg 06/29/20 17:22 91-20-306/29/20 10:456.3 3.5 1
n-Propylbenzene ND ug/kg 06/29/20 17:22 103-65-106/29/20 10:456.3 4.4 1
Styrene ND ug/kg 06/29/20 17:22 100-42-506/29/20 10:456.3 3.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/29/20 17:22 630-20-606/29/20 10:456.3 4.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/29/20 17:22 79-34-506/29/20 10:456.3 5.6 1
Tetrachloroethene ND ug/kg 06/29/20 17:22 127-18-406/29/20 10:456.3 3.1 1
Toluene ND ug/kg 06/29/20 17:22 108-88-306/29/20 10:456.3 3.6 1
1,2,3-Trichlorobenzene ND ug/kg 06/29/20 17:22 87-61-606/29/20 10:456.3 3.9 1
1,2,4-Trichlorobenzene ND ug/kg 06/29/20 17:22 120-82-106/29/20 10:456.3 3.5 1
1,1,1-Trichloroethane ND ug/kg 06/29/20 17:22 71-55-606/29/20 10:456.3 2.5 1
1,1,2-Trichloroethane ND ug/kg 06/29/20 17:22 79-00-506/29/20 10:456.3 4.7 1
Trichloroethene ND ug/kg 06/29/20 17:22 79-01-606/29/20 10:456.3 3.9 1
Trichlorofluoromethane ND ug/kg 06/29/20 17:22 75-69-406/29/20 10:456.3 1.6 1
1,2,3-Trichloropropane ND ug/kg 06/29/20 17:22 96-18-406/29/20 10:456.3 5.1 1
1,2,4-Trimethylbenzene ND ug/kg 06/29/20 17:22 95-63-606/29/20 10:456.3 4.5 1
1,3,5-Trimethylbenzene ND ug/kg 06/29/20 17:22 108-67-806/29/20 10:456.3 3.8 1
Vinyl acetate ND ug/kg 06/29/20 17:22 108-05-406/29/20 10:4563.1 5.4 1
Vinyl chloride ND ug/kg 06/29/20 17:22 75-01-406/29/20 10:4512.6 2.4 1
Xylene (Total)ND ug/kg 06/29/20 17:22 1330-20-706/29/20 10:4512.6 3.6 1
m&p-Xylene ND ug/kg 06/29/20 17:22 179601-23-106/29/20 10:4512.6 9.7 1
o-Xylene ND ug/kg 06/29/20 17:22 95-47-606/29/20 10:456.3 3.6 1
Surrogates
Toluene-d8 (S)100 %06/29/20 17:22 2037-26-506/29/20 10:4570-130 1
4-Bromofluorobenzene (S)98 %06/29/20 17:22 460-00-406/29/20 10:4570-130 1
1,2-Dichloroethane-d4 (S)113 %06/29/20 17:22 17060-07-006/29/20 10:4570-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.1 %06/25/20 16:360.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 76.9 %06/30/20 16:1806/30/20 16:091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-2 Lab ID:92483554006 Collected:06/24/20 16:30 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 07/02/20 16:38 18540-29-907/01/20 19:051.30 0.332 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-DUP Lab ID:92483554007 Collected:06/24/20 00:00 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 6.44 mg/kg 06/30/20 22:14 7440-38-206/29/20 17:521.24 0.523 5
Barium 106 mg/kg 06/30/20 22:14 7440-39-306/29/20 17:523.10 1.55 5
Cadmium 1.37 mg/kg 06/30/20 22:14 7440-43-906/29/20 17:521.24 0.503 5
Chromium 19.5 mg/kg 06/30/20 22:14 7440-47-306/29/20 17:526.20 2.78 5
Lead 101 mg/kg 06/30/20 22:14 7439-92-106/29/20 17:522.48 1.24 5
Selenium ND mg/kg 06/30/20 22:14 7782-49-206/29/20 17:523.10 1.25 5
Silver ND mg/kg 06/30/20 22:14 7440-22-406/29/20 17:520.620 0.264 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0370J mg/kg 06/30/20 09:32 7439-97-6 J06/29/20 21:510.0496 0.0223 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 06/30/20 19:56 83-32-906/26/20 15:4619805085
Acenaphthylene ND ug/kg 06/30/20 19:56 208-96-806/26/20 15:4619804685
Aniline ND ug/kg 06/30/20 19:56 62-53-306/26/20 15:4619804445
Anthracene ND ug/kg 06/30/20 19:56 120-12-706/26/20 15:4619805135
Benzo(a)anthracene ND ug/kg 06/30/20 19:56 56-55-306/26/20 15:4619806295
Benzo(a)pyrene ND ug/kg 06/30/20 19:56 50-32-806/26/20 15:4619808565
Benzo(b)fluoranthene ND ug/kg 06/30/20 19:56 205-99-206/26/20 15:4619807965
Benzo(g,h,i)perylene ND ug/kg 06/30/20 19:56 191-24-206/26/20 15:4619807735
Benzo(k)fluoranthene ND ug/kg 06/30/20 19:56 207-08-906/26/20 15:4619808325
Benzoic Acid ND ug/kg 06/30/20 19:56 65-85-006/26/20 15:46988021305
Benzyl alcohol ND ug/kg 06/30/20 19:56 100-51-606/26/20 15:46395010505
4-Bromophenylphenyl ether ND ug/kg 06/30/20 19:56 101-55-306/26/20 15:4619805195
Butylbenzylphthalate ND ug/kg 06/30/20 19:56 85-68-706/26/20 15:4619805265
4-Chloro-3-methylphenol ND ug/kg 06/30/20 19:56 59-50-706/26/20 15:46395012005
4-Chloroaniline ND ug/kg 06/30/20 19:56 106-47-806/26/20 15:46395012105
bis(2-Chloroethoxy)methane ND ug/kg 06/30/20 19:56 111-91-106/26/20 15:4619805285
bis(2-Chloroethyl) ether ND ug/kg 06/30/20 19:56 111-44-406/26/20 15:4619804205
2-Chloronaphthalene ND ug/kg 06/30/20 19:56 91-58-706/26/20 15:4619804405
2-Chlorophenol ND ug/kg 06/30/20 19:56 95-57-806/26/20 15:4619804605
4-Chlorophenylphenyl ether ND ug/kg 06/30/20 19:56 7005-72-306/26/20 15:4619805135
Chrysene ND ug/kg 06/30/20 19:56 218-01-906/26/20 15:4619805745
Dibenz(a,h)anthracene ND ug/kg 06/30/20 19:56 53-70-306/26/20 15:4619807915
Dibenzofuran ND ug/kg 06/30/20 19:56 132-64-906/26/20 15:4619804945
1,2-Dichlorobenzene ND ug/kg 06/30/20 19:56 95-50-106/26/20 15:4619804285
1,3-Dichlorobenzene ND ug/kg 06/30/20 19:56 541-73-106/26/20 15:4619804455
1,4-Dichlorobenzene ND ug/kg 06/30/20 19:56 106-46-706/26/20 15:4619804355
3,3'-Dichlorobenzidine ND ug/kg 06/30/20 19:56 91-94-106/26/20 15:46395013805
2,4-Dichlorophenol ND ug/kg 06/30/20 19:56 120-83-206/26/20 15:4619806535
Diethylphthalate ND ug/kg 06/30/20 19:56 84-66-206/26/20 15:4619804295
2,4-Dimethylphenol ND ug/kg 06/30/20 19:56 105-67-906/26/20 15:4619804925
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-DUP Lab ID:92483554007 Collected:06/24/20 00:00 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 06/30/20 19:56 131-11-306/26/20 15:4619804475
Di-n-butylphthalate ND ug/kg 06/30/20 19:56 84-74-206/26/20 15:4619804875
4,6-Dinitro-2-methylphenol ND ug/kg 06/30/20 19:56 534-52-106/26/20 15:46395031905
2,4-Dinitrophenol ND ug/kg 06/30/20 19:56 51-28-506/26/20 15:46988063105
2,4-Dinitrotoluene ND ug/kg 06/30/20 19:56 121-14-206/26/20 15:4619805235
2,6-Dinitrotoluene ND ug/kg 06/30/20 19:56 606-20-206/26/20 15:4619805175
Di-n-octylphthalate ND ug/kg 06/30/20 19:56 117-84-006/26/20 15:46198011305
bis(2-Ethylhexyl)phthalate ND ug/kg 06/30/20 19:56 117-81-706/26/20 15:4619806475
Fluoranthene ND ug/kg 06/30/20 19:56 206-44-0 L206/26/20 15:4619805975
Fluorene ND ug/kg 06/30/20 19:56 86-73-706/26/20 15:4619805295
Hexachloro-1,3-butadiene ND ug/kg 06/30/20 19:56 87-68-306/26/20 15:4619804805
Hexachlorobenzene ND ug/kg 06/30/20 19:56 118-74-106/26/20 15:4619805025
Hexachlorocyclopentadiene ND ug/kg 06/30/20 19:56 77-47-406/26/20 15:4619807915
Hexachloroethane ND ug/kg 06/30/20 19:56 67-72-106/26/20 15:4619804505
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/20 19:56 193-39-506/26/20 15:4619809045
Isophorone ND ug/kg 06/30/20 19:56 78-59-106/26/20 15:4619804295
1-Methylnaphthalene ND ug/kg 06/30/20 19:56 90-12-006/26/20 15:4619805265
2-Methylnaphthalene ND ug/kg 06/30/20 19:56 91-57-606/26/20 15:4619805035
2-Methylphenol(o-Cresol)ND ug/kg 06/30/20 19:56 95-48-706/26/20 15:4619804385
3&4-Methylphenol(m&p Cresol)ND ug/kg 06/30/20 19:56 15831-10-406/26/20 15:4619804975
Naphthalene ND ug/kg 06/30/20 19:56 91-20-306/26/20 15:4619804735
2-Nitroaniline ND ug/kg 06/30/20 19:56 88-74-406/26/20 15:4698809945
3-Nitroaniline ND ug/kg 06/30/20 19:56 99-09-206/26/20 15:46988010505
4-Nitroaniline ND ug/kg 06/30/20 19:56 100-01-606/26/20 15:4639509765
Nitrobenzene ND ug/kg 06/30/20 19:56 98-95-306/26/20 15:4619804725
2-Nitrophenol ND ug/kg 06/30/20 19:56 88-75-506/26/20 15:4619806115
4-Nitrophenol ND ug/kg 06/30/20 19:56 100-02-706/26/20 15:46988031505
N-Nitrosodimethylamine ND ug/kg 06/30/20 19:56 62-75-906/26/20 15:4619805565
N-Nitroso-di-n-propylamine ND ug/kg 06/30/20 19:56 621-64-706/26/20 15:4619805535
N-Nitrosodiphenylamine ND ug/kg 06/30/20 19:56 86-30-606/26/20 15:4619805045
2,2'-Oxybis(1-chloropropane)ND ug/kg 06/30/20 19:56 108-60-106/26/20 15:4619805495
Pentachlorophenol ND ug/kg 06/30/20 19:56 87-86-506/26/20 15:4639509045
Phenanthrene ND ug/kg 06/30/20 19:56 85-01-806/26/20 15:4619804985
Phenol ND ug/kg 06/30/20 19:56 108-95-206/26/20 15:4619804725
Pyrene ND ug/kg 06/30/20 19:56 129-00-006/26/20 15:4619805445
Pyridine ND ug/kg 06/30/20 19:56 110-86-106/26/20 15:4619805005
1,2,4-Trichlorobenzene ND ug/kg 06/30/20 19:56 120-82-106/26/20 15:4619804535
2,4,5-Trichlorophenol ND ug/kg 06/30/20 19:56 95-95-406/26/20 15:4619805135
2,4,6-Trichlorophenol ND ug/kg 06/30/20 19:56 88-06-206/26/20 15:4619804965
Surrogates
Nitrobenzene-d5 (S)34 %06/30/20 19:56 4165-60-0 D306/26/20 15:4623-110 5
2-Fluorobiphenyl (S)37 %06/30/20 19:56 321-60-806/26/20 15:4630-110 5
Terphenyl-d14 (S)40 %06/30/20 19:56 1718-51-006/26/20 15:4628-110 5
Phenol-d6 (S)20 %06/30/20 19:56 13127-88-3 S506/26/20 15:4622-110 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-DUP Lab ID:92483554007 Collected:06/24/20 00:00 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)16 %06/30/20 19:56 367-12-406/26/20 15:4613-110 5
2,4,6-Tribromophenol (S)28 %06/30/20 19:56 118-79-606/26/20 15:4627-110 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 06/29/20 17:41 67-64-106/29/20 10:4510940.5 1
Benzene ND ug/kg 06/29/20 17:41 71-43-206/29/20 10:455.4 3.8 1
Bromobenzene ND ug/kg 06/29/20 17:41 108-86-106/29/20 10:455.4 3.7 1
Bromochloromethane ND ug/kg 06/29/20 17:41 74-97-506/29/20 10:455.4 4.1 1
Bromodichloromethane ND ug/kg 06/29/20 17:41 75-27-406/29/20 10:455.4 3.6 1
Bromoform ND ug/kg 06/29/20 17:41 75-25-206/29/20 10:455.4 2.9 1
Bromomethane ND ug/kg 06/29/20 17:41 74-83-9 v206/29/20 10:4510.9 8.6 1
2-Butanone (MEK)ND ug/kg 06/29/20 17:41 78-93-306/29/20 10:4510946.1 1
n-Butylbenzene ND ug/kg 06/29/20 17:41 104-51-806/29/20 10:455.4 2.9 1
sec-Butylbenzene ND ug/kg 06/29/20 17:41 135-98-806/29/20 10:455.4 3.4 1
tert-Butylbenzene ND ug/kg 06/29/20 17:41 98-06-606/29/20 10:455.4 2.9 1
Carbon tetrachloride ND ug/kg 06/29/20 17:41 56-23-506/29/20 10:455.4 2.4 1
Chlorobenzene ND ug/kg 06/29/20 17:41 108-90-706/29/20 10:455.4 3.5 1
Chloroethane ND ug/kg 06/29/20 17:41 75-00-306/29/20 10:4510.9 5.7 1
Chloroform ND ug/kg 06/29/20 17:41 67-66-306/29/20 10:455.4 2.7 1
Chloromethane ND ug/kg 06/29/20 17:41 74-87-306/29/20 10:4510.9 7.6 1
2-Chlorotoluene ND ug/kg 06/29/20 17:41 95-49-806/29/20 10:455.4 3.9 1
4-Chlorotoluene ND ug/kg 06/29/20 17:41 106-43-406/29/20 10:455.4 3.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 06/29/20 17:41 96-12-806/29/20 10:455.4 5.0 1
Dibromochloromethane ND ug/kg 06/29/20 17:41 124-48-106/29/20 10:455.4 2.9 1
1,2-Dibromoethane (EDB)ND ug/kg 06/29/20 17:41 106-93-406/29/20 10:455.4 3.8 1
Dibromomethane ND ug/kg 06/29/20 17:41 74-95-306/29/20 10:455.4 2.7 1
1,2-Dichlorobenzene ND ug/kg 06/29/20 17:41 95-50-106/29/20 10:455.4 3.2 1
1,3-Dichlorobenzene ND ug/kg 06/29/20 17:41 541-73-106/29/20 10:455.4 4.5 1
1,4-Dichlorobenzene ND ug/kg 06/29/20 17:41 106-46-706/29/20 10:455.4 4.1 1
Dichlorodifluoromethane ND ug/kg 06/29/20 17:41 75-71-806/29/20 10:4510.9 1.9 1
1,1-Dichloroethane ND ug/kg 06/29/20 17:41 75-34-306/29/20 10:455.4 2.4 1
1,2-Dichloroethane ND ug/kg 06/29/20 17:41 107-06-2 v206/29/20 10:455.4 2.2 1
1,1-Dichloroethene ND ug/kg 06/29/20 17:41 75-35-406/29/20 10:455.4 1.7 1
cis-1,2-Dichloroethene ND ug/kg 06/29/20 17:41 156-59-206/29/20 10:455.4 3.1 1
trans-1,2-Dichloroethene ND ug/kg 06/29/20 17:41 156-60-506/29/20 10:455.4 2.4 1
1,2-Dichloropropane ND ug/kg 06/29/20 17:41 78-87-506/29/20 10:455.4 3.4 1
1,3-Dichloropropane ND ug/kg 06/29/20 17:41 142-28-906/29/20 10:455.4 3.8 1
2,2-Dichloropropane ND ug/kg 06/29/20 17:41 594-20-706/29/20 10:455.4 3.0 1
1,1-Dichloropropene ND ug/kg 06/29/20 17:41 563-58-606/29/20 10:455.4 2.6 1
cis-1,3-Dichloropropene ND ug/kg 06/29/20 17:41 10061-01-506/29/20 10:455.4 3.5 1
trans-1,3-Dichloropropene ND ug/kg 06/29/20 17:41 10061-02-606/29/20 10:455.4 4.6 1
Diisopropyl ether ND ug/kg 06/29/20 17:41 108-20-306/29/20 10:455.4 2.2 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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Page 34 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-DUP Lab ID:92483554007 Collected:06/24/20 00:00 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 06/29/20 17:41 100-41-406/29/20 10:455.4 5.1 1
Hexachloro-1,3-butadiene ND ug/kg 06/29/20 17:41 87-68-306/29/20 10:455.4 5.2 1
2-Hexanone ND ug/kg 06/29/20 17:41 591-78-606/29/20 10:4554.3 10.8 1
Isopropylbenzene (Cumene)ND ug/kg 06/29/20 17:41 98-82-806/29/20 10:455.4 3.4 1
p-Isopropyltoluene 101 ug/kg 06/29/20 17:41 99-87-606/29/20 10:455.4 3.0 1
Methylene Chloride ND ug/kg 06/29/20 17:41 75-09-206/29/20 10:4521.7 8.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 06/29/20 17:41 108-10-106/29/20 10:4554.3 46.0 1
Methyl-tert-butyl ether ND ug/kg 06/29/20 17:41 1634-04-406/29/20 10:455.4 3.5 1
Naphthalene 5.9 ug/kg 06/29/20 17:41 91-20-306/29/20 10:455.4 3.1 1
n-Propylbenzene ND ug/kg 06/29/20 17:41 103-65-106/29/20 10:455.4 3.7 1
Styrene ND ug/kg 06/29/20 17:41 100-42-506/29/20 10:455.4 2.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 06/29/20 17:41 630-20-606/29/20 10:455.4 3.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 06/29/20 17:41 79-34-506/29/20 10:455.4 4.8 1
Tetrachloroethene ND ug/kg 06/29/20 17:41 127-18-406/29/20 10:455.4 2.7 1
Toluene 3.6J ug/kg 06/29/20 17:41 108-88-306/29/20 10:455.4 3.1 1
1,2,3-Trichlorobenzene ND ug/kg 06/29/20 17:41 87-61-606/29/20 10:455.4 3.3 1
1,2,4-Trichlorobenzene ND ug/kg 06/29/20 17:41 120-82-106/29/20 10:455.4 3.0 1
1,1,1-Trichloroethane ND ug/kg 06/29/20 17:41 71-55-606/29/20 10:455.4 2.2 1
1,1,2-Trichloroethane ND ug/kg 06/29/20 17:41 79-00-506/29/20 10:455.4 4.0 1
Trichloroethene ND ug/kg 06/29/20 17:41 79-01-606/29/20 10:455.4 3.4 1
Trichlorofluoromethane ND ug/kg 06/29/20 17:41 75-69-406/29/20 10:455.4 1.3 1
1,2,3-Trichloropropane ND ug/kg 06/29/20 17:41 96-18-406/29/20 10:455.4 4.4 1
1,2,4-Trimethylbenzene ND ug/kg 06/29/20 17:41 95-63-606/29/20 10:455.4 3.9 1
1,3,5-Trimethylbenzene ND ug/kg 06/29/20 17:41 108-67-806/29/20 10:455.4 3.2 1
Vinyl acetate ND ug/kg 06/29/20 17:41 108-05-406/29/20 10:4554.3 4.7 1
Vinyl chloride ND ug/kg 06/29/20 17:41 75-01-406/29/20 10:4510.9 2.1 1
Xylene (Total)ND ug/kg 06/29/20 17:41 1330-20-706/29/20 10:4510.9 3.1 1
m&p-Xylene ND ug/kg 06/29/20 17:41 179601-23-106/29/20 10:4510.9 8.4 1
o-Xylene ND ug/kg 06/29/20 17:41 95-47-606/29/20 10:455.4 3.1 1
Surrogates
Toluene-d8 (S)98 %06/29/20 17:41 2037-26-506/29/20 10:4570-130 1
4-Bromofluorobenzene (S)96 %06/29/20 17:41 460-00-406/29/20 10:4570-130 1
1,2-Dichloroethane-d4 (S)111 %06/29/20 17:41 17060-07-006/29/20 10:4570-132 1
Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 15.1 %06/25/20 16:360.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.7 %06/30/20 16:1806/30/20 16:091
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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Page 35 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:COMP-DUP Lab ID:92483554007 Collected:06/24/20 00:00 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 07/02/20 16:53 18540-29-907/01/20 19:051.24 0.316 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 36 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:BKG-1 Lab ID:92483554008 Collected:06/24/20 16:10 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic ND mg/kg 06/30/20 22:17 7440-38-206/29/20 17:521.36 0.572 5
Barium 17.4 mg/kg 06/30/20 22:17 7440-39-306/29/20 17:523.39 1.69 5
Cadmium ND mg/kg 06/30/20 22:17 7440-43-906/29/20 17:521.36 0.550 5
Chromium 4.66J mg/kg 06/30/20 22:17 7440-47-3 J06/29/20 17:526.78 3.04 5
Lead 7.92 mg/kg 06/30/20 22:17 7439-92-106/29/20 17:522.71 1.36 5
Selenium ND mg/kg 06/30/20 22:17 7782-49-206/29/20 17:523.39 1.37 5
Silver ND mg/kg 06/30/20 22:17 7440-22-406/29/20 17:520.678 0.289 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury ND mg/kg 06/30/20 09:35 7439-97-606/29/20 21:510.0542 0.0244 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 73.8 %06/30/20 18:3806/30/20 18:301
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 07/02/20 16:58 18540-29-907/01/20 19:051.36 0.346 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:BKG-2 Lab ID:92483554009 Collected:06/24/20 16:15 Received:06/25/20 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051
Pace National - Mt. Juliet
Metals (ICPMS) 6020B
Arsenic 2.81 mg/kg 06/30/20 22:20 7440-38-206/29/20 17:521.17 0.494 5
Barium 39.3 mg/kg 06/30/20 22:20 7440-39-306/29/20 17:522.92 1.46 5
Cadmium ND mg/kg 06/30/20 22:20 7440-43-906/29/20 17:521.17 0.475 5
Chromium 24.3 mg/kg 06/30/20 22:20 7440-47-306/29/20 17:525.85 2.62 5
Lead 12.6 mg/kg 06/30/20 22:20 7439-92-106/29/20 17:522.34 1.17 5
Selenium ND mg/kg 06/30/20 22:20 7782-49-206/29/20 17:522.92 1.18 5
Silver ND mg/kg 06/30/20 22:20 7440-22-406/29/20 17:520.585 0.249 5
Analytical Method: EPA 7471B Preparation Method: 7471A
Pace National - Mt. Juliet
Mercury 7471B
Mercury 0.0267J mg/kg 06/30/20 09:42 7439-97-6 J06/29/20 21:510.0468 0.0211 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 85.5 %06/30/20 18:3806/30/20 18:301
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 07/02/20 17:04 18540-29-907/01/20 19:051.17 0.298 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TRIP BLANK Lab ID:92483554010 Collected:06/24/20 00:00 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 06/27/20 00:58 67-64-125.0 6.2 1
Benzene ND ug/L 06/27/20 00:58 71-43-21.0 0.15 1
Bromobenzene ND ug/L 06/27/20 00:58 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 06/27/20 00:58 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 06/27/20 00:58 75-27-41.0 0.26 1
Bromoform ND ug/L 06/27/20 00:58 75-25-2 v11.0 0.62 1
Bromomethane ND ug/L 06/27/20 00:58 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 06/27/20 00:58 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 06/27/20 00:58 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 06/27/20 00:58 108-90-71.0 0.23 1
Chloroethane ND ug/L 06/27/20 00:58 75-00-31.0 0.49 1
Chloroform ND ug/L 06/27/20 00:58 67-66-35.0 2.3 1
Chloromethane ND ug/L 06/27/20 00:58 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 06/27/20 00:58 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 06/27/20 00:58 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 06/27/20 00:58 96-12-8 v15.0 0.26 1
Dibromochloromethane ND ug/L 06/27/20 00:58 124-48-1 v11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 06/27/20 00:58 106-93-41.0 0.26 1
Dibromomethane ND ug/L 06/27/20 00:58 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 06/27/20 00:58 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 06/27/20 00:58 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 06/27/20 00:58 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 06/27/20 00:58 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 06/27/20 00:58 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 06/27/20 00:58 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 06/27/20 00:58 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 06/27/20 00:58 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 06/27/20 00:58 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 06/27/20 00:58 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 06/27/20 00:58 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 06/27/20 00:58 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 06/27/20 00:58 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 06/27/20 00:58 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 06/27/20 00:58 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 06/27/20 00:58 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 06/27/20 00:58 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 06/27/20 00:58 87-68-31.0 0.44 1
2-Hexanone ND ug/L 06/27/20 00:58 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 06/27/20 00:58 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 06/27/20 00:58 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 06/27/20 00:58 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 06/27/20 00:58 1634-04-41.0 0.28 1
Naphthalene ND ug/L 06/27/20 00:58 91-20-31.0 0.35 1
Styrene ND ug/L 06/27/20 00:58 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 06/27/20 00:58 630-20-6 v11.0 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 85
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92483554
BCP-145
Sample:TRIP BLANK Lab ID:92483554010 Collected:06/24/20 00:00 Received:06/25/20 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 06/27/20 00:58 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 06/27/20 00:58 127-18-4 v11.0 0.16 1
Toluene ND ug/L 06/27/20 00:58 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 06/27/20 00:58 87-61-6 v11.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 06/27/20 00:58 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 06/27/20 00:58 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 06/27/20 00:58 79-00-51.0 0.24 1
Trichloroethene ND ug/L 06/27/20 00:58 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 06/27/20 00:58 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 06/27/20 00:58 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 06/27/20 00:58 108-05-4 IK2.0 1.4 1
Vinyl chloride ND ug/L 06/27/20 00:58 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 06/27/20 00:58 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 06/27/20 00:58 179601-23-12.0 0.41 1
o-Xylene ND ug/L 06/27/20 00:58 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)99 %06/27/20 00:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %06/27/20 00:58 17060-07-070-130 1
Toluene-d8 (S)99 %06/27/20 00:58 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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Page 40 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1500580
3015
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92483554001, 92483554002, 92483554003, 92483554004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3544819-1
Associated Lab Samples:92483554001, 92483554002, 92483554003, 92483554004
Matrix:Water
AnalyzedMDL
Arsenic ug/L ND 2.00 06/30/20 15:340.735
Barium ug/L ND 20.0 06/30/20 15:347.78
Cadmium ug/L ND 1.00 06/30/20 15:340.478
Chromium ug/L ND 2.00 06/30/20 15:341.49
Lead ug/L ND 5.00 06/30/20 15:342.49
Selenium ug/L ND 2.00 06/30/20 15:340.657
Silver ug/L ND 2.00 06/30/20 15:340.513
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3544819-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 48.050.0 96.1 80.0-120
Barium ug/L 50.050.0 99.9 80.0-120
Cadmium ug/L 51.350.0 103 80.0-120
Chromium ug/L 49.850.0 99.5 80.0-120
Lead ug/L 50.350.0 101 80.0-120
Selenium ug/L 54.050.0 108 80.0-120
Silver ug/L 52.250.0 104 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3544819-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1233127-06
R3544819-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 50.0 96.6 75.0-12598.4 1.73 2050.02.17 50.5 51.4
Barium ug/L 50.0 93.4 75.0-12590.3 0.674 2050.0189 236 234
Cadmium ug/L 50.0 105 75.0-125105 0.707 2050.06.63 58.9 59.3
Chromium ug/L 50.0 97.3 75.0-12599.1 1.75 2050.02.23 50.9 51.8
Lead ug/L 50.0 104 75.0-125104 0.604 2050.0ND 51.9 52.2
Selenium ug/L 50.0 109 75.0-125105 3.45 2050.0ND 54.3 52.4
Silver ug/L 50.0 106 75.0-125106 0.167 2050.0ND 53.1 53.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1517393
3015
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92483554003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3554885-1
Associated Lab Samples:92483554003
Matrix:Water
AnalyzedMDL
Chromium ug/L ND 2.00 07/30/20 14:551.49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3554885-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 51.350.0 103 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3554885-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1244445-04
R3554885-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium ug/L 50.0 95.4 75.0-12595.7 0.308 2050.0ND 47.7 47.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1500535
3051
EPA 6020B
Metals (ICPMS) 6020B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92483554005, 92483554006, 92483554007, 92483554008, 92483554009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3544914-1
Associated Lab Samples:92483554005, 92483554006, 92483554007, 92483554008, 92483554009
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 1.00 06/30/20 19:340.422
Barium mg/kg ND 2.50 06/30/20 19:341.25
Cadmium mg/kg ND 1.00 06/30/20 19:340.406
Chromium mg/kg ND 5.00 06/30/20 19:342.24
Lead mg/kg ND 2.00 06/30/20 19:341.00
Selenium mg/kg ND 2.50 06/30/20 19:341.01
Silver mg/kg ND 0.500 06/30/20 19:340.213
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3544914-2LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 92.4100 92.4 80.0-120
Barium mg/kg 99.2100 99.2 80.0-120
Cadmium mg/kg 97.7100 97.7 80.0-120
Chromium mg/kg 94.6100 94.6 80.0-120
Lead mg/kg 102100 102 80.0-120
Selenium mg/kg 100100 100 80.0-120
Silver mg/kg 19.720.0 98.6 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3544914-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1232913-01
R3544914-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 22.3 81.6 75.0-12576.8 5.36 2022.311.2 102 96.7
Barium mg/kg 22.3 107 75.0-125113 2.60 2022.3152 271 278
Cadmium mg/kg 22.3 95.4 75.0-12595.1 0.266 2022.3ND 106 106
Chromium mg/kg 22.3 83.8 75.0-12583.1 0.757 2022.316.6 110 109
Lead mg/kg ML22.3 32.8 75.0-12520.6 7.12 2022.3162 198 184
Selenium mg/kg 22.3 90.3 75.0-12592.8 2.77 2022.3ND 101 103
Silver mg/kg 4.45 94.1 75.0-12595.3 1.26 204.45ND 20.9 21.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1500765
7470A
EPA 7470A
Mercury 7470A
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92483554001, 92483554002, 92483554003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3544495-1
Associated Lab Samples:92483554001, 92483554002, 92483554003
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.200 06/29/20 18:060.100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3544495-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.613.00 86.9 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3544495-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1233024-01
R3544495-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 3.00 92.6 75.0-12593.5 1.00 203.00ND 2.78 2.80
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1500766
7470A
EPA 7470A
Mercury 7470A
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92483554004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3544639-1
Associated Lab Samples:92483554004
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.200 06/30/20 07:250.100
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3544639-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.803.00 93.4 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3544639-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1234386-06
R3544639-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 3.00 104 75.0-125105 0.990 203.00ND 3.13 3.16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1501369
7471A
EPA 7471B
Mercury 7471B
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92483554005, 92483554006, 92483554007, 92483554008, 92483554009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3544583-1
Associated Lab Samples:92483554005, 92483554006, 92483554007, 92483554008, 92483554009
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0400 06/30/20 08:520.0180
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3544583-2LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.5050.500 101 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3544583-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1233418-02
R3544583-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg ML0.781 79.9 75.0-12572.5 7.05 200.7810.227 0.851 0.793
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
550146
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92483554005, 92483554006, 92483554007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2925338
Associated Lab Samples:92483554005, 92483554006, 92483554007
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 06/29/20 13:413.3
1,1,1-Trichloroethane ug/kg ND 5.0 06/29/20 13:412.0
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 06/29/20 13:414.4
1,1,2-Trichloroethane ug/kg ND 5.0 06/29/20 13:413.7
1,1-Dichloroethane ug/kg ND 5.0 06/29/20 13:412.2
1,1-Dichloroethene ug/kg ND 5.0 06/29/20 13:411.6
1,1-Dichloropropene ug/kg ND 5.0 06/29/20 13:412.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 06/29/20 13:413.1
1,2,3-Trichloropropane ug/kg ND 5.0 06/29/20 13:414.1
1,2,4-Trichlorobenzene ug/kg ND 5.0 06/29/20 13:412.8
1,2,4-Trimethylbenzene ug/kg ND 5.0 06/29/20 13:413.6
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 06/29/20 13:414.6
1,2-Dibromoethane (EDB)ug/kg ND 5.0 06/29/20 13:413.5
1,2-Dichlorobenzene ug/kg ND 5.0 06/29/20 13:413.0
1,2-Dichloroethane ug/kg ND 5.0 v206/29/20 13:412.0
1,2-Dichloropropane ug/kg ND 5.0 06/29/20 13:413.1
1,3,5-Trimethylbenzene ug/kg ND 5.0 06/29/20 13:413.0
1,3-Dichlorobenzene ug/kg ND 5.0 06/29/20 13:414.1
1,3-Dichloropropane ug/kg ND 5.0 06/29/20 13:413.5
1,4-Dichlorobenzene ug/kg ND 5.0 06/29/20 13:413.8
2,2-Dichloropropane ug/kg ND 5.0 06/29/20 13:412.8
2-Butanone (MEK)ug/kg ND 100 06/29/20 13:4142.4
2-Chlorotoluene ug/kg ND 5.0 06/29/20 13:413.6
2-Hexanone ug/kg ND 50.0 06/29/20 13:419.9
4-Chlorotoluene ug/kg ND 5.0 06/29/20 13:413.2
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 06/29/20 13:4142.3
Acetone ug/kg 42.0J 100 06/29/20 13:4137.3
Benzene ug/kg ND 5.0 06/29/20 13:413.5
Bromobenzene ug/kg ND 5.0 06/29/20 13:413.4
Bromochloromethane ug/kg ND 5.0 06/29/20 13:413.8
Bromodichloromethane ug/kg ND 5.0 06/29/20 13:413.3
Bromoform ug/kg ND 5.0 06/29/20 13:412.7
Bromomethane ug/kg ND 10.0 v206/29/20 13:417.9
Carbon tetrachloride ug/kg ND 5.0 06/29/20 13:412.2
Chlorobenzene ug/kg ND 5.0 06/29/20 13:413.2
Chloroethane ug/kg ND 10.0 06/29/20 13:415.3
Chloroform ug/kg ND 5.0 06/29/20 13:412.5
Chloromethane ug/kg ND 10.0 06/29/20 13:417.0
cis-1,2-Dichloroethene ug/kg ND 5.0 06/29/20 13:412.9
cis-1,3-Dichloropropene ug/kg ND 5.0 06/29/20 13:413.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2925338
Associated Lab Samples:92483554005, 92483554006, 92483554007
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 06/29/20 13:412.7
Dibromomethane ug/kg ND 5.0 06/29/20 13:412.5
Dichlorodifluoromethane ug/kg ND 10.0 06/29/20 13:411.7
Diisopropyl ether ug/kg ND 5.0 06/29/20 13:412.0
Ethylbenzene ug/kg ND 5.0 06/29/20 13:414.7
Hexachloro-1,3-butadiene ug/kg ND 5.0 06/29/20 13:414.7
Isopropylbenzene (Cumene)ug/kg ND 5.0 06/29/20 13:413.2
m&p-Xylene ug/kg ND 10.0 06/29/20 13:417.7
Methyl-tert-butyl ether ug/kg ND 5.0 06/29/20 13:413.2
Methylene Chloride ug/kg ND 20.0 06/29/20 13:417.4
n-Butylbenzene ug/kg ND 5.0 06/29/20 13:412.7
n-Propylbenzene ug/kg ND 5.0 06/29/20 13:413.4
Naphthalene ug/kg ND 5.0 06/29/20 13:412.8
o-Xylene ug/kg ND 5.0 06/29/20 13:412.8
p-Isopropyltoluene ug/kg ND 5.0 06/29/20 13:412.8
sec-Butylbenzene ug/kg ND 5.0 06/29/20 13:413.2
Styrene ug/kg ND 5.0 06/29/20 13:412.4
tert-Butylbenzene ug/kg ND 5.0 06/29/20 13:412.7
Tetrachloroethene ug/kg ND 5.0 06/29/20 13:412.5
Toluene ug/kg ND 5.0 06/29/20 13:412.9
trans-1,2-Dichloroethene ug/kg ND 5.0 06/29/20 13:412.2
trans-1,3-Dichloropropene ug/kg ND 5.0 06/29/20 13:414.2
Trichloroethene ug/kg ND 5.0 06/29/20 13:413.1
Trichlorofluoromethane ug/kg ND 5.0 06/29/20 13:411.2
Vinyl acetate ug/kg ND 50.0 06/29/20 13:414.3
Vinyl chloride ug/kg ND 10.0 06/29/20 13:411.9
Xylene (Total)ug/kg ND 10.0 06/29/20 13:412.8
1,2-Dichloroethane-d4 (S)%117 70-132 06/29/20 13:41
4-Bromofluorobenzene (S)%97 70-130 06/29/20 13:41
Toluene-d8 (S)%98 70-130 06/29/20 13:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2925339LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11401250 91 70-130
1,1,1-Trichloroethane ug/kg 10701250 85 70-130
1,1,2,2-Tetrachloroethane ug/kg 11501250 92 55-130
1,1,2-Trichloroethane ug/kg 10801250 86 70-130
1,1-Dichloroethane ug/kg 10701250 86 68-130
1,1-Dichloroethene ug/kg 11401250 91 70-130
1,1-Dichloropropene ug/kg 10901250 87 70-130
1,2,3-Trichlorobenzene ug/kg 11101250 89 70-130
1,2,3-Trichloropropane ug/kg 11401250 91 70-130
1,2,4-Trichlorobenzene ug/kg 10901250 87 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2925339LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 11501250 92 69-130
1,2-Dibromo-3-chloropropane ug/kg 12501250 100 57-141
1,2-Dibromoethane (EDB)ug/kg 11601250 93 70-130
1,2-Dichlorobenzene ug/kg 11501250 92 70-130
1,2-Dichloroethane ug/kg 975 v312507870-130
1,2-Dichloropropane ug/kg 10901250 87 70-130
1,3,5-Trimethylbenzene ug/kg 12001250 96 70-130
1,3-Dichlorobenzene ug/kg 11701250 94 70-130
1,3-Dichloropropane ug/kg 11401250 91 70-130
1,4-Dichlorobenzene ug/kg 11401250 91 70-130
2,2-Dichloropropane ug/kg 10601250 85 70-130
2-Butanone (MEK)ug/kg 23202500 93 60-130
2-Chlorotoluene ug/kg 12501250 100 70-130
2-Hexanone ug/kg 25502500 102 70-132
4-Chlorotoluene ug/kg 12401250 99 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 23302500 93 69-130
Acetone ug/kg 23802500 95 49-148
Benzene ug/kg 10501250 84 70-130
Bromobenzene ug/kg 12401250 99 70-130
Bromochloromethane ug/kg 11701250 94 70-130
Bromodichloromethane ug/kg 10401250 83 70-130
Bromoform ug/kg 11701250 93 68-136
Bromomethane ug/kg 1020 v312508260-140
Carbon tetrachloride ug/kg 11301250 90 70-130
Chlorobenzene ug/kg 11201250 90 70-130
Chloroethane ug/kg 11301250 90 51-147
Chloroform ug/kg 10701250 86 70-130
Chloromethane ug/kg 9571250 77 48-130
cis-1,2-Dichloroethene ug/kg 11001250 88 70-130
cis-1,3-Dichloropropene ug/kg 10801250 87 70-130
Dibromochloromethane ug/kg 11901250 96 70-130
Dibromomethane ug/kg 10901250 87 70-130
Dichlorodifluoromethane ug/kg 10701250 86 49-130
Diisopropyl ether ug/kg 10801250 86 66-130
Ethylbenzene ug/kg 10501250 84 70-130
Hexachloro-1,3-butadiene ug/kg 11801250 94 70-130
Isopropylbenzene (Cumene)ug/kg 11001250 88 70-130
m&p-Xylene ug/kg 21302500 85 70-130
Methyl-tert-butyl ether ug/kg 11001250 88 70-130
Methylene Chloride ug/kg 11301250 90 50-137
n-Butylbenzene ug/kg 11401250 91 70-130
n-Propylbenzene ug/kg 11901250 95 70-130
Naphthalene ug/kg 12401250 99 70-131
o-Xylene ug/kg 11401250 92 70-130
p-Isopropyltoluene ug/kg 11201250 90 70-130
sec-Butylbenzene ug/kg 11301250 90 70-130
Styrene ug/kg 11901250 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2925339LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 11201250 89 69-130
Tetrachloroethene ug/kg 11301250 90 56-130
Toluene ug/kg 11001250 88 70-130
trans-1,2-Dichloroethene ug/kg 11201250 90 70-130
trans-1,3-Dichloropropene ug/kg 10301250 82 70-130
Trichloroethene ug/kg 10901250 87 70-141
Trichlorofluoromethane ug/kg 11101250 88 67-130
Vinyl acetate ug/kg 23602500 94 10-136
Vinyl chloride ug/kg 12001250 96 67-130
Xylene (Total)ug/kg 32703750 87 70-130
1,2-Dichloroethane-d4 (S)%100 70-132
4-Bromofluorobenzene (S)%93 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2925340MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92483534001
2925341
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 549 97 52-13390 7 30549ND532493
1,1,1-Trichloroethane ug/kg 549 93 49-13784 10 30549ND511462
1,1,2,2-Tetrachloroethane ug/kg 549 104 39-15091 14 30549ND570498
1,1,2-Trichloroethane ug/kg 549 90 48-14077 16 30549ND495423
1,1-Dichloroethane ug/kg 549 93 46-13583 12 30549ND510453
1,1-Dichloroethene ug/kg 549 100 38-14989 12 30549ND552491
1,1-Dichloropropene ug/kg 549 95 41-14086 11 30549ND524472
1,2,3-Trichlorobenzene ug/kg 549 94 10-15888 7 30549ND518483
1,2,3-Trichloropropane ug/kg 549 101 33-15790 11 30549ND556495
1,2,4-Trichlorobenzene ug/kg 549 82 10-15579 3 30549ND450435
1,2,4-Trimethylbenzene ug/kg 549 85 24-15478 8 305498.9 475 440
1,2-Dibromo-3-
chloropropane ug/kg 549 90 33-15886 5 30549ND493471
1,2-Dibromoethane (EDB)ug/kg v154910240-13694 8 30549ND561518
1,2-Dichlorobenzene ug/kg 549 89 27-14681 9 30549ND487447
1,2-Dichloroethane ug/kg 549 84 49-14076 10 30549ND461416
1,2-Dichloropropane ug/kg 549 92 44-14381 13 30549ND506445
1,3,5-Trimethylbenzene ug/kg 549 83 40-14476 8 3054912.1 469 431
1,3-Dichlorobenzene ug/kg 549 86 33-14078 9 30549ND474431
1,3-Dichloropropane ug/kg v154910547-14795 10 30549ND575522
1,4-Dichlorobenzene ug/kg 549 87 35-13979 11 30549ND480432
2,2-Dichloropropane ug/kg 549 91 41-14083 9 30549ND501458
2-Butanone (MEK)ug/kg 1100 82 10-18173 11 301100ND898807
2-Chlorotoluene ug/kg 549 93 38-14786 8 30549ND512472
2-Hexanone ug/kg v1110010818-16997 11 301100ND11901070
4-Chlorotoluene ug/kg 549 93 36-14586 8 30549ND512472
4-Methyl-2-pentanone
(MIBK)ug/kg 1100 93 16-17582 13 301100ND1020900
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 50 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2925340MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92483534001
2925341
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acetone ug/kg 1100 97 10-20087 11 301100ND1070960
Benzene ug/kg 549 91 46-13680 13 30549ND502440
Bromobenzene ug/kg 549 101 38-14992 9 30549ND552506
Bromochloromethane ug/kg 549 97 44-14286 12 30549ND535472
Bromodichloromethane ug/kg 549 84 41-14074 13 30549ND462407
Bromoform ug/kg v15499834-14585 14 30549ND541468
Bromomethane ug/kg 549 97 14-16282 16 3054916.7 549 469
Carbon tetrachloride ug/kg 549 95 44-14182 15 30549ND524452
Chlorobenzene ug/kg 549 98 39-14189 9 30549ND539491
Chloroethane ug/kg 549 26 10-18223 10 30549ND141128
Chloroform ug/kg 549 89 45-14083 7 30549ND490455
Chloromethane ug/kg 549 87 19-14978 11 30549ND483435
cis-1,2-Dichloroethene ug/kg 549 95 38-15086 10 30549ND524473
cis-1,3-Dichloropropene ug/kg 549 89 30-14479 13 30549ND491433
Dibromochloromethane ug/kg v154910636-14597 9 30549ND583534
Dibromomethane ug/kg 549 84 41-14578 8 30549ND463428
Dichlorodifluoromethane ug/kg 549 96 16-14686 11 30549ND528473
Diisopropyl ether ug/kg 549 94 41-14383 12 30549ND514456
Ethylbenzene ug/kg 549 87 35-14480 8 305499.6 486 447
Hexachloro-1,3-butadiene ug/kg 549 136 10-160125 8 30549ND745688
Isopropylbenzene
(Cumene)ug/kg 549 85 30-15281 5 30549ND467445
m&p-Xylene ug/kg 1100 88 33-14580 9 30110013.8 977 893
Methyl-tert-butyl ether ug/kg 549 92 49-14081 12 30549ND504447
Methylene Chloride ug/kg 549 97 10-17485 13 30549ND534469
n-Butylbenzene ug/kg 549 89 10-16079 12 30549ND488434
n-Propylbenzene ug/kg 549 87 24-15979 9 30549ND477435
Naphthalene ug/kg 549 82 10-17182 1 3054916.2 469 466
o-Xylene ug/kg 549 96 31-15089 8 30549ND534494
p-Isopropyltoluene ug/kg 549 82 21-15475 10 30549ND453411
sec-Butylbenzene ug/kg 549 84 19-15976 9 30549ND460419
Styrene ug/kg 549 98 15-15290 8 30549ND540497
tert-Butylbenzene ug/kg 549 79 31-14173 7 30549ND432403
Tetrachloroethene ug/kg 549 96 19-14189 8 30549ND530488
Toluene ug/kg 549 90 31-14680 11 305498.8 502 451
trans-1,2-Dichloroethene ug/kg 549 96 28-15788 9 30549ND530486
trans-1,3-Dichloropropene ug/kg 549 84 25-14674 13 30549ND459404
Trichloroethene ug/kg 549 94 34-14983 12 30549ND516457
Trichlorofluoromethane ug/kg 549 31 10-16727 13 30549ND170149
Vinyl acetate ug/kg 1100 93 10-20082 12 301100ND1020901
Vinyl chloride ug/kg v154911236-155100 11 30549ND614549
Xylene (Total)ug/kg 1650 91 29-14883 9 30165013.8 1510 1390
1,2-Dichloroethane-d4 (S)%113 70-132117
4-Bromofluorobenzene (S)%95 70-13095
Toluene-d8 (S)%95 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
549759
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92483554001, 92483554002, 92483554003, 92483554004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2923508
Associated Lab Samples:92483554001, 92483554002, 92483554003, 92483554004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/25/20 23:020.34
1,1,1-Trichloroethane ug/L ND 1.0 06/25/20 23:020.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/25/20 23:020.22
1,1,2-Trichloroethane ug/L ND 1.0 06/25/20 23:020.24
1,1-Dichloroethane ug/L ND 1.0 06/25/20 23:020.27
1,1-Dichloroethene ug/L ND 1.0 v206/25/20 23:020.24
1,1-Dichloropropene ug/L ND 1.0 06/25/20 23:020.21
1,2,3-Trichlorobenzene ug/L ND 1.0 06/25/20 23:020.34
1,2,3-Trichloropropane ug/L ND 1.0 06/25/20 23:020.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/25/20 23:020.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 06/25/20 23:020.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/25/20 23:020.26
1,2-Dichlorobenzene ug/L ND 1.0 06/25/20 23:020.29
1,2-Dichloroethane ug/L ND 1.0 06/25/20 23:020.34
1,2-Dichloropropane ug/L ND 1.0 06/25/20 23:020.19
1,3-Dichlorobenzene ug/L ND 1.0 06/25/20 23:020.22
1,3-Dichloropropane ug/L ND 1.0 06/25/20 23:020.16
1,4-Dichlorobenzene ug/L ND 1.0 06/25/20 23:020.26
2,2-Dichloropropane ug/L ND 1.0 06/25/20 23:020.27
2-Butanone (MEK)ug/L ND 5.0 06/25/20 23:023.3
2-Chlorotoluene ug/L ND 1.0 06/25/20 23:020.20
2-Hexanone ug/L ND 5.0 06/25/20 23:020.57
4-Chlorotoluene ug/L ND 1.0 06/25/20 23:020.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/25/20 23:024.5
Acetone ug/L ND 25.0 06/25/20 23:026.2
Benzene ug/L ND 1.0 06/25/20 23:020.15
Bromobenzene ug/L ND 1.0 06/25/20 23:020.22
Bromochloromethane ug/L ND 1.0 06/25/20 23:020.34
Bromodichloromethane ug/L ND 1.0 06/25/20 23:020.26
Bromoform ug/L ND 1.0 06/25/20 23:020.62
Bromomethane ug/L ND 2.0 v206/25/20 23:020.62
Carbon tetrachloride ug/L ND 1.0 06/25/20 23:020.22
Chlorobenzene ug/L ND 1.0 06/25/20 23:020.23
Chloroethane ug/L ND 1.0 06/25/20 23:020.49
Chloroform ug/L ND 5.0 06/25/20 23:022.3
Chloromethane ug/L ND 1.0 v206/25/20 23:020.39
cis-1,2-Dichloroethene ug/L ND 1.0 06/25/20 23:020.29
cis-1,3-Dichloropropene ug/L ND 1.0 06/25/20 23:020.30
Dibromochloromethane ug/L ND 1.0 06/25/20 23:020.41
Dibromomethane ug/L ND 1.0 06/25/20 23:020.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2923508
Associated Lab Samples:92483554001, 92483554002, 92483554003, 92483554004
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 06/25/20 23:020.23
Diisopropyl ether ug/L ND 1.0 06/25/20 23:020.22
Ethylbenzene ug/L ND 1.0 06/25/20 23:020.26
Hexachloro-1,3-butadiene ug/L 0.50J 1.0 06/25/20 23:020.44
m&p-Xylene ug/L ND 2.0 06/25/20 23:020.41
Methyl-tert-butyl ether ug/L ND 1.0 06/25/20 23:020.28
Methylene Chloride ug/L ND 5.0 06/25/20 23:023.7
Naphthalene ug/L ND 1.0 06/25/20 23:020.35
o-Xylene ug/L ND 1.0 06/25/20 23:020.22
p-Isopropyltoluene ug/L ND 1.0 06/25/20 23:020.21
Styrene ug/L ND 1.0 06/25/20 23:020.27
Tetrachloroethene ug/L ND 1.0 06/25/20 23:020.16
Toluene ug/L ND 1.0 06/25/20 23:020.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/25/20 23:020.25
trans-1,3-Dichloropropene ug/L ND 1.0 06/25/20 23:020.31
Trichloroethene ug/L ND 1.0 06/25/20 23:020.22
Trichlorofluoromethane ug/L ND 1.0 06/25/20 23:020.31
Vinyl acetate ug/L ND 2.0 IK06/25/20 23:021.4
Vinyl chloride ug/L ND 1.0 v206/25/20 23:020.24
Xylene (Total)ug/L ND 1.0 06/25/20 23:020.63
1,2-Dichloroethane-d4 (S)%91 70-130 06/25/20 23:02
4-Bromofluorobenzene (S)%99 70-130 06/25/20 23:02
Toluene-d8 (S)%97 70-130 06/25/20 23:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2923509LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 60.550 121 70-130
1,1,1-Trichloroethane ug/L 48.950 98 70-130
1,1,2,2-Tetrachloroethane ug/L 55.750 111 70-130
1,1,2-Trichloroethane ug/L 54.250 108 70-130
1,1-Dichloroethane ug/L 46.150 92 70-130
1,1-Dichloroethene ug/L 47.7 v3509570-130
1,1-Dichloropropene ug/L 50.850 102 70-130
1,2,3-Trichlorobenzene ug/L 59.350 119 70-130
1,2,3-Trichloropropane ug/L 56.550 113 70-130
1,2,4-Trichlorobenzene ug/L 58.850 118 70-130
1,2-Dibromo-3-chloropropane ug/L 63.350 127 70-130
1,2-Dibromoethane (EDB)ug/L 58.850 118 70-130
1,2-Dichlorobenzene ug/L 57.650 115 70-130
1,2-Dichloroethane ug/L 46.250 92 70-130
1,2-Dichloropropane ug/L 50.150 100 70-130
1,3-Dichlorobenzene ug/L 58.450 117 70-130
1,3-Dichloropropane ug/L 56.250 112 70-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2923509LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 57.950 116 70-130
2,2-Dichloropropane ug/L 46.050 92 69-130
2-Butanone (MEK)ug/L 107100 107 64-135
2-Chlorotoluene ug/L 56.550 113 70-130
2-Hexanone ug/L 114100 114 66-135
4-Chlorotoluene ug/L 55.250 110 70-130
4-Methyl-2-pentanone (MIBK)ug/L 105100 105 70-130
Acetone ug/L 107100 107 61-157
Benzene ug/L 50.850 102 70-130
Bromobenzene ug/L 60.550 121 70-130
Bromochloromethane ug/L 49.650 99 70-130
Bromodichloromethane ug/L 48.550 97 70-130
Bromoform ug/L 63.850 128 70-130
Bromomethane ug/L 33.4 v3506738-130
Carbon tetrachloride ug/L 53.750 107 70-130
Chlorobenzene ug/L 56.850 114 70-130
Chloroethane ug/L 38.650 77 37-142
Chloroform ug/L 48.750 97 70-130
Chloromethane ug/L 35.2 v3507048-130
cis-1,2-Dichloroethene ug/L 45.950 92 70-130
cis-1,3-Dichloropropene ug/L 54.350 109 70-130
Dibromochloromethane ug/L 62.150 124 70-130
Dibromomethane ug/L 55.950 112 70-130
Dichlorodifluoromethane ug/L 46.350 93 53-134
Diisopropyl ether ug/L 47.550 95 70-135
Ethylbenzene ug/L 54.050 108 70-130
Hexachloro-1,3-butadiene ug/L 56.750 113 68-132
m&p-Xylene ug/L 108100 108 70-130
Methyl-tert-butyl ether ug/L 51.650 103 70-130
Methylene Chloride ug/L 43.050 86 67-132
Naphthalene ug/L 57.850 116 70-130
o-Xylene ug/L 55.050 110 70-131
p-Isopropyltoluene ug/L 55.450 111 70-130
Styrene ug/L 56.950 114 70-130
Tetrachloroethene ug/L 59.250 118 69-130
Toluene ug/L 52.050 104 70-130
trans-1,2-Dichloroethene ug/L 46.550 93 70-130
trans-1,3-Dichloropropene ug/L 51.650 103 70-130
Trichloroethene ug/L 55.850 112 70-130
Trichlorofluoromethane ug/L 44.850 90 63-130
Vinyl acetate ug/L 96.7 IK1009755-143
Vinyl chloride ug/L 45.1 v3509070-131
Xylene (Total)ug/L 163150 109 70-130
1,2-Dichloroethane-d4 (S)%88 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2923510MATRIX SPIKE SAMPLE:
MSSpike
Result
92483273010
1,1,1,2-Tetrachloroethane ug/L 19.620 98 73-134ND
1,1,1-Trichloroethane ug/L 21.420 107 82-143ND
1,1,2,2-Tetrachloroethane ug/L 21.820 109 70-136ND
1,1,2-Trichloroethane ug/L 20.620 103 70-135ND
1,1-Dichloroethane ug/L 23.820 119 70-139ND
1,1-Dichloroethene ug/L 24.220 121 70-154ND
1,1-Dichloropropene ug/L 23.520 117 70-149ND
1,2,3-Trichlorobenzene ug/L 20.020 100 70-135ND
1,2,3-Trichloropropane ug/L 19.220 96 71-137ND
1,2,4-Trichlorobenzene ug/L 19.920 99 73-140ND
1,2-Dibromo-3-chloropropane ug/L 18.220 91 65-134ND
1,2-Dibromoethane (EDB)ug/L 21.020 105 70-137ND
1,2-Dichlorobenzene ug/L 20.820 104 70-133ND
1,2-Dichloroethane ug/L 21.220 106 70-137ND
1,2-Dichloropropane ug/L 23.020 115 70-140ND
1,3-Dichlorobenzene ug/L 20.520 102 70-135ND
1,3-Dichloropropane ug/L 21.820 109 70-143ND
1,4-Dichlorobenzene ug/L 21.220 106 70-133ND
2,2-Dichloropropane ug/L 22.720 113 61-148ND
2-Butanone (MEK)ug/L 45.340 113 60-139ND
2-Chlorotoluene ug/L 22.120 111 70-144ND
2-Hexanone ug/L 43.740 109 65-138ND
4-Chlorotoluene ug/L 22.020 110 70-137ND
4-Methyl-2-pentanone (MIBK)ug/L 43.240 108 65-135ND
Acetone ug/L 45.940 115 60-148ND
Benzene ug/L 22.020 110 70-151ND
Bromobenzene ug/L 21.120 105 70-136ND
Bromochloromethane ug/L 22.620 113 70-141ND
Bromodichloromethane ug/L 19.620 98 70-138ND
Bromoform ug/L 17.320 87 63-130ND
Bromomethane ug/L 17.9 v3209015-152ND
Carbon tetrachloride ug/L 20.820 104 70-143ND
Chlorobenzene ug/L 20.720 104 70-138ND
Chloroethane ug/L 23.4 IK,v12011752-163ND
Chloroform ug/L 22.320 112 70-139ND
Chloromethane ug/L 19.720 99 41-139ND
cis-1,2-Dichloroethene ug/L 23.320 117 70-141ND
cis-1,3-Dichloropropene ug/L 21.720 108 70-137ND
Dibromochloromethane ug/L 19.620 98 70-134ND
Dibromomethane ug/L 19.120 95 70-138ND
Dichlorodifluoromethane ug/L 19.220 96 47-155ND
Diisopropyl ether ug/L 24.420 122 63-144ND
Ethylbenzene ug/L 21.120 106 66-153ND
Hexachloro-1,3-butadiene ug/L 19.6 v3209865-149ND
m&p-Xylene ug/L 42.340 106 69-152ND
Methyl-tert-butyl ether ug/L 22.520 113 54-156ND
Methylene Chloride ug/L 24.420 122 42-159ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2923510MATRIX SPIKE SAMPLE:
MSSpike
Result
92483273010
Naphthalene ug/L 19.620 98 61-148ND
o-Xylene ug/L 20.420 102 70-148ND
p-Isopropyltoluene ug/L 20.820 104 70-146ND
Styrene ug/L 20.120 101 70-135ND
Tetrachloroethene ug/L 19.520 97 59-143ND
Toluene ug/L 20.920 105 59-148ND
trans-1,2-Dichloroethene ug/L 24.020 120 70-146ND
trans-1,3-Dichloropropene ug/L 19.920 99 70-135ND
Trichloroethene ug/L 20.120 101 70-147ND
Trichlorofluoromethane ug/L 19.920 100 70-148ND
Vinyl acetate ug/L 46.540 116 49-151ND
Vinyl chloride ug/L 23.520 118 70-156ND
Xylene (Total)ug/L 62.760 104 63-158ND
1,2-Dichloroethane-d4 (S)%112 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92483559001
2923511SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92483559001
2923511SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND v230ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND IK,v130ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND v230ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L 44.7 20 3054.4
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%11291
4-Bromofluorobenzene (S)%9998
Toluene-d8 (S)%9997
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
549993
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92483554010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2924848
Associated Lab Samples:92483554010
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 v106/27/20 00:230.34
1,1,1-Trichloroethane ug/L ND 1.0 06/27/20 00:230.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/27/20 00:230.22
1,1,2-Trichloroethane ug/L ND 1.0 06/27/20 00:230.24
1,1-Dichloroethane ug/L ND 1.0 06/27/20 00:230.27
1,1-Dichloroethene ug/L ND 1.0 06/27/20 00:230.24
1,1-Dichloropropene ug/L ND 1.0 06/27/20 00:230.21
1,2,3-Trichlorobenzene ug/L ND 1.0 v106/27/20 00:230.34
1,2,3-Trichloropropane ug/L ND 1.0 06/27/20 00:230.35
1,2,4-Trichlorobenzene ug/L ND 1.0 06/27/20 00:230.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 v106/27/20 00:230.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 06/27/20 00:230.26
1,2-Dichlorobenzene ug/L ND 1.0 06/27/20 00:230.29
1,2-Dichloroethane ug/L ND 1.0 06/27/20 00:230.34
1,2-Dichloropropane ug/L ND 1.0 06/27/20 00:230.19
1,3-Dichlorobenzene ug/L ND 1.0 06/27/20 00:230.22
1,3-Dichloropropane ug/L ND 1.0 06/27/20 00:230.16
1,4-Dichlorobenzene ug/L ND 1.0 06/27/20 00:230.26
2,2-Dichloropropane ug/L ND 1.0 06/27/20 00:230.27
2-Butanone (MEK)ug/L ND 5.0 06/27/20 00:233.3
2-Chlorotoluene ug/L ND 1.0 06/27/20 00:230.20
2-Hexanone ug/L ND 5.0 06/27/20 00:230.57
4-Chlorotoluene ug/L ND 1.0 06/27/20 00:230.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 06/27/20 00:234.5
Acetone ug/L ND 25.0 06/27/20 00:236.2
Benzene ug/L ND 1.0 06/27/20 00:230.15
Bromobenzene ug/L ND 1.0 06/27/20 00:230.22
Bromochloromethane ug/L ND 1.0 06/27/20 00:230.34
Bromodichloromethane ug/L ND 1.0 06/27/20 00:230.26
Bromoform ug/L ND 1.0 v106/27/20 00:230.62
Bromomethane ug/L ND 2.0 v206/27/20 00:230.62
Carbon tetrachloride ug/L ND 1.0 06/27/20 00:230.22
Chlorobenzene ug/L ND 1.0 06/27/20 00:230.23
Chloroethane ug/L ND 1.0 06/27/20 00:230.49
Chloroform ug/L ND 5.0 06/27/20 00:232.3
Chloromethane ug/L ND 1.0 v206/27/20 00:230.39
cis-1,2-Dichloroethene ug/L ND 1.0 06/27/20 00:230.29
cis-1,3-Dichloropropene ug/L ND 1.0 06/27/20 00:230.30
Dibromochloromethane ug/L ND 1.0 v106/27/20 00:230.41
Dibromomethane ug/L ND 1.0 06/27/20 00:230.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2924848
Associated Lab Samples:92483554010
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 06/27/20 00:230.23
Diisopropyl ether ug/L ND 1.0 06/27/20 00:230.22
Ethylbenzene ug/L ND 1.0 06/27/20 00:230.26
Hexachloro-1,3-butadiene ug/L ND 1.0 06/27/20 00:230.44
m&p-Xylene ug/L ND 2.0 06/27/20 00:230.41
Methyl-tert-butyl ether ug/L ND 1.0 06/27/20 00:230.28
Methylene Chloride ug/L ND 5.0 06/27/20 00:233.7
Naphthalene ug/L ND 1.0 06/27/20 00:230.35
o-Xylene ug/L ND 1.0 06/27/20 00:230.22
p-Isopropyltoluene ug/L ND 1.0 06/27/20 00:230.21
Styrene ug/L ND 1.0 06/27/20 00:230.27
Tetrachloroethene ug/L ND 1.0 v106/27/20 00:230.16
Toluene ug/L ND 1.0 06/27/20 00:230.24
trans-1,2-Dichloroethene ug/L ND 1.0 06/27/20 00:230.25
trans-1,3-Dichloropropene ug/L ND 1.0 06/27/20 00:230.31
Trichloroethene ug/L ND 1.0 06/27/20 00:230.22
Trichlorofluoromethane ug/L ND 1.0 06/27/20 00:230.31
Vinyl acetate ug/L ND 2.0 IK06/27/20 00:231.4
Vinyl chloride ug/L ND 1.0 06/27/20 00:230.24
Xylene (Total)ug/L ND 1.0 06/27/20 00:230.63
1,2-Dichloroethane-d4 (S)%91 70-130 06/27/20 00:23
4-Bromofluorobenzene (S)%98 70-130 06/27/20 00:23
Toluene-d8 (S)%99 70-130 06/27/20 00:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2924849LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 60.6 v15012170-130
1,1,1-Trichloroethane ug/L 49.250 98 70-130
1,1,2,2-Tetrachloroethane ug/L 55.550 111 70-130
1,1,2-Trichloroethane ug/L 53.850 108 70-130
1,1-Dichloroethane ug/L 46.850 94 70-130
1,1-Dichloroethene ug/L 47.950 96 70-130
1,1-Dichloropropene ug/L 51.450 103 70-130
1,2,3-Trichlorobenzene ug/L 60.1 v15012070-130
1,2,3-Trichloropropane ug/L 56.050 112 70-130
1,2,4-Trichlorobenzene ug/L 59.850 120 70-130
1,2-Dibromo-3-chloropropane ug/L 61.0 v15012270-130
1,2-Dibromoethane (EDB)ug/L 59.350 119 70-130
1,2-Dichlorobenzene ug/L 58.550 117 70-130
1,2-Dichloroethane ug/L 46.650 93 70-130
1,2-Dichloropropane ug/L 49.150 98 70-130
1,3-Dichlorobenzene ug/L 58.950 118 70-130
1,3-Dichloropropane ug/L 56.750 113 70-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2924849LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 58.350 117 70-130
2,2-Dichloropropane ug/L 47.550 95 69-130
2-Butanone (MEK)ug/L 102100 102 64-135
2-Chlorotoluene ug/L 56.450 113 70-130
2-Hexanone ug/L 108100 108 66-135
4-Chlorotoluene ug/L 55.050 110 70-130
4-Methyl-2-pentanone (MIBK)ug/L 99.0100 99 70-130
Acetone ug/L 103100 103 61-157
Benzene ug/L 50.850 102 70-130
Bromobenzene ug/L 59.350 119 70-130
Bromochloromethane ug/L 53.050 106 70-130
Bromodichloromethane ug/L 47.750 95 70-130
Bromoform ug/L 62.7 v15012570-130
Bromomethane ug/L 35.0 v3507038-130
Carbon tetrachloride ug/L 54.350 109 70-130
Chlorobenzene ug/L 57.550 115 70-130
Chloroethane ug/L 42.850 86 37-142
Chloroform ug/L 49.150 98 70-130
Chloromethane ug/L 34.4 v3506948-130
cis-1,2-Dichloroethene ug/L 46.650 93 70-130
cis-1,3-Dichloropropene ug/L 53.250 106 70-130
Dibromochloromethane ug/L 62.1 v15012470-130
Dibromomethane ug/L 55.650 111 70-130
Dichlorodifluoromethane ug/L 48.050 96 53-134
Diisopropyl ether ug/L 46.850 94 70-135
Ethylbenzene ug/L 54.550 109 70-130
Hexachloro-1,3-butadiene ug/L 58.950 118 68-132
m&p-Xylene ug/L 110100 110 70-130
Methyl-tert-butyl ether ug/L 51.550 103 70-130
Methylene Chloride ug/L 43.750 87 67-132
Naphthalene ug/L 57.950 116 70-130
o-Xylene ug/L 55.350 111 70-131
p-Isopropyltoluene ug/L 56.550 113 70-130
Styrene ug/L 57.050 114 70-130
Tetrachloroethene ug/L 60.2 v15012069-130
Toluene ug/L 51.250 102 70-130
trans-1,2-Dichloroethene ug/L 47.150 94 70-130
trans-1,3-Dichloropropene ug/L 50.450 101 70-130
Trichloroethene ug/L 56.650 113 70-130
Trichlorofluoromethane ug/L 47.050 94 63-130
Vinyl acetate ug/L 95.0 IK1009555-143
Vinyl chloride ug/L 46.650 93 70-131
Xylene (Total)ug/L 165150 110 70-130
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2925982MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92483488006
2925983
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 117 73-134121 3 3020ND23.4 24.2
1,1,1-Trichloroethane ug/L 20 109 82-143113 4 3020ND21.9 22.7
1,1,2,2-Tetrachloroethane ug/L 20 107 70-136108 1 3020ND21.4 21.6
1,1,2-Trichloroethane ug/L 20 107 70-135111 4 3020ND21.3 22.2
1,1-Dichloroethane ug/L 20 100 70-139105 5 3020ND20.0 20.9
1,1-Dichloroethene ug/L 20 105 70-154111 5 3020ND21.1 22.1
1,1-Dichloropropene ug/L 20 112 70-149115 3 3020ND22.3 23.0
1,2,3-Trichlorobenzene ug/L 20 116 70-135120 3 3020ND23.1 23.9
1,2,3-Trichloropropane ug/L 20 105 71-137106 1 3020ND21.1 21.3
1,2,4-Trichlorobenzene ug/L 20 115 73-140120 4 3020ND23.0 23.9
1,2-Dibromo-3-
chloropropane ug/L 20 119 65-134116 2 3020ND23.8 23.2
1,2-Dibromoethane (EDB)ug/L 20 115 70-137117 2 3020ND22.9 23.3
1,2-Dichlorobenzene ug/L 20 114 70-133118 3 3020ND22.8 23.5
1,2-Dichloroethane ug/L 20 99 70-137102 3 3020ND20.2 20.7
1,2-Dichloropropane ug/L 20 102 70-140106 4 3020ND20.5 21.3
1,3-Dichlorobenzene ug/L 20 115 70-135119 4 3020ND22.9 23.9
1,3-Dichloropropane ug/L 20 109 70-143114 4 3020ND21.9 22.7
1,4-Dichlorobenzene ug/L 20 113 70-133119 5 3020ND22.6 23.7
2,2-Dichloropropane ug/L 20 102 61-148105 3 3020ND20.5 21.1
2-Butanone (MEK)ug/L 40 104 60-139102 2 3040ND41.4 40.6
2-Chlorotoluene ug/L 20 113 70-144117 4 3020ND22.5 23.4
2-Hexanone ug/L 40 103 65-138102 2 3040ND41.3 40.6
4-Chlorotoluene ug/L 20 109 70-137115 5 3020ND21.9 22.9
4-Methyl-2-pentanone
(MIBK)ug/L 40 93 65-13593 0 3040ND37.3 37.3
Acetone ug/L 40 106 60-148107 1 3040ND42.3 42.6
Benzene ug/L 20 107 70-151111 4 3020ND21.4 22.2
Bromobenzene ug/L 20 117 70-136122 4 3020ND23.4 24.4
Bromochloromethane ug/L 20 118 70-141122 3 3020ND23.6 24.4
Bromodichloromethane ug/L 20 100 70-138104 4 3020ND20.0 20.9
Bromoform ug/L v12012463-130125 1 3020ND24.8 25.1
Bromomethane ug/L v32010015-15293 7 3020ND19.9 18.6
Carbon tetrachloride ug/L 20 118 70-143122 4 3020ND23.5 24.4
Chlorobenzene ug/L 20 114 70-138119 4 3020ND22.8 23.8
Chloroethane ug/L 20 103 52-163111 8 3020ND20.6 22.3
Chloroform ug/L 20 106 70-139108 2 3020ND21.2 21.6
Chloromethane ug/L 20 79 41-13978 2 3020ND15.9 15.6
cis-1,2-Dichloroethene ug/L 20 98 70-141103 2 302042.2 61.7 62.7
cis-1,3-Dichloropropene ug/L 20 109 70-137112 2 3020ND21.8 22.3
Dibromochloromethane ug/L v12012270-134125 2 3020ND24.4 24.9
Dibromomethane ug/L 20 114 70-138120 5 3020ND22.9 24.0
Dichlorodifluoromethane ug/L 20 95 47-15599 4 3020ND19.0 19.8
Diisopropyl ether ug/L 20 92 63-14495 2 3020ND18.6 19.1
Ethylbenzene ug/L 20 111 66-153115 4 3020ND22.2 23.1
Hexachloro-1,3-butadiene ug/L 20 118 65-149123 4 3020ND23.6 24.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2925982MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92483488006
2925983
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 112 69-152116 4 3040ND44.7 46.5
Methyl-tert-butyl ether ug/L 20 104 54-156108 3 3020ND20.8 21.5
Methylene Chloride ug/L 20 94 42-15997 3 3020ND18.8 19.4
Naphthalene ug/L 20 108 61-148110 1 3020ND21.6 21.9
o-Xylene ug/L 20 112 70-148115 2 3020ND22.4 22.9
p-Isopropyltoluene ug/L 20 112 70-146115 3 3020ND22.4 23.1
Styrene ug/L 20 112 70-135118 5 3020ND22.4 23.6
Tetrachloroethene ug/L 20 119 59-143124 4 3020ND23.8 24.8
Toluene ug/L 20 106 59-148110 3 3020ND21.3 22.0
trans-1,2-Dichloroethene ug/L 20 100 70-146110 2 302053.2 73.3 75.1
trans-1,3-Dichloropropene ug/L 20 104 70-135106 3 3020ND20.7 21.3
Trichloroethene ug/L 20 121 70-147126 4 3020ND24.2 25.2
Trichlorofluoromethane ug/L 20 105 70-148109 4 3020ND20.9 21.8
Vinyl acetate ug/L IK4010149-151102 1 3040ND40.5 40.8
Vinyl chloride ug/L 20 100 70-156105 5 30200.50J 20.6 21.6
Xylene (Total)ug/L 60 112 63-158116 3 3060ND67.1 69.4
1,2-Dichloroethane-d4 (S)%95 70-13092
4-Bromofluorobenzene (S)%98 70-13099
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
549828
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92483554001, 92483554002, 92483554003, 92483554004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2923795
Associated Lab Samples:92483554001, 92483554002, 92483554003, 92483554004
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 06/28/20 11:341.6
1,2-Dichlorobenzene ug/L ND 10.0 06/28/20 11:341.4
1,3-Dichlorobenzene ug/L ND 10.0 06/28/20 11:341.4
1,4-Dichlorobenzene ug/L ND 10.0 06/28/20 11:341.5
1-Methylnaphthalene ug/L ND 10.0 06/28/20 11:341.4
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 06/28/20 11:341.3
2,4,5-Trichlorophenol ug/L ND 10.0 06/28/20 11:341.5
2,4,6-Trichlorophenol ug/L ND 10.0 06/28/20 11:341.4
2,4-Dichlorophenol ug/L ND 10.0 06/28/20 11:341.5
2,4-Dimethylphenol ug/L ND 10.0 06/28/20 11:341.5
2,4-Dinitrophenol ug/L ND 50.0 06/28/20 11:347.3
2,4-Dinitrotoluene ug/L ND 10.0 06/28/20 11:341.7
2,6-Dinitrotoluene ug/L ND 10.0 06/28/20 11:341.7
2-Chloronaphthalene ug/L ND 10.0 06/28/20 11:341.4
2-Chlorophenol ug/L ND 10.0 06/28/20 11:341.4
2-Methylnaphthalene ug/L ND 10.0 06/28/20 11:341.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 06/28/20 11:341.2
2-Nitroaniline ug/L ND 20.0 06/28/20 11:343.0
2-Nitrophenol ug/L ND 10.0 06/28/20 11:341.7
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 06/28/20 11:341.2
3,3'-Dichlorobenzidine ug/L ND 20.0 06/28/20 11:342.7
3-Nitroaniline ug/L ND 20.0 06/28/20 11:342.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 06/28/20 11:344.5
4-Bromophenylphenyl ether ug/L ND 10.0 06/28/20 11:341.2
4-Chloro-3-methylphenol ug/L ND 10.0 06/28/20 11:342.8
4-Chloroaniline ug/L ND 20.0 06/28/20 11:342.8
4-Chlorophenylphenyl ether ug/L ND 10.0 06/28/20 11:341.5
4-Nitroaniline ug/L ND 20.0 06/28/20 11:343.1
4-Nitrophenol ug/L ND 50.0 06/28/20 11:349.4
Acenaphthene ug/L ND 10.0 06/28/20 11:341.4
Acenaphthylene ug/L ND 10.0 06/28/20 11:341.5
Aniline ug/L ND 10.0 06/28/20 11:341.6
Anthracene ug/L ND 10.0 06/28/20 11:341.6
Benzo(a)anthracene ug/L ND 10.0 06/28/20 11:341.5
Benzo(a)pyrene ug/L ND 10.0 06/28/20 11:341.8
Benzo(b)fluoranthene ug/L ND 10.0 06/28/20 11:341.7
Benzo(g,h,i)perylene ug/L ND 10.0 06/28/20 11:341.6
Benzo(k)fluoranthene ug/L ND 10.0 06/28/20 11:341.5
Benzoic Acid ug/L ND 50.0 06/28/20 11:3419.5
Benzyl alcohol ug/L ND 20.0 06/28/20 11:342.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2923795
Associated Lab Samples:92483554001, 92483554002, 92483554003, 92483554004
Matrix:Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/28/20 11:341.3
bis(2-Chloroethyl) ether ug/L ND 10.0 06/28/20 11:341.7
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 06/28/20 11:342.0
Butylbenzylphthalate ug/L ND 10.0 06/28/20 11:341.9
Chrysene ug/L ND 10.0 06/28/20 11:341.4
Di-n-butylphthalate ug/L ND 10.0 06/28/20 11:341.6
Di-n-octylphthalate ug/L ND 10.0 06/28/20 11:342.2
Dibenz(a,h)anthracene ug/L ND 10.0 06/28/20 11:341.6
Dibenzofuran ug/L ND 10.0 06/28/20 11:341.3
Diethylphthalate ug/L ND 10.0 06/28/20 11:341.6
Dimethylphthalate ug/L ND 10.0 06/28/20 11:341.4
Fluoranthene ug/L ND 10.0 06/28/20 11:341.6
Fluorene ug/L ND 10.0 06/28/20 11:341.4
Hexachloro-1,3-butadiene ug/L ND 10.0 06/28/20 11:341.6
Hexachlorobenzene ug/L ND 10.0 06/28/20 11:341.3
Hexachlorocyclopentadiene ug/L ND 10.0 06/28/20 11:342.4
Hexachloroethane ug/L ND 10.0 06/28/20 11:341.3
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 06/28/20 11:341.7
Isophorone ug/L ND 10.0 06/28/20 11:341.3
N-Nitroso-di-n-propylamine ug/L ND 10.0 06/28/20 11:341.3
N-Nitrosodimethylamine ug/L ND 10.0 06/28/20 11:341.8
N-Nitrosodiphenylamine ug/L ND 10.0 06/28/20 11:341.4
Naphthalene ug/L ND 10.0 06/28/20 11:341.6
Nitrobenzene ug/L ND 10.0 06/28/20 11:341.5
Pentachlorophenol ug/L ND 20.0 06/28/20 11:342.8
Phenanthrene ug/L ND 10.0 06/28/20 11:341.4
Phenol ug/L ND 10.0 06/28/20 11:341.5
Pyrene ug/L ND 10.0 06/28/20 11:341.5
2,4,6-Tribromophenol (S)%117 10-137 06/28/20 11:34
2-Fluorobiphenyl (S)%106 13-130 06/28/20 11:34
2-Fluorophenol (S)%77 10-130 06/28/20 11:34
Nitrobenzene-d5 (S)%109 13-130 06/28/20 11:34
Phenol-d6 (S)%63 10-130 06/28/20 11:34
Terphenyl-d14 (S)%149 25-130 S306/28/20 11:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2923796LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 50.750 101 30-130
1,2-Dichlorobenzene ug/L 48.450 97 30-130
1,3-Dichlorobenzene ug/L 47.950 96 20-130
1,4-Dichlorobenzene ug/L 50.050 100 30-130
1-Methylnaphthalene ug/L 51.150 102 30-130
2,2'-Oxybis(1-chloropropane)ug/L 47.450 95 20-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 64 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2923796LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 59.850 120 40-130
2,4,6-Trichlorophenol ug/L 56.550 113 40-130
2,4-Dichlorophenol ug/L 55.850 112 31-130
2,4-Dimethylphenol ug/L 57.250 114 30-130
2,4-Dinitrophenol ug/L 322250 129 30-130
2,4-Dinitrotoluene ug/L 57.150 114 49-130
2,6-Dinitrotoluene ug/L 58.750 117 50-130
2-Chloronaphthalene ug/L 52.450 105 30-130
2-Chlorophenol ug/L 49.950 100 30-130
2-Methylnaphthalene ug/L 53.250 106 30-130
2-Methylphenol(o-Cresol)ug/L 47.450 95 30-130
2-Nitroaniline ug/L 110100 110 40-130
2-Nitrophenol ug/L 55.050 110 20-130
3&4-Methylphenol(m&p Cresol)ug/L 46.350 93 20-130
3,3'-Dichlorobenzidine ug/L 109100 109 10-150
3-Nitroaniline ug/L 108100 108 40-130
4,6-Dinitro-2-methylphenol ug/L 125100 125 40-130
4-Bromophenylphenyl ether ug/L 55.550 111 30-130
4-Chloro-3-methylphenol ug/L 111100 111 30-130
4-Chloroaniline ug/L 93.4100 93 20-130
4-Chlorophenylphenyl ether ug/L 54.150 108 20-130
4-Nitroaniline ug/L 110100 110 40-130
4-Nitrophenol ug/L 171250 69 10-130
Acenaphthene ug/L 53.250 106 30-130
Acenaphthylene ug/L 54.750 109 30-130
Aniline ug/L 15.750 31 20-130
Anthracene ug/L 55.350 111 50-130
Benzo(a)anthracene ug/L 57.250 114 50-130
Benzo(a)pyrene ug/L 58.250 116 50-130
Benzo(b)fluoranthene ug/L 56.350 113 50-130
Benzo(g,h,i)perylene ug/L 55.650 111 50-130
Benzo(k)fluoranthene ug/L 58.450 117 50-130
Benzoic Acid ug/L 177250 71 10-130
Benzyl alcohol ug/L 101100 101 20-130
bis(2-Chloroethoxy)methane ug/L 52.250 104 30-130
bis(2-Chloroethyl) ether ug/L 50.250 100 30-130
bis(2-Ethylhexyl)phthalate ug/L 60.150 120 50-130
Butylbenzylphthalate ug/L 59.950 120 50-150
Chrysene ug/L 56.550 113 50-130
Di-n-butylphthalate ug/L 58.350 117 50-130
Di-n-octylphthalate ug/L 62.650 125 50-130
Dibenz(a,h)anthracene ug/L 57.050 114 40-130
Dibenzofuran ug/L 53.450 107 40-130
Diethylphthalate ug/L 55.950 112 40-130
Dimethylphthalate ug/L 55.650 111 40-130
Fluoranthene ug/L 57.550 115 30-130
Fluorene ug/L 55.250 110 20-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2923796LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 50.550 101 10-130
Hexachlorobenzene ug/L 55.150 110 30-130
Hexachlorocyclopentadiene ug/L 49.650 99 10-150
Hexachloroethane ug/L 47.050 94 10-130
Indeno(1,2,3-cd)pyrene ug/L 56.550 113 40-130
Isophorone ug/L 55.550 111 30-130
N-Nitroso-di-n-propylamine ug/L 52.150 104 30-130
N-Nitrosodimethylamine ug/L 41.350 83 10-130
N-Nitrosodiphenylamine ug/L 54.550 109 30-130
Naphthalene ug/L 50.950 102 20-130
Nitrobenzene ug/L 53.550 107 20-130
Pentachlorophenol ug/L 125100 125 10-140
Phenanthrene ug/L 54.350 109 50-130
Phenol ug/L 29.950 60 10-130
Pyrene ug/L 55.450 111 50-130
2,4,6-Tribromophenol (S)%S014210-137
2-Fluorobiphenyl (S)%121 13-130
2-Fluorophenol (S)%87 10-130
Nitrobenzene-d5 (S)%122 13-130
Phenol-d6 (S)%72 10-130
Terphenyl-d14 (S)%S015125-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2923797MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92483488006
2923798
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L M1502930-13018 3050ND14.6 8.8J
1,2-Dichlorobenzene ug/L M1502830-13018 3050ND13.8 8.9J
1,3-Dichlorobenzene ug/L M1502720-13016 3050ND13.4 8.1J
1,4-Dichlorobenzene ug/L M1502930-13018 3050ND14.3 8.8J
1-Methylnaphthalene ug/L M1,R1503030-13022 33 3050ND15.2 10.8
2,2'-Oxybis(1-
chloropropane)
ug/L 50 35 20-13042 16 3050ND17.7 20.8
2,4,5-Trichlorophenol ug/L 50 50 40-13066 27 3050ND25.2 33.0
2,4,6-Trichlorophenol ug/L 50 49 40-13063 24 3050ND24.7 31.5
2,4-Dichlorophenol ug/L 50 48 31-13063 26 3050ND24.0 31.3
2,4-Dimethylphenol ug/L 50 50 30-13065 27 3050ND25.0 32.7
2,4-Dinitrophenol ug/L 250 59 30-13078 28 30250ND148196
2,4-Dinitrotoluene ug/L 50 58 49-13073 23 3050ND28.9 36.4
2,6-Dinitrotoluene ug/L 50 52 50-13065 22 3050ND26.1 32.5
2-Chloronaphthalene ug/L M1503130-13024 29 3050ND15.7 11.8
2-Chlorophenol ug/L 50 44 30-13058 28 3050ND21.9 29.0
2-Methylnaphthalene ug/L M1503130-13023 30 3050ND15.3 11.4
2-Methylphenol(o-Cresol)ug/L R1504330-13059 32 3050ND21.3 29.3
2-Nitroaniline ug/L 100 51 40-13063 22 30100ND50.5 62.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2923797MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92483488006
2923798
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitrophenol ug/L 50 46 20-13062 29 3050ND23.1 30.8
3&4-Methylphenol(m&p
Cresol)ug/L R1504420-13059 31 3050ND21.8 29.7
3,3'-Dichlorobenzidine ug/L R11005010-15071 33 30100ND50.4 70.6
3-Nitroaniline ug/L 100 52 40-13067 25 30100ND52.3 67.1
4,6-Dinitro-2-methylphenol ug/L 100 63 40-13082 26 30100ND63.2 81.7
4-Bromophenylphenyl ether ug/L 50 44 30-13054 22 3050ND21.8 27.2
4-Chloro-3-methylphenol ug/L 100 50 30-13065 26 30100ND49.8 64.7
4-Chloroaniline ug/L 100 41 20-13053 26 30100ND41.1 53.1
4-Chlorophenylphenyl ether ug/L 50 36 20-13041 14 3050ND18.0 20.7
4-Nitroaniline ug/L R11005440-13076 33 30100ND54.2 75.8
4-Nitrophenol ug/L 250 45 10-13059 27 30250ND112146
Acenaphthene ug/L M1503330-13029 13 3050ND16.7 14.6
Acenaphthylene ug/L 50 34 30-13032 7 3050ND17.2 16.0
Aniline ug/L R1502220-13043 67 3050ND10.9 21.7
Anthracene ug/L 50 55 50-13068 21 3050ND27.6 33.9
Benzo(a)anthracene ug/L 50 66 50-13082 21 3050ND33.1 40.9
Benzo(a)pyrene ug/L 50 67 50-13084 22 3050ND33.4 41.8
Benzo(b)fluoranthene ug/L 50 67 50-13083 22 3050ND33.4 41.6
Benzo(g,h,i)perylene ug/L 50 67 50-13077 14 3050ND33.3 38.3
Benzo(k)fluoranthene ug/L 50 66 50-13084 24 3050ND33.2 42.1
Benzoic Acid ug/L R12503110-13050 47 30250ND78.2 126
Benzyl alcohol ug/L 100 47 20-13063 30 30100ND46.7 63.0
bis(2-
Chloroethoxy)methane
ug/L 50 45 30-13059 27 3050ND22.4 29.5
bis(2-Chloroethyl) ether ug/L 50 41 30-13054 26 3050ND20.5 26.8
bis(2-Ethylhexyl)phthalate ug/L 50 71 50-13088 21 3050ND35.7 44.2
Butylbenzylphthalate ug/L 50 69 50-15086 22 3050ND34.3 42.8
Chrysene ug/L 50 66 50-13080 19 3050ND33.2 40.2
Di-n-butylphthalate ug/L 50 66 50-13080 20 3050ND33.0 40.2
Di-n-octylphthalate ug/L 50 73 50-13089 20 3050ND36.3 44.5
Dibenz(a,h)anthracene ug/L 50 67 40-13078 15 3050ND33.6 39.0
Dibenzofuran ug/L M1503640-13037 2 3050ND18.0 18.3
Diethylphthalate ug/L 50 57 40-13069 20 3050ND28.3 34.7
Dimethylphthalate ug/L 50 53 40-13064 19 3050ND26.5 32.2
Fluoranthene ug/L 50 65 30-13078 18 3050ND32.3 38.8
Fluorene ug/L 50 40 20-13046 15 3050ND19.8 23.0
Hexachloro-1,3-butadiene ug/L 50 30 10-13014 3050ND14.9 6.9J
Hexachlorobenzene ug/L 50 50 30-13063 22 3050ND25.1 31.4
Hexachlorocyclopentadiene ug/L 50 25 10-15013 3050ND12.4 6.3J
Hexachloroethane ug/L 50 26 10-13013 3050ND12.8 6.7J
Indeno(1,2,3-cd)pyrene ug/L 50 66 40-13078 16 3050ND33.2 38.9
Isophorone ug/L 50 47 30-13062 27 3050ND23.4 30.8
N-Nitroso-di-n-propylamine ug/L 50 44 30-13059 30 3050ND22.1 29.7
N-Nitrosodimethylamine ug/L 50 41 10-13055 30 3050ND20.4 27.6
N-Nitrosodiphenylamine ug/L 50 50 30-13062 21 3050ND24.9 30.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2923797MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92483488006
2923798
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Naphthalene ug/L 50 30 20-13024 21 3050ND14.9 12.0
Nitrobenzene ug/L 50 41 20-13053 25 3050ND20.6 26.5
Pentachlorophenol ug/L 100 63 10-14082 26 30100ND63.5 82.5
Phenanthrene ug/L 50 52 50-13065 21 3050ND26.1 32.4
Phenol ug/L R1503210-13046 35 3050ND16.2 23.1
Pyrene ug/L 50 63 50-13081 25 3050ND31.6 40.7
2,4,6-Tribromophenol (S)%68 10-13782
2-Fluorobiphenyl (S)%44 13-13056
2-Fluorophenol (S)%42 10-13055
Nitrobenzene-d5 (S)%51 13-13066
Phenol-d6 (S)%38 10-13052
Terphenyl-d14 (S)%88 25-130107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
549972
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92483554005, 92483554006, 92483554007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2924575
Associated Lab Samples:92483554005, 92483554006, 92483554007
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 336 06/30/20 09:1276.9
1,2-Dichlorobenzene ug/kg ND 336 06/30/20 09:1272.6
1,3-Dichlorobenzene ug/kg ND 336 06/30/20 09:1275.6
1,4-Dichlorobenzene ug/kg ND 336 06/30/20 09:1273.8
1-Methylnaphthalene ug/kg ND 336 06/30/20 09:1289.4
2,2'-Oxybis(1-chloropropane)ug/kg ND 336 06/30/20 09:1293.3
2,4,5-Trichlorophenol ug/kg ND 336 06/30/20 09:1287.2
2,4,6-Trichlorophenol ug/kg ND 336 06/30/20 09:1284.3
2,4-Dichlorophenol ug/kg ND 336 06/30/20 09:12111
2,4-Dimethylphenol ug/kg ND 336 06/30/20 09:1283.6
2,4-Dinitrophenol ug/kg ND 1680 06/30/20 09:121070
2,4-Dinitrotoluene ug/kg ND 336 06/30/20 09:1288.9
2,6-Dinitrotoluene ug/kg ND 336 06/30/20 09:1287.8
2-Chloronaphthalene ug/kg ND 336 06/30/20 09:1274.7
2-Chlorophenol ug/kg ND 336 06/30/20 09:1278.1
2-Methylnaphthalene ug/kg ND 336 06/30/20 09:1285.4
2-Methylphenol(o-Cresol)ug/kg ND 336 06/30/20 09:1274.3
2-Nitroaniline ug/kg ND 1680 06/30/20 09:12169
2-Nitrophenol ug/kg ND 336 06/30/20 09:12104
3&4-Methylphenol(m&p Cresol)ug/kg ND 336 06/30/20 09:1284.4
3,3'-Dichlorobenzidine ug/kg ND 671 06/30/20 09:12234
3-Nitroaniline ug/kg ND 1680 06/30/20 09:12178
4,6-Dinitro-2-methylphenol ug/kg ND 671 06/30/20 09:12541
4-Bromophenylphenyl ether ug/kg ND 336 06/30/20 09:1288.1
4-Chloro-3-methylphenol ug/kg ND 671 06/30/20 09:12204
4-Chloroaniline ug/kg ND 671 06/30/20 09:12205
4-Chlorophenylphenyl ether ug/kg ND 336 06/30/20 09:1287.2
4-Nitroaniline ug/kg ND 671 06/30/20 09:12166
4-Nitrophenol ug/kg ND 1680 06/30/20 09:12535
Acenaphthene ug/kg ND 336 06/30/20 09:1286.3
Acenaphthylene ug/kg ND 336 06/30/20 09:1279.4
Aniline ug/kg ND 336 06/30/20 09:1275.4
Anthracene ug/kg ND 336 06/30/20 09:1287.1
Benzo(a)anthracene ug/kg ND 336 06/30/20 09:12107
Benzo(a)pyrene ug/kg ND 336 06/30/20 09:12145
Benzo(b)fluoranthene ug/kg ND 336 06/30/20 09:12135
Benzo(g,h,i)perylene ug/kg ND 336 06/30/20 09:12131
Benzo(k)fluoranthene ug/kg ND 336 06/30/20 09:12141
Benzoic Acid ug/kg ND 1680 06/30/20 09:12362
Benzyl alcohol ug/kg ND 671 06/30/20 09:12178
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2924575
Associated Lab Samples:92483554005, 92483554006, 92483554007
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 336 06/30/20 09:1289.6
bis(2-Chloroethyl) ether ug/kg ND 336 06/30/20 09:1271.3
bis(2-Ethylhexyl)phthalate ug/kg ND 336 06/30/20 09:12110
Butylbenzylphthalate ug/kg ND 336 06/30/20 09:1289.4
Chrysene ug/kg ND 336 06/30/20 09:1297.4
Di-n-butylphthalate ug/kg ND 336 06/30/20 09:1282.8
Di-n-octylphthalate ug/kg ND 336 06/30/20 09:12191
Dibenz(a,h)anthracene ug/kg ND 336 06/30/20 09:12134
Dibenzofuran ug/kg ND 336 06/30/20 09:1283.9
Diethylphthalate ug/kg ND 336 06/30/20 09:1272.8
Dimethylphthalate ug/kg ND 336 06/30/20 09:1275.9
Fluoranthene ug/kg ND 336 06/30/20 09:12101
Fluorene ug/kg ND 336 06/30/20 09:1289.8
Hexachloro-1,3-butadiene ug/kg ND 336 06/30/20 09:1281.6
Hexachlorobenzene ug/kg ND 336 06/30/20 09:1285.2
Hexachlorocyclopentadiene ug/kg ND 336 06/30/20 09:12134
Hexachloroethane ug/kg ND 336 06/30/20 09:1276.5
Indeno(1,2,3-cd)pyrene ug/kg ND 336 06/30/20 09:12154
Isophorone ug/kg ND 336 06/30/20 09:1272.9
N-Nitroso-di-n-propylamine ug/kg ND 336 06/30/20 09:1294.0
N-Nitrosodimethylamine ug/kg ND 336 06/30/20 09:1294.4
N-Nitrosodiphenylamine ug/kg ND 336 06/30/20 09:1285.6
Naphthalene ug/kg ND 336 06/30/20 09:1280.3
Nitrobenzene ug/kg ND 336 06/30/20 09:1280.1
Pentachlorophenol ug/kg ND 671 06/30/20 09:12154
Phenanthrene ug/kg ND 336 06/30/20 09:1284.5
Phenol ug/kg ND 336 06/30/20 09:1280.1
Pyrene ug/kg ND 336 06/30/20 09:1292.3
Pyridine ug/kg ND 336 06/30/20 09:1284.9
2,4,6-Tribromophenol (S)%55 27-110 06/30/20 09:12
2-Fluorobiphenyl (S)%55 30-110 06/30/20 09:12
2-Fluorophenol (S)%62 13-110 06/30/20 09:12
Nitrobenzene-d5 (S)%72 23-110 06/30/20 09:12
Phenol-d6 (S)%58 22-110 06/30/20 09:12
Terphenyl-d14 (S)%71 28-110 06/30/20 09:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2924576LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10801690 64 52-130
1,2-Dichlorobenzene ug/kg 11001690 65 51-130
1,3-Dichlorobenzene ug/kg 11501690 68 50-130
1,4-Dichlorobenzene ug/kg 11901690 70 49-130
1-Methylnaphthalene ug/kg 10801690 64 55-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2924576LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 11101690 66 30-130
2,4,5-Trichlorophenol ug/kg 11401690 67 55-130
2,4,6-Trichlorophenol ug/kg 10801690 64 57-130
2,4-Dichlorophenol ug/kg 10901690 65 56-130
2,4-Dimethylphenol ug/kg 11101690 66 51-130
2,4-Dinitrophenol ug/kg 47008450 56 27-133
2,4-Dinitrotoluene ug/kg 10801690 64 61-130
2,6-Dinitrotoluene ug/kg 10901690 64 60-130
2-Chloronaphthalene ug/kg 11101690 66 52-130
2-Chlorophenol ug/kg 11601690 69 54-130
2-Methylnaphthalene ug/kg 11001690 65 54-130
2-Methylphenol(o-Cresol)ug/kg 11301690 67 51-130
2-Nitroaniline ug/kg 23003380 68 51-130
2-Nitrophenol ug/kg 11101690 65 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 11201690 66 11-163
3,3'-Dichlorobenzidine ug/kg 17403380 51 10-132
3-Nitroaniline ug/kg 20303380 60 55-130
4,6-Dinitro-2-methylphenol ug/kg 21103380 62 47-142
4-Bromophenylphenyl ether ug/kg 10801690 64 59-130
4-Chloro-3-methylphenol ug/kg 22403380 66 55-130
4-Chloroaniline ug/kg 21603380 64 54-130
4-Chlorophenylphenyl ether ug/kg 10501690 62 58-130
4-Nitroaniline ug/kg 21303380 63 54-130
4-Nitrophenol ug/kg 53808450 64 48-130
Acenaphthene ug/kg 11201690 66 60-130
Acenaphthylene ug/kg 11401690 67 60-130
Aniline ug/kg 10601690 63 43-130
Anthracene ug/kg 10901690 64 63-130
Benzo(a)anthracene ug/kg 10601690 63 59-130
Benzo(a)pyrene ug/kg 11001690 65 57-130
Benzo(b)fluoranthene ug/kg 10401690 62 54-130
Benzo(g,h,i)perylene ug/kg 11901690 71 59-130
Benzo(k)fluoranthene ug/kg 11501690 68 54-130
Benzoic Acid ug/kg 37708450 45 19-130
Benzyl alcohol ug/kg 21803380 64 50-130
bis(2-Chloroethoxy)methane ug/kg 10801690 64 54-130
bis(2-Chloroethyl) ether ug/kg 11301690 67 48-130
bis(2-Ethylhexyl)phthalate ug/kg 11201690 66 45-134
Butylbenzylphthalate ug/kg 10901690 65 46-138
Chrysene ug/kg 11301690 67 58-130
Di-n-butylphthalate ug/kg 10701690 63 60-130
Di-n-octylphthalate ug/kg 10901690 64 53-130
Dibenz(a,h)anthracene ug/kg 11501690 68 59-130
Dibenzofuran ug/kg 10801690 64 60-130
Diethylphthalate ug/kg 10801690 64 60-130
Dimethylphthalate ug/kg 11001690 65 60-130
Fluoranthene ug/kg 1060 L216906365-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2924576LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 11201690 66 63-130
Hexachloro-1,3-butadiene ug/kg 11101690 66 46-130
Hexachlorobenzene ug/kg 10701690 63 58-130
Hexachlorocyclopentadiene ug/kg 8851690 52 23-130
Hexachloroethane ug/kg 11401690 68 47-130
Indeno(1,2,3-cd)pyrene ug/kg 11701690 70 60-130
Isophorone ug/kg 11201690 67 49-130
N-Nitroso-di-n-propylamine ug/kg 11001690 65 47-130
N-Nitrosodimethylamine ug/kg 11601690 69 45-130
N-Nitrosodiphenylamine ug/kg 10801690 64 59-130
Naphthalene ug/kg 11201690 67 55-130
Nitrobenzene ug/kg 11401690 68 49-130
Pentachlorophenol ug/kg 18703380 55 10-132
Phenanthrene ug/kg 11101690 65 62-130
Phenol ug/kg 11401690 67 46-130
Pyrene ug/kg 11301690 67 53-130
Pyridine ug/kg 9661690 57 37-130
2,4,6-Tribromophenol (S)%69 27-110
2-Fluorobiphenyl (S)%65 30-110
2-Fluorophenol (S)%70 13-110
Nitrobenzene-d5 (S)%66 23-110
Phenol-d6 (S)%70 22-110
Terphenyl-d14 (S)%73 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2924577MATRIX SPIKE SAMPLE:
MSSpike
Result
92483385010
1,2,4-Trichlorobenzene ug/kg 8031840 44 18-130ND
1,2-Dichlorobenzene ug/kg 8131840 44 14-130ND
1,3-Dichlorobenzene ug/kg 8501840 46 12-130ND
1,4-Dichlorobenzene ug/kg 8881840 48 10-130ND
1-Methylnaphthalene ug/kg 7971840 43 12-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 8221840 45 10-130ND
2,4,5-Trichlorophenol ug/kg 8361840 45 13-130ND
2,4,6-Trichlorophenol ug/kg 7971840 43 17-130ND
2,4-Dichlorophenol ug/kg 8081840 44 10-130ND
2,4-Dimethylphenol ug/kg 8151840 44 10-130ND
2,4-Dinitrophenol ug/kg 35309220 38 10-130ND
2,4-Dinitrotoluene ug/kg 7841840 42 24-130ND
2,6-Dinitrotoluene ug/kg 8101840 44 23-130ND
2-Chloronaphthalene ug/kg 8111840 44 19-130ND
2-Chlorophenol ug/kg 8631840 47 10-130ND
2-Methylnaphthalene ug/kg 8161840 44 18-130ND
2-Methylphenol(o-Cresol)ug/kg 8441840 46 10-130ND
2-Nitroaniline ug/kg 1700J3690 46 17-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2924577MATRIX SPIKE SAMPLE:
MSSpike
Result
92483385010
2-Nitrophenol ug/kg 8161840 44 10-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 8501840 46 10-130ND
3,3'-Dichlorobenzidine ug/kg 11803690 32 10-130ND
3-Nitroaniline ug/kg 1470J3690 40 24-130ND
4,6-Dinitro-2-methylphenol ug/kg 15403690 42 10-152ND
4-Bromophenylphenyl ether ug/kg 7561840 41 29-130ND
4-Chloro-3-methylphenol ug/kg 16403690 44 17-130ND
4-Chloroaniline ug/kg 15403690 42 14-130ND
4-Chlorophenylphenyl ether ug/kg 7451840 40 25-130ND
4-Nitroaniline ug/kg 15403690 42 22-130ND
4-Nitrophenol ug/kg 39309220 43 10-130ND
Acenaphthene ug/kg 8191840 44 20-130ND
Acenaphthylene ug/kg 8331840 45 25-130ND
Aniline ug/kg 3681840 20 10-130ND
Anthracene ug/kg 7901840 43 29-130ND
Benzo(a)anthracene ug/kg 7831840 42 19-130ND
Benzo(a)pyrene ug/kg 7951840 43 12-130ND
Benzo(b)fluoranthene ug/kg 7331840 40 14-130ND
Benzo(g,h,i)perylene ug/kg 9051840 49 10-130ND
Benzo(k)fluoranthene ug/kg 7651840 41 14-130ND
Benzoic Acid ug/kg 42609220 46 10-130ND
Benzyl alcohol ug/kg 16503690 45 13-130ND
bis(2-Chloroethoxy)methane ug/kg 8151840 44 16-130ND
bis(2-Chloroethyl) ether ug/kg 8201840 44 11-130ND
bis(2-Ethylhexyl)phthalate ug/kg 8081840 44 21-130ND
Butylbenzylphthalate ug/kg 7841840 42 23-130ND
Chrysene ug/kg 8411840 46 22-130ND
Di-n-butylphthalate ug/kg 7471840 40 30-130ND
Di-n-octylphthalate ug/kg 8091840 44 23-142ND
Dibenz(a,h)anthracene ug/kg 8271840 45 10-130ND
Dibenzofuran ug/kg 7801840 42 24-130ND
Diethylphthalate ug/kg 7921840 43 26-130ND
Dimethylphthalate ug/kg 7991840 43 22-130ND
Fluoranthene ug/kg 7681840 42 33-130ND
Fluorene ug/kg 7991840 43 22-130ND
Hexachloro-1,3-butadiene ug/kg 7991840 43 13-130ND
Hexachlorobenzene ug/kg 7381840 40 29-130ND
Hexachlorocyclopentadiene ug/kg 5901840 32 10-130ND
Hexachloroethane ug/kg 8451840 46 10-130ND
Indeno(1,2,3-cd)pyrene ug/kg 8281840 45 10-130ND
Isophorone ug/kg 8561840 46 13-130ND
N-Nitroso-di-n-propylamine ug/kg 8161840 44 12-130ND
N-Nitrosodimethylamine ug/kg 8161840 44 11-130ND
N-Nitrosodiphenylamine ug/kg 7521840 41 15-130ND
Naphthalene ug/kg 8451840 46 15-130ND
Nitrobenzene ug/kg 8411840 46 12-130ND
Pentachlorophenol ug/kg 13403690 36 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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Page 73 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2924577MATRIX SPIKE SAMPLE:
MSSpike
Result
92483385010
Phenanthrene ug/kg 7981840 43 27-130ND
Phenol ug/kg 8071840 44 10-130ND
Pyrene ug/kg 8161840 44 19-130ND
Pyridine ug/kg 139J M11840810-130ND
2,4,6-Tribromophenol (S)%45 27-110
2-Fluorobiphenyl (S)%43 30-110
2-Fluorophenol (S)%46 13-110
Nitrobenzene-d5 (S)%44 23-110
Phenol-d6 (S)%46 22-110
Terphenyl-d14 (S)%43 28-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92483385011
2924578SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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Huntersville, NC 28078
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Page 74 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92483385011
2924578SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%4750
2-Fluorobiphenyl (S)%4849
2-Fluorophenol (S)%5455
Nitrobenzene-d5 (S)%6062
Phenol-d6 (S)%5153
Terphenyl-d14 (S)%5960
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
549708
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92483554005, 92483554006, 92483554007
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92481502042
2923252SAMPLE DUPLICATE:
Percent Moisture %23.6 1 2523.3
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92483591001
2923358SAMPLE DUPLICATE:
Percent Moisture %46.4 7 2543.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1500991
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92483554005, 92483554006, 92483554007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3545123-1
Associated Lab Samples:92483554005, 92483554006, 92483554007
Matrix:Solid
AnalyzedMDL
Total Solids %ND 06/30/20 16:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3545123-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1234168-03
R3545123-3SAMPLE DUPLICATE:
Total Solids %94.4 0.332 1094.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
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Huntersville, NC 28078
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Page 77 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1501490
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92483554008, 92483554009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3545168-1
Associated Lab Samples:92483554008, 92483554009
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 06/30/20 18:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3545168-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1234179-13
R3545168-3SAMPLE DUPLICATE:
Total Solids %84.8 2.81 1087.2
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
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Page 78 of 85
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92483554
BCP-145
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1500521
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92483554005, 92483554006, 92483554007, 92483554008, 92483554009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3545824-1
Associated Lab Samples:92483554005, 92483554006, 92483554007, 92483554008, 92483554009
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 07/02/20 14:480.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3545824-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.4110.0 94.1 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3545824-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1233138-02
R3545824-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 25.4 92.9 75.0-12592.7 0.210 2025.4ND 23.6 23.5
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3545824-6MATRIX SPIKE SAMPLE:
MSSpike
Result
L1233138-02
Chromium, Hexavalent mg/kg 778841 92.5 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1233138-01
R3545824-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92483554009
R3545824-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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Page 79 of 85
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92483554
BCP-145
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 80 of 85
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92483554
BCP-145
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92483554001 1500580 1500580TMW-3 3015 EPA 6020B
92483554002 1500580 1500580TMW-4 3015 EPA 6020B
92483554003 1500580 1500580TMW-5 3015 EPA 6020B
92483554003 1517393 1517393TMW-5 3015 EPA 6020B
92483554004 1500580 1500580DUP-1 3015 EPA 6020B
92483554005 1500535 1500535COMP-1 3051 EPA 6020B
92483554006 1500535 1500535COMP-2 3051 EPA 6020B
92483554007 1500535 1500535COMP-DUP 3051 EPA 6020B
92483554008 1500535 1500535BKG-1 3051 EPA 6020B
92483554009 1500535 1500535BKG-2 3051 EPA 6020B
92483554001 1500765 1500765TMW-3 7470A EPA 7470A
92483554002 1500765 1500765TMW-4 7470A EPA 7470A
92483554003 1500765 1500765TMW-5 7470A EPA 7470A
92483554004 1500766 1500766DUP-1 7470A EPA 7470A
92483554005 1501369 1501369COMP-1 7471A EPA 7471B
92483554006 1501369 1501369COMP-2 7471A EPA 7471B
92483554007 1501369 1501369COMP-DUP 7471A EPA 7471B
92483554008 1501369 1501369BKG-1 7471A EPA 7471B
92483554009 1501369 1501369BKG-2 7471A EPA 7471B
92483554001 549828 550090TMW-3 EPA 3510C EPA 8270E
92483554002 549828 550090TMW-4 EPA 3510C EPA 8270E
92483554003 549828 550090TMW-5 EPA 3510C EPA 8270E
92483554004 549828 550090DUP-1 EPA 3510C EPA 8270E
92483554005 549972 550363COMP-1 EPA 3546 EPA 8270E
92483554006 549972 550363COMP-2 EPA 3546 EPA 8270E
92483554007 549972 550363COMP-DUP EPA 3546 EPA 8270E
92483554005 550146 550161COMP-1 EPA 5035A/5030B EPA 8260D
92483554006 550146 550161COMP-2 EPA 5035A/5030B EPA 8260D
92483554007 550146 550161COMP-DUP EPA 5035A/5030B EPA 8260D
92483554001 549759TMW-3 EPA 8260D
92483554002 549759TMW-4 EPA 8260D
92483554003 549759TMW-5 EPA 8260D
92483554004 549759DUP-1 EPA 8260D
92483554010 549993TRIP BLANK EPA 8260D
92483554005 549708COMP-1 ASTM D2974-87
92483554006 549708COMP-2 ASTM D2974-87
92483554007 549708COMP-DUP ASTM D2974-87
92483554005 1500991 1500991COMP-1 SM 2540 G SM 2540G
92483554006 1500991 1500991COMP-2 SM 2540 G SM 2540G
92483554007 1500991 1500991COMP-DUP SM 2540 G SM 2540G
92483554008 1501490 1501490BKG-1 SM 2540 G SM 2540G
92483554009 1501490 1501490BKG-2 SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 85
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92483554
BCP-145
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92483554005 1500521 1500521COMP-1 3060A EPA 7199
92483554006 1500521 1500521COMP-2 3060A EPA 7199
92483554007 1500521 1500521COMP-DUP 3060A EPA 7199
92483554008 1500521 1500521BKG-1 3060A EPA 7199
92483554009 1500521 1500521BKG-2 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/31/2020 02:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 85
Page 83 of 85
Page 84 of 85
Page 85 of 85

Appendix D

Field Sampling Forms
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record/DVW8SGDWHG://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/BCP-145Kroehler ManufacturingUpgradient6/25/2040.0032.24AEM35Sunny 80s09:1509:2509:3509:4532.2433.5434.6134.785001,5002,5003,500100 mL/min 5.455.695.655.6419.920.320.220.269.168.268.067.95.855.845.845.84-47.0-41.3-38.6-37.2105.6045.3316.516.33YSI Pro Plus and HACH 2100QcourierVOCs by8260(3 40-mL voas), SVOCs by8270(2 100-mL unpreserveambers), RCRA metals by6020/7471(1 250-mLplastic, nitric acid)PeristalticPVC1-inch09:50Pace AnalyticalTMW-33040Polyethylene bgs
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record/DVW8SGDWHG://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/BCP-145Kroehler ManufacturingDowngradient6/25/2040.0030.41AEM35Sunny 80s08:0508:1008:1508:2008:2508:3531.5331.3931.4031.4831.6031.775001,0001,5002,0002,5003,500100 mL/min 3.643.573.893.813.753.7127.927.527.827.727.627.6190.6182.6182.0179.6174.4176.26.226.226.196.186.176.16-98.8-95.7-78.6-62.4-59.7-58.996.6072.6072.2043.2020.307.41YSI Pro Plus and HACH 2100QcourierVOCs by8260(3 40-mL voas), SVOCs by8270(2 100-mL unpreserveambers), RCRA metals by6020/7471(1 250-mLplastic, nitric acid)PeristalticPVC1-inch08:40Pace AnalyticalTMW-43040Polyethylene bgs
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record/DVW8SGDWHG://201Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\6HFRQGDU\LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERS6WDELOL]DWLRQFULWHULDJXLGHOLQHVIURPWKH(3$6(6'2SHUDWLQJ3URFHGXUHIRU*URXQGZDWHU6DPSOLQJGDWHG$SULO7XUE178VIRUPHWDOV:DWHU/HYHOVOLJKWRUVWDEOHGUDZGRZQGXULQJSXUJLQJS+XQLW6 &RQG253P9'2PJ/BCP-145Kroehler ManufacturingDowngradient6/25/2033.0030.11AEM31Sunny 80sDUP-1 collected06:5006:5306:5606:5907:0231.2231.2331.2331.2331.235008001,1001,4001,700100 mL/min 2.182.161.671.691.6522.322.322.322.322.3165.0164.8150.6144.0142.45.575.575.515.495.48-81.1-81.0-86.1-89.7-90.168.4032.1026.5016.505.66YSI Pro Plus and HACH 2100QcourierVOCs by8260(3 40-mL voas), SVOCs by8270(2 100-mL unpreserveambers), RCRA metals by6020/7471(1 250-mLplastic, nitric acid)PeristalticPVC1-inch07:05Pace AnalyticalTMW-52333Polyethylene bgs

Appendix E

DEQ Risk Calculator (July 2020)
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
7/31/2020
Prepared By:H&H
Worst-Case Groundwater
North Carolina Department of Environmental Quality
Risk Calculator
Kroehler Manufacturing
3412 Monroe Road
DEQ DWM Brownfields
23081-19-060
July 2020
May 2020 EPA RSL Table
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 23081-19-060
Exposure Unit ID: Worst-Case Groundwater
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 23081-19-060
Exposure Unit ID: Worst-Case Groundwater
Description of Exposure Point Concentration Selection:
Exposure Point
Concentration
(ug/L)
Notes:CAS Number Chemical
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection
Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
4.9 67-66-3 Chloroform ug/L
1.5 75-35-4 Dichloroethylene, 1,1-ug/L
1.7 79-01-6 Trichloroethylene ug/L
Input Form 2B
Groundwater Exposure Point Concentration Table
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 23081-19-060
Exposure Unit ID: Worst-Case Groundwater
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 7.5E-06 3.4E-01 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 1.6E-06 8.2E-02 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Groundwater to Indoor Air
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 23081-19-060
Exposure Unit ID: Worst-Case Groundwater
CAS #Chemical Name:
Groundwater
Concentration
(ug/L)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-66-3 Chloroform 4.9 0.735200327 1.2E-01 2.0E+01 6.0E-06 7.2E-03
75-35-4 Dichloroethylene, 1,1-1.5 1.600572363 -4.2E+01 7.7E-03
79-01-6 Trichloroethylene 1.7 0.684587081 4.8E-01 4.2E-01 1.4E-06 3.3E-01
Cumulative:7.5E-06 3.4E-01
Groundwater concentrations are in ug/L. Air concentrations are in ug/m3.
Output Form 3A
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Groundwater to Indoor Air
Version Date: July 2020
Basis: May 2020 EPA RSL Table
Site ID: 23081-19-060
Exposure Unit ID: Worst-Case Groundwater
CAS #Chemical Name:
Groundwater
Concentration
(ug/L)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-66-3 Chloroform 4.9 0.735200327 5.3E-01 8.6E+01 1.4E-06 1.7E-03
75-35-4 Dichloroethylene, 1,1-1.5 1.600572363 -1.8E+02 1.8E-03
79-01-6 Trichloroethylene 1.7 0.684587081 3.0E+00 1.8E+00 2.3E-07 7.8E-02
Cumulative:1.6E-06 8.2E-02
Groundwater concentrations are in ug/L. Air concentrations are in ug/m3.
Output Form 3D
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator