15004_Gastonia Poplar_Phase II Report 20110217

S:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-025 National Textile Phase II ESA\Phase II ESA\FDP National Textile Phase II Letter.doc
Via Email and US Mail

February 17, 2011

ForSite Development Partners
5320 Old Pineville Road
Charlotte, NC 28217

Attention: Mr. Houston Roberts

Re: Phase II ESA
National Textiles Facility
1925 West Poplar Street
Gastonia, North Carolina
H&H Job No. FDP-025

Dear Houston:

1.0 Introduction

Hart & Hickman, PC (H&H) is pleased to present this Phase II Environmental Site Assessment
(ESA) report for the former National Textiles facility located at 1925 West Poplar Street in
Gastonia, North Carolina. A site location map is provided as Figure 1 and a site aerial is
provided as Figure 2. Based on the Phase I ESA dated April 4, 2010, the Addendum to the Phase
I ESA letter dated May 13, 2009 (both prepared by Professional Service Industries, Inc), historic
aerial photography, and Sanborn fire insurance maps, H&H identified the following on-site
potential environmental concerns associated with the site:

1. A 10,000-gallon heating oil underground storage tank (UST) was closed in-place in the
central portion of the property in 2002. Soil and groundwater assessment were not
conducted following closure of this UST.

2. A UST of unknown size and contents was reportedly located near the used oil storage
area in the central portion of the site. Based on an interview with site personnel during
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the Phase I ESA, the UST was removed in the early 1990s. Additional details of this
UST are not available.

3. Sanborn maps indicate the presence of a machine shop in the central portion of the site
from prior 1922 to at least 1963. Machine shops at textile facilities were typically the
place where maintenance of large equipment including degreasing took place.

On January 19, 2011, H&H contracted Carolina Soil Investigations, LLC (CSI), a direct push
technology (DPT) contractor, to advance a total of five soil borings and install one temporary
monitoring well to assess soil and groundwater in the vicinity of the areas of concern listed
above. The assessment was conducted to determine if a release to soil or groundwater had
occurred as a result of historic site operations. The methods, results, and conclusions of our
assessment activities are presented in the following sections.

2.0 Soil Assessment

2.1 Sampling Procedures

According to the Phase I ESA and addendum, two USTs were formerly located in the central
portion of the site, including a 10,000-gallon heating oil tank and a UST of unknown size and
contents. The heating oil tank was reportedly closed in place in 2002, and the UST of unknown
contents was removed in the early 1990s. As such, Phase II ESA soil assessment activities were
conducted in the areas of these USTs. Soil borings SB-1, SB-2, and SB-5 where advanced near a
large rectangular cut observed in the asphalt near the oil storage room which was interpreted to
be the location of the former 10,000-gallon heating oil tank. Soil borings SB-3 and SB-4 were
advanced near the inferred location of the former UST of unknown contents. The locations of
borings SB-3 and SB-4 were based on photographs included in the Phase I ESA depicting the
area near the former waste oil storage area (south of the above ground storage tank platform)
where the former UST basin was believed to have been located.
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To screen each location for buried utilities, the initial 5 ft of each boring was advanced using a
decontaminated stainless steel hand auger. Soil borings were then completed from 5 ft to 15 ft
(or refusal) below ground surface (bgs) by DPT methods using a track mounted Geoprobe® rig.
Soil cores were collected at 5-ft intervals with a macro-core sampler lined with acetate sleeves
during the advancement of each soil boring.

Following collection, the soil cores were described for lithologic purposes, inspected for the
presence of staining, and field-screened for the presence of organic vapors with a calibrated
photo-ionization detector (PID). In accordance with our Phase II ESA proposal, two soil samples
were collected for laboratory analysis near the 10,000-gallon heating oil UST and one soil sample
was collected for laboratory analysis near the former UST of unknown contents. Sample
collection depths were based on field screening results. Because there was no field evidence of
impact, sampling locations were biased towards the interval which produced the highest
(although less than 2 part per million) PID response. Soil samples for laboratory analysis were
collected from the 12 ft to 14 ft interval at SB-1 and SB-5, and from the 8 ft to 10 ft interval at
SB-3. Soil boring logs are provided in Appendix A.

Following the collection of the appropriate soil samples, each borehole was properly abandoned
with bentonite pellets to six inches below ground surface. The ground surface was then patched
with asphalt to match the surrounding land surface at each boring location.

2.2 Sample Handling Procedures

Following collection, soil samples were immediately placed in an iced sample cooler. A chain-
of-custody record was then completed which included the sample identification, date collected,
time collected, matrix, sample container information, and requested analyses. At the conclusion
of sampling, the completed chain-of-custody was signed by H&H sampling personnel and
delivered with the samples to the analytical laboratory. Soil samples were submitted to Prism
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Laboratories Inc. (Prism), a North Carolina certified laboratory, for analysis. Soil samples SB-1
(12-14’), SB-3 (8-10’) and SB-5 (12-14’) were submitted to Prism for analysis of total petroleum
hydrocarbons (TPH) as gasoline-range organics (GRO) by EPA Method 5030/8015 and TPH as
diesel-range organics (DRO) by EPA Method 3550/8015. In addition, soil sample SB-3 (8-10’)
was analyzed for volatile organic compounds (VOCs) by EPA Method 8260B as the potential
contents of the former UST in this area were unknown.

3.0 Groundwater Assessment

3.1 Sampling Procedures

Based on a review of historical Sanborn fire insurance maps, a machine shop was formerly
located in the central portion of the site. Maintenance of machinery was a typical activity
conducted at textile machine shops, and the activities may have involved the use of solvents. To
assess the potential for impact from the machine shop, one temporary monitoring well (TMW-1)
was installed downgradient of the former machine shop. The temporary monitoring well was
installed to a total depth of 36 ft bgs where refusal was encountered. Upon encountering refusal,
the drilling rods where removed from the subsurface and a temporary monitoring well was
installed. The well was constructed with one-inch diameter PVC casing from ground surface to
21 ft bgs and one-inch diameter PVC well screen from 21 ft bgs to 36 ft bgs.

Following installation, the temporary monitoring well was developed using a peristaltic pump to
remove sediments from the water column. Upon adequate development, groundwater samples
were collecting from the well using a disposable polyethylene bailer then transferred to
laboratory supplied sample containers.

Once the groundwater samples were collected, the PVC well casing and well screen were
removed from the subsurface, and the borehole was properly abandoned with bentonite pellets to
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six inches below ground surface. The ground surface was then patched with asphalt to match the
surrounding land surface.

3.2 Sample Handling Procedures

Following collection, the groundwater sample was immediately placed in an iced sample cooler.
A chain-of-custody record was then completed which included the sample identification, date
collected, time collected, matrix, sample container information, and requested analyses. At the
conclusion of sampling, the completed chain-of-custody was signed by H&H sampling personnel
and delivered with the samples to the analytical laboratory. The groundwater sample was
submitted to Prism for analysis of VOCs by EPA Method 6200B and semi-volatile organic
compounds (SVOCs) by EPA Method 8270D.

4.0 Assessment Results

Assessment results are summarized below by sample matrix. The laboratory analytical report is
provided in Appendix B.

4.1 Soil Analytical Results

TPH-GRO, TPH-DRO, and VOCs were not detected in the soil samples collected during the
Phase II ESA above laboratory method detection limits. The soil sample results provide no
indication of soil impacts associated with the former USTs at the site.

4.2 Groundwater Analytical Results

The analytical results of the groundwater sample collected from temporary monitoring well
TMW-1 indicated the presence of several chlorinated solvent compounds. Of the compounds
present, only tetrachloroethene (PCE) detected at a concentration of 3.47 µg/l slightly exceeded
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its North Carolina Administrative Code (NCAC) 2L groundwater standard of 0.7 µg/l. Other
chlorinated solvent compounds that were detected at concentrations exceeding the laboratory
method detection limits, but below their respective groundwater standards, were 1,1-
dichloroethane (1,1-DCA), 1,1-dichloroethene (1,1-DCE), 1,1,1-trichloroethane (1,1,1-TCA),
and trichloroethene (TCE). SVOCs were not detected at concentrations above laboratory method
detection limits. Groundwater analytical results are summarized on Table 1.

5.0 Conclusion and Recommendations

H&H assessed three areas of concern to determine if historic site activities resulted in a release to
site soils or groundwater. H&H advanced and screened five soil borings and collected three soil
samples in the vicinity of two former USTs. H&H also installed a temporary monitoring well
and collected one groundwater sample to address a historic machine shop at the property.

Target organic and petroleum-related compounds were not detected above their respective
laboratory method detection limits in the soil samples collected during this Phase II ESA. As
such, there is no evidence of impact associated with the former USTs. However, PCE was
detected in the groundwater sample collected near the former machine shop at a concentration of
3.47 µg/l, which slightly exceeds its groundwater standard of 0.7 µg/l. No other compounds
exceeded their ground water standards.

Based upon the low concentration of PCE detected slightly above its ground water standard, it is
highly unlikely that the North Carolina Department of Environment and Natural Resources
(DENR) would actively pursue further assessment or remediation of the identified impacts.
Nevertheless, if you would like to further reduce the low probability that DENR would actively
pursue further actions associated with the impacts, ForSite Development Partners could enter
into a Brownfields agreement for the site. The Brownfields agreement would provide for State
liability protection from the identified impacts in exchange for making the site safe for
redevelopment. This is usually accomplished by implementing site land use restrictions such as
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agreeing to not use groundwater at the site. It is highly unlikely that any active remediation of
impacts would be required by DENR under the Brownfields agreement.

Thank you for the opportunity to provide environmental consulting services. Please contact us if
you have any questions or require additional information.

Very truly yours,

Hart & Hickman, PC

Steve C. Hart, PG
Principal
Table 1
Summary of Groundwater Analytical Data
National Textiles Facility
Gastonia, North Carolina
H&H Job No. FDP-025
Area of Concern Historic Machine
Shop
Screening
Criteria
Sample ID TMW-1
Sample Date 1/19/2011
Units (µg/l) (µg/l)
VOCs (6200B)
Tetrachloroethene (PCE)3.47 0.7
Trichloroethene (TCE) 1.33 3
1,1-Dichloroethene (1,1-DCE) 1.44 7
1,1,1-Trichloroethane (1,1,1-TCA) 10.3 200
1,1-Dichloroethane (1,1-DCA) 0.860 6
SVOCs (8270D)BRL
Notes:
1) North Carolina Administrative Code 2L Groundwater Standards
Only those compounds detected in at least one sample are shown above
Method number follows parameter in parenthesis
Bold indicates an exceedance of the 2L standard
VOCs = volatile organic compounds
SVOCs = semi-volatile organic compounds
NS = screening criteria not specified
BRL = All compounds below reporting limit
µg/l = micrograms per liter
2L Groundwater
Standards1
S:\AAA-Master Projects\ForSite Development Partners (FDP)\FDP-025 National Textile Phase II ESA\Phase II ESA\Phase II ESA GW Table.xlsm2/17/2011
Table 1 (Page 1 of 1)
Hart & Hickman, PC
TITLE
PROJECT
SITE LOCATION MAP
NATIONAL TEXTILES FACILITY1925 WEST POPLAR STREETGASTONIA, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
01-17-11 0
1FDP-025
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
GASTONIA NORTH, NC 1993
SITE

Appendix A

Soil Boring and
Temporary Monitoring Well Logs
0.7
0.5
0.6
0.5
0.5
0.4
0.7
0.5
Asphalt
Moist, soft, tan brown, silty SAND
Slightly moist, slightly firm , orange, sandy CLAY
Slight moist, firm, tan brown, fine sandy CLAY
Dry, brittle, grey white black, SAPROLITE
Slightly moist, brittle, orange tan, silty fine to coarse SAND
Slighty moist, slightly firm, grey white green, SAPROLITE
Bottom of borehole at 15.0 feet.
0
0
0
0
0
0
0
0
GB
DRAWN BY:JRL
BORING COMPLETED:1/19/11
DRILLING CONTRACTOR:CSI Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / Direct Push
SAMPLING METHOD:DPT Sleeves Sample collected from 12' to 14' bgs forlaboratory analysis TPH-GRO 5030/8015
and TPH-DRO 3350/8015
BORING STARTED:1/19/11
LOGGED BY:JRL
TOTAL DEPTH: 15 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER SB-1
PROJECT:National Textile Facility
JOB NUMBER:FDP-025
LOCATION:Gastonia, NA
BORING LOG - HART HICKMAN.GDT - 1/20/11 15:24 - S:\AAA-MASTER GINT PROJECTS\FDP-025.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
0
5
10
15
0.1
0
0.3
1
0.8
0.5
0.7
0.7
Asphalt
Slightly moist, firm, orange, fine to medium sandy CLAY
Slightly moist, soft, tan white, silty fine to medium SAND
Slightly moist, slightly firm, orange, clayey fine to coarse SAND
Slightly moist, brittle, grey white, SAPROLITE
Bottom of borehole at 15.0 feet.
0
0
0
0
0
0
0
0
DRAWN BY:JRL
BORING COMPLETED:1/19/11
DRILLING CONTRACTOR:CSI Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / Direct Push
SAMPLING METHOD:DPT Sleeves No sample collected
BORING STARTED:1/19/11
LOGGED BY:JRL
TOTAL DEPTH: 15 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER SB-2
PROJECT:National Textile Facility
JOB NUMBER:FDP-025
LOCATION:Gastonia, NA
BORING LOG - HART HICKMAN.GDT - 1/20/11 15:24 - S:\AAA-MASTER GINT PROJECTS\FDP-025.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
0
5
10
15
0.1
0.2
0.2
0.7
1.1
0.7
Asphlat
Slighty moist, soft, brown, silty SAND
Dry, loose, white black green, silty fine to coasre SAND
Slightly moist, firm, orange, fine sandy CLAY
Dry, brittle, white black gray, SAPROLITE
Bottom of borehole at 12.0 feet.
0
0
0
0
0
0
GB
DRAWN BY:JRL
BORING COMPLETED:1/19/11
DRILLING CONTRACTOR:CSI Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / Direct Push
SAMPLING METHOD:DPT Sleeves Sample collected from 8' to 10' bgs forlaboratory analysis TPH-GRO 5030/8015
TPH-DRO 3350/8015, and VOCs 8260.
BORING STARTED:1/19/11
LOGGED BY:JRL
TOTAL DEPTH: 12 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER SB-3
PROJECT:National Textile Facility
JOB NUMBER:FDP-025
LOCATION:Gastonia, NA
BORING LOG - HART HICKMAN.GDT - 1/20/11 15:24 - S:\AAA-MASTER GINT PROJECTS\FDP-025.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
7.5
10.0
12.5
15.0
0.0
2.5
5.0
7.5
10.0
12.5
15.0
0
0.1
0.2
0.1
0.2
0.1
0.1
0.1
Asphalt
Slightly moist, loose, orange tan, clayey fine to medium SAND
Slightly moist, brittle, gray white black, SAPROLITE
Bottom of borehole at 15.0 feet.
0
0
0
0
0
0
0.1
0.1
DRAWN BY:JRL
BORING COMPLETED:1/19/11
DRILLING CONTRACTOR:CSI Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / Direct Push
SAMPLING METHOD:DPT Sleeves No sample collected
BORING STARTED:1/19/11
LOGGED BY:JRL
TOTAL DEPTH: 15 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER SB-4
PROJECT:National Textile Facility
JOB NUMBER:FDP-025
LOCATION:Gastonia, NA
BORING LOG - HART HICKMAN.GDT - 1/20/11 15:24 - S:\AAA-MASTER GINT PROJECTS\FDP-025.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
0
5
10
15
0.1
0.1
0.1
0.1
0.1
0.3
0.1
0.6
Asphlat
Slightly moist, firm, orange, sandy CLAY
Slightly moist, brittle, orqnge tan, clayey fine to medium SAND
Slightly moist, soft, white black gray, fine to medium SAND, with silt
Slightly moist, soft, orange, clay fine to medium SAND
Bottom of borehole at 15.0 feet.
0.1
0.1
0.1
0.1
0.1
0.1
0.1
0.1
GB
DRAWN BY:JRL
BORING COMPLETED:1/19/11
DRILLING CONTRACTOR:CSI Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / Direct Push
SAMPLING METHOD:DPT Sleeves Sample collected from 12' to 14' bgs forlaboratory analysis TPH-GRO 5030/8015
and TPH-DRO 3350/8015
BORING STARTED:1/19/11
LOGGED BY:JRL
TOTAL DEPTH: 15 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER SB-5
PROJECT:National Textile Facility
JOB NUMBER:FDP-025
LOCATION:Gastonia, NA
BORING LOG - HART HICKMAN.GDT - 1/20/11 15:24 - S:\AAA-MASTER GINT PROJECTS\FDP-025.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
0
5
10
15
100
90
90
80
90
80
0.1
0.1
0.3
0.4
0.5
0.4
0.4
0.5
0.4
0.7
0.5
0.6
1
0.5
0.8
0.5
0.6
0.5
Asphalt
Slightly moist, slightly firm, orange, clayey fine to medium SAND
Dry, loose, tan, fine SAND, with silt and relict structure
Dry, loose, white tan green, fine SAND, with silt, small gravels, andsome relict structure
Slightly moist, brittle, white gray green, SAPROLITE, saturated from 35to 35.5'
Bottom of borehole at 36.0 feet.
0.1
0
0.1
0
0.1
0
0
0
0
0
0
0
0
0
0
0
0
0
1" dia PVC
riser
MachineSlottedScreen
DRAWN BY:JRL
BORING COMPLETED:1/19/11
DRILLING CONTRACTOR:CSI Remarks:
DRILL RIG/ METHOD:Geopobe 6620DT / Direct Push
SAMPLING METHOD:DPT Sleeves Sample collected for laboratory analysisVOCs 6200B and SVOCs 8270
BORING STARTED:1/19/11
LOGGED BY:JRL
TOTAL DEPTH: 36 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)LITHOLOGYRECOVERY (%)SAMP.MATERIAL DESCRIPTIONOVA (ppm)BKG.SAMPLE TYPENUMBERBORING DIAGRAM
Sheet 1 of 1
BORING NUMBER TMW-1
PROJECT:National Textile Facility
JOB NUMBER:FDP-025
LOCATION:Gastonia, NA
BORING LOG - HART HICKMAN.GDT - 1/20/11 15:24 - S:\AAA-MASTER GINT PROJECTS\FDP-025.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
25
30
35
40
0
5
10
15
20
25
30
35
40

Appendix B

Laboratory Analytical Data
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

January 28, 2011
Client:
Attn:
Work Order:
Project Name:
Project Nbr:
Date Received:
National Textiles Facility
FDP-025
NUA2663
01/21/11
Charlotte, NC 28203-5449
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Nathan O'Leary P/O Nbr:
1:24:28PM
SAMPLE IDENTIFICATION LAB NUMBER COLLECTION DATE AND TIME
NUA2663-01SB-1 (12-14')01/19/11 14:00
NUA2663-02SB-3 (8-10')01/19/11 15:00
NUA2663-03SB-5 (12-14')01/19/11 17:00
NUA2663-04TMW-1 01/19/11 15:30
An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum
to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at
1-800-765-0980. Any opinions, if expressed, are outside the scope of the Laboratory's accreditation.
This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is
privileged and confidential. If you are not the intended recipient, or the employee or agent responsible for delivering this material to the
intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited. If you
have received this material in error, please notify us immediately at 615-726-0177.
Additional Laboratory Comments:
FINAL REPORT: 01/28/11 KAH - To report all requested analyses. This report replaces the Preliminary Report generated
on 01/28/11 @ 10.32
North Carolina Certification Number: 387
These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory.
Report Approved By:
Ken A. Hayes
Senior Project Manager
The Chain(s) of Custody, 2 pages, are included and are an integral part of this report.
Estimated uncertainty is available upon request.
This report has been electronically signed.
All solids results are reported in wet weight unless specifically stated.
Page 1 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
ANALYTICAL REPORT

Analyte FlagResult Units
Dilution
FactorMRL Method Batch
Analysis
Date/Time
Sample ID: NUA2663-01 (SB-1 (12-14') - Soil) Sampled: 01/19/11 14:00
General Chemistry Parameters
0.50085.6 01/25/11 11:051 SW-846% Dry Solids %11A4254
Extractable Petroleum Hydrocarbons
5.70ND 01/25/11 15:551 SW846 8015CDieselmg/kg dry 11A4223
68 %Surr: o-Terphenyl (53-140%)01/25/11 15:55 SW846 8015C 11A4223
Purgeable Petroleum Hydrocarbons
5.41ND 01/25/11 16:3550 SW846 8015CGRO as Gasoline mg/kg dry 11A4142
87 %Surr: a,a,a-Trifluorotoluene (60-150%)01/25/11 16:35 SW846 8015C 11A4142
Sample ID: NUA2663-02 (SB-3 (8-10') - Soil) Sampled: 01/19/11 15:00
General Chemistry Parameters
0.50081.5 01/26/11 10:201 SW-846% Dry Solids %11A4382
Volatile Organic Compounds by EPA Method 8260B
0.0532ND 01/25/11 15:011 SW846 8260BAcetonemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BBenzenemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BBromobenzenemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BBromochloromethanemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BBromodichloromethanemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BBromoformmg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BBromomethanemg/kg dry 11A4151
0.00532ND 01/25/11 15:011 SW846 8260B1,2-Dibromo-3-chloropropane mg/kg dry 11A4151
0.0532ND 01/25/11 15:011 SW846 8260B2-Butanone mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260Bsec-Butylbenzene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260Bn-Butylbenzene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260Btert-Butylbenzene mg/kg dry 11A4151
0.00532ND 01/25/11 15:011 SW846 8260BCarbon disulfide mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BCarbon Tetrachloride mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BChlorobenzenemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BChlorodibromomethanemg/kg dry 11A4151
0.00532ND 01/25/11 15:011 SW846 8260BChloroethanemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BChloroformmg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BChloromethanemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B2-Chlorotoluene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B4-Chlorotoluene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,2-Dibromoethane (EDB)mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BDibromomethanemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,4-Dichlorobenzene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,3-Dichlorobenzene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,2-Dichlorobenzene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BDichlorodifluoromethanemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,1-Dichloroethane mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,2-Dichloroethane mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260Bcis-1,2-Dichloroethene mg/kg dry 11A4151
Page 2 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
ANALYTICAL REPORT

Analyte FlagResult Units
Dilution
FactorMRL Method Batch
Analysis
Date/Time
Sample ID: NUA2663-02 (SB-3 (8-10') - Soil) - cont. Sampled: 01/19/11 15:00
Volatile Organic Compounds by EPA Method 8260B - cont.
0.00213ND 01/25/11 15:011 SW846 8260B1,1-Dichloroethene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260Btrans-1,2-Dichloroethene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,3-Dichloropropane mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,2-Dichloropropane mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B2,2-Dichloropropane mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260Bcis-1,3-Dichloropropene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260Btrans-1,3-Dichloropropene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,1-Dichloropropene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BEthylbenzenemg/kg dry 11A4151
0.00532ND 01/25/11 15:011 SW846 8260BHexachlorobutadienemg/kg dry 11A4151
0.0532ND 01/25/11 15:011 SW846 8260B2-Hexanone mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BIsopropylbenzenemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260Bp-Isopropyltoluene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BMethyl tert-Butyl Ether mg/kg dry 11A4151
0.0106ND 01/25/11 15:011 SW846 8260BMethylene Chloride mg/kg dry 11A4151
0.0532ND 01/25/11 15:011 SW846 8260B4-Methyl-2-pentanone mg/kg dry 11A4151
0.00532ND 01/25/11 15:011 SW846 8260BNaphthalenemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260Bn-Propylbenzene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BStyrenemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,1,1,2-Tetrachloroethane mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,1,2,2-Tetrachloroethane mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BTetrachloroethenemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BToluenemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,2,3-Trichlorobenzene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,2,4-Trichlorobenzene mg/kg dry 11A4151
0.00532ND 01/25/11 15:011 SW846 8260B1,1,2-Trichloroethane mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,1,1-Trichloroethane mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BTrichloroethenemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BTrichlorofluoromethanemg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,2,3-Trichloropropane mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,3,5-Trimethylbenzene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,2,4-Trimethylbenzene mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BVinyl chloride mg/kg dry 11A4151
0.00532ND 01/25/11 15:011 SW846 8260BXylenes, total mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260BDiisopropyl Ether mg/kg dry 11A4151
0.00213ND 01/25/11 15:011 SW846 8260B1,2-Dichloroethene (total)mg/kg dry 11A4151
109 %Surr: 1,2-Dichloroethane-d4 (67-138%)01/25/11 15:01 SW846 8260B 11A4151
101 %Surr: Dibromofluoromethane (75-125%)01/25/11 15:01 SW846 8260B 11A4151
108 %Surr: Toluene-d8 (76-129%)01/25/11 15:01 SW846 8260B 11A4151
101 %Surr: 4-Bromofluorobenzene (67-147%)01/25/11 15:01 SW846 8260B 11A4151
Extractable Petroleum Hydrocarbons
6.11ND 01/25/11 16:141 SW846 8015CDieselmg/kg dry 11A4223
63 %Surr: o-Terphenyl (53-140%)01/25/11 16:14 SW846 8015C 11A4223
Page 3 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
ANALYTICAL REPORT

Analyte FlagResult Units
Dilution
FactorMRL Method Batch
Analysis
Date/Time
Sample ID: NUA2663-02 (SB-3 (8-10') - Soil) - cont. Sampled: 01/19/11 15:00
Purgeable Petroleum Hydrocarbons
5.71ND 01/25/11 16:5450 SW846 8015CGRO as Gasoline mg/kg dry 11A4142
82 %Surr: a,a,a-Trifluorotoluene (60-150%)01/25/11 16:54 SW846 8015C 11A4142
Sample ID: NUA2663-03 (SB-5 (12-14') - Soil) Sampled: 01/19/11 17:00
General Chemistry Parameters
0.50090.8 01/26/11 10:201 SW-846% Dry Solids %11A4382
Extractable Petroleum Hydrocarbons
5.47ND 01/25/11 16:331 SW846 8015CDieselmg/kg dry 11A4223
66 %Surr: o-Terphenyl (53-140%)01/25/11 16:33 SW846 8015C 11A4223
Purgeable Petroleum Hydrocarbons
5.75ND 01/25/11 17:1450 SW846 8015CGRO as Gasoline mg/kg dry 11A4142
85 %Surr: a,a,a-Trifluorotoluene (60-150%)01/25/11 17:14 SW846 8015C 11A4142
Sample ID: NUA2663-04 (TMW-1 - Water) Sampled: 01/19/11 15:30
Volatile Organic Compounds by SM6200 B
0.500ND 01/26/11 15:441 SM6200 BBenzeneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BBromobenzeneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BBromochloromethaneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BBromodichloromethaneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BBromoformug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BBromomethaneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 Bn-Butylbenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 Btert-Butylbenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 Bsec-Butylbenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BCarbon Tetrachloride ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BChlorobenzeneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BChlorodibromomethaneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BChloroethaneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BChloroformug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BChloromethaneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B4-Chlorotoluene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B2-Chlorotoluene ug/L 11A4967
5.00ND 01/26/11 15:441 SM6200 B1,2-Dibromo-3-chloropropane ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,2-Dibromoethane (EDB)ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BDibromomethaneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,4-Dichlorobenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,2-Dichlorobenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,3-Dichlorobenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BDichlorodifluoromethaneug/L 11A4967
0.5000.860 01/26/11 15:441 SM6200 B1,1-Dichloroethane ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,2-Dichloroethane ug/L 11A4967
50.0ND 01/26/11 15:441 SM6200 BEthanolug/L 11A4967
Page 4 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
ANALYTICAL REPORT

Analyte FlagResult Units
Dilution
FactorMRL Method Batch
Analysis
Date/Time
Sample ID: NUA2663-04 (TMW-1 - Water) - cont. Sampled: 01/19/11 15:30
Volatile Organic Compounds by SM6200 B - cont.
0.500ND 01/26/11 15:441 SM6200 Btrans-1,2-Dichloroethene ug/L 11A4967
0.5001.44 01/26/11 15:441 SM6200 B1,1-Dichloroethene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 Bcis-1,2-Dichloroethene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,2-Dichloropropane ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,3-Dichloropropane ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B2,2-Dichloropropane ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 Btrans-1,3-Dichloropropene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 Bcis-1,3-Dichloropropene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,1-Dichloropropene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BEthylbenzeneug/L 11A4967
1.00ND 01/26/11 15:441 SM6200 BHexachlorobutadieneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BIsopropylbenzeneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 Bp-Isopropyltoluene ug/L 11A4967
10.0ND 01/26/11 15:441 SM6200 BMethylene Chloride ug/L 11A4967
5.00ND 01/26/11 15:441 SM6200 BNaphthaleneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 Bn-Propylbenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BStyreneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,1,2,2-Tetrachloroethane ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,1,1,2-Tetrachloroethane ug/L 11A4967
0.5003.47 01/26/11 15:441 SM6200 BTetrachloroetheneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BTolueneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,2,3-Trichlorobenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,2,4-Trichlorobenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,1,2-Trichloroethane ug/L 11A4967
0.50010.3 01/26/11 15:441 SM6200 B1,1,1-Trichloroethane ug/L 11A4967
0.5001.33 01/26/11 15:441 SM6200 BTrichloroetheneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BTrichlorofluoromethaneug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,2,3-Trichloropropane ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,3,5-Trimethylbenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 B1,2,4-Trimethylbenzene ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BVinyl chloride ug/L 11A4967
1.00ND 01/26/11 15:441 SM6200 BXylenes, total ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BMethyl tert-Butyl Ether ug/L 11A4967
0.500ND 01/26/11 15:441 SM6200 BDiisopropyl Ether ug/L 11A4967
102 %Surr: 1,2-Dichloroethane-d4 (70-130%)01/26/11 15:44 SM6200 B 11A4967
101 %Surr: Dibromofluoromethane (70-130%)01/26/11 15:44 SM6200 B 11A4967
98 %Surr: Toluene-d8 (70-130%)01/26/11 15:44 SM6200 B 11A4967
97 %Surr: 4-Bromofluorobenzene (70-130%)01/26/11 15:44 SM6200 B 11A4967
Semivolatile Organic Compounds by EPA Method 8270D
2.04ND 01/26/11 16:521 SW846 8270DAcenaphtheneug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DAcenaphthyleneug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DAnthraceneug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DBenzo (a) anthracene ug/L 11A4345
Page 5 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
ANALYTICAL REPORT

Analyte FlagResult Units
Dilution
FactorMRL Method Batch
Analysis
Date/Time
Sample ID: NUA2663-04 (TMW-1 - Water) - cont. Sampled: 01/19/11 15:30
Semivolatile Organic Compounds by EPA Method 8270D - cont.
2.04ND 01/26/11 16:521 SW846 8270DBenzo (a) pyrene ug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DBenzo (b) fluoranthene ug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DBenzo (g,h,i) perylene ug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DBenzo (k) fluoranthene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D4-Bromophenyl phenyl ether ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DButyl benzyl phthalate ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DCarbazoleug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D4-Chloro-3-methylphenol ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D4-Chloroaniline ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DBis(2-chloroethoxy)methane ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DBis(2-chloroethyl)ether ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DBis(2-chloroisopropyl)ether ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D2-Chloronaphthalene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D2-Chlorophenol ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D4-Chlorophenyl phenyl ether ug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DChryseneug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DDibenz (a,h) anthracene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DDibenzofuranug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DDi-n-butyl phthalate ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D1,4-Dichlorobenzene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D1,2-Dichlorobenzene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D1,3-Dichlorobenzene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D3,3-Dichlorobenzidine ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D2,4-Dichlorophenol ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DDiethyl phthalate ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D2,4-Dimethylphenol ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DDimethyl phthalate ug/L 11A4345
25.5ND 01/26/11 16:521 SW846 8270D4,6-Dinitro-2-methylphenol ug/L 11A4345
25.5ND 01/26/11 16:521 SW846 8270D2,4-Dinitrophenol ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D2,6-Dinitrotoluene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D2,4-Dinitrotoluene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DDi-n-octyl phthalate ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DBis(2-ethylhexyl)phthalate ug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DFluorantheneug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DFluoreneug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DHexachlorobenzeneug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DHexachlorobutadieneug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DHexachlorocyclopentadieneug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DHexachloroethaneug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DIndeno (1,2,3-cd) pyrene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DIsophoroneug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270D2-Methylnaphthalene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D2-Methylphenol ug/L 11A4345
Page 6 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
ANALYTICAL REPORT

Analyte FlagResult Units
Dilution
FactorMRL Method Batch
Analysis
Date/Time
Sample ID: NUA2663-04 (TMW-1 - Water) - cont. Sampled: 01/19/11 15:30
Semivolatile Organic Compounds by EPA Method 8270D - cont.
10.2ND 01/26/11 16:521 SW846 8270D3/4-Methylphenol ug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DNaphthaleneug/L 11A4345
25.5ND 01/26/11 16:521 SW846 8270D3-Nitroaniline ug/L 11A4345
25.5ND 01/26/11 16:521 SW846 8270D2-Nitroaniline ug/L 11A4345
25.5ND 01/26/11 16:521 SW846 8270D4-Nitroaniline ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DNitrobenzeneug/L 11A4345
25.5ND 01/26/11 16:521 SW846 8270D4-Nitrophenol ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D2-Nitrophenol ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DN-Nitrosodiphenylamine ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DN-Nitrosodi-n-propylamine ug/L 11A4345
25.5ND 01/26/11 16:521 SW846 8270DPentachlorophenolug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DPhenanthreneug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270DPhenolug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270DPyreneug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D1,2,4-Trichlorobenzene ug/L 11A4345
2.04ND 01/26/11 16:521 SW846 8270D1-Methylnaphthalene ug/L 11A4345
10.2ND 01/26/11 16:521 SW846 8270D2,4,6-Trichlorophenol ug/L 11A4345
25.5ND 01/26/11 16:521 SW846 8270D2,4,5-Trichlorophenol ug/L 11A4345
47 %Surr: Terphenyl-d14 (13-120%)01/26/11 16:52 SW846 8270D 11A4345
65 %Surr: 2,4,6-Tribromophenol (29-132%)01/26/11 16:52 SW846 8270D 11A4345
20 %Surr: Phenol-d5 (10-120%)01/26/11 16:52 SW846 8270D 11A4345
50 %Surr: 2-Fluorobiphenyl (29-120%)01/26/11 16:52 SW846 8270D 11A4345
32 %Surr: 2-Fluorophenol (10-120%)01/26/11 16:52 SW846 8270D 11A4345
53 %Surr: Nitrobenzene-d5 (27-120%)01/26/11 16:52 SW846 8270D 11A4345
Page 7 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
SAMPLE EXTRACTION DATA
Parameter
Wt/Vol
Extracted Extract Vol Date Analyst
Extraction
MethodLab NumberBatch
Extractable Petroleum Hydrocarbons
25.62 EPA 3550BSAS01/25/11 07:2511A4223SW846 8015C NUA2663-01 1.00
25.11 EPA 3550BSAS01/25/11 07:2511A4223SW846 8015C NUA2663-02 1.00
25.16 EPA 3550BSAS01/25/11 07:2511A4223SW846 8015C NUA2663-03 1.00
Purgeable Petroleum Hydrocarbons
5.40 EPA 5035A (GC)JRL01/19/11 14:0011A4142SW846 8015C NUA2663-01 5.00
5.37 EPA 5035A (GC)JRL01/19/11 15:0011A4142SW846 8015C NUA2663-02 5.00
4.79 EPA 5035A (GC)JRL01/19/11 17:0011A4142SW846 8015C NUA2663-03 5.00
Semivolatile Organic Compounds by EPA Method 8270D
980.00 EPA 3510CTDM01/25/11 12:0011A4345SW846 8270D NUA2663-04 1.00
Volatile Organic Compounds by EPA Method 8260B
5.77 EPA 5035JRL01/19/11 15:0011A4151SW846 8260B NUA2663-02 5.00
Page 8 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
Blank
Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time
Volatile Organic Compounds by EPA Method 8260B
11A4151-BLK1
mg/kg wet 11A4151<0.0250 11A4151-BLK1 01/25/11 14:31Acetone
mg/kg wet 11A4151<0.00110 11A4151-BLK1 01/25/11 14:31Benzene
mg/kg wet 11A4151<0.000880 11A4151-BLK1 01/25/11 14:31Bromobenzene
mg/kg wet 11A4151<0.000780 11A4151-BLK1 01/25/11 14:31Bromochloromethane
mg/kg wet 11A4151<0.000460 11A4151-BLK1 01/25/11 14:31Bromodichloromethane
mg/kg wet 11A4151<0.000650 11A4151-BLK1 01/25/11 14:31Bromoform
mg/kg wet 11A4151<0.000880 11A4151-BLK1 01/25/11 14:31Bromomethane
mg/kg wet 11A4151<0.00150 11A4151-BLK1 01/25/11 14:311,2-Dibromo-3-chloropropane
mg/kg wet 11A4151<0.00710 11A4151-BLK1 01/25/11 14:312-Butanone
mg/kg wet 11A4151<0.000890 11A4151-BLK1 01/25/11 14:31sec-Butylbenzene
mg/kg wet 11A4151<0.00170 11A4151-BLK1 01/25/11 14:31n-Butylbenzene
mg/kg wet 11A4151<0.000840 11A4151-BLK1 01/25/11 14:31tert-Butylbenzene
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:31Carbon disulfide
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:31Carbon Tetrachloride
mg/kg wet 11A4151<0.000720 11A4151-BLK1 01/25/11 14:31Chlorobenzene
mg/kg wet 11A4151<0.000640 11A4151-BLK1 01/25/11 14:31Chlorodibromomethane
mg/kg wet 11A4151<0.00100 11A4151-BLK1 01/25/11 14:31Chloroethane
mg/kg wet 11A41510.000530 11A4151-BLK1 01/25/11 14:31Chloroform
mg/kg wet 11A4151<0.00110 11A4151-BLK1 01/25/11 14:31Chloromethane
mg/kg wet 11A4151<0.000970 11A4151-BLK1 01/25/11 14:312-Chlorotoluene
mg/kg wet 11A4151<0.000530 11A4151-BLK1 01/25/11 14:314-Chlorotoluene
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:311,2-Dibromoethane (EDB)
mg/kg wet 11A4151<0.00100 11A4151-BLK1 01/25/11 14:31Dibromomethane
mg/kg wet 11A4151<0.000720 11A4151-BLK1 01/25/11 14:311,4-Dichlorobenzene
mg/kg wet 11A4151<0.00150 11A4151-BLK1 01/25/11 14:311,3-Dichlorobenzene
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:311,2-Dichlorobenzene
mg/kg wet 11A4151<0.00140 11A4151-BLK1 01/25/11 14:31Dichlorodifluoromethane
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:311,1-Dichloroethane
mg/kg wet 11A4151<0.000510 11A4151-BLK1 01/25/11 14:311,2-Dichloroethane
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:31cis-1,2-Dichloroethene
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:311,1-Dichloroethene
mg/kg wet 11A4151<0.000760 11A4151-BLK1 01/25/11 14:31trans-1,2-Dichloroethene
mg/kg wet 11A4151<0.000840 11A4151-BLK1 01/25/11 14:311,3-Dichloropropane
mg/kg wet 11A4151<0.000620 11A4151-BLK1 01/25/11 14:311,2-Dichloropropane
mg/kg wet 11A4151<0.000890 11A4151-BLK1 01/25/11 14:312,2-Dichloropropane
mg/kg wet 11A4151<0.000350 11A4151-BLK1 01/25/11 14:31cis-1,3-Dichloropropene
mg/kg wet 11A4151<0.000550 11A4151-BLK1 01/25/11 14:31trans-1,3-Dichloropropene
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:311,1-Dichloropropene
mg/kg wet 11A4151<0.000980 11A4151-BLK1 01/25/11 14:31Ethylbenzene
mg/kg wet 11A4151<0.000700 11A4151-BLK1 01/25/11 14:31Hexachlorobutadiene
mg/kg wet 11A4151<0.00850 11A4151-BLK1 01/25/11 14:312-Hexanone
Page 9 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
Blank - Cont.
Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time
Volatile Organic Compounds by EPA Method 8260B
11A4151-BLK1
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:31Isopropylbenzene
mg/kg wet 11A4151<0.000940 11A4151-BLK1 01/25/11 14:31p-Isopropyltoluene
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:31Methyl tert-Butyl Ether
mg/kg wet 11A41510.00782 11A4151-BLK1 01/25/11 14:31Methylene Chloride
mg/kg wet 11A4151<0.00340 11A4151-BLK1 01/25/11 14:314-Methyl-2-pentanone
mg/kg wet 11A4151<0.00170 11A4151-BLK1 01/25/11 14:31Naphthalene
mg/kg wet 11A4151<0.000860 11A4151-BLK1 01/25/11 14:31n-Propylbenzene
mg/kg wet 11A4151<0.000740 11A4151-BLK1 01/25/11 14:31Styrene
mg/kg wet 11A4151<0.00100 11A4151-BLK1 01/25/11 14:311,1,1,2-Tetrachloroethane
mg/kg wet 11A4151<0.000890 11A4151-BLK1 01/25/11 14:311,1,2,2-Tetrachloroethane
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:31Tetrachloroethene
mg/kg wet 11A4151<0.000890 11A4151-BLK1 01/25/11 14:31Toluene
mg/kg wet 11A4151<0.000630 11A4151-BLK1 01/25/11 14:311,2,3-Trichlorobenzene
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:311,2,4-Trichlorobenzene
mg/kg wet 11A4151<0.00119 11A4151-BLK1 01/25/11 14:311,1,2-Trichloroethane
mg/kg wet 11A4151<0.000850 11A4151-BLK1 01/25/11 14:311,1,1-Trichloroethane
mg/kg wet 11A4151<0.00100 11A4151-BLK1 01/25/11 14:31Trichloroethene
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:31Trichlorofluoromethane
mg/kg wet 11A4151<0.000790 11A4151-BLK1 01/25/11 14:311,2,3-Trichloropropane
mg/kg wet 11A4151<0.000830 11A4151-BLK1 01/25/11 14:311,3,5-Trimethylbenzene
mg/kg wet 11A4151<0.00127 11A4151-BLK1 01/25/11 14:311,2,4-Trimethylbenzene
mg/kg wet 11A4151<0.00101 11A4151-BLK1 01/25/11 14:31Vinyl chloride
mg/kg wet 11A4151<0.00190 11A4151-BLK1 01/25/11 14:31Xylenes, total
mg/kg wet 11A4151<0.000670 11A4151-BLK1 01/25/11 14:31Diisopropyl Ether
mg/kg wet 11A4151<0.00143 11A4151-BLK1 01/25/11 14:311,2-Dichloroethene (total)
11A4151 11A4151-BLK1 01/25/11 14:31110%Surrogate: 1,2-Dichloroethane-d4
11A4151 11A4151-BLK1 01/25/11 14:31102%Surrogate: Dibromofluoromethane
11A4151 11A4151-BLK1 01/25/11 14:31107%Surrogate: Toluene-d8
11A4151 11A4151-BLK1 01/25/11 14:3199%Surrogate: 4-Bromofluorobenzene
Volatile Organic Compounds by SM6200 B
11A4967-BLK1
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Benzene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Bromobenzene
ug/L 11A4967<0.240 11A4967-BLK1 01/26/11 13:28Bromochloromethane
ug/L 11A4967<0.180 11A4967-BLK1 01/26/11 13:28Bromodichloromethane
ug/L 11A4967<0.180 11A4967-BLK1 01/26/11 13:28Bromoform
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Bromomethane
ug/L 11A4967<0.180 11A4967-BLK1 01/26/11 13:28n-Butylbenzene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28tert-Butylbenzene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28sec-Butylbenzene
Page 10 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
Blank - Cont.
Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time
Volatile Organic Compounds by SM6200 B
11A4967-BLK1
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Carbon Tetrachloride
ug/L 11A4967<0.190 11A4967-BLK1 01/26/11 13:28Chlorobenzene
ug/L 11A4967<0.210 11A4967-BLK1 01/26/11 13:28Chlorodibromomethane
ug/L 11A4967<0.210 11A4967-BLK1 01/26/11 13:28Chloroethane
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Chloroform
ug/L 11A4967<0.300 11A4967-BLK1 01/26/11 13:28Chloromethane
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:284-Chlorotoluene
ug/L 11A4967<0.140 11A4967-BLK1 01/26/11 13:282-Chlorotoluene
ug/L 11A4967<0.270 11A4967-BLK1 01/26/11 13:281,2-Dibromo-3-chloropropane
ug/L 11A4967<0.180 11A4967-BLK1 01/26/11 13:281,2-Dibromoethane (EDB)
ug/L 11A4967<0.160 11A4967-BLK1 01/26/11 13:28Dibromomethane
ug/L 11A4967<0.150 11A4967-BLK1 01/26/11 13:281,4-Dichlorobenzene
ug/L 11A4967<0.130 11A4967-BLK1 01/26/11 13:281,2-Dichlorobenzene
ug/L 11A4967<0.140 11A4967-BLK1 01/26/11 13:281,3-Dichlorobenzene
ug/L 11A4967<0.140 11A4967-BLK1 01/26/11 13:28Dichlorodifluoromethane
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:281,1-Dichloroethane
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:281,2-Dichloroethane
ug/L 11A4967<30.0 11A4967-BLK1 01/26/11 13:28Ethanol
ug/L 11A4967<0.160 11A4967-BLK1 01/26/11 13:28trans-1,2-Dichloroethene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:281,1-Dichloroethene
ug/L 11A4967<0.150 11A4967-BLK1 01/26/11 13:28cis-1,2-Dichloroethene
ug/L 11A4967<0.180 11A4967-BLK1 01/26/11 13:281,2-Dichloropropane
ug/L 11A4967<0.110 11A4967-BLK1 01/26/11 13:281,3-Dichloropropane
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:282,2-Dichloropropane
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28trans-1,3-Dichloropropene
ug/L 11A4967<0.150 11A4967-BLK1 01/26/11 13:28cis-1,3-Dichloropropene
ug/L 11A4967<0.110 11A4967-BLK1 01/26/11 13:281,1-Dichloropropene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Ethylbenzene
ug/L 11A49670.510 11A4967-BLK1 01/26/11 13:28Hexachlorobutadiene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Isopropylbenzene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28p-Isopropyltoluene
ug/L 11A49671.85 11A4967-BLK1 01/26/11 13:28Methylene Chloride
ug/L 11A4967<1.70 11A4967-BLK1 01/26/11 13:28Naphthalene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28n-Propylbenzene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Styrene
ug/L 11A4967<0.140 11A4967-BLK1 01/26/11 13:281,1,2,2-Tetrachloroethane
ug/L 11A4967<0.180 11A4967-BLK1 01/26/11 13:281,1,1,2-Tetrachloroethane
ug/L 11A4967<0.190 11A4967-BLK1 01/26/11 13:28Tetrachloroethene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Toluene
ug/L 11A4967<0.250 11A4967-BLK1 01/26/11 13:281,2,3-Trichlorobenzene
ug/L 11A4967<0.180 11A4967-BLK1 01/26/11 13:281,2,4-Trichlorobenzene
Page 11 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
Blank - Cont.
Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time
Volatile Organic Compounds by SM6200 B
11A4967-BLK1
ug/L 11A4967<0.150 11A4967-BLK1 01/26/11 13:281,1,2-Trichloroethane
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:281,1,1-Trichloroethane
ug/L 11A4967<0.180 11A4967-BLK1 01/26/11 13:28Trichloroethene
ug/L 11A4967<0.180 11A4967-BLK1 01/26/11 13:28Trichlorofluoromethane
ug/L 11A4967<0.270 11A4967-BLK1 01/26/11 13:281,2,3-Trichloropropane
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:281,3,5-Trimethylbenzene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:281,2,4-Trimethylbenzene
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Vinyl chloride
ug/L 11A4967<0.390 11A4967-BLK1 01/26/11 13:28Xylenes, total
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Methyl tert-Butyl Ether
ug/L 11A4967<0.170 11A4967-BLK1 01/26/11 13:28Diisopropyl Ether
11A4967 11A4967-BLK1 01/26/11 13:28100%Surrogate: 1,2-Dichloroethane-d4
11A4967 11A4967-BLK1 01/26/11 13:28100%Surrogate: Dibromofluoromethane
11A4967 11A4967-BLK1 01/26/11 13:2898%Surrogate: Toluene-d8
11A4967 11A4967-BLK1 01/26/11 13:2898%Surrogate: 4-Bromofluorobenzene
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-BLK1
ug/L 11A4345<0.500 11A4345-BLK1 01/25/11 16:02Acenaphthene
ug/L 11A4345<0.400 11A4345-BLK1 01/25/11 16:02Acenaphthylene
ug/L 11A4345<0.200 11A4345-BLK1 01/25/11 16:02Anthracene
ug/L 11A4345<0.700 11A4345-BLK1 01/25/11 16:02Benzo (a) anthracene
ug/L 11A4345<0.600 11A4345-BLK1 01/25/11 16:02Benzo (a) pyrene
ug/L 11A4345<0.700 11A4345-BLK1 01/25/11 16:02Benzo (b) fluoranthene
ug/L 11A4345<0.500 11A4345-BLK1 01/25/11 16:02Benzo (g,h,i) perylene
ug/L 11A4345<0.800 11A4345-BLK1 01/25/11 16:02Benzo (k) fluoranthene
ug/L 11A4345<3.00 11A4345-BLK1 01/25/11 16:024-Bromophenyl phenyl ether
ug/L 11A4345<3.70 11A4345-BLK1 01/25/11 16:02Butyl benzyl phthalate
ug/L 11A4345<0.400 11A4345-BLK1 01/25/11 16:02Carbazole
ug/L 11A4345<2.80 11A4345-BLK1 01/25/11 16:024-Chloro-3-methylphenol
ug/L 11A4345<4.80 11A4345-BLK1 01/25/11 16:024-Chloroaniline
ug/L 11A4345<2.60 11A4345-BLK1 01/25/11 16:02Bis(2-chloroethoxy)methane
ug/L 11A4345<4.10 11A4345-BLK1 01/25/11 16:02Bis(2-chloroethyl)ether
ug/L 11A4345<3.50 11A4345-BLK1 01/25/11 16:02Bis(2-chloroisopropyl)ether
ug/L 11A4345<2.90 11A4345-BLK1 01/25/11 16:022-Chloronaphthalene
ug/L 11A4345<2.40 11A4345-BLK1 01/25/11 16:022-Chlorophenol
ug/L 11A4345<2.80 11A4345-BLK1 01/25/11 16:024-Chlorophenyl phenyl ether
ug/L 11A4345<0.500 11A4345-BLK1 01/25/11 16:02Chrysene
ug/L 11A4345<0.600 11A4345-BLK1 01/25/11 16:02Dibenz (a,h) anthracene
ug/L 11A4345<0.700 11A4345-BLK1 01/25/11 16:02Dibenzofuran
ug/L 11A4345<3.20 11A4345-BLK1 01/25/11 16:02Di-n-butyl phthalate
Page 12 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
Blank - Cont.
Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-BLK1
ug/L 11A4345<2.10 11A4345-BLK1 01/25/11 16:021,4-Dichlorobenzene
ug/L 11A4345<2.20 11A4345-BLK1 01/25/11 16:021,2-Dichlorobenzene
ug/L 11A4345<2.10 11A4345-BLK1 01/25/11 16:021,3-Dichlorobenzene
ug/L 11A4345<6.40 11A4345-BLK1 01/25/11 16:023,3-Dichlorobenzidine
ug/L 11A4345<2.30 11A4345-BLK1 01/25/11 16:022,4-Dichlorophenol
ug/L 11A4345<2.80 11A4345-BLK1 01/25/11 16:02Diethyl phthalate
ug/L 11A4345<2.60 11A4345-BLK1 01/25/11 16:022,4-Dimethylphenol
ug/L 11A4345<2.70 11A4345-BLK1 01/25/11 16:02Dimethyl phthalate
ug/L 11A4345<3.30 11A4345-BLK1 01/25/11 16:024,6-Dinitro-2-methylphenol
ug/L 11A4345<3.10 11A4345-BLK1 01/25/11 16:022,4-Dinitrophenol
ug/L 11A4345<3.00 11A4345-BLK1 01/25/11 16:022,6-Dinitrotoluene
ug/L 11A4345<3.00 11A4345-BLK1 01/25/11 16:022,4-Dinitrotoluene
ug/L 11A4345<3.70 11A4345-BLK1 01/25/11 16:02Di-n-octyl phthalate
ug/L 11A4345<3.30 11A4345-BLK1 01/25/11 16:02Bis(2-ethylhexyl)phthalate
ug/L 11A4345<0.700 11A4345-BLK1 01/25/11 16:02Fluoranthene
ug/L 11A4345<0.700 11A4345-BLK1 01/25/11 16:02Fluorene
ug/L 11A4345<2.70 11A4345-BLK1 01/25/11 16:02Hexachlorobenzene
ug/L 11A4345<2.70 11A4345-BLK1 01/25/11 16:02Hexachlorobutadiene
ug/L 11A4345<1.90 11A4345-BLK1 01/25/11 16:02Hexachlorocyclopentadiene
ug/L 11A4345<2.40 11A4345-BLK1 01/25/11 16:02Hexachloroethane
ug/L 11A4345<0.500 11A4345-BLK1 01/25/11 16:02Indeno (1,2,3-cd) pyrene
ug/L 11A4345<2.80 11A4345-BLK1 01/25/11 16:02Isophorone
ug/L 11A4345<0.600 11A4345-BLK1 01/25/11 16:022-Methylnaphthalene
ug/L 11A4345<2.60 11A4345-BLK1 01/25/11 16:022-Methylphenol
ug/L 11A4345<2.30 11A4345-BLK1 01/25/11 16:023/4-Methylphenol
ug/L 11A4345<0.500 11A4345-BLK1 01/25/11 16:02Naphthalene
ug/L 11A4345<2.90 11A4345-BLK1 01/25/11 16:023-Nitroaniline
ug/L 11A4345<2.30 11A4345-BLK1 01/25/11 16:022-Nitroaniline
ug/L 11A4345<3.40 11A4345-BLK1 01/25/11 16:024-Nitroaniline
ug/L 11A4345<2.50 11A4345-BLK1 01/25/11 16:02Nitrobenzene
ug/L 11A4345<5.30 11A4345-BLK1 01/25/11 16:024-Nitrophenol
ug/L 11A4345<3.00 11A4345-BLK1 01/25/11 16:022-Nitrophenol
ug/L 11A4345<4.00 11A4345-BLK1 01/25/11 16:02N-Nitrosodiphenylamine
ug/L 11A4345<2.70 11A4345-BLK1 01/25/11 16:02N-Nitrosodi-n-propylamine
ug/L 11A4345<2.60 11A4345-BLK1 01/25/11 16:02Pentachlorophenol
ug/L 11A4345<0.700 11A4345-BLK1 01/25/11 16:02Phenanthrene
ug/L 11A4345<1.70 11A4345-BLK1 01/25/11 16:02Phenol
ug/L 11A4345<0.600 11A4345-BLK1 01/25/11 16:02Pyrene
ug/L 11A4345<2.60 11A4345-BLK1 01/25/11 16:021,2,4-Trichlorobenzene
ug/L 11A4345<1.60 11A4345-BLK1 01/25/11 16:021-Methylnaphthalene
ug/L 11A4345<3.00 11A4345-BLK1 01/25/11 16:022,4,6-Trichlorophenol
Page 13 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
Blank - Cont.
Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-BLK1
ug/L 11A4345<2.70 11A4345-BLK1 01/25/11 16:022,4,5-Trichlorophenol
11A4345 11A4345-BLK1 01/25/11 16:0267%Surrogate: Terphenyl-d14
11A4345 11A4345-BLK1 01/25/11 16:0289%Surrogate: 2,4,6-Tribromophenol
11A4345 11A4345-BLK1 01/25/11 16:0226%Surrogate: Phenol-d5
11A4345 11A4345-BLK1 01/25/11 16:0268%Surrogate: 2-Fluorobiphenyl
11A4345 11A4345-BLK1 01/25/11 16:0241%Surrogate: 2-Fluorophenol
11A4345 11A4345-BLK1 01/25/11 16:0271%Surrogate: Nitrobenzene-d5
Extractable Petroleum Hydrocarbons
11A4223-BLK1
mg/kg wet 11A4223<0.700 11A4223-BLK1 01/25/11 14:38Diesel
11A4223 11A4223-BLK1 01/25/11 14:3879%Surrogate: o-Terphenyl
Purgeable Petroleum Hydrocarbons
11A4142-BLK1
mg/kg wet 11A4142<0.500 11A4142-BLK1 01/25/11 12:28GRO as Gasoline
11A4142 11A4142-BLK1 01/25/11 12:2877%Surrogate: a,a,a-Trifluorotoluene
11A4142-BLK2
mg/kg wet 11A41421.31 11A4142-BLK2 01/25/11 12:48GRO as Gasoline
11A4142 11A4142-BLK2 01/25/11 12:4885%Surrogate: a,a,a-Trifluorotoluene
11A4142-BLK3
mg/kg wet 11A41421.01 11A4142-BLK3 01/26/11 14:13GRO as Gasoline
11A4142 11A4142-BLK3 01/26/11 14:1381%Surrogate: a,a,a-Trifluorotoluene
11A4142-BLK4
mg/kg wet 11A4142<0.500 11A4142-BLK4 01/26/11 14:32GRO as Gasoline
11A4142 11A4142-BLK4 01/26/11 14:3281%Surrogate: a,a,a-Trifluorotoluene
Page 14 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
Duplicate
Analyte UnitsOrig. Val.Duplicate RPD Batch
Sample
DuplicatedQ
Analyzed
Date/TimeLimit% Rec.
General Chemistry Parameters
11A4254-DUP1
%81.9 83.0 20 11A4254 NUA2612-01 01/25/11 11:05% Dry Solids 1
11A4382-DUP1
%90.6 89.3 20 11A4382 NUA2510-01 01/26/11 10:20% Dry Solids 1
Page 15 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
LCS
Analyte UnitsKnown Val.Analyzed Val % Rec. BatchQ
Target
Range
Analyzed
Date/Time
Volatile Organic Compounds by EPA Method 8260B
11A4151-BS1
60 - 150 11A4151250257103% ug/kg 01/25/11 12:31Acetone
78 - 126 11A415150.0 50.6 101% ug/kg 01/25/11 12:31Benzene
79 - 126 11A415150.0 52.8 106% ug/kg 01/25/11 12:31Bromobenzene
78 - 126 11A415150.0 47.0 94% ug/kg 01/25/11 12:31Bromochloromethane
75 - 129 11A415150.0 51.3 103% ug/kg 01/25/11 12:31Bromodichloromethane
74 - 133 11A415150.0 38.4 77% ug/kg 01/25/11 12:31Bromoform
50 - 150 11A415150.0 55.5 111% ug/kg 01/25/11 12:31Bromomethane
62 - 150 11A415150.0 40.6 81% ug/kg 01/25/11 12:311,2-Dibromo-3-chloropropane
68 - 149 11A415125022389% ug/kg 01/25/11 12:312-Butanone
76 - 135 11A415150.0 53.3 107% ug/kg 01/25/11 12:31sec-Butylbenzene
73 - 143 11A415150.0 57.4 115% ug/kg 01/25/11 12:31n-Butylbenzene
80 - 129 11A415150.0 52.2 104% ug/kg 01/25/11 12:31tert-Butylbenzene
80 - 132 11A415150.0 58.2 116% ug/kg 01/25/11 12:31Carbon disulfide
70 - 138 11A415150.0 58.5 117% ug/kg 01/25/11 12:31Carbon Tetrachloride
80 - 123 11A415150.0 52.7 105% ug/kg 01/25/11 12:31Chlorobenzene
80 - 127 11A415150.0 48.3 97% ug/kg 01/25/11 12:31Chlorodibromomethane
55 - 150 11A415150.0 54.0 108% ug/kg 01/25/11 12:31Chloroethane
70 - 127 11A415150.0 52.6 105% ug/kg 01/25/11 12:31Chloroform
36 - 137 11A415150.0 42.0 84% ug/kg 01/25/11 12:31Chloromethane
80 - 130 11A415150.0 54.6 109% ug/kg 01/25/11 12:312-Chlorotoluene
77 - 132 11A415150.0 54.0 108% ug/kg 01/25/11 12:314-Chlorotoluene
80 - 131 11A415150.0 50.6 101% ug/kg 01/25/11 12:311,2-Dibromoethane (EDB)
78 - 128 11A415150.0 47.8 96% ug/kg 01/25/11 12:31Dibromomethane
80 - 129 11A415150.0 53.2 106% ug/kg 01/25/11 12:311,4-Dichlorobenzene
80 - 131 11A415150.0 52.0 104% ug/kg 01/25/11 12:311,3-Dichlorobenzene
80 - 127 11A415150.0 52.2 104% ug/kg 01/25/11 12:311,2-Dichlorobenzene
30 - 150 11A415150.0 38.5 77% ug/kg 01/25/11 12:31Dichlorodifluoromethane
71 - 126 11A415150.0 53.5 107% ug/kg 01/25/11 12:311,1-Dichloroethane
70 - 139 11A415150.0 53.5 107% ug/kg 01/25/11 12:311,2-Dichloroethane
75 - 126 11A415150.0 53.8 108% ug/kg 01/25/11 12:31cis-1,2-Dichloroethene
70 - 125 11A415150.0 52.3 105% ug/kg 01/25/11 12:311,1-Dichloroethene
73 - 128 11A415150.0 56.5 113% ug/kg 01/25/11 12:31trans-1,2-Dichloroethene
79 - 128 11A415150.0 52.2 104% ug/kg 01/25/11 12:311,3-Dichloropropane
75 - 120 11A415150.0 48.6 97% ug/kg 01/25/11 12:311,2-Dichloropropane
60 - 139 11A415150.0 58.6 117% ug/kg 01/25/11 12:312,2-Dichloropropane
74 - 136 11A415150.0 60.6 121% ug/kg 01/25/11 12:31cis-1,3-Dichloropropene
73 - 128 11A415150.0 50.9 102% ug/kg 01/25/11 12:31trans-1,3-Dichloropropene
78 - 125 11A415150.0 54.9 110% ug/kg 01/25/11 12:311,1-Dichloropropene
79 - 130 11A415150.0 54.8 110% ug/kg 01/25/11 12:31Ethylbenzene
75 - 150 11A415150.0 51.1 102% ug/kg 01/25/11 12:31Hexachlorobutadiene
65 - 150 11A4151250252101% ug/kg 01/25/11 12:312-Hexanone
Page 16 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
LCS - Cont.
Analyte UnitsKnown Val.Analyzed Val % Rec. BatchQ
Target
Range
Analyzed
Date/Time
Volatile Organic Compounds by EPA Method 8260B
11A4151-BS1
65 - 121 11A415150.0 54.6 109% ug/kg 01/25/11 12:31Isopropylbenzene
76 - 133 11A415150.0 54.4 109% ug/kg 01/25/11 12:31p-Isopropyltoluene
70 - 128 11A415150.0 52.6 105% ug/kg 01/25/11 12:31Methyl tert-Butyl Ether
69 - 140 11A415150.0 48.8 98% ug/kg 01/25/11 12:31Methylene Chloride
67 - 147 11A4151250253101% ug/kg 01/25/11 12:314-Methyl-2-pentanone
72 - 150 11A415150.0 53.0 106% ug/kg 01/25/11 12:31Naphthalene
76 - 133 11A415150.0 55.9 112% ug/kg 01/25/11 12:31n-Propylbenzene
80 - 140 11A415150.0 50.3 101% ug/kg 01/25/11 12:31Styrene
80 - 132 11A415150.0 56.5 113% ug/kg 01/25/11 12:311,1,1,2-Tetrachloroethane
75 - 135 11A415150.0 48.0 96% ug/kg 01/25/11 12:311,1,2,2-Tetrachloroethane
76 - 130 11A415150.0 53.5 107% ug/kg 01/25/11 12:31Tetrachloroethene
76 - 126 11A415150.0 54.4 109% ug/kg 01/25/11 12:31Toluene
75 - 150 11A415150.0 55.6 111% ug/kg 01/25/11 12:311,2,3-Trichlorobenzene
64 - 150 11A415150.0 57.3 115% ug/kg 01/25/11 12:311,2,4-Trichlorobenzene
73 - 133 11A415150.0 49.3 99% ug/kg 01/25/11 12:311,1,2-Trichloroethane
70 - 132 11A415150.0 54.8 110% ug/kg 01/25/11 12:311,1,1-Trichloroethane
79 - 129 11A415150.0 46.9 94% ug/kg 01/25/11 12:31Trichloroethene
52 - 148 11A415150.0 53.8 108% ug/kg 01/25/11 12:31Trichlorofluoromethane
70 - 125 11A415150.0 49.9 100% ug/kg 01/25/11 12:311,2,3-Trichloropropane
80 - 134 11A415150.0 55.0 110% ug/kg 01/25/11 12:311,3,5-Trimethylbenzene
80 - 132 11A415150.0 53.0 106% ug/kg 01/25/11 12:311,2,4-Trimethylbenzene
53 - 142 11A415150.0 51.2 102% ug/kg 01/25/11 12:31Vinyl chloride
80 - 130 11A4151150166110% ug/kg 01/25/11 12:31Xylenes, total
71 - 125 11A415150.0 57.4 115% ug/kg 01/25/11 12:31Diisopropyl Ether
74 - 126 11A4151100110110% ug/kg 01/25/11 12:311,2-Dichloroethene (total)
67 - 138 11A415150.0 55.6Surrogate: 1,2-Dichloroethane-d4 111% 01/25/11 12:31
75 - 125 11A415150.0 51.0Surrogate: Dibromofluoromethane 102% 01/25/11 12:31
76 - 129 11A415150.0 53.6Surrogate: Toluene-d8 107% 01/25/11 12:31
67 - 147 11A415150.0 50.4Surrogate: 4-Bromofluorobenzene 101% 01/25/11 12:31
Volatile Organic Compounds by SM6200 B
11A4967-BS1
70 - 130 11A496750.0 49.9 100% ug/L 01/26/11 11:39Benzene
70 - 130 11A496750.0 50.4 101% ug/L 01/26/11 11:39Bromobenzene
70 - 130 11A496750.0 46.0 92% ug/L 01/26/11 11:39Bromochloromethane
70 - 130 11A496750.0 53.3 107% ug/L 01/26/11 11:39Bromodichloromethane
70 - 130 11A496750.0 47.6 95% ug/L 01/26/11 11:39Bromoform
60 - 140 11A496750.0 54.8 110% ug/L 01/26/11 11:39Bromomethane
70 - 130 11A496750.0 57.6 115% ug/L 01/26/11 11:39n-Butylbenzene
70 - 130 11A496750.0 54.0 108% ug/L 01/26/11 11:39tert-Butylbenzene
70 - 130 11A496750.0 55.3 111% ug/L 01/26/11 11:39sec-Butylbenzene
Page 17 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
LCS - Cont.
Analyte UnitsKnown Val.Analyzed Val % Rec. BatchQ
Target
Range
Analyzed
Date/Time
Volatile Organic Compounds by SM6200 B
11A4967-BS1
70 - 130 11A496750.0 53.2 106% ug/L 01/26/11 11:39Carbon Tetrachloride
70 - 130 11A496750.0 49.9 100% ug/L 01/26/11 11:39Chlorobenzene
70 - 130 11A496750.0 57.6 115% ug/L 01/26/11 11:39Chlorodibromomethane
60 - 140 11A496750.0 45.1 90% ug/L 01/26/11 11:39Chloroethane
70 - 130 11A496750.0 50.1 100% ug/L 01/26/11 11:39Chloroform
60 - 140 11A496750.0 42.4 85% ug/L 01/26/11 11:39Chloromethane
70 - 130 11A496750.0 52.5 105% ug/L 01/26/11 11:394-Chlorotoluene
70 - 130 11A496750.0 51.3 103% ug/L 01/26/11 11:392-Chlorotoluene
70 - 130 11A496750.0 47.4 95% ug/L 01/26/11 11:391,2-Dibromo-3-chloropropane
70 - 130 11A496750.0 53.0 106% ug/L 01/26/11 11:391,2-Dibromoethane (EDB)
70 - 130 11A496750.0 50.9 102% ug/L 01/26/11 11:39Dibromomethane
70 - 130 11A496750.0 51.4 103% ug/L 01/26/11 11:391,4-Dichlorobenzene
70 - 130 11A496750.0 52.4 105% ug/L 01/26/11 11:391,2-Dichlorobenzene
70 - 130 11A496750.0 52.2 104% ug/L 01/26/11 11:391,3-Dichlorobenzene
60 - 140 11A496750.0 37.9 76% ug/L 01/26/11 11:39Dichlorodifluoromethane
70 - 130 11A496750.0 49.6 99% ug/L 01/26/11 11:391,1-Dichloroethane
70 - 130 11A496750.0 50.8 102% ug/L 01/26/11 11:391,2-Dichloroethane
60 - 140 11A496750006140123% ug/L 01/26/11 11:39Ethanol
70 - 130 11A496750.0 49.7 99% ug/L 01/26/11 11:39trans-1,2-Dichloroethene
70 - 130 11A496750.0 57.6 115% ug/L 01/26/11 11:391,1-Dichloroethene
70 - 130 11A496750.0 50.4 101% ug/L 01/26/11 11:39cis-1,2-Dichloroethene
70 - 130 11A496750.0 49.3 99% ug/L 01/26/11 11:391,2-Dichloropropane
70 - 130 11A496750.0 51.4 103% ug/L 01/26/11 11:391,3-Dichloropropane
70 - 130 11A496750.0 51.9 104% ug/L 01/26/11 11:392,2-Dichloropropane
70 - 130 11A496750.0 55.6 111% ug/L 01/26/11 11:39trans-1,3-Dichloropropene
70 - 130 11A496750.0 56.6 113% ug/L 01/26/11 11:39cis-1,3-Dichloropropene
70 - 130 11A496750.0 50.7 101% ug/L 01/26/11 11:391,1-Dichloropropene
70 - 130 11A496750.0 51.6 103% ug/L 01/26/11 11:39Ethylbenzene
70 - 130 11A496750.0 50.3 101% ug/L 01/26/11 11:39Hexachlorobutadiene
70 - 130 11A496750.0 57.4 115% ug/L 01/26/11 11:39Isopropylbenzene
70 - 130 11A496750.0 54.9 110% ug/L 01/26/11 11:39p-Isopropyltoluene
70 - 130 11A496750.0 53.7 107% ug/L 01/26/11 11:39Methylene Chloride
70 - 130 11A496750.0 55.2 110% ug/L 01/26/11 11:39Naphthalene
70 - 130 11A496750.0 53.2 106% ug/L 01/26/11 11:39n-Propylbenzene
70 - 130 11A496750.0 54.1 108% ug/L 01/26/11 11:39Styrene
70 - 130 11A496750.0 52.8 106% ug/L 01/26/11 11:391,1,2,2-Tetrachloroethane
70 - 130 11A496750.0 54.6 109% ug/L 01/26/11 11:391,1,1,2-Tetrachloroethane
70 - 130 11A496750.0 49.8 100% ug/L 01/26/11 11:39Tetrachloroethene
70 - 130 11A496750.0 49.3 99% ug/L 01/26/11 11:39Toluene
70 - 130 11A496750.0 54.4 109% ug/L 01/26/11 11:391,2,3-Trichlorobenzene
70 - 130 11A496750.0 56.0 112% ug/L 01/26/11 11:391,2,4-Trichlorobenzene
Page 18 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
LCS - Cont.
Analyte UnitsKnown Val.Analyzed Val % Rec. BatchQ
Target
Range
Analyzed
Date/Time
Volatile Organic Compounds by SM6200 B
11A4967-BS1
70 - 130 11A496750.0 51.7 103% ug/L 01/26/11 11:391,1,2-Trichloroethane
70 - 130 11A496750.0 50.6 101% ug/L 01/26/11 11:391,1,1-Trichloroethane
70 - 130 11A496750.0 49.7 99% ug/L 01/26/11 11:39Trichloroethene
60 - 140 11A496750.0 46.3 93% ug/L 01/26/11 11:39Trichlorofluoromethane
70 - 130 11A496750.0 52.5 105% ug/L 01/26/11 11:391,2,3-Trichloropropane
70 - 130 11A496750.0 53.5 107% ug/L 01/26/11 11:391,3,5-Trimethylbenzene
70 - 130 11A496750.0 51.9 104% ug/L 01/26/11 11:391,2,4-Trimethylbenzene
60 - 140 11A496750.0 47.8 96% ug/L 01/26/11 11:39Vinyl chloride
70 - 130 11A4967150153102% ug/L 01/26/11 11:39Xylenes, total
70 - 130 11A496750.0 51.5 103% ug/L 01/26/11 11:39Methyl tert-Butyl Ether
70 - 130 11A496750.0 49.5 99% ug/L 01/26/11 11:39Diisopropyl Ether
70 - 130 11A496725.0 24.9Surrogate: 1,2-Dichloroethane-d4 99% 01/26/11 11:39
70 - 130 11A496725.0 25.3Surrogate: Dibromofluoromethane 101% 01/26/11 11:39
70 - 130 11A496725.0 24.9Surrogate: Toluene-d8 100% 01/26/11 11:39
70 - 130 11A496725.0 24.9Surrogate: 4-Bromofluorobenzene 100% 01/26/11 11:39
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-BS1
50 - 120 11A434550.0 38.2 76% ug/L 01/26/11 15:02Acenaphthene
53 - 120 11A434550.0 41.8 84% ug/L 01/26/11 15:02Acenaphthylene
63 - 120 11A434550.0 43.4 87% ug/L 01/26/11 15:02Anthracene
57 - 122 11A434550.0 42.7 85% ug/L 01/26/11 15:02Benzo (a) anthracene
46 - 138 11A434550.0 43.0 86% ug/L 01/26/11 15:02Benzo (a) pyrene
45 - 138 11A434550.0 40.0 80% ug/L 01/26/11 15:02Benzo (b) fluoranthene
48 - 137 11A434550.0 45.8 92% ug/L 01/26/11 15:02Benzo (g,h,i) perylene
44 - 134 11A434550.0 46.4 93% ug/L 01/26/11 15:02Benzo (k) fluoranthene
52 - 120 11A434550.0 40.2 80% ug/L 01/26/11 15:024-Bromophenyl phenyl ether
61 - 133 11A434550.0 42.7 85% ug/L 01/26/11 15:02Butyl benzyl phthalate
60 - 120 11A434550.0 44.6 89% ug/L 01/26/11 15:02Carbazole
49 - 120 11A434550.0 38.7 77% ug/L 01/26/11 15:024-Chloro-3-methylphenol
39 - 120 11A434550.0 35.2 70% ug/L 01/26/11 15:024-Chloroaniline
43 - 120 11A434550.0 38.9 78% ug/L 01/26/11 15:02Bis(2-chloroethoxy)methane
43 - 120 11A434550.0 37.3 75% ug/L 01/26/11 15:02Bis(2-chloroethyl)ether
45 - 120 11A434550.0 33.2 66% ug/L 01/26/11 15:02Bis(2-chloroisopropyl)ether
43 - 120 11A434550.0 38.2 76% ug/L 01/26/11 15:022-Chloronaphthalene
40 - 120 11A434550.0 40.5 81% ug/L 01/26/11 15:022-Chlorophenol
56 - 120 11A434550.0 38.4 77% ug/L 01/26/11 15:024-Chlorophenyl phenyl ether
54 - 123 11A434550.0 40.4 81% ug/L 01/26/11 15:02Chrysene
50 - 136 11A434550.0 45.2 90% ug/L 01/26/11 15:02Dibenz (a,h) anthracene
55 - 120 11A434550.0 41.0 82% ug/L 01/26/11 15:02Dibenzofuran
64 - 120 11A434550.0 43.1 86% ug/L 01/26/11 15:02Di-n-butyl phthalate
Page 19 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
LCS - Cont.
Analyte UnitsKnown Val.Analyzed Val % Rec. BatchQ
Target
Range
Analyzed
Date/Time
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-BS1
27 - 120 11A434550.0 30.7 61% ug/L 01/26/11 15:021,4-Dichlorobenzene
29 - 120 11A434550.0 29.7 59% ug/L 01/26/11 15:021,2-Dichlorobenzene
27 - 120 11A434550.0 30.5 61% ug/L 01/26/11 15:021,3-Dichlorobenzene
49 - 120 11A434550.0 44.8 90% ug/L 01/26/11 15:023,3-Dichlorobenzidine
39 - 120 11A434550.0 35.9 72% ug/L 01/26/11 15:022,4-Dichlorophenol
53 - 120 11A434550.0 41.0 82% ug/L 01/26/11 15:02Diethyl phthalate
28 - 123 11A434550.0 43.2 86% ug/L 01/26/11 15:022,4-Dimethylphenol
59 - 120 11A434550.0 43.2 86% ug/L 01/26/11 15:02Dimethyl phthalate
35 - 132 11A434550.0 44.4 89% ug/L 01/26/11 15:024,6-Dinitro-2-methylphenol
21 - 145 11A434550.0 42.8 86% ug/L 01/26/11 15:022,4-Dinitrophenol
62 - 123 11A434550.0 39.6 79% ug/L 01/26/11 15:022,6-Dinitrotoluene
61 - 124 11A434550.0 42.5 85% ug/L 01/26/11 15:022,4-Dinitrotoluene
51 - 141 11A434550.0 39.2 78% ug/L 01/26/11 15:02Di-n-octyl phthalate
54 - 134 11A434550.0 40.4 81% ug/L 01/26/11 15:02Bis(2-ethylhexyl)phthalate
62 - 120 11A434550.0 42.9 86% ug/L 01/26/11 15:02Fluoranthene
58 - 120 11A434550.0 40.2 80% ug/L 01/26/11 15:02Fluorene
60 - 120 11A434550.0 40.5 81% ug/L 01/26/11 15:02Hexachlorobenzene
24 - 120 11A434550.0 29.1 58% ug/L 01/26/11 15:02Hexachlorobutadiene
19 - 120 11A434550.0 24.4 49% ug/L 01/26/11 15:02Hexachlorocyclopentadiene
26 - 120 11A434550.0 33.3 67% ug/L 01/26/11 15:02Hexachloroethane
50 - 136 11A434550.0 46.9 94% ug/L 01/26/11 15:02Indeno (1,2,3-cd) pyrene
46 - 120 11A434550.0 36.4 73% ug/L 01/26/11 15:02Isophorone
34 - 120 11A434550.0 32.9 66% ug/L 01/26/11 15:022-Methylnaphthalene
38 - 120 11A434550.0 29.8 60% ug/L 01/26/11 15:022-Methylphenol
34 - 120 11A434550.0 29.9 60% ug/L 01/26/11 15:023/4-Methylphenol
32 - 120 11A434550.0 31.2 62% ug/L 01/26/11 15:02Naphthalene
54 - 120 11A434550.0 44.6 89% ug/L 01/26/11 15:023-Nitroaniline
59 - 121 11A434550.0 40.5 81% ug/L 01/26/11 15:022-Nitroaniline
55 - 124 11A434550.0 38.6 77% ug/L 01/26/11 15:024-Nitroaniline
44 - 120 11A434550.0 33.9 68% ug/L 01/26/11 15:02Nitrobenzene
10 - 120 11A434550.0 19.2 38% ug/L 01/26/11 15:024-Nitrophenol
42 - 120 11A434550.0 38.4 77% ug/L 01/26/11 15:022-Nitrophenol
59 - 120 11A434550.0 51.5 103% ug/L 01/26/11 15:02N-Nitrosodiphenylamine
50 - 121 11A434550.0 40.4 81% ug/L 01/26/11 15:02N-Nitrosodi-n-propylamine
36 - 143 11A434550.0 26.7 53% ug/L 01/26/11 15:02Pentachlorophenol
60 - 120 11A434550.0 43.4 87% ug/L 01/26/11 15:02Phenanthrene
10 - 120 11A434550.0 17.1 34% ug/L 01/26/11 15:02Phenol
57 - 124 11A434550.0 43.9 88% ug/L 01/26/11 15:02Pyrene
27 - 120 11A434550.0 31.0 62% ug/L 01/26/11 15:021,2,4-Trichlorobenzene
34 - 120 11A434550.0 31.2 62% ug/L 01/26/11 15:021-Methylnaphthalene
48 - 125 11A434550.0 39.4 79% ug/L 01/26/11 15:022,4,6-Trichlorophenol
Page 20 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
PROJECT QUALITY CONTROL DATA
LCS - Cont.
Analyte UnitsKnown Val.Analyzed Val % Rec. BatchQ
Target
Range
Analyzed
Date/Time
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-BS1
51 - 125 11A434550.0 39.5 79% ug/L 01/26/11 15:022,4,5-Trichlorophenol
13 - 120 11A434550.0 37.7Surrogate: Terphenyl-d14 75% 01/26/11 15:02
29 - 132 11A434550.0 42.9Surrogate: 2,4,6-Tribromophenol 86% 01/26/11 15:02
10 - 120 11A434550.0 13.4Surrogate: Phenol-d5 27% 01/26/11 15:02
29 - 120 11A434550.0 36.6Surrogate: 2-Fluorobiphenyl 73% 01/26/11 15:02
10 - 120 11A434550.0 22.0Surrogate: 2-Fluorophenol 44% 01/26/11 15:02
27 - 120 11A434550.0 32.7Surrogate: Nitrobenzene-d5 65% 01/26/11 15:02
Extractable Petroleum Hydrocarbons
11A4223-BS1
65 - 127 11A422340.0 37.6 94% mg/kg wet 01/25/11 14:57Diesel
53 - 140 11A42230.800 0.732Surrogate: o-Terphenyl 91% 01/25/11 14:57
Purgeable Petroleum Hydrocarbons
11A4142-BS1
70 - 130 11A414210.0 10.5 105% mg/kg wet 01/25/11 10:54GRO as Gasoline
60 - 150 11A414220.0 21.4Surrogate: a,a,a-Trifluorotoluene 107% 01/25/11 10:54
11A4142-BS2
70 - 130 11A414210.0 9.00 90% mg/kg wet 01/25/11 11:22GRO as Gasoline
60 - 150 11A414220.0 73.2Surrogate: a,a,a-Trifluorotoluene 366%Z2 01/25/11 11:22
11A4142-BS3
70 - 130 11A414210.0 10.5 105% mg/kg wet 01/26/11 13:34GRO as Gasoline
60 - 150 11A414220.0 79.9Surrogate: a,a,a-Trifluorotoluene 400%Z2 01/26/11 13:34
11A4142-BS4
70 - 130 11A414210.0 10.5 105% mg/kg wet 01/26/11 13:54GRO as Gasoline
60 - 150 11A414220.0 20.6Surrogate: a,a,a-Trifluorotoluene 103% 01/26/11 13:54
Page 21 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
LCS Dup
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Volatile Organic Compounds by EPA Method 8260B
11A4151-BSD1
246 4 50 11A4151 250 99%ug/kg 60 - 150 01/25/11 13:01Acetone
50.7 0.2 50 11A4151 50.0 101%ug/kg 78 - 126 01/25/11 13:01Benzene
52.2 1 50 11A4151 50.0 104%ug/kg 79 - 126 01/25/11 13:01Bromobenzene
47.5 1 50 11A4151 50.0 95%ug/kg 78 - 126 01/25/11 13:01Bromochloromethane
51.7 0.8 50 11A4151 50.0 103%ug/kg 75 - 129 01/25/11 13:01Bromodichloromethane
38.3 0.2 43 11A4151 50.0 77%ug/kg 74 - 133 01/25/11 13:01Bromoform
52.5 6 46 11A4151 50.0 105%ug/kg 50 - 150 01/25/11 13:01Bromomethane
42.5 4 45 11A4151 50.0 85%ug/kg 62 - 150 01/25/11 13:011,2-Dibromo-3-chloropropane
220 1 50 11A4151 250 88%ug/kg 68 - 149 01/25/11 13:012-Butanone
56.8 6 50 11A4151 50.0 114%ug/kg 76 - 135 01/25/11 13:01sec-Butylbenzene
61.9 7 50 11A4151 50.0 124%ug/kg 73 - 143 01/25/11 13:01n-Butylbenzene
56.1 7 50 11A4151 50.0 112%ug/kg 80 - 129 01/25/11 13:01tert-Butylbenzene
55.9 4 48 11A4151 50.0 112%ug/kg 80 - 132 01/25/11 13:01Carbon disulfide
58.3 0.4 44 11A4151 50.0 117%ug/kg 70 - 138 01/25/11 13:01Carbon Tetrachloride
54.3 3 50 11A4151 50.0 109%ug/kg 80 - 123 01/25/11 13:01Chlorobenzene
48.4 0.06 48 11A4151 50.0 97%ug/kg 80 - 127 01/25/11 13:01Chlorodibromomethane
52.1 4 50 11A4151 50.0 104%ug/kg 55 - 150 01/25/11 13:01Chloroethane
51.7 2 50 11A4151 50.0 103%ug/kg 70 - 127 01/25/11 13:01Chloroform
38.9 8 44 11A4151 50.0 78%ug/kg 36 - 137 01/25/11 13:01Chloromethane
52.8 3 50 11A4151 50.0 106%ug/kg 80 - 130 01/25/11 13:012-Chlorotoluene
55.8 3 50 11A4151 50.0 112%ug/kg 77 - 132 01/25/11 13:014-Chlorotoluene
52.8 4 45 11A4151 50.0 106%ug/kg 80 - 131 01/25/11 13:011,2-Dibromoethane (EDB)
48.4 1 50 11A4151 50.0 97%ug/kg 78 - 128 01/25/11 13:01Dibromomethane
57.3 7 50 11A4151 50.0 115%ug/kg 80 - 129 01/25/11 13:011,4-Dichlorobenzene
56.3 8 50 11A4151 50.0 113%ug/kg 80 - 131 01/25/11 13:011,3-Dichlorobenzene
56.6 8 50 11A4151 50.0 113%ug/kg 80 - 127 01/25/11 13:011,2-Dichlorobenzene
31.5 20 50 11A4151 50.0 63%ug/kg 30 - 150 01/25/11 13:01Dichlorodifluoromethane
53.4 0.1 50 11A4151 50.0 107%ug/kg 71 - 126 01/25/11 13:011,1-Dichloroethane
54.0 1 50 11A4151 50.0 108%ug/kg 70 - 139 01/25/11 13:011,2-Dichloroethane
54.3 0.9 50 11A4151 50.0 109%ug/kg 75 - 126 01/25/11 13:01cis-1,2-Dichloroethene
51.3 2 50 11A4151 50.0 103%ug/kg 70 - 125 01/25/11 13:011,1-Dichloroethene
56.0 0.9 40 11A4151 50.0 112%ug/kg 73 - 128 01/25/11 13:01trans-1,2-Dichloroethene
54.0 3 42 11A4151 50.0 108%ug/kg 79 - 128 01/25/11 13:011,3-Dichloropropane
48.8 0.5 50 11A4151 50.0 98%ug/kg 75 - 120 01/25/11 13:011,2-Dichloropropane
57.7 2 39 11A4151 50.0 115%ug/kg 60 - 139 01/25/11 13:012,2-Dichloropropane
62.7 4 50 11A4151 50.0 125%ug/kg 74 - 136 01/25/11 13:01cis-1,3-Dichloropropene
51.4 1 48 11A4151 50.0 103%ug/kg 73 - 128 01/25/11 13:01trans-1,3-Dichloropropene
54.4 0.8 50 11A4151 50.0 109%ug/kg 78 - 125 01/25/11 13:011,1-Dichloropropene
56.0 2 50 11A4151 50.0 112%ug/kg 79 - 130 01/25/11 13:01Ethylbenzene
57.0 11 50 11A4151 50.0 114%ug/kg 75 - 150 01/25/11 13:01Hexachlorobutadiene
254 0.7 50 11A4151 250 102%ug/kg 65 - 150 01/25/11 13:012-Hexanone
Page 22 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
LCS Dup - Cont.
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Volatile Organic Compounds by EPA Method 8260B
11A4151-BSD1
56.2 3 50 11A4151 50.0 112%ug/kg 65 - 121 01/25/11 13:01Isopropylbenzene
58.2 7 50 11A4151 50.0 116%ug/kg 76 - 133 01/25/11 13:01p-Isopropyltoluene
53.3 1 50 11A4151 50.0 107%ug/kg 70 - 128 01/25/11 13:01Methyl tert-Butyl Ether
49.8 2 50 11A4151 50.0 100%ug/kg 69 - 140 01/25/11 13:01Methylene Chloride
255 0.8 45 11A4151 250 102%ug/kg 67 - 147 01/25/11 13:014-Methyl-2-pentanone
57.4 8 50 11A4151 50.0 115%ug/kg 72 - 150 01/25/11 13:01Naphthalene
54.1 3 50 11A4151 50.0 108%ug/kg 76 - 133 01/25/11 13:01n-Propylbenzene
51.9 3 50 11A4151 50.0 104%ug/kg 80 - 140 01/25/11 13:01Styrene
57.8 2 50 11A4151 50.0 116%ug/kg 80 - 132 01/25/11 13:011,1,1,2-Tetrachloroethane
47.4 1 45 11A4151 50.0 95%ug/kg 75 - 135 01/25/11 13:011,1,2,2-Tetrachloroethane
54.2 1 50 11A4151 50.0 108%ug/kg 76 - 130 01/25/11 13:01Tetrachloroethene
55.0 1 50 11A4151 50.0 110%ug/kg 76 - 126 01/25/11 13:01Toluene
61.8 11 50 11A4151 50.0 124%ug/kg 75 - 150 01/25/11 13:011,2,3-Trichlorobenzene
64.1 11 50 11A4151 50.0 128%ug/kg 64 - 150 01/25/11 13:011,2,4-Trichlorobenzene
51.3 4 50 11A4151 50.0 103%ug/kg 73 - 133 01/25/11 13:011,1,2-Trichloroethane
55.1 0.7 41 11A4151 50.0 110%ug/kg 70 - 132 01/25/11 13:011,1,1-Trichloroethane
47.4 1 50 11A4151 50.0 95%ug/kg 79 - 129 01/25/11 13:01Trichloroethene
52.2 3 47 11A4151 50.0 104%ug/kg 52 - 148 01/25/11 13:01Trichlorofluoromethane
48.3 3 47 11A4151 50.0 97%ug/kg 70 - 125 01/25/11 13:011,2,3-Trichloropropane
56.0 2 50 11A4151 50.0 112%ug/kg 80 - 134 01/25/11 13:011,3,5-Trimethylbenzene
57.5 8 50 11A4151 50.0 115%ug/kg 80 - 132 01/25/11 13:011,2,4-Trimethylbenzene
49.2 4 39 11A4151 50.0 98%ug/kg 53 - 142 01/25/11 13:01Vinyl chloride
169 2 50 11A4151 150 113%ug/kg 80 - 130 01/25/11 13:01Xylenes, total
58.3 2 50 11A4151 50.0 117%ug/kg 71 - 125 01/25/11 13:01Diisopropyl Ether
110 0.03 41 11A4151 100 110%ug/kg 74 - 126 01/25/11 13:011,2-Dichloroethene (total)
54.1 11A4151 50.0 108%Surrogate: 1,2-Dichloroethane-d4 ug/kg 67 - 138 01/25/11 13:01
50.6 11A4151 50.0 101%Surrogate: Dibromofluoromethane ug/kg 75 - 125 01/25/11 13:01
54.4 11A4151 50.0 109%Surrogate: Toluene-d8 ug/kg 76 - 129 01/25/11 13:01
52.1 11A4151 50.0 104%Surrogate: 4-Bromofluorobenzene ug/kg 67 - 147 01/25/11 13:01
Volatile Organic Compounds by SM6200 B
11A4967-BSD1
49.3 1 20 11A4967 50.0 99%ug/L 70 - 130 01/26/11 12:07Benzene
49.2 2 20 11A4967 50.0 98%ug/L 70 - 130 01/26/11 12:07Bromobenzene
45.1 2 20 11A4967 50.0 90%ug/L 70 - 130 01/26/11 12:07Bromochloromethane
52.6 1 20 11A4967 50.0 105%ug/L 70 - 130 01/26/11 12:07Bromodichloromethane
47.2 0.9 20 11A4967 50.0 94%ug/L 70 - 130 01/26/11 12:07Bromoform
53.8 2 20 11A4967 50.0 108%ug/L 60 - 140 01/26/11 12:07Bromomethane
56.1 3 20 11A4967 50.0 112%ug/L 70 - 130 01/26/11 12:07n-Butylbenzene
52.3 3 20 11A4967 50.0 105%ug/L 70 - 130 01/26/11 12:07tert-Butylbenzene
53.6 3 20 11A4967 50.0 107%ug/L 70 - 130 01/26/11 12:07sec-Butylbenzene
Page 23 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
LCS Dup - Cont.
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Volatile Organic Compounds by SM6200 B
11A4967-BSD1
51.7 3 20 11A4967 50.0 103%ug/L 70 - 130 01/26/11 12:07Carbon Tetrachloride
48.8 2 20 11A4967 50.0 98%ug/L 70 - 130 01/26/11 12:07Chlorobenzene
56.8 1 20 11A4967 50.0 114%ug/L 70 - 130 01/26/11 12:07Chlorodibromomethane
44.0 2 20 11A4967 50.0 88%ug/L 60 - 140 01/26/11 12:07Chloroethane
49.6 1 20 11A4967 50.0 99%ug/L 70 - 130 01/26/11 12:07Chloroform
41.1 3 20 11A4967 50.0 82%ug/L 60 - 140 01/26/11 12:07Chloromethane
51.2 3 20 11A4967 50.0 102%ug/L 70 - 130 01/26/11 12:074-Chlorotoluene
49.6 3 20 11A4967 50.0 99%ug/L 70 - 130 01/26/11 12:072-Chlorotoluene
47.8 0.9 20 11A4967 50.0 96%ug/L 70 - 130 01/26/11 12:071,2-Dibromo-3-chloropropane
51.8 2 20 11A4967 50.0 104%ug/L 70 - 130 01/26/11 12:071,2-Dibromoethane (EDB)
50.2 1 20 11A4967 50.0 100%ug/L 70 - 130 01/26/11 12:07Dibromomethane
50.1 2 20 11A4967 50.0 100%ug/L 70 - 130 01/26/11 12:071,4-Dichlorobenzene
51.1 3 20 11A4967 50.0 102%ug/L 70 - 130 01/26/11 12:071,2-Dichlorobenzene
50.8 3 20 11A4967 50.0 102%ug/L 70 - 130 01/26/11 12:071,3-Dichlorobenzene
36.9 3 20 11A4967 50.0 74%ug/L 60 - 140 01/26/11 12:07Dichlorodifluoromethane
48.4 3 20 11A4967 50.0 97%ug/L 70 - 130 01/26/11 12:071,1-Dichloroethane
50.2 1 20 11A4967 50.0 100%ug/L 70 - 130 01/26/11 12:071,2-Dichloroethane
6310 3 20 11A4967 5000 126%ug/L 60 - 140 01/26/11 12:07Ethanol
48.6 2 20 11A4967 50.0 97%ug/L 70 - 130 01/26/11 12:07trans-1,2-Dichloroethene
56.4 2 20 11A4967 50.0 113%ug/L 70 - 130 01/26/11 12:071,1-Dichloroethene
49.5 2 20 11A4967 50.0 99%ug/L 70 - 130 01/26/11 12:07cis-1,2-Dichloroethene
48.7 1 20 11A4967 50.0 97%ug/L 70 - 130 01/26/11 12:071,2-Dichloropropane
50.8 1 20 11A4967 50.0 102%ug/L 70 - 130 01/26/11 12:071,3-Dichloropropane
50.4 3 20 11A4967 50.0 101%ug/L 70 - 130 01/26/11 12:072,2-Dichloropropane
54.6 2 20 11A4967 50.0 109%ug/L 70 - 130 01/26/11 12:07trans-1,3-Dichloropropene
55.8 2 20 11A4967 50.0 112%ug/L 70 - 130 01/26/11 12:07cis-1,3-Dichloropropene
49.6 2 20 11A4967 50.0 99%ug/L 70 - 130 01/26/11 12:071,1-Dichloropropene
50.2 3 20 11A4967 50.0 100%ug/L 70 - 130 01/26/11 12:07Ethylbenzene
49.0 3 20 11A4967 50.0 98%ug/L 70 - 130 01/26/11 12:07Hexachlorobutadiene
56.3 2 20 11A4967 50.0 113%ug/L 70 - 130 01/26/11 12:07Isopropylbenzene
53.0 3 20 11A4967 50.0 106%ug/L 70 - 130 01/26/11 12:07p-Isopropyltoluene
52.7 2 20 11A4967 50.0 105%ug/L 70 - 130 01/26/11 12:07Methylene Chloride
54.0 2 20 11A4967 50.0 108%ug/L 70 - 130 01/26/11 12:07Naphthalene
51.7 3 20 11A4967 50.0 103%ug/L 70 - 130 01/26/11 12:07n-Propylbenzene
53.0 2 20 11A4967 50.0 106%ug/L 70 - 130 01/26/11 12:07Styrene
52.0 2 20 11A4967 50.0 104%ug/L 70 - 130 01/26/11 12:071,1,2,2-Tetrachloroethane
53.3 2 20 11A4967 50.0 107%ug/L 70 - 130 01/26/11 12:071,1,1,2-Tetrachloroethane
48.0 4 20 11A4967 50.0 96%ug/L 70 - 130 01/26/11 12:07Tetrachloroethene
47.9 3 20 11A4967 50.0 96%ug/L 70 - 130 01/26/11 12:07Toluene
53.4 2 20 11A4967 50.0 107%ug/L 70 - 130 01/26/11 12:071,2,3-Trichlorobenzene
54.4 3 20 11A4967 50.0 109%ug/L 70 - 130 01/26/11 12:071,2,4-Trichlorobenzene
Page 24 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
LCS Dup - Cont.
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Volatile Organic Compounds by SM6200 B
11A4967-BSD1
51.2 1 20 11A4967 50.0 102%ug/L 70 - 130 01/26/11 12:071,1,2-Trichloroethane
49.8 2 20 11A4967 50.0 100%ug/L 70 - 130 01/26/11 12:071,1,1-Trichloroethane
48.9 2 20 11A4967 50.0 98%ug/L 70 - 130 01/26/11 12:07Trichloroethene
45.6 2 20 11A4967 50.0 91%ug/L 60 - 140 01/26/11 12:07Trichlorofluoromethane
51.4 2 20 11A4967 50.0 103%ug/L 70 - 130 01/26/11 12:071,2,3-Trichloropropane
51.7 3 20 11A4967 50.0 103%ug/L 70 - 130 01/26/11 12:071,3,5-Trimethylbenzene
50.6 2 20 11A4967 50.0 101%ug/L 70 - 130 01/26/11 12:071,2,4-Trimethylbenzene
47.6 0.4 20 11A4967 50.0 95%ug/L 60 - 140 01/26/11 12:07Vinyl chloride
150 2 20 11A4967 150 100%ug/L 70 - 130 01/26/11 12:07Xylenes, total
51.3 0.4 20 11A4967 50.0 103%ug/L 70 - 130 01/26/11 12:07Methyl tert-Butyl Ether
49.1 0.9 20 11A4967 50.0 98%ug/L 70 - 130 01/26/11 12:07Diisopropyl Ether
25.1 11A4967 25.0 100%Surrogate: 1,2-Dichloroethane-d4 ug/L 70 - 130 01/26/11 12:07
25.2 11A4967 25.0 101%Surrogate: Dibromofluoromethane ug/L 70 - 130 01/26/11 12:07
24.8 11A4967 25.0 99%Surrogate: Toluene-d8 ug/L 70 - 130 01/26/11 12:07
24.9 11A4967 25.0 100%Surrogate: 4-Bromofluorobenzene ug/L 70 - 130 01/26/11 12:07
Page 25 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Analyte Units
PROJECT QUALITY CONTROL DATA
Orig. Val.MS Val Spike Conc % Rec.
Target
Range
Matrix Spike
Q
Analyzed
Date/Time
Sample
SpikedBatch
Volatile Organic Compounds by EPA Method 8260B
11A4151-MS1
0.265 0.279 NUA2649-09 95%ND 11A415129 - 181mg/kg dry 01/25/11 21:30Acetone
0.0445 0.0559 NUA2649-09 80%ND 11A415142 - 141mg/kg dry 01/25/11 21:30Benzene
0.0328 0.0559 NUA2649-09 59%ND 11A415119 - 154mg/kg dry 01/25/11 21:30Bromobenzene
0.0300 0.0559 NUA2649-09 54%ND 11A415141 - 146mg/kg dry 01/25/11 21:30Bromochloromethane
0.0301 0.0559 NUA2649-09 54%ND 11A415132 - 155mg/kg dry 01/25/11 21:30Bromodichloromethane
0.0192 0.0559 NUA2649-09 34%ND 11A415110 - 155mg/kg dry 01/25/11 21:30Bromoform
0.0449 0.0559 NUA2649-09 80%ND 11A415110 - 199mg/kg dry 01/25/11 21:30Bromomethane
0.0229 0.0559 NUA2649-09 41%ND 11A415110 - 167mg/kg dry 01/25/11 21:301,2-Dibromo-3-chloropropane
0.188 0.279 NUA2649-09 67%ND 11A415138 - 161mg/kg dry 01/25/11 21:302-Butanone
0.0462 0.0559 NUA2649-09 83%ND 11A415110 - 170mg/kg dry 01/25/11 21:30sec-Butylbenzene
0.0418 0.0559 NUA2649-09 75%ND 11A415110 - 183mg/kg dry 01/25/11 21:30n-Butylbenzene
0.0481 0.0559 NUA2649-09 86%ND 11A415111 - 165mg/kg dry 01/25/11 21:30tert-Butylbenzene
0.0558 0.0559 NUA2649-09 100%ND 11A415150 - 136mg/kg dry 01/25/11 21:30Carbon disulfide
0.0536 0.0559 NUA2649-09 96%ND 11A415130 - 159mg/kg dry 01/25/11 21:30Carbon Tetrachloride
0.0401 0.0559 NUA2649-09 72%ND 11A415125 - 151mg/kg dry 01/25/11 21:30Chlorobenzene
0.0260 0.0559 NUA2649-09 47%ND 11A415127 - 150mg/kg dry 01/25/11 21:30Chlorodibromomethane
0.0524 0.0559 NUA2649-09 94%ND 11A415115 - 197mg/kg dry 01/25/11 21:30Chloroethane
0.0410 0.0559 NUA2649-09 72%0.000712 11A415133 - 148mg/kg dry 01/25/11 21:30Chloroform
0.0388 0.0559 NUA2649-09 70%ND 11A415110 - 166mg/kg dry 01/25/11 21:30Chloromethane
0.0408 0.0559 NUA2649-09 73%ND 11A415125 - 166mg/kg dry 01/25/11 21:302-Chlorotoluene
0.0396 0.0559 NUA2649-09 71%ND 11A415119 - 163mg/kg dry 01/25/11 21:304-Chlorotoluene
0.0286 0.0559 NUA2649-09 51%ND 11A415130 - 155mg/kg dry 01/25/11 21:301,2-Dibromoethane (EDB)
0.0261 0.0559 NUA2649-09 47%ND 11A415130 - 149mg/kg dry 01/25/11 21:30Dibromomethane
0.0334 0.0559 NUA2649-09 60%ND 11A415110 - 170mg/kg dry 01/25/11 21:301,4-Dichlorobenzene
0.0353 0.0559 NUA2649-09 63%ND 11A415110 - 173mg/kg dry 01/25/11 21:301,3-Dichlorobenzene
0.0316 0.0559 NUA2649-09 57%ND 11A415110 - 168mg/kg dry 01/25/11 21:301,2-Dichlorobenzene
0.0427 0.0559 NUA2649-09 76%ND 11A415110 - 188mg/kg dry 01/25/11 21:30Dichlorodifluoromethane
0.0460 0.0559 NUA2649-09 82%ND 11A415151 - 135mg/kg dry 01/25/11 21:301,1-Dichloroethane
0.0314 0.0559 NUA2649-09 56%ND 11A415132 - 155mg/kg dry 01/25/11 21:301,2-Dichloroethane
0.0434 0.0559 NUA2649-09 78%ND 11A415132 - 150mg/kg dry 01/25/11 21:30cis-1,2-Dichloroethene
0.0524 0.0559 NUA2649-09 94%ND 11A415146 - 141mg/kg dry 01/25/11 21:301,1-Dichloroethene
0.0501 0.0559 NUA2649-09 90%ND 11A415141 - 146mg/kg dry 01/25/11 21:30trans-1,2-Dichloroethene
0.0326 0.0559 NUA2649-09 58%ND 11A415135 - 148mg/kg dry 01/25/11 21:301,3-Dichloropropane
0.0369 0.0559 NUA2649-09 66%ND 11A415134 - 139mg/kg dry 01/25/11 21:301,2-Dichloropropane
0.0576 0.0559 NUA2649-09 103%ND 11A415129 - 152mg/kg dry 01/25/11 21:302,2-Dichloropropane
0.0398 0.0559 NUA2649-09 71%ND 11A415123 - 152mg/kg dry 01/25/11 21:30cis-1,3-Dichloropropene
0.0301 0.0559 NUA2649-09 54%ND 11A415124 - 151mg/kg dry 01/25/11 21:30trans-1,3-Dichloropropene
Page 26 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Analyte Units
PROJECT QUALITY CONTROL DATA
Orig. Val.MS Val Spike Conc % Rec.
Target
Range
Matrix Spike - Cont.
Q
Analyzed
Date/Time
Sample
SpikedBatch
Volatile Organic Compounds by EPA Method 8260B
11A4151-MS1
0.0548 0.0559 NUA2649-09 98%ND 11A415140 - 151mg/kg dry 01/25/11 21:301,1-Dichloropropene
0.0474 0.0559 NUA2649-09 85%ND 11A415121 - 165mg/kg dry 01/25/11 21:30Ethylbenzene
0.0319 0.0559 NUA2649-09 57%ND 11A415110 - 173mg/kg dry 01/25/11 21:30Hexachlorobutadiene
0.155 0.279 NUA2649-09 55%ND 11A415113 - 174mg/kg dry 01/25/11 21:302-Hexanone
0.0434 0.0559 NUA2649-09 78%ND 11A415120 - 139mg/kg dry 01/25/11 21:30Isopropylbenzene
0.0433 0.0559 NUA2649-09 78%ND 11A415110 - 164mg/kg dry 01/25/11 21:30p-Isopropyltoluene
0.0307 0.0559 NUA2649-09 55%ND 11A415134 - 154mg/kg dry 01/25/11 21:30Methyl tert-Butyl Ether
0.0421 0.0559 NUA2649-09 62%0.00770 11A415136 - 163mg/kg dry 01/25/11 21:30Methylene Chloride
0.144 0.279 NUA2649-09 52%ND 11A415119 - 176mg/kg dry 01/25/11 21:304-Methyl-2-pentanone
0.0238 0.0559 NUA2649-09 43%ND 11A415110 - 160mg/kg dry 01/25/11 21:30Naphthalene
0.0454 0.0559 NUA2649-09 81%ND 11A415116 - 174mg/kg dry 01/25/11 21:30n-Propylbenzene
0.0273 0.0559 NUA2649-09 49%ND 11A415110 - 177mg/kg dry 01/25/11 21:30Styrene
0.0374 0.0559 NUA2649-09 67%ND 11A415131 - 150mg/kg dry 01/25/11 21:301,1,1,2-Tetrachloroethane
0.0238 0.0559 NUA2649-09 43%ND 11A415127 - 163mg/kg dry 01/25/11 21:301,1,2,2-Tetrachloroethane
0.915 0.0559 NUA2649-09MHA 743%0.500 11A415133 - 155mg/kg dry 01/25/11 21:30Tetrachloroethene
0.0493 0.0559 NUA2649-09 88%ND 11A415145 - 145mg/kg dry 01/25/11 21:30Toluene
0.0250 0.0559 NUA2649-09 45%ND 11A415110 - 182mg/kg dry 01/25/11 21:301,2,3-Trichlorobenzene
0.0273 0.0559 NUA2649-09 49%ND 11A415110 - 175mg/kg dry 01/25/11 21:301,2,4-Trichlorobenzene
0.0291 0.0559 NUA2649-09 52%ND 11A415143 - 145mg/kg dry 01/25/11 21:301,1,2-Trichloroethane
0.0527 0.0559 NUA2649-09 94%ND 11A415139 - 148mg/kg dry 01/25/11 21:301,1,1-Trichloroethane
0.0446 0.0559 NUA2649-09 80%ND 11A415139 - 150mg/kg dry 01/25/11 21:30Trichloroethene
0.0524 0.0559 NUA2649-09 94%ND 11A415125 - 174mg/kg dry 01/25/11 21:30Trichlorofluoromethane
0.0250 0.0559 NUA2649-09 45%ND 11A415110 - 152mg/kg dry 01/25/11 21:301,2,3-Trichloropropane
0.0443 0.0559 NUA2649-09 79%ND 11A415138 - 148mg/kg dry 01/25/11 21:301,3,5-Trimethylbenzene
0.0423 0.0559 NUA2649-09 76%ND 11A415122 - 164mg/kg dry 01/25/11 21:301,2,4-Trimethylbenzene
0.0532 0.0559 NUA2649-09 95%ND 11A415132 - 163mg/kg dry 01/25/11 21:30Vinyl chloride
0.132 0.168 NUA2649-09 79%ND 11A415131 - 159mg/kg dry 01/25/11 21:30Xylenes, total
0.0422 0.0559 NUA2649-09 75%ND 11A415144 - 141mg/kg dry 01/25/11 21:30Diisopropyl Ether
0.0936 0.112 NUA2649-09 84%ND 11A415138 - 147mg/kg dry 01/25/11 21:301,2-Dichloroethene (total)
48.4 50.0 NUA2649-09 Surrogate: 1,2-Dichloroethane-d4 97%11A415167 - 138ug/kg 01/25/11 21:30
45.9 50.0 NUA2649-09 Surrogate: Dibromofluoromethane 92%11A415175 - 125ug/kg 01/25/11 21:30
53.9 50.0 NUA2649-09 Surrogate: Toluene-d8 108%11A415176 - 129ug/kg 01/25/11 21:30
50.8 50.0 NUA2649-09 Surrogate: 4-Bromofluorobenzene 102%11A415167 - 147ug/kg 01/25/11 21:30
Volatile Organic Compounds by SM6200 B
11A4967-MS1
49.6 50.0 NUA2478-01 99%ND 11A496770 - 130ug/L 01/26/11 21:09Benzene
Page 27 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Analyte Units
PROJECT QUALITY CONTROL DATA
Orig. Val.MS Val Spike Conc % Rec.
Target
Range
Matrix Spike - Cont.
Q
Analyzed
Date/Time
Sample
SpikedBatch
Volatile Organic Compounds by SM6200 B
11A4967-MS1
51.4 50.0 NUA2478-01 103%ND 11A496770 - 130ug/L 01/26/11 21:09Bromobenzene
39.8 50.0 NUA2478-01 80%ND 11A496770 - 130ug/L 01/26/11 21:09Bromochloromethane
54.9 50.0 NUA2478-01 110%ND 11A496770 - 130ug/L 01/26/11 21:09Bromodichloromethane
47.3 50.0 NUA2478-01 95%ND 11A496770 - 130ug/L 01/26/11 21:09Bromoform
54.5 50.0 NUA2478-01 109%ND 11A496760 - 140ug/L 01/26/11 21:09Bromomethane
61.5 50.0 NUA2478-01 123%ND 11A496770 - 130ug/L 01/26/11 21:09n-Butylbenzene
57.9 50.0 NUA2478-01 116%ND 11A496770 - 130ug/L 01/26/11 21:09tert-Butylbenzene
59.5 50.0 NUA2478-01 119%ND 11A496770 - 130ug/L 01/26/11 21:09sec-Butylbenzene
55.3 50.0 NUA2478-01 111%ND 11A496770 - 130ug/L 01/26/11 21:09Carbon Tetrachloride
50.2 50.0 NUA2478-01 100%ND 11A496770 - 130ug/L 01/26/11 21:09Chlorobenzene
58.9 50.0 NUA2478-01 118%ND 11A496770 - 130ug/L 01/26/11 21:09Chlorodibromomethane
41.9 50.0 NUA2478-01 84%ND 11A496760 - 140ug/L 01/26/11 21:09Chloroethane
52.2 50.0 NUA2478-01 104%ND 11A496770 - 130ug/L 01/26/11 21:09Chloroform
34.8 50.0 NUA2478-01 70%ND 11A496760 - 140ug/L 01/26/11 21:09Chloromethane
53.6 50.0 NUA2478-01 107%ND 11A496770 - 130ug/L 01/26/11 21:094-Chlorotoluene
52.4 50.0 NUA2478-01 105%ND 11A496770 - 130ug/L 01/26/11 21:092-Chlorotoluene
47.1 50.0 NUA2478-01 94%ND 11A496770 - 130ug/L 01/26/11 21:091,2-Dibromo-3-chloropropane
51.2 50.0 NUA2478-01 102%ND 11A496770 - 130ug/L 01/26/11 21:091,2-Dibromoethane (EDB)
49.7 50.0 NUA2478-01 99%ND 11A496770 - 130ug/L 01/26/11 21:09Dibromomethane
52.6 50.0 NUA2478-01 105%ND 11A496770 - 130ug/L 01/26/11 21:091,4-Dichlorobenzene
53.7 50.0 NUA2478-01 107%ND 11A496770 - 130ug/L 01/26/11 21:091,2-Dichlorobenzene
53.4 50.0 NUA2478-01 107%ND 11A496770 - 130ug/L 01/26/11 21:091,3-Dichlorobenzene
30.4 50.0 NUA2478-01 61%ND 11A496760 - 140ug/L 01/26/11 21:09Dichlorodifluoromethane
50.4 50.0 NUA2478-01 101%ND 11A496770 - 130ug/L 01/26/11 21:091,1-Dichloroethane
50.0 50.0 NUA2478-01 100%ND 11A496770 - 130ug/L 01/26/11 21:091,2-Dichloroethane
7910 5000 NUA2478-01M7 158%ND 11A496770 - 130ug/L 01/26/11 21:09Ethanol
46.6 50.0 NUA2478-01 93%ND 11A496770 - 130ug/L 01/26/11 21:09trans-1,2-Dichloroethene
56.0 50.0 NUA2478-01 112%ND 11A496770 - 130ug/L 01/26/11 21:091,1-Dichloroethene
51.3 50.0 NUA2478-01 103%ND 11A496770 - 130ug/L 01/26/11 21:09cis-1,2-Dichloroethene
50.3 50.0 NUA2478-01 101%ND 11A496770 - 130ug/L 01/26/11 21:091,2-Dichloropropane
51.1 50.0 NUA2478-01 102%ND 11A496770 - 130ug/L 01/26/11 21:091,3-Dichloropropane
53.2 50.0 NUA2478-01 106%ND 11A496770 - 130ug/L 01/26/11 21:092,2-Dichloropropane
54.3 50.0 NUA2478-01 109%ND 11A496770 - 130ug/L 01/26/11 21:09trans-1,3-Dichloropropene
56.0 50.0 NUA2478-01 112%ND 11A496770 - 130ug/L 01/26/11 21:09cis-1,3-Dichloropropene
50.3 50.0 NUA2478-01 101%ND 11A496770 - 130ug/L 01/26/11 21:091,1-Dichloropropene
52.1 50.0 NUA2478-01 104%ND 11A496770 - 130ug/L 01/26/11 21:09Ethylbenzene
56.2 50.0 NUA2478-01 112%ND 11A496770 - 130ug/L 01/26/11 21:09Hexachlorobutadiene
Page 28 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Analyte Units
PROJECT QUALITY CONTROL DATA
Orig. Val.MS Val Spike Conc % Rec.
Target
Range
Matrix Spike - Cont.
Q
Analyzed
Date/Time
Sample
SpikedBatch
Volatile Organic Compounds by SM6200 B
11A4967-MS1
60.1 50.0 NUA2478-01 120%ND 11A496770 - 130ug/L 01/26/11 21:09Isopropylbenzene
57.6 50.0 NUA2478-01 115%ND 11A496770 - 130ug/L 01/26/11 21:09p-Isopropyltoluene
51.2 50.0 NUA2478-01 102%ND 11A496770 - 130ug/L 01/26/11 21:09Methylene Chloride
56.1 50.0 NUA2478-01 112%ND 11A496770 - 130ug/L 01/26/11 21:09Naphthalene
55.0 50.0 NUA2478-01 110%ND 11A496770 - 130ug/L 01/26/11 21:09n-Propylbenzene
54.6 50.0 NUA2478-01 109%ND 11A496770 - 130ug/L 01/26/11 21:09Styrene
52.7 50.0 NUA2478-01 105%ND 11A496770 - 130ug/L 01/26/11 21:091,1,2,2-Tetrachloroethane
56.6 50.0 NUA2478-01 113%ND 11A496770 - 130ug/L 01/26/11 21:091,1,1,2-Tetrachloroethane
48.2 50.0 NUA2478-01 96%ND 11A496770 - 130ug/L 01/26/11 21:09Tetrachloroethene
48.4 50.0 NUA2478-01 97%ND 11A496770 - 130ug/L 01/26/11 21:09Toluene
56.1 50.0 NUA2478-01 112%ND 11A496770 - 130ug/L 01/26/11 21:091,2,3-Trichlorobenzene
57.6 50.0 NUA2478-01 115%ND 11A496770 - 130ug/L 01/26/11 21:091,2,4-Trichlorobenzene
52.6 50.0 NUA2478-01 105%ND 11A496770 - 130ug/L 01/26/11 21:091,1,2-Trichloroethane
53.4 50.0 NUA2478-01 107%ND 11A496770 - 130ug/L 01/26/11 21:091,1,1-Trichloroethane
49.6 50.0 NUA2478-01 99%ND 11A496770 - 130ug/L 01/26/11 21:09Trichloroethene
54.0 50.0 NUA2478-01 108%ND 11A496760 - 140ug/L 01/26/11 21:09Trichlorofluoromethane
51.0 50.0 NUA2478-01 102%ND 11A496770 - 130ug/L 01/26/11 21:091,2,3-Trichloropropane
54.7 50.0 NUA2478-01 109%ND 11A496770 - 130ug/L 01/26/11 21:091,3,5-Trimethylbenzene
53.1 50.0 NUA2478-01 106%ND 11A496770 - 130ug/L 01/26/11 21:091,2,4-Trimethylbenzene
42.8 50.0 NUA2478-01 86%ND 11A496760 - 140ug/L 01/26/11 21:09Vinyl chloride
154 150 NUA2478-01 102%ND 11A496770 - 130ug/L 01/26/11 21:09Xylenes, total
76.6 50.0 NUA2478-01 104%24.4 11A496770 - 130ug/L 01/26/11 21:09Methyl tert-Butyl Ether
50.2 50.0 NUA2478-01 100%ND 11A496770 - 130ug/L 01/26/11 21:09Diisopropyl Ether
24.6 25.0 NUA2478-01 Surrogate: 1,2-Dichloroethane-d4 98%11A496770 - 130ug/L 01/26/11 21:09
25.3 25.0 NUA2478-01 Surrogate: Dibromofluoromethane 101%11A496770 - 130ug/L 01/26/11 21:09
24.7 25.0 NUA2478-01 Surrogate: Toluene-d8 99%11A496770 - 130ug/L 01/26/11 21:09
24.8 25.0 NUA2478-01 Surrogate: 4-Bromofluorobenzene 99%11A496770 - 130ug/L 01/26/11 21:09
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-MS1
43.6 50.0 NUA2165-01R
E1
87%ND 11A434550 - 120ug/L 01/25/11 17:08Acenaphthene
44.1 50.0 NUA2165-01R
E1
88%ND 11A434553 - 120ug/L 01/25/11 17:08Acenaphthylene
45.2 50.0 NUA2165-01R
E1
90%ND 11A434556 - 124ug/L 01/25/11 17:08Anthracene
43.5 50.0 NUA2165-01R
E1
87%ND 11A434557 - 122ug/L 01/25/11 17:08Benzo (a) anthracene
42.9 50.0 NUA2165-01R
E1
86%ND 11A434546 - 138ug/L 01/25/11 17:08Benzo (a) pyrene
Page 29 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Analyte Units
PROJECT QUALITY CONTROL DATA
Orig. Val.MS Val Spike Conc % Rec.
Target
Range
Matrix Spike - Cont.
Q
Analyzed
Date/Time
Sample
SpikedBatch
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-MS1
39.5 50.0 NUA2165-01R
E1
79%ND 11A434545 - 138ug/L 01/25/11 17:08Benzo (b) fluoranthene
41.2 50.0 NUA2165-01R
E1
82%ND 11A434548 - 137ug/L 01/25/11 17:08Benzo (g,h,i) perylene
46.4 50.0 NUA2165-01R
E1
93%ND 11A434544 - 134ug/L 01/25/11 17:08Benzo (k) fluoranthene
40.8 50.0 NUA2165-01R
E1
82%ND 11A434550 - 120ug/L 01/25/11 17:084-Bromophenyl phenyl ether
42.1 50.0 NUA2165-01R
E1
84%ND 11A434559 - 134ug/L 01/25/11 17:08Butyl benzyl phthalate
45.2 50.0 NUA2165-01R
E1
90%ND 11A434553 - 120ug/L 01/25/11 17:08Carbazole
37.4 50.0 NUA2165-01R
E1
75%ND 11A434538 - 120ug/L 01/25/11 17:084-Chloro-3-methylphenol
34.3 50.0 NUA2165-01R
E1
69%ND 11A434535 - 120ug/L 01/25/11 17:084-Chloroaniline
39.4 50.0 NUA2165-01R
E1
79%ND 11A434541 - 120ug/L 01/25/11 17:08Bis(2-chloroethoxy)methane
39.4 50.0 NUA2165-01R
E1
79%ND 11A434542 - 120ug/L 01/25/11 17:08Bis(2-chloroethyl)ether
38.8 50.0 NUA2165-01R
E1
78%ND 11A434545 - 120ug/L 01/25/11 17:08Bis(2-chloroisopropyl)ether
40.2 50.0 NUA2165-01R
E1
80%ND 11A434543 - 120ug/L 01/25/11 17:082-Chloronaphthalene
41.8 50.0 NUA2165-01R
E1
84%ND 11A434540 - 120ug/L 01/25/11 17:082-Chlorophenol
42.6 50.0 NUA2165-01R
E1
85%ND 11A434556 - 120ug/L 01/25/11 17:084-Chlorophenyl phenyl ether
41.7 50.0 NUA2165-01R
E1
83%ND 11A434554 - 123ug/L 01/25/11 17:08Chrysene
43.4 50.0 NUA2165-01R
E1
87%ND 11A434550 - 136ug/L 01/25/11 17:08Dibenz (a,h) anthracene
45.1 50.0 NUA2165-01R
E1
90%ND 11A434555 - 120ug/L 01/25/11 17:08Dibenzofuran
44.8 50.0 NUA2165-01R
E1
90%ND 11A434563 - 120ug/L 01/25/11 17:08Di-n-butyl phthalate
36.5 50.0 NUA2165-01R
E1
73%ND 11A434542 - 120ug/L 01/25/11 17:081,4-Dichlorobenzene
37.0 50.0 NUA2165-01R
E1
74%ND 11A434529 - 120ug/L 01/25/11 17:081,2-Dichlorobenzene
37.0 50.0 NUA2165-01R
E1
74%ND 11A434527 - 120ug/L 01/25/11 17:081,3-Dichlorobenzene
24.2 50.0 NUA2165-01R
E1
48%ND 11A434510 - 130ug/L 01/25/11 17:083,3-Dichlorobenzidine
36.1 50.0 NUA2165-01R
E1
72%ND 11A434539 - 120ug/L 01/25/11 17:082,4-Dichlorophenol
42.1 50.0 NUA2165-01R
E1
84%ND 11A434553 - 120ug/L 01/25/11 17:08Diethyl phthalate
Page 30 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Analyte Units
PROJECT QUALITY CONTROL DATA
Orig. Val.MS Val Spike Conc % Rec.
Target
Range
Matrix Spike - Cont.
Q
Analyzed
Date/Time
Sample
SpikedBatch
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-MS1
44.1 50.0 NUA2165-01R
E1
88%ND 11A434511 - 130ug/L 01/25/11 17:082,4-Dimethylphenol
42.9 50.0 NUA2165-01R
E1
86%ND 11A434559 - 120ug/L 01/25/11 17:08Dimethyl phthalate
37.8 50.0 NUA2165-01R
E1
76%ND 11A434510 - 157ug/L 01/25/11 17:084,6-Dinitro-2-methylphenol
43.5 50.0 NUA2165-01R
E1
87%ND 11A434510 - 176ug/L 01/25/11 17:082,4-Dinitrophenol
45.1 50.0 NUA2165-01R
E1
90%ND 11A434562 - 120ug/L 01/25/11 17:082,6-Dinitrotoluene
43.3 50.0 NUA2165-01R
E1
87%ND 11A434561 - 124ug/L 01/25/11 17:082,4-Dinitrotoluene
39.8 50.0 NUA2165-01R
E1
80%ND 11A434556 - 141ug/L 01/25/11 17:08Di-n-octyl phthalate
41.5 50.0 NUA2165-01R
E1
83%ND 11A434544 - 134ug/L 01/25/11 17:08Bis(2-ethylhexyl)phthalate
44.3 50.0 NUA2165-01R
E1
89%ND 11A434560 - 120ug/L 01/25/11 17:08Fluoranthene
44.0 50.0 NUA2165-01R
E1
88%ND 11A434559 - 120ug/L 01/25/11 17:08Fluorene
42.6 50.0 NUA2165-01R
E1
85%ND 11A434554 - 120ug/L 01/25/11 17:08Hexachlorobenzene
33.1 50.0 NUA2165-01R
E1
66%ND 11A434524 - 120ug/L 01/25/11 17:08Hexachlorobutadiene
9.98 50.0 NUA2165-01R
E1
20%ND 11A434510 - 120ug/L 01/25/11 17:08Hexachlorocyclopentadiene
36.4 50.0 NUA2165-01R
E1
73%ND 11A434526 - 120ug/L 01/25/11 17:08Hexachloroethane
43.2 50.0 NUA2165-01R
E1
86%ND 11A434550 - 136ug/L 01/25/11 17:08Indeno (1,2,3-cd) pyrene
35.1 50.0 NUA2165-01R
E1
70%ND 11A434542 - 120ug/L 01/25/11 17:08Isophorone
34.6 50.0 NUA2165-01R
E1
69%ND 11A434534 - 120ug/L 01/25/11 17:082-Methylnaphthalene
35.3 50.0 NUA2165-01R
E1
71%ND 11A434536 - 120ug/L 01/25/11 17:082-Methylphenol
31.0 50.0 NUA2165-01R
E1
62%ND 11A434532 - 120ug/L 01/25/11 17:083/4-Methylphenol
33.8 50.0 NUA2165-01R
E1
68%ND 11A434532 - 120ug/L 01/25/11 17:08Naphthalene
42.8 50.0 NUA2165-01R
E1
86%ND 11A434538 - 120ug/L 01/25/11 17:083-Nitroaniline
44.4 50.0 NUA2165-01R
E1
89%ND 11A434551 - 126ug/L 01/25/11 17:082-Nitroaniline
46.0 50.0 NUA2165-01R
E1
92%ND 11A434547 - 124ug/L 01/25/11 17:084-Nitroaniline
33.8 50.0 NUA2165-01R
E1
68%ND 11A434541 - 120ug/L 01/25/11 17:08Nitrobenzene
Page 31 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Analyte Units
PROJECT QUALITY CONTROL DATA
Orig. Val.MS Val Spike Conc % Rec.
Target
Range
Matrix Spike - Cont.
Q
Analyzed
Date/Time
Sample
SpikedBatch
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-MS1
22.7 50.0 NUA2165-01R
E1
45%ND 11A434510 - 120ug/L 01/25/11 17:084-Nitrophenol
39.8 50.0 NUA2165-01R
E1
80%ND 11A434535 - 120ug/L 01/25/11 17:082-Nitrophenol
52.8 50.0 NUA2165-01R
E1
106%ND 11A434545 - 124ug/L 01/25/11 17:08N-Nitrosodiphenylamine
42.5 50.0 NUA2165-01R
E1
85%ND 11A434550 - 121ug/L 01/25/11 17:08N-Nitrosodi-n-propylamine
40.8 50.0 NUA2165-01R
E1
82%ND 11A434546 - 159ug/L 01/25/11 17:08Pentachlorophenol
45.9 50.0 NUA2165-01R
E1
92%ND 11A434553 - 120ug/L 01/25/11 17:08Phenanthrene
20.9 50.0 NUA2165-01R
E1
42%ND 11A434510 - 120ug/L 01/25/11 17:08Phenol
38.0 50.0 NUA2165-01R
E1
76%ND 11A434550 - 129ug/L 01/25/11 17:08Pyrene
31.1 50.0 NUA2165-01R
E1
62%ND 11A434527 - 120ug/L 01/25/11 17:081,2,4-Trichlorobenzene
32.6 50.0 NUA2165-01R
E1
65%ND 11A434534 - 120ug/L 01/25/11 17:081-Methylnaphthalene
44.0 50.0 NUA2165-01R
E1
88%ND 11A434548 - 125ug/L 01/25/11 17:082,4,6-Trichlorophenol
40.8 50.0 NUA2165-01R
E1
82%ND 11A434551 - 125ug/L 01/25/11 17:082,4,5-Trichlorophenol
32.1 50.0 NUA2165-01R
E1
Surrogate: Terphenyl-d14 64%11A434513 - 120ug/L 01/25/11 17:08
49.4 50.0 NUA2165-01R
E1
Surrogate: 2,4,6-Tribromophenol 99%11A434529 - 132ug/L 01/25/11 17:08
15.4 50.0 NUA2165-01R
E1
Surrogate: Phenol-d5 31%11A434510 - 120ug/L 01/25/11 17:08
38.0 50.0 NUA2165-01R
E1
Surrogate: 2-Fluorobiphenyl 76%11A434529 - 120ug/L 01/25/11 17:08
25.5 50.0 NUA2165-01R
E1
Surrogate: 2-Fluorophenol 51%11A434510 - 120ug/L 01/25/11 17:08
34.0 50.0 NUA2165-01R
E1
Surrogate: Nitrobenzene-d5 68%11A434527 - 120ug/L 01/25/11 17:08
Extractable Petroleum Hydrocarbons
11A4223-MS1
39.7 48.3 NUA2663-02 76%2.89 11A422323 - 138mg/kg dry 01/25/11 15:16Diesel
0.748 0.967 NUA2663-02 Surrogate: o-Terphenyl 77%11A422353 - 140mg/kg dry 01/25/11 15:16
Purgeable Petroleum Hydrocarbons
11A4142-MS1
1250 500 NUA2619-12M1 249%11A414263 - 134mg/kg wet 01/26/11 11:39GRO as Gasoline
0.00 20.0 NUA2619-12Z Surrogate: a,a,a-Trifluorotoluene 0%11A414260 - 150ug/L 01/26/11 11:39
Page 32 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Analyte Units
PROJECT QUALITY CONTROL DATA
Orig. Val.MS Val Spike Conc % Rec.
Target
Range
Matrix Spike - Cont.
Q
Analyzed
Date/Time
Sample
SpikedBatch
Purgeable Petroleum Hydrocarbons
11A4142-MS2
866 500 NUA2619-13M1 136%186 11A414263 - 134mg/kg wet 01/26/11 12:17GRO as Gasoline
20.3 20.0 NUA2619-13 Surrogate: a,a,a-Trifluorotoluene 102%11A414260 - 150ug/L 01/26/11 12:17
Page 33 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
Matrix Spike Dup
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Volatile Organic Compounds by EPA Method 8260B
11A4151-MSD1
ND 0.331 22 50 11A4151 NUA2649-09 0.283 117%mg/kg dry 29 - 181 01/25/11 22:00Acetone
ND 0.0529 17 50 11A4151 NUA2649-09 0.0566 93%mg/kg dry 42 - 141 01/25/11 22:00Benzene
ND 0.0433 28 50 11A4151 NUA2649-09 0.0566 77%mg/kg dry 19 - 154 01/25/11 22:00Bromobenzene
ND 0.0377 23 50 11A4151 NUA2649-09 0.0566 67%mg/kg dry 41 - 146 01/25/11 22:00Bromochloromethane
ND 0.0385 25 50 11A4151 NUA2649-09 0.0566 68%mg/kg dry 32 - 155 01/25/11 22:00Bromodichloromethane
ND 0.0238 21 43 11A4151 NUA2649-09 0.0566 42%mg/kg dry 10 - 155 01/25/11 22:00Bromoform
ND 0.0520 15 46 11A4151 NUA2649-09 0.0566 92%mg/kg dry 10 - 199 01/25/11 22:00Bromomethane
ND 0.0314 32 45 11A4151 NUA2649-09 0.0566 56%mg/kg dry 10 - 167 01/25/11 22:001,2-Dibromo-3-chloropropane
ND 0.235 22 50 11A4151 NUA2649-09 0.283 83%mg/kg dry 38 - 161 01/25/11 22:002-Butanone
ND 0.0601 26 50 11A4151 NUA2649-09 0.0566 106%mg/kg dry 10 - 170 01/25/11 22:00sec-Butylbenzene
ND 0.0572 31 50 11A4151 NUA2649-09 0.0566 101%mg/kg dry 10 - 183 01/25/11 22:00n-Butylbenzene
ND 0.0611 24 50 11A4151 NUA2649-09 0.0566 108%mg/kg dry 11 - 165 01/25/11 22:00tert-Butylbenzene
ND 0.0642 14 48 11A4151 NUA2649-09 0.0566 114%mg/kg dry 50 - 136 01/25/11 22:00Carbon disulfide
ND 0.0624 15 44 11A4151 NUA2649-09 0.0566 110%mg/kg dry 30 - 159 01/25/11 22:00Carbon Tetrachloride
ND 0.0507 23 50 11A4151 NUA2649-09 0.0566 90%mg/kg dry 25 - 151 01/25/11 22:00Chlorobenzene
ND 0.0332 24 48 11A4151 NUA2649-09 0.0566 59%mg/kg dry 27 - 150 01/25/11 22:00Chlorodibromomethane
ND 0.0585 11 50 11A4151 NUA2649-09 0.0566 104%mg/kg dry 15 - 197 01/25/11 22:00Chloroethane
0.000712 0.0488 17 50 11A4151 NUA2649-09 0.0566 85%mg/kg dry 33 - 148 01/25/11 22:00Chloroform
ND 0.0451 15 44 11A4151 NUA2649-09 0.0566 80%mg/kg dry 10 - 166 01/25/11 22:00Chloromethane
ND 0.0524 25 50 11A4151 NUA2649-09 0.0566 93%mg/kg dry 25 - 166 01/25/11 22:002-Chlorotoluene
ND 0.0516 26 50 11A4151 NUA2649-09 0.0566 91%mg/kg dry 19 - 163 01/25/11 22:004-Chlorotoluene
ND 0.0389 30 45 11A4151 NUA2649-09 0.0566 69%mg/kg dry 30 - 155 01/25/11 22:001,2-Dibromoethane (EDB)
ND 0.0349 29 50 11A4151 NUA2649-09 0.0566 62%mg/kg dry 30 - 149 01/25/11 22:00Dibromomethane
ND 0.0459 31 50 11A4151 NUA2649-09 0.0566 81%mg/kg dry 10 - 170 01/25/11 22:001,4-Dichlorobenzene
ND 0.0474 29 50 11A4151 NUA2649-09 0.0566 84%mg/kg dry 10 - 173 01/25/11 22:001,3-Dichlorobenzene
ND 0.0435 32 50 11A4151 NUA2649-09 0.0566 77%mg/kg dry 10 - 168 01/25/11 22:001,2-Dichlorobenzene
ND 0.0493 14 50 11A4151 NUA2649-09 0.0566 87%mg/kg dry 10 - 188 01/25/11 22:00Dichlorodifluoromethane
ND 0.0535 15 50 11A4151 NUA2649-09 0.0566 95%mg/kg dry 51 - 135 01/25/11 22:001,1-Dichloroethane
ND 0.0400 24 50 11A4151 NUA2649-09 0.0566 71%mg/kg dry 32 - 155 01/25/11 22:001,2-Dichloroethane
ND 0.0518 17 50 11A4151 NUA2649-09 0.0566 92%mg/kg dry 32 - 150 01/25/11 22:00cis-1,2-Dichloroethene
ND 0.0603 14 50 11A4151 NUA2649-09 0.0566 107%mg/kg dry 46 - 141 01/25/11 22:001,1-Dichloroethene
ND 0.0586 16 40 11A4151 NUA2649-09 0.0566 104%mg/kg dry 41 - 146 01/25/11 22:00trans-1,2-Dichloroethene
ND 0.0432 28 42 11A4151 NUA2649-09 0.0566 76%mg/kg dry 35 - 148 01/25/11 22:001,3-Dichloropropane
ND 0.0451 20 50 11A4151 NUA2649-09 0.0566 80%mg/kg dry 34 - 139 01/25/11 22:001,2-Dichloropropane
ND 0.0661 14 39 11A4151 NUA2649-09 0.0566 117%mg/kg dry 29 - 152 01/25/11 22:002,2-Dichloropropane
ND 0.0508 24 50 11A4151 NUA2649-09 0.0566 90%mg/kg dry 23 - 152 01/25/11 22:00cis-1,3-Dichloropropene
ND 0.0391 26 48 11A4151 NUA2649-09 0.0566 69%mg/kg dry 24 - 151 01/25/11 22:00trans-1,3-Dichloropropene
ND 0.0634 15 50 11A4151 NUA2649-09 0.0566 112%mg/kg dry 40 - 151 01/25/11 22:001,1-Dichloropropene
ND 0.0587 21 50 11A4151 NUA2649-09 0.0566 104%mg/kg dry 21 - 165 01/25/11 22:00Ethylbenzene
ND 0.0465 37 50 11A4151 NUA2649-09 0.0566 82%mg/kg dry 10 - 173 01/25/11 22:00Hexachlorobutadiene
ND 0.212 31 50 11A4151 NUA2649-09 0.283 75%mg/kg dry 13 - 174 01/25/11 22:002-Hexanone
Page 34 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
Matrix Spike Dup - Cont.
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Volatile Organic Compounds by EPA Method 8260B
11A4151-MSD1
ND 0.0547 23 50 11A4151 NUA2649-09 0.0566 97%mg/kg dry 20 - 139 01/25/11 22:00Isopropylbenzene
ND 0.0573 28 50 11A4151 NUA2649-09 0.0566 101%mg/kg dry 10 - 164 01/25/11 22:00p-Isopropyltoluene
ND 0.0404 27 50 11A4151 NUA2649-09 0.0566 71%mg/kg dry 34 - 154 01/25/11 22:00Methyl tert-Butyl Ether
0.00770 0.0508 19 50 11A4151 NUA2649-09 0.0566 76%mg/kg dry 36 - 163 01/25/11 22:00Methylene Chloride
ND 0.199 32 45 11A4151 NUA2649-09 0.283 70%mg/kg dry 19 - 176 01/25/11 22:004-Methyl-2-pentanone
ND 0.0366 42 50 11A4151 NUA2649-09 0.0566 65%mg/kg dry 10 - 160 01/25/11 22:00Naphthalene
ND 0.0579 24 50 11A4151 NUA2649-09 0.0566 102%mg/kg dry 16 - 174 01/25/11 22:00n-Propylbenzene
ND 0.0301 10 50 11A4151 NUA2649-09 0.0566 53%mg/kg dry 10 - 177 01/25/11 22:00Styrene
ND 0.0471 23 50 11A4151 NUA2649-09 0.0566 83%mg/kg dry 31 - 150 01/25/11 22:001,1,1,2-Tetrachloroethane
ND 0.0334 34 45 11A4151 NUA2649-09 0.0566 59%mg/kg dry 27 - 163 01/25/11 22:001,1,2,2-Tetrachloroethane
0.500 0.717 24 50 11A4151 NUA2649-09MHA 0.0566 384%mg/kg dry 33 - 155 01/25/11 22:00Tetrachloroethene
ND 0.0580 16 50 11A4151 NUA2649-09 0.0566 102%mg/kg dry 45 - 145 01/25/11 22:00Toluene
ND 0.0381 41 50 11A4151 NUA2649-09 0.0566 67%mg/kg dry 10 - 182 01/25/11 22:001,2,3-Trichlorobenzene
ND 0.0404 39 50 11A4151 NUA2649-09 0.0566 71%mg/kg dry 10 - 175 01/25/11 22:001,2,4-Trichlorobenzene
ND 0.0377 26 50 11A4151 NUA2649-09 0.0566 67%mg/kg dry 43 - 145 01/25/11 22:001,1,2-Trichloroethane
ND 0.0608 14 41 11A4151 NUA2649-09 0.0566 107%mg/kg dry 39 - 148 01/25/11 22:001,1,1-Trichloroethane
ND 0.0528 17 50 11A4151 NUA2649-09 0.0566 93%mg/kg dry 39 - 150 01/25/11 22:00Trichloroethene
ND 0.0597 13 47 11A4151 NUA2649-09 0.0566 106%mg/kg dry 25 - 174 01/25/11 22:00Trichlorofluoromethane
ND 0.0354 35 47 11A4151 NUA2649-09 0.0566 63%mg/kg dry 10 - 152 01/25/11 22:001,2,3-Trichloropropane
ND 0.0572 25 50 11A4151 NUA2649-09 0.0566 101%mg/kg dry 38 - 148 01/25/11 22:001,3,5-Trimethylbenzene
ND 0.0552 27 50 11A4151 NUA2649-09 0.0566 98%mg/kg dry 22 - 164 01/25/11 22:001,2,4-Trimethylbenzene
ND 0.0602 12 39 11A4151 NUA2649-09 0.0566 106%mg/kg dry 32 - 163 01/25/11 22:00Vinyl chloride
ND 0.165 22 50 11A4151 NUA2649-09 0.170 97%mg/kg dry 31 - 159 01/25/11 22:00Xylenes, total
ND 0.0512 19 50 11A4151 NUA2649-09 0.0566 91%mg/kg dry 44 - 141 01/25/11 22:00Diisopropyl Ether
ND 0.110 16 41 11A4151 NUA2649-09 0.113 98%mg/kg dry 38 - 147 01/25/11 22:001,2-Dichloroethene (total)
49.8 11A4151 NUA2649-09 50.0 100%Surrogate: 1,2-Dichloroethane-d4 ug/kg 67 - 138 01/25/11 22:00
46.5 11A4151 NUA2649-09 50.0 93%Surrogate: Dibromofluoromethane ug/kg 75 - 125 01/25/11 22:00
53.3 11A4151 NUA2649-09 50.0 107%Surrogate: Toluene-d8 ug/kg 76 - 129 01/25/11 22:00
50.1 11A4151 NUA2649-09 50.0 100%Surrogate: 4-Bromofluorobenzene ug/kg 67 - 147 01/25/11 22:00
Volatile Organic Compounds by SM6200 B
11A4967-MSD1
ND 48.1 3 20 11A4967 NUA2478-01 50.0 96%ug/L 70 - 130 01/26/11 21:37Benzene
ND 50.6 1 20 11A4967 NUA2478-01 50.0 101%ug/L 70 - 130 01/26/11 21:37Bromobenzene
ND 41.5 4 20 11A4967 NUA2478-01 50.0 83%ug/L 70 - 130 01/26/11 21:37Bromochloromethane
ND 53.9 2 20 11A4967 NUA2478-01 50.0 108%ug/L 70 - 130 01/26/11 21:37Bromodichloromethane
ND 47.0 0.6 20 11A4967 NUA2478-01 50.0 94%ug/L 70 - 130 01/26/11 21:37Bromoform
ND 50.5 8 20 11A4967 NUA2478-01 50.0 101%ug/L 60 - 140 01/26/11 21:37Bromomethane
ND 60.6 1 20 11A4967 NUA2478-01 50.0 121%ug/L 70 - 130 01/26/11 21:37n-Butylbenzene
ND 56.7 2 20 11A4967 NUA2478-01 50.0 113%ug/L 70 - 130 01/26/11 21:37tert-Butylbenzene
ND 58.2 2 20 11A4967 NUA2478-01 50.0 116%ug/L 70 - 130 01/26/11 21:37sec-Butylbenzene
Page 35 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
Matrix Spike Dup - Cont.
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Volatile Organic Compounds by SM6200 B
11A4967-MSD1
ND 53.2 4 20 11A4967 NUA2478-01 50.0 106%ug/L 70 - 130 01/26/11 21:37Carbon Tetrachloride
ND 49.4 2 20 11A4967 NUA2478-01 50.0 99%ug/L 70 - 130 01/26/11 21:37Chlorobenzene
ND 58.8 0.1 20 11A4967 NUA2478-01 50.0 118%ug/L 70 - 130 01/26/11 21:37Chlorodibromomethane
ND 40.0 5 20 11A4967 NUA2478-01 50.0 80%ug/L 60 - 140 01/26/11 21:37Chloroethane
ND 50.9 3 20 11A4967 NUA2478-01 50.0 102%ug/L 70 - 130 01/26/11 21:37Chloroform
ND 33.3 5 20 11A4967 NUA2478-01 50.0 67%ug/L 60 - 140 01/26/11 21:37Chloromethane
ND 52.9 1 20 11A4967 NUA2478-01 50.0 106%ug/L 70 - 130 01/26/11 21:374-Chlorotoluene
ND 51.6 2 20 11A4967 NUA2478-01 50.0 103%ug/L 70 - 130 01/26/11 21:372-Chlorotoluene
ND 47.3 0.4 20 11A4967 NUA2478-01 50.0 95%ug/L 70 - 130 01/26/11 21:371,2-Dibromo-3-chloropropane
ND 51.3 0.2 20 11A4967 NUA2478-01 50.0 103%ug/L 70 - 130 01/26/11 21:371,2-Dibromoethane (EDB)
ND 49.1 1 20 11A4967 NUA2478-01 50.0 98%ug/L 70 - 130 01/26/11 21:37Dibromomethane
ND 51.9 1 20 11A4967 NUA2478-01 50.0 104%ug/L 70 - 130 01/26/11 21:371,4-Dichlorobenzene
ND 53.2 1 20 11A4967 NUA2478-01 50.0 106%ug/L 70 - 130 01/26/11 21:371,2-Dichlorobenzene
ND 52.5 2 20 11A4967 NUA2478-01 50.0 105%ug/L 70 - 130 01/26/11 21:371,3-Dichlorobenzene
ND 28.6 6 20 11A4967 NUA2478-01M8 50.0 57%ug/L 60 - 140 01/26/11 21:37Dichlorodifluoromethane
ND 49.3 2 20 11A4967 NUA2478-01 50.0 99%ug/L 70 - 130 01/26/11 21:371,1-Dichloroethane
ND 49.4 1 20 11A4967 NUA2478-01 50.0 99%ug/L 70 - 130 01/26/11 21:371,2-Dichloroethane
ND 7960 0.6 20 11A4967 NUA2478-01M7 5000 159%ug/L 70 - 130 01/26/11 21:37Ethanol
ND 45.2 3 20 11A4967 NUA2478-01 50.0 90%ug/L 70 - 130 01/26/11 21:37trans-1,2-Dichloroethene
ND 53.8 4 20 11A4967 NUA2478-01 50.0 108%ug/L 70 - 130 01/26/11 21:371,1-Dichloroethene
ND 49.5 4 20 11A4967 NUA2478-01 50.0 99%ug/L 70 - 130 01/26/11 21:37cis-1,2-Dichloroethene
ND 49.5 2 20 11A4967 NUA2478-01 50.0 99%ug/L 70 - 130 01/26/11 21:371,2-Dichloropropane
ND 50.9 0.5 20 11A4967 NUA2478-01 50.0 102%ug/L 70 - 130 01/26/11 21:371,3-Dichloropropane
ND 52.1 2 20 11A4967 NUA2478-01 50.0 104%ug/L 70 - 130 01/26/11 21:372,2-Dichloropropane
ND 54.1 0.3 20 11A4967 NUA2478-01 50.0 108%ug/L 70 - 130 01/26/11 21:37trans-1,3-Dichloropropene
ND 55.4 1 20 11A4967 NUA2478-01 50.0 111%ug/L 70 - 130 01/26/11 21:37cis-1,3-Dichloropropene
ND 49.0 3 20 11A4967 NUA2478-01 50.0 98%ug/L 70 - 130 01/26/11 21:371,1-Dichloropropene
ND 51.2 2 20 11A4967 NUA2478-01 50.0 102%ug/L 70 - 130 01/26/11 21:37Ethylbenzene
ND 55.3 2 20 11A4967 NUA2478-01 50.0 111%ug/L 70 - 130 01/26/11 21:37Hexachlorobutadiene
ND 59.3 1 20 11A4967 NUA2478-01 50.0 119%ug/L 70 - 130 01/26/11 21:37Isopropylbenzene
ND 56.6 2 20 11A4967 NUA2478-01 50.0 113%ug/L 70 - 130 01/26/11 21:37p-Isopropyltoluene
ND 50.6 1 20 11A4967 NUA2478-01 50.0 101%ug/L 70 - 130 01/26/11 21:37Methylene Chloride
ND 56.5 0.7 20 11A4967 NUA2478-01 50.0 113%ug/L 70 - 130 01/26/11 21:37Naphthalene
ND 54.1 2 20 11A4967 NUA2478-01 50.0 108%ug/L 70 - 130 01/26/11 21:37n-Propylbenzene
ND 53.5 2 20 11A4967 NUA2478-01 50.0 107%ug/L 70 - 130 01/26/11 21:37Styrene
ND 52.5 0.3 20 11A4967 NUA2478-01 50.0 105%ug/L 70 - 130 01/26/11 21:371,1,2,2-Tetrachloroethane
ND 56.3 0.4 20 11A4967 NUA2478-01 50.0 113%ug/L 70 - 130 01/26/11 21:371,1,1,2-Tetrachloroethane
ND 47.1 2 20 11A4967 NUA2478-01 50.0 94%ug/L 70 - 130 01/26/11 21:37Tetrachloroethene
ND 47.6 2 20 11A4967 NUA2478-01 50.0 95%ug/L 70 - 130 01/26/11 21:37Toluene
ND 56.4 0.6 20 11A4967 NUA2478-01 50.0 113%ug/L 70 - 130 01/26/11 21:371,2,3-Trichlorobenzene
ND 57.7 0.2 20 11A4967 NUA2478-01 50.0 115%ug/L 70 - 130 01/26/11 21:371,2,4-Trichlorobenzene
Page 36 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
Matrix Spike Dup - Cont.
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Volatile Organic Compounds by SM6200 B
11A4967-MSD1
ND 52.0 1 20 11A4967 NUA2478-01 50.0 104%ug/L 70 - 130 01/26/11 21:371,1,2-Trichloroethane
ND 52.0 2 20 11A4967 NUA2478-01 50.0 104%ug/L 70 - 130 01/26/11 21:371,1,1-Trichloroethane
ND 48.2 3 20 11A4967 NUA2478-01 50.0 96%ug/L 70 - 130 01/26/11 21:37Trichloroethene
ND 50.5 7 20 11A4967 NUA2478-01 50.0 101%ug/L 60 - 140 01/26/11 21:37Trichlorofluoromethane
ND 51.0 0.04 20 11A4967 NUA2478-01 50.0 102%ug/L 70 - 130 01/26/11 21:371,2,3-Trichloropropane
ND 53.8 2 20 11A4967 NUA2478-01 50.0 108%ug/L 70 - 130 01/26/11 21:371,3,5-Trimethylbenzene
ND 52.1 2 20 11A4967 NUA2478-01 50.0 104%ug/L 70 - 130 01/26/11 21:371,2,4-Trimethylbenzene
ND 41.0 5 20 11A4967 NUA2478-01 50.0 82%ug/L 60 - 140 01/26/11 21:37Vinyl chloride
ND 151 2 20 11A4967 NUA2478-01 150 101%ug/L 70 - 130 01/26/11 21:37Xylenes, total
24.4 76.8 0.2 20 11A4967 NUA2478-01 50.0 105%ug/L 70 - 130 01/26/11 21:37Methyl tert-Butyl Ether
ND 50.0 0.4 20 11A4967 NUA2478-01 50.0 100%ug/L 70 - 130 01/26/11 21:37Diisopropyl Ether
24.6 11A4967 NUA2478-01 25.0 99%Surrogate: 1,2-Dichloroethane-d4 ug/L 70 - 130 01/26/11 21:37
25.0 11A4967 NUA2478-01 25.0 100%Surrogate: Dibromofluoromethane ug/L 70 - 130 01/26/11 21:37
24.7 11A4967 NUA2478-01 25.0 99%Surrogate: Toluene-d8 ug/L 70 - 130 01/26/11 21:37
24.8 11A4967 NUA2478-01 25.0 99%Surrogate: 4-Bromofluorobenzene ug/L 70 - 130 01/26/11 21:37
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-MSD1
ND 35.3 21 24 11A4345 NUA2165-01R
E1
50.0 71%ug/L 50 - 120 01/25/11 17:29Acenaphthene
ND 36.8 18 22 11A4345 NUA2165-01R
E1
50.0 74%ug/L 53 - 120 01/25/11 17:29Acenaphthylene
ND 40.3 11 18 11A4345 NUA2165-01R
E1
50.0 81%ug/L 56 - 124 01/25/11 17:29Anthracene
ND 36.4 18 20 11A4345 NUA2165-01R
E1
50.0 73%ug/L 57 - 122 01/25/11 17:29Benzo (a) anthracene
ND 38.4 11 24 11A4345 NUA2165-01R
E1
50.0 77%ug/L 46 - 138 01/25/11 17:29Benzo (a) pyrene
ND 35.6 10 36 11A4345 NUA2165-01R
E1
50.0 71%ug/L 45 - 138 01/25/11 17:29Benzo (b) fluoranthene
ND 37.2 10 19 11A4345 NUA2165-01R
E1
50.0 74%ug/L 48 - 137 01/25/11 17:29Benzo (g,h,i) perylene
ND 40.1 14 34 11A4345 NUA2165-01R
E1
50.0 80%ug/L 44 - 134 01/25/11 17:29Benzo (k) fluoranthene
ND 37.8 8 16 11A4345 NUA2165-01R
E1
50.0 76%ug/L 50 - 120 01/25/11 17:294-Bromophenyl phenyl ether
ND 36.0 16 19 11A4345 NUA2165-01R
E1
50.0 72%ug/L 59 - 134 01/25/11 17:29Butyl benzyl phthalate
ND 40.6 11 18 11A4345 NUA2165-01R
E1
50.0 81%ug/L 53 - 120 01/25/11 17:29Carbazole
ND 32.3 15 37 11A4345 NUA2165-01R
E1
50.0 65%ug/L 38 - 120 01/25/11 17:294-Chloro-3-methylphenol
ND 27.3 23 36 11A4345 NUA2165-01R
E1
50.0 55%ug/L 35 - 120 01/25/11 17:294-Chloroaniline
ND 33.4 16 28 11A4345 NUA2165-01R
E1
50.0 67%ug/L 41 - 120 01/25/11 17:29Bis(2-chloroethoxy)methane
Page 37 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
Matrix Spike Dup - Cont.
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-MSD1
ND 33.2 17 19 11A4345 NUA2165-01R
E1
50.0 66%ug/L 42 - 120 01/25/11 17:29Bis(2-chloroethyl)ether
ND 36.4 7 20 11A4345 NUA2165-01R
E1
50.0 73%ug/L 45 - 120 01/25/11 17:29Bis(2-chloroisopropyl)ether
ND 33.8 17 25 11A4345 NUA2165-01R
E1
50.0 68%ug/L 43 - 120 01/25/11 17:292-Chloronaphthalene
ND 39.7 5 18 11A4345 NUA2165-01R
E1
50.0 79%ug/L 40 - 120 01/25/11 17:292-Chlorophenol
ND 34.0 22 19 11A4345 NUA2165-01R
E1
R 50.0 68%ug/L 56 - 120 01/25/11 17:294-Chlorophenyl phenyl ether
ND 36.2 14 20 11A4345 NUA2165-01R
E1
50.0 72%ug/L 54 - 123 01/25/11 17:29Chrysene
ND 37.0 16 18 11A4345 NUA2165-01R
E1
50.0 74%ug/L 50 - 136 01/25/11 17:29Dibenz (a,h) anthracene
ND 35.4 24 20 11A4345 NUA2165-01R
E1
R 50.0 71%ug/L 55 - 120 01/25/11 17:29Dibenzofuran
ND 39.6 12 19 11A4345 NUA2165-01R
E1
50.0 79%ug/L 63 - 120 01/25/11 17:29Di-n-butyl phthalate
ND 32.7 11 33 11A4345 NUA2165-01R
E1
50.0 65%ug/L 42 - 120 01/25/11 17:291,4-Dichlorobenzene
ND 32.0 15 33 11A4345 NUA2165-01R
E1
50.0 64%ug/L 29 - 120 01/25/11 17:291,2-Dichlorobenzene
ND 30.9 18 34 11A4345 NUA2165-01R
E1
50.0 62%ug/L 27 - 120 01/25/11 17:291,3-Dichlorobenzene
ND 16.2 39 27 11A4345 NUA2165-01R
E1
R 50.0 32%ug/L 10 - 130 01/25/11 17:293,3-Dichlorobenzidine
ND 29.8 19 21 11A4345 NUA2165-01R
E1
50.0 60%ug/L 39 - 120 01/25/11 17:292,4-Dichlorophenol
ND 35.7 16 25 11A4345 NUA2165-01R
E1
50.0 71%ug/L 53 - 120 01/25/11 17:29Diethyl phthalate
ND 37.8 15 50 11A4345 NUA2165-01R
E1
50.0 76%ug/L 11 - 130 01/25/11 17:292,4-Dimethylphenol
ND 38.1 12 20 11A4345 NUA2165-01R
E1
50.0 76%ug/L 59 - 120 01/25/11 17:29Dimethyl phthalate
ND 31.7 17 24 11A4345 NUA2165-01R
E1
50.0 63%ug/L 10 - 157 01/25/11 17:294,6-Dinitro-2-methylphenol
ND 31.7 31 28 11A4345 NUA2165-01R
E1
R 50.0 63%ug/L 10 - 176 01/25/11 17:292,4-Dinitrophenol
ND 39.3 14 24 11A4345 NUA2165-01R
E1
50.0 79%ug/L 62 - 120 01/25/11 17:292,6-Dinitrotoluene
ND 35.0 21 21 11A4345 NUA2165-01R
E1
50.0 70%ug/L 61 - 124 01/25/11 17:292,4-Dinitrotoluene
ND 35.2 12 21 11A4345 NUA2165-01R
E1
50.0 70%ug/L 56 - 141 01/25/11 17:29Di-n-octyl phthalate
ND 35.8 15 19 11A4345 NUA2165-01R
E1
50.0 72%ug/L 44 - 134 01/25/11 17:29Bis(2-ethylhexyl)phthalate
ND 38.8 13 18 11A4345 NUA2165-01R
E1
50.0 78%ug/L 60 - 120 01/25/11 17:29Fluoranthene
ND 34.7 24 21 11A4345 NUA2165-01R
E1
R 50.0 69%ug/L 59 - 120 01/25/11 17:29Fluorene
ND 39.3 8 19 11A4345 NUA2165-01R
E1
50.0 79%ug/L 54 - 120 01/25/11 17:29Hexachlorobenzene
Page 38 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
Matrix Spike Dup - Cont.
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-MSD1
ND 27.8 17 38 11A4345 NUA2165-01R
E1
50.0 56%ug/L 24 - 120 01/25/11 17:29Hexachlorobutadiene
ND 8.06 21 38 11A4345 NUA2165-01R
E1
50.0 16%ug/L 10 - 120 01/25/11 17:29Hexachlorocyclopentadiene
ND 31.6 14 40 11A4345 NUA2165-01R
E1
50.0 63%ug/L 26 - 120 01/25/11 17:29Hexachloroethane
ND 36.7 16 18 11A4345 NUA2165-01R
E1
50.0 73%ug/L 50 - 136 01/25/11 17:29Indeno (1,2,3-cd) pyrene
ND 30.9 13 34 11A4345 NUA2165-01R
E1
50.0 62%ug/L 42 - 120 01/25/11 17:29Isophorone
ND 32.5 6 48 11A4345 NUA2165-01R
E1
50.0 65%ug/L 34 - 120 01/25/11 17:292-Methylnaphthalene
ND 32.8 7 19 11A4345 NUA2165-01R
E1
50.0 66%ug/L 36 - 120 01/25/11 17:292-Methylphenol
ND 29.6 4 24 11A4345 NUA2165-01R
E1
50.0 59%ug/L 32 - 120 01/25/11 17:293/4-Methylphenol
ND 29.7 13 45 11A4345 NUA2165-01R
E1
50.0 59%ug/L 32 - 120 01/25/11 17:29Naphthalene
ND 34.1 23 23 11A4345 NUA2165-01R
E1
50.0 68%ug/L 38 - 120 01/25/11 17:293-Nitroaniline
ND 38.2 15 25 11A4345 NUA2165-01R
E1
50.0 76%ug/L 51 - 126 01/25/11 17:292-Nitroaniline
ND 38.2 18 23 11A4345 NUA2165-01R
E1
50.0 76%ug/L 47 - 124 01/25/11 17:294-Nitroaniline
ND 28.6 17 34 11A4345 NUA2165-01R
E1
50.0 57%ug/L 41 - 120 01/25/11 17:29Nitrobenzene
ND 17.7 25 29 11A4345 NUA2165-01R
E1
50.0 35%ug/L 10 - 120 01/25/11 17:294-Nitrophenol
ND 35.9 10 35 11A4345 NUA2165-01R
E1
50.0 72%ug/L 35 - 120 01/25/11 17:292-Nitrophenol
ND 48.0 9 23 11A4345 NUA2165-01R
E1
50.0 96%ug/L 45 - 124 01/25/11 17:29N-Nitrosodiphenylamine
ND 34.5 21 19 11A4345 NUA2165-01R
E1
R 50.0 69%ug/L 50 - 121 01/25/11 17:29N-Nitrosodi-n-propylamine
ND 35.0 15 24 11A4345 NUA2165-01R
E1
50.0 70%ug/L 46 - 159 01/25/11 17:29Pentachlorophenol
ND 41.8 9 19 11A4345 NUA2165-01R
E1
50.0 84%ug/L 53 - 120 01/25/11 17:29Phenanthrene
ND 17.0 21 27 11A4345 NUA2165-01R
E1
50.0 34%ug/L 10 - 120 01/25/11 17:29Phenol
ND 35.8 6 19 11A4345 NUA2165-01R
E1
50.0 72%ug/L 50 - 129 01/25/11 17:29Pyrene
ND 30.1 3 34 11A4345 NUA2165-01R
E1
50.0 60%ug/L 27 - 120 01/25/11 17:291,2,4-Trichlorobenzene
ND 29.6 10 45 11A4345 NUA2165-01R
E1
50.0 59%ug/L 34 - 120 01/25/11 17:291-Methylnaphthalene
ND 35.8 21 26 11A4345 NUA2165-01R
E1
50.0 72%ug/L 48 - 125 01/25/11 17:292,4,6-Trichlorophenol
ND 31.5 26 26 11A4345 NUA2165-01R
E1
50.0 63%ug/L 51 - 125 01/25/11 17:292,4,5-Trichlorophenol
28.6 11A4345 NUA2165-01R
E1
50.0 57%Surrogate: Terphenyl-d14 ug/L 13 - 120 01/25/11 17:29
Page 39 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
Orig. Val.UnitsAnalyte
Sample
DuplicatedBatchRPDDuplicate
Matrix Spike Dup - Cont.
PROJECT QUALITY CONTROL DATA
Q
Spike
Conc % Rec.
Target
Range
Analyzed
Date/TimeLimit
Semivolatile Organic Compounds by EPA Method 8270D
11A4345-MSD1
36.4 11A4345 NUA2165-01R
E1
50.0 73%Surrogate: 2,4,6-Tribromophenol ug/L 29 - 132 01/25/11 17:29
11.4 11A4345 NUA2165-01R
E1
50.0 23%Surrogate: Phenol-d5 ug/L 10 - 120 01/25/11 17:29
31.2 11A4345 NUA2165-01R
E1
50.0 62%Surrogate: 2-Fluorobiphenyl ug/L 29 - 120 01/25/11 17:29
21.2 11A4345 NUA2165-01R
E1
50.0 42%Surrogate: 2-Fluorophenol ug/L 10 - 120 01/25/11 17:29
29.2 11A4345 NUA2165-01R
E1
50.0 58%Surrogate: Nitrobenzene-d5 ug/L 27 - 120 01/25/11 17:29
Extractable Petroleum Hydrocarbons
11A4223-MSD1
2.89 40.1 0.8 40 11A4223 NUA2663-02 48.7 76%mg/kg dry 23 - 138 01/25/11 15:35Diesel
0.774 11A4223 NUA2663-02 0.974 80%Surrogate: o-Terphenyl mg/kg dry 53 - 140 01/25/11 15:35
Purgeable Petroleum Hydrocarbons
11A4142-MSD1
1220 2 50 11A4142 NUA2619-12M1 500 243%mg/kg wet 63 - 134 01/26/11 11:58GRO as Gasoline
28.1 11A4142 NUA2619-12 20.0 140%Surrogate: a,a,a-Trifluorotoluene ug/L 60 - 150 01/26/11 11:58
11A4142-MSD2
186 682 24 50 11A4142 NUA2619-13 500 99%mg/kg wet 63 - 134 01/26/11 12:37GRO as Gasoline
20.3 11A4142 NUA2619-13 20.0 102%Surrogate: a,a,a-Trifluorotoluene ug/L 60 - 150 01/26/11 12:37
Page 40 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
CERTIFICATION SUMMARY
Method Matrix
TestAmerica Nashville
AIHA Nelac North Carolina
Water XSM6200 B
Soil XXSW846 8015C
Soil XN/A XSW846 8260B
Water XXSW846 8270D
SoilSW-846
Page 41 of 42
2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax [phone]

Client
Attn
Hart & Hickman (2162)
2923 South Tryon Street, Suite 100
Charlotte, NC 28203-5449
Nathan O'Leary
Project Name:
Work Order:
National Textiles Facility
Received:
Project Number:FDP-025
01/21/11 08:55
NUA2663
DATA QUALIFIERS AND DEFINITIONS
M1 The MS and/or MSD were above the acceptance limits due to sample matrix interference. See Blank Spike (LCS).
M7 The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).
M8 The MS and/or MSD were below the acceptance limits. See Blank Spike (LCS).
MHA Due to high levels of analyte in the sample, the MS/MSD calculation does not provide useful spike recovery information. See
Blank Spike (LCS).
R The RPD exceeded the method control limit. The individual analyte QA/QC recoveries, however, were within acceptance limits.
Z Due to sample matrix effects, the surrogate recovery was below the acceptance limits.
Z2 Surrogate recovery was above the acceptance limits. Data not impacted.
ND Not detected at the reporting limit (or method detection limit if shown)
METHOD MODIFICATION NOTES
Page 42 of 42