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HomeMy WebLinkAbout23079_Northern Telecom_PH II_20170126'orpr 00 �r0x% 0' 0 0Oprro0Ox r 0 \\ `` ��rr�0u.rfi0yr7rrprpr0�rromv rry�\\�r \% 00 o0 000rr0rVr0off 0��' % 00rp 0�r01/'• 0i rO1yppyr ,0j°700yrJ0067rgoes •10/0 r0q i 0 0r°,°DTr°0��r0000000640606040 ! bibs '000,"00000r"r0II/1i*0 / ry0o0pr0°r0o'orO0r °o70"ro07�C . 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Chapel Hill -Nelson Highway Research Triangle Park, North Carolina 27709 CBRE Proiect No.: E60405045 Dear Ms. Dossani: CBRE 55 West Red Oak Lane White Plains, New York 10604 914.694.9600 Tel 914.694.1335 Fax CBRE, Inc., a Delaware corporation ("CBRE") has completed a Limited Phase II Environmental Site Assessment of the above referenced property. The work was conducted in accordance with CBRE's letter of engagement and generally accepted industry standards. This report was prepared solely for the use of Zurich Alternative Asset Management, LLC (hereinafter "Client" or "User") and any party specifically referenced in Section 1.4 User Reliance. No other party shall use or rely on this report or the findings herein, without the prior written consent of CBRE. Thank you for the opportunity to provide our services. If you have any questions or need any additional information please contact the undersigned at (204) 331-1265. Sincerely, CBRE, Inc. —ASSESSMENT AND CONSULTING SERVICES Prepared By: Bo Cappleman, PG Project Manager Reviewed By: David Lent Managing Director Property Condition Assessments I Environmental Site Assessments I Seismic Studies I Zoning Analysis Locations Nationwide 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina TABLE OF CONTENTS 1.0 INTRODUCTION...................................................................................................... 1 1 .1 . BACKGROUND AND PURPOSE......................................................................................... 1 1.2. LIMITATIONS AND EXCEPTIONS......................................................................................... 2 1.3. SPECIAL TERMS AND CONDITIONS.................................................................................... 2 1.4. USER RELIANCE............................................................................................................ 2 2.0 PROPERTY DESCRIPTION........................................................................................... 2 3.0 SCOPE OF WORK.................................................................................................... 2 4.0 SUBSURFACE INVESTIGATION................................................................................... 3 4.1 . UTILITY CLEARANCE...................................................................................................... 3 4.2. SOIL BORINGS............................................................................................................. 3 4.3. MONITORING WELL ABANDONMENT................................................................................ 4 4.4. DISCUSSION OF ANALYTICAL RESULTS............................................................................... 5 5.0 CONCLUSIONS AND RECOMMENDATIONS............................................................... 6 APPENDICES APPENDIXA................................................................................................................. FIGURES APPENDIXB....................................................................................................... BORING LOGS APPENDIX C............................................................................. WELL ABANDONMENT RECORD APPENDIX D...................................................................................................................TABLES APPENDIX E............................................................................................. ANALYTICAL REPORTS CBRE 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina 1.0 INTRODUCTION CBRE is pleased to submit our Limited Phase II Environmental Site Assessment (Assessment) of the vacant industrial facility located at 4001 E. Chapel Hill -Nelson Highway, Research Triangle Park, North Carolina herein referred to as the "Subject". l.l. Background and Purpose The property, which is situated in an urban area characterized by light industrial and commercial office development, consists of an approximately 99-acre, four -parcel property improved with a 37-year-old (built in 1979, with several additional in the 1980s), approximate 700,000 square -foot (SF) office/warehouse (former industrial) facility. Prior to the construction of the existing improvements, the site was mostly undeveloped, wooded land with minor residential improvements. The purpose of this Assessment was to investigate a Recognized Environmental Condition (REC) identified in a Phase I Environmental Site Assessment (ESA) prepared by CBRE, dated February 5, 2016. Specifically, the following REC was identified, which warranted investigation at this time. Past Use of Property for Circuit Board Manufacturing Although approximately 350,000 SF of the facility is now designated as warehouse, that same area (the southern portion of the facility) was formerly used as manufacturing space when the facility was occupied by Nortel. According to the site contact, among other operations, circuit board assembly was conducted at the facility from approximately 1979/1980 to the late-1990s. These types of manufacturers typically use chlorinated solvents as parts degreasers. Chlorinated solvents include tetrachlorothene, trichorothene, 1,2-dichloroethene and l,l,l-trichloroethane. The improper storage, usage and disposal of chlorinated solvents commonly results in subsurface impacts. Although there are no known releases of such solvents at the subject property, the historical use of the facility as a manufacturer of circuit boards and electronics in general is indicative of a significant environmental concern to the property. Also, the facility formerly operated as a Resource Conservation and Recovery Act (RCRA)-Small Quantity Generator (SQG) of hazardous waste, with several violations/enforcement actions on record in the 1980s and early 1990s. Additionally, the following Business Environmental Risk (BER) was identified: Monitoring Well One inactive apparent monitoring well was observed just east of the central side of the facility. The purpose of the well is unknown, but the site contact indicated that it is likely a "test well." The well is fitted with secured cap, and appeared to be quite old (a stamp on the cap indicated it was from pre-2000). Wells such as the one observed can act as conduits to groundwater and contaminate same if harmful materials are permitted to enter the well. Page 1 CBRE 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina 1.2. Limitations and Exceptions • The scope of work completed was designed solely to meet the needs of the Client. CBRE shall not be liable for any unattended usage of this report by another party. • No subsurface investigation can wholly eliminate uncertainty regarding the presence of contamination on a property. This Assessment was designed to reduce, but not eliminate the potential for RECs at the Subject, within reasonable limits of time and cost. The ESA is not intended to be exhaustive or all-inclusive and does not represent a guarantee of the identification of all possible environmental risk. Client is advised that if the ESA is obtained with the intent of qualifying the purchaser as an innocent landowner, contiguous property owner, or bona fide prospective purchaser under CERCLA, there will be continuing obligations of due care and responsiveness and additional legal requirements that likely apply to such status. CBRE accepts and undertakes no responsibility as to such requirements and advises that counsel be separately consulted with respect to such requirements. 1.3. Special Terms and Conditions There are no special terms and conditions associated with this assignment. 1.4. User Reliance This investigation was conducted on behalf of and for the exclusive use of the Client. This report, and the findings contained herein, shall not, in whole or part, be disseminated or conveyed to or used by any other party without the prior written consent of CBRE. 2.0 PROPERTY DESCRIPTION Project Address: 4001 E. Chapel Hill -Nelson Highway City, State Zip Code: Research Triangle Park, North Carolina 27709 3.0 SCOPE OF WORK This Assessment was prepared in accordance with CBRE's Proposal for Limited Phase II Environmental Site Assessment, dated April 18, 2016. Specifically, this Assessment included the following activities: • Notification to North Carolina's one -call system for underground utilities mark out; • Geophysical survey for confirmation of utilities mark out; • Advancement of eight (8) borings; • Installation of six (6) sub -slab soil vapor probes; • Collection and field screening of soil samples for volatile organic compound (VOC) contamination with a photoionization detector (PID); • Collection of six (6) soil samples, one (1) groundwater sample and six (6) sub -slab vapor samples for laboratory analysis; and • Abandonment of one existing monitoring well. Page 2 CBRE 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina 4.0 SUBSURFACE INVESTIGATION 4.1. Utility Clearance Prior to conducting any subsurface drilling, CBRE contacted the North Carolina underground utility mark -out system. In addition, CBRE retained the services of Probe Utility Locating, LLC, a private utility locator, to "clear' CBREs boring locations for underground utilities. The mark out for the boring locations was conducted using ground penetrating radar (GPR) and electromagnetic equipment. 4.2. Soil Borings Soil Sampling CBRE directed the advancement of eight (8) borings on the Subject for investigation of the above referenced REC. The borings were advanced by Innovative Environmental Technologies, Inc. (IET) using a direct -push drill rig. Prior to the advancement of each boring, all down -hole drilling equipment was decontaminated by IET in accordance with U.S. EPA protocols and good commercial and customary practice. S13-1 through SB-6 were advanced to 5 feet below ground surface (bgs) in the former manufacturing area located in the southern portion of the building. SB-7 and S13-8 were advanced to up to 17 feet bgs to the south and southwest (downgradient) of the building. No soil samples were collected from S13-7 and SB-8, as these borings were not locating in the immediate vicinity of a potential source area. Sample locations are shown on the Sample Location Plan, attached as Figure 1 in Appendix A. Soil samples were collected at continuous 5-foot intervals using a macro -core sampler and inspected for evidence of VOC contamination using a PID. No staining, odors or PID readings above background levels were identified in any of the borings. Observed soil conditions encountered in the borings consisted of predominantly stiff, brown, fine sandy silt to approximately 10 to 12 feet bgs. Very dense, silty sand was identified near the bottom of SB-7 and S13-8. Refusal was encountered in SB-7 and SB-8 at depths of 17 feet bgs and 15 feet bgs, respectively. Groundwater was encountered at approximately 12 feet bgs in S13-7. No groundwater was encountered in the remaining soil borings. PID readings and detailed soil descriptions are provided on the boring logs presented in Appendix B. CBRE collected one soil sample from S13-1 through SB-6 for laboratory analysis. Based on the lack of field indications of soil impacts, a shallow sample (1 foot bgs) was collected in an effort to identify a surface release. Collected samples were transferred to laboratory supplied sample containers, packed on ice in a cooler and shipped under proper chain of custody to TestAmerica Laboratories, Inc. (TestAmerica) in Nashville, Tennessee. Soil samples were analyzed for VOCs by EPA Method 8260B and RCRA metals by EPA Method 6010D/7471 B. Page 3 CBRE 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina Groundwater Sampling In order to evaluate groundwater quality at the Subject, SB-7 was converted into a temporary groundwater monitoring well (TMW-1) consisting of one -inch inside diameter poly -vinyl chloride (PVC) well screen and riser pipe. A stainless steel check valve with dedicated, disposable tubing was utilized to purge the wells and collect the groundwater sample. Shallow refusal was encountered in three borings in the vicinity of SB-8; therefore, no groundwater sample was able to be collected. The groundwater sample was transferred to laboratory supplied sample containers, packed on ice in a cooler and shipped under proper chain of custody to TestAmerica. The sample was analyzed for VOCs by EPA Method 8260B and dissolved RCRA Metals by EPA Method 6010D/7470A. Upon completion of sampling, all borings were backfilled flush to grade with bentonite and the ground surface repaired with concrete. Sub -Slab Vapor Sampling CBRE advanced six (6) sub -slab vapor probes adjacent to each of the interior soil borings noted above (former manufacturing area). The soil vapor probe locations denoted as SG-1 through SG-6 are depicted on Sample Location Plan in Appendix A. The sub -slab vapor probes were advanced by CBRE using hand-held sampling equipment, six inches beneath the concrete slab. A sacrificial vapor point connected to Teflon tubing was inserted into each borehole. The annular space of the borehole was filled with sand to the base of the concrete slab, followed by a hydrated bentonite seal. Prior to sampling, the tubing system was purged of ambient air with a low -flow pump. The samples were collected from each point into laboratory supplied 6-liter summa canisters equipped with regulators and manometers to ensure a flow rate of less than 200 ml/min. To serve as a quality assurance/quality control (QA/QC) device, a tracer gas was used to serve to verify the integrity of the soil vapor probe seal. Helium was used as the tracer gas. A portable monitoring device was used to analyze the integrity of the seal. After adjustments to prevent infiltration and prior to sampling, each location was proven to not show a significant presence of Helium. Upon completion of sampling the vapor points were removed, the boreholes were backfilled and the ground surface was repaired. The summa canisters where shipped under proper chain of custody to TestAmerica's Knoxville, Tennessee laboratory for analysis of VOCs in accordance with EPA method TO-15. 4.3. Monitoring Well Abandonment CBRE directed IET to perform the abandonment of the on -site monitoring well in accordance with the North Carolina Department of Environmental Quality (NCDEQ) guidelines. Specifically, the well abandonment will include the following procedures. • Removal of the exposed steel riser pipe; • Filling the well casing with a fluid bentonite grout mixture using a tremie pipe; Page 4 CBRE 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina • Restoring the ground surface to conform with the surrounding area. A copy of the Well Abandonment Record is provided in Appendix C. 4.4. Discussion of Analytical Results The soil, groundwater and sub -slab vapor sampling results for this Assessment are discussed below. CBRE has compared the soil analytical data to the NCDEQ, Inactive Hazardous Sites Branch Preliminary Soil Remediation goals (PSRGs) for protection of groundwater, residential soil and commercial/industrial soil (updated October 2016). In addition, metals data were compared to North Carolina background values published in Elements in North American Soils, Second Edition (2005). Groundwater data were compared to the North Carolina 2L Groundwater Standards (2L Standards). Soil vapor data were compared to the NCDEQ, Division of Waste Management Soil Gas screening levels (SGSLs) for residential and non-residential sites (updated October 2016. The analytical data are presented on Tables 1 through 3 in Appendix D. The laboratory reports are provided in Appendix E. Soil Analvtical Results Soil analytical data indicate the presence of benzene in SB-1 (1') at a concentration of 0.00166 mg/kg, which is below the most stringent PSRG (i.e. protection of groundwater) of 0.0073 mg/kg. The data indicate that the remaining VOCs are not present above the laboratory reporting limits (RSLs). • Metals data indicate the presence of arsenic, barium, chromium and lead. A summary of each constituent is provided as follows: • Arsenic was detected in SB-3 (1') at a concentration of 2.32 mg/kg. The detected concentration exceeds the residential PSRG but is within the range of published North Carolina background levels. • Barium was detected at concentrations ranging from 59.2 mg/kg to 121 mg/kg. The concentrations are well below the PSRGs and are consistent with published North Carolina background levels. • Chromium was detected at concentrations ranging from 6.88 mg/kg to 12.0 mg/kg. The concentrations are consistent with published North Carolina background levels. • Lead was detected at concentrations ranging from 11 .7 mg/kg to 22.6 mg/kg. The concentrations are well below the PSRGs and are consistent with published North Carolina background levels. Page 5 CBRE 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina Groundwater Analytical Results • Groundwater analytical data do not indicate the presence of VOCs in TMW-1 above laboratory reporting limits. Barium was detected at a concentration of 222 /fig/L, which is well below the 2L Standard of 700 pg/L. Sub -Slab Soil Vapor Results Soil vapor analytical data indicate the presence of numerous VOCs in SG-1 through SG-6. Dichlorodifluoromethane (Freon 12) was detected in SG-2 and SG-5 at a concentration of 1,100 Pg/m3, which exceeds the residential SGSL of 695 pg/m3. However, the detected concentration is well below the applicable non-residential SGSL of 8,760 pg/m3. 5.0 CONCLUSIONS AND RECOMMENDATIONS The results of this Assessment are summarized below: • Soil borings were advanced within and immediately downgradient of the former manufacturing facility. In addition, six (6) soil samples, one (1) groundwater sample and six (6) sub -slab vapor samples were collected for laboratory analysis. • Soil analytical data indicated the presence of benzene in SB-1 (1'); however, the detected concentration was below the PSRGs. Metals detected in SB-1 (1') through SB-6 (1') were present at concentrations below the PSRGs and/or consistent with published North Carolina background levels. • Only barium was detected in groundwater. The detected concentration is well below the 2L Standard. • Dichlorodifluoromethane (Freon 12) was detected in two sub -slab vapor samples (SG-2 and SG-5) at a concentration of 1,100 µg/m3, which exceeds the residential SGSL of 695 Ng/m3. However, the detected concentration is well below the applicable non-residential SGSL of 8,760 µg/m3. Only trace concentrations of VOCs were detected in the remaining sub -slab vapor samples. Based on the anticipated future commercial use of the Subject, the level of Freon 12 detected in sub -slab vapor is appropriate for the site's intended use. Based on the results of this Assessment, no additional investigation is recommended at this time. CBRE's conclusions and recommendations are based on the results this Assessment. This Assessment was intended solely to investigate the REC identified in the Phase I Report. It was not intended to satisfy the level of inquiry that may be necessary to support remedial solutions or determine migration pathways related to a release from the REC. Page 6 CBRE 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina APPENDIX A Figures CBRE Underwriters Laboratories, hic. �E11�111111111RST TE 40 BD Technologies 'b� e 0 0 0 , waY�Park ng Presumed groundwater v� flow direction o ■ ,! offices ; parking TSB-1/SG-1 ' / SB-6/SG-6 , 0 parking 0 ;M■ NEW MILLENIUM WAY Fidelity Investments Legend Property Boundary As -Built Structure Pad -Mounted Transformer Pole -Mounted Transformer Former UST AST Q Soil & Soil Vapor Sample Soil Boring/Temporary • Monitoring Well 4001 EAST CHAPEL HILL — NELSON HIGHWAY RESEARCH TRIANGLE PARK, NORTH CAROLINA SB-2/SG-2 SB-8 0i0 SB-5/SG-5 �� 0 (no sample) ti well Em 0 0 SB-3/SG-3 SB-4/SG-4 i O • fi°Q water tanks i oro SB-7/ TMW-1 volleyball II area par Zing tennis courts playing (\fields substation wooded SAMPLE LOCATION PLAN A = 1 ;1 Hilton Garden hin Hotel Warehouse (former manufacturing area) cell tower Holiday Express hotel gas station Project No: E60405045 Boundaries are approximate. Not to scale 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina APPENDIX B Soil Boring Logs CBRE CBRE 55 West Red Oak Lane White Plains, New York 10604 (914) 694-9600 (tel) (914) 694-2903 (fax) Boring Log Project No.: E60405045 Project Name: 4001 E. Chapel Hill -Nelson Hwy Project Manager: Bo Cappleman Total depth: 5 feet bgs Depth to Groundwater: Not encountered Date: January 10, 2017 Location: Research Triangle Park, North Carolina Drilling Company: Innovative Environmental Technologies, Inc. Method Used: Direct Push Boring No.: SB-1 Depth Sample Penetration/ PID Soil Identification and Remarks (feet) Interval Recovery Screening (feet) (percent) Result (ppm) 5 0-5 100 0.0 0-0.5' — Concrete 0.5-5' — Dry, stiff, brown, fine sandy SILT • Soil sample S13-1 (1') was collected for laboratory analysis of VOCs and RCRA Metals CBRE 55 West Red Oak Lane White Plains, New York 10604 (914) 694-9600 (tel) (914) 694-2903 (fax) Boring Log Project No.: E60405045 Project Name: 4001 E. Chapel Hill -Nelson Hwy Project Manager: Bo Cappleman Total depth: 5 feet bgs Depth to Groundwater: Not encountered Date: January 10, 2017 Location: Research Triangle Park, North Carolina Drilling Company: Innovative Environmental Technologies, Inc. Method Used: Direct Push Boring No.: SB-2 Depth Sample Penetration/ PID Soil Identification and Remarks (feet) Interval Recovery Screening (feet) (percent) Result (ppm) 5 0-5 100 0.0 0-0.5' — Concrete 0.5-5' — Dry, stiff, brown, fine sandy SILT • Soil sample SB-2 (1') was collected for laboratory analysis of VOCs and RCRA Metals CBRE 55 West Red Oak Lane White Plains, New York 10604 (914) 694-9600 (tel) (914) 694-2903 (fax) Boring Log Project No.: E60405045 Project Name: 4001 E. Chapel Hill -Nelson Hwy Project Manager: Bo Cappleman Total depth: 5 feet bgs Depth to Groundwater: Not encountered Date: January 10, 2017 Location: Research Triangle Park, North Carolina Drilling Company: Innovative Environmental Technologies, Inc. Method Used: Direct Push Boring No.: SB-3 Depth Sample Penetration/ PID Soil Identification and Remarks (feet) Interval Recovery Screening (feet) (percent) Result (ppm) 5 0-5 100 0.0 0-0.5' — Concrete 0.5-5' — Dry, stiff, brownish red, fine sandy SILT • Soil sample SB-3 (1') was collected for laboratory analysis of VOCs and RCRA Metals CBRE 55 West Red Oak Lane White Plains, New York 10604 (914) 694-9600 (tel) (914) 694-2903 (fax) Boring Log Project No.: E60405045 Project Name: 4001 E. Chapel Hill -Nelson Hwy Project Manager: Bo Cappleman Total depth: 5 feet bgs Depth to Groundwater: Not encountered Date: January 10, 2017 Location: Research Triangle Park, North Carolina Drilling Company: Innovative Environmental Technologies, Inc. Method Used: Direct Push Boring No.: SB-4 Depth Sample Penetration/ PID Soil Identification and Remarks (feet) Interval Recovery Screening (feet) (percent) Result (ppm) 5 0-5 100 0.0 0-0.5' — Concrete 0.5-5' — Dry, stiff, brownish red, fine sandy SILT with trace clay • Soil sample S13-4 (1') was collected for laboratory analysis of VOCs and RCRA Metals CBRE 55 West Red Oak Lane White Plains, New York 10604 (914) 694-9600 (tel) (914) 694-2903 (fax) Boring Log Project No.: E60405045 Project Name: 4001 E. Chapel Hill -Nelson Hwy Project Manager: Bo Cappleman Total depth: 5 feet bgs Depth to Groundwater: Not encountered Date: January 10, 2017 Location: Research Triangle Park, North Carolina Drilling Company: Innovative Environmental Technologies, Inc. Method Used: Direct Push Boring No.: SB-5 Depth Sample Penetration/ PID Soil Identification and Remarks (feet) Interval Recovery Screening (feet) (percent) Result (ppm) 5 0-5 100 0.0 0-0.5' — Concrete 0.5-5' — Dry, stiff, brown, fine sandy SILT • Soil sample SB-5 (1') was collected for laboratory analysis of VOCs and RCRA Metals CBRE 55 West Red Oak Lane White Plains, New York 10604 (914) 694-9600 (tel) (914) 694-2903 (fax) Boring Log Project No.: E60405045 Project Name: 4001 E. Chapel Hill -Nelson Hwy Project Manager: Bo Cappleman Total depth: 5 feet bgs Depth to Groundwater: Not encountered Date: January 10, 2017 Location: Research Triangle Park, North Carolina Drilling Company: Innovative Environmental Technologies, Inc. Method Used: Direct Push Boring No.: SB-6 Depth Sample Penetration/ PID Soil Identification and Remarks (feet) Interval Recovery Screening (feet) (percent) Result (ppm) 5 0-5 100 0.0 0-0.5' — Concrete 0.5-5' — Dry, stiff, brown, fine sandy SILT • Soil sample SB-6 (1') was collected for laboratory analysis of VOCs and RCRA Metals CBRE 55 West Red Oak Lane White Plains, New York 10604 (914) 694-9600 (tel) (914) 694-2903 (fax) Boring Log Project No.: E60405045 Project Name: 4001 E. Chapel Hill -Nelson Hwy Project Manager: Bo Cappleman Total depth: 17 feet bgs Depth to Groundwater: 12 feet bgs Date: January 10, 2017 Location: Research Triangle Park, North Carolina Drilling Company: Innovative Environmental Technologies, Inc. Method Used: Direct Push Boring No.: SB-7/TMW-1 Depth (feet) Sample Interval (feet) Penetration/ Recovery (percent) PID Screening Result (ppm) Soil Identification and Remarks 5 0-5 100 0.0 0-1' — Wet, loose, gray/brown, SAND and GRAVEL 1-5' — Dry, medium stiff, reddish brown, fine sandy SILT 10 5-10 100 0.0 Moist, medium stiff, reddish brown, fine sandy SILT 15 10-15 100 0.0 10-12' — Moist, medium stiff, reddish brown, fine sandy SILT 12-15' — Saturated, dense, brown, silty SAND 17 15-17 100 0.0 Saturated, very dense, brown, silty SAND Temporary monitoring well TMW-1 was installed at 17 feet bgs; Screened interval: 7-17 feet bgs Groundwater sample collected for laboratory analysis of VOCs and dissolved RCRA Metals No soil samples were collected for laboratory analysis. CBRE 55 West Red Oak Lane White Plains, New York 10604 (914) 694-9600 (tel) (914) 694-2903 (fax) Boring Log Project No.: E60405045 Project Name: 4001 E. Chapel Hill -Nelson Hwy Project Manager: Bo Cappleman Total depth: 15 feet bgs Depth to Groundwater: Not encountered Date: January 10, 2017 Location: Research Triangle Park, North Carolina Drilling Company: Innovative Environmental Technologies, Inc. Method Used: Direct Push Boring No.: SB-8 Depth (feet) Sample Interval (feet) Penetration/ Recovery (percent) PID Screening Result (ppm) Soil Identification and Remarks 5 0-5 100 0.0 0-0.25' — Asphalt 0.25-2' — Moist, stiff, dark brown, silty CLAY 2-5' — Slightly moist, stiff, red, clayey SILT w/ fine sand 10 5-10 100 0.0 Slightly moist, stiff, red, clayey SILT w/ fine sand 15 10-15 100 0.0 Slightly moist, very dense, red, clayey SILT w/ fine sand Direct push refusal encountered at 15 feet bgs. • No groundwater was encountered in S13-8; therefore, a sample was unable to be collected. 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina APPENDIX C Well Abandonment Record WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: Mike Tynan Well Contractor Name (or well owner personally abandoning well on his/her property) 2725-A NC Well Contractor Certification Number Innovative Environmental Technologies, Inc Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, Injection, etc.) ifknown 3. Well use (check well use): Water Supply Well: ❑Agricultural ❑Municipal/Public ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑Industrial/Commercial ❑Residential Water Supply (shared) ❑ltri ation Non -Water Supply Well: El Aquifer Recharge ❑Aquifer Storage and Recovery ❑Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling 4. Date well(s) abandoned: 1 /09/17 5a. Well location: Former Avaya Plant El Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage El Subsidence Control ❑Tracer El Other (explain under 7g) Facility/Owner Name Facility ID# (if applicable) 4001 Chapel Hill -Nelson Hwy, RTP 27709 Physical Address, City, and Zip Wake County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 35 53 21.61 N 7851 08.53 W CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well construction record(s) if available. For multiple injection or non -water supply wells ONLY with the same constructionlabandonment, you can submit one form. 6a. Well ID#: MW i 6b. Total well depth: 45 (ft.) 6c. Borehole diameter: 6° casing (in ) 6d. Water level below ground surface: 11 (ft.) 6e. Outer casing length (if known): (ft.) 6f. Inner casing/tubing length (if known): (ft.) For Internal Use ONLY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: One For multiple injection or non -water supply wells ONLY with the same construction/abandonment, you can submit one form. 7b. Approximate volume of water remaining in well(s): —50 (gal.) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: 7d. Amount of disinfectant used: 7e. Sealing materials used (check all that apply): El Neat Cement Grout ❑ Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑ Concrete Grout ❑ Drill Cuttings ❑ Specialty Grout ❑ Gravel ❑ Bentonite Slurry ❑ Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: 650 Ibs portland cement 30 Ibs bentonite 7g. Provide a brief description of the abandonment procedure: Removed 18" of steel casing. Filled MW completely from bottom to top with portland cement (5% bentonite) through tremmie pipe. 8. Certification: 1/11/17 Signature of Ce ied Well Contractor or Well Owner Date By signing this form., I hereby certify that the well(s) was (were) abandoned in accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 10a. For All Wells: Submit this form within 30 days of completion of well abandonment to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Iniection Wells: hi addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. 6g. Screen length (if known): (ft.) Form GW-30 North Carolina Department of Environment and Natural Resources — Division of Water Resources Revised August 2013 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina APPENDIX D Tables CBRE Table 1 Summary of Soil Analytical Results 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina Project #E60405045 NCDEQ PSRGs Client Sample ID: SB-1 (1') SB-2 (1) SB-3 (1') SB-4 (1') SB-5 (1') SB-6 (1') Range of Protection of Groundwater Residential Commercial/ Industrial North Carolina Background Date Sampled: 1/10/2017 1/10/2017 1/10/2017 1/10/2017 1/10/2017 1/10/2017 Levels 3 VOCs (8260B) Benzene 0.00166 <0.00187 <0.00159 <0.00164 <0.00148 <0.00175 0.0073 1.2 5.1 NA RCRA Metals (6010D/7471 B) <2.25 <2.09 2.32 <2.06 <2.25 <2.22 5.8 0.68 3.0 1.0 - 18 Arsenic Barium 109 121 115 80.9 95.8 59.2 580 3,000 44,000 50 - 1,000 Chromium 12.0 7.45 8.46 7.88 11.0 6.88 360,000/3.8 2 24,000/0.3 2 100,000/6.3 2 7.0 - 300 Lead 11.7 16.1 22.6 18.2 16.7 19.0 270 400 800 ND - 50 Notes: Values reported in milligrams per kilogram (mg/kg) Only detected compounds are shown. Method number follows the parameter in parenthesis Values were obtained from the North Carolina Department of Environmental Quality (NCDEQ), Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (PSRGs) Summary Table (October 2016) z PSRGs are shown for trivalent and hexavalent chromium, respectively. s North Carolina background levels were obtained from Elements in North American Soils, Second Edition (2005) NA = not applicable ND = non -detect VOCs = volatile organic compounds RCRA = Resource Conservation and Recovery Act CBE Table 2 Summary of Groundwater Analytical Results 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina Project #E60405045 Client Sample ID: TMW-1 North Carolina 2L Groundwater Standard Date Sampled: 1/10/2017 VOCs (826013) All BRL --- RCRA Metals (601013/7470A) Barium 222 700 Notes: Values reported in micrograms per liter (fag/L) Only detected compounds are shown. Method number follows the parameter in parenthesis The North Carolina 2L Groundwater Standard was obtained from North Carolina Administrative Code Title 15A, Subchapter 2L, dated April 1, 2013. BRL = below reporting limit VOCs = volatile organic compounds RCRA = Resource Conservation and Recovery Act CBRE Table 3 Summary of Soil Gas Analytical Results 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina Project #E60405045 Project Sample ID SG-1 SG-2 SG-3 SG-4 SG-5 SG-6 Residential Sub -Slab Soil Gas Screening Level' (10"5 Risk Level/HQ=0.2) Non -Residential Sub -Slab Soil Gas Screening Level' (10"5 Risk Level/HQ=0.2) (Ng/m3) (Ng/m3) Date Collected 1/10/2017 1/10/2017 1/10/2017 1/10/2017 1/10/2017 1/10/2017 VOCs (TO-15) Acetone 140 <32 <32 66 J <50 1,400 216,000 2,720,000 Benzene 2.0 J <1.7 <1.7 1.7 J <2.7 4.0 J 120 1,570 Bromodichloromethane 3.2 J <2.9 <2.9 <1.9 <4.4 <2.8 25.3 331 2-Butanone (MEK) 18 J <5.8 <5.8 24 <8.9 110 34,800 438,000 Carbon disulfide 2.2 J 1.3 J <0.94 <0.62 3.4 J 1.8 J 4,870 61,300 Chloroform 29 4.7 J 6.8 J 4.0 J <2.8 11 40.7 533 Cyclohexane <1.3 <1.3 <1.3 1.9J <2.1 <1.3 41,700 526,000 Dichlorodifluoromethane <3.2 1,100 17 J 3.9 J 1,100 <3.1 695 8,760 1,4-Dioxane <2.8 <2.8 <2.8 <1.9 <4.3 75 J 187 2,450 Ethylbenzene 5.2 J <2.9 <2.9 3.9 J <4.4 8.5 374 4,910 Hexane <1.1 <1.1 <1.1 9.5 J <1.7 2.0 J 4,870 61,300 Isopropyl alcohol 38 J 5.0 J 3.0 J 32 J 191 580 1,390 17,500 Methylene Chloride 13 J 10 J 12 J 19 181 13 J 4,170 52,600 4-Methyl-2-pentanone (MIBK) 18 J 1.8 J 15 J 2.5 J <2.8 71 20,900 263,000 m-Xylene & p-Xylene 23 J <5.1 <5.1 6.3 J <7.8 33 695 8,760 Naphthalene <4.5 <4.6 <4.6 <3.0 <7.1 4.9 J 20.9 263 o-Xylene 8.5 <2.6 <2.6 2.4 J <4.0 12 695 8,760 Styrene <2.4 <2.4 <2.4 3.7 J <3.7 <2.3 6,950 87,600 Tetrahydrofuran <1.8 <1.8 <1.8 <1.2 <2.8 19 J 13,900 175,000 Toluene 15 <4.4 <4.4 44 <6.8 21 34,800 438,000 trans- 1,2-dichloroethene <1.9 2.0 J 2.3 J 1.4 J <3.0 <1.9 NE NE 1,1,1-Trichloroethane <1.6 <1.6 <1.6 1.3 J <2.5 <1.5 34,800 438,000 Trichlorofluoromethane 1.4 J <1.3 <1.3 1.3 J <2.0 1.3 J NE NE 1,1,2-Trichloro-1,2,2-trifluoroethane 770 150 32 320 3.6 J 12 J 209,000 2,630,000 1,2,4-Trimethylbenzene 19 <3.0 <3.0 <2.0 <4.7 24 48.7 613 1,3,5-Trimethylbenzene 4.8 J <3.1 <3.1 <2.1 <4.8 4.5 J NE NE Vinyl acetate <4.7 <4.8 <4.8 5.4 J <7.4 <4.6 1,390 17,500 Notes: Data reported in micrograms per cubic meter (pg/rr3) Bold values exceed the residential deep soil gas screening level Method number follows the parameter in parenthesis. 1 Sub -Slab Soil Gas Screening Levels were establlished by the North Carolina Department of Environmental Quality (NCDEQ), Division of Waste Management (updated October 2016) VOCs = volatile organic compounds HQ = hazard quotient NE = not established CBRE 4001 East Chapel Hill -Nelson Highway Research Triangle Park, North Carolina APPENDIX E Analytical Reports TestAmerica ° THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177 TestAmerica Job ID: 490-119827-1 TestAmerica SDG: Research Triangle Park, NC Client Project/Site: E. Chapel Hill -Nelson Hwy, For: CBRE, Inc. 201 S College Street, Suite 1700 Charlotte, North Carolina 28244 Attn: Mr. Bo Cappleman Authorized for release by. 111812017 5:13:02 PM Ken Hayes, Project Manager II (615)301-5035 ken.hayes@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Table of Contents TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Cover Page .............................................. 1 Table of Contents ......................................... 2 Sample Summary ......................................... 3 Case Narrative ........................................... 4 Definitions............................................... 5 Client Sample Results ...................................... 6 QC Sample Results ........................................ 20 QC Association ........................................... 41 Chronicle................................................ 45 Method Summary ......................................... 49 Certification Summary ...................................... 50 Chain of Custody .......................................... 54 Receipt Checklists ......................................... 56 TestAmerica Nashville Page 2 of 56 1/18/2017 Sample Summary Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Lab Sample ID Client Sample ID Matrix Collected Received 490-119827-1 SB-1 (1') Solid 0111011 008:45 01/11/17 09:40 490-119827-2 SB-2 (1') Solid 01/10/17 09:10 01/11/17 09:40 490-119827-3 SB-3 (1') Solid 01/10/17 09:30 01/11/17 09:40 490-119827-4 SB-4 (1') Solid 01/10/17 09:50 01/11/17 09:40 490-119827-5 SB-5 (1') Solid 01/10/17 10:10 01/11/17 09:40 490-119827-6 SB-6 (1') Solid 01/10/17 10:30 01/11/17 09:40 490-119827-7 TMW-1 Water 01/10/17 13:25 01/11/17 09:40 TestAmerica Nashville Page 3 of 56 1 /18/2017 Case Narrative C Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Job ID: 490-119827-1 Laboratory: TestAmerica Nashville Narrative Job Narrative 490-119827-1 Comments No additional comments. Receipt The samples were received on 1/11/2017 9:40 AM; the samples arrived in good condition, properly preserved and, where required, on ice The temperature of the cooler at receipt was 2.91 C. GC/MS VOA Method 8260B: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for analytical batch 490-400532 recovered outside control limits for the following analytes: 2-Chlorotoluene. Method 8260B: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for analytical batch 490-400760 recovered outside control limits for the following analytes: Dibromomethane, dichlorobromomethane, chlorobromomethane, cis-1,2-Dichloroethene, 1,3-Dichloropropane, Chloroform, Methylene Chloride, 1,2-Dichloroethane, 1,2-Dichloropropane and Chlorodibromomethane. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Organic Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. TestAmerica Nashville Page 4 of 56 1 /18/2017 Definitions/Glossary Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Qualifiers GC/MS VOA Qualifier Qualifier Description E Result exceeded calibration range. F1 MS and/or MSD Recovery is outside acceptance limits. * RPD of the LCS and LCSD exceeds the control limits F2 MS/MSD RPD exceeds control limits Metals Qualifier Qualifier Description 4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not applicable. Glossary E: Abbreviation These commonly used abbreviations may or may not be present in this report. c Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Nashville Page 5 of 56 1 /18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-1 (1) Lab Sample ID: 490-119827-1 Date Collected: 01/10/17 08:45 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 89.6 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 0.0390 mg/Kg 0 01/10/17 07:45 01/13/17 05:11 1 Benzene 0.00166 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Bromobenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Bromochloromethane ND * 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Bromodichloromethane ND * 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Bromoform ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Bromomethane ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 2-Butanone (MEK) ND 0.0390 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Carbon disulfide ND 0.00390 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Carbon tetrachloride ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Chlorobenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Chlorodibromomethane ND * 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Chloroethane ND 0.00390 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Chloroform ND * 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Chloromethane ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 2-Chlorotoluene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 4-Chlorotoluene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 cis-1,2-Dichloroethene ND * 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 cis-1,3-Dichloropropene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,2-Dibromo-3-Chloropropane ND 0.00390 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,2-Dibromoethane (EDB) ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Dibromomethane ND * 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,2-Dichlorobenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,3-Dichlorobenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,4-Dichlorobenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Dichlorodifluoromethane ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,1-Dichloroethane ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,2-Dichloroethane ND * 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,1-Dichloroethene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,2-Dichloroethene, Total ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,2-Dichloropropane ND * 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,3-Dichloropropane ND * 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 2,2-Dichloropropane ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,1-Dichloropropene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Diisopropyl ether ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Ethylbenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Hexachlorobutadiene ND 0.00390 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 2-Hexanone ND 0.0390 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Isopropylbenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Methylene Chloride ND 0.00780 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 4-Methyl-2-pentanone (MIBK) ND 0.0390 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Methyl tert-butyl ether ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Naphthalene ND 0.00390 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 n-Butylbenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 N-Propylbenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 p-Isopropyltoluene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 sec- Butylbenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Styrene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 tert-Butylbenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 TestAmerica Nashville Page 6 of 56 1 /18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-1 (1) Lab Sample ID: 490-119827-1 Date Collected: 01/10/17 08:45 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 89.6 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,1,2,2-Tetrachloroethane ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 w 1 Tetrachloroethene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Y Toluene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 trans- 1,2-Dichloroethene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 trans- 1,3-Dichloropropene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,2,3-Trichlorobenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,2,4-Trichlorobenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,1,1-Trichloroethane ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,1,2-Trichloroethane ND 0.00390 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Trichloroethene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Trichlorofluoromethane ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,2,3-Trichloropropane ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,2,4-Trimethylbenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 1,3,5-Trimethylbenzene ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Vinyl chloride ND 0.00156 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Xylenes, Total ND 0.00468 mg/Kg 01/10/17 07:45 01/13/17 05:11 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 70 - 130 01110117 07:45 01/13117 05:11 1 Dibromofluoromethane (Surr) 114 70 - 130 01110117 07:45 01113117 05:11 1 1, 2-Dichloroethane-d4 (Surr) 113 70 - 130 01110117 07:45 01113117 05:11 1 Toluene-d8 (Surr) 91 70 - 130 01110117 07:45 01113117 05:11 1 Method: 6010D - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Silver ND 1.13 mg/Kg 01/16/1710:06 01/16/1717:26 1 Arsenic ND 2.25 mg/Kg 01/12/17 13:02 01/12/17 21:01 1 Barium 109 2.25 mg/Kg 01/12/17 13:02 01/12/17 21:01 1 Cadmium ND 1.12 mg/Kg 01/12/17 13:02 01/12/17 21:01 1 Chromium 12.0 1.12 mg/Kg 01/12/17 13:02 01/12/17 21:01 1 Lead 11.7 1.12 mg/Kg 01/12/17 13:02 01/12/17 21:01 1 Selenium ND 2.25 mg/Kg 01/12/17 13:02 01/12/17 21:01 1 Method: 7471 B - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.109 mg/Kg 01/13/17 09:48 01/16/17 15:55 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Percent Solids 89.6 0.1 % 01/12/ 77 13:00 1 TestAmerica Nashville Page 7 of 56 1 /18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-2 (1') Lab Sample ID: 490-119827-2 Date Collected: 01/10/17 09:10 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 91.0 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 0.0468 mg/Kg * 01/10/17 08:10 01/13/17 05:40 1 Benzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Bromobenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Bromochloromethane ND * 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Bromodichloromethane ND * 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Bromoform ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Bromomethane ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 2-Butanone (MEK) ND 0.0468 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Carbon disulfide ND 0.00468 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Carbon tetrachloride ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Chlorobenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Chlorodibromomethane ND * 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Chloroethane ND 0.00468 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Chloroform ND * 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Chloromethane ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 2-Chlorotoluene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 4-Chlorotoluene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 cis-1,2-Dichloroethene ND * 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 cis-1,3-Dichloropropene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,2-Dibromo-3-Chloropropane ND 0.00468 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,2-Dibromoethane (EDB) ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Dibromomethane ND * 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,2-Dichlorobenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,3-Dichlorobenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,4-Dichlorobenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Dichlorodifluoromethane ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,1-Dichloroethane ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,2-Dichloroethane ND * 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,1-Dichloroethene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,2-Dichloroethene, Total ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,2-Dichloropropane ND * 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,3-Dichloropropane ND * 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 2,2-Dichloropropane ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,1-Dichloropropene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Diisopropyl ether ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Ethylbenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Hexachlorobutadiene ND 0.00468 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 2-Hexanone ND 0.0468 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Isopropylbenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Methylene Chloride ND 0.00936 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 4-Methyl-2-pentanone (MIBK) ND 0.0468 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Methyl tert-butyl ether ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Naphthalene ND 0.00468 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 n-Butylbenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 N-Propylbenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 p-Isopropyltoluene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 sec- Butylbenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Styrene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 tert-Butylbenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 TestAmerica Nashville Page 8 of 56 1 /18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-2 (1) Lab Sample ID: 490-119827-2 Date Collected: 01/10/17 09:10 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 91.0 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,1,2,2-Tetrachloroethane ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Tetrachloroethene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Toluene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 trans- 1,2-Dichloroethene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 trans- 1,3-Dichloropropene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,2,3-Trichlorobenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,2,4-Trichlorobenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,1,1-Trichloroethane ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,1,2-Trichloroethane ND 0.00468 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Trichloroethene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Trichlorofluoromethane ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,2,3-Trichloropropane ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,2,4-Trimethylbenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 1,3,5-Trimethylbenzene ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Vinyl chloride ND 0.00187 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Xylenes, Total ND 0.00562 mg/Kg 01/10/17 08:10 01/13/17 05:40 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 70 - 130 01110117 08:10 01113117 05:40 1 Dibromofluoromethane (Surr) 115 70 - 130 01110117 08:10 01113117 05:40 1 1, 2-Dichloroethane-d4 (Surr) 116 70 - 130 01110117 08:10 01113117 05:40 1 Toluene-d8 (Surr) 90 70 - 130 01110117 08:10 01113117 05:40 1 Method: 6010D - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Silver ND 1.08 mg/Kg 01/16/1710:06 01/16/1717:31 1 Arsenic ND 2.09 mg/Kg 01/12/17 13:02 01/12/17 21:06 1 Barium 121 2.09 mg/Kg 01/12/17 13:02 01/12/17 21:06 1 Cadmium ND 1.05 mg/Kg 01/12/17 13:02 01/12/17 21:06 1 Chromium 7.45 1.05 mg/Kg 01/12/17 13:02 01/12/17 21:06 1 Lead 16.1 1.05 mg/Kg 01/12/17 13:02 01/12/17 21:06 1 Selenium ND 2.09 mg/Kg 01/12/17 13:02 01/12/17 21:06 1 Method: 7471 B - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.106 mg/Kg 01/13/17 09:48 01/16/17 16:03 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Percent Solids 91.0 0.1 % 01/12/ 77 13:00 1 TestAmerica Nashville Page 9 of 56 1 /18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-3 (1') Lab Sample ID: 490-119827-3 Date Collected: 01/10/17 09:30 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 90.6 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 0.0397 mg/Kg * 01/10/17 08:30 01/13/17 06:10 1 Benzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Bromobenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Bromochloromethane ND * 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Bromodichloromethane ND * 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Bromoform ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Bromomethane ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 2-Butanone (MEK) ND 0.0397 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Carbon disulfide ND 0.00397 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Carbon tetrachloride ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Chlorobenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Chlorodibromomethane ND * 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Chloroethane ND 0.00397 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Chloroform ND * 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Chloromethane ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 2-Chlorotoluene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 4-Chlorotoluene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 cis-1,2-Dichloroethene ND * 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 cis-1,3-Dichloropropene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,2-Dibromo-3-Chloropropane ND 0.00397 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,2-Dibromoethane (EDB) ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Dibromomethane ND * 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,2-Dichlorobenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,3-Dichlorobenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,4-Dichlorobenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Dichlorodifluoromethane ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,1-Dichloroethane ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,2-Dichloroethane ND * 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,1-Dichloroethene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,2-Dichloroethene, Total ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,2-Dichloropropane ND * 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,3-Dichloropropane ND * 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 2,2-Dichloropropane ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,1-Dichloropropene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Diisopropyl ether ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Ethylbenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Hexachlorobutadiene ND 0.00397 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 2-Hexanone ND 0.0397 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Isopropylbenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Methylene Chloride ND 0.00794 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 4-Methyl-2-pentanone (MIBK) ND 0.0397 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Methyl tert-butyl ether ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Naphthalene ND 0.00397 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 n-Butylbenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 N-Propylbenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 p-Isopropyltoluene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 sec- Butylbenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Styrene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 tert-Butylbenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 TestAmerica Nashville Page 10 of 56 1/18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-3 (1) Lab Sample ID: 490-119827-3 Date Collected: 01/10/17 09:30 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 90.6 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,1,2,2-Tetrachloroethane ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Tetrachloroethene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Toluene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 trans- 1,2-Dichloroethene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 trans- 1,3-Dichloropropene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,2,3-Trichlorobenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,2,4-Trichlorobenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,1,1-Trichloroethane ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,1,2-Trichloroethane ND 0.00397 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Trichloroethene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Trichlorofluoromethane ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,2,3-Trichloropropane ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,2,4-Trimethylbenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 1,3,5-Trimethylbenzene ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Vinyl chloride ND 0.00159 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Xylenes, Total ND 0.00477 mg/Kg 01/10/17 08:30 01/13/17 06:10 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 101 70 - 130 01110117 08:30 01113117 06:10 1 Dibromofluoromethane (Surr) 116 70 - 130 01110117 08:30 01113117 06:10 1 1, 2-Dichloroethane-d4 (Surr) 118 70 - 130 01110117 08:30 01113117 06:10 1 Toluene-d8 (Surr) 90 70 - 130 01110117 08:30 01113117 06:10 1 Method: 6010D - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Silver ND 1.10 mg/Kg 01/16/1710:06 01/16/1717:36 1 Arsenic 2.32 2.16 mg/Kg 01/12/17 13:02 01/12/17 21:11 1 Barium 115 2.16 mg/Kg 01/12/17 13:02 01/12/17 21:11 1 Cadmium ND 1.08 mg/Kg 01/12/17 13:02 01/12/17 21:11 1 Chromium 8.46 1.08 mg/Kg 01/12/17 13:02 01/12/17 21:11 1 Lead 22.6 1.08 mg/Kg 01/12/17 13:02 01/12/17 21:11 1 Selenium ND 2.16 mg/Kg 01/12/17 13:02 01/12/17 21:11 1 Method: 7471 B - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.110 mg/Kg 01/13/17 09:48 01/16/17 16:06 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Percent Solids 90.6 0.1 % 01/12/17 13:00 1 TestAmerica Nashville Page 11 of 56 1/18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-4 (1') Lab Sample ID: 490-119827-4 Date Collected: 01/10/17 09:50 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 94.1 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 0.0409 mg/Kg * 01/10/17 08:50 01/13/17 06:39 1 Benzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Bromobenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Bromochloromethane ND * 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Bromodichloromethane ND * 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Bromoform ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Bromomethane ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 2-Butanone (MEK) ND 0.0409 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Carbon disulfide ND 0.00409 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Carbon tetrachloride ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Chlorobenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Chlorodibromomethane ND * 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Chloroethane ND 0.00409 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Chloroform ND * 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Chloromethane ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 2-Chlorotoluene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 4-Chlorotoluene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 cis-1,2-Dichloroethene ND * 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 cis-1,3-Dichloropropene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,2-Dibromo-3-Chloropropane ND 0.00409 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,2-Dibromoethane (EDB) ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Dibromomethane ND * 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,2-Dichlorobenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,3-Dichlorobenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,4-Dichlorobenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Dichlorodifluoromethane ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,1-Dichloroethane ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,2-Dichloroethane ND * 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,1-Dichloroethene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,2-Dichloroethene, Total ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,2-Dichloropropane ND * 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,3-Dichloropropane ND * 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 2,2-Dichloropropane ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,1-Dichloropropene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Diisopropyl ether ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Ethylbenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Hexachlorobutadiene ND 0.00409 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 2-Hexanone ND 0.0409 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Isopropylbenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Methylene Chloride ND 0.00818 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 4-Methyl-2-pentanone (MIBK) ND 0.0409 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Methyl tert-butyl ether ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Naphthalene ND 0.00409 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 n-Butylbenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 N-Propylbenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 p-Isopropyltoluene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 sec- Butylbenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Styrene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 tert-Butylbenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 TestAmerica Nashville Page 12 of 56 1/18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-4 (1) Lab Sample ID: 490-119827-4 Date Collected: 01/10/17 09:50 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 94.1 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,1,2,2-Tetrachloroethane ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Tetrachloroethene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Toluene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 trans- 1,2-Dichloroethene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 trans- 1,3-Dichloropropene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,2,3-Trichlorobenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,2,4-Trichlorobenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,1,1-Trichloroethane ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,1,2-Trichloroethane ND 0.00409 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Trichloroethene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Trichlorofluoromethane ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,2,3-Trichloropropane ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,2,4-Trimethylbenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 1,3,5-Trimethylbenzene ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Vinyl chloride ND 0.00164 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Xylenes, Total ND 0.00491 mg/Kg 01/10/17 08:50 01/13/17 06:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 102 70 - 130 01110117 08:50 01113117 06:39 1 Dibromofluoromethane (Surr) 116 70 - 130 01110117 08:50 01113117 06:39 1 1, 2-Dichloroethane-d4 (Surr) 115 70 - 130 01110117 08:50 01113117 06:39 1 Toluene-d8 (Surr) 90 70 - 130 01110117 08:50 01113117 06:39 1 Method: 6010D - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Silver ND 1.03 mg/Kg 01/16/1710:06 01/16/1717:51 1 Arsenic ND 2.06 mg/Kg 01/12/17 13:02 01/12/17 21:16 1 Barium 80.9 2.06 mg/Kg 01/12/17 13:02 01/12/17 21:16 1 Cadmium ND 1.03 mg/Kg 01/12/17 13:02 01/12/17 21:16 1 Chromium 7.88 1.03 mg/Kg 01/12/17 13:02 01/12/17 21:16 1 Lead 18.2 1.03 mg/Kg 01/12/17 13:02 01/12/17 21:16 1 Selenium ND 2.06 mg/Kg 01/12/17 13:02 01/12/17 21:16 1 Method: 7471 B - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.103 mg/Kg 01/13/17 09:48 01/16/17 16:08 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Percent Solids 94.1 0.1 % 01/12/ 77 13:00 1 TestAmerica Nashville Page 13 of 56 1/18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-5 (1') Lab Sample ID: 490-119827-5 Date Collected: 01/10/17 10:10 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 88.3 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 0.0369 mg/Kg * 01/10/17 09:10 01/13/17 07:09 1 Benzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Bromobenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Bromochloromethane ND * 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Bromodichloromethane ND * 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Bromoform ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Bromomethane ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 2-Butanone (MEK) ND 0.0369 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Carbon disulfide ND 0.00369 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Carbon tetrachloride ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Chlorobenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Chlorodibromomethane ND * 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Chloroethane ND 0.00369 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Chloroform ND * 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Chloromethane ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 2-Chlorotoluene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 4-Chlorotoluene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 cis-1,2-Dichloroethene ND * 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 cis-1,3-Dichloropropene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,2-Dibromo-3-Chloropropane ND 0.00369 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,2-Dibromoethane (EDB) ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Dibromomethane ND * 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,2-Dichlorobenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,3-Dichlorobenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,4-Dichlorobenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Dichlorodifluoromethane ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,1-Dichloroethane ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,2-Dichloroethane ND * 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,1-Dichloroethene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,2-Dichloroethene, Total ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,2-Dichloropropane ND * 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,3-Dichloropropane ND * 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 2,2-Dichloropropane ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,1-Dichloropropene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Diisopropyl ether ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Ethylbenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Hexachlorobutadiene ND 0.00369 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 2-Hexanone ND 0.0369 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Isopropylbenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Methylene Chloride ND 0.00739 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 4-Methyl-2-pentanone (MIBK) ND 0.0369 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Methyl tert-butyl ether ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Naphthalene ND 0.00369 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 n-Butylbenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 N-Propylbenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 p-Isopropyltoluene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 sec- Butylbenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Styrene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 tert-Butylbenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 TestAmerica Nashville Page 14 of 56 1/18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-5 (1) Lab Sample ID: 490-119827-5 Date Collected: 01/10/17 10:10 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 88.3 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,1,2,2-Tetrachloroethane ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Tetrachloroethene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Toluene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 trans- 1,2-Dichloroethene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 trans- 1,3-Dichloropropene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,2,3-Trichlorobenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,2,4-Trichlorobenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,1,1-Trichloroethane ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,1,2-Trichloroethane ND 0.00369 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Trichloroethene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Trichlorofluoromethane ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,2,3-Trichloropropane ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,2,4-Trimethylbenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 1,3,5-Trimethylbenzene ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Vinyl chloride ND 0.00148 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Xylenes, Total ND 0.00443 mg/Kg 01/10/17 09:10 01/13/17 07:09 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 103 70 - 130 01110117 09:10 01113117 07:09 1 Dibromofluoromethane (Surr) 114 70 - 130 01110117 09:10 01113117 07:09 1 1, 2-Dichloroethane-d4 (Surr) 115 70 - 130 01110117 09:10 01113117 07:09 1 Toluene-d8 (Surr) 93 70 - 130 01110117 09:10 01113117 07:09 1 Method: 6010D - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Silver ND 1.08 mg/Kg 01/16/1710:06 01/16/1717:56 1 Arsenic ND 2.25 mg/Kg 01/12/17 13:02 01/12/17 21:22 1 Barium 95.8 2.25 mg/Kg 01/12/17 13:02 01/12/17 21:22 1 Cadmium ND 1.12 mg/Kg 01/12/17 13:02 01/12/17 21:22 1 Chromium 11.0 1.12 mg/Kg 01/12/17 13:02 01/12/17 21:22 1 Lead 16.7 1.12 mg/Kg 01/12/17 13:02 01/12/17 21:22 1 Selenium ND 2.25 mg/Kg 01/12/17 13:02 01/12/17 21:22 1 Method: 7471 B - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.109 mg/Kg 01/13/17 09:48 01/16/17 16:11 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Percent Solids 88.3 0.1 % 01/12/ 77 13:00 1 TestAmerica Nashville Page 15 of 56 1/18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-6 (1') Lab Sample ID: 490-119827-6 Date Collected: 01/10/17 10:30 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 88.0 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 0.0437 mg/Kg * 01/10/17 09:30 01/13/17 07:38 1 Benzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Bromobenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Bromochloromethane ND * 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Bromodichloromethane ND * 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Bromoform ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Bromomethane ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 2-Butanone (MEK) ND 0.0437 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Carbon disulfide ND 0.00437 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Carbon tetrachloride ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Chlorobenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Chlorodibromomethane ND * 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Chloroethane ND 0.00437 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Chloroform ND * 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Chloromethane ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 2-Chlorotoluene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 4-Chlorotoluene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 cis-1,2-Dichloroethene ND * 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 cis-1,3-Dichloropropene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,2-Dibromo-3-Chloropropane ND 0.00437 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,2-Dibromoethane (EDB) ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Dibromomethane ND * 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,2-Dichlorobenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,3-Dichlorobenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,4-Dichlorobenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Dichlorodifluoromethane ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,1-Dichloroethane ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,2-Dichloroethane ND * 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,1-Dichloroethene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,2-Dichloroethene, Total ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,2-Dichloropropane ND * 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,3-Dichloropropane ND * 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 2,2-Dichloropropane ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,1-Dichloropropene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Diisopropyl ether ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Ethylbenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Hexachlorobutadiene ND 0.00437 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 2-Hexanone ND 0.0437 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Isopropylbenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Methylene Chloride ND 0.00875 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 4-Methyl-2-pentanone (MIBK) ND 0.0437 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Methyl tert-butyl ether ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Naphthalene ND 0.00437 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 n-Butylbenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 N-Propylbenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 p-Isopropyltoluene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 sec- Butylbenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Styrene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 tert-Butylbenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 TestAmerica Nashville Page 16 of 56 1/18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-6 (1) Lab Sample ID: 490-119827-6 Date Collected: 01/10/17 10:30 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 88.0 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,1,2,2-Tetrachloroethane ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Tetrachloroethene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Toluene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 trans- 1,2-Dichloroethene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 trans- 1,3-Dichloropropene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,2,3-Trichlorobenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,2,4-Trichlorobenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,1,1-Trichloroethane ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,1,2-Trichloroethane ND 0.00437 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Trichloroethene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Trichlorofluoromethane ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,2,3-Trichloropropane ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,2,4-Trimethylbenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 1,3,5-Trimethylbenzene ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Vinyl chloride ND 0.00175 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Xylenes, Total ND 0.00525 mg/Kg 01/10/17 09:30 01/13/17 07:38 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 100 70 - 130 01110117 09:30 01113117 07:38 1 Dibromofluoromethane (Surr) 113 70 - 130 01110117 09:30 01113117 07:38 1 1, 2-Dichloroethane-d4 (Surr) 115 70 - 130 01110117 09:30 01113117 07:38 1 Toluene-d8 (Surr) 92 70 - 130 01110117 09:30 01113117 07:38 1 Method: 6010D - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Silver ND 1.13 mg/Kg 01/16/1710:06 01/16/1718:01 1 Arsenic ND 2.22 mg/Kg 01/12/17 13:02 01/12/17 21:38 1 Barium 59.2 2.22 mg/Kg 01/12/17 13:02 01/12/17 21:38 1 Cadmium ND 1.11 mg/Kg 01/12/17 13:02 01/12/17 21:38 1 Chromium 6.88 1.11 mg/Kg 01/12/17 13:02 01/12/17 21:38 1 Lead 19.0 1.11 mg/Kg 01/12/17 13:02 01/12/17 21:38 1 Selenium ND 2.22 mg/Kg 01/12/17 13:02 01/12/17 21:38 1 Method: 7471 B - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.114 mg/Kg 01/13/17 09:48 01/16/17 16:19 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Percent Solids 88.0 0.1 % 01/12/ 77 13:00 1 TestAmerica Nashville Page 17 of 56 1/18/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: TMW-1 Lab Sample ID: 490-119827-7 Date Collected: 01/10/17 13:25 Matrix: Water Date Received: 01/11/17 09:40 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 25.0 ug/L 01/12/17 18:42 1 Benzene ND 1.00 ug/L 01/12/17 18:42 1 Bromobenzene ND 1.00 ug/L 01/12/17 18:42 1 Bromochloromethane ND 1.00 ug/L 01/12/17 18:42 1 Bromodichloromethane ND 1.00 ug/L 01/12/17 18:42 1 Bromoform ND 1.00 ug/L 01/12/17 18:42 1 Bromomethane ND 1.00 ug/L 01/12/17 18:42 1 2-Butanone (MEK) ND 50.0 ug/L 01/12/17 18:42 1 Diisopropyl ether ND 2.00 ug/L 01/12/17 18:42 1 Carbon disulfide ND 1.00 ug/L 01/12/17 18:42 1 Carbon tetrachloride ND 1.00 ug/L 01/12/17 18:42 1 Chlorobenzene ND 1.00 ug/L 01/12/17 18:42 1 Chlorodibromomethane ND 1.00 ug/L 01/12/17 18:42 1 Chloroethane ND 1.00 ug/L 01/12/17 18:42 1 Chloroform ND 1.00 ug/L 01/12/17 18:42 1 Chloromethane ND 1.00 ug/L 01/12/17 18:42 1 2-Chlorotoluene ND 1.00 ug/L 01/12/17 18:42 1 4-Chlorotoluene ND 1.00 ug/L 01/12/17 18:42 1 cis-1,2-Dichloroethene ND 1.00 ug/L 01/12/17 18:42 1 cis-1,3-Dichloropropene ND 1.00 ug/L 01/12/17 18:42 1 1,2-Dibromo-3-Chloropropane ND 10.0 ug/L 01/12/17 18:42 1 1,2-Dibromoethane (EDB) ND 1.00 ug/L 01/12/17 18:42 1 Dibromomethane ND 1.00 ug/L 01/12/17 18:42 1 1,2-Dichlorobenzene ND 1.00 ug/L 01/12/17 18:42 1 1,3-Dichlorobenzene ND 1.00 ug/L 01/12/17 18:42 1 1,4-Dichlorobenzene ND 1.00 ug/L 01/12/17 18:42 1 Dichlorodifluoromethane ND 1.00 ug/L 01/12/17 18:42 1 1,1-Dichloroethane ND 1.00 ug/L 01/12/17 18:42 1 1,2-Dichloroethane ND 1.00 ug/L 01/12/17 18:42 1 1,1-Dichloroethene ND 1.00 ug/L 01/12/17 18:42 1 1,2-Dichloropropane ND 1.00 ug/L 01/12/17 18:42 1 1,3-Dichloropropane ND 1.00 ug/L 01/12/17 18:42 1 2,2-Dichloropropane ND 1.00 ug/L 01/12/17 18:42 1 1,1-Dichloropropene ND 1.00 ug/L 01/12/17 18:42 1 Ethylbenzene ND 1.00 ug/L 01/12/17 18:42 1 Hexachlorobutadiene ND 2.00 ug/L 01/12/17 18:42 1 2-Hexanone ND 10.0 ug/L 01/12/17 18:42 1 Isopropylbenzene ND 1.00 ug/L 01/12/17 18:42 1 Methylene Chloride ND 5.00 ug/L 01/12/17 18:42 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L 01/12/17 18:42 1 Methyl tert-butyl ether ND 1.00 ug/L 01/12/17 18:42 1 Naphthalene ND 5.00 ug/L 01/12/17 18:42 1 n-Butylbenzene ND 1.00 ug/L 01/12/17 18:42 1 N-Propylbenzene ND 1.00 ug/L 01/12/17 18:42 1 1,2-Dichloroethene, Total ND 1.00 ug/L 01/12/17 18:42 1 p-Isopropyltoluene ND 1.00 ug/L 01/12/17 18:42 1 sec- Butylbenzene ND 1.00 ug/L 01/12/17 18:42 1 Styrene ND 1.00 ug/L 01/12/17 18:42 1 tert-Butylbenzene ND 1.00 ug/L 01/12/17 18:42 1 TestAmerica Nashville Page 18 of 56 1/18/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Client Sample ID: TMW-1 Lab Sample ID: 490-119827-7 Date Collected: 01/10/17 13:25 Matrix: Water Date Received: 01/11/17 09:40 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 1.00 ug/L 01/12/17 18:42 1 1,1,2,2-Tetrachloroethane ND 1.00 ug/L 01/12/17 18:42 1 Tetrachloroethene ND 1.00 ug/L 01/12/17 18:42 1 Toluene ND 1.00 ug/L 01/12/17 18:42 1 trans- 1,2-Dichloroethene ND 1.00 ug/L 01/12/17 18:42 1 trans- 1,3-Dichloropropene ND 1.00 ug/L 01/12/17 18:42 1 1,2,3-Trichlorobenzene ND 1.00 ug/L 01/12/17 18:42 1 1,2,4-Trichlorobenzene ND 1.00 ug/L 01/12/17 18:42 1 1,1,1-Trichloroethane ND 1.00 ug/L 01/12/17 18:42 1 1,1,2-Trichloroethane ND 1.00 ug/L 01/12/17 18:42 1 Trichloroethene ND 1.00 ug/L 01/12/17 18:42 1 Trichlorofluoromethane ND 1.00 ug/L 01/12/17 18:42 1 1,2,3-Trichloropropane ND 1.00 ug/L 01/12/17 18:42 1 1,2,4-Trimethylbenzene ND 1.00 ug/L 01/12/17 18:42 1 1,3,5-Trimethylbenzene ND 1.00 ug/L 01/12/17 18:42 1 Vinyl chloride ND 1.00 ug/L 01/12/17 18:42 1 Xylenes, Total ND 3.00 ug/L 01/12/17 18:42 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 70 - 130 01112117 18:42 1 Dibromofluoromethane (Surr) 96 70 - 130 01112117 18:42 1 1,2-Dichloroethane-d4 (Surr) 90 70- 130 01112117 18:42 1 Toluene-d8 (Surr) 99 70 - 130 01112117 18:42 1 Method: 6010D - Metals (ICP) - Dissolved Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Silver ND 0.00500 mg/L 01/17/17 07:58 01/17/17 14:56 1 Arsenic ND 0.0100 mg/L 01/17/17 07:58 01/17/17 14:56 1 Barium 0.222 0.0100 mg/L 01/17/17 07:58 01/17/17 14:56 1 Cadmium ND 0.00100 mg/L 01/17/17 07:58 01/17/17 14:56 1 Chromium ND 0.00500 mg/L 01/17/17 07:58 01/17/17 14:56 1 Lead ND 0.00500 mg/L 01/17/17 07:58 01/17/17 14:56 1 Selenium ND 0.0100 mg/L 01/17/17 07:58 01/17/17 14:56 1 Method: 7470A - Mercury (CVAA) - Dissolved Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.000200 mg/L 01/17/17 08:12 01/17/17 13:02 1 0 TestAmerica Nashville Page 19 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) Lab Sample ID: MB 490-400532/7 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 400532 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 25.0 ug/L 01/12/17 12:10 1 Benzene ND 1.00 ug/L 01/12/17 12:10 1 Bromobenzene ND 1.00 ug/L 01/12/17 12:10 1 Bromochloromethane ND 1.00 ug/L 01/12/17 12:10 1 Bromodichloromethane ND 1.00 ug/L 01/12/17 12:10 1 Bromoform ND 1.00 ug/L 01/12/17 12:10 1 Bromomethane ND 1.00 ug/L 01/12/17 12:10 1 2-Butanone (MEK) ND 50.0 ug/L 01/12/17 12:10 1 Carbon disulfide ND 1.00 ug/L 01/12/17 12:10 1 Carbon tetrachloride ND 1.00 ug/L 01/12/17 12:10 1 Chlorobenzene ND 1.00 ug/L 01/12/17 12:10 1 Chlorodibromomethane ND 1.00 ug/L 01/12/17 12:10 1 Chloroethane ND 1.00 ug/L 01/12/17 12:10 1 Chloroform ND 1.00 ug/L 01/12/17 12:10 1 Chloromethane ND 1.00 ug/L 01/12/17 12:10 1 2-Chlorotoluene ND 1.00 ug/L 01/12/17 12:10 1 4-Chlorotoluene ND 1.00 ug/L 01/12/17 12:10 1 cis-1,2-Dichloroethene ND 1.00 ug/L 01/12/17 12:10 1 cis-1,3-Dichloropropene ND 1.00 ug/L 01/12/17 12:10 1 1,2-Dibromo-3-Chloropropane ND 10.0 ug/L 01/12/17 12:10 1 1,2-Dibromoethane (EDB) ND 1.00 ug/L 01/12/17 12:10 1 Dibromomethane ND 1.00 ug/L 01/12/17 12:10 1 1,2-Dichlorobenzene ND 1.00 ug/L 01/12/17 12:10 1 1,3-Dichlorobenzene ND 1.00 ug/L 01/12/17 12:10 1 1,4-Dichlorobenzene ND 1.00 ug/L 01/12/17 12:10 1 Dichlorodifluoromethane ND 1.00 ug/L 01/12/17 12:10 1 1,1-Dichloroethane ND 1.00 ug/L 01/12/17 12:10 1 1,2-Dichloroethane ND 1.00 ug/L 01/12/17 12:10 1 1,1-Dichloroethene ND 1.00 ug/L 01/12/17 12:10 1 1,2-Dichloropropane ND 1.00 ug/L 01/12/17 12:10 1 1,3-Dichloropropane ND 1.00 ug/L 01/12/17 12:10 1 2,2-Dichloropropane ND 1.00 ug/L 01/12/17 12:10 1 1,1-Dichloropropene ND 1.00 ug/L 01/12/17 12:10 1 Diisopropyl ether ND 2.00 ug/L 01/12/17 12:10 1 Ethylbenzene ND 1.00 ug/L 01/12/17 12:10 1 Hexachlorobutadiene ND 2.00 ug/L 01/12/17 12:10 1 2-Hexanone ND 10.0 ug/L 01/12/17 12:10 1 Isopropylbenzene ND 1.00 ug/L 01/12/17 12:10 1 Methylene Chloride ND 5.00 ug/L 01/12/17 12:10 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L 01/12/17 12:10 1 Methyl tert-butyl ether ND 1.00 ug/L 01/12/17 12:10 1 Naphthalene ND 5.00 ug/L 01/12/17 12:10 1 n-Butylbenzene ND 1.00 ug/L 01/12/17 12:10 1 1,2-Dichloroethene, Total ND 1.00 ug/L 01/12/17 12:10 1 N-Propylbenzene ND 1.00 ug/L 01/12/17 12:10 1 p-Isopropyltoluene ND 1.00 ug/L 01/12/17 12:10 1 sec-Butylbenzene ND 1.00 ug/L 01/12/17 12:10 1 Styrene ND 1.00 ug/L 01/12/17 12:10 1 TestAmerica Nashville Page 20 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 490-40053217 Matrix: Water Analysis Batch: 400532 MB MB Analyte Result Qualifier RL MDL Unit Client Sample ID: Method Blank Prep Type: Total/NA D Prepared Analyzed Dil Fac tert-Butylbenzene ND 1.00 ug/L 01/12/17 12:10 1 1,1,1,2-Tetrachloroethane ND 1.00 ug/L 01/12/17 12:10 1 1,1,2,2-Tetrachloroethane ND 1.00 ug/L 01/12/17 12:10 1 Tetrachloroethene ND 1.00 ug/L 01/12/17 12:10 1 Toluene ND 1.00 ug/L 01/12/17 12:10 1 trans- 1,2-Dichloroethene ND 1.00 ug/L 01/12/17 12:10 1 trans- 1,3-Dichloropropene ND 1.00 ug/L 01/12/17 12:10 1 1,2,3-Trichlorobenzene ND 1.00 ug/L 01/12/17 12:10 1 1,2,4-Trichlorobenzene ND 1.00 ug/L 01/12/17 12:10 1 1,1,1-Trichloroethane ND 1.00 ug/L 01/12/17 12:10 1 1,1,2-Trichloroethane ND 1.00 ug/L 01/12/17 12:10 1 Trichloroethene ND 1.00 ug/L 01/12/17 12:10 1 Trichlorofluoromethane ND 1.00 ug/L 01/12/17 12:10 1 1,2,3-Trichloropropane ND 1.00 ug/L 01/12/17 12:10 1 1,2,4-Trimethylbenzene ND 1.00 ug/L 01/12/17 12:10 1 1,3,5-Trimethylbenzene ND 1.00 ug/L 01/12/17 12:10 1 Vinyl chloride ND 1.00 ug/L 01/12/17 12:10 1 Xylenes, Total ND 3.00 ug/L 01/12/17 12:10 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 99 70 - 130 01112117 12:10 1 Dibromofluoromethane (Surr) 94 70 - 130 01112117 12:10 1 1,2-Dichloroethane-d4 (Surr) 89 70- 130 01112117 12:10 1 Toluene-d8 (Surr) 92 70 - 130 01112117 12:10 1 Lab Sample ID: LCS 490-400532/3 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 400532 Analyte Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene cis-1.2-Dichloroethene Spike LCS LCS Added Result Qualifier 100 86.38 20.0 18.89 20.0 18.65 20.0 17.58 20.0 16.67 20.0 21.01 20.0 18.19 100 96.46 20.0 22.21 20.0 17.94 20.0 18.70 20.0 19.03 20.0 20.75 20.0 17.21 20.0 26.02 20.0 20.95 20.0 18.42 20.0 19.41 %Rec. Unit D %Rec Limits ug/L 86 39-150 ug/L 94 70-130 ug/L 93 70-130 ug/L 88 70-130 ug/L 83 70-130 ug/L 105 70-137 ug/L 91 53-150 ug/L 96 55-143 ug/L ill 64-135 ug/L 90 70-147 ug/L 93 70-130 ug/L 95 70-133 ug/L 104 60-138 ug/L 86 70-130 ug/L 130 33-150 ug/L 105 70-130 ug/L 92 70-130 ug/L 97 70-130 TestAmerica Nashville Page 21 of 56 1/18/2017 QC Sample Results C Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 490-400532/3 Matrix: Water Analysis Batch: 400532 Client Sample ID: Lab Control Sample Prep Type: Total/NA Analyte Spike Added LCS LCS Result Qualifier Unit D %Rec %Rec. Limits cis-1,3-Dichloropropene 20.0 16.83 ug/L 84 70 -133 1,2-Dibromo-3-Chloropropane 20.0 17.95 ug/L 90 45-138 1,2-Dibromoethane(EDB) 20.0 16.87 ug/L 84 70-130 Dibromomethane 20.0 16.33 ug/L 82 70 -130 1,2-Dichlorobenzene 20.0 17.64 ug/L 88 70 -130 1,3-Dichlorobenzene 20.0 18.09 ug/L 90 70 -130 1,4-Dichlorobenzene 20.0 17.87 ug/L 89 70 -130 Dichlorodifluoromethane 20.0 19.58 ug/L 98 48 -150 1,1-Dichloroethane 20.0 20.88 ug/L 104 70-130 1,2-Dichloroethane 20.0 16.53 ug/L 83 70 -130 1,1-Dichloroethene 20.0 19.62 ug/L 98 70-132 1,2-Dichloropropane 20.0 18.94 ug/L 95 70 -130 1,3-Dichloropropane 20.0 17.67 ug/L 88 70 -130 2,2-Dichloropropane 20.0 17.46 ug/L 87 60 -143 1,1-Dichloropropene 20.0 18.22 ug/L 91 70-130 Diisopropyl ether 20.0 20.10 ug/L 100 66 -142 Ethylbenzene 20.0 18.31 ug/L 92 70 -130 Hexachlorobutadiene 20.0 20.72 ug/L 104 70 -138 2-Hexanone 100 89.76 ug/L 90 54-142 Isopropylbenzene 20.0 18.05 ug/L 90 70 -131 Methylene Chloride 20.0 18.26 ug/L 91 70 -130 4-Methyl-2-pentanone (MIBK) 100 90.49 ug/L 90 60-137 Methyl tert-butyl ether 20.0 16.35 ug/L 82 70 -130 Naphthalene 20.0 15.56 ug/L 78 54 -150 n-Butylbenzene 20.0 18.00 ug/L 90 68 -137 1,2-Dichloroethene, Total 40.0 37.97 ug/L 95 70 -130 N-Propylbenzene 20.0 19.20 ug/L 96 70 -134 p-Isopropyltoluene 20.0 18.02 ug/L 90 66 -130 sec- Butylbenzene 20.0 18.28 ug/L 91 70 -135 Styrene 20.0 18.37 ug/L 92 70 -130 tert-Butylbenzene 20.0 18.61 ug/L 93 70 -130 1,1,1,2-Tetrachloroethane 20.0 19.22 ug/L 96 70-130 1,1,2,2-Tetrachloroethane 20.0 18.91 ug/L 95 69-131 Tetrachloroethene 20.0 18.93 ug/L 95 70 -130 Toluene 20.0 18.40 ug/L 92 70 -130 trans- 1,2-Dichloroethene 20.0 18.56 ug/L 93 70-130 trans- 1,3-Dichloropropene 20.0 15.88 ug/L 79 63-142 1,2,3-Trichlorobenzene 20.0 18.00 ug/L 90 46-150 1,2,4-Trichlorobenzene 20.0 18.21 ug/L 91 58-147 1,1,1-Trichloroethane 20.0 16.96 ug/L 85 70-135 1,1,2-Trichloroethane 20.0 17.18 ug/L 86 70-130 Trichloroethene 20.0 18.34 ug/L 92 70 -130 Trichlorofluoromethane 20.0 18.47 ug/L 92 59 -150 1,2,3-Trichloropropane 20.0 17.37 ug/L 87 70-131 1,2,4-Trimethylbenzene 20.0 17.77 ug/L 89 70 -130 1,3,5-Trimethylbenzene 20.0 18.37 ug/L 92 70 -130 Vinyl chloride 20.0 21.27 ug/L 106 57 -137 Xylenes, Total 40.0 36.53 ug/L 91 70 -132 TestAmerica Nashville Page 22 of 56 1/18/2017 QC Sample Results C Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 490-400532/3 Matrix: Water Analysis Batch: 400532 Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 100 70 - 130 Dibromofluoromethane (Surr) 94 70 - 130 1,2-Dichloroethane-d4 (Surr) 86 70- 130 Toluene-d8 (Surr) 98 70 - 130 Lab Sample ID: LCSD 490-400532/4 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 400532 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Acetone 100 90.10 ug/L 90 39 -150 4 23 Benzene 20.0 18.50 ug/L 93 70 -130 2 12 Bromobenzene 20.0 18.31 ug/L 92 70 -130 2 16 Bromochloromethane 20.0 17.40 ug/L 87 70 -130 1 16 Bromodichloromethane 20.0 16.26 ug/L 81 70 -130 3 14 E: Bromoform 20.0 20.74 ug/L 104 70 -137 1 14 Bromomethane 20.0 17.95 ug/L 90 53 -150 1 19 2-Butanone (MEK) 100 94.67 ug/L 95 55 -143 2 19 Carbon disulfide 20.0 22.33 ug/L 112 64 -135 1 16 Carbon tetrachloride 20.0 18.11 ug/L 91 70 -147 1 16 Chlorobenzene 20.0 18.16 ug/L 91 70 -130 3 12 Chlorodibromomethane 20.0 18.61 ug/L 93 70 -133 2 13 Chloroethane 20.0 20.35 ug/L 102 60 -138 2 15 Chloroform 20.0 17.74 ug/L 89 70 -130 3 14 Chloromethane 20.0 24.93 ug/L 125 33 -150 4 20 2-Chlorotoluene 20.0 16.85 ug/L 84 70 -130 22 15 4-Chlorotoluene 20.0 17.83 ug/L 89 70 -130 3 15 cis-1,2-Dichloroethene 20.0 18.66 ug/L 93 70 -130 4 15 cis-1,3-Dichloropropene 20.0 15.56 ug/L 78 70 -133 8 15 1,2-Dibromo-3-Chloropropane 20.0 19.00 ug/L 95 45-138 6 19 1,2-Dibromoethane(EDB) 20.0 16.75 ug/L 84 70-130 1 13 Dibromomethane 20.0 16.03 ug/L 80 70 -130 2 14 1,2-Dichlorobenzene 20.0 17.46 ug/L 87 70 -130 1 12 1,3-Dichlorobenzene 20.0 17.98 ug/L 90 70 -130 1 13 1,4-Dichlorobenzene 20.0 17.39 ug/L 87 70 -130 3 12 Dichlorodifluoromethane 20.0 19.30 ug/L 97 48 -150 1 16 1,1-Dichloroethane 20.0 20.22 ug/L 101 70-130 3 17 1,2-Dichloroethane 20.0 16.55 ug/L 83 70 -130 0 13 1,1-Dichloroethene 20.0 19.57 ug/L 98 70-132 0 20 1,2-Dichloropropane 20.0 18.98 ug/L 95 70 -130 0 15 1,3-Dichloropropane 20.0 17.41 ug/L 87 70 -130 1 12 2,2-Dichloropropane 20.0 16.73 ug/L 84 60 -143 4 20 1,1-Dichloropropene 20.0 18.15 ug/L 91 70-130 0 16 Diisopropyl ether 20.0 19.86 ug/L 99 66 -142 1 14 Ethylbenzene 20.0 17.75 ug/L 89 70 -130 3 12 Hexachlorobutadiene 20.0 20.65 ug/L 103 70 -138 0 16 2-Hexanone 100 91.00 ug/L 91 54 -142 1 17 Isopropylbenzene 20.0 17.47 ug/L 87 70 -131 3 13 TestAmerica Nashville Page 23 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 490-400532/4 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 400532 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Methylene Chloride 20.0 18.04 ug/L 90 70 -130 1 15 4-Methyl-2-pentanone (MIBK) 100 89.14 ug/L 89 60-137 2 21 Methyl tert-butyl ether 20.0 16.22 ug/L 81 70 -130 1 16 Naphthalene 20.0 15.56 ug/L 78 54 -150 0 15 n-Butylbenzene 20.0 18.04 ug/L 90 68 -137 0 14 1,2-Dichloroethene, Total 40.0 38.13 ug/L 95 70 -130 0 14 N-Propylbenzene 20.0 18.70 ug/L 93 70-134 3 14 p-Isopropyltoluene 20.0 17.53 ug/L 88 66 -130 3 13 sec-Butylbenzene 20.0 17.81 ug/L 89 70 -135 3 14 Styrene 20.0 17.95 ug/L 90 70 -130 2 12 tert-Butylbenzene 20.0 18.37 ug/L 92 70 -130 1 14 1,1,1,2-Tetrachloroethane 20.0 18.83 ug/L 94 70-130 2 13 1,1,2,2-Tetrachloroethane 20.0 18.60 ug/L 93 69-131 2 15 Tetrachloroethene 20.0 18.46 ug/L 92 70 -130 3 17 Toluene 20.0 17.56 ug/L 88 70 -130 5 13 trans- 1,2-Dichloroethene 20.0 19.47 ug/L 97 70-130 5 15 trans- 1,3-Dichloropropene 20.0 15.59 ug/L 78 63 -142 2 13 1,2,3-Trichlorobenzene 20.0 17.56 ug/L 88 46-150 2 16 1,2,4-Trichlorobenzene 20.0 18.05 ug/L 90 58-147 1 15 1,1,1-Trichloroethane 20.0 16.55 ug/L 83 70-135 2 15 1,1,2-Trichloroethane 20.0 17.03 ug/L 85 70-130 1 13 Trichloroethene 20.0 17.86 ug/L 89 70 -130 3 14 Trichlorofluoromethane 20.0 18.10 ug/L 91 59 -150 2 22 1,2,3-Trichloropropane 20.0 17.15 ug/L 86 70-131 1 14 1,2,4-Trimethylbenzene 20.0 17.37 ug/L 87 70 -130 2 13 1,3,5-Trimethylbenzene 20.0 17.92 ug/L 90 70-130 2 14 Vinyl chloride 20.0 20.68 ug/L 103 57 -137 3 15 Xylenes, Total 40.0 35.04 ug/L 88 70 -132 4 11 LCSD LCSD Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 98 70 - 130 Dibromofluoromethane (Surr) 94 70 - 130 1,2-Dichloroethene-d4 (Surr) 90 70- 130 Toluene-d8 (Surr) 95 70 - 130 Lab Sample ID: 490-119778-A-2 MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA Analysis Batch: 400532 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Acetone ND 6250 5302 ug/L 85 39 -150 Benzene 77.3 1250 1250 ug/L 94 55-147 Bromobenzene ND 1250 1217 ug/L 97 60 -133 Bromochloromethane ND 1250 1106 ug/L 88 59 -132 Bromodichloromethane ND 1250 1173 ug/L 94 70-140 Bromoform ND 1250 1307 ug/L 105 53 -150 Bromomethane ND 1250 1172 ug/L 94 30 -150 2-Butanone (MEK) ND 6250 5763 ug/L 92 50 -143 TestAmerica Nashville Page 24 of 56 1/18/2017 QC Sample Results C Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-119778-A-2 MS Matrix: Water Analysis Batch: 400532 Client Sample ID: Matrix Spike Prep Type: Total/NA Analyte Sample Sample Result Qualifier Spike Added MS MS Result Qualifier Unit D %Rec %Rec. Limits Carbon disulfide ND 1250 1308 ug/L 105 35-150 Carbon tetrachloride ND 1250 1228 ug/L 98 56 -150 Chlorobenzene ND 1250 1156 ug/L 93 70 -130 Chlorodibromomethane ND 1250 1220 ug/L 98 66 -140 Chloroethane ND 1250 1256 ug/L 100 58 -141 Chloroform ND 1250 1201 ug/L 96 66 -138 Chloromethane ND 1250 1589 ug/L 127 10 -150 2-Chlorotoluene ND 1250 1207 ug/L 97 67 -138 4-Chlorotoluene ND 1250 1169 ug/L 93 69 -138 cis-1,2-Dichloroethene ND 1250 1256 ug/L 100 68-131 cis-1,3-Dichloropropene ND 1250 1148 ug/L 92 70-133 1,2-Dibromo-3-Chloropropane ND 1250 1219 ug/L 98 38-138 1,2-Dibromoethane(EDB) ND 1250 1065 ug/L 85 65-137 Dibromomethane ND 1250 1128 ug/L 90 70 -130 1,2-Dichlorobenzene ND 1250 1138 ug/L 91 70-130 1,3-Dichlorobenzene ND 1250 1186 ug/L 95 68-131 1,4-Dichlorobenzene ND 1250 1167 ug/L 93 70-130 Dichlorodifluoromethane ND 1250 1153 ug/L 92 10-150 1,1-Dichloroethane ND 1250 1349 ug/L 108 61-139 1,2-Dichloroethane ND 1250 1052 ug/L 84 64 -136 1,1-Dichloroethene ND 1250 1231 ug/L 98 54-150 1,2-Dichloropropane ND 1250 1318 ug/L 105 67-130 1,3-Dichloropropane ND 1250 1106 ug/L 88 70-130 2,2-Dichloropropane ND 1250 1157 ug/L 93 50 -146 1,1-Dichloropropene ND 1250 1220 ug/L 98 54-150 Diisopropyl ether ND 1250 1244 ug/L 100 56 -142 Ethylbenzene 2420 F1 1250 2916 EF1 ug/L 39 65-139 Hexachlorobutadiene ND 1250 1407 ug/L 113 61 -141 2-Hexanone ND 6250 5334 ug/L 85 44 -150 Isopropylbenzene 124 1250 1231 ug/L 89 70 -137 Methylene Chloride ND 1250 1304 ug/L 104 64 -130 4-Methyl-2-pentanone (MIBK) ND 6250 5533 ug/L 89 50-140 Methyl tert-butyl ether ND 1250 1033 ug/L 81 55 -141 Naphthalene 631 1250 1656 ug/L 82 32 -150 n-Butylbenzene 36.2 1250 1264 ug/L 98 61 -141 1,2-Dichloroethene, Total ND 2500 2514 ug/L 101 60-134 N-Propylbenzene 329 1250 1468 ug/L 91 53-150 p-Isopropyltoluene ND 1250 1189 ug/L 95 66-137 sec-Butylbenzene ND 1250 1218 ug/L 96 55 -136 Styrene ND 1250 1164 ug/L 93 70 -130 tert-Butylbenzene ND 1250 1229 ug/L 98 70 -138 1,1,1,2-Tetrachloroethane ND 1250 1264 ug/L 101 70-131 1,1,2,2-Tetrachloroethane ND 1250 1175 ug/L 94 56-145 Tetrachloroethene ND 1250 1214 ug/L 97 57 -138 Toluene 593 1250 1595 ug/L 80 64 -136 trans- 1,2-Dichloroethene ND 1250 1258 ug/L 101 59-143 trans- 1,3-Dichloropropene ND 1250 1043 ug/L 83 63 -142 1,2,3-Trichlorobenzene ND 1250 1160 ug/L 93 36-150 TestAmerica Nashville Page 25 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-119778-A-2 MS Client Sample ID: Matrix Spike Matrix: Water Prep Type: Total/NA Analysis Batch: 400532 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits 1,2,4-Trichlorobenzene ND 1250 1229 ug/L 98 47-147 1,1,1-Trichloroethane ND 1250 1143 ug/L 91 68-144 1,1,2-Trichloroethane ND 1250 1090 ug/L 87 70-130 Trichloroethene ND 1250 1196 ug/L 96 63 -135 Trichlorofluoromethane ND 1250 1186 ug/L 95 44 -150 1,2,3-Trichloropropane ND 1250 1125 ug/L 90 65-131 1,2,4-Trimethylbenzene 939 1250 1900 ug/L 77 64 -136 1,3,5-Trimethylbenzene 191 1250 1309 ug/L 89 69-139 Vinyl chloride ND 1250 1281 ug/L 102 57-150 Xylenes, Total 3850 F1 2500 5329 F1 ug/L 59 69-132 MS MS Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 101 70 - 130 Dibromofluoromethane (Surr) 95 70 - 130 1,2-Dichloroethane-d4 (Surr) 88 70- 130 Toluene-d8 (Surr) 97 70 - 130 Lab Sample ID: 490-119778-A-2 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA Analysis Batch: 400532 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Acetone ND 6250 5417 ug/L 87 39 -150 2 28 Benzene 77.3 1250 1271 ug/L 96 55-147 2 22 Bromobenzene ND 1250 1226 ug/L 98 60 -133 1 18 Bromochloromethane ND 1250 1153 ug/L 92 59 -132 4 21 Bromodichloromethane ND 1250 1242 ug/L 99 70-140 6 196 Bromoform ND 1250 1332 ug/L 107 53 -150 2 20 Bromomethane ND 1250 1240 ug/L 99 30 -150 6 44 2-Butanone (MEK) ND 6250 6064 ug/L 97 50 -143 5 28 Carbon disulfide ND 1250 1308 ug/L 105 35-150 0 34 Carbon tetrachloride ND 1250 1288 ug/L 103 56 -150 5 18 Chlorobenzene ND 1250 1189 ug/L 95 70 -130 3 15 Chlorodibromomethane ND 1250 1290 ug/L 103 66 -140 6 19 Chloroethane ND 1250 1288 ug/L 103 58 -141 3 31 Chloroform ND 1250 1238 ug/L 99 66 -138 3 21 Chloromethane ND 1250 1634 ug/L 131 10 -150 3 43 2-Chlorotoluene ND 1250 1223 ug/L 98 67 -138 1 17 4-Chlorotoluene ND 1250 1174 ug/L 94 69 -138 0 15 cis-1,2-Dichloroethene ND 1250 1301 ug/L 104 68-131 4 21 cis-1,3-Dichloropropene ND 1250 1176 ug/L 94 70-133 2 19 1,2-Dibromo-3-Chloropropane ND 1250 1273 ug/L 102 38-138 4 26 1,2-Dibromoethane(EDB) ND 1250 1114 ug/L 89 65-137 4 21 Dibromomethane ND 1250 1171 ug/L 94 70 -130 4 19 1,2-Dichlorobenzene ND 1250 1167 ug/L 93 70-130 2 15 1,3-Dichlorobenzene ND 1250 1204 ug/L 96 68-131 2 14 1,4-Dichlorobenzene ND 1250 1176 ug/L 94 70-130 1 14 Dichlorodifluoromethane ND 1250 1101 ug/L 88 10-150 5 50 TestAmerica Nashville Page 26 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-119778-A-2 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Total/NA Analysis Batch: 400532 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit 1,1-Dichloroethane ND 1250 1406 ug/L 113 61-139 4 23 1,2-Dichloroethane ND 1250 1095 ug/L 88 64 -136 4 22 1,1-Dichloroethene ND 1250 1280 ug/L 102 54-150 4 24 1,2-Dichloropropane ND 1250 1400 ug/L 112 67-130 6 19 1,3-Dichloropropane ND 1250 1134 ug/L 91 70-130 3 17 2,2-Dichloropropane ND 1250 1162 ug/L 93 50 -146 0 20 1,1-Dichloropropene ND 1250 1256 ug/L 100 54-150 3 24 Diisopropyl ether ND 1250 1301 ug/L 104 56 -142 4 22 Ethylbenzene 2420 F1 1250 2885 EF1 ug/L 37 65-139 1 18 Hexachlorobutadiene ND 1250 1486 ug/L 119 61 -141 5 26 2-Hexanone ND 6250 5537 ug/L 89 44 -150 4 21 Isopropylbenzene 124 1250 1260 ug/L 91 70 -137 2 17 Methylene Chloride ND 1250 1337 ug/L 107 64 -130 3 22 4-Methyl-2-pentanone (MIBK) ND 6250 5807 ug/L 93 50-140 5 24 Methyl tert-butyl ether ND 1250 1082 ug/L 85 55 -141 5 24 Naphthalene 631 1250 1735 ug/L 88 32 -150 5 40 n-Butylbenzene 36.2 1250 1284 ug/L 100 61 -141 2 17 1,2-Dichloroethene, Total ND 2500 2618 ug/L 105 60-134 4 22 N-Propylbenzene 329 1250 1477 ug/L 92 53-150 1 18 p-Isopropyltoluene ND 1250 1201 ug/L 96 66-137 1 16 sec-Butylbenzene ND 1250 1234 ug/L 97 55 -136 1 50 Styrene ND 1250 1194 ug/L 96 70 -130 3 16 tert-Butylbenzene ND 1250 1259 ug/L 101 70 -138 2 17 1,1,1,2-Tetrachloroethane ND 1250 1298 ug/L 104 70-131 3 16 1,1,2,2-Tetrachloroethane ND 1250 1211 ug/L 97 56-145 3 19 Tetrachloroethene ND 1250 1228 ug/L 98 57 -138 1 17 Toluene 593 1250 1604 ug/L 81 64 -136 1 18 trans- 1,2-Dichloroethene ND 1250 1317 ug/L 105 59-143 5 25 trans- 1,3-Dichloropropene ND 1250 1091 ug/L 87 63-142 4 18 1,2,3-Trichlorobenzene ND 1250 1220 ug/L 98 36-150 5 43 1,2,4-Trichlorobenzene ND 1250 1297 ug/L 104 47-147 5 24 1,1,1-Trichloroethane ND 1250 1176 ug/L 94 68-144 3 17 1,1,2-Trichloroethane ND 1250 1115 ug/L 89 70-130 2 18 Trichloroethene ND 1250 1271 ug/L 102 63 -135 6 17 Trichlorofluoromethane ND 1250 1204 ug/L 96 44 -150 2 32 1,2,3-Trichloropropane ND 1250 1138 ug/L 91 65-131 1 19 1,2,4-Trimethylbenzene 939 1250 1895 ug/L 76 64 -136 0 18 1,3,5-Trimethylbenzene 191 1250 1316 ug/L 90 69-139 1 17 Vinyl chloride ND 1250 1315 ug/L 105 57-150 3 37 Xylenes, Total 3850 F1 2500 5318 F1 ug/L 59 69-132 0 17 MSD MSD Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 100 70 - 130 Dibromofluoromethane (Surr) 95 70 - 130 1,2-Dichloroethane-d4 (Surr) 87 70- 130 Toluene-d8 (Surr) 97 70 - 130 TestAmerica Nashville Page 27 of 56 1/18/2017 QC Sample Results C Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-119880-A-14-A MSD Matrix: Solid Analysis Batch: 400760 Analyte Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chlorodibromomethane Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene cis-1,2-Dichloroethene cis-1,3-Dichloropropene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene Diisopropyl ether Ethylbenzene Hexachlorobutadiene 2-Hexanone Isopropylbenzene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Naphthalene n-Butylbenzene 1,2-Dichloroethene, Total N-Propylbenzene p-Isopropyltoluene sec-Butylbenzene Styrene Sample Sample Result Qualifier ND ND ND ND * ND * ND ND ND ND ND ND ND ND ND ND ND ND 0.00680 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.00680 ND ND ND ND F1 F2 Spike Added 0.240 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.240 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.0480 0.240 0.0480 0.0480 0.240 0.0480 0.0480 0.0480 0.0960 0.0480 0.0480 0.0480 0.0480 MSD MSD Result Qualifier 0.2000 0.03441 0.02560 0.03038 0.02869 0.02182 0.02872 0.1637 0.03363 0.03437 0.02891 0.02303 0.03755 0.03407 0.02853 0.02871 0.02787 0.03440 0.02476 0.01973 0.02443 0.02742 0.02243 0.02421 0.02400 0.04333 0.03162 0.03004 0.03509 0.02944 0.02486 0.03248 0.03352 0.02744 0.03285 0.01657 0.09399 0.02974 0.03095 0.1120 0.02635 0.01317 0.02375 0.06729 0.02867 0.02491 0.02675 0.002715 F1 F2 Client Sample ID: Matrix Spike Duplicate Prep Type: Total/NA Prep Batch:400721 %Rec. RPD Unit D %Rec Limits RPD Limit mg/Kg 7 80 10-150 36 50 mg/Kg # 72 21 -150 9 50 mg/Kg # 53 10-150 11 50 mg/Kg 63 10-150 11 50 mg/Kg 60 10-150 13 50 mg/Kg 45 10-150 29 50 mg/Kg 11'� 60 10 -150 17 50 mg/Kg 11'� 68 10 -150 29 50 mg/Kg ;� 70 10 -150 10 50 mg/Kg 72 10-150 2 50 mg/Kg 60 10-150 11 50 mg/Kg # 48 10-150 20 50 mg/Kg 78 10-150 16 50 mg/Kg 71 10-150 11 50 mg/Kg 59 10-150 2 50 mg/Kg 60 10-150 3 50 mg/Kg 58 10-150 4 50 mg/Kg 57 10-150 3 50 mg/Kg 52 10-150 15 50 mg/Kg 41 10-150 32 50 mg/Kg 51 10-150 16 50 mg/Kg 57 10-150 12 50 mg/Kg 47 10-150 8 50 mg/Kg 50 10-150 7 50 mg/Kg 50 10-150 6 50 mg/Kg 90 10-150 1 50 mg/Kg 66 10-150 7 50 mg/Kg 3� 63 24-138 16 50 mg/Kg 3� 73 10-150 4 50 mg/Kg 3� 61 10-150 12 50 mg/Kg 52 10-150 19 50 mg/Kg 68 10-150 2 50 mg/Kg 70 10-150 4 50 mg/Kg 57 27-144 6 50 mg/Kg 68 10-150 4 50 mg/Kg 35 10-150 11 50 mg/Kg 39 10-150 25 50 mg/Kg 62 10-150 4 50 mg/Kg 64 24-150 12 50 mg/Kg 47 10-150 27 50 mg/Kg 55 10-150 17 50 mg/Kg 27 10-150 30 50 mg/Kg 49 10-150 6 50 mg/Kg 63 10-150 5 50 mg/Kg 60 10-150 4 50 mg/Kg 52 10-150 7 50 mg/Kg 56 10-150 8 50 mg/Kg 6 10-150 97 50 TestAmerica Nashville Page 28 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-119880-A-14-A MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA Analysis Batch: 400760 Prep Batch: 400721 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit tert-Butylbenzene ND 0.0480 0.02648 mg/Kg 55 10 -150 8 50 1,1,1,2-Tetrachloroethane ND 0.0480 0.02899 mg/Kg 60 10-150 13 50 1,1,2,2-Tetrachloroethane ND 0.0480 0.02480 mg/Kg 52 10-150 25 50 Tetrachloroethene ND 0.0480 0.03076 mg/Kg # 64 10 -150 0 50 Toluene ND 0.0480 0.03131 mg/Kg # 65 17 -150 6 50 trans-1,2-Dichloroethene ND 0.0480 0.03289 mg/Kg # 69 10-150 7 50 trans- 1,3-Dichloropropene ND 0.0480 0.02276 mg/Kg 47 10-150 21 50 1,2,3-Trichlorobenzene ND 0.0480 0.01304 mg/Kg 27 10-150 17 50 1,2,4-Trichlorobenzene ND 0.0480 0.01457 mg/Kg 30 10-150 12 50 1,1,1-Trichloroethane ND 0.0480 0.03609 mg/Kg 75 10-150 5 50 1,1,2-Trichloroethane ND 0.0480 0.02565 mg/Kg 53 10-150 15 50 Trichloroethene ND 0.0480 0.03543 mg/Kg 72 10 -150 9 50 Trichlorofluoromethane ND 0.0480 0.04038 mg/Kg 84 10 -150 3 50 1,2,3-Trichloropropane ND 0.0480 0.02589 mg/Kg 54 10 -150 27 50 1,2,4-Trimethylbenzene ND 0.0480 0.02542 mg/Kg 53 10-150 2 50 1,3,5-Trimethylbenzene ND 0.0480 0.02893 mg/Kg 60 10-150 1 50 Vinyl chloride ND 0.0480 0.03489 mg/Kg 73 10-150 11 50 Xylenes, Total ND 0.0960 0.06166 mg/Kg 64 10 -150 6 50 MSD MSD Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 102 70 - 130 Dibromofluoromethane (Surr) 97 70 - 130 1,2-Dichloroethane-d4 (Surr) 105 70- 130 Toluene-d8 (Surr) 91 70 - 130 Lab Sample ID: 490-119880-A-14-B MS Matrix: Solid Analysis Batch: 400760 Analyte Sample Sample Result Qualifier Acetone ND Benzene ND Bromobenzene ND Bromochloromethane ND Bromodichloromethane ND Bromoform ND Bromomethane ND 2-Butanone (MEK) ND Carbon disulfide ND Carbon tetrachloride ND Chlorobenzene ND Chlorodibromomethane ND Chloroethane ND Chloroform ND Chloromethane ND 2-Chlorotoluene ND 4-Chlorotoluene ND cis-1.2-Dichloroethene 0.00680 Client Sample ID: Matrix Spike Prep Type: Total/NA Prep Batch: 400721 Spike Added MS MS Result Qualifier Unit D %Rec %Rec. Limits 0.233 0.1391 mg/Kg 56 10 -150 0.0467 0.03148 mg/Kg 67 21 -150 0.0467 0.02283 mg/Kg 49 10 -150 0.0467 0.02720 mg/Kg 3� 58 10 -150 0.0467 0.02511 mg/Kg 3� 54 10 -150 0.0467 0.01637 mg/Kg 3� 35 10 -150 0.0467 0.03395 mg/Kg 73 10 -150 0.233 0.1220 mg/Kg 52 10 -150 0.0467 0.03058 mg/Kg 66 10 -150 0.0467 0.03354 mg/Kg 72 10 -150 0.0467 0.02601 mg/Kg 56 10 -150 0.0467 0.01885 mg/Kg 40 10 -150 0.0467 0.03194 mg/Kg 68 10 -150 0.0467 0.03045 mg/Kg 65 10 -150 0.0467 0.02809 mg/Kg 60 10 -150 0.0467 0.02796 mg/Kg 60 10 -150 0.0467 0.02670 mg/Kg 57 10 -150 0.0467 0.03349 mg/Kg 57 10 -150 TestAmerica Nashville Page 29 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-119880-A-14-B MS Matrix: Solid Analysis Batch: 400760 Sample Sample Spike MS MS Analyte Result Qualifier Added Result Qualifier Unit Client Sample ID: Matrix Spike Prep Type: Total/NA Prep Batch: 400721 %Rec. D %Rec Limits cis-1,3-Dichloropropene ND 0.0467 0.02136 mg/Kg 46 10-150 1,2-Dibromo-3-Chloropropane ND 0.0467 0.01430 mg/Kg 31 10-150 1,2-Dibromoethane(EDB) ND 0.0467 0.02087 mg/Kg 45 10-150 Dibromomethane ND 0.0467 0.02424 mg/Kg # 52 10 -150 1,2-Dichlorobenzene ND 0.0467 0.02078 mg/Kg # 45 10-150 1,3-Dichlorobenzene ND 0.0467 0.02264 mg/Kg # 49 10-150 1,4-Dichlorobenzene ND 0.0467 0.02249 mg/Kg 48 10-150 Dichlorodifluoromethane ND 0.0467 0.04365 mg/Kg 94 10-150 1,1-Dichloroethane ND 0.0467 0.02937 mg/Kg 63 10-150 1,2-Dichloroethane ND * 0.0467 0.02549 mg/Kg 55 24 -138 1,1-Dichloroethene ND 0.0467 0.03356 mg/Kg 72 10-150 1,2-Dichloropropane ND * 0.0467 0.02615 mg/Kg 56 10 -150 1,3-Dichloropropane ND * 0.0467 0.02052 mg/Kg 44 10 -150 2,2-Dichloropropane ND 0.0467 0.03169 mg/Kg 68 10 -150 1,1-Dichloropropene ND 0.0467 0.03227 mg/Kg 69 10-150 Diisopropyl ether ND 0.0467 0.02588 mg/Kg 55 27 -144 Ethylbenzene ND 0.0467 0.03142 mg/Kg 67 10 -150 Hexachlorobutadiene ND 0.0467 0.01858 mg/Kg 40 10-150 2-Hexanone ND 0.233 0.07310 mg/Kg 31 10 -150 Isopropylbenzene ND 0.0467 0.03082 mg/Kg 66 10 -150 Methylene Chloride ND 0.0467 0.02739 mg/Kg 59 24 -150 4-Methyl-2-pentanone (MIBK) ND 0.233 0.08523 mg/Kg 37 10-150 Methyl tert-butyl ether ND 0.0467 0.02230 mg/Kg 48 10 -150 Naphthalene ND 0.0467 0.009755 mg/Kg 21 10 -150 n-Butylbenzene ND 0.0467 0.02511 mg/Kg 54 10 -150 1,2-Dichloroethene, Total 0.00680 0.0933 0.06404 mg/Kg 61 10 -150 N-Propylbenzene ND 0.0467 0.02976 mg/Kg 64 10 -150 p-Isopropyltoluene ND 0.0467 0.02666 mg/Kg 57 10-150 sec- Butylbenzene ND 0.0467 0.02911 mg/Kg 62 10 -150 Styrene ND F1 F2 0.0467 0.007824 mg/Kg 17 10-150 tert-Butylbenzene ND 0.0467 0.02860 mg/Kg 61 10 -150 1,1,1,2-Tetrachloroethane ND 0.0467 0.02552 mg/Kg 55 10-150 1,1,2,2-Tetrachloroethane ND 0.0467 0.01922 mg/Kg 41 10-150 Tetrachloroethene ND 0.0467 0.03090 mg/Kg # 66 10 -150 Toluene ND 0.0467 0.02958 mg/Kg # 63 17 -150 trans- 1,2-Dichloroethene ND 0.0467 0.03055 mg/Kg # 65 10-150 trans- 1,3-Dichloropropene ND 0.0467 0.01843 mg/Kg 39 10-150 1,2,3-Trichlorobenzene ND 0.0467 0.01100 mg/Kg 24 10-150 1,2,4-Trichlorobenzene ND 0.0467 0.01293 mg/Kg 28 10 -150 1,1,1-Trichloroethane ND 0.0467 0.03420 mg/Kg 73 10-150 1,1,2-Trichloroethane ND 0.0467 0.02197 mg/Kg 47 10-150 Trichloroethene ND 0.0467 0.03238 mg/Kg 67 10 -150 Trichlorofluoromethane ND 0.0467 0.03909 mg/Kg # 84 10 -150 1,2,3-Trichloropropane ND 0.0467 0.01983 mg/Kg 0 42 10-150 1,2,4-Trimethylbenzene ND 0.0467 0.02496 mg/Kg 0 53 10-150 1,3,5-Trimethylbenzene ND 0.0467 0.02918 mg/Kg 63 10-150 Vinyl chloride ND 0.0467 0.03118 mg/Kg 67 10-150 Xylenes, Total ND 0.0933 0.05822 mg/Kg 62 10 -150 TestAmerica Nashville Page 30 of 56 1/18/2017 QC Sample Results C Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-119880-A-14-B MS Matrix: Solid Analysis Batch: 400760 MS MS Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 102 70 - 130 Dibromofluoromethane (Surr) 97 70 - 130 1,2-Dichloroethane-d4 (Surr) 98 70- 130 Toluene-d8 (Surr) 92 70 - 130 Lab Sample ID: MB 490-400760/8 Matrix: Solid Analysis Batch: 400760 Client Sample ID: Matrix Spike Prep Type: Total/NA Prep Batch: 400721 0 F Client Sample ID: Method Blank Prep Type: Total/NA Analyte MB MB Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 0.0500 mg/Kg 01/13/17 04:12 1 Benzene ND 0.00200 mg/Kg 01/13/17 04:12 1 Bromobenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 Bromochloromethane ND 0.00200 mg/Kg 01/13/17 04:12 1 Bromodichloromethane ND 0.00200 mg/Kg 01/13/17 04:12 1 Bromoform ND 0.00200 mg/Kg 01/13/17 04:12 1 Bromomethane ND 0.00200 mg/Kg 01/13/17 04:12 1 2-Butanone (MEK) ND 0.0500 mg/Kg 01/13/17 04:12 1 Carbon disulfide ND 0.00500 mg/Kg 01/13/17 04:12 1 Carbon tetrachloride ND 0.00200 mg/Kg 01/13/17 04:12 1 Chlorobenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 Chlorodibromomethane ND 0.00200 mg/Kg 01/13/17 04:12 1 Chloroethane ND 0.00500 mg/Kg 01/13/17 04:12 1 Chloroform ND 0.00200 mg/Kg 01/13/17 04:12 1 Chloromethane ND 0.00200 mg/Kg 01/13/17 04:12 1 2-Chlorotoluene ND 0.00200 mg/Kg 01/13/17 04:12 1 4-Chlorotoluene ND 0.00200 mg/Kg 01/13/17 04:12 1 cis-1,2-Dichloroethene ND 0.00200 mg/Kg 01/13/17 04:12 1 cis-1,3-Dichloropropene ND 0.00200 mg/Kg 01/13/17 04:12 1 1,2-Dibromo-3-Chloropropane ND 0.00500 mg/Kg 01/13/17 04:12 1 1,2-Dibromoethane (EDB) ND 0.00200 mg/Kg 01/13/17 04:12 1 Dibromomethane ND 0.00200 mg/Kg 01/13/17 04:12 1 1,2-Dichlorobenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 1,3-Dichlorobenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 1,4-Dichlorobenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 Dichlorodifluoromethane ND 0.00200 mg/Kg 01/13/17 04:12 1 1,1-Dichloroethane ND 0.00200 mg/Kg 01/13/17 04:12 1 1,2-Dichloroethane ND 0.00200 mg/Kg 01/13/17 04:12 1 1,1-Dichloroethene ND 0.00200 mg/Kg 01/13/17 04:12 1 1,2-Dichloropropane ND 0.00200 mg/Kg 01/13/17 04:12 1 1,3-Dichloropropane ND 0.00200 mg/Kg 01/13/17 04:12 1 2,2-Dichloropropane ND 0.00200 mg/Kg 01/13/17 04:12 1 1,1-Dichloropropene ND 0.00200 mg/Kg 01/13/17 04:12 1 Diisopropyl ether ND 0.00200 mg/Kg 01/13/17 04:12 1 Ethylbenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 Hexachlorobutadiene ND 0.00500 mg/Kg 01/13/17 04:12 1 2-Hexanone ND 0.0500 mg/Kg 01/13/17 04:12 1 Isopropylbenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 TestAmerica Nashville Page 31 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 490-400760/8 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 400760 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Methylene Chloride ND 0.0100 mg/Kg 01/13/17 04:12 1 4-Methyl-2-pentanone (MIBK) ND 0.0500 mg/Kg 01/13/17 04:12 1 Methyl tert-butyl ether ND 0.00200 mg/Kg 01/13/17 04:12 1 Naphthalene ND 0.00500 mg/Kg 01/13/17 04:12 1 n-Butylbenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 1,2-Dichloroethene, Total ND 0.00200 mg/Kg 01/13/17 04:12 1 N-Propylbenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 p-Isopropyltoluene ND 0.00200 mg/Kg 01/13/17 04:12 1 sec-Butylbenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 Styrene ND 0.00200 mg/Kg 01/13/17 04:12 1 tert-Butylbenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 1,1,1,2-Tetrachloroethane ND 0.00200 mg/Kg 01/13/17 04:12 1 1,1,2,2-Tetrachloroethane ND 0.00200 mg/Kg 01/13/17 04:12 1 Tetrachloroethene ND 0.00200 mg/Kg 01/13/17 04:12 1 Toluene ND 0.00200 mg/Kg 01/13/17 04:12 1 trans- 1,2-Dichloroethene ND 0.00200 mg/Kg 01/13/17 04:12 1 trans- 1,3-Dichloropropene ND 0.00200 mg/Kg 01/13/17 04:12 1 1,2,3-Trichlorobenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 1,2,4-Trichlorobenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 1,1,1-Trichloroethane ND 0.00200 mg/Kg 01/13/17 04:12 1 1,1,2-Trichloroethane ND 0.00500 mg/Kg 01/13/17 04:12 1 Trichloroethene ND 0.00200 mg/Kg 01/13/17 04:12 1 Trichlorofluoromethane ND 0.00200 mg/Kg 01/13/17 04:12 1 1,2,3-Trichloropropane ND 0.00200 mg/Kg 01/13/17 04:12 1 1,2,4-Trimethylbenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 1,3,5-Trimethylbenzene ND 0.00200 mg/Kg 01/13/17 04:12 1 Vinyl chloride ND 0.00200 mg/Kg 01/13/17 04:12 1 Xylenes, Total ND 0.00600 mg/Kg 01/13/17 04:12 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 106 70 - 130 01113117 04:12 1 Dibromofluoromethane (Surr) 119 70 - 130 01113117 04:12 1 1,2-Dichloroethene-d4 (Surr) 120 70- 130 01113117 04:12 1 Toluene-d8 (Surr) 90 70 - 130 01113117 04:12 1 Lab Sample ID: LCS 490-400760/25 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 400760 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Acetone 0.250 0.2099 mg/Kg 84 45 -145 Benzene 0.0500 0.04081 mg/Kg 82 70 -130 Bromobenzene 0.0500 0.04341 mg/Kg 87 67 -130 Bromochloromethane 0.0500 0.04336 mg/Kg 87 70 -133 Bromodichloromethane 0.0500 0.03934 mg/Kg 79 70 -130 Bromoform 0.0500 0.03843 mg/Kg 77 59 -137 Bromomethane 0.0500 0.03071 mg/Kg 61 32 -150 2-Butanone (MEK) 0.250 0.2142 mg/Kg 86 50 -149 TestAmerica Nashville Page 32 of 56 1/18/2017 QC Sample Results C Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 490-400760/25 Matrix: Solid Analysis Batch: 400760 Client Sample ID: Lab Control Sample Prep Type: Total/NA Analyte Spike Added LCS LCS Result Qualifier Unit D %Rec %Rec. Limits Carbon disulfide 0.0500 0.03489 mg/Kg 70 66 -138 Carbon tetrachloride 0.0500 0.03834 mg/Kg 77 70 -131 Chlorobenzene 0.0500 0.04047 mg/Kg 81 70 -130 Chlorodibromomethane 0.0500 0.03516 mg/Kg 70 70 -130 Chloroethane 0.0500 0.03819 mg/Kg 76 37 -150 Chloroform 0.0500 0.04092 mg/Kg 82 70 -130 Chloromethane 0.0500 0.03310 mg/Kg 66 53 -150 2-Chlorotoluene 0.0500 0.04460 mg/Kg 89 70 -132 4-Chlorotoluene 0.0500 0.04665 mg/Kg 93 67 -135 cis-1,2-Dichloroethene 0.0500 0.04238 mg/Kg 85 70 -132 cis-1,3-Dichloropropene 0.0500 0.03769 mg/Kg 75 70 -130 1,2-Dibromo-3-Chloropropane 0.0500 0.04044 mg/Kg 81 47-144 1,2-Dibromoethane(EDB) 0.0500 0.04234 mg/Kg 85 69-130 Dibromomethane 0.0500 0.04246 mg/Kg 85 70 -130 1,2-Dichlorobenzene 0.0500 0.04741 mg/Kg 95 70 -134 1,3-Dichlorobenzene 0.0500 0.04730 mg/Kg 95 69 -137 1,4-Dichlorobenzene 0.0500 0.04862 mg/Kg 97 66 -134 Dichlorodifluoromethane 0.0500 0.04774 mg/Kg 95 32 -150 1,1-Dichloroethane 0.0500 0.03567 mg/Kg 71 70-130 1,2-Dichloroethane 0.0500 0.04206 mg/Kg 84 65 -134 1,1-Dichloroethene 0.0500 0.03768 mg/Kg 75 70-131 1,2-Dichloropropane 0.0500 0.03704 mg/Kg 74 70 -130 1,3-Dichloropropane 0.0500 0.03898 mg/Kg 78 70 -130 2,2-Dichloropropane 0.0500 0.03768 mg/Kg 75 57 -150 1,1-Dichloropropene 0.0500 0.03767 mg/Kg 75 70-130 Diisopropyl ether 0.0500 0.03671 mg/Kg 73 68 -134 Ethylbenzene 0.0500 0.04346 mg/Kg 87 70 -130 Hexachlorobutadiene 0.0500 0.04748 mg/Kg 95 64 -137 2-Hexanone 0.250 0.2001 mg/Kg 80 47 -148 Isopropylbenzene 0.0500 0.04222 mg/Kg 84 70 -130 Methylene Chloride 0.0500 0.04124 mg/Kg 82 69 -130 4-Methyl-2-pentanone (MIBK) 0.250 0.1990 mg/Kg 80 48-150 Methyl tert-butyl ether 0.0500 0.04101 mg/Kg 82 54 -145 Naphthalene 0.0500 0.05033 mg/Kg 101 55 -149 n-Butylbenzene 0.0500 0.04778 mg/Kg 96 57 -150 1,2-Dichloroethene, Total 0.100 0.07858 mg/Kg 79 70 -130 N-Propylbenzene 0.0500 0.04442 mg/Kg 89 62 -150 p-Isopropyltoluene 0.0500 0.04382 mg/Kg 88 66 -147 sec-Butylbenzene 0.0500 0.04453 mg/Kg 89 68 -147 Styrene 0.0500 0.04171 mg/Kg 83 70 -131 tert-Butylbenzene 0.0500 0.04158 mg/Kg 83 70 -138 1,1,1,2-Tetrachloroethane 0.0500 0.04170 mg/Kg 83 70-130 1,1,2,2-Tetrachloroethane 0.0500 0.04593 mg/Kg 92 61-134 Tetrachloroethene 0.0500 0.04096 mg/Kg 82 70 -130 Toluene 0.0500 0.03993 mg/Kg 80 70 -130 trans- 1,2-Dichloroethene 0.0500 0.03620 mg/Kg 72 70-130 trans- 1,3-Dichloropropene 0.0500 0.03615 mg/Kg 72 67-130 1,2,3-Trichlorobenzene 0.0500 0.05576 mg/Kg 112 57-146 TestAmerica Nashville Page 33 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 490-400760/25 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 400760 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 1,2,4-Trichlorobenzene 0.0500 0.05822 mg/Kg 116 47-150 1,1,1-Trichloroethane 0.0500 0.03929 mg/Kg 79 70-130 1,1,2-Trichloroethane 0.0500 0.04113 mg/Kg 82 70-130 Trichloroethene 0.0500 0.04072 mg/Kg 81 70 -130 Trichlorofluoromethane 0.0500 0.04302 mg/Kg 86 53 -150 1,2,3-Trichloropropane 0.0500 0.04678 mg/Kg 94 60-139 1,2,4-Trimethylbenzene 0.0500 0.04276 mg/Kg 86 70 -140 1,3,5-Trimethylbenzene 0.0500 0.04474 mg/Kg 89 69-141 Vinyl chloride 0.0500 0.03716 mg/Kg 74 63 -150 Xylenes, Total 0.100 0.08381 mg/Kg 84 70 -130 LCS LCS Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 103 70 - 130 Dibromofluoromethane (Surr) 96 70 - 130 1,2-Dichloroethane-d4 (Surr) 98 70- 130 Toluene-d8 (Surr) 93 70 - 130 Lab Sample ID: LCSD 490-400760126 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 400760 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Acetone 0.250 0.2412 mg/Kg 96 45 -145 14 38 Benzene 0.0500 0.05127 mg/Kg 103 70-130 23 37 Bromobenzene 0.0500 0.05127 mg/Kg 103 67 -130 17 40 Bromochloromethane 0.0500 0.05497 * mg/Kg 110 70 -133 24 15 Bromodichloromethane 0.0500 0.04953 * mg/Kg 99 70 -130 23 20 Bromoform 0.0500 0.04515 mg/Kg 90 59 -137 16 17 Bromomethane 0.0500 0.04063 mg/Kg 81 32 -150 28 45 2-Butanone (MEK) 0.250 0.2612 mg/Kg 104 50 -149 20 39 Carbon disulfide 0.0500 0.04700 mg/Kg 94 66 -138 30 41 Carbon tetrachloride 0.0500 0.05124 mg/Kg 102 70 -131 29 41 Chlorobenzene 0.0500 0.04828 mg/Kg 97 70 -130 18 40 Chlorodibromomethane 0.0500 0.04114 * mg/Kg 82 70 -130 16 14 Chloroethane 0.0500 0.05467 mg/Kg 109 37 -150 36 50 Chloroform 0.0500 0.05302 * mg/Kg 106 70 -130 26 15 Chloromethane 0.0500 0.04083 mg/Kg 82 53 -150 21 47 2-Chlorotoluene 0.0500 0.05429 mg/Kg 109 70 -132 20 41 4-Chlorotoluene 0.0500 0.05681 mg/Kg 114 67 -135 20 41 cis-1,2-Dichloroethene 0.0500 0.05140 * mg/Kg 103 70 -132 19 18 cis-1,3-Dichloropropene 0.0500 0.04498 mg/Kg 90 70 -130 18 42 1,2-Dibromo-3-Chloropropane 0.0500 0.04707 mg/Kg 94 47-144 15 38 1,2-Dibromoethane(EDB) 0.0500 0.04943 mg/Kg 99 69-130 15 17 Dibromomethane 0.0500 0.05504 * mg/Kg 110 70 -130 26 19 1,2-Dichlorobenzene 0.0500 0.05584 mg/Kg 112 70 -134 16 40 1,3-Dichlorobenzene 0.0500 0.05572 mg/Kg 111 69 -137 16 41 1,4-Dichlorobenzene 0.0500 0.05469 mg/Kg 109 66 -134 12 41 Dichlorodifluoromethane 0.0500 0.06386 mg/Kg 128 32 -150 29 50 TestAmerica Nashville Page 34 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 490-400760/26 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 400760 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit 1,1-Dichloroethane 0.0500 0.04768 mg/Kg 95 70-130 29 42 1,2-Dichloroethane 0.0500 0.05386 " mg/Kg 108 65 -134 25 16 1,1-Dichloroethene 0.0500 0.05121 mg/Kg 102 70-131 30 43 1,2-Dichloropropane 0.0500 0.04789 " mg/Kg 96 70 -130 26 15 1,3-Dichloropropane 0.0500 0.04619 ' mg/Kg 92 70 -130 17 15 2,2-Dichloropropane 0.0500 0.05049 mg/Kg 101 57 -150 29 42 1,1-Dichloropropene 0.0500 0.04888 mg/Kg 98 70-130 26 41 Diisopropyl ether 0.0500 0.04496 mg/Kg 90 68 -134 20 36 Ethylbenzene 0.0500 0.05234 mg/Kg 105 70 -130 19 38 Hexachlorobutadiene 0.0500 0.05545 mg/Kg 111 64 -137 15 44 2-Hexanone 0.250 0.2365 mg/Kg 95 47 -148 17 38 Isopropylbenzene 0.0500 0.05438 mg/Kg 109 70 -130 25 39 Methylene Chloride 0.0500 0.05375 mg/Kg 108 69 -130 26 19 4-Methyl-2-pentanone (MIBK) 0.250 0.2379 mg/Kg 95 48-150 18 41 Methyl tert-butyl ether 0.0500 0.05078 mg/Kg 102 54 -145 21 36 Naphthalene 0.0500 0.05592 mg/Kg 112 55 -149 11 37 n-Butylbenzene 0.0500 0.05566 mg/Kg 111 57 -150 15 39 1,2-Dichloroethene, Total 0.100 0.1002 mg/Kg 100 70 -130 24 41 N-Propylbenzene 0.0500 0.05499 mg/Kg 110 62-150 21 38 p-Isopropyltoluene 0.0500 0.05204 mg/Kg 104 66 -147 17 38 sec-Butylbenzene 0.0500 0.05381 mg/Kg 108 68 -147 19 38 Styrene 0.0500 0.05279 mg/Kg 106 70 -131 23 40 tert-Butylbenzene 0.0500 0.05178 mg/Kg 104 70 -138 22 38 1,1,1,2-Tetrachloroethane 0.0500 0.04686 mg/Kg 94 70-130 12 41 1,1,2,2-Tetrachloroethane 0.0500 0.04926 mg/Kg 99 61-134 7 16 Tetrachloroethene 0.0500 0.04797 mg/Kg 96 70 -130 16 41 Toluene 0.0500 0.05005 mg/Kg 100 70 -130 22 40 trans- 1,2-Dichloroethene 0.0500 0.04884 mg/Kg 98 70-130 30 41 trans- 1,3-Dichloropropene 0.0500 0.04293 mg/Kg 86 67-130 17 41 1,2,3-Trichlorobenzene 0.0500 0.06156 mg/Kg 123 57-146 10 42 1,2,4-Trichlorobenzene 0.0500 0.06489 mg/Kg 130 47-150 11 43 1,1,1-Trichloroethane 0.0500 0.05190 mg/Kg 104 70-130 28 41 1,1,2-Trichloroethane 0.0500 0.04756 mg/Kg 95 70-130 15 17 Trichloroethene 0.0500 0.05179 mg/Kg 104 70 -130 24 41 Trichlorofluoromethane 0.0500 0.05819 mg/Kg 116 53 -150 30 49 1,2,3-Trichloropropane 0.0500 0.05354 mg/Kg 107 60-139 13 16 1,2,4-Trimethylbenzene 0.0500 0.05174 mg/Kg 103 70 -140 19 38 1,3,5-Trimethylbenzene 0.0500 0.05493 mg/Kg 110 69-141 20 38 Vinyl chloride 0.0500 0.05093 mg/Kg 102 63 -150 31 46 Xylenes, Total 0.100 0.1041 mg/Kg 104 70 -130 22 38 LCSD LCSD Surrogate %Recovery Qualifier Limits 4-Bromofluorobenzene (Surr) 104 70 - 130 Dibromofluoromethane (Surr) 103 70 - 130 1,2-Dichloroethane-d4 (Surr) 106 70- 130 Toluene-d8 (Surr) 96 70 - 130 TestAmerica Nashville Page 35 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Method: 6010D - Metals (ICP) Lab Sample ID: MB 490-400683/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 400979 Prep Batch: 400683 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Arsenic ND 1.97 mg/Kg 01/12/1713:02 01/12/1719:06 1 Barium ND 1.97 mg/Kg 01/12/1713:02 01/12/1719:06 1 Cadmium ND 0.986 mg/Kg 01/12/1713:02 01/12/1719:06 1 Chromium ND 0.986 mg/Kg 01/12/1713:02 01/12/1719:06 1 Lead ND 0.986 mg/Kg 01/12/1713:02 01/12/1719:06 1 Selenium ND 1.97 mg/Kg 01/12/1713:02 01/12/1719:06 1 Lab Sample ID: LCS 490-400683/2-A Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 400979 Prep Batch: 400683 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Arsenic 20.0 19.08 mg/Kg 96 80 -120 Barium 20.0 19.76 mg/Kg 99 80-120 Cadmium 20.0 19.64 mg/Kg 98 80 -120 Chromium 20.0 19.16 mg/Kg 96 80 -120 Lead 20.0 19.94 mg/Kg 100 80 -120 Selenium 20.0 18.88 mg/Kg 95 80 -120 Lab Sample ID: LCSD 490-400683/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 400979 Prep Batch: 400683 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Arsenic 20.0 17.76 mg/Kg 89 80 -120 7 20 Barium 20.0 19.12 mg/Kg 96 80-120 3 20 Cadmium 20.0 19.02 mg/Kg 95 80 -120 3 20 Chromium 20.0 17.88 mg/Kg 89 80 -120 7 20 Lead 20.0 19.44 mg/Kg 97 80 -120 3 20 Selenium 20.0 18.34 mg/Kg 92 80 -120 3 20 Lab Sample ID: 550-74906-A-1-H MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA Analysis Batch: 400979 Prep Batch: 400683 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Arsenic 12.4 19.3 28.38 mg/Kg 83 75 -125 Barium 132 19.3 137.5 4 mg/Kg 30 75-125 Cadmium ND 19.3 17.21 mg/Kg 88 75-125 Chromium 113 19.3 124.8 4 mg/Kg 61 75 -125 Lead 13.3 19.3 31.04 mg/Kg 92 75 -125 Selenium ND 19.3 16.94 mg/Kg 78 75-125 Lab Sample ID: 550-74906-A-1-1 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA Analysis Batch: 400979 Prep Batch: 400683 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Arsenic 12.4 19.6 31.55 mg/Kg 98 75 -125 11 20 TestAmerica Nashville Page 36 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Method: 6010D - Metals (ICP) (Continued) Lab Sample ID: 550-74906-A-1-1 MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA Analysis Batch: 400979 Prep Batch: 400683 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Barium 132 19.6 155.7 4 mg/Kg 122 75-125 12 20 Cadmium ND 19.6 18.04 mg/Kg 91 75-125 5 20 Chromium 113 19.6 141.0 4 mg/Kg 143 75 -125 12 20 Lead 13.3 19.6 33.55 mg/Kg 103 75 -125 8 20 Selenium ND 19.6 17.65 mg/Kg 81 75-125 4 20 Lab Sample ID: MB 490-401267/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 401552 Prep Batch: 401267 MB MB Analyte Result Qualifier Silver ND Lab Sample ID: LCS 490-401267/2-A Matrix: Solid Analysis Batch: 401552 Analyte Silver Spike Added 20.2 RL MDL Unit D Prepared Analyzed Dil Fac 0.984 mg/Kg 01/16/1710:06 01/16/1713:42 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 401267 LCS LCS %Rec. Result Qualifier Unit D %Rec Limits 18.99 mg/Kg 94 80 -120 Lab Sample ID: LCSD 490-401267/3-A Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 401552 Prep Batch: 401267 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Silver 20.0 18.54 mg/Kg 93 80 -120 2 20 Lab Sample ID: 550-74906-A-1-K MS Client Sample ID: Matrix Spike Matrix: Solid Prep Type: Total/NA Analysis Batch: 401552 Prep Batch: 401267 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Silver ND 19.1 16.35 mg/Kg 86 75-125 Lab Sample ID: 550-74906-A-1-L MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA Analysis Batch: 401552 Prep Batch: 401267 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Silver ND 19.5 16.90 mg/Kg 87 75-125 3 20 Lab Sample ID: MB 490-401367/1-B Client Sample ID: Method Blank Matrix: Water Prep Type: Dissolved Analysis Batch: 401731 Prep Batch: 401455 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Silver ND 0.00500 mg/L 01/17/17 07:58 01/17/17 14:02 1 Arsenic ND 0.0100 mg/L 01/17/17 07:58 01/17/17 14:02 1 Barium ND 0.0100 mg/L 01/17/17 07:58 01/17/17 14:02 1 Cadmium ND 0.00100 mg/L 01/17/17 07:58 01/17/17 14:02 1 Page 37 of 56 TestAmerica Nashville 1/18/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Method: 6010D - Metals (ICP) (Continued) Lab Sample ID: MB 490-401367/1-B Matrix: Water Analysis Batch: 401731 MB MB Analyte Result Qualifier Chromium ND Lead ND Selenium ND Lab Sample ID: LCS 490-401367/2-B Matrix: Water Analysis Batch: 401731 Analyte Silver Arsenic Barium Cadmium Chromium Lead Selenium Lab Sample ID: 490-120048-D-2-E MS Matrix: Water Analysis Batch: 401731 Sample Sample Analyte Result Qualifier Silver ND Arsenic ND Barium 0.0335 Cadmium ND Chromium ND Lead ND Selenium ND TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC RL MDL Unit Client Sample ID: Method Blank Prep Type: Dissolved Prep Batch: 401455 D Prepared Analyzed Dil Fac 0.00500 mg/L 01/17/17 07:58 01/17/17 14:02 1 0.00500 mg/L 01/17/17 07:58 01/17/17 14:02 1 0.0100 mg/L 01/17/17 07:58 01/17/17 14:02 1 Client Sample ID: Lab Control Sample Prep Type: Dissolved Prep Batch: 401455 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 0.100 0.09320 mg/L 93 80 -120 0.100 0.09640 mg/L 96 80 -120 0.100 0.09980 mg/L 100 80 -120 0.100 0.09730 mg/L 97 80 -120 0.100 0.1010 mg/L 101 80 -120 0.100 0.1018 mg/L 102 80 -120 0.100 0.1014 mg/L 101 80 -120 Spike MS MS Added Result Qualifier 0.100 0.09500 0.100 0.09920 0.100 0.1328 0.100 0.09690 0.100 0.1027 0.100 0.1013 0.100 0.1033 Client Sample ID: Matrix Spike Prep Type: Dissolved Prep Batch: 401455 %Rec. Unit D %Rec Limits mg/L 95 75 -125 mg/L 99 75 -125 mg/L 99 75 -125 mg/L 97 75 -125 mg/L 103 75 -125 mg/L 101 75 -125 mg/L 103 75 -125 Lab Sample ID: 490-120048-D-2-F MSD Client Sample ID: Matrix Spike Duplicate Matrix: Water Prep Type: Dissolved Analysis Batch: 401731 Prep Batch: 401455 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Silver ND 0.100 0.09630 mg/L 96 75-125 1 20 Arsenic ND 0.100 0.09990 mg/L 100 75 -125 1 20 Barium 0.0335 0.100 0.1358 mg/L 102 75-125 2 20 Cadmium ND 0.100 0.09880 mg/L 99 75-125 2 20 Chromium ND 0.100 0.1030 mg/L 103 75-125 0 20 Lead ND 0.100 0.1043 mg/L 104 75 -125 3 20 Selenium ND 0.100 0.1058 mg/L 106 75-125 2 20 Page 38 of 56 TestAmerica Nashville 1/18/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Method: 7470A - Mercury (CVAA) Lab Sample ID: MB 490-401454/1-B Matrix: Water Analysis Batch: 401664 MB MB Analyte Result Qualifier RL Mercury ND 0.000200 Lab Sample ID: LCS 490-401454/2-B Matrix: Water Analysis Batch: 401664 [Analyte Mercury Lab Sample ID: 490-119827-7 MS Matrix: Water Analysis Batch: 401664 Sample Sample Analyte Result Qualifier Mercury ND FLab Sample ID: 490-119827-7 MSD Matrix: Water Analysis Batch: 401664 Analyte Mercury Sample Sample Result Qualifier ND Method: 7471 B - Mercury (CVAA) Lab Sample ID: MB 490-400874/1-A Matrix: Solid Analysis Batch: 401676 MB MB Analyte Result Qualifier Mercury ND Lab Sample ID: LCS 490-400874/2-A Matrix: Solid Analysis Batch: 401676 Analyte Mercury Lab Sample ID: LCSD 490-400874/3-A Matrix: Solid Analysis Batch: 401676 Analyte Mercury TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Client Sample ID: Method Blank Prep Type: Dissolved Prep Batch: 401460 MDL Unit D Prepared Analyzed Dil Fac mg/L 01/17/17 08:12 01/17/17 13:49 1 Spike LCS LCS Added Result Qualifier 0.00100 0.001195 Client Sample ID: Lab Control Sample Prep Type: Dissolved Prep Batch: 401460 %Rec. — Unit D %Rec Limits mg/L 120 80 -120 Client Sample ID: TMW-1 Prep Type: Dissolved Prep Batch: 401460 Spike MS MS %Rec. Added Result Qualifier Unit D %Rec Limits 0.00100 0.0008610 mg/L 86 75 - 125 Client Sample ID: TMW-1 Prep Type: Dissolved Prep Batch: 401460 Spike MSD MSD %Rec. RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 0.00100 0.0009285 mg/L 93 75 -125 8 20 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 400874 RL MDL Unit D Prepared Analyzed Dil Fac 0.0988 mg/Kg 01/13/17 09:48 01/16/17 15:47 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 400874 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 0.164 0.1754 mg/Kg 107 80 -120 Spike LCSD LCSD Added Result Qualifier 0.166 0.1655 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Prep Batch: 400874 %Rec. RPD Unit D %Rec Limits RPD Limit mg/Kg 100 80-120 6 20 TestAmerica Nashville Page 39 of 56 1/18/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Method: 7471 B - Mercury (CVAA) (Continued) TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Lab Sample ID: 490-119827-1 MS Client Sample ID: SBA (1') Matrix: Solid Prep Type: Total/NA Analysis Batch: 401676 Prep Batch: 400874 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Mercury ND 0.179 0.2050 mg/Kg 114 80-120 Lab Sample ID: 490-119827-1 MSD Client Sample ID: SBA (1) Matrix: Solid Prep Type: Total/NA Analysis Batch: 401676 Prep Batch: 400874 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Mercury ND 0.182 0.1914 mg/Kg 105 80-120 7 20 Method: Moisture - Percent Moisture Lab Sample ID: 460-126646-A-1 DU Matrix: Solid Analysis Batch: 400681 Sample Sample Analyte Result Qualifier Percent Solids 52.7 DU DU Result Qualifier Unit D 50.3 % Client Sample ID: Duplicate Prep Type: Total/NA RPD RPD Limit 5 20 Page 40 of 56 TestAmerica Nashville 1 /18/2017 QC Association Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, GC/MS VOA Analysis Batch: 400532 Lab Sample ID 490-119827-7 MB 490-400532/7 LCS 490-400532/3 LCSD 490-400532/4 490-119778-A-2 MS 490-119778-A-2 MSD Prep Batch: 400685 Lab Sample ID 490-119827-1 490-119827-2 490-119827-3 490-119827-4 490-119827-5 490-119827-6 Prep Batch: 400721 Client Sample ID Method Blank Lab Control Sample Lab Control Sample Dup Matrix Spike Matrix Spike Duplicate Client Sample ID SB-1 (1') SB-2 (1') SB-3 (1') SB-4 (1') SB-5 (1') SB-6 (1') Lab Sample ID Client Sample ID 490-119880-A-14-A MSD Matrix Spike Duplicate 490-119880-A-14-B MS Matrix Spike Analysis Batch: 400760 Lab Sample ID Client Sample ID 490-119827-1 SB-1 (1') 490-119827-2 SB-2 (1') 490-119827-3 SB-3 (1') 490-119827-4 SB-4 (1') 490-119827-5 SB-5 (1') 490-119827-6 SB-6 (1') MB 490-400760/8 Method Blank LCS 490-400760/25 Lab Control Sample LCSD 490-400760/26 Lab Control Sample Dup 490-119880-A-14-A MSD Matrix Spike Duplicate 490-119880-A-14-B MS Matrix Spike TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Prep Type Matrix Method Prep Batch Total/NA Water 8260B Total/NA Water 8260B Total/NA Water 8260B Total/NA Water 8260B Total/NA Water 8260B Total/NA Water 8260B i Prep Type Matrix Method Prep Batch Total/NA Solid 5035 Total/NA Solid 5035 Total/NA Solid 5035 Total/NA Solid 5035 Total/NA Solid 5035 Total/NA Solid 5035 Prep Type Matrix Method Prep Batch Total/NA Solid 5035 Total/NA Solid 5035 Prep Type Matrix Method Prep Batch Total/NA Solid 8260B 400685 Total/NA Solid 8260B 400685 Total/NA Solid 8260B 400685 Total/NA Solid 8260B 400685 Total/NA Solid 8260B 400685 Total/NA Solid 8260B 400685 Total/NA Solid 8260B Total/NA Solid 8260B Total/NA Solid 8260B Total/NA Solid 8260B 400721 Total/NA Solid 8260B 400721 Metals Prep Batch: 400683 Lab Sample ID Client Sample ID Prep Type Matrix Method 490-119827-1 SB-1 (1') Total/NA Solid 3051A 490-119827-2 SB-2 (1') Total/NA Solid 3051A 490-119827-3 SB-3 (1') Total/NA Solid 3051A 490-119827-4 SB-4 (1') Total/NA Solid 3051A 490-119827-5 SB-5 (1') Total/NA Solid 3051A 490-119827-6 SB-6 (1') Total/NA Solid 3051A MB 490-400683/1-A Method Blank Total/NA Solid 3051A LCS 490-400683/2-A Lab Control Sample Total/NA Solid 3051A LCSD 490-400683/3-A Lab Control Sample Dup Total/NA Solid 3051A 550-74906-A-1-H MS Matrix Spike Total/NA Solid 3051A 550-74906-A-1-1 MSD Matrix Spike Duplicate Total/NA Solid 3051A Prep Batch TestAmerica Nashville Page 41 of 56 1/18/2017 QC Association Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Metals (Continued) Prep Batch: 400874 Lab Sample ID 490-119827-1 490-119827-2 490-119827-3 490-119827-4 490-119827-5 490-119827-6 MB 490-400874/1-A LCS 490-400874/2-A LCSD 490-400874/3-A 490-119827-1 MS 490-119827-1 MSD Analysis Batch: 400979 Lab Sample ID 490-119827-1 490-119827-2 490-119827-3 490-119827-4 490-119827-5 490-119827-6 MB 490-400683/1-A LCS 490-400683/2-A LCSD 490-400683/3-A 550-74906-A-1-H MS 550-74906-A-1-1 MSD Prep Batch: 401267 Lab Sample ID 490-119827-1 490-119827-2 490-119827-3 490-119827-4 490-119827-5 490-119827-6 MB 490-401267/1-A LCS 490-401267/2-A LCSD 490-401267/3-A 550-74906-A-1-K MS 550-74906-A-1-L MSD Filtration Batch: 401367 Lab Sample ID 490-119827-7 MB 490-401367/1-B LCS 490-401367/2-B 490-120048-D-2-E MS 490-120048-D-2-F MSD TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Client Sample ID Prep Type Matrix Method Prep Batch SB-1 (1') Total/NA Solid 7471B SB-2 (1') Total/NA Solid 7471B SB-3 (1') Total/NA Solid 7471B SB-4 (1') Total/NA Solid 7471B SB-5 (1') Total/NA Solid 7471B SB-6 (1') Total/NA Solid 7471B Method Blank Total/NA Solid 7471 B Lab Control Sample Total/NA Solid 7471 B Lab Control Sample Dup Total/NA Solid 7471 B SB-1 (1') Total/NA Solid 7471B SB-1 (1') Total/NA Solid 7471B Client Sample ID Prep Type Matrix Method Prep Batch SB-1 (1') Total/NA Solid 6010D 400683 SB-2 (1') Total/NA Solid 6010D 400683 SB-3 (1') Total/NA Solid 6010D 400683 SB-4 (1') Total/NA Solid 6010D 400683 SB-5 (1') Total/NA Solid 6010D 400683 SB-6 (1') Total/NA Solid 6010D 400683 Method Blank Total/NA Solid 6010D 400683 Lab Control Sample Total/NA Solid 6010D 400683 Lab Control Sample Dup Total/NA Solid 6010D 400683 Matrix Spike Total/NA Solid 6010D 400683 Matrix Spike Duplicate Total/NA Solid 6010D 400683 Client Sample ID Prep Type Matrix Method Prep Batch SB-1 (1') Total/NA Solid 3051A SB-2 (1') Total/NA Solid 3051A SB-3 (1') Total/NA Solid 3051A SB-4 (1') Total/NA Solid 3051A SB-5 (1') Total/NA Solid 3051A SB-6 (1') Total/NA Solid 3051A Method Blank Total/NA Solid 3051A Lab Control Sample Total/NA Solid 3051A Lab Control Sample Dup Total/NA Solid 3051A Matrix Spike Total/NA Solid 3051A Matrix Spike Duplicate Total/NA Solid 3051A Client Sample ID Method Blank Lab Control Sample Matrix Spike Matrix Spike Duplicate Filtration Batch: 401454 Lab Sample ID Client Sample ID 490-119827-7 TMW-1 Prep Type Matrix Method Prep Batch Dissolved Water Filtration Dissolved Water Filtration Dissolved Water Filtration Dissolved Water Filtration Dissolved Water Filtration Prep Type Matrix Method Prep Batch Dissolved Water Filtration TestAmerica Nashville Page 42 of 56 1/18/2017 QC Association Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Metals (Continued) Filtration Batch: 401454 (Continued) TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch MB 490-401454/1-B Method Blank Dissolved Water Filtration LCS 490-401454/2-B Lab Control Sample Dissolved Water Filtration 490-119827-7 MS TMW-1 Dissolved Water Filtration 490-119827-7 MSD TMW-1 Dissolved Water Filtration Prep Batch: 401455 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 490-119827-7 TMW-1 Dissolved Water 3005A 401367 ' MB 490-401367/1-B Method Blank Dissolved Water 3005A 401367 LCS 490-401367/2-B Lab Control Sample Dissolved Water 3005A 401367 490-120048-D-2-E MS Matrix Spike Dissolved Water 3005A 401367 490-120048-D-2-F MSD Matrix Spike Duplicate Dissolved Water 3005A 401367 Prep Batch: 401460 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 490-119827-7 TMW-1 Dissolved Water 7470A 401454 MB 490-401454/1-B Method Blank Dissolved Water 7470A 401454 LCS 490-401454/2-B Lab Control Sample Dissolved Water 7470A 401454 490-119827-7 MS TMW-1 Dissolved Water 7470A 401454 490-119827-7 MSD TMW-1 Dissolved Water 7470A 401454 Analysis Batch: 401552 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 490-119827-1 SB-1 (1') Total/NA Solid 6010D 401267 490-119827-2 SB-2 (1') Total/NA Solid 6010D 401267 490-119827-3 SB-3 (1') Total/NA Solid 6010D 401267 490-119827-4 SB-4 (1') Total/NA Solid 6010D 401267 490-119827-5 SB-5 (1') Total/NA Solid 6010D 401267 490-119827-6 SB-6 (1') Total/NA Solid 6010D 401267 MB 490-401267/1-A Method Blank Total/NA Solid 6010D 401267 LCS 490-401267/2-A Lab Control Sample Total/NA Solid 6010D 401267 LCSD 490-401267/3-A Lab Control Sample Dup Total/NA Solid 6010D 401267 550-74906-A-1-K MS Matrix Spike Total/NA Solid 6010D 401267 550-74906-A-1-L MSD Matrix Spike Duplicate Total/NA Solid 6010D 401267 Analysis Batch: 401664 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 490-119827-7 TMW-1 Dissolved Water 7470A 401460 MB 490-401454/1-B Method Blank Dissolved Water 7470A 401460 LCS 490-401454/2-B Lab Control Sample Dissolved Water 7470A 401460 490-119827-7 MS TMW-1 Dissolved Water 7470A 401460 490-119827-7 MSD TMW-1 Dissolved Water 7470A 401460 Analysis Batch: 401676 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 490-119827-1 SB-1 (1') Total/NA Solid 7471E 400874 490-119827-2 SB-2 (1') Total/NA Solid 7471E 400874 490-119827-3 SB-3 (1') Total/NA Solid 7471E 400874 490-119827-4 SB-4 (1') Total/NA Solid 7471B 400874 490-119827-5 SB-5 (1') Total/NA Solid 7471B 400874 490-119827-6 SB-6 (1') Total/NA Solid 7471B 400874 TestAmerica Nashville Page 43 of 56 1/18/2017 QC Association Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Metals (Continued) Analysis Batch: 401676 (Continued) Lab Sample ID Client Sample ID MB 490-400874/1-A Method Blank LCS 490-400874/2-A Lab Control Sample LCSD 490-400874/3-A Lab Control Sample Dup 490-119827-1 MS SB-1 (1') 490-119827-1 MSD SB-1 (1') Analysis Batch: 401731 Lab Sample ID Client Sample ID 490-119827-7 TMW-1 MB 490-401367/1-B Method Blank LCS 490-401367/2-B Lab Control Sample 490-120048-D-2-E MS Matrix Spike 490-120048-D-2-F MSD Matrix Spike Duplicate General Chemistry Analysis Batch: 400681 Lab Sample ID 490-119827-1 490-119827-2 490-119827-3 490-119827-4 490-119827-5 490-119827-6 460-126646-A-1 DU TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Prep Type Matrix Method Prep Batch Total/NA Solid 7471 B 400874 Total/NA Solid 7471 B 400874 Total/NA Solid 7471 B 400874 Total/NA Solid 7471 B 400874 Total/NA Solid 7471 B 400874 Prep Type Matrix Method Prep Batch Dissolved Water 6010D 401455 Dissolved Water 6010D 401455 Dissolved Water 6010D 401455 Dissolved Water 6010D 401455 Dissolved Water 6010D 401455 Client Sample ID Prep Type Matrix Method SB-1 (1') Total/NA Solid Moisture SB-2 (1') Total/NA Solid Moisture SB-3 (1') Total/NA Solid Moisture SB-4 (1') Total/NA Solid Moisture SB-5 (1') Total/NA Solid Moisture SB-6 (1') Total/NA Solid Moisture Duplicate Total/NA Solid Moisture Prep Batch C TestAmerica Nashville Page 44 of 56 1/18/2017 Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Client Sample ID: SBA (1') Date Collected: 01/10/17 08:45 Date Received: 01/11/17 09:40 Batch Batch Prep Type Type Method Run Total/NA Analysis Moisture Client Sample ID: S13-1 (1') Date Collected: 01/10/17 08:45 Date Received: 01/11/17 09:40 Batch Batch Prep Type Type Method Run Total/NA Prep 5035 Total/NA Analysis 8260B Total/NA Prep 3051A Total/NA Analysis 6010D Total/NA Prep 3051A Total/NA Analysis 6010D Total/NA Prep 7471 B Total/NA Analysis 7471 B Client Sample ID: S13-2 (1') Date Collected: 01/10/17 09:10 Date Received: 01/11/17 09:40 Lab Chronicle C TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Lab Sample ID: 490-119827-1 Matrix: Solid Dil Initial Final Batch Prepared Factor Amount Amount Number or Analyzed Analyst Lab 1 400681 01/12/17 13:00 BAA TAL NSH Lab Sample ID: 490-119827-1 Matrix: Solid Percent Solids: 89.6 Dil Initial Final Batch Prepared Factor Amount Amount Number or Analyzed Analyst Lab 7.156 g 5.0 mL 400685 01/10/17 07:45 JLP TAL NSH 1 5 g 5 mL 400760 01/13/17 05:11 TSC TAL NSH 0.496 g 100 mL 400683 01/12/17 13:02 PG1 TAL NSH 1 400979 01/12/17 21:01 RDF TAL NSH 0.495 g 100 mL 401267 01/16/17 10:06 PG1 TAL NSH 1 401552 01/16/17 17:26 RDF TAL NSH 0.615 g 100 mL 400874 01/13/17 09:48 CAH TAL NSH 1 401676 01/16/17 15:55 LCS TAL NSH Lab Sample ID: 490-119827-2 Matrix: Solid Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis Moisture 1 400681 01/12/17 13:00 BAA TAL NSH Client Sample ID: S13-2 (1') Lab Sample ID: 490-119827-2 Date Collected: 01/10/17 09:10 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 91.0 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 5035 5.871 g 5.0 mL 400685 01/10/17 08:10 JLP TAL NSH Total/NA Analysis 8260B 1 5 g 5 mL 400760 01/13/17 05:40 TSC TAL NSH Total/NA Prep 3051A 0.525 g 100 mL 400683 01/12/17 13:02 PG1 TAL NSH Total/NA Analysis 6010D 1 400979 01/12/17 21:06 RDF TAL NSH Total/NA Prep 3051A 0.508 g 100 mL 401267 01/16/17 10:06 PG1 TAL NSH Total/NA Analysis 6010D 1 401552 01/16/17 17:31 RDF TAL NSH Total/NA Prep 7471B 0.622 g 100 mL 400874 01/13/17 09:48 CAH TAL NSH Total/NA Analysis 7471B 1 401676 01/16/17 16:03 LCS TAL NSH Page 45 of 56 TestAmerica Nashville 1/18/2017 Lab Chronicle Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Client Sample ID: S13-3 (1') Lab Sample ID: 490-119827-3 Date Collected: 01/10/17 09:30 Matrix: Solid Date Received: 01/11/17 09:40 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis Moisture 1 400681 01/12/17 13:00 BAA TAL NSH Client Sample ID: S13-3 (1') Lab Sample ID: 490-119827-3 Date Collected: 01/10/17 09:30 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 90.6 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount • Amount Number or Analyzed Analyst Lab Total/NA Prep 5035 Total/NA Analysis 8260B Total/NA Prep 3051A Total/NA Analysis 6010D Total/NA Prep 3051A Total/NA Analysis 6010D Total/NA Prep 7471 B Total/NA Analysis 7471 B 6.947 g 5.0 mL 400685 01/10/17 08:30 JLP TAL NSH 1 5 g 5 mL 400760 01/13/17 06:10 TSC TAL NSH 0.510 g 100 mL 400683 01/12/17 13:02 PG1 TAL NSH 1 400979 01/12/17 21:11 RDF TAL NSH 0.500 g 100 mL 401267 01/16/17 10:06 PG1 TAL NSH 1 401552 01/16/17 17:36 RDF TAL NSH 0.604 g 100 mL 400874 01/13/17 09:48 CAH TAL NSH 1 401676 01/16/17 16:06 LCS TAL NSH Client Sample ID: S13-4 (1) Lab Sample ID: 490-119827-4 Date Collected: 01/10/17 09:50 Matrix: Solid Date Received: 01/11/17 09:40 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis Moisture 1 400681 01/12/17 13:00 BAA TAL NSH Client Sample ID: S13-4 (1') Lab Sample ID: 490-119827-4 Date Collected: 01/10/17 09:50 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 94.1 Prep Type Batch Type Batch Method Dil Run Factor Initial Amount Final Amount Batch Number Prepared or Analyzed Analyst Lab Total/NA Prep 5035 6.492 g 5.0 mL 400685 01/10/17 08:50 JLP TAL NSH Total/NA Analysis 8260B 1 5 g 5 mL 400760 01/13/17 06:39 TSC TAL NSH Total/NA Prep 3051A 0.515 g 100 mL 400683 01/12/17 13:02 PG1 TAL NSH Total/NA Analysis 6010D 1 400979 01/12/17 21:16 RDF TAL NSH Total/NA Prep 3051A 0.518 g 100 mL 401267 01/16/17 10:06 PG1 TAL NSH Total/NA Analysis 6010D 1 401552 01/16/17 17:51 RDF TAL NSH Total/NA Prep 7471B 0.621 g 100 mL 400874 01/13/17 09:48 CAH TAL NSH Total/NA Analysis 7471B 1 401676 01/16/17 16:08 LCS TAL NSH Client Sample ID: S13-5 (1') Date Collected: 01/10/17 10:10 Date Received: 01/11/17 09:40 Lab Sample ID: 490-119827-5 Matrix: Solid Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis Moisture 1 400681 01/12/17 13:00 BAA TAL NSH Page 46 of 56 TestAmerica Nashville 1/18/2017 Lab Chronicle Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Client Sample ID: S13-5 (1') Lab Sample ID: 490-119827-5 Date Collected: 01/10/17 10:10 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 88.3 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 5035 7. 666 g 5.0 mL 400 885 01/ 00/17 09:10 JLP TAL NSH Total/NA Analysis 8260B 1 5 g 5 mL 400760 01/13/17 07:09 TSC TAL NSH Total/NA Prep 3051A 0.504 g 100 mL 400683 01/12/17 13:02 PG1 TAL NSH Total/NA Analysis 6010D 1 400979 01/12/17 21:22 RDF TAL NSH Total/NA Prep 3051A 0.523 g 100 mL 401267 01/16/17 10:06 PG1 TAL NSH Total/NA Analysis 6010D 1 401552 01/16/17 17:56 RDF TAL NSH Total/NA Prep 7471B 0.622 g 100 mL 400874 01/13/17 09:48 CAH TAL NSH Total/NA Analysis 7471B 1 401676 01/16/17 16:11 LCS TAL NSH Client Sample ID: S13-6 (1') Lab Sample ID: 490-119827-6 Date Collected: 01/10/17 10:30 Matrix: Solid Date Received: 01/11/17 09:40 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis Moisture 1 400681 01/12/17 13:00 BAA TAL NSH Client Sample ID: S13-6 (1') Lab Sample ID: 490-119827-6 Date Collected: 01/10/17 10:30 Matrix: Solid Date Received: 01/11/17 09:40 Percent Solids: 88.0 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 5035 6.498 g 5.0 mL 400 885 01/ 00/17 09:30 JLP TAL NSH Total/NA Analysis 8260B 1 5 g 5 mL 400760 01/13/17 07:38 TSC TAL NSH Total/NA Prep 3051A 0.512 g 100 mL 400683 01/12/17 13:02 PG1 TAL NSH Total/NA Analysis 6010D 1 400979 01/12/17 21:38 RDF TAL NSH Total/NA Prep 3051A 0.504 g 100 mL 401267 01/16/17 10:06 PG1 TAL NSH Total/NA Analysis 6010D 1 401552 01/16/17 18:01 RDF TAL NSH Total/NA Prep 7471B 0.597 g 100 mL 400874 01/13/17 09:48 CAH TAL NSH Total/NA Analysis 7471B 1 401676 01/16/17 16:19 LCS TAL NSH Client Sample ID: TMW-1 Lab Sample ID: 490-119827-7 Date Collected: 01/10/17 13:25 Matrix: Water Date Received: 01/11/17 09:40 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 10 mL 10 mL 400532 01/12/17 18:42 RP TAL NSH Dissolved Filtration Filtration 50 mL 50 mL 401367 01/16/17 13:51 CAH TAL NSH Dissolved Prep 3005A 50 mL 50 mL 401455 01/17/17 07:58 CAH TAL NSH Dissolved Analysis 6010D 1 401731 01/17/17 14:56 RDF TAL NSH Dissolved Filtration Filtration 30 mL 30 mL 401454 01/17/17 07:56 LCS TAL NSH Dissolved Prep 7470A 30 mL 30 mL 401460 01/17/17 08:12 LCS TAL NSH Dissolved Analysis 7470A 1 401664 01/17/17 13:02 LCS TAL NSH TestAmerica Nashville Page 47 of 56 1/18/2017 Lab Chronicle Client: CBRE, Inc. TestAmerica Job ID: 490-119827-1 Project/Site: E. Chapel Hill -Nelson Hwy, SDG: Research Triangle Park, NC Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 48 of 56 1/18/2017 Method Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Method Method Description Protocol Laboratory 8260B Volatile Organic Compounds (GC/MS) SW846 TAL NSH 6010D Metals (ICP) SW846 TAL NSH 7470A Mercury (CVAA) SW846 TAL NSH 7471B Mercury (CVAA) SW846 TAL NSH Moisture Percent Moisture EPA TAL NSH Protocol References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 49 of 56 1/18/2017 Certification Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Laboratory: TestAmerica Nashville Unless otherwise noted, all analytes for this laboratory were covered under each certification below. Authority Florida Program NELAP EPA Region Certification ID 4 E87358 The following analytes are included in this report, but are not certified under this certification: Analysis Method Prep Method Matrix Analyte 8260B 5035 Solid 1,2-Dichloroethene, Total The following analytes are included in this report, but certification is not offered by the governing authority Analysis Method Prep Method Matrix Analyte 6010D 3005A Water Arsenic 6010D 3005A Water Barium 6010D 3005A Water Cadmium 6010D 3005A Water Chromium 6010D 3005A Water Lead 6010D 3005A Water Selenium 6010D 3005A Water Silver 6010D 3051A Solid Arsenic 6010D 3051A Solid Barium 6010D 3051A Solid Cadmium 6010D 3051A Solid Chromium 6010D 3051A Solid Lead 6010D 3051A Solid Selenium 6010D 3051A Solid Silver 8260E Water 1,2-Dichloroethene, Total Moisture Solid Percent Solids New York NELAP 2 11342 The following analytes are included in this report, but certification is not offered by the governing authority Analysis Method Prep Method Matrix Analyte 6010D 3005A Water Arsenic 6010D 3005A Water Barium 6010D 3005A Water Cadmium 6010D 3005A Water Chromium 6010D 3005A Water Lead 6010D 3005A Water Selenium 6010D 3005A Water Silver 6010D 3051A Solid Arsenic 6010D 3051A Solid Barium 6010D 3051A Solid Cadmium 6010D 3051A Solid Chromium 6010D 3051A Solid Lead 6010D 3051A Solid Selenium 6010D 3051A Solid Silver 8260B Water 1,1,1,2-Tetrachloroethane 8260B Water 1,1,1-Trichloroethane 8260B Water 1,1,2,2-Tetrachloroethane 8260B Water 1,1,2-Trichloroethane 8260B Water 1,1-Dichloroethane 8260B Water 1,1-Dichloroethene 8260B Water 1,1-Dichloropropene 8260B Water 1,2,3-Trichlorobenzene 8260B Water 1,2,3-Trichloropropane TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Expiration Date 06-30-17 GXII0QiN Page 50 of 56 TestAmerica Nashville 1/18/2017 Certification Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Laboratory: TestAmerica Nashville (Continued) Unless otherwise noted, all analytes for this laboratory were covered under each certification below. TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Authority Program EPA Region Certification ID Expiration Date New York N ELAP 2 11342 03-31-17 The following analytes are included in this report, but certification is not offered by the governing authority Analysis Method Prep Method Matrix Analyte 8260B Water 1,2,4-Trichlorobenzene 8260B Water 1,2,4-Trimethylbenzene 8260B Water 1,2-Dibromo-3-Chloropropane 8260B Water 1,2-Dibromoethane (EDB) 8260B Water 1,2-Dichlorobenzene 8260B Water 1,2-Dichloroethane 8260B Water 1,2-Dichloroethene, Total 8260B Water 1,2-Dichloropropane 8260B Water 1,3,5-Trimethylbenzene 8260B Water 1,3-Dichlorobenzene 8260B Water 1,3-Dichloropropane 8260B Water 1,4-Dichlorobenzene 8260B Water 2,2-Dichloropropane 8260B Water 2-Butanone (MEK) 8260B Water 2-Chlorotoluene 8260B Water 2-Hexanone 8260B Water 4-Chlorotoluene 8260B Water 4-Methyl-2-pentanone (MIBK) 8260B Water Acetone 8260B Water Benzene 8260B Water Bromobenzene 8260B Water Bromochloromethane 8260B Water Bromodichloromethane 8260B Water Bromoform 8260B Water Bromomethane 8260B Water Carbon disulfide 8260B Water Carbon tetrachloride 8260B Water Chlorobenzene 8260B Water Chlorodibromomethane 8260B Water Chloroethane 8260B Water Chloroform 8260B Water Chloromethane 8260B Water cis-1,2-Dichloroethene 8260B Water cis-1,3-Dichloropropene 8260B Water Dibromomethane 8260B Water Dichlorodifluoromethane 8260B Water Diisopropyl ether 8260B Water Ethylbenzene 8260B Water Hexachlorobutadiene 8260B Water Isopropylbenzene 8260B Water Methyl tert-butyl ether 8260B Water Methylene Chloride 8260B Water Naphthalene 8260B Water n-Butylbenzene 8260B Water N-Propylbenzene 8260B Water p-Isopropyltoluene TestAmerica Nashville Page 51 of 56 1/18/2017 Certification Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Laboratory: TestAmerica Nashville (Continued) Unless otherwise noted, all analytes for this laboratory were covered under each certification below. TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Authority Program EPA Region Certification ID Expiration Date New York N ELAP 2 11342 03-31-17 The following analytes are included in this report, but certification is not offered by the governing authority Analysis Method Prep Method Matrix Analyte 8260B Water sec-Butylbenzene 8260B Water Styrene 8260B Water tert-Butylbenzene 8260B Water Tetrachloroethene 8260B Water Toluene 8260B Water trans- 1,2-Dichloroethene 8260B Water trans- 1,3-Dichloropropene 8260B Water Trichloroethene 8260B Water Trichlorofluoromethane 8260B Water Vinyl chloride 8260B Water Xylenes, Total 8260B 5035 Solid 1,1,1,2-Tetrachloroethane 8260B 5035 Solid 1,1,1-Trich loroethane 8260B 5035 Solid 1,1,2,2-Tetrachloroethane 8260B 5035 Solid 1,1,2-Trichloroethane 8260B 5035 Solid 1,1-Dichloroethane 8260B 5035 Solid 1,1-Dichloroethene 8260B 5035 Solid 1,1-Dichloropropene 8260B 5035 Solid 1,2,3-Trichlorobenzene 8260B 5035 Solid 1,2,3-Trichloropropane 8260B 5035 Solid 1,2,4-Trichlorobenzene 8260B 5035 Solid 1,2,4-Trimethylbenzene 8260B 5035 Solid 1,2-Dibromo-3-Chloropropane 8260B 5035 Solid 1,2-Dibromoethane (EDB) 8260B 5035 Solid 1,2-Dichlorobenzene 8260B 5035 Solid 1,2-Dichloroethane 8260B 5035 Solid 1,2-Dichloroethene, Total 8260B 5035 Solid 1,2-Dichloropropane 8260B 5035 Solid 1,3,5-Trimethylbenzene 8260B 5035 Solid 1,3-Dichlorobenzene 8260B 5035 Solid 1,3-Dichloropropane 8260B 5035 Solid 1,4-Dichlorobenzene 8260B 5035 Solid 2,2-Dichloropropane 8260B 5035 Solid 2-Butanone (MEK) 8260B 5035 Solid 2-Chlorotoluene 8260B 5035 Solid 2-Hexanone 8260B 5035 Solid 4-Chlorotoluene 8260B 5035 Solid 4-Methyl-2-pentanone (MIBK) 8260B 5035 Solid Acetone 8260B 5035 Solid Benzene 8260B 5035 Solid Bromobenzene 8260B 5035 Solid Bromochloromethane 8260B 5035 Solid Bromodichloromethane 8260B 5035 Solid Bromoform 8260B 5035 Solid Bromomethane 8260B 5035 Solid Carbon disulfide TestAmerica Nashville Page 52 of 56 1/18/2017 Certification Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Laboratory: TestAmerica Nashville (Continued) Unless otherwise noted, all analytes for this laboratory were covered under each certification below. TestAmerica Job ID: 490-119827-1 SDG: Research Triangle Park, NC Authority Program EPA Region Certification ID Expiration Date New York N ELAP 2 11342 03-31-17 The following analytes are included in this report, but certification is not offered by the governing authority Analysis Method Prep Method Matrix Analyte 8260B 5035 Solid Carbon tetrachloride 8260B 5035 Solid Chlorobenzene 8260B 5035 Solid Chlorodibromomethane 8260B 5035 Solid Chloroethane 8260B 5035 Solid Chloroform 8260B 5035 Solid Chloromethane 8260B 5035 Solid cis-1,2-Dichloroethene 8260B 5035 Solid cis-1,3-Dichloropropene 8260B 5035 Solid Dibromomethane 8260B 5035 Solid Dichlorodifluoromethane 8260B 5035 Solid Diisopropyl ether 8260B 5035 Solid Ethylbenzene 8260B 5035 Solid Hexachlorobutadiene 8260B 5035 Solid Isopropylbenzene 8260B 5035 Solid Methyl tert-butyl ether 8260B 5035 Solid Methylene Chloride 8260B 5035 Solid Naphthalene 8260B 5035 Solid n-Butylbenzene 8260B 5035 Solid N-Propylbenzene 8260B 5035 Solid p-Isopropyltoluene 8260B 5035 Solid sec-Butylbenzene 8260B 5035 Solid Styrene 8260B 5035 Solid tert-Butylbenzene 8260B 5035 Solid Tetrachloroethene 8260B 5035 Solid Toluene 8260B 5035 Solid trans- 1,2-Dichloroethene 8260B 5035 Solid trans- 1,3-Dichloropropene 8260B 5035 Solid Trichloroethene 8260B 5035 Solid Trichlorofluoromethane 8260B 5035 Solid Vinyl chloride 8260B 5035 Solid Xylenes, Total Moisture Solid Percent Solids South Carolina State Program 4 84009 (001) 02-18-17 " The following analytes are included in this report, but are not certified under this certification: Analysis Method Prep Method Matrix Analyte 8260E 5035 Solid Diisopropyl ether The following analytes are included in this report, but certification is not offered by the governing authority: Analysis Method Prep Method Matrix Analyte 8260E Water 1,2-Dichloroethene, Total 8260B 5035 Solid 1,2-Dichloroethene, Total Moisture Solid Percent Solids " Certification renewal pending - certification considered valid. TestAmerica Nashville Page 53 of 56 1/18/2017 Testmerica THE LEADER IN ENVIRONMENTAL TESTING 1111111111111111111111111111111111111111 Nashville, TN COOLER RECEIPT FORM 490-119827 Chain of Custody Cooler Received/Opened On Ill1/2017 a0940 , Time Samples Removed From Cooler r' Time Samples Placed In Storage rc (2 Hour Window) 1. Tracking # / ` 0 (Mast 4 digits, FedEx) Courier: Fedex_ IR Gun ID_97310166_ pH Strip Lott Chlorine Strip Lot O 2. Temperature of rep. sample or temp blank when opened:2111 Degrees Celsius 3. If Item #2 temperature is 0°C or less, was the representative sample or temp blank frozen? YES NO.40 4. Were custody seals on outside of cooler? ..NO ... NA If yes, how many and where: � � (- - 5. Were the seals intact, signed, and dated correctly? I�.NO... NA 6. Were custody papers inside cooler? F8...NO... NA certify that I opened the cooler and answered questions 1-6 (intial) 7. Were custody seals on containers: YES �O% and Intact YES ... NO. . Were these signed and dated correctly? YES ... NO.r.".4) 8. Packing mat'I used? ubblewr p Plastic bag eanuts Vermiculite Foam Insert Paper Other None` 9. Cooling process: — Ice Ice -pack Ice (direct contact) Dry is 10. Did all containers arrive in good condition (unbroken)? 11. Were all container labels complete (#, date, signed, pres., etc)? 12. Did all container labels and tags agree with custody papers? 13a. Were VOA vials received? b. Was there any observable headspace present in any VOA vial? e Other None :YE�. - NO ... NA ES ..NO ... NA J ..NA trl Z_Z097 E ... NO ... NA YES. NA 14. Was there a Trip Blank in this cooler? YES.. NO ..NA If multiple coofe s quence # certifv that I unloaded the cooler and answered auestions 7-14 (intial) 1 D 15a. On pres'd bottles, did pH test strips suggest preservation reached the correct pH level? YES..NO(O. b. Did the bottle labels indicate that the correct preservatives were used 1'ES}... NO ... NA 16. Was residual chlorine present? YES... NO.�NA� 1 certify that I checked for chlorine and pH as per SOP and answered questions 15-16 (intial) 9 17. Were custody papers properly filled out (ink, signed, etc)? YE ...NO ... NA 18. Did you sign the custody papers in the appropriate place? YE ... NO ... NA 19. Were correct containers used for the analysis requested? YE9...NO...NA 20. Was sufficient amount of sample sent in each container? 'E ...N0..;N& fn 1 certity that I attached a label with the unique LIM5 number to each container intial 21. Were there Non -Conformance issues at login? OE.(9 Was a NCM generated? S(E51.. # Kil 0�-,Z zd� BIS = Broken in shipment Cooler Receipt Fonn.doc LF-1 — —End of Form— Page 54 of 56 Revised 12/15/15 1/18/2017 ^? - -• V-� -F Gil �,3 — a 9 s (V m r m ' A D V m ��♦ m m z m z 3 0 z K m z (D a r Page 55 of 56 1 /18/2017 Login Sample Receipt Checklist Client: CBRE, Inc. Login Number: 119827 List Number: 1 Creator: Dawson, Keith M Question Job Number: 490-119827-1 SDG Number: Research Triangle Park, NC List Source: TestAmerica Nashville Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey True meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. N/A The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A TestAmerica Nashville Page 56 of 56 1/18/2017 TestAmerica ° THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Knoxville 5815 Middlebrook Pike Knoxville, TN 37921 Tel: (865)291-3000 TestAmerica Job ID: 140-6789-1 Client Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria roi CBRE, Inc. 201 S College Street, Suite 1700 Charlotte, North Carolina 28244 Attn: Mr. Bo Cappleman 'A n v\�" Authorized for release by: 1/1712017 3:39:15 PM Terry Walker Wasmund, Project Manager II (865) 291-3065 terry.wasmund@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Table of Contents TestAmerica Job ID: 140-6789-1 CoverPage .............................................. 1 Table of Contents ......................................... 2 Definitions/Glossary....................................... 3 Case Narrative ........................................... 4 Detection Summary ........................................ 5 Client Sample Results ...................................... 9 Default Detection Limits .................................... 27 QC Sample Results ........................................ 30 QC Association Summary ................................... 35 Lab Chronicle ............................................ 36 Method Summary ......................................... 38 Sample Summary ......................................... 39 Chain of Custody .......................................... 40 Receipt Checklists ......................................... 42 TestAmerica Knoxville Page 2 of 42 1/17/2017 Definitions/Glossary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Qualifiers TestAmerica Job ID: 140-6789-1 Air - GC/MS VOA Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. B Compound was found in the blank and sample. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. a Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference) Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Knoxville Page 3 of 42 1 /17/2017 Case Narrative C Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Job ID: 140-6789-1 Laboratory: TestAmerica Knoxville Narrative Job Narrative 140-6789-1 Receipt The samples were received on 1/12/2017 at 2:20 PM. The samples arrived in good condition and properly preserved. Air - GC/MS VOA Method(s) D1946, TO 15 LL, TO-14A, TO-15: EPA methods TO-14A and TO-15 specify the use of humidified "zero air" as the blank reagent for canister cleaning, instrument calibration and sample analysis. Ultra -high purity humidified nitrogen from a cryogenic reservoir is used in place of "zero air" by TestAmerica Knoxville. Method(s) TO-15: The continuing calibration verification (CCV) associated with batch 140-7733 exhibited % difference of > 30% for 1,2,4-trichlorobenzene; however, the results were within the LCS acceptance limits. The EPA method requires that all target analytes in the continuing calibration verification standard be within 30% difference from the initial calibration. According to the laboratory standard operating procedure, the continuing calibration is acceptable if it meets the laboratory control sample acceptance criteria. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Comments No additional comments. TestAmerica Knoxville Page 4 of 42 1 /17/2017 Detection Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-1 Lab Sample ID: 140-6789-1 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Acetone 59 48 13 ppb v/v 1.53 TO-15 Total/NA Benzene 0.61 J 1.9 0.54 ppb v/v 1.53 TO-15 Total/NA Bromodichloromethane 0.47 J 1.9 0.42 ppb v/v 1.53 TO-15 Total/NA 2-Butanone (MEK) 5.9 J 9.6 1.9 ppb v/v 1.53 TO-15 Total/NA Carbon disulfide 0.71 J 4.8 0.30 ppb v/v 1.53 TO-15 Total/NA Chloroform 5.9 1.9 0.36 ppb v/v 1.53 TO-15 Total/NA Ethylbenzene 1.2 J 1.9 0.65 ppb v/v 1.53 TO-15 Total/NA Isopropyl alcohol 15 J 48 0.90 ppb v/v 1.53 TO-15 Total/NA Methylene Chloride 3.8 J B 4.8 1.2 ppb v/v 1.53 TO-15 Total/NA 4-Methyl-2-pentanone (MIBK) 4.5 J 4.8 0.43 ppb v/v 1.53 TO-15 Total/NA m-Xylene & p-Xylene 5.2 J 7.7 1.1 ppb v/v 1.53 TO-15 Total/NA o-Xylene 2.0 1.9 0.58 ppb v/v 1.53 TO-15 Total/NA Toluene 4.0 1.9 1.1 ppb v/v 1.53 TO-15 Total/NA Trichlorofluoromethane 0.25 J 1.9 0.23 ppb v/v 1.53 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 100 1.9 0.30 ppb v/v 1.53 TO-15 Total/NA 1,2,4-Trimethylbenzene 3.8 1.9 0.60 ppb v/v 1.53 TO-15 Total/NA 1,3,5-Trimethylbenzene 0.98 J 1.9 0.62 ppb v/v 1.53 TO-15 Total/NA Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Acetone 140 110 32 ug/m3 1.53 TO-15 Total/NA F Benzene 2.0 J 6.1 1.7 ug/m3 1.53 TO-15 Total/NA Bromodichloromethane 3.2 J 13 2.8 ug/m3 1.53 TO-15 Total/NA 2-Butanone (MEK) 18 J 28 5.6 ug/m3 1.53 TO-15 Total/NA Carbon disulfide 2.2 J 15 0.92 ug/m3 1.53 TO-15 Total/NA Chloroform 29 9.3 1.8 ug/m3 1.53 TO-15 Total/NA Ethylbenzene 5.2 J 8.3 2.8 ug/m3 1.53 TO-15 Total/NA Isopropyl alcohol 38 J 120 2.2 ug/m3 1.53 TO-15 Total/NA Methylene Chloride 13 J B 17 4.3 ug/m3 1.53 TO-15 Total/NA 4-Methyl-2-pentanone (MIBK) 18 J 20 1.8 ug/m3 1.53 TO-15 Total/NA m-Xylene & p-Xylene 23 J 33 5.0 ug/m3 1.53 TO-15 Total/NA o-Xylene 8.5 8.3 2.5 ug/m3 1.53 TO-15 Total/NA Toluene 15 7.2 4.3 ug/m3 1.53 TO-15 Total/NA Trichlorofluoromethane 1.4 J 11 1.3 ug/m3 1.53 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 770 15 2.3 ug/m3 1.53 TO-15 Total/NA 1,2,4-Trimethylbenzene 19 9.4 3.0 ug/m3 1.53 TO-15 Total/NA 1,3,5-Trimethylbenzene 4.8 J 9.4 3.1 ug/m3 1.53 TO-15 Total/NA Client Sample ID: SG-2 Lab Sample ID: 140-6789-2 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Carbon disulfide 0.42 J 4.9 0.30 ppb v/v 1.56 TO-15 Total/NA Chloroform 0.97 J 2.0 0.37 ppb v/v 1.56 TO-15 Total/NA Dichlorodifluoromethane 230 4.9 0.66 ppb v/v 1.56 TO-15 Total/NA Isopropyl alcohol 2.1 J 49 0.92 ppb v/v 1.56 TO-15 Total/NA Methylene Chloride 2.9 J B 4.9 1.3 ppb v/v 1.56 TO-15 Total/NA 4-Methyl-2-pentanone (MIBK) 0.44 J 4.9 0.44 ppb v/v 1.56 TO-15 Total/NA trans- 1,2-Dichloroethene 0.51 J 2.0 0.49 ppb v/v 1.56 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 20 2.0 0.30 ppb v/v 1.56 TO-15 Total/NA Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Carbon disulfide 1.3 J 15 0.94 ug/m3 1.56 TO-15 Total/NA Chloroform 4.7 J 9.5 1.8 ug/m3 1.56 TO-15 Total/NA This Detection Summary does not include radiochemical test results. TestAmerica Knoxville Page 5 of 42 1 /17/2017 Detection Summary Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Client Sample ID: SG-2 (Continued) Lab Sample ID: 140-6789-2 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Dichlorodifluoromethane 1100 24 3.3 ug/m3 1.56 TO-15 Total/NA Isopropyl alcohol 5.0 J 120 2.3 ug/m3 1.56 TO-15 Total/NA Methylene Chloride 10 J B 17 4.4 ug/m3 1.56 TO-15 Total/NA 4-Methyl-2-pentanone (MIBK) 1.8 J 20 1.8 ug/m3 1.56 TO-15 Total/NA trans- 1,2-Dichloroethene 2.0 J 7.7 1.9 ug/m3 1.56 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 150 15 2.3 ug/m3 1.56 TO-15 Total/NA Client Sample ID: SG-3 Lab Sample ID: 140-6789-3 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Chloroform 1.4 J 2.0 0.37 ppb v/v 1.56 TO-15 Total/NA Dichlorodifluoromethane 3.4 J 4.9 0.66 ppb v/v 1.56 TO-15 Total/NA Isopropyl alcohol 1.2 J 49 0.92 ppb v/v 1.56 TO-15 Total/NA Methylene Chloride 3.4 J B 4.9 1.3 ppb v/v 1.56 TO-15 Total/NA 4-Methyl-2-pentanone (MIBK) 3.8 J 4.9 0.44 ppb v/v 1.56 TO-15 Total/NA trans- 1,2-Dichloroethene 0.57 J 2.0 0.49 ppb v/v 1.56 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 4.1 2.0 0.30 ppb v/v 1.56 TO-15 Total/NA Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Chloroform 6.8 J 9.5 1.8 ug/m3 1.56 TO-15 Total/NA Dichlorodifluoromethane 17 J 24 3.3 ug/m3 1.56 TO-15 Total/NA Isopropyl alcohol 3.0 J 120 2.3 ug/m3 1.56 TO-15 Total/NA Methylene Chloride 12 J B 17 4.4 ug/m3 1.56 TO-15 Total/NA 4-Methyl-2-pentanone (MIBK) 15 J 20 1.8 ug/m3 1.56 TO-15 Total/NA trans- 1,2-Dichloroethene 2.3 J 7.7 1.9 ug/m3 1.56 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 32 15 2.3 ug/m3 1.56 TO-15 Total/NA Client Sample ID: SG-4 Lab Sample ID: 140-6789-4 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Acetone 28 J 32 9.0 ppb v/v 1 TO-15 Total/NA Benzene 0.54 J 1.3 0.36 ppb v/v 1 TO-15 Total/NA 2-Butanone (MEK) 8.2 6.5 1.3 ppb v/v 1 TO-15 Total/NA Chloroform 0.81 J 1.3 0.25 ppb v/v 1 TO-15 Total/NA Cyclohexane 0.55 J 3.2 0.26 ppb v/v 1 TO-15 Total/NA Dichlorodifluoromethane 0.80 J 3.2 0.44 ppb v/v 1 TO-15 Total/NA Ethylbenzene 0.90 J 1.3 0.44 ppb v/v 1 TO-15 Total/NA Hexane 2.7 J 5.2 0.21 ppb v/v 1 TO-15 Total/NA Isopropyl alcohol 13 J 32 0.61 ppb v/v 1 TO-15 Total/NA Methylene Chloride 5.3 B 3.2 0.84 ppb v/v 1 TO-15 Total/NA 4-Methyl-2-pentanone (MIBK) 0.61 J 3.2 0.29 ppb v/v 1 TO-15 Total/NA m-Xylene & p-Xylene 1.5 J 5.2 0.77 ppb v/v 1 TO-15 Total/NA o-Xylene 0.56 J 1.3 0.39 ppb v/v 1 TO-15 Total/NA Styrene 0.88 J 1.3 0.37 ppb v/v 1 TO-15 Total/NA Toluene 12 1.3 0.77 ppb v/v 1 TO-15 Total/NA trans- 1,2-Dichloroethene 0.36 J 1.3 0.32 ppb v/v 1 TO-15 Total/NA 1,1,1-Trichloroethane 0.23 J 1.3 0.19 ppb v/v 1 TO-15 Total/NA Trichlorofluoromethane 0.23 J 1.3 0.15 ppb v/v 1 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 41 1.3 0.20 ppb v/v 1 TO-15 Total/NA Vinyl acetate 1.5 J 32 0.90 ppb v/v 1 TO-15 Total/NA This Detection Summary does not include radiochemical test results. TestAmerica Knoxville Page 6 of 42 1 /17/2017 Detection Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-4 (Continued) Lab Sample ID: 140-6789-4 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Acetone 66 J 77 21 ug/m3 1 TO-15 Total/NA Benzene 1.7 J 4.1 1.2 ug/m3 1 TO-15 Total/NA 2-Butanone (MEK) 24 19 3.8 ug/m3 1 TO-15 Total/NA Chloroform 4.0 J 6.3 1.2 ug/m3 1 TO-15 Total/NA Cyclohexane 1.9 J 11 0.89 ug/m3 1 TO-15 Total/NA Dichlorodifluoromethane 3.9 J 16 2.2 ug/m3 1 TO-15 Total/NA Ethylbenzene 3.9 J 5.6 1.9 ug/m3 1 TO-15 Total/NA Hexane 9.5 J 18 0.73 ug/m3 1 TO-15 Total/NA Isopropyl alcohol 32 J 79 1.5 ug/m3 1 TO-15 Total/NA Methylene Chloride 19 B 11 2.9 ug/m3 1 TO-15 Total/NA 4-Methyl-2-pentanone (MIBK) 2.5 J 13 1.2 ug/m3 1 TO-15 Total/NA m-Xylene & p-Xylene 6.3 J 22 3.4 ug/m3 1 TO-15 Total/NA o-Xylene 2.4 J 5.6 1.7 ug/m3 1 TO-15 Total/NA Styrene 3.7 J 5.5 1.6 ug/m3 1 TO-15 Total/NA Toluene 44 4.9 2.9 ug/m3 1 TO-15 Total/NA trans- 1,2-Dichloroethene 1.4 J 5.1 1.3 ug/m3 1 TO-15 Total/NA 1,1,1-Trichloroethane 1.3 J 7.0 1.1 ug/m3 1 TO-15 Total/NA Trichlorofluoromethane 1.3 J 7.2 0.87 ug/m3 1 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 320 9.9 1.5 ug/m3 1 TO-15 Total/NA Vinyl acetate 5.4 J 110 3.2 ug/m3 1 TO-15 Total/NA Client Sample ID: SG-5 Lab Sample ID: 140-6789-5 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Carbon disulfide 1.1 J 7.5 0.47 ppb v/v 1.58 TO-15 Total/NA Dichlorodifluoromethane 210 7.5 1.0 ppb v/v 1.58 TO-15 Total/NA Isopropyl alcohol 7.6 J 75 1.4 ppb v/v 1.58 TO-15 Total/NA Methylene Chloride 5.3 J B 7.5 2.0 ppb v/v 1.58 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 0.47 J 3.0 0.47 ppb v/v 1.58 TO-15 Total/NA Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Carbon disulfide 3.4 J 23 1.5 ug/m3 1.58 TO-15 Total/NA Dichlorodifluoromethane 1100 37 5.1 ug/m3 1.58 TO-15 Total/NA Isopropyl alcohol 19 J 180 3.5 ug/m3 1.58 TO-15 Total/NA Methylene Chloride 18 J B 26 6.8 ug/m3 1.58 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 3.6 J 23 3.6 ug/m3 1.58 TO-15 Total/NA Client Sample ID: SG-6 Lab Sample ID: 140-6789-6 Analyte Result Qualifier Acetone 580 Benzene 1.3 J 2-Butanone (MEK) 36 Carbon disulfide 0.59 J Chloroform 2.3 1,4-Dioxane 21 J Ethylbenzene 2.0 Hexane 0.57 J Isopropyl alcohol 230 Methylene Chloride 3.7 J B 4-Methyl-2-pentanone (MIBK) 17 This Detection Summary does not include radiochemical test results. RL MDL Unit Dil Fac D Method Prep Type 47 13 ppb v/v 1.54 TO-15 Total/NA 1.9 0.52 ppb v/v 1.54 TO-15 Total/NA 9.3 1.9 ppb v/v 1.54 TO-15 Total/NA 4.7 0.29 ppb v/v 1.54 TO-15 Total/NA 1.9 0.35 ppb v/v 1.54 TO-15 Total/NA 47 0.75 ppb v/v 1.54 TO-15 Total/NA 1.9 0.63 ppb v/v 1.54 TO-15 Total/NA 7.5 0.30 ppb v/v 1.54 TO-15 Total/NA 47 0.88 ppb v/v 1.54 TO-15 Total/NA 4.7 1.2 ppb v/v 1.54 TO-15 Total/NA 4.7 0.42 ppb v/v 1.54 TO-15 Total/NA Page 7 of 42 TestAmerica Knoxville 1/17/2017 Detection Summary Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Client Sample ID: SG-6 (Continued) Lab Sample ID: 140-6789-6 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type m-Xylene & p-Xylene 7.5 7.5 1.1 ppb v/v 1.54 TO-15 Total/NA Naphthalene 0.94 J 4.7 0.84 ppb v/v 1.54 TO-15 Total/NA o-Xylene 2.9 1.9 0.57 ppb v/v 1.54 TO-15 Total/NA Tetrahydrofuran 6.4 J 47 0.59 ppb v/v 1.54 TO-15 Total/NA Toluene 5.7 1.9 1.1 ppb v/v 1.54 TO-15 Total/NA Trichlorofluoromethane 0.23 J 1.9 0.22 ppb v/v 1.54 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 1.5 J 1.9 0.29 ppb v/v 1.54 TO-15 Total/NA 1,2,4-Trimethylbenzene 4.9 1.9 0.59 ppb v/v 1.54 TO-15 Total/NA 1,3,5-Trimethylbenzene 0.92 J 1.9 0.61 ppb v/v 1.54 TO-15 Total/NA Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Acetone 1400 110 31 ug/m3 1.54 TO-15 Total/NA Benzene 4.0 J 6.0 1.7 ug/m3 1.54 TO-15 Total/NA 2-Butanone (MEK) 110 28 5.5 ug/m3 1.54 TO-15 Total/NA Carbon disulfide 1.8 J 15 0.90 ug/m3 1.54 TO-15 Total/NA Chloroform 11 9.1 1.7 ug/m3 1.54 TO-15 Total/NA 1,4-Dioxane 75 J 170 2.7 ug/m3 1.54 TO-15 Total/NA Ethylbenzene 8.5 8.1 2.8 ug/m3 1.54 TO-15 Total/NA Hexane 2.0 J 26 1.1 ug/m3 1.54 TO-15 Total/NA Isopropyl alcohol 580 110 2.2 ug/m3 1.54 TO-15 Total/NA Methylene Chloride 13 J B 16 4.2 ug/m3 1.54 TO-15 Total/NA 4-Methyl-2-pentanone (MIBK) 71 19 1.7 ug/m3 1.54 TO-15 Total/NA m-Xylene & p-Xylene 33 32 4.9 ug/m3 1.54 TO-15 Total/NA Naphthalene 4.9 J 24 4.4 ug/m3 1.54 TO-15 Total/NA o-Xylene 12 8.1 2.5 ug/m3 1.54 TO-15 Total/NA Tetrahydrofuran 19 J 140 1.7 ug/m3 1.54 TO-15 Total/NA Toluene 21 7.0 4.2 ug/m3 1.54 TO-15 Total/NA Trichlorofluoromethane 1.3 J 10 1.3 ug/m3 1.54 TO-15 Total/NA 1,1,2-Trichloro-1,2,2-trifluoroethane 12 J 14 2.2 ug/m3 1.54 TO-15 Total/NA 1,2,4-Trimethylbenzene 24 9.2 2.9 ug/m3 1.54 TO-15 Total/NA 1,3,5-Trimethylbenzene 4.5 J 9.2 3.0 ug/m3 1.54 TO-15 Total/NA This Detection Summary does not include radiochemical test results. TestAmerica Knoxville Page 8 of 42 1 /17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-1 Lab Sample ID: 140-6789-1 Date Collected: 01/10/17 12:15 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone 59 48 13 ppb v/v 01/14/17 07:11 1.53 Benzene 0.61 J 1.9 0.54 ppb v/v 01/14/17 07:11 1.53 Benzyl chloride ND 7.7 0.75 ppb v/v 01/14/17 07:11 1.53 Bromodichloromethane 0.47 J 1.9 0.42 ppb v/v 01/14/17 07:11 1.53 Bromoform ND 1.9 0.46 ppb v/v 01/14/17 07:11 1.53 Bromomethane ND 1.9 0.31 ppb v/v 01/14/17 07:11 1.53 2-Butanone (MEK) 5.9 J 9.6 1.9 ppb v/v 01/14/17 07:11 1.53 Carbon disulfide 0.71 J 4.8 0.30 ppb v/v 01/14/17 07:11 1.53 Carbon tetrachloride ND 1.9 0.36 ppb v/v 01/14/17 07:11 1.53 Chlorobenzene ND 1.9 0.47 ppb v/v 01/14/17 07:11 1.53 Chloroethane ND 7.7 0.33 ppb v/v 01/14/17 07:11 1.53 Chloroform 5.9 1.9 0.36 ppb v/v 01/14/17 07:11 1.53 Chloromethane ND 4.8 1.5 ppb v/v 01/14/17 07:11 1.53 cis-1,2-Dichloroethene ND 1.9 0.57 ppb v/v 01/14/17 07:11 1.53 cis-1,3-Dichloropropene ND 1.9 0.71 ppb v/v 01/14/17 07:11 1.53 Cyclohexane ND 4.8 0.38 ppb v/v 01/14/17 07:11 1.53 Dibromochloromethane ND 1.9 0.40 ppb v/v 01/14/17 07:11 1.53 1,2-Dibromoethane (EDB) ND 1.9 0.42 ppb v/v 01/14/17 07:11 1.53 1,2-Dichlorobenzene ND 1.9 0.67 ppb v/v 01/14/17 07:11 1.53 1,3-Dichlorobenzene ND 1.9 0.62 ppb v/v 01/14/17 07:11 1.53 1,4-Dichlorobenzene ND 1.9 0.61 ppb v/v 01/14/17 07:11 1.53 Dichlorodifluoromethane ND 4.8 0.65 ppb v/v 01/14/17 07:11 1.53 1,1-Dichloroethane ND 1.9 0.25 ppb v/v 01/14/17 07:11 1.53 1,2-Dichloroethane ND 1.9 0.45 ppb v/v 01/14/17 07:11 1.53 1,1-Dichloroethene ND 1.9 0.33 ppb v/v 01/14/17 07:11 1.53 1,2-Dichloropropane ND 1.9 0.50 ppb v/v 01/14/17 07:11 1.53 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 1.9 0.31 ppb v/v 01/14/17 07:11 1.53 1,4-Dioxane ND 48 0.77 ppb v/v 01/14/17 07:11 1.53 Ethylbenzene 1.2 J 1.9 0.65 ppb v/v 01/14/17 07:11 1.53 Hexachlorobutadiene ND 1.9 0.75 ppb v/v 01/14/17 07:11 1.53 Hexane ND 7.7 0.31 ppb v/v 01/14/17 07:11 1.53 Isopropyl alcohol 15 J 48 0.90 ppb v/v 01/14/17 07:11 1.53 Isopropylbenzene ND 7.7 0.57 ppb v/v 01/14/17 07:11 1.53 Methylene Chloride 3.8 J B 4.8 1.2 ppb v/v 01/14/17 07:11 1.53 4-Methyl-2-pentanone (MIBK) 4.5 J 4.8 0.43 ppb v/v 01/14/17 07:11 1.53 Methyl tert-butyl ether ND 9.6 1.6 ppb v/v 01/14/17 07:11 1.53 m-Xylene & p-Xylene 5.2 J 7.7 1.1 ppb v/v 01/14/17 07:11 1.53 Naphthalene ND 4.8 0.86 ppb v/v 01/14/17 07:11 1.53 o-Xylene 2.0 1.9 0.58 ppb v/v 01/14/17 07:11 1.53 Styrene ND 1.9 0.55 ppb v/v 01/14/17 07:11 1.53 1,1,2,2-Tetrachloroethane ND 1.9 0.58 ppb v/v 01/14/17 07:11 1.53 Tetrachloroethene ND 1.9 0.38 ppb v/v 01/14/17 07:11 1.53 Tetrahydrofuran ND 48 0.60 ppb v/v 01/14/17 07:11 1.53 Toluene 4.0 1.9 1.1 ppb v/v 01/14/17 07:11 1.53 trans- 1,2-Dichloroethene ND 1.9 0.48 ppb v/v 01/14/17 07:11 1.53 trans- 1,3-Dichloropropene ND 1.9 0.46 ppb v/v 01/14/17 07:11 1.53 1,2,4-Trichoorobenzene ND 19 0.94 ppb v/v 01/14/17 07:11 1.53 1,1, 1 -Trichloroethane ND 1.9 0.29 ppb v/v 01/14/17 07:11 1.53 0 TestAmerica Knoxville Page 9 of 42 1 /17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-1 Lab Sample ID: 140-6789-1 Date Collected: 01/10/17 12:15 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,2-Trichloroethane ND 1.9 0.52 ppb v/v 01/14/17 07:11 1.53 Trichloroethene ND 1.9 0.34 ppb v/v 01/14/17 07:11 1.53 Trichlorofluoromethane 0.25 J 1.9 0.23 ppb v/v 01/14/17 07:11 1.53 1,1,2-Trichloro-1,2,2-trifluoroetha 100 1.9 0.30 ppb v/v 01/14/17 07:11 1.53 ne 1,2,4-Trimethyl benzene 3.8 1.9 0.60 ppb v/v 01/14/17 07:11 1.53 1,3,5-Trimethyl benzene 0.98 J 1.9 0.62 ppb v/v 01/14/17 07:11 1.53 Vinyl acetate ND 48 1.3 ppb v/v 01/14/17 07:11 1.53 Vinyl bromide ND 1.9 0.33 ppb v/v 01/14/17 07:11 1.53 Vinyl chloride ND 1.9 0.68 ppb v/v 01/14/17 07:11 1.53 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone 140 110 32 ug/m3 01/14/17 07:11 1.53 Benzene 2.0 J 6.1 1.7 ug/m3 01/14/17 07:11 1.53 Benzyl chloride ND 40 3.9 ug/m3 01/14/17 07:11 1.53 Bromodichloromethane 3.2 J 13 2.8 ug/m3 01/14/17 07:11 1.53 Bromoform ND 20 4.7 ug/m3 01/14/17 07:11 1.53 Bromomethane ND 7.4 1.2 ug/m3 01/14/17 07:11 1.53 2-Butanone (MEK) 18 J 28 5.6 ug/m3 01/14/17 07:11 1.53 Carbon disulfide 2.2 J 15 0.92 ug/m3 01/14/17 07:11 1.53 Carbon tetrachloride ND 12 2.3 ug/m3 01/14/17 07:11 1.53 Chlorobenzene ND 8.8 2.2 ug/m3 01/14/17 07:11 1.53 Chloroethane ND 20 0.88 ug/m3 01/14/17 07:11 1.53 Chloroform 29 9.3 1.8 ug/m3 01/14/17 07:11 1.53 Chloromethane ND 9.9 3.2 ug/m3 01/14/17 07:11 1.53 cis-1,2-Dichloroethene ND 7.6 2.3 ug/m3 01/14/17 07:11 1.53 cis-1,3-Dichloropropene ND 8.7 3.2 ug/m3 01/14/17 07:11 1.53 Cyclohexane ND 16 1.3 ug/m3 01/14/17 07:11 1.53 Dibromochloromethane ND 16 3.4 ug/m3 01/14/17 07:11 1.53 1,2-Dibromoethane (EDB) ND 15 3.2 ug/m3 01/14/17 07:11 1.53 1,2-Dichlorobenzene ND 11 4.0 ug/m3 01/14/17 07:11 1.53 1,3-Dichlorobenzene ND 11 3.7 ug/m3 01/14/17 07:11 1.53 1,4-Dichlorobenzene ND 11 3.7 ug/m3 01/14/17 07:11 1.53 Dichlorodifluoromethane ND 24 3.2 ug/m3 01/14/17 07:11 1.53 1,1-Dichloroethane ND 7.7 1.0 ug/m3 01/14/17 07:11 1.53 1,2-Dichloroethane ND 7.7 1.8 ug/m3 01/14/17 07:11 1.53 1,1-Dichloroethene ND 7.6 1.3 ug/m3 01/14/17 07:11 1.53 1,2-Dichloropropane ND 8.8 2.3 ug/m3 01/14/17 07:11 1.53 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 13 2.1 ug/m3 01/14/17 07:11 1.53 1,4-Dioxane ND 170 2.8 ug/m3 01/14/17 07:11 1.53 Ethylbenzene 5.2 J 8.3 2.8 ug/m3 01/14/17 07:11 1.53 Hexachlorobutadiene ND 20 8.0 ug/m3 01/14/17 07:11 1.53 Hexane ND 27 1.1 ug/m3 01/14/17 07:11 1.53 Isopropyl alcohol 38 J 120 2.2 ug/m3 01/14/17 07:11 1.53 Isopropylbenzene ND 38 2.8 ug/m3 01/14/17 07:11 1.53 Methylene Chloride 13 J B 17 4.3 ug/m3 01/14/17 07:11 1.53 4-Methyl-2-pentanone (MIBK) 18 J 20 1.8 ug/m3 01/14/17 07:11 1.53 Methyl tert-butyl ether ND 34 5.9 ug/m3 01/14/17 07:11 1.53 m-Xylene & p-Xylene 23 J 33 5.0 ug/m3 01/14/17 07:11 1.53 TestAmerica Knoxville Page 10 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Client Sample ID: SG-1 Lab Sample ID: 140-6789-1 Date Collected: 01/10/17 12:15 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Naphthalene ND 25 4.5 ug/m3 01/14/17 07:11 1.53 o-Xylene 8.5 8.3 2.5 ug/m3 01/14/17 07:11 1.53 Styrene ND 8.1 2.4 ug/m3 01/14/17 07:11 1.53 1,1,2,2-Tetrachloroethane ND 13 4.0 ug/m3 01/14/17 07:11 1.53 Tetrachloroethene ND 13 2.6 ug/m3 01/14/17 07:11 1.53 Tetrahydrofuran ND 140 1.8 ug/m3 01/14/17 07:11 1.53 Toluene 15 7.2 4.3 ug/m3 01/14/17 07:11 1.53 trans- 1,2-Dichloroethene ND 7.6 1.9 ug/m3 01/14/17 07:11 1.53 trans- 1,3-Dichloropropene ND 8.7 2.1 ug/m3 01/14/17 07:11 1.53 1,2,4-Trichlorobenzene ND 140 7.0 ug/m3 01/14/17 07:11 1.53 1,1,1-Trichloroethane ND 10 1.6 ug/m3 01/14/17 07:11 1.53 1,1,2-Trichloroethane ND 10 2.8 ug/m3 01/14/17 07:11 1.53 Trichloroethene ND 10 1.8 ug/m3 01/14/17 07:11 1.53 Trichlorofluoromethane 1.4 J 11 1.3 ug/m3 01/14/17 07:11 1.53 1,1,2-Trichloro-1,2,2-trifluoroetha 770 15 2.3 ug/m3 01/14/17 07:11 1.53 ne 1,2,4-Trimethylbenzene 19 9.4 3.0 ug/m3 01/14/17 07:11 1.53 1,3,5-Trimethylbenzene 4.8 J 9.4 3.1 ug/m3 01/14/17 07:11 1.53 Vinyl acetate ND 170 4.7 ug/m3 01/14/17 07:11 1.53 Vinyl bromide ND 8.4 1.5 ug/m3 01/14/17 07:11 1.53 Vinyl chloride ND 4.9 1.7 ug/m3 01/14/17 07:11 1.53 0 TestAmerica Knoxville Page 11 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-2 Lab Sample ID: 140-6789-2 Date Collected: 01/10/17 12:20 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 49 14 ppb v/v 01/14/17 02:42 1.56 Benzene ND 2.0 0.55 ppb v/v 01/14/17 02:42 1.56 Benzyl chloride ND 7.8 0.76 ppb v/v 01/14/17 02:42 1.56 Bromodichloromethane ND 2.0 0.43 ppb v/v 01/14/17 02:42 1.56 Bromoform ND 2.0 0.47 ppb v/v 01/14/17 02:42 1.56 Bromomethane ND 2.0 0.31 ppb v/v 01/14/17 02:42 1.56 2-Butanone (MEK) ND 9.8 2.0 ppb v/v 01/14/17 02:42 1.56 Carbon disulfide 0.42 J 4.9 0.30 ppb v/v 01/14/17 02:42 1.56 Carbon tetrachloride ND 2.0 0.37 ppb v/v 01/14/17 02:42 1.56 Chlorobenzene ND 2.0 0.48 ppb v/v 01/14/17 02:42 1.56 Chloroethane ND 7.8 0.34 ppb v/v 01/14/17 02:42 1.56 Chloroform 0.97 J 2.0 0.37 ppb v/v 01/14/17 02:42 1.56 Chloromethane ND 4.9 1.6 ppb v/v 01/14/17 02:42 1.56 cis-1,2-Dichloroethene ND 2.0 0.59 ppb v/v 01/14/17 02:42 1.56 cis-1,3-Dichloropropene ND 2.0 0.72 ppb v/v 01/14/17 02:42 1.56 Cyclohexane ND 4.9 0.39 ppb v/v 01/14/17 02:42 1.56 Dibromochloromethane ND 2.0 0.41 ppb v/v 01/14/17 02:42 1.56 1,2-Dibromoethane (EDB) ND 2.0 0.43 ppb v/v 01/14/17 02:42 1.56 1,2-Dichlorobenzene ND 2.0 0.68 ppb v/v 01/14/17 02:42 1.56 1,3-Dichlorobenzene ND 2.0 0.63 ppb v/v 01/14/17 02:42 1.56 1,4-Dichlorobenzene ND 2.0 0.62 ppb v/v 01/14/17 02:42 1.56 Dichlorodifluoromethane 230 4.9 0.66 ppb v/v 01/14/17 02:42 1.56 1,1-Dichloroethane ND 2.0 0.25 ppb v/v 01/14/17 02:42 1.56 1,2-Dichloroethane ND 2.0 0.46 ppb v/v 01/14/17 02:42 1.56 1,1-Dichloroethene ND 2.0 0.33 ppb v/v 01/14/17 02:42 1.56 1,2-Dichloropropane ND 2.0 0.51 ppb v/v 01/14/17 02:42 1.56 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 2.0 0.31 ppb v/v 01/14/17 02:42 1.56 1,4-Dioxane ND 49 0.78 ppb v/v 01/14/17 02:42 1.56 Ethylbenzene ND 2.0 0.66 ppb v/v 01/14/17 02:42 1.56 Hexachlorobutadiene ND 2.0 0.76 ppb v/v 01/14/17 02:42 1.56 Hexane ND 7.8 0.31 ppb v/v 01/14/17 02:42 1.56 Isopropyl alcohol 2.1 J 49 0.92 ppb v/v 01/14/17 02:42 1.56 Isopropylbenzene ND 7.8 0.59 ppb v/v 01/14/17 02:42 1.56 Methylene Chloride 2.9 J B 4.9 1.3 ppb v/v 01/14/17 02:42 1.56 4-Methyl-2-pentanone (MIBK) 0.44 J 4.9 0.44 ppb v/v 01/14/17 02:42 1.56 Methyl tert-butyl ether ND 9.8 1.7 ppb v/v 01/14/17 02:42 1.56 m-Xylene & p-Xylene ND 7.8 1.2 ppb v/v 01/14/17 02:42 1.56 Naphthalene ND 4.9 0.88 ppb v/v 01/14/17 02:42 1.56 o-Xylene ND 2.0 0.59 ppb v/v 01/14/17 02:42 1.56 Styrene ND 2.0 0.57 ppb v/v 01/14/17 02:42 1.56 1,1,2,2-Tetrachloroethane ND 2.0 0.59 ppb v/v 01/14/17 02:42 1.56 Tetrachloroethene ND 2.0 0.39 ppb v/v 01/14/17 02:42 1.56 Tetrahydrofuran ND 49 0.61 ppb v/v 01/14/17 02:42 1.56 Toluene ND 2.0 1.2 ppb v/v 01/14/17 02:42 1.56 trans-1,2-Dichloroethene 0.51 J 2.0 0.49 ppb v/v 01/14/17 02:42 1.56 trans- 1,3-Dichloropropene ND 2.0 0.47 ppb v/v 01/14/17 02:42 1.56 1,2,4-Trichoorobenzene ND 20 0.96 ppb v/v 01/14/17 02:42 1.56 1,1, 1 -Trichloroethane ND 2.0 0.29 ppb v/v 01/14/17 02:42 1.56 0 TestAmerica Knoxville Page 12 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-2 Lab Sample ID: 140-6789-2 Date Collected: 01/10/17 12:20 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,2-Trichloroethane ND 2.0 0.53 ppb v/v 01/14/17 02:42 1.56 Trichloroethene ND 2.0 0.35 ppb v/v 01/14/17 02:42 1.56 Trichlorofluoromethane ND 2.0 0.23 ppb v/v 01/14/17 02:42 1.56 1,1,2-Trichloro-1,2,2-trifluoroetha 20 2.0 0.30 ppb v/v 01/14/17 02:42 1.56 ne 1,2,4-Trimethylbenzene ND 2.0 0.61 ppb v/v 01/14/17 02:42 1.56 1,3,5-Trimethylbenzene ND 2.0 0.63 ppb v/v 01/14/17 02:42 1.56 Vinyl acetate ND 49 1.4 ppb v/v 01/14/17 02:42 1.56 Vinyl bromide ND 2.0 0.34 ppb v/v 01/14/17 02:42 1.56 Vinyl chloride ND 2.0 0.69 ppb v/v 01/14/17 02:42 1.56 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 126 32 ug/m3 01/14/17 02A2 1.56 Benzene ND 6.2 1.7 ug/m3 01/14/17 02:42 1.56 Benzyl chloride ND 40 3.9 ug/m3 01/14/17 02:42 1.56 Bromodichloromethane ND 13 2.9 ug/m3 01/14/17 02:42 1.56 Bromoform ND 20 4.8 ug/m3 01/14/17 02:42 1.56 Bromomethane ND 7.6 1.2 ug/m3 01/14/17 02:42 1.56 2-Butanone (MEK) ND 29 5.8 ug/m3 01/14/17 02:42 1.56 Carbon disulfide 1.3 J 15 0.94 ug/m3 01/14/17 02:42 1.56 Carbon tetrachloride ND 12 2.3 ug/m3 01/14/17 02:42 1.56 Chlorobenzene ND 9.0 2.2 ug/m3 01/14/17 02:42 1.56 Chloroethane ND 21 0.90 ug/m3 01/14/17 02:42 1.56 Chloroform 4.7 J 9.5 1.8 ug/m3 01/14/17 02:42 1.56 Chloromethane ND 10 3.2 ug/m3 01/14/17 02:42 1.56 cis-1,2-Dichloroethene ND 7.7 2.3 ug/m3 01/14/17 02:42 1.56 cis-1,3-Dichloropropene ND 8.9 3.3 ug/m3 01/14/17 02:42 1.56 Cyclohexane ND 17 1.3 ug/m3 01/14/17 02:42 1.56 Dibromochloromethane ND 17 3.5 ug/m3 01/14/17 02:42 1.56 1,2-Dibromoethane (EDB) ND 15 3.3 ug/m3 01/14/17 02:42 1.56 1,2-Dichlorobenzene ND 12 4.1 ug/m3 01/14/17 02:42 1.56 1,3-Dichlorobenzene ND 12 3.8 ug/m3 01/14/17 02:42 1.56 1,4-Dichlorobenzene ND 12 3.8 ug/m3 01/14/17 02:42 1.56 Dichlorodifluoromethane 1100 24 3.3 ug/m3 01/14/17 02:42 1.56 1,1-Dichloroethane ND 7.9 1.0 ug/m3 01/14/17 02:42 1.56 1,2-Dichloroethane ND 7.9 1.9 ug/m3 01/14/17 02:42 1.56 1,1-Dichloroethene ND 7.7 1.3 ug/m3 01/14/17 02:42 1.56 1,2-Dichloropropane ND 9.0 2.3 ug/m3 01/14/17 02:42 1.56 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 14 2.2 ug/m3 01/14/17 02:42 1.56 1,4-Dioxane ND 180 2.8 ug/m3 01/14/17 02:42 1.56 Ethylbenzene ND 8.5 2.9 ug/m3 01/14/17 02:42 1.56 Hexachlorobutadiene ND 21 8.1 ug/m3 01/14/17 02:42 1.56 Hexane ND 27 1.1 ug/m3 01/14/17 02:42 1.56 Isopropyl alcohol 5.0 J 120 2.3 ug/m3 01/14/17 02:42 1.56 Isopropylbenzene ND 38 2.9 ug/m3 01/14/17 02:42 1.56 Methylene Chloride 10 J B 17 4.4 ug/m3 01/14/17 02:42 1.56 4-Methyl-2-pentanone (MIBK) 1.8 J 20 1.8 ug/m3 01/14/17 02:42 1.56 Methyl tert-butyl ether ND 35 6.0 ug/m3 01/14/17 02:42 1.56 m-Xylene & p-Xylene ND 34 5.1 ug/m3 01/14/17 02:42 1.56 TestAmerica Knoxville Page 13 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Client Sample ID: SG-2 Lab Sample ID: 140-6789-2 Date Collected: 01/10/17 12:20 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Naphthalene ND 26 4.6 ug/m3 01/14/17 02:42 1.56 o-Xylene ND 8.5 2.6 ug/m3 01/14/17 02:42 1.56 Styrene ND 8.3 2.4 ug/m3 01/14/17 02:42 1.56 1,1,2,2-Tetrachloroethane ND 13 4.1 ug/m3 01/14/17 02:42 1.56 Tetrachloroethene ND 13 2.6 ug/m3 01/14/17 02:42 1.56 Tetrahydrofuran ND 140 1.8 ug/m3 01/14/17 02:42 1.56 Toluene ND 7.3 4.4 ug/m3 01/14/17 02:42 1.56 trans-1,2-Dichloroethene 2.0 J 7.7 1.9 ug/m3 01/14/17 02:42 1.56 trans- 1,3-Dichloropropene ND 8.9 2.1 ug/m3 01/14/17 02:42 1.56 1,2,4-Trichlorobenzene ND 140 7.1 ug/m3 01/14/17 02:42 1.56 1,1,1-Trichloroethane ND 11 1.6 ug/m3 01/14/17 02:42 1.56 1,1,2-Trichloroethane ND 11 2.9 ug/m3 01/14/17 02:42 1.56 Trichloroethene ND 10 1.9 ug/m3 01/14/17 02:42 1.56 Trichlorofluoromethane ND 11 1.3 ug/m3 01/14/17 02:42 1.56 1,1,2-Trichloro-1,2,2-trifluoroetha 150 15 2.3 ug/m3 01/14/17 02:42 1.56 ne 1,2,4-Trimethyl benzene ND 9.6 3.0 ug/m3 01/14/17 02:42 1.56 1,3,5-Trimethyl benzene ND 9.6 3.1 ug/m3 01/14/17 02:42 1.56 Vinyl acetate ND 170 4.8 ug/m3 01/14/17 02:42 1.56 Vinyl bromide ND 8.5 1.5 ug/m3 01/14/17 02:42 1.56 Vinyl chloride ND 5.0 1.8 ug/m3 01/14/17 02:42 1.56 0 TestAmerica Knoxville Page 14 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-3 Lab Sample ID: 140-6789-3 Date Collected: 01/10/17 12:25 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 49 14 ppb v/v 01/14/17 03:27 1.56 Benzene ND 2.0 0.55 ppb v/v 01/14/17 03:27 1.56 Benzyl chloride ND 7.8 0.76 ppb v/v 01/14/17 03:27 1.56 Bromodichloromethane ND 2.0 0.43 ppb v/v 01/14/17 03:27 1.56 Bromoform ND 2.0 0.47 ppb v/v 01/14/17 03:27 1.56 Bromomethane ND 2.0 0.31 ppb v/v 01/14/17 03:27 1.56 2-Butanone (MEK) ND 9.8 2.0 ppb v/v 01/14/17 03:27 1.56 Carbon disulfide ND 4.9 0.30 ppb v/v 01/14/17 03:27 1.56 Carbon tetrachloride ND 2.0 0.37 ppb v/v 01/14/17 03:27 1.56 Chlorobenzene ND 2.0 0.48 ppb v/v 01/14/17 03:27 1.56 Chloroethane ND 7.8 0.34 ppb v/v 01/14/17 03:27 1.56 Chloroform 1.4 J 2.0 0.37 ppb v/v 01/14/17 03:27 1.56 Chloromethane ND 4.9 1.6 ppb v/v 01/14/17 03:27 1.56 cis-1,2-Dichloroethene ND 2.0 0.59 ppb v/v 01/14/17 03:27 1.56 cis-1,3-Dichloropropene ND 2.0 0.72 ppb v/v 01/14/17 03:27 1.56 Cyclohexane ND 4.9 0.39 ppb v/v 01/14/17 03:27 1.56 Dibromochloromethane ND 2.0 0.41 ppb v/v 01/14/17 03:27 1.56 1,2-Dibromoethane (EDB) ND 2.0 0.43 ppb v/v 01/14/17 03:27 1.56 1,2-Dichlorobenzene ND 2.0 0.68 ppb v/v 01/14/17 03:27 1.56 1,3-Dichlorobenzene ND 2.0 0.63 ppb v/v 01/14/17 03:27 1.56 1,4-Dichlorobenzene ND 2.0 0.62 ppb v/v 01/14/17 03:27 1.56 Dichlorodifluoromethane 3.4 J 4.9 0.66 ppb v/v 01/14/17 03:27 1.56 1,1-Dichloroethane ND 2.0 0.25 ppb v/v 01/14/17 03:27 1.56 1,2-Dichloroethane ND 2.0 0.46 ppb v/v 01/14/17 03:27 1.56 1,1-Dichloroethene ND 2.0 0.33 ppb v/v 01/14/17 03:27 1.56 1,2-Dichloropropane ND 2.0 0.51 ppb v/v 01/14/17 03:27 1.56 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 2.0 0.31 ppb v/v 01/14/17 03:27 1.56 1,4-Dioxane ND 49 0.78 ppb v/v 01/14/17 03:27 1.56 Ethylbenzene ND 2.0 0.66 ppb v/v 01/14/17 03:27 1.56 Hexachlorobutadiene ND 2.0 0.76 ppb v/v 01/14/17 03:27 1.56 Hexane ND 7.8 0.31 ppb v/v 01/14/17 03:27 1.56 Isopropyl alcohol 1.2 J 49 0.92 ppb v/v 01/14/17 03:27 1.56 Isopropylbenzene ND 7.8 0.59 ppb v/v 01/14/17 03:27 1.56 Methylene Chloride 3.4 J B 4.9 1.3 ppb v/v 01/14/17 03:27 1.56 4-Methyl-2-pentanone (MIBK) 3.8 J 4.9 0.44 ppb v/v 01/14/17 03:27 1.56 Methyl tert-butyl ether ND 9.8 1.7 ppb v/v 01/14/17 03:27 1.56 m-Xylene & p-Xylene ND 7.8 1.2 ppb v/v 01/14/17 03:27 1.56 Naphthalene ND 4.9 0.88 ppb v/v 01/14/17 03:27 1.56 o-Xylene ND 2.0 0.59 ppb v/v 01/14/17 03:27 1.56 Styrene ND 2.0 0.57 ppb v/v 01/14/17 03:27 1.56 1,1,2,2-Tetrachloroethane ND 2.0 0.59 ppb v/v 01/14/17 03:27 1.56 Tetrachloroethene ND 2.0 0.39 ppb v/v 01/14/17 03:27 1.56 Tetrahydrofuran ND 49 0.61 ppb v/v 01/14/17 03:27 1.56 Toluene ND 2.0 1.2 ppb v/v 01/14/17 03:27 1.56 trans-1,2-Dichloroethene 0.57 J 2.0 0.49 ppb v/v 01/14/17 03:27 1.56 trans- 1,3-Dichloropropene ND 2.0 0.47 ppb v/v 01/14/17 03:27 1.56 1,2,4-Trichoorobenzene ND 20 0.96 ppb v/v 01/14/17 03:27 1.56 1,1, 1 -Trichloroethane ND 2.0 0.29 ppb v/v 01/14/17 03:27 1.56 0 TestAmerica Knoxville Page 15 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-3 Lab Sample ID: 140-6789-3 Date Collected: 01/10/17 12:25 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,2-Trichloroethane ND 2.0 0.53 ppb v/v 01/14/17 03:27 1.56 Trichloroethene ND 2.0 0.35 ppb v/v 01/14/17 03:27 1.56 Trichlorofluoromethane ND 2.0 0.23 ppb v/v 01/14/17 03:27 1.56 1,1,2-Trichloro-1,2,2-trifluoroetha 4.1 2.0 0.30 ppb v/v 01/14/17 03:27 1.56 ne 1,2,4-Trimethylbenzene ND 2.0 0.61 ppb v/v 01/14/17 03:27 1.56 1,3,5-Trimethylbenzene ND 2.0 0.63 ppb v/v 01/14/17 03:27 1.56 Vinyl acetate ND 49 1.4 ppb v/v 01/14/17 03:27 1.56 Vinyl bromide ND 2.0 0.34 ppb v/v 01/14/17 03:27 1.56 Vinyl chloride ND 2.0 0.69 ppb v/v 01/14/17 03:27 1.56 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 126 32 ug/m3 01/14/17 03:27 1.56 Benzene ND 6.2 1.7 ug/m3 01/14/17 03:27 1.56 Benzyl chloride ND 40 3.9 ug/m3 01/14/17 03:27 1.56 Bromodichloromethane ND 13 2.9 ug/m3 01/14/17 03:27 1.56 Bromoform ND 20 4.8 ug/m3 01/14/17 03:27 1.56 Bromomethane ND 7.6 1.2 ug/m3 01/14/17 03:27 1.56 2-Butanone (MEK) ND 29 5.8 ug/m3 01/14/17 03:27 1.56 Carbon disulfide ND 15 0.94 ug/m3 01/14/17 03:27 1.56 Carbon tetrachloride ND 12 2.3 ug/m3 01/14/17 03:27 1.56 Chlorobenzene ND 9.0 2.2 ug/m3 01/14/17 03:27 1.56 Chloroethane ND 21 0.90 ug/m3 01/14/17 03:27 1.56 Chloroform 6.8 J 9.5 1.8 ug/m3 01/14/17 03:27 1.56 Chloromethane ND 10 3.2 ug/m3 01/14/17 03:27 1.56 cis-1,2-Dichloroethene ND 7.7 2.3 ug/m3 01/14/17 03:27 1.56 cis-1,3-Dichloropropene ND 8.9 3.3 ug/m3 01/14/17 03:27 1.56 Cyclohexane ND 17 1.3 ug/m3 01/14/17 03:27 1.56 Dibromochloromethane ND 17 3.5 ug/m3 01/14/17 03:27 1.56 1,2-Dibromoethane (EDB) ND 15 3.3 ug/m3 01/14/17 03:27 1.56 1,2-Dichlorobenzene ND 12 4.1 ug/m3 01/14/17 03:27 1.56 1,3-Dichlorobenzene ND 12 3.8 ug/m3 01/14/17 03:27 1.56 1,4-Dichlorobenzene ND 12 3.8 ug/m3 01/14/17 03:27 1.56 Dichlorodifluoromethane 17 J 24 3.3 ug/m3 01/14/17 03:27 1.56 1,1-Dichloroethane ND 7.9 1.0 ug/m3 01/14/17 03:27 1.56 1,2-Dichloroethane ND 7.9 1.9 ug/m3 01/14/17 03:27 1.56 1,1-Dichloroethene ND 7.7 1.3 ug/m3 01/14/17 03:27 1.56 1,2-Dichloropropane ND 9.0 2.3 ug/m3 01/14/17 03:27 1.56 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 14 2.2 ug/m3 01/14/17 03:27 1.56 1,4-Dioxane ND 180 2.8 ug/m3 01/14/17 03:27 1.56 Ethylbenzene ND 8.5 2.9 ug/m3 01/14/17 03:27 1.56 Hexachlorobutadiene ND 21 8.1 ug/m3 01/14/17 03:27 1.56 Hexane ND 27 1.1 ug/m3 01/14/17 03:27 1.56 Isopropyl alcohol 3.0 J 120 2.3 ug/m3 01/14/17 03:27 1.56 Isopropylbenzene ND 38 2.9 ug/m3 01/14/17 03:27 1.56 Methylene Chloride 12 J B 17 4.4 ug/m3 01/14/17 03:27 1.56 4-Methyl-2-pentanone (MIBK) 15 J 20 1.8 ug/m3 01/14/17 03:27 1.56 Methyl tert-butyl ether ND 35 6.0 ug/m3 01/14/17 03:27 1.56 m-Xylene & p-Xylene ND 34 5.1 ug/m3 01/14/17 03:27 1.56 TestAmerica Knoxville Page 16 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Client Sample ID: SG-3 Lab Sample ID: 140-6789-3 Date Collected: 01/10/17 12:25 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Naphthalene ND 26 4.6 ug/m3 01/14/17 03:27 1.56 o-Xylene ND 8.5 2.6 ug/m3 01/14/17 03:27 1.56 Styrene ND 8.3 2.4 ug/m3 01/14/17 03:27 1.56 1,1,2,2-Tetrachloroethane ND 13 4.1 ug/m3 01/14/17 03:27 1.56 Tetrachloroethene ND 13 2.6 ug/m3 01/14/17 03:27 1.56 Tetrahydrofuran ND 140 1.8 ug/m3 01/14/17 03:27 1.56 Toluene ND 7.3 4.4 ug/m3 01/14/17 03:27 1.56 trans-1,2-Dichloroethene 2.3 J 7.7 1.9 ug/m3 01/14/17 03:27 1.56 trans- 1,3-Dichloropropene ND 8.9 2.1 ug/m3 01/14/17 03:27 1.56 1,2,4-Trichlorobenzene ND 140 7.1 ug/m3 01/14/17 03:27 1.56 1,1,1-Trichloroethane ND 11 1.6 ug/m3 01/14/17 03:27 1.56 1,1,2-Trichloroethane ND 11 2.9 ug/m3 01/14/17 03:27 1.56 Trichloroethene ND 10 1.9 ug/m3 01/14/17 03:27 1.56 Trichlorofluoromethane ND 11 1.3 ug/m3 01/14/17 03:27 1.56 1,1,2-Trichloro-1,2,2-trifluoroetha 32 15 2.3 ug/m3 01/14/17 03:27 1.56 ne 1,2,4-Trimethylbenzene ND 9.6 3.0 ug/m3 01/14/17 03:27 1.56 1,3,5-Trimethylbenzene ND 9.6 3.1 ug/m3 01/14/17 03:27 1.56 Vinyl acetate ND 170 4.8 ug/m3 01/14/17 03:27 1.56 Vinyl bromide ND 8.5 1.5 ug/m3 01/14/17 03:27 1.56 Vinyl chloride ND 5.0 1.8 ug/m3 01/14/17 03:27 1.56 0 TestAmerica Knoxville Page 17 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-4 Lab Sample ID: 140-6789-4 Date Collected: 01/10/17 12:30 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone 28 J 32 9.0 ppb v/v 01/14/17 04:12 1 Benzene 0.54 J 1.3 0.36 ppb v/v 01/14/17 04:12 1 Benzyl chloride ND 5.2 0.50 ppb v/v 01/14/17 04:12 1 Bromodichloromethane ND 1.3 0.28 ppb v/v 01/14/17 04:12 1 Bromoform ND 1.3 0.31 ppb v/v 01/14/17 04:12 1 Bromomethane ND 1.3 0.21 ppb v/v 01/14/17 04:12 1 2-Butanone (MEK) 8.2 6.5 1.3 ppb v/v 01/14/17 04:12 1 Carbon disulfide ND 3.2 0.20 ppb v/v 01/14/17 04:12 1 Carbon tetrachloride ND 1.3 0.25 ppb v/v 01/14/17 04:12 1 Chlorobenzene ND 1.3 0.32 ppb v/v 01/14/17 04:12 1 Chloroethane ND 5.2 0.23 ppb v/v 01/14/17 04:12 1 Chloroform 0.81 J 1.3 0.25 ppb v/v 01/14/17 04:12 1 Chloromethane ND 3.2 1.0 ppb v/v 01/14/17 04:12 1 cis-1,2-Dichloroethene ND 1.3 0.39 ppb v/v 01/14/17 04:12 1 cis-1,3-Dichloropropene ND 1.3 0.48 ppb v/v 01/14/17 04:12 1 Cyclohexane 0.55 J 3.2 0.26 ppb v/v 01/14/17 04:12 1 Dibromochloromethane ND 1.3 0.27 ppb v/v 01/14/17 04:12 1 1,2-Dibromoethane (EDB) ND 1.3 0.28 ppb v/v 01/14/17 04:12 1 1,2-Dichlorobenzene ND 1.3 0.45 ppb v/v 01/14/17 04:12 1 1,3-Dichlorobenzene ND 1.3 0.42 ppb v/v 01/14/17 04:12 1 1,4-Dichlorobenzene ND 1.3 0.41 ppb v/v 01/14/17 04:12 1 Dichlorodifluoromethane 0.80 J 3.2 0.44 ppb v/v 01/14/17 04:12 1 1,1-Dichloroethane ND 1.3 0.17 ppb v/v 01/14/17 04:12 1 1,2-Dichloroethane ND 1.3 0.30 ppb v/v 01/14/17 04:12 1 1,1-Dichloroethene ND 1.3 0.22 ppb v/v 01/14/17 04:12 1 1,2-Dichloropropane ND 1.3 0.34 ppb v/v 01/14/17 04:12 1 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 1.3 0.21 ppb v/v 01/14/17 04:12 1 1,4-Dioxane ND 32 0.52 ppb v/v 01/14/17 04:12 1 Ethylbenzene 0.90 J 1.3 0.44 ppb v/v 01/14/17 04:12 1 Hexachlorobutadiene ND 1.3 0.50 ppb v/v 01/14/17 04:12 1 Hexane 2.7 J 5.2 0.21 ppb v/v 01/14/17 04:12 1 Isopropyl alcohol 13 J 32 0.61 ppb v/v 01/14/17 04:12 1 Isopropylbenzene ND 5.2 0.39 ppb v/v 01/14/17 04:12 1 Methylene Chloride 5.3 B 3.2 0.84 ppb v/v 01/14/17 04:12 1 4-Methyl-2-pentanone (MIBK) 0.61 J 3.2 0.29 ppb v/v 01/14/17 04:12 1 Methyl tert-butyl ether ND 6.5 1.1 ppb v/v 01/14/17 04:12 1 m-Xylene & p-Xylene 1.5 J 5.2 0.77 ppb v/v 01/14/17 04:12 1 Naphthalene ND 3.2 0.58 ppb v/v 01/14/17 04:12 1 o-Xylene 0.56 J 1.3 0.39 ppb v/v 01/14/17 04:12 1 Styrene 0.88 J 1.3 0.37 ppb v/v 01/14/17 04:12 1 1,1,2,2-Tetrachloroethane ND 1.3 0.39 ppb v/v 01/14/17 04:12 1 Tetrachloroethene ND 1.3 0.26 ppb v/v 01/14/17 04:12 1 Tetrahydrofuran ND 32 0.41 ppb v/v 01/14/17 04:12 1 Toluene 12 1.3 0.77 ppb v/v 01/14/17 04:12 1 trans-1,2-Dichloroethene 0.36 J 1.3 0.32 ppb v/v 01/14/17 04:12 1 trans- 1,3-Dichloropropene ND 1.3 0.31 ppb v/v 01/14/17 04:12 1 1,2,4-Trichoorobenzene ND 13 0.63 ppb v/v 01/14/17 04:12 1 1,1,1-Trichloroethane 0.23 J 1.3 0.19 ppb v/v 01/14/17 04:12 1 M TestAmerica Knoxville Page 18 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-4 Lab Sample ID: 140-6789-4 Date Collected: 01/10/17 12:30 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,2-Trichloroethane ND 1.3 0.35 ppb v/v 01/14/17 04:12 w 1 Trichloroethene ND 1.3 0.23 ppb v/v 01/14/17 04:12 1 Y Trichlorofluoromethane 0.23 J 1.3 0.15 ppb v/v 01/14/17 04:12 1 1,1,2-Trichloro-1,2,2-trifluoroetha 41 1.3 0.20 ppb v/v 01/14/17 04:12 1 ne 1,2,4-Trimethylbenzene ND 1.3 0.41 ppb v/v 01/14/17 04:12 1 1,3,5-Trimethylbenzene ND 1.3 0.42 ppb v/v 01/14/17 04:12 1 Vinyl acetate 1.5 J 32 0.90 ppb v/v 01/14/17 04:12 1 Vinyl bromide ND 1.3 0.23 ppb v/v 01/14/17 04:12 1 Vinyl chloride ND 1.3 0.46 ppb v/v 01/14/17 04:12 1 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone 66 J 77 21 ug/m3 01/14/17 04:12 1 Benzene 1.7 J 4.1 1.2 ug/m3 01/14/17 04:12 1 Benzyl chloride ND 27 2.6 ug/m3 01/14/17 04:12 1 Bromodichloromethane ND 8.6 1.9 ug/m3 01/14/17 04:12 1 Bromoform ND 13 3.2 ug/m3 01/14/17 04:12 1 Bromomethane ND 5.0 0.80 ug/m3 01/14/17 04:12 1 2-Butanone (MEK) 24 19 3.8 ug/m3 01/14/17 04:12 1 Carbon disulfide ND 10 0.62 ug/m3 01/14/17 04:12 1 Carbon tetrachloride ND 8.1 1.5 ug/m3 01/14/17 04:12 1 Chlorobenzene ND 5.9 1.5 ug/m3 01/14/17 04:12 1 Chloroethane ND 14 0.60 ug/m3 01/14/17 04:12 1 Chloroform 4.0 J 6.3 1.2 ug/m3 01/14/17 04:12 1 Chloromethane ND 6.7 2.1 ug/m3 01/14/17 04:12 1 cis-1,2-Dichloroethene ND 5.1 1.5 ug/m3 01/14/17 04:12 1 cis-1,3-Dichloropropene ND 5.9 2.2 ug/m3 01/14/17 04:12 1 Cyclohexane 1.9 J 11 0.89 ug/m3 01/14/17 04:12 1 Dibromochloromethane ND 11 2.3 ug/m3 01/14/17 04:12 1 1,2-Dibromoethane (EDB) ND 9.9 2.2 ug/m3 01/14/17 04:12 1 1,2-Dichlorobenzene ND 7.8 2.7 ug/m3 01/14/17 04:12 1 1,3-Dichlorobenzene ND 7.8 2.5 ug/m3 01/14/17 04:12 1 1,4-Dichlorobenzene ND 7.8 2.5 ug/m3 01/14/17 04:12 1 Dichlorodifluoromethane 3.9 J 16 2.2 ug/m3 01/14/17 04:12 1 1,1-Dichloroethane ND 5.2 0.68 ug/m3 01/14/17 04:12 1 1,2-Dichloroethane ND 5.2 1.2 ug/m3 01/14/17 04:12 1 1,1-Dichloroethene ND 5.1 0.87 ug/m3 01/14/17 04:12 1 1,2-Dichloropropane ND 6.0 1.6 ug/m3 01/14/17 04:12 1 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 9.0 1.4 ug/m3 01/14/17 04:12 1 1,4-Dioxane ND 120 1.9 ug/m3 01/14/17 04:12 1 Ethylbenzene 3.9 J 5.6 1.9 ug/m3 01/14/17 04:12 1 Hexachlorobutadiene ND 14 5.4 ug/m3 01/14/17 04:12 1 Hexane 9.5 J 18 0.73 ug/m3 01/14/17 04:12 1 Isopropyl alcohol 32 J 79 1.5 ug/m3 01/14/17 04:12 1 Isopropylbenzene ND 25 1.9 ug/m3 01/14/17 04:12 1 Methylene Chloride 19 B 11 2.9 ug/m3 01/14/17 04:12 1 4-Methyl-2-pentanone (MIBK) 2.5 J 13 1.2 ug/m3 01/14/17 04:12 1 Methyl tert-butyl ether ND 23 4.0 ug/m3 01/14/17 04:12 1 m-Xylene & p-Xylene 6.3 J 22 3.4 ug/m3 01/14/17 04:12 1 TestAmerica Knoxville Page 19 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-4 Lab Sample ID: 140-6789-4 Date Collected: 01/10/17 12:30 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit Naphthalene ND 17 3.0 ug/m3 o-Xylene 2.4 J 5.6 1.7 ug/m3 Styrene 3.7 J 5.5 1.6 ug/m3 1,1,2,2-Tetrachloroethane ND 8.9 2.7 ug/m3 Tetrachloroethene ND 8.8 1.8 ug/m3 Tetrahydrofuran ND 95 1.2 ug/m3 Toluene 44 4.9 2.9 ug/m3 trans-1,2-Dichloroethene 1.4 J 5.1 1.3 ug/m3 trans- 1,3-Dichloropropene ND 5.9 1.4 ug/m3 1,2,4-Trichlorobenzene ND 96 4.7 ug/m3 1,1,1-Trichloroethane 1.3 J 7.0 1.1 ug/m3 1,1,2-Trichloroethane ND 7.0 1.9 ug/m3 Trichloroethene ND 6.9 1.2 ug/m3 Trichlorofluoromethane 1.3 J 7.2 0.87 ug/m3 1,1,2-Trichloro-1,2,2-trifluoroetha 320 9.9 1.5 ug/m3 ne 1,2,4-Trimethylbenzene ND 6.3 2.0 ug/m3 1,3,5-Trimethylbenzene ND 6.3 2.1 ug/m3 Vinyl acetate 5.4 J 110 3.2 ug/m3 Vinyl bromide ND 5.6 0.99 ug/m3 Vinyl chloride ND 3.3 1.2 ug/m3 D Prepared Analyzed 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 01/14/17 04:12 Dil Fac 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 B TestAmerica Knoxville Page 20 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-5 Lab Sample ID: 140-6789-5 Date Collected: 01/10/17 12:35 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 75 21 ppb v/v 01/14/17 04:57 1.58 Benzene ND 3.0 0.84 ppb v/v 01/14/17 04:57 1.58 Benzyl chloride ND 12 1.2 ppb v/v 01/14/17 04:57 1.58 Bromodichloromethane ND 3.0 0.66 ppb v/v 01/14/17 04:57 1.58 Bromoform ND 3.0 0.72 ppb v/v 01/14/17 04:57 1.58 Bromomethane ND 3.0 0.48 ppb v/v 01/14/17 04:57 1.58 2-Butanone (MEK) ND 15 3.0 ppb v/v 01/14/17 04:57 1.58 Carbon disulfide 1.1 J 7.5 0.47 ppb v/v 01/14/17 04:57 1.58 Carbon tetrachloride ND 3.0 0.57 ppb v/v 01/14/17 04:57 1.58 Chlorobenzene ND 3.0 0.74 ppb v/v 01/14/17 04:57 1.58 Chloroethane ND 12 0.53 ppb v/v 01/14/17 04:57 1.58 Chloroform ND 3.0 0.57 ppb v/v 01/14/17 04:57 1.58 Chloromethane ND 7.5 2.4 ppb v/v 01/14/17 04:57 1.58 cis-1,2-Dichloroethene ND 3.0 0.90 ppb v/v 01/14/17 04:57 1.58 cis-1,3-Dichloropropene ND 3.0 1.1 ppb v/v 01/14/17 04:57 1.58 Cyclohexane ND 7.5 0.60 ppb v/v 01/14/17 04:57 1.58 Dibromochloromethane ND 3.0 0.63 ppb v/v 01/14/17 04:57 1.58 1,2-Dibromoethane (EDB) ND 3.0 0.66 ppb v/v 01/14/17 04:57 1.58 1,2-Dichlorobenzene ND 3.0 1.1 ppb v/v 01/14/17 04:57 1.58 1,3-Dichlorobenzene ND 3.0 0.98 ppb v/v 01/14/17 04:57 1.58 1,4-Dichlorobenzene ND 3.0 0.96 ppb v/v 01/14/17 04:57 1.58 Dichlorodifluoromethane 210 7.5 1.0 ppb v/v 01/14/17 04:57 1.58 1,1-Dichloroethane ND 3.0 0.39 ppb v/v 01/14/17 04:57 1.58 1,2-Dichloroethane ND 3.0 0.71 ppb v/v 01/14/17 04:57 1.58 1,1-Dichloroethene ND 3.0 0.51 ppb v/v 01/14/17 04:57 1.58 1,2-Dichloropropane ND 3.0 0.78 ppb v/v 01/14/17 04:57 1.58 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 3.0 0.48 ppb v/v 01/14/17 04:57 1.58 1,4-Dioxane ND 75 1.2 ppb v/v 01/14/17 04:57 1.58 Ethylbenzene ND 3.0 1.0 ppb v/v 01/14/17 04:57 1.58 Hexachlorobutadiene ND 3.0 1.2 ppb v/v 01/14/17 04:57 1.58 Hexane ND 12 0.48 ppb v/v 01/14/17 04:57 1.58 Isopropyl alcohol 7.6 J 75 1.4 ppb v/v 01/14/17 04:57 1.58 Isopropylbenzene ND 12 0.90 ppb v/v 01/14/17 04:57 1.58 Methylene Chloride 5.3 J B 7.5 2.0 ppb v/v 01/14/17 04:57 1.58 4-Methyl-2-pentanone (MIBK) ND 7.5 0.68 ppb v/v 01/14/17 04:57 1.58 Methyl tert-butyl ether ND 15 2.6 ppb v/v 01/14/17 04:57 1.58 m-Xylene & p-Xylene ND 12 1.8 ppb v/v 01/14/17 04:57 1.58 Naphthalene ND 7.5 1.4 ppb v/v 01/14/17 04:57 1.58 o-Xylene ND 3.0 0.92 ppb v/v 01/14/17 04:57 1.58 Styrene ND 3.0 0.87 ppb v/v 01/14/17 04:57 1.58 1,1,2,2-Tetrachloroethane ND 3.0 0.92 ppb v/v 01/14/17 04:57 1.58 Tetrachloroethene ND 3.0 0.60 ppb v/v 01/14/17 04:57 1.58 Tetrahydrofuran ND 75 0.95 ppb v/v 01/14/17 04:57 1.58 Toluene ND 3.0 1.8 ppb v/v 01/14/17 04:57 1.58 trans- 1,2-Dichloroethene ND 3.0 0.75 ppb v/v 01/14/17 04:57 1.58 trans- 1,3-Dichloropropene ND 3.0 0.72 ppb v/v 01/14/17 04:57 1.58 1,2,4-Trichoorobenzene ND 30 1.5 ppb v/v 01/14/17 04:57 1.58 1,1, 1 -Trichloroethane ND 3.0 0.45 ppb v/v 01/14/17 04:57 1.58 0 TestAmerica Knoxville Page 21 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-5 Lab Sample ID: 140-6789-5 Date Collected: 01/10/17 12:35 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,2-Trichloroethane ND 3.0 0.81 ppb v/v 01/14/17 04:57 1.58 Trichloroethene ND 3.0 0.54 ppb v/v 01/14/17 04:57 1.58 Trichlorofluoromethane ND 3.0 0.36 ppb v/v 01/14/17 04:57 1.58 1,1,2-Trichloro-1,2,2-trifluoroetha 0.47 J 3.0 0.47 ppb v/v 01/14/17 04:57 1.58 ne 1,2,4-Trimethylbenzene ND 3.0 0.95 ppb v/v 01/14/17 04:57 1.58 1,3,5-Trimethylbenzene ND 3.0 0.98 ppb v/v 01/14/17 04:57 1.58 Vinyl acetate ND 75 2.1 ppb v/v 01/14/17 04:57 1.58 Vinyl bromide ND 3.0 0.53 ppb v/v 01/14/17 04:57 1.58 Vinyl chloride ND 3.0 1.1 ppb v/v 01/14/17 04:57 1.58 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 186 50 ug/m3 01/14/17 04:57 1.58 Benzene ND 9.6 2.7 ug/m3 01/14/17 04:57 1.58 Benzyl chloride ND 62 6.1 ug/m3 01/14/17 04:57 1.58 Bromodichloromethane ND 20 4.4 ug/m3 01/14/17 04:57 1.58 Bromoform ND 31 7.5 ug/m3 01/14/17 04:57 1.58 Bromomethane ND 12 1.9 ug/m3 01/14/17 04:57 1.58 2-Butanone (MEK) ND 44 8.9 ug/m3 01/14/17 04:57 1.58 Carbon disulfide 3.4 J 23 1.5 ug/m3 01/14/17 04:57 1.58 Carbon tetrachloride ND 19 3.6 ug/m3 01/14/17 04:57 1.58 Chlorobenzene ND 14 3.4 ug/m3 01/14/17 04:57 1.58 Chloroethane ND 32 1.4 ug/m3 01/14/17 04:57 1.58 Chloroform ND 15 2.8 ug/m3 01/14/17 04:57 1.58 Chloromethane ND 16 5.0 ug/m3 01/14/17 04:57 1.58 cis-1,2-Dichloroethene ND 12 3.6 ug/m3 01/14/17 04:57 1.58 cis-1,3-Dichloropropene ND 14 5.1 ug/m3 01/14/17 04:57 1.58 Cyclohexane ND 26 2.1 ug/m3 01/14/17 04:57 1.58 Dibromochloromethane ND 26 5.4 ug/m3 01/14/17 04:57 1.58 1,2-Dibromoethane (EDB) ND 23 5.1 ug/m3 01/14/17 04:57 1.58 1,2-Dichlorobenzene ND 18 6.3 ug/m3 01/14/17 04:57 1.58 1,3-Dichlorobenzene ND 18 5.9 ug/m3 01/14/17 04:57 1.58 1,4-Dichlorobenzene ND 18 5.8 ug/m3 01/14/17 04:57 1.58 Dichlorodifluoromethane 1100 37 5.1 ug/m3 01/14/17 04:57 1.58 1,1-Dichloroethane ND 12 1.6 ug/m3 01/14/17 04:57 1.58 1,2-Dichloroethane ND 12 2.9 ug/m3 01/14/17 04:57 1.58 1,1-Dichloroethene ND 12 2.0 ug/m3 01/14/17 04:57 1.58 1,2-Dichloropropane ND 14 3.6 ug/m3 01/14/17 04:57 1.58 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 21 3.4 ug/m3 01/14/17 04:57 1.58 1,4-Dioxane ND 270 4.3 ug/m3 01/14/17 04:57 1.58 Ethylbenzene ND 13 4.4 ug/m3 01/14/17 04:57 1.58 Hexachlorobutadiene ND 32 13 ug/m3 01/14/17 04:57 1.58 Hexane ND 42 1.7 ug/m3 01/14/17 04:57 1.58 Isopropyl alcohol 19 J 180 3.5 ug/m3 01/14/17 04:57 1.58 Isopropylbenzene ND 59 4.4 ug/m3 01/14/17 04:57 1.58 Methylene Chloride 18 J B 26 6.8 ug/m3 01/14/17 04:57 1.58 4-Methyl-2-pentanone (MIBK) ND 31 2.8 ug/m3 01/14/17 04:57 1.58 Methyl tert-butyl ether ND 54 9.2 ug/m3 01/14/17 04:57 1.58 m-Xylene & p-Xylene ND 52 7.8 ug/m3 01/14/17 04:57 1.58 TestAmerica Knoxville Page 22 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Client Sample ID: SG-5 Lab Sample ID: 140-6789-5 Date Collected: 01/10/17 12:35 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Naphthalene ND 39 7.1 ug/m3 01/14/17 04:57 1.58 o-Xylene ND 13 4.0 ug/m3 01/14/17 04:57 1.58 Styrene ND 13 3.7 ug/m3 01/14/17 04:57 1.58 1,1,2,2-Tetrachloroethane ND 21 6.3 ug/m3 01/14/17 04:57 1.58 Tetrachloroethene ND 20 4.1 ug/m3 01/14/17 04:57 1.58 Tetrahydrofuran ND 220 2.8 ug/m3 01/14/17 04:57 1.58 Toluene ND 11 6.8 ug/m3 01/14/17 04:57 1.58 trans- 1,2-Dichloroethene ND 12 3.0 ug/m3 01/14/17 04:57 1.58 trans- 1,3-Dichloropropene ND 14 3.3 ug/m3 01/14/17 04:57 1.58 1,2,4-Trichlorobenzene ND 220 11 ug/m3 01/14/17 04:57 1.58 1,1,1-Trichloroethane ND 16 2.5 ug/m3 01/14/17 04:57 1.58 1,1,2-Trichloroethane ND 16 4.4 ug/m3 01/14/17 04:57 1.58 Trichloroethene ND 16 2.9 ug/m3 01/14/17 04:57 1.58 Trichlorofluoromethane ND 17 2.0 ug/m3 01/14/17 04:57 1.58 1,1,2-Trichloro-1,2,2-trifluoroetha 3.6 J 23 3.6 ug/m3 01/14/17 04:57 1.58 ne 1,2,4-Trimethyl benzene ND 15 4.7 ug/m3 01/14/17 04:57 1.58 1,3,5-Trimethyl benzene ND 15 4.8 ug/m3 01/14/17 04:57 1.58 Vinyl acetate ND 260 7.4 ug/m3 01/14/17 04:57 1.58 Vinyl bromide ND 13 2.3 ug/m3 01/14/17 04:57 1.58 Vinyl chloride ND 7.7 2.7 ug/m3 01/14/17 04:57 1.58 0 TestAmerica Knoxville Page 23 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-6 Lab Sample ID: 140-6789-6 Date Collected: 01/10/17 12:40 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone 580 47 13 ppb v/v 01/14/17 05:41 1.54 Benzene 1.3 J 1.9 0.52 ppb v/v 01/14/17 05:41 1.54 Benzyl chloride ND 7.5 0.73 ppb v/v 01/14/17 05:41 1.54 Bromodichloromethane ND 1.9 0.41 ppb v/v 01/14/17 05:41 1.54 Bromoform ND 1.9 0.45 ppb v/v 01/14/17 05:41 1.54 Bromomethane ND 1.9 0.30 ppb v/v 01/14/17 05:41 1.54 2-Butanone (MEK) 36 9.3 1.9 ppb v/v 01/14/17 05:41 1.54 Carbon disulfide 0.59 J 4.7 0.29 ppb v/v 01/14/17 05:41 1.54 Carbon tetrachloride ND 1.9 0.35 ppb v/v 01/14/17 05:41 1.54 Chlorobenzene ND 1.9 0.46 ppb v/v 01/14/17 05:41 1.54 Chloroethane ND 7.5 0.33 ppb v/v 01/14/17 05:41 1.54 Chloroform 2.3 1.9 0.35 ppb v/v 01/14/17 05:41 1.54 Chloromethane ND 4.7 1.5 ppb v/v 01/14/17 05:41 1.54 cis-1,2-Dichloroethene ND 1.9 0.56 ppb v/v 01/14/17 05:41 1.54 cis-1,3-Dichloropropene ND 1.9 0.69 ppb v/v 01/14/17 05:41 1.54 Cyclohexane ND 4.7 0.37 ppb v/v 01/14/17 05:41 1.54 Dibromochloromethane ND 1.9 0.39 ppb v/v 01/14/17 05:41 1.54 1,2-Dibromoethane (EDB) ND 1.9 0.41 ppb v/v 01/14/17 05:41 1.54 1,2-Dichlorobenzene ND 1.9 0.65 ppb v/v 01/14/17 05:41 1.54 1,3-Dichlorobenzene ND 1.9 0.61 ppb v/v 01/14/17 05:41 1.54 1,4-Dichlorobenzene ND 1.9 0.60 ppb v/v 01/14/17 05:41 1.54 Dichlorodifluoromethane ND 4.7 0.63 ppb v/v 01/14/17 05:41 1.54 1,1-Dichloroethane ND 1.9 0.24 ppb v/v 01/14/17 05:41 1.54 1,2-Dichloroethane ND 1.9 0.44 ppb v/v 01/14/17 05:41 1.54 1,1-Dichloroethene ND 1.9 0.32 ppb v/v 01/14/17 05:41 1.54 1,2-Dichloropropane ND 1.9 0.49 ppb v/v 01/14/17 05:41 1.54 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 1.9 0.30 ppb v/v 01/14/17 05:41 1.54 1,4-Dioxane 21 J 47 0.75 ppb v/v 01/14/17 05:41 1.54 Ethylbenzene 2.0 1.9 0.63 ppb v/v 01/14/17 05:41 1.54 Hexachlorobutadiene ND 1.9 0.73 ppb v/v 01/14/17 05:41 1.54 Hexane 0.57 J 7.5 0.30 ppb v/v 01/14/17 05:41 1.54 Isopropyl alcohol 230 47 0.88 ppb v/v 01/14/17 05:41 1.54 Isopropylbenzene ND 7.5 0.56 ppb v/v 01/14/17 05:41 1.54 Methylene Chloride 3.7 J B 4.7 1.2 ppb v/v 01/14/17 05:41 1.54 4-Methyl-2-pentanone (MIBK) 17 4.7 0.42 ppb v/v 01/14/17 05:41 1.54 Methyl tert-butyl ether ND 9.3 1.6 ppb v/v 01/14/17 05:41 1.54 m-Xylene & p-Xylene 7.5 7.5 1.1 ppb v/v 01/14/17 05:41 1.54 Naphthalene 0.94 J 4.7 0.84 ppb v/v 01/14/17 05:41 1.54 o-Xylene 2.9 1.9 0.57 ppb v/v 01/14/17 05:41 1.54 Styrene ND 1.9 0.54 ppb v/v 01/14/17 05:41 1.54 1,1,2,2-Tetrachloroethane ND 1.9 0.57 ppb v/v 01/14/17 05:41 1.54 Tetrachloroethene ND 1.9 0.37 ppb v/v 01/14/17 05:41 1.54 Tetrahydrofuran 6.4 J 47 0.59 ppb v/v 01/14/17 05:41 1.54 Toluene 5.7 1.9 1.1 ppb v/v 01/14/17 05:41 1.54 trans- 1,2-Dichloroethene ND 1.9 0.47 ppb v/v 01/14/17 05:41 1.54 trans- 1,3-Dichloropropene ND 1.9 0.45 ppb v/v 01/14/17 05:41 1.54 1,2,4-Trichoorobenzene ND 19 0.91 ppb v/v 01/14/17 05:41 1.54 1,1, 1 -Trichloroethane ND 1.9 0.28 ppb v/v 01/14/17 05:41 1.54 TestAmerica Knoxville Page 24 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-6 Lab Sample ID: 140-6789-6 Date Collected: 01/10/17 12:40 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,2-Trichloroethane ND 1.9 0.50 ppb v/v 01/14/17 05:41 1.54 Trichloroethene ND 1.9 0.34 ppb v/v 01/14/17 05:41 1.54 Trichlorofluoromethane 0.23 J 1.9 0.22 ppb v/v 01/14/17 05:41 1.54 1,1,2-Trichloro-1,2,2-trifluoroetha 1.5 J 1.9 0.29 ppb v/v 01/14/17 05:41 1.54 ne 1,2,4-Trimethyl benzene 4.9 1.9 0.59 ppb v/v 01/14/17 05:41 1.54 1,3,5-Trimethyl benzene 0.92 J 1.9 0.61 ppb v/v 01/14/17 05:41 1.54 Vinyl acetate ND 47 1.3 ppb v/v 01/14/17 05:41 1.54 Vinyl bromide ND 1.9 0.33 ppb v/v 01/14/17 05:41 1.54 Vinyl chloride ND 1.9 0.66 ppb v/v 01/14/17 05:41 1.54 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone 1400 116 31 ug/m3 01/14/17 05Al 1.54 Benzene 4.0 J 6.0 1.7 ug/m3 01/14/17 05:41 1.54 Benzyl chloride ND 39 3.8 ug/m3 01/14/17 05:41 1.54 Bromodichloromethane ND 13 2.8 ug/m3 01/14/17 05:41 1.54 Bromoform ND 19 4.6 ug/m3 01/14/17 05:41 1.54 Bromomethane ND 7.2 1.2 ug/m3 01/14/17 05:41 1.54 2-Butanone (MEK) 110 28 5.5 ug/m3 01/14/17 05:41 1.54 Carbon disulfide 1.8 J 15 0.90 ug/m3 01/14/17 05:41 1.54 Carbon tetrachloride ND 12 2.2 ug/m3 01/14/17 05:41 1.54 Chlorobenzene ND 8.6 2.1 ug/m3 01/14/17 05:41 1.54 Chloroethane ND 20 0.86 ug/m3 01/14/17 05:41 1.54 Chloroform 11 9.1 1.7 ug/m3 01/14/17 05:41 1.54 Chloromethane ND 9.6 3.1 ug/m3 01/14/17 05:41 1.54 cis-1,2-Dichloroethene ND 7.4 2.2 ug/m3 01/14/17 05:41 1.54 cis-1,3-Dichloropropene ND 8.5 3.1 ug/m3 01/14/17 05:41 1.54 Cyclohexane ND 16 1.3 ug/m3 01/14/17 05:41 1.54 Dibromochloromethane ND 16 3.3 ug/m3 01/14/17 05:41 1.54 1,2-Dibromoethane (EDB) ND 14 3.2 ug/m3 01/14/17 05:41 1.54 1,2-Dichlorobenzene ND 11 3.9 ug/m3 01/14/17 05:41 1.54 1,3-Dichlorobenzene ND 11 3.6 ug/m3 01/14/17 05:41 1.54 1,4-Dichlorobenzene ND 11 3.6 ug/m3 01/14/17 05:41 1.54 Dichlorodifluoromethane ND 23 3.1 ug/m3 01/14/17 05:41 1.54 1,1-Dichloroethane ND 7.6 0.98 ug/m3 01/14/17 05:41 1.54 1,2-Dichloroethane ND 7.6 1.8 ug/m3 01/14/17 05:41 1.54 1,1-Dichloroethene ND 7.4 1.3 ug/m3 01/14/17 05:41 1.54 1,2-Dichloropropane ND 8.6 2.2 ug/m3 01/14/17 05:41 1.54 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 13 2.1 ug/m3 01/14/17 05:41 1.54 1,4-Dioxane 75 J 170 2.7 ug/m3 01/14/17 05:41 1.54 Ethylbenzene 8.5 8.1 2.8 ug/m3 01/14/17 05:41 1.54 Hexachlorobutadiene ND 20 7.8 ug/m3 01/14/17 05:41 1.54 Hexane 2.0 J 26 1.1 ug/m3 01/14/17 05:41 1.54 Isopropyl alcohol 580 110 2.2 ug/m3 01/14/17 05:41 1.54 Isopropylbenzene ND 37 2.8 ug/m3 01/14/17 05:41 1.54 Methylene Chloride 13 J B 16 4.2 ug/m3 01/14/17 05:41 1.54 4-Methyl-2-pentanone (MIBK) 71 19 1.7 ug/m3 01/14/17 05:41 1.54 Methyl tert-butyl ether ND 34 5.7 ug/m3 01/14/17 05:41 1.54 m-Xylene & p-Xylene 33 32 4.9 ug/m3 01/14/17 05:41 1.54 TestAmerica Knoxville Page 25 of 42 1/17/2017 Client Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria TestAmerica Job ID: 140-6789-1 Client Sample ID: SG-6 Lab Sample ID: 140-6789-6 Date Collected: 01/10/17 12:40 Matrix: Air Date Received: 01/12/17 14:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte Result Qualifier RL MDL Unit Naphthalene 4.9 J 24 4.4 ug/m3 o-Xylene 12 8.1 2.5 ug/m3 Styrene ND 8.0 2.3 ug/m3 1,1,2,2-Tetrachloroethane ND 13 3.9 ug/m3 Tetrachloroethene ND 13 2.5 ug/m3 Tetrahydrofuran 19 J 140 1.7 ug/m3 Toluene 21 7.0 4.2 ug/m3 trans-1,2-Dichloroethene ND 7.4 1.9 ug/m3 trans- 1,3-Dichloropropene ND 8.5 2.0 ug/m3 1,2,4-Trichlorobenzene ND 140 6.8 ug/m3 1,1,1-Trichloroethane ND 10 1.5 ug/m3 1,1,2-Trichloroethane ND 10 2.8 ug/m3 Trichloroethene ND 10 1.8 ug/m3 TrichlorofIuoromethane 1.3 J 10 1.3 ug/m3 1,1,2-Trichloro-1,2,2-trifIuoroetha 12 J 14 2.2 ug/m3 ne 1,2,4-Trimethylbenzene 24 9.2 2.9 ug/m3 1,3,5-Trimethylbenzene 4.5 J 9.2 3.0 ug/m3 Vinyl acetate ND 160 4.6 ug/m3 Vinyl bromide ND 8.2 1.4 ug/m3 Vinyl chloride ND 4.8 1.7 ug/m3 D Prepared Analyzed 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 01/14/17 05:41 Dil Fac 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 1.54 0 TestAmerica Knoxville Page 26 of 42 1/17/2017 Default Detection Limits Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Method: TO-15 - Volatile Organic Compounds in Ambient Air FAnalyte RL MDL Units Method 1,1,1-Trichloroethane 0.20 0.030 ppb v/v TO-15 1,1,1-Trichloroethane 1.1 0.16 ug/m3 TO-15 1,1,2,2-Tetrachloroethane 0.20 0.061 ppb v/v TO-15 1,1,2,2-Tetrachloroethane 1.4 0.42 ug/m3 TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane 0.20 0.031 ppb v/v TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane 1.5 0.24 ug/m3 TO-15 1,1,2-Trichloroethane 0.20 0.054 ppb v/v TO-15 1,1,2-Trichloroethane 1.1 0.29 ug/m3 TO-15 1,1-Dichloroethane 0.20 0.026 ppb v/v TO-15 1,1-Dichloroethane 0.81 0.11 ug/m3 TO-15 1,1-Dichloroethene 0.20 0.034 ppb v/v TO-15 1,1-Dichloroethene 0.79 0.13 ug/m3 TO-15 1,2,4-Trichlorobenzene 2.0 0.098 ppb v/v TO-15 1,2,4-Trichlorobenzene 15 0.73 ug/m3 TO-15 1,2,4-Trimethylbenzene 0.20 0.063 ppb v/v TO-15 1,2,4-Trimethylbenzene 0.98 0.31 ug/m3 TO-15 1,2-Dibromoethane (EDB) 0.20 0.044 ppb v/v TO-15 1,2-Dibromoethane (EDB) 1.5 0.34 ug/m3 TO-15 1,2-Dichloro-1,1,2,2-tetrafluoroethane 0.20 0.032 ppb v/v TO-15 1,2-Dichloro-1,1,2,2-tetrafluoroethane 1.4 0.22 ug/m3 TO-15 1,2-Dichlorobenzene 0.20 0.070 ppb v/v TO-15 1,2-Dichlorobenzene 1.2 0.42 ug/m3 TO-15 1,2-Dichloroethane 0.20 0.047 ppb v/v TO-15 1,2-Dichloroethane 0.81 0.19 ug/m3 TO-15 1,2-Dichloropropane 0.20 0.052 ppb v/v TO-15 1,2-Dichloropropane 0.92 0.24 ug/m3 TO-15 1,3,5-Trimethylbenzene 0.20 0.065 ppb v/v TO-15 1,3,5-Trimethylbenzene 0.98 0.32 ug/m3 TO-15 1,3-Dichlorobenzene 0.20 0.065 ppb v/v TO-15 1,3-Dichlorobenzene 1.2 0.39 ug/m3 TO-15 1,4-Dichlorobenzene 0.20 0.064 ppb v/v TO-15 1,4-Dichlorobenzene 1.2 0.38 ug/m3 TO-15 1,4-Dioxane 5.0 0.080 ppb v/v TO-15 1,4-Dioxane 18 0.29 ug/m3 TO-15 2-Butanone (MEK) 1.0 0.20 ppb v/v TO-15 2-Butanone (MEK) 2.9 0.59 ug/m3 TO-15 4-Methyl-2-pentanone (MIBK) 0.50 0.045 ppb v/v TO-15 4-Methyl-2-pentanone (MIBK) 2.0 0.18 ug/m3 TO-15 Acetone 5.0 1.4 ppb v/v TO-15 Acetone 12 3.3 ug/m3 TO-15 Benzene 0.20 0.056 ppb v/v TO-15 Benzene 0.64 0.18 ug/m3 TO-15 Benzyl chloride 0.80 0.078 ppb v/v TO-15 Benzyl chloride 4.1 0.40 ug/m3 TO-15 Bromodichloromethane 0.20 0.044 ppb v/v TO-15 Bromodichloromethane 1.3 0.29 ug/m3 TO-15 Bromoform 0.20 0.048 ppb v/v TO-15 Bromoform 2.1 0.50 ug/m3 TO-15 Bromomethane 0.20 0.032 ppb v/v TO-15 Bromomethane 0.78 0.12 ug/m3 TO-15 Carbon disulfide 0.50 0.031 ppb v/v TO-15 Carbon disulfide 1.6 0.097 ug/m3 TO-15 TestAmerica Knoxville Page 27 of 42 1/17/2017 Default Detection Limits Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) TestAmerica Job ID: 140-6789-1 Analyte RL MDL Units Method Carbon tetrachloride 0.20 0.038 ppb v/v TO-15 Carbon tetrachloride 1.3 0.24 ug/m3 TO-15 Chlorobenzene 0.20 0.049 ppb v/v TO-15 Chlorobenzene 0.92 0.23 ug/m3 TO-15 Chloroethane 0.80 0.035 ppb v/v TO-15 Chloroethane 2.1 0.092 ug/m3 TO-15 Chloroform 0.20 0.038 ppb v/v TO-15 Chloroform 0.98 0.19 ug/m3 TO-15 Chloromethane 0.50 0.16 ppb v/v TO-15 Chloromethane 1.0 0.33 ug/m3 TO-15 cis-1,2-Dichloroethene 0.20 0.060 ppb v/v TO-15 cis-1,2-Dichloroethene 0.79 0.24 ug/m3 TO-15 cis-1,3-Dichloropropene 0.20 0.074 ppb v/v TO-15 cis-1,3-Dichloropropene 0.91 0.34 ug/m3 TO-15 Cyclohexane 0.50 0.040 ppb v/v TO-15 Cyclohexane 1.7 0.14 ug/m3 TO-15 Dibromochloromethane 0.20 0.042 ppb v/v TO-15 Dibromochloromethane 1.7 0.36 ug/m3 TO-15 Dichlorodifluoromethane 0.50 0.068 ppb v/v TO-15 Dichlorodifluoromethane 2.5 0.34 ug/m3 TO-15 Ethylbenzene 0.20 0.068 ppb v/v TO-15 Ethylbenzene 0.87 0.30 ug/m3 TO-15 Hexachlorobutadiene 0.20 0.078 ppb v/v TO-15 Hexachlorobutadiene 2.1 0.83 ug/m3 TO-15 Hexane 0.80 0.032 ppb v/v TO-15 Hexane 2.8 0.11 ug/m3 TO-15 Isopropyl alcohol 5.0 0.094 ppb v/v TO-15 Isopropyl alcohol 12 0.23 ug/m3 TO-15 Isopropylbenzene 0.80 0.060 ppb v/v TO-15 Isopropylbenzene 3.9 0.29 ug/m3 TO-15 Methyl tert-butyl ether 1.0 0.17 ppb v/v TO-15 Methyl tert-butyl ether 3.6 0.61 ug/m3 TO-15 Methylene Chloride 0.50 0.13 ppb v/v TO-15 Methylene Chloride 1.7 0.45 ug/m3 TO-15 m-Xylene & p-Xylene 0.80 0.12 ppb v/v TO-15 m-Xylene & p-Xylene 3.5 0.52 ug/m3 TO-15 Naphthalene 0.50 0.090 ppb v/v TO-15 Naphthalene 2.6 0.47 ug/m3 TO-15 o-Xylene 0.20 0.061 ppb v/v TO-15 o-Xylene 0.87 0.26 ug/m3 TO-15 Styrene 0.20 0.058 ppb v/v TO-15 Styrene 0.85 0.25 ug/m3 TO-15 Tetrachloroethene 0.20 0.040 ppb v/v TO-15 Tetrachloroethene 1.4 0.27 ug/m3 TO-15 Tetrahydrofuran 5.0 0.063 ppb v/v TO-15 Tetrahydrofuran 15 0.19 ug/m3 TO-15 Toluene 0.20 0.12 ppb v/v TO-15 Toluene 0.75 0.45 ug/m3 TO-15 trans- 1,2-Dichloroethene 0.20 0.050 ppb v/v TO-15 trans- 1,2-Dichloroethene 0.79 0.20 ug/m3 TO-15 trans- 1,3-Dichloropropene 0.20 0.048 ppb v/v TO-15 trans- 1,3-Dichloropropene 0.91 0.22 ug/m3 TO-15 TestAmerica Knoxville Page 28 of 42 1/17/2017 Default Detection Limits Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Analyte RL MDL Units Method Trichloroethene 0.20 0.036 ppb v/v TO-15 Trichloroethene 1.1 0.19 ug/m3 TO-15 Trichlorofluoromethane 0.20 0.024 ppb v/v TO-15 Trichlorofluoromethane 1.1 0.13 ug/m3 TO-15 Vinyl acetate 5.0 0.14 ppb v/v TO-15 Vinyl acetate 18 0.49 ug/m3 TO-15 Vinyl bromide 0.20 0.035 ppb v/v TO-15 Vinyl bromide 0.87 0.15 ug/m3 TO-15 Vinyl chloride 0.20 0.071 ppb v/v TO-15 Vinyl chloride 0.51 0.18 ug/m3 TO-15 TestAmerica Knoxville Page 29 of 42 1/17/2017 QC Sample Results C Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Method: TO-15 - Volatile Organic Compounds in Ambient Air Lab Sample ID: MB 140-7733/21 Client Sample ID: Method Blank Matrix: Air Prep Type: Total/NA Analysis Batch: 7733 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 5.0 1.4 ppb v/v 01/14/17 01:57 1 Benzene ND 0.20 0.056 ppb v/v 01/14/17 01:57 1 Benzyl chloride ND 0.80 0.078 ppb v/v 01/14/17 01:57 1 Bromodichloromethane ND 0.20 0.044 ppb v/v 01/14/17 01:57 1 Bromoform ND 0.20 0.048 ppb v/v 01/14/17 01:57 1 • Bromomethane ND 0.20 0.032 ppb v/v 01/14/17 01:57 1 2-Butanone (MEK) ND 1.0 0.20 ppb v/v 01/14/17 01:57 1 Carbon disulfide ND 0.50 0.031 ppb v/v 01/14/17 01:57 1 Carbon tetrachloride ND 0.20 0.038 ppb v/v 01/14/17 01:57 1 Chlorobenzene ND 0.20 0.049 ppb v/v 01/14/17 01:57 1 Chloroethane ND 0.80 0.035 ppb v/v 01/14/17 01:57 1 Chloroform ND 0.20 0.038 ppb v/v 01/14/17 01:57 1 Chloromethane ND 0.50 0.16 ppb v/v 01/14/17 01:57 1 cis-1,2-Dichloroethene ND 0.20 0.060 ppb v/v 01/14/17 01:57 1 cis-1,3-Dichloropropene ND 0.20 0.074 ppb v/v 01/14/17 01:57 1 Cyclohexane ND 0.50 0.040 ppb v/v 01/14/17 01:57 1 Dibromochloromethane ND 0.20 0.042 ppb v/v 01/14/17 01:57 1 1,2-Dibromoethane (EDB) ND 0.20 0.044 ppb v/v 01/14/17 01:57 1 1,2-Dichlorobenzene ND 0.20 0.070 ppb v/v 01/14/17 01:57 1 1,3-Dichlorobenzene ND 0.20 0.065 ppb v/v 01/14/17 01:57 1 1,4-Dichlorobenzene ND 0.20 0.064 ppb v/v 01/14/17 01:57 1 Dichlorodifluoromethane ND 0.50 0.068 ppb v/v 01/14/17 01:57 1 1,1-Dichloroethane ND 0.20 0.026 ppb v/v 01/14/17 01:57 1 1,2-Dichloroethane ND 0.20 0.047 ppb v/v 01/14/17 01:57 1 1,1-Dichloroethene ND 0.20 0.034 ppb v/v 01/14/17 01:57 1 1,2-Dichloropropane ND 0.20 0.052 ppb v/v 01/14/17 01:57 1 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 0.20 0.032 ppb v/v 01/14/17 01:57 1 1,4-Dioxane ND 5.0 0.080 ppb v/v 01/14/17 01:57 1 Ethylbenzene ND 0.20 0.068 ppb v/v 01/14/17 01:57 1 Hexachlorobutadiene ND 0.20 0.078 ppb v/v 01/14/17 01:57 1 Hexane ND 0.80 0.032 ppb v/v 01/14/17 01:57 1 Isopropyl alcohol ND 5.0 0.094 ppb v/v 01/14/17 01:57 1 Isopropylbenzene ND 0.80 0.060 ppb v/v 01/14/17 01:57 1 Methylene Chloride 0.170 J 0.50 0.13 ppb v/v 01/14/17 01:57 1 4-Methyl-2-pentanone (MIBK) ND 0.50 0.045 ppb v/v 01/14/17 01:57 1 Methyl tert-butyl ether ND 1.0 0.17 ppb v/v 01/14/17 01:57 1 m-Xylene & p-Xylene ND 0.80 0.12 ppb v/v 01/14/17 01:57 1 Naphthalene ND 0.50 0.090 ppb v/v 01/14/17 01:57 1 o-Xylene ND 0.20 0.061 ppb v/v 01/14/17 01:57 1 Styrene ND 0.20 0.058 ppb v/v 01/14/17 01:57 1 1,1,2,2-Tetrachloroethane ND 0.20 0.061 ppb v/v 01/14/17 01:57 1 Tetrachloroethene ND 0.20 0.040 ppb v/v 01/14/17 01:57 1 Tetrahydrofuran ND 5.0 0.063 ppb v/v 01/14/17 01:57 1 Toluene ND 0.20 0.12 ppb v/v 01/14/17 01:57 1 trans- 1,2-Dichloroethene ND 0.20 0.050 ppb v/v 01/14/17 01:57 1 trans- 1,3-Dichloropropene ND 0.20 0.048 ppb v/v 01/14/17 01:57 1 1,2,4-Trichoorobenzene ND 2.0 0.098 ppb v/v 01/14/17 01:57 1 1,1, 1 -Trichloroethane ND 0.20 0.030 ppb v/v 01/14/17 01:57 1 TestAmerica Knoxville Page 30 of 42 1/17/2017 QC Sample Results C Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Lab Sample ID: MB 140-7733/21 Client Sample ID: Method Blank Matrix: Air Prep Type: Total/NA Analysis Batch: 7733 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,2-Trichloroethane ND 0.20 0.054 ppb v/v 01/14/17 01:57 1 Trichloroethene ND 0.20 0.036 ppb v/v 01/14/17 01:57 1 Trichlorofluoromethane ND 0.20 0.024 ppb v/v 01/14/17 01:57 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.20 0.031 ppb v/v 01/14/17 01:57 1 1,2,4-Trimethylbenzene ND 0.20 0.063 ppb v/v 01/14/17 01:57 1 1,3,5-Trimethylbenzene ND 0.20 0.065 ppb v/v 01/14/17 01:57 1 Vinyl acetate ND 5.0 0.14 ppb v/v 01/14/17 01:57 1 Vinyl bromide ND 0.20 0.035 ppb v/v 01/14/17 01:57 1 Vinyl chloride ND 0.20 0.071 ppb v/v 01/14/17 01:57 1 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 12 3.3 ug/m3 01/14/17 01:57 1 Benzene ND 0.64 0.18 ug/m3 01/14/17 01:57 1 Benzyl chloride ND 4.1 0.40 ug/m3 01/14/17 01:57 1 Bromodichloromethane ND 1.3 0.29 ug/m3 01/14/17 01:57 1 Bromoform ND 2.1 0.50 ug/m3 01/14/17 01:57 1 Bromomethane ND 0.78 0.12 ug/m3 01/14/17 01:57 1 2-Butanone (MEK) ND 2.9 0.59 ug/m3 01/14/17 01:57 1 Carbon disulfide ND 1.6 0.097 ug/m3 01/14/17 01:57 1 Carbon tetrachloride ND 1.3 0.24 ug/m3 01/14/17 01:57 1 Chlorobenzene ND 0.92 0.23 ug/m3 01/14/17 01:57 1 Chloroethane ND 2.1 0.092 ug/m3 01/14/17 01:57 1 Chloroform ND 0.98 0.19 ug/m3 01/14/17 01:57 1 Chloromethane ND 1.0 0.33 ug/m3 01/14/17 01:57 1 cis-1,2-Dichloroethene ND 0.79 0.24 ug/m3 01/14/17 01:57 1 cis-1,3-Dichloropropene ND 0.91 0.34 ug/m3 01/14/17 01:57 1 Cyclohexane ND 1.7 0.14 ug/m3 01/14/17 01:57 1 Dibromochloromethane ND 1.7 0.36 ug/m3 01/14/17 01:57 1 1,2-Dibromoethane (EDB) ND 1.5 0.34 ug/m3 01/14/17 01:57 1 1,2-Dichlorobenzene ND 1.2 0.42 ug/m3 01/14/17 01:57 1 1,3-Dichlorobenzene ND 1.2 0.39 ug/m3 01/14/17 01:57 1 1,4-Dichlorobenzene ND 1.2 0.38 ug/m3 01/14/17 01:57 1 Dichlorodifluoromethane ND 2.5 0.34 ug/m3 01/14/17 01:57 1 1,1-Dichloroethane ND 0.81 0.11 ug/m3 01/14/17 01:57 1 1,2-Dichloroethane ND 0.81 0.19 ug/m3 01/14/17 01:57 1 1,1-Dichloroethene ND 0.79 0.13 ug/m3 01/14/17 01:57 1 1,2-Dichloropropane ND 0.92 0.24 ug/m3 01/14/17 01:57 1 1,2-Dichloro-1,1,2,2-tetrafluoroethane ND 1.4 0.22 ug/m3 01/14/17 01:57 1 1,4-Dioxane ND 18 0.29 ug/m3 01/14/17 01:57 1 Ethylbenzene ND 0.87 0.30 ug/m3 01/14/17 01:57 1 Hexachlorobutadiene ND 2.1 0.83 ug/m3 01/14/17 01:57 1 Hexane ND 2.8 0.11 ug/m3 01/14/17 01:57 1 Isopropyl alcohol ND 12 0.23 ug/m3 01/14/17 01:57 1 Isopropylbenzene ND 3.9 0.29 ug/m3 01/14/17 01:57 1 Methylene Chloride 0.591 J 1.7 0.45 ug/m3 01/14/17 01:57 1 4-Methyl-2-pentanone (MIBK) ND 2.0 0.18 ug/m3 01/14/17 01:57 1 Methyl tert-butyl ether ND 3.6 0.61 ug/m3 01/14/17 01:57 1 m-Xylene & p-Xylene ND 3.5 0.52 ug/m3 01/14/17 01:57 1 TestAmerica Knoxville Page 31 of 42 1/17/2017 QC Sample Results Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Lab Sample ID: MB 140-7733/21 Client Sample ID: Method Blank Matrix: Air Prep Type: Total/NA Analysis Batch: 7733 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Naphthalene ND 2.6 0.47 ug/m3 01/14/17 01:57 1 o-Xylene ND 0.87 0.26 ug/m3 01/14/17 01:57 1 Styrene ND 0.85 0.25 ug/m3 01/14/17 01:57 1 1,1,2,2-Tetrachloroethane ND 1.4 0.42 ug/m3 01/14/17 01:57 1 Tetrachloroethene ND 1.4 0.27 ug/m3 01/14/17 01:57 1 Tetrahydrofuran ND 15 0.19 ug/m3 01/14/17 01:57 1 Toluene ND 0.75 0.45 ug/m3 01/14/17 01:57 1 trans- 1,2-Dichloroethene ND 0.79 0.20 ug/m3 01/14/17 01:57 1 trans- 1,3-Dichloropropene ND 0.91 0.22 ug/m3 01/14/17 01:57 1 1,2,4-Trichlorobenzene ND 15 0.73 ug/m3 01/14/17 01:57 1 1,1,1-Trichloroethane ND 1.1 0.16 ug/m3 01/14/17 01:57 1 1,1,2-Trichloroethane ND 1.1 0.29 ug/m3 01/14/17 01:57 1 Trichloroethene ND 1.1 0.19 ug/m3 01/14/17 01:57 1 Trichlorofluoromethane ND 1.1 0.13 ug/m3 01/14/17 01:57 1 1,1,2-Trichloro-1,2,2-trifluoroethane ND 1.5 0.24 ug/m3 01/14/17 01:57 1 1,2,4-Trimethylbenzene ND 0.98 0.31 ug/m3 01/14/17 01:57 1 1,3,5-Trimethylbenzene ND 0.98 0.32 ug/m3 01/14/17 01:57 1 Vinyl acetate ND 18 0.49 ug/m3 01/14/17 01:57 1 Vinyl bromide ND 0.87 0.15 ug/m3 01/14/17 01:57 1 Vinyl chloride ND 0.51 0.18 ug/m3 01/14/17 01:57 1 Lab Sample ID: LCS 140-7733/1002 Client Sample ID: Lab Control Sample Matrix: Air Prep Type: Total/NA Analysis Batch: 7733 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Acetone 6.00 5.88 ppb v/v 98 60 -140 Benzene 2.00 1.92 ppb v/v 96 70 -130 Benzyl chloride 2.00 2.31 ppb v/v 115 70 -130 Bromodichloromethane 2.00 1.82 ppb v/v 91 70 -130 Bromoform 2.00 1.82 ppb v/v 91 60 -140 Bromomethane 2.00 1.89 ppb v/v 94 70 -130 2-Butanone (MEK) 2.00 1.98 ppb v/v 99 60 -140 Carbon disulfide 2.00 1.84 ppb v/v 92 70 -130 Carbon tetrachloride 2.00 1.92 ppb v/v 96 70 -130 Chlorobenzene 2.00 1.97 ppb v/v 98 70 -130 Chloroethane 2.00 1.89 ppb v/v 94 70 -130 Chloroform 2.00 1.89 ppb v/v 95 70 -130 Chloromethane 2.00 1.96 ppb v/v 98 60 -140 cis-1,2-Dichloroethene 2.00 1.91 ppb v/v 95 70 -130 cis-1,3-Dichloropropene 2.00 1.89 ppb v/v 95 70 -130 Cyclohexane 2.00 1.68 ppb v/v 84 70 -130 Dibromochloromethane 2.00 1.95 ppb v/v 97 70 -130 1,2-Dibromoethane (EDB) 2.00 1.92 ppb v/v 96 70-130 1,2-Dichlorobenzene 2.00 2.08 ppb v/v 104 70 -130 1,3-Dichlorobenzene 2.00 2.07 ppb v/v 104 70 -130 1,4-Dichlorobenzene 2.00 2.34 ppb v/v 117 70 -130 Dichlorodifluoromethane 2.00 1.82 ppb v/v 91 60 -140 0 TestAmerica Knoxville Page 32 of 42 1/17/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Lab Sample ID: LCS 140-7733/1002 Matrix: Air Analysis Batch: 7733 Analyte 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene 1,2-Dichloropropane 1,2-Dichloro-1,1,2,2-tetrafluoroet hane 1,4-Dioxane Ethylbenzene Hexachlorobutadiene Hexane Isopropyl alcohol Isopropylbenzene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether m-Xylene & p-Xylene Naphthalene o-Xylene Styrene 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene trans- 1,2-Dichloroethene trans- 1,3-Dichloropropene 1,2,4-Trichlorobenzene 1,1,1-Trich loroethane 1,1,2-Trich loroethane Trichloroethene Trichlorofluoromethane 1,1,2-Trich loro-1,2,2-trifluoroetha ne 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl bromide Vinyl chloride Analyte Acetone Benzene Benzyl chloride Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene TestAmerica Job ID: 140-6789-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 2.00 1.93 ppb v/v 97 70 -130 2.00 1.86 ppb v/v 93 70 -130 2.00 1.87 ppb v/v 94 70 -130 2.00 2.00 ppb v/v 100 70 -130 2.00 2.21 ppb v/v 110 60 -140 2.00 1.80 J ppb v/v 90 60 -140 2.00 1.95 ppb v/v 97 70 -130 2.00 1.91 ppb v/v 95 60 -140 2.00 1.87 ppb v/v 94 70 -130 6.00 4.92 ppb v/v 82 60 -140 2.00 2.03 ppb v/v 102 70 -130 2.00 1.79 ppb v/v 90 70 -130 2.00 1.94 ppb v/v 97 60 -140 2.00 1.87 ppb v/v 93 60 -140 4.00 4.05 ppb v/v 101 70 -130 2.00 2.02 ppb v/v 101 60 -140 2.00 1.95 ppb v/v 97 70 -130 2.00 2.04 ppb v/v 102 70 -130 2.00 1.95 ppb v/v 97 70 -130 2.00 1.87 ppb v/v 93 70 -130 2.00 2.05 ppb v/v 103 60 -140 2.00 2.00 ppb v/v 100 70 -130 2.00 1.85 ppb v/v 92 70 -130 2.00 1.83 ppb v/v 91 70 -130 2.00 2.66 ppb v/v 133 60 -140 2.00 1.89 ppb v/v 94 70 -130 2.00 1.90 ppb v/v 95 70 -130 2.00 1.94 ppb v/v 97 70 -130 2.00 1.85 ppb v/v 92 60 -140 2.00 1.89 ppb v/v 95 70 -130 2.00 2.01 ppb v/v 101 70 -130 2.00 2.06 ppb v/v 103 70 -130 2.00 2.12 ppb v/v 106 60 -140 2.00 1.95 ppb v/v 97 60 -140 2.00 1.93 ppb v/v 97 70 -130 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 14 14.0 ug/m3 98 60 -140 6.4 6.13 ug/m3 96 70 -130 10 12.0 ug/m3 115 70 -130 13 12.2 ug/m3 91 70 -130 21 18.8 ug/m3 91 60 -140 7.8 7.34 ug/m3 94 70 -130 5.9 5.85 ug/m3 99 60 -140 6.2 5.73 ug/m3 92 70 -130 13 12.1 ug/m3 96 70 -130 9.2 9.06 ug/m3 98 70 -130 0 TestAmerica Knoxville Page 33 of 42 1/17/2017 QC Sample Results Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Lab Sample ID: LCS 140-7733/1002 Matrix: Air Analysis Batch: 7733 Analyte Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Cyclohexane Dibromochloromethane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene 1,2-Dichloropropane 1,2-Dichloro-1,1,2,2-tetrafluoroet hane 1,4-Dioxane Ethylbenzene Hexachlorobutadiene Hexane Isopropyl alcohol Isopropylbenzene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether m-Xylene & p-Xylene Naphthalene o-Xylene Styrene 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene trans- 1,2-Dichloroethene trans- 1,3-Dichloropropene 1,2,4-Trichoorobenzene 1,1,1-Trich loroethane 1,1,2-Trich loroethane Trichloroethene Trichlorofluoromethane 1,1,2-Trich loro-1,2,2-trifluoroetha ne 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl bromide Vinyl chloride TestAmerica Job ID: 140-6789-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits 5.3 4.98 ug/m3 94 70 -130 9.8 9.24 ug/m3 95 70 -130 4.1 4.05 ug/m3 98 60 -140 7.9 7.56 ug/m3 95 70 -130 9.1 8.59 ug/m3 95 70 -130 6.9 5.77 ug/m3 84 70 -130 17 16.6 ug/m3 97 70 -130 15 14.7 ug/m3 96 70 -130 12 12.5 ug/m3 104 70 -130 12 12.5 ug/m3 104 70 -130 12 14.1 ug/m3 117 70 -130 9.9 9.01 ug/m3 91 60 -140 8.1 7.82 ug/m3 97 70 -130 8.1 7.54 ug/m3 93 70 -130 7.9 7.43 ug/m3 94 70 -130 9.2 9.24 ug/m3 100 70 -130 14 15.4 ug/m3 110 60 -140 7.2 6.50 J ug/m3 90 60 -140 8.7 8.47 ug/m3 97 70 -130 21 20.4 ug/m3 95 60 -140 7.1 6.60 ug/m3 94 70 -130 15 12.1 ug/m3 82 60 -140 9.8 9.99 ug/m3 102 70 -130 7.0 6.23 ug/m3 90 70 -130 8.2 7.95 ug/m3 97 60 -140 7.2 6.74 ug/m3 93 60 -140 17 17.6 ug/m3 101 70 -130 10 10.6 ug/m3 101 60 -140 8.7 8.45 ug/m3 97 70 -130 8.5 8.68 ug/m3 102 70 -130 14 13.4 ug/m3 97 70 -130 14 12.7 ug/m3 93 70 -130 5.9 6.06 ug/m3 103 60 -140 7.5 7.52 ug/m3 100 70 -130 7.9 7.33 ug/m3 92 70 -130 9.1 8.29 ug/m3 91 70 -130 15 19.8 ug/m3 133 60 -140 11 10.3 ug/m3 94 70 -130 11 10.4 ug/m3 95 70 -130 11 10.4 ug/m3 97 70 -130 11 10.4 ug/m3 92 60 -140 15 14.5 ug/m3 95 70 -130 9.8 9.89 ug/m3 101 70 -130 9.8 10.1 ug/m3 103 70 -130 7.0 7.47 ug/m3 106 60 -140 8.8 8.53 ug/m3 97 60 -140 5.1 4.94 ug/m3 97 70 -130 0 Page 34 of 42 TestAmerica Knoxville 1/17/2017 QC Association Summary Client: CBRE, Inc. Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Air - GC/MS VOA Analysis Batch: 7733 Lab Sample ID Client Sample ID 140-6789-1 SG-1 140-6789-2 SG-2 140-6789-3 SG-3 140-6789-4 SG-4 140-6789-5 SG-5 140-6789-6 SG-6 MB 140-7733/21 Method Blank LCS 140-7733/1002 Lab Control Sample TestAmerica Job ID: 140-6789-1 Prep Type Matrix Method Prep Batch Total/NA Air TO-15 Total/NA Air TO-15 Total/NA Air TO-15 Total/NA Air TO-15 Total/NA Air TO-15 Total/NA Air TO-15 Total/NA Air TO-15 Total/NA Air TO-15 0 Page 35 of 42 TestAmerica Knoxville 1/17/2017 Lab Chronicle C Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Client Sample ID: SG-1 Lab Sample ID: 140-6789-1 Date Collected: 01/10/17 12:15 Matrix: Air Date Received: 01/12/17 14:20 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis TO-15 1.53 32 mL 500 mL 7733 01/14/17 07:11 HMT TAL KNX Instrument ID: MJ Client Sample ID: SG-2 Lab Sample ID: 140-6789-2 Date Collected: 01/10/17 12:20 Matrix: Air C Date Received: 01/12/17 14:20 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis TO-15 1.56 32 mL 500 mL 7733 01/14/17 02:42 HMT TAL KNX m Instrument ID: MJ Client Sample ID: SG-3 Lab Sample ID: 140-6789-3 Date Collected: 01/10/17 12:25 Matrix: Air Date Received: 01/12/17 14:20 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis TO-15 1.56 32 mL 500 mL 7733 01/14/17 03:27 HMT TAL KNX Instrument ID: MJ Client Sample ID: SG-4 Lab Sample ID: 140-6789-4 Date Collected: 01/10/17 12:30 Matrix: Air Date Received: 01/12/17 14:20 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis TO-15 1 31 mL 500 mL 7733 01/14/17 04:12 HMT TAL KNX Instrument ID: MJ Client Sample ID: SG-5 Lab Sample ID: 140-6789-5 Date Collected: 01/10/17 12:35 Matrix: Air Date Received: 01/12/17 14:20 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis TO-15 1.58 21 mL 500 mL 7733 01/14/17 04:57 HMT TAL KNX Instrument ID: MJ Client Sample ID: SG-6 Lab Sample ID: 140-6789-6 Date Collected: 01/10/17 12:40 Matrix: Air Date Received: 01/12/17 14:20 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis TO-15 1.54 33 mL 500 mL 7733 01/14/17 05:41 HMT TAL KNX Instrument ID: MJ TestAmerica Knoxville Page 36 of 42 1/17/2017 Lab Chronicle Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Client Sample ID: Method Blank Lab Sample ID: MB 140-7733/21 Date Collected: N/A Matrix: Air Date Received: N/A Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis TO-15 1 200 mL _666-mL 7733 01/14/17 01:57 HMT TAL KNX Instrument ID: MJ Client Sample ID: Lab Control Sample Lab Sample ID: LCS 140-7733/1002 Date Collected: N/A Matrix: Air Date Received: N/A Batch Batch DII Initial Final Batch Prepared C Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis TO-15 1 500 mL 500 mL 7733 01/13/17 10:35 HMT TAL KNX m Instrument ID: MJ Laboratory References: TAL KNX = TestAmerica Knoxville, 5815 Middlebrook Pike, Knoxville, TN 37921, TEL (865)291-3000 F TestAmerica Knoxville Page 37 of 42 1/17/2017 Method Summary Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Method Method Description Protocol Laboratory TO-15 Volatile Organic Compounds in Ambient Air EPA TAL KNX Protocol References: EPA = US Environmental Protection Agency Laboratory References: TAL KNX = TestAmerica Knoxville, 5815 Middlebrook Pike, Knoxville, TN 37921, TEL (865)291-3000 TestAmerica Knoxville Page 38 of 42 1/17/2017 Sample Summary Client: CBRE, Inc. TestAmerica Job ID: 140-6789-1 Project/Site: E. Chapel Hill -Nelson Hwy, Research Tria Lab Sample ID Client Sample ID Matrix Collected Received 140-6789-1 SG-1 Air 01/10/1712:15 01/12/1714:20 140-6789-2 SG-2 Air 01/10/1712:20 01/12/1714:20 140-6789-3 SG-3 Air 01/10/1712:25 01/12/1714:20 140-6789-4 SG-4 Air 01/10/1712:30 01/12/1714:20 140-6789-5 SG-5 Air 01/10/1712:35 01/12/1714:20 140-6789-6 SG-6 Air 01/10/1712:40 01/12/1714:20 TestAmerica Knoxville Page 39 of 42 1/17/2017 QJ � Lij O �W Li 0 N 4- •�r i N a E co •E m tU M, Cl) 00 00 u; 00 x M o x o �zN Y 00 c oQ ° I— LO x a (uolloas salou ul /gpeds aseald) je4ao SLD IMPus'I 1 jlV auelgLuV U VO v V HIV Joopul ad�fl a/dwes o p r G' (uolloas salou ul./qloads aseald) J84)0 91?66-a W1SV 09Z Vd3 0 OE Vd3 6 Vol 1 V c 4 ( m Gl w O o� N e p ` k fn � h \® \ � `. \ ® \ N 0 `p t 2A AtOi .O A - ° u v y a y� p ` V N, ` �„ O ">LL_ p e 4) c V K 6 � m E 0 ,V=I C tm V U,LL- V < V < o V � 1 Q ne \e \VC c \�%;,� � a ®a N tM N i ac .f; .f; (0 N E N \. tee, a� V y y c C C d (� N E N E N E_ ai a � r t o ALa in o 0 u 0 110 E V U oa o m E c 6 w aci V cr c a ` y V t i 4 o w 1 a ai c (V�` V � ` �\ ` 9- c n O > N r , �, N U O a iC ,FN, N CL '7 UU QUdt¢i� v� (n U U10) Page 40 of 42 1/17/2017 b d 00 A F � y 0 x� d o !� U CD z Q9 u d eV U CA U o 0 p" 4x A. w q Z q u Z Z OU 8 o eoi w0 w o�� El 0 0 dd'�y oaoo z z���yy 8 � � �u 3.�' 0 i Z .2.2 y C .� ►.i UU z � U Cl o 0 0 000 00 000 0� 0•�da�u•ro�0.l U Utz U 0UUUoUUUvU0 mC%uuu U pq �" ao ❑ ❑❑ ❑ U ❑W ❑ ❑ U ❑ ❑ ❑ ❑ ❑ ❑ U ❑ ❑ ❑ ❑ ❑ ❑ ❑ S") ❑ ❑ ❑ ❑ ❑ Z \ z r• r aoi 7 O Ar, rai 0 a ^O chi w `�••� O O r, U r OR N e0 'ap v� ,ba) G. W r. •Ua) N z �UOU qU a'U ) .0 r• It � N 0 •by A � ? � Z 41) o.�,� �> i.. �, •� c a� 2 a� 'v p o 00 .�4 'I'� �. 'fd L'i G b • • y N 1 y ,� 4-I 1•n '� F Vl � A v „ � „ U i ;, ' r. 3���3 33In 3'Ar;�Uw°w >, r, �d"3H n 033 A� 3 o 4 °+.' E� U 00 N a Page 41 of 42 1 /17/2017 Gauge ID: Date: G5 1/13/2017 TestAmerica Knoxville - Air Canister Initial Pressure Check Analyst Sample ID Asset # Cleaning Job Cert Size (L) Pressure @ Receipt (-in Hg or +psig) Time Comments AFB 140-6789-a-1 10171 6713 B 6 -8.4 1110 1.5 AFB 140-6789-a-2 10265 6713 B 1 6 -9.1 1111 11.3 AFB 140-6789-a-3 10807 6713 B 6 -9.0 1112 1.3 AFB 140-6789-a-4 10829 6713 B 6 1 0 1113 AFB 140-6789-a-5 09777 6713 B 6 -9.1 1114 1.5 AFB 140-6789-a-6 09780 6713 B 6 -8.1 1115 1.8 14 140-6789 MS038 r14, 6/19/15 Page 42 of 42 1/17/2017