23043_Rogers Oil_Assessment Rpt_20050708

ffl
OF NORTH CAROLORA, P.C.
July 8, 2005
2725 E. Millbrook Road, Suite 121
Raleigh, NC 27604
wwwatc-eiiviro.corr)
919.871,0999
Fax [phone]
Mr. Bob Davies
North Carolina Department of Environment and Natural Resources
Raleigh Reglional Office
Division of Waste Management - Underground Storage Tank Section
1628 Mail Service Center
Raleigh, North Carolina 27699-1628
RE: Assessment Report
Carolina Trailways
1201 South Blount Street
Raleigh, North Carolina
Facility ID No. 2758
NCDENR Incident No. 5051
ATC Project No. 73,75092.0011
Dear Mr. Davies:
ATC Associates of North Carolina, P.C. (ATC), on behalf of our client Greyhound Lilies,
Inc. (Greyhound), is submitting this assessment report for the referenced site. The report
presents the laboratory analytical results for the groundwater and soil sampling events.
If you have any questions or require additional information, please contact our off -ice at
[phone].
Sincerely,
I
<
Brian Bauer
Project Scientist
cc: Mr. James Cowles — ATC
Mr. Nic Howard -- GLI
Gabriel Araos, P.E.
Senior Project Manager

Assessment Report
Carolina Trailways
1201 South Blount Street
Raleigh, North Carolina
Facility ID No. 2758
NCDENR Incident No. 5051
July 8, 2005

Assessment Report
Carolina Trailways
1201 South Blount Street
Raleigh, North Carolina
Facility ID No. 0-015071
Facility ID No. 2758
NCDENR Incident No. 5051
ATC Project No. 73.75092.0011
Prepared By:
Brian Bauer
Project Scientist
Gabriel Araos, P.E.
Senior Project Manager
NC Professional Engineer #022569
SEAL
&
Submitted To:
State of North Carolina
Department of Environment and Natural Resources
Raleigh Regional Office
Division of Waste Management
Underground Storage Tank Section
1628 Mail Service Center
Raleigh, North Carolina 27699-1628
Greyhound Lines, Inc.
350 N. St. Pauls Street MS 0084
Dallas, Texas 75201
Submitted By:
ATC Associates of North Carolina, P.C.
2725 East Millbrook Road, Suite 121
Raleigh, North Carolina 27604
Phone: [phone]
Fax: [phone]
U11

3.0 ADDITIONAL ASSESSMENT .................................................................................2
3.1 Soil Sampling.........................................................................................................2
3.2 Soil Analytical Results...........................................................................................3
4.0 GROUNDWATER CHARACTERIZATION ..........................................................4
4.1 Groundwater Elevations.........................................................................................4
4.2 Groundwater Quality..............................................................................................5
5.0 SUMMARY .................................................................................................................6
Table 1
Soil Analytical Results
Table 2
Monitoring Well Construction Details
Table 3
Groundwater Elevation Data
Table 4
Groundwater Analytical Results
Figure I Site Topographic Map
Figure 2 Site Vicinity Map
Figure 3 Site Map
Figure 4 Chemicals of Concern in Soil
Figure 5 Groundwater Elevation Contour Map
Figure 6 Dissolved Benzene Isoconcentration Contour Map
Appendix A Soil Boring Logs
Appendix B Methods
Appendix C Laboratory Analytical Results

11
71 41
ATC Associates of North Carolina, P.C. (ATC), on behalf of Greyhound Lines Inc. (GLI),
is submitting this assessment report for the Carolina Trailways facility (Facility ID No.
2758) located at 1201 South Blount Street, Raleigh, Wake County, North Carolina
(Incident #5051). A site topographic map is presented as Figure 1, and a site vicinity map
is included as Figure 2. The scope of services included soil sampling, groundwater
sampling, laboratory testing, groundwater elevation monitoring, and report preparation.
The work was performed in response to the North Carolina Department of Environment and
Natural Resources (NCDENR) letter dated July 1, 2004, requesting groundwater sampling
and additional soil sampling in order to move the site towards closure.
Approximately 22 underground storage tanks (USTs) have been registered at the site and
have been removed or closed -in -place within the past ten years. The location and
presence of the two USTs (#21 and #22) is suspected at this time and could not be
confirmed. A site map included as Figure 3 shows the locations of the USTs. Three
separate releases have occurred at the site related to the former UST systems.
The first release occurred in June 1992 with an unknown quantity of fuel from the diesel
UST system (Tank # 1 A and #2A).
A Comprehensive Site Assessment Report (CSA) was submitted to NCDENR on May
23, 1994, by Precision Environmental Services (Precision), classifying the site as an
intermediate risk.
A second release occurred in September 1998 with an unknown quantity on fuel from the
same diesel UST system.
1

t
A CSA Addendum was submitted to NCDENR on July 2, 2001, by Green Star
Environmental (Greenstar). The CSA Addendum included additional information not
included in the original CSA submitted by Precision.
The third release occurred on October 15, 2001, at the bus wash bay, when approximately
I I I -gallons of diesel fuels was released and traveled into the oil/water separator in the
area of the release. Approximately 28-gallons of the diesel fuel was recovered.
Subsequently, free product was detected in monitoring well MW-9.
A second CSA Addendum was submitted to NCDENR on December 3, 20031) by
Greenstar.
On July 1, 2004, the NCDENR issued a letter requesting groundwater sampling and
additional soil assessment at the site in order to move the site towards closure. In 2004,
Greyhound retained ATC to provide environmental services. Eased on the July 1, 2004,
letter, review of previous site investigations, and conversations with Mr. Walter Plekan
(NCDENR Incident Manager), ATC has prepared this Assessment Report to address
groundwater and soil conditions at the site.
M
On February 7, 2005, ATC was on -site to oversee the advancement of ten geoprobe soil
borings (GP-1 through GP-10) at the facility. The location of the soil borings were
chosen in an effort to move toward site closure with regards to impacted soils at the
facility per the NCDENR letter dated July 1, 2004. GP-1 and GP-2 were advanced in the
vicinity of former geoprobe boring GP-6 where soil contamination was detected above
the residential and industrial/commercial soil -to -groundwater Maximum Soil
Contaminant Concentrations (MSCCs). GP-3 and GP-4 were advanced on the eastern
2

edge of suspected USTs #21 and #22. Blount Street precluded the advancement of
additional soil borings on the northern, southern, and western edges of suspected USTs
#21 and 422. GP-5 through GP-8 were advanced on the northern and southern edges of
UST #11. Blount Street precluded the advancement of additional soil borings on the
northern, southern, and western edges of UST # 11. Additionally, GP-9 and GP-10 were
advanced on the northern and southern edges of USTs # 16 and USTs # 17, respectively.
Soil boring locations are indicated on Figure 3.
Based on the soils encountered during the drilling operations for GP-1 through GP-10, the
on -site geology mainly consists of asphalt/concrete and gravel sub -base from the surface
to approximately 6 inches below grade. From 6 inches to approximately 15 feet below
land surface (bls), a gray to red sandy clay was encountered with boring locations
containing alternating layers of a micaceous clay. No bedrock was encountered during
the installation of the monitoring wells. Soil boring logs are included as Appendix A.
3.2 Soil Analytical
On February 7, 2005, ATC collected ten soil samples (GP-1 through GP-10). Sampling
activities were performed in accordance with the standard operating procedures presented
in Appendix B. Soil samples were obtained from various intervals and screened for
VOCs using an organic vapor analyzer (OVA). The OVA provides an approximation of
the presence of VOCs in the soil. Field screening results from GP -I, through GP-10 are
presented in Table 1. The soil sample exhibiting the highest total VOC reading, or in the
case of no OVA reading the sample directly above the water table, were submitted for
laboratory analysis. The soil samples were shipped to Southern Petroleum Laboratories
(SPL) in Scott, Louisiana for analysis for benzene, toluene, ethylbenzene, and xylenes
(BTEX) by EPA Method 8260, polyaromatic hydrocarbons (PAHs) by EPA Method
8270, and Massachusetts Department of Environmental Protection (MADEP) Method for
volatile petroleum hydrocarbons and extractable hydrocarbons (MADEP VPH, and
MADEP EPH).
3

According to the laboratory analytical report for the February 2005 sampling event, the
soil -to -groundwater MSCCs were exceeded for the following compounds:
• Ethylbenzene: GP-5 and GP-7;
• Total Xylenes: GP-5 and GP-7;
® Trichloroethene: GP-4;
• 1,1,2,2 Tetrachloroethane: GP-2;
• Naphthalene: GP-5 and GP-7;
® C5-C8 Aliphatics: GP-5 and GP-7; and
® C9-C l O Aromatics: GP-1, GP-2, GP-5, and GP-7.
MSCCs are referenced in the "Guidelines for Assessment and Corrective Action", April,
2001. The soil analytical results are summarized in Table 1. Figure 4 presents the soil
analytical results. Copies of the analytical reports are presented in Appendix C. The soil
analytical results did not exceed the residential or industrial/commercial MSCCs.
On January 4, 2005, ATC gauged monitoring wells MW-1, MW-2, MW-3, MW-4, MW-5,
MW-7, MW-8, MW-9, MW-10, MW-11, DW-1, and DW-2 for groundwater elevations.
An oil/water interface probe was used to measure the depth to water. Based on the gauging
event, groundwater depths in the shallow monitoring wells ranged from 13.42 to 16.78 feet
below land surface (bls). Monitoring wells MW-6 and MW-12 were not gauged due to
their location in the right-of-way of Blount Street.
Depth to water was measured from the top of each well casing and then converted into
relative elevations using previously established well elevations. The well casing elevations
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are referenced to an arbitrary on -site benchmark with an assigned datum of 100 feet. Well
construction details are summarized in Table 2. Groundwater elevations for the January
2005 gauging event are summarized in Table 3. A groundwater elevation contour map
based on the January 2005 gauging data is included as Figure S. Based on the water table
elevations, groundwater flow is generally towards the southwest.
4.2 Groundwater Quality
On January 4, 2005, ATC personnel collected groundwater samples from monitoring
wells MW-1, MW-2, MW-3, MW-4, MW-5, MW-7, MW-10, MW-11, DW-1, and DW-
2. Groundwater samples were not collected from MW-9 due to the presence of
approximately 1.93 feet of free product, MW-8 did not contain sufficient water, and MW-6
and MW-12 were located within the right-of-way of Blount Street. Prior to sampling, a
minimum of three well volumes of groundwater were removed from each well. A
dedicated, disposable, one -liter plastic bailer was used to collect each water sample. The
samples were then placed in appropriate containers, properly labeled, and preserved on ice.
The samples were transported under chain of custody to Southern Petroleum Laboratories
(SPL) in Scott, Louisiana for analysis by EPA Methods EPA Methods 601/602 including
benzene, toluene, ethylbenzene, and xylenes (BTEX), naphthalene, methyl tertiary butyl
ether (MTBE), isopropyl ether (IPE), and ethylene dibromide (EDB). Sampling and
analytical methods are included in Appendix B.
Based on the analytical results, the following chemicals of concern (COCs) exceeded the
NCDENR Groundwater Quality 2L Standards (2L Standards):
® Benzene: MW-3 and MW-4;
® Naphthalene: MW-1 and MW-3;
• Trichloroethene: MW-4, MW-5, MW-7, and MW-11; and
• Chloroform: MW-I, DW-1, and DW-2.
M

The groundwater analytical results are attached as Appendix C and summarized in Table 4.
Figure 6 presents the benzene isoconcentration contour map.
During this reporting period, ATC obtained ten soil borings (GP-1 through GP-10),
measured groundwater levels and collected groundwater samples from monitoring wells
MW-L MW-2, MW-3, MW-4, MW-5, MW-7, MW-10, MW-11, DW-1, and DW-2.
Based on field activities, observations, and soil and groundwater analytical results, ATC
concludes the following:
® The site appears to meet the criteria for intermediate risk classification because of
the presence of free product in monitoring well MW-9. Based on the intermediate
risk classification, the appropriate groundwater cleanup standards will be the 2L
Standards;
The land use classification for the site will likely be industrial/commercial since
the properties within 500 feet of the site are zoned for industrial and commercial
use. Based on land use classification, the appropriate soil cleanup standards will
likely be the soil -to -groundwater MSCCs;
0 The soil analytical results from the assessment activities indicated that COCs were
detected above the soil -to -groundwater MSCCs in GP -I, GP-2, GP-4, GP-5, and
GP-7;
0 Approximately 1.93 feet of free product was detected in monitoring well MW-9;
and
on

The groundwater analytical results indicated Benzene, naphthalene,
trichloroethene, and chloroform above the corresponding 2L Standards, but below
GCLs.
Based on the results of the assessment report soil and groundwater appears to be impacted
above the appropriate risk -based cleanup levels. At this time, ATC recommends free
product recovery in monitoring well MW-9. Once free product is abated, the site risk
may be lowered and site closure can be pursued.

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CAROLINA TRAILVATS
1201 SOUTH BLOUNT STREET
AALEIGH, NORTH CAROLINA
ATC PROJECT NO.
73.75092.0011
Welt
Total Well
Screen
0C
Monitoring
Construction
Diameter
Slot Size =
Depth
'Interval
Elevation
Well
Date
(inches)
(inches)
(feet)
(feet)
(feet)
Mw- 1
4/10/1990
4
0.10
20
10-20
100.79
MW-2
4/11/1990
4
0.10
20
10-20
97.82
MW-3
4//11/90
4
0.10
23
13-23
99.80
MW-4
2/25/1993
4
0.10
25
10-20
100.33
MW-5
2/25/1993
4
0.10
25
10-20
100.31
MW-6
"",3/4/1993
2
0.10
25
10-20
101.64
MW-7
11/22/1993
2
0.10
26
11-26
98.22
MW-8
3/23/1994
2
0.10
20
5-20
99.77
MW-9
3/23/1994
2
0.10
20
5-20
99.74
MW-10
3/24/1994
2-
0.10
20
5-20
100.67
Mw- 11
10/13/1994
2
0.10
19.5
9.4-19.5
99.21
MW-12
5/31/1995
2
0.10
19
9-19
97.1
DW- 1
3/24/1994
2
0.10
40
35-40
100.14
DW-2
3/24/1994
2
0.10
40
3540
100.54
Notes:
1. Elevations are measured using an arbitrary benchmark of 100.00.
2. TOC = Top of Casing.

fm
Monitoring
Well
TOC Elevation
(feet)
Depth to Product
( feet)
January 4, 2005
Depth To Groundwater
(feet)
Product Thickness
(feet)
Groundwater Elevation
(feet)
MW_ 1
100.79
NM
15.84
NA
84.95
MW-2
97.82
NM
13.42
NA
84.40
MW-3
99.80
NM
15.31
NA
84.49
MW-4
100.33
NM
15.75
NA
84.58
MW-5
100.31
NM
15.52
NA
84.79
MW-6
101.64,,,,
NM
NM
NA
NA
MW-7
98.22
NM
14.38
NA
83.84
MW-8
99.77
NM
NM
NA
NA
MW_9
99.74
14.85
16.78
1.93
84.50*
MW-10
100.67
NM
15.56
NA
85.11
MW-11
99.21
NM
14.92
NA
84.29
MW-12
97.10
NM
NM
NA
NA
DW- 1
100.14
NM
15.53
NA
84.61
DW-2
100.54
NM
15.45
NA
85.09
Notes:
1. TOC = Top of Casing.
2. Depth to groundwater measured from top of casing.
Elevations are measured using an arbitrary benchmark of 100.00,
4. NM = Not Measured.
NA = Not Applicable.
Monitoring well MW-6 and MW-12 are located in Blount St. and were not sampled.
Monitoring well MW-8 was dry.
* Groundwater elevation = TOC - [DTW-(0.80x(DTW-DTP))).

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aounoE: 1eaguuoonxLexa*WEST QUADRANGLE, NORTH oARouwx-WAKE COUNTY, 7.5 MINUTE SERIES TOPOGRAPHIC
MAP, SCALE 1:24,000.
2725EMiUbrookRoad, Ste 121
Raleigh, NC 27604
PROJECT NO: 73.75UA2.0011
NTS I DATE: 02/20051 REVIEWED BY: BB
CAR[>L|NATRA|LVVAY8
12O1S.BLC)UNTSTREET
RALBGH.NORTH CAROLiNA

EJPV.
i
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s 3 LEE ♦ ai 3 aJRw 'N r b". `Yda l,✓ �.�.4.
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t k
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9
ij rr r�11 k" nt
SAINTS
Notes: circle indicates 11000 foot radius.
SOURCE: WAKE COUNTY YAPS AT http://imaps.co.wake.nc.us/imaps/main
IC 2725 E. Millbrook Road, Ste 121 FIGURE 2
10, T—AT , - o Raleigh, NC 27604 SITE VICINITY MAP
A s S o A T E 3 IN C [phone] CAROLINA TRAILWAYS
PROJECT NO: 73.75092.0011 1201 S. BLOUNT STREET
RALEIGH, NORTH CAROLINA
SCALE:1" = 450' DATE: 02/2005 REVIEWED BY: BB

LEGEND:
i? MONITORING WELL (TYPE II)
MONITORING WELL (TYPE III)
GEOPROBE BORING LOCATION
f.--TANK #5
L_I
RESIDENCES
OFFICE BUILDING
GP-9
TANK #16
I 560-GALLON
' t REMOVED 12/199
I 1
t J
GP-10 TANK #17
300-GALLON
REMOVED 12/199
OVERHANG
OFFICE
OFFICE
SPACE
BUILDING
MW-6
co
TANK #14
4'0 GALLON DIESEL
Z_
GP-7 REMOVED 7/1992 GARAGE
+GP-5
TANK *11
8000-GALLON DIESEL
- - MW-5
L GP-8 I
REMOVED 7/1992Frnm
I
- �GP-6
TANK #15
1000-GALLON DIESEL
MW-4 DW-1 REMOVED 7/1992 � # - _ TANK 19 STORAGE I
1000-GALLON SHED
--I
TANK *12 REMOVED 7/1998
SUSPECTED
TANK *21
5OOO-GALLON
f -
4000-GALLON
P= _ , REMOVED 12/1992
L -
r -
J
,
I-- - J MW-7 TANK #8 TANK #9 4
I- - -,
SUSPECTED #
TANK 22
I_ _
I_ _ _ 1000-GALLON 1000-GALLON
J"�_TANK #13 REMOVED 7/1992 REMOVED 7/1992
8000-GALLON
MW-11
GP-4 4000-GALLON #
_I REMOVED 12/1992 MW-10 TANK 1 8
INSTALLED t989
TANK #6 I
i
I 560-GALLON II TANK #1
I t ---TANK #10 REMOVED 7/t992 TANK #2A
, _I CLOSED IN PLACE INSTALLED 1989
5000-GALLON 6/1988
REMOVED 12/1992 TANK #7 DW-2
OFFICE
I MIN -1 r l r I
560-GALLON , -' TANK #2
SPACE
REMOVED 7/1992
WASH = _ = J CLOSED IN PLACE I I I I
+'— BAY ' s/lsae I I I I
J TANK #3 II I
i LA CLOSED IN PLACE
I_
SANDERS FORD r -i ' _ _ J 4/1989
MW-12
BUILDING ' ' I - - - , TANK #4
'
TANK #20 —►I
i CLOSED IN PLACE
10O0-GALLON I_ J - - -
MW-8 4/1989
GP -1
x--x-x-x-x- -=--*-k-x-x-#-
�GP-2
MW-9
BRANCH STREET
MW-2
MW-3
VACANT
LOT
CONVENIENCE
STORE
C
I`
O
CO
o O
z
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rn
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F- N
0-)
o O
N
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LEGEND:
MONITORING WELL (TYPE II)
MONITORING WELL (TYPE III)
GEOPROBE BORING LOCATION
GP-5 SOIL
NAPHTHALENE m /k
6.6
C5-C8 ALIPHATICS mg/kg
170
C9-CIO AROMATICS mg/kg
230
ETHYLBENZENE mg/kg
2.2
XYLENES mg/kgmg/kg
13.3
OFFICE
SPACE
GP-7 SOIL
NAPHTHALENE mg/kg
4.1
C5-C8 ALIPHATICS mg/kg
210
C9-ClO AROMATICS mg/kg
250
ETHYLBENZENE mg/kq
8.5
XYLENES mg/kg
43
GP-8 SOIL
NO COCc IN SOIL
ABOVE SOIL TO GROUNDWATER
MSCCs.
GP-3 SOIL
NO COCc IN SOIL
ABOVE SOIL TO GROUNDWATER
MSCCs.
OFFICE
SPACE
GP-4 SOIL
TRICHLOROETHENE mo/kq 1 0.019
�.. -TANK #5
L _ I
RESIDENCES
OFFICE BUILDING
OFFICE GP-6 SOIL
BUILDING NO COCc IN SOIL
ABOVE SOIL TO GROUNDWATER
MW-6 MSCCs.
z
TANK #11
8000-GALLON DIESEL
m
m
SUSPECTED
TANK #21
5000-GALLON
_-SUSPECTE
APdi�"
8000-GALLON
MW-11
GP-9
TANK #16
I 560-GALLON
I REMOVED 12/191
II
t J
mm
OVERHANG
TA #14
4000- ON DIESEL
GP-7 R VIED 7/1992 GARAGE
I
I
PIAGP-
i GP r - - MW-5
�} GP-6 TANK "15 _
1000-GALLON DIESEL r TANK "19
MW-4 DW-1 REMOVED 7/1992 _ ._ STORAGE
1000-GALLON SHED
TANK #12 REMOVED 7/1998
4000 GALLON
G P_ 'a _ , REMOVED 12/1992
M W - 7 TANK *8 TANK #9
1000-GALLON 1000-GALLON
I J
_
TANK #13 REMOVED 7/1992 REMOVED 7/1992
GP-4 4000-GALLON TANK #lA
REMOVED 12/1992 MW-10 T ED 1989
0
TANK #6 INS ALL
I I 560-GALLON i�i� TANK *1 TANK 2A
I t- ----TANK *10 REMOVED 7/1992 #
i CLOSED IN PLACE INSTALLED t
-I 5000-GALLON 6/1988
REMOVED 12/1992 TANK #7 OW-2
REMOVED 7/01992 I MW-1 TANK #2 r 1 1 I
WASH = - = J CLOSED IN PLACE I I
'�--- BAY I 6/1988 I I I
t J TANK # ,
SANDERS FORD _I �OSED IN cE I _
_ J 4
BUILDING TANK #4
TANK #20 —►I I
CLOSED IN P
1000-GALLON I_ J W-8
GP-1�-k-
P-2
MW-9
BRANCH STREET
Mw-2
VACANT
LOT
CONVENIENCE
STORE
300-GALLON
REMOVED 12/19
m
m
GP-9 SOIL
NO COCc IN SOIL
ABOVE SOIL TO GROUNDWATER
MSCCs.
GP-10 SOIL
NO COCc IN SOIL
ABOVE SOIL TO GROUNDWATER
MSCCs.
GP--1 SOIL
C9-C10 AROMATICS ma/kcl 1 170
GP-2 SOIL
1,1,2,2-TETRACHLOROETHANE mg/kg
0.34 ,-
C9-C10 AROMATICS mg/kg
200
LO
m
ch
C
r-
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co
c
LEGEND 9R, z 0
MONITORING WELL (TYPE II) T
MONITORING WELL (TYPE III) o O
® 84.5 ® GROUNDWATER ELEVATION CONTOUR (ft.) a RESIDENCES rr
o Ln
z rn
(85.11) GROUNDWATER ELEVATION (ft.)
C
•�— INFERRED GROUNDWATER FLOW DIRECTION U'
(NM) NOT MEASURED Q �' Ln
_ O
f.t -TANK «5 BRAGG STREET o
o Q I
cl) o
_ I r - TANK *16 < CDN
I 560-GALLON
1 REMOVED 12/199 % N O
OFFICE BUILDING ca
I I �
lJ O
TANK #17 m O
300-GALLON U �p
REMOVED 12/199
tf w
OVERHANG z � II
N
OFFICE OFFICE
SPACE BUILDING
e MW-6 ♦ m
e (NM) e >
eW TANK #14 Q
b .470-GALLON
DIESEL m
ZMOVED 7/1992 ` GARAGE m
♦TANK #11 cn
i - - W-5 z O a 8000 GALLON DIESEL I _ _ _ i (84.79) z a m
rn
REMOVED 7/1992 - pWTANK #15
(84.61) 1000-GALLON DIESEL _ _ TANK #19 O
REMOVED 7/1992 STORAGE v Q
m 1000-GALLON
-mil MW- TANK #12 REMOVED 7/1998 SHED m z
SUSPECTED ♦ (84.58) 4000-GALLON
m o w o
TANK #21 ♦ _ _ _ EMOVED 12/1992 Cn � � � w CD0
5000-GALLON I -
F-
- J I_ _ J MW-7 TANK #8 TANK #9 Q Q 0-
r - '- - , (83.84) 1000-GALLON 1000-GALLON > U '}
SUSPECTED i_ _ _ _ _ _ J W 3
TANK #22 TA #13 REMOVED 7/1992 REMOVED 7/1992
a000- LON TANK #1A —1 —I ~ _
8000-GALLON 4000-EMOVEON MW-10 INSTALLED 1989 w ~ Z 1—
MW-11 �- i TANK #6 (85.11) Q = cl-
(84.29) I 560-GALLON I DW-2 TANK #2A W � � CD CD
�--- NK 01 REMOVED 7/1992 zi (85'09) TANK 01cr
I -1 50 -GALLON � CLOSED IN PLACE INSTALLED 1989 <E � m a O
T REMOV 12/199 TANK #7 6/1988
I - OFFICE # CDU) L7 uo
r I r I �-
560-GALLON I TANK 2 , , I I
SPACE REMOVED 7/1992 _ _ _ J ~
SED IN PLACE 1 I I I � Z -� ~ �
CD— w N
w
(84.95) BAY ' tsaa Ld O � � - Ln
STANK I II I Q CV Q N
SANDERS FORD r _I i CLOSED IN PLACE I �J I- J CD U � o
_ _ J 4/1989
MW-12 BUILDING TANK #4 8s
TAN #20 —►I
1000-GALL �- JD
MW_8 CLOS�OII9N89 LACE ®0
(NM)
BRANCH STR NJ MW-9
(84.50) MW-2-__"" 84.5--------
(84.40)0
MW-3
(84.49)
VACANT 84.0 CONVENIENCE
LOT STORE
w
0
z

Lo
co
C
LEGEND o o O
_rn Z
MONITORING WELL (TYPE II) N
MONITORING WELL (TYPE III) o O
1 Ln
DISSOLVED BENZENE ISOCONCENTRATION CONTOUR ug/L RESIDENCES - 0
Z
(5.2) DISSOLVED BENZENE CONCENTRATION ug/L - q r�
(0) BELOW LABORATORY DETECTION LIMITS ug/L
w
(NS) NOT SAMPLED Q °' Ln
O
(NS/FP) NOT SAMPLE/FREE PRODUCT _ BRAGG STREET O
(NS/DRY) NOT SAMPLED/DRY i �-. -TANK *5 0 a N
m tD
a, O
TANK *16 0 N
I
I 560-GALLON ti
1 REMOVED 12/199 N
O
OFFICE BUILDING ; c
tJ O
TANK *17 m O
300-GALLON U LQ
REMOVED 12/199 O
1`o w
OVERHANG z II
r V)
OFFICE OFFICE cri
SPACE BUILDING
MW-6 m
(NS) >
co
r TANK *14 -o 0
C 4000-GALLON DIESEL m Z
Z -� REMOVED 7/1992 GARAGE (L CD
-1 I I >-
TANK *11 , - - , _ _ .Q. MW-5 0 z m
___
8000-GALLON DIESEL I I r 1 (<1) Z CD a cc
REMOVED 7/1992 J.Lu �� f— m
TANK *15 _
--� o DW-1 1000-GALLON DIESEL ,TANK *19 �
(<1) REMOVED 7/1992 L _ __ STORAGE 1— Q
m o ^* 1000-GALLON SHED z z
m MW-4 TANK *12 REMOVED 7/1998 rri L1J
SUSPECTED (2•5) TANK
rn
TANK *21 _ _ _ REMOVED 12/1992 O W CDo
5000 GALLON L _ J i_ _ _ MW-7 O }- Q wa
_ _ _ TANK *8 TANK *9 cn 3 U
r �' ' , (<1) 1000 GALLON 1000-GALLON
TANK SUSPECTED*2 I_ _ I I_ _ _ J _TANK *13 REMOVED 7/1992 REMOVED 7/1992 * W � _
8000-GALLON 4000-GALLON MW-10 TANK 1A (Q z H
MW-11 I- i REMOVED 12/1992 TANK *6 (<j) INSTALLED 1989 N Q � rr
(0.rj8) I I 560-GALLON I'I' * LLJ z n- CD 0 Z
' [,---TANK *10 REMOVED 7/1992 �: DWl)2 TANK "1 IN' sAALKEO 989 � mL'i � m z CD
L -I 5000-GALLON :1 CLOSED IN PLACE
jjj REMOVED 12/1992 TANK *7 _ _ 6/1988 (' o z o =
OFFICE 560-GALLON ; I TANK *2 , , , `—' '—' C) C
REMOVED 7/1992 J J � CD
SPACE ' _ _ _ CLOSED IN PLACE I I I I �' O .-A w N
MW-1 H I 6/1988 I I I 1 cn n- � Ln
cn
(<1) BAY I J TANK *3 �_ QV Q CN
�} SANDERS FORD r
_ i CLOSED IN PLACE I _ J I _ J ~ m U c,
MW-12 BUILDING I I I - _ - J 4/1989 TANK *4
(NS) TANK *20 --►' IN
1000-CALLON �- - - - I MW-8 CLOSED 19LACE
89
(NS/DRY)
® MW-9
BRANCH STREET , (NS/FP) MW-2
(<1) _
o MW-3
® (5.2)
� 0
VACANT % ® CONVENIENCE
LOT STORE
w
0
z

�. ��� t� �. �,
/" � ,' � ,°

MONITORIO WEEE �MMUUIM 7 901E 95R117; EM;
PROJECT NAME: Carolina Trailways BORING I.D.: GP-1
PROJECT NO.: 73.75092.0011 DATE(S) DRILLED: 2/7/2005
PROJECT LOCATION: 1201 South Blount Street DRILLING CONTR.: SEI
Raleigh, North Carolina DRILL METHOD: Geoprobe
I BORING DIAMETER: 2"
CLIENT: Carolina Trailways ISAMPLING METHOD/INTERVAL: Split Spoon
LOGGED BY: Brian Bauer IREMARKS: - Indicates Sample Taken
DESCRIPTIVE LOG (page I of 2)
SAMPLE SAMPLE BLOWS P ID/FID GRAPHIC DEPTH
INTERVAL REC. (IN.) PER 6" (PPM) COLUMN (FT) DESCRIPTION OF MATERIAL
0-6" NA NA NA 0.5 ASPHALT, underlain w/ gravel and silty clay
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
51 NA NA 7.6 5.0 Clay, brown, tight
5.5
6.0
6.5
7.0
7.5
8.0
8.5
9.0
9.5
10, NA NA 14.8 10.0 Clay, brown, tight
10.5
11.0
11.5
12.0
12.5
13.0
13.5
14.0
14.5
151* NA NA 232--j 15.01Clay, brown, tight -END OF BORING
DRILLING METHODS SAMPLING METHODS
AIR - AIR ROTARY SS - SPLIT SPOON
CFA - CONTINUOUS FLIGHT AUGER ST - SHELBY TUBE
DC - DRIVEN CASING
HA-HANDAUGER GRAPHIC COLUMN IIAW.ASSOCIATES INC.
HSA - HOLLOW STEM AUGER
MD - MUD DRILLING GROUT 2725 East Millbrook Road Suite 121
RC - ROCK CORING BENTONITE 7
WR - WATER ROTARY SAND Raleigh, North Carolina 27604
Sample c Ilected for analysis

MONITMIW; WEEE ZMOTRU',755N I 951E 195RINU EM
PROJECT NAME: Carolina Trailways IBORING I.D.: GP-2
PROJECT NO.: 73.75092.0011 IbTT-E(S) DRILLED: ' 2/7/2005
PROJECT LOCATION: 1201 South Blount Street DRILLING CON'TR.: SEI
Raleigh, North Carolina DRILL METHOD: Geoprobe
BORING DIAMETER: 2"
CLIENT: Carolina Trailways IIISAMPLING METHOD/INTERVAL: Split Spoon
LOGGED BY: Brian Bauer IREMARKS: *Indicates Sample T-aken
DESCRIPTIVE LOG (page 1 of 2)
SAMPLE SAMPLE BLOWS PID/FID GRAPHIC DEPTH
INTERVAL REC. (IN.) PER 6" (ppm) COLUMN (FO DESCRIPTION OF MATERIAL
0-6" NA NA NA 0.5 ASPHALT, underlain w/ gravel and silty clay
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5' NA NA 20.1 5.0 Clay, brown, tight
5.5
6.0
6.5
7.0
7.5
8.0
8.5
9.0
9.5
10, NA NA 272 10.0 Silt, gray, micaceous
10.5
11.0
11.5
12.0
12.5
13.0
13.5
14.0
14.5
NA NA 415 15.0 Silt, gray, micaceous -END OF BORING
DRILLING METHODS SAMPLING METHODS
AIR - AIR ROTARY SS - SPLIT SPOON
CFA - CONTINUOUS FLIGHT AUGER ST-SHELBYTUBE
DC - DRIVEN CASING
HA - HAND AUGER GRAPHIC COLUMN SS0C1A7WS1JWm
HSA - HOLLOW STEM AUGER
MD - MUD DRILLING GROUT 2725 East Millbrook Road, Suite 121
RC - ROCK CORING BENTONITE
WR - WATE ROTARY SAND Raleigh, North Carolina 27604
Sample collected for analysis = 'zr1PE=r-1\1

PROJECT NAME: Carolina Trailways BORING I.D.: GP-3
PROJECT NO.: 73.75092.0011 DATE(S) DRILLED: 2/7/2005
PROJECT LOCATION: 1201 South Blount Street DRILLING CONTR.: SEI
Raleigh, North Carolina DRILL METHOD: Geoprobe
BORING DIAMETER: 2"
CLIENT: Carolina Trailways SAMPLING METHOD/INTERVAL: Split Spoon
LOGGED
DESCRIPTIVE
SAMPLE
INTERVAL
0-6"
BY:
LOG
SAMPLE
REC. (IN.)
NA
Brian Bauer
(page 1 of
BLOWS
PER 6"
NA
2)
PID/FID
(PPM)
NA
GRAPHIC
COLUMN
1
DEPTH
(FT)
0,5
IREMARKS: *Indicates Sample Taken
DESCRIPTION OF MATERIAL
ASPHALT, underlain w/ gravel and silty clay
Clay, white to tan, tight
Clay, white to tan, tight
white to tan, tight -END OF BORING
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5'
NA
NA
0.3
5.0
5.5
6.0
6.5
7.0
7.5
8.0
8.5
9.0
9.5
101*
NA
NA
1.5
10.0
10.5
11.0
11.5
12.0
12.5
13.0
13.5
14.0
14.5
157
NA
NA
0.9
15.01CIay,
DRILLING METHODS SAMPLING METHODS
AIR - AIR ROTARY SS - SPLIT SPOON
CFA - CONTINUOUS FLIGHT AUGER ST - SHELBY TUBE
DC - DRIVEN CASING IV"ASSOCIAMS 11W.
HA-HANDAUGER GRAPHIC COLUMN
HSA - HOLLOW STEM AUGER
MD - MUD DRILLING GROUT 2725 East Millbrook Road, Suite 121
RC - ROCK CORING BENTONITE
WR - WATER ROTARY El SAND Raleigh, North Carolina 27604
LSample c Ilected for analysis 11 Qr1Pr:3=t11

MONITORINU WEE C50TROU15P 7 9151E 195R117; [5i511
PROJECT NAME: Carolina Trailways BORING I.D.: GP-4
PROJECT NO.: 73.75092.0011 DATE(S) DRILLED: 2/7/2005
PROJECT LOCATION: 1201 South Blount Street DRILLING CONTR.: SEI
Raleigh, North Carolina DRILL METHOD: Geoprobe
BORING DIAMETER: 2"
CLIENT: Carolina Trailways SAMPLING METHOD/INTERVAL: Split Spoon
LOGGED BY: Brian Bauer REMARKS: * Indicates Sample Taken
DESCRIPTIVE LOG (page 1 of 2)
SAMPLE SAMPLE BLOWS ID/FID GRAPHIC DEPTH
INTERVAL REC. (IN.) PER 6" (PPM) COLUMN (FT) DESCRIPTION OF MATERIAL
0-6" NA NA NA 0.5 ASPHALT, underlain w/ gravel and silty clay
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5- NA NA ND 5.0 Clay, white to tan, tight
5.5
6.0
6.5
7�O
7.5
8.0
8.5
9.0
9.5
10, NA NA 1.1 10.0 Sand, white to tan, clayey
10.5
11.0
11.5
12.0
12.5
13.0
13.5
14.0
14.5
15'* NA NA 1.7 15.0'Silt, tan, sandy -END OF BORING
DRILLING METHODS SAMPLING METHODS
AIR - AIR ROTARY SS - SPLIT SPOON
CFA - CONTINUOUS FLIGHT AUGER ST - SHELBY TUBE
DC - DRIVEN CASING
HA-HANDAUGER GRAPHIC COLUMN ASSOCIAMS INC.
HSA - HOLLOW STEM AUGER
MD - MUD DRILLING GROUT 2725 East Millbrook Road, Suite 121
RC - ROCK CORING BENTONITE
WR - WATER ROTARY SAND Raleigh, North Carolina 27604
Samp le c Ilected for analysis E3 Qr� D C= r7 KI

Mi5NlT5R1N6 Wr,[[
7ROJECT NAME: Carolina Trailways
?� RMOCTMN 7 951USURTO 05?5
BORIN I.D.: GP-5
PROJECT NO.: 73.75092.0011 IDATE(S) DRILLED: 2/7/2005
PROJECT LOCATION: 1201 South Blount Street DRILLING CONTR.: SEI
Raleigh, North Carolina DRILL METHOD: Geoprobe
BORING DIAMETER: 2"
CLIENT: Carolina Trailways
ISAMPLING METHOD/INTERVAL: Split Spoon
LOGGED BY: Brian Bauer
DESCRIPTIVE LOG (page 1 of 2)
SAMPLE SAMPLE BLOWS PID/FID
INTERVAL REC. (IN.) PER 6" (PPM)
IREMARKS: *Indicates Sample Taken
GRAPHIC DEPTH
COLUMN (FT) DESCRIPTION OF MATERIAL
0-6"
NA
NA
NA
0.5
CONCRETE, underlain w/ gravel and silty clay
Clay, gray, tight
Clay, gray, sandy, micaceous
gray, sandy, micaceous -END OF BORING
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5'
NA
NA
74,5
5.0
5.5
6.0
6.5
7.0
7.5
8.0
8.5
9.0
9.5
101*
NA
NA
1,376
10.0
10.5
11.0
11.5
12.0
12.5
13.0
13.5
14.0
14.5
15
NA
NA
13.8
15.0'_Clay,
DRILLING METHODS
AIR - AIR ROTARY
CFA - CONTINUOUS FLIGHT AUGER
DC - DRIVEN CASING
HA-HANDAUGER
HSA - HOLLOW STEM AUGER
MD - MUD DRILLING
RC - ROCK CORING
WR - WATER ROTARY
Sample collected for analysis
SAMPLING METHODS
SS - SPLIT SPOON
ST - SHELBY TUBE
GRAPHIC COLUMN
GROUT
BENTONITE
SAND
P-9
IA'WASSOCIAMS 1AC.
2725 East Millbrook Road, Suite 121
Raleigh, North Carolina 27604

MONIMM9 ECE ?!5N9TR0?7F51q I 951E MORIN 15G
PROJECT NAME: Carolina Trailways BORING I.D.: GP-6
PROJECT NO.: 73.75092.0011 1 DATE(S) DRILLED: 2/7/2005
PROJECT LOCATION: 1201 South Blount Street DRILLING CONTR.: SEI
Raleigh, North Carolina IDRILL METHOD: Geoprobe
BORING DIAMETER: 2"
CLIENT: Carolina Trailways ISAMPLING METHOD/INTERVAL: Split Spoon
LOGGED BY: Brian Bauer ]REMARKS: * Indicates Sample Taken
DESCRIPTIVE LOG (page 1 of 2)
SAMPLE SAMPLE BLOWS PID/FID GRAPHIC DEPTH
INTERVAL REC. (IN.) PER 6" (ppm) COLUMN (FT) DESCRIPTION OF MATERIAL
0-6" NA NA NA 0.5 CONCRETE, underlain wl gravel and silty clay
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
51 NA NA NA 5.0 Gravel
5.5
6.0
6.5
7.0
7.5
8.0
8.5
9.0
9.5
101* NA NA 2.3 10.0 Clay, white, tight
10.5
11.0
11.5
12.0
12.5
13.0
13.5
14.0
14.5
15 NA NA ND I 15.01CIay, white, tight -END OF BORING
-6-RILLING METHODS SAMPLING METHODS
AIR - AIR ROTARY SS - SPLIT SPOON
CFA - CONTINUOUS FLIGHT AUGER ST - SHELBY TUBE
DC - DRIVEN CASING
HA-HANDAUGER GRAPHIC COLUMN 1AWASSOCIAMS IIW,,
HSA - HOLLOW STEM AUGER
MID - MUD DRILLING GROUT 2725 East Millbrook Road, Suite 121
RC - ROCK CORING BENTONITE
WR - WATER ROTARY Raleigh, North Carolina 27604
SAND
Sample collected for analysis

RMITMUM WEE ?'M51q9TR0Z!Ti51q 7 011 195R10 EM15C
PROJECT NAME: Carolina Trailways BORING I.D.: GP-7
PROJECT NO.: 73.75092.0011 DATE(S) DRILLED: 2/7/2005
PROJECT LOCATION: 1201 South Blount Street DRILLING CONTR.: SEI
Raleigh, North Carolina DRILL METHOD: Geoprobe
]BORING DIAMETER: 2"
CLIENT: Carolina Trailways SAMPLIN METHOD/INTERVAL: Split Spoon
IREMARKS:
LOGGED
DESCRIPTIVE
SAMPLE
INTERVAL
0-61'
BY:
LOG
SAMPLE
REC. (IN)
NA
Brian Bauer,
(page 1 of
BLOWS
PER 6"
NA
2)
PID/FID
(ppm)
NA
GRAPHIC
COLUMN
DEPTH
(F-0
0.5
* Indicates Sample Taken
DESCRIPTION OF MATERIAL
CONCRETE, underlain w/ gravel and silty clay
Sand, gray
Clay, gray, sandy
gray, sandy -END OF BORING
1.0
1.5
2.0
2.5
3.0
3.5
4.0
51
NA
NA
ND
-4.5
5.0
5.5
6.0
6.5
7.0
7.5
8.0
8.5
9.0
9.5
10,
NA
NA
12.5
10.0
10.5
11.0
11.5
12.0
12.5
13.0
13.5
14.0
14.5
77T57.7
NA
NA
ND
15.01CIay,
DRILLING METHODS SAMPLING METHODS
AIR - AIR ROTARY SS - SPLIT SPOON
CFA - CONTINUOUS FLIGHT AUGER ST - SHELBY TUBE
DC - DRIVEN CASING
HA - HAND AUGER GRAPHIC COLUMN 1AWA SSOCIA 7WS 1M.,
HSA - HOLLOW STEM AUGER
MD - MUD DRILLING GROUT 2725 East Millbrook Road, Suite 121
RC - ROCK CORING BENTONITE
WR - WATER ROTARY SAND Raleigh, North Carolina 27604
F"
Sample c Ilected for analysis 9

1910PIT5RIMi WELL C PSTROZ,715P 7 951E 195RINU E55
PROJECT NAME: Carolina Trailways BORING I.D.: GP-8
PROJECT NO.: 73.75092.0011 1 DATE(S) DRILLED: 2/7/2005
PROJECT LOCATION: 1201 South Blount Street DRILLING CONTR.: SEI
Raleigh, North Carolina DRILL METHOD: Geoprobe
BORING DIAMETER: 2"
CLIENT: Carolina Trailways
SAMPLING METHOD/INTERVAL: Split Spoon
LOGGED
DESCRIPTIVE
SAMPLE
INTERVAL
0-6"
BY:
LOG
SAMPLE
REC. (IN.)
NA
Brian Bauer
(page 1 of
BLOWS
PER 6"
NA
2)
P11 /FID
(ppm)
NA
GRAPHIC
COLUMN
DEPTH
(FT)
0.5
REMARKS: *Indicates Sample Taken
DESCRIPTION OF MATERIAL
GRASS, underlain w/ gravel and silty clay
Sand, gray
Clay, gray, sandy
Clay, gray, sandy -END OF BORING
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
51
NA
NA
ND
5.0
5.5
6.0
6.5
7.0
7.5
8.0
8.5
9.0
9.5
10,
NA
NA
0.4
10.0
10.5
11.0
11.5
12.0
12.5
13.0
13.5
14.0
14.5'
7T5-7
NA
NA
3.1
15.0
DRILLING METHODS SAMPLING METHODS
AIR - AIR ROTARY SS - SPLIT SPOON
CFA - CONTINUOUS FLIGHT AUGER ST - SHELBY TUBE
DC - DRIVEN CASING
HA - HAND AUGER GRAPHIC COLUMN VAWASSOCIAMS 11w.
HSA - HOLLOW STEM AUGER
MID - MUD DRILLING GROUT 2725 East Millbrook Road, Suite 121
RC - ROCK CORING BENTONITE
WR -WATER ROTARY M.1 Raleigh, North Carolina 27604
SAND
Sample collected for analysis

M51TT5RING Ell
UF3N9TR0i'7151q 7 951E 9FDRING LOG
PROJECT NAME: Carolina Trailways
BORING I.D.: GP-9
PROJECT NO.: 73.75092.0011
1 DATE(S) DRILLED: 2/7/2005
PROJECT LOCATION: 1201 South Blount Street DRILLING CONTR.: SEI
Raleigh, North Carolina DRILL METHOD: Geoprobe
TBORING
DIAMETER: 2"
CLIENT: Carolina Trailways
SAMPLING METHOD/INTERVAL: Split Spoon
LOGGED BY: Brian Bauer
VEMARKS: * Indicates Sample Taken
DESCRIPTIVE LOG (page I of 2)
SAMPLE SAMPLE BLOWS
GRAPHIC DEPTH
INTERVAL REC. (IN.) PER 6" (ppm)
COLUMN (FT) DESCRIPTION OF MATERIAL
0-6" NA NA NA
0.5 GRASS, underlain w/ gravel and silty clay
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5' NA NA 0.5
5.0 Clay, red
5.5
6.0
6.5
7.0
7.5
8.0
8.5
9.0
9.5
101* NA NA 1.2
10.0 Clay, red -END OF BORING
10.5
11.0
11.5
12.0
12.5
13.0
13.5
14.0
14.5
15.0
DRILLING METHODS SAMPLING METHODS
AIR - AIR ROTARY SS - SPLIT SPOON
CFA - CONTINUOUS FLIGHT AUGER ST - SHELBY TUBE
DC - DRIVEN CASING
HA - HAND AUGER GRAPHIC COLUMN
ASSOCIATESM.
HSA - HOLLOW STEM AUGER
11
MID - MUD DRILLING GROUT
RC - ROCK CORING 19
2725 East Millbrook Road, Suite 121
BENTONITE
WR - WATER ROTARY
Raleigh, North Carolina 27604
El SAND
Sample collected for analysis

R55NIMR117; Ell ZT1q9TR0Z!T1Z5fq 7 951E 96RIN6 07;
PROJECT NAME: Carolina Trailways BORING I.D.: G,P-1 0
PROJECT NO.: 73.75092.0011 1 DATE(S) DRILLED: 2/7/2005
PROJECT LOCATION: 1201 South Blount Street DRILLING CONTR.: SEI
I
Raleigh, North Carolina DRILL METHOD: Geoprobe
I
BORING DIAMETER: 2"
11
CLIENT: Carolina Trailways a SAMPLING METHOD/INTERVAL: Split Spoon
LOGGED BY: Brian Bauer IREMARKS: *Indicates Sample Taken
DESCRIPTIVE LOG (page I of 2)
SAMPLE SAMPLE BLOWS ID/FID GRAPHIC DEPTH
INTERVAL REC. (IN.) PER 6" (ppm) COLUMN (FT) DESCRIPTION OF MATERIAL
0-6" NA NA NA 0.5 GRASS, underlain w/ gravel and silty clay
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
51 NA NA ND 5.0 Clay, red
5.5
6.0
6.5
7.0
7.5
8.0
8.5
9.0
9.5
101* NA NA 2.7 10.0 Clay, red -END OF BORING
10.5
11.0
11.5
12.0
12.5
13.0
13.5
14.0
14.5
15.01
DRILLING METHODS SAMPLING METHODS
AIR - AIR ROTARY SS - SPLIT SPOON
CFA - CONTINUOUS FLIGHT AUGER ST - SHELBY TUBE
DC - DRIVEN CASING
HA-HANDAUGER GRAPHIC COLUMN IAMASSOCIAMS 11w,
HSA - HOLLOW STEM AUGER
MID - MUD DRILLING GROUT 2725 East Millbrook Road, Suite 121
RC - ROCK CORING BENTONITE
WR - WATER ROTARY r7l Raleigh, North Carolina 27604
Li j. S A N D
Sample collected for analysis

� � � �� :�'
�r

All groundwater level measurements were obtained by using an electronic
sounding/interface detection device which registers when a probe makes contact with
petroleum product and/or water. Depth to groundwater measurements were obtained by
lowering the device into the well until it indicated that the water surface had been
encountered, at which point the level was recorded to the nearest 0.01 foot.
Groundwater Sampling
Groundwater samples were collected using new, dedicated plastic bailers at each monitoring
well. Before obtaining a sample, a minimum of three well volumes of groundwater were
removed to ensure collection of a sample representative of the in -situ groundwater
conditions. Samples were collected using dedicated bailers, transferred to containers
supplied by the laboratory, and placed in an ice -filled cooler. Chain of custody forms were
completed for each sampling event and accompanied the samples to Southern Petroleum
Laboratories (SPL).
Chemical Analyses
Chemical analyses were performed on groundwater samples by Lancaster Laboratories, Inc.
Extractions and analyses were completed in accordance with standard EPA methods. The
chemical analyses performed are outlined below:
PARAMETER
METHOD
Purgeable Halocarbons (Water)
EPA 601
Purgeable Aromatics (Water)
EPA 602

I

LAFAYETTE LABORATORY '
500 AMBASSADOR CAFFERY PARKWAY
rs SCOTT, LA 70583
[phone]
Case Narrative for:
GREYHOUND LINES, ES, INC.
Certificate of Analysis Number:
05020306
Report To:
Proiect Name:
GREYHOUND BLOUNT / 73.75029.001
ATC ASSOCIATES, INC.
Site:
GREYHOUND TERMINAL-RALEIGH
GABE ARAOS
Site Address:
#3145
2725 EAST MILBROOK RD SUITE 121
RALEIGH NC
PO Number:
RALEIGH
NC
State:
North Carolina
27604-
State Cert. No.:
487
ph [phone] fax:
Date Reported:
2/28/2005
Matrix spike (MS) and matrix spike duplicate (MSD) samples are chosen and tested at random from an analytical batch of "like" matrix to
check for possible matrix effect. The MS and MSD will provide site specific matrix data only for those samples which are spiked by the
laboratory. Since the MS and MSD are chosen at random from an analytical batch, the sample chosen for spike purposes mayor may not
have been a sample: submitted in this sample delivery group. The validity of the analytical procedures for which data is reported in this
analytical report is determined by the Laboratory Control Sample (LCS) and the Method Blank (MB). The Laboratory Control Sample (LCS)
and the Method Blank (MB) are processed with the samples and the MS/MSD to ensure method criteria are achieved throughout the entire
analytical process.
EPH: The LCS/LCSD and MS/MSD recoveries for the C9-C18 Aliphatic ranges failed to meet the LCL, indicating probable loss during the
concentration phase of the extraction process.
Any other exceptions associated with this report will be footnoted in the analytical result page(s) or the quality control summary page(s).
Please do not hesitate to contact us if you have any questions or comments pertaining to this data report. Please reference the above
Certificate of Analysis Number.
This report shall not be reproduced except in full, without the written approval of the laboratory. The reported results are only representativ
of the samples submitted for testing.
SPL, Inc. is pleased to be of service to you. We anticipate working with you in fulfilling all your current and future analytical needs.
TOTAL NUMBER OF PAGES IN THIS REPORT: PAGES
,s s
Ralph Frye
Project Manager
3/1 /2005
"I

Certificate of Analysis umber:
05020306
Report To: ATC ASSOCIATES, INC.
GABE ARAOS
2725 EAST MILBROOK RD SUITE 121
RALEIGH
NC
27604
ph: [phone] fax: [phone]
Fax To:
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Project Name: GREYHOUND BLOUNT / 73.75029.0011
i e: GREYHOUND TERM INAL-RALEIGH
Site Address: #3145
LEIGH NC
PO Number:
State: North Carolina
State Cert. No.: 487
Date Reported:
Client Sample ID
Lab Sample ID
Matrix
Date Collected
Date Received
COC ID
HOLD
GP-1 15'
05020306-01
Sal
2/7/2005 11:30:00 AM
2/8/2005 11:00:00 AM
235023
❑
GP-2 15'
05020306-02
Soil
2/7/2005 12:15:00 PM
2/8/2005 11:00:00 AM
235023
[❑
GP-3 10'
05020306-03
Sal
2/7/2005 12:45:00 PM
2/8/2005 11:00:00 AM
235023
❑
GP-4 15'
05020306-04
Soil
2/7/2005 1:15:00 PM
2/8/2005 11:00:00 AM
235023
11
GP-5 10'
05020306-05
Soil
2/7/2005 2:00:00 PM
2/8/2005 11:00:00 AM
235023
❑
GP-6 10'
05020306-06
Sal
2/7/2005 2:30:00 PM
2/8/2005 11:00:00 AM
235023
❑
GP-7 15'
05020306-07
Sal
2/7/2005 3:00:00 PM
2/8/2005 11:00:00 AM
235023
❑
GP-8 15'
05020306-08
Soil
2/7/2005 3:30:00 PM
2/8/2005 11:00:00 AM
235023
❑
GP-9 10'
05020306-09
Soil .
2/7/2005 4:00:00 PM
2/8/2005 11:00:00 AM
235023
❑
GP-10 10'
05020306-10
Soil
2/7/2005 4:30:00 PM
2/8/2005 11:00:00 AM
235023
❑
Project Manager
John D. Trahan
Laboratory Director
Tristan Davis
Quality Assurance Officer
2/28/2005
Date
2/28/2005 5:04:58 PM

7'
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
(337) 2374775
Client Sample ID:GP-1 15'
Collected: 02/07/2005 11:30 SPL Sample ID: 05020306-01
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method Result
Rep.Limit
Dil. Factor (DUAL Date Analyzed Analyst
Seq.
EXTRACTABLE PETROLEUM HYDROCARBONS -
MCL MA VPH EPH Units: mg/Kg-dry
C11-C22 Aromatics 33
14
1 02/24/05 21:39 CH
1361532
C19-C36 ' Aliphatics 21
21
1 02/26/05 20:17 CH
1361519
C9-C18 Aliphatics 250
68
5 02/26/05 17:57 CH
1361515
Sum 2-Bromonaphthalene 51.3
%
40-140
1 02/24/05 21:39 CH
1361532
Surr: 2-Fluorobiphenyi 51.4
%
40-140
1 02/24/05 21:39 CH
1361532
Surr: Chloro-octadecane 210
%
40-140
5 MI 02/26/05 17:57 CH
1361515
Surr: Chloro-octadecane 201
%
40-140
1 MI 02/26/05 20:17 CH
1361519
Surr: o-Terphenyl 57.2
%
40-140
1 02/24/05 21:39 CH
1361532
Prep Method Prep Dam
a&
S S W3,1550B .102/09/2005 18:29
Factor
Prep F-pr&P-F�
CLT 1.00
PERCENT MOISTURE
MCL D2216 Units: wt%
Percent Moisture 27
0.1
1 02/09/05 15:55 CAM
1343953
Qualifiers: ND/LJ - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:18 PM

'00or
'A n. MAr�
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-1 15'
Collected: 02/07/2005 11:30
SPL Sample ID: 05020306-01
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
SEMIVOLATILE ORGANICS
BY METHOD 8270C
MCL SW8270C
Units: ug Kg -dry
1,2,4-Trichlorobenzene
ND
230
1
02/16/05 15:46 MKM
1351856
1,2-Dichlorobenzene
ND
230
1
02/16/05 15:46 MKM
1351856
1,2-Diphenohydrazine
ND
230
1
02/16/05 15:46 MKM
1351856
1,3-Dichlorobenzene
ND
230
1
02/16/05 15:46 MKM
1351856
1,4-Dichlorobenzene
ND
230
1
02/16/05 15:46 MKM
1351856
2,4,5-Trichlorophenol
ND
230
1
02/16/05 15:46 MKM
1351856
2,4,6-Trichlorophenol
ND
230
1
02/16/05 15:46 MKM
1351856
2,4-Dichlorophenol
ND
230
1
02/16/05 15:46 MKM
1351856
2,4-Dimethylphenol
ND
230
1
02/16/05 15:46 MKM
1351856
2,4-Dinitrophenol
ND
900
1
02/16/05 15:46 MKM
1351856
2,4-Dinitrotoluene
ND
230
1
02/16/05 15:46 MKM
1351856
2,6-Dinitrotoluene
ND
230
1
02/16/05 15:46 MKM
1351856
2-Chloronaphthalene
ND
230
1
02/16/05 15:46 MKM
1351856
2-Chlorophenol
ND
230
1
02/16/05 15:46 MKM
1351856
2-Methyin apht hale ne >
2100
230
1
02/16/05 15:46 MKM
1351856
2-Nitroaniline
ND
450
1
02/16/05 15:46 MKM
1351856
2-Nitrophenol
ND
230
1
02/16/05 15:46 MKM
1351856
3,3'-Dichlorobenzi dine
ND
230
1
02/16/05 15:46 MKM
1351856
3-Nitroaniline
ND
450
1
02/16/05 15:46 MKM
135185-6
4,6-Dinitro-2-methyiphenol
ND
900
1
02/16/05 15:46 MKM
1351856
4-Bromophenyl phenyl ether
ND
230
1
02/16/05 15:46 MKM
1351856-
4-Chloro-3-m ethyl phenol
ND
230
1
02/16/05 15:46 MKM
1351856
4-Chloroaniline
ND
230
1
02/16/05 15:46 MKM
1351856
4-Chlorophenyi phenyl ether
ND
230
1
02/16/05 15:46 MKM
1351856
4-Nitroaniline
ND
450
1
02/16/05 15:46 MKM
1351856
4-Nitrophenol
ND
900
1
02/16/05 15:46 MKM
1351856
Acenaphthene
ND
230
1
02/16/05 15:46 MKM
1351856
Acenaphthylene
ND
230
1
02/16/05 15:46 MKM
1351856
Aniline
ND
230
1
02/16/05 15:46 MKM
1351856
Anthracene
ND
230
1
02/16/05 15:46 MKM
1351856
Benz(a)anthracene
ND
230
1
02/16/05 15:46 MKM
1351856
Benzo(a)pyrene
ND
230
1
02/16/05 15:46 MKM
1351856
Benzo(b)fluoranthene
ND
230
1
02/16/05 15:46 MKM
1351856
Benzo(g,hJ)perylene
ND
230
1
02/16/05-15:46 MKM
1351856
Benzo(k)fluoranthene
ND
230
1
02/16/05 15:46 MKM
1351856
Benzoic acid
ND
930
1
02/16/05 15:46 MKM
1351856
Benzyl alcohol
ND
230
1
02/16/05 15:46 MKM
1351856
Bis (2-chloroeth oxy) methane
ND
230
1
02/16/05 15:46 MKM
1351856
Bis(2-chloroethyl)ether
ND
230
1
02/16/05 15:46 MKM
1351856
Bis(2-chloroisopropyi)ether
ND
230
1
02/16/05 15:46 MKM
1351856
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and POL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:19 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
Client Sample ID:GP-1 15'
Collected: 02/07/2005 11:30
SPL Sample ID: 05020306-01
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Bis(2-ethylhexyi)phthalate
ND
230
1
02/16/05 15:46 MKM
1351856
Butyl benzyl phthalate
ND
230
1
02/16/05 15:46 MKM
1351856
Carbazole
ND
230
1
02/16/05 15:46 MKM
1351856
Chrysene
ND
230
1
02/16/05 15:46 MKM
1351856
Dibenz(a,h)anthracene
ND
230
1
02/16/05 15:46 MKM
1351856
Dibenzofuran
ND
230
1
02/16/05 15:46 MKM
1351856
Diethyl phthalate
ND
230
1
02/16/05 15:46 MKM
1351856
Dimethyt phthaJate
ND
230
1
02/16/05 15:46 MKM
1351856
Di-n-butyl phthalate
ND
230
1
02/16/05 15:46 MKM
1351856
Di-n-octyl phthalate
ND
230
1
02/16/05 15:46 MKM
1351856
Fluoranthene
ND
230
1
02/16/05 15:46 MKM
1351856
Fluorene
ND
230
1
02/16/05 15.46 MKM
1351856
Hexachlorobenzene
ND
230
1
02/16/05 15:46 MKM
1351856
Hexachlorobutadiene
ND
230
1
02/16/05 15:46 MKM
1351856
Hexachlorocyclopentadiene
ND
450
1
02/16/05 15:46 MKM
1351856
Hexachloroethane
ND
230
1
02/16/05 15:46 MKM
1351856
lndeno(1,2,3-cd)pyrene
ND
230
1
02/16/05 15:46 MKM
1351856
lsophorone
ND
230
1
02/16/05 15:46 MKM
1351856
Naphthalene
ND
230
1
02/16/05 15:46 MKM
1351856
Nitrobenzene
ND
230
1
02/16/05 15:46 MKM
1351856
N-Nitrosodi-n-propyiamine
ND
230
1
02/16/05 15:46 MKM
1351856
N-Nitrosodiphenyiamine
ND
230
1
02/16/05 15:46 MKM
1351856
Pentachlorophenol
ND
900
1
02/16/05 15:46 MKM
1351856
Phenanthrene
ND
230
1
02/16/05 15:46 MKM
1351856
Phenol
ND
230
1
02/16/05 15:46 MKM
1351856
Pyrene
ND
230
1
02/16/05 15:46 MKM
1351856
2-Methylphenol
ND
230
1
02/16/05 15:46 MKM
1351856
m,p-Cresols
ND
230
1
02/16/05 15:46 MKM
1351856
Surr: 2,4,6-Tribromophenol
102
% 14.3-114
1
02/16/05 15:46 MKM
1351856
Surr: 2-Fluorobiphenyl
72.0
% 36.6-109
1
02/16105 15:46 MKM
1351856
Surr: 2-Fluorophenol
88.1
% 30.9-91
1
02/16/05 15:46 MKM
1351856
Surr: 4-Terphenyl-d14
71.4
% 51.1-124
1
02/16/05 15:46 MKM
1351856
Surr: Nitrobenzene-d5
83.8
% 33.7-97.2
1
02/16/05 15:46 MKM
1351856
Surr: Phenol-d5
79.7
% 34.5-94.6
1
02/16/05 15:46 MKM
1351856
Pre
Prep MethodDate
SW3550B 02/09/2005 16:39
Prep Initials I Prep. Factor
—
RDH 1.00
1
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:19 PM

rR)
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-1 15'
Collected: 02/07/2005 11:30
SPL Sample ID: 05020306-01
Site:
GREYHOUND TERMINAL- LEIG
Analyses/Method
Result
Relp.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
VOLATILE ORGANICS METHOD 8260B +MTBE
MCL SW8260B
Units: ug/Kg-dry
1, 1, 1 -Trichloroethane
ND
340
50
02/16/05 15:54 GJH
1353980
1, 1,2,2-Tetrachloroethane
ND
340
50
02/16/05 15:54 GJH
1353980
1, 1,2-Trichloroethane
ND
340
50
02/16/05 15:54 GJH
1353980
1,1-Dichloroethane
ND
340
50
02/16/05 15:54 GJH
1353980
1, 1 -Dichloroethene
ND
340
50
02/16/05 15:54 GJH
1353980
1,2-Dichloroethane
ND
340
50
02/16/05 15:54 GJH
1353980
1,2-Dichloropropane
ND
340
50
02/16/05 15:54 GJH
1353980
2-Butanone
ND
1300
50
02/16/05 15:54 GJH
1353980
2-Hexanone
ND
670
50
02/16/05 15:54 GJH
1353980
4-Methyl-2-pentanone
ND
670
50
02/16/05 15:54 GJH
1353980
Acetone
ND
6700
50
02/16/05 15:54 GJH
1353980
Benzene
ND
340
50
02/16/05 15:54 GJH
1353980
Bromodichloromethane
ND
340
50
02/16/05 15:54 GJH
1353980
Bromoform
ND
340
50
02/16/05 15:54 GJH
1353980
Bromomethane
ND
670
50
02/16/05 15:54 GJH
1353980
Carbon disulfide
ND
340
50
02/16/05 15:54 GJH
1353980
Carbon tetrachloride
ND
340
50
02/16/05 15:54 GJH
1353980
Chlorobenzene
ND
340
50
02/16/05 15:54 GJH
1353980
Chloroethane
ND
670
50
02/16/05 15:54 GJH
1353980
Chloroform
ND
340
50
02/16/05 15:54 GJH
1353980
Chloromethane
ND
340
50
02/16/05 15:54 GJH
1353980
cis- 1, 3-Dichloropropene
ND
340
50
02/16/05 15:54 GJH
1353980
Dibromochloromethane
ND
340
50
02/16/05 15:54 GJH
1353980
Ethyibenzene
ND
340
50
02/16/05 15:54 GJH
1353980
Methyi tert-butyl ether
ND
340
50
02/16/05 15:54 GJH
1353980
Methylene chloride
ND
670
50
02/16/05 15:54 GJH
1353980
Styrene
ND
340
50
02/16/05 15:54 GJH
1353980
Tetrachloroethene
ND
340
50
02/16/05 15:54 GJH
1353980
Toluene
ND
340
50
02/16/05 15:54 GJH
1353980
trans- 1,3-Dichloropropene
ND
340
50
02/16/05 15:54 GJH
1353980
Trichloroethene
ND
340
50
02/16/05 15:54 GJH
1353980
Trichlorofluoromethane
ND
340
50
02/16/05 15:54 GJH
1353980
Vinyl acetate
ND
670
50
02/16/05 15:54 GJH
1353980
Vinyl chloride
ND
670
50
02/16/05'J5;154 GJH
1353980
cis- 1,2-Dichloroethene
ND
340
50
02/16/05 15:54 GJH
1353980
m,p-Xylene
ND
340
50
02/16/05 15:54 GJH
1353980
o-Xylene
ND
340
50
02/16/05 15:54 GJH
1353980
trans- 1,2-Di chloroethene
ND
340
50
02/16/05 15:54 GJH
1353980
1,2-Dichloroethene (total)
ND
340
50
02/16/05 15:54 GJH
1353980
—Xylenes,Total
ND
340
50
02/16/05 15:54 GJH
1353980
Qualifiers: ND/IJ - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and POL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:20 PM

R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-1 15'
Collected: 02/07/2005 11:30
SPL Sample ID: 05020306-01
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method Result
Rep.Lirnit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Surr: 1,2-Dichlorc)ethane-d4 97.3
%
66.1-151
50
02/16/05 15:54 GJH
1353980
Surr: 4-Bromafluorobenzene 125
%
62-139
50
02/16/05 15:54 GJH
1353980
Surr: Toluene-d8 99.2
%
74.8-118
50
02/16105 15:54 GJH
1353980
Prep Method Prep Date
SW5035 02/07/2005 0.00
Pre Initials 1Pre p Factor
IGJH 10.98
VOLATILE PETROLEUM HYDROCARBONS
MCL MA VPH EPH
Units: ug/Kg-dry
C5-C8 Aliphatics 12000
10000
50
02/10/05 15:15 NDG
1347186
C9-C10 Aromatics 170000
15000
500
02/11/05 15:41 NDG
1349003
C9-C12 Aliphatics 340000
51000
500
02/11/05 15:41 NDG
1349026
Surr: 1,4-Difluorobenzene 114
%
70-130
500
02/11/0515:41 NDG
1349026
Surr: 1,4-Difluorobenzene 107
%
70-130
500
02/11/05 15:41 NDG
1349003
Surr: 1,4-Difluorobenzene 101
%
70-130
50
02/10/05 15:15 NDG
1347186
Surr: 4-Bromafluorobenzene 116
%
70-130
500
02/11/05 15:41 NDG
1349026
Surr: 4-Bromofluorobenzene 94.0
%
70-130
500
02/11/05 15:41 NDG
1349003
Surr: 4-Bromofluorobe'nzene 154
%
70-130
50 MI
02/10/05 15-15 NDG
1347186
Prep Method
FLqp Dale
ELeS INLi,21—s
_Prep Factor
SW8015B
02/10/2005 0:00
FT
SW8015B
02/07/2005 0:00
FT
.0.74
0.74
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:20 PM

Client Sample ID:GP-2 15'
Collected: 02/07/2005 12:15
SPL Sample ID: 05020306-02
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
EXTRACTABLE PETROLEUM HYDROCARBONS MCL
MA VPH EPH
Units: mg/Kg-dry
C11-C22 Aromatics
22
14
1
02/24/05 22:16
CH
1361533
C19-C36 Aliphatics
ND
21
1
02/26/05 21:28
CH
1361521
C9-C18 Aliphatics
260
71
5
02/26/05 18:32
CH
1361516
Surr: 2-Bromonaphthalene
52.8
%
40-140
1
02/24/05 22:16
CH
1361533
Surr: 2-Fluorobiphenyl
49.0
%
40-140
1
02/24/05 22:16
CH
1361533
Sum Chloro-octadecane
90.6
%
40-140
5
02/26/05 18:32
CH
1361516
Surr: Chloro-octadecane
96.2
%
40-140
1
02/26/05 21:28
CH
1361521
Surr: o-Terphenyi
50.3
%
40-140
1
02/24/05 22:16
CH
1361533
Prep Method Prep Date
SW3550B 102/09/2005 18:29
Prep Initials Prep Factor
JCLT 11.00
PERCENT MOISTURE
MCL
D2216
Units: wt%
Percent Moisture
30
0.1
1
02/09/05 15:55 CAM
1343952
Qualifiers: ND/U
Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside
QC Limits MI - Matrix Interference
J - Estimated Value between MDL and
2/2812005 5:05:21 PM
-Not
Advisable
PAL
-Not
Advisable
PAL

AV'
-01W 'M
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-2 15'
Collected: 02/07/2005 12:15 SPL Sample ID: 05020306-02
Site:
GREYHOUND TERM I NAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dill. Factor QUAL Date Analyzed Analyst
Seq. #
-SEMIVOLATILE ORGANICS
BY METHOD
8270C
MCL SW8270C Units• ug/Kg-dry
1,2,4-Tdchlorobenzene
ND
240
1 02/17/05 15:56 MKM
1356591
1,2-Dichlorobenzene
ND
240
1 02/17/05 15:56 MKM
1356591
1,2-Dipheny1hydrazine
ND
240
1 02/17/05 15:56 MKM
1356591
1,3-Dichlorobenzene
ND
240
1 02/17/05 15:56 MKM
1356591
1,4-Dichlorobenzene
ND
240
1 02/17/05 15:56 MKM
1356591
2,4,5-Trichlorophenol
ND
240
1 02/17/05 15:56 MKM
1356591
2,4,6-Trichlorophenol
ND
240
1 02/17/05 15:56 MKM
1356591
- 2,4-Dichlorophenol
ND
240
1 02/17/05 15:56 MKM
1356591
- 2,4-Dimethylphend
ND
240
1 02/17/05 15:56 MKM
1356591
- 2,4-Dinitrophenol
ND
940
1 02/17/05 15:56 MKM
1356591
2,4-Dinitrotoluene
ND
240
1 02/17/05 15:56 MKM
1356591
2,6-Dinitrotoluene
ND
240
1 02/17/05 15:56 MKM
1356591
- 2-Chloronaphthalene
ND
240
1 02/17/05 15:56 MKM
1356591
- 2-Chlorophenol
ND
240
1 02/17/05 15:56 MKM
1356591
- 2-Methonaphthalene
1100
240
1 02/17/0515 :56 MKM
1356591
2-Nitroaniline
ND
470
1 02/17/0515:56 MKM
1356591
- 2-Nitrophenol
ND
240
1 02/17/05 15:56 MKM
1356591
3,3'-D i chlorobenzi dine
ND
240
1 02/17/05 15:56 MKM
1356591
3-Nitroaniline
ND
470
1 02/17/05 15:56 MKM
1356591
4,6-Dinitro-2-methyiphenol
ND
940
1 02/17/05 15:56 MKM
1356591
- 4-Bromophenyl phenyl ether
ND
240
1 02/17/05 15:56 MKM
1356591
4-Chloro-3-m ethyl phenol
ND
240
1 02/17/05 15:56 MKM
1356591
4-Chloroaniline
ND
240
1 02/17/05 15:56 MKM
1356591
- 4-Chlorophenyl phenyi ether
ND
240
1 02/17/05 15:56 MKM
1356591
4-Nitroaniline
ND
470
1 02/17/05 15.56 MKM
1356591
4-Nitrophenol
ND
940
1 02/17/05 15:56 MKM
1356591
- Acenaphthene
ND
240
1 02/17/05 15:56 MKM
1356591
- Acenaphthylene
ND
240
1 02/17/05 15:56 MKM
1356591
Aniline
ND
240
1 02/17/05 15:56 MKM
1356591
Anthracene
ND
240
1 02/17/05 15:56 MKM
1356591
- Benz(a)anthracene
ND
240
1 02/17/05 15:56 MKM
1356591
- Benzo(a)pyrene
ND
240
1 02/17/05 15:56 MKM
1356591
- Benzo(b)fluoranthene
ND
240
1 02/17/05 15:56 MKM
1356591
- Benzo(g,h,i)peryiene
ND
240
1 02/17/051,115:56 MKM
1356591
- Benzo(k)fluoranthene
ND
240
1 02/17/05 15:56 MKM
1356591
Benzoic acid
ND
970
1 02/17/05 15:56 MKM
1356591
Benzyi alcohol
ND
240
1 02/17/05 15:56 MKM
1356591
-Bis(2-chloroethoxy)m ethane
ND
240
1 02/17/05 15:56 MKM
1356591
-Bis(2-chloroethyi)ether
ND
240
1 02/17/05 15:56 MKM
1356591
Bis(2-chloroisopropyl)ether
ND
240
1 02/17/05 15:56 MKM
1356591
Qualifiers: ND/L) - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:22 PM

Client Sample ID:GP-2 15'
Collected: 02/07/2005 12:15
SPL Sample ID: 05020306-02
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Lirnit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Bis(2-ethy1hexyi)phthalate
ND
240
1
02/17/05 15:56 MKM
1356591
Butyl benzyi phthalate
ND
240
1
02/17/05 15:56 MKM
135659-1
Carbazole
ND
240
1
02/17/05 15:56 MKM
1356591
Chrysene
ND
240
1
02/17/05 15:56 MKM
1356591
Dibenz(a,h)anthracene
ND
240
1
02/17/05 15:56 MKM
1356591
Dibenzofuran
ND
240
1
02/17/05 15:56 MKM
1356591
Diethyl phthalate
ND
240
1
02/17/05 15:56 MKM
1356591
Dimethyi phthalate
ND
240
1
02/17/05 15:56 MKM
1356591
Di-n-butyl phthalate
ND
240
1
02/17/05 15:56 MKM
1356591
Di-n-octyi phthalate
ND
240
1
02/17/05 15:56 MKM
1356591
Fluoranthene
ND
240
1
02/17/05 15:56 MKM
1356591
Fluorene
ND
240
1
02/17/05 15:56 MKM
1356591
Hexachlorobenzene
ND
240
1
02/17/05 15:56 MKM
1356591
Hexachlorobutadiene
ND
240
1
02/17/05 15:56 MKM
1356591
Hexachlorocyclopentadiene
ND
470
1
02/17/05 15:56 MKM
1356591
Hexachloroethane
ND
240
1
02/17/05 15:56 MKM
1356591
Indeno,(1,2,3-cd)pyren6
ND
240
1
02/17/05 15:56 MKM
1356591
Isophorone
ND
240
1
02/17/05 15:56 MKM
1356591
Naphthalene
ND
240
1
02/17/05 15:56 MKM
1356591
Nitrobenzene
ND
240
1
02/17/05 15:56 MKM
1356591
N-Nitrosodi-n-propylamine
ND
240
1
02/17/05 15:56 MKM
1356591
N-Nitrosodiphenylamine
ND
240
1
02/17105 15:56 MKM
1356591
Pentachlorophenol
ND
940
1
02/17/05 15:56 MKM
1356591
Phenanthrene
ND
240
1
02/17/05 15:56 MKM
1356591
Phenol
ND
240
1
02/17/05 15:56 MKM
1356591
Pyrene
ND
240
1
02/17/05 15:56 MKM
1356591
2-Methyiphenol
ND
240
1
02/17/05 15:56 MKM
1356591
m,p-Cresols
ND
240
1
02/17/05 15:56 MKM
1356591
Surr: 2,4,6-Tribromophenol
116
% 14.3-114
1
02/17/05 15:56 MKM
1356591
Surr: 2-Fluorobiphenyl
58.6
% 36.6-109
1
02/17/05 15:56 MKM
1356591
Surr: 2-Fluorophenol
101
% 30.9-91
1
02/17/05 15:56 MKM
1356591
Surr: 4-Terphenyl-d14
71.7
% 51.1-124
1
02/17/05 15:56 MKM
1356591
Surr: Nitrobenzene-d5
95.6
% 33.7-97.2
1
02/17/05 15:56 MKM
1356591
Surr: Phenol-d5
84.8
% 34.5-94.6
1
02/17/05 15:56 MKM
1356591
Prer) Mglbgd Preg Date
SW3550B 02/09/2005 16:39
1
Prep Initials Prep Factor
RDH 1.00
Qualifiers: ND/L1 - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:22 PM

AV- AV
.W Aff
16'r
Air
R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-2 15'
Collected: 02/07/2005 12:15
SPL Sample ID: 05020306-02
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq.
VOLATILE ORGANICS METHOD 8260B +MTBE
MCL SW8260B
Units: ug/Kg-dry
1, 1, 1 -Trichloroethane
ND
5.7
1
02/16/05 16:52
GJH
1353982
1, 1,2,2-Tetrachloroethane
340
5.7
1
02/16/05 16:52
GJH
1353982
1, 1,2-Trichloroethane
ND
5.7
1
02/16/05 16:52
GJH
1353982
1,1-Dichloroethane
ND
5.7
1
02/16/05 16:52
GJH
1353982
1, 1 -Dichloroethene
ND
5.7
1
02/16/05 16:52
GJH
1353982
1,2-Dichloroethane
ND
5.7
1
02/16/05 16:52
GJH
1353982
1,2-Dichloropropane
ND
5.7
1
02/16/05 16:52
GJH
1353982
2-Butanone
ND
23
1
02/16/05 16:52
GJH
1353982
2-Hexanone
ND
11
1
02/16/05 16:52
GJH
1353982
4-Methyl-2-pentanone
ND
11
1
02/16/05 16:52
GJH
1353982
Acetone
ND
110
1
02/16/05 16:52
GJH
1353982
Benzene
ND
5.7
1
02/16/05 16:52
GJH
1353982
Bromodichloromethane
ND
5.7
1
02/16/05 16:52
GJH
1353982
Bromoform
ND
5.7
1
02/16/05 16:52
GJH
1353982
Bromomethane
ND
11
1
02/16/05 16:52
GJH
1353982
Carbon disulfide
ND
5.7
1
02/16/05 16:52
GJH
1353982
Carbon tetrachloride
ND
5.7
1
02/16/05 16:52
GJH
1353982
Chlorobenzene
ND
5.7
1
02/16/05 16:52
GJH
1353982
Chloroethane
ND
11
1
02/16/05 16:52
GJH
1353982
Chloroform
ND
5.7
1
02/16/05 16:52
GJH
1353982
Chloromethane
ND
5.7
1
02/16/05 16:52
GJH
1353982
cis- 11,3-Dichloropropene
ND
5.7
1
02/16/05 16:52
GJH
1353982
Dibromochloromethane
ND
5.7
1
02/16/05 16:52
GJH
1353982
Ethylbenzene
ND
5.7
1
02/16/05 16:52
GJH
1353982
Methyl tert-butyl ether
ND
5.7
1
02/16/05 16:52
GJH
1353982
Methylene chloride
ND
11
1
02/16/05 16:52
GJH
1353982
Styrene
ND
5.7
1
02/16/05 16:52
GJH
1353982
Tetrachloroethene
ND
5.7
1
02/16/05 16:52
GJH
1353982
Toluene
ND
5.7
1
02/16/05 16:52
GJH
1353982
trans- 1, 3-Dichloropropene
ND
5.7
1
02/16/05 16:52
GJH
1353982
Trichloroethene
ND
5.7
1
02/16/05 16:52
GJH
1353982
Trichlorofluoromethane
ND
5.7
1
02/16/05 16:52
GJH
1353982
Vinyl acetate
ND
11
1
02/16/05 16:52
GJH
1353982
Vinyl chloride
ND
11
1
02/16/05 -1,61:52
GJH
1353982
cis- 1, 2-D ichloroethene
ND
5.7
1
02/16/05 16:52
GJH
1353982
m,p-Xylene
ND
5.7
1
02/16/05 16:52
GJH
1353982
o-Xyiene
ND
5.7
1
02/16/05 16:52
GJH
1353982
trans- 1,2-Dichloroethene
ND
5.7
1
02/16/05 16:52
GJH
1353982
1,2-Dichloroethene (total)
ND
5.7
1
02/16/05 16:52
GJH
1353982
-Xyienes,Total
ND
5.7
1
02/16/05 16:52
GJH
1353982
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:23 PM

Client Sample ID:GP-2 15'
Collected: 02/07/2005 12:15
SPL Sample ID: 05020306-02
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Surr: 1,2-Dichloroethane-d4
117
%
66.1-151
1
02/16/05 16:52 GJH
1353982
Surr: 4-Bromofluorobenzene
555
%
62-139
1 MI
02/16/05 16:52 GJH
1353982
Surr: Toluene-d8
109
%
74.8-118
1
02/16/05 16:52 GJH
1353982
I Prep Method Prep Date
SW5035 02/07/2005 0:00 1
Preg Initials Prep
VOLATILE PETROLEUM HYDROCARBONS
MCL
MA VPH EPH
Units: ug/Kg-dry
C5-C8 Aliphatics
ND
11000
50
02/10/05 15:44 NDG
1347187
C9-C 10 Aromatics 200000
17000
500
02/11/05 16:10 NDG
1349004
C9-C12AIiphatics 440000
57000
500
02/11/05 16:10 NDG
1349028
Surr: 1,4-Difluorobenzene
106
%
70-130
500
02/11/05 16:10 NDG
1349004
Surr: 1,4-Dffluorobenzene
101
%
70-130
500
02/11/05 16:10 NDG
1349028
Surr: 1,4-Difluorobenzene
101
%
70-130
50
02/10/05 15:44 NDG
1347187
Surr: 4-Bromofluorobenzene
121
%
70-130
500
02/11/05 16:10 NDG
1349028
Surr: 4-Bromafluorobenzene
96.2
%
70-130
500
02/11/05 16:10 NDG
1349004
Surr: 4-Bromofluorobenzene
154
%
70-130
50 MI
02/10/05 15:44 NDG
1347187
Prep MethodFjfp D _@&t
SW8015B 02/10/2005 0:00
SW8015B 02/07/2005 0:00
Prep Initials Prep Facto[
FT 0.80
FT 0.80
Qualifiers: ND/U
Factor
GJH
0.80
-Not

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
(337) 2374775
Client Sample ID:GP-3 10'
Collected: 02/07/2005 12:45 SPL Sample ID: 05020306-03
Site:
GREYHOUND TERM I NAL-RALEIG H
Analyses/Method Result
Rep.Limit
Dil. Factor QUAL Date Analyzed Analyst
Seq. #
-EXTRACTABLE PETROLEUM HYDROCARBONS
MCL MA VPH EPH Units: mg/Kg-dry
C11-C22 Aromatics ND
12
1 02/24/05 22:52 CH
1361534
C19-C36 Aliphatics ND
18
1 02/26/05 22:04 CH
1361522
C9-C18 Aliphatics ND
12
1 02/26/05 22:04 CH
1361522
Sum 2-Bromonaphthalene 50.2
% 40-140
1 02/24/05 22:52 CH
1361534
Surr: 2-Fluorobiphenyi 52.1
% 40-140
1 02/24/05 22:52 CH
1361534
Surr: Chloro-octadecane 80.9
% 40-140
1 02/26/05 22:04 CH
1361522
Surr: o-Terphenyl 48.0
1% 40-140
1 02/24/05 22:52 CH
1361534
Prep Method JEW Date
ISW3550B 102/09/2005 18:29
Pre g Initials Prep Factor
JCLT 11.00
PERCENT MOISTURE
MCL D2216 Units: wt%
Percent Moisture 15
0.1
1 02/09/05 15:55 CAM
1343951
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
6 - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:24 PM

10- "Ir
R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-3 10'
Collected: 02/07/2005 12:45
SPL Sample ID: 05020306-03
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
SEMIVOLATILE ORGANICS
BY METHOD 8270C
MCL SW8270C
Units: ug/Kg-dry
1,2,4-Trichlorobenzene
ND
200
1
02/19/05 0:22 LMK
1355343
1,2-Dichlorobenzene
ND
200
1
02/19/05 0:22 LMK
1355343
1,2-Diphenohydrazine
ND
200
1
02/19/05 0:22 LMK
1355343
1,3-Dichlorobenzene
ND
200
1
02/19/05 0:22 LMK
1355343
1,4-Dichlorobenzene
ND
200
1
02/19/05 0:22 LMK
1355343
2,4,5-Trichlorophenol
ND
200
1
02/19/05 0:22 LMK
1355343
2,4,6-T rich lorop henol
ND
200
1
02/19/05 0:22 LMK
1355343
2,4-Dichlorophenol
ND
200
1
02/19/05 0:22 LMK
1355343
2,4-Dimethyiphenol
ND
200
1
02/19/05 0:22 LMK.
1355343
2,4-Dinitrophenol
ND
780
1
02/19/05 0:22 LMK
1355343
2,4-Dinitrotoluene
ND
200
1
02/19/05 0:22 LMK
1355343
2,6-Dinitrotoluene
ND
200
1
02/19/05 0:22 LMK
1355343
2-Chloronaphthalene
ND
200
1
02/19/05 0:22 LMK
1355343
2-Chlorophenol
ND
200
1
02/19/05 0:22 LMK
1355343
2-Methyinaphthalene
ND
200
1
02/19/05 0:22 LMK
1355343
2-Nitroaniline
ND
390
1
02/19/05 0:22 LMK
1355343
2-Nitrophenol
ND
200
1
02/19/05 0:22 LMK
1355343
3,3'-Dich lorobenzi dine
ND
200
1
02/19/05 0:22 LMK
1355343
3-Nitroaniline
ND
390
1
02/19/05 0:22 LMK
1355343
4,6-D i nitro-2-m et ho phenol
ND
780
1
02/19/05 0:22 LMK
1355343
4-Bromophenyl phenyl ether
ND
200
1
02/19/05 0:22 LMK
1355343
4-Chloro-3-methyiphenol
ND
200
1
02/19/05 0:22 LMK
1355343
4-Chloroaniline
ND
200
1
02/19/05 0:22 LMK
1355343
4-Chlorophenyl phenyl ether
ND
200
1
02/19/05 0:22 LMK
1355343
4-Nitroaniline
ND
390
1
02/19/05 0.22 LMK
1355343
4-Nitrophenol
ND
780
1
02/19/05 0:22, LMK
1355343
Acenaphthene
ND
200
1
02/19/05 0:22 LMK
1355343
Acenaphthylene
ND
200
1
02/19/05 0:22 LMK
1355343
Aniline
ND
200
1
02/19/05 0:22 LMK.
1355343
Anthracene
ND
200
1
02/19/05 0:22 LMK
1355343
Benz(a)anthracene
ND
200
1
02/19/05 0:22 LMK
1355343
Benzo(a)pyrene
ND
200
1
02/19/05 0:22 LMK
1355343
Benzo(b)fluoranthene
ND
200
1
02/19/05 0:22 LMK
1355343
Benzo(g,h,i)per)dene
ND
200
1
02/19/Q5 Q:22 LMK
1355343
Benzo(k)fluoranthene
ND
200
1
02/19/05 0:22 LMK
1355343
Benzoic acid
ND
800
1
02/19/05 0:22 LMK
1355343
Benzyl alcohol
ND
200
1
02/19/05 0:22 LMK
1355343
Bis (2-chloroethoxy)m ethane
ND
200
1
02/19/05 0:22 LMK
1355343
Bis(2-chloroethyl)ether
ND
200
1
02/19/05 0:22 LMK
1355343
Bis(2-chloroisopropyl)ether
ND
200
1
02/19/05 0:22 LMK
1355343
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:25 PM

'400 Ana A 0 A- C-n.?
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-3 10'
Collected: 02/07/2005 12:45
SPL Sample ID: 05020306-03
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Di 1. Factor QUAL
Date Analyzed
Analyst
Seq. #
B is (2-ethylhexyl)phthal ate
ND
200
1
02/19/05 0:22
LMK
1355343
Butyl benzyl phthalate
ND
200
1
02/19/05 0:22
LMK
1355343
Carbazole
ND
200
1
02/19/05 0:22
LMK
1355343
Chrysene
ND
200
1
02/19/05 0:22
LMK
1355343
Dibenz(a,h)anthracene
ND
200
1
02/19/05 0:22
LMK
1355343
Dibenzofuran
ND
200
1
02/19/05 0:22
LMK
1355343
Diethyl phthalate
ND
200
1
02/19/05 0:22
LMK
1355343
Dimethyl phthalate
ND
200
1
02/19/05 0:22
LMK
1355343
Di-n-butyl phthalate
ND
200
1
02/19/05 0:22
LMK
1355343
Di-n-octyi phthalate
ND
200
1
02/19/05 0:22
LMK
1355343
Fluoranthene
ND
200
1
02/19/05 0:22
LMK
1355343
Fluorene
ND
200
1
02/19/05 0:22
LMK
1355343
Hexachlorobenzene
ND
200
1
02/19/05 0:22
LMK
1355343
Hexachlorobutadiene
ND
200
1
02/19/05 0:22
LMK
1355343
Hexachlorocyclopentacliene
ND
390
1
02/19/05 0:22
LMK
1355343
Hexachloroethane
ND
200
1
02/19/05 0:22
LMK
1355343
Indeno(1,2,3-cd)pyrene
ND
200
1
02/19/05 0:22
LMK
1355343
Isophorone
ND
200
1
02/19/05 0:22
LMK
1355343
Naphthalene
ND
200
1
02/19/05 0:22
LMK
1355343
Nitrobenzene
ND
200
1
02/19/05 0:22
LMK
1355343
N-Nitrosodi-n-propylamine
ND
200
1
02/19/05 0:22
LMK
1355343
N-N itrosocliphenyla mine
ND
200
1
02/19/05 0:22
LMK
1355343
Pentachlorophenol
ND
780
1
02/19/05 0:22
LMK
1355343
Phenanthrene
ND
200
1
02/19/05 0:22
LMK
1355343
Phenol
ND
200
1
02/19/05 0:22
LMK
1355343
Pyrene
ND
200
1
02/19/05 0:22
LMK
1355343
2-Methylphenol
ND
200
1
02/19/05 0:22
LMK
1355343
m,p-Cresols
ND
200
1
02/19/05 0:22
LMK
1355343
Surr: 2,4,6-Tribromophenol
97.2
% 14.3-114
1
02/19/05 0:22
LMK
1355343
Surr: 2-Fluorobipheno
69.9
% 36.6-109
1
02/19/05 0:22
LMK
1355343
Surr: 2-Fluorophenol
78.4
% 30.9-91
1
02/19/05 0:22
LMK
1355343
Surr: 4-Terphenyl-d14
80.1
% 51.1-124
1
02/19/05 0:22
LMK
1355343
Surr: Nitrobenzene-d5
67.3
% 33.7-97.2
1
02/19/05 0:22
LMK
1355343
Surr: Phenol-d5
75.5
% 34.5-94.6
1
02/19/05 0:22
LMK
1355343
Prep Method Pre Q te
SW35508 102/09/2005 16:39
_Prey Initials Prep Factor
IRDH 11.00
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2128/2005 5:05:25 PM

AMA AwArn.
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-3 10'
Collected: 02/07/2005 12:45
SPL Sample ID: 05020306-03
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result Rep.Lirnit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS METHOD 8260B +MTBE
MCL SW8260B
Units: ug/Kg-dry
1,1,1-Trichloroethane
ND
5
1
02/15/05 20:29
GJH
1350186
1, 1,2,2-Tetrachloroethane
ND
5
1
02/15/05 20:29
GJH
1350186
1, 1,2-T rich loroeth ane
ND
5
1
02/15/05 20:29
GJH
1350186
1,1-Dichloroethane
ND
5
1
02/15/05 20:29
GJH
1350186
1,1-Dichloroethene
ND
5
1
02/15/05 20:29
GJH
1350186
1,2-Dichloroethane
ND
5
1
02/15/05 20:29
GJH
1350186
1,2-Dichloropropane
ND
5
1
02/15/05 20:29
GJH
1350186
2-Butanone
ND
20
1
02/15105 20:29
GJH
1350186
2-Hexanone
ND
10
1
02/15/05 20:29
GJH
1350186
4-Methyl-2-pentanone
ND
10
1
02/15/05 20:29
GJH
1350186
Acetone
ND
100
1
02/15/05 20:29
GJH
1350186
Benzene
ND
5
1
02/15/05 20:29
GJH
1350186
Bromodichloromethane
ND
5
1
02/15/05 20:29
GJH
1350186
Bromoform
ND
5
1
02/15/05 20:29
GJH
1350186
Bromomethane
ND
10
1
02/15/05 20:29
GJH
1350186
Carbon disulfide
ND
5
1
02/15/05 20:29
GJH
1350186
Carbon tetrachloride
ND
5
1
02/15/05 20:29
GJH
1350186
Chlorobenzene
ND
5
1
02/15/05 20:29
GJH
1350186
Chloroethane
ND
10
1
02/15/05 20:29
GJH
1350186
Chloroform
ND
5
1
02/15/05 20:29
GJH
1350186
Chloromethane
ND
5
1
02/15/05 20:29
GJH
1350186
cis - 1, 3-Dichloropropene
ND
5
1
02/15/05 20:29
GJH
1350186
Dibromochloromethane
ND
5
1
02/15/05 20:29
GJH
1350186
Ethylbenzene
ND
5
1
02/15105 20:29
GJH
1350186
Methyl tert-butyl ether
ND
5
1
02/15/05 20:29
GJH
1350186
Methylene chloride
ND
10
1
02/15/05 20:29
GJH
1350186
Styrene
ND
5
1
02/15/05 20:29
GJH
1350186
Tetrachloroethene
ND
5
1
02/15/05 20:29
GJH
1350186
Toluene
ND
5
1
02/15/05 20:29
GJH
1350186
trans- 1, 3-Dichloropropen.e
ND
5
1
02/15105 20:29
GJH
1350186
Trichloroethene
5.5
5
1
02/15/05 20:29
GJH
1350186
Trichlorofluoromethane
ND
5
1
02/15/05 20:29
GJH
1350186
Vinyl acetate
ND
10
1
02/15/05 20:29
GJH
1350186
Vinyl chloride
ND
10
1
02/15/05 20:29
GJH
1350186
cis- 1,2-Dichloroethene
ND
5
1
02/15/05 20:29
GJH
1350186
m,p-Xylene
ND
5
1
02/15/05 20:29
GJH
1350186
o-XyIene
ND
5
1
02/15/05 20:29
GJH
1350186
trans- 1,2-Di chloroethene
ND
5
1
02/15/05 20:29
GJH
1350186
1,2-Dichloroethene (total)
ND
5
1
02/15/05 20:29
GJH
1350186
Xyienes,Total
ND
5
1
02115/05 20:29
GJH
1350186
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(IVICL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:25 PM

Client Sample ID:GP-3 10'
Collected: 02/0712005 12:45
SPL Sample ID: 05020306-03
Site: GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Surr: 1,2-Dichloroethane-d4
118
% 66.1-151
1
02/15/05 20:29 GJH
1350186
Surr: 4-Bromofluorobenzene
100
% 62-139
1
02/15/05 20:29 GJH
1350186
Surr: Toluene-d8
96.7
% 74.8-118
1
02/15/05 20:29 GJH
1350186
Prep Method PrQkDate
SW5035 02/07/2005 0:00
Prei) Initials Prev Factor
FT 0.85
VOLATILE PETROLEUM HYDROCARBONS MCL
MA VPH EPH
Units: ug/Kg-dry
C5-C8 Aliphatics
ND
12000
50
02/10/05 16:12 NDG
1347188
C9-C10 Aromatics
ND
1800
50
02/10/05 16:12 NDG
1347261
C9-C12 Aliphatics
ND
6100
50
02/10/05 16:12 NDG
1347188
Surr: 1,4-Difluorobenzene
105
% 70-130
50
02/10/05 16:12 NDG
1347261
Surr: 1,4-Difluorobenzene
104
% 70-130
50
02/10/05 16:12 NDG
1347188
Surr: 4-Brornofluorobenzene
95.6
% 70-130
50
02/10/05 16:12 NDG
1347188
Surr: 4-Bromofluorobenzene
92.5
% 70-130
50
02/10/05 16:12 NDG
1347261
Preo Method'Prep Date
SW8015B 02/10/2005 0:00
SW8015B 02/10/2005 0:00
Prep Initials Prep Factor
IFT 11.03
IFT 11.03
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:26 PM

R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
(337) 2374775
Client Sample ID:GP-4 15'
Collected: 02/07/2005 13:15 SPL Sample ID: 05020306-04
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method Result
Rep.Limit
Dil. Factor QUAL Date Analyzed Analyst
Seq. #
EXTRACTABLE PETROLEUM HYDROCARBONS
-
MCL MA VPH EPH Units: m.g/Kg-dg
C11-C22 Aromatics ND
13
1 02/24/05 23:27 CH
1361535
C19-C36 Aliphatics ND
19
1 02/26/05 22:39 CH
1361523
C9-C18 Aliphatics ND
13
1 02/26/05 22:39 CH
1361523
Surr 2-Bromonaphthalene 42.0
% 40-140
1 02/24/05 23:27 CH
1361535
Surr: 2-Fluorobipheny! 45.5
% 40-140
1 02/24/05 23:27 CH
1361535
Sum Chloro-octadecane 79.7
% 40-140
1 02/26/05 22:39 CH
1361523
Surr: o-Terphenyl 50.4
% 40-140
1 02/24/05 23:27 CH
1361535
Prep Method Prep Date
FS'W3550B 102/09/2005 18:29
Pre Lniti_gls a= Factor j
CLT 1.00
PERCENT MOISTURE -
-
MCL D2216 Units: wt%
Percent Moisture 23
0.1
1 02/09/05 15:55 CAM
1343950
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:27 PM

AW40 �Aw
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-4 15'
Collected: 02/07/2005 13:15
SPL Sample ID: 05020306-04_
Site:
GREYHOUND TERMINAL LEIGH
Analyses/Method
Result
Rep.Lirnit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
.SEMIVOLATILE ORGANICS
BY METHOD
8270C
MCL SW8270C
Units: ug/Kg-dry
-
1,2,4-Trichlorobenzene
ND
220
1
02/19/05 0:54 LMK
135534-4
1,2-Dichlorobenzene
ND
220
1
02/19/05 0:54 LMK
1355344
1,2-Diphenohydrazine
ND
220
1
02/19/05 0:54 LMK
1355344
1,3-Dichlorobenzene
ND
220
1
02/19/05 0:54 LMK
1355344
1,4-Dichiorobenzene
ND
220
1
02/19/05 0:54 LMK
1355344
2,4,5-Trichlorophenol
ND
220
1
02/19/05 0:54 LMK
1355344
2,4,6-Trichlorophenol
ND
220
1
02/19/05 0:54 LMK
1355344
2,4-Dichlorophenol
ND
220
1
02/19/05 0:54 LMK
1355344
2,4-Dimethophenol
ND
220
1
02/19/05 0:54 LMK
1355344
2,4-Dinitrophenol
ND
860
1
02/19/05 0:54 LMK
1355344
2,4-Dinitrotoluene
ND
220
1
02/19/05 0:54 LMK
1355344
2,6-Dinitrotoluene
ND
220
1
02/19/05 0:54 LMK
1355344
2-Chloronaphthalene
ND
220
1
02/19/05 0:54 LMK
1355344
2-Chlorophenol
ND
220
1
02/19/05 0:54 LMK
1355344
2-Methonaphthalene
ND
220
1
02/19/05 0:54 LMK
1355344
2-Nitroaniline
ND
430
1
02/19/05 0:54 LMK
1355344
2-Nitrophenol
ND
220
1
02/19/05 0:54 LMK
1355344
3,3'-Dichlorobenzidine
ND
220
1
02/19/05 0:54 LMK
1355344
3-Nitroaniline
ND
430
1
02/19/05 0:54 LMK
1355344
4,6-D initro-2-m et hyi phenol
ND
860
1
02/19/05 0:54 LMK
1355344
4-Bromophenyl phenyl ether
ND
220
1
02/19/05 0:54 LMK
1355344
4-Chloro-3-methyl phenol
ND
220
1
02/19/05 0:54 LMK
1355344
4-Chloroaniline
ND
220
1
02/19/05 0:54 LMK
1355344
4-Chlorophenyi phenyl ether
ND
220
1
02/19/05 0:54 LMK
1355344
4-Nitroaniline
ND
430
1
02/19/05 0:54 LMK
1355344
4-Nitrophenol
ND
860
1
02/19/05 0:54 LMK
1355344
Acenaphthene
ND
220
1
02/19/05 0:54 LMK
1355344
Acenaphthylene
ND
220
1
02/19/05 0:54 LMK
1355344
Aniline
ND
220
1
02/19/05 0:54 LMK
1355344
Anthracene
ND
220
1
02/19/05 0:54 LMK
1355344
Benz(a)anthracene
ND
220
1
02/19/05 0:54 LMK
1355344
Benzo(a)pyrene
ND
220
1
02/19/05 0:54 LMK
1355344
Benzo(b)fluoranthene
ND
220
1
02/19/05 0:54 LMK
1355344
Benzo(g,h,i)peryiene
ND
220
1
02/19/05 0:54 LMK
1355344
Benzo(k)fluoranthene
ND
220
1
02/19/05 0:54 LMK
1355344
Benzoic acid
ND
880
1
02/19/05 0:54 LMK
1355344
Benzyl alcohol
ND
220
1
02/19/05 0:54 LMK
1355344
Bis (2-chloroethoxy)m ethane
ND
220
1
02/19/05 0:54 LMK
1355344
Bis(2-chloroethyl)ether
ND
220
1
02/19/05 0:54 LMK
1355344
Bis(2-chloroisopropo)ether
ND
220
1
02119/05 0:54 LMK
1355344
Qualifiers: ND/U - Not Detected at the Reporting Limit
6 - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:27 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-4 15'
Collected: 02/07/2005 13:15
SPL Sample ID: 05020306-04
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
Bis (2-ethylhexyi)phthal ate
ND
220
1
02/19/05 0:54
LMK
1355344
Butyl benzo phthalate
ND
220
1
02/19/05 0:54
LMK
1355344
Carbazole
ND
220
1
02/19/05 0:54
LMK
1355344
Chrysene
ND
220
1
02/19/05 0:54
LMK
1355344
Dibenz(a,h)anthracene
ND
220
1
02/19/05 0:54
LMK
1355344
Dibenzofuran
ND
220
1
02/19/05 0:54
LMK
1355344
Diethyl phthalate
ND
220
1
02/19/05 0:54
LMK
1355344
Dimethyi phthalate
ND
220
1
02/19/05 0:54
LMK
1355344
Di-n-butyl phthalate
ND
220
1
02/19/05 0:54
LMK
1355344
Di-n-octyl phthalate
ND
220
1
02/19/05 0:54
LMK
1355344
Fluoranthene
ND
220
1
02/19/05 0:54
LMK
1355344
Fluorene
ND
220
1
02/19/05 0:54
LMK
1355344
Hexachlorobenzene
ND
220
1
02/19/05 0:54
LMK
1355344
Hexachlorobutadiene
ND
220
1
02/19/05 0:54
LMK
1355344
Hexachlorocyclopentadiene, ,
ND
430
1
02/19/05 0:54
LMK
1355344
Hexachloroethane
ND
220
1
02/19/05 0:54
LMK
1355344
lndeno(1,2,3-cd)pyrene
ND
220
1
02/19/05 0:54
LMK
1355344
Isophorone
ND
220
1
02/19/05 0:54
LMK
1355344
Naphthalene
ND
220
1
02/19/05 0:54
LMK
1355344
Nitrobenzene
ND
220
1
02/19/05 0:54
LMK
1355344
N-Nitrosodi-n-propyiamine
ND
220
1
02/19/05 0:54
LMK
1355344
N-Nitrosodiphenylamine
ND
220
1
02/19/05 0:54
LMK
1355344
Pentachlorophend
ND
860
1
02/19/05 0:54
LMK
1355344
Phenanthrene
ND
220
1
02/19/05 0:54
LMK
1355344
Phenol
ND
220
1
02/19/05 0:54
LMK
1355344
Pyrene
ND
220
1
02/19/05 0:54
LMK
1355344
2-Methyiphenol
ND
220
1
02/19/05 0:54
LMK
1355344
m,p-Cresols
ND
220
1
02/19/05 0:54
LMK
1355344
Surr: 2,4,6-Tribromophenol
89.5
% 14.3-114
1
02/19/05 0:54
LMK
1355344
Surr: 2-Fluorobiphenyl
67.9
% 36.6-109
1
02/19/05 0:54
LMK
1355344
Surr: 2-Fluorophenol
75.1
% 30.9-91
1
02/19105 0:54
LMK
1355344
Surr: 4-Terphenyl-d14
75.2
% 51.1-124
1
02/19/05 0:54
LMK
1355344
Surr: Nitrobenzene-d5
64.1
% 33.7-97.2
1
02/19/05 0:54
LMK
1355344
Surr: Phenol-d5
73.3
% 34.5-94.6
1
02/19/05 0:54
LMK
1355344
Prep Method Prep Date
-Dat
SW3550B 02/09/2005 16:39
EEgInitials Pre® Factor
RDH 1.00
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:28 PM

ilk ''g°4141Y
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-4 15'
Collected: 02/07/2005 13:15 SPL Sample ID: 05020306-04
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result Rep.Limit
Dil. Factor QUAL Date Analyzed Analyst
Seq. #
VOLATILE ORGANICS METHOD 8260B +MTBE
MCL SW8260B Units• ug/Kg-dry
1, 1, 1 -Trichloroethane
ND
4.9
1 02/15/05 20:58 GJH
1350187
1, 1,2,2-Tetrachloroethane
ND
4.9
1 02/15/05 20:58 GJH
1350187
1, 1,2-Trichloroethane
ND
4.9
1 02/15/05 20:58 GJH
1350187
1,1-Dichloroethane
ND
4.9
1 02/15/05 20:58 GJH
1350187
1, 1-Dichloroethene
ND
4.9
1 02/15/05 20:58 GJH
1350187
1,2-Dichloroethane
ND
4.9
1 02/15/05 20:58 GJH
1350187
1,2-Dichloropropane
ND
4.9
1 02/15/05 20:58 GJH
1350187
2-Butanone
ND
20
1 02/15/05 20:58 GJH
1350187
2-Hexanone
ND
9.9
1 02/15/05 20:58 GJH
1350187
4-Methyl-2-pentanone
ND
9.9
1 02/15/05 20:58 GJH
1350187
Acetone
ND
99
1 02/15/05 20:58 GJH
1350187
Benzene
ND
4.9
1 02/15/05 20:58 GJH
1350187
Bromodichloromethane
ND
4.9
1 02/15/05 20:58 GJH
1350187-
Bromoform
ND
4.9
1 02/15/05 20:58 GJH
1350187
Bromomethane
ND
9.9
1 02/15/05 20:58 GJH
1350187
Carbon disulfide
ND
4.9
1 02/15/05 20:58 GJH
1350187
Carbon tetrachloride
ND
4.9
1 02/15/05 20:58 GJH
1350187
Chlorobenzene
ND
4.9
1 02/15/05 20:58 GJH
1350187
Chloroethane
ND
9.9
1 02/15/05 20:58 GJH
1350187
Chloroform
ND
4.9
1 02/15/05 20:58 GJH
1350187
Chloromethane
ND
4.9
1 02/15/05 20:58 GJH
1350187
cis- 1, 3-Dichloropropene
ND
4.9
1 02/15/05 20:58 GJH
1350187
- Dibromochloromethane
ND
4.9
1 02/15/05 20:58 GJH
1350187
Ethylbenzene
ND
4.9
1 02/15/05 20:58 GJH
1350187
- Methyl tert-butyl ether
ND
4.9
1 02/15/05 20:58 GJH
1350187
Methylene chloride
ND
9.9
1 02/15/05 20:58 GJH
1350187
- Styrene
ND
4.9
1 02/15/05 20:58 GJH
1350187
Tetrachloroethene
ND
4.9
1 02/15/05 20:58 GJH
1350187
Toluene
ND
4.9
1 02/15/05 20:58 GJH
1350187
trans- 1,3-Dichloropropene
ND
4.9
1 02/15/05 20:58 GJH
1350187
Trichloroethene
19
4.9
1 02/15/05 20:58 GJH
1350187
Trichlorofluoromethane
ND
4.9
1 02/15/05 20:58 GJH
1350187
-Vinyl acetate
ND
9.9
1 02/15/05 20:58 GJH
1350187
Vinyl chloride
ND
9.9
1 02/15/05 20:58 GJH
1350187
cis- 1,2-Dichloroethene
ND
4.9
1 02/15/05 20:58 GJH
1350187
m,p-Xylene
ND
4.9
1 02/15/05 20:58 GJH
1350187
-o-Xyiene
ND
4.9
1 02/15/05 20:58 GJH
1350187
trans- 1, 2-Dichloroethene
ND
4.9
1 02/15/05 20:58 GJH
1350187
1,2-Dichloroethene (total)
ND
4.9
1 02/15/05 20:58 GJH
1350187
Xyi mes,Total
ND
4.9
1 02/15/05 20:58 GJH
1350187
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:28 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-4 15'
Collected: 02/07/2005 13:15
SPL Sample ID: 05020306-04
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Lirnit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Surr: 1,2-Dichloroethane-d4
119
% 66.1-151
1
02/15/05 20:58 GJH
1350187
Surr: 4-Bromofluorobenzene
98.4
% 62-139
1
02/15/05 20.58 GJH
1350187
Surr: Toluene-d8
93.5
% 74.8-118
1
02/15/05 20:58 GJH
1350187
Prey Method PrW
Date
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:29 PM

AV,
LAFAYETTE LABOPATORY
'door
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-5 10'
Collected: 02/07/2005 14:00 SPL Sample ID: 05020306-05
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method Result
Rep.Lirnit
Dil. Factor QUAL Date Analyzed Analyst
Seq. #
EXTRACTABLE PETROLEUM HYDROCARBONS
C11-C22 Aromatics 16 12
C19-C36 Aliphatics ND 18
C9-C18 Ahphatics 140 36
Surr: 2-Bromonaphthalene 53.4 % 40-140
Surr: 2-Fluorobiphenyi 54.4 % 40-140
MCL MA VPH EPH Units: mg/Kg-d!y___
1 02/25/05 0:38 CH
1 02/26/05 23:15 CH ---13-61524
3 02/26/05 19:07 CH
1 02/25/05 0:38 CH
1 02/25/05 0:38 CH --1-3-61537
1361537 .
1361517
1361537
Surr: Chloro-octadecane 127
Sum Chloro-octaclecane 125
Surr: o-Terphenyl 55.8
%
%
%
40-140
40-140
40-140
3 02/26/05 19:07 CH
1 02/26/05 23:15 CH
1 02/25/05 0:38 CH
1361517
1361524
1361537
Prep Method
Prep Date
Prep Initials
Prep Factor
SW35506 _]02/09/2005
18:29
CLT
1.00
PERCENT MOISTURE
Percent Moisture 17
-
0.1
MCL D2216 Units: wt%
1 02/09/05 15:55 CAM
1-343949
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:30 PM

ZLAFAYETTE
—Ad
LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-5 10'
Collected: 02/07/2005 14:00
SPL Sample ID: 05020306-05
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
SEMIVOLATILE ORGANICS
BY METHOD 8270C
MCL SW8270C
Units: ug/Kg-dry
1,2,4-Trichlorobenzene
ND
200
1
02/19/05 1:26
LMK
1355345
1,2-Dichlorobenzene
ND
200
1
02/19/051:26
LMK
1355345
1,2-Diphenyihydrazine
ND
200
1
02/19/05 1:26
LMK
1355345
1,3-Dichlorobenzene
ND
200
1
02/19/05 1:26
LMK
1355345
1,4-Dichlorobenzene
ND
200
1
02/19/05 1:26
LMK
1355345
2,4,5-Tdchlorophenol
ND
200
1
02/19/05 1:26
LMK
1355345
2,4,6-Trichlorophenol
ND
200
1
02/19/05 1:26
LMK
1355345
2,4-Dichlorophenol
ND
200
1
02/19/05 1:26
LMK
1355345
2,4-Dimethyl phenol
ND
200
1
02/19/05 1:26
LMK
1355345
2,4-Dinitrophenol
ND
800
1
02/19/05 1:26
LMK
1355345
2,4-Dinitrotoluene
ND
200
1
02/19/05 1:26
LMK
1355345
2,6-Dinitrotoluene
ND
200
1
02/19/05 1:26
LMK
1355345
2-Chloronaphthalene
ND
200
1
02/19/05 1:26
LMK
1355345
2-Chlorophenol
ND
200
1
02/19/05 1:26
LMK
1355345
2-Methyinaphthalene
2700
200
1
02/19/05 1:26
LMK
1355345
2-Nitroaniline
ND
400
1
02/19/05 1:26
LMK
1355345
2-Nitrophenol
ND
200
1
02/19/05 1:26
LMK
1355345
3,3'-Dichlorobenzidine
ND
200
1
02/19/05 1:26
LMK
1355345
3-Nitroaniline
ND
400
1
02/19/05 1:26
LMK
1355345
4,6-Dinitro-2-m etho phenol
ND
800
1
02/19/05 1:26
LMK
1355345
4-Bromophenyl phenyl ether
ND
200
1
02/19/05 1:26
LMK
1355345
4-Chloro-3-methophenol
ND
200
1
02/19/05 1:26
LMK
1355345
4-Chloroaniline
ND
200
1
02/19/05 1:26
LMK
1355345
4-Chlorophenyi phenyl ether
ND
200
1
02/19/05 1:26
LMK
1355345
4-Nitroaniline
ND
400
1
02/19/05 1:26
LMK
1355345
4-Nitrophenol
ND
800
1
02/19/05 1:26
LMK
1355345
Acenaphthene
ND
200
1
02/19/05 1:26
LMK
1355345
Acenaphthyiene
ND
200
1
02/19/05 1:26
LMK
1355345
Aniline
ND
200
1
02/19/05 1:26
LMK
1355345
Anthracene
ND
200
1
02/19/05 1:26
LMK
1355345
Benz(a)anthracene
ND
200
1
02/19/05 1:26
LMK
1355345
Benzo(a)pyrene
ND
200
1
02/19/05 1:26
LMK
1355345
Benzo(b)fluor.anthene
ND
200
1
02/19/05 1:26
LMK
1355345
Benzo(g,h,i)peryiene
ND
200
1
02/19/051.26
LMK
1355345
Benzo(k)fl uoran then e
ND
200
1
02/19/05 1:26
LMK
1355345
Benzoic acid
ND
820
1
02/19/05 1:26
LMK
1355345
Benzyl alcohol
ND
200
1
02/19/05 1:26
LMK
1355345
Bis(2-chloroeth oxy)m ethane
ND
200
1
02/19/05 1:26
LMK
1355345
Bis(2-chloroethyi)ether
ND
200
1
02/19105 1:26
LMK
1355345
Bis(2-chloroisopropo)ether
ND
200
1
02/19/05 1:26
LMK
1355345
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:30 PM

R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-5 10'
Collected: 02/07/2005 14:00
SPL Sample ID: 05020306-05
Site.:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Bis(2-ethylhexyi)phthalate
ND
200
1
02/19/05 1:26 LMK
1355345
Butyl benzo phthalate
ND
200
1
02/19/05 1:26 LMK
1355345
Carbazole
ND
200
1
02/19/05 1:26 LMK
1355345
Chrysene
ND
200
1
02/19/05 1:26 LMK
1355345
Dibenz(a,h)anthracene
ND
200
1
02/19/05 1:26 LMK
1355345
Dibenzofuran
ND
200
1
02/19/05 1:26 LMK
1355345
Diethyl phthalate
ND
200
1
02/19/05 1:26 LMK
1355345
Dimethyl phthalate
ND
200
1
02/19/05 1:26 LMK
1355345
Di-n-butyl phthalate
ND
200
1
02/19/05 1:26 LMK
1355345
Di-n-octyl phthalate
ND
200
1
02/19/05 1:26 LMK
1355345
Ruoranthene
ND
200
1
02/19/05 1:26 LMK
1355345
Fluorene
ND
200
1
02/19/05 1:26 LMK
1355345
Hexachlorobenzene
ND
200
1
02/19/05 1:26 LMK
1355345
Hexachlorobutadiene
ND
200
1
02/19/05 1:26 LMK
1355345
Hexachlorocyclopentadiene
ND
400
1
02/19/05 1:26 LMK
1355345
Hexachloroethane
ND
200
1
02/19/05 1:26 LMK
1355345
Indeno(1,2,3-cd)pyrene
ND
200
1
02/19/05 1:26 LMK
1355345
lsophorone
ND
200
1
02/19105 1:26 LMK
1355345
Naphthalene
6600
1000
5
02/21/05 18,50 MKM
1356138
Nitrobenzene
ND
200
1
02/19/05 1:26 LMK
1355345
N-Nitrosodi-n-propoamine
ND
200
1
02/19/05 1:26 LMK
1355345
N-Nitrosodiphenylamine
ND
200
1
02/19/05 1:26 LMK
1355345
Pentachlorophenol
ND
800
1
02/19/05 1:26 LMK
1355345
Phenanthrene
ND
200
1
02/19/05 1:26 LMK
1355345
Phenol
ND
200
1
02/19/05 1:26 LMK
1355345
Pyrene
ND
200
1
02/19/05 1:26 LMK
1355345
2-Methylphenol
ND
200
1
02/19/05 1:26 LMK
1355345
m,p-Cresols
ND
200
1
02/19/05 1:26 LMK
1355345
Surr: 2,4,6-Tribromophenol
106
% 14.3-114
5
02/21/05 18:50 MKM
1356138
Surr: 2,4,6-Tribromophenol
114
% 14.3-114
1
02/19/05 1:26 LMK
1355345
Surr: 2-Fluorobipheny�l
99.9
% 36.6-109
5
02/21/05 18:50 MKM
1356138
Surr: 2-Fluorobiphenyi
87.2
% 36.6-109
1
02/19/05 1:26 LMK
1355345
Surr: 2-Fluorophenol
118
% 30.9-91
1
02/19/05 1:26 LMK
1355345
Surr: 2-Fluorophenol
111
% 30.9-91
5 *
02/21/05 18:50 MKM
1356138
Surr: 4-Terphenyl-d14
73.3
% 51.1-124
1
02/19/05 1:26 LMK
1355345
S urr: 4-T erp henyl -d 14
92.9
% 51.1-124
5
02/21/05 18:50 MKM
1356138
Surr: Nitrobenzene-d5
82.2
% 33.7-97.2
1
02/19/05 1:26 LMK
1355345
Surr: Nitrobenzene-d5
114
% 33.7-97.2
5 *
02/21/05 18:50 MKM
1356138
Surr: Phenol-d5
85.7
% 34.5-94.6
5
02/21/05 18:50 MKM
1356138
Surr: Phenol-d5
74.8
% 34.5-94.6
1
02/19/05 1:26 LMK
1355345
Qualifiers: ND/L) - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference -
2/2812005 5:05:31 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-5 10' Collected: 02/07/2005 14:00 SPL Sample ID: 05020306-05
Analyses/Method
Site: GREYHOUND TERM INAL-RALEIGH
Result Rep.1-imit Dil. Factor QUAL Date Analyzed Analyst Seq. #
Prep Method
Prgk Date
lPrep Initials
Prep Factor
SW3550B
02/09/2005 16:39
JRDH
1.00
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank 0 - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/2812005 5:05:31 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-5 10'
Collected: 02/07/2005 14:00
SPL Sample ID: 05020306-05
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
VOLATILE ORGANICS METHOD 8260B +MTBE
MCL SW8260B
Units• ug/Kg-dry
1, 1, 1 -Trichloroethane
N D
240
50
02/16/05 16:23 GJH
135398-1
1, 1,2,2-Tetrachloroethane
ND
240
50
02/16/05 16:23 GJH
1353981
1, 1,2-Trichloroethane
ND
240
50
02/16/05 16:23 GJH
1353981
1,1-Dichloroethane
ND
240
50
02/16/05 16:23 GJH
1353981
1,1-Dichloroethene
ND
240
50
02/16/05 16:23 GJH
1353981
1,2-Dichloroethane
ND
240
50
02/16/05 16:23 GJH
1353981
1,2-Dichloropropane
ND
240
50
02/16/05 16:23 GJH
1353981
2-Butanone
ND
950
50
02/16/05 16:23 GJH
1353981
2-Hexanone
ND
470
50
02/16/05 16:23 GJH
1353981
4-Methyl-2-penta none
ND
470
50
02/16/05 16:23 GJH
1353981
Acetone
ND
4700
50
02/16/05 16:23 GJH
1353981
Benzene
ND
240
50
02/16/05 16:23 GJH
1353981
Bromodichloromethane
ND
240
50
02/16/05 16:23 GJH
1353981
Bromoform
ND
240
50
02/16/05 16:23 GJH
1353981
Bromomethane
ND
470
50
02/16/05 16:23 GJH
1353981
Carbon disulfide
ND
240
50
02/16/05 16:23 GJH
1353981
Carbon tetrachloride
ND
240
50
02/16/05 16:23 GJH
1353981
Chlorobenzene
450
240
50
02/16/05 16:23 GJH
1353981
Chloroethane
ND
470
50
02/16/05 16:23 GJH
1353981
Chloroform
ND
240
50
02/16/05 16:23 GJH
1353981
Chloromethane
ND
240
50
02/16/05 16:23 GJH
1353981
cis- 1,3-Dichloropropene
ND
240
50
02/16/05 16:23 GJH
1353981
Dibromochloromethane
ND
240
50
02/16/05 16:23 GJH
1353981
Ethylbenzene
2200
240
50
0 2/16/05 16:23 GJH
1353981
Methyl tert-butyl ether
ND
240
50
02/16/05 16:23 GJH
1353981
Methylene chloride
ND
470
50
02/16/05 16:23 GJH
1353981
Styrene
ND
240
50
02/16/05 16:23 GJH
1353981
Tetrachloroethene
ND
240
50
02/16/05 16:23 GJH
1353981
Toluene
ND
240
50
02/16/05 16:23 GJH
1353981
trans- 1,3-Di chloropropene
ND
240
50
02/16/05 16:23 GJH
1353981
Trichloroethene
ND
240
50
02/16/05 16:23 GJH
1353981
Trichlorofluoromethane
ND
240
50
02/16/05 16:23 GJH
1353981
Vinyl acetate
ND
470
50
02/16/05 16:23 GJH
1353981
Vinyl chloride
ND
470
50
02/16/05,16'23 GJH
1353981
cis- 1,2-Dichloroethene
ND
240
50
02/16/05 16:23 GJH
1353981
m,p-Xylene
9400
240
50
02/16/05 16:23 GJH
1353981
o-Xyiene
3900
240
50
02/16/05 16:23 GJH
1353981
trans- 1,2-Dichloroethene
ND
240
50
02/16/05 16:23 GJH
1353981
1,2-Dichloroethene (total)
ND
240
50
02/16/05 16:23 GJH
1353981
Xylenes,Total
13300
240
50
02/16/05 16:23 GJH
1353981
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2128/2005 5:05:32 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-5 10'
Collected: 02/07/2005 14:00
SPL Sample ID: 05020306-05
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Surr: 1,2-Dichloroethane-d4
103
%
66.1-151
50
02/16/05 16:23 GJH
1353981
Surr: 4-Bromofluorobenzene
160
%
62-139
50 MI
02/16/05 16:23 GJH
1353981
Surr: Toluene-d8
102
%
74.8-118
50
02/16/05 16:23 GJH
1353981
Prep Method Prep Date
a Q�
SW5035 02/07/2005 0:00
Pre INtiala Factor
----
GJH 0.79
VOLATILE PETROLEUM HYDROCARBONS
MCL
MA VPH EPH
Units: ug/Kg-dry
C5-C8 Aliphatics
170000
9500
50
02/10/05 17:09 NDG
1347190
C9-C10 Aromatics
230000
28000
1000
02/11/05 16:38 NDG
1349005
C9-C12 Aliphatics
500000
95000
1000
02/11/05 16:38 NDG
1349030
Surr: 1,4-Difluorobenzene
162
%
70-130
50 MI
02/10/05 17:09 NDG
1347190
Surr: 1,4-Difluorobenzene
104
%
70-130
1000
02/11/05 16:38 NDG
1349005
Surr: 1,4-Difluorobenzene
103
%
70-130
1000
02/11/05 16:38 NDG
1349030
Surr: 4-Bromofluorobenzene
2140
%
70-130
50 MI
02/10/05 17:09 NDG
1347190
Surr: 4-Bromofluorobenzene
116
%
70-130
1000
02/11/05 16:38 NDG
1349030
Surr: 4-Bromofluorobenzene
94.5
%
70-130
1000
02/11/05 16:38 NDG
1349005
Prep MgjtQd
RLW DaLe
—Prep Initials
EL Factor
Qp--- A—
SW80158
02/10/2005 0:00
FT
0.79
SW8015B
02/07/2005 0:00
FT
0.79
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:32 PM

Z @
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-6 10'
Collected: 02/07/2005 14:30
SPL Sample ID: 05020306-06
Site: GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor ®UAL
Date Analyzed Analyst
Seq. #
EXTRACTABLE PETROLEUM HYDROCARBONS MCL
MA VPH EPH
Units: mgft-dry
C11-C22 Aromatics
ND
14
1
02/25/05 1:14 CH
1361538
C19-C36 Aliphatics
ND
21
1
02/25/05 1:14 CH
1361503
C9-C18 Aliphatics
ND
14
1
02/25/05 1:14 CH
1361503
Surr: 2-Bromonaphthalene
52.5
%
40-140
1
02/25/05 1:14 CH
1361538
Surr: 2-Fluorobiphenyl
53.7
%
40-140
1
02/25/05 1:14 CH
1361538
Surr: Chloro-octadecane
13.4
%
40-140
1
02/25/05 1:14 CH
1361503
Surr: o-Terphenyl
9.60
%
40-140
1
02/25/05 1:14 CH
1361538
Prep Method JaM Date
ISW35506 102/09/2005 18:26
I Prep Initials I Prep Factor
CLT j1.60
PERCENT MOISTURE
MCL
D2216
Units: wt%
Percent Moisture
29
0.1
1
02/09/05 15:55 CAM
1343948
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
6 - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:33 PM

Apr
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-6 10'
Collected: 02/07/2005 14:30
SPL Sample ID: 05020306-06
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
SEMIVOLATILE ORGANICS
BY METHOD 8270C
MCL SW8270C
Units: ug/Kg-dry
1,2,4-Trichlorobenzene
ND
240
1
02/19/05 1:58
LMK
1355346
1,2-Dichlorobenzene
ND
240
1
02/19/05 1:58
LMK
1355346
1,2-Diphenythydrazine
ND
240
1
02/19/05 1:58
LMK
1355346
ND
240
1
02/19/05 1:58
LMK
1355346
—1,3-Dichlorobenzene
1,4-Dichlorobenzene
ND
240
1
02/19/05 1:58
LMK
1355346
2,4,5-Trichlorophenol
ND
240
1
02/19/05 1:58
LMK
1355346
ND
240
1
02/19/05 1:58
LMK
1355346
—2,4,6-Trichlorophenol
ND
240
1
02/19/05 1:58
LMK
1355346
—2,4-Dichlorophenol
ND
240
1
02/19/05 1:58
LMK
1355346
—2,4-Dimethyiphenol
ND
930
1
02/19/05 1:58
LMK
1355346
—2,4-Dinitrophenol
ND
240
1
02/19/05 1:58
LMK
1355346
—2,4-Dinitrotoluene
ND
240
1
02/19/05 1:58
LMK
1355346
—2,6-Dinitrotoluene
2-ChloronaphthaJene
ND
240
1
02/19/05 1:58
LMK
1355346
ND
240
1
02/19/05 1:58
LMK
1355346
—2-Chlorophenol
2-Methonaphthalene
ND
240
1
02/19/05 1:58
LMK
1355346
2-Nitroaniline
ND
460
1
02/19/05 1:58
LMK
1355346
2-Nitrophenol
ND
240
1
02/19/05 1:58
LMK
1355346
3,3 *-Dichlorobenzidine
ND
240
1
02/19/05 1:58
LMK
1355346
3-Nitroaniline
ND
460
1
02/19/05 1:58
LMK
1355346
ethyl phenol
ND
930
1
02/19/05 1:58
LMK
1355346
—4,6-Dinitro-2-m
phenyl ether
ND
240
1
02/19/05 1:58
LMK
1355346
—4-Bromophenyl
4-Chloro-3-methyiphenol
ND
240
1
02/19/05 1:58
LMK
1355346
4-Chloroaniline
ND
240
1
02/19/05 1:58
LMK
1355346
4-Chlorophenyl phenyl ether
ND
240
1
02/19/05 1:58
LMK
1355346
4-Nitroaniline
ND
460
1
02/19/05 1:58
LMK
1355346
ND
930
1
02/19/05 1:58
LMK
1355346
—4-Nitrophenol
Acenaphthene
ND
240
1
02/19/05 1:58
LMK
1355346
Acenaphthyiene
ND
240
1
02/19/05 1:58
LMK
1355346
Aniline
ND
240
1
02/19/05 1:58
LMK
1355346
Anthracene
ND
240
1
02/19/05 1:58
LMK
1355346
ND
240
1
02/19/05 1:58
LMK
1355346
—Benz(a)anthracene
ND
240
1
02/19/05 1:58
LMK
1355346
—Benzo(a)pyrene
Benzo(b)fluoranthene
ND
240
1
02/19/05 1:58
LMK
1355346
Benzo(g,h,i)peryiene
ND
240
1
02/19/05,-1:58
LMK
1355346
Benzo(k)fluoranthene
ND
240
1
02/19105 1:58
LMK
1355346
Benzoic acid
ND
960
1
02/19/05 1:58
LMK
1355346
Benzyi alcohol
ND
240
1
02/19/05 1:58
LMK
1355346
Bis(2-chloroethoxy)m ethane
ND
240
1
02/19/05 1:58
LMK
1355346
Bis(2-chloroethyi)ether
ND
240
1
02/19/05 1:58
LMK
1355346
Bis (2-chloroi sop ropyl)ether
ND
240
1
02/19/05 1:58
LMK
1355346
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination
D - Surrogate Recovery Unreportable due
MI - Matrix Interference
Limit(MCL)
to Dilution
2/28/2005 5:05:34 PM

R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-6 10'
Collected: 02/07/2005 14:30
SPL Sample ID: 05020306-06
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
Bis(2-ethyihexyl)phthalate
ND
240
1
02/19/05 1:58
LMK
1355346
Butyi benzyi phthalate
ND
240
1
02/19/05 1:58
LMK
1355346
Carbazole
ND
240
1
02/19/05 1:58
LMK
1355346
Chrysene
ND
240
1
02/19/05 1:58
LMK
1355346
Dibenz(a,h)anthracene
ND
240
1
02/19/05 1:58
LMK
1355346
Dibenzofuran
ND
240
1
02/19/05 1:58
LMK
1355346
Diethyl phthalate
ND
240
1
02/19/05 1:58
LMK
1355346
Dimethyl phthalate
ND
240
1
02/19/05 1:58
LMK
1355346
Di-n-butyl phthalate
ND
240
1
02/19/05 1:58
LMK
1355346
Di-n-octyi phthalate
ND
240
1
02/19/05 1:58
LMK
1355346
Fluoranthene
ND
240
1
02/19/05 1:58
LMK
1355346
Fluorene
ND
240
1
02/19/05 1:58
LMK
1355346
Hexachlorobenzene
ND
240
1
02/19/05 1:58
LMK
1355346
Hexachlorobutadiene
ND
240
1
02/19/05 1:58
LMK
1355346
Hexachlorocyclopentadiene,
ND
460
1
02/19/05 1:58
LMK
1355346
Hexachloroethane
ND
240
1
02/19/05 1:58
LMK
1355346
lndeno(1,2,3-cd)pyrene
ND
240
1
02/19/05 1:58
LMK
1355346
Isophorone
ND
240
1
02/19/05 1:58
LMK
1355346
Naphthalene
ND
240
1
02/19/05 1:58
LMK
1355346
Nitrobenzene
ND
240
1
02/19/05 1:58
LMK
1355346
N-Nitrosodi-n-propylamine
ND
240
1
02/19/05 1:58
LMK
1355346
N-Nitrosodiphenylamine
ND
240
1
02/19/05 1:58
LMK
1355346
Pentachlorophenol
ND
930
1
02/19/05 1:58
LMK
1355346
Phenanthrene
ND
240
1
02/19/05 1:58
LMK
1355346
Phenol
ND
240
1
02/19/05 1:58
LMK
1355346
Pyrene
ND
240
1
02/19/05 1:58
LMK
1355346
2-Methophenol
ND
240
1
02/19/05 1:58
LMK
1355346
m,p-Cresols
ND
240
1
02/19/05 1:58
LMK
1355346
Surr: 2,4,6-Tribromophenol
88.0
% 14.3-114
1
02/19/05 1:58
LMK
1355346
Surr: 2-Fluorobiphenyl
67.8
% 36.6-109
1
02/19/05 1:58
LMK
1355346
Surr: 2-Fluorophenol
78.7
% 30.9-91
1
02/19/05 1:58
LMK
1355346
Sum 4-Terphenyl-d14
74.5
% 51.1-124
1
02/19/05 1:58
LMK
1355346
Surr: Nitrobenzene-d5
66.5
% 33.7-97.2
1
02/19/05 1:58
LMK
1355346
Surr: Phenol-d5
76.2
% 34.5-94.6
1
02/19/05 1:58
LMK
1355346
Prep Method PrepDate
SW3550B 102/09/2005 16:39
Prep 1�nifils I Pre r) Factor
IRDH 11.00
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and POL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:34 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-6 10'
Collected: 02/07/2005 14:30
SPL Sample ID: 05020306-06
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
VOLATILE ORGANICS METHOD 8260B +MTBE
MCL SW8260B
Units: ug/Kg-dry
1,1,1-Trichloroethane
ND
6.1
1
02/16/05 17:21 GJH
1353983
1, 1,2,2-Tetrachloroethane
ND
6.1
1
02/16/05 17:21 GJH
1353983
1, 1,2-Trichloroethane
ND
6.1
1
02/16/05 17:21 GJH
1353983
1,1-Dichloroethane
ND
6.1
1
02/16/05 17:21 GJH
1353983
1,1-Dichloroethene
ND
6.1
1
02/16/05 17:21 GJH
1353983
1,2-Dichloroethane
ND
6.1
1
02/16/05 17:21 GJH
1353983
1,2-Dichioropropane
ND
6.1
1
02/16/05 17:21 GJH
1353983
2-Butanone
ND
24
1
02/16/05 17:21 GJH
1353983
2-Hexanone
ND
12
1
02/16/05 17:21 GJH
1353983
4-Methyl-2-pentanone
ND
12
1
02/16/05 17:21 GJH
1353983
Acetone
ND
120
1
02/16/05 17:21 GJH
1353983
Benzene
ND
6.1
1
02/16/05 17:21 GJH
1353983
Bromodichloromethane
ND
6.1
1
02/16/05 17:21 GJH
1353983
Bromoform
ND
6.1
1
02/16/05 17:21 GJH
1353983
Bromomethane
ND
12
1
02/16/05 17:21 GJH
1353983
Carbon disulfide
ND
6.1
1
02/16/05 17:21 GJH
1353983
Carbon tetrachloride
ND
6.1
1
02/16/05 17:21 GJH
1353983
Chlorobenzene
ND
6.1
1
02/16/05 17:21 GJH
1353983
Chloroethane
ND
12
1
02/16/05 17:21 GJH
1353983
Chloroform
ND
6.1
1
02/16/05 17:21 GJH
1353983
Chloromethane
ND
6.1
1
02/16/05 17:21 GJH
1353983
cis- 1,3-Dichloropropene
ND
6.1
1
02/16/05 17:21 GJH
1353983
Dibromochloromethane
ND
6.1
1
02/16/05 17:21 GJH
1353983
Ethyibenzene
ND
6.1
1
02/16/05 17:21 GJH
1353983
Methyl tert-butyl ether
ND
6.1
1
02/16/05 17:21 GJH
1353983
Methylene chloride
ND
12
1
02/16/05 17:21 GJH
1353983
Styrene
ND
6.1
1
02/16/05 17:21 GJH
1353983
Tetrachloroethene
ND
6.1
1
02/16/05 17:21 GJH
1353983
Toluene
ND
6.1
1
02/16/05 17:21 GJH
1353983
trans- 1,3-Dichloropropene
ND
6.1
1
02/16/05 17:21 GJH
1353983
Trichloroethene
6.6
6.1
1
02/16/05 17:21 GJH
1353983
Trichlorofluoromethane
ND
6.1
1
02/16/05 17:21 GJH
1353983
Vinyl acetate
ND
12
1
02/16/05 17:21 GJH
1353983
Vinyl chloride
ND
12
1
02/16/05 17:21 GJH
1353983
cis- 1,2-Dichloroethene
ND
6.1
1
02/16/05 17:21 GJH
1353983
m,p-Xyiene
ND
6.1
1
02/16/05 17:21 GJH
1353983
o-Xyiene
ND
6.1
1
02/16/05 17:21 GJH
1353983
trans- 1,2-Dichloroethene
ND
6.1
1
02/16/05 17:21 GJH
1353983
1,2-Dichloroethene (total)
ND.
6.1
1
02/16/05 17:21 GJH
1353983
Xylenes,Total
ND
6.1
1
02/16/05 17:21 GJH
1353983
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/2812005 5:05.35 PM

'40or LAFAYETTE LABORATORY
Av 500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
Client Sample ID:GP-6 10'
Collected: 02/07/2005 14:30
SPL Sample ID: 05020306-06
Site: GREYHOUND TERMINAL- LEIGH
.Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Surr: 1,2-Dichloroethane-&
108
%
66.1-151
1
02/16/05 17:21 GJH
1353983
Surr: 4-Bromofluorobenzene
99.0
%
62-139
1
02/16/05 17:21 GJH
1353983
Surr: Toluene-d8
94.4
%
74.8-118
1
02/16/05 17:21 GJH
1353983
Prep Method Pre Date
,p
SW5035 02/07/2005 0:00
ni Ui Pre
a[Wj__ Is Prep Factor
GJH 0.87 1
VOLATILE PETROLEUM HYDROCARBONS
MCL
MA VPH EPH
Units: ug/Kg-dry
C5-C8 Aliphatics
ND
12000
50
02/10/05 17:38 NDG
1347191
C9-C 10 Aromatics
1900
1800
50
02/11/05 17:07 NDG
1349006
C9-C12AIiphatics
ND
6200
50
02/11/05 17:07 NDG
1349034
Surr: 1,4-Difluorobenzene
104
%
70-130
50
02/11/05 17:07 NDG
1349034
Surr: 1,4-Difluorobenzene
102
%
70-130
50
02/11/05 17:07 NDG
1349006
Surr: 1,4-Difluorobenzene
105
%
70-130
50
02/10/05 17:38 NDG
1347191
Surr: 4-Bromofluorobenzene
99.3
%
70-130
50
02/11/05 17:07 NDG
1349034
Surr: 4-Brornafluorobenzehe
92.4
%
70-130
50
02/11/05 17:07 NDG
1349006
Surr: 4-Bromofluorobenzene
102
%
70-130
50
02/10/05 17:38 NDG
1347191
Prep Method Prep Date
SW8015B 02/10/2005 0:00
SW8015B 02/07/2005 0:00
E[WInitials _Prep Factor
FT 0.87
FT 0.87
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:35 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-7 15'
Collected: 02/07/2005 15:00
SPL Sample ID: 05020306-07
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
EXTRACTABLE PETROLEUM HYDROCARBONS MCL
MA VPH EPH
Units: mg/Kg-dry
C1 1-C22 Aromatics
18
12
1
02/25/05 1:50 CH
1361539
C19-C36 Aliphatics
ND
18
1
02/25/05 1:50 CH
1361504
C9-C18 AJiphabcs
140
24
2
02/26/05 19:42 CH
1361518
Sum 2-Bromonaphthalene
51.3
%
40-140
1
02/25/05 1:50 CH
1361539
Surr: 2-Fluorobiphenyi
52.9
%
40-140
1
02/25/05 1:50 CH
1361539
Surr: Chloro-octadecane
107
%
40-140
2
02/26/05 19:42 CH
1361518
Surr: Chloro-octadecane
92.6
%
40-140
1
02/25/05 1:50 CH
1361504
Surr: o-Terphenyt
50.0
%
40-140
1
02/25/05 1:50 CH
1361539
Prep MethodPrep Date
S 3550B 02/09/2005 18:29
Prep Initials Pre Factor
CLT 1.00
PERCENT MOISTURE
MCL
D2216
Units: wt%
Percent Moisture
18
0.1
1
02/09/05 15:55 CAM
1343947
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:36 PM

'40or
'M Ana AMA—
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
(337) 2374775
Client Sample ID:GP-7 15'
Collected: 02/07/2005 15:00
SPL Sample ID: 05020306-07
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
.SEMIVOLATILE ORGANICS
BY METHOD 8270C
MCL SW8270C
Units: ug/Kg-dry
1,2,4-Trichlorobenzene
ND
210
1
02/19/05 2:30 LMK
1355347
1,2-Dichlorobenzene
ND
210
1
02/19/05 2:30 LMK
1355347
1,2-Diphenythydrazine
ND
210
1
02/19/05 2:30 LMK
1355347
1,3-Dichlorobenzene
ND
210
1
02/19/05 2:30 LMK
1355347
1,4-Dichlorobenzene
ND
210
1
02/19/05 2:30 LMK
1355347
2,4,5-Tdchlorophenol
ND
210
1
02/19/05 2:30 LMK
1355347
2,4,6-Trichlorophenol
ND
210
1
02/19/05 2:30 LMK
1355347
2,4-Dichlorophenol
ND
210
1
02/19/05 2:30 LMK
1355347
2,4-Dimethylphend
ND
210
1
02/19/05 2:30 LMK
1355347
2,4-Dinitrophenol
ND
800
1
02/19/05 2:30 LMK
1355347
2,4-Dinitrobluene
ND
210
1
02/19/05 2:30 LMK
1355347
2,6-Dinitrotoluene
ND
210
1
02/19/05 2:30 LMK
1355347
2-Chloronaphthalene
ND
210
1
02/19/05 2:30 LMK
1355347
2-Chlorophenol
ND
210
1
02/19/05 2:30 LMK
1355347
2-Methonaphthalene
2800
210
1
02/19/05 2:30 LMK
1355347
2-Nitroaniline
ND
400
1
02/19/05 2:30 LMK
1355347
2-Nitrophenol
ND
210
1
02/19/05 2:30 LMK
1355347
3,3'-D ichlorobenzi dine
ND
210
1
02/19/05 2:30 LMK
1355347
3-Nitroaniline
ND
400
1
02/19/05 2:30 LMK
1355347
4,6-Di nitro-2-m et hyi phenol
ND
800
1
02/19105 2:30 LMK
1355347
4-Bromophenyi phenyl ether
ND
210
1
02/19/05 2:30 LMK
1355347
4-Chloro-3-methyiphenol
ND
210
1
02/19/05 2:30 LMK
1355347
4-Chloroaniline
ND
210
1
02/19/05 2:30 LMK
1355347
4-Chlorophenyl phenyl ether
ND
210
1
02/19/05 2:30 LMK
1355347
4-Nitroaniline
ND
400
1
02/19/05 2:30 LMK
1355347
4-Nitrophenol
ND
800
1
02/19/05 2:30 LMK
1355347
Acenaphthene
ND
210
1
02/19/05 2:30 LMK
1355347
Acenaphthylene
ND
210
1
02/19/05 2:30 LMK
1355347
Aniline
ND
210
1
02/19/05 2:30 LMK
1355347
Anthracene
ND
210
1
02/19/05 2:30 LMK
1355347
Benz(a)anthracene
ND
210
1
02/19/05 2:30 LMK
1355347
Benzo(a)pyrene
ND
210
1
02/19/05 2:30 LMK
1355347
Benzo(b)fluoranthene
ND
210
1
02/19/05 2:30 LMK
1355347
Benzo(g,h,i)peryiene
ND
210
1
02/19/05 2:30 LMK
1355347
Benzo(k)fluoranthene
ND
210
1
02/19/05 2:30 LMK
1355347
Benzoic acid
ND
830
1
02/19/05 2:30 LMK
1355347
Benzyl alcohol
ND
210
1
02/19/05 2:30 LMK
1355347
B is (2-chloroeth oxy)m ethane
ND
210
1
02/19/05 2:30 LMK
1355347
Bis(2-chloroethyl)ether
ND
210
1
02/19/05 2:30 LMK
1355347
Bis(2-chloroisopropyl)ether
ND
210
1
02/19/05 2:30 LMK
1355347
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:37 PM

o
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-7 15'
Collected: 02/07/2005 15:00
SPL Sample ID: 05020306-07
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
Bis(2-ethylhexyl)phthalate
ND
210
1
02/19/05 2:30
LMK
1355347
Butyl benzy! phthalate
ND
210
1
02/19/05 2:30
LMK
1355347
Carbazole
ND
210
1
02/19/05 2:30
LMK
1355347
Chrysene
ND
210
1
02/19/05 2:30
LMK
1355347
Dibenz(a,h)anthracene
ND
210
1
02/19/05 2:30
LMK
1355347
Dibenzofuran
ND
210
1
02/19/05 2:30
LMK
1355347
Diethyl phthalate
ND
210
1
02/19/05 2:30
LMK
1355347
Dimethyl phthalate
ND
210
1
02/19/05 2:30
LMK
1355347
Di-n-butyl phthalate
ND
210
1
02/19/05 2:30
LMK
1355347
Di-n-octyi phthalate
ND
210
1
02/19/05 2:30
LMK
1355347
Fluoranthene
ND
210
1
02/19/05 2:30
LMK
1355347
Fluorene
ND
210
1
02/19/05 2:30
LMK
1355347
Hexachlorobenzene
ND
210
1
02/19/05 2:30
LMK
1355347
Hexachlorobutadiene
ND
210
1
02/19/05 2:30
LMK
1355347
Hexachlorocyclopentadielne
ND
400
1
02/19/05 2:30
LMK
1355347
Hexachloroethane
ND
210
1
02/19/05 2:30
LMK
1355347
lndeno(1,2,3-cd)pyrene
ND
210
1
02/19/05 2:30
LMK
1355347
Isophorone
ND
210
1
02/19/05 2:30
LMK
1355347
Naphthalene
4100
210
1
02/19/05 2:30
LMK
1355347
Nitrobenzene
ND
210
1
02/19/05 2:30
LMK
1355347
N-Nitrosodi-n-propylamine
ND
210
1
02/19/05 2:30
LMK
1355347
N-Nitrosodiphenyiamine
ND
210
1
02/19/05 2:30
LMK
1355347
Pentachlorophenol
ND
800
1
02/19/05 2:30
LMK
1355347
Phenanthrene
ND
210
1
02/19/05 2:30
LMK
1355347
Phenol
ND
210
1
02/19/05 2:30
LMK
1355347
Pyrene
ND
210
1
02/19/05 2:30
LMK
1355347
2-Methophenol
ND
210
1
02/19/05 2:30
LMK
1355347
m,p-Cresols
ND
210
1
02/19/05 2:30
LMK
1355347
Surr: 2,4,6-Thbromophenol
91.7
% 14.3-114
1
02/19/05 2:30
LMK
1355347
Surr: 2-Fluorobiphenyl
69.1
% 36.6-109
1
02/19/05 2:30
LMK
1355347
Surr: 2-Fluorophenol
82.9
% 30.9-91
1
02/19/05 2:30
LMK
1355347
Surr: 4-Terphen"14
72.3
% 51.1-124
1
02/19/05 2:30
LMK
1355347
Surr: Nitrobenzene-d5
77.3
% 33.7-97.2
1
02/19/05 2:30
LMK
1355347
Surr: Phenol-d5
70.2
% 34.5-94.6
1
02/19/05 2:30
LMK
1355347
Prep Method Prep Date
SW3550B _A2/09/2005 16.39
Em-Lnitiala Prep Factor
1 RDH 11.00
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination
D —Surrogate Recovery Unreportable due
MI - Matrix Interference
Limit(MCL)
to Dilution
2/28/2005 5:05:37 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-7 15'
Collected: 02/07/2005 15:00
SPL Sample ID: 05020306-07
Site:
GREYHOUND TERM I NAL-RALEIG H
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
VOLATILE ORGANICS METHOD 8260B +MTBE
MCL SW8260B
Units: ug/Kg-dry
1, 1, 1 -Trichloroethane
ND
530
100
02/16/05 18:01 MHW
1352757
1, 1,2,2-Tetrachloroethane
ND
530
100
02/16/05 18:01 MHW
1352757
1, 1,2-Trichloroethane
ND
530
100
02/16/05 18:01 MHW
1352757
1, 1 -Dichloroethane
ND
530
100
02/16/05 18:01 MHW
1352757
1,1-Dichloroethene
ND
530
100
02/16/05 18:01 MHW
1352757
1,2-Dichloroethane
ND
530
100
02/16/05 18:01 MHW
1352757
1,2-Dichloropropane
ND
530
100
02/16/05 18:01 MHW
1352757
2-Butanone
ND
2100
100
02/16/05 18:01 MHW
1352757
2-Hexanone
ND
1100
100
02/16/05 18:01 MHW
1352757
4- Methyl-2-penta none
ND
1100
100
02/16/05 18:01 MHW
1352757
Acetone
ND
11000
100
02/16/05 18:01 MHW
1352757
Benzene
ND
530
100
02/16/05 18:01 MHW
1352757
Bromodichloromethane
ND
530
100
02/16/05 18:01 MHW
1352757
Bromoform
ND
530
100
02/16/05 18:01 MHW
1352757
Bromomethane
ND
1100
100
02/16/05 18:01 MHW
1352757
Carbon disulfide
ND
530
100
02/16/05 18:01 MHW
1352757
Carbon tetrachloride
ND
530
100
02/16/05 18:01 MHW
1352757
Chlorobenzene
ND
530
100
02/16/05 18:01 MHW
1352757
Chloroethane
ND
1100
100
02/16/05 18:01 MHW
1352757
Chloroform
ND
530
100
02/16/05 18:01 MHW
1352757
Chloromethane
ND
530
100
02/16/05 18:01 MHW
1352757
cis- 1, 3-Dichloropropene
ND
530
100
02/16/05 18:01 MHW
1352757
Dibromochloromethane
ND
530
100
02/16/05 18:01 MHW
1352757
Ethylbenzene
8500
530
100
02/16/05 18:01 MHW
1352757
Methyi tert-butyl ether
ND
530
100
02/16/05 18:01 MHW
1352757
Methylene chloride
ND
1100
100
02/16/05 18:01 MHW
1352757
Styrene
ND
530
100
02/16/05 18:01 MHW
1352757
Tetrachloroethene
ND
530
100
02/16/05 18:01 MHW
1352757
Toluene
5100
530
100
02/16/05 18:01 MHW
1352757
trans- 1, 3-Dichloropropene
ND
530
100
02/16/05 18:01 MHW
1352757
Trichloroethene
ND
530
100
02/16/05 18:01 MHW
1352757
Trichlorofluoromethane
ND
530
100
02/16/05 18:01 MHW
1352757
Vinyl acetate
ND
1100
100
02/16/05 18:01 MHW
1352757
Vinyl chloride
ND
1100
100
02/16/05 18:01 MHW
1352757
cis- 1,2-Dichloroethene
ND
530
100
02/16/05 18:01 MHW
1352757
m,p-Xyiene
30000
530
100
02/16/05 18:01 MHW
1352757
o-Xylene
13000
530
100
02/16/05 18:01 MHW
1352757
trans- 1,2-Di chloroethene
ND
530
100
02/16/05 18:01 MHW
1352757
1,2-Dichloroethene (total)
ND
530
100
02/16/05 18:01 MHW
1352757
Xyienes,Total
43000
530
100
02/16/05 18:01 MHW
1352757
Qualifiers: ND/LI - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:38 PM

Air
AMAC'no UR �n.
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-7 15'
Collected: 02/07/2005 15:00
SPL Sample ID: 05020306-07
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Surr: 1,2-Dichloroethane-d4 98.5
%
66.1-151
100
02/16/05 18:01 MHW
1352757
Surr: 4-Bromofluorobenzene 102
%
62-139
100
02/16/05 18:01 MHW
1352757
Surr: Toluene-d8 94.3
%
74.8-118
100
02/16/05 18:01 MHW
1352757
Prep Method Prep Date
SW5035 102/07/2005 0:00
Pre g Initipl.s Prep Factor
FT 0.87
VOLATILE PETROLEUM HYDROCARBONS
MCL
MA VPH EPH
Units: ug/Kg-dry
C5-C8 Aliphatics 210000
21000
100
02/10/05 18:06 NDG
1347192
C9-C 10 Aromatics 250000
32000
1000
02/11/05 17:54 NDG
1349007
C9-C 12 Aliphatics 520000
110000
1000
02/11/05 17:54 NDG
1349037
Surr: 1,4-Difluorobenzene 110
%
70-130
1000
02/11/05 17:54 NDG
1349037
Surr: 1,4-Difluorobenzene 102
%
70-130
1000
02/11/05 17:54 NDG
1349007
Surr: 1,4-Difluorobenzene 174
%
70-130
100 MI
02/10/05 18:06 NDG e
1347192
Surr: 4-Bromafluorobenzene 118
%
70-130
1000
02/11/05 17:54 NDG
1349037
Surr: 4-Bromofluorobenz:e"ne ill
%
70-130
1000
02/11/05 17:54 NDG
1349007
Surr: 4-Bromofluorobenzene 310
%
70-130
100 MI
02/10/05 18:06 NDG
1347192
PromoMethodELW DaLe
SW801513' 02/10/2005 0:00
SW80158 02107/2005 0:00
Prep Initials Prep Factor
FT 0.87
FT 0.87
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportabie due to Dilution
* - Surrogate Recovery Outside Advisable OC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:38 PM

Client Sample ID:GP-8 15'
Collected: 02/07/2005 15:30
SPL Sample ID: 05020306-08
Site: GREYHOUND TERM INAL-RALEIGH
Analyses/Method Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
EXTRACTABLE PETROLEUM HYDROCARBONS MCL
MA VPH EPH
Units: mg/Kg-dry
C11-C22 Aromatics
13
11
1
02/25/05 2:26 CH
1361540
C19-C36 Aliphatics
ND
16
1
02/25/05 2:26 CH
1361505
C9-C18 Aliphafics
ND
11
1
02/25/05 2:26 CH
1361505
Surr- 2-Bromonaphthalene
46.0
% 40-140
1
02/25/05 2:26 CH
1361540
Surr: 2-Fluorobipheny!
45.0
% 40-140
1
02/25/05 2:26 CH
1361540
Surr: Chloro-octaclecane
84.0
% 40-140
1
02/25/05 2:26 CH
1361505
Surr: o-Terphenyl
61.1
% 40-140
1
02/25/05 2:26 CH
1361540
Prep Method Prep Date
FS-W35506 102/09/2005 18:29
ELep initials ELW Factor
CLT 1.00
PERCENT MOISTURE
MCL
D2216
Units: wt%
Percent Moisture
5.9
0.1
1
02/09/05 15:55 CAM
1343946
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:39 PM

PW7
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-8 15'
Collected: 02/07/2005 15:30
SPL Sample ID: 05020306-08
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dill. Factor QUAL
Date Analyzed Analyst
Seq. #
-SEMIVOLATILE ORGANICS
BY METHOD 8270C
MCL SW8270C
Units• ug/Kg-dry
1,2,4-Trichlorobenzene
ND
180
1
02/19/05 3:03 LMK
1355348
1,2-Dichlorobenzene
ND
180
1
02/19/05 3:03 LMK
1355348
1,2-Diphenyihydrazine
ND
180
1
02/19/05 3:03 LMK
1355348
1,3-Dichlorobenzene
ND
180
1
02/19/05 3:03 LMK
1355348
1,4-Dichlorobenzene
ND
180
1
02/19/05 3:03 LMK
1355348
2,4,5-Trichlorophenol
ND
180
1
02/19/05 3:03 LMK
1355348
2,4,6-Trichlorophenol
ND
180
1
02/19/05 3:03 LMK
1355348
2,4-Dichlorophenol
ND
180
1
02/19/05 3:03 LMK
1355348
2,4-Dimethophenol
ND
180
1
02/19/05 3:03 LMK
1355348
2,4-Dinitrophenol
ND
700
1
02/19/05 3:03 LMK
1355348
2,4-Dinitrotoluene
ND
180
1
02/19/05 3:03 LMK
1355348
2,6-Dinitrotoluene
ND
180
1
02/19/05 3:03 LMK
1355348
2-Chloronaphthadene
ND
180
1
02/19/05 3:03 LMK
1355348
2-Chlorophenol
ND
180
1
02/19/05 3:03 LMK
1355348
2-Methonaphthalene
ND
180
1
02/19/05 3:03 LMK
1355348
2-Nitroaniline
ND
350
1
02/19/05 3:03 LMK
1355348
2-Nitrophenol
ND
180
1
02/19/05 3:03 LMK
1355348
3,3'-D ich lorobe nzi dine
ND
180
1
02/19/05 3:03 LMK
1355348
3-Nitroaniline
ND
350
1
02/19/05 3:03 LMK
1355348
4,6-Dinitro-2-m ethyl phenol
ND
700
1
02/19/05 3:03 LMK
1355348
4-Bromophenyl phenyi ether
ND
180
1
02/19/05 3:03 LMK
1355348
4-Chloro-3-methyl phenol
ND
180
1
02/19/05 3:03 LMK
1355348
4-Chloroaniline
ND
180
1
02/19/05 3:03 LMK
1355348
4-Chlorophenyl phenyl ether
ND
180
1
02/19/05 3:03 LMK
1355348
4-Nitroaniline
ND
350
1
02/19/05 3:03 LMK
1355348
4-Nitrophenol
ND
700
1
02/19/05 3:03 LMK
1355348
Acenaphthene
ND
180
1
02/19/05 3:03 LMK
1355348
Acenaphthylene
ND
180
1
02/19/05 3:03 LMK
1355348
Aniline
ND
180
1
02/19/05 3:03 LMK
1355348
Anthracene
ND
180
1
02/19/05 3:03 LMK
1355348
Benz(a)anthracene
ND
180
1
02/19/05 3:03 LMK
1355348
Benzo(a)pyrene
ND
180
1
02/19/05 3:03 LMK
1355348
Benzo(b)fluoranthene
ND
180
1
02/19/05 3:03 LMK
1355348
Benzo(g,h,i)peryiene
ND
180
1
02/19/05,3:03 LMK
1355348
Benzo(k)fluoranthene
ND
180
1
02/19/05 3:03 LMK
1355348
Benzoic acid
ND
720
1
02/19/05 3:03 LMK
1355348
Benzyl alcohol
ND
180
1
02/19/05 3:03 LMK
1355348
Bis (2-chloroethoxy)m ethane
ND
180
1
02/19/05 3:03 LMK
1355348
Bis(2-chloroethyi)ether
ND
180
1
02/19/05 3:03 LMK
1355348
B is (2-chloroi sop ropyl) ether
ND
180
1
02/19/05 3:03 LMK
1355348
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:40 PM

Awl
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-8 15'
Collected: 02/07/2005 15:30
SPL Sample ID: 05020306-08
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Bis(2-ethyihexyi)phthalate
ND
180
1
02/19/05 3:03 LMK
1355348
Butyl benzy! phthalate
ND
180
1
02/19/05 3:03 LMK
1355348
Carbazole
ND
180
1
02/19/05 3:03 LMK
1355348
Chrysene
ND
180
1
02/19/05 3:03 LMK
1355348
Dibenz(a,h)anthracene
ND
180
1
02/19/05 3:03 LMK
1355348
Dibenzofuran
ND
180
1
02/19/05 3:03 LMK
1355348
Diethyl phthalate
ND
180
1
02/19/05 3:03 LMK
1355348
Dimethyl phthalate
ND
180
1
02/19/05 3:03 LMK
1355348
Di-n-butyl phthalate
ND
180
1
02/19/05 3:03 LMK
1355348
Di-n-octyl phthalate
ND
180
1
02/19/05 3:03 LMK
1355348
Fluoranthene
ND
180
1
02/19/05 3:03 LMK
1355348
Fluorene
ND
180
1
02/19/05 3:03 LMK
1355348
Hexachlorobenzene
ND
180
1
02/19/05 3:03 LMK
1355348
Hexachlorobutadiene
ND
180
1
02/19/05 3:03 LMK
1355348
Hexachlorocyclopentadiene,�`
ND
350
1
02/19/05 3:03 LMK
1355348
Hexachloroethane I
ND
180
1
02/19/05 3:03 LMK
1355348
Inden(>(1,2,3-cd)pyrene
ND
180
1
02/19/05 3:03 LMK
1355348
Isophorone
ND
180
1
02/19/05 3:03 LMK
1355348
Naphthalene
ND
180
1
02/19/05 3:03 LMK
1355348
Nitrobenzene
ND
180
1
02/19/05 3:03 LMK
1355348
N-Nitrosodi-n-propoamine
ND
180
1
02/19/05 3:03 LMK
1355348
N-Nitrosodiphenylamine
ND
180
1
02/19/05 3:03 LMK
1355348
Pentachlorophenol
ND
700
1
02/19/05 3:03 LMK
1355348
Phenanthrene
ND
180
1
02/19/05 3:03 LMK
1355348
Phenol
ND
180
1
02/19/05 3:03 LMK
1355348
Pyrene
ND
180
1
02/19/05 3:03 LMK
1355348
2-Methyiphenol
ND
180
1
02/19/05 3:03 LMK
1355348
m,p-Cresols
ND
180
1
02/19/05 3:03 LMK
1355348
Surr: 2,4,6-Tribromophenol
3.40
% 14.3-114
1
02/19/05 3:03 LMK
1355348
Surr: 2-Fluorobiphenyl
72.9
% 36.6-109
1
02/19/05 3:03 LMK
1355348
Surr: 2-Fluorophenol
41.1
% 30.9-91
1
02/19/05 3:03 LMK
1355348
Surr: 4-Terphenyl-d14
71.4
% 51.1-124
1
02/19/05 3:03 LMK
1355348
Surr: Nitrobenzene-d5
65.4
% 33.7-97.2
1
02/19/05 3:03 LMK
1355348
Surr: Phenol-d5
71.1
% 34.5-94.6
1
02/19/05 3:03 LMK
1355348
Preg Method BLQp D&
SW3550B �02/09/2005 1 . 6:39
Prep Initials Prep Factor
RDH 1.00
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and POL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:40 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
(337) 2374775
Client Sample ID:GP-8 15'
Collected: 02/07/2005 15:30
SPIL Sample ID: 05020306-08
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result Rep.Lirnit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
VOLATILE ORGANICS METHOD 8260B +MTBE
MCL SW8260B
Units• ug/Kg-dry
1, 1, 1 -Trichloroethane
N D
4.4
1
02/15/05 22:21 GJH
1350190
1, 1,2,2-Tetrachloroethane
ND
4.4
1
02/15/05 22:21 GJH
1350190
1, 1,2-Trichloroethane
ND
4.4
1
02/15/05 22:21 GJH
1350190
1,1-Dichloroethane
ND
4.4
1
02/15/05 22:21 GJH
1350190
1,1-Dichloroethene
ND
4.4
1
02/15/05 22:21 GJH
1350190
1,2-Dichloroethane
ND
4.4
1
02/15/05 22:21 GJH
1350190
1,2-Dichloropropane
ND
4.4
1
02/15/05 22:21 GJH
1350190
2-Butanone
ND
18
1
02/15/05 22:21 GJH
1350190
2-Hexanone
ND
8.9
1
02/15/05 22:21 GJH
1350190
4-Methyl-2-pentanone
ND
8.9
1
02/15/05 22:21 GJH
1350190
Acetone
ND
89
1
02/15/05 22:21 GJH
1350190
Benzene
ND
4.4
1
02/15/05 22:21 GJH
1350190
Bromodichloromethane
ND
4.4
1
02/15/05 22:21 GJH
1350190
Bromoform
ND
4.4
1
02/15/05 22:21 GJH
1350190
Bromomethane
ND
8.9
1
02/15/05 22:21 GJH
1350190
Carbon disulfide
ND
4.4
1
02/15/05 22:21 GJH
1350190
Carbon tetrachloride
ND
4.4
1
02/15/05 22:21 GJH
1350190
Chlorobenzene
ND
4.4
1
02/15/05 22:21 GJH
1350190
Chloroethane
ND
8.9
1
02/15/05 22:21 GJH
1350190
Chloroform
ND
4.4
1
02/15/05 22:21 GJH
1350190
Chloromethane
ND
4.4
1
02/15/05 22:21 GJH
1350190
cis- 1, 3-Dichloropropene
ND
4.4
1
02/15/05 22:21 GJH
1350190
Dibromochloromethane
ND
4.4
1
02/15/05 22:21 GJH
1350190
Ethylbenzene
ND
4.4
1
02/15/05 22:21 GJH
1350190
Methyi tert-butyl ether
ND
4.4
1
02/15/05 22:21 GJH
1350190
Methylene chloride
ND
8.9
1
02/15/05 22:21 GJH
1350190
Styrene
ND
4.4
1
02/15/05 22:21 GJH
1350190
Tetrachloroethene
ND
4.4
1
02/15/05 22:21 GJH
1350190
Toluene
ND
4.4
1
02/15/05 22:21 GJH
1350190-
trans- 1,3-Dichloropropene
ND
4.4
1
02/15/05 22:21 GJH
1350190
Trichloroethene
ND
4.4
1
02/15/05 22:21 GJH
1350190
Trichlorofluoromethane
ND
4.4
1
02/15/05 22:21 GJH
1350190
Vinyl acetate
ND
8.9
1
02/15/05 22:21 GJH
1350190
Vinyl chloride
ND
8.9
1
02/15/05'22:2-1 GJH
1350190
cis- 1,2-Dichloroethene
ND
4.4
1
02/15/05 22:21 GJH
1350190
m,p-Xyiene
ND
4.4
1
02/15/05 22:21 GJH
1350190
o-Xylene
ND
4.4
1
02/15/05 22:21 GJH
1350190
trans- 1,2-Di chloroethene
ND
4.4
1
02/15/05 22:21 GJH
1350190
1,2-Dichloroethene (total)
ND
4.4
1
02/15/05 22:21 GJH
1350190
Xylenesjotal
ND
4.4
1
02/15/05 22:21 GJH
1350190
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and POL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/2812005 5:05:40 PM

Ar
Ar
R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-8 15'
Collected: 02/07/2005 15:30
SPL Sample ID: 05020306-08
Site: GREYHOUND TERM INAL-R-ALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Surr: 1,2-Dichloroethane-d4
118
%
66.1-151
1
02/15/05 22:21 GJH
1350190
Surr: 4-Bromofluorobenzene
96.8
%
62-139
1
02/15/05 22:21 GJH
1350190
Surr: Toluene-d8
95.9
%
74.8-118
1
02/15/05 22:21 GJH
1350190
Prep Method Prep Date
SW5035 02/07/2005 0:00
jPre p initials 1Prep Factor
IFT ]0.84
VOLATILE PETROLEUM HYDROCARBONS
MCL MA VPH EPH
Units: ug/Kg-dry
C5-C8 Aliphatics
ND
8700
50
02/10/05 18:34 NDG
1347193
C9-C 10 Aromatics
ND
1300
50
02/11/05 18:22 NDG
1349008
C9-C12 Aliphatics
ND
4300
50
02/11/05 18:22 NDG
1349042
C9-C 12 Aliphatics
6100
4400
50
02/10/05 18:34 NDG
1347193
Sum 1,4-Difluorobenzene
106
%
70-130
50
02/11/05 18:22 NDG
1349008
Surr: 1,4-Difluorobenzene
99.9
%
70-130
50
02/11/05 18:22 NDG
1349042
Surr: 1,4-Difluorobenzene
102
%
70-130
50
02/10/05 18:34 NDG
1347193
Surr: 4-Bromofluorobenz" ere
102
%
70-130
50
02/11/05 18:22 NDG
1349042
Surr: 4-Bromofluorobenzene
93.2
%
70-130
50
02/11/05 18:22 NDG
1349008
Surr: 4-Bromofluorobenzene
104
%
70-130
50
02/10/05 18:34 NDG
1347193
Prep Method
ELQ2 Date
Prep ini Initials
EL Factor
W
SW8015B
02/10/2005 0:00
FT
0.82
SW8015B
02/07/2005 0:00
FT
0.81
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:41 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-9 10'
Collected: 02/07/2005 16:00
SPL Sample ID: 05020306-09
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
EXTRACTABLE PETROLEUM HYDROCARBONS MCL
MA VPH EPH
Units: mg/Kg-dry
C11-C22 Aromatics
ND
14
1
02/25/05 3:02 CH
1361541
C19-C36 Aliphatics
ND
21
1
02/25/05 3:02 CH
1361506
C9-C18 Aliphatics
ND
14
1
02/25/05 3:02 CH
1361506
Surr: 2-Bromonaphthalene
45.4
%
40-140
1
02/25/05 3:02 CH
1361541
Surr: 2-Fluorobiphenyl
42.2
%
40-140
1
02/25/05 3:02 CH
1361541
Surr: Chloro-octadecane
93.4
%
40-140
1
02/25/05 3:02 CH
1361506
Surr: o-Terphenyl
46.9
%
40-140
1
02/25/05 3:02 CH
1361541
Prep Method Prep Dat
ISW3550B 102/09/2005 18:29
Pre Initials jErpp Factor
JCLT I 1-=-00
PERCENT MOISTURE
MCL
D2216
Units: wt%
Percent Moisture
30
0.1
1
02/09/05 15:55 CAM
1343945
Qualifiers: NDIIJ - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:42 PM

'OOOV
d F Jul
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-9 10'
Collected: 02/07/2005 16:00
SPL Sample ID: 05020306-09
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
SEMIVOLATILE ORGANICS
BY METHOD
8270C
MCL SW8270C
Units: ug/Kg-dry
1,2,4-Trichlorobenzene
ND
240
1
02/19/05 3:35
LMK
1355349
1,2-Dichlorobenzene
ND
240
1
02/19/05 3:35
LMK
1355349
1,2-Diphenyihydrazine
ND
240
1
02/19/05 3:35
LMK
1355349
1,3-Dichlorobenzene
ND
240
1
02/19/05 3:35
LMK
1355349
1,4-Dichlorobenzene
ND
240
1
02/19/05 3:35
LMK
1355349
2,4,5-Thchlorophenol
ND
240
1
02/19/05 3:35
LMK
1355349
2,4,6-T rich lorop, henol
ND
240
1
02/19/05 3:35
LMK
1355349
2,4-Dichlorophenol
ND
240
1
02/19/05 3:35
LMK
1355349
2,4-Dimethyiphenol
ND
240
1
02/19/05 3:35
LMK
1355349
2,4-Dinitrophenol
ND
940
1
02/19/05 3:35
LMK
1355349
2,4-Dinitrotoluene
ND
240
1
02/19/05 3:35
LMK
1355349
2,6-Dinitrotoluene
ND
240
1
02/19/05 3:35
LMK
1355349
2-Chloronaphthalene
ND
240
1
02/19/05 3:35
LMK
1355349
2-Chlorophenol
ND
240
1
02/19/05 3:35
LMK
1355349
2-Methyl naphthalene
ND
240
1
02/19/05 3:35
LMK
1355349
2-Nitroaniline
ND
470
1
02/19/05 3:35
LMK
1355349
2-Nitrophenol
ND
240
1
02/19/05 3:35
LMK
1355349
3,3'-Dichlorobenzi dine
ND
240
1
02/19/05 3:35
LMK
1355349
3-Nitroaniline
ND
470
1
02/19/05 3:35
LMK
1355349
4,6- D initro-2-m ethyl phenol
ND
940
1
02/19/05 3:35
LMK
1355349
4-Bromophenyl phenyl ether
ND
240
1
02/19/05 3:35
LMK
1355349
4-Chloro-3-methyl phenol
ND
240
1
02/19/05 3:35
LMK
1355349
4-Chloroaniline
ND
240
1
02/19/05 3:35
LMK
1355349
4-Chlorophenyl phenyl ether
ND
240
1
02/19/05 3:35
LMK
1355349
4-Nitroaniline
ND
470
1
02/19/05 3:35
LMK
1355349
4-Nitrophen ol
ND
940
1
02/19/05 3:35
LMK
1355349
Acenaphthene
ND
240
1
02/19/05 3:35
LMK
1355349
Acenaphthyiene
ND
240
1
02/19/05 3:35
LMK
1355349
Aniline
ND
240
1
02/19/05 3:35
LMK
1355349
Anthracene
ND
240
1
02/19/05 3:35
LMK
1355349
Benz(a)anthracene
ND
240
1
02/19/05 3:35
LMK
1355349
Benzo(a)pyrene
ND
240
1
02/19105 3:35
LMK
1355349
Benzo(b)fluoranthene
ND
240
1
02/19/05 3:35
LMK
1355349
Benzo(g,h,i)peryiene
ND
240
1
02/19/05,3:35
LMK
1355349
Benzo(k)fluoranthene
ND
240
1
02/19/05 3:35
LMK
1355349
Benzoic acid
ND
970
1
02/19/05 3:35
LMK
1355349
Benzyi alcohol
ND
240
1
02/19/05 3:35
LMK
1355349
Bis(2-chloroethoxy)m ethane
ND
240
1
02/19/05 3:35
LMK
1355349
Bis(2-chloroethyi)ether
ND
240
1
02/19/05 3:35
LMK
1355349
Bis (2-chloroi sop ropyl)ether
ND
240
1
02/19/05 3:35
LMK
1355349
Qualifiers: ND/U - Not Detected at the Reporting Limit
6 - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:42 PM

'40 Amodo �M—
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-9 10'
Collected: 02/07/2005 16:00
SPL Sample ID: 05020306-09
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method Result
Rep.Lirnit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
Bis(2-ethytheq)phthalate
ND
240
1
02/19/05 3:35
LMK
1355349
Butyl benzyl phthalate
ND
240
1
02/19/05 3:35
LMK
1355349
Carbazole
ND
240
1
02/19/05 3:35
LMK
1355349
Chrysene
ND
240
1
02/19/05 3:35
LMK
1355349
Dibenz(a,h)anthracene
ND
240
1
02/19/05 3:35
LMK
1355349
Dibenzofuran
ND
240
1
02/19/05 3:35
LMK
1355349
Diethyl phthalate
ND
240
1
02/19/05 3:35
LMK.
1355349
Dimethyl phthalate
ND
240
1
02/19/05 3:35
LMK
1355349
Di-n-butyl phthalate
ND
240
1
02/19/05 3:35
LMK
1355349
Di-n-octyi phthalate
ND
240
1
02/19/05 3:35
LMK
1355349
Fluoranthene
ND
240
1
02/19/05 3:35
LMK
1355349
Fluorene
ND
240
1
02/19/05 3:35
LMK.
1355349
Hexachlorobenzene
ND
240
1
02/19/05 3:35
LMK
1355349
Hexachlorobutadiene
ND
240
1
02/19/05 3:35
LMK
1355349
Hexachlorocyclopentadiene"
ND
470
1
02/19/05 3:35
LMK
1355349
Hexachloroethane
ND
240
1
02/19/05 3:35
LMK
1355349
lndeno(1,2,3-cd)pyrene
ND
240
1
02/19/05 3:35
LMK
1355349
Isophorone
ND
240
1
02/19/05 3:35
LMK
1355349
Naphthalene
ND
240
1
02/19/05 3:35
LMK
1355349
Nitrobenzene
ND
240
1
02/19/05 3:35
LMK
1355349
N-Nitrosodi-n-propylamine
ND
240
1
02/19/05 3:35
LMK
1355349
N-Nitrosodiphenylamine
ND
240
1
02/19/05 3:35
LMK
1355349
Pentachlorophenol
ND
940
1
02/19/05 3:35
LMK
1355349
Phenanthrene
ND
240
1
02/19/05 3:35
LMK
1355349
Phenol
ND
240
1
02/19/05 3:35
LMK
1355349
Pyrene
ND
240
1
02/19/05 3:35
LMK
1355349
2-Methylphenol
ND
240
1
02/19/05 3:35
LMK
1355349
m,p-Cresols
ND
240
1
02/19/05 3:35
LMK
1355349
Surr: 2,4,6-Tribromophenol
85.9
% 14.3-114
1
02/19/05 3:35
LMK
1355349
Surr: 2-Fluorobiphenyl
64.9
% 36.6-109
1
02/19/05 3:35
LMK
1355349
Sum 2-Fluorophenol
73.6
% 30.9-91
1
02/19/05 3:35
LMK
1355349
Surr: 4-Terphenyl-d14
70.8
% 51.1-124
1
02/19/05 3:35
LMK
1355349
Surr: Nitrobenzene-d5
63.4
% 33.7-97.2
1
02/19/05 3:35
LMK
1355349
Surr: Phenol-d5
70.4
% 34.5-94.6
1
02/19/05 3:35
LMK
1355349
Prep Method BLW D &I e
Prep InitialsPr
Factor

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
(337) 2374775
Client Sample ID:GP-9 10'
Collected: 02/07/2005 16:00 SPL Sample ID: 05020306-09
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result Rep.Limit
Dil. Factor QUAL Date Analyzed Analyst
Seq. #
VOLATILE ORGANICS METHOD 8260B +MTBE
MCL SW8260B Units: uq/Kq-dry
1, 1, 1 -T rich loroethane
ND
8
—
1 02/15/05 22:48 GJH
1350191
1, 1,2,2-Tetrachloroethane
ND
8
1 02/15/05 22:48 GJH
1350191
1, 1,2-Trichloroethane
ND
8
1 02/15/05 22:48 GJH
1350191
1,1-Dichloroethane
ND
8
1 02/15/05 22:48 GJH
1350191
1,1-Dichloroethene
ND
8
1 02/15/05 22:48 GJH
1350191
1,2-Dichloroethane
ND
8
1 02/15/05 22:48 GJH
1350191
1,2-Dichloropropane
ND
8
1 02/15/05 22:48 GJH
1350191
2-Butanone
33
32
1 02/15/05 22:48 GJH
1350191
2-Hexanone
ND
16
1 02/15/05 22:48 GJH
1350191
4-Methyl-2-pentanone
ND
16
1 02/15/05 22:48 GJH
1350191
Acetone
ND
160
1 02/15/05 22:48 GJH
1350191
Benzene
ND
8
1 02/15/05 22:48 GJH
1350191
Bromodichloromethane
ND
8
1 02/15/05 22:48 GJH
1350191
Bromoform
ND
8
1 02/15/05 22:48 GJH
1350191
Bromomethane
ND
16
1 02/15/05 22:48 GJH
1350191
Carbon disulfide
ND
8
1 02/15/05 22:48 GJH
1350191
Carbon tetrachloride
ND
8
1 02/15/05 22:48 GJH
1350191
Chlorobenzene
ND
8
1 02/15/05 22:48 GJH
1350191
Chloroethane
ND
16
1 02/15/05 22:48 GJH
1350191
Chloroform
ND
8
1 02/15/05 22:48 GJH
1350191
Chloromethane
ND
8
1 02/15/05 22:48 GJH
1350191
— cis- 1,3-Dichloropropene
ND
8
1 02/15/05 22:48 GJH
1350191
Dibromoch loromethane
ND
8
1 02/15/05 22:48 GJH
1350191
— Ethylbenzene
ND
8
1 02/15/05 22:48 GJH
1350191
— Methyl tert-butyl ether
ND
8
1 02/15/05 22:48 GJH
1350191
Methylene chloride
ND
16
1 02/15/05 22:48 GJH
1350191
Styrene
ND
8
1 02/15/05 22:48 GJH
1350191
Tetrachloroethene
ND
8
1 02/15/05 22:48 GJH
1350191
Toluene
ND
8
1 02/15/05 22:48 GJH
1350191
trans- 1,3-Dichloropropene
ND
8
1 02/15/05 22:48 GJH
1350191
Trichloroethene
ND
8
1 02/15/05 22:48 GJH
1350191
Trichlorofluoromethane
ND
8
1 02/15/05 22:48 GJH
1350191
—Vinyl acetate
ND
16
1 02/15/05 22:48 GJH
1350191
—Vinyl chloride
ND
16
1 02/15/0522:48 GJH
1350191
cis- 1,2-Dichloroethene
ND
8
1 02/15/05 22:48 GJH
1350191
M,P-Xyiene
ND
8
1 02/15/05 22:48 GJH
1350191
o-Xyiene
ND
8
1 02/15/05 22:48 GJH
1350191
trans- 1,2-Dichloroethene
ND
8
1 02/15/05 22:48 GJH
1350191
1,2-Dichloroethene (total)
ND
8
1 02/15/05 22:48 GJH
1350191
Xylenesjotal
ND
8
1 02/15/05 22:48 GJH
1350191
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and POL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unrepdrtable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:43 PM

'44 -Ma
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-9 10'
Collected: 02/07/2005 16:00
SPL Sample ID: 05020306-09
Site: GREYHOUND TERM INAL- RALEIGH
Analyses/Method
Result
Rep.Lirnit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Surr: 1,2-Dichloroethane-d4
110
%
66.1-151
1
02/15/05 22:48 GJH
1350191
Surr: 4-Bromofluorobenzene
96.9
%
62-139
1
02/15/05 22:48 GJH
1350191
Surr: Toluene-d8
93.1
%
74.8-118
1
02/15/05 22:48 GJH
1350191
Prep Method Prep Date
SW5035 02/07/2005 0:00
Prep Initials Prep Factor
FT 11.12
VOLATILE PETROLEUM HYDROCARBONS
MCL MA VPH EPH
Units: ug/Kg-dry
C5-C8 Aliphatics
ND
13000
50
02/10/05 19:03 NDG
1347194
C9-C 10 Aromatics
ND
1900
50
02/10/05 19:03 NDG
1347267
C9-C 12 Aliphatics
ND
6400
50
02/10/05 19:03 NDG
1347194
Surr: 1,4-Dffluorobenzene
106
%
70-130
50
02/10/05 19:03 NDG
1347267
Surr: 1,4-Difluorobenzene
106
%
70-130
50
02/10/05 19:03 NDG
1347194
Surr: 4-Bromofluorobenzene
98.6
%
70-130
50
02/10/05 19:03 NDG
1347194
Surr: 4-Bromofluorobenzene
92.7
%
70-130
50
02/10/05 19:03 NDG
1347267
Prep Method
ErWft a
iFa
nLigls
ELWj_
?jWg tor
SW8015B
02/10/2005 0:00
FT
0.89
SW8015B
02/10/2005 0:00
FT
0.89
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:44 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-10 10'
Collected: 02/07/2005 16:30
SPL Sample ID: 05020306-10
Site: GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
EXTRACTABLE PETROLEUM HYDROCARBONS MCL
MA VPH EPH
Units: mg/Kg-dry
C11-C22 Aromatics
ND
12
1
02/25/05 3:37 CH
1361542
C19-C36 Aliphatics
ND
18
1
02/25/05 3:37 CH
1361507
C9-C18 AJiphabcs
ND
12
1
02/25/05 3:37 CH
1361507
Surr: 2-Bromonaphthalene
41.8
%
40-140
1
02/25/05 3:37 CH
1361542
Surr: 2-Fluorobiphenyi
44.1
%
40-140
1
02/25/05 3:37 CH
1361542
Surr: Chloro-octadecane
93.3
%
40-140
1
02/25/05 3:37 CH
1361507
Sum o-Terphenyi
51.6
%
40-140
1
02/25/05 3:37 CH
1361542
Prep Method Prep Date
SW3550B 102/09/2005 18:29
Prep Initials ELW Factor
CLT 11.00
PERCENT MOISTURE
MCL
D2216
Units: wt%
Percent Moisture
16
0.1
1
02/09/05 15:55 CAM
1343944
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
2/28/2005 5:05:45 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-10 10'
Collected: 02/07/2005 16:30
SPL Sample ID: 05020306-10
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
Rep.Lirnit
Dil. Factor ®UAL
Date Analyzed Analyst
Seq. #
SEMIVOLATILE ORGANICS
BY METHOD 8270C
MCL SW8270C
Units• ug/Kg-dry
1,2,4-Trichlorobenzene
ND
200
1
02/19/05 4:07 LMK
135535-0
1,2-Dichlorobenzene
ND
200
1
02/19/05 4:07 LMK
1355350
1,2-Diphenyihydrazine
ND
200
1
02/19/05 4:07 LMK
1355350
1,3-Dichlorobenzene
ND
200
1
02/19/05 4:07 LMK
1355350
1,4-Dichlorobenzene
ND
200
1
02/19/05 4:07 LMK
1355350
2,4,5-Trichlorophenol
ND
200
1
02/19/05 4:07 LMK
1355350
2,4,6-Trichlorophenol
ND
200
1
02/19/05 4:07 LMK
1355350
2,4-Dichlorophenol
ND
200
1
02/19/05 4:07 LMK
1355350
2,4-Dimethylphenol
ND
200
1
02/19/05 4:07 LMK
1355350
2,4-Dinitrophenol
ND
790
1
02/19/05 4:07 LMK
1355350
2,4-Dinitrotoluene
ND
200
1
02/19/05 4:07 LMK
1355350
2,6-Dinitrotoluene
ND
200
1
02/19/05 4:07 LMK
1355350
2-Chloronaphthalene
ND
200
1
02/19/05 4:07 LMK
1355350
2-Chlorophenol
ND
200
1
02/19/05 4:07 -LMK
1355350
2-Methyinaphthalene
ND
200
1
02/19/05 4.07 LMK
1355350
2-Nitroaniline
ND
390
1
02/19/05 4:07 LMK
1355350
2-Nitrophenol
ND
200
1
02/19/05 4:07 LMK
1355350
3,3'-Dichlorobenzidine
ND
200
1
02/19/05 4:07 LMK
1355350
3-Nitroaniline
ND
390
1
02/19/05 4:07 LMK
1355350
4,6-Dinitro-2-m ethyi phenol
ND
790
1
02/19/05 4:07 LMK
1355350
4-Bromophenyi phenyl ether
ND
200
1
02/19/05 4:07 LMK
1355350
4-Chloro-3-methyiphenol
ND
200
1
02/19/05 4:07 LMK
1355350
4-Chloroaniline
ND
200
1
02/19/05 4:07 LMK
1355350
4-Chlorophenyl phenyl ether
ND
200
1
02/19/05 4:07 LMK
1355350
4-Nitroaniline
ND
390
1
02/19/05 4:07 LMK
1355350
4-Nitrophenol
ND
790
1
02/19/05 4:07 LMK
1355350
Acenaphthene
ND
200
1
02/19/05 4:07 LMK
1355350
Acenaphthyiene
ND
200
1
02/19/05 4:07 LMK
1355350
Aniline
ND
200
1
02/19/05 4:07 LMK
1355350
Anthracene
ND
200
1
02/19/05 4:07 LMK
1355350
Benz(a)anthracene
ND
200
1
02/19/05 4:07 LMK
1355350
Benzo(a)pyrene
ND
200
1
02/19/05 4:07 LMK
1355350
Benzo(b)fluoranthene
ND
200
1
02/19/05 4:07 LMK
1355350
Benzo(g,h,i)peryiene
ND
200
1
02/19/05 4:07 LMK
1355350
Benzo(k)fluoranthene
ND
200
1
02/19/05 4:07 LMK
1355350
Benzoic acid
ND
810
1
02/19/05 4:07 LMK
1355350
Benzyl alcohol
ND
200
1
02/19/05 4:07 LMK
1355350
Bis(2-ch loroeth oxy) methane
ND
200
1
02/19/05 4:07 LMK
1355350
Bis(2-chloroethyl)ether
ND
200
1
02/19/05 4:07 LMK
1355350
Bis(2-chloroisopropyi)ether
ND
200
1
02/19/05 4:07 LMK
1355350
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2128/2005 5:05:45 PM

R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-10 10'
Collected: 02/07/2005 16:30
SPL Sample ID: 05020306-10
Site: GREYHOUND TERMINAL- LEIGH
Analyses/Method Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
Bis(2-ethyihexyi)phthalate
ND
200
1
02/19/05 4:07
LMK
1355350
Butyl benzyi phthalate
ND
200
1
02/19/05 4:07
LMK
1355350
Carbazole
ND
200
1
02/19/05 4:07
LMK
1355350
Chrysene
ND
200
1
02/19/05 4:07
LMK
1355350
Dibenz(a,h)a.nthracene
ND
200
1
02/19/05 4:07
LMK
1355350
Dibenzofuran
ND
200
1
02/19/05 4:07
LMK
1355350
Diethyl phthalate
ND
200
1
02/19/05 4:07
LMK
1355350
Dimethyi phthalate
ND
200
1
02/19/05 4:07
LMK
1355350
Di-n-butyl phthalate
ND
200
1
02/19/05 4:07
LMK
1355350
Di-n-octyI phthalate
ND
200
1
02/19/05 4:07
LMK
1355350
Fluoranthene
ND
200
1
02/19/05 4:07
LMK
1355350
Fluorene
ND
200
1
02/19/05 4:07
LMK
1355350
Hexachlorobenzene
ND
200
1
02/19/05 4:07
LMK
1355350
Hexachlorobutadiene
ND
200
1
02/19/05 4:07
LMK
1355350
Hexachiorocydopentadiene
ND
390
1
02/19/05 4:07
LMK
1355350
Hexachloroethane
ND
200
1
02/19/05 4:07
LMK
1355350
Indeno(1,2,3-cd)pyrene
ND
200
1
02/19/05 4:07
LMK
1355350
Isophorone
ND
200
1
02/19/05 4:07
LMK
1355350
Naphthalene
ND
200
1
02/19/05 4:07
LMK
1355350
Nitrobenzene
ND
200
1
02/19/05 4:07
LMK
1355350
N-Nitrosodi-n-propylamine
ND
200
1
02/19/05 4:07
LMK
1355350
N-Nitrosodiphenytamine
ND
200
1
02/19105 4:07
LMK
1355350
Pentachlorophenol
ND
790
1
02/19/05 4:07
LMK
1355350
Phenanthrene
ND
200
1
02/19/05 4:07
LMK
1355350
Phenol
ND
200
1
02/19/05 4:07
LMK
1355350
Pyrene
ND
200
1
02/19/05 4:07
LMK
1355350
2-Methylphenol
ND
200
1
02/19/05 4:07
LMK
1355350
m,p-Cresols
ND
200
1
02/19/05 4:07
LMK
1355350
Surr: 2,4,6-Thbromophenol
93.0
% 14.3-114
1
02/19/05 4:07
LMK
1355350
Surr: 2-Fluorobiphenyt
71.8
% 36.6-109
1
02/19/05 4:07
LMK
1355350
Surr: 2-Fluorophenol
82.3
% 30.9-91
1
02/19/05 4:07
LMK
1355350
Surr: 4-Terphenyl-d14
77.0
% 51.1-124
1
02/19/05 4:07
LMK
1355350
Surr: Nitrobenzene-d5
69.3
% 33.7-97.2
1
02/19/05 4:07
LMK
1355350
Surr: Phenol-d5
80.1
% 34.5-94.6
1
02/19/05 4:07
LMK
1355350
Prep Method e _Date
p� FLS -L
--A
SW3550B 2/09/2005 7739
) initials JET2 Factor
I Preg _qq
RDH 1.00]
J1
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and POL
>MCL - Result Over Maximum Contamination
D - Surrogate Recovery Unreportable due
MI - Matrix Interference
Limit(MCL)
to Dilution
2/2812005 5:05:46 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-10 10'
Collected: 02/07/2005 16:30
SPL Sample ID: 05020306-10
Site:
GREYHOUND TERMINAL- LEIG
Analyses/Method
Result Rep.Lirnit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS METHOD 8260B +MTBE
MCL SW8260B
Units: ug/Kg-dry
1, 1, 1 -Trichloroethane
ND
4.3
1
02/15/05 23:15
GJH
1350192
1, 1,2,2-Tetrachloroethane
ND
4.3
1
02/15/05 23:15
GJH
1350192
1,1,2-Trichloroethane
ND
4.3
1
02/15/05 23:15
GJH
1350192
1,1-Dichloroethane
ND
4.3
1
02/15/05 23:15
GJH
1350192
1,1-Dichloroethene
ND
4.3
1
02/15/05 23:15
GJH
1350192
1,2-Dichloroethane
ND
4.3
1
02/15/05 23:15
GJH
1350192
1,2-Dichloropropane
ND
4.3
1
02/15/05 23:15
GJH
1350192
2-Butanone
ND
17
1
02/15/05 23:15
GJH
1350192
2-Hexanone
ND
8.5
1
02/15/05 23:15
GJH
1350192
4-Methyl-2-pentanone
ND
8.5
1
02/15/05 23:15
GJH
1350192
Acetone
ND
85
1
02/15/05 23:15
GJH
1350192
Benzene
ND
4.3
1
02/15/05 23:15
GJH
1350192
Bromodichloromethane
ND
4.3
1
02/15/05 23:15
GJH
1350192
Bromoform
ND
4.3
1
02/15/05 23:15
GJH
1350192
Bromomethane
ND
8.5
1
02/15/05 23:15
GJH
1350192
Carbon disulfide
ND
4.3
1
02/15/05 23:15
GJH
1350192
Carbon tetrachloride
ND
4.3
1
02/15/05 23:15
GJH
1350192
Chlorobenzene
ND
4.3
1
.02/15/05 23:15
GJH
1350192
Chloroethane
ND
8.5
1
02/15/05 23:15
GJH
1350192
Chloroform
ND
4.3
1
02/15/05 23:15
GJH
1350192
Chloromethane
ND
4.3
1
02/15/05 23:15
GJH
1350192
cis-1,3-Dichloropropene
ND
4.3
1
02/15/05 23:15
GJH
1350192
Dibromochloromethane
ND
4.3
1
02/15/05 23:15
GJH
1350192
Ethylbenzene
ND
4.3
1
02/15/05 23:15
GJH
1350192
Methyi tert-butyl ether
ND
4.3
1
02/15/05 23:15
GJH
1350192
Methylene chloride
ND
8.5
1
02/15/05 23:15
GJH
1350192
Styrene
ND
4.3
1
02/15/05 23:15
GJH
1350192
Tetrachloroethene
ND
4.3
1
02/15/05 23:15
GJH
1350192
Toluene
ND
4.3
1
02/15/05 23:15
GJH
1350192
trans- 1,3-Dichloropropene
ND
4.3
1
02/15/05 23:15
GJH
1350192
Trichloroethene
ND
4.3
1
02/15/05 23:15
GJH
1350192
Trichlorofluoromethane
ND
4.3
1
02/15/05 23:15
GJH
1350192
Vinyl acetate
ND
8.5
1
02/15/05 23:15
GJH
1350192
Vinyl chloride
ND
8.5
1
02/15/05 23:15
GJH
1350192
cis-1,2-Dichloroethene
ND
4.3
1
02/15/05 23:15
GJH
1350192
m,p-Xylene
ND
4.3
1
02/15/05 23:15
GJH
1350192
o-Xyiene
ND
4.3
1
02/15/05 23:15
GJH
1350192
trans- 1,2-Dichloroethene
ND
4.3
1
02/15/05 23:15
GJH
1350192
1,2-Dichloroethene (total)
ND
4.3
1
02/15/05 23:15
GJH
1350192
Xylenes,Total
ND
4.3
1
02/15/05 23:15
GJH
1350192
Qualifiers: ND/U - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and PQL
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
2/28/2005 5:05:46 PM

R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID:GP-10 10'
Collected: 02/07/2005 16:30
SPL Sample ID: 05020306-10
Site: GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
Surr: 1,2-Dichloroethane-d4
118
% 66.1-151
1
02/15/05 23:15 GJH
1350192
Sum 4-Bromofluorobenzene
99.5
% 62-139
1
02/15/05 23:15 GJH
1350192
Surr: Toluene-d8
94.6
% 74.8-118
1
02/15/05 23:15 GJH
1350192
Pre Method Pre
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Initial Calibration Date _ 1/27/2005
Calibration Ranqes and Limits
NOTE: Please include units as appropriate
Method of Quantitation (circle one): Curve or Average Response Factor
Calibration Concentration Levels
30
C9 -C 1,8
60
9.98
Aliphatics
120
300
600
900
40
C 19 -C36
80
_
7.43
Aliphatics
160
400
800
1200
85
C 11 - C22
170
10.43
Aromatics
340
850
1700
2550
NOTE: Please indicate units as appropriate.
Calibration Check Date _ 2/25/2005
Calibration Check
MDL = Method Detection Limit RPD = Relative Percent Difference
ML = Mimimum Limit %RSD = Percent Relative Standard Deviation
RL = Reportable Limit CCC = Correlation Coefficient of Curve
revision 5/6/98

ios-cu/uiphuucn | 24ugo{o ! coouo�o -------20oug�g ---'-1
' i ~
'Ce'o1u/uipxxoos | oouoxKg / 100uoxKg �oouo�g
| |
o10
'oe -- Aromatics - ! 3ugxKg aoug»Kg / aouoa{q_ |
NOTE: Please include units as appropriate
Method mouanntauon (check ono): Curve or Average Response Facto,
Calibration Concentration Levels
LVA
75
�
|
100
750
Aliphatics
1500
'
2300
3000
6500
55
220
1650
10
20
40
300
400
NOTE: Please include units asappropriate
Calibration Check Date 2/10/2005
Calibration Check
aso e
c9-o12/uipoaucs 000 15
--- -- --- -�-' l - ---- ----' -- -1- --- -----'
cs-c1oAromatics 100 *
MoL~Method Detection Limit
ML =Minimum Limit
RL=Reportable Limit
nPo= Relative Percent Difference
mRoo=Percent Relative Standard Deviation
000=Correlation Coefficient oxCurve
revision e/6/9e

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2/28/2005 5:05:47 PM

Analysis: PERCENT MOISTURE
Method: D2216
GREYHOUND LINES, INC.
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: R93917
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05020306-01 B
GP-1 15'
05020306-02B
GP-2 15'
05020306-03B
GP-3 10'
05020306-04B
GP-4 15'
05020306-05B
GP-5 10'
05020306-06B
GP-6 10'
05020306-07B
GP-7 15'
05020306-08B
GP-8 15'
05020306-09B
GP-9 10'
05020306-10B
GP-10 10'
Sample Duplicate
Original Sample: 05020301-01
RunID: WET_050209V-1343959 Units: wt%
Analysis Date: 02/09/2005 15:55 Analyst: CAM
Analyte
Sample
Result
DUP
Result
RPD
RPD
Limit
Percent Moisture
19
16.6
12
20
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL ° - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:53 PM

Analysis: Extractable Petroleum Hydrocarbons
Method: MA VPH EPH
(Method Blank
RunID: TPHA_050224C-1361527 Units: mg/Kg
Analysis Date: 02/24/2005 18:40 Analyst: CH
Preparation Date: 02/09/2005 18:29 Prep By: CLT Method SW3550B
Analyte
Result
Rep Limit
C11-C22 Aromatics
ND
10
Surr:2-Bromona hthalene
44.2
40-140
Surr:2-Fluorobi hen
45.3
40-140
Surr: o-Ter hen
46.3
40-140
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: 35296
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05020306-01 B
GP-1 15'
05020306-02B
GP-2 15'
05020306-03B
GP-3 10'
05020306-04B
GP-4 15'
05020306-056
GP-5 10'
05020306-06B
GP-6 10'
05020306-07B
GP-7 15'
05020306-086
GP-8 15'
05020306-09B
GP-9 10'
05020306-10B
GP-10 10'
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: TPHA_050224C-1361528 Units: mg/Kg
Analysis Date: 02/24/2005 19:17 Analyst: CH
Preparation Date: 02/09/2005 18:29 Prep By: CLT Method SW3550B
Analyte
LCS
LCS
LCS
LCSD
LCSD
LCSD
RPD
RPD
Lower
Upper
Spike
Result
Percent
Spike
Result
Percent
Limit
Limit
Limit
Added
Recovery
Added
Recovery
C11-C22 Aromatics
57
31.4
55.2
57.0
29.0
50.9
8.1
50
40
140
Matrix Spike (M$) / Matrix Spike Duplicate (MSD)
Sample Spiked: 05020306-10
RunID: TPHA_050224C-1361530 Units: mg/Kg-dry
Analysis Date: 02/24/2005 20:29 Analyst: CH
Preparation Date: 02/09/2005 18:29 Prep By: CLT Method SW3550B
Analyte
Sample
MS
MS
MS %
MSD
MSD
MSD %
RPD
RPD
Low
High
Result
Spike
Result
Recovery
Spike
Result
Recovery
Limit
Limit
Limit
Added
Added
C11-C22 Aromatics
ND
67.9
36.0
41.21
67.91
32.7
36.3 "
9.721
50
40
140
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL ` - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 212ei2005 5:05:54 PM

r
Analysis: Extractable Petroleum Hydrocarbons
Method: MA VPH EPH
Method Blank
RunID: TPHA_050225B-1361510 Units: mg/Kg
Analysis Date: 02/26/2005 15:01 Analyst: CH
Preparation Date: 02/09/2005 18:29 Prep By: CLT Method SW3550B
Analyte
Result
Rep Limit
C19-C36 Aliphatics
ND
15
C9-C18 Aliphatics
ND
10
Surr: Chloro-octadecane
83.8
40-140
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: 35296
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05020306-01 B
GP-1 15'
05020306-02 B
GP-2 15'
05020306-038
GP-3 10'
05020306-04 B
GP-4 15'
05020306-05B
GP-5 10'
05020306-066
GP-6 10'
05020306-07B
GP-7 15'
05020306-086
GP-8 15'
05020306-09B
GP-9 10'
05020306-10B
GP-10 10'
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: TPHA_0502258-1361511 Units: mg/Kg
Analysis Date: 02/26/2005 15:36 Analyst: CH
Preparation Date: 02/09/2005 18:29 Prep By: CLT Method SW3550B
Analyte
LCS
LCS
LCS
LCSD
LCSD
LCSD
RPD
RPD
Lower
Upper
Spike
Result
Percent
Spike
Result
Percent
Limit
Limit
Limit
Added
Recovery
Added
Recovery
C19-C36 Aliphatics
20
15.6
77.9
20.0
15.0
75.0
3.7
50
40
140
C9-C 18 Aliphatics
271
8.551
31.7 *
27.0
8.28
30.7 *
3.3
50
40
140
Matrix Spike (MS) / Matrix Spike Duplicate fMSD)
Sample Spiked: 05020306-10
RunID: TPHA_050225B-1361513 Units: mg/Kg-dry
Analysis Date: 02/26/2005 16:46 Analyst: CH
Preparation Date: 02/09/2005 18:29 Prep By: CLT Method SW3550B
Analyte
Sample
MS
MS
MS %
MSD
MSD
MSD %
RPD
RPD
Low
High
Result
Spike
Result
Recovery
Spike
Result
Recovery -
Limit
Limit
Limit
Added
Added
C19-C36 Aliphatics
ND
23.8
17.8
74.7
23.81
16.1
67.4
10.3
50
40
140
69-C18 Aliphatics
!.11
9.161
28.5 *
32.11
8.491
26.4-1
40
140
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL * - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:54 PM

i 7.
Analysis: Volatile Petroleum Hydrocarbons
Method: NIA VPH EPH
Method Blank
RunID: HPCC_05021OB-1347258 Units: ug/Kg
Analysis Date: 02/10/2005 14:47 Analyst: NDG
Preparation Date: 02/10/2005 0:00 Prep By: FT Method SW8015B
Analyte
Result
Rep Limit
C9-C10 Aromatics
ND
30
Surr: 1 4-Difluorobenzene
105.1
70-130
Surr:4-Bromofluorobenzene
93.7
70-130
FAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: 35423
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05020306-03A
GP-3 10'
05020306-04A
GP-4 15'
05020306-09A
GP-9 10'
05020306-10A
GP-10 10'
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: HPCC_05021OB-1347256 Units: ug/Kg
AnalysisDate: 02/10/200512:25 Analyst: NDG
Preparation Date: 02/10/2005 0:00 Prep By: FT Method SW8015B
Analyte
LCS
LCS
LCS
LCSD
LCSD
LCSD
RPD
RPD Lower
Upper
Spike
Result
Percent
Spike
Result
Percent
Limit Limit
Limit
Added
Recovery
Added
Recovery
C9-C 10 Aromatics
50
52.4
105
50.0
53.7
107
2.4
20 70
130
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL " - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:55 Pin

Analysis: Volatile Petroleum Hydrocarbons
Method: MA VPH EPH
Method Blank
RunID: HPCC_050210B-1347258 Units: ug/Kg
Analysis Date: 02/10/2005 14:47 Analyst: NDG
Preparation Date: 02/10/2005 0:00 Prep By: FT Method SW8015B
Analyte
Result
Rep Limit
C9-C10 Aromatics
ND
30
Surr: 1 4-Difluorobenzene
105.1
70-130
Sum 4-Bromofluorobenzene
93.7
70-130
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: 35423
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05020306-03A
GP-3 10'
05020306-04A
GP4 15'
05020306-09A
GP-9 10'
05020306-10A
GP-10 10'
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: HPCC_05021OC-1347183 Units: ug/Kg
Analysis' Date: 02/10/2005 12:25 Analyst: NDG
Preparation Date: 02/10/2005 0:00 Prep By: FT Method SW8015B
Analyte
LCS
LCS
LCS
LCSD
LCSD
LCSD
RPD
RPD
Lower
Upper
Spike
Result
Percent
Spike
Result
Percent
Limit
Limit
Limit
Added
Recovery
Added
Recovery
C5-C8 Aliphatics
300
340
113
300
365
122
7.1
20
70
130
C9-C 12 Aliphatics
300
2571
85.7
3001
270
89.9
4.8
20
70
130
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL ' - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:55 PM

GREYHOUND LINES, INC.
Analysis: Volatile Petroleum Hydrocarbons
Method: MA VPH EPH
Method Bank
RunID: HPCC_05021OC-1347185 Units: ug/Kg
Analysis Date: 02/10/2005 14:47 Analyst: NDG
Preparation Date: 02/10/2005 0:00 Prep By: FT Method SW8015B
Analyte
Result
Rep Limit
C5-C8 Ali hatics
ND
200
C9-C12 Ali hatics
ND
100
Surr:14-Difluorobenzene
107.9
70-130
Surr:4-Bromofluorobenzene
1 101.7
70-130
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: 35423
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05020306-01 A
GP-1 15'
05020306-02A
GP-2 15'
05020306-03A
GP-3 10'
05020306-04A
GP-4 15'
05020306-05A
GP-5 10'
05020306-06A
GP-6 10'
05020306-07A
GP-7 15'
05020306-08A
GP-8 15'
05020306-09A
GP-9 10'
05020306-10A
GP-10 10'
,Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: HPCC_05021OC-1347183 Units: ug/Kg
Analysis Date: 02/10/2005 12:25 Analyst: NDG
Preparation Date: 02/10/2005 0:00 Prep By: FT Method SW8015B
Analyte
LCS
LCS
LCS
LCSD
LCSD
LCSD
RPD
RPD
Lower
Upper
Spike
Result
Percent
Spike
Result
Percent
Limit
Limit
Limit
Added
Recovery
Added
Recovery
C5-C8 Aliphatics
300
340
113
300
365
122
7.1
20
70
130
C9-C 12 Aliphatics
1 3001
2671
85.71
3001
2701
89.91
4.81
201
701
130
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL " - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:55 Pry

Analysis: Volatile Petroleum Hydrocarbons
Method: MA VPH EPH
Method Blank
RunID: HPCC_050211E-1349024 Units: ug/Kg
Analysis Date: 02/11/2005 14:51 Analyst: NDG
Preparation Date: 02/07/2005 0:00 Prep By: FT Method SW8015B
Analyte
Result
Rep Limit
C9-C12 Ali hatics
ND
100
Surr:14-Difluorobenzene
105.2
70-130
Surr:4-Bromofluorobenzene
102.5
70-130
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: 354.66
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05020306-01 A
GP-1 15'
05020306-02A
GP-2 15'
05020306-05A
GP-5 10'
05020306-06A
GP-6 10'
05020306-07A
GP-7 15'
05020306-08A
GP-8 15'
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: HPCC_050211E-1349020 Units: ug/Kg
Analysis'Date: 02/11/200513:25 Analyst: NDG
Preparation Date: 02/07/2005 0:00 Prep By: FT Method SW8015B
Analyte
LCS
LCS
LCS
LCSD
LCSD
LCSD
RPD
RPD
Lower
Upper
Spike
Result
Percent
Spike
Result
Percent
Limit
Limit
Limit
Added
Recovery
Added
Recovery
C9-C 12 Aliphatics
300
262
87.4
300
270
89.9
2.8
20
70
130
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL " - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:56 PM

GREYHOUND
GIEYVDUIJD BLOU I
Analysis: Volatile Petroleum Hydrocarbons
Method: MA VPH EPH
Method Blank
RunID: HPCC_050211D-1349002 Units: ug/Kg
Analysis Date: 02/11/2005 14:51 Analyst: NDG
Preparation Date: 02/07/2005 0:00 Prep By: FT Method SW8015B
Analyte
Result
Rep Limit
C9-C10 Aromatics
ND
30
Surr:14-Difluorobenzene
105.5
70-130
Surr:4-Bromofluorobenzene
95.3
70-130
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: 35466
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05020306-01 A
GP-1 15'
05020306-02A
GP-2 15'
05020306-05A
GP-5 10'
05020306-06A
GP-6 10'
05020306-07A
GP-7 15'
05020306-08A
GP-8 15'
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: HPCC_050211D-1349000 Units: ug/Kg
Analysis'. Date: 02/11/200513:25 Analyst: NDG
Preparation Date: 02/07/2005 0:00 Prep By: FT Method SW 8015E
Analyte
LCS
LCS
LCS
LCSD
LCSD
LCSD
RPD
RPD
Lower
Upper
Spike
Result
Percent
Spike
Result
Percent
Limit
Limit
Limit
Added
Recovery
Added
Recovery
C9-C 10 Aromatics
50
53.3
107
50.0
58.5
117
9.3
201
70
130
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL * - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported.
2/28/2005 5:05:56 Pit

er 7
11 10
'
7-1
Quality Control Report
GREYHOUND LINES, INC.
GREYHOUND BLOUNT / 73.75029.0011
Analysis: Semivolatile Organics by Method 8270C
Method: SW8270C
Method Blank
RunID: A_050216C-1351852 Units: ug/Kg
Analysis Date: 02/16/2005 14:07 Analyst: MKM
Preparation Date: 02/09/2005 16:39 Prep By: RDH Method SW3550B
Analyte
Result
Rep Limit
1 2 4-Trichlorobenzene
ND
170
12-Dichlorobenzene
ND
170
1 2-Di hen h razine
ND
170
13-Dichlorobenzene
ND
170
14-Dichlorobenzene
ND
170
2 4 5-Trichloro henol
ND
170
2 4 6-Trichloro henol
ND
170
2 4-Dichloro henol
ND
170
2 4-Dimeth phenol
ND
170
2 4-Dinitro henol
ND
660
2 4-Dinitrotoluene
ND
170
2 6-Dinitrotoluene
ND
170
2-Chlorona hthalene
ND
170
2-Chloro henol-
ND
170
2-Meth na hthalene
ND
170
2-Nitroaniline
ND
330
2-Nitro henol
ND
170
3 3'-Dichlorobenzidine
ND
170
3-Nitroaniline
ND
330
4 6-Dinitro-2-meth phenol
ND
660
4-Bromo hen hen ether
ND
170
4-Chloro-3-meth henol
ND
170
4-Chloroaniline
ND
170
4-Chloro hen hen ether
ND
170
4-Nitroaniline
ND
330
4-Nitrophenol
ND
660
Acena hthene
ND
170
Acena hth ene
ND
170
Aniline
ND
170
Anthracene
ND
170
Benz a anthracene
ND
170
Benzo a ene
ND
170
Benzo b fluoranthene
ND
170
Benzo h i e ene
ND
170
Benzo k fluoranthene
ND
170
Benzoic acid
ND
680
Ben alcohol
ND
170
Bis 2-chloroetho methane
ND
170
Bis 2-chloroeth ether
ND
170
Bis 2-chloroiso ro ether
ND
170
Bis 2-eth he hthalate
ND
170
But benz phthalate
ND
170
Carbazole
ND
170
Ch ene
ND
170
Dibenz a h anthracene
ND
170
Dibenzofuran
ND
170
Dieth hthalate
ND
170
Dimeth phthalate
ND
170
ND/U -Plot Detected at the Re o in
FAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: 35292
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05020306-01 B
GP-1 15'
05020306-02B
GP-2 15'
05020306-03B
GP-3 10'
05020306-046
GP-4 15'
05020306-05B
GP-5 10'
05020306-06B
GP-6 10'
05020306-078
GP-7 15'
05020306-08B
GP-8 15'
05020306-09B
GP-9 10'
05020306-10B
GP-10 10'
6ualifiers: p rt g Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL ° - Recovery Outside Advisable OC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for OC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported.
2/28/2005 5:05:57 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
® SCOTT, LA 70583
Quality Control Report [phone]
GREYHOUND LINES, INC.
GREYHOUND BLOUNT / 73.75029.0011
Analysis: Semivolatile Organics by Method 8270C WorkOrder: 05020306
Method: SW8270C Lab Batch ID: 35292
Method Blank
RunlD: A_050216C-1351852 Units: ug/Kg
Analysis Date: 02/16/2005 14:07 Analyst: MKM
Preparation Date: 02/09/2005 16:39 Prep By: RDH Method SW3550B
Analyte
Result
Rep Limit'
Di-n-butylhthalate
ND
170
Di-n-oct hthalate
ND
170
Fluoranthene
ND
170
Fluorene
ND
170
Hexachlorobenzene
ND
170
Hexachlorobutadiene
ND
170
Flexachlorocyclopentadiene
ND
330
Hexachloroethane
ND
170
Indeno 1 2,3-cd ene
ND
170
Iso horone
ND
170
Naphthalene
ND
170
Nitrobenzene
ND
170
N-Nitrosodkn- ro amine
ND
170
N-Nitrosodi hen amine
ND
170
Pentachloro henol
ND
660
Phenanthrene
ND
170
Phenol
ND
170
Pyrene
ND
170
2-Methylphenol
ND
170
m -Cresols
ND
170
Surr: 2 4 6-Tribromo henol
75.5
14.3-114
Surr: 2-Fluorobi hen
65.6
36.6-109
Surr: 2-Fluoro henol
78.7
30.9-91
Surr: 4-Ter hen A14
73.5
51.1-124
Surr: Nitrobenzene-d5
62.7
33.7-97.2
Surr: Phenol-d5
72.4
34.5-94.6
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: A_050216C-1351854 Units: ug/Kg
Analysis Date: 02/16/2005 14:40 Analyst: MKM
Preparation Date: 02/09/2005 16:39 Prep By: RDH Method SW3550B
Analyte
LCS
Spike
Added
LCS
Result
LCS
Percent
Recovery
LCSD
Spike
Added
LCSD
Result
LCSD
Percent
Recovery
RPD,
RPD
Limit
Lower
Limit
Upper
Limit
1,2,4-Trichlorobenzene
1670
1240
74.1
1670
1130
67.6
9.1
23
22.8
130
1,4-Dichlorobenzene
1670
1090
65.4
1670
981
58.9
10.5
27
17.1
128
2,4-Dinitrotoluene
1670
1280
76.7
1670
1250
75.0
2.2
47
38.9
109
2-Chkxophenol
2500
1740
69.5
2500
1570
62.6
10.4
50
31.8
127
4-Chloro-3-methylphenol
2500
1750
70.1
2500
1640
65.7
6.5
33
37.7
126
4-Nitrophenol
2500
2130
85.2
2500
2110
84.5
0.9
50
26.3
114
Acenaphthene
1670
11201
67.2
1670
1090
65.2
3.0
19
32.2
122
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL * - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported.
2/28/2005 5:05:57 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
-die® SCOTT, LA 70583
Quality Control Report [phone]
GREYHOUND LINES, INC.
GREYHOUND BLOUNT / 73.75029.0011
Analysis: Sernivolatile Organics by Method 8270C WorkOrder: 05020306
Method: SW8270C Lab Batch ID: 35292
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: A_050216C-1351854 Units: ug/Kg
Analysis Date: 02/16/2005 14:40 Analyst: MKM
Preparation Date: 02/09/2005 16:39 Prep By: RDH Method SW 3550E
Analyte
LCS
Spike
Added
LCS
Result
LCS
Percent
Recovery
LCSD
Spike
Added
LCSD
Result
LCSD
Percent
Recovery
RPD
RPD
Limit
Lower
Limit
Upper
Limit
N-Nitrosodi-n-propylamine
1670
1120
67.1
1670
1070
64.3
4.2
38
16.7
127
Pentachlorophenol
2500
2070
83.0
2500
2160
86.4
4.1
47
42.6
103
Phenol
2500
1820
72.9
2500
1670
67.0
8.5
35
29.7
116
Pyrene
1670
1130
67.9
1670
1120
67.0
1.3
36
67
117
1,2-Dichlorobenzene-d4
1670
0
0*
1670
0
0*
0.0
0
29.3
105
2-Chlorophenol-d4
25001
01
0*
2500
0
0*
0.01
0
35.6
103
Matrix Spike (M$) / Matrix Spike Duplicate (MSD)
Sample Spiked: 05020306-01
RunID: A_050216C-1351857 Units: ug/Kg-dry
Analysis Date: 02/16/2005 16:19 Analyst: MKM
Preparation Date: 02/09/2005 16:39 Prep By: RDH Method SW3550B
Analyte
Sample
Result
MS
Spike
Added
MS
Result
MS %
Recovery
MSD
Spike
Added
MSD
Result
MSD %
Recovery
RPD
RPD
Limit
Low
Limit
High
Limit
1,2,4-Trichlorobenzene
ND
2280
1740
76.4
22801
1690
74.1
3.09
23
25
98.8
1,4-Dichlorobenzene
ND
2280
1420
62.1
22801
1330
58.31
6.17
271
10
94.8
2,4-Dinitrotoluene
ND
2280
1910
83.7
22801
1890
82.8
1.10
47
34.5
116
2-Chlorophenol
ND
3420
2380
69.6
3420
2290
66.8
4.10
50
22.51
104
4-Ch loro-3-methyl phenol
ND
3420
2310
67.5
3420
2110
61.5
9.19
33
40.8
113
4-Nitrophenol
ND
3420
2840
83.0
3420
2920
85.2
2.68
50
24.9
116
Acenaphthene
ND
2280
1720
75.2
22801
16101
70.4
6.66
19
17.8
135
N-Nitrosodi-n-propylamine
ND
2280
1400
61.4
22801
13701
59.8
2.59
38
20.81
107
Pentachlorophenol
ND
3420
2760
80.6
3420
2640
77.0
4.60
47
15.4
109
Phenol
ND
3420
2390
69.9
3420
2320
67.7
3.301
35
29.2
94.5
Pyrene
ND
2280
1410
61.8
2280
1370
60.0
3.04
36
27
139
1,2-Dichlorobenzene-d4
ND
2280
0
0*
2280
0
0 *
0
0
29.3
105
2-Chlorophenol-d4
ND
3420
01
0*
3420
01
0*
01
0
35.61
103
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL * - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:57 PM

3
t,
t �m
STY
t n �
Quality Control Report
GREYHOUND LINES, ES, INC.
GREYHOUND BLOUNT / 73.75029.0011
Analysis: Volatile Organics Method 8260B +MTBE
Method: SW8260B
Method Blank
RunID: 1_050215E-1350180 Units: ug/Kg
Analysis Date: 02/15/2005 17:33 Analyst: GJH
Preparation Date: 02/07/2005 0:00 Prep By: FT Method SW5035
Analyte
Result
Rep Limit
111-Trichloroethane
ND
5.0
1 1 2 2-Tetrachloroethane
ND
5.0
112-Trichloroethane
ND
5.0
11-Dichloroethane
ND
5.0
11-Dichloroethene
ND
5.0
12-Dichloroethane
ND
5.0
1 2-Dichloro ro ane
ND
5.0
2-Butanone
ND
20
2-Hexanone
ND
10
4-Meth -2- entanone '
ND
10
Acetone
ND
100
Benzene
ND
5.0
Bromodichloromethane
ND
5.0
Bromoform
ND
5.0
Bromomethane
ND
10
Carbon disulfide
ND
5.0
Carbon tetrachloride
ND
5.0
Chlorobenzene
ND
5.0
Chloroethane
ND
10
Chloroform
ND
5.0
Chloromethane
ND
5.0
cis-1 3-Dichloro ro ene
ND
5.0
Dibromochloromethane
ND
5.0
Ethyibenzene
ND
5.0
Meth te -butyi ether
NDI
5.0
Methyiene chloride
ND
10
Styrene
ND
5.0
Tetrachloroethene
ND
5.0
Toluene
ND
5.0
trans-1 3-Dichloro ro ene
ND
5.0
Trichloroethene
ND
5.0
Trichlorofluoromethane
ND
5.0
Vinyt acetate
ND
10
Vino chloride
ND
10
cis-1,2-Dichloroethene
ND
5.0
m,p-Xyiene
ND
5.0
o-Xylene
ND
5.0
trans-l2-Dichloroethene
ND
5.0
12-Dichloroethene total
ND
5.0
Xvienes.Total
ND
5.0
Surr:12-Dichloroethane-d4
130.3
66.1-151
Surr:4-Bromofluorobenzene
96.2
62-139
Surr: Toluene-d8
94.4
74.8-118
LAFAYETTELABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
orkOrder: 05020306
Lab Batch ID: 35495
Samples in Analytical Batch:
Lab Sample ID
05020306-03A
05020306-04A
05020306-08A
05020306-09A
05020306-10A
Laboratory Control Sample (LCS)
Client Sample ID
GP-3 10'
GP-4 15'
GP-8 15'
GP-9 10'
GP-10 10'
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL ° - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:58 PM

GREYHOUND LINES, INC.
Analysis: Volatile Organics Method 8260B + TBE
Method: SW8260B
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: 35495
RunID: 1_050215E-1350179 Units: ug/Kg
Analysis Date: 02/15/2005 17:04 Analyst: GJH
Preparation Date: 02/07/2005 0:00 Prep By: FT Method SW5035
Analyte
Spike
Added
Result
Percent
Recovery
Lower
Limit
Upper
Limit
1, 1 -Dichioroethene
50
55.6
111
62.9
136
Benzene
50
49.6
99.2
73
124
Chlorobenzene
50
51.8
104
79.5
120
Toluene
50
47.5
95.0
75.8
116
Trichloroethene 1
50
52.4
105
75.1
F777T,8
Matrix Spike (MS) / Matrix Spike Duplicate (MSD)
Sample Spiked:
05020572-02
RunID:
1_050215E-1350195 Units: ug/Kg
Analysis Date:
02/16/2005 0:36 Analyst: GJH
Preparation Date:
02/07/2005 0:00 Prep By: FT Method SW5035
Analyte
Sample
Result
MS
Spike
Added
MS
Result
MS %
Recovery'
MSD
Spike
Added
MSD
Result
MSD %
Recovery
RPD
RPD
Limit
Low
Limit
High
Limit
1,1-Dichloroethene
ND
44.8
25.5
56.81
59.2
56.31
95.11
75.4 '
136.71
23.81
153
,Benzene
ND
44.8
33.5
70.81
59.2
48.21
78.31
35.91
42.21
23.91
149
Chlorobenzene
ND
44.8
28.2
62.8
59.2
33.31
56.11
16.6
43.7
19.8
141
Toluene
NDI
44.8
31.31
7E01
56.2j
42.71
72.11
30.7
43.6
21.1
144
Trichloroethene
ND
44.81
34.9
77.91
59.2
46.5
78.5
28.6
44.6
22.3
149
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL ' - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:58 PM

LAFAYETTELABORATORY
500 AMBASSADOR CAFFERY PARKWAY
®
SCOTT, LA 70583
Quality Control Report
[phone]
GREYHOUND HOUND LINES, INC.
GREYHOUND BLOUNT / 73.75029.0011
Analysis:
Volatile Organics Method 8260B +TBE
orkOrder: 05020306
Method:
SW8260B
Lab Batch ID: 35554
Method Blank Samples in Analytical Batch:
RunID:
Q_050216D-1352756 Units: ug/Kg Lab Sample ID
Client Sample ID
Analysis Date:
02/16/2005 17:33 Analyst: MHW 05020306-07A
GP-7 15'
Preparation Date:
02/07/2005 0:00 Prep By: FT Method SW5035
Analyte
Result
Rep Limit
111-Trichloroethane
ND
5.0
1 1 2 2-Tetrachloroethane
ND
5.0
112-Trichloroethane
ND
5.0
11-Dichloroethane
ND
5.0
11-Dichloroethene
ND
5.0
12-Dichloroethane
ND
5.0
1 2-Dichloro ro ane
ND
5.0
2-Butanone
ND
20
2-Hexanone
ND
10
4-Meth -2- entanone `
ND
10
Acetone
ND
100
Benzene
ND
5.0
Bromodichloromethane
ND
5.0
Bromoform
ND
5.0
Bromomethane
ND
10
Carbon disulfide
ND
5.0
Carbon tetrachloride
ND
5.0
Chlorobenzene
ND
5.0
Chloroethane
ND
10
Chloroform
ND
5.0
Chloromethane
ND
5.0
cis-1 3-Dichloro ro ene
ND
5.0
Dibromochloromethane
ND
5.0
Eth benzene
ND
5.0
Methyl tent -but ether
ND
5.0
Methylene chloride
ND
10
Styrene
ND
5.0
Tetrachloroethene
ND
5.0
Toluene
ND
5.0
trans-1 3-Dichloro ro ene
ND
5.0
Trichloroethene
ND
5.0
Trichlorofluoromethane
ND
5.0
Vinyi acetate
ND
10
Vinyl chloride
ND
10
cis-1,2-Dichloroethene
ND
5.0
rn,P-Xviene
ND
5.0
o-Xylene
ND
5.0
trans-l2-Dichloroethene
ND
5.0
1 2-Dichloroethene total
ND
5.0
XylenesJotal
ND
5.0
Surr:12-Dichloroethane-d4
96.6
66.1-151
Sum 4-Bromofluorobenzene
97.6
62-139
Surr: Toluene-d8
96.11
74.8-118
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL ° - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:58 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
GREYHOUND LINES, INC.
• i73,75029,001
Analysis: Volatile Organics Method 8260B +MTBE
Method: SW8260B
RunlD, Q_050216D-1352754 Units: ug/Kg
Analysis Date: 02/16/2005 16:08 Analyst: MHW
Preparation Date: 02/07/2005 0:00 Prep By: FT Method SW5035
WorkOrder: 05020306
Lab Batch ID: 35554
Analyte
LCS
Spike
Added
LCS
Result
LCS
Percent
Recovery
LCSD
Spike
Added
LCSD
Result
LCSD
Percent
Recovery
RPD
RPD
Limit
Lower
Limit
Upper
Limit
1,1-Dichloroethene
50
51.9
104
50.0
49.1
98.3
5.5
18.3
62.9
136
Benzene
50
55.1
110
50.0
53.2
106
3.5
20.9
73
124
Chlorobenzene
50
52.7
105
50.0
51.8
104
1.7
20.1
79.5
120
Toluene
50
47.6
95.1
50.0
43.1
86.2
9.8
17.8
75.8
116
Trichloroethene
501
51.6
1031
50.01
48.6
97.3
5.81
18.61
75.1
118
Matrix Spike (MS) / Matrix Spike Duplicate (MSD)
Sample Spiked:
05020306-07
RunID:
Q_050216D-1352758
Analysis Date:
02/16/2005 18:29
Preparation Date:
02/07/2005 0:00
Units: ug/Kg-dry
Analyst: MHW
Prep By: FT Method SW5035
Analyte
Sample
Result
MS
Spike
Added
MS
Result
MS %
Recovery
MSD
Spike
Added
MSD
Result
MSD %
Recovery
RPD
RPD
Limit
Low
Limit
High
Limit
1,1-Dichloroethene
ND
5330
4970
93.2
5330
4730
88.8
4.86
36.7
23.8
153
Benzene
ND
5330
6050
106
53301
6010
105
0.778
42.2
23.9
149
Chlorobenzene
ND
5330
5730
108
5330
5530
104
3.69
43.7
19.8
141
Toluene
5140
5330
9790
87.3
5330
9580
83.4
2.18
43.6
21.1
144
Trichloroethene
ND
53301
51001
95.8
5330
4940
92.6
3,331
44.6
22.31
149
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL ' - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:58 PM

Quality Control Report
GREYHOUND LINES, INC.
GREYHOUND BLOUT / 73.75029.0011
Analysis: Volatile Organics Method 8260B +MTBE
Method: SW8260B
Method Blank
RunID: 1_050216C-1353977 Units: ug/Kg
Analysis Date: 02/16/2005 14:26 Analyst: GJH
Preparation Date: 02/07/2005 0:00 Prep By: GJH Method SW5035
Analyte
Result
Rep Limit
11 1-Trichloroethane
ND
5.0
1 1 2 2-Tetrachloroethane
ND
5.0
112-Trichloroethane
ND
5.0
11-Dichloroethane
ND
5.0
11-Dichloroethene
ND
5.0
12-Dichloroethane
ND
5.0
1 2-Dichloro ro ane
ND
5.0
2-Butanone
ND
20
2-Hexanone
ND
10
4-Meth -2- entanone `
ND
10
Acetone
ND
100
Benzene
ND
5.0
Bromodichlorom ethane
ND
5.0
Bromoform
ND
5.0
Bromomethane
ND
10
Carbon disulfide
ND
5.0
Carbon tetrachloride
ND
5.0
Chlorobenzene
ND
5.0
Chloroethane
ND
10
Chloroform
ND
5.0
Chloromethane
ND
5.0
cis-1 3-Dichloro ro ene
ND
5.0
Dibromochloromethane
ND
5.0
Ethylbenzene
ND
5.0
Methyl tert-butyi ether
ND
5.0
Meth ene chloride
ND
10
Styrene
ND
5.0
Tetrachloroethene
ND
5.0
Toluene
ND
5.0
trans-1 3-Dichloro ro ene
ND
5.0
Trichloroethene
ND
5.0
T richlorofluorom ethane
ND
5.0
Vinyl acetate
ND
10
Vinyl chloride
ND
10
cis-12-Dichloroethene
ND
5.0
mp-Xyfene
ND
5.0
o-Xyiene
ND
5.0
trans-l2-Dichloroethene
ND
5.0
1,2-Dichloroethene total
ND
5.0
Xvienes,Total
ND
5.0
Surr:12-Dichloroethane-d4
114.9
66.1-151
Surr:4-Bromofluorobenzene
99.0
62-139
Surr: Toluene-d8
94.31
74.8-118
FAYETTELABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05020306
Lab Batch ID: 35597
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05020306-01 A
GP-1 15'
05020306-02A
GP-2 15'
05020306-05A
GP-5 10'
05020306-06A
GP-6 10'
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL ° - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported.
212812005 5:05:59 PM

I=AYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
GREYHOUND
t / • l
Analysis: Volatile Organics Method 8260B ¢MTBE
Method: SW8260B
RunID: 1_050216C-1353975 Units: ug/Kg
Analysis Date: 02/16/2005 13:27 Analyst: GJH
Preparation Date: 02/07/2005 0:00 Prep By: GJH Method SW5035
WorkOrder: 05020306
Lab Batch ID: 35597
Analyte
LCS
Spike
Added
LCS
Result
LCS
Percent
Recovery
LCSD
Spike
Added
LCSD
Result
LCSD
Percent
Recovery
RPD
RPD
Limit
Lower
Limit
Upper
Limit
1,1-Dichloroethene
50
56.9
114
50.0
48.1
96.2
16.8
18.3
62.9
136
Benzene
50
51.4
103
50.0
46.5
93.0
10.0
20.9
73
124
Chlorobenzene
50
51.4
103
50.0
49.0
98.1
4.7
20.1
79.5
120
Toluene
50
49.0
98.1
50.0
44.2
88.4
10.4
17.8
75.8
116
Trichloroethene
50
53.5
107
50.01
49.41
98.9
7.81
18.61
75,1
118
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL " - Recovery Outside Advisable QC Limits
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported. 2/28/2005 5:05:59 PM

Chain of Custody
2/28/2005 5:05:59 PM

Workorder: 05020306
Date and Time Received: 2/8/2005 11:00:00 AM
Temperature: 40C
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Received By: ALS
Carrier name: FedEx-Std 1 Day PM
Chilled by: Water Ice
1 .
Shipping container/cooler in good condition?
Yes
RI
No El
Not Present r-1
2.
Custody seals intact on shippping container/cooler?
Yes
No 0
Not Present El
3.
Custody seals intact on sample bottles?
Yes
❑
No ❑
Not Present
4.
Chain of custody present?
Yes
P-11
No ❑
5
Chain of custody signed when relinquished and received?
Yes
No ❑
®
Chain of custody agrees with sample labels?
Yes
0
No E]
7.
Samples in proper container/bottle?
Yes
No M
8.
Sample containers intact?
Yes
No 0
9.
Sufficient sample volume for indicated test?
Yes
No ❑
10.
All samples received within holding time?
Yes
F-/-]
No ❑
11.
Container/Temp Blank temperature in compliance?
Yes
No ❑
12.
Water - VOA vials have zero headspace?
Yes
❑
No ❑
Not Applicable
13.
Water - pH acceptable upon receipt?
Yes
❑
No ❑
Not Applicable
SPL Representative: I I
Client Name Contacted:
Non Conformance
Issues:
Client Instructions:
Contact Date & Time: 1 1
2/28/2005 5:06:00 PM

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LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
R"P. C E I V E D Case Narrative for:
GREYHOUND LINES, INC.
Certificate of Analysis Number:
,RALEIGH, NC 05010148
Report To: Project Flame: GREYHOUND BLOUNT ST./73.75092.0 �
ATC ASSOCIATES, INC. Site: GREYHOUND TERMINAL-RALEIGH
GABE ARAOS Site Address: #3145
2725 EAST MILBROOK RD SUITE 121 RALEIGH NC
PO Number:
RALEIGH
NC State: North Carolina
27604 State Cert. No.: 487
ph [phone] fax: Date Reported:
Matrix spike (MS) and matrix spike duplicate (MSD) samples are chosen and tested at random from an analytical batch of "like" matrix ',to check for
possible matrix effect. The MS and MSD will provide site specific matrix data only for those samples which are spiked by the laboratory. Since the
MS and MSD are chosen at random from an analytical batch, the sample chosen for spike purposes may or may not have been a sample
submitted in this sample;delivery group. The validity of the analytical procedures for which data is reported in this analytical report is determined by
the Laboratory Control Sample (LCS) and the Method Blank (MB). The Laboratory Control Sample (LCS) and the Method Blank (MB) are
processed with the samples and the MS/MSD to ensure method criteria are achieved throughout the entire analytical process.
Any other exceptions; associated with this report will be footnoted in the analytical result page(s) or the quality control summary page(s).
Please do not hesitate to contact us if you have any questions or comments pertaining to this data report. Please reference the above Certificate of
Analysis Number.
This report shall not be reproduced except in full, without the written approval of the laboratory. The reported results are only representative of the
samples submitted for testing.
SPL, Inc. is pleased to be of service to you. We anticipate working with you in fulfilling all your current and future analytical needs.
TOTAL NUMBER OF PAGES IN THIS REPORT: 3-0-- PAGES
1 / 12/2005
alph Frye �� Date
Project Manager

Certificate of Analysis Number:
05010148
Report To: ATC ASSOCIATES, INC.
GABE ARAOS
2725 EAST MILBROOK RD SUITE 121
RALEIGH
INC
27604-
ph [phone] fax: [phone]
Fax To:
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Project Name: GREYHOUND BLOUNT ST./73.75092.0
Site: GREYHOUND TERMINAL-RALEIGH
Site Address: #3145
RALEIGH NC
PO Number:
State: North Carolina
State Cert. No.: 487
Date Reported:
Client Sample ID
Lab Sample ID
Matrix
Date Collected
Date Received
COC ID
HOLD
MW-1
05010148-01
Water
1l4/2005 9:00:00 AM
1/5/2005 10:30:00 AM
245065
❑
MW-2
05010148-02
Water
1/4/2005 7:00:00 AM
1/5/2005 10:30:00 AM
245065
C]
MW-3
05010148-03
Water
1/4/2005 8:00:00 AM
1/5/2005 10:30:00 AM
245065
(�
MW-4
05010148-04
Water
1/4/2005 12:00:00 PM
1/5/2005 10:30:00 AM
245065
iMW-5
05010148-05
Water
1/4/2005 2:00:00 PM
1/5/2005 10:30:00 AM
245065
❑
MW-7
05010148-06
Water
1/4/2005 3:00:00 PM
1/5/2005 10:30:00 AM
245065
MW-10
05010148-07
Water
1/4/2005 11:00:00 AM
1/5/2005 10:30:00 AM
245065
MW-11
05010148-08
Water
1/4/2005 3:30:00 PM
1/5/2005 10:30:00 AM
245065
DW-1
05010148-09
Water
1/4/2005 1:00:00 PM
1/5/2005 10:30:00 AM
245065
DW-2
05010148-10
Water
1/4/2005 10:00:00 AM
1/5/2005 10:30:00 AM
245065
El
Rafph Frye
Project Manager
John D. Trahan
Laboratory Director
Tristan Davis
Quality Assurance Officer
1 /12/2005
Date
17JIM0011-10VI&I av

7001n
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-1
Collected: 01/04/2005 9:00
SPL Sample ID: 05010148-01
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
AROMATICS BY EPA 602
MCL E602
Units: ug/L
-PURGEABLE
Benzene
ND
0.3
1
1
01/07/05 15:52 P-C
1312876
Ethylbenzene
ND
0.23
1
1
01/07/05 15:52 P-C
1312876
Isopropyl ether
ND
0.11
1
1
01/07/05 15:52 P-C-
1312876
Methyl tert-butyl ether
ND
0.22
8
1
01/07/05 15:52 P-C
1312876
Naphthalene
30
0.25
10
1
01/07/05 15:52 P-C
1312876
Toluene
ND
0.94
1
1
01/07/05 15:52 P-C
1312876
m,p-Xylene
ND
0.75
2
1
01/07/05 15:52 P-C
1312876
o-Xylene
3.6
0.34
1
1
01/07/05 15:52 P-C
1312876
Xylenesjotal
3.6
0.34
1
1
01/07/05 15:52 P-C
1312876
Surr: 1,4-Difluorobenzene
89.6
0
% 41-143
1
01/07/05 15:52 P - C
1312876
Surr: 4-Bromofluorobenzene
104
0
% 39-160
1
01/07/05 15:52 P-C
1312876
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2-22 21 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-1
Collected: 01/04/2005 9:00 SPL Sample ID: 05010148-01-
Site:
GREYHOUND TERMINAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Lirnit
Dil. Factor QUAL Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS BY METHOD 624
MCL _E6 2 4 Units:_uq/L
1, 1, 1 -Trichloroethane
N D
0.48
5
1 01/06/05 12:06
FJA
1311353
1, 1,2,2-Tetrachloroethane
ND
1.4
5
1 01/06/05 12:06
FJA
1311353
1, 1,2-Trichloroethane
1, 1 -Dichloroethane
ND
N D
1.3
0.58
5
5
1 01/06/05 12:06
1 01/06/05 12:06
FJA
FJA
1311353
1311353
1, 1 -Dichloroethene
ND
0.78
5
1 01/06/05 12:06
FJA
1311353
1,2-Dibromoethane
ND
0.53
5
1 01/06/05 12:06
FJA
1311353
1,2-Dichlorobenzene
ND
0.77
5
1 01/06/05 12:06
FJA
1311353
1,2-Dichloroethane
ND
0.59
5
1 01/06/05 12:06
FJA
1311353
1,2-Dichloropropane
ND
0.49
5
1 01/06/05 12:06
FJA
1311353
1,3-Dichlorobenzene
ND
0.62
5
1 01/06/05 12:06
FJA
1311353
1,4-Dichlorobenzene
ND
0.71
5
1 01/06/05 12:06
FJA
1311353
2-Chloroethyl vinyl ether
ND
1.1
10
1 01/06/05 12:06
FJA
1311353
Bromodichlorom ethane
ND
0.68
5
1 01/06/05 12:06
FJA
1311353
Bromoform
ND
0.59
5
1 01/06/05 12:06
FJA
1311353
Bromomethane
Carbon tetrachloride
ND
ND
1.4
0.16
10
5
1 01/06/05 12:06
1 01/06/05 12:06
FJA
FJA
1311353
1311353
Chlorobenzene
ND
0.98
5
1 01/06/05 12:06
FJA
1311353
Chloroethane
ND
0.5
10
1 01/06/05 12:06
FJA
1311353
Chloroform
1.2
0.55
5
1 1 01/06/05 12:06
FJA
1311353
Chloromethane
ND
0.55
10
1 01/06/05 12:06
FJA
1311353
cis- 1,3-Dichloropropene
ND
0.52
5
1 01/06/05 12:06
FJA
1311353
Dibromochloromethane
ND
0.6
5
1 01/06/05 12:06
FJA
1311353
Dichlorodifluoromethane
ND
0.29
5
1 01/06/05 12:06
FJA
1311353
Methyl tert-butyl ether
ND
0.69
5
1 01/06/05 12:06
FJA
1311353
Methylene chloride
ND
1.8
5
1 01/06/05 12:06
FJA
1311353
Tetrachloroethene
ND
2.8
5
1 01/06/05 12:06
FJA
1311353
trans- 1, 3-D ichloropropene
ND
0.49
5
1 01/06/05 12:06
FJA
1311353
Trichloroethene
ND
0.28
5
1 01/06/05 12:06
FJA
1311353
Trichlorofluoromethane
ND
0.21
5
1 01/06/05 12:06
FJA
1311353
Vinyl chloride
ND
0.81
10
1 01/06/05 12:06
FJA
1311353
cis- 1,2-Dichloroethene
ND
0.62
5
1 01/06/05 12:06
FJA
1311353
trans- 1,2-Dichloroethene
ND
0.61
5
1 01/06/05 12:06
FJA
1311353
1,2-Dichloroethene, Total
Surr: 1,2-Dichloroethane-d4
ND
96.5
0.6
0 Yo
5
72.6-128
1 01/06/05 12:06
1 01/06/05 12:06
FJA
FJA
1311353
1311353
Surr: Toluene-c18
95.4
0 %
84.9-111
1 01/06/0512`06
FJA
1311353
Sirr: 4-Bromofluorobenzene
90.3
0 %
76.6-114
1 01/06/05 12:06
FJA
1311353
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2.22-21 PM

®R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-2
Collected: 01/04/2005 7:00
SPL Sample ID: 05010148-02
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
PURGEABLE AROMATICS BY EPA 602
MCL E602
Units: ug/L
Benzene
ND
0.3
1
1
01/07/05 16:24 P-C
1312877
Ethylbenzene
ND
0.23
1
1
01/07/05 16:24 P-C
1312877
Isopropyl ether
ND
0.11
1
1
01/07/05 16:24 P-C
1312877
Methyl tert-butyl ether
ND
0.22
8
1
01/07/05 16:24 P-C
1312877
ND
0.25
10
1
01/07/05 16:24 P-C
1312877
—Naphthalene
Toluene
ND
0.94
1
1
01/07/05 16:24 P-C
1312877
m,p-Xylene
ND
0.75
2
1
01/07/05 16:24 P-C
1312877
o-Xylene
ND
0.34
1
1
01/07/05 16:24 P-C
1312877
Xylenes,Total
ND
0.34
1
1
01/07/05 16:24 P-C
1312877
Surr: 1,4-Difluorobenzene
89.2
0
% 41-143
1
01/07/05 16:24 P-C
1312877
Surr: 4-Bromofluorobenzene
91.8
0
% 39-160
1
01/07/05 16:24 P-C
1312877
Qualifiers: ND/LI - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2:22 22 PM

.Z4
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-2
Collected: 01/04/2005 7.00
SPL Sample ID: 05010148-02
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
YOLATILE ORGANICS BY METHOD 624
MCL E624
Units: ug/L
1,1,1-Trichloroethane
ND
0.48
5
1
01/06/05 12:32
FJA
1311354
1,1,2,2-Tetrachloroethane
ND
1.4
5
1
01/06/05 12:32
FJA
1311354
1,1,2-Trichloroethane
ND
1.3
5
1
01/06/05 12:32
FJA
1311354
1,1-Dichloroethane
ND
0.58
5
1
01/06/05 12:32
FJA
1311354
1,1-Dichloroethene
ND
0.78
5
1
01/06/05 12:32
FJA
1311354
1,2-Dibromoethane
ND
0.53
5
1
01/06/05 12:32
FJA
1311354
1,2-Dichlorobenzene
ND
0.77
5
1
01/06/05 12:32
FJA
1311354
1,2-Dichloroethane
ND
0.59
5
1
01/06/05 12:32
FJA
1311354
1,2-Dichloropropane
ND
0.49
5
1
01/06/05 12:32
FJA
1311354
1,3-Dichlorobenzene
ND
0.62
5
1
01/06/05 12:32
FJA
1311354
1,4-Dichlorobenzene
ND
0.71
5
1
01/06/05 12:32
FJA
1311354
vinyl ether
ND
1.1
10
1
01/06/05 12:32
FJA
1311354
-2-Chloroethyl
Bromodichlorom ethane
ND
0.68
5
1
01/06/05 12:32
FJA
1311354
Bromoform
ND
0.59
5
1
01/06/05 12:32
FJA
1311354
Bromomethane
ND
1A
10
1
01/06/05 12:32
FJA
1311354
Carbon tetrachloride
ND
0.16
5
1
01/06/05 12:32
FJA
1311354
Chlorobenzene
ND
0.98
5
1
01/06/05 12:32
FJA
1311354
Chloroethane
ND
0.5
10
1
01/06/05 12:32
FJA
1311354
Chloroform
ND
0.55
5
1
01/06/05 12:32
FJA
1311354
Chloromethane
ND
0.55
10
1
01/06/05 12:32
FJA
1311354
cis- 1,3-Dichloropropene
ND
0.52
5
1
01/06/05 12:32
FJA
1311354
Dibromochloromethane
ND
0.6
5
1
01/06/05 12:32
FJA
1311354
Dichlorodifluoromethane
ND
0.29
5
1
01/06/05 12:32
FJA
1311354
tert-butyl ether
ND
0.69
5
1
01/06/05 12:32
FJA
1311354
-Methyl
Methylene chloride
ND
1.8
5
1
01/06/05 12:32
FJA
1311354
Tetrachloroethene
ND
2.8
5
1
01/06/05 12:32
FJA
1311354
trans- 1,3-Dichloropropene
ND
0.49
5
1
01/06/05 12:32
FJA
1311354
Trichloroethene
ND
0.28
5
1
01/06/05 12:32
FJA
1311354
Trichlorofluoromethane
ND
0.21
5
1
01/06/05 12:32
FJA
1311354
Vinyl chloride
ND
0.81
10
1
01/06/05 12:32
FJA
1311354
cis- 1,2-Dichloroethene
ND
0.62
5
1
01/06/05 12:32
FJA
1311354
trans- 1,2-Dichloroethene
ND
0.61
5
1
01/06/05 12:32
FJA
1311354
1,2-Dichloroethene, Total
ND
0.6
5
1
01/06/05 12:32
FJA
1311354
Surr: 1,2-Dichloroethane-d4
90.9
0 1/o
72.6-128
1
01/06/0512:32
FJA
1311354
Surr: Toluene-d8
94.8
0 '/o
84.9-111
1
01/06/05 12:32
FJA
1311354
Surr: 4-Bromofluorobenzene
85.6
0 1/o
76.6-114
1
01/06/05 12:32
FJA
1311354
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and POL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2:22:22 PM

AMAC)z
Am, R.
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-3
Collected: 01/04/2005 8:00 SPL Sample ID: 05010148-03
Site:
GREYHOUND TERM INAL-R.ALE IG H
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL Date Analyzed Analyst
Seq. #
AROMATICS BY EPA 602
MCL E602 Units: ug/L
-PURGEABLE
Benzene
5.2
0.3
1
1 01/07/05 16:54 P-C
1312878
1.3
0.23
1
1 01/07/05 16:54 P-C
1312878
-Ethylbenzene
Isopropyl ether
ND
0.11
1
1 01/07/05 16:54 P-C
1312878
Methyl tert-butyl ether
ND
0.22
8
1 01/07/05 16:54 P-C
1312878
100
0.25
10
1 01/07/05 16:54 P-C
1312878
-Naphthalene
Toluene
1.3
0.94
1
1 01/07/05 16:54 P-C
1312878
11
0.75
2
1 01/07/05 16:54 P-C
1312878
-m,p-Xylene
o-Xylene
11
0.34
1
1 01/07/05 16:54 P-C
1312878
Xylenesjotal
22
0.34
1
1 01/07/05 16:54 P-C
1312878
Surr: 1,4-Difluorobenzene
88.8
0
% 41-143
1 01/07/05 16:54 P-C
1312878
Surr: 4-Bromofluorobenzene
108
0
% 39-160
1 01/07/05 16:54 P-C
1312878
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2:22:23 PM

40 Z
ia Awd
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-3
Collected: 01/04/2005 8:00
SPL Sample ID: 05010148-03
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Lirnit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS BY METHOD 624
MCL E624
Units: ug/L
1, 1, 1 -Trichloroethane
ND
0.48
5
1
01/06/05 12:57
FJA
1311355
1, 1,2,2-Tetrachloroethane
ND
1.4
5
1
01/06/05 12:57
FJA
1311355
1, 1,2-Trichloroethane
ND
1.3
5
1
01/06/05 12:57
FJA
1311355
1,1-Dichloroethane
ND
0.58
5
1
01/06/05 12:57
FJA
1311355
1, 1 -Dichloroethene
ND
0.78
5
1
01/06/05 12:57
FJA
1311355
1,2-Dibromoethane
ND
0.53
5
1
01/06/05 12:57
FJA
1311355
1,2-Dichlorobenzene
ND
0.77
5
1
01/06/05 12:57
FJA
1311355
1,2-Dichloroethane
ND
0.59
5
1
01/06/05 12:57
FJA
1311355
1,2-Dichloropropane
ND
0.49
5
1
01/06/05 12:57
FJA
1311355
1,3-Dichlorobenzene
ND
0.62
5
1
01/06/05 12:57
FJA
1311355
1,4-Dichlorobenzene
ND
0.71
5
1
01/06/05 12:57
FJA
1311355
2-Chloroethyl vinyl ether
ND
1.1
10
1
01/06/05 12:57
FJA
1311355
Bromodichloromethane
ND
0.68
5
1
01/06/05 12:57
FJA
1311355
Bromoform
ND
0.59
5
1
01/06/05 12:57
FJA
1311355
Bromomethane
ND
1.4
10
1
01/06/05 12:57
FJA
1311355
Carbon tetrachloride
ND
0.16
5
1
01/06/05 12:57
FJA
1311355
Chlorobenzene
ND
0.98
5
1
01/06/05 12:57
FJA
1311355
Chloroethane
ND
0.5
10
1
01/06/05 12:57
FJA
1311355
Chloroform
ND
0.55
5
1
01/06/05 12:57
FJA
1311355
Chloromethane
ND
0.55
10
1
01/06/05 12:57
FJA
1311355
cis- 1,3-Dichloropropene
ND
0.52
5
1
01/06/05 12:57
FJA
1311355
Dibromochloromethane
ND
0.6
5
1
01/06/05 12:57
FJA
1311355
Dichlorodifluoromethane
ND
0.29
5
1
01/06/05 12:57
FJA
1311355
Methyl tert-butyl ether
ND
0.69
5
1
01/06/05 12:57
FJA
1311355
Methylene chloride
ND
1.8
5
1
01/06/05 12:57
FJA
1311355
Tetrachloroethene
ND
2.8
5
1
01/06/05 12:57
FJA
1311355
trans- 1,3-Dichloropropene
ND
0.49
5
1
01/06/05 12:57
FJA
1311355
Trichloroethene
ND
0.28
5
1
01/06/05 12:57
FJA
1311355
Trichlorofluoromethane
ND
0.21
5
1
01/06/05 12:57
FJA
1311355
chloride
ND
0.81
10
1
01/06/05 12:57
FJA
1311355
-Vinyl
cis- 1,2-Dichloroethene
ND
0.62
5
1
01/06/05 12:57
FJA
1311355
trans- 1,2-Dichloroethene
ND
0.61
5
1
01/06/05 12:57
FJA
1311355
1,2-Dichloroethene, Total
ND
0.6
5
1
01/06/05 12:57
FJA
1311355
Sum 1,2-Dichloroethane-d4
91.4
0 1/o
72.6-128
1
01/06/05 12-.57
FJA
1311355
Surr: Toluene-d8
95.5
0 Yo
84.9-111
1
01/06/05 12:57
FJA
1311355
Surr: 4-Bromofluorobenzene
95.3
0 %
76.6-114
1
01/06/05 12:57
FJA
1311355
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2-22:23 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-4
Collected: 01/04/2005 12:00
SPL Sample ID: 05010148-04
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Lirnit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
AROMATICS BY EPA 602
MCL E602
Units: u /L
-PURGEABLE
Benzene
2.5
0.3
1
1
01/07/05 17:24 P-C
1312879
Ethylbenzene
ND
0.23
1
1
01/07/05 17:24 P-C
1312879
Isopropyl Ether
22
0.11
1
1
01/07/05 17:24 P-C
1312879
Methyl tert-butyl ether
ND
0.22
8
1
01/07/05 17:24 P-C
1312879
Naphthalene
3.5
0.25
10
1
01/07/05 17:24 P-C
1312879
Toluene
ND
0.94
1
1
01/07/05 17:24 P-C
1312879
m,p-Xylene
ND
0.75
2
1
01/07/05 17:24 P-C
1312879
o-Xylene
ND
0.34
1
1
01/07/05 17:24 P-C
1312879
Xylenesjotal
ND
0.34
1
1
01/07/05 17:24 P-C
1312879
Surr: 1,4-Difluorobenzene
106
0
% 41-143
1
01/07/05 17:24 P - C
1312879
Surr: 4-Bromofluorobenzene
94.6
0
% 39-160
1
01/07/05 17:24 P-C
1312879
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2 22:23 PM

®R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-4
Collected: 01/04/2005 12:00
SPL Sample ID: 05010148-04
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
ORGANICS BY METHOD 624
MCL E624
Units: ug/L
_VOLATILE
1,1,1-Trichloroethane
ND
0.48
5
1
01/06/05 13:22
FJA
1311356
1, 1,2,2-Tetrachloroethane
ND
1.4
5
1
01/06/05 13:22
FJA
1311356
1, 1,2-T rich loroethane
ND
1.3
5
1
01/06/05 13:22
FJA
1311356
1,1-Dichloroethane
ND
0.58
5
1
01/06/05 13:22
FJA
1311356
1,1 -Dichloroethene
ND
0.78
5
1
01/06/05 13:22
FJA
1311356
1,2-Dibromoethane
ND
0.53
5
1
01/06/05 13:22
FJA
1311356
1,2-Dichlorobenzene
ND
0.77
5
1
01/06/05 13:22
FJA
1311356
1,2-Dichloroethane
ND
0.59
5
1
01/06/05 13:22
FJA
1311356
1,2-Dichloropropane
ND
0.49
5
1
01/06/05 13:22
FJA
1311356
1,3-Dichlorob.enzene
ND
0.62
5
1
01/06/05 13:22
FJA
1311356
1,4-Dichlorobenzene
ND
0.71
5
1
01/06/05 13:22
FJA
1311356
vinyl ether
ND
1.1
10
1
01/06/05 13:22
FJA
1311356
-2-Chloroethyl
Bromodich lorom ethane
ND
0.68
5
1
01/06/05 13:22
FJA
1311356
Bromoform
ND
0.59
5
1
01/06/05 13:22
FJA
1311356
Bromomethane
ND
1.4
10
1
01/06/05 13:22
FJA
1311356
Carbon tetrachloride
ND
0.16
5
1
01/06/05 13:22
FJA
1311356
Chlorobenzene
23
0.98
5
1
01/06/05 13:22
FJA
1311356
Chloroethane
ND
0.5
10
1
01/06/05 13:22
FJA
1311356
Chloroform
ND
0.55
5
1
01/06/05 13:22
FJA
1311356
Chloromethane
ND
0.55
10
1
01/06/05 13:22
FJA
1311356
cis- 1, 3-Dichloropropene
ND
0.52
5
1
01/06/05 13:22
FJA
1311356
Dibromochloromethane
ND
0.6
5
1
01/06/05 13:22
FJA
1311356
Dichlorodifluoromethane
ND
0.29
5
1
01/06/05 13:22
FJA
1311356
tert-butyl ether
ND
0.69
5
1
01/06/05 13:22
FJA
1311356
-Methyl
Methylene chloride
ND
1.8
5
1
01/06/05 13:22
FJA
1311356
Tetrachloroethene
ND
2.8
5
1
01/06/05 13:22
FJA
1311356
trans- 1,3-Dichloropropene
ND
0.49
5
1
01/06/05 13:22
FJA
1311356
Trichloroethene
32
0.28
5
1
01/06/05 13:22
FJA
1311356
Trichlorof luorom ethane
ND
0.21
5
1
01/06/05 13:22
FJA
1311356
chloride
ND
0.81
10
1
01/06/05 13:22
FJA
1311356
-Vinyl
cis- 1,2-Dichloroethene
ND
0.62
5
1
01/06/05 13:22
FJA
1311356
trans- 1,2-Dichloroethene
ND
0.61
5
1
01/06/05 13:22
FJA
1311356
1,2-Dichloroethene, Total
ND
0.6
5
1
01/06/05 13:22
FJA
1311356
Surr: 1,2-Dichloroethane-d4
95.2
0 1/o
72.6-128
1
01/06/05 13:22
FJA
1311356
Surr: Toluene-d8
96.0
0 %
84.9-111
1
01/06/05 13:22
FJA
1311356
Surr: 4-Bromofluorobenzene
87.1
0 1/o
76.6-114
1
01/06/05 13:22
FJA
1311356
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2 22 24 PM

®R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-5
Collected: 01/04/2005 14:00
SPL Sample ID: 05010148-05
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
AROMATICS BY EPA 602
MCL E602
Units: ug/L
-PURGEABLE
Benzene
ND
0.3
1
1
01/07/05 17:55 P-C
1312880
ND
0.23
1
1
01/07/05 17:55 P-C
1312880
-Ethylbenzene
Isopropyl Ether
1.3
0.11
1
1
01/07/05 17:55 P-C
1312880
Methyl tert-butyl ether
5.2
0.22
8
1
01/07/05 17:55 P-C
1312880
ND
0.25
10
1
01/07/05 17:55 P-C
1312880
-Naphthalene
Toluene
ND
0.94
1
1
01/07/05 17:55 P - C
1312880
m,p-Xylene
ND
0.75
2
1
01/07/05 17:55 P-C
1312880
ND
0.34
1
1
01/07/05 17:55 P-C
1312880
-o-Xylene
ND
0.34
1
1
01/07/05 17:55 P-C
1312880
-Xylenes,Total
Surr: 1,4-Difluorobenzene
88.9
0
% 41-143
1
01/07/05 17:55 P-C
1312880
Surr: 4-Bromofluorobenzene
90.8
0
% 39-160
1
01/07/05 17:55 P-C
1312880
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2-22'24 PM

®R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-5
Collected: 01/04/2005 14:00
SPL Sample ID: 05010148-05
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method
Result
MDL
Rep.Lirnit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS BY METHOD 624
MCL E624
Units: ug/L
1,1,1-Trichloroethane
ND
0.48
5
1
01/06/05 13:47
FJA
1311357
1; 1,2,2-Tetrachloroethane
ND
1.4
5
1
01/06/05 13:47
FJA
1311357
1, 1,2-Trichloroethane
ND
1.3
5
1
01/06/05 13:47
FJA
1311357
1,1-Dichloroethane
ND
0.58
5
1
01/06/05 13:47
FJA
1311357
1,1-Dichloroethene
-ND
0.78
5
1
01/06/05 13:47
FJA
1311357
1,2-Dibromoethane
ND
0.53
5
1
01/06/05 13:47
FJA
1311357
1,2-Dichlorobenzene
ND
0.77
5
1
01/06/05 13:47
FJA
1311357
1,2-Dichloroethane
ND
0.59
5
1
01/06/05 13:47
FJA
1311357
1,2-Dichloropropane
ND
0.49
5
1
01/06/05 13:47
FJA
1311357
1,3-Dichlorobenzene
ND
0.62
5
1
01/06/05 13:47
FJA
1311357
1,4-Dichlorobenzene
ND
0.71
5
1
01/06/05 13:47
FJA
1311357
2-Chloroethyl vinyl ether
ND
1.1
10
1
01/06/05 13:47
FJA
1311357
Bromodichloromethane
ND
0.68
5
1
01/06/05 13:47
FJA
1311357
Bromoform
ND
0.59
5
1
01/06/05 13:47
FJA
1311357
Bromomethane
ND
1.4
10
1
01/06/05 13:47
FJA
1311357
Carbon tetrachloride
ND
0.16
5
1
01/06/05 13:47
FJA
1311357
Chlorobenzene
ND
0.98
5
1
01/06/05 13:47
FJA
1311357
Chloroethane
ND
0.5
10
1
01/06/05 13:47
FJA
1311357
Chloroform
ND
0.55
5
1
01/06/05 13:47
FJA
1311357
Chloromethane
ND
0.55
10
1
01/06/05 13:47
FJA
1311357
cis- 1, 3-Dichloropropene
ND
0.52
5
1
01/06/05 13:47
FJA
1311357
Dibromochloromethane
ND
0.6
5
1
01/06/05 13:47
FJA
1311357
Dichlorodifluoromethane
ND
0.29
5
1
01/06/05 13:47
FJA
1311357
tert-butyl ether
5.1
0.69
5
1
01/06/05 13:47
FJA
1311357
-Methyl
chloride
ND
1.8
5
1
01/06/05 13:47
FJA
1311357
-Methylene
Tetrachloroethene
ND
2,8
5
1
01/06/05 13:47
FJA
1311357
trans- 1,3-Dichloropropene
ND
0.49
5
1
01/06/05 13:47
FJA
1311357
Trichloroethene
6.7
0.28
5
1
01/06/05 13:47
FJA
1311357
Trichlorofluoromethane
ND
0.21
5
1
01/06/05 13:47
FJA
1311357
Vinyl chloride
ND
0.81
10
1
01/06/05 13:47
FJA
1311357
cis- 1,2-Dichloroethene
ND
0.62
5
1
01/06/05 13:47
FJA
1311357
trans- 1,2-Dichloroethene
ND
0.61
5
1
01/06/05 13:47
FJA
1311357
1,2-Dichloroethene, Total
ND
0.6
5
1
01/06/05 13:47
FJA
1311357
Surr: 1,2-Dichloroethane-d4
93.3
0 %
72.6-128
1
01/06/05'13;47
FJA
1311357
Surr: Toluene-d8
93.8
0 %
84.9-111
1
01/06/05 13:47
FJA
1311357
Surr: 4-Bromofluorobenzene
84.0
0 %
76.6-114
1
01/06/05 13:47
FJA
1311357
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2,22:25 PM

0IR
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-7
Collected: 01/04/2005 15:00
SPL Sample ID: 05010148-06
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
PURGEABLE AROMATICS BY EPA 602
MCL E602
Units: ug/L
Benzene
ND
0.3
1
1
01/07/05 18:25 P—C
1312881
Ethylbenzene
ND
0.23
1
1
01/07/05 18:25 P—C
1312881
Isopropyl Ether
21
0.11
1
1
01/07/05 18:25 P—C
1312881
Methyl tert-butyl ether
5.7
0.22
8
1
01/07/05 18:25 P—C
1312881
Naphthalene
ND
0.25
10
1
01/07/05 18:25 P—C
1312881
Toluene
ND
0.94
1
1
01/07/05 18:25 P—C
1312881
m,p-Xylene
ND
0.75
2
1
01/07/05 18:25 P—C
1312881
o-Xylene
ND
0.34
1
1
01/07/05 18:25 P—C
1312881
Xylenes,Total
ND
0.34
1
1
01/07/05 18:25 P—C
1312881
Surr: 1,4-Difluorobenzene
89.8
0
% 41-143
1
01/07/05 18:25 P—C
1312881
Surr: 4-Bromofluorobenzene
91.1
0
% 39-160
1
01/07/05 18:25 P—C
1312881
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2:22.25 PM

®
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-7
Collected: 01/04/2005 15:00
SPL Sample ID: 05010148-06
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS BY METHOD 624
MCL E624
Units: ug/L
1, 1, 1 -Trichloroethane
ND
0.48
5
1
01/06/05 14:13
FJA
1311358
1, 1,2,2-Tetrachloroethane
ND
1.4
5
1
01/06/05 14:13
FJA
1311358
1, 1,2-Trichloroethane
N D
1.3
5
1
01/06/05 14:13
FJA
1311358
1,1-Dichloroethane
ND
0.58
5
1
01/06/05 14:13
FJA
1311358
1,1-Dichloroethene
ND
0.78
5
1
01/06/05 14:13
FJA
1311358
1,2-Dibromoethane
ND
0.53
5
1
01/06/05 14:13
FJA
1311358
1,2-Dichlorobenzene
ND
0.77
5
1
01/06/05 14:13
FJA
1311358
1,2-Dichloroethane
ND
0.59
5
1
01/06/05 14:13
FJA
1311358
1,2-Dichloropropane
ND
0.49
5
1
01/06/05 14:13
FJA
1311358
1,3-Dichlorobenzene
ND
0.62
5
1
01/06/05 14:13
FJA
1311358
1,4-Dichlorobenzene
ND
0.71
5
1
01/06/05 14:13
FJA
1311358
2-Chloroethyl vinyl ether
ND
1.1
10
1
01/06/05 14:13
FJA
1311358
Bromodichloromethane
ND
0.68
5
1
01/06/05 14:13
FJA
1311358
Bromoform
ND
0.59
5
1
01/06/05 14:13
FJA
1311358
Bromomethane
ND
1.4
10
1
01/06/05 14:13
FJA
1311358
Carbon tetrachloride
ND
0.16
5
1
01/06/05 14:13
FJA
1311358
Chlorobenzene
ND
0.98
5
1
01/06/05 14:13
FJA
1311358
Chloroethane
ND
0.5
10
1
01/06/05 14:13
FJA
1311358
Chloroform
ND
0.55
5
1
01/06/05 14:13
FJA
1311358
Chloromethane
ND
0.55
10
1
01/06/05 14:13
FJA
1311358
cis- 1, 3-Dichloropropene
ND
0.52
5
1
01/06/05 14:13
FJA
1311358
Dibromochloromethane
ND
0.6
5
1
01/06/05 14:13
FJA
1311358
Dichlorodifluoromethane
ND
0.29
5
1
01/06/05 14:13
FJA
1311358
Methyl tert-butyl ether
5.1
0.69
5
1
01/06/05 14:13
FJA
1311358
chloride
ND
1.8
5
1
01/06/,05 14:13
FJA
1311358
-Methylene
Tetrachloroethene
ND
2.8
5
1
01/06/05 14:13
FJA
1311358
trans- 1, 3-Dichloropropene
ND
0.49
5
1
01/06/05 14:13
FJA
1311358
Trichloroethene
76
0.28
5
1
01/06/05 14:13
FJA
1311358
Trichlorofluoromethane
ND
0.21
5
1
01/06/05 14:13
FJA
1311358
chloride
ND
0.81
10
1
01/06/05 14:13
FJA
1311358
-Vinyl
cis- 1, 2-Dichloroethene
ND
0.62
5
1
01/06/05 14:13
FJA
1311358
trans- 1,2-Dichloroethenb
ND
0.61
5
1
01/06/05 14:13
FJA
1311358
1,2-Dichloroethene, Total
ND
0.6
5
1
01/06/05 14:13
FJA
1311358
Surr: 1,2-Dichloroethane-d4
93.1
0 %
72.6-128
1
01/06/05 1413
FJA
1311358
Surr: Toluene-d8
92.6
0 %
84.9-111
1
01/06/05 14:13
-FJA
1311358
Surr: 4-Bromofluorobenzene
84.0
0 %
76.6-114
1
01/06/05 14:13
FJA
1311358
Qualifiers: ND/Ll - Not Detected at the Reporting Limit
B - Analyte detected in the associated Method Blank
* - Surrogate Recovery Outside Advisable QC Limits
J - Estimated Value between MDL and POL
E - Concentrations exceeding Calibration range of Instrument
>MCL - Result Over Maximum Contamination Limit(MCL)
D - Surrogate Recovery Unreportable due to Dilution
MI - Matrix Interference
1/12/2005 2-22:26 PM

_Z4 ®R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-10
Collected: 01/04/2005 11:00
SPL Sample ID: 05010148-07
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
AROMATICS BY EPA 602
MCL E602
Units: ug/L
-PURGEABLE
Benzene
ND
0.3
1
1
01/07/05 18:55 P-C
1312882
Ethylbenzene
ND
0.23
1
1
01/07/05 18:55 P-C
1312882
Isopropyl ether
ND
0.11
1
1
01/07/05 18:55 P-C
1312882
Methyl tert-butyl ether
ND
0.22
8
1
01/07105 18:55 P-C
1312882
Naphthalene
IND
0.25
10
1
01/07/05 18:55 P-C
1312882
Toluene
ND
0.94
1
1
01/07/05 18:55 P-C
1312882
m,p-Xylene
ND
0.75
2
1
01/07/05 18:55 P-C
1312882
o-Xylene
ND
0.34
1
1
01/07/05 18:55 P-C
1312882
Xylenesjotal
ND
0.34
1
1
01/07/05 18:55 P-C
1312882
Surr: 1,4-Difluorobenzene
88.3
0
% 41-143
1
01/07/05 18:55 P-C
1312882
Surr: 4-Bromofluorobenzene
90.3
0
% 39-160
1
01/07/05 18:55 P-C
1312882
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and POL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2 22 26 PM

t Ago AAC A 009MOME01 U11
00 rR�
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-10
Collected: 01/04/2005 11:00
SPL Sample ID: 05010148-07
Site:
GREYHOUND TERM I NAL-RALEIG H
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS BY METHOD 624
MCL E624
Units: ug/L
-
1, 1, 1 -Trichloroethane
ND
0.48
5
1
01/06/05 14:38
FJA
1311359
1, 1,2,2-Tetrachloroethane
ND
1.4
5
1
01/06/05 14:38
FJA
1311359
1, 1,2-Trichloroethane
ND
1.3
5
1
01/06/05 14:38
FJA
1311359
1,1-Dichloroethane
ND
0.58
5
1
01/06/05 14:38
FJA
1311359
1,1-Dichloroethene
ND
0.78
5
1
01/06/05 14:38
FJA
1311359
1,2-Dibromoethane
ND
0.53
5
1
01/06/05 14:38
FJA
1311359
1,2-Dichlorobenzene
ND
0.77
5
1
01/06/05 14:38
FJA
1311359
1,2-Dichloroethane
ND
0.59
5
1
01/06/05 14:38
FJA
1311359
1,2-Dichloropropane
ND
0,49
5
1
01/06/05 14:38
FJA
1311359
1,3-Dichlorobenzene
ND
0.62
5
1
01/06/05 14:38
FJA
1311359
1,4-Dichlorobenzene
ND
0.71
5
1
01/06/05 14:38
FJA
1311359
2-Chloroethyl vinyl ether
ND
1.1
10
1
01/06/05 14:38
FJA
1311359
B romodichlorom ethane
ND
0.68
5
1
01/06/05 14:38
FJA
1311359
Bromoform
ND
0.59
5
1
01/06/05 14:38
FJA
1311359
Bromomethane
ND
1.4
10
1
01/06/05 14:38
FJA
1311359
Carbon tetrachloride
ND
0.16
5
1
01/06/05 14:38
FJA
1311359
Chlorobenzene
ND
0.98
5
1
01/06/05 14:38
FJA
1311359
Chloroethane
ND
0.5
10
1
01/06/05 14:38
FJA
1311359
Chloroform
ND
0.55
5
1
01/06/05 14:38
FJA
1311359
Chloromethane
ND
0.55
10
1
01/06/05 14:38
FJA
1311359
cis- 1, 3-Dichloropropene
ND
0.52
5
1
01/06/05 14:38
FJA
1311359
Dibromochloromethane
ND
0.6
5
1
01/06/05 14:38
FJA
1311359
Dichlorodifluoromethane
ND
0.29
5
1
01/06/05 14:38
FJA
1311359
Methyl tert-butyl ether
ND
0.69
5
1
01/06/05 14:38
FJA
1311359
Methylene chloride
ND
1.8
5
1
01/06/05 14:38
FJA
1311359
Tetrachloroethene
ND
2.8
5
1
01/06/05 14:38
FJA
1311359
trans- 1 , 3-Dichloropropene
ND
0.49
5
1
01/06/05 14:38
FJA
1311359
Trichloroethene
ND
0,28
5
1
01/06/05 14:38
FJA
1311359
Trichlorofluoromethane
ND
021
5
1
01/06/05 14:38
FJA
1311359
Vinyl chloride
ND
0.81
10
1
01/06/05 14:38
FJA
1311359
cis- 1 2-Dichloroethene
ND
0.62
5
1
01/06/05 14:38
FJA
1311359
trans - 1, 2-Dich loroethene
ND
0.61
5
1
01/06/05 14:38
FJA
1311359
1,2-Dichloroethene, Total
ND
0.6
5
1
01/06/05 14:38
FJA
1311359
Surr: 1,2-Dichloroethane-d4
92.0
0 %
72.6-128
1
01/06/05,14-38
FJA
1311359
Sum Toluene-d8
90.7
0 %
84.9-111
1
01/06/05 14:38
FJA
1311359
Surr: 4-Bromofluorobenzene
84.2
0 %
76.6-114
1
01/06/05 14:38
FJA
1311359
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2:22.26 PM

AOF
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-11
Collected: 01/04/2005 15:30
SPIL Sample ID: 05010148-08
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed Analyst
Seq. #
-PURGEABLE AROMATICS BY EPA 602
MCL E602
Units: ug/L
Benzene
0.58
0.3
1
1
-
01/07/05 19:25 P C
1312883
Ethylbenzene
ND
0.23
1
1
01/07/05 19:25 P C
1312883
Isopropyl Ether
31
0.11
1
1
01/07/05 19:25 P-C
1312883
Methyl tert-butyl ether
ND
0.22
8
1
01/07/05 19:25 P-C
1312883
Naphthalene
ND
0.25
10
1
01/07/05 19:25 P--c
1312883
Toluene
ND
0.94
1
1
01/07/05 19:25 P-C
1312883
m,p-Xylene
ND
0.75
2
1
01/07/05 19:25 P-C
1312883
o-Xylene
ND
0.34
1
1
01/07/05 19:25 P-C
1312883
Xylenesjotal
ND
0.34
1
1
01/07/05 19:25
1312883
Sum 1,4-Difluorobenzene
89.1
0
% 41-143
1
01/07/05 19:25 P-C
1312883
Surr: 4-Bromofluorobenzene
92.6
0
% 39-160
1
01/07/05 19:25 P-C
1312883
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2:22 27 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID MW-1 1
Collected: 01/04/2005 15:30
SPL Sample ID: 05010148-08
Site:
GREYHOUND TER MINAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS BY METHOD 624
MCL E624
Units: ug/L
1,1,1-Trichloroethane
ND
0.48
5
1
01/06/05 15:03
FJA
1311360
1, 1,2,2-Tetrachloroethane
ND
1.4
5
1
01/06/05 15:03
FJA
1311360
1, 1,2-Trichloroethane
ND
1.3
5
1
01/06/05 15:03
FJA
1311360
1,1-Dichloroethane
N D
0.58
5
1
01/06/05 15:03
FJA
1311360
M-Dichloroethene
ND
0.78
5
1
01/06/05 15:03
FJA
1311360
1,2-Dibromoethane
ND
0,53
5
1
01/06/05 15:03
FJA
1311360
1,2-Dichlorobenzene
7
0.77
5
1
01/06/05 15:03
FJA
1311360
1,2-Dichloroethane
ND
0.59
5
1
01/06/05 15:03
FJA
1311360
ND
0.49
5
1
01/06/05 15:03
FJA
1311360
-1,2-Dichloropropane
1,3-Dichlorobenzene
ND
0.62
5
1
01/06/05 15:03
FJA
1311360
1,4-Dichlorobenzene
ND
0.71
5
1
01/06/05 15:03
FJA
1311360
2-Chloroethyl vinyl ether
ND
1.1
10
1
01/06/05 15:03
FJA
1311360
Bromodichloromethane
ND
0.68
5
1
01/06/05 15:03
FJA
1311360
Bromoform
ND
0.59
5
1
01/06/05 15:03
FJA
1311360
Bromomethane
ND
1.4
10
1
01/06/05 15:03
FJA
1311360
Carbon tetrachloride
ND
0.16
5
1
01/06/05 15:03
FJA
1311360
Chlorobenzene
ND
0.98
5
1
01/06/05 15:03
FJA
1311360
Chloroethane
ND
0.5
10
1
01/06/05 15:03
FJA
1311360
Chloroform
ND
0.55
5
1
01/06/05 15:03
FJA
1311360
Chloromethane
ND
0.55
10
1
01/06/05 15:03
FJA
1311360
cis- 1, 3-Dichloropropene
ND
0.52
5
1
01/06/05 15:03
FJA
1311360
Di bromochlorom ethane
ND
0.6
5
1
01/06/05 15:03
FJA
1311360
Dichlorodifluoromethane
ND
0.29
5
1
01/06/05 15:03
FJA
1311360
Methyl tert-butyl ether
ND
0.69
5
1
01/06/05 15:03
FJA
1311360
Methylene chloride
ND
1.8
5
1
01/06/05 15:03
FJA
1311360
Tetrachloroethene
ND
2.8
5
1
01/06/05 15:03
FJA
1311360
trans- 1, 3-Dichloropropene
ND
0.49
5
1
01/06/05 15:03
FJA
1311360
Trichloroethene
60
0.28
5
1
01/06/05 15:03
FJA
1311360
Trichlorof luorom ethane
ND
0.21
5
1
01/06/05 15:03
FJA
1311360
Vinyl chloride
ND
0.81
10
1
01/06/05 15:03
FJA
1311360
cis- 1, 2-Dichloroethene
ND
0.62
5
1
01/06/05 15:03
FJA
1311360
trans- 1,2-Dichloroethene
ND
0.61
5
1
01/06/05 15:03
FJA
1311360
1,2-Dichloroethene, Total
ND
0.6
5
1
01/06/05 15:03
FJA
1311360
Surr: 1,2-Dichloroethane-d4
91.2
0 %
72.6-128
1
01/06/05 15:03
FJA
1311360
Surr: Toluene-d8
93.1
0 1/o
84.9-111
1
01/06/05 15:03
FJA
1311360
Surr: 4-Bromofluorobenzene
83.5
0 1/o
76.6-114
1
01/06/05 15:03
FJA
1311360
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2.22:27 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID DW-1
Collected: 01/04/2005 13:00 SPL Sample ID: 05010148-09
Site:
GREYHOUND TERMINAL- LEIGH
Analyses/Method Result
MDL
Rep.Lirnit
Dil. Factor QUAL Date Analyzed Analyst
Seq. #
-PURGEABLE AROMATICS BY EPA 602
MCL
E602 Units: uq/L
Benzene ND
0.3
1
1
-
01/07/05 19:56 P-C
1312884
Ethylbenzene ND
0.23
1
1
01/07/05 19:56 P C
1312884
Isopropyl ether ND
0.11
1
1
01/07/05 19:56 P-C
1312884
Methyl tert-butyl ether ND
0.22
8
1
01/07/05 19:56 P-C
1312884
Naphthalene -ND
0.25
10
1
01/07/05 19:56 P-C
1312884
Toluene ND
0.94
1
1
01/07/05 19:56 P-C
1312884
m,p-Xylene ND
0.75
2
1
01/07/05 19:56 P-C
1312884
o-Xylene ND
0.34
1
1
01/07/05 19:56 P-C
1312884
Xylenes,Total ND
0.34
1
1
01/07/05 19:56 P-C
1312884
Surr: 1,4-Difluorobenzene 87.4
0
% 41-143
1
01/07/05 19:56 P-C
1312884
Surr: 4-Bromofluorobenzene 88.9
0
% 39-160
1
01/07/05 19:56 P-C
1312884
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2:22:28 PM

LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID DW-1
Collected: 01/04/2005 13:00
SPL Sample ID: 05010148-09
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
ORGANICS BY METHOD 624
MCL E624
Units: ug/L
-VOLATILE
1,1,1-Trichloroethane
ND
0.48
5
1
01/06/05 15:29
FJA
1311361
1,1,2,2-Tetrachloroethane
ND
1.4
5
1
01/06/05 15:29
FJA
1311361
1, 1,2-Trichloroethane
ND
1.3
5
1
01/06/05 15:29
FJA
1311361
1,1-Dichloroethane
ND
0.58
5
1
01/06/05 15:29
FJA
1311361
1,1-Dichloroethene
IND
0.78
5
1
01/06/05 15:29
FJA
1311361
1,2-Dibromoethane
ND
0.53
5
1
01/06/05 15:29
FJA
1311361
1,2-Dichlorobenzene
ND
0.77
5
1
01/06/05 15:29
FJA
1311361
1,2-Dichloroethane
ND
0.59
5
1
01/06/05 15:29
FJA
1311361
1,2-Dichloropropane
ND
0.49
5
1
01/06/05 15:29
FJA
1311361
1,3-Dichlorobenzene
ND
0.62
5
1
01/06/05 15:29
FJA
1311361
1,4-Dichlorobenzene
ND
0.71
5
1
01/06/05 15:29
FJA
1311361
2-Chloroethyl vinyl ether
ND
1.1
10
1
01/06/05 15:29
FJA
1311361
Bromodichloromethane
ND
0.68
5
1
01/06/05 15:29
FJA
1311361
Bromoform
ND
0.59
5
1
01/06/05 15:29
FJA
1311361
Bromomethane
ND
1.4
10
1
01/06/05 15:29
FJA
1311361
Carbon tetrachloride
ND
0.16
5
1
01/06/05 15:29
FJA
1311361
Chlorobenzene
ND
0.98
5
1
01/06/05 15:29
FJA
1311361
Chloroethane
ND
0.5
10
1
01/06/05 15:29
FJA
1311361
Chloroform
10
0.55
5
1
01/06/05 15:29
FJA
1311361
Chloromethane
ND
0.55
10
1
01/06/05 15:29
FJA
1311361
cis- 1,3-Dichloropropene
ND
0.52
5
1
01/06/05 15:29
FJA
1311361
Dibromochloromethane
ND
0.6
5
1
01/06/05 15:29
FJA
1311361
Dichlorodifluoromethane
ND
0.29
5
1
01/06/05 15:29
FJA
1311361
Methyl tert-butyl ether
ND
0.69
5
1
01/06/05 15:29 ,
FJA
1311361
chloride
ND
1.8
5
1
01/06/05 15:29
FJA
1311361
-Methylene
Tetrachloroethene
ND
2.8
5
1
01/06/05 15:29
FJA
1311361
trans- 1, 3-Dichloropropene
ND
0.49
5
1
01/06/05 15:29
FJA
1311361
Trichloroethene
ND
0.28
5
1
01/06/05 15:29
FJA
1311361
Trichlorofluoromethane
ND
0.21
5
1
01/06/05 15:29
FJA
1311361
chloride
ND
0.81
10
1
01/06/05 15:29
FJA
1311361
-Vinyl
cis- 1,2-Dichloroethene
ND
0.62
5
1
01/06/05 15:29
FJA
1311361
trans- 1, 2-Dichloroethene
ND
0.61
5
1
01/06/05 15:29
FJA
1311361
1,2-Dichloroethene, Total
ND
0.6
5
1
01/06/05 15:29 .
FJA
1311361
Surr: 1,2-Dichloroethane-d4
90.9
0 3/o
72.6-128
1
01/06/0515:29
FJA
1311361
Surr: Toluene-d8
92.5
0 :/Io
84.9-111
1
01/06/05 15:29
FJA
1311361
Surr: 4-Bromofluorobenzene
82.1
0 Yo
76.6-114
1
01/06/05 15:29
FJA
1311361
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable, due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2,22,28 PM

R 0
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID DW-2
Collected: 01/04/2005 10:00 SPL Sample ID: 05010148-10
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method Result
MDL
Rep.Lirnit
Dil. Factor QUAL Date Analyzed Analyst
Seq. #
PURGEABLE AROMATICS BY EPA 602
MCL E602 Units: uq/L
Benzene ND
0.3
1
-
1 01/07/05 20:26 P-C
1312885
Ethylbenzene ND
0.23
1
1 01/07/05 20:26 P C
1312885
Isopropyl ether ND
0.11
1
1 01/07/05 20:26 P C
1312885
- Methyl tert-butyl ether ND
0.22
8
1 01/07/05 20:26 P-C
1312885
- Naphthalene ND
0.25
10
1 01/07/05 20:26 P-C
1312885
Toluene ND
0.94
1
1 01/07/05 20:26 P-C
1312885
m,p-Xylene ND
0.75
2
1 01/07/05 20:26 P C
1312885
- o-Xylene ND
0.34
1
1 01/07/05 20:26 P C
1312885
-Xylenes,Total ND
0.34
1
1 01/07/05 20:26 P-C
1312885
Surr: 1,4-Difluorobenzene 87.2
0
% 41-143
1 01/07/05 20:26 P-C
1312885
Surr: 4-Bromofluorobenzene 89.3 0 % 39-160
01/07/05 20:26 P-C 1312885
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2:22:29 PM

®R
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
Client Sample ID DW-2
Collected: 01/04/2005 10:00
SPL Sample ID: 05010148-10
Site:
GREYHOUND TERM INAL-RALEIGH
Analyses/Method
Result
MDL
Rep.Limit
Dil. Factor QUAL
Date Analyzed
Analyst
Seq. #
VOLATILE ORGANICS BY METHOD 624
MCL E624
Units: ug/L
1,1,1-Trichloroethane
ND
0.48
5
1
01/06/05 15:54
FJA
1311362
1,1,2,2-Tetrachloroethane
ND
1.4
5
1
01/06/05 15:54
FJA
1311362
1, 1,2-Trichloroethane
ND
1.3
5
1
01/06/05 15:54
FJA
1311362
1, 1 -Dichloroethane
ND
0.58
5
1
01/06/05 15:54
FJA
1311362
1,1-Dichloroethene
ND
0.78
5
1
01/06/05 15:54
FJA
1311362
1,2-Dibromoethane
ND
0.53
5
1
01/06/05 15:54
FJA
1311362
1,2-Dichlorobenzene
ND
0.77
5
1
01/06/05 15:54
FJA
1311362
1,2-Dichloroethane
ND
0.59
5
1
01/06/05 15:54
FJA
1311362
1,2-Dichloropropane
ND
0.49
5
1
01/06/05 15:54
FJA
1311362
1,3-Dichlorobenzene
ND
0.62
5
1
01/06/05 15:54
FJA
1311362
1,4-Dichlorobenzene
ND
0.71
5
1
01/06/05 15:54
FJA
1311362
2-Chloroethyl vinyl ether
ND
1.1
10
1
01/06/05 15:54
FJA
1311362
Bromodichloromethane
ND
0.68
5
1
01/06/05 15:54
FJA
1311362
Bromoform
ND
0.59
5
1
01/06/05 15:54
FJA
1311362
Bromomethane
ND
1.4
10
1
01/06/05 15:54
FJA
1311362
Carbon tetrachloride
ND
0.16
5
1
01/06/05 15:54
FJA
1311362
Chlorobenzene
ND
0.98
5
1
01/06/05 15:54
FJA
1311362
Chloroethane
ND
0.5
10
1
01/06/05 15:54
FJA
1311362
Chloroform
3.7
0.55
5
1 1
01/06/05 15:54
FJA
1311362
Chloromethane
ND
0.55
10
1
01/06/05 15:54
FJA
1311362
cis- 1, 3-Dichloropropene
ND
0.52
5
1
01/06/05 15:54
FJA
1311362
Dibromochloromethane
ND
0.6
5
1
01/06/05 15:54
FJA
1311362
Dichlorodifluoromethane
ND
0.29
5
1
01/06/05 15:54
FJA
1311362
Methyl tert-butyl ether
ND
0.69
5
1
01/06/05 15:54
FJA
1311362
Methylene chloride
ND
1.8
5
1
01/06/05 15:54
FJA
1311362
Tetrachloroethene
ND
2.8
5
1
01/06/05 15:54
FJA
1311362
trans- 1,3-Dichloropropene
ND
0.49
5
1
01/06/05 15:54
FJA
1311362
Trichloroethene
ND
0.28
5
1
01/06/05 15:54
FJA
1311362
Trichlorofluoromethane
ND
0.21
5
1
01/06/05 15:54
FJA
1311362
Vinyl chloride
ND
0.81
10
1
01/06/05 15:54
FJA
1311362
cis- 1,2-Dichloroethene
ND
0.62
5
1
01/06/05 15:54
FJA
1311362
trans- 1,2-Dichlbroethene
ND
0.61
5
1
01/06/05 15:54
FJA
1311362
1,2-Dichloroethene, Total
ND
0.6
5
1
01/06/05 15:54
FJA
1311362
Surr: 1,2-Dichloroethane-d4
92.2
0 %
72.6-128
1
01/06/05-15:54
FJA
1311362
Surr: Toluene-d8
94.2
0 %
84.9-111
1
01/06/05 15:54
FJA
1311362
Surr: 4-Bromofluorobenzene
84.1
0 %
76.6-114
1
01/06/05 15:54
FJA
1311362
Qualifiers: ND/U - Not Detected at the Reporting Limit >MCL - Result Over Maximum Contamination Limit(MCL)
B - Analyte detected in the associated Method Blank D - Surrogate Recovery Unreportable due to Dilution
* - Surrogate Recovery Outside Advisable QC Limits MI - Matrix Interference
J - Estimated Value between MDL and PQL
E - Concentrations exceeding Calibration range of Instrument 1/12/2005 2:22 29 PM

��Mm � i I I MSY
1/12/2005 2:22:07 PM

y.
Z .
Quality Control Report
GREYHOUND LINES, INC.
GREYHOUND BLOUNT ST./73.75092.0011
Analysis: Purgeable Aromatics by EPA 602
Method: E602
Method Blank
RunID: HPCC_050107D-1312875 Units: ug/L
Analysis Date: 01/07/2005 15:21 Analyst: P_C
Analyte
Result
Qua]
Rep Limit
Benzene
ND
1.0
Ethylbenzene
ND
1.0
Isopropyi ether
ND
1.0
Methyt tert-butyl ether
NDI
8.0
Naphthalene
ND
10
Toluene
ND
1.0
m,p-Xyiene
ND
2.0
o-Xylene
ND
1.0
X Ienes,Total
ND
1.0
Surr: 1 4-Difluorobenzene
90.3
67-141
Surr: 4-Bromofluorobenzene
92.1
63 135
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05010148
Lab Batch ID: R91533
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05010148-01A
MW-1
05010148-02A
MW-2
05010148-03A
MW-3
05010148-04A
MW-4
05010148-05A
M W -5
05010148-06A
MW-7
05010148-07A
MW-10
05010148-08A
MW-11
05010148-09A
DW-1
05010148-10A
DW-2
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: HPCC_050107D-1315479 Units: ug/L
Analysis Date: 01/07/2005 13:36 Analyst: P_C
Analyte
LCS
Spike
Added
LCS
Result
LCS
Percent
Recovery
LCSD
Spike
Added
LCSD
Result
LCSD
Percent
Recovery
RPD
RPD
Limit
Lower
Limit
Upper
Limit
Benzene
50
53.8
108
50.0
53.1
106
1.3
20
70
130
Ethylbenzene
50
49.3
98.5
50.0
48.6
97.2
1.4
20
70
130
Isopropyl Ether
50
51.4
103
50.0
50.9
102
1.0
20
70
130
Methyl tert-butyl ether
50
46.8
93.5
50.0
47.0
94.0
0.5
20
70
130
Naphthalene
50
62.8
126
50.0
63.6
127
1.3
20
70
130
Toluene
50
47.8
95.6
50.0
47.2
94.4
1.2
20
70
130
m,p-Xylene
100
102
102
100
100
100
1.3
20
70
130
o-Xylene
50
48.6
97.1
50.0
47.9
95.9
1.3
20
70
130
Xylenes,Total
150
150.6
100.1
150.0
147.9
98.77
1.3
20
70
130
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL " - Recovery Outside Advisable QC Limits
E - Concentrations exceeding Calibration range of Instrument
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported.
1/12/2005 222:00 PM

Quality Control Report
GREYHOUND LINES, INC.
GREYHOUND BLOUNT ST./73.75092.0011
Analysis: Volatile Organics by Method 624
Method: E624
Method Blank
RunID: X_050106A-1311352 Units: ug/L
Analysis Date: 01/06/2005 11:41 Analyst: FJA
Analyte
Result
Qual
Rep Limit
1 1 1-Trichloroethane
ND
5.0
1 1 2 2-Tetrachloroethane
ND
5.0
1 1 2-Trichloroethane
ND
5.0
1 1-Dichloroethane
ND
5.0
1 1-Dichloroethene
ND
5.0
1 2-Dichloroethane
ND
5.0
1 2-Dichloro ro ane
ND
5.0
2-Chloroethyi vinyl ether
ND
10
Bromodichloromethane
ND
5.0
Bromoform
ND
5.0
Bromomethane
ND
10
Carbon tetrachloride
ND
5.0
Chlorobenzene
ND
5.0
Chloroethane
ND
10
Chloroform
ND
5.0
Chloromethane
ND
10
cis-1 3-Dichloro ro ene
ND
5.0
Dibromochloromethane
ND
5.0
Methyiene chloride
ND
5.0
Tetrachloroethene
ND
5.0
trans-1 3-Dichloro ro ene
ND
5.0
Trichloroethene
ND
5.0
Trichlorofluoromethane
ND
5.0
Vinyl chloride
ND
10
cis-1 2-Dichloroethene
ND
5.0
trans-1 2-Dichloroethene
ND
5.0
1 2-Dichloroethene Total
ND
5.0
Surr:12-Dichloroethane-d4
94.0
72.6-128
Surr:4-Bromofluorobenzene
90.4
76.6-114
Surr: Toluene-d8
96.0
84.9-111
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05010148
Lab Batch ID: R91426
Samples in Analytical Batch:
Lab Sample ID
Client Sample ID
05010148-01A
MW-1
05010148-02A
MW-2
05010148-03A
MW-3
05010148-04A
M W -4
05010148-05A
M W -5
05010148-06A
MW-7
05010148-07A
MW-10
05010148-08A
M W -11
05010148-09A
DW-1
05010148-10A
DW-2
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD)
RunID: X_050106A-1311350 Units: ug/L
Analysis Date: 01/06/2005 10:39 Analyst: FJA
Analyte
LCS
LCS
LCS
LCSD
LCSD
LCSD
RPD
RPD
Lower
Upper
Spike
Result
Percent
Spike
Result
Percent
Limit
Limit
Limit
Added
Recovery
Added
Recovery
1, 1, 1 -Trichloroethane
20
19.6
98.2
20.0
20.6
103
5.0
20
52
162
1,1,2,2-Tetrachloroethane 1
201
16.71
83.61
20.01
17.41
87.21
4.21
20
46
157
Qualifiers: ND/U Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL * - Recovery Outside Advisable QC Limits
E - Concentrations exceeding Calibration range of Instrument
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported.
1/12/2005 2,22-01 PM

Quality Control Report
GREYHOUND LINES, INC.
GREYHOUND BLOUNT ST./73.75092.0011
Analysis: Volatile Organics by Method 624
Method: E624
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
WorkOrder: 05010148
Lab Batch ID: R91426
Laboratory Control Sample/Laboratory Control Sample Duplicate(LCS/LCSD)
RunID: X_050106A-1311350 Units: ug/L
Analysis Date: 01/06/2005 10:39 Analyst: FJA
Analyte
LCS
Spike
Added
LCS
Result
LCS
Percent
Recovery
LCSD
Spike
Added
LCSD
Result
LCSD
Percent
Recovery
RPD
RPD
Limit
Lower
Limit
Upper
Limit
1,1,2-Trichloroethane
20
18.1
90.4
20.0
18.6
93.0
2.9
20
52
150
1, 1 -Dichloroethane
20
19.2
96.0
20.0
20.4
102
6.2
20
59
155
1, 1 -Dichloroethene
20
19.1
95.4
20.0
20.3
102
6.1
20
0
234
1,2-Dichloroethane
20
18.1
90.4
20.0
18.6
93.2
3.1
20
49
155
1,2-Dichloropropane
20
20.4
102
20.0
21.0
105
3.0
20
0
210
2-Chloroethyl vinyl ether
20
0
0
20
0
0
0.0
20
0
305
Benzene
20
20.2
101
20.0
21.1
105
4.3
20
37
151
Bromodichloromethane
20
18.5
92.5
20.0
19.4
97.2
4.9
20
35
151
Bromoform
20
15.2
75.8
20.0
16.5
82.7
8.7
20
45
169
Bromomethane
20
16.3
81.6
20.0
19.1
95.6
15.9
20
0
242
Carbon tetrachloride
20
18.7
93.7
20.0
20.3
101
7.8
20
70
140
Chlorobenzene
20
16.91
84.4
20.0
17.6
88.0
4.2
20
37
160
Chloroethane
20
19.3
96.5
20.0
21.0
105
8.4
20
14
230
Chloroform
20
19.5
97.41
20.0
20.6
103
5.5
20
51
138
Chloromethane
20
16.3
81.6
20.0
18.0
90.0
9.8
20
0
273
Icis -1,3-Dichloropropene
20
17.2
86.0
20.0
18.3
91.6
6.3
20
0
227
Dibromochloromethane
20
17.2
85.8
20.0
18.2
91.0
5.9
20
53
149
Ethylbenzene
20
17.1
85.6
20.0
17.8
89.0
3.9
20
37
162
Methylene chloride
20
19.9
99.3
20.0
20.8
104
4.7
20
0
221
Tetrachloroethene
20
17.1
85.6
20.0
18.3
91.6
6.9
20
64
168
Toluene
20
17.4
87.0
20.0
18.1
90.3
3.8
20
47
150
trans -1,3-Dichloropropene
20
16.7
83.3
20.0
18.2
91.0
8.8
20
17
183
Trichloroethene
20
19.8
98.8
20.0
20.4
102
3.2
20
71
157
Trichlorofluoromethane
20
21.6
108
20.0
22.4
112
3.7
20
17
181
Vinyl chloride
20
19.8
98.8
20.0
21.5
107
8.2
20
0
251
,trans -1,2-Dichloroethene
20
19.5
97.6
21
105
-7.5
20
54
156
Qualifiers: ND/U - Not Detected at the Reporting Limit MI - Matrix Interference
B - Analyte detected in the associated Method Blank D - Recovery Unreportable due to Dilution
J - Estimated value between MDL and PQL " - Recovery Outside Advisable QC Limits
E - Concentrations exceeding Calibration range of Instrument
N/C - Not Calculated - Sample concentration is greater than 4 times the amount of spike added. Control limits do not apply.
The percent recoveries for QC samples are correct as reported. Due to significant figures and
rounding, the reported RPD may differ from the displayed RPD values but is correct as reported.
1/12/2005 2 22:01 PM

C,hain
.aCustody
1/12/2005 2:21:51 PM

lf@
LAFAYETTE LABORATORY
500 AMBASSADOR CAFFERY PARKWAY
SCOTT, LA 70583
[phone]
F—
Workorder:
05010148
Received By:
LAR
Date and Time Received:
1/5/2005 10:30:00 AM
Carrier name:
FedEx-Std 1 Day PM
Temperature:
40C
Chilled by:
Water Ice
1
Shipping container/cooler in good condition?
Yes
W
No ❑
Not Present ❑
2.
Custody seals intact on shippping container/cooler?
Yes
FV_1
No D
Not Present ❑
3,
Custody seals intact on sample bottles?
Yes
❑
No ❑
Not Present
4.
Chain of custody present?
Yes
EV1
No ❑
5.
Chain of custody signed when relinquished and received?
Yes
No ❑
6.
Chain of custody agrees with sample labels?
Yes
No ❑
7.
Samples in proper container/bottle?
Yes
Ev—j
No ❑
3.
Sample containers intact?
Yes
0
No ❑
9e
Sufficient sample volume for indicated test?
Yes
®
No ❑
10.
All samples received within holding time?
Yes
No ❑
11 ,
Container/Temp Blank temperature in compliance?
Yes
k
No ❑
12.
Water - VOA vials have zero headspace?
Yes
R]
No ❑
Not Applicable ❑
13.
Water - pH acceptable upon receipt?
Yes
❑
No ❑
Not Applicable 0
SPL Representative: Contact Date & Time:
Client Name Contacted:
Non Conformance
Issues:
Client Instructions:
1/12/2005 2:21:39 PM

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