13025_Davis Drive_Environmental Services During Building Slab Demolition_2011.01.27

January 27, 2011
Mr. Will Service
Toxicologist/Project Manager
North Carolina Department of Environmental Natural Resources (NCDENR)-
Brownfields Program
1601 Mail Service Center, Raleigh,
Raleigh, NC 27699

RE: Environmental Services during Building Slab Demolition
Former Hercules Incorporated Site
9 Davis Drive
Research Triangle Park (RTP), North Carolina
ECS Project Number 06.16997-B

Dear Mr. Service:

ECS Carolinas, LLP (ECS) appreciates the opportunity to submit the findings from services
provided at the referenced site. As outlined in the ECS Proposal 06:13856 for “Soil Screening
Services during Building Slab Demolition” which was performed in accordance with our signed
proposal dated July 21, 2010. In addition, ECS submitted a letter report to NCDENR on
December 2, 2010, outlining our proposed work plan. This report details our site observations,
site sketch, findings, conclusions and recommendations.

PROJECT UNDERSTANDING

The subject property is a 50.68-acre parcel identified by Parcel Identification Number (PIN) 0748-
03-21-3871, located at 9 Davis Drive, RTP, North Carolina. The subject property was previously
developed with a two-story, 150,000 square-foot brick building and associated asphalt parking
lot areas. Currently, the building has been demolished, the sub-slab and associated footings
have also been removed.

SITE OBSERVATIONS

ECS personnel started soil “screening” activities on-site, October 28, 2010 while Environmental
Holdings Group, Inc (EHG) conducted demolition activities of the existing concrete slab and
associated building footing foundations. ECS personnel screened exposed soils by collecting
random samples, placing them in clean plastic bags and after fifteen minutes, VOC vapor
concentrations were measured in the aliquot headspace using a photo-ionization detector (PID).
During soil screening activities, ECS personnel did not encounter elevated PID readings
throughout the building slab which exceeded 10 parts per million (ppm).

On November 9, 2010, EHG began excavation activities for removal of the building footings
located in the southeastern corner of the building. A chemical odor was encountered while
removing soils immediately adjacent to the concrete footings located at a depth of
approximately five (5) below ground surface (bgs). Excavation activities ceased as ECS
personnel began delineating the impacted area (See Figure 2A). Soils screened from the area
of interest (AOI) in the southeastern corner of the building exhibited PID readings ranging from
1.6 ppm to 548 ppm at ECS screening locations (ECS-1 through ECS-12).
Former Hercules Incorporated Site- 9 Davis Drive
Research Triangle Park (RTP), North Carolina
ECS Project No. 06.16997-B
January 27, 2011

The soils collected from locations ECS-3, ECS-4 and ECS-9 which exhibited the highest PID
values, were transferred into laboratory-provided containers, labeled, and placed on ice and
submitted for laboratory analysis by EPA Method 8260 for volitale organic compounds (VOCs)
by a North Carolina-certified laboratory (SGS Environmental Services, (SGS)). The laboratory
analytical results are attached.

Summary of Soil Analytical Results
Sample ID

PID Readings (ppm)
EPA Analytical Methods Analytical Results (mg/kg)
NC Action Level (mg/kg)
ECS-3 548 sec-Butylbenzene, 3.72 3.3
ECS-4 42.1 sec-Butylbenzene, 0.49 3.3
ECS-9 202

VOCs

sec-Butylbenzene, 35.8
4-Methyl-2-pentanone, 6.20
3.3
3.6
Notes: mg/kg = micrograms per kilogram = parts per million (ppm)
*The above are the North Carolina, Division of Waste Management, Hazardous Waste Section
(NCDENR-DWM) Soil Screening Levels.

To define the extent of potentially impacted soils, ECS conducted screening activities along the
building footings and down-gradient, to the south of the impacted area. ECS observed the
excavation of three (3) tests pits, two of which were located east of the AOI outside the building
footprint, and one test pit was located west of AOI, inside the building footprint. The purpose of
the test pits was to determine if elevated soils were located beyond the limits of the current
excavation pit. Soils screened that were located in these three test pits at approximately 4 feet
bgs did not exhibit elevated PID readings (See Figure 2B).

Based upon our excavations and screening, it appeared that the impacted area is restricted to
the immediate area south of the former tower location. A concentrated area (point source) of
impact was identified along the south wall of the tower extension as indicated as “Former
Source Area” on Figure 2A. It appears that impact may have migrated along the footings with
slightly elevated impact dispersing through the Area of Concern. It was estimated that
approximately 4,000 to 4,500 tons of impacted material may require removal and disposal. The
soils in this area consisted of heavy plastic clays that are not conducive to fluid migration.

FINDINGS
On November 15th, a field meeting was held on-site with representatives from ECS, EHG and
Syngenta to determine a course of action in accordance to recommendations provided from Mr.
Will Service, representative of NCDENR, for impacted soils encountered in the southeastern
corner of the building footprint.

As a result of that field meeting, disturbed soils that were excavated and potentially
contaminated could not be reused on-site. ECS measured off an approximate 80 foot wide x
150 foot long area starting from the southeastern building corner. The soils encountered in this
area, to a depth of approximately 5 feet, were scheduled to be excavated and stockpiled on-site,
on the existing building sub-slab to minimize cross-contamination with clean soils. These stock-
piled soils were covered each evening to minimize potential surface runoff. As per NCDENR
Former Hercules Incorporated Site- 9 Davis Drive
Research Triangle Park (RTP), North Carolina
ECS Project No. 06.16997-B
January 27, 2011

requirements, the contaminated, stock-piled soils were transported to Soilworks, Inc located at
7534 Highway 42 East, Selma, NC.

During excavation activities on-site, ECS maintained continuous air monitoring of the soil
removal process. All on-site workers were required to use appropriate personal protection
equipment (PPE). Soils located in the northwestern corner of the building footprint which
exhibited previous non-elevated PID readings were selected for “clean-fill” replacement near the
SW building corner.

On November 23, EHG resumed excavation activities and stock-piling of impacted soils. Under
NCDENR Permit # SRU600075, EHG transported approximately 4,668 tons of impacted soil
from the site to Soilworks, Inc, from December 2 to December 11.

On December 7, ECS personnel collected several soil samples from the former source area
along the previous building footprint. Three (3) representative soil samples were collected from
the excavation floor, which were identified as S24, S25 and S26, respectively. Those soil
samples are representative of residual soils that remain after impact removal. The purpose of
the linear sampling methodology was to screen, collect and analyze soil samples located along
the former building footprint and from the former source area. These soil samples were selected
for laboratory analysis by EPA Method 8260 for VOCs. The laboratory analytical results are
attached with a summary in the table below.

Summary of Soil Analytical Results
Sample ID

PID Readings (ppm)
EPA Analytical Methods Analytical Results (mg/kg)
NC Action Level (mg/kg)
S-24 2.4 BQL -
S-25 22.2 BQL -
S-26 1.6

VOCs

BQL -
Notes: mg/kg = micrograms per kilogram = parts per million (ppm)
*The above are the North Carolina, Division of Waste Management, Hazardous Waste Section
(NCDENR-DWM) Soil Screening Levels.
* BQL- Below quantification limits

In addition to the confirmation samples on residual soils, NCDENR requested sampling
excavation backfill to confirm that “clean” backfill was utilized in the excavation area. On
December 21, EHG was completing final grading activities at the site. With the use of on-site
construction equipment, ECS personnel collected representative soil samples from four (4)
separate test pits installed along the previous building footprint and former source area at
approximately one (1) foot and six (6) bgs, labeled as B1, B2, B3 and B4. These soil samples
are representative of backfill placed after impacted soil removal. Samples were taken along the
former footing line, which was generally the centerline of the excavation. These soil samples
were selected for laboratory analysis by EPA Method 8260 for VOCs. The laboratory analytical
results are attached with a summary in the table below.

Former Hercules Incorporated Site- 9 Davis Drive
Research Triangle Park (RTP), North Carolina
ECS Project No. 06.16997-B
January 27, 2011

Summary of Soil Analytical Results
Sample ID
EPA Analytical Methods Analytical Results (mg/kg)
NC Action Level (mg/kg)
B1 BQL -
B2 BQL -
B3 BQL -
B4

VOCs

BQL -
Notes: mg/kg = micrograms per kilogram = parts per million (ppm)
*The above are the North Carolina, Division of Waste Management, Hazardous Waste Section
(NCDENR-DWM) Soil Screening Levels.
* BQL- Below quantification limits

CONCLUSIONS

Based on the findings presented in this report, it’s ECS opinion that the impacted soils
previously identified at sampling locations (ECS-3, ECS-4 and ECS-9) along the former building
footprint at the south end of the former tower were properly excavated, stock-piled, transported
and disposed of at Soilworks, Inc. Confirmatory samples taken after impact removal (S-24, S-
25 and S-26) showed no quantifiable impact of residual soils located at an approximate depth of
six (6) feet below ground surface (bgs). In addition, backfill soils utilized in this area (samples
B-1, B-2, B-3 and B-4) also indicated no quantifiable impact. It is ECS’ opinion that No Further
Action be required for this incident.

CLOSING

ECS appreciates the opportunity to work with Syngenta and NCDENR on this important project.
Please contact the undersigned with any additional questions.

Respectfully Submitted,
ECS Carolinas, LLP

Ryan Conchilla Aric V. Geda, P.E.
Environmental Project Manager Principal Engineer

Attachments: Figures, Laboratory Data Sheets, Chain of Custody Record, Soilworks, Inc.
Permit and Disposal Manifests.
SOURCE:
MapQuest
N
FIGURE 1
SITE LOCATION MAP
Former Hercules Incorporated Site
9 Davis Drive
Research Triangle Park (RTP), NC
ECS PROJECT NO. 16997-B
Approximate
Site Location
SOURCE:
Durham County on-line GIS
2005 Aerial Photograph
LEGEND
Site Boundary N
FIGURE 2
AERIAL SITE MAP
Former Hercules Incorporated Site
9 Davis Drive
Research Triangle Park (RTP), NC
ECS PROJECT NO. 16997-B
Approximate Location
of Subject Property
Interstate 40
Davis Drive
SOURCE:
Durham County on-line GIS
2005 Aerial Photograph
N
FIGURE 2A
(Zoomed) AERIAL SITE MAP
Former Hercules Incorporated Site
9 Davis Drive
Research Triangle Park (RTP), NC
ECS PROJECT NO. 16997-B
Approximate Location
of Subject Property
Area of Interest
Former Source Area
SOURCE:
Durham County on-line GIS
2005 Aerial Photograph
N
FIGURE 2B
(Zoomed) AERIAL SITE MAP
Former Hercules Incorporated Site
9 Davis Drive
Research Triangle Park (RTP), NC
ECS PROJECT NO. 16997-B
95’
Former Source Area
30’
B1
55’
100’80’
B 2
B3
B4
ECS-3 and S-24
ECS-9 and S-25
ECS-4 and S-26
LEGEND
ECS soil sampling locations on 11-09-2010 ECS test pit locations
ECS soil sampling locations on 11-23-2010 ECS excavation area-
ECS soil sampling locations on 12-21-2010 Total depth of 6ft bgs.
Excavation Area80’
150’
SOURCE:
United States Geological Survey 7.5-
Minute Series Topographic Map:
RTP, North Carolina,
Created 2002 DeLorme Maps
Contour = 5 feet
FIGURE 3
USGS TOPOGRAPHIC MAP
Former Hercules Incorporated Site
9 Davis Drive
Research Triangle Park (RTP), NC
ECS PROJECT NO. 16997-B
N
W
S
E Approximate Site Location
SITE
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Report Number:G161-2912
Client Project:
Dear Ryan Conchilla,
Enclosed are the results of the analytical services performed under the referenced project for the received
samples and associated QC as applicable. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be
retained in our files for a period of five years in the event they are required for future reference. Any samples
submitted to our laboratory will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or services performed during this project, please call Lori Lockamy at
[phone]. We will be happy to answer any questions or concerns which you may have.
Thank you for using SGS North America, Inc. for your analytical services. We look forward to working with you
again on any additional analytical needs.
Sincerely,
SGS North America, Inc.
__________________________________________________________________
Project Manager Date
Lori Lockamy
Ryan Conchilla
ECS
9001 Glenwood Ave
Raleigh, NC 27617
Syngenta-9 Davis Drive
Member of SGS
Group
SGS North America, Inc.5500 Business Drive, Wilmington, NC 28405
t 910.350.1903 f 910.350.1557 www.us.sgs.com
List of Reporting Abbreviations
and Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantitation Limit (RL or MDL)
DF = Dilution Factor
Dup = Duplicate
D = Detected, but RPD is > 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL/CL = Reporting Limit / Control Limit
RPD = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
MI34.021208.4
Client Sample ID: B1 @ 1'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-1A
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:00
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 78.0
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Acetone BQL MG/KG 1 27-Dec-10 23:150.0695
Benzene BQL MG/KG 1 27-Dec-10 23:150.00695
Bromobenzene BQL MG/KG 1 27-Dec-10 23:150.00695
Bromochloromethane BQL MG/KG 1 27-Dec-10 23:150.00695
Bromodichloromethane BQL MG/KG 1 27-Dec-10 23:150.00695
Bromoform BQL MG/KG 1 27-Dec-10 23:150.00695
Bromomethane BQL MG/KG 1 27-Dec-10 23:150.00695
2-Butanone BQL MG/KG 1 27-Dec-10 23:150.0348
n-Butylbenzene BQL MG/KG 1 27-Dec-10 23:150.00695
sec-Butylbenzene BQL MG/KG 1 27-Dec-10 23:150.00695
tert-Butylbenzene BQL MG/KG 1 27-Dec-10 23:150.00695
Carbon disulfide BQL MG/KG 1 27-Dec-10 23:150.00695
Carbon tetrachloride BQL MG/KG 1 27-Dec-10 23:150.00695
Chlorobenzene BQL MG/KG 1 27-Dec-10 23:150.00695
Chloroethane BQL MG/KG 1 27-Dec-10 23:150.00695
Chloroform BQL MG/KG 1 27-Dec-10 23:150.00695
Chloromethane BQL MG/KG 1 27-Dec-10 23:150.00695
2-Chlorotoluene BQL MG/KG 1 27-Dec-10 23:150.00695
4-Chlorotoluene BQL MG/KG 1 27-Dec-10 23:150.00695
Dibromochloromethane BQL MG/KG 1 27-Dec-10 23:150.00695
1,2-Dibromo-3-chloropropane BQL MG/KG 1 27-Dec-10 23:150.0348
Dibromomethane BQL MG/KG 1 27-Dec-10 23:150.00695
1,2-Dibromoethane (EDB)BQL MG/KG 1 27-Dec-10 23:150.00695
1,2-Dichlorobenzene BQL MG/KG 1 27-Dec-10 23:150.00695
1,3-Dichlorobenzene BQL MG/KG 1 27-Dec-10 23:150.00695
1,4-Dichlorobenzene BQL MG/KG 1 27-Dec-10 23:150.00695
trans-1,4-Dichloro-2-butene BQL MG/KG 1 27-Dec-10 23:150.0348
1,1-Dichloroethane BQL MG/KG 1 27-Dec-10 23:150.00695
1,1-Dichloroethene BQL MG/KG 1 27-Dec-10 23:150.00695
1,2-Dichloroethane BQL MG/KG 1 27-Dec-10 23:150.00695
cis-1,2-Dichloroethene BQL MG/KG 1 27-Dec-10 23:150.00695
trans-1,2-dichloroethene BQL MG/KG 1 27-Dec-10 23:150.00695
1,2-Dichloropropane BQL MG/KG 1 27-Dec-10 23:150.00695
1,3-Dichloropropane BQL MG/KG 1 27-Dec-10 23:150.00695
2,2-Dichloropropane BQL MG/KG 1 27-Dec-10 23:150.00695
1,1-Dichloropropene BQL MG/KG 1 27-Dec-10 23:150.00695
cis-1,3-Dichloropropene BQL MG/KG 1 27-Dec-10 23:150.00695
trans-1,3-Dichloropropene BQL MG/KG 1 27-Dec-10 23:150.00695
Dichlorodifluoromethane BQL MG/KG 1 27-Dec-10 23:150.00695
Diisopropyl ether (DIPE)BQL MG/KG 1 27-Dec-10 23:150.00695
Ethylbenzene BQL MG/KG 1 27-Dec-10 23:150.00695
Hexachlorobutadiene BQL MG/KG 1 27-Dec-10 23:150.00695
2-Hexanone BQL MG/KG 1 27-Dec-10 23:150.0174
Iodomethane BQL MG/KG 1 27-Dec-10 23:150.00695
Isopropylbenzene BQL MG/KG 1 27-Dec-10 23:150.00695
4-Isopropyltoluene BQL MG/KG 1 27-Dec-10 23:150.00695
Client Sample ID: B1 @ 1'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-1A
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:00
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 78.0
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Methylene chloride BQL MG/KG 1 27-Dec-10 23:150.0278
4-Methyl-2-pentanone BQL MG/KG 1 27-Dec-10 23:150.0174
Methyl-tert-butyl ether (MTBE)BQL MG/KG 1 27-Dec-10 23:150.00695
Naphthalene BQL MG/KG 1 27-Dec-10 23:150.00695
n-Propyl benzene BQL MG/KG 1 27-Dec-10 23:150.00695
Styrene BQL MG/KG 1 27-Dec-10 23:150.00695
1,1,1,2-Tetrachloroethane BQL MG/KG 1 27-Dec-10 23:150.00695
1,1,2,2-Tetrachloroethane BQL MG/KG 1 27-Dec-10 23:150.00695
Tetrachloroethene BQL MG/KG 1 27-Dec-10 23:150.00695
Toluene BQL MG/KG 1 27-Dec-10 23:150.00695
1,2,3-Trichlorobenzene BQL MG/KG 1 27-Dec-10 23:150.00695
1,2,4-Trichlorobenzene BQL MG/KG 1 27-Dec-10 23:150.00695
Trichloroethene BQL MG/KG 1 27-Dec-10 23:150.00695
1,1,1-Trichloroethane BQL MG/KG 1 27-Dec-10 23:150.00695
1,1,2-Trichloroethane BQL MG/KG 1 27-Dec-10 23:150.00695
Trichlorofluoromethane BQL MG/KG 1 27-Dec-10 23:150.00695
1,2,3-Trichloropropane BQL MG/KG 1 27-Dec-10 23:150.00695
1,2,4-Trimethylbenzene BQL MG/KG 1 27-Dec-10 23:150.00695
1,3,5-Trimethylbenzene BQL MG/KG 1 27-Dec-10 23:150.00695
Vinyl chloride BQL MG/KG 1 27-Dec-10 23:150.00695
m-,p-Xylene BQL MG/KG 1 27-Dec-10 23:150.0139
o-Xylene BQL MG/KG 1 27-Dec-10 23:150.00695
Surrogates
1,2-Dichloroethane-d4 133 %1 27-Dec-10 23:1555-173
Toluene-d8 93 %1 27-Dec-10 23:1557-134
4-Bromofluorobenzene 98 %1 27-Dec-10 23:1523-141
Batch Information
Analytical Batch: 9122710
Analytical Method: 8260SOLO
Instrument: MSD9
Analyst: DVO
Prep Batch:
Prep Method:
Prep Date/Time:
Initial Prep Wt./Vol.: 4.610000134
Prep Extract Vol: 5
Client Sample ID: B1 @ 6'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-2A
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:05
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 85.4
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Acetone BQL MG/KG 1 27-Dec-10 23:440.0574
Benzene BQL MG/KG 1 27-Dec-10 23:440.00574
Bromobenzene BQL MG/KG 1 27-Dec-10 23:440.00574
Bromochloromethane BQL MG/KG 1 27-Dec-10 23:440.00574
Bromodichloromethane BQL MG/KG 1 27-Dec-10 23:440.00574
Bromoform BQL MG/KG 1 27-Dec-10 23:440.00574
Bromomethane BQL MG/KG 1 27-Dec-10 23:440.00574
2-Butanone BQL MG/KG 1 27-Dec-10 23:440.0287
n-Butylbenzene BQL MG/KG 1 27-Dec-10 23:440.00574
sec-Butylbenzene BQL MG/KG 1 27-Dec-10 23:440.00574
tert-Butylbenzene BQL MG/KG 1 27-Dec-10 23:440.00574
Carbon disulfide BQL MG/KG 1 27-Dec-10 23:440.00574
Carbon tetrachloride BQL MG/KG 1 27-Dec-10 23:440.00574
Chlorobenzene BQL MG/KG 1 27-Dec-10 23:440.00574
Chloroethane BQL MG/KG 1 27-Dec-10 23:440.00574
Chloroform BQL MG/KG 1 27-Dec-10 23:440.00574
Chloromethane BQL MG/KG 1 27-Dec-10 23:440.00574
2-Chlorotoluene BQL MG/KG 1 27-Dec-10 23:440.00574
4-Chlorotoluene BQL MG/KG 1 27-Dec-10 23:440.00574
Dibromochloromethane BQL MG/KG 1 27-Dec-10 23:440.00574
1,2-Dibromo-3-chloropropane BQL MG/KG 1 27-Dec-10 23:440.0287
Dibromomethane BQL MG/KG 1 27-Dec-10 23:440.00574
1,2-Dibromoethane (EDB)BQL MG/KG 1 27-Dec-10 23:440.00574
1,2-Dichlorobenzene BQL MG/KG 1 27-Dec-10 23:440.00574
1,3-Dichlorobenzene BQL MG/KG 1 27-Dec-10 23:440.00574
1,4-Dichlorobenzene BQL MG/KG 1 27-Dec-10 23:440.00574
trans-1,4-Dichloro-2-butene BQL MG/KG 1 27-Dec-10 23:440.0287
1,1-Dichloroethane BQL MG/KG 1 27-Dec-10 23:440.00574
1,1-Dichloroethene BQL MG/KG 1 27-Dec-10 23:440.00574
1,2-Dichloroethane BQL MG/KG 1 27-Dec-10 23:440.00574
cis-1,2-Dichloroethene BQL MG/KG 1 27-Dec-10 23:440.00574
trans-1,2-dichloroethene BQL MG/KG 1 27-Dec-10 23:440.00574
1,2-Dichloropropane BQL MG/KG 1 27-Dec-10 23:440.00574
1,3-Dichloropropane BQL MG/KG 1 27-Dec-10 23:440.00574
2,2-Dichloropropane BQL MG/KG 1 27-Dec-10 23:440.00574
1,1-Dichloropropene BQL MG/KG 1 27-Dec-10 23:440.00574
cis-1,3-Dichloropropene BQL MG/KG 1 27-Dec-10 23:440.00574
trans-1,3-Dichloropropene BQL MG/KG 1 27-Dec-10 23:440.00574
Dichlorodifluoromethane BQL MG/KG 1 27-Dec-10 23:440.00574
Diisopropyl ether (DIPE)BQL MG/KG 1 27-Dec-10 23:440.00574
Ethylbenzene BQL MG/KG 1 27-Dec-10 23:440.00574
Hexachlorobutadiene BQL MG/KG 1 27-Dec-10 23:440.00574
2-Hexanone BQL MG/KG 1 27-Dec-10 23:440.0143
Iodomethane BQL MG/KG 1 27-Dec-10 23:440.00574
Isopropylbenzene BQL MG/KG 1 27-Dec-10 23:440.00574
4-Isopropyltoluene BQL MG/KG 1 27-Dec-10 23:440.00574
Client Sample ID: B1 @ 6'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-2A
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:05
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 85.4
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Methylene chloride BQL MG/KG 1 27-Dec-10 23:440.0230
4-Methyl-2-pentanone BQL MG/KG 1 27-Dec-10 23:440.0143
Methyl-tert-butyl ether (MTBE)BQL MG/KG 1 27-Dec-10 23:440.00574
Naphthalene BQL MG/KG 1 27-Dec-10 23:440.00574
n-Propyl benzene BQL MG/KG 1 27-Dec-10 23:440.00574
Styrene BQL MG/KG 1 27-Dec-10 23:440.00574
1,1,1,2-Tetrachloroethane BQL MG/KG 1 27-Dec-10 23:440.00574
1,1,2,2-Tetrachloroethane BQL MG/KG 1 27-Dec-10 23:440.00574
Tetrachloroethene BQL MG/KG 1 27-Dec-10 23:440.00574
Toluene BQL MG/KG 1 27-Dec-10 23:440.00574
1,2,3-Trichlorobenzene BQL MG/KG 1 27-Dec-10 23:440.00574
1,2,4-Trichlorobenzene BQL MG/KG 1 27-Dec-10 23:440.00574
Trichloroethene BQL MG/KG 1 27-Dec-10 23:440.00574
1,1,1-Trichloroethane BQL MG/KG 1 27-Dec-10 23:440.00574
1,1,2-Trichloroethane BQL MG/KG 1 27-Dec-10 23:440.00574
Trichlorofluoromethane BQL MG/KG 1 27-Dec-10 23:440.00574
1,2,3-Trichloropropane BQL MG/KG 1 27-Dec-10 23:440.00574
1,2,4-Trimethylbenzene BQL MG/KG 1 27-Dec-10 23:440.00574
1,3,5-Trimethylbenzene BQL MG/KG 1 27-Dec-10 23:440.00574
Vinyl chloride BQL MG/KG 1 27-Dec-10 23:440.00574
m-,p-Xylene BQL MG/KG 1 27-Dec-10 23:440.0115
o-Xylene BQL MG/KG 1 27-Dec-10 23:440.00574
Surrogates
1,2-Dichloroethane-d4 127 %1 27-Dec-10 23:4455-173
Toluene-d8 96 %1 27-Dec-10 23:4457-134
4-Bromofluorobenzene 99 %1 27-Dec-10 23:4423-141
Batch Information
Analytical Batch: 9122710
Analytical Method: 8260SOLO
Instrument: MSD9
Analyst: DVO
Prep Batch:
Prep Method:
Prep Date/Time:
Initial Prep Wt./Vol.: 5.099999905
Prep Extract Vol: 5
Client Sample ID: B2 @ 1'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-3C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:15
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 77.1
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Acetone BQL MG/KG 1 28-Dec-10 15:070.0562
Benzene BQL MG/KG 1 28-Dec-10 15:070.00562
Bromobenzene BQL MG/KG 1 28-Dec-10 15:070.00562
Bromochloromethane BQL MG/KG 1 28-Dec-10 15:070.00562
Bromodichloromethane BQL MG/KG 1 28-Dec-10 15:070.00562
Bromoform BQL MG/KG 1 28-Dec-10 15:070.00562
Bromomethane BQL MG/KG 1 28-Dec-10 15:070.00562
2-Butanone BQL MG/KG 1 28-Dec-10 15:070.0281
n-Butylbenzene BQL MG/KG 1 28-Dec-10 15:070.00562
sec-Butylbenzene BQL MG/KG 1 28-Dec-10 15:070.00562
tert-Butylbenzene BQL MG/KG 1 28-Dec-10 15:070.00562
Carbon disulfide BQL MG/KG 1 28-Dec-10 15:070.00562
Carbon tetrachloride BQL MG/KG 1 28-Dec-10 15:070.00562
Chlorobenzene BQL MG/KG 1 28-Dec-10 15:070.00562
Chloroethane BQL MG/KG 1 28-Dec-10 15:070.00562
Chloroform BQL MG/KG 1 28-Dec-10 15:070.00562
Chloromethane BQL MG/KG 1 28-Dec-10 15:070.00562
2-Chlorotoluene BQL MG/KG 1 28-Dec-10 15:070.00562
4-Chlorotoluene BQL MG/KG 1 28-Dec-10 15:070.00562
Dibromochloromethane BQL MG/KG 1 28-Dec-10 15:070.00562
1,2-Dibromo-3-chloropropane BQL MG/KG 1 28-Dec-10 15:070.0281
Dibromomethane BQL MG/KG 1 28-Dec-10 15:070.00562
1,2-Dibromoethane (EDB)BQL MG/KG 1 28-Dec-10 15:070.00562
1,2-Dichlorobenzene BQL MG/KG 1 28-Dec-10 15:070.00562
1,3-Dichlorobenzene BQL MG/KG 1 28-Dec-10 15:070.00562
1,4-Dichlorobenzene BQL MG/KG 1 28-Dec-10 15:070.00562
trans-1,4-Dichloro-2-butene BQL MG/KG 1 28-Dec-10 15:070.0281
1,1-Dichloroethane BQL MG/KG 1 28-Dec-10 15:070.00562
1,1-Dichloroethene BQL MG/KG 1 28-Dec-10 15:070.00562
1,2-Dichloroethane BQL MG/KG 1 28-Dec-10 15:070.00562
cis-1,2-Dichloroethene BQL MG/KG 1 28-Dec-10 15:070.00562
trans-1,2-dichloroethene BQL MG/KG 1 28-Dec-10 15:070.00562
1,2-Dichloropropane BQL MG/KG 1 28-Dec-10 15:070.00562
1,3-Dichloropropane BQL MG/KG 1 28-Dec-10 15:070.00562
2,2-Dichloropropane BQL MG/KG 1 28-Dec-10 15:070.00562
1,1-Dichloropropene BQL MG/KG 1 28-Dec-10 15:070.00562
cis-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 15:070.00562
trans-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 15:070.00562
Dichlorodifluoromethane BQL MG/KG 1 28-Dec-10 15:070.00562
Diisopropyl ether (DIPE)BQL MG/KG 1 28-Dec-10 15:070.00562
Ethylbenzene BQL MG/KG 1 28-Dec-10 15:070.00562
Hexachlorobutadiene BQL MG/KG 1 28-Dec-10 15:070.00562
2-Hexanone BQL MG/KG 1 28-Dec-10 15:070.0140
Iodomethane BQL MG/KG 1 28-Dec-10 15:070.00562
Isopropylbenzene BQL MG/KG 1 28-Dec-10 15:070.00562
4-Isopropyltoluene BQL MG/KG 1 28-Dec-10 15:070.00562
Client Sample ID: B2 @ 1'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-3C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:15
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 77.1
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Methylene chloride BQL MG/KG 1 28-Dec-10 15:070.0225
4-Methyl-2-pentanone BQL MG/KG 1 28-Dec-10 15:070.0140
Methyl-tert-butyl ether (MTBE)BQL MG/KG 1 28-Dec-10 15:070.00562
Naphthalene BQL MG/KG 1 28-Dec-10 15:070.00562
n-Propyl benzene BQL MG/KG 1 28-Dec-10 15:070.00562
Styrene BQL MG/KG 1 28-Dec-10 15:070.00562
1,1,1,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 15:070.00562
1,1,2,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 15:070.00562
Tetrachloroethene BQL MG/KG 1 28-Dec-10 15:070.00562
Toluene BQL MG/KG 1 28-Dec-10 15:070.00562
1,2,3-Trichlorobenzene BQL MG/KG 1 28-Dec-10 15:070.00562
1,2,4-Trichlorobenzene BQL MG/KG 1 28-Dec-10 15:070.00562
Trichloroethene BQL MG/KG 1 28-Dec-10 15:070.00562
1,1,1-Trichloroethane BQL MG/KG 1 28-Dec-10 15:070.00562
1,1,2-Trichloroethane BQL MG/KG 1 28-Dec-10 15:070.00562
Trichlorofluoromethane BQL MG/KG 1 28-Dec-10 15:070.00562
1,2,3-Trichloropropane BQL MG/KG 1 28-Dec-10 15:070.00562
1,2,4-Trimethylbenzene BQL MG/KG 1 28-Dec-10 15:070.00562
1,3,5-Trimethylbenzene BQL MG/KG 1 28-Dec-10 15:070.00562
Vinyl chloride BQL MG/KG 1 28-Dec-10 15:070.00562
m-,p-Xylene BQL MG/KG 1 28-Dec-10 15:070.0112
o-Xylene BQL MG/KG 1 28-Dec-10 15:070.00562
Surrogates
1,2-Dichloroethane-d4 126 %1 28-Dec-10 15:0755-173
Toluene-d8 99 %1 28-Dec-10 15:0757-134
4-Bromofluorobenzene 98 %1 28-Dec-10 15:0723-141
Batch Information
Analytical Batch: 9122810
Analytical Method: 8260SOLO
Instrument: MSD9
Analyst: DVO
Prep Batch:
Prep Method:
Prep Date/Time:
Initial Prep Wt./Vol.: 5.769999981
Prep Extract Vol: 5
Client Sample ID: B2 @ 6'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-4C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:20
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 76.5
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Acetone BQL MG/KG 1 28-Dec-10 15:360.0493
Benzene BQL MG/KG 1 28-Dec-10 15:360.00493
Bromobenzene BQL MG/KG 1 28-Dec-10 15:360.00493
Bromochloromethane BQL MG/KG 1 28-Dec-10 15:360.00493
Bromodichloromethane BQL MG/KG 1 28-Dec-10 15:360.00493
Bromoform BQL MG/KG 1 28-Dec-10 15:360.00493
Bromomethane BQL MG/KG 1 28-Dec-10 15:360.00493
2-Butanone BQL MG/KG 1 28-Dec-10 15:360.0247
n-Butylbenzene BQL MG/KG 1 28-Dec-10 15:360.00493
sec-Butylbenzene BQL MG/KG 1 28-Dec-10 15:360.00493
tert-Butylbenzene BQL MG/KG 1 28-Dec-10 15:360.00493
Carbon disulfide BQL MG/KG 1 28-Dec-10 15:360.00493
Carbon tetrachloride BQL MG/KG 1 28-Dec-10 15:360.00493
Chlorobenzene BQL MG/KG 1 28-Dec-10 15:360.00493
Chloroethane BQL MG/KG 1 28-Dec-10 15:360.00493
Chloroform BQL MG/KG 1 28-Dec-10 15:360.00493
Chloromethane BQL MG/KG 1 28-Dec-10 15:360.00493
2-Chlorotoluene BQL MG/KG 1 28-Dec-10 15:360.00493
4-Chlorotoluene BQL MG/KG 1 28-Dec-10 15:360.00493
Dibromochloromethane BQL MG/KG 1 28-Dec-10 15:360.00493
1,2-Dibromo-3-chloropropane BQL MG/KG 1 28-Dec-10 15:360.0247
Dibromomethane BQL MG/KG 1 28-Dec-10 15:360.00493
1,2-Dibromoethane (EDB)BQL MG/KG 1 28-Dec-10 15:360.00493
1,2-Dichlorobenzene BQL MG/KG 1 28-Dec-10 15:360.00493
1,3-Dichlorobenzene BQL MG/KG 1 28-Dec-10 15:360.00493
1,4-Dichlorobenzene BQL MG/KG 1 28-Dec-10 15:360.00493
trans-1,4-Dichloro-2-butene BQL MG/KG 1 28-Dec-10 15:360.0247
1,1-Dichloroethane BQL MG/KG 1 28-Dec-10 15:360.00493
1,1-Dichloroethene BQL MG/KG 1 28-Dec-10 15:360.00493
1,2-Dichloroethane BQL MG/KG 1 28-Dec-10 15:360.00493
cis-1,2-Dichloroethene BQL MG/KG 1 28-Dec-10 15:360.00493
trans-1,2-dichloroethene BQL MG/KG 1 28-Dec-10 15:360.00493
1,2-Dichloropropane BQL MG/KG 1 28-Dec-10 15:360.00493
1,3-Dichloropropane BQL MG/KG 1 28-Dec-10 15:360.00493
2,2-Dichloropropane BQL MG/KG 1 28-Dec-10 15:360.00493
1,1-Dichloropropene BQL MG/KG 1 28-Dec-10 15:360.00493
cis-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 15:360.00493
trans-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 15:360.00493
Dichlorodifluoromethane BQL MG/KG 1 28-Dec-10 15:360.00493
Diisopropyl ether (DIPE)BQL MG/KG 1 28-Dec-10 15:360.00493
Ethylbenzene BQL MG/KG 1 28-Dec-10 15:360.00493
Hexachlorobutadiene BQL MG/KG 1 28-Dec-10 15:360.00493
2-Hexanone BQL MG/KG 1 28-Dec-10 15:360.0123
Iodomethane BQL MG/KG 1 28-Dec-10 15:360.00493
Isopropylbenzene BQL MG/KG 1 28-Dec-10 15:360.00493
4-Isopropyltoluene BQL MG/KG 1 28-Dec-10 15:360.00493
Client Sample ID: B2 @ 6'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-4C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:20
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 76.5
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Methylene chloride BQL MG/KG 1 28-Dec-10 15:360.0197
4-Methyl-2-pentanone BQL MG/KG 1 28-Dec-10 15:360.0123
Methyl-tert-butyl ether (MTBE)BQL MG/KG 1 28-Dec-10 15:360.00493
Naphthalene BQL MG/KG 1 28-Dec-10 15:360.00493
n-Propyl benzene BQL MG/KG 1 28-Dec-10 15:360.00493
Styrene BQL MG/KG 1 28-Dec-10 15:360.00493
1,1,1,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 15:360.00493
1,1,2,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 15:360.00493
Tetrachloroethene BQL MG/KG 1 28-Dec-10 15:360.00493
Toluene BQL MG/KG 1 28-Dec-10 15:360.00493
1,2,3-Trichlorobenzene BQL MG/KG 1 28-Dec-10 15:360.00493
1,2,4-Trichlorobenzene BQL MG/KG 1 28-Dec-10 15:360.00493
Trichloroethene BQL MG/KG 1 28-Dec-10 15:360.00493
1,1,1-Trichloroethane BQL MG/KG 1 28-Dec-10 15:360.00493
1,1,2-Trichloroethane BQL MG/KG 1 28-Dec-10 15:360.00493
Trichlorofluoromethane BQL MG/KG 1 28-Dec-10 15:360.00493
1,2,3-Trichloropropane BQL MG/KG 1 28-Dec-10 15:360.00493
1,2,4-Trimethylbenzene BQL MG/KG 1 28-Dec-10 15:360.00493
1,3,5-Trimethylbenzene BQL MG/KG 1 28-Dec-10 15:360.00493
Vinyl chloride BQL MG/KG 1 28-Dec-10 15:360.00493
m-,p-Xylene BQL MG/KG 1 28-Dec-10 15:360.00986
o-Xylene BQL MG/KG 1 28-Dec-10 15:360.00493
Surrogates
1,2-Dichloroethane-d4 131 %1 28-Dec-10 15:3655-173
Toluene-d8 97 %1 28-Dec-10 15:3657-134
4-Bromofluorobenzene 100 %1 28-Dec-10 15:3623-141
Batch Information
Analytical Batch: 9122810
Analytical Method: 8260SOLO
Instrument: MSD9
Analyst: DVO
Prep Batch:
Prep Method:
Prep Date/Time:
Initial Prep Wt./Vol.: 6.630000114
Prep Extract Vol: 5
Client Sample ID: B3 @ 1'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-5C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:30
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 79.3
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Acetone BQL MG/KG 1 28-Dec-10 16:040.0529
Benzene BQL MG/KG 1 28-Dec-10 16:040.00529
Bromobenzene BQL MG/KG 1 28-Dec-10 16:040.00529
Bromochloromethane BQL MG/KG 1 28-Dec-10 16:040.00529
Bromodichloromethane BQL MG/KG 1 28-Dec-10 16:040.00529
Bromoform BQL MG/KG 1 28-Dec-10 16:040.00529
Bromomethane BQL MG/KG 1 28-Dec-10 16:040.00529
2-Butanone BQL MG/KG 1 28-Dec-10 16:040.0264
n-Butylbenzene BQL MG/KG 1 28-Dec-10 16:040.00529
sec-Butylbenzene BQL MG/KG 1 28-Dec-10 16:040.00529
tert-Butylbenzene BQL MG/KG 1 28-Dec-10 16:040.00529
Carbon disulfide BQL MG/KG 1 28-Dec-10 16:040.00529
Carbon tetrachloride BQL MG/KG 1 28-Dec-10 16:040.00529
Chlorobenzene BQL MG/KG 1 28-Dec-10 16:040.00529
Chloroethane BQL MG/KG 1 28-Dec-10 16:040.00529
Chloroform BQL MG/KG 1 28-Dec-10 16:040.00529
Chloromethane BQL MG/KG 1 28-Dec-10 16:040.00529
2-Chlorotoluene BQL MG/KG 1 28-Dec-10 16:040.00529
4-Chlorotoluene BQL MG/KG 1 28-Dec-10 16:040.00529
Dibromochloromethane BQL MG/KG 1 28-Dec-10 16:040.00529
1,2-Dibromo-3-chloropropane BQL MG/KG 1 28-Dec-10 16:040.0264
Dibromomethane BQL MG/KG 1 28-Dec-10 16:040.00529
1,2-Dibromoethane (EDB)BQL MG/KG 1 28-Dec-10 16:040.00529
1,2-Dichlorobenzene BQL MG/KG 1 28-Dec-10 16:040.00529
1,3-Dichlorobenzene BQL MG/KG 1 28-Dec-10 16:040.00529
1,4-Dichlorobenzene BQL MG/KG 1 28-Dec-10 16:040.00529
trans-1,4-Dichloro-2-butene BQL MG/KG 1 28-Dec-10 16:040.0264
1,1-Dichloroethane BQL MG/KG 1 28-Dec-10 16:040.00529
1,1-Dichloroethene BQL MG/KG 1 28-Dec-10 16:040.00529
1,2-Dichloroethane BQL MG/KG 1 28-Dec-10 16:040.00529
cis-1,2-Dichloroethene BQL MG/KG 1 28-Dec-10 16:040.00529
trans-1,2-dichloroethene BQL MG/KG 1 28-Dec-10 16:040.00529
1,2-Dichloropropane BQL MG/KG 1 28-Dec-10 16:040.00529
1,3-Dichloropropane BQL MG/KG 1 28-Dec-10 16:040.00529
2,2-Dichloropropane BQL MG/KG 1 28-Dec-10 16:040.00529
1,1-Dichloropropene BQL MG/KG 1 28-Dec-10 16:040.00529
cis-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 16:040.00529
trans-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 16:040.00529
Dichlorodifluoromethane BQL MG/KG 1 28-Dec-10 16:040.00529
Diisopropyl ether (DIPE)BQL MG/KG 1 28-Dec-10 16:040.00529
Ethylbenzene BQL MG/KG 1 28-Dec-10 16:040.00529
Hexachlorobutadiene BQL MG/KG 1 28-Dec-10 16:040.00529
2-Hexanone BQL MG/KG 1 28-Dec-10 16:040.0132
Iodomethane BQL MG/KG 1 28-Dec-10 16:040.00529
Isopropylbenzene BQL MG/KG 1 28-Dec-10 16:040.00529
4-Isopropyltoluene BQL MG/KG 1 28-Dec-10 16:040.00529
Client Sample ID: B3 @ 1'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-5C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:30
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 79.3
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Methylene chloride BQL MG/KG 1 28-Dec-10 16:040.0212
4-Methyl-2-pentanone BQL MG/KG 1 28-Dec-10 16:040.0132
Methyl-tert-butyl ether (MTBE)BQL MG/KG 1 28-Dec-10 16:040.00529
Naphthalene BQL MG/KG 1 28-Dec-10 16:040.00529
n-Propyl benzene BQL MG/KG 1 28-Dec-10 16:040.00529
Styrene BQL MG/KG 1 28-Dec-10 16:040.00529
1,1,1,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 16:040.00529
1,1,2,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 16:040.00529
Tetrachloroethene BQL MG/KG 1 28-Dec-10 16:040.00529
Toluene BQL MG/KG 1 28-Dec-10 16:040.00529
1,2,3-Trichlorobenzene BQL MG/KG 1 28-Dec-10 16:040.00529
1,2,4-Trichlorobenzene BQL MG/KG 1 28-Dec-10 16:040.00529
Trichloroethene BQL MG/KG 1 28-Dec-10 16:040.00529
1,1,1-Trichloroethane BQL MG/KG 1 28-Dec-10 16:040.00529
1,1,2-Trichloroethane BQL MG/KG 1 28-Dec-10 16:040.00529
Trichlorofluoromethane BQL MG/KG 1 28-Dec-10 16:040.00529
1,2,3-Trichloropropane BQL MG/KG 1 28-Dec-10 16:040.00529
1,2,4-Trimethylbenzene BQL MG/KG 1 28-Dec-10 16:040.00529
1,3,5-Trimethylbenzene BQL MG/KG 1 28-Dec-10 16:040.00529
Vinyl chloride BQL MG/KG 1 28-Dec-10 16:040.00529
m-,p-Xylene BQL MG/KG 1 28-Dec-10 16:040.0106
o-Xylene BQL MG/KG 1 28-Dec-10 16:040.00529
Surrogates
1,2-Dichloroethane-d4 131 %1 28-Dec-10 16:0455-173
Toluene-d8 97 %1 28-Dec-10 16:0457-134
4-Bromofluorobenzene 97 %1 28-Dec-10 16:0423-141
Batch Information
Analytical Batch: 9122810
Analytical Method: 8260SOLO
Instrument: MSD9
Analyst: DVO
Prep Batch:
Prep Method:
Prep Date/Time:
Initial Prep Wt./Vol.: 5.960000038
Prep Extract Vol: 5
Client Sample ID: B3 @ 6'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-6C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:40
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 82.3
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Acetone BQL MG/KG 1 28-Dec-10 16:330.0695
Benzene BQL MG/KG 1 28-Dec-10 16:330.00695
Bromobenzene BQL MG/KG 1 28-Dec-10 16:330.00695
Bromochloromethane BQL MG/KG 1 28-Dec-10 16:330.00695
Bromodichloromethane BQL MG/KG 1 28-Dec-10 16:330.00695
Bromoform BQL MG/KG 1 28-Dec-10 16:330.00695
Bromomethane BQL MG/KG 1 28-Dec-10 16:330.00695
2-Butanone BQL MG/KG 1 28-Dec-10 16:330.0348
n-Butylbenzene BQL MG/KG 1 28-Dec-10 16:330.00695
sec-Butylbenzene BQL MG/KG 1 28-Dec-10 16:330.00695
tert-Butylbenzene BQL MG/KG 1 28-Dec-10 16:330.00695
Carbon disulfide BQL MG/KG 1 28-Dec-10 16:330.00695
Carbon tetrachloride BQL MG/KG 1 28-Dec-10 16:330.00695
Chlorobenzene BQL MG/KG 1 28-Dec-10 16:330.00695
Chloroethane BQL MG/KG 1 28-Dec-10 16:330.00695
Chloroform BQL MG/KG 1 28-Dec-10 16:330.00695
Chloromethane BQL MG/KG 1 28-Dec-10 16:330.00695
2-Chlorotoluene BQL MG/KG 1 28-Dec-10 16:330.00695
4-Chlorotoluene BQL MG/KG 1 28-Dec-10 16:330.00695
Dibromochloromethane BQL MG/KG 1 28-Dec-10 16:330.00695
1,2-Dibromo-3-chloropropane BQL MG/KG 1 28-Dec-10 16:330.0348
Dibromomethane BQL MG/KG 1 28-Dec-10 16:330.00695
1,2-Dibromoethane (EDB)BQL MG/KG 1 28-Dec-10 16:330.00695
1,2-Dichlorobenzene BQL MG/KG 1 28-Dec-10 16:330.00695
1,3-Dichlorobenzene BQL MG/KG 1 28-Dec-10 16:330.00695
1,4-Dichlorobenzene BQL MG/KG 1 28-Dec-10 16:330.00695
trans-1,4-Dichloro-2-butene BQL MG/KG 1 28-Dec-10 16:330.0348
1,1-Dichloroethane BQL MG/KG 1 28-Dec-10 16:330.00695
1,1-Dichloroethene BQL MG/KG 1 28-Dec-10 16:330.00695
1,2-Dichloroethane BQL MG/KG 1 28-Dec-10 16:330.00695
cis-1,2-Dichloroethene BQL MG/KG 1 28-Dec-10 16:330.00695
trans-1,2-dichloroethene BQL MG/KG 1 28-Dec-10 16:330.00695
1,2-Dichloropropane BQL MG/KG 1 28-Dec-10 16:330.00695
1,3-Dichloropropane BQL MG/KG 1 28-Dec-10 16:330.00695
2,2-Dichloropropane BQL MG/KG 1 28-Dec-10 16:330.00695
1,1-Dichloropropene BQL MG/KG 1 28-Dec-10 16:330.00695
cis-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 16:330.00695
trans-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 16:330.00695
Dichlorodifluoromethane BQL MG/KG 1 28-Dec-10 16:330.00695
Diisopropyl ether (DIPE)BQL MG/KG 1 28-Dec-10 16:330.00695
Ethylbenzene BQL MG/KG 1 28-Dec-10 16:330.00695
Hexachlorobutadiene BQL MG/KG 1 28-Dec-10 16:330.00695
2-Hexanone BQL MG/KG 1 28-Dec-10 16:330.0174
Iodomethane BQL MG/KG 1 28-Dec-10 16:330.00695
Isopropylbenzene BQL MG/KG 1 28-Dec-10 16:330.00695
4-Isopropyltoluene BQL MG/KG 1 28-Dec-10 16:330.00695
Client Sample ID: B3 @ 6'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-6C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:40
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 82.3
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Methylene chloride BQL MG/KG 1 28-Dec-10 16:330.0278
4-Methyl-2-pentanone BQL MG/KG 1 28-Dec-10 16:330.0174
Methyl-tert-butyl ether (MTBE)BQL MG/KG 1 28-Dec-10 16:330.00695
Naphthalene BQL MG/KG 1 28-Dec-10 16:330.00695
n-Propyl benzene BQL MG/KG 1 28-Dec-10 16:330.00695
Styrene BQL MG/KG 1 28-Dec-10 16:330.00695
1,1,1,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 16:330.00695
1,1,2,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 16:330.00695
Tetrachloroethene BQL MG/KG 1 28-Dec-10 16:330.00695
Toluene BQL MG/KG 1 28-Dec-10 16:330.00695
1,2,3-Trichlorobenzene BQL MG/KG 1 28-Dec-10 16:330.00695
1,2,4-Trichlorobenzene BQL MG/KG 1 28-Dec-10 16:330.00695
Trichloroethene BQL MG/KG 1 28-Dec-10 16:330.00695
1,1,1-Trichloroethane BQL MG/KG 1 28-Dec-10 16:330.00695
1,1,2-Trichloroethane BQL MG/KG 1 28-Dec-10 16:330.00695
Trichlorofluoromethane BQL MG/KG 1 28-Dec-10 16:330.00695
1,2,3-Trichloropropane BQL MG/KG 1 28-Dec-10 16:330.00695
1,2,4-Trimethylbenzene BQL MG/KG 1 28-Dec-10 16:330.00695
1,3,5-Trimethylbenzene BQL MG/KG 1 28-Dec-10 16:330.00695
Vinyl chloride BQL MG/KG 1 28-Dec-10 16:330.00695
m-,p-Xylene BQL MG/KG 1 28-Dec-10 16:330.0139
o-Xylene BQL MG/KG 1 28-Dec-10 16:330.00695
Surrogates
1,2-Dichloroethane-d4 125 %1 28-Dec-10 16:3355-173
Toluene-d8 99 %1 28-Dec-10 16:3357-134
4-Bromofluorobenzene 101 %1 28-Dec-10 16:3323-141
Batch Information
Analytical Batch: 9122810
Analytical Method: 8260SOLO
Instrument: MSD9
Analyst: DVO
Prep Batch:
Prep Method:
Prep Date/Time:
Initial Prep Wt./Vol.: 4.369999886
Prep Extract Vol: 5
Client Sample ID: B4 @ 1'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-7C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:45
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 79.1
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Acetone BQL MG/KG 1 28-Dec-10 17:020.0573
Benzene BQL MG/KG 1 28-Dec-10 17:020.00573
Bromobenzene BQL MG/KG 1 28-Dec-10 17:020.00573
Bromochloromethane BQL MG/KG 1 28-Dec-10 17:020.00573
Bromodichloromethane BQL MG/KG 1 28-Dec-10 17:020.00573
Bromoform BQL MG/KG 1 28-Dec-10 17:020.00573
Bromomethane BQL MG/KG 1 28-Dec-10 17:020.00573
2-Butanone BQL MG/KG 1 28-Dec-10 17:020.0286
n-Butylbenzene BQL MG/KG 1 28-Dec-10 17:020.00573
sec-Butylbenzene BQL MG/KG 1 28-Dec-10 17:020.00573
tert-Butylbenzene BQL MG/KG 1 28-Dec-10 17:020.00573
Carbon disulfide BQL MG/KG 1 28-Dec-10 17:020.00573
Carbon tetrachloride BQL MG/KG 1 28-Dec-10 17:020.00573
Chlorobenzene BQL MG/KG 1 28-Dec-10 17:020.00573
Chloroethane BQL MG/KG 1 28-Dec-10 17:020.00573
Chloroform BQL MG/KG 1 28-Dec-10 17:020.00573
Chloromethane BQL MG/KG 1 28-Dec-10 17:020.00573
2-Chlorotoluene BQL MG/KG 1 28-Dec-10 17:020.00573
4-Chlorotoluene BQL MG/KG 1 28-Dec-10 17:020.00573
Dibromochloromethane BQL MG/KG 1 28-Dec-10 17:020.00573
1,2-Dibromo-3-chloropropane BQL MG/KG 1 28-Dec-10 17:020.0286
Dibromomethane BQL MG/KG 1 28-Dec-10 17:020.00573
1,2-Dibromoethane (EDB)BQL MG/KG 1 28-Dec-10 17:020.00573
1,2-Dichlorobenzene BQL MG/KG 1 28-Dec-10 17:020.00573
1,3-Dichlorobenzene BQL MG/KG 1 28-Dec-10 17:020.00573
1,4-Dichlorobenzene BQL MG/KG 1 28-Dec-10 17:020.00573
trans-1,4-Dichloro-2-butene BQL MG/KG 1 28-Dec-10 17:020.0286
1,1-Dichloroethane BQL MG/KG 1 28-Dec-10 17:020.00573
1,1-Dichloroethene BQL MG/KG 1 28-Dec-10 17:020.00573
1,2-Dichloroethane BQL MG/KG 1 28-Dec-10 17:020.00573
cis-1,2-Dichloroethene BQL MG/KG 1 28-Dec-10 17:020.00573
trans-1,2-dichloroethene BQL MG/KG 1 28-Dec-10 17:020.00573
1,2-Dichloropropane BQL MG/KG 1 28-Dec-10 17:020.00573
1,3-Dichloropropane BQL MG/KG 1 28-Dec-10 17:020.00573
2,2-Dichloropropane BQL MG/KG 1 28-Dec-10 17:020.00573
1,1-Dichloropropene BQL MG/KG 1 28-Dec-10 17:020.00573
cis-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 17:020.00573
trans-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 17:020.00573
Dichlorodifluoromethane BQL MG/KG 1 28-Dec-10 17:020.00573
Diisopropyl ether (DIPE)BQL MG/KG 1 28-Dec-10 17:020.00573
Ethylbenzene BQL MG/KG 1 28-Dec-10 17:020.00573
Hexachlorobutadiene BQL MG/KG 1 28-Dec-10 17:020.00573
2-Hexanone BQL MG/KG 1 28-Dec-10 17:020.0143
Iodomethane BQL MG/KG 1 28-Dec-10 17:020.00573
Isopropylbenzene BQL MG/KG 1 28-Dec-10 17:020.00573
4-Isopropyltoluene BQL MG/KG 1 28-Dec-10 17:020.00573
Client Sample ID: B4 @ 1'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-7C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:45
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 79.1
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Methylene chloride BQL MG/KG 1 28-Dec-10 17:020.0229
4-Methyl-2-pentanone BQL MG/KG 1 28-Dec-10 17:020.0143
Methyl-tert-butyl ether (MTBE)BQL MG/KG 1 28-Dec-10 17:020.00573
Naphthalene BQL MG/KG 1 28-Dec-10 17:020.00573
n-Propyl benzene BQL MG/KG 1 28-Dec-10 17:020.00573
Styrene BQL MG/KG 1 28-Dec-10 17:020.00573
1,1,1,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 17:020.00573
1,1,2,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 17:020.00573
Tetrachloroethene BQL MG/KG 1 28-Dec-10 17:020.00573
Toluene BQL MG/KG 1 28-Dec-10 17:020.00573
1,2,3-Trichlorobenzene BQL MG/KG 1 28-Dec-10 17:020.00573
1,2,4-Trichlorobenzene BQL MG/KG 1 28-Dec-10 17:020.00573
Trichloroethene BQL MG/KG 1 28-Dec-10 17:020.00573
1,1,1-Trichloroethane BQL MG/KG 1 28-Dec-10 17:020.00573
1,1,2-Trichloroethane BQL MG/KG 1 28-Dec-10 17:020.00573
Trichlorofluoromethane BQL MG/KG 1 28-Dec-10 17:020.00573
1,2,3-Trichloropropane BQL MG/KG 1 28-Dec-10 17:020.00573
1,2,4-Trimethylbenzene BQL MG/KG 1 28-Dec-10 17:020.00573
1,3,5-Trimethylbenzene BQL MG/KG 1 28-Dec-10 17:020.00573
Vinyl chloride BQL MG/KG 1 28-Dec-10 17:020.00573
m-,p-Xylene BQL MG/KG 1 28-Dec-10 17:020.0115
o-Xylene BQL MG/KG 1 28-Dec-10 17:020.00573
Surrogates
1,2-Dichloroethane-d4 128 %1 28-Dec-10 17:0255-173
Toluene-d8 98 %1 28-Dec-10 17:0257-134
4-Bromofluorobenzene 99 %1 28-Dec-10 17:0223-141
Batch Information
Analytical Batch: 9122810
Analytical Method: 8260SOLO
Instrument: MSD9
Analyst: DVO
Prep Batch:
Prep Method:
Prep Date/Time:
Initial Prep Wt./Vol.: 5.519999981
Prep Extract Vol: 5
Client Sample ID: B4 @ 6'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-8C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:50
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 79.3
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Acetone BQL MG/KG 1 28-Dec-10 17:300.0587
Benzene BQL MG/KG 1 28-Dec-10 17:300.00587
Bromobenzene BQL MG/KG 1 28-Dec-10 17:300.00587
Bromochloromethane BQL MG/KG 1 28-Dec-10 17:300.00587
Bromodichloromethane BQL MG/KG 1 28-Dec-10 17:300.00587
Bromoform BQL MG/KG 1 28-Dec-10 17:300.00587
Bromomethane BQL MG/KG 1 28-Dec-10 17:300.00587
2-Butanone BQL MG/KG 1 28-Dec-10 17:300.0294
n-Butylbenzene BQL MG/KG 1 28-Dec-10 17:300.00587
sec-Butylbenzene BQL MG/KG 1 28-Dec-10 17:300.00587
tert-Butylbenzene BQL MG/KG 1 28-Dec-10 17:300.00587
Carbon disulfide BQL MG/KG 1 28-Dec-10 17:300.00587
Carbon tetrachloride BQL MG/KG 1 28-Dec-10 17:300.00587
Chlorobenzene BQL MG/KG 1 28-Dec-10 17:300.00587
Chloroethane BQL MG/KG 1 28-Dec-10 17:300.00587
Chloroform BQL MG/KG 1 28-Dec-10 17:300.00587
Chloromethane BQL MG/KG 1 28-Dec-10 17:300.00587
2-Chlorotoluene BQL MG/KG 1 28-Dec-10 17:300.00587
4-Chlorotoluene BQL MG/KG 1 28-Dec-10 17:300.00587
Dibromochloromethane BQL MG/KG 1 28-Dec-10 17:300.00587
1,2-Dibromo-3-chloropropane BQL MG/KG 1 28-Dec-10 17:300.0294
Dibromomethane BQL MG/KG 1 28-Dec-10 17:300.00587
1,2-Dibromoethane (EDB)BQL MG/KG 1 28-Dec-10 17:300.00587
1,2-Dichlorobenzene BQL MG/KG 1 28-Dec-10 17:300.00587
1,3-Dichlorobenzene BQL MG/KG 1 28-Dec-10 17:300.00587
1,4-Dichlorobenzene BQL MG/KG 1 28-Dec-10 17:300.00587
trans-1,4-Dichloro-2-butene BQL MG/KG 1 28-Dec-10 17:300.0294
1,1-Dichloroethane BQL MG/KG 1 28-Dec-10 17:300.00587
1,1-Dichloroethene BQL MG/KG 1 28-Dec-10 17:300.00587
1,2-Dichloroethane BQL MG/KG 1 28-Dec-10 17:300.00587
cis-1,2-Dichloroethene BQL MG/KG 1 28-Dec-10 17:300.00587
trans-1,2-dichloroethene BQL MG/KG 1 28-Dec-10 17:300.00587
1,2-Dichloropropane BQL MG/KG 1 28-Dec-10 17:300.00587
1,3-Dichloropropane BQL MG/KG 1 28-Dec-10 17:300.00587
2,2-Dichloropropane BQL MG/KG 1 28-Dec-10 17:300.00587
1,1-Dichloropropene BQL MG/KG 1 28-Dec-10 17:300.00587
cis-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 17:300.00587
trans-1,3-Dichloropropene BQL MG/KG 1 28-Dec-10 17:300.00587
Dichlorodifluoromethane BQL MG/KG 1 28-Dec-10 17:300.00587
Diisopropyl ether (DIPE)BQL MG/KG 1 28-Dec-10 17:300.00587
Ethylbenzene BQL MG/KG 1 28-Dec-10 17:300.00587
Hexachlorobutadiene BQL MG/KG 1 28-Dec-10 17:300.00587
2-Hexanone BQL MG/KG 1 28-Dec-10 17:300.0147
Iodomethane BQL MG/KG 1 28-Dec-10 17:300.00587
Isopropylbenzene BQL MG/KG 1 28-Dec-10 17:300.00587
4-Isopropyltoluene BQL MG/KG 1 28-Dec-10 17:300.00587
Client Sample ID: B4 @ 6'
Client Project ID: Syngenta-9 Davis Drive
Lab Sample ID: G161-2912-8C
Lab Project ID: G161-2912
Collection Date: 21-Dec-10 11:50
Received Date: 22-Dec-10
Matrix: SOIL
Print Date: 12/30/2010
Solids: 79.3
Basis: Dry
Results by 8260SOLO
Parameter DFUnits Date AnalyzedResultRL/CL
Methylene chloride BQL MG/KG 1 28-Dec-10 17:300.0235
4-Methyl-2-pentanone BQL MG/KG 1 28-Dec-10 17:300.0147
Methyl-tert-butyl ether (MTBE)BQL MG/KG 1 28-Dec-10 17:300.00587
Naphthalene BQL MG/KG 1 28-Dec-10 17:300.00587
n-Propyl benzene BQL MG/KG 1 28-Dec-10 17:300.00587
Styrene BQL MG/KG 1 28-Dec-10 17:300.00587
1,1,1,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 17:300.00587
1,1,2,2-Tetrachloroethane BQL MG/KG 1 28-Dec-10 17:300.00587
Tetrachloroethene BQL MG/KG 1 28-Dec-10 17:300.00587
Toluene BQL MG/KG 1 28-Dec-10 17:300.00587
1,2,3-Trichlorobenzene BQL MG/KG 1 28-Dec-10 17:300.00587
1,2,4-Trichlorobenzene BQL MG/KG 1 28-Dec-10 17:300.00587
Trichloroethene BQL MG/KG 1 28-Dec-10 17:300.00587
1,1,1-Trichloroethane BQL MG/KG 1 28-Dec-10 17:300.00587
1,1,2-Trichloroethane BQL MG/KG 1 28-Dec-10 17:300.00587
Trichlorofluoromethane BQL MG/KG 1 28-Dec-10 17:300.00587
1,2,3-Trichloropropane BQL MG/KG 1 28-Dec-10 17:300.00587
1,2,4-Trimethylbenzene BQL MG/KG 1 28-Dec-10 17:300.00587
1,3,5-Trimethylbenzene BQL MG/KG 1 28-Dec-10 17:300.00587
Vinyl chloride BQL MG/KG 1 28-Dec-10 17:300.00587
m-,p-Xylene BQL MG/KG 1 28-Dec-10 17:300.0117
o-Xylene BQL MG/KG 1 28-Dec-10 17:300.00587
Surrogates
1,2-Dichloroethane-d4 132 %1 28-Dec-10 17:3055-173
Toluene-d8 97 %1 28-Dec-10 17:3057-134
4-Bromofluorobenzene 101 %1 28-Dec-10 17:3023-141
Batch Information
Analytical Batch: 9122810
Analytical Method: 8260SOLO
Instrument: MSD9
Analyst: DVO
Prep Batch:
Prep Method:
Prep Date/Time:
Initial Prep Wt./Vol.: 5.369999886
Prep Extract Vol: 5